WorldWideScience

Sample records for corrosion crack growth

  1. The Growth of Small Corrosion Fatigue Cracks in Alloy 7075

    Science.gov (United States)

    Piascik, Robert S.

    2015-01-01

    The corrosion fatigue crack growth characteristics of small (greater than 35 micrometers) surface and corner cracks in aluminum alloy 7075 is established. The early stage of crack growth is studied by performing in situ long focal length microscope (500×) crack length measurements in laboratory air and 1% sodium chloride (NaCl) environments. To quantify the "small crack effect" in the corrosive environment, the corrosion fatigue crack propagation behavior of small cracks is compared to long through-the-thickness cracks grown under identical experimental conditions. In salt water, long crack constant K(sub max) growth rates are similar to small crack da/dN.

  2. Frequency dependence of fatigue and corrosion fatigue crack growth rate

    Energy Technology Data Exchange (ETDEWEB)

    Marvasti, Mohammad Hassan; Chen, Weixing [Department of Chemical and Materials Engineering, University of Alberta, Edmonton, AB (Canada); Kania, Richard; Worthingham, Robert [TransCanada Pipelines Limited, Calgary, AB (Canada); Van Boven, Gregory [Spectra Energy Transmission Limited, Vancouver, BC (Canada)

    2010-07-01

    It was in the mid-1980s that stress corrosion cracking (SCC) was first found in near-neutral pH conditions on the TransCanada pipeline system. Since then, there have been many reports of pipeline cracking in Canada in these conditions. The huge quantity of pipelines in Canada and the number of failures have brought great interest in investigation of this cracking. A study was conducted on one X52 pipeline steel. It used compact tension specimens for corrosion fatigue and fatigue tests in air. The following conclusions were drawn: 1) crack growth in near-neutral pH conditions can be explained by a factor, which reflects the combined action of the mechanical driving force and the hydrogen effects; 2) mechanical dormancy can be common when oil and gas pipelines are in operation; 3) hydrogen is a determining factor of crack growth when pipeline steels are exposed to near-neutral pH conditions.

  3. Corrosion Fatigue Crack Growth Behavior at Notched Hole in 7075-T6 Under Biaxial and Uniaxial Fatigue with Different Phases

    Science.gov (United States)

    2015-09-17

    CORROSION FATIGUE CRACK GROWTH BEHAVIOR AT NOTCHED HOLE IN 7075-T6 UNDER BIAXIAL AND UNIAXIAL FATIGUE WITH DIFFERENT PHASES... CORROSION FATIGUE CRACK GROWTH BEHAVIOR AT NOTCHED HOLE IN 7075-T6 UNDER BIAXIAL AND UNIAXIAL FATIGUE WITH DIFFERENT PHASES THESIS...UNLIMITED AFIT-ENY-MS-15-S-065 CORROSION FATIGUE CRACK GROWTH BEHAVIOR AT NOTCHED HOLE IN 7075-T6 UNDER BIAXIAL AND UNIAXIAL FATIGUE WITH

  4. Effect of cold work on the growth rates of stress corrosion cracks in structural materials of nuclear systems

    Energy Technology Data Exchange (ETDEWEB)

    Magdowski, R.; Speidel, M.O. [Swiss Federal Inst. of Tech., Zurich (Switzerland). Inst. of Metallurgy

    1996-10-01

    The growth rates of stress corrosion cracks in austenitic stainless steels and nickel base alloy 600 exposed to simulated boiling water reactor coolant were measured by fracture mechanics testing techniques. Cold work may increase the crack growth rates up to one hundred times. In both, the annealed condition and the cold worked condition, the stress corrosion crack growth rates are independent of stress intensity over a wide K-range and crack growth rates correlate well with yield strength and hardness. In the annealed condition the fracture path is intergranular, but higher degrees of cold work introduce higher proportions of transgranular stress corrosion cracking.

  5. Modelling of Corrosion Cracks

    DEFF Research Database (Denmark)

    Thoft-Christensen, Palle

    Modelling of corrosion cracking of reinforced concrete structures is complicated as a great number of uncertain factors are involved. To get a reliable modelling a physical and mechanical understanding of the process behind corrosion in needed.......Modelling of corrosion cracking of reinforced concrete structures is complicated as a great number of uncertain factors are involved. To get a reliable modelling a physical and mechanical understanding of the process behind corrosion in needed....

  6. Stress Corrosion Cracking and Fatigue Crack Growth Studies Pertinent to Spacecraft and Booster Pressure Vessels

    Science.gov (United States)

    Hall, L. R.; Finger, R. W.

    1972-01-01

    This experimental program was divided into two parts. The first part evaluated stress corrosion cracking in 2219-T87 aluminum and 5Al-2.5Sn (ELI) titanium alloy plate and weld metal. Both uniform height double cantilever beam and surface flawed specimens were tested in environments normally encountered during the fabrication and operation of pressure vessels in spacecraft and booster systems. The second part studied compatibility of material-environment combinations suitable for high energy upper stage propulsion systems. Surface flawed specimens having thicknesses representative of minimum gage fuel and oxidizer tanks were tested. Titanium alloys 5Al-2.5Sn (ELI), 6Al-4V annealed, and 6Al-4V STA were tested in both liquid and gaseous methane. Aluminum alloy 2219 in the T87 and T6E46 condition was tested in fluorine, a fluorine-oxygen mixture, and methane. Results were evaluated using modified linear elastic fracture mechanics parameters.

  7. Stress Corrosion Crack Growth Behavior of Titanium Alloy/Bioactive Glasses Sandwiches in Simulated Human Physiological Environment

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    Based on a series of newly developed bioactive glasses having suitable thermo-mechanical properties to allow application as fixation agents between bone and titanium alloy biomedical implants, the stress corrosion crack growth(SCCG) behavior of their interfaces with Ti6Al4V was investigated in simulated body fluid (SBF) with the objectiveof discerning the salient mechanisms of crack advance and to assess the reliability of the bonds. Results indicatedthat crack growth rates in Ti6Al4V/glass/Ti6Al4V sandwich specimens were nearly the same as or slightly lowerthan those in the bulk glasses at comparable stress intensities; indeed, cracks would prefer to propagate off theinterface, suggesting that the Ti6Al4V/glass interface has relatively good crack-growth resistance. Mechanistically,interfacial crack growth appears to be controlled by the classic stress corrosion mechanisms for silicate glasses, withno discernible effect of bioactivity on the SCCG behavior being observed.

  8. Methodology to evaluate the crack growth rate by stress corrosion cracking in dissimilar metals weld in simulated environment of PWR nuclear reactor

    Energy Technology Data Exchange (ETDEWEB)

    Paula, Raphael G.; Figueiredo, Celia A.; Rabelo, Emerson G., E-mail: raphaelmecanica@gmail.com, E-mail: caf@cdtn.br, E-mail: egr@cdtn.br [Centro de Desenvolvimento da Tecnologia Nuclear (CDTN/CNEN-MG), Belo Horizonte, MG (Brazil)

    2013-07-01

    Inconel alloys weld metal is widely used to join dissimilar metals in nuclear reactors applications. It was recently observed failures of weld components in plants, which have triggered an international effort to determine reliable data on the stress corrosion cracking behavior of this material in reactor environment. The objective of this work is to develop a methodology to determine the crack growth rate caused by stress corrosion in Inconel alloy 182, using the specimen (Compact Tensile) in simulated PWR environment. (author)

  9. Strain rate effects in stress corrosion cracking

    Energy Technology Data Exchange (ETDEWEB)

    Parkins, R.N. (Newcastle upon Tyne Univ. (UK). Dept. of Metallurgy and Engineering Materials)

    1990-03-01

    Slow strain rate testing (SSRT) was initially developed as a rapid, ad hoc laboratory method for assessing the propensity for metals an environments to promote stress corrosion cracking. It is now clear, however, that there are good theoretical reasons why strain rate, as opposed to stress per se, will often be the controlling parameter in determining whether or not cracks are nucleated and, if so, are propagated. The synergistic effects of the time dependence of corrosion-related reactions and microplastic strain provide the basis for mechanistic understanding of stress corrosion cracking in high-pressure pipelines and other structures. However, while this may be readily comprehended in the context of laboratory slow strain tests, its extension to service situations may be less apparent. Laboratory work involving realistic stressing conditions, including low-frequency cyclic loading, shows that strain or creep rates give good correlation with thresholds for cracking and with crack growth kinetics.

  10. Crack Initiation and Growth Behavior at Corrosion Pit in 7075-T6 High Strength Aluminum Alloy

    Science.gov (United States)

    2013-06-01

    was not used to measure the transition from corrosion pit to long crack [25]. . . . . . . . . . . 22 3.1 Composition of a typical sample of 7075 -T6...lives. 24 III. Methodology 3.1 Material Research was conducted using 7075 -T6 aluminum. This alloy is commonly used in aerospace applications and as a... material properties of this alloy. It is important to note that these properties were also used in all finite element models. Table 3.1: Composition of

  11. Cracking and corrosion recovery boiler

    Energy Technology Data Exchange (ETDEWEB)

    Suik, H. [Tallinn Technical University, Horizon Pulp and Paper, Tallinn (Estonia)

    1998-12-31

    The corrosion of heat surfaces and the cracking the drums are the main problems of the recovery boiler. These phenomena have been appeared during long-term operation of boiler `Mitsubishi - 315` erected at 1964. Depth of the crack is depending on the number of shutdowns and on operation time. Corrosion intensity of different heat surfaces is varying depend on the metal temperature and the conditions at place of positioning of tube. The lowest intensity of corrosion is on the bank tubes and the greatest is on the tubes of the second stage superheater and on the tubes at the openings of air ports. (orig.) 5 refs.

  12. Stress-corrosion cracking of titanium alloys.

    Science.gov (United States)

    Blackburn, M. J.; Feeney, J. A.; Beck, T. R.

    1973-01-01

    In the light of research material published up to May 1970, the current understanding of the experimental variables involved in the stress-corrosion cracking (SCC) behavior of titanium and its alloys is reviewed. Following a brief summary of the metallurgy and electrochemistry of titanium alloys, the mechanical, electrochemical, and metallurgical parameters influencing SCC behavior are explored with emphasis on crack growth kinetics. Macro- and microfeatures of fractures are examined, and it is shown that many transgranular SCC failures exhibit morphological and crystallographic features similar to mechanical cleavage failures. Current SCC models are reviewed with respect to their ability to explain the observed SCC behavior of titanium and its alloys. Possible methods for eliminating or minimizing stress corrosion hazards in titanium or titanium alloy components are described.

  13. Numerical Study of Corrosion Crack Opening

    DEFF Research Database (Denmark)

    Thoft-Christensen, Palle; Frandsen, Henrik Lund; Svensson, Staffan

    2008-01-01

    for the corrosion crack opening. Experiments and theoretical analysis by a numerical method, FEM, support that the relation between the reduction of the reinforcement bar diameter due to corrosion and the corresponding increase in crack width for a given time interval, measured on the surface of a concrete specimen...... is proportional. More recently, the constant of proportionality, the so-called crack-corrosion index, has been studied further with respect to its dependence on the diameter of the reinforcement and the concrete cover. In the present paper the above-mentioned work is presented and extended with more realistic 3D......-models of the cracked concrete beam. The crack-corrosion index is evaluated for a variation of different parameters, i.e. bar diameter, concrete cover, crack length and type of corrosion product. This paper is an extended version of a paper by Thoft-Christensen et al. (2005) presented at the IFIP WG 7.5 Conference...

  14. Stress corrosion cracking of copper canisters

    Energy Technology Data Exchange (ETDEWEB)

    King, Fraser (Integrity Corrosion Consulting Limited (Canada)); Newman, Roger (Univ. of Toronto (Canada))

    2010-12-15

    films appear to be insufficiently adherent. A critical review of the surface mobility model is presented. It is argued that the formulation of the crack growth law is flawed and that, in its corrected form, predicted crack growth rates would be of the order of 10.20 m/s. Therefore, even if cracking were to occur via this mechanism, the crack velocity would be too small to lead to canister failure, even over repository timescales. Two other SCC mechanisms, the adsorption-induced dislocation emission and vacancy injection and embrittlement models, are also discussed. Although these models are still in the development stage, it is considered unlikely that they could induce cracking during the long-term anaerobic phase. Therefore, we conclude that the probability of SCC during the early aerobic period is low because of the absence of the necessary conditions for cracking and that there is no well-founded SCC mechanism that would result in cracking during the long-term anaerobic phase in the repository. Nevertheless, it is felt prudent to continue to study SCC of copper, especially under anaerobic conditions, in order to provide more support for the position that the stress corrosion cracking of copper canisters in the repository will not limit their service life

  15. Principles of inhibiting of corrosion-static crack growth in constructional steels caused by hydrogen embrittlement

    Energy Technology Data Exchange (ETDEWEB)

    Romaniv, O.N.; Nikiforchin, G.N.; Tsirul' nik, A.T.

    1987-11-01

    The effectiveness of a range of organic and inorganic corrosion inhibitors was studied on a series of structural chromium steels--including 45KhN2MFA, 60KhS, and 30KhGSN2A--of different strength levels and certain principles are formulated for developing and selecting inhibitors based on the hydrogen mechanism of corrosive media. The inhibitors tested include monoethanol amine, urotropin, sodium benzoate, thiourea, sodium phosphates and chromates, various nitrates, and the IRT range of inhibitors.

  16. A STUDY OF CORROSION AND STRESS CORROSION CRACKING OF CARBON STEEL NUCLEAR WASTE STORAGE TANKS

    Energy Technology Data Exchange (ETDEWEB)

    BOOMER, K.D.

    2007-08-21

    The Hanford reservation Tank Farms in Washington State has 177 underground storage tanks that contain approximately 50 million gallons of liquid legacy radioactive waste from cold war plutonium production. These tanks will continue to store waste until it is treated and disposed. These nuclear wastes were converted to highly alkaline pH wastes to protect the carbon steel storage tanks from corrosion. However, the carbon steel is still susceptible to localized corrosion and stress corrosion cracking. The waste chemistry varies from tank to tank, and contains various combinations of hydroxide, nitrate, nitrite, chloride, carbonate, aluminate and other species. The effect of each of these species and any synergistic effects on localized corrosion and stress corrosion cracking of carbon steel have been investigated with electrochemical polarization, slow strain rate, and crack growth rate testing. The effect of solution chemistry, pH, temperature and applied potential are all considered and their role in the corrosion behavior will be discussed.

  17. Corrosion and Cracking of Reinforced Concrete

    DEFF Research Database (Denmark)

    Thoft-Christensen, Palle

    Modelling of the deterioration of reinforced concrete has in recent years changed from being a deterministic modelling based on experience to be stochastic modelling based on sound and consistent physical, chemical and mechanical principles. In this paper is presented a brief review of modern mod...... for time to initial corrosion, time to initial cracking, and time to a given crack width may be obtained....

  18. A novel technique for measuring stress-corrosion crack-growth rates in single-crystal experiments

    Energy Technology Data Exchange (ETDEWEB)

    Lichter, B.D. [Vanderbilt Univ., Nashville, TN (United States)]|[Delft Univ. of Technology (Netherlands); Flanagan, W.F. [Vanderbilt Univ., Nashville, TN (United States)

    1994-12-31

    Crack-growth occurs discontinuously in oriented copper-gold single-crystals during slow-strain rate experiments performed under anodic polarization in aqueous NaCl solutions. Crack advance between major crack arrests is accompanied by load-drops and current-transients which can be quantitatively related to the length of the advance as well as yielding the average instantaneous rate of advance. Two independent but self-consistent methods are used: (1) mechanical analysis of the load-drops, taking into account the elastic displacement of the load-train and of the specimen, due to both the load and the crack advance, and (2) analysis of the current-transients in which it is argued that the current is proportional to the rate of new surface production. Results show that the crack velocity is on the order of 50--400{mu}/s, depending on the environment and potential, too slow to be explained by a running brittle crack, and too fast to be explained by Faradaic dissolution.

  19. A Calculation Model for Corrosion Cracking in RC Structures

    Institute of Scientific and Technical Information of China (English)

    Xu Gang; Wei Jun; Zhang Keqiang; Zhou Xiwu

    2007-01-01

    A novel calculation model is proposed aiming at the problem of concrete cover cracking induced by reinforcement corrosion. In this article, the relationship between the corrosion depth of the bar and the thickness of the rust layer is established. By deducing the radial displacement expression of concrete, the formula for corrosion depth and corrosion pressure before cracking is proposed. The crack depth of cover in accordance with the maximum corrosion pressure is deduced; furthermore, the corrosion depth and corrosion pressure at the cracking time are obtained. Finally, the theoretical model is validated by several experiments, and the calculated values agree well with the experiment results.

  20. Stress Corrosion Cracking of Pipeline Steels

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    This paper provides a review of the differences between high pH and near-neutral pH stress corrosion cracking ofpipeline steels, influencing factors, and mechanisms. The characteristics and historical information on both forms ofSCC are discussed. The prospect for research in the future is also presented.

  1. Consideration on corrosion fatigue crack life assessment; Fushoku hiro kiretsu hassei jumyo hyoka ni kansuru ichikosatsu

    Energy Technology Data Exchange (ETDEWEB)

    Yajima, H.; Yamamoto, M.; Saito, T. [Hiroshima University, Hiroshima (Japan). Faculty of Engineering; Morita, K. [Mitsubishi Heavy Industries, Ltd., Tokyo (Japan)

    1996-10-01

    Discussions were given on corrosion fatigue crack life by using corrosion fatigue crack initiation test and analysis. The test used 13Cr-based stainless steel as a test material, and aquamarine at 60{degree}C as a corrosion environment. The fatigue test was performed under a tension loading condition with a stress ratio of 0.1 and an iterative velocity of 1.7 Hz by using a 10-tonf fatigue testing machine. In the corrosion fatigue crack initiation test, a pit has been generated on a boundary of an exposed part and a painted part for masking, hence direct observation was impossible on pit growth behavior. Therefore, an intrinsic crack model was introduced from pit dimensions as observed from a fracture face, and analysis was made on corrosion fatigue crack growth by using the linear fracture dynamics, wherein clarification was made on a phenomenon occurring after the crack growth passes the pit growth until the test piece is fractured. A proposal was made to define the time when fatigue crack initiates and grows from the bottom of a pit as a result of surpassing the growth of corrosion pit as the corrosion fatigue crack life. 4 refs., 7 figs., 1 tab.

  2. Computational modeling of the mechanism of hydrogen embrittlement (HE) and stress corrosion cracking (SCC) in metals

    Science.gov (United States)

    Cendales, E. D.; Orjuela, F. A.; Chamarraví, O.

    2016-02-01

    In this article theoretical models and some existing data sets were examined in order to model the two main causes (hydrogen embrittlement and corrosion-cracking under stress) of the called environmentally assisted cracking phenomenon (EAC). Additionally, a computer simulation of flat metal plate subject to mechanical stress and cracking due both to hydrogen embrittlement and corrosion was developed. The computational simulation was oriented to evaluate the effect on the stress-strain behavior, elongation percent and the crack growth rate of AISI SAE 1040 steel due to three corrosive enviroments (H2 @ 0.06MPa; HCl, pH=1.0; HCl, pH=2.5). From the computer simulation we conclude that cracking due to internal corrosion of the material near to the crack tip limits affects more the residual strength of the flat plate than hydrogen embrittlement and generates a failure condition almost imminent of the mechanical structural element.

  3. Sizing stress corrosion cracks using laser ultrasonics

    Energy Technology Data Exchange (ETDEWEB)

    Rehman, Hamood; McNealy, Rick; Fingerhut, Martin [Applus-RTD. Houston, TX (United States); Klein, Marvin; Ansari, Homayoon [Intelligent Optical Systems, Inc. Los Angeles, CA (United States); Kania Richard [TransCanada. Calgary, AB (Canada); Rapp, Steve [Spectra Energy, Houston, TX (United States)

    2010-07-01

    Despite various efforts, no reliable tools and techniques are available to enable an operator to quantify the impact of an SCC (Stress Corrosion Cracking) colony on the safety and integrity of a pipeline. Reliable non-destructive detection and measurement tools are not available either. There is therefore a large gap between current technology and the needs of the pipeline industry. Recent developments promise that with a concentrated effort, a comprehensive solution can be devised. This paper describes technical work performed to develop and validate both the inspection tool and the time of flight diffraction (TOFD) technique for sizing the depth of SCC. It also presents preliminary results of work on a closely related project that provides, on the basis of this technology, an integrated approach and tool for mapping, sizing, and evaluating SCC, through which significant cracks are filtered from more benign cracks within an SCC colony.

  4. Concrete cover cracking with localized corrosion of reinforcing steel

    Energy Technology Data Exchange (ETDEWEB)

    Torres-Acosta, A. A.; Sagues, A. A. [South Florida Univ., Dept of Civil and Environmental Engineering, Tampa FL (United States)

    2000-07-01

    The critical amount of steel corrosion needed for concrete cover cracking of a reinforced concrete element was measured, focusing on cases where only a fraction of the steel bar length is corroding. The amount of corrosion needed to crack the concrete cover was found to range between 49 micrometre to 137 micrometre in specimens of localized corrosion. In contrast, in cases of uniform corrosion of comparable systems the corrosion needed to crack the concrete cover varied from 15 micrometre to 75 micrometer. Based on this and previous work on this problem, an empirical equation is proposed for the critical amount of steel corrosion as a function of specimen dimensions. The model proposed for estimating the critical amount of steel corrosion showed reasonable agreement between estimates of the work of corrosion expansion and the energy required to crack the concrete. 23 refs., 3 tabs., 8 figs.

  5. Effect of prior corrosion state on the fatigue small cracking behaviour of 6151-T6 aluminum alloy

    Energy Technology Data Exchange (ETDEWEB)

    Li Xudong [Department of Engineering Mechanics, AML, Tsinghua University, Beijing 100084 (China); Naval Aeronautical Engineering Academy Qingdao Branch, Qingdao 266000 (China); Wang Xishu, E-mail: xshwang@tsinghua.edu.cn [Department of Engineering Mechanics, AML, Tsinghua University, Beijing 100084 (China); Ren Huaihui; Chen Yinlong [Department of Engineering Mechanics, AML, Tsinghua University, Beijing 100084 (China); Mu Zhitao [Naval Aeronautical Engineering Academy Qingdao Branch, Qingdao 266000 (China)

    2012-02-15

    Highlights: Black-Right-Pointing-Pointer Relationship of corrosion pit and fatigue crack is established based on SEM. Black-Right-Pointing-Pointer An equivalent relationship between accelerated and natural corrosion is build up. Black-Right-Pointing-Pointer Prior corrosion damage is crucial to the subsequent fatigue cracking behaviour. Black-Right-Pointing-Pointer The prior corrosion fatigue crack growth rate is expressed by the term of k{sigma}{sub max}{sup n}a. Black-Right-Pointing-Pointer Corrosion states such as SC15, are defined based on corrosion spectrum. - Abstract: The purpose of this paper was to estimate the reliable effect of prior corrosion state on fatigue micro crack initiation and early stage propagation behaviour of aluminum alloy based on scanning electron microscopy (SEM) in situ observation. Results indicated that multi-cracks initiation occurred almost at the corrosion pits and the early stage of fatigue micro crack propagation behaviour can be described by K{sub I}/K{sub II}-mixed mode. The importance of crack-face interaction via crack-face corrosion pits interlocking/bridging was emphasised in the mixed mode. The fatigue crack growth rate in the corrosion states can be empirically expressed by the term of k{sigma}{sub max}{sup n}a.

  6. Effect of Stress on Corrosion at Crack Tip on Pipeline Steel in a Near-Neutral pH Solution

    Science.gov (United States)

    Yang, Yao; Cheng, Y. Frank

    2016-10-01

    In this work, the local corrosion at crack tip on an API 5L X46 pipeline steel specimens was investigated under various applied loads in a near-neutral pH solution. Electrochemical measurements, including potentiodynamic polarization and electrochemical impedance spectroscopy, combined with micro-electrochemical technique and surface characterization, were conducted to investigate the effect of stress on local anodic solution of the steel at the crack tip. The stress corrosion cracking of the steel was dominated by an anodic dissolution mechanism, while the effect of hydrogen was negligible. The applied load (stress) increased the corrosion rate at the crack tip, contributing to crack propagation. The deposit of corrosion products at the crack tip could protect somewhat from further corrosion. At sufficiently large applied loads such as 740 N in the work, it was possible to generate separated cathode and anode, further accelerating the crack growth.

  7. Effect of Stress on Corrosion at Crack Tip on Pipeline Steel in a Near-Neutral pH Solution

    Science.gov (United States)

    Yang, Yao; Cheng, Y. Frank

    2016-11-01

    In this work, the local corrosion at crack tip on an API 5L X46 pipeline steel specimens was investigated under various applied loads in a near-neutral pH solution. Electrochemical measurements, including potentiodynamic polarization and electrochemical impedance spectroscopy, combined with micro-electrochemical technique and surface characterization, were conducted to investigate the effect of stress on local anodic solution of the steel at the crack tip. The stress corrosion cracking of the steel was dominated by an anodic dissolution mechanism, while the effect of hydrogen was negligible. The applied load (stress) increased the corrosion rate at the crack tip, contributing to crack propagation. The deposit of corrosion products at the crack tip could protect somewhat from further corrosion. At sufficiently large applied loads such as 740 N in the work, it was possible to generate separated cathode and anode, further accelerating the crack growth.

  8. Corrosion fatigue behavior of fastening hole structure and virtual crack propagation tests

    Institute of Scientific and Technical Information of China (English)

    Youhong Zhang; Xinlong Chang; Guozhi Lv; Hui Wang; Zhong Li; Yueliang Cheng

    2008-01-01

    The fatigue crack propagation behavior of the LY12CZ aluminum alloy fastener involving a central hole in air or in 3.5wt% NaC1 solution was investigated. The experimental results indicated that the corrosion fatigue crack growth rate decreased with the increasing loading frequency, and in a corrosive environment, the crack growth rate was slightly larger than that in air.Based on the experimental results, the virtual corrosion fatigue crack propagation tests were investigated and the stochastic process method and the AFGROW simulation method were presented. The normal process and lognormal process were considered for the stochastic process method based on the numerically fitted Paris equation. The distribution of crack size and the corresponding prob-abilistic model of crack length distribution for a given number of cycles can be found by integrating the stochastic process over time.Using the AFGROW software, the virtual simulation was carried out to analyze the corrosion fatigue crack growth behavior and the predicted crack growth curve was in good agreement with the experimental results.

  9. Hydrogen embrittlement and stress corrosion cracking in metals

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Young Suk; Cheong, Yong Mu; Im, Kyung Soo

    2004-10-15

    The objective of this report is to elucidate the mechanism for hydrogen embrittlement (HE) and stress corrosion cracking (SCC) in metals. To this end, we investigate the common features between delayed hydride cracking (DHC) in zirconium alloys and HE in metals with no precipitation of hydrides including Fe base alloys, Nickel base alloys, Cu alloys and Al alloys. Surprisingly, as with the crack growth pattern for the DHC in zirconium alloy, the metals mentioned above show a discontinuous crack growth, striation lines and a strong dependence of yield strength when exposed to hydrogen internally and externally. This study, for the first time, analyzes the driving force for the HE in metals in viewpoints of Kim's DHC model that a driving force for the DHC in zirconium alloys is a supersaturated hydrogen concentration coming from a hysteresis of the terminal solid solubility of hydrogen, not by the stress gradient, As with the crack growing only along the hydride habit plane during the DHC in zirconium alloys, the metals exposed to hydrogen seem to have the crack growing by invoking the dislocation slip along the preferential planes as a result of some interactions of the dislocations with hydrogen. Therefore, it seems that the hydrogen plays a role in inducing the slip only on the preferential planes so as to cause a strain localization at the crack tip. Sulfur in metals is detrimental in causing a intergranular cracking due to a segregation of the hydrogens at the grain boundaries. In contrast, boron in excess of 500 ppm added to the Ni3Al intermetallic compound is found to be beneficial in suppressing the HE even though further details of the mechanism for the roles of boron and sulfur are required. Carbon, carbides precipitating semi-continuously along the grain boundaries and the CSL (coherent site lattice) boundaries is found to suppress the intergranular stress corrosion cracking (IGSCC) in Alloy 600. The higher the volume fraction of twin boundaries, the

  10. Hydrogen embrittlement and stress corrosion cracking in metals

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Young Suk; Cheong, Yong Mu; Im, Kyung Soo

    2004-10-15

    The objective of this report is to elucidate the mechanism for hydrogen embrittlement (HE) and stress corrosion cracking (SCC) in metals. To this end, we investigate the common features between delayed hydride cracking (DHC) in zirconium alloys and HE in metals with no precipitation of hydrides including Fe base alloys, Nickel base alloys, Cu alloys and Al alloys. Surprisingly, as with the crack growth pattern for the DHC in zirconium alloy, the metals mentioned above show a discontinuous crack growth, striation lines and a strong dependence of yield strength when exposed to hydrogen internally and externally. This study, for the first time, analyzes the driving force for the HE in metals in viewpoints of Kim's DHC model that a driving force for the DHC in zirconium alloys is a supersaturated hydrogen concentration coming from a hysteresis of the terminal solid solubility of hydrogen, not by the stress gradient, As with the crack growing only along the hydride habit plane during the DHC in zirconium alloys, the metals exposed to hydrogen seem to have the crack growing by invoking the dislocation slip along the preferential planes as a result of some interactions of the dislocations with hydrogen. Therefore, it seems that the hydrogen plays a role in inducing the slip only on the preferential planes so as to cause a strain localization at the crack tip. Sulfur in metals is detrimental in causing a intergranular cracking due to a segregation of the hydrogens at the grain boundaries. In contrast, boron in excess of 500 ppm added to the Ni3Al intermetallic compound is found to be beneficial in suppressing the HE even though further details of the mechanism for the roles of boron and sulfur are required. Carbon, carbides precipitating semi-continuously along the grain boundaries and the CSL (coherent site lattice) boundaries is found to suppress the intergranular stress corrosion cracking (IGSCC) in Alloy 600. The higher the volume fraction of twin boundaries, the

  11. Corrosion-Fatigue Cracking in Al 7075 Alloys

    Science.gov (United States)

    2014-12-09

    Naval Research Laboratory Washington, DC 20375-5320 NRL/MR/6355--14-9582 Corrosion -Fatigue Cracking in Al 7075 Alloys December 9, 2014 P.S. Pao...PERSON 19b. TELEPHONE NUMBER (include area code) b. ABSTRACT c. THIS PAGE 18. NUMBER OF PAGES 17. LIMITATION OF ABSTRACT Corrosion -Fatigue Cracking in Al...Memorandum Report Corrosion -fatigue Aluminum alloys Environmental effect October 2011 – September 2014 63-2634-A4 Unclassified Unlimited Unclassified

  12. Crack Initiation and Growth Behavior at Corrosion Pit in 7075-T6 Under Biaxial and Uniaxial Fatigue

    Science.gov (United States)

    2014-06-19

    general conical , hemispherical, and roughly saucer-shaped for steel and many alloys [41], as shown in Figure 2.2. Pits usually nucleate at chemical or...performed in a piezoelectric resonance system. Their results indicated that the presence of corrosion pits notably reduces the fatigue life of the

  13. Effect of dissolved oxygen content on stress corrosion cracking of a cold worked 316L stainless steel in simulated pressurized water reactor primary water environment

    Science.gov (United States)

    Zhang, Litao; Wang, Jianqiu

    2014-03-01

    Stress corrosion crack growth tests of a cold worked nuclear grade 316L stainless steel were conducted in simulated pressurized water reactor (PWR) primary water environment containing various dissolved oxygen (DO) contents but no dissolved hydrogen. The crack growth rate (CGR) increased with increasing DO content in the simulated PWR primary water. The fracture surface exhibited typical intergranular stress corrosion cracking (IGSCC) characteristics.

  14. Transport and Corrosion Behavior of Cracked Reinforced Concrete

    DEFF Research Database (Denmark)

    Pease, Bradley Justin

    to enter the concrete. This is, among others, important in the corrosion of reinforcing steel. When cracks protrude to the depth of reinforcing steel, liquids containing aggressive ions (i.e. chlorides associated with salts and sea water) may rapidly access and initiate corrosion of the reinforcing...... structures. These models currently lack some of the scientific validity to fully represent actual field structures, i.e. structures containing cracks. Further understanding, therefore is needed on the effect cracks have on transport and corrosion in reinforced concrete. The fundamental mechanisms...... of transport and corrosion in cracked, reinforced concrete are not yet fully understood. The scope of this study therefore is to develop a link between concrete cracks and the relevant transport mechanism(s) under particular environmental conditions. It is envisioned that a finite element model...

  15. Some important considerations in the development of stress corrosion cracking test methods.

    Science.gov (United States)

    Wei, R. P.; Novak, S. R.; Williams, D. P.

    1972-01-01

    Discussion of some of the precaution needs the development of fracture-mechanics based test methods for studying stress corrosion cracking involves. Following a review of pertinent analytical fracture mechanics considerations and of basic test methods, the implications for test corrosion cracking studies of the time-to-failure determining kinetics of crack growth and life are examined. It is shown that the basic assumption of the linear-elastic fracture mechanics analyses must be clearly recognized and satisfied in experimentation and that the effects of incubation and nonsteady-state crack growth must also be properly taken into account in determining the crack growth kinetics, if valid data are to be obtained from fracture-mechanics based test methods.

  16. Relationship among Parameters Evaluating Stress Corrosion Cracking

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    @@The threshold stress, σc, for sulfide stress corrosion cracking (SCC) of seven pipeline steels and five other steels, the critical stress, SC, for seven pipeline steels and two drill rod steels with various strengths and the susceptibility to SCC, IRA or σf(SCC)/σf, for four pipeline steels, two drill rod steels and five other steels were measured. The results showed that there are no definite elationships among σc, SC and IRA or σf(SCC)/σf. The threshold stress for hydrogen induced cracking (HIC) during charging with loading in the H2SO4 solution, σc(H), decreased linearly with logarithm of the concentration of diffusible hydrogen c0, i.e., σC(H)=A-B Inc0 for four pipeline steels. σc(H) obtained with a special cathodic current ic, which was corresponding to the diffusible hydrogen concentration during immersing in the H2S solution, were consistent with σc for sulfide SCC for four pipeline steels.Therefore, σc for sulfide SCC can be measured using dynamically charging in the H2SO4 solution with the special cathodic current ic.

  17. Corrosion-Induced Concrete Cracking Model Considering Corrosion-Filled Paste

    OpenAIRE

    Dong, Jianfeng; Zhao, Yuxi; Wu, Yingyao; Jin, Weiliang

    2016-01-01

    A TCP–TCL model is established to describe the relationship between the thickness of the corrosion-filled paste (CP) and that of the corrosion layer (CL). This model can describe the phenomenon that the corrosion filling in the concrete pores and accumulating at the steel/concrete interface occur synchronously. Based on the TCP–TCL model, a corrosion-induced concrete cracking model, which can quantitatively consider corrosion-filled paste at concrete/steel interface, is proposed. Combined wit...

  18. Three-dimensional characterization of stress corrosion cracks

    DEFF Research Database (Denmark)

    Lozano-Perez, S.; Rodrigo, P.; Gontard, Lionel Cervera

    2011-01-01

    Understanding crack propagation and initiation is fundamental if stress corrosion cracking (SCC) mechanisms are to be understood. However, cracking is a three-dimensional (3D) phenomenon and most characterization techniques are restricted to two-dimensional (2D) observations. In order to overcome...... the best spatial resolution. To illustrate the power of these techniques, different parts of dominant stress corrosion cracks in Ni-alloys and stainless steels have been reconstructed in 3D. All relevant microstructural features can now be studied in detail and its relative orientation respect...

  19. A Monitoring Method Based on FBG for Concrete Corrosion Cracking

    Science.gov (United States)

    Mao, Jianghong; Xu, Fangyuan; Gao, Qian; Liu, Shenglin; Jin, Weiliang; Xu, Yidong

    2016-01-01

    Corrosion cracking of reinforced concrete caused by chloride salt is one of the main determinants of structure durability. Monitoring the entire process of concrete corrosion cracking is critical for assessing the remaining life of the structure and determining if maintenance is needed. Fiber Bragg Grating (FBG) sensing technology is extensively developed in photoelectric monitoring technology and has been used on many projects. FBG can detect the quasi-distribution of strain and temperature under corrosive environments, and thus it is suitable for monitoring reinforced concrete cracking. According to the mechanical principle that corrosion expansion is responsible for the reinforced concrete cracking, a package design of reinforced concrete cracking sensors based on FBG was proposed and investigated in this study. The corresponding relationship between the grating wavelength and strain was calibrated by an equal strength beam test. The effectiveness of the proposed method was verified by an electrically accelerated corrosion experiment. The fiber grating sensing technology was able to track the corrosion expansion and corrosion cracking in real time and provided data to inform decision-making for the maintenance and management of the engineering structure. PMID:27428972

  20. A Monitoring Method Based on FBG for Concrete Corrosion Cracking

    Directory of Open Access Journals (Sweden)

    Jianghong Mao

    2016-07-01

    Full Text Available Corrosion cracking of reinforced concrete caused by chloride salt is one of the main determinants of structure durability. Monitoring the entire process of concrete corrosion cracking is critical for assessing the remaining life of the structure and determining if maintenance is needed. Fiber Bragg Grating (FBG sensing technology is extensively developed in photoelectric monitoring technology and has been used on many projects. FBG can detect the quasi-distribution of strain and temperature under corrosive environments, and thus it is suitable for monitoring reinforced concrete cracking. According to the mechanical principle that corrosion expansion is responsible for the reinforced concrete cracking, a package design of reinforced concrete cracking sensors based on FBG was proposed and investigated in this study. The corresponding relationship between the grating wavelength and strain was calibrated by an equal strength beam test. The effectiveness of the proposed method was verified by an electrically accelerated corrosion experiment. The fiber grating sensing technology was able to track the corrosion expansion and corrosion cracking in real time and provided data to inform decision-making for the maintenance and management of the engineering structure.

  1. A Monitoring Method Based on FBG for Concrete Corrosion Cracking.

    Science.gov (United States)

    Mao, Jianghong; Xu, Fangyuan; Gao, Qian; Liu, Shenglin; Jin, Weiliang; Xu, Yidong

    2016-07-14

    Corrosion cracking of reinforced concrete caused by chloride salt is one of the main determinants of structure durability. Monitoring the entire process of concrete corrosion cracking is critical for assessing the remaining life of the structure and determining if maintenance is needed. Fiber Bragg Grating (FBG) sensing technology is extensively developed in photoelectric monitoring technology and has been used on many projects. FBG can detect the quasi-distribution of strain and temperature under corrosive environments, and thus it is suitable for monitoring reinforced concrete cracking. According to the mechanical principle that corrosion expansion is responsible for the reinforced concrete cracking, a package design of reinforced concrete cracking sensors based on FBG was proposed and investigated in this study. The corresponding relationship between the grating wavelength and strain was calibrated by an equal strength beam test. The effectiveness of the proposed method was verified by an electrically accelerated corrosion experiment. The fiber grating sensing technology was able to track the corrosion expansion and corrosion cracking in real time and provided data to inform decision-making for the maintenance and management of the engineering structure.

  2. Characterizing the effect of creep on stress corrosion cracking of cold worked Alloy 690 in supercritical water environment

    Science.gov (United States)

    Zhang, Lefu; Chen, Kai; Du, Donghai; Gao, Wenhua; Andresen, Peter L.; Guo, Xianglong

    2017-08-01

    The effect of creep on stress corrosion cracking (SCC) was studied by measuring crack growth rates (CGRs) of 30% cold worked (CW) Alloy 690 in supercritical water (SCW) and inert gas environments at temperatures ranging from 450 °C to 550 °C. The SCC crack growth rate under SCW environments can be regarded as the cracking induced by the combined effect of corrosion and creep, while the CGR in inert gas environment can be taken as the portion of creep induced cracking. Results showed that the CW Alloy 690 sustained high susceptibility to intergranular (IG) cracking, and creep played a dominant role in the SCC crack growth behavior, contributing more than 80% of the total crack growth rate at each testing temperature. The temperature dependence of creep induced CGRs follows an Arrhenius dependency, with an apparent activation energy (QE) of about 225 kJ/mol.

  3. Stress corrosion cracking resistance of aluminum alloy 7000 series after two-step aging

    Directory of Open Access Journals (Sweden)

    Jegdić Bore V.

    2015-01-01

    Full Text Available The effect of one step-and a new (short two-step aging on the resistance to stress corrosion cracking of an aluminum alloy 7000 series was investigated, using slow strain rate test and fracture mechanics method. Aging level in the tested alloy was evaluated by means of scanning electron microscopy and measurements of electrical resistivity. It was shown that the alloy after the new two-step aging is significantly more resistant to stress corrosion cracking. Values of tensile properties and fracture toughness are similar for both thermal states. Processes that take place at the crack tip have been considered. The effect of the testing solution temperature on the crack growth rate on the plateau was determined. Two values of the apparent activation energy were obtained. These values correspond to different processes that control crack growth rate on the plateau at higher and lower temperatures. [Projekat Ministarstva nauke Republike Srbije, br. TR 34028 i br. TR 34016

  4. Failure analysis of corrosion cracking and simulated testing for a fluid catalytic cracking unit

    Institute of Scientific and Technical Information of China (English)

    Hua Chen; Xiaogang Li; Chaofang Dong; Ming Li; Jinwen Yang

    2005-01-01

    The failure of a fluid catalysis and cracking unit (FCCU) in a Chinese refinery was investigated by using nondestructive detection methods, fracture surface examination, hardness measurement, chemical composition and corrosion products analysis. The results showed that the failure was caused by the dew point nitrate stress corrosion cracking. For a long operation period, the wall temperature of the regenerator in the FCCU was below the fume dew point. As a result, an acid fume NOx-SOx-H2O medium presented on the surface, resulting in stress corrosion cracking of the component with high residual stress. In order to confirm the relative conclusion, simulated testing was conducted in laboratory, and the results showed similar cracking characteristics. Finally, some suggestions have been made to prevent the stress corrosion cracking of an FCCU from re-occurring in the future.

  5. Analytical Solutions for Corrosion-Induced Cohesive Concrete Cracking

    Directory of Open Access Journals (Sweden)

    Hua-Peng Chen

    2012-01-01

    Full Text Available The paper presents a new analytical model to study the evolution of radial cracking around a corroding steel reinforcement bar embedded in concrete. The concrete cover for the corroding rebar is modelled as a thick-walled cylinder subject to axisymmetrical displacement constraint at the internal boundary generated by expansive corrosion products. A bilinear softening curve reflecting realistic concrete property, together with the crack band theory for concrete fracture, is applied to model the residual tensile stress in the cracked concrete. A governing equation for directly solving the crack width in cover concrete is established for the proposed analytical model. Closed-form solutions for crack width are then obtained at various stages during the evolution of cracking in cover concrete. The propagation of crack front with corrosion progress is studied, and the time to cracking on concrete cover surface is predicted. Mechanical parameters of the model including residual tensile strength, reduced tensile stiffness, and radial pressure at the bond interface are investigated during the evolution of cover concrete cracking. Finally, the analytical predictions are examined by comparing with the published experimental data, and mechanical parameters are analysed with the progress of reinforcement corrosion and through the concrete cover.

  6. Propagation of stress corrosion cracks in alpha-brasses

    Energy Technology Data Exchange (ETDEWEB)

    Beggs, Dennis Vinton [Univ. of Illinois, Urbana-Champaign, IL (United States)

    1981-01-01

    Transgranular and intergranular stress corrosion cracks were investigated in alpha-brasses in a tarnishing ammoniacal solution. Surface observation indicated that the transgranular cracks propagated discontinuously by the sudden appearance of a fine crack extending several microns ahead of the previous crack tip, often associated with the detection of a discrete acoustic emission (AE). By periodically increasing the deflection, crack front markings were produced on the resulting fracture surfaces, showing that the discontinuous propagation of the crack trace was representative of the subsurface cracking. The intergranular crack trace appeared to propagate continuously at a relatively blunt crack tip and was not associated with discrete AE. Under load pulsing tests with a time between pulses, Δt greater than or equal to 3 s, the transgranular fracture surfaces always exhibited crack front markings which corresponded with the applied pulses. The spacing between crack front markings, Δx, decreased linearly with Δt. With Δt less than or equal to 1.5 s, the crack front markings were in a one-to-one correspondence with applied pulses only at relatively long crack lengths. In this case, Δx = Δx* which approached a limiting value of 1 μm. No crack front markings were observed on intergranular fracture surfaces produced during these tests. It is concluded that transgranular cracking occurs by discontinuous mechanical fracture of an embrittled region around the crack tip, while intergranular cracking results from a different mechanism with cracking occurring via the film-rupture mechanism.

  7. Stress Corrosion Cracking Behavior of X80 Pipeline Steel in Acid Soil Environment with SRB

    Science.gov (United States)

    Wang, Dan; Xie, Fei; Wu, Ming; Liu, Guangxin; Zong, Yue; Li, Xue

    2017-06-01

    Self-designed experimental device was adopted to ensure the normal growth of sulphate-reducing bacteria (SRB) in sterile simulated Yingtan soil solution. Stress corrosion cracking (SCC) behavior of X80 pipeline steel in simulated acid soil environment was investigated by electrochemical impedance spectroscopy, slow strain rate test, and scanning electron microscope. Results show that the presence of SRB could promote stress corrosion cracking susceptibility. In a growth cycle, polarization resistance first presents a decrease and subsequently an increase, which is inversely proportional to the quantities of SRB. At 8 days of growth, SRB reach their largest quantity of 1.42 × 103 cells/g. The corrosion behavior is most serious at this time point, and the SCC mechanism is hydrogen embrittlement. In other SRB growth stages, the SCC mechanism of X80 steel is anodic dissolution. With the increasing SRB quantities, X80 steel is largely prone to SCC behavior, and the effect of hydrogen is considerably obvious.

  8. Study of the Effect of Swelling on Irradiation Assisted Stress Corrosion Cracking

    Energy Technology Data Exchange (ETDEWEB)

    Teysseyre, Sebastien Paul [Idaho National Lab. (INL), Idaho Falls, ID (United States)

    2016-09-01

    This report describes the methodology used to study the effect of swelling on the crack growth rate of an irradiation-assisted stress corrosion crack that is propagating in highly irradiated stainless steel 304 material irradiated to 33 dpa in the Experimental Breeder Reactor-II. The material selection, specimens design, experimental apparatus and processes are described. The results of the current test are presented.

  9. Stress Corrosion Cracks Initiation Process Model Involving Repetition of Growth and Breaking of Oxide Passive Film or Hydride Layer on Stainless Alloy

    Energy Technology Data Exchange (ETDEWEB)

    Nakayama, G.; Sakakibara, Y. [Research Laboratory, IHI Corporation (Japan)

    2009-07-01

    The surface of stainless alloy is covered with oxide film such as Cr{sub 2}O{sub 3} and is passivated in neutral aqueous solution. This film attains a thickness that may be expressed in micro meter units({mu}m) and may undergo partial rupture physically in a high-temperature oxygen enriched water environment. Crack propagation occurs through repeated growth and rupture of the oxide film; the rupturing process is designated as tarnish rupture type SCC. Individual cracks are initiated randomly for film of uniform thickness and this process may be described by the stochastic model. Hydride layer formation occurs on the alloy surface under the proper conditions, using titanium in a reducing neutral water environment. Crack initiation may thus also be described by a model similar to that for film rupture. (authors)

  10. The effect of heat treatment and test parameters on the aqueous stress corrosion cracking of D6AC steel

    Science.gov (United States)

    Gilbreath, W. P.; Adamson, M. J.

    1974-01-01

    The crack growth behavior of D6AC steel as a function of stress intensity, stress and corrosion history and test technique, under sustained load in natural seawater, 3.3 percent NaCl solution, distilled water, and high humidity air was investigated. Reported investigations of D6AC were considered with emphasis on thermal treatment, specimen configuration, fracture toughness, crack-growth rates, initiation period, threshold, and the extension of corrosion fatigue data to sustained load conditions. Stress history effects were found to be most important in that they controlled incubation period, initial crack growth rates, and apparent threshold.

  11. The crack growth mechanism in asphaltic mixes

    NARCIS (Netherlands)

    Jacobs, .M.M.J.; Hopman, P.C.; Molenaar, A.A.A.

    1995-01-01

    The crack growth mechanism in asphalt concrete (Ac) mixes is studied. In cyclic tests on several asphaltic mixes crack growth is measured, both with crack foils and with cOD-gauges. It is found that crack growth in asphaltic mixes is described by three processes which are parallel in time: cohesive

  12. Concrete cover cracking due to uniform reinforcement corrosion

    DEFF Research Database (Denmark)

    Solgaard, Anders Ole Stubbe; Michel, Alexander; Geiker, Mette Rica;

    2013-01-01

    is calculated using literature data on corrosion rate and Faraday’s law. The parameters varied comprise reinforcement diameter, concrete cover thickness and concrete material properties, viz. concrete tensile strength and ductility (plain concrete and fibre reinforced concrete). Results obtained from......Service life design (SLD) is an important tool for civil engineers to ensure that the structural integrity and functionality of the structure is not compromised within a given time frame, i.e. the service life. In SLD of reinforced concrete structures, reinforcement corrosion is of major concern...... and reinforcement de-passivation is a frequently used limit state. The present paper investigates an alternative limit state: corrosion-induced cover cracking. Results from numerical simulations of concrete cover cracking due to reinforcement corrosion are presented. The potential additional service life...

  13. Three-dimensional characterization of stress corrosion cracks

    Energy Technology Data Exchange (ETDEWEB)

    Lozano-Perez, S., E-mail: sergio.lozano-perez@materials.ox.ac.u [University of Oxford, Department of Materials, Parks Road, Oxford OX1 3PH (United Kingdom); Rodrigo, P. [Universidad Rey Juan Carlos, Dpto. de Ciencia e Ingenieria de Materiales, c/ Tulipan s.n., 28933 Mostoles (Madrid) (Spain); Gontard, Lionel C. [Danish Technical University, Center for Electron Nanoscopy, Matematiktorvet Building 307, Room 115, 2800 Kogens Lyngby (Denmark)

    2011-01-31

    Understanding crack propagation and initiation is fundamental if stress corrosion cracking (SCC) mechanisms are to be understood. However, cracking is a three-dimensional (3D) phenomenon and most characterization techniques are restricted to two-dimensional (2D) observations. In order to overcome this problem, different approaches to extract 3D information have been used in the recent years. In this work we will present the benefits of using 3D focused ion beam (FIB) slicing and electron tomography. 3D FIB slicing offers a fast and high throughput characterization while electron tomography offers the best spatial resolution. To illustrate the power of these techniques, different parts of dominant stress corrosion cracks in Ni-alloys and stainless steels have been reconstructed in 3D. All relevant microstructural features can now be studied in detail and its relative orientation respect to the strain direction and grain boundary plane accurately measured.

  14. A non-destructive test method to monitor corrosion products and corrosion-induced cracking in reinforced cement based materials

    DEFF Research Database (Denmark)

    Michel, Alexander; Pease, Bradley Justin; Peterova, Adela;

    2011-01-01

    ) was conducted to describe the impact of water-to-cement ratio and corrosion current density (i.e., corrosion rate) on the reinforcement corrosion process. Focus was placed, in particular on the determination of the corrosion accommodating region (CAR) and time to corrosion-induced cracking. Experimental results...

  15. Modeling time-dependent corrosion fatigue crack propagation in 7000 series aluminum alloys

    Science.gov (United States)

    Mason, Mark E.; Gangloff, Richard P.

    1994-01-01

    Stress corrosion cracking and corrosion fatigue experiments were conducted with the susceptible S-L orientation of AA7075-T651, immersed in acidified and inhibited NaCl solution, to provide a basis for incorporating environmental effects into fatigue crack propagation life prediction codes such as NASA FLAGRO. This environment enhances da/dN by five to ten-fold compared to fatigue in moist air. Time-based crack growth rates from quasi-static load experiments are an order of magnitude too small for accurate linear superposition prediction of da/dN for loading frequencies above 0.001 Hz. Alternate methods of establishing da/dt, based on rising-load or ripple-load-enhanced crack tip strain rate, do not increase da/dt and do not improve linear superposition. Corrosion fatigue is characterized by two regimes of frequency dependence; da/dN is proportional to f(exp -1) below 0.001 Hz and to F(exp 0) to F(exp -0.1) for higher frequencies. Da/dN increases mildly both with increasing hold-time at K(sub max) and with increasing rise-time for a range of loading waveforms. The mild time-dependence is due to cycle-time-dependent corrosion fatigue growth. This behavior is identical for S-L nd L-T crack orientations. The frequency response of environmental fatigue in several 7000 series alloys is variable and depends on undefined compositional or microstructural variables. Speculative explanations are based on the effect of Mg on occluded crack chemistry and embritting hydrogen uptake, or on variable hydrogen diffusion in the crack tip process zone. Cracking in the 7075/NaCl system is adequately described for life prediction by linear superposition for prolonged load-cycle periods, and by a time-dependent upper bound relationship between da/dN and delta K for moderate loading times.

  16. Detection of corrosion processes and fatigue cracks by means of acoustic emission monitoring

    Energy Technology Data Exchange (ETDEWEB)

    Jagenbrein, Andreas; Tscheliesnig, Peter [TUEV Austria Services GmbH, Vienna (Austria); Wachsmuth, Janne; Bohse, Juergen [Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin (Germany)

    2012-07-01

    Fatigue crack growth and active corrosion processes are the main causes for structural failures of transport products like road tankers, railway tank cars, and ships. Within the 7{sup th} EC framework programme the aim of project CORFAT is to develop a new monitoring technology based on acoustic emission testing (AT) of the structural integrity in terms of proceeding degradation. Differentiation of acoustic emission (AE) signals of real degradation processes by fatigue crack growth or active corrosion from operational or environmental background noise requires the signal classification using also pattern recognition. Therefore, a data base of AE signals related to the different source mechanisms was built up experimentally. In this article selected results of corrosion and fatigue tests in the laboratory as well as results of monitoring background noise during moving of a road tanker are described. (orig.)

  17. De-alloying and stress-corrosion cracking. Final report

    Energy Technology Data Exchange (ETDEWEB)

    Sieradzki, K.

    1998-09-01

    This research program has had two major areas of focus that are related: (1) alloy corrosion and (2) the role of selective dissolution in the stress corrosion cracking of alloy systems. These interrelated issues were examined using model systems such as Ag-Au and Cu-Au by conventional electrochemical techniques, in situ scanning tunneling microscopy (STM), in situ small angle neutron scattering (SANS), ultrahigh speed digital photography of fracture events, and computer simulations. The STM and SANS work were specifically aimed at addressing a roughening transition known to occur in alloy systems undergoing corrosion at electrochemical potentials greater than the so-called critical potential. Analytical models of de-alloying processes including the roughening transition were developed that specifically include curvature effects that are important in alloy corrosion processes. Stress-corrosion experiments were performed on the same model systems using rapid optical and electrochemical techniques on 50 {micro}m--250 {micro}m thick sheets and small diameter wires. The primary goal of this work was to develop a fundamental understanding of the corrosion and electrochemistry of alloys and the stress-corrosion cracking processes these alloys undergo. Computer simulations and analytical work identified surface stress and an important parameter in environmentally assisted fracture. The major results of the research on this program since the summer of 1993 are briefly summarized.

  18. Chemical milling solution reveals stress corrosion cracks in titanium alloy

    Science.gov (United States)

    Braski, D. N.

    1967-01-01

    Solution of hydrogen flouride, hydrogen peroxide, and water reveals hot salt stress corrosion cracks in various titanium alloys. After the surface is rinsed in water, dried, and swabbed with the solution, it can be observed by the naked eye or at low magnification.

  19. Smeared crack modelling approach for corrosion-induced concrete damage

    DEFF Research Database (Denmark)

    Thybo, Anna Emilie Anusha; Michel, Alexander; Stang, Henrik

    2017-01-01

    compared to experimental data obtained by digital image correlation and published in the literature. Excellent agreements between experimentally observed and numerically predicted crack patterns at the micro and macro scale indicate the capability of the modelling approach to accurately capture corrosion...

  20. Irradiation-Assisted Stress Corrosion Cracking of Austenitic Stainless Steels in BWR Environments

    Energy Technology Data Exchange (ETDEWEB)

    Chen, Y. [Argonne National Lab. (ANL), Argonne, IL (United States); Chopra, O. K. [Argonne National Lab. (ANL), Argonne, IL (United States); Gruber, Eugene E. [Argonne National Lab. (ANL), Argonne, IL (United States); Shack, William J. [Argonne National Lab. (ANL), Argonne, IL (United States)

    2010-06-01

    The internal components of light water reactors are exposed to high-energy neutron irradiation and high-temperature reactor coolant. The exposure to neutron irradiation increases the susceptibility of austenitic stainless steels (SSs) to stress corrosion cracking (SCC) because of the elevated corrosion potential of the reactor coolant and the introduction of new embrittlement mechanisms through radiation damage. Various nonsensitized SSs and nickel alloys have been found to be prone to intergranular cracking after extended neutron exposure. Such cracks have been seen in a number of internal components in boiling water reactors (BWRs). The elevated susceptibility to SCC in irradiated materials, commonly referred to as irradiation-assisted stress corrosion cracking (IASCC), is a complex phenomenon that involves simultaneous actions of irradiation, stress, and corrosion. In recent years, as nuclear power plants have aged and irradiation dose increased, IASCC has become an increasingly important issue. Post-irradiation crack growth rate and fracture toughness tests have been performed to provide data and technical support for the NRC to address various issues related to aging degradation of reactor-core internal structures and components. This report summarizes the results of the last group of tests on compact tension specimens from the Halden-II irradiation. The IASCC susceptibility of austenitic SSs and heat-affected-zone (HAZ) materials sectioned from submerged arc and shielded metal arc welds was evaluated by conducting crack growth rate and fracture toughness tests in a simulated BWR environment. The fracture and cracking behavior of HAZ materials, thermally sensitized SSs and grain-boundary engineered SSs was investigated at several doses (≤3 dpa). These latest results were combined with previous results from Halden-I and II irradiations to analyze the effects of neutron dose, water chemistry, alloy compositions, and welding and processing conditions on IASCC

  1. Effect of hydrogen on stress corrosion cracking of copper

    Institute of Scientific and Technical Information of China (English)

    Li-jie QIAO

    2008-01-01

    The effects of hydrogen on electrochemical behavior and susceptibility of stress corrosion cracking (SCC) of pure copper were studied. SCC susceptibility of pure copper in a 1 M NaNO2 solution was increased by pre-charged hydrogen. The effect of hydrogen on the sus-ceptibility is more obvious in the low stress region due to the longer fracture time, which resulted in a longer time for more hydrogen to diffuse toward the crack tip. Synergistic effects of hydrogen and stress on corrosion and SCC pro-cesses were discussed. The results showed that an inter-action between stress and hydrogen at the crack tip could increase the anodic dissolution rate remarkably.

  2. Microbial Corrosion and Cracking in Steel

    DEFF Research Database (Denmark)

    Hilbert, Lisbeth Rischel

    1998-01-01

    and for recommendations in regards to electrochemical monitoring of MIC. The work presented here and further studies are also planned to lead to a Ph.D. thesis on "MIC monitoring based on mechanisms of corrosion".The results of laboratory experiments conducted in the period 1995 to 1997 are summarised. Conclusions...... will be based on results from the entire 3 year period, but only selected experimental data primarily from the latest experiments will be presented in detail here.Microbial corrosion of carbon steel under influence of sulphate-reducing bacteria (SRB) is characterised by the formation of both biofilm...... and corrosion products (ferrous sulphides) on the metal surface. Experiments have been conducted on carbon steel exposed in near neutral (pH 6 to 8.5) saline hydrogen sulphide environment (0 to 100 mg/l total dissolved sulphide) for a period of 14 days. Furthermore coupons have been exposed in a bioreactor...

  3. Inhibiting Corrosion Cracking: Crack Tip Chemistry and Physics.

    Science.gov (United States)

    1986-03-14

    5 5. Swuzary 113 Rferences 114 wl NO 4L iv . List of Figuring 1. Microipette pulling machine . 29 2. Anodic polarization of 7075-T6 Al alloy in dilute...environment has a strong effect on microplastic behavior at the tip of a fatigue crack. Stolz and Pelloux suggest that nitrate ion competes with chloride...Crystalline Na2 N 20 29H20 precipitates when the filtrate is placed in a vacunm desiccator over sulfuric acid. The filtered precipitate is washed

  4. A Fundamental study of remedial technology development to prevent stress corrosion cracking of steam generator tubing

    Energy Technology Data Exchange (ETDEWEB)

    Park, In Gyu; Lee, Chang Soon [Sunmoon University, Asan (Korea)

    1998-04-01

    Most of the PWR Steam generators with tubes in Alloy 600 alloy are affected by Stress Corrosion Cracking, such as PWSCC(Primary Water Stress Corrosion Cracking) and ODSCC(Outside Diameter Stress Corrosion Cracking). This study was undertaken to establish the background for remedial technology development to prevent SCC. in the report are included the following topics: (1) General: (i) water chemistry related factors, (ii) Pourbaix(Potential-pH) Diagram, (iii) polarization plot, (iv) corrosion mode of Alloy 600, 690, and 800, (v) IGA/SCC growth rate, (vi) material suspetibility of IGA/SCC, (vii) carbon solubility of Alloy 600 (2) Microstructures of Alloy 600 MA, Alloy 600 TT, Alloy 600 SEN Alloy 690 TT(Optical, SEM, and TEM) (3) Influencing factors for PWSCC initiation rate of Alloy 600: (i) microstructure, (ii) water chemistry(B, Li), (iii) temperature, (iv) plastic deformation, (v) stress relief annealing (4) Influencing factors for PWSCC growth rate of Alloy 600: (i) water chemistry(B, Li), (ii) Scott Model, (iii) intergranular carbide, (iv) temperature, (v) hold time (5) Laboratory conditions for ODSCC initiation rate: 1% NaOH, 316 deg C; 1% NaOH, 343 deg C; 50% NaOH, 288 deg C; 10% NaOH, 302 deg C; 10% NaOH, 316 deg C; 50% NaOH, 343 deg C (6) Sludge effects for ODSCC initiation rate: CuO, Cr{sub 2}O{sub 3}, Fe{sub 3}O{sub 4} (7) Influencing factors for PWSCC growth rate of Alloy 600: (i) Caustic concentration effect, (ii) carbonate addition effect (8) Sulfate corrosion: (i) sulfate ratio and pH effect, (ii) wastage rate of Alloy 600 and Alloy 690 (9) Crevice corrosion: (i) experimental setup for crevice corrosion, (ii) organic effect, (iii) (Na{sub 2}SO{sub 4} + NaOH) effect (10) Remedial measures for SCC: (i) Inhibitors, (ii) ZnO effect. (author). 30 refs., 174 figs., 51 tabs.

  5. A Global Refiability Assessment Method on Aging Offshore Platforms with Corrosion and Cracks

    Institute of Scientific and Technical Information of China (English)

    JI Chun-yan; LI Shan-shan; CHEN Ming-lu

    2009-01-01

    Corrosion and fatigue cracks are major threats to the structural integrity of aging offshore platforms.For the rational estimation of the safety levels of aging platforms,a global reliability assessment approach for aging offshore platforms with corrosion and fatigue cracks is presented in this paper.The base shear capacity is taken as the global ultimate strength of the offshore plaffoms,it is modeled as a random process that decreases with time in the presence of corrosion and fatigue crack propagation.And the corrosion and fatigue crack growth rates in the main members and key joints are modeled as random variables.A simulation method of the extreme wave loads which are applied to the structures of offshore platforms is proposed too.Furthermore,the statistics of global base shear capacity and extreme wave loads are obtained by Monte Carlo simulation method.On the basis of the limit state equation of global failure mode,the instantaneous reliability and time dependent reliability assessment methods are both presented in this paper.Finally the instantaueous reliability index and time dependent failure probability of a jacket platform are estimated with different ages in the demonstration example.

  6. Microbial Corrosion and Cracking in Steel

    DEFF Research Database (Denmark)

    Hilbert, Lisbeth Rischel

    1998-01-01

    and corrosion products (ferrous sulphides) on the metal surface. Experiments have been conducted on carbon steel exposed in near neutral (pH 6 to 8.5) saline hydrogen sulphide environment (0 to 100 mg/l total dissolved sulphide) for a period of 14 days. Furthermore coupons have been exposed in a bioreactor...... for a period of up to 120 days in sulphide-producing environment controlled by biological activity of (SRB).Electrochemical studies have been conducted in order to characterise the electrochemical response of the biofilm / ferrous sulphide / metal interface and clarify whether the tested electrochemical...... and not electrochemically active film. The polarisation resistance increases with the film resistance and an small underestimation of corrosion rate is possible, if film resistance is large.· An electrochemically reactive film (ferrous sulphides) results in current contributions that will be added to the metal dissolution...

  7. Mechanical factors in primary water stress corrosion cracking of cold-worked stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Hammadi, Rashid Al, E-mail: rashid.alhammadi@fanr.gov.ae [Nuclear Security Division, Federal Authority for Nuclear Regulation, Abu Dhabi (United Arab Emirates); Yi, Yongsun, E-mail: yongsun.yi@kustar.ac.ae [Department of Nuclear Engineering, Khalifa University, Abu Dhabi (United Arab Emirates); Zaki, Wael, E-mail: wael.zaki@kustar.ac.ae [Department of Mechanical Engineering, Khalifa University, Abu Dhabi (United Arab Emirates); Cho, Pyungyeon, E-mail: pyungyeon.cho@kustar.ac.ae [Department of Nuclear Engineering, Khalifa University, Abu Dhabi (United Arab Emirates); Jang, Changheui, E-mail: chjang@kaist.ac.kr [Nuclear and Quantum Engineering Department, Korea Advanced Institute of Science and Technology, Daejeon (Korea, Republic of)

    2016-05-15

    Highlights: • PWSCC of cold-worked austenitic stainless steel was studied. • Finite element analysis was performed on a compact tension specimen. • Mechanical fields near a crack tip were evaluated using FEA. • The dependence of mechanical factors on K{sub I} and yield stress was investigated. • The crack tip normal stress was identified as a main factor controlling PWSCC. - Abstract: Finite element analysis was performed on a compact tension specimen to determine the stress and strain distributions near a crack tip. Based on the results, the crack tip stain rates by crack advance and creep rates near crack tip were estimated. By comparing the dependence of the mechanical factors on the stress intensity factor and yield stress with that of the SCC crack growth rates, it was tried to identify the main mechanical factor for the primary water stress corrosion cracking (PWSCC) of cold-worked austenitic stainless steels. The analysis results showed that the crack tip normal stress could be the main mechanical factor controlling the PWSCC, suggesting that the internal oxidation mechanism might be the most probable PWSCC mechanism of cold-worked austenitic stainless steels.

  8. Stress Corrosion Cracking in Al-Zn-Mg-Cu Aluminum Alloys in Saline Environments

    Science.gov (United States)

    Holroyd, N. J. Henry; Scamans, G. M.

    2013-03-01

    Stress corrosion cracking of Al-Zn-Mg-Cu (AA7xxx) aluminum alloys exposed to saline environments at temperatures ranging from 293 K to 353 K (20 °C to 80 °C) has been reviewed with particular attention to the influences of alloy composition and temper, and bulk and local environmental conditions. Stress corrosion crack (SCC) growth rates at room temperature for peak- and over-aged tempers in saline environments are minimized for Al-Zn-Mg-Cu alloys containing less than ~8 wt pct Zn when Zn/Mg ratios are ranging from 2 to 3, excess magnesium levels are less than 1 wt pct, and copper content is either less than ~0.2 wt pct or ranging from 1.3 to 2 wt pct. A minimum chloride ion concentration of ~0.01 M is required for crack growth rates to exceed those in distilled water, which insures that the local solution pH in crack-tip regions can be maintained at less than 4. Crack growth rates in saline solution without other additions gradually increase with bulk chloride ion concentrations up to around 0.6 M NaCl, whereas in solutions with sufficiently low dichromate (or chromate), inhibitor additions are insensitive to the bulk chloride concentration and are typically at least double those observed without the additions. DCB specimens, fatigue pre-cracked in air before immersion in a saline environment, show an initial period with no detectible crack growth, followed by crack growth at the distilled water rate, and then transition to a higher crack growth rate typical of region 2 crack growth in the saline environment. Time spent in each stage depends on the type of pre-crack ("pop-in" vs fatigue), applied stress intensity factor, alloy chemistry, bulk environment, and, if applied, the external polarization. Apparent activation energies ( E a) for SCC growth in Al-Zn-Mg-Cu alloys exposed to 0.6 M NaCl over the temperatures ranging from 293 K to 353 K (20 °C to 80 °C) for under-, peak-, and over-aged low-copper-containing alloys (alloys (>~0.8 wt pct), they are typically

  9. Crack growth simulation in heterogeneous material by S-FEM and comparison with experiments

    Directory of Open Access Journals (Sweden)

    Masanori Kikuchi

    2015-10-01

    Full Text Available Fully automatic fatigue crack growth simulation system is developed using S-version FEM (SFEM. This system is extended to fracture in heterogeneous material. In the heterogeneous material, crack tip stress field becomes mixed mode condition, and crack growth path is affected by inhomogeneous materials and mixed mode conditions. Stress Intensity Factors (SIF in mixed mode condition are evaluated using Virtual Crack Closure Method (VCCM. Criteria for crack growth amount and crack growth path are used based on these SIFs, and growing crack configurations are obtained. Three crack growth problems are simulated. One is crack growth in bi-materila made of CFRP plate and Aluminum alloy. Initial crack is located in CFRP plate, and grows toward Aluminum alloy. Crack growing direction changes and results are compared with experimental one. Second problem is crack growth in bimaterial made of PMMA and Aluminum alloy. Initial crack is located in PMMA plate and parallel to phase boundary. By cahnging loading conditions, several cases are simulated and compared with experimental ones. In the experiment, crack grows into pahse boundary and grow along it. This case is simulated precisely, and the effect of pahse boundary is discussed. Last case is Stress Corrosion Cracking (SCC at Hot-Leg Safe-End of Pressurized Water Rreactor. This location is made of many kinds of steels by welding. In some steel, SCC does not occur and in other steel, SCC is accelerated. As a result, small surface crack grows in complicated manner.

  10. 核电汽轮机转子结构应力腐蚀裂纹扩展研究%Study on Stress Corrosion Cracking Growth of Turbine Rotor in Power Plant

    Institute of Scientific and Technical Information of China (English)

    焦广臣; 王炜哲; 蒋浦宁; 刘应征

    2013-01-01

    建立二维轴对称转子模型,有限元计算转子结构的应力场和稳态温度场.以这些计算结果为基础,采用Clark裂纹扩展模型和Paris裂纹扩展模型分析在不同的裂纹尺寸下转子结构中某点的应力腐蚀裂纹扩展速率,比较两种模型在工程实际应用中的优劣.%The stress fields and steady temperature fields are obtained by calculating the rotor model of 2D axisymmetric model by using the finite element analysis ( FEA). Based on the numerical results, the stress corrosion crack ( SCC ) growths at a certain point of the model are calculated by using the Clark model and the Paris model, and the comparative analysis of the results of two crack growth model is made for advantage in practical application.

  11. Stress corrosion cracking of titanium alloys

    Science.gov (United States)

    Statler, G. R.; Spretnak, J. W.; Beck, F. H.; Fontana, M. G.

    1974-01-01

    The effect of hydrogen on the properties of metals, including titanium and its alloys, was investigated. The basic theories of stress corrosion of titanium alloys are reviewed along with the literature concerned with the effect of absorbed hydrogen on the mechanical properties of metals. Finally, the basic modes of metal fracture and their importance to this study is considered. The experimental work was designed to determine the effects of hydrogen concentration on the critical strain at which plastic instability along pure shear directions occurs. The materials used were titanium alloys Ti-8Al-lMo-lV and Ti-5Al-2.5Sn.

  12. Application of new experimental methods to pipeline stress corrosion cracking. Annual report, March 1992-February 1993

    Energy Technology Data Exchange (ETDEWEB)

    Schmidt, C.G.; Kobayashi, T.; Becker, C.H.; Pound, B.G.; Simons, J.W.

    1993-04-01

    The objective of the investigation is to develop a physically based understanding of the mechanisms of stress corrosion cracking (SCC) in pipeline steels by applying advanced fracture surface and electrochemical characterization techniques to samples taken from fielded pipeline. The investigations found that the effect of pressure fluctuations on the propagation of stress corrosion cracks was readily evident from an analysis of the topographies of conjugate fracture surfaces. Substantial crack blunting was produced under normal pipeline operating conditions. Corrosion deposits were removed from the fracture surfaces of a stress corrosion crack in a pipeline specimen recovered from service. The topography of the underlying metal surface appears to be preserved with little corrosion damage after crack formation. This allowed the cracking process to be reconstructed from the surface topography. In some cases, deposits on the fracture surfaces of stress corrosion cracks contain significant concentrations of metallic elements that are not found in pipeline steels but are likely to be commonplace in the surrounding environment.

  13. Susceptibility to Stress Corrosion Cracking of 254SMO SS

    Directory of Open Access Journals (Sweden)

    De Micheli Lorenzo

    2002-01-01

    Full Text Available The susceptibility to stress corrosion cracking (SCC of solubilized and sensitized 254SMO SS was studied in sodium chloride, and sodium fluoride solutions at 80 °C and sulfuric acid solutions in presence of sodium chloride at 25 °C. The influence of salt concentration, pH values and the addition of thiosulfate was examined. The susceptibility to SCC was evaluated by Slow Strain Rate Tests (SSRT, at 1.5 x 10-6 s-1 strain rate. The behavior of 254SMO was compared to those of AISI 316L SS and Hastelloy C276. 254SMO showed an excellent resistance to SCC in all conditions, except in the more acidic solutions (pH <= 1 where, in the sensitized conditions, intergranular stress corrosion cracking occurred.

  14. Uncertainty quantification methodologies development for stress corrosion cracking of canister welds

    Energy Technology Data Exchange (ETDEWEB)

    Dingreville, Remi Philippe Michel [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Bryan, Charles R. [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)

    2016-09-30

    This letter report presents a probabilistic performance assessment model to evaluate the probability of canister failure (through-wall penetration) by SCC. The model first assesses whether environmental conditions for SCC – the presence of an aqueous film – are present at canister weld locations (where tensile stresses are likely to occur) on the canister surface. Geometry-specific storage system thermal models and weather data sets representative of U.S. spent nuclear fuel (SNF) storage sites are implemented to evaluate location-specific canister surface temperature and relative humidity (RH). As the canister cools and aqueous conditions become possible, the occurrence of corrosion is evaluated. Corrosion is modeled as a two-step process: first, pitting is initiated, and the extent and depth of pitting is a function of the chloride surface load and the environmental conditions (temperature and RH). Second, as corrosion penetration increases, the pit eventually transitions to a SCC crack, with crack initiation becoming more likely with increasing pit depth. Once pits convert to cracks, a crack growth model is implemented. The SCC growth model includes rate dependencies on both temperature and crack tip stress intensity factor, and crack growth only occurs in time steps when aqueous conditions are predicted. The model suggests that SCC is likely to occur over potential SNF interim storage intervals; however, this result is based on many modeling assumptions. Sensitivity analyses provide information on the model assumptions and parameter values that have the greatest impact on predicted storage canister performance, and provide guidance for further research to reduce uncertainties.

  15. Stress corrosion cracking of brass in ammonia solution

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    Brass foil with a protective layer formed on one side was deflected during corrosion in an ammonia solution under various applied potentials, and then corrosion-induced stress generated at brass/dezincification layer under different potentials could be measured. At the same time, susceptibility to stress corrosion cracking(SCC) of brass in the ammonia solution under various applied potentials was measured using a single-edge notched specimen. At open-circuit potential, both corrosion-induced tensile stress and susceptibility to SCC(Iσ) had a maximum value. Both tensile stress σp and susceptibility Iσ decreased slightly under anodic polarization, but reduced steeply with the decrease in potential of cathodic polarization. At the cathodic potential of -500  mV(vs SCE), corrosion-induced stress became compressive because of copper-plating layer, correspondingly, susceptibility to SCC was zero. Therefore, the variation of SCC susceptibility with potential is consistent with that of the corrosion-induced additive stress.

  16. Stress corrosion crack initiation of alloy 600 in PWR primary water

    Energy Technology Data Exchange (ETDEWEB)

    Zhai, Ziqing; Toloczko, Mychailo B.; Olszta, Matthew J.; Bruemmer, Stephen M.

    2017-07-01

    Stress corrosion crack (SCC) initiation of three mill-annealed (MA) alloy 600 heats in simulated pressurized water reactor primary water has been investigated using constant load tests equipped with in-situ direct current potential drop (DCPD) measurement capabilities. SCC initiation times were greatly reduced by a small amount of cold work. Shallow intergranular (IG) attack and/or cracks were found on most high-energy grain boundaries intersecting the surface with only a small fraction evolving into larger cracks and IGSCC growth. Crack depth profiles were measured and related to DCPD-detected initiation response. Processes controlling the SCC initiation in MA alloy 600 are discussed. IN PRESS, CORRECTED PROOF, 05/02/2017 - mfl

  17. Modeling of Stress Corrosion Cracking for High Level Radioactive-Waste Packages

    Energy Technology Data Exchange (ETDEWEB)

    Lu, S C; Gordon, G M; Andresen, P L; Herrera, M L

    2003-06-20

    A stress corrosion cracking (SCC) model has been adapted for performance prediction of high level radioactive-waste packages to be emplaced in the proposed Yucca Mountain radioactive-waste repository. SCC is one form of environmentally assisted cracking due to three factors, which must be present simultaneously: metallurgical susceptibility, critical environment, and static (or sustained) tensile stresses. For waste packages of the proposed Yucca Mountain repository, the outer barrier material is Alloy 22, a highly corrosion resistant alloy, the environment is represented by the water film present on the surface of the waste package from dripping or deliquescence of soluble salts present in any surface deposits, and the stress is principally the weld induced residual stress. SCC has historically been separated into ''initiation'' and ''propagation'' phases. Initiation of SCC will not occur on a smooth surface if the surface stress is below a threshold value defined as the threshold stress. Cracks can also initiate at and propagate from flaws (or defects) resulting from manufacturing processes (such as welding). To account for crack propagation, the slip dissolution/film rupture (SDFR) model is adopted to provide mathematical formulas for prediction of the crack growth rate. Once the crack growth rate at an initiated SCC is determined, the time to through-wall penetration for the waste package can be calculated. The SDFR model relates the advance (or propagation) of cracks, subsequent to the crack initiation from bare metal surface, to the metal oxidation transients that occur when the protective film at the crack tip is continually ruptured and repassivated. A crack, however, may reach the ''arrest'' state before it enters the ''propagation'' phase. There exists a threshold stress intensity factor, which provides a criterion for determining if an initiated crack or pre

  18. Concrete Cracking Prediction Including the Filling Proportion of Strand Corrosion Products

    Directory of Open Access Journals (Sweden)

    Lei Wang

    2016-12-01

    Full Text Available The filling of strand corrosion products during concrete crack propagation is investigated experimentally in the present paper. The effects of stirrups on the filling of corrosion products and concrete cracking are clarified. A prediction model of crack width is developed incorporating the filling proportion of corrosion products and the twisting shape of the strand. Experimental data on cracking angle, crack width, and corrosion loss obtained from accelerated corrosion tests of concrete beams are presented. The proposed model is verified by experimental data. Results show that the filling extent of corrosion products varies with crack propagation. The rust filling extent increases with the propagating crack until a critical width. Beyond the critical width, the rust-filling extent remains stable. Using stirrups can decrease the critical crack width. Stirrups can restrict crack propagation and reduce the rust filling. The tangent of the cracking angle increases with increasing corrosion loss. The prediction of corrosion-induced crack is sensitive to the rust-filling extent.

  19. Reliability Model of Corrosion Fatigue Crack Growth Rate Evaluation of LD10CS Aluminum Alloy%LD10CS腐蚀疲劳裂纹扩展速率评价的可靠性模型

    Institute of Scientific and Technical Information of China (English)

    贾明明; 李旭东; 吕航

    2014-01-01

    腐蚀损伤会加速疲劳载荷下的飞机铝合金结构裂纹的萌生和扩展,威胁结构安全性。针对腐蚀影响下的疲劳裂纹扩展的随机性本质,对预腐蚀 LD10CS 合金的预腐蚀疲劳试验进行了数据分析,提出了基于可靠性的腐蚀裂纹扩展速率表征方法,与试验结果对比表明,该方法可以给出 LD10CS 腐蚀疲劳裂纹扩展速率的上下限,进而给出该种材料铝合金构件的疲劳裂纹扩展寿命的上下限,为评估铝合金构件的寿命提供了依据。%Fatigue loadings and environmental corrosion damage can decrease the mechanical properties of LD10CS alu-minum alloy.The paper made a research on the fatigue crack growth rate (FCG)of AA LD10CS with corrosion damage, and proposed a reliability-based method to evaluate FCG.Compare of predicted FCG and experimental results indicated that the proposed method was able to give the lower and upper limit of FCG of LD10CS with corrosion damage,which provided the basis of aluminum alloy component safe life prediction.

  20. Stress corrosion cracking of several high strength ferrous and nickel alloys

    Science.gov (United States)

    Nelson, E. E.

    1971-01-01

    The stress corrosion cracking resistance of several high strength ferrous and nickel base alloys has been determined in a sodium chloride solution. Results indicate that under these test conditions Multiphase MP35N, Unitemp L605, Inconel 718, Carpenter 20Cb and 20Cb-3 are highly resistant to stress corrosion cracking. AISI 410 and 431 stainless steels, 18 Ni maraging steel (250 grade) and AISI 4130 steel are susceptible to stress corrosion cracking under some conditions.

  1. Threshold Stress Intensity of Hydrogen-Induced Cracking and Stress Corrosion Cracking of High Strength Steel

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    The threshold stress intensity of stress corrosion cracking (SCC) for 40CrMo steel in 3.5 % NaCl solution decreased exponentially with the increase of yield strength. The threshold stress intensity of hydrogen-induced cracking during dynamical charging for 40CrMo steel decreased linearly with the logarithm of the concentration of diffusible hydrogen. This equation was also applicable to SCC of high strength steel in aqueous solution. The critical hydrogen enrichment concentration necessary for SCC of high strength steel in water decreased exponentially with the increase of yield strength. Based on the results, the relationship between KISCC and σys could be deduced.

  2. FEM Modelling of the Evolution of Corrosion Cracks in Reinforced Concrete Structures

    DEFF Research Database (Denmark)

    Thoft-Christensen, Palle

    Corrosion cracks are caused by the increasing volume of corrosion products during the corrosion of the reinforcement. After corrosion initiation the rust products from the corroded reinforcement will initially fill the porous zone near the reinforcement and the result in an expansion of the concr...

  3. Accelerated crack growth, residual stress, and a cracked zinc coated pressure shell

    Science.gov (United States)

    Dittman, Daniel L.; Hampton, Roy W.; Nelson, Howard G.

    1987-01-01

    During a partial inspection of a 42 year old, operating, pressurized wind tunnel at NASA-Ames Research Center, a surface connected defect 114 in. long having an indicated depth of a 0.7 in. was detected. The pressure shell, constructed of a medium carbon steel, contains approximately 10 miles of welds and is cooled by flowing water over its zinc coated external surface. Metallurgical and fractographic analysis showed that the actual detect was 1.7 in. deep, and originated from an area of lack of weld penetration. Crack growth studies were performed on the shell material in the laboratory under various loading rates, hold times, and R-ratios with a simulated shell environment. The combination of zinc, water with electrolyte, and steel formed an electrolytic cell which resulted in an increase in cyclic crack growth rate by as much as 500 times over that observed in air. It was concluded that slow crack growth occurred in the pressure shell by a combination of stress corrosion cracking due to the welding residual stress and corrosion fatigue due to the cyclic operating stress.

  4. Accelerated crack growth, residual stress, and a cracked zinc coated pressure shell

    Science.gov (United States)

    Dittman, Daniel L.; Hampton, Roy W.; Nelson, Howard G.

    1987-01-01

    During a partial inspection of a 42 year old, operating, pressurized wind tunnel at NASA-Ames Research Center, a surface connected defect 114 in. long having an indicated depth of a 0.7 in. was detected. The pressure shell, constructed of a medium carbon steel, contains approximately 10 miles of welds and is cooled by flowing water over its zinc coated external surface. Metallurgical and fractographic analysis showed that the actual detect was 1.7 in. deep, and originated from an area of lack of weld penetration. Crack growth studies were performed on the shell material in the laboratory under various loading rates, hold times, and R-ratios with a simulated shell environment. The combination of zinc, water with electrolyte, and steel formed an electrolytic cell which resulted in an increase in cyclic crack growth rate by as much as 500 times over that observed in air. It was concluded that slow crack growth occurred in the pressure shell by a combination of stress corrosion cracking due to the welding residual stress and corrosion fatigue due to the cyclic operating stress.

  5. In Situ X-ray Microtomography of Stress Corrosion Cracking and Corrosion Fatigue in Aluminum Alloys

    Science.gov (United States)

    Singh, Sudhanshu S.; Stannard, Tyler J.; Xiao, Xianghui; Chawla, Nikhilesh

    2017-08-01

    Structural materials are subjected to combinations of stress and corrosive environments that work synergistically to cause premature failure. Therefore, studies on the combined effect of stress and corrosive environments on material behavior are required. Existing studies have been performed in two dimensions that are inadequate for full comprehension of the three-dimensional (3D) processes related to stress corrosion cracking (SCC) and corrosion-fatigue (CF) behavior. Recently, x-ray synchrotron tomography has evolved as an excellent technique to obtain the microstructure in 3D. Moreover, being nondestructive in nature, x-ray synchrotron tomography is well suited to study the evolution of microstructure with time (4D, or fourth dimension in time). This article presents our recent 4D studies on SCC and CF of Al 7075 alloys using x-ray synchrotron tomography.

  6. A Fracture Probability Competition Mechanism of Stress Corrosion Cracking

    Institute of Scientific and Technical Information of China (English)

    Yanliang HUANG

    2001-01-01

    The stress corrosion cracking (SCC) of austenitic stainless steel was studied via polarization,slow strain rate and scanning electron microscope (SEM) techniques. Many SCC mechanisms have been proposed in which hydrogen embrittlement and passive film rupture-repassivation theories are generally accepted, but they can hardly explain the SCC mechanism of austenitic stainless steel in acidic chloride solution adequately, because the steel is in active dissolution state and cathodic polarization can prevent it from occurring. Our experiment shows that the anodic current increases the creep rate and decreases the plastic strength of the material on single smooth specimen as well as at the SCC crack tip. The fractured surface was characterized as brittle cleavage, while the surface crack of smooth specimen was almost vertical to the tensile strength, which can confirm that the cracks were caused by tensile stresses. A fracture probability competition mechanism of SCC was proposed on the basis of the experimental results combined with the viewpoint of ductile-brittle fracture competition. When the anodic dissolution current is increased to a certain degree, the probability of fracture by tensile stress will exceed that by shear stress, and the brittle fracture will occur. The proposed SCC mechanism can not only explain the propagation of SCC cracks but can explain the crack initiation as well. The strain on the surface distributes unevenly when a smooth specimen is deformed, so does the anodic current distribution. The crack will initiate at a point where the anodic current density is large enough to cause the material at a specific point to fracture in brittle manner.

  7. Report on Status of Shipment of High Fluence Austenitic Steel Samples for Characterization and Stress Corrosion Crack Testing

    Energy Technology Data Exchange (ETDEWEB)

    Clark, Scarlett R. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Leonard, Keith J. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

    2016-09-01

    The goal of the Mechanisms of Irradiation Assisted Stress Corrosion Cracking (IASCC) task in the LWRS Program is to conduct experimental research into understanding how multiple variables influence the crack initiation and crack growth in materials subjected to stress under corrosive conditions. This includes understanding the influences of alloy composition, radiation condition, water chemistry and metallurgical starting condition (i.e., previous cold work or heat treatments and the resulting microstructure) has on the behavior of materials. Testing involves crack initiation and growth testing on irradiated specimens of single-variable alloys in simulated Light Water Reactor (LWR) environments, tensile testing, hardness testing, microstructural and microchemical analysis, and detailed efforts to characterize localized deformation. Combined, these single-variable experiments will provide mechanistic understanding that can be used to identify key operational variables to mitigate or control IASCC, optimize inspection and maintenance schedules to the most susceptible materials/locations, and, in the long-term, design IASCC-resistant materials.

  8. Intergranular stress corrosion cracking of austenitic piping materials in BWR conditions. Research results - Phase 4: Crack growth; Interkristalline Spannungsrisskorrosion austenitischer Rohrleitungswerkstoffe unter SWR-Bedingungen. Ergebnisse der Forschungsvorhaben - Phase 4: Risswachstum

    Energy Technology Data Exchange (ETDEWEB)

    Kilian, R. [Siemens Nuclear Power GmbH, Erlangen (Germany); Bruemmer, G. [Hamburgische Electricitaetswerke AG, Hamburg (Germany); Hoffmann, H. [VGB, Essen (Germany); Ilg, U. [EnBW Kraftwerke AG, Philippsburg (Germany); Maier, V. [Bayernwerk Kernenergie GmbH, Muenchen (Germany); Wachter, O. [E.ON Kernkraft GmbH, Hannover (Germany); Widera, M. [RWE Energie AG, Essen (Germany)

    2001-07-01

    A charge of Ti-stabilised austenitic steel 1.4541 and three charges of Ni-stabilised steel 1.4550 with different carbon concentrations and stabilisation ratios were selected as samples. Water chemical boundary conditions and the material state were varied during the crack growth experiments. Apart from the basic material in the sensitised and solution-annealed state, also HAZ states of specially produced welds were investigated. [German] Als Probenmaterial wurde eine Charge des Titan-stabilisierten austenitischen Stahles W.-Nr. 1.4541 und drei Chargen des Niob-stabilisierten Stahles W.-Nr. 1.4550 mit unterschiedlichen Kohlenstoffgehalten und Stabilisierungsverhaeltnissen ausgewaehlt. Neben wasserchemischen Randbedingungen wurde bei den Risswachstumsversuche vor allem der Parameter Werkstoffzustand variiert. Neben dem Grundwerkstoff im sensibilisierten und loesungsgegluehten Zustand - wurden auch Waermeeinflusszonen-Zustaende von speziell hierfuer hergestellten Schweissnaehten geprueft. (orig.)

  9. Penetration of corrosion products and corrosion-induced cracking in reinforced cementitious materials

    DEFF Research Database (Denmark)

    Michel, Alexander; Pease, Brad J.; Peterova, Adela;

    2014-01-01

    This paper describes experimental investigations on corrosion-induced deterioration in reinforced cementitious materials and the subsequent development and implementation of a novel conceptual model. Rejnforced mortar specimens of varying water-to-cement ratios were subjected to current-induced c......This paper describes experimental investigations on corrosion-induced deterioration in reinforced cementitious materials and the subsequent development and implementation of a novel conceptual model. Rejnforced mortar specimens of varying water-to-cement ratios were subjected to current......-induced corrosion (10, 50, and 100 mu A/cm(2)). X-ray attenuation measurements and visual investigations provided both qualitative and quantitative information on the penetration of solid corrosion products into the surrounding cementitious matrix. X-ray attenuation measurements provided time- and location......-dependent concentrations of corrosion products averaged through the specimen thickness. Digital image correlation (DIC) was used to measure corrosion-induced deformations including deformations between steel and cementitious matrix as well as formation and propagation of corrosion-induced cracks. Based on experimental...

  10. 当量加速腐蚀条件下7 B04-T6高强度铝合金疲劳裂纹扩展规律研究%The fatigue crack growth rule of 7B04-T6 high strength aluminum alloy under equivalently accelerated corrosion environment

    Institute of Scientific and Technical Information of China (English)

    谭晓明; 王海东; 王刚

    2015-01-01

    Based on an accelerated corrosion testing spectrum complicated for the servicing field environment, the equivalently accelerated corrosion testing of high strength aluminum alloy 7B04-T6 specimens for critical structure were carried out. Corrosion damage under the field environment was successfully simulated and reappeared, and corrosion damage evolvement rule was obtained. By prior⁃corrosion fatigue testing and fractography quantitative analysis, the fatigue crack length (a) and fatigue cycles (N) were gotten, and relationship between fatigue crack growth rate (da/dN) and stress intensify factors rang (ΔK) was analyzed. Moreover the effect of different corrosion damage on fatigue crack growth behavior was quantitatively characterized. The result shows that there is obvious short crack growth behavior during early corrosion stage, the fatigue crack growth rate increases when the corrosion damage is more serious, and the fatigue performance is greatly degraded.%基于编制的机场环境加速试验谱,针对关键结构高强度铝合金件进行当量腐蚀试验,在实验室条件下成功地模拟和再现了服役环境条件的腐蚀损伤,借助复型法观测得到了腐蚀损伤的演化规律;通过预腐蚀疲劳试验和疲劳断口扫描电镜定量分析,得到了裂纹长度a与循环次数N数据集,分析了裂纹扩展速率da/dN与应力强度因子幅值ΔK的对应关系,定量表征了不同程度腐蚀损伤对疲劳裂纹扩展行为的影响规律。结果表明,在腐蚀初期,疲劳裂纹扩展过程中有经典的小裂纹扩展阶段;随着腐蚀损伤的加重,小裂纹行为不明显;腐蚀损伤越严重,疲劳裂纹扩展速率越快,结构抗疲劳性能显著退化。

  11. Environmentally assisted crack growth rates of high-strength aluminum alloys

    Science.gov (United States)

    Connolly, Brain J.; Deffenbaugh, Kristen L.; Moran, Angela L.; Koul, Michelle G.

    2003-01-01

    The scope of this project is to evaluate the environmentally assisted long crack growth behavior of candidate high-strength aluminum alloys/tempers, specifically AA7150-T7751 and AA7040-T7651, for consideration as viable replacements/refurbishment for stress-corrosion cracking in susceptible AA7075-T6 aircraft components found in aging aircraft systems.

  12. EXPERT PANEL OVERSIGHT COMMITTEE ASSESSMENT OF FY2008 CORROSION AND STRESS CORROSION CRACKING SIMULANT TESTING PROGRAM

    Energy Technology Data Exchange (ETDEWEB)

    BOOMER KD

    2009-01-08

    The Expert Panel Oversight Committee (EPOC) has been overseeing the implementation of selected parts of Recommendation III of the final report, Expert Panel workshop for Hanford Site Double-Shell Tank Waste Chemistry Optimization, RPP-RPT-22126. Recommendation III provided four specific requirements necessary for Panel approval of a proposal to revise the chemistry control limits for the Double-Shell Tanks (DSTs). One of the more significant requirements was successful performance of an accelerated stress corrosion cracking (SCC) experimental program. This testing program has evaluated the optimization of the chemistry controls to prevent corrosion in the interstitial liquid and supernatant regions of the DSTs.

  13. Hierarchical petascale simulation framework for stress corrosion cracking

    Science.gov (United States)

    Vashishta, P.; Kalia, R. K.; Nakano, A.; Kaxiras, E.; Grama, A.; Lu, G.; Eidenbenz, S.; Voter, A. F.; Hood, R. Q.; Moriarty, J. A.; Yang, L. H.

    2008-07-01

    We are developing a scalable parallel and distributed computational framework consisting of methods, algorithms, and integrated software tools for multi-terascle-to-petascale simulations of stress corrosion cracking (SCC) with quantum-level accuracy. We have performed multimillion- to billion-atom molecular dynamics (MD) simulations of deformation, flow, and fracture in amorphous silica with interatomic potentials and forces validated by density functional theory (DFT) calculations. Optimized potentials have been developed to study sulfur embrittlement of nickel with multimillion-to-multibillion atom MD simulations based on DFT and temperature dependent model generalized pseudopotential theory. We have also developed a quasi-continuum method embedded with quantum simulations based on DFT to reach macroscopic length scales and an accelerated molecular dynamics scheme to reach macroscopic time scales in simulations of solid-fluid interfaces that are relevant to SCC. A hybrid MD and mesoscale lattice Boltzmann simulation algorithm is being designed to study fluid flow through cracks.

  14. Fatigue crack growth detect, assess, avoid

    CERN Document Server

    Richard, Hans Albert

    2016-01-01

    This book offers a concise introduction to fatigue crack growth, based on practical examples. It discusses the essential concepts of fracture mechanics, fatigue crack growth under constant and variable amplitude loading and the determination of the fracture-mechanical material parameters. The book also introduces the analytical and numerical simulation of fatigue crack growth as well as crack initiation. It concludes with a detailed description of several practical case studies and some exercises. The target group includes graduate students, researchers at universities and practicing engineers.

  15. Chemical and metallurgical aspects of environmentally assisted fatigue crack growth in 7075-T651 aluminum alloy

    Science.gov (United States)

    Gao, Ming; Wei, R. P.; Pao, P. S.

    1988-07-01

    A comprehensive study has been carried out on a 7075-T651 alloy to examine the influence of water vapor on fatigue crack growth. The kinetics of fatigue crack growth were determined as a function of water vapor pressure at room temperature and at 353 K. Detailed fractographic analyses and surface chemistry studies were carried out to identify the micromechanisms and to quantify the chemical interactions for corrosion fatigue crack growth in this alloy. Experiments were also carried out in ultra-high vacuum and in oxygen to provide for comparisons. Two regions of fatigue crack growth response were identified. In the low pressure region (below 67 Pa at 5 Hz), crack growth is controlled by the rate of transport of water vapor to the crack tip, and the response can be described by a model for transport controlled crack growth. At pressures above 67 Pa, additional increases in crack growth rate occurred, which are attributed to the further reactions of water vapor with segregated magnesium in this alloy. Different micromechanisms for crack growth have been identified for vacuum, oxygen, and water vapor. These micromechanisms are considered in relation to the environmental parameters through a modified superposition model for corrosion fatigue.

  16. Elasto-Plasticity Critical Corrosive Ratio Model for RC Structure Corrosive Expanding Crack

    Institute of Scientific and Technical Information of China (English)

    CHEN Yueshun; LU Yiyan; LIU Li

    2007-01-01

    The parameter of filling expanding ratio n, plasticity factor k1 and deformation parameter k2 is raised, and then the elasto-plasticity critical corrosive ratio model for RC structure corrosive expanding crack based on elasto-plasticity theory is constructed in this paper. The influences of parameters such as filling expansion ratio n, plasticity factor k1, deformation parameter k2, Poisson ratio of concrete v, diameter of reinforced bar d and protective layer thickness c on the critical corrosive ratio are researched by theory analysis and experiments. The experimental results validate the accuracy of the model. According to the experimental study, the least squares solution is calculated as n=1.8,k1 =0.61,k2 =0.5.

  17. Cracks propagation by stress corrosion cracking in conditions of Boiling Water Reactor (BWR); Propagacion de grietas por corrosion bajo esfuerzo en condiciones de reactor de agua hirviente (BWR)

    Energy Technology Data Exchange (ETDEWEB)

    Fuentes C, P

    2003-07-01

    This work presents the results of the assays carried out in the Laboratory of Hot Cells of the National Institute of Nuclear Research (ININ) to a type test tube Compact Tension (CT), built in steel austenitic stainless type 304L, simulating those conditions those that it operates a Boiling Water Reactor (BWR), at temperature 288 C and pressure of 8 MPa, to determine the speed to which the cracks spread in this material that is of the one that different components of a reactor are made, among those that it highlights the reactor core vessel. The application of the Hydrogen Chemistry of the Water is presented (HWC) that is one alternative to diminish the corrosion effect low stress in the component, this is gets controlling the quantity of oxygen and of hydrogen as well as the conductivity of the water. The rehearsal is made following the principles of the Mechanics of Elastic Lineal Fracture (LEFM) that considers a crack of defined size with little plastic deformation in the tip of this; the measurement of crack advance is continued with the technique of potential drop of direct current of alternating signal, this is contained inside the standard Astm E-647 (Method of Test Standard for the Measurement of Speed of Growth of Crack by fatigue) that is the one that indicates us as carrying out this test. The specifications that should complete the test tubes that are rehearsed as for their dimensions, it forms, finish and determination of mechanical properties (tenacity to the fracture mainly) they are contained inside the norm Astm E-399, the one which it is also based on the principles of the fracture mechanics. The obtained results were part of a database to be compared with those of other rehearsals under different conditions, Normal Chemistry of the Water (NWC) and it dilutes with high content of O{sub 2}; to determine the conditions that slow more the phenomena of stress corrosion cracking, as well as the effectiveness of the used chemistry and of the method of

  18. Research on mechanisms of stress corrosion cracking in Zircaloy

    Energy Technology Data Exchange (ETDEWEB)

    Knorr, D.B.; Pelloux, R.M.

    1981-06-01

    The results of internal gas pressurization tests, primarily at 320/sup 0/C, on cladding tubes from two suppliers, Supplier A and Supplier B, are presented. The two lots show a substantial difference in iodine SCC susceptibility so a test matrix is used to resolve the relative contributions of surface condition, residual stress, and texture. Additional tests with constant deflection split-ring specimens and with unstressed cladding segments are used to understand crack initiation and the early crack growth stages of SCC. The difference in SCC susceptibility is due to crystallographic texture. Other variables such as surface finish, stress relief temperature, and residual stress have little or no effect. Mechanical properties, crack initiation, and crack propagation all depend on texture. Both initiation and propagation features are analyzed by scanning electron microscopy. A mechanism for crack initiation consistent with most observations in this study and with the work of other investigators is proposed. At 320/sup 0/C, lifetime is crack initiation limited while several tests at 390/sup 0/C indicate that lifetime is less initiation limited at higher temperature. 31 figures, 9 tables.

  19. Uncertainty Quantification in Fatigue Crack Growth Prognosis

    Directory of Open Access Journals (Sweden)

    Shankar Sankararaman

    2011-01-01

    Full Text Available This paper presents a methodology to quantify the uncertainty in fatigue crack growth prognosis, applied to structures with complicated geometry and subjected to variable amplitude multi-axial loading. Finite element analysis is used to address the complicated geometry and calculate the stress intensity factors. Multi-modal stress intensity factors due to multi-axial loading are combined to calculate an equivalent stress intensity factor using a characteristic plane approach. Crack growth under variable amplitude loading is modeled using a modified Paris law that includes retardation effects. During cycle-by-cycle integration of the crack growth law, a Gaussian process surrogate model is used to replace the expensive finite element analysis. The effect of different types of uncertainty – physical variability, data uncertainty and modeling errors – on crack growth prediction is investigated. The various sources of uncertainty include, but not limited to, variability in loading conditions, material parameters, experimental data, model uncertainty, etc. Three different types of modeling errors – crack growth model error, discretization error and surrogate model error – are included in analysis. The different types of uncertainty are incorporated into the crack growth prediction methodology to predict the probability distribution of crack size as a function of number of load cycles. The proposed method is illustrated using an application problem, surface cracking in a cylindrical structure.

  20. Characterization of Cracking and Crack Growth Properties of the C5A Aircraft Tie-Box Forging

    Science.gov (United States)

    Piascik, Robert S.; Smith, Stephen W.; Newman, John A.; Willard, Scott A.

    2003-01-01

    Detailed destructive examinations were conducted to characterize the integrity and material properties of two aluminum alloy (7075-T6) horizontal stabilizer tie box forgings removed.from US. Air Force C5A and C5B transport aircraft. The C5B tie box forging was,found to contain no evidence of cracking. Thirteen cracks were found in the CSA,forging. All but one of the cracks observed in the C5A component were located along the top cap region (one crack was located in the bottom cap region). The cracks in the C5A component initiated at fastener holes and propagated along a highly tunneled intergranular crack path. The tunneled crack growth configuration is a likelv result of surface compressive stress produced during peening of the .forging suijace. The tie box forging ,fatigue crack growth, fracture and stress corrosion cracking (SCC) properties were characterized. Reported herein are the results of laboratory air ,fatigue crack growth tests and 95% relative humidity SCC tests conducted using specimens machined from the C5A ,forging. SCC test results revealed that the C5A ,forging material was susceptible to intergranular environmental assisted cracking: the C5A forging material exhibited a SCC crack-tip stress-intensity factor threshold of less than 6 MPadn. Fracture toughness tests revealed that the C5A forging material exhibited a fracture toughness that was 25% less than the C5B forging. The C5A forging exhibited rapid laboratory air fatigue crack growth rates having a threshold crack-tip stress-intensity factor range of less than 0.8 MPa sup m. Detailed fractographic examinations revealed that the ,fatigue crack intergranular growth crack path was similar to the cracking observed in the C5A tie box forging. Because both fatigue crack propagation and SCC exhibit similar intergranular crack path behavior, the damage mechanism resulting in multi-site cracking of tie box forgings cannot be determined unless local cyclic stresses can be quantified.

  1. Computer Simulation of Intergranular Stress Corrosion Cracking via Hydrogen Embrittlement

    Energy Technology Data Exchange (ETDEWEB)

    Smith, R.W.

    2000-04-01

    Computer simulation has been applied to the investigation of intergranular stress corrosion cracking in Ni-based alloys based on a hydrogen embrittlement mechanism. The simulation employs computational modules that address (a) transport and reactions of aqueous species giving rise to hydrogen generation at the liquid-metal interface, (b) solid state transport of hydrogen via intergranular and transgranular diffusion pathways, and (c) fracture due to the embrittlement of metallic bonds by hydrogen. A key focus of the computational model development has been the role of materials microstructure (precipitate particles and grain boundaries) on hydrogen transport and embrittlement. Simulation results reveal that intergranular fracture is enhanced as grain boundaries are weakened and that microstructures with grains elongated perpendicular to the stress axis are more susceptible to cracking. The presence of intergranular precipitates may be expected to either enhance or impede cracking depending on the relative distribution of hydrogen between the grain boundaries and the precipitate-matrix interfaces. Calculations of hydrogen outgassing and in gassing demonstrate a strong effect of charging method on the fracture behavior.

  2. Stress corrosion cracking in canistered waste package containers: Welds and base metals

    Energy Technology Data Exchange (ETDEWEB)

    Huang, J.S.

    1998-03-01

    The current design of waste package containers include outer barrier using corrosion allowable material (CAM) such as A516 carbon steel and inner barrier of corrosion resistant material (CRM) such as alloy 625 and C22. There is concern whether stress corrosion cracking would occur at welds or base metals. The current memo documents the results of our analysis on this topic.

  3. Sensitization, intergranular attack, stress corrosion cracking, and irradiation effects on the corrosion of iron--chromium--nickel alloys

    Energy Technology Data Exchange (ETDEWEB)

    Wu, P.C.S.

    1978-04-01

    A literature review is presented on the sensitization, intergranular attack, and stress corrosion cracking of austenitic stainless steels with emphasis on dilute solutions at temperatures below the boiling point of water. An attempt is made to list the possible sources of contaminants during manufacture, shipping, construction and all phases of operation of the sodium containing components. The susceptibility of the different materials to stress corrosion cracking in the various contaminants is discussed and suggestions to prevent serious problems are made. (GHT)

  4. Relativity between corrosion-induced stress and stress corrosion cracking of brass in an ammonia solution

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    The susceptibility to stress corrosion cracking (SCC) of brass in an ammonia solution with various pH values or under various applied potentials was measured at slow strain rate tests. The additive stress in the same solution was measured using two methods. The results indicate that the variation of the susceptibility to SCC with pH value or with potential is in an excellent agreement with the corrosion (passive film or dezincification layer)-induced stress. When pH ? 7, the corrosion-induced tensile stress and the susceptibility to SCC have maximum values and hardly change with increasing the pH value. However, when pH < 7, both the corrosion-induced tensile stress and the susceptibility to SCC reduce rapidly with decreasing the pH value. Both the corrosion-induced tensile stress and the susceptibility to SCC have maximum values at the open-circuit potential, decrease slightly under the anodic polarization, and reduce gradually to zero under the cathodic polarization.

  5. Stress corrosion cracking for 316 stainless steel clips in a condensate stabilizer

    Energy Technology Data Exchange (ETDEWEB)

    Al-Awar, A.; Aldajah, S.; Harhara, A. [Department of Mechanical Engineering, United Arab Emirates University, P. O. Box 17555 Al-AIn 17555 (United Arab Emirates)

    2011-09-15

    In one of the gas processing facilities in Abu Dhabi, UAE; a case of 316L stainless steel material failure occurred in the fractionating column due to stress cracking corrosion twice in a cycle of less than 2 years. This paper studies the stress corrosion cracking behavior of the 316L stainless steel in an accelerated corrosion environment and compares it with a higher corrosion resistant nickel alloy (Inconel 625). The experimental work was designed according to ASTM G36 standard, the samples were immersed in a boiling magnesium chloride medium which provided the accelerated corrosion environment and the tested samples were shaped into U-bend specimens as they underwent both plastic and elastic stresses. The specimens were then tested to determine the time required for cracks to initiate. The results of the experimental work showed that the main mode of failure was stress corrosion cracking initiated by the proven presence of chlorides, hydrogen sulfide, and water at elevated temperatures. Inconel 625 samples placed in the controlled environment showed better corrosion resistance as it took them an average of 56 days to initiate cracks, whereas it took an average of 24 days to initiate cracks in the stainless steel 316L samples. The scanning electron microscopy (SEM) micrographs showed that the cracks in the stainless steel 316L samples were longer, wider, and deeper compared to the cracks of Inconel 625. (Copyright copyright 2011 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

  6. The effects of cold rolling orientation and water chemistry on stress corrosion cracking behavior of 316L stainless steel in simulated PWR water environments

    Science.gov (United States)

    Chen, Junjie; Lu, Zhanpeng; Xiao, Qian; Ru, Xiangkun; Han, Guangdong; Chen, Zhen; Zhou, Bangxin; Shoji, Tetsuo

    2016-04-01

    Stress corrosion cracking behaviors of one-directionally cold rolled 316L stainless steel specimens in T-L and L-T orientations were investigated in hydrogenated and deaerated PWR primary water environments at 310 °C. Transgranular cracking was observed during the in situ pre-cracking procedure and the crack growth rate was almost not affected by the specimen orientation. Locally intergranular stress corrosion cracks were found on the fracture surfaces of specimens in the hydrogenated PWR water. Extensive intergranular stress corrosion cracks were found on the fracture surfaces of specimens in deaerated PWR water. More extensive cracks were found in specimen T-L orientation with a higher crack growth rate than that in the specimen L-T orientation with a lower crack growth rate. Crack branching phenomenon found in specimen L-T orientation in deaerated PWR water was synergistically affected by the applied stress direction as well as the preferential oxidation path along the elongated grain boundaries, and the latter was dominant.

  7. Dissolution Condensation Mechanism of Stress Corrosion Cracking in Liquid Metals: Driving Force and Crack Kinetics

    Science.gov (United States)

    Glickman, Evgeny E.

    2011-02-01

    Stress corrosion cracking (SCC) in aqueous solution is driven by exothermic reactions of metal oxidation. This stimulus, as well as classical mechanisms of SCC, does not apply to SCC in liquid metals (LMs). In the framework of the dissolution-condensation mechanism (DCM), we analyzed the driving force and crack kinetics for this nonelectrochemical mode of SCC that is loosely called "liquid metal embrittlement" (LME). According to DCM, a stress-induced increase in chemical potential at the crack tip acts as the driving force for out-of-the-tip diffusion mass transfer that is fast because diffusion in LMs is very fast and surface energy at the solid-liquid interface is small. In this article, we review two versions of DCM mechanism, discuss the major physics behind them, and develop DCM further. The refined mechanism is applied then to the experimental data on crack velocity V vs stress intensity factor, the activation energy of LME, and alloying effects. It is concluded that DCM provides a good conceptual framework for analysis of a unified kinetic mechanism of LME and may also contribute to SCC in aqueous solutions.

  8. Ultrasonic inspection reliability for intergranular stress corrosion cracks

    Energy Technology Data Exchange (ETDEWEB)

    Heasler, P G; Taylor, T T; Spanner, J C; Doctor, S R; Deffenbaugh, J D [Pacific Northwest Lab., Richland, WA (USA)

    1990-07-01

    A pipe inspection round robin entitled Mini-Round Robin'' was conducted at Pacific Northwest Laboratory from May 1985 through October 1985. The research was sponsored by the US Nuclear Regulatory Commission, Office of Nuclear Regulatory Research under a program entitled Evaluation and Improvement of NDE Reliability for Inservice Inspection of Light Water Reactors.'' The Mini-Round Robin (MRR) measured the intergranular stress corrosion (GSC) crack detection and sizing capabilities of inservice inspection (ISI) inspectors that had passed the requirements of IEB 83-02 and the Electric Power Research Institute (EPRI) sizing training course. The MRR data base was compared with an earlier Pipe Inspection Round Robin (PIRR) that had measured the performance of inservice inspection prior to 1982. Comparison of the MRR and PIRR data bases indicates no significant change in the inspection capability for detecting IGSCC. Also, when comparing detection of long and short cracks, no difference in detection capability was measured. An improvement in the ability to differentiate between shallow and deeper IGSCC was found when the MRR sizing capability was compared with an earlier sizing round robin conducted by the EPRI. In addition to the pipe inspection round robin, a human factors study was conducted in conjunction with the Mini-Round Robin. The most important result of the human factors study is that the Relative Operating Characteristics (ROC) curves provide a better methodology for describing inspector performance than only probability of detection (POD) or single-point crack/no crack data. 6 refs., 55 figs., 18 tabs.

  9. Subcritical crack growth in two titanium alloys.

    Science.gov (United States)

    Williams, D. N.

    1973-01-01

    Measurement of subcritical crack growth during static loading of precracked titanium alloys in salt water using samples too thin for plane strain loading to predominate was examined as a method for determining the critical stress intensity for crack propagation in salt water. Significant internal crack growth followed by arrest was found at quite low stress intensities, but crack growth rates were relatively low. Assuming these techniques provided a reliable measurement of the critical stress intensity, the value for annealed Ti-4Al-1.5Mo-0.5V alloy was apparently about 35 ksi-in. to the 1/2 power, while that for annealed Ti-4Al-3Mo-1V was below 45 ksi-in. to the 1/2 power. Crack growth was also observed in tests conducted in both alloys in an air environment. At 65 ksi-in. to the 1/2 power, the extent of crack growth was greater in air than in salt water. Ti-4Al-3Mo-1V showed arrested crack growth in air at a stress intensity of 45 ksi-in. to the 1/2 power.

  10. Effect of layerwise structural inhomogeneity on stress- corrosion cracking of steel tubes

    Science.gov (United States)

    Perlovich, Yu A.; Krymskaya, O. A.; Isaenkova, M. G.; Morozov, N. S.; Fesenko, V. A.; Ryakhovskikh, I. V.; Esiev, T. S.

    2016-04-01

    Based on X-ray texture and structure analysis data of the material of main gas pipelines it was shown that the layerwise inhomogeneity of tubes is formed during their manufacturing. The degree of this inhomogeneity affects on the tendency of tubes to stress- corrosion cracking under exploitation. Samples of tubes were cut out from gas pipelines located under various operating conditions. Herewith the study was conducted both for sections with detected stress-corrosion defects and without them. Distributions along tube wall thickness for lattice parameters and half-width of X-ray lines were constructed. Crystallographic texture analysis of external and internal tube layers was also carried out. Obtained data testifies about considerable layerwise inhomogeneity of all samples. Despite the different nature of the texture inhomogeneity of gas pipeline tubes, the more inhomogeneous distribution of texture or structure features causes the increasing of resistance to stress- corrosion. The observed effect can be explained by saturation with interstitial impurities of the surface layer of the hot-rolled sheet and obtained therefrom tube. This results in rising of lattice parameters in the external layer of tube as compared to those in underlying metal. Thus, internal layers have a compressive effect on external layers in the rolling plane that prevents cracks opening at the tube surface. Moreover, the high mutual misorientation of grains within external and internal layers of tube results in the necessity to change the moving crack plane, so that the crack growth can be inhibited when reaching the layer with a modified texture.

  11. A non-destructive test method to monitor corrosion products and corrosion-induced cracking in reinforced cement based materials

    DEFF Research Database (Denmark)

    Michel, Alexander; Pease, Bradley Justin; Peterova, Adela

    2011-01-01

    This paper introduces a non-destructive test method to monitor the development of corrosion products as well as the corrosion-induced formation and propagation of cracks in cementitious materials. A parametric experimental investigation (utilizing x-ray attenuation measurement technique...

  12. Monitoring reinforcement corrosion and corrosion-induced cracking using non-destructive x-ray attenuation measurements

    DEFF Research Database (Denmark)

    Michel, Alexander; Pease, Bradley Justin; Geiker, Mette Rica

    2011-01-01

    To test the applicability of the x-ray attenuation method to monitor the movement of corrosion products as well as the formation and propagation of cracks in cementitious materials reinforced mortar samples were prepared and tested under accelerated corrosion conditions. It is evident from...

  13. Strain-induced corrosion cracking in ferritic components of BWR primary circuits; Risskorrosion in druckfuehrenden ferritischen Komponenten des Primaerkreislaufes von Siedewasserreaktoren

    Energy Technology Data Exchange (ETDEWEB)

    Seifert, H.-P.; Ritter, S.; Ineichen, U.; Tschanz, U.; Gerodetti, B

    2003-04-01

    The present final report of the RIKORR project is a summary of a literature survey and of the experimental work performed by PSI on the environmentally-assisted cracking (EAC) and dynamic strain ageing (DSA) susceptibility of low-alloy steels (LAS) in high-temperature (HT) water. Within this project, the EAC crack growth behaviour of different low-alloy RPV steels, weld filler and weld heat-affected zone materials has been investigated under simulated transient and steady-state BWR/NWC power operation conditions. The strain-induced corrosion cracking (SICC) / low-frequency corrosion fatigue (CF) and stress corrosion cracking (SCC) crack growth behaviour of different low-alloy RPV steels under simulated transient and stationary BWR/NWC conditions was characterized by slow rising load / low-frequency corrosion fatigue and constant load / periodical partial unloading / ripple load tests with pre-cracked fracture mechanics specimens in oxygenated HT water at temperatures of either 288, 250, 200 or 150 {sup o}C. Modern high-temperature water loops, on-line crack growth monitoring and fractographic analysis by scanning electron microscopy (SEM) were used to quantify the cracking response. (author)

  14. Factors affecting stress assisted corrosion cracking of carbon steel under industrial boiler conditions

    Science.gov (United States)

    Yang, Dong

    Failure of carbon steel boiler tubes from waterside has been reported in the utility boilers and industrial boilers for a long time. In industrial boilers, most waterside tube cracks are found near heavy attachment welds on the outer surface and are typically blunt, with multiple bulbous features indicating a discontinuous growth. These types of tube failures are typically referred to as stress assisted corrosion (SAC). For recovery boilers in the pulp and paper industry, these failures are particularly important as any water leak inside the furnace can potentially lead to smelt-water explosion. Metal properties, environmental variables, and stress conditions are the major factors influencing SAC crack initation and propagation in carbon steel boiler tubes. Slow strain rate tests (SSRT) were conducted under boiler water conditions to study the effect of temperature, oxygen level, and stress conditions on crack initation and propagation on SA-210 carbon steel samples machined out of boiler tubes. Heat treatments were also performed to develop various grain size and carbon content on carbon steel samples, and SSRTs were conducted on these samples to examine the effect of microstructure features on SAC cracking. Mechanisms of SAC crack initation and propagation were proposed and validated based on interrupted slow strain tests (ISSRT). Water chemistry guidelines are provided to prevent SAC and fracture mechanics model is developed to predict SAC failure on industrial boiler tubes.

  15. Statistical model of stress corrosion cracking based on extended form of Dirichlet energy: Part 2

    Indian Academy of Sciences (India)

    HARRY YOSH

    2016-10-01

    In the previous paper ({\\it Pramana – J. Phys.} 81(6), 1009 (2013)), the mechanism of stress corrosion cracking (SCC) based on non-quadratic form of Dirichlet energy was proposed and its statistical features were discussed. Following those results, we discuss here how SCC propagates on pipe wall statistically. It reveals that SCC growth distribution is described with Cauchy problem of time-dependent first-order partial differential equation characterized by the convolution of the initial distribution of SCC over time. We also discuss the extension of the above results to the SCC in two-dimensional space and its statistical features with a simple example.

  16. Crack growth behavior of warm-rolled 316L austenitic stainless steel in high-temperature hydrogenated water

    Science.gov (United States)

    Choi, Kyoung Joon; Yoo, Seung Chang; Jin, Hyung-Ha; Kwon, Junhyun; Choi, Min-Jae; Hwang, Seong Sik; Kim, Ji Hyun

    2016-08-01

    To investigate the effects of warm rolling on the crack growth of 316L austenitic stainless steel, the crack growth rate was measured and the oxide structure was characterized in high-temperature hydrogenated water. The warm-rolled specimens showed a higher crack growth rate compared to the as-received specimens because the slip bands and dislocations produced during warm rolling served as paths for corrosion and cracking. The crack growth rate increased with the dissolved hydrogen concentration. This may be attributed to the decrease in performance and stability of the protective oxide layer formed on the surface of stainless steel in high-temperature water.

  17. Behavior of Stress Corrosion Cracking in a Magnesium Alloy

    Institute of Scientific and Technical Information of China (English)

    SONG Renguo; YANG Fanger; BLAWERT Carsten; DIETZEL Wolfgang

    2009-01-01

    Slow strain rate testing (SSRT) was employed to study the stress corrosion cracking (SCC) behavior of ZE41 magnesium alloy in 0.01 M NaCl solution. Smooth tensile specimens with different thicknesses were strained dynamically in both longitudinal and transverse direction under permanent immersions at a strain rate of 10-6 s-1. It is found that ZE41 magnesium alloy is susceptible to SCC in 0.01 M NaCl solution. The SCC susceptibility of the thinner specimen is lower than that of the thicker specimen. Also, the longitudinal specimens are slightly more susceptible to SCC than the transverse specimens. The SCC mechanism of magnesium alloy is attributed to the combination of anodic dissolution with hydrogen embrittlement.

  18. Quantitative characterization of initiation and propagation in stress corrosion cracking. An approach of a phenomenological model; Caracterisation quantitative de l`amorcage et de la propagation en corrosion sous contrainte. Approche d`une modelisation phenomenologique

    Energy Technology Data Exchange (ETDEWEB)

    Raquet, O.

    1994-11-25

    A purely phenomenological study of stress corrosion cracking was performed using the couple Z2CN 18.10 (304L) austenitic stainless steel/boiling MgCl{sub 2} aqueous solution. The exploitation of the morphological information (shape of the cracks and size distribution) available after constant elongation rate tests led to the proposal of an analytical expression of the crack initiation and growth rates. This representation allowed to quantitatively characterize the influence of the applied strain rate as well as the effect of corrosion inhibitors on the crack initiation and propagation phases. It can be used in the search for the stress corrosion cracking mechanisms as a `riddle` for the determination of the rate controlling steps. As a matter of fact, no mechanistic hypothesis has been used for its development. (author).

  19. Effect of cold work and processing orientation on stress corrosion cracking behavior of alloy 600

    Energy Technology Data Exchange (ETDEWEB)

    Moshier, W.C.; Brown, C.M.

    2000-03-01

    Cold work accelerates stress corrosion cracking (SCC) growth rates in Alloy 600 (UNS N06600). However, the variation in crack growth rates generated from cold-worked material has been significant, and the effect has been difficult to quantify. A study was performed in hydrogenated water adjusted to pH 10.2 to evaluate systematically the effect of cold work on Alloy 600 as a function of temperature, amount of cold work, stress intensity factor, and processing orientation. Cold work was introduced into the material by tensile prestraining or cold-rolling plate product. Crack growth rates were determined between 252 C and 360 C, stress intensity factors between 21 MPa{radical}m and 55 MPa{radical}m, and yield strengths between 201 MPa and 827 MPa. The material with the highest yield strength was cold-rolled and tested in the longitudinal-transverse (LT) and short-transverse (ST) orientations. Crack growth rates increased with increasing temperature, stress intensity factor, and yield strength. Furthermore, crack growth rates were a strong function of the processing orientation in the cold-rolled plate, with growth rates approximately an order of magnitude greater in the ST orientation compared to the LT orientation. Crack growth rates in the LT orientation were measured between 0.003 x 10{sup {minus}9} m/s and 1.95 x 10{sup {minus}9} m/s and between 0.066 x 10{sup {minus}9} m/s and 6.3 x 10{sup {minus}9} m/s in the ST orientation. Activation energies were slightly greater in the ST orientation, ranging from 154 kcal/mol to 191 kcal/mol, compared to activation energies between 126 kJ/mol and 157 kJ/mol in the LT orientation. Results of this study demonstrated that, although cold work can be used to accelerate SCC, the orientation of crack growth significantly can affect the results and must be taken into account when analyzing data from cold-worked material.

  20. Corrosion and stress corrosion cracking of ferritic/martensitic steel in super critical pressurized water

    Energy Technology Data Exchange (ETDEWEB)

    Hirose, T. [Naka Fusion Research Institute, JAEA, 801-1 Mukouyama, Naka, Ibaraki 311-0193 (Japan)]. E-mail: hirose.takanori@jaea.go.jp; Shiba, K. [Naka Fusion Research Institute, JAEA, 801-1 Mukouyama, Naka, Ibaraki 311-0193 (Japan); Enoeda, M. [Naka Fusion Research Institute, JAEA, 801-1 Mukouyama, Naka, Ibaraki 311-0193 (Japan); Akiba, M. [Naka Fusion Research Institute, JAEA, 801-1 Mukouyama, Naka, Ibaraki 311-0193 (Japan)

    2007-08-01

    A water-cooled solid breeder (WCSB) blanket cooled by high temperature SCPW (super critical pressurized water) is a practical option of DEMO reactor. Therefore, it is necessary to check the compatibility of the steel with SCPW. In this work, reduced activation ferritic/martensitic steel, F82H has been tested through slow strain rate tests (SSRT) in 23.5 MPa SCPW. And weight change behavior was measured up to 1000 h. F82H did not demonstrated stress corrosion cracking and its weight simply increased with surface oxidation. The weight change of F82H was almost same as commercial 9%-Cr steels. According to a cross-sectional analysis and weight change behavior, corrosion rate of F82H in the 823 K SCPW is estimated to be 0.04 mm/yr.

  1. Slow crack growth in spinel in water

    Science.gov (United States)

    Schwantes, S.; Elber, W.

    1983-01-01

    Magnesium aluminate spinel was tested in a water environment at room temperature to establish its slow crack-growth behavior. Ring specimens with artificial flaws on the outside surface were loaded hydraulically on the inside surface. The time to failure was measured. Various precracking techniques were evaluated and multiple precracks were used to minimize the scatter in the static fatigue tests. Statistical analysis techniques were developed to determine the strength and crack velocities for a single flaw. Slow crack-growth rupture was observed at stress intensities as low as 70 percent of K sub c. A strengthening effect was observed in specimens that had survived long-time static fatigue tests.

  2. Review of environmental effects on fatigue crack growth of austenitic stainless steels

    Energy Technology Data Exchange (ETDEWEB)

    Shack, W.J.; Kassner, T.F. [Argonne National Lab., IL (United States)

    1994-05-01

    Fatigue and environmentally assisted cracking of piping, pressure vessel cladding, and core components in light water reactors are potential concerns to the nuclear industry and regulatory agencies. The degradation processes include intergranular stress corrosion cracking of austenitic stainless steel (SS) piping in boiling water reactors (BWRs), and propagation of fatigue or stress corrosion cracks (which initiate in sensitized SS cladding) into low-alloy ferritic steels in BWR pressure vessels. Crack growth data for wrought and cast austenitic SSs in simulated BWR water, developed at Argonne National Laboratory under US Nuclear Regulatory Commission sponsorship over the past 10 years, have been compiled into a data base along with similar data obtained from the open literature. The data were analyzed to develop corrosion-fatigue curves for austenitic SSs in aqueous environments corresponding to normal BWR water chemistries, for BWRs that add hydrogen to the feedwater, and for pressurized water reactor primary-system-coolant chemistry.

  3. Characterization of crack growth under combined loading

    Science.gov (United States)

    Feldman, A.; Smith, F. W.; Holston, A., Jr.

    1977-01-01

    Room-temperature static and cyclic tests were made on 21 aluminum plates in the shape of a 91.4x91.4-cm Maltese cross with 45 deg flaws to develop crack growth and fracture toughness data under mixed-mode conditions. During cyclic testing, it was impossible to maintain a high proportion of shear-mode deformation on the crack tips. Cracks either branched or turned. Under static loading, cracks remained straight if shear stress intensity exceeded normal stress intensity. Mixed-mode crack growth rate data compared reasonably well with published single-mode data, and measured crack displacements agreed with the straight and branched crack analyses. Values of critical strain energy release rate at fracture for pure shear were approximately 50% higher than for pure normal opening, and there was a large reduction in normal stress intensity at fracture in the presence of high shear stress intensity. Net section stresses were well into the inelastic range when fracture occurred under high shear on the cracks.

  4. Crack growth monitoring at CFRP bond lines

    Science.gov (United States)

    Rahammer, M.; Adebahr, W.; Sachse, R.; Gröninger, S.; Kreutzbruck, M.

    2016-02-01

    With the growing need for lightweight technologies in aerospace and automotive industries, fibre-reinforced plastics, especially carbon-fibre (CFRP), are used with a continuously increasing annual growth rate. A promising joining technique for composites is adhesive bonding. While rivet holes destroy the fibres and cause stress concentration, adhesive bond lines distribute the load evenly. Today bonding is only used in secondary structures due to a lack of knowledge with regard to long-term predictability. In all industries, numerical simulation plays a critical part in the development process of new materials and structures, while it plays a vital role when it comes to CFRP adhesive bondings conducing the predictability of life time and damage tolerance. The critical issue with adhesive bondings is crack growth. In a dynamic tensile stress testing machine we dynamically load bonded CFRP coupon specimen and measure the growth rate of an artificially started crack in order to feed the models with the results. We also investigate the effect of mechanical crack stopping features. For observation of the bond line, we apply two non-contact NDT techniques: Air-coupled ultrasound in slanted transmission mode and active lockin-thermography evaluated at load frequencies. Both methods give promising results for detecting the current crack front location. While the ultrasonic technique provides a slightly higher accuracy, thermography has the advantage of true online monitoring, because the measurements are made while the cyclic load is being applied. The NDT methods are compared to visual inspection of the crack front at the specimen flanks and show high congruence. Furthermore, the effect of crack stopping features within the specimen on the crack growth is investigated. The results show, that not all crack fronts are perfectly horizontal, but all of them eventually come to a halt in the crack stopping feature vicinity.

  5. Strain energy density-distance criterion for the initiation of stress corrosion cracking of alloy X-750

    Energy Technology Data Exchange (ETDEWEB)

    Hall, M.M. Jr.; Symons, D.M.

    1996-05-01

    A strain energy density-distance criterion was previously developed and used to correlate rising-load K{sub c} initiation data for notched and fatigue precracked specimens of hydrogen precharged Alloy X-750. This criterion, which was developed for hydrogen embrittlement (HE) cracking, is used here to correlate static-load stress corrosion cracking (SCC) initiation times obtained for smooth geometry, notched and fatigue precracked specimens. The onset of SCC crack growth is hypothesized to occur when a critical strain, which is due to environment-enhanced creep, is attained within the specimen interior. For notched and precracked specimens, initiation is shown by analysis to occur at a variable distance from notch and crack tips. The initiation site varies from very near the crack tip, for highly loaded sharp cracks, to a site that is one grain diameter from the notch, for lower loaded, blunt notches. The existence of hydrogen gradients, which are due to strain-induced hydrogen trapping in the strain fields of notch and crack tips, is argued to be controlling the site for initiation of cracking. By considering the sources of the hydrogen, these observations are shown to be consistent with those from the previous HE study, in which the characteristic distance for crack initiation was found to be one grain diameter from the notch tip, independent of notch radius, applied stress intensity factor and hydrogen level.

  6. The Effects of Salt Water on the Slow Crack Growth of Soda Lime Silicate Glass

    Science.gov (United States)

    Hausmann, Bronson D.; Salem, Jonathan A.

    2016-01-01

    The slow crack growth parameters of soda-lime silicate were measured in distilled and salt water of various concentrations in order to determine if stress corrosion susceptibility is affected by the presence of salt and the contaminate formation of a weak sodium film. Past research indicates that solvents effect the rate of crack growth, however, the effects of salt have not been studied. The results indicate a small but statistically significant effect on the slow crack growth parameters A and n. However, for typical engineering purposes, the effect can be ignored.

  7. Pacific Northwest National Laboratory Investigation of the Stress Corrosion Cracking in Nickel-Base Alloys, Volume 2

    Energy Technology Data Exchange (ETDEWEB)

    Bruemmer, Stephen M.; Toloczko, Mychailo B.; Olszta, Matthew J.

    2012-03-01

    The objective of this program is to evaluate the primary water stress corrosion cracking (PWSCC) susceptibility of high chromium alloy 690 and its weld metals, establish quantitative measurements of crack-growth rates and determine relationships among cracking susceptibility, environmental conditions and metallurgical characteristics. Stress-corrosion, crack-growth rates have been determined for 12 alloy 690 specimens, 11 alloy 152/52/52M weld metal specimens, 4 alloy 52M/182 overlay specimens and 2 alloy 52M/82 inlay specimens in simulated PWR primary water environments. The alloy 690 test materials included three different heats of extruded control-rod-drive mechanism (CRDM) tubing with variations in the initial material condition and degree of cold work for one heat. Two cold-rolled (CR) alloy 690 plate heats were also obtained and evaluated enabling comparisons to the CR CRDM materials. Weld metal, overlay and inlay specimens were machined from industry mock ups to provide plant-representative materials for testing. Specimens have been tested for one alloy 152 weld, two alloy 52 welds and three alloy 52M welds. The overlay and inlay specimens were prepared to propagate stress-corrosion cracks from the alloy 182 or 82 material into the more resistant alloy 52M. In all cases, crack extension was monitored in situ by direct current potential drop (DCPD) with length resolution of about +1 µm making it possible to measure extremely low growth rates approaching 5x10-10 mm/s. Most SCC tests were performed at 325-360°C with hydrogen concentrations from 11-29 cc/kg; however, environmental conditions were modified during a few experiments to evaluate the influence of temperature, water chemistry or electrochemical potential on propagation rates. In addition, low-temperature (~50°C) cracking behavior was examined for selected alloy 690 and weld metal specimens. Extensive characterizations have been performed on material microstructures and stress-corrosion cracks by

  8. The mechanism of stress-corrosion cracking in 7075 aluminum alloy

    Science.gov (United States)

    Jacobs, A. J.

    1970-01-01

    Various aspects of stress-corrosion cracking in 7075 aluminum alloy are discussed. A model is proposed in which the continuous anodic path along which the metal is preferentially attacked consists of two phases which alternate as anodes.

  9. Thermally activated processes of fatigue crack growth in steels

    Science.gov (United States)

    Tanaka, Masaki; Fujii, Atsushi; Noguchi, Hiroshi; Higashida, Kenji

    2014-02-01

    Fatigue crack growth rates in steels at high and low temperatures have been investigated using Paris curves. The fatigue crack growth rates at high temperatures are quite different from those at low temperatures. Arrhenius plots between fatigue crack growth rate (da/dN) and test temperatures at constant stress intensity factor range (ΔKI) indicate a difference of the rate-controlling process for fatigue crack growth with temperature. Slip deformation at the crack tip governs fatigue crack growth at high temperatures, while hydrogen diffusion is associated with crack growth at low temperatures.

  10. Mesh sensitivity effects on fatigue crack growth by crack-tip blunting and re-sharpening

    DEFF Research Database (Denmark)

    Tvergaard, Viggo

    2007-01-01

    Crack-tip blunting under tensile loads and re-sharpening of the crack-tip during unloading is one of the basic mechanisms for fatigue crack growth in ductile metals. Based on an elastic–perfectly plastic material model, crack growth computations have been continued up to 700 full cycles by using...

  11. Fatigue crack growth from a cracked elastic particle into a ductile matrix

    NARCIS (Netherlands)

    Groh, S.; Olarnrithinun, S.; Curtin, W. A.; Needleman, A.; Deshpande, V. S.; Van der Giessen, E.

    2008-01-01

    The monotonic and cyclic crack growth rate of cracks is strongly influenced by the microstructure. Here, the growth of cracks emanating from pre-cracked micron-scale elastic particles and growing into single crystals is investigated, with a focus on the effects of (i) plastic confinement due to the

  12. Electrochemical investigation of crack initiation during corrosion fatigue of stainless steels in the passive state. Elektrochemische Untersuchung der Rissbildung bei Schwingungsrisskorrosion im stabil-passiven Werkstoffzustand

    Energy Technology Data Exchange (ETDEWEB)

    Spaehn, R. (Technische Hochschule Darmstadt (Germany, F.R.))

    1991-03-01

    The corrosion fatigue behaviour of three stainless steels - ferritic (12% Cr), austenitic (type 316 Ti) and austenitic-ferritic (type 31803; Duplex stainless steel) - was studied under rotating bending moments in aqueous sulphuric acid of 30deg C. An instrumental set-up for recording the transient currents of specimens during potentiostatically controlled corrosion fatigue is described. Based on this transient current signal technique, three stages on the corrosion fatigue process can be discerned. In the incubation period, small stochastic current transients are caused by the response of the passive layer to alternating stresses and environmental conditions. The appearance of sinusoidal current signals indicates crack initiation whereas the phase angle between a fixed marker - i.e. a light barrier signal -, and the anodic amplitude represents the site of initiating cracks. Finally, the crack growth period is characterized by an increasing cell current and steadily growing sinusoidal current signals caused by the interplay of microplastic and repassivation processes at the crack tip. (orig.).

  13. Numerical investigation on stress corrosion cracking behavior of dissimilar weld joints in pressurized water reactor plants

    Directory of Open Access Journals (Sweden)

    Lingyan Zhao

    2014-07-01

    Full Text Available There have been incidents recently where stress corrosion cracking (SCC observed in the dissimilar metal weld (DMW joints connecting the reactor pressure vessel (RPV nozzle with the hot leg pipe. Due to the complex microstructure and mechanical heterogeneity in the weld region, dissimilar metal weld joints are more susceptible to SCC than the bulk steels in the simulated high temperature water environment of pressurized water reactor (PWR. Tensile residual stress (RS, in addition to operating loads, has a great contribution to SCC crack growth. Limited experimental conditions, varied influence factors and diverging experimental data make it difficult to accurately predict the SCC behavior of DMW joints with complex geometry, material configuration, operating loads and crack shape. Based on the film slip/dissolution oxidation model and elastic-plastic finite element method (EPFEM, an approach is developed to quantitatively predict the SCC growth rate of a RPV outlet nozzle DMW joint. Moreover, this approach is expected to be a pre-analytical tool for SCC experiment of DMW joints in PWR primary water environment.

  14. Fatigue Crack Growth Analysis Under Spectrum Loading in Various Environmental Conditions

    Science.gov (United States)

    Mikheevskiy, S.; Glinka, G.; Lee, E.

    2013-03-01

    model. The method can be also used to predict fatigue crack growth under constant amplitude and spectrum loading in various environmental conditions such as vacuum, air, and corrosive environment providing that appropriate limited constant amplitude fatigue crack growth data obtained in the same environment are available. The proposed methodology is equally suitable for fatigue analysis of smooth, notched, and cracked components.

  15. Precursor Evolution and Stress Corrosion Cracking Initiation of Cold-Worked Alloy 690 in Simulated Pressurized Water Reactor Primary Water

    Energy Technology Data Exchange (ETDEWEB)

    Zhai, Ziqing [Pacific Northwest National Laboratory, 622 Horn Rapids Road, P.O. Box 999, Richland, Washington 99352.; Toloczko, Mychailo [Pacific Northwest National Laboratory, 622 Horn Rapids Road, P.O. Box 999, Richland, Washington 99352.; Kruska, Karen [Pacific Northwest National Laboratory, 622 Horn Rapids Road, P.O. Box 999, Richland, Washington 99352.; Bruemmer, Stephen [Pacific Northwest National Laboratory, 622 Horn Rapids Road, P.O. Box 999, Richland, Washington 99352.

    2017-05-22

    Stress corrosion crack initiation of two thermally-treated, cold-worked (CW) alloy 690 (UNS N06690) materials was investigated in 360oC simulated PWR primary water using constant load tensile (CLT) tests and blunt notch compact tension (BNCT) tests equipped with direct current potential drop (DCPD) for in-situ detection of cracking. SCC initiation was not detected by DCPD for either the 21% or 31%CW CLT specimens loaded at their yield stress after ~9,220 hours, however intergranular (IG) precursor damage and isolated surface cracks were observed on the specimens. The two 31%CW BNCT specimens loaded at moderate stress intensity after several cyclic loading ramps showed DCPD-indicated crack initiation after 10,400 hours of exposure at constant stress intensity, which was resulted from significant growth of IG cracks. The 21%CW BNCT specimens only exhibited isolated small IG surface cracks and showed no apparent DCPD change throughout the test. Post-test cross-section examinations revealed many grain boundary (GB) nano-cavities in the bulk of all the CLT and BNCT specimens particularly for the 31%CW materials. Cavities were also found along GBs extending to the surface suggesting an important role in crack nucleation. This paper provides an overview of the evolution of GB cavities and discusses their effects on crack initiation in CW alloy 690.

  16. ENDOFEM INTEGRATED METHODOLOGY FOR FATIGUE CRACK GROWTH

    Institute of Scientific and Technical Information of China (English)

    C.F.Lee; L.T.Hsiao

    2002-01-01

    In this paper, the FEM with the incremental endochronic cyclic plasticity (EndoFEM) and the rc controlled node-released strategy are employed to study the fatigue crack opened/closed load (Pop) of A1 2024-T3 CCT specimens provided by Mageed and Pandey under several crack lengths and the constant amplitude with various load ratio (R). After statisfactory results are achieved by comparisons of computed Pop values and cited experimental data, the simulations will be extended to the crack lengths with significant bending effect due to short ligaments or high peak (Pmax) or high positive or very low negative R cyclic loads. Through these simulations, the complete map of Pop/Pmax vs. Kmax and R can be constructed and thereafter its correspondant empirical formulae can be proposed. Using these formulae and selecting the traditional fatigue crack growth parameter ΔKeff, the A1 2024-T3 fatigue crack growth rate da/dN vs. ΔK and R data, provided by Hiroshi and Schijve, can be employed to proposed empirical formulae of da/dN vs. ΔKeff and R. After integration, fatigue-crack-growth length a vs. N curves computed by EndoFEM can be obtained. The results are agreed very well with the existing experimental curves. According to the above procedures of simulation and steps of comparions with experiment, this paper may provides an integrate methodology of numerical simulation in the studies of fatigue crack growth for academic and industrial researches and design analysis.

  17. Stress corrosion cracking and hydrogen embrittlement of thick section high strength low alloy steel.

    OpenAIRE

    Needham, William Donald

    1986-01-01

    An experimental study was conducted to evaluate the corrosion performance of weldments of a high strength low alloy(HSLA) steel in a simulated seawater environment. This steel, designated HSLA80, was developed by the United States Navy for use in ship structural applications. Stress corrosion CRACKING(SCC) and hydrogen embrittlement(HEM) were investigated by conducting 42 Wedge-Opening load(WOL) tests as a function of stress intensity and corrosion potential and 33 Slow Strain Rate(SSR) tests...

  18. Fatigue crack growth under variable amplitude loading

    Science.gov (United States)

    Sidawi, Jihad A.

    1994-01-01

    Fatigue crack growth tests were conducted on an Fe 510 E C-Mn steel and a submerged arc welded joint from the same material under constant, variable, and random loading amplitudes. Paris-Erdogan's crack growth rate law was tested for the evaluation of m and C using the stress intensity factor K, the J-integral, the effective stress intensity factor K(sub eff), and the root mean square stress intensity factor K(sub rms) fracture mechanics concepts. The effect of retardation and residual stresses resulting from welding was also considered. It was found that all concepts gave good life predictions in all cases.

  19. Modeling Threshold of Stress Intensity Factor in Iodine Induced Stress Corrosion Crack of Zirconium

    Institute of Scientific and Technical Information of China (English)

    SHANG; Xin-yuan; CHEN; Peng

    2013-01-01

    KISCC,which is the threshold of stress intensity factor of iodine induced stress corrosion crack(ISCC)of Zirconium,reflects the susceptibility of ISCC of zirconium.Once the stress intensity factor surpasses the threshold,the cracking propagation modality in material will transform to transgranular from intergranular immediately and the velocity of the cracking will increase rapidly.Four key factors that’s

  20. Accelerated Stress Corrosion Crack Initiation of Alloys 600 and 690 in Hydrogenated Supercritical Water

    Science.gov (United States)

    Moss, Tyler; Was, Gary S.

    2017-04-01

    The objective of this study is to determine whether stress corrosion crack initiation of Alloys 600 and 690 occurs by the same mechanism in subcritical and supercritical water. Tensile bars of Alloys 690 and 600 were strained in constant extension rate tensile experiments in hydrogenated subcritical and supercritical water from 593 K to 723 K (320 °C to 450 °C), and the crack initiation behavior was characterized by high-resolution electron microscopy. Intergranular cracking was observed across the entire temperature range, and the morphology, structure, composition, and temperature dependence of initiated cracks in Alloy 690 were consistent between hydrogenated subcritical and supercritical water. Crack initiation of Alloy 600 followed an Arrhenius relationship and did not exhibit a discontinuity or change in slope after crossing the critical temperature. The measured activation energy was 121 ± 13 kJ/mol. Stress corrosion crack initiation in Alloy 690 was fit with a single activation energy of 92 ± 12 kJ/mol across the entire temperature range. Cracks were observed to propagate along grain boundaries adjacent to chromium-depleted metal, with Cr2O3 observed ahead of crack tips. All measures of the SCC behavior indicate that the mechanism for stress corrosion crack initiation of Alloy 600 and Alloy 690 is consistent between hydrogenated subcritical and supercritical water.

  1. Accelerated Stress Corrosion Crack Initiation of Alloys 600 and 690 in Hydrogenated Supercritical Water

    Science.gov (United States)

    Moss, Tyler; Was, Gary S.

    2017-01-01

    The objective of this study is to determine whether stress corrosion crack initiation of Alloys 600 and 690 occurs by the same mechanism in subcritical and supercritical water. Tensile bars of Alloys 690 and 600 were strained in constant extension rate tensile experiments in hydrogenated subcritical and supercritical water from 593 K to 723 K (320 °C to 450 °C), and the crack initiation behavior was characterized by high-resolution electron microscopy. Intergranular cracking was observed across the entire temperature range, and the morphology, structure, composition, and temperature dependence of initiated cracks in Alloy 690 were consistent between hydrogenated subcritical and supercritical water. Crack initiation of Alloy 600 followed an Arrhenius relationship and did not exhibit a discontinuity or change in slope after crossing the critical temperature. The measured activation energy was 121 ± 13 kJ/mol. Stress corrosion crack initiation in Alloy 690 was fit with a single activation energy of 92 ± 12 kJ/mol across the entire temperature range. Cracks were observed to propagate along grain boundaries adjacent to chromium-depleted metal, with Cr2O3 observed ahead of crack tips. All measures of the SCC behavior indicate that the mechanism for stress corrosion crack initiation of Alloy 600 and Alloy 690 is consistent between hydrogenated subcritical and supercritical water.

  2. Fatigue cracks in Eurofer 97 steel: Part II. Comparison of small and long fatigue crack growth

    Science.gov (United States)

    Kruml, T.; Hutař, P.; Náhlík, L.; Seitl, S.; Polák, J.

    2011-05-01

    The fatigue crack growth rate in the Eurofer 97 steel at room temperature was measured by two different methodologies. Small crack growth data were obtained using cylindrical specimens with a shallow notch and no artificial crack starters. The growth of semicircular cracks of length between 10-2000 μm was followed in symmetrical cycling with constant strain amplitude ( R ɛ = -1). Long crack data were measured using standard CT specimen and ASTM methodology, i.e. R = 0.1. The growth of cracks having the length in the range of 10-30 mm was measured. It is shown that the crack growth rates of both types of cracks are in a very good agreement if J-integral representation is used and usual assumptions of the crack closure effects are taken into account.

  3. Fatigue cracks in Eurofer 97 steel: Part II. Comparison of small and long fatigue crack growth

    Energy Technology Data Exchange (ETDEWEB)

    Kruml, T., E-mail: kruml@ipm.cz [Institute of Physics of Materials, Academy of Sciences of the Czech Republic, Zizkova 22, CZ 61662 Brno (Czech Republic); Hutar, P.; Nahlik, L.; Seitl, S.; Polak, J. [Institute of Physics of Materials, Academy of Sciences of the Czech Republic, Zizkova 22, CZ 61662 Brno (Czech Republic)

    2011-05-01

    The fatigue crack growth rate in the Eurofer 97 steel at room temperature was measured by two different methodologies. Small crack growth data were obtained using cylindrical specimens with a shallow notch and no artificial crack starters. The growth of semicircular cracks of length between 10-2000 {mu}m was followed in symmetrical cycling with constant strain amplitude (R{sub {epsilon}} = -1). Long crack data were measured using standard CT specimen and ASTM methodology, i.e. R = 0.1. The growth of cracks having the length in the range of 10-30 mm was measured. It is shown that the crack growth rates of both types of cracks are in a very good agreement if J-integral representation is used and usual assumptions of the crack closure effects are taken into account.

  4. Influence of oxide films on primary water stress corrosion cracking initiation of alloy 600

    Science.gov (United States)

    Panter, J.; Viguier, B.; Cloué, J.-M.; Foucault, M.; Combrade, P.; Andrieu, E.

    2006-01-01

    In the present study alloy 600 was tested in simulated pressurised water reactor (PWR) primary water, at 360 °C, under an hydrogen partial pressure of 30 kPa. These testing conditions correspond to the maximum sensitivity of alloy 600 to crack initiation. The resulting oxidised structures (corrosion scale and underlying metal) were characterised. A chromium rich oxide layer was revealed, the underlying metal being chromium depleted. In addition, analysis of the chemical composition of the metal close to the oxide scale had allowed to detect oxygen under the oxide scale and particularly in a triple grain boundary. Implication of such a finding on the crack initiation of alloy 600 is discussed. Significant diminution of the crack initiation time was observed for sample oxidised before stress corrosion tests. In view of these results, a mechanism for stress corrosion crack initiation of alloy 600 in PWR primary water was proposed.

  5. Stress corrosion cracking of AISI 321 stainless steel in acidic chloride solution

    Indian Academy of Sciences (India)

    Yanliang Huang

    2002-02-01

    The stress corrosion cracking (SCC) of AISI 321 stainless steel in acidic chloride solution was studied by slow strain rate (SSR) technique and fracture mechanics method. The fractured surface was characterized by cleavage fracture. In order to clarify the SCC mechanism, the effects of inhibitor KI on SCC behaviour were also included in this paper. A study showed that the inhibition effects of KI on SCC were mainly attributed to the anodic reaction of the corrosion process. The results of strain distribution in front of the crack tip of the fatigue pre-cracked plate specimens in air, in the blank solution (acidic chloride solution without inhibitor KI) and in the solution added with KI measured by speckle interferometry (SPI) support the unified mechanism of SCC and corrosion fatigue cracking (CFC).

  6. EFFECTS OF CHEMISTRY AND OTHER VARIABLES ON CORROSION AND STRESS CORROSION CRACKING IN HANFORD DOUBLE SHELL TANKS

    Energy Technology Data Exchange (ETDEWEB)

    BROWN MH

    2008-11-13

    Laboratory testing was performed to develop a comprehensive understanding of the corrosivity of the tank wastes stored in Double-Shell Tanks using simulants primarily from Tanks 241-AP-105, 241-SY-103 and 241-AW-105. Additional tests were conducted using simulants of the waste stored in 241-AZ-102, 241-SY-101, 241-AN-107, and 241-AY-101. This test program placed particular emphasis on defining the range of tank waste chemistries that do not induce the onset of localized forms of corrosion, particularly pitting and stress corrosion cracking. This document summarizes the key findings of the research program.

  7. Microstructural and Stress Corrosion Cracking Characteristics of Austenitic Stainless Steels Containing Silicon

    Science.gov (United States)

    Andresen, Peter L.; Chou, Peter H.; Morra, Martin M.; Lawrence Nelson, J.; Rebak, Raul B.

    2009-12-01

    Austenitic stainless steels (SSs) core internal components in nuclear light water reactors (LWRs) are susceptible to irradiation-assisted stress corrosion cracking (IASCC). One of the effects of irradiation is the hardening of the SS and a change in the dislocation distribution in the alloy. Irradiation may also alter the local chemistry of the austenitic alloys; for example, silicon may segregate and chromium may deplete at the grain boundaries. The segregation or depletion phenomena at near-grain boundaries may enhance the susceptibility of these alloys to environmentally assisted cracking (EAC). The objective of the present work was to perform laboratory tests in order to better understand the role of Si in the microstructure, properties, electrochemical behavior, and susceptibility to EAC of austenitic SSs. Type 304 SS can dissolve up to 2 pct Si in the bulk while maintaining a single austenite microstructure. Stainless steels containing 12 pct Cr can dissolve up to 5 pct bulk Si while maintaining an austenite structure. The crack growth rate (CGR) results are not conclusive about the effect of the bulk concentration of Si on the EAC behavior of SSs.

  8. Fatigue crack growth simulations of 3-D linear elastic cracks under thermal load by XFEM

    Institute of Scientific and Technical Information of China (English)

    Himanshu PATHAK[1; Akhilendra SINGH[2; I.V. SINGH[3; S. K. YADAV[3

    2015-01-01

    This paper deals with the fatigue crack growth simulations of three-dimensional linear elastic cracks by XFEM under cyclic thermal load. Both temperature and displacement approximations are extrinsically enriched by Heaviside and crack front enrichment functions. Crack growth is modelled by successive linear extensions, and the end points of these linear extensions are joined by cubic spline segments to obtain a modified crack front. Different crack geometries such as planer, non-planer and arbitrary spline shape cracks are simulated under thermal shock, adiabatic and isothermal loads to reveal the sturdiness and versatility of the XFEM approach.

  9. Role of {delta}-ferrite in stress corrosion cracking retardation near fusion boundary of 316NG welds

    Energy Technology Data Exchange (ETDEWEB)

    Abe, Hiroshi, E-mail: hiroshi.abe@qse.tohoku.ac.jp [Graduate School of Engineering, Tohoku University, 6-6-01-2, Aoba, Aramaki, Aoba-ku, Sendai, Miyagi 980-8579 (Japan); Watanabe, Yutaka [Graduate School of Engineering, Tohoku University, 6-6-01-2, Aoba, Aramaki, Aoba-ku, Sendai, Miyagi 980-8579 (Japan)

    2012-05-15

    Stress corrosion cracking (SCC) near the fusion boundary of a 316NG stainless steel (SS) welded joint in high-temperature water was investigated with emphasis on the relation to the microstructural characteristics. {delta}-Ferrite islands were distributed on the crack paths (grain boundary in the partially melted zone and cell boundary in the unmixed zone) near the fusion boundary of 316NG SS piping. SCC retardation near the fusion boundary was clearly observed in our experiments. The relative crack growth rate (CGR) at the {delta}-{gamma} interface was estimated to be 0.043 times lower than that at the {gamma}-{gamma} interface. The cracks remained for a considerable period of time just after they reached the {delta}-ferrite islands. Even those cracks that passed through an initial set of {delta}-ferrite islands were retarded when they encountered a subsequent set of {delta}-ferrite islands. High corrosion resistance due to the presence of large amounts of Cr and the island-shaped morphology of {delta}-ferrite are dominant factors in SCC retardation.

  10. Environmental Cracking of Corrosion Resistant Alloys in the Chemical Process Industry - A Review

    Energy Technology Data Exchange (ETDEWEB)

    Rebak, R B

    2006-12-04

    A large variety of corrosion resistant alloys are used regularly in the chemical process industry (CPI). The most common family of alloys include the iron (Fe)-based stainless steels, nickel (Ni) alloys and titanium (Ti) alloys. There also other corrosion resistant alloys but their family of alloys is not as large as for the three groups mentioned above. All ranges of corrosive environments can be found in the CPI, from caustic solutions to hot acidic environments, from highly reducing to highly oxidizing. Stainless steels are ubiquitous since numerous types of stainless steels exist, each type tailored for specific applications. In general, stainless steels suffer stress corrosion cracking (SCC) in hot chloride environments while high Ni alloys are practically immune to this type of attack. High nickel alloys are also resistant to caustic cracking. Ti alloys find application in highly oxidizing solutions. Solutions containing fluoride ions, especially acid, seem to be aggressive to almost all corrosion resistant alloys.

  11. Film-induced stress enhancing stress corrosion cracking of austenitic stainless steel

    Institute of Scientific and Technical Information of China (English)

    李金许; 陈浩; 王燕斌; 乔利杰; 褚武扬

    2001-01-01

    A constant deflection device designed for use within a transmission electron microscopy (TEM) was used to investigate the change in dislocation configuration ahead of a crack tip during stress corrosion cracking (SCC) of type 310 austenitic stainless steel in a boiling MgCl2 solution, and the initiation process of stress corrosion microcrack. Results showed that corrosion process during SCC enhanced dislocation emission, multiplication and motion. Microcracks of SCC were initiated when the corrosion-enhanced dislocation emission and motion reached critical state.   A passive film formed during corrosion of austenitic stainless steel in the boiling MgCl2 solution generated a tensile stress. During SCC, the additive tensile stress generated at the metal/passive film interface helps enhance dislocation emission and motion.

  12. Subcritical crack growth in fibrous materials

    CERN Document Server

    Santucci, Stéphane; Deschanel, Stéphanie; Vanel, Loic; Ciliberto, Sergio

    2006-01-01

    We present experiments on the slow growth of a single crack in a fax paper sheet submitted to a constant force $F$. We find that statistically averaged crack growth curves can be described by only two parameters : the mean rupture time $\\tau$ and a characteristic growth length $\\zeta$. We propose a model based on a thermally activated rupture process that takes into account the microstructure of cellulose fibers. The model is able to reproduce the shape of the growth curve, the dependence of $\\zeta$ on $F$ as well as the effect of temperature on the rupture time $\\tau$. We find that the length scale at which rupture occurs in this model is consistently close to the diameter of cellulose microfibrils.

  13. Relationship between localized strain and irradiation assisted stress corrosion cracking in an austenitic alloy

    Energy Technology Data Exchange (ETDEWEB)

    McMurtrey, M.D., E-mail: mdmcm@umich.edu [Department of Nuclear Engineering and Radiological Sciences, University of Michigan, Ann Arbor, MI 48109 (United States); Was, G.S. [Department of Nuclear Engineering and Radiological Sciences, University of Michigan, Ann Arbor, MI 48109 (United States); Patrick, L.; Farkas, D. [Department of Materials Science and Engineering, Virginia Tech, Blacksburg, VA 24061 (United States)

    2011-04-25

    Research highlights: {yields} Austenitic steel is more susceptible to intergranular corrosion after irradiation. {yields} Simulation and experiment used to study cracking in irradiated austentic steel. {yields} Cracking occurs at random high angle boundaries normal to the tensile stress. {yields} Cracking at boundaries with high normal stress and inability to accommodate strain. {yields} Boundary type, angle, and Taylor and Schmid factors affect strain accommodation. - Abstract: Irradiation assisted stress corrosion cracking may be linked to the local slip behavior near grain boundaries that exhibit high susceptibility to cracking. Fe-13Cr-15Ni austenitic steel was irradiated with 2 MeV protons at 360 deg. C to 5 dpa and strained in 288 deg. C simulated BWR conditions. Clusters of grains from the experiment were created in an atomistic simulation and then virtually strained using molecular dynamic simulation techniques. Cracking and grain orientation data were characterized in both the experiment and the simulation. Random high angle boundaries with high surface trace angles with respect to the tensile direction were found to be the most susceptible to cracking. Grain boundary cracking susceptibility was also found to correlate strongly with slip continuity, indicating that the strain accommodation at the boundary is related to cracking resistance. Higher cracking susceptibility was also found at grain boundaries adjacent to grains with low Schmid factor or high Taylor factor. The basic trends reported here are supported by both the experiments and the simulations.

  14. Development of chloride-induced corrosion in pre-cracked RC beams under sustained loading: Effect of load-induced cracks, concrete cover, and exposure conditions

    Energy Technology Data Exchange (ETDEWEB)

    Yu, Linwen [Université de Toulouse, UPS, INSA, LMDC, Toulouse (France); Université de Sherbrooke, Quebec (Canada); François, Raoul, E-mail: raoul.francois@insa-toulouse.fr [Université de Toulouse, UPS, INSA, LMDC, Toulouse (France); Dang, Vu Hiep [Hanoi Architectural University, Faculty of Civil Engineering, Hanoi (Viet Nam); L' Hostis, Valérie [CEA Saclay, CEA, DEN, DPC, SECR, Laboratoire d' Etude du Comportement des Bétons et des Argiles, Gif-sur-Yvette (France); Gagné, Richard [Université de Sherbrooke, Quebec (Canada)

    2015-01-15

    This paper deals with corrosion initiation and propagation in pre-cracked reinforced concrete beams under sustained loading during exposure to a chloride environment. Specimen beams that were cast in 2010 were compared to specimens cast in 1984. The only differences between the two sets of beams were the casting direction in relation to tensile reinforcement and the exposure conditions in the salt-fog chamber. The cracking maps, corrosion maps, chloride profiles, and cross-sectional loss of one group of two beams cast in 2010 were studied and their calculated corrosion rates were compared to that of beams cast in 1984 in order to investigate the factors influencing the natural corrosion process. Experimental results show that, after rapid initiation of corrosion at the crack tip, the corrosion process practically halted and the time elapsing before corrosion resumed depended on the exposure conditions and cover depth.

  15. Analysis of acoustic emission signals of fatigue crack growth and corrosion processes. Investigation of the possibilities for continuous condition monitoring of transport containers by acoustic emission testing; Analyse der Schallemissionssignale aus Ermuedungsrisswachstum und Korrosionsprozessen. Untersuchung der Moeglichkeiten fuer die kontinuierliche Zustandsueberwachung von Transportbehaeltern mittels Schallemissionspruefung

    Energy Technology Data Exchange (ETDEWEB)

    Wachsmuth, Janne

    2016-05-01

    Fatigue crack growth and active corrosion processes are the main causes of structural failures of transport products like road tankers, railway tank cars and ships. To prevent those failures, preventive, time-based maintenance is performed. However, preventive inspections are costly and include the risk of not detecting a defect, which could lead to a failure within the next service period. An alternative is the idea of continuous monitoring of the whole structure by means of acoustic emission testing (AT). With AT, defects within the material shall be detected and repaired directly after their appearance. Acoustic emission testing is an online non-destructive testing method. Acoustic emission (AE) arises from changes within the material and is transported by elastic waves through the material. If the AE event generates enough energy, the elastic wave propagates to the boundaries of the component, produces a displacement in the picometre scale and can be detected by a piezoelectric sensor. The sensor produces an electrical signal. From this AE signal, AE features such as the maximum amplitude or the frequency can be extracted. Methods of signal analysis are used to investigate the time and frequency dependency of signal groups. The purpose of the signal analysis is to connect the AE signal with the originating AE source. If predefined damage mechanisms are identified, referencing the damage condition of the structure is possible. Acoustic emission from events of the actual crack propagation process can for example lead to the crack growth rate or the stress intensity factor, both specific values from fracture mechanics. A new development in the domain of acoustic emission testing is the pattern recognition of AE signals. Specific features are extracted from the AE signals to assign them to their damage mechanisms. In this thesis the AE signals from the damage mechanisms corrosion and fatigue crack growth are compared and analysed. The damage mechanisms were

  16. A test procedure for determining the influence of stress ratio on fatigue crack growth

    Science.gov (United States)

    Fitzgerald, J. H.; Wei, R. P.

    1974-01-01

    A test procedure is outlined by which the rate of fatigue crack growth over a range of stress ratios and stress intensities can be determined expeditiously using a small number of specimens. This procedure was developed to avoid or circumvent the effects of load interactions on fatigue crack growth, and was used to develop data on a mill annealed Ti-6Al-4V alloy plate. Experimental data suggest that the rates of fatigue crack growth among the various stress ratios may be correlated in terms of an effective stress intensity range at given values of K max. This procedure is not to be used, however, for determining the corrosion fatigue crack growth characteristics of alloys when nonsteady-state effects are significant.

  17. Crack Growth along Interfaces in Porous Ceramic Layers

    DEFF Research Database (Denmark)

    Sørensen, Bent F.; Horsewell, Andy

    2001-01-01

    Crack growth along porous ceramic layers was studied experimentally. Double cantilever beam sandwich specimens were loaded with pure bending moments to obtain stable crack growth. The experiments were conducted in an environmental scanning electron microscope enabling in situ observations...

  18. Hydrogen embrittlement, grain boundary segregation, and stress corrosion cracking of alloy X-750 in low- and high-temperature water

    Energy Technology Data Exchange (ETDEWEB)

    Mills, W. J.; Lebo, M. R.; Kearns, J. J. [Bettis Atomic Power Lab., West Mifflin, PA (United States)

    1997-04-01

    The nature of intergranular stress corrosion cracking (SCC) of alloy X-750 was characterized in low- and high-temperature water by testing as-notched and precracked fracture mechanics specimens. Materials given the AH, BH, and HTH heat treatments were studied. While all heat treatments were susceptible to rapid low-temperature crack propagation (LTCP) below 150 C, conditions AH and BH were particularly susceptible. Low-temperature tests under various loading conditions (e.g., constant displacement, constant load, and increasing load) revealed that the maximum stress intensity factors (K{sub P{sub max}}) from conventional rising load tests provide conservative estimates of the critical loading conditions in highly susceptible heats, regardless of the load path history. For resistant heats, K{sub P{sub max}} provides a reasonable, but not necessarily conservative, estimate of the critical stress intensity factor for LTCP. Testing of as-notched specimens showed that LTCP will not initiate at a smooth surface or notch, but will readily occur if a cracklike defect is present. Comparison of the cracking response in water with that for hydrogen-precharged specimens tested in air demonstrated that LTCP is associated with hydrogen embrittlement of grain boundaries. The stress corrosion crack initiation and growth does occur in high-temperature water (>250 C), but crack growth rates are orders of magnitude lower than LTCP rates. The SCC resistance of HTH heats is far superior to that of AH heats as crack initiation times are two to three orders of magnitude greater and growth rates are one to two orders of magnitude lower.

  19. Controlling fatigue crack paths for crack surface marking and growth investigations

    Directory of Open Access Journals (Sweden)

    S. Barter

    2016-01-01

    Full Text Available While it is well known that fatigue crack growth in metals that display confined slip, such as high strength aluminium alloys, develop crack paths that are responsive to the loading direction and the local microstructural orientation, it is less well known that such paths are also responsive to the loading history. In these materials, certain loading sequences can produce highly directional slip bands ahead of the crack tip and by adjusting the sequence of loads, distinct fracture surface features or progression marks, even at very small crack depths can result. Investigating the path a crack selects in fatigue testing when particular combinations of constant and variable amplitude load sequences are applied is providing insight into crack growth. Further, it is possible to design load sequences that allow very small amounts of crack growth to be measured, at very small crack sizes, well below the conventional crack growth threshold in the aluminium alloy discussed here. This paper reports on observations of the crack path phenomenon and a novel test loading method for measuring crack growth rates for very small crack depths in aluminium alloy 7050-T7451 (an important aircraft primary structural material. The aim of this work was to firstly generate short- crack constant amplitude growth data and secondly, through the careful manipulation of the applied loading, to achieve a greater understanding of the mechanisms of fatigue crack growth in the material being investigated. A particular focus of this work is the identification of the possible sources of crack growth retardation and closure in these small cracks. Interpreting these results suggests a possible mechanism for why small fatigue crack growth through this material under variable amplitude loading is faster than predicted from models based on constant amplitude data alone.

  20. Fatigue Crack Extension Model of Aluminium Alloy with Prior Corrosion Damage Based on Localised Corrosion Damage%基于局部腐蚀损伤的铝合金预腐蚀疲劳裂纹扩展模型

    Institute of Scientific and Technical Information of China (English)

    孔光明; 李旭东; 穆志韬

    2014-01-01

    目的:建立铝合金预腐蚀疲劳裂纹扩展模型。方法采用表征局部环境腐蚀损伤影响程度的参数孔蚀率对腐蚀疲劳裂纹扩展速率进行修正。结果修正后的腐蚀铝合金试件的疲劳裂纹扩展速率与试验结果吻合程度良好。结论修正后的铝合金预腐蚀疲劳裂纹扩展速率模型合理有效,试验数据和预测模型可为海军飞机结构的损伤容限设计提供参考。%Objective To establish a modified model for pre-corrosion fatigue crack growth rate of aluminum alloy. Methods Considering that the local damage around the crack tip was more reasonable for accelerating crack growth rate in corrosive environment, the pitting rate, which was a parameter characterizing the influence of corrosion in local environ-ment, was used to correct the corrosion fatigue crack growth rate. Results The experimental results were in good agreement with predictions of the amended fatigue crack growth rate model for corroded aluminum alloy specimens. Conclusion The corrected aluminum alloy pre-corrosion fatigue crack growth rate model was reasonable and effective, and the test data and the prediction model could provide a reference for the damage tolerance design of navy aircraft structure.

  1. The role of local strains from prior cold work on stress corrosion cracking of α-brass in Mattsson's solution

    Energy Technology Data Exchange (ETDEWEB)

    Ulaganathan, Jaganathan, E-mail: jagan.ulaganathan@mail.utoronto.ca; Newman, Roger C., E-mail: roger.newman@utoronto.ca

    2014-06-01

    The dynamic strain rate ahead of a crack tip formed during stress corrosion cracking (SCC) under a static load is assumed to arise from the crack propagation. The strain surrounding the crack tip would be redistributed as the crack grows, thereby having the effect of dynamic strain. Recently, several studies have shown cold work to cause accelerated crack growth rates during SCC, and the slip-dissolution mechanism has been widely applied to account for this via a supposedly increased crack-tip strain rate in cold worked material. While these interpretations consider cold work as a homogeneous effect, dislocations are generated inhomogeneously within the microstructure during cold work. The presence of grain boundaries results in dislocation pile-ups that cause local strain concentrations. The local strains generated from cold working α-brass by tensile elongation were characterized using electron backscatter diffraction (EBSD). The role of these local strains in SCC was studied by measuring the strain distributions from the same regions of the sample before cold work, after cold work, and after SCC. Though, the cracks did not always initiate or propagate along boundaries with pre-existing local strains from the applied cold work, the local strains surrounding the cracked boundaries had contributions from both the crack propagation and the prior cold work. - Highlights: • Plastic strain localization has a complex relationship with SCC susceptibility. • Surface relief created by cold work creates its own granular strain localization. • Cold work promotes crack growth but several other factors are involved.

  2. Analysis of stress corrosion cracking in alloy 718 following commercial reactor exposure

    Science.gov (United States)

    Leonard, Keith J.; Gussev, Maxim N.; Stevens, Jacqueline N.; Busby, Jeremy T.

    2015-11-01

    Alloy 718 is generally considered a highly corrosion-resistant material but can still be susceptible to stress corrosion cracking (SCC). The combination of factors leading to SCC susceptibility in the alloy is not always clear enough. In the present work, alloy 718 leaf spring (LS) materials that suffered stress corrosion damage during two 24-month cycles in pressurized water reactor service, operated to >45 MWd/mtU burn-up, was investigated. Compared to archival samples fabricated through the same processing conditions, little microstructural and property changes occurred in the material with in-service irradiation, contrary to high dose rate laboratory-based experiments reported in literature. Though the lack of delta phase formation along grain boundaries would suggest a more SCC resistant microstructure, grain boundary cracking in the material was extensive. Crack propagation routes were explored through focused ion beam milling of specimens near the crack tip for transmission electron microscopy as well as in polished plan view and cross-sectional samples for electron backscatter diffraction analysis. It has been shown in this study that cracks propagated mainly along random high-angle grain boundaries, with the material around cracks displaying a high local density of dislocations. The slip lines were produced through the local deformation of the leaf spring material above their yield strength. The cause for local SCC appears to be related to oxidation of both slip lines and grain boundaries, which under the high in-service stresses resulted in crack development in the material.

  3. The design of an instrumented rebar for assessment of corrosion in cracked reinforced concrete

    DEFF Research Database (Denmark)

    Pease, Bradley Justin; Geiker, Mette Rica; Stang, Henrik;

    2011-01-01

    An instrumented rebar is presented which was designed to have a realistic mechanical performance and to provide location dependent measurements to assess the environment with regards to reinforcement corrosion. The instrumented rebar was constructed from a hollowed 10 mm nominal diameter standard...... between the steel and concrete. Cracked beams with cast-in instrumented and standard rebars were ponded with a 10\\% chloride solution and the open circuit corrosion potential (OCP) of the 17 sensors was measured for up to 62 days. Measurements from the individual sensors indicate when and where active...... rebar with 17 electronically isolated corrosion sensors. Instrumented and standard rebars were cast into concrete beams and bending cracks were induced and held open using steel frames. Epoxy impregnation was used to assess and compare cracks in the concrete around the instrumented and standard rebar...

  4. Interplay of microbiological corrosion and alloy microstructure in stress corrosion cracking of weldments of advanced stainless steels

    Indian Academy of Sciences (India)

    R K Singh Raman

    2003-06-01

    This paper presents an overview of the phenomenon of stress corrosion cracking (SCC) of duplex stainless steels and their weldments in marine environments and the potential role of microbial activity in inducing SCC susceptibility. As a precursor to the topic the paper also reviews the performance of the traditional corrosion-resistant alloys and their weldments and the necessity of using duplex stainless steels (DSS), in order to alleviate corrosion problems in marine environments. Given that the performance of weldments of such steels is often unsatisfactory, this review also assesses the research needs in this area. In this context the paper also discusses the recent reports on the role of microorganisms in inducing hydrogen embrittlements and corrosion fatigue.

  5. Modeling the Time-to Corrosion Cracking of the Cover Concrete in Chloride Contaminated Reinforced Concrete Structures

    OpenAIRE

    Liu, Youping

    1996-01-01

    Significant factors on steel corrosion in chloride contaminated reinforced concrete and time-to-corrosion cracking were investigated in this study. Sixty specimens were designed with seven admixed chloride contents, three concrete cover depths, two reinforcing steel bar diameters, two exposure conditions, and a typical concrete with water to cement ratio of 0.45. Corrosion current density (corrosion rate), corrosion potential, ohmic resistance of concrete and temperature were measured monthly...

  6. Effects of alloy chemistry, cold work, and water chemistry on corrosion fatigue and stress corrosion cracking of nickel alloys and welds.

    Energy Technology Data Exchange (ETDEWEB)

    Chopra, O. K.; Soppet, W. K.; Shack, W. J.; Energy Technology

    2001-04-01

    Reactor vessel internal components made of nickel-base alloys are susceptible to environmentally assisted cracking (EAC). A better understanding of the causes and mechanisms of this cracking may permit less conservative estimates of damage accumulation and requirements on inspection intervals. The objective of this work is to evaluate and compare the resistance of Alloys 600 and 690 and their welds, such as Alloys 82, 182, 52, and 152, to EAC in simulated light water reactor environments. The existing crack growth rate (CGR) data for these alloys under cyclic and constant loads have been evaluated to establish the effects of alloy chemistry, cold work, and water chemistry. The experimental fatigue CGRs are compared with CGRs that would be expected in air under the same mechanical loading conditions to obtain a qualitative understanding of the degree and range of conditions for significant environmental enhancement in growth rates. The existing stress corrosion cracking (SCC) data on Alloys 600 and 690 and Alloy 82, 182, and 52 welds have been compiled and analyzed to determine the influence of key parameters on growth rates in simulated PWR and BWR environments. The SCC data for these alloys have been evaluated with correlations developed by Scott and by Ford and Andresen.

  7. The Effect of Welding Residual Stress for Making Artificial Stress Corrosion Crack in the STS 304 Pipe

    Directory of Open Access Journals (Sweden)

    Jae-Seong Kim

    2015-01-01

    Full Text Available The stress corrosion crack is one of the fracture phenomena for the major structure components in nuclear power plant. During the operation of a power plant, stress corrosion cracks are initiated and grown especially in dissimilar weldment of primary loop components. In particular, stress corrosion crack usually occurs when the following three factors exist at the same time: susceptible material, corrosive environment, and tensile stress (residual stress included. Thus, residual stress becomes a critical factor for stress corrosion crack when it is difficult to improve the material corrosivity of the components and their environment under operating conditions. In this study, stress corrosion cracks were artificially produced on STS 304 pipe itself by control of welding residual stress. We used the instrumented indentation technique and 3D FEM analysis (using ANSYS 12 to evaluate the residual stress values in the GTAW area. We used the custom-made device for fabricating the stress corrosion crack in the inner STS 304 pipe wall. As the result of both FEM analysis and experiment, the stress corrosion crack was quickly generated and could be reproduced, and it could be controlled by welding residual stress.

  8. Stress-Corrosion Cracking of Metallic Materials. Part III. Hydrogen Entry and Embrittlement in Steel

    Science.gov (United States)

    1975-04-01

    Strength Steels," Stress Corrosion Cracking in High-Strength Steels and in Titanium and Altuninum Alloys, Naval Rasearch Laboratory, Washington, D.C...to pickling solutions. In all of these examples, the sulfide, cyanide, etc., caused a hydrogen-related problem that would not have existed in their...desorption reaction. In studying the pickling of low-carbon steel in various strong acids, Hudson’ 4 measured the corrosion rate and amount of hydr-ogen

  9. SCC crack growth rate of cold-worked austenitic stainless steels in PWR primary water conditions

    Energy Technology Data Exchange (ETDEWEB)

    Guerre, C.; Raquet, O.; Herms, E. [Commissariat a l' Energie Atomique (CEA), DEN/DPC/SCCME/LECA, Gif-sur-Yvette Cedex (France); Marie, S. [Commissariat a l' Energie Atomique (CEA), DEN/DM2S/SEMT/LISN, Gif-sur-Yvette Cedex (France); Le Calvar, M. [Inst. for Radiological Protection and Nuclear Safety (IRSN), DSR/SAMS, Fontenay-aux-Roses Cedex (France)

    2007-07-01

    Stress corrosion cracking (SCC) of stainless steels (SS) is a significant cause of failure in the pressurized water reactors (PWR). Most of the reported case history failures of SS in PWR can be attributed to pollutants (chloride, sulphate) and / or locally oxygenated environments, even to sensitisation of the SS. However, some failures have been attributed to heavy cold work (CW) of SS. In laboratory tests, SCC initiation of cold-worked SS has been obtained using slow strain rate tests (SSRT) in nominal PWR environment. This paper describes constant load and cyclic crack growth rate (CGR) tests on cold-worked SS, on CT specimens. 304L and 316L have been tested with a CW up to 60 %. CW 316L is more prone to cracking than 304L. Over 30 % of CW, 316L is susceptible to crack propagation under constant load. CW is the main controlling parameter for cracking. (author))

  10. Crack growth analysis due to PWSCC in dissimilar metal butt weld for reactor piping considering hydrostatic and normal operating conditions

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Hwee Sueng; Huh, Nam Su [Seoul Nat' l Univ., Seoul (Korea, Republic of); Lee, Seung Gun; Park, Heung Bae [KEPCO Engineering and Construction Company, Gyeonggi (Korea, Republic of); Lee, Sung Ho [KHNP Central Research Institute, Daejeon (Korea, Republic of)

    2013-01-15

    This study investigates the crack growth behavior due to primary water stress corrosion cracking (PWSCC) in the dissimilar metal butt weld of a reactor piping using Alloy 82/182. First, detailed finite element stress analyses were performed to predict the stress distribution of the dissimilar metal butt weld in which the hydrostatic and the normal operating loads as well as the weld residual stresses were considered to evaluate the stress redistribution due to mechanical loadings. Based on the stress distributions along the wall thickness of the dissimilar metal butt weld, the crack growth behavior of the postulated axial and circumferential cracks were predicted, from which the crack growth diagram due to PWSCC was proposed. The present results can be applied to predict the crack growth rate in the dissimilar metal butt weld of reactor piping due to PWSCC.

  11. Probabilistic Lifetime Assessment of Marine Reinforced Concrete with Steel Corrosion and Cover Cracking

    Institute of Scientific and Technical Information of China (English)

    LU Chun-hua; JIN Wei-liang; LIU Rong-gui

    2011-01-01

    In order to study the durability behavior of marine reinforced concrete structure suffering from chloride attack, the structural service life is assumed to be divided into three critical stages, which can be characterized by steel corrosion and cover cracking. For each stage, a calculated model used to predict the lifetime is developed. Based on the definition of durability limit state, a probabilistic lifetime model and its time-dependent reliability analytical method are proposed considering the random natures of influencing factors. Then, the probabilistic lifetime prediction models are applied to a bridge pier located in the Hangzhou Bay with Monte Carlo simulation. It is found that the time to corrosion initiation to follows a lognonnal distribution, while that the time from corrosion initiation to cover cracking t and the time for crack to develop from hairline crack to a limit crack width t can be described by Weibull distributions. With the permitted failure probability of 5.0%, it is also observed that the structural durability lifetime mainly depends on the durability life to and that the percentage of participation of tbe life t to the total service life grows from 61.5% to 83.6% when the cover thickness increases from 40 mm to 80 mm. Therefore, for any part of the marine RC bridge, the lifetime predictions and maintenance efforts should also be directed toward controlling the stage of corrosion initiation induced by chloride ion.

  12. Assessment of NDE Technologies for Detection and Characterization of Stress Corrosion Cracking in LWRs

    Energy Technology Data Exchange (ETDEWEB)

    Meyer, Ryan M.; Ramuhalli, Pradeep; Toloczko, Mychailo B.; Bond, Leonard J.; Montgomery, Robert O.

    2012-12-31

    Stress corrosion cracking (SCC) in light water reactors (LWRs) has been a persistent form of degradation in the nuclear industry. Examples of SCC can be found for a range of materials in boiling and pressurized water reactor environments, including carbon steels, stainless steels, and nickel-base stainless alloys. The evolution of SCC is often characterized by a long initiation stage followed by a phase of more rapid crack growth to failure. This provides a relatively short window of opportunity to detect the start of observable SCC, and it is conceivable that SCC could progress from initiation to failure between subsequent examinations when managed by applying periodic in-service inspection techniques. Implementation of advanced aging management paradigms in the current fleet of LWRs will require adaptation of existing measurement technologies and development of new technologies to perform on-line measurements during reactor operation to ensure timely detection of material degradation and to support the implementation of advanced diagnostics and prognostics. This paper considers several non-destructive examination (NDE) technologies with known sensitivity to detection of indicators for SCC initiation and/or propagation, and assesses these technologies with respect to their ability to detect and accurately characterize the significance of an SCC flaw. Potential strategies to improve SCC inspection or monitoring performance are offered to benefit management of SCC degradation in LWRs.

  13. Effect of Stress Ratio on Fatigue Crack Growth Rate at Notched Hole in 7075-T6 Aluminum Alloy Under Biaxial Fatigue

    Science.gov (United States)

    2016-08-18

    crack tips. The crack growth rate was observed using optical microscopy. In addition, the test generates more accurate definition of the Walker...48 xvi List of Symbols Symbol Definition a crack length (mm) α angle between the y-axis and the...of loads and moments in different directions. And that not in an ideal environment, corrosive environment while enhance and accelerate the crack

  14. Parameters influencing the transgranular stress corrosion cracking behaviour of austenitic stainless steels in systems conveying reactor coolant

    Energy Technology Data Exchange (ETDEWEB)

    Kilian, R.; Wesseling, U. [Framatome ANP (Germany); Wachter, O. [E.ON Kernkraft (Germany); Widera, M. [RWE Power (Germany); Brummer, G. [HEW - (Germany); Ilg, U. [EnBW - (Germany)

    2002-07-01

    During replacement of an auxiliary system in the German PWR KKS (NPP Stade) a damage was detected in a valve housing and in the connected piping both made from stabilised austenitic stainless steel. During operation stagnant conditions are present in this area. Based on the failure analysis chloride induced stress corrosion cracking (SCC) was found as the dominating root cause. In the open literature many cases of corrosion observed in the water/steam interface in valve components as well as in adjacent portions of auxiliary circuits made of un-stabilized stainless steels are mentioned. A common feature of the reported cases is that transgranular cracking was found. Extensive laboratory investigations revealed that non-stabilised austenitic stainless steels are also sensitive to transgranular cracking in boric acid solutions particularly in concentrated solutions. Often these solutions are contaminated with chlorides and/or oxygen is present. Taking into account the literature data the question could arise whether the above mentioned cracking may be also caused by boric acid attack. Thus, for stabilised stainless steels laboratory exposure tests at 80 C in saturated aerated boric acid solution and at 300 C in (at 100 C) saturated, oxygen free boric acid solution have been performed. Double-U-bend specimens and wedge loaded 1T-CT specimens made of Ti- and Nb-stabilised austenitic stainless steels were used. The results revealed no evidence of crack initiation and crack growth. Based on the laboratory results and the literature data an attempt is undertaken to separate parameters influencing chloride induced SCC from the effect of boric acid. (authors)

  15. Effects of Aqueous Solutions on the Slow Crack Growth of Soda-Lime-Silicate Glass

    Science.gov (United States)

    Hausmann, Bronson D.; Salem, Jonathan A.

    2016-01-01

    The slow crack growth (SCG) parameters of soda-lime-silicate were measured in distilled and saltwater of various concentrations in order to determine if the presence of salt and the contaminate formation of a weak sodium film affects stress corrosion susceptibility. Past research indicates that solvents affect the rate of crack growth; however, the effects of salt have not been studied. The results indicate a small but statistically significant effect on the SCG parameters A and n at high concentrations; however, for typical engineering purposes, the effect can be ignored.

  16. Partial discharge-induced crack growth in dielectric materials

    Institute of Scientific and Technical Information of China (English)

    2010-01-01

    Partial discharge(PD) of an air-filled semi-permeable crack in a dielectric material is studied based on the streamer-type discharge mechanism to explore the effects of applied mechanical-electric fields on crack growth.Within the frame of two-dimensional deformation,the electric field inside the crack is first derived by taking the crack deformation into account.Then,the effects of electric field before PD are discussed through considering the contribution of the induced electric field inside the deformed crack space to the total energy release rate.Finally,PD and its effects on crack growth are investigated.It is found that:(1) before PD,the applied electric field always retards crack growth;(2) during PD,the applied electric field can induce crack growth in dielectric materials.

  17. On fatigue crack growth in ductile materials by crack-tip blunting

    DEFF Research Database (Denmark)

    Tvergaard, Viggo

    2004-01-01

    One of the basic mechanisms for fatigue crack growth in ductile metals is that depending on crack-tip blunting under tensile loads and re-sharpening of the crack-tip during unloading. In a standard numerical analysis accounting for finite strains it is not possible to follow this process during...

  18. Review of environmental effects on fatigue crack growth of austenitic stainless steels.

    Energy Technology Data Exchange (ETDEWEB)

    Shack, W. J.; Kassner, T. F.; Energy Technology

    1994-07-11

    Fatigue and environmentally assisted cracking of piping, pressure vessel cladding, and core components in light water reactors are potential concerns to the nuclear industry and regulatory agencies. The degradation processes include intergranular stress corrosion cracking of austenitic stainless steel (SS) piping in boiling water reactors (BWRs), and propagation of fatigue or stress corrosion cracks (which initiate in sensitized SS cladding) into low-alloy ferritic steels in BWR pressure vessels. Crack growth data for wrought and cast austenitic SSs in simulated BWR water, developed at Argonne National Laboratory under US Nuclear Regulatory Commission sponsorship over the past 10 years, have been compiled into a data base along with similar data obtained from the open literature. The data were analyzed to develop corrosion-fatigue curves for austenitic SSs in aqueous environments corresponding to normal BWR water chemistries, for BWRs that add hydrogen to the feedwater, and for pressurized water reactor primary-system-coolant chemistry. The corrosion-fatigue data and curves in water were compared with the air line in Section XI of the ASME Code.

  19. The influence of modified water chemistries on metal oxide films, activity build-up and stress corrosion cracking of structural materials in nuclear power plants

    Energy Technology Data Exchange (ETDEWEB)

    Maekelae, K.; Laitinen, T.; Bojinov, M. [VTT Manufacturing Technology, Espoo (Finland)

    1999-03-01

    The primary coolant oxidises the surfaces of construction materials in nuclear power plants. The properties of the oxide films influence significantly the extent of incorporation of actuated corrosion products into the primary circuit surfaces, which may cause additional occupational doses for the maintenance personnel. The physical and chemical properties of the oxide films play also an important role in different forms of corrosion observed in power plants. This report gives a short overview of the factors influencing activity build-up and corrosion phenomena in nuclear power plants. Furthermore, the most recent modifications in the water chemistry to decrease these risks are discussed. A special focus is put on zinc water chemistry, and a preliminary discussion on the mechanism via which zinc influences activity build-up is presented. Even though the exact mechanisms by which zinc acts are not yet known, it is assumed that Zn may block the diffusion paths within the oxide film. This reduces ion transport through the oxide films leading to a reduced rate of oxide growth. Simultaneously the number of available adsorption sites for {sup 60}Co is also reduced. The current models for stress corrosion cracking assume that the anodic and the respective cathodic reactions contributing to crack growth occur partly on or in the oxide films. The rates of these reactions may control the crack propagation rate and therefore, the properties of the oxide films play a crucial role in determining the susceptibility of the material to stress corrosion cracking. Finally, attention is paid also on the novel techniques which can be used to mitigate the susceptibility of construction materials to stress corrosion cracking. (orig.) 127 refs.

  20. A consistent partly cracked XFEM element for cohesive crack growth

    DEFF Research Database (Denmark)

    Asferg, Jesper L.; Poulsen, Peter Noe; Nielsen, Leif Otto

    2007-01-01

    capable of modelling variations in the discontinuous displacement field on both sides of the crack and hence also capable of modelling the case where equal stresses are present on each side of the crack. The enrichment was implemented for the 3-node constant strain triangle (CST) and a standard algorithm...... was used to solve the non-linear equations. The performance of the element is illustrated by modelling fracture mechanical benchmark tests. Investigations were carried out on the performance of the element for different crack lengths within one element. The results are compared with previously obtained...

  1. Crack Tip Plasticity Associated with Corrosion Assisted Fatigue.

    Science.gov (United States)

    1982-11-15

    growing. The model presented is very similar to those previously developed by Antolovich , Saxena and I Chanani[83 and by Lanteigne and BailonE9] but...in crack tip plasticity associated with environment. The model used here is conceptually similar to those formulated by * Antolovich , et al,[ and...Lankford, J. ’Fatigue-Crack-Tip I Plastic Strains by the Stereoimaging Technique’ Exp. Mech. 1980 20, 3 134-139. 8. Antolovich , S. D., Saxena, A., and

  2. Fundamental understanding and life prediction of stress corrosion cracking in BWRs and energy systems

    Energy Technology Data Exchange (ETDEWEB)

    Andresen, P.L.; Ford, F.P. [General Electric, Schenectady, NY (United States). Corporate Research and Development Center

    1998-03-01

    The objective of this paper is to present an approach for design and lifetime evaluation of environmental cracking based on experimental and fundamental modeling of the underlying processes operative in crack advance. In detailed this approach and its development and quantification for energy (hot water) systems, the requirements for a life prediction methodology will be highlighted and the shortcomings of the existing design and lifetime evaluation codes reviewed. Examples are identified of its use in a variety of cracking systems, such as stainless steels, low alloy steels, nickel base alloys, and irradiation assisted stress corrosion cracking in boiling water reactor (BWR) water, as well as preliminary use for low alloy steel and Alloy 600 in pressurized water reactors (PWRs) and turbine steels in steam turbines. Identification of the common aspects with environmental cracking in other hot water systems provides a secure basis for its extension to related energy systems. 166 refs., 49 figs.

  3. Modeling of concrete cracking due to corrosion process of reinforcement bars

    Energy Technology Data Exchange (ETDEWEB)

    Bossio, Antonio, E-mail: antonio.bossio@unina.it [Department of Chemical Engineering, Materials and Production, University of Naples “Federico II”, Napoli, Piazzale V. Tecchio 80, I-80125 Italy (Italy); Monetta, Tullio, E-mail: monetta@unina.it [Department of Chemical Engineering, Materials and Production, University of Naples “Federico II”, Napoli, Piazzale V. Tecchio 80, I-80125 Italy (Italy); Bellucci, Francesco, E-mail: bellucci@unina.it [Department of Chemical Engineering, Materials and Production, University of Naples “Federico II”, Napoli, Piazzale V. Tecchio 80, I-80125 Italy (Italy); Lignola, Gian Piero, E-mail: glignola@unina.it [Department of Structures for Engineering and Architecture, University of Naples “Federico II”, Via Claudio 21, I-80125 Napoli (Italy); Prota, Andrea, E-mail: aprota@unina.it [Department of Structures for Engineering and Architecture, University of Naples “Federico II”, Via Claudio 21, I-80125 Napoli (Italy)

    2015-05-15

    The reinforcement corrosion in Reinforced Concrete (RC) is a major reason of degradation for structures and infrastructures throughout the world leading to their premature deterioration before design life was attained. The effects of corrosion of reinforcement are: (i) the reduction of the cross section of the bars, and (ii) the development of corrosion products leading to the appearance of cracks in the concrete cover and subsequent cover spalling. Due to their intrinsic complex nature, these issues require an interdisciplinary approach involving both material science and structural design knowledge also in terms on International and National codes that implemented the concept of durability and service life of structures. In this paper preliminary FEM analyses were performed in order to simulate pitting corrosion or general corrosion aimed to demonstrate the possibility to extend the results obtained for a cylindrical specimen, reinforced by a single bar, to more complex RC members in terms of geometry and reinforcement. Furthermore, a mechanical analytical model to evaluate the stresses in the concrete surrounding the reinforcement bars is proposed. In addition, a sophisticated model is presented to evaluate the non-linear development of stresses inside concrete and crack propagation when reinforcement bars start to corrode. The relationships between the cracking development (mechanical) and the reduction of the steel section (electrochemical) are provided. Finally, numerical findings reported in this paper were compared to experimental results available in the literature and satisfactory agreement was found.

  4. Fatigue crack growth retardation in spot heated mild steel sheet

    Indian Academy of Sciences (India)

    B B Verma; P K Ray

    2002-08-01

    A fatigue crack can be effectively retarded by heating a spot near the crack tip under nil remote stress condition. The subcritical spot heating at a proper position modifies the crack growth behaviour in a way, more or less, similar to specimen subjected to overload spike. It is observed that the extent of crack growth retardation increases with increasing level of overload as well as with increasing spot temperature. It is also observed that modification in crack growth behaviour is a function of location of heating spot and maximum retardation is observed at + 5 position.

  5. Cracking process of Fe-26Cr-1Mo during low cycle corrosion fatigue

    Energy Technology Data Exchange (ETDEWEB)

    Wang, J.Q.; Li, J.; Wang, Z.F.; Zhu, Z.Y.; Ke, W. (Academia Sinica, Shenyang (China). Corrosion Science Lab.); Zang, Q.S.; Wang, Z.G. (Academia Sinica, Shenyang (China). State Key Lab. for Fatigue and Fracture of Materials)

    1994-12-01

    The corrosion fatigue (CF) life has been divided classically into the initiation'' and propagation'' periods. Usually, the crack initiation process dominates the component lifetime under the low cycle CF condition because the crack propagates rapidly one initiated. Despite much work done on the research of the CF crack initiation mechanisms, however, a full understanding of crack initiation is still lacking. There are some limitations in explaining the CF crack initiation in an aqueous solution using the above four mechanisms individually. And, it is difficult to conduct experiments in which one mechanism along can be examined. Although CF is complicated, it is possible to reproduce a specific experiment condition which will have the dominant factor affecting the CF crack initiation. Once the cracks initiate on the smooth metal surface, their coalescence, micropropagation and macropropagation will take place successively. The initiated cracks propagate first in the range of several grains, and the behavior of the microcrack propagation is different from that of macrocrack propagation. For Fe-26Cr-1Mo ferritic stainless steel, the fundamental research work of straining electrode has been done by many investigators, but the observation of the material surface at different deformation processes has not been reported. In the present study, the detailed observation of the cracking process of the material has been carried out in low cycle CF.

  6. Stress corrosion crack initiation of alloy 182 weld metal in primary coolant - Influence of chemical composition

    Energy Technology Data Exchange (ETDEWEB)

    Calonne, O.; Foucault, M.; Steltzlen, F. [AREVA (France); Amzallag, C. [EDF SEPTEN (France)

    2011-07-01

    Nickel-base alloys 182 and 82 have been used extensively for dissimilar metal welds. Typical applications are the J-groove welds of alloy 600 vessel head penetrations, pressurizer penetrations, heater sleeves and bottom mounted instrumented nozzles as well as some safe end butt welds. While the overall performance of these weld metals has been good, during the last decade, an increasing number of cases of stress corrosion cracking of Alloy 182 weld metal have been reported in PWRs. In this context, the role of weld defects has to be examined. Their contribution in the crack initiation mechanism requires laboratory investigations with small scale characterizations. In this study, the influence of both alloy composition and weld defects on PWSCC (Stress Corrosion Cracking in Primary Water) initiation was investigated using U-bend specimens in simulated primary water at 320 C. The main results are the following: -) the chemical compositions of the weld deposits leading to a large propensity to hot cracking are not the most susceptible to PWSCC initiation, -) macroscopically, superficial defects did not evolve during successive exposures. They can be included in large corrosion cracks but their role as 'precursors' is not yet established. (authors)

  7. Role of pH on the stress corrosion cracking of titanium alloys

    Science.gov (United States)

    Khokhar, M. I.; Beck, F. H.; Fontana, M. G.

    1973-01-01

    Stress corrosion cracking (SCC) experiments were conducted on Ti-8-1-1 wire specimens in hydrochloric and sulfuric acids of variable pH in order to determine the effect of pH on the susceptibility to cracking. The alloy exhibited increasing susceptibility with decreasing pH. By varying the applied potential, it was observed that susceptibility zones exist both in the cathodic and the anodic ranges. In the cathodic range, susceptibility also increased with decreasing applied potential. Corrosion potential-time data in hydrochloric acid (pH 1.7) and sulfuric acid (pH 1.7) indicate that chloride ions lower the corrosion potential of the specimen which, in turn, increases the susceptibility.

  8. Role of pH on the stress corrosion cracking of titanium alloys

    Science.gov (United States)

    Khokhar, M. I.; Beck, F. H.; Fontana, M. G.

    1973-01-01

    Stress corrosion cracking (SCC) experiments were conducted on Ti-8-1-1 wire specimens in hydrochloric and sulfuric acids of variable pH in order to determine the effect of pH on the susceptibility to cracking. The alloy exhibited increasing susceptibility with decreasing pH. By varying the applied potential, it was observed that susceptibility zones exist both in the cathodic and the anodic ranges. In the cathodic range, susceptibility also increased with decreasing applied potential. Corrosion potential-time data in hydrochloric acid (pH 1.7) and sulfuric acid (pH 1.7) indicate that chloride ions lower the corrosion potential of the specimen which, in turn, increases the susceptibility.

  9. NASCRAC - A computer code for fracture mechanics analysis of crack growth

    Science.gov (United States)

    Harris, D. O.; Eason, E. D.; Thomas, J. M.; Bianca, C. J.; Salter, L. D.

    1987-01-01

    NASCRAC - a computer code for fracture mechanics analysis of crack growth - is described in this paper. The need for such a code is increasing as requirements grow for high reliability and low weight in aerospace components. The code is comprehensive and versatile, as well as user friendly. The major purpose of the code is calculation of fatigue, corrosion fatigue, or stress corrosion crack growth, and a variety of crack growth relations can be selected by the user. Additionally, crack retardation models are included. A very wide variety of stress intensity factor solutions are contained in the code, and extensive use is made of influence functions. This allows complex stress gradients in three-dimensional crack problems to be treated easily and economically. In cases where previous stress intensity factor solutions are not adequate, new influence functions can be calculated by the code. Additional features include incorporation of J-integral solutions from the literature and a capability for estimating elastic-plastic stress redistribution from the results of a corresponding elastic analysis. An example problem is presented which shows typical outputs from the code.

  10. Stress corrosion cracking in low-pressure turbine discs in an NaCl solution

    Energy Technology Data Exchange (ETDEWEB)

    Hitomi, Itoh [Mitsubishi Heavy Industries, Ltd., Takasago Research and Development Center (Japan); Takashi, Momoo [Mitsubishi Heavy Industries, Ltd., Takasago Machinery Works (Japan)

    2001-07-01

    From past research, it is known that stress corrosion cracking in low-pressure turbine discs occurs in an environment near that of deaerated pure water. Nevertheless, in units with molar ratio control, there is a possibility of NaCl concentrating as an impurity in the dry/wet boundary region. Long-term immersion tests were conducted at 373 K to 473 K with the NaCl concentration predicted to become 5%. It was found that, when FeCl{sub 3} or other oxidizer was added, corrosion increased remarkably and SCC was initiated. When cracks were initiated, they were primarily transgranular; as the test temperature was decreased, initiation was accelerated but conversely crack propagation was reduced. (author)

  11. Fatigue crack growth in additive manufactured products

    Directory of Open Access Journals (Sweden)

    A. Riemer

    2015-10-01

    Full Text Available Additive Manufacturing (AM is a new innovative technique that allows the direct fabrication of complex, individual, delicate and high-strength products, based on their 3D data. Selective Laser Melting (SLM is one of the AM processes that generates metallic components layer by layer using powder-bed technique. The irradiation and consequent melting of metallic powder is realised by the laser source. Employing SLM, especially complex and individual products, such as implants or aerospace parts, are well suited for economic production in small batches. The first important issue in this work was to analyse the fatigue crack growth (FCG in titanium alloy Ti-6-4 and stainless steel 316L processed by SLM. As a first step, stress intensity range decreasing tests were performed on SLM samples in their “as-built” condition. The next step was to adopt measures for optimisation of fatigue crack growth performance of SLM parts. For this purpose various heat treatments such as stress relief annealing and hot isostatic pressing (HIP were applied to the CT specimens. Finally, the strong impact of heat treatment on the residual lifetime was demonstrated by numerical fatigue crack growth simulations. For this purpose, the hip joint implant consisting of Ti-6-4 and processed by SLM was taken into account. It was found that residual stresses have a strong influence on the crack growth in Ti-6-4, while the influence of the micro-pores on the threshold values remains low. In contrast the results for 316L show that its fracturemechanical behaviour is not affected by residual stresses, whereas the microstructural features lead to modification in the da/dN-K-data. The second fundamental aim of this work was to demonstrate the possibilities of the SLM process. For that reason, the individually tailored bicycle crank was optimised regarding its weight and local stresses and finally manufactured using the SLM system. The iterative optimisation procedure was based on

  12. A cohesive segments method for the simulation of crack growth

    NARCIS (Netherlands)

    Remmers, J.J.C.; De Borst, R.; Needleman, A.

    2003-01-01

    A numerical method for crack growth is described in which the crack is not regarded as a single discontinuity that propagates continuously. Instead, the crack is represented by a set of overlapping cohesive segments. These cohesive segments are inserted into finite elements as discontinuities in the

  13. Characterisation of Fatigue Crack Growth in Silicone for Deap Technology

    DEFF Research Database (Denmark)

    Thorup, Thor

    2012-01-01

    In this paper, the fatigue crack growth characteristics of Elastosil R RT 625 are determined by performing fatigue crack experiments based on ISO 27727. Elastosil R RT 625 is a silicone rubber used by Danfoss PolyPower A/S as the dielectric material in their DEAP elements. Cracks were characteris...

  14. Laboratory evaluation of soil stress corrosion cracking and hydrogen embrittlement of API grade steels

    Energy Technology Data Exchange (ETDEWEB)

    Bueno, A.H.S.; Castro, B.B.; Ponciano, J.A.C. [Federal Univ. of Rio de Janeiro (Brazil). COPPE

    2004-07-01

    Stress corrosion cracking (SCC) in carbon steels is a form of deterioration that can occur during the service life of a pipeline that is exposed to mechanical stress and strains. A study was conducted to investigate SCC and hydrogen embrittlement (HE) of API grade steels in contact with soil. The physical, chemical and bacteriological characteristics of different soil samples were determined. Slow strain rate tests were performed using electrolytes obtained in the soil samples taken from different points near buried pipelines. Stress versus strain curves were obtained at different electrode potentials for API X46, X60 and X80 steels. The results showed the conjoint incidence of SCC and HE, depending on the potential imposed. It was revealed that HE contributes to the initiation of cracking and crack propagation. Cracking morphology was similar to the SCC found in field situations where transgranular cracking was detected in a pipeline that had collapsed as a result of land creeping. The material exhibited signs of secondary cracking and lower ductility, even under cathodic potentials. It was noted that the methodology used in this study was not able to reproduce the possible effect of microbial induced corrosion. 10 refs., 3 tabs., 3 figs.

  15. Fatigue crack growth in an aluminum alloy-fractographic study

    Science.gov (United States)

    Salam, I.; Muhammad, W.; Ejaz, N.

    2016-08-01

    A two-fold approach was adopted to understand the fatigue crack growth process in an Aluminum alloy; fatigue crack growth test of samples and analysis of fractured surfaces. Fatigue crack growth tests were conducted on middle tension M(T) samples prepared from an Aluminum alloy cylinder. The tests were conducted under constant amplitude loading at R ratio 0.1. The stress applied was from 20,30 and 40 per cent of the yield stress of the material. The fatigue crack growth data was recorded. After fatigue testing, the samples were subjected to detailed scanning electron microscopic (SEM) analysis. The resulting fracture surfaces were subjected to qualitative and quantitative fractographic examinations. Quantitative fracture analysis included an estimation of crack growth rate (CGR) in different regions. The effect of the microstructural features on fatigue crack growth was examined. It was observed that in stage II (crack growth region), the failure mode changes from intergranular to transgranular as the stress level increases. In the region of intergranular failure the localized brittle failure was observed and fatigue striations are difficult to reveal. However, in the region of transgranular failure the crack path is independent of the microstructural features. In this region, localized ductile failure mode was observed and well defined fatigue striations were present in the wake of fatigue crack. The effect of interaction of growing fatigue crack with microstructural features was not substantial. The final fracture (stage III) was ductile in all the cases.

  16. Hydrogen-related stress corrosion cracking in line pipe steel

    DEFF Research Database (Denmark)

    Nielsen, Lars Vendelbo

    1997-01-01

    A correlation between hydrogen concentration (C0) and the critical stress intensity factor for propagation of hydrogen-related cracks has been established by fracture mechanical testing of CT-specimens for the heat affected zone of an X-70 pipeline steel. This has been compared with field...

  17. Numerical simulations of material mismatch and ductile crack growth

    Energy Technology Data Exchange (ETDEWEB)

    Oestby, Erling

    2002-07-01

    Both the global geometry and inhomogeneities in material properties will influence the fracture behaviour of structures in presence of cracks. In this thesis numerical simulations have been used to investigate how some aspects of both these issues affect the conditions at the crack-tip. The thesis is organised in an introduction chapter, summarising the major findings and conclusions, a review chapter, presenting the main aspects of the developments in the field of fracture mechanics, and three research papers. Paper I considers the effect of mismatch in hardening exponent on the local near-tip stress field for stationary interface cracks in bi-materials under small scale yielding conditions. It is demonstrated that the stress level in the weaker material increases compared to what is found in the homogeneous material for the same globally applied load level, with the effect being of increasing importance as the crack-tip is approached. Although a coupling between the radial and angular dependence of the stress fields exists, the evolving stress field can still be normalised with the applied J. The effect on the increase in stress level can closely be characterised by the difference in hardening exponent, {delta}n, termed the hardening mismatch, and is more or less independent of the absolute level of hardening in the two materials. Paper II and Ill deal with the effects of geometry, specimen size, hardening level and yield stress mismatch in relation to ductile crack growth. The ductile crack growth is simulated through use of the Gurson model. In Paper H the effect of specimen size on the crack growth resistance is investigated for deep cracked bend and shallow cracked tensile specimens. At small amounts of crack growth the effect of specimen size on the crack growth resistance is small, but a more significant effect is found for larger amounts of crack growth. The crack growth resistance decreases in smaller specimens loaded in tension, whereas the opposite is

  18. Inhibition of Ce3+ on Stress Corrosion Crack of High Strength Aluminum Alloy

    Directory of Open Access Journals (Sweden)

    LI Wen-ting

    2017-05-01

    Full Text Available The stress corrosion cracking (SCC susceptibility of 7A04 high strength aluminum alloy in 3.5% (mass fraction NaCl solution and the Ce3+ inhibition of SCC were investigated by slow stress rate test(SSRT, using constant current polarization, electrochemical noise (ECN and electrochemical impedance spectroscopy (EIS techniques. The inhibition mechanism of Ce3+ ions on the initiation and propagation of cracking was also analyzed. The results indicate that both anodic and cathodic galvanostatic polarizations can accelerate the SCC of 7A04, the former increases anodic dissolution but the latter accelerates hydrogen embrittlement of crack tip. SCC susceptibility of 7A04 can be reduced effectively by the addition of cerium ions, the fracture time is delayed and slowed down, but only during the initiation other than the propagation stage of cracking. Ce3+ ions can restrain the initiation of metastable pitting on the surface of 7A04 specimen, which therefore increase the induction time of the cracking since that the micro pits are usually the source of cracking.However, once the crack begins to propagate or the specimen is notched, the addition of cerium ions can rarely inhibit the cracking process. This is possibly attributed to that the radius of Ce3+ ion is too large to diffuse into the crack tip or it is hard to form protective CeO2 layer, Ce3+ ion therefore fails to rehabilitate the active alloy at the crack tip and further reduce the SCC developing rate of 7A04. SEM also indicates that the crack initiation of smooth 7A04 specimens is mainly induced by metastable or stable pits.

  19. Stress Corrosion Cracking of Zircaloy-4 in Halide Solutions: Effect of Temperature

    Directory of Open Access Journals (Sweden)

    Farina S.B.

    2002-01-01

    Full Text Available Zircaloy-4 was found to be susceptible to stress corrosion cracking in 1 M NaCl, 1 M KBr and 1 M KI aqueous solutions at potentials above the pitting potential. In all the solutions tested crack propagation was initially intergranular and then changed to transgranular. The effect of strain rate and temperature on the SCC propagation was investigated. An increase in the strain rate was found to lead to an increase in the crack propagation rate. The crack propagation rate increases in the three solutions tested as the temperatures increases between 20 and 90 °C. The Surface-Mobility SCC mechanism accounts for the observation made in the present work, and the activation energy predicted in iodide solutions is similar to that found in the literature.

  20. Chloride stress corrosion cracking of Alloy 600 in boric acid solutions

    Energy Technology Data Exchange (ETDEWEB)

    Berge, Ph. [Electricite de France, 92 - Paris la Defense (France); Noel, D.; Gras, J.M.; Prieux, B. [Electricite de France, 77 - Moret-sur-Loing (France). Direction des Etudes et Recherches

    1997-10-01

    The high nickel austenitic alloys are generally considered to have good resistance to chloride stress corrosion cracking. In the standard boiling magnesium chloride solution tests, alloys with more than 40% nickel are immune. Nevertheless, more recent data show that cracking can occur in both Alloys 600 and 690 if the solution is acidified. In other low pH media, such as boric acid solution at 100 deg C, transgranular and intergranular cracking are observed in Alloy 600 in the presence of minor concentrations of sodium chloride (2g/I). In concentrated boric acid at higher temperatures (250 and 290 deg C), intergranular cracking also occurs, either when the chloride concentration is high, or at low chloride contents and high oxygen levels. The role of pH and a possible specific action of boric acid are discussed, together with the influence of electrochemical potential. (author) 21 refs.

  1. Stress-corrosion cracking of sensitized stainless steel by sulfur-containing compounds

    Energy Technology Data Exchange (ETDEWEB)

    Isaacs, H.S.; Vyas, B.; Kendig, M.W.

    1981-01-01

    The stress corrosion cracking (SCC) of sensitized Type 304 stainless steel in thiosulfate solutions has been studied using constant extension rate tests. Very low concentrations of about 6.10/sup -7/M Na/sub 2/S/sub 2/O/sub 3/ (0.1ppm) gave cracking. With boric acid added, higher concentrations (1ppm) were required. The SCC was shown to be electrochemically controlled. Below -0.5v/sub SCE/ (-0.75/sub SHE/) no SCC took place; above this potential the rate of SCC increased with potential. An induction period was required before SCC continued above -0.5v if the potential was held at or below this value for extended times. This period was associated with the build up of an aggressive solution of thiosulfate decomposition products within the crack. The cracking process has been considered to be controlled by rupture of a salt layer and not a passivating oxide.

  2. Hydrogen embrittlement and hydrogen induced stress corrosion cracking of high alloyed austenitic materials; Wasserstoffversproedung und wasserstoffinduzierte Spannungsrisskorrosion hochlegierter austenitischer Werkstoffe

    Energy Technology Data Exchange (ETDEWEB)

    Mummert, K.; Uhlemann, M.; Engelmann, H.J. [Institut fuer Festkoerper- und Werkstofforschung Dresden e.V. (Germany)

    1998-11-01

    The susceptiblity of high alloyed austenitic steels and nickel base alloys to hydrogen-induced cracking is particularly determined by 1. the distribution of hydrogen in the material, and 2. the microstructural deformation behaviour, which last process is determined by the effects of hydrogen with respect to the formation of dislocations and the stacking fault energy. The hydrogen has an influence on the process of slip localization in slip bands, which in turn affects the microstructural deformation behaviour. Slip localization increases with growing Ni contents of the alloys and clearly reduces the ductility of the Ni-base alloy. Although there is a local hydrogen source involved in stress corrosion cracking, emanating from the corrosion process at the cathode, crack growth is observed only in those cases when the hydrogen concentration in a small zone ahead of the crack tip reaches a critical value with respect to the stress conditions. Probability of onset of this process gets lower with growing Ni content of the alloy, due to increasing diffusion velocity of the hydrogen in the austenitic lattice. This is why particularly austenitic steels with low Ni contents are susceptible to transcrystalline stress corrosion cracking. In this case, the microstructural deformation process at the crack tip is also influenced by analogous processes, as could be observed in hydrogen-loaded specimens. (orig./CB) [Deutsch] Die Empfindlichkeit von hochlegierten austentischen Staehlen und Nickelbasislegierungen gegen wasserstoffinduziertes Risswachstum wird im wesentlichen bestimmt durch 1. die Verteilung von Wasserstoff im Werkstoff und 2. das mikrostrukturelle Verformungsverhalten. Das mikrostrukturelle Deformationsverhalten ist wiederum durch den Einfluss von Wasserstoff auf die Versetzungsbildung und die Stapelfehlerenergie charakterisiert. Das mikrostrukturelle Verformungsverhalten wird durch wasserstoffbeeinflusste Gleitlokalisierung in Gleitbaendern bestimmt. Diese nimmt mit

  3. Electro chemical studies on stress corrosion cracking of Incoloy-800 in caustic solution, part I: As received samples

    Directory of Open Access Journals (Sweden)

    Dinu Alice

    2005-01-01

    Full Text Available Many non-volatile impurities accidentally introduced into the steam generator tend to Concentrate on its surface in restricted flow areas. In this way these impurities can lead to stress corrosion cracking (SCC on stressed tubes of the steam generator. Such impurities can be strong alkaline or acid solutions. To evaluate the effect of alkaline concentrated environments on SCC of steam generator tubes, the tests were con ducted on stressed samples of Incoloy-800 in 10% NaOH solution. To accelerate the SCC process, stressed specimens were anodically polarised in a caustic solution in an electro chemical cell. The method of stressing of Incoloy-800 tubes used in our experiments was the C-ring. Using the cathodic zone of the potentiodynamic curves it was possible to calculate the most important electrochemical parameters: the corrosion current, the corrosion rate, and the polarization resistance. We found that the value of the corrosion potential to initiate the SCC microcracks was -100 mV. The tested samples were examined using the metallographic method. The main experimental results showed that the in crease of the stress state promoted the in crease of the SCC susceptibility of Incoloy-800 samples tested under the same conditions, and that the length of the SCC-type microcracks in creased with the growth of the stress value.

  4. Stochastic modeling of thermal fatigue crack growth

    CERN Document Server

    Radu, Vasile

    2015-01-01

    The book describes a systematic stochastic modeling approach for assessing thermal-fatigue crack-growth in mixing tees, based on the power spectral density of temperature fluctuation at the inner pipe surface. It shows the development of a frequency-temperature response function in the framework of single-input, single-output (SISO) methodology from random noise/signal theory under sinusoidal input. The frequency response of stress intensity factor (SIF) is obtained by a polynomial fitting procedure of thermal stress profiles at various instants of time. The method, which takes into account the variability of material properties, and has been implemented in a real-world application, estimates the probabilities of failure by considering a limit state function and Monte Carlo analysis, which are based on the proposed stochastic model. Written in a comprehensive and accessible style, this book presents a new and effective method for assessing thermal fatigue crack, and it is intended as a concise and practice-or...

  5. Stress Corrosion Cracking of an Austenitic Stainless Steel in Nitrite-Containing Chloride Solutions

    Directory of Open Access Journals (Sweden)

    R. K. Singh Raman

    2014-12-01

    Full Text Available This article describes the susceptibility of 316L stainless steel to stress corrosion cracking (SCC in a nitrite-containing chloride solution. Slow strain rate testing (SSRT in 30 wt. % MgCl2 solution established SCC susceptibility, as evidenced by post-SSRT fractography. Addition of nitrite to the chloride solution, which is reported to have inhibitive influence on corrosion of stainless steels, was found to increase SCC susceptibility. The susceptibility was also found to increase with nitrite concentration. This behaviour is explained on the basis of the passivation and pitting characteristics of 316L steel in chloride solution.

  6. Time-dependent corrosion fatique crack propagation in 7000 series aluminum alloys. M.S. Thesis

    Science.gov (United States)

    Mason, Mark E.

    1995-01-01

    The goal of this research is to characterize environmentally assisted subcritical crack growth for the susceptible short-longitudinal orientation of aluminum alloy 7075-T651, immersed in acidified and inhibited NaCl solution. This work is necessary in order to provide a basis for incorporating environmental effects into fatigue crack propagation life prediction codes such as NASA-FLAGRO (NASGRO). This effort concentrates on determining relevant inputs to a superposition model in order to more accurately model environmental fatigue crack propagation.

  7. Effect of Sensitization on Corrosion-Fatigue Cracking in Al 5083 Alloy

    Science.gov (United States)

    2015-01-21

    1% NaCl solution, the observed environmental effects on fatigue crack growth can be explained by the hydrogen embrittlement mechanism and are...using a superposition model and a two-parameter approach to environment- assisted cracking . The superposition model is essentially a summation of...Metall. Trans. A. Vol. 11A, 1980, pp. 151-158. 15. A. Bonakdar, F. Wang, J.J. Williams, and N. Chawla, “ Environmental Effects on Fatigue Crack

  8. Statistical model of stress corrosion cracking based on extended form of Dirichlet energy

    Indian Academy of Sciences (India)

    Harry Yosh

    2013-12-01

    The mechanism of stress corrosion cracking (SCC) has been discussed for decades. Here I propose a model of SCC reflecting the feature of fracture in brittle manner based on the variational principle under approximately supposed thermal equilibrium. In that model the functionals are expressed with extended forms of Dirichlet energy, and Dirichlet principle is applied to them to solve the variational problem that represents SCC and normal extension on pipe surface. Based on the model and the maximum entropy principle, the statistical nature of SCC colony is discussed and it is indicated that the crack has discrete energy and length under ideal isotropy of materials and thermal equilibrium.

  9. Corrosion-Fatigue Cracking in HY-80 and HY-130 Steels

    Science.gov (United States)

    2015-01-22

    on HY80 steel and HY-130 steel are shown in Fig. A-13 through A-16 for various specimens tested at different load ratios and environments. Because...Naval Research Laboratory Washington, DC 20375-5320 NRL/MR/6355--15-9584 Corrosion-Fatigue Cracking in HY-80 and HY-130 Steels January 22, 2015 P.S...Cracking in HY-80 and HY-130 Steels P.S. Pao and R.L. Holtz Naval Research Laboratory 4555 Overlook Avenue, SW Washington, DC 20375-5328 Office of Naval

  10. A phenomenological study of initiation and propagation of stress corrosion cracks. Application to AISI 304L stainless steel in magnesium chloride; Etude phenomenologique de l`amorcage et de la propagation de fissures de corrosion sous contraintes. Application a l`acier inoxydable Z 2CN 18.10 dans le chlorure de magnesium

    Energy Technology Data Exchange (ETDEWEB)

    Peyrat, C.; Raquet, O.; Helie, M.; Santarini, G. [CEA Fontenay-aux-Roses, 92 (France). Service de la Corrosion, d`Electrochimie et Chimie des Fluides

    1999-04-01

    A purely phenomenological study of Stress Corrosion Cracking (SCC) was performed using the couple AISI 304L austenitic stainless steel/boiling magnesium chloride aqueous solution. The exploitation of the morphological information (shape of the cracks and size distribution) available after constant elongation rate tests led to the apparent initiation of the cracks and to their growth rate. A law for the real initiation is proposed too and the elongation rate effect in quantitatively characterized. (authors) 8 refs.

  11. 49 CFR 192.929 - What are the requirements for using Direct Assessment for Stress Corrosion Cracking (SCCDA)?

    Science.gov (United States)

    2010-10-01

    ... requirements for using Direct Assessment for Stress Corrosion Cracking (SCCDA)? (a) Definition. Stress..., appendix A3, and remediate the threat in accordance with ASME/ANSI B31.8S, appendix A3, section A3.4....

  12. Growth of inclined fatigue cracks using the biaxial CJP model

    Directory of Open Access Journals (Sweden)

    G. Laboviciute

    2015-07-01

    Full Text Available The CJP model of crack tip stresses is a modified version of the Williams crack tip stress field which takes account of simplified stress distributions that arise from the presence of a zone of plastic deformation associated with the crack flanks and crack tip, and that act on the elastic field responsible for driving crack growth. The elastic stress field responsible for crack growth is therefore controlled by the applied loading and by the induced boundary stresses at the interface with the plastic zone. This meso-scale model of crack tip stresses leads to a modified set of crack tip stress intensity factors that include the resultant influence of plastic wake-induced crack tip shielding, and which therefore have the potential to help resolve some longstanding controversies associated with plasticity-induced closure. A full-field approach has now been developed for stress using photoelasticity and also for displacement using digital image correlation. This paper considers the characterisation of crack growth rate data with the biaxial CJP model, using compact tension specimens that contain inclined cracks at the notch tip with initial angles of 30°, 45° and 60° to the horizontal axis. Significant experimental difficulties are experienced in growing cracks in a biaxial field under uniaxial tensile loading, as the natural tendency of the crack is to turn so that it becomes perpendicular to the maximum principal stress direction. However, crack angle is not an issue in the CJP model which calculates the stress field parallel with, and perpendicular to, the crack plane. These stress components can be rotated into directions comparable with the usual KI and KII directions and used to calculate stress intensity parameters that should be directly comparable with the standard stress intensity formulations. Another difficulty arises, however, in finding published expressions for KI and KII for CT specimens with curved or kinked cracks. The CJP model

  13. Fatigue-crack growth behavior of Type 347 stainless steels under simulated PWR water conditions

    Energy Technology Data Exchange (ETDEWEB)

    Hong, Seokmin; Min, Ki-Deuk; Yoon, Ji-Hyun; Kim, Min-Chul; Lee, Bong-Sang [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2015-10-15

    Fatigue crack growth rate (FCGR) curve of stainless steel exists in ASME code section XI, but it is still not considering the environmental effects. The longer time nuclear power plant is operated, the more the environmental degradation issues of materials pop up. There are some researches on fatigue crack growth rate of S304 and S316, but researches of FCGR of S347 used in Korea nuclear power plant are insufficient. In this study, the FCGR of S347 stainless steel was evaluated in the PWR high temperature water conditions. The FCGRs of S347 stainless steel under pressurized-water conditions were measured by using compact-tension (CT) specimens at different levels of dissolved oxygen (DO) and frequency. 1. FCGRs of SS347 were slower than that in ASME XI and environmental effect did not occur when frequency was higher than 1Hz. 2. Fatigue crack growth is accelerated by corrosion fatigue and it is more severe when frequency is slower than 0.1Hz. 3. Increase of crack tip opening time increased corrosion fatigue and it deteriorated environmental fatigue properties.

  14. Preliminary study for extension and improvement on modeling of primary water stress corrosion cracking at control rod drive mechanism nozzles of pressurized water reactors

    Energy Technology Data Exchange (ETDEWEB)

    Aly, Omar F.; Mattar Neto, Miguel M. [Instituto de Pesquisas Energeticas e Nucleares (IPEN-CNEN/SP), Sao Paulo, SP (Brazil)], e-mail: ofaly@ipen.br, e-mail: mmattar@ipen.br; Schvartzman, Monica M.M.A.M. [Centro de Desenvolvimento da Tecnologia Nuclear (CDTN), Belo Horizonte, MG (Brazil)], e-mail: monicas@cdtn.br

    2009-07-01

    This study is for to extend, to improve the existing models, and to propose a local approach to assess the primary water stress corrosion cracking in nickel-based components. It is includes a modeling of new data for Alloy 182 and new considerations about initiation and crack growth according a developing method based on EPRI-MRP-115 (2004), and USNRC NUREG/CR-6964 (2008). The experimental data is obtained from CDTN-Brazilian Nuclear Technology Development Center, by tests through slow strain rate test (SSRT) equipment. The model conception assumed is a built diagram which indicates a thermodynamic condition for the occurrence of corrosion submodes in essayed materials, through Pourbaix diagrams, for Nickel Alloys in high temperature primary water. Over them, are superimposed different models, including a semi-empiric-probabilistic one to quantify the primary water stress corrosion cracking susceptibility, and a crack growth model. These constructed models shall be validated with the experimental data. This development aims to extent some of the models obtained to weld metals like the Alloy 182, and to improve the originals obtained according methodologies exposed in above referred reports. These methodologies comprise laboratory testing procedures, data collecting, data screening, modeling procedures, assembling of data from some laboratories in the world, plotting of results, compared analysis and discussion of these results. Preliminary results for Alloy 182 will be presented. (author)

  15. The corrosion and stress corrosion cracking behavior of a novel alumina-forming austenitic stainless steel in supercritical water

    Science.gov (United States)

    Sun, Hongying; Yang, Haijie; Wang, Man; Giron-Palomares, Benjamin; Zhou, Zhangjian; Zhang, Lefu; Zhang, Guangming

    2017-02-01

    The general corrosion and stress corrosion behavior of Fe-27Ni-15Cr-5Al-2Mo-0.4Nb alumina-forming austenitic (AFA) steel were investigated in supercritical water under different conditions. A double layer oxide structure was formed: a Fe-rich outer layer (Fe2O3 and Fe3O4) and an Al-Cr-rich inner layer. And the inner layer has a low growth rate with exposing time, which is good for improvement of corrosion resistance. Additionally, some internal nodular Al-Cr-rich oxides were also observed, which resulted in a local absence of inner layer. Stress corrosion specimens exhibited a combination of high strength, good ductility and low susceptibility. The stress strength and elongation was reduced by increasing temperature and amount of dissolved oxygen. In addition, the corresponding susceptibility was increased with decreased temperatures and increased oxygen contents.

  16. Fatigue crack growth rate test using a frequency sweep method

    Institute of Scientific and Technical Information of China (English)

    Xun ZHOU; Xiao-li YU

    2008-01-01

    Fatigue crack propagation characteristics of a diesel engine crankshaft are studied by measuring the fatigue crack growth rate using a frequency sweep method on a resonant fatigue test rig. Based on the phenomenon that the system frequency will change when the crack becomes large, this method can be directly applied to a complex component or structure. Finite element analyses (FEAs) are performed to calibrate the relation between the frequency change and the crack size, and to obtain the natural frequency of the test rig and the stress intensity factor (SIF) of growing cracks. The crack growth rate i.e. da/dN-AK of each crack size is obtained by combining the testing-time monitored data and FEA results. The results show that the crack growth rate of engine crankshaft, which is a component with complex geometry and special surface treatment, is quite different from that of a pure material. There is an apparent turning point in the Paris's crack partition. The cause of the fatigue crack growth is also dis-cussed.

  17. An Industrial Perspective on Environmentally Assisted Cracking of Some Commercially Used Carbon Steels and Corrosion-Resistant Alloys

    Science.gov (United States)

    Ashida, Yugo; Daigo, Yuzo; Sugahara, Katsuo

    2017-08-01

    Commercial metals and alloys like carbon steels, stainless steels, and nickel-based super alloys frequently encounter the problem of environmentally assisted cracking (EAC) and resulting failure in engineering components. This article aims to provide a perspective on three critical industrial applications having EAC issues: (1) corrosion and cracking of carbon steels in automotive applications, (2) EAC of iron- and nickel-based alloys in salt production and processing, and (3) EAC of iron- and nickel-based alloys in supercritical water. The review focuses on current industrial-level understanding with respect to corrosion fatigue, hydrogen-assisted cracking, or stress corrosion cracking, as well as the dominant factors affecting crack initiation and propagation. Furthermore, some ongoing industrial studies and directions of future research are also discussed.

  18. SRNL SHELF LIFE STUDIES - SCC STUDIES AT ROOM TEMPERTURE [stress corrosion cracking

    Energy Technology Data Exchange (ETDEWEB)

    Mickalonis, J.; Duffey, J.

    2014-11-12

    Phase II, Series 2 corrosion testing performed by the Savannah River National Laboratory (SRNL) for the Department of Energy 3013 container has been completed. The corrosion tests are part of an integrated plan conducted jointly by Los Alamos National Laboratory and the Savannah River Site. SRNL was responsible for conducting corrosion studies in small-scale vessels to address the influence of salt composition, water loading, and type of oxide/salt contact on the relative humidity inside a 3013 container and on the resulting corrosion of Type 304L and 316L stainless steel (304L and 316L). This testing was conducted in two phases: Phase I evaluated a broad spectrum of salt compositions and initial water loadings on the salt mixtures exposed to 304L and 316L and the resulting corrosion; Phase II evaluated the corrosion of 304L at specific water loadings and a single salt composition. During Phase I testing at high initial moisture levels (0.35 to 1.24 wt%)a, the roomtemperature corrosion of 304L exposed to a series of plutonium oxide/chloride salt mixtures ranged from superficial staining to pitting and stress corrosion cracking (SCC). 304L teardrop coupons that exhibited SCC were directly exposed to a mixture composed of 98 wt % PuO2, 0.9 wt % NaCl, 0.9 wt % KCl, and 0.2 wt % CaCl2. Cracking was not observed in a 316L teardrop coupon. Pitting was also observed in this environment for both 304L and 316L with depths ranging from 20 to 100 μm. Neither pitting nor SCC was observed in mixtures with a greater chloride salt concentration (5 and 28 wt%). These results demonstrated that for a corrosive solution to form a balance existed between the water loading and the salt chloride concentration. This chloride solution results from the interaction of loaded water with the hydrating CaCl2 salt. In Phase II, Series 1 tests, the SCC results were shown to be reproducible with cracking occurring in as little as 85 days. The approximate 0.5 wt% moisture level was found to

  19. Stress Corrosion Cracking Behavior of Alloy 22 in Multi-Ionic Aqueous Environments

    Energy Technology Data Exchange (ETDEWEB)

    K.J. King; J.C. Estill; R.B. Rebak

    2002-07-15

    The US Department of Energy is characterizing a potential repository site for nuclear waste in Yucca Mountain (NV). In its current design, the nuclear waste containers consist of a double metallic layer. The external layer would be made of NO6022 or Alloy 22 (Ni-22Cr-13Mo-3W-3Fe). Since over their lifetime, the containers may be exposed to multi-ionic aqueous environments, a potential degradation mode of the outer layer could be environmentally assisted cracking (EAC) or stress corrosion cracking (SCC). In general, Alloy 22 is extremely resistant to SCC, especially in concentrated chloride solutions. Current results obtained through slow strain rate testing (SSRT) shows that Alloy 22 may suffer SCC in simulated concentrated water (SCW) at applied potentials approximately 400 mV more anodic than the corrosion potential (E{sub rr}).

  20. Literature Survey on the Stress Corrosion Cracking of Low-Alloy Steels in High Temperature Water

    Energy Technology Data Exchange (ETDEWEB)

    Seifert, H.P

    2002-02-01

    The present report is a summary of a literature survey on the stress corrosion cracking (SCC) behaviour/ mechanisms in low-alloy steels (LAS) in high-temperature water with special emphasis to primary-pressure-boundary components of boiling water reactors (BWR). A brief overview on the current state of knowledge concerning SCC of low-alloy reactor pressure vessel and piping steels under BWR conditions is given. After a short introduction on general aspects of SCC, the main influence parameter and available quantitative literature data concerning SCC of LAS in high-temperature water are discussed on a phenomenological basis followed by a summary of the most popular SCC models for this corrosion system. The BWR operating experience and service cracking incidents are discussed with respect to the existing laboratory data and background knowledge. Finally, the most important open questions and topics for further experimental investigations are outlined. (author)

  1. Thermo-Mechanical Fatigue Crack Growth of RR1000

    Directory of Open Access Journals (Sweden)

    Christopher John Pretty

    2017-01-01

    Full Text Available Non-isothermal conditions during flight cycles have long led to the requirement for thermo-mechanical fatigue (TMF evaluation of aerospace materials. However, the increased temperatures within the gas turbine engine have meant that the requirements for TMF testing now extend to disc alloys along with blade materials. As such, fatigue crack growth rates are required to be evaluated under non-isothermal conditions along with the development of a detailed understanding of related failure mechanisms. In the current work, a TMF crack growth testing method has been developed utilising induction heating and direct current potential drop techniques for polycrystalline nickel-based superalloys, such as RR1000. Results have shown that in-phase (IP testing produces accelerated crack growth rates compared with out-of-phase (OOP due to increased temperature at peak stress and therefore increased time dependent crack growth. The ordering of the crack growth rates is supported by detailed fractographic analysis which shows intergranular crack growth in IP test specimens, and transgranular crack growth in 90° OOP and 180° OOP tests. Isothermal tests have also been carried out for comparison of crack growth rates at the point of peak stress in the TMF cycles.

  2. Thermo-Mechanical Fatigue Crack Growth of RR1000

    Science.gov (United States)

    Pretty, Christopher John; Whitaker, Mark Thomas; Williams, Steve John

    2017-01-01

    Non-isothermal conditions during flight cycles have long led to the requirement for thermo-mechanical fatigue (TMF) evaluation of aerospace materials. However, the increased temperatures within the gas turbine engine have meant that the requirements for TMF testing now extend to disc alloys along with blade materials. As such, fatigue crack growth rates are required to be evaluated under non-isothermal conditions along with the development of a detailed understanding of related failure mechanisms. In the current work, a TMF crack growth testing method has been developed utilising induction heating and direct current potential drop techniques for polycrystalline nickel-based superalloys, such as RR1000. Results have shown that in-phase (IP) testing produces accelerated crack growth rates compared with out-of-phase (OOP) due to increased temperature at peak stress and therefore increased time dependent crack growth. The ordering of the crack growth rates is supported by detailed fractographic analysis which shows intergranular crack growth in IP test specimens, and transgranular crack growth in 90° OOP and 180° OOP tests. Isothermal tests have also been carried out for comparison of crack growth rates at the point of peak stress in the TMF cycles. PMID:28772394

  3. Thermo-Mechanical Fatigue Crack Growth of RR1000.

    Science.gov (United States)

    Pretty, Christopher John; Whitaker, Mark Thomas; Williams, Steve John

    2017-01-04

    Non-isothermal conditions during flight cycles have long led to the requirement for thermo-mechanical fatigue (TMF) evaluation of aerospace materials. However, the increased temperatures within the gas turbine engine have meant that the requirements for TMF testing now extend to disc alloys along with blade materials. As such, fatigue crack growth rates are required to be evaluated under non-isothermal conditions along with the development of a detailed understanding of related failure mechanisms. In the current work, a TMF crack growth testing method has been developed utilising induction heating and direct current potential drop techniques for polycrystalline nickel-based superalloys, such as RR1000. Results have shown that in-phase (IP) testing produces accelerated crack growth rates compared with out-of-phase (OOP) due to increased temperature at peak stress and therefore increased time dependent crack growth. The ordering of the crack growth rates is supported by detailed fractographic analysis which shows intergranular crack growth in IP test specimens, and transgranular crack growth in 90° OOP and 180° OOP tests. Isothermal tests have also been carried out for comparison of crack growth rates at the point of peak stress in the TMF cycles.

  4. Near-neutral pH Stress Corrosion Crack Initiation under Simulated Coating Disbondment

    Science.gov (United States)

    Eslami, Abdoulmajid

    This research is aimed at understanding near-neutral pH SCC initiation under disbonded coatings of pipeline steels, and the effect of different environmental and operational factors on crack initiation. Understanding near-neutral pH stress corrosion cracking (SCC) could answer many of the primary questions on crack initiation of SCC which have not yet been answered. It could also assist the development of effective mitigative measures dealing with thousands of kilometer of pipelines containing this form of cracking, in addition to preventive action for future pipeline installations. Near-neutral pH SCC usually occurs under polyethylene tape (PE tape) coated pipelines, at locations where the coating becomes disbonded and/or damaged. Ground water can then penetrate under the damaged/disbonded coating, become trapped and form a suitable environment for corrosion and cracking. Despite extensive studies on this topic the details of crack initiation mechanisms in addition to the exact role of environmental and operational factors on crack initiation are not thoroughly understood. Most previous laboratory tests have been done in aggressive loading conditions and ignored the effect of coatings and cathodic protections (CP). In order to simulate the conditions responsible for crack initiation, a novel testing setup capable of simulating the synergistic effects of coating disbondment, cathodic protection and cyclic loading was implemented. Using this setup and long term laboratory tests near-neutral pH SCC initiation mechanisms and the effect of some environmental and operational factors on crack initiation were investigated. It was found that near-neutral pH SCC initiation does not necessarily occur in near-neutral pH environments as commonly believed. Depending on the level of CP and CO2 in the underground environment, different localized environments with varying pH values from near-neutral to high values above 10 can form under the disbonded coatings. This significantly

  5. Fatigue Reliability of Deck Structures Subjected to Correlated Crack Growth

    Institute of Scientific and Technical Information of China (English)

    G.Q. Feng; Y. Garbatov; C. Guedes Soares

    2013-01-01

    The objective of this work is to analyse fatigue reliability of deck structures subjected to correlated crack growth. The stress intensity factors of the correlated cracks are obtained by finite element analysis and based on which the geometry correction functions are derived. The Monte Carlo simulations are applied to predict the statistical descriptors of correlated cracks based on the Paris-Erdogan equation. A probabilistic model of crack growth as a function of time is used to analyse the fatigue reliability of deck structures accounting for the crack propagation correlation. A deck structure is modelled as a series system of stiffened panels, where a stiffened panel is regarded as a parallel system composed of plates and are longitudinal. It has been proven that the method developed here can be conveniently applied to perform the fatigue reliability assessment of structures subjected to correlated crack growth.

  6. The influence of loading on the corrosion of steel in cracked ordinary Portland cement and high performance concretes

    Science.gov (United States)

    Jaffer, Shahzma Jafferali

    Most studies that have examined chloride-induced corrosion of steel in concrete have focused on sound concrete. However, reinforced concrete is seldom uncracked and very few studies have investigated the influence of cracked concrete on rebar corrosion. Furthermore, the studies that have examined the relationship between cracks and corrosion have focused on unloaded or statically loaded cracks. However, in practice, reinforced concrete structures (e.g. bridges) are often dynamically loaded. Hence, the cracks in such structures open and close which could influence the corrosion of the reinforcing steel. Consequently, the objectives of this project were (i) to examine the effect of different types of loading on the corrosion of reinforcing steel, (ii) the influence of concrete mixture design on the corrosion behaviour and (iii) to provide data that can be used in service-life modelling of cracked reinforced concretes. In this project, cracked reinforced concrete beams made with ordinary Portland cement concrete (OPCC) and high performance concrete (HPC) were subjected to no load, static loading and dynamic loading. They were immersed in salt solution to just above the crack level at their mid-point for two weeks out of every four (wet cycle) and, for the remaining two weeks, were left in ambient laboratory conditions to dry (dry cycle). The wet cycle led to three conditions of exposure for each beam: (i) the non-submerged region, (ii) the sound, submerged region and (iii) the cracked mid-section, which was also immersed in the solution. Linear polarization resistance and galvanostatic pulse techniques were used to monitor the corrosion in the three regions. Potentiodynamic polarization, electrochemical current noise and concrete electrical resistance measurements were also performed. These measurements illustrated that (i) rebar corroded faster at cracks than in sound concrete, (ii) HPC was more protective towards the rebar than OPCC even at cracks and (iii) there

  7. Crack growth rate in core shroud horizontal welds using two models for a BWR

    Energy Technology Data Exchange (ETDEWEB)

    Arganis Juárez, C.R., E-mail: carlos.arganis@inin.gob.mx; Hernández Callejas, R.; Medina Almazán, A.L.

    2015-05-15

    Highlights: • Two models were used to predict SCC growth rate in a core shroud of a BWR. • A weld residual stress distribution with 30% stress relaxation by neutron was used. • Agreement is shown between the measurements of SCC growth rate and the predictions. • Slip–oxidation model is better at low fluences and empirical model at high fluences. - Abstract: An empirical crack growth rate correlation model and a predictive model based on the slip–oxidation mechanism for Stress Corrosion Cracking (SCC) were used to calculate the crack growth rate in a BWR core shroud. In this study, the crack growth rate was calculated by accounting for the environmental factors related to aqueous environment, neutron irradiation to high fluence and the complex residual stress conditions resulting from welding. In estimating the SCC behavior the crack growth measurements data from a Boiling Water Reactor (BWR) plant are referred to, and the stress intensity factor vs crack depth throughout thickness is calculated using a generic weld residual stress distribution for a core shroud, with a 30% stress relaxation induced by neutron irradiation. Quantitative agreement is shown between the measurements of SCC growth rate and the predictions of the slip–oxidation mechanism model for relatively low fluences (5 × 10{sup 24} n/m{sup 2}), and the empirical model predicted better the SCC growth rate than the slip–oxidation model for high fluences (>1 × 10{sup 25} n/m{sup 2}). The relevance of the models predictions for SCC growth rate behavior depends on knowing the model parameters.

  8. Anomalous mechanical behavior and crack growth of oxide glasses

    Science.gov (United States)

    Seaman, Jared Hilliard

    This thesis is concerned with analytically describing anomalous mechanical behaviors of glass. A new slow crack growth model is presented that considers a semi-elliptical crack in a cylindrical glass rod subjected to 4-point bending that is both loaded statically and under a time-dependent load. This model is used to explain a suppression of the loading-rate dependency of ion-exchanged strengthened glass. The stress relaxation behavior of an ion-exchanged strengthened glass is then analyzed in view of a newly observed water-assisted surface stress relaxation mechanism. By making refinements to a time-dependent Maxwell material model for stress buildup and relaxation, the anomalous subsurface compressive stress peak in ion-exchanged strengthened glass is explained. The notion of water-assisted stress relaxation is extended to the crack tip, where high tensile stresses exist. A toughening effect has historically been observed for cracks aged at subcritical stress intensity factors, where crack tip stress relaxation is hypothesized. A simple fracture mechanics model is developed that estimates a shielding stress intensity factor that is then superimposed with the far-field stress intensity factor. The model is used to estimate anomalous "restart" times for aged cracks. The same model predicts a non-linear crack growth rate for cracks loaded near the static fatigue limit. Double cantilever beam slow crack growth experiments were performed and new slow crack growth data for soda-lime silicate glass was collected. Interpretation of this new experimental slow crack growth data suggests that the origin of the static fatigue limit in glass is due to water-assisted stress relaxation. This thesis combines a number of studies that offer a new unified understanding of historical anomalous mechanical behaviors of glass. These anomalies are interpreted as simply the consequence of slow crack growth and water-assisted surface stress relaxation.

  9. Flaw growth of 7075, 7475, 7050 and 7049 aluminum alloy plate in stress corrosion environments: 4-year marine atmosphere results

    Science.gov (United States)

    Hasse, K. R.; Dorward, R. C.

    1981-01-01

    After nearly 53 months of exposure to marine atmosphere, crack growth in SL DCB specimens from 7075, 7475, 7050, and 7049-T7X plate has slowed to the arbitrary 10 to the -10 power m/sec used to define threshold stress intensity. Because some specimens appear to be approaching crack arrest, the importance of self-loading from corrosion product wedging as a significant driving force for crack propagation in overaged materials is questioned. Crack length-time data were analyzed using a computer curve fitting program which minimized the effects of normal data scatter, and provided a clearer picture of material performance. Precracked specimen data are supported by the results of smooth specimen tests. Transgranular stress corrosion cracking was observed in TL DCB specimens from all four alloys. This process is extremely slow and is characterized by a striated surface morphology.

  10. Study on Localized Corrosion Cracking of Alloy 600 using EN-DCPD Technique

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Yeonju; Kim, Sungwoo; Kim, Hongpyo; Hwang, Seongsik [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2013-02-15

    The object of this work is to establish an electrochemical noise(EN) measurement technique combined with a direct current potential drop(DCPD) method for monitoring of localized corrosion cracking of nickel-based alloy, and to analyze its mechanism. The electrochemical current and potential noises were measured under various conditions of applied stress to a compact tension specimen in a simulated primary water chemistry of a pressurized water reactor. The amplitude and frequency of the EN signals were evaluated in both time and frequency domains based on a shot noise theory, and then quantitatively analyzed using statistical Weibull distribution function. From the spectral analysis, the effect of the current application in DCPD was found to be effectively excluded from the EN signals generated from the localized corrosion cracking. With the aid of a microstructural analysis, the relationship between EN signals and the localized corrosion cracking mechanism was investigated by comparing the shape parameter of Weibull distribution of a mean time-to-failure.

  11. Evaluation of the stress corrosion cracking resistance of several high strength low alloy steels

    Science.gov (United States)

    Humphries, T. S.; Nelson, E. E.

    1980-01-01

    The stress corrosion cracking resistance was studied for high strength alloy steels 4130, 4340, for H-11 at selected strength levels, and for D6AC and HY140 at a single strength. Round tensile and C-ring type specimens were stressed up to 100 percent of their yield strengths and exposed to alternate immersion in salt water, salt spray, the atmosphere at Marshall Space Flight Center, and the seacoast at Kennedy Space Center. Under the test conditions, 4130 and 4340 steels heat treated to a tensile strength of 1240 MPa (180 ksi), H-11 and D6AC heat treated to a tensile strength of 1450 MPa (210 ksi), and HY140 (1020 MPa, 148 ksi) are resistant to stress corrosion cracking because failures were not encountered at stress levels up to 75 percent of their yield strengths. A maximum exposure period of one month for alternate immersion in salt water or salt spray and three months for seacoast is indicated for alloy steel to avoid false indications of stress corrosion cracking because of failure resulting from severe pitting.

  12. Stress corrosion cracking and its anisotropy of a PZT ferroelectric ceramics

    Institute of Scientific and Technical Information of China (English)

    2003-01-01

    Stress corrosion cracking (SCC) of a PZT ferroelectric ceramics in various media, such as moist atmosphere, silicon oil, methanol, water and formamide, and its anisotropy have been investigated at constant load test using a single-edge notched tensile specimen. The results showed that SCC could occur in all media, and the threshold stress intensity factor of SCC in water and formamide, KISCC, revealed anisotropy. The KISCC for poling direction parallel to the crack plane, was greater than that perpendicular to the crack plane, similar to the anisotropy of fracture toughness KIC; however, the anisotropy factor of KISCC, which was =1.8 (in formamide) and 2.1 (in water), was larger than that of KIC, which is =1.4. The stress-induced 90° domain switching causes the anisotropy of KIC and KISCC, besides, the resistance of SCC also has anisotropy.

  13. Analysis of steady-state ductile crack growth

    DEFF Research Database (Denmark)

    Niordson, Christian

    1999-01-01

    the finite element mesh remains fixed relative to the tip of the growing crack. Fracture is modelled using two different local crack growth criteria. One is a crack opening displacement criterion, while the other is a model in which a cohesive zone is imposed in front of the crack tip along the fracture zone......The fracture strength under quasi-static steady-state crack growth in an elastic-plastic material joined by a laser weld is analyzed. Laser welding gives high mismatch between the yield stress within the weld and the yield stress in the base material. This is due to the fast termic cycle, which....... Both models predict that in general a thinner laser weld gives higher interface strength. Furthermore, both fracture criteria show, that the preferred path of the crack is close outside the weld material; a phenomenon also observed in experiments....

  14. Monitoring Growth of Closed Fatigue Crack Using Subharmonic Phased Array

    Science.gov (United States)

    Ohara, Y.; Endo, H.; Hashimoto, M.; Shintaku, Y.; Yamanaka, K.

    2010-02-01

    To ensure the safety and reliability of atomic power plants and airplanes, the technique of monitoring closed fatigue cracks is requisite. Here we monitored the distribution of the crack depths and closure behavior in the length direction after 48000 and 87000 fatigue cycles using subharmonic phased array for crack evaluation (SPACE). The crack depths in the subharmonic images were larger than those in the fundamental images. Specifically, the difference was larger at near the side surface than at the center. The percentage of the closed part varied with the crack growth in the specimen. In addition, we fabricated shoe for SPACE to facilitate mechanical scanning. Thus, it was demonstrated that SPACE is useful in monitoring closed fatigue crack growth.

  15. Fundamental aspects of stress corrosion cracking of copper relevant to the Swedish deep geologic repository concept

    Energy Technology Data Exchange (ETDEWEB)

    Bhaskaran, Ganesh; Carcea, Anatolie; Ulaganathan, Jagan; Wang, Shengchun; Huang, Yin; Newman, Roger C. [Dept. of Chemical Engineering and Applied Chemistry, Univ. of Toronto, Toronto (Canada)

    2013-03-15

    Phosphorus-doped oxygen-free copper will be used as the outer barrier in canisters that will contain spent nuclear fuel in the proposed Swedish underground repository. The possibility of stress corrosion cracking (SCC) is a concern, in view of isolated reports of cracking or intergranular corrosion of pure copper in sulfide solutions. This concern was addressed in the present work using copper tensile specimens provided by SKB. Methods included slow strain rate testing, constant strain tensile testing, electrochemical and surface analytical studies of corrosion products, and electron backscatter diffraction analysis of grain orientation effects on corrosion. The base solutions were prepared from NaCl or synthetic sea water with addition of varying amounts of sodium sulfide at room temperature and 80 degree Celsius. No SCC was found in any of the testing, for a range of sulfide concentrations from 5-50 mM at room temperature or 8 C, including tests where small anodic or cathodic potential displacements were applied from the open-circuit (corrosion) potential. Neither was SCC found in constant-strain immersion testing with very large strain. The Cu2S corrosion product is generally very coarse, fragile, and easily spalled off in severe corrosion environments, i.e. high sulfide concentration, high temperature, less perfect de aeration, etc. But it could also consist of very fine grains, relatively compact and adherent, on particular grain orientations when it was formed on an electro polished surface in a very well-deaerated solution. These orientations have not yet been identified statistically, although some preference for thin, adherent films was noted on orientations close to (100). The notion that the corrosion reaction is always controlled by inward aqueous-phase diffusion of sulfide may thus not be unconditionally correct for this range of sulfide concentrations; however it is hard to distinguish the role of diffusion within pores in the film. In the actual

  16. Crack initiation and crack growth behavior of carbon and low-alloy steels

    Energy Technology Data Exchange (ETDEWEB)

    Gavenda, D.J.; Luebbers, P.R.; Chopra, O.K. [Argonne National Lab., IL (United States). Energy Technology Div.

    1997-01-01

    Section III of the ASME Boiler and Pressure Vessel Code specifies fatigue design curves for structural materials. These curves were based on tests of smooth polished specimens at room temperature in air. The effects of reactor coolant environments are not explicitly addressed by the Code design curves, but recent test data illustrate potentially significant effects of LWR coolant environments on the fatigue resistance of carbon and low-alloy steels. Under certain loading and environmental conditions, fatigue lives of test specimens may be a factor of {approx}70 shorter than in air. Results of fatigue tests that examine the influence of reactor environment on crack imitation and crack growth of carbon and low-alloy steels are presented. Crack lengths as a function of fatigue cycles were determined in air by a surface replication technique, and in water by block loading that leaves marks on the fracture surface. Decreases in fatigue life of low-alloy steels in high-dissolved-oxygen (DO) water are primarily caused by the effects of environment during early stages of fatigue damage, i.e., growth of short cracks <100 {micro}m in depth. For crack sizes of >100 {micro}m, crack growth rates in high-DO water are higher than in air by one order of magnitude. The effects of LWR environments on growth of short cracks are discussed.

  17. A study on the mechanism of stress corrosion cracking of duplex stainless steels in hot alkaline-sulfide solution

    Science.gov (United States)

    Chasse, Kevin Robert

    Duplex stainless steels (DSS) generally have superior strength and corrosion resistance as compared to most standard austenitic and ferritic stainless grades owing to a balanced microstructure of austenite and ferrite. As a result of having favorable properties, DSS have been selected for the construction of equipment in pulp and paper, chemical processing, nuclear, oil and gas as well as other industries. The use of DSS has been restricted in some cases because of stress corrosion cracking (SCC), which can initiate and grow in either the ferrite or austenite phase depending on the environment. Thorough understanding of SCC mechanisms of DSS in chloride- and hydrogen sulfide-containing solutions has been useful for material selection in many environments. However, understanding of SCC mechanisms of DSS in sulfide-containing caustic solutions is limited, which has restricted the capacity to optimize process and equipment design in pulp and paper environments. Process environments may contain different concentrations of hydroxide, sulfide, and chloride, altering corrosion and SCC susceptibility of each phase. Crack initiation and growth behavior will also change depending on the relative phase distribution and properties of austenite and ferrite. The role of microstructure and environment on the SCC of standard grade UNS S32205 and lean grade UNS S32101 in hot alkaline-sulfide solution were evaluated in this work using electrochemical, film characterization, mechanical testing, X-ray diffraction, and microscopy techniques. Microstructural aspects, which included residual stress state, phase distribution, phase ratio, and microhardness, were related to the propensity for SCC crack initiation in different simulated alkaline pulping liquors at 170 °C. Other grades of DSS and reference austenitic and superferritic grades of stainless steel were studied using exposure coupons for comparison to understand compositional effects and individual phase susceptibility

  18. Fracture Mechanical Markov Chain Crack Growth Model

    DEFF Research Database (Denmark)

    Gansted, L.; Brincker, Rune; Hansen, Lars Pilegaard

    1991-01-01

    On the basis of the B-model developed in [J. L. Bogdanoff and F. Kozin, Probabilistic Models of Cumulative Damage. John Wiley, New York (1985)] a new numerical model incorporating the physical knowledge of fatigue crack propagation is developed. The model is based on the assumption that the crack...

  19. Microstructural investigation of vintage pipeline steels highly susceptible to stress corrosion cracking

    Science.gov (United States)

    Torres, Monica

    The use of pipelines for the transmission of gas offers not only efficiency, but a number of economic advantages. Nevertheless, pipelines are subject to aggressive operating conditions and environments which can lead to in-service degradation [1] and thus to failures. These failures can have catastrophic consequences, such as environmental damage and loss of life [2]. One of the most dangerous threats to pipeline integrity is stress corrosion cracking (SCC). Despite the substantial progress that has been achieved in the field, due to the complex nature of this phenomenon there is still not a complete understanding of this form of external corrosion. This makes its detection and prevention a challenge and therefore a risk to pipeline integrity, and most importantly, to the safety of the population. SCC cracks are the result of the interaction between a corrosive environment, applied stresses, and a susceptible microstructure. To date, what defines a susceptible microstructure remains ambiguous, as SCC has been observed in a range of steel grades, microstructures, chemical composition, and grain sizes. Therefore, in order to be able to accurately predict and prevent this hazardous form of corrosion, it is imperative to advance our knowledge on the subject and gain a better understanding on the microstructural features of highly susceptible pipeline materials, especially in the subsurface zone where crack nucleation must take place. Therefore, a microstructural characterization of the region near the surface layer was carried-out utilizing TEM. TEM analysis revealed the dislocation character, ferrite morphology, and apparent carbide precipitation in some grain boundaries. Furthermore, light microscopy, SEM, and hardness testing were performed to expand our knowledge on the microscopical features of highly SCC susceptible service components. This investigation presents a new approach to SCC characterization, which exposed the sub-surface region microscopical

  20. The role of local strains from prior cold work on stress corrosion cracking

    Science.gov (United States)

    Ulaganathan, Jaganathan

    Several studies have recently reported that cold working exacerbates stress corrosion cracking (SCC) of materials in various environments, including those in which they were previously thought to be immune. While these studies usually consider cold work as a homogeneous effect, the presence of grain boundaries results in local strain concentrations that are inhomogeneously distributed within the microstructure. In order to understand the underlying mechanisms by which the local strains generated by cold work influences SCC, α-brass and Alloy 600 were used in this study. The microscopic changes in the local strains caused by cold work and by SCC were measured using electron backscatter diffraction (EBSD) and polychromatic X-ray microdiffraction (PXM). While the plastic strains were qualitatively expressed through the local misorientation calculated from the orientation data measured by both EBSD and PXM, the elastic strains were determined from the Laue patterns measured by PXM. The interaction between the local strains, and the crack initiation and propagation during SCC was studied by comparing the strain distribution from the same area measured before cold work, after cold work, and again after SCC. In this way, apart from obtaining insights on the interaction, the relative importance of pre-existing strain concentrations and those created by crack propagation can be identified. Additionally, statistical analysis of the EBSD data from uncracked and cracked grain boundaries in Alloy 600 showed the susceptibility of the boundaries to increase when they were surrounded by high local strain concentrations and when the grains sharing the boundary had similar deformation tendency, but to be independent of the grain boundary angle. Finally, one of the contributors for the changes in the strain distribution during SCC can be the corrosion process itself which was examined by intermittently measuring the changes in local strains caused by intergranular corrosion on an

  1. Prevention of stress-corrosion cracking in nuclear waste storage tanks

    Energy Technology Data Exchange (ETDEWEB)

    Ondrejcin, R S

    1984-01-01

    Stress corrosion cracking (SCC) has occurred in the early versions of carbon steel primaries of nuclear waste tanks at the Savannah River Plant. (Secondary containment was provided by a vessel surrounding the lower portion of the primary tank.) Evaporated alkaline nitrate wastes in the form of crystallized salts are being dissolved from some of these tanks for transfer to new tanks of a different design. To prevent the SCC sequence from occurring during salt dissolution, the levels of inhibitors required to prevent cracking at yield stresses were determined. Special statistically designed experiments were performed to evaluate the probability of cracking under the combined influences of nitrate, nitrite, hydroxide, and temperature. Experimentlly, samples were tested by a potentially controlled constant extension rate test and by wedge opening loaded samples. Two equations were derived by multivariable regression analyses that correlated probability of cracking as the dependent variable to nitrate, nitrite, and hydroxide concentrations and temperature as the independent variables. From these equations, simple operating standards were developed by setting the probability of cracking equal to zero and solving for the four independent variables. 15 references, 15 figures, 8 tables.

  2. Mechanism of intergranular stress corrosion cracking in HAZ for super-martensitic stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Miyata, Yukio; Kimura, Mitsuo [Tubular Products and Casting Research Dept., JFE Steel Corporation, 1-1, Kawasaki-cho, Handa (Japan); Nakamichi, Haruo; Sato, Kaoru [Analysis and Characterization Research Dept., JFE Steel Corporation, 1-1, Minamiwatarida-cho, Kawasaki-ku, Kawasaki (Japan); Itakura, Noritsugu [Products Service and Development Dept., Chita Works, JFE Steel Corporation. 1-1, Kawasaki-cho, Handa (Japan); Masamura, Katsumi [Tubular Products Business Planning Dept., JFE Steel Corporation, 2-2-3, Uchisaiwai-sho, Chiyoda-ku, Tokyo (Japan)

    2004-07-01

    Mechanism of intergranular stress corrosion cracking (IGSCC) for heat affected zone (HAZ) of super-martensitic stainless steel was studied using two types of the steel. One was a lean grade, which was Mo free and low Ni, and the other was a high grade, which was Mo added and high Ni. Specimens received heat treatments simulating welding thermal cycles were applied to SCC tests. Cracks were observed in some specimens after U-bend SCC test under low pH environments. Thermal cycle conditions with sensitization were verified from the results. No crack was observed in the specimen with the thermal cycle simulating post welding heat treatment (PWHT) after sensitizing conditions. Therefore, PWHT was clarified to be effective to prevent the cracking. Cr carbides were observed along prior austenite grain boundary intermittently, and Cr depleted zone was confirmed on the grain boundary adjacent to carbides that precipitated on the grain boundary. It is, therefore, concluded that the cracking results from Cr depletion on prior austenite grain boundary accompanied by precipitation of Cr carbides under specific welding conditions. (authors)

  3. Corrosion and cracking behaviour of steel and alloys in liquid H{sub 2}S

    Energy Technology Data Exchange (ETDEWEB)

    Longaygue, X. [Institut Francais du Petrole, 1 et 4 avenue de Bois Preau 92852 Rueil-Malmaison (France); Duval, S. [Institut Francais du Petrole, BP no 3, 69390 Vernaison (France)

    2004-07-01

    When oil and gas wells with very high partial pressure of H{sub 2}S, e.g. H{sub 2}S-rich gas, are under production, the presence of liquid H{sub 2}S is highly probable in the process operations. Until now, corrosion engineers and materials designers have paid little attention to this situation because it is rarely encountered in practice. However, such a scenario recently met an increasing interest in the context of the Sprex development, a new H{sub 2}S pre-extraction process used for the treatment of very sour natural gases, which produces the separated acid gases as a liquid phase for re-injection to a disposal reservoir. It is generally accepted that pure liquid H{sub 2}S is not corrosive by itself towards carbon or low alloy steels, but the presence of water in production and reservoir fluids could make this medium much more corrosive, although this latter assumption is poorly documented. The aim of this paper is to present the corrosion and cracking behaviour of a pipeline carbon steel and of corrosion resistant alloys (CRA) (with Cr > 16%) after exposure to the following media: i) liquid H{sub 2}S saturated with water, and ii) liquid H{sub 2}O saturated with H{sub 2}S. For both solutions, the addition of solid sulphur on some specimens was considered to take into account the possible introduction of oxygen into the system, followed by a reaction with H{sub 2}S. The tests were performed at 80 deg. C in a laboratory autoclave where both phases coexisted, using U-bend specimens as well as rectangular corrosion coupons. The main conclusion of this study is that liquid H{sub 2}S is rather less critical for corrosion and cracking of construction alloys than 'classical' sour solutions, like H{sub 2}S-saturated water. As a consequence, the materials selection will be governed by the same criteria, with the following alternatives: i) use of carbon steels in conjunction with corrosion inhibitors, e.g. higher operation expense; or ii) selection of a CRA

  4. Prediction of Crack Growth in Aqueous Environments.

    Science.gov (United States)

    1986-07-01

    Impedance for the Propagation of a Crack Through HY80 Steel in 3.5Z NaCl Solution at 25*C Under Sinusoidal Loading Condi t ions...THE PROPAGATION OF A CRACK THROUGH HY80 STEEL IN 3.5% NaCI SOLUTION AT 25°C UNDER SINUSOIDAL LOADING CONDITIONS 49 and the properties of greatest...VELOCITY AS A FUNCTION OF TIME FOR A CRACK GROWN AT CONSTANT CURRENT IN HY80 STEEL Initial conditions CI in Table 5. 66 400 UJ x v> l/> L. 0

  5. Evaluation of irradiation assisted stress corrosion cracking (IASCC) of type 316 stainless steel irradiated in FBR

    Energy Technology Data Exchange (ETDEWEB)

    Tsukada, T. (Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan)); Jitsukawa, S. (Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan)); Shiba, K. (Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan)); Sato, Y. (Power Reactor and Nuclear Fuel Development Corp., Oarai, Ibaraki (Japan)); Shibahara, I. (Power Reactor and Nuclear Fuel Development Corp., Oarai, Ibaraki (Japan)); Nakajima, H. (Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan))

    1993-12-01

    Type 316 stainless steel from the core of the experimental fast breeder reactor (FBR) JOYO was examined by the slow strain rate tensile (SSRT) test in pure, oxygenated-water and air and by the electrochemical potentiokinetic reactivation (EPR) test to evaluate a susceptibility to the irradiation assisted stress corrosion cracking (IASCC) and the radiation-induced segregation (RIS). The solution annealed and 20% cold-worked materials had been irradiated at 425 C to a neutron fluence of 8.3x10[sup 26] n/m[sup 2] (> 0.1 MeV) which is equivalent to 40 displacement per atom (dpa). Intergranular cracking was induced by the SSRT in water at 200 and 300 C, but was not observed on specimen tested in water at 60 C and in air at 300 C. This indicates that irradiation increased a susceptibility to stress corrosion cracking (SCC) in water. After the EPR test, grain boundary etching was observed in addition to grain face etching. This suggests Cr depletion may have occurred both at grain boundary and at defect clusters during the irradiation. The results are compared with the behavior of similar materials irradiated with different neutron spectrum. (orig.)

  6. Aircraft corrosion and crack inspection using advanced magneto-optic imaging technology

    Science.gov (United States)

    Thome, David K.; Fitzpatrick, Gerald L.; Skaugset, Richard L.; Shih, William C.

    1996-11-01

    A next generation magneto-optic imaging system, the MOI 303, has recently been introduced with the ability to generate real-time, complete, 2D eddy current images of cracks and corrosion in aircraft. The new imaging system described features advanced, digital remote control operation and on- screen display of setup parameters for ease of use. This instrument gives the inspector the capability to more rapidly scan large surfaces areas. The magneto-optic/eddy current imaging technology has already been formally approved for inspection of surface cracking on an aircraft fuselage. The improved magneto-optic imager is now poised to aid rapid inspection for corrosion and subsurface cracking. Previous magneto-optic imaging systems required the inspector to scan the surface twice for complete inspection coverage: a second scan was necessary with the imager rotated about 90 degrees from the orientation of the first pass. However, by providing eddy current excitation simultaneously from two orthogonal directions, complete, filled-in magneto-optic images are now generated regardless of the orientation of the imager. THese images are considerably easier to interpret and evaluate. In addition, there is a synergism obtained in applying eddy current excitation simultaneously in multiple directions: better penetration is obtained and the resulting images have better signal to noise levels compared to those produced with eddy current excitation applied only in one direction. Examples of these improved images are presented.

  7. Mitigation of Intergranular Stress Corrosion Cracking in Al-Mg by Electrochemical Potential Control

    Science.gov (United States)

    McMahon, M. E.; Scully, J. R.; Burns, J. T.

    2017-08-01

    Intergranular stress corrosion cracking in the Al-Mg alloy AA5456-H116 is suppressed via cathodic polarization in 0.6 M NaCl, saturated (5.45 M) NaCl, 2 M MgCl2, and saturated (5 M) MgCl2. Three zones of intergranular stress corrosion cracking (IG-SCC) susceptibility correlate with pitting potentials of unsensitized AA5456-H116 and pure β phase (Al3Mg2) in each solution. These critical potentials reasonably describe the influence of α Al matrix and β phase dissolution rates on IG-SCC severity. Complete inhibition occurred at applied potentials of -1.0 V and -1.1 V versus saturated calomel electrode ( V SCE) in 0.6 M NaCl. Whereas only partial mitigation of IG-SCC was achieved at -0.9 V SCE in 0.6 M NaCl and at -0.9, -1.0, and -1.1 V SCE in the more aggressive environments. Correlation of pitting potentials in bulk environments with IG-SCC behavior suggests an effect of bulk environment [Cl-] and pH on the stabilized crack tip chemistry.

  8. Electrochemical studies on stress corrosion cracking of incoloy-800 in caustic solution. Part II: Precracking samples

    Directory of Open Access Journals (Sweden)

    Dinu Alice

    2006-01-01

    Full Text Available Stress corrosion cracking (SCC in a caustic medium may affect the secondary circuit tubing of a CANDU NPP cooled with river water, due to an accidental formation of a concentrated alkaline environment in the areas with restricted circulation, as a result of a leakage of cooling water from the condenser. To evaluate the susceptibility of Incoloy-800 (used to manufacture steam generator tubes for CANDU NPP to SCC, some accelerated corrosion tests were conducted in an alkaline solution (10% NaOH, pH = 13. These experiments were performed at ambient temperature and 85 °C. We used the potentiodynamic method and the potentiostatic method, simultaneously monitoring the variation of the open circuit potential during a time period (E corr/time curve. The C-ring method was used to stress the samples. In order to create stress concentrations, mechanical precracks with a depth of 100 or 250 μm were made on the outer side of the C-rings. Experimental results showed that the stressed samples were more susceptible to SCC than the unstressed samples whereas the increase in temperature and crack depth lead to an increase in SCC susceptibility. Incipient micro cracks of a depth of 30 μm were detected in the area of the highest peak of the mechanical precrack.

  9. Standard test method for creep-fatigue crack growth testing

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2010-01-01

    1.1 This test method covers the determination of creep-fatigue crack growth properties of nominally homogeneous materials by use of pre-cracked compact type, C(T), test specimens subjected to uniaxial cyclic forces. It concerns fatigue cycling with sufficiently long loading/unloading rates or hold-times, or both, to cause creep deformation at the crack tip and the creep deformation be responsible for enhanced crack growth per loading cycle. It is intended as a guide for creep-fatigue testing performed in support of such activities as materials research and development, mechanical design, process and quality control, product performance, and failure analysis. Therefore, this method requires testing of at least two specimens that yield overlapping crack growth rate data. The cyclic conditions responsible for creep-fatigue deformation and enhanced crack growth vary with material and with temperature for a given material. The effects of environment such as time-dependent oxidation in enhancing the crack growth ra...

  10. Growth and corrosion behavior of molybdate passivation film on hot dip galvanized steel

    Institute of Scientific and Technical Information of China (English)

    卢锦堂; 孔纲; 陈锦虹; 许乔瑜; 眭润舟

    2003-01-01

    Hot dip galvanized steel sheets were passivated by molybdate aqueous solution containing 10 g/LNa2 MoO4 @ 2H2O, and the growth behavior and corrosion resistance of the passivation film were investigated. Inthe initial stage of passivation, the mass gain of film increases with passivation time proportionally. The film growsup more quickly and is apt to cracking at grain boundaries of zinc, then the cracks spread gradually on the whole sur-face of the film, and eventually the film will flake off with the increasing of film thickness. XPS results indicate thatMo compounds are present in Mo(Ⅵ) state on the surface of the film, and Mo(Ⅵ) and Mo(Ⅳ ) states inside thefilm. NSS test shows that, the corrosion resistance of the passivation film decreases as the cracks occur, but inAASS test, the thicker the film is, the better the corrosion resistance is, the cracks of film have little effect on thecorrosion resistance.

  11. Simulating Fatigue Crack Growth in Spiral Bevel Gears

    Science.gov (United States)

    Spievak, Lisa E.; Wawrzynek, Paul A.; Ingraffea, Anthony R.

    2000-01-01

    The majority of helicopter transmission systems utilize spiral bevel gears to convert the horizontal power from the engine into vertical power for the rotor. Due to the cyclical loading on a gear's tooth, fatigue crack propagation can occur. In rotorcraft applications, a crack's trajectory determines whether the gear failure will be benign or catastrophic for the aircraft. As a result, the capability to predict crack growth in gears is significant. A spiral bevel gear's complex shape requires a three dimensional model of the geometry and cracks. The boundary element method in conjunction with linear elastic fracture mechanics theories is used to predict arbitrarily shaped three dimensional fatigue crack trajectories in a spiral bevel pinion under moving load conditions. The predictions are validated by comparison to experimental results. The sensitivity of the predictions to variations in loading conditions and crack growth rate model parameters is explored. Critical areas that must be understood in greater detail prior to predicting more accurate crack trajectories and crack growth rates in three dimensions are identified.

  12. Crack growth threshold under hold time conditions in DA Inconel 718 – A transition in the crack growth mechanism

    Directory of Open Access Journals (Sweden)

    E. Fessler

    2016-01-01

    Full Text Available Aeroengine manufacturers have to demonstrate that critical components such as turbine disks, made of DA Inconel 718, meet the certification requirements in term of fatigue crack growth. In order to be more representative of the in service loading conditions, crack growth under hold time conditions is studied. Modelling crack growth under these conditions is challenging due to the combined effect of fatigue, creep and environment. Under these conditions, established models are often conservative but the degree of conservatism can be reduced by introducing the crack growth threshold in models. Here, the emphasis is laid on the characterization of crack growth rates in the low ΔK regime under hold time conditions and in particular, on the involved crack growth mechanism. Crack growth tests were carried out at high temperature (550 °C to 650 °C under hold time conditions (up to 1200 s in the low ΔK regime using a K-decreasing procedure. Scanning electron microscopy was used to identify the fracture mode involved in the low ΔK regime. EBSD analyses and BSE imaging were also carried out along the crack path for a more accurate identification of the fracture mode. A transition from intergranular to transgranular fracture was evidenced in the low ΔK regime and slip bands have also been observed at the tip of an arrested crack at low ΔK. Transgranular fracture and slip bands are usually observed under pure fatigue loading conditions. At low ΔK, hold time cycles are believed to act as equivalent pure fatigue cycles. This change in the crack growth mechanism under hold time conditions at low ΔK is discussed regarding results related to intergranular crack tip oxidation and its effect on the crack growth behaviour of Inconel 718 alloy. A concept based on an “effective oxygen partial pressure” at the crack tip is proposed to explain the transition from transgranular to intergranular fracture in the low ΔK regime.

  13. Stress Corrosion Cracking of the Drip Shield, the Waste Package Outer Barrier, and the Stainless Steel Structural Material

    Energy Technology Data Exchange (ETDEWEB)

    G. Gordon

    2004-10-13

    Stress corrosion cracking is one of the most common corrosion-related causes for premature breach of metal structural components. Stress corrosion cracking is the initiation and propagation of cracks in structural components due to three factors that must be present simultaneously: metallurgical susceptibility, critical environment, and static (or sustained) tensile stresses. This report was prepared according to ''Technical Work Plan for: Regulatory Integration Modeling and Analysis of the Waste Form and Waste Package'' (BSC 2004 [DIRS 171583]). The purpose of this report is to provide an evaluation of the potential for stress corrosion cracking of the engineered barrier system components (i.e., the drip shield, waste package outer barrier, and waste package stainless steel inner structural cylinder) under exposure conditions consistent with the repository during the regulatory period of 10,000 years after permanent closure. For the drip shield and waste package outer barrier, the critical environment is conservatively taken as any aqueous environment contacting the metal surfaces. Appendix B of this report describes the development of the SCC-relevant seismic crack density model (SCDM). The consequence of a stress corrosion cracking breach of the drip shield, the waste package outer barrier, or the stainless steel inner structural cylinder material is the initiation and propagation of tight, sometimes branching, cracks that might be induced by the combination of an aggressive environment and various tensile stresses that can develop in the drip shields or the waste packages. The Stainless Steel Type 316 inner structural cylinder of the waste package is excluded from the stress corrosion cracking evaluation because the Total System Performance Assessment for License Application (TSPA-LA) does not take credit for the inner cylinder. This document provides a detailed description of the process-level models that can be applied to assess the

  14. Fatigue Crack Growth on Double Butt Weld with Toe Crack of Pipelines Steel

    OpenAIRE

    HADJOUI, Féthi; Benachour, Mustapha; Benguediab,Mohamed

    2012-01-01

    The welded structures have a broad applicability (car industry, aeronautical, marine, pipelines, etc.). The welding being an assembled process, presents both advantages and disadvantages. A simple existing defect after welding can generate a catastrophic fracture. This work studies the fatigue crack growth of double butt weld with toe crack. Two types of pipeline material are studied with knowing API 5L grades X60 and X70 where tension form of loading is applied. In order to p...

  15. Hydrogen-increased dezincification layer-induced stress and susceptibility to stress corrosion cracking of brass

    Institute of Scientific and Technical Information of China (English)

    李会录; 高克玮; 褚武扬; 刘亚萍; 乔利杰

    2003-01-01

    Dezincification layer formed during corrosion or stress corrosion cracking (SCC) of brass in an ammonia solution could induce an additive stress. The effect of hydrogen on the dezincification layer-induced stress and the susceptibility to SCC were studied. The dezincification layer-induced stress was measured using the deflection method and the flowing stress differential method, respectively. The latter measures the difference between the flowing stress of a specimen before unloading and the yield stress of the same specimen after unloading and forming a dezincification layer. The susceptibility to SCC was measured using slow strain rate test. Results show that both the dezincification layer-induced stress and the susceptibility to SCC increase with increasing hydrogen concentration in a specimen. This implies that hydrogen-enhanced dezincification layer-induced stress is consistence with the hydrogen-increased susceptibility to SCC of brass in the ammonia solution.

  16. Diffusion-Coupled Cohesive Interface Simulations of Stress Corrosion Intergranular Cracking in Polycrystalline Materials

    Energy Technology Data Exchange (ETDEWEB)

    Pu, Chao; Gao, Yanfei; Wang, Yanli; Sham, T.-L.

    2017-09-01

    To study the stress corrosion intergranular cracking mechanism, a diffusion-coupled cohesive zone model (CZM) is proposed for the simulation of the stress-assisted diffusional process along grain boundaries and the mechanical response of grain boundary sliding and separation. This simulation methodology considers the synergistic effects of impurity diffusion driven by pressure gradient and degradation of grain boundary strength by impurity concentration. The diffusion-coupled CZM is combined with crystal plasticity finite element model (CPFEM) to simulate intergranular fracture of polycrystalline material under corrosive environment. Significant heterogeneity of the stress field and extensive impurity accumulation is observed at grain boundaries and junction points. Deformation mechanism maps are constructed with respect to the grain boundary degradation factor and applied strain rate, which dictate the transition from internal to near-surface intergranular fracture modes under various strain amplitudes and grain sizes.

  17. Influence of hydrogen environments on crack growth in Inconel 718

    Science.gov (United States)

    Walter, R. J.; Chandler, W. T.

    1978-01-01

    The effect of hydrogen environments on sustained-load and cyclic-load crack growth in Inconel 718 was investigated using fracture-mechanics-type specimens. The sustained-load crack growth was determined to be a function of heat-treatment condition, temperature, and hydrogen pressure. The threshold stress intensity for subcritical crack growth was independent of hydrogen pressure at pressures greater than 21 MN/sq m (3000 psi). The cyclic-load crack growth rate in Inconel 718 at low and moderate stress intensity ranges increased with increasing hydrogen pressure. Decreasing the cyclic frequency from 1.0 to 0.1 Hz considerably increased the cyclic crack growth rate at 0.069 MN/sq m (10 psi) and at 68.9 MN/sq m (10,000 psi) hydrogen pressure. A series of measurements performed between 1.0 and 0.1 Hz showed that the crack growth rate increased as a complex function of the time per cycle.

  18. Anomolous Fatigue Crack Growth Phenomena in High-Strength Steel

    Science.gov (United States)

    Forth, Scott C.; James, Mark A.; Johnston, William M., Jr.; Newman, James C., Jr.

    2004-01-01

    The growth of a fatigue crack through a material is the result of a complex interaction between the applied loading, component geometry, three-dimensional constraint, load history, environment, material microstructure and several other factors. Previous studies have developed experimental and computational methods to relate the fatigue crack growth rate to many of the above conditions, with the intent of discovering some fundamental material response, i.e. crack growth rate as a function of something. Currently, the technical community uses the stress intensity factor solution as a simplistic means to relate fatigue crack growth rate to loading, geometry and all other variables. The stress intensity factor solution is a very simple linear-elastic representation of the continuum mechanics portion of crack growth. In this paper, the authors present fatigue crack growth rate data for two different high strength steel alloys generated using standard methods. The steels exhibit behaviour that appears unexplainable, compared to an aluminium alloy presented as a baseline for comparison, using the stress intensity factor solution.

  19. Report on Status of Shipment of High Fluence Austenitic Steel Samples for Characterization and Stress Corrosion Crack Testing

    Energy Technology Data Exchange (ETDEWEB)

    Clark, Scarlett R. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Leonard, Keith J. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

    2016-09-01

    The goal of the Mechanisms of Irradiation Assisted Stress Corrosion Cracking (IASCC) task in the LWRS Program is to conduct experimental research into understanding how multiple variables influence the crack initiation and crack growth in materials subjected to stress under corrosive conditions. This includes understanding the influences of alloy composition, radiation condition, water chemistry and metallurgical starting condition (i.e., previous cold work or heat treatments and the resulting microstructure) has on the behavior of materials. Testing involves crack initiation and growth testing on irradiated specimens of single-variable alloys in simulated Light Water Reactor (LWR) environments, tensile testing, hardness testing, microstructural and microchemical analysis, and detailed efforts to characterize localized deformation. Combined, these single-variable experiments will provide mechanistic understanding that can be used to identify key operational variables to mitigate or control IASCC, optimize inspection and maintenance schedules to the most susceptible materials/locations, and, in the long-term, design IASCC-resistant materials. In support of this research, efforts are currently underway to arrange shipment of “free” high fluence austenitic alloys available through Électricité de France (EDF) for post irradiation testing at the Oak Ridge National Laboratory (ORNL) and IASCC testing at the University of Michigan. These high fluence materials range in damage values from 45 to 125 displacements per atom (dpa). The samples identified for transport to the United States, which include nine, no-cost, 304, 308 and 316 tensile bars, were relocated from the Research Institute of Atomic Reactors (RIAR) in Dimitrovgrad, Ulyanovsk Oblast, Russia, and received at the Halden Reactor in Halden, Norway, on August 23, 2016. ORNL has been notified that a significant amount of work is required to prepare the samples for further shipment to Oak Ridge, Tennessee. The

  20. Fatigue Crack Growth Rate of Type 347 Stainless Steel at the PWR Environment

    Energy Technology Data Exchange (ETDEWEB)

    Min, Ki Deuk; Kim, Seon Jin [Hanyang University, Seoul (Korea, Republic of); Kim, Dae Whan; Lee, Bong Sang [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2010-10-15

    Materials used in nuclear power plants are low alloy steel, stainless steel, and superalloy steel. Understanding the characteristics of these materials is important in the development of nuclear power plant related technology. Nb-stabilized Type 347 stainless steel is used for the coolant pressurizer surge line of Korea Standard Nuclear Power Plant (KSNPP). Surge line of PWR nuclear reactor are damaged by thermal fatigue due to thermal gradient during heat-up and cool-down, mechanical fatigue due to mechanical stress, and corrosion fatigue due to nuclear reactor water environment. Fatigue is an important factor which limits the life of structure. Fatigue crack growth rate curves in nuclear reactor environment are needed to evaluate the integrity of nuclear reactor structure but that result is not sufficient. In this study, fatigue crack growth rates at nuclear reactor environment are produced to evaluate integrity of nuclear power plant section 5

  1. INHIBITION OF STRESS CORROSION CRACKING OF CARBON STEEL STORAGE TANKS AT HANFORD

    Energy Technology Data Exchange (ETDEWEB)

    BOOMER, K.D.

    2007-01-31

    The stress corrosion cracking (SCC) behavior of A537 tank steel was investigated in a series of environments designed to simulate the chemistry of legacy nuclear weapons production waste. Tests consisted of both slow strain rate tests using tensile specimens and constant load tests using compact tension specimens. Based on the tests conducted, nitrite was found to be a strong SCC inhibitor. Based on the test performed and the tank waste chemistry changes that are predicted to occur over time, the risk for SCC appears to be decreasing since the concentration of nitrate will decrease and nitrite will increase.

  2. Intergranular stress corrosion cracking of welded ferritic stainless steels in high temperature aqueous environments

    Energy Technology Data Exchange (ETDEWEB)

    Fukuzuka, Toshio; Shimogori, Kazutoshi; Fujiwara, Kazuo; Tomari, Haruo (Kobe Steel Ltd. (Japan). Central Research and Development Lab.); Kanda, Masao

    1982-07-01

    In considering the application of ferritic stainless steels to heat exchanger tubing materials for moisture separator-reheaters in LWRs, the effects of environmental conditions (temperature, chloride, dissolved oxygen, pH), thermal history, and steel composition (content of C, N, Cr and Ti) on the Inter-Granular Stress Corrosion Cracking (IGSCC) in high temperature aqueous environments, were studied. The IGSCC was proved to depend on steel composition and thermal history rather than environment. From these results, a steel was designed to prevent IGSCC of the welding HAZ for 18Cr and 13Cr steels.

  3. High-Performance Laser Peening for Effective Mitigation of Stress Corrosion Cracking

    Energy Technology Data Exchange (ETDEWEB)

    Hackel, L; Hao-Lin, C; Wong, F; Hill, M

    2002-10-02

    Stress corrosion cracking (SCC) in the Yucca Mountain waste package closure welds is believed to be the greatest threat to long-term containment. Use of stress mitigation to eliminate tensile stresses resulting from welding can prevent SCC. A laser technology with sufficient average power to achieve high throughput has been developed and commercially deployed with high peak power and sufficiently high average power to be an effective laser peening system. An appropriately applied version of this process could be applied to eliminate SCC in the waste package closure welds.

  4. Thermomechanical fatigue crack growth in a cast polycrystalline superalloy

    Directory of Open Access Journals (Sweden)

    Moverare Johan J.

    2014-01-01

    Full Text Available Thermomechanical fatigue (TMF crack growth testing has been performed on the polycrystalline superalloy IN792. All tests were conducted in mechanical strain control in the temperature range between 100 and 750 °C. The influence of in-phase (IP and out-of-phase (OP TMF cycles was investigated as well as the influence of applying extended dwell times (up to 6 hours at the maximum temperature. The crack growth rates were also evaluated based on linear elastic fracture mechanics and described as a function of the stress intensity factor KI. Without dwell time at the maximum temperature, the crack growth rates are generally higher for the OP-TMF cycle compared to the IP-TMF cycle, when equivalent nominal strain ranges are compared. However, due to the fact that the tests were conducted in mechanical strain control, the stress response is very different for the IP and OP cycles. Also the crack closure level differs significantly between the cycle types. By taking the stress response into account and comparing the crack growth rates for equivalent effective stress intensity factor rages ΔKeff defined as Kmax − Kclosure, very similar crack growth rates were actually noticed independent of whether an IP or OP cycle were used. While the introduction of a 6 hour dwell time significantly increased the crack growth rates for the IP-TMF cycle, a decrease in crack growth rates versus ΔKeff were actually seen for the OP-TMF cycle. The fracture behaviour during the different test conditions has been investigated using scanning electron microscopy.

  5. Effect of proton irradiation on irradiation assisted stress corrosion cracking in PWR

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Han Ok; Hwang, Mi Jin; Kim, Sung Woo; Hwang, Seong Sik [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2014-05-15

    Irradiation assisted stress corrosion cracking (IASCC) involves the cracking and failure of materials under irradiation environment in nuclear power plant water environment. The major factors and processes governing an IASCC are suggested by others. The IASCC of the reactor core internals due to the material degradation and the water chemistry change has been reported in high stress stainless steel components, such as fuel elements (Boiling Water Reactors) in the 1960s, a control rod in the 1970s, and a baffle former bolt in recent years of light water reactors (Pressurized Water Reactors). Many irradiated stainless steels that are resistant to inergranular cracking in 288 .deg. C argon are susceptible to IG cracking in the simulated BWR environment at the same temperature. Under the circumstances, a lot works have been performed on IASCC in BWR. Recent efforts have been devoted to investigate an IASCC in a PWR, but the mechanism in a PWR is not fully understood yet as compared with that in a BWR owing to a lack of data from laboratories and fields. Therefore, it is strongly necessary to review and analyze recent researches of an IASCC in both BWR and PWR for establishing a proactive management technology for the IASCC of core internals in Korean PWRs. The objective of this research to find IASCC behavior of proton irradiated 316 stainless steels in a high-temperature water chemistry environment. The IASCC initiation susceptibility on 1, 3, 5 DPA proton irradiated 316 austenite stainless steel was evaluated in PWR environment. SCC area ratio on the fracture surface was similar regardless of irradiation level. Total crack length on the irradiated surface increases in order of specimen 1, 3, 5 DPA. The total crack length at the side surface is a better measure in evaluating IASCC initiation susceptibility for proton-irradiated samples.

  6. Effect of laser shock processing on fatigue crack growth of duplex stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Rubio-Gonzalez, C., E-mail: crubio@cidesi.mx [Centro de Ingenieria y Desarrollo Industrial, Pie de la Cuesta, 702, Desarrollo San Pablo, Queretaro, Qro., 76130 (Mexico); Felix-Martinez, C. [Centro de Ingenieria y Desarrollo Industrial, Pie de la Cuesta, 702, Desarrollo San Pablo, Queretaro, Qro., 76130 (Mexico); Gomez-Rosas, G. [Universidad de Guadalajara, Guadalajara, Jal (Mexico); Ocana, J.L.; Morales, M.; Porro, J.A. [Departamento de Fisica Aplicada a la Ingenieria Industrial, E.T.S.I.I., Universidad Politecnica de Madrid (Spain)

    2011-01-25

    Research highlights: {yields} LSP is an effective surface treatment to improve fatigue properties of duplex stainless steel. {yields} Increasing pulse density, fatigue crack growth rate is reduced. {yields} Microstructure is not affected by LSP. {yields} Compressive residual stresses increases increasing pulse density. - Abstract: Duplex stainless steels have wide application in different fields like the ship, petrochemical and chemical industries that is due to their high strength and excellent toughness properties as well as their high corrosion resistance. In this work an investigation is performed to evaluate the effect of laser shock processing on some mechanical properties of 2205 duplex stainless steel. Laser shock processing (LSP) or laser shock peening is a new technique for strengthening metals. This process induces a compressive residual stress field which increases fatigue crack initiation life and reduces fatigue crack growth rate. A convergent lens is used to deliver 2.5 J, 8 ns laser pulses by a Q-switched Nd:YAG laser, operating at 10 Hz with infrared (1064 nm) radiation. The pulses are focused to a diameter of 1.5 mm. Effect of pulse density in the residual stress field is evaluated. Residual stress distribution as a function of depth is determined by the contour method. It is observed that the higher the pulse density the greater the compressive residual stress. Pulse densities of 900, 1600 and 2500 pul/cm{sup 2} are used. Pre-cracked compact tension specimens were subjected to LSP process and then tested under cyclic loading with R = 0.1. Fatigue crack growth rate is determined and the effect of LSP process parameters is evaluated. In addition fracture toughness is determined in specimens with and without LSP treatment. It is observed that LSP reduces fatigue crack growth and increases fracture toughness if this steel.

  7. Lead-induced stress-corrosion cracking of alloy 600 in plausible steam generator crevice environments

    Energy Technology Data Exchange (ETDEWEB)

    Wright, M.D. [Atomic Energy of Canada Limited, Chalk River, Ontario (Canada); Manolescu, A. [Ontario Hydro Technologies, Toronto, Ontario (Canada); Mirzai, M. [Ontario Hydro, Toronto, Ontario (Canada)

    1999-03-01

    Laboratory stress-corrosion cracking (SCC) test environments were developed to simulate crevice chemistries representative of Bruce Nuclear Generating Station A (BNPD A) steam generators (SGs); these test environments were used to determine the susceptibility of Alloy 600 to lead-induced SCC under plausible SG conditions. Test environments were based on plant SG hideout return data and analysis of removed tubes and deposits. Deviations from the normal near-neutral crevice pH environment were considered to simulate possible faulted excursion crevice chemistry and to bound the postulated crevice pH range of 3 to 9 (at temperature). The effect of lead contamination up to 1000 ppm, but with an emphasis on the 100- to 500-ppm range, was determined. SCC susceptibility was investigated using constant extension rate tensile (CERT) tests and encapsulated C-ring tests. CERT tests were performed at 305 degrees C on tubing representative of BNPD A SG U-bends. The C-ring test method allowed a wider test matrix, covering 3 temperatures (280 degrees C, 304 degrees C and 315 degrees C), 3 strain levels (0.2%, 2% and 4%), and tubing representative of U-bends plus tubing given a simulated stress relief to represent material at the tube sheet. The results of this test program confirmed that in the absence of lead contamination, cracking does not occur in these concentrated, 3.3 to 8.9 pH range, crevice environments. Also, it appears that the concentrated crevice environments suppress lead-induced cracking relative to that seen in all-volatile-treatment (AVT) water. For the (static) C-ring tests, lead-induced SCC was only produced in the near-neutral crevice environment and was more severe at 500 ppm than at 100 ppm PbO. This trend was also observed in CERT tests, but some cracking-grain boundary attack occurred in acidic (pH 3.3) and alkaline (pH 8.9) environments. The C-ring tests indicated that a certain amount of resistance to cracking was imparted by simulated stress relief of

  8. Corrosion Fatigue in District Heating Water Tanks

    DEFF Research Database (Denmark)

    Maahn, Ernst Emanuel

    1996-01-01

    Three candidate materials for construction of buffer tanks for district heating water have been tested for corrosion fatigue properties in a district heating water environment. The investigation included Slow Strain Rate Testing of plain tensile specimens, crack initiation testing by corrosion...... fatigue of plain tensile specimens and crack growth rate determination for Compact Tensile Specimens under corrosion fatigue conditions. The three materials are equal with respect to stress corrosion sensibility and crack initiation. Crack growth rate is increased with a factor of 4-6 relative to an inert...

  9. Dynamic crack growth in a nonlocal progressively cavitating solid

    DEFF Research Database (Denmark)

    Needleman, A.; Tvergaard, Viggo

    1998-01-01

    Dynamic crack growth is analyzed numerically using a nonlocal constitutive formulation for a porous ductile material. The delocalization relates to the void growth and coalescence mechanism and is incorporated in terms of an integral condition on the rate of increase of the void volume fraction....... The material is modeled as elastic-viscoplastic with the thermal softening due to adiabatic heating accounted for. Finite element computations are carried our for edge cracked specimens subject to tensile impact loading. Two values of the material characteristic length and two finite-element discretizations...... to increase and the crack speed to decrease with increasing values of the material characteristic length. The crack growth predictions using the nonlocal constitutive model exhibit less mesh sensitivity than the corresponding ones based on the local constitutive relation. However, for the largest value...

  10. Origins of Negative Strain Rate Dependence of Stress Corrosion Cracking Initiation in Alloy 690, and Intergranular Crack Formation in Thermally Treated Alloy 690

    Science.gov (United States)

    Kim, Young Suk; Kim, Sung Soo

    2016-09-01

    We show that enhanced stress corrosion cracking (SCC) initiation in cold-rolled Alloy 690 with decreasing strain rate is related to the rate of short-range ordering (SRO) but not to the time-dependent corrosion process. Evidence for SRO is provided by aging tests on cold-rolled Alloy 690 at 623 K and 693 K (350 °C and 420 °C), respectively, which demonstrate its enhanced lattice contraction and hardness increase with aging temperature and time, respectively. Secondary intergranular cracks formed only in thermally treated and cold-rolled Alloy 690 during SCC tests, which are not SCC cracks, are caused by its lattice contraction by SRO before SCC tests but not by the orientation effect.

  11. Thermographic characterization of stress during crack growth

    Science.gov (United States)

    Cramer, K. E.; Dawicke, David S.; Welch, Christopher S.

    1992-01-01

    A full-field-thermographic technique for imaging stress patterns in dynamically loaded structures using general purpose IR imaging and image processing hardware is described. The inspection technique is based on the thermoelastic effect. A simple geometry is examined, and the experimentally determined values for the stress invariant are shown to be consistent with theoretical and numerical calculations. The application of full-field-thermographic measurement would ensure that the observed stress field has a common sampling period, thus allowing the observation of rapidly occurring stress anomalies such as the propagation of a fatigue crack. Fatigue crack propagation in two consecutive thermoelastic stress images from an aluminum sample is shown.

  12. Subcritical crack growth and mechanical weathering: a new consideration of how moisture influences rock erosion rates.

    Science.gov (United States)

    Eppes, Martha-Cary; Keanini, Russell; Hancock, Gregory S.

    2016-04-01

    The contributions of moisture to the mechanical aspects of rock weathering and regolith production are poorly quantified. In particular, geomorphologists have largely overlooked the role of subcritical crack growth processes in physical weathering and the fact that moisture strongly influences the rates of those processes. This influence is irrespective of the function that moisture plays in stress loading mechanisms like freezing or hydration. Here we present a simple numerical model that explores the efficacy of subcritical crack growth in granite rock subaerially exposed under a range of moisture conditions. Because most weathering-related stress loading for rocks found at, or near, Earth's surface (hereafter surface rocks) is cyclic, we modeled crack growth using a novel combination of Paris' Law and Charles' Law. This combination allowed us to apply existing empirically-derived data for the stress corrosion index of Charles' Law to fatigue cracking. For stress, we focused on the relatively straightforward case of intergranular stresses that arise during solar-induced thermal cycling by conductive heat transfer, making the assumption that such stresses represent a universal minimum weathering stress experienced by all surface rocks. Because all other tensile weathering-related stresses would be additive in the context of crack growth, however, our model can be adapted to include other stress loading mechanisms. We validated our calculations using recently published thermal-stress-induced cracking rates. Our results demonstrate that 1) weathering-induced stresses as modeled herein, and as published by others, are sufficient to propagate fractures subcritically over long timescales with or without the presence of water 2) fracture propagation rates increase exponentially with respect to moisture, specifically relative humidity 3) fracture propagation rates driven by thermal cycling are strongly dependent on the magnitude of diurnal temperature ranges and the

  13. Microstructural mechanisms of cyclic deformation, fatigue crack initiation and early crack growth.

    Science.gov (United States)

    Mughrabi, Haël

    2015-03-28

    In this survey, the origin of fatigue crack initiation and damage evolution in different metallic materials is discussed with emphasis on the responsible microstructural mechanisms. After a historical introduction, the stages of cyclic deformation which precede the onset of fatigue damage are reviewed. Different types of cyclic slip irreversibilities in the bulk that eventually lead to the initiation of fatigue cracks are discussed. Examples of trans- and intercrystalline fatigue damage evolution in the low cycle, high cycle and ultrahigh cycle fatigue regimes in mono- and polycrystalline face-centred cubic and body-centred cubic metals and alloys and in different engineering materials are presented, and some microstructural models of fatigue crack initiation and early crack growth are discussed. The basic difficulties in defining the transition from the initiation to the growth of fatigue cracks are emphasized. In ultrahigh cycle fatigue at very low loading amplitudes, the initiation of fatigue cracks generally occupies a major fraction of fatigue life and is hence life controlling.

  14. Fatigue crack growth in Aluminium Alloys

    NARCIS (Netherlands)

    Van Kranenburg, C.

    2010-01-01

    Fatigue is a gradual process of local strength reduction. It is a phenomenon of damage accumulation at stress concentrations caused by fluctuating stresses and/or strains. In metals this results in microscopic cracks. These will start to grow under continued cyclic loading until final failure occurs

  15. Estimating crack growth in temperature damaged concrete

    Science.gov (United States)

    Recalde, Juan Jose

    2009-12-01

    Evaluation of the structural condition of deteriorated concrete infrastructure and evaluation of new sustainable cementitious materials require an understanding of how the material will respond to applied loads and environmental exposures. A fundamental understanding of how microstructural changes in these materials relate to changes in mechanical properties and changes in fluid penetrability is needed. The ability to provide rapid, inexpensive assessment of material characteristics and relevant engineering properties is valuable for decision making and asset management purposes. In this investigation, the effects of changes in dynamic elastic properties with water content and fluid penetrability properties before and after a 300°C exposure were investigated based on estimates of the crack density parameter from dry and saturated cracked media. The experimental and analytical techniques described in this dissertation allow calculation of a value for the crack density parameter using nondestructive determination of wet and dry dynamic shear modulus of relatively thin disks. The techniques were used to compare a conventional concrete mixture to several mixtures with enhanced sustainability characteristics. The three enhanced sustainable materials investigated were a very high fly ash mixture, a magnesium phosphate cement based mortar, and a magnesium phosphate cement based concrete, and were compared to a conventional concrete mixture. The analysis provided both quantitative assessment of changes with high temperature damage and autogenous healing, and estimates of changes in mean crack trace lengths. The results showed that water interaction, deterioration due to damage, and autogenous healing recovery were different for the magnesium phosphate cement based mixtures than the portland cement based concrete mixtures. A strong correlation was found between log-transformed Air Permeability Index, dynamic shear modulus, and crack density parameter. The findings imply

  16. The effect of fatigue cracks on fastener flexibility, load distribution, and fatigue crack growth

    Science.gov (United States)

    Whitman, Zachary Layne

    Fatigue cracks typically occur at stress risers such as geometry changes and holes. This type of failure has serious safety and economic repercussions affecting structures such as aircraft. The need to prevent catastrophic failure due to fatigue cracks and other discontinuities has led to durability and damage tolerant methodologies influencing the design of aircraft structures. Holes in a plate or sheet filled with a fastener are common fatigue critical locations in aircraft structure requiring damage tolerance analysis (DTA). Often, the fastener is transferring load which leads to a loading condition involving both far-field stresses such as tension and bending, and localized bearing at the hole. The difference between the bearing stress and the tensile field at the hole is known as load transfer. The ratio of load transfer as well as the magnitude of the stresses plays a significant part in how quickly a crack will progress to failure. Unfortunately, the determination of load transfer in a complex joint is far from trivial. Many methods exist in the open literature regarding the analysis of splices, doublers and attachment joints to determine individual fastener loads. These methods work well for static analyses but greater refinement is needed for crack growth analysis. The first fastener in a splice or joint is typically the most critical but different fastener flexibility equations will all give different results. The constraint of the fastener head and shop end, along with the type of fastener, affects the stiffness or flexibility of the fastener. This in turn will determine the load that the fastener will transfer within a given fastener pattern. However, current methods do not account for the change in flexibility at a fastener as the crack develops. It is put forth that a crack does indeed reduce the stiffness of a fastener by changing its constraint, thus lessening the load transfer. A crack growth analysis utilizing reduced load transfer will result in

  17. Electrochemical investigation on the hydrogen permeation behavior of 7075-T6 Al alloy and its influence on stress corrosion cracking

    Science.gov (United States)

    Zheng, Chuan-bo; Yan, Bing-hao; Zhang, Ke; Yi, Guo

    2015-07-01

    The hydrogen permeation behavior and stress corrosion cracking (SCC) susceptibility of precharged 7075-T6 Al alloy were investigated in this paper. Devanthan-Stachurski (D-S) cell tests were used to measure the apparent hydrogen diffusivity and hydrogen permeation current density of specimens immersed in 3.5wt% NaCl solution. Electrochemical experiment results show that the SCC susceptibility is low during anodic polarization. Both corrosion pits and hydrogen-induced cracking are evident in scanning electron microscope images after the specimens have been charging for 24 h.

  18. Scaling invariance of fatigue crack growth in gigacycle loading regime

    Science.gov (United States)

    Oborin, V.; Bannikov, M.; Naimark, O.; Palin-Luc, T.

    2010-11-01

    The role of the collective behavior of defect ensembles at the crack tip and the laws of fatigue crack propagation in R4 high-strength steel have been studied under conditions of symmetric tension-compression gigacycle loading at 20 kHz. At every stage of the fatigue crack growth, replicas from the sample side surface were taken and studied by the method of three-dimensional relief profilometry (using NewView interferometer profilometer) so as to study the scaling-invariant laws of defect-related structure evolution.

  19. Fatigue crack growth behaviour of Al-Li alloys

    Science.gov (United States)

    Saravanakumar, R.; Ramakrishna, K. S.; Kanna, B. Avinash

    2013-06-01

    Al-Li alloys are being used in aircraft structures due to its low density and inherent mechanical properties. Fatigue Crack Growth (FCG) resistance is usually high compared to conventional Al-alloys attributed to increased modulus and crack closure. Extensive investigations concern about the FCG resistance and crack closure in Al-Li alloys. The present work reviews the FCG resistance in Al-Li alloys and the mechanisms associated with it. The alloy 8090 is taken for the consideration and sometimes compared with 2024.

  20. A comparison of the stress corrosion cracking susceptibility of commercially pure titanium grade 4 in Ringer's solution and in distilled water: a fracture mechanics approach.

    Science.gov (United States)

    Roach, Michael D; Williamson, R Scott; Thomas, Joseph A; Griggs, Jason A; Zardiackas, Lyle D

    2014-01-01

    From the results of laboratory investigations reported in the literature, it has been suggested that stress corrosion cracking (SCC) mechanisms may contribute to early failures in titanium alloys that have elevated oxygen concentrations. However, the susceptibility of titanium alloys to SCC in physiological environments remains unclear. In this study, a fracture mechanics approach was used to examine the SCC susceptibility of CP titanium grade 4 in Ringer's solution and distilled de-ionized (DI) water, at 37°C. The study duration was 26 weeks, simulating the non-union declaration of a plated fracture. Four wedge loads were used corresponding to 86-95% of the alloy's ligament yield load. The longest cracks were measured to be 0.18 mm and 0.10 mm in Ringer's solution and DI water, respectively. SEM analysis revealed no evidence of extensive fluting and quasi-cleavage fracture features which, in literature reports, were attributed to SCC. We thus postulate that the Ringer's solution accelerated the wedge-loaded crack growth without producing the critical stresses needed to change the fracture mechanism. Regression analysis of the crack length results led to a significant best-fit relationship between crack growth velocity (independent variable) and test electrolyte, initial wedge load, and time of immersion of specimen in electrolyte (dependent variables).

  1. Numerical investigation of ductile crack growth behavior in a dissimilar metal welded joint

    Energy Technology Data Exchange (ETDEWEB)

    Wang, H.T. [MOE Key Laboratory of Pressurized System and Safety, School of Mechanical and Power Engineering, East China University of Science and Technology, Shanghai 200237 (China); Wang, G.Z., E-mail: gzwang@ecust.edu.cn [MOE Key Laboratory of Pressurized System and Safety, School of Mechanical and Power Engineering, East China University of Science and Technology, Shanghai 200237 (China); Xuan, F.Z.; Tu, S.T. [MOE Key Laboratory of Pressurized System and Safety, School of Mechanical and Power Engineering, East China University of Science and Technology, Shanghai 200237 (China)

    2011-08-15

    Highlights: > Ductile crack growth behavior in a dissimilar metal welded joint was simulated. > Interface crack growth tends to deviate into material with lower yield stress. > Crack locations and mismatches affect local stress-strain distribution. > Local stress-strain leads to different crack growth resistances and paths. - Abstract: In this paper, the finite element method (FEM) based on GTN model is used to investigate the ductile crack growth behavior in single edge-notched bend (SENB) specimens of a dissimilar metal welded joint (DMWJ) composed of four materials in the primary systems of nuclear power plants. The J-{Delta}a resistance curves, crack growth paths and local stress-strain distributions in front of crack tips are calculated for eight initial cracks with different locations in the DMWJ and four cracks in the four homogenous materials. The results show that the initial cracks with different locations in the DMWJ have different crack growth resistances and growth paths. When the initial crack lies in the centers of the weld Alloy182 and buttering Alloy82, the crack-tip plastic and damage zones are symmetrical, and the crack grow path is nearly straight along the initial crack plane. But for the interface cracks between materials and near interface cracks, the crack-tip plastic and damage zones are asymmetric, and the crack growth path has significant deviation phenomenon. The crack growth tends to deviate into the material whose yield stress is lower between the two materials on both sides of the interface. The different initial crack locations and mismatches in yield stress and work hardening between different materials in the DMWJ affect the local stress triaxiality and plastic strain distributions in front of crack tips, and lead to different ductile crack growth resistances and growth paths. For the accurate integrity assessment for the DMWJ, the fracture toughness data and resistance curves for the initial cracks with different locations in the

  2. Microstructure and stress corrosion cracking of the fusion boundary region in an alloy 182-A533B low alloy steel dissimilar weld joint

    Energy Technology Data Exchange (ETDEWEB)

    Hou, Juan [Fracture and Reliability Research Institute, Tohoku University, 6-6-01, Aramaki Aoba, Aoba-ku, Sendai City 980-8579 (Japan); State Key Laboratory for Corrosion and Protection, Institute of Metal Research, Chinese Academy of Sciences, 62 Wencui Road, Shenyang 110016 (China); Peng, Qunjia, E-mail: qpeng@rift.mech.tohoku.ac.j [Fracture and Reliability Research Institute, Tohoku University, 6-6-01, Aramaki Aoba, Aoba-ku, Sendai City 980-8579 (Japan); Takeda, Yoichi; Kuniya, Jiro; Shoji, Tetsuo [Fracture and Reliability Research Institute, Tohoku University, 6-6-01, Aramaki Aoba, Aoba-ku, Sendai City 980-8579 (Japan)

    2010-12-15

    Research highlights: {yields} High-angle misorientation at FB, type-II and type-I boundaries. {yields} Highest residual strain and hardness in the zone between FB and type-II boundary. {yields} Type-II and type-I boundaries had lower resistance to SCC growth than the FB. {yields} Crack growth blunted by pitting at the FB. {yields} Reactivation of crack growth from the pitting by oxidation along the grain boundary. - Abstract: Stress corrosion cracking (SCC) in the fusion boundary (FB) region of an Alloy 182-A533B low alloy steel (LAS) dissimilar weld joint in high temperature water doped with sulfate was studied following a microstructure characterization of the FB region. The microstructure characterization suggested the type-II and type-I boundaries in the dilution zone (DZ) adjacent to the FB had lower resistance to SCC growth than the FB. Crack propagating perpendicular to the FB in the DZ was observed to be blunted by pitting at the FB, followed by the reactivation from the pitting by localized oxidation along the grain boundary in LAS.

  3. Stress corrosion cracking behaviour in welded X-70 linepipe steel under near-neutral pH conditions

    Energy Technology Data Exchange (ETDEWEB)

    Adeleke, A.H.; Luo, J.L.; Ivey, D.G. [Alberta Univ., Edmonton, AB (Canada). Dept. of Chemical and Materials Engineering

    2005-07-01

    This study examined the relationship between the near neutral pH stress corrosion cracking (SCC) resistance and the yield strength of pipelines steels. In particular, double-edge-notched flat tensile samples of X70 steel were used for both slow strain-rate testing (SSRT) and cyclic loading testing with the notch located in the zone of interest. This included the weld metal (WM), base metal (BM) and heat-affected zone (HAZ). In all samples, the mode of failure was mostly transgranular with cleavage facets around the edges of the fracture surface. One of the objectives of this study was to better understand the microstructural effect of the relationship. The 3 main parameters that were used to assess the SCC susceptibility in a near-neutral pH environment were the elongation ratio, the estimated percentage of the fracture surface that showed brittle fractures, and the relative crack growth at a given exposure time. It was shown that resistance to near-neutral pH SCC depends greatly on the microstructure of the pipeline steels. Fine-grained bainite and ferrite structured steels were found to have a much better combination of strength and SCC resistance compared to ferrite and pearlite structures. The high-to-low sensitivity ranking of the X70 linepipe steel to SCC was established to be: WM is greater than HAZ which is greater than BM. 20 refs., 1 tab., 9 figs.

  4. Assessment of Initial Test Conditions for Experiments to Assess Irradiation Assisted Stress Corrosion Cracking Mechanisms

    Energy Technology Data Exchange (ETDEWEB)

    Busby, Jeremy T [ORNL; Gussev, Maxim N [ORNL

    2011-04-01

    Irradiation-assisted stress corrosion cracking is a key materials degradation issue in today s nuclear power reactor fleet and affects critical structural components within the reactor core. The effects of increased exposure to irradiation, stress, and/or coolant can substantially increase susceptibility to stress-corrosion cracking of austenitic steels in high-temperature water environments. . Despite 30 years of experience, the underlying mechanisms of IASCC are unknown. Extended service conditions will increase the exposure to irradiation, stress, and corrosive environment for all core internal components. The objective of this effort within the Light Water Reactor Sustainability program is to evaluate the response and mechanisms of IASCC in austenitic stainless steels with single variable experiments. A series of high-value irradiated specimens has been acquired from the past international research programs, providing a valuable opportunity to examine the mechanisms of IASCC. This batch of irradiated specimens has been received and inventoried. In addition, visual examination and sample cleaning has been completed. Microhardness testing has been performed on these specimens. All samples show evidence of hardening, as expected, although the degree of hardening has saturated and no trend with dose is observed. Further, the change in hardening can be converted to changes in mechanical properties. The calculated yield stress is consistent with previous data from light water reactor conditions. In addition, some evidence of changes in deformation mode was identified via examination of the microhardness indents. This analysis may provide further insights into the deformation mode under larger scale tests. Finally, swelling analysis was performed using immersion density methods. Most alloys showed some evidence of swelling, consistent with the expected trends for this class of alloy. The Hf-doped alloy showed densification rather than swelling. This observation may be

  5. Monitoring of fatigue crack growth using guided ultrasonic waves

    Science.gov (United States)

    Masserey, B.; Kostson, E.; Fromme, P.

    2010-04-01

    Varying loading conditions of aircraft structures result in stress concentration at fastener holes, where multi layer components are connected, possibly leading to the development of fatigue cracks. Guided ultrasonic waves propagating along a structure allow in principle for the efficient non-destructive testing of large plate-like structures, such as aircraft wings. This contribution presents a study of the detection and monitoring of fatigue crack growth using both low frequency and higher frequency guided ultrasonic wave modes. Two types of structures were used, single layer aluminum tensile specimens, and multi layer structures consisting of two adhesively bonded aluminum plate-strips. Fatigue experiments were carried out and it was shown that fatigue crack detection and growth monitoring at a fastener hole during cyclic loading using both guided wave types is possible. The sensitivity and repeatability of the measurements were ascertained, having the potential for fatigue crack detection at critical and difficult to access fastener locations. Good agreement was observed between the experimental results and predictions from full three-dimensional numerical simulations of the scattering of the low frequency guided ultrasonic wave at the fastener hole and crack. The robustness of the methodology for practical in-situ ultrasonic monitoring of fatigue crack growth is discussed.

  6. Tensile stress corrosion cracking of type 304 stainless steel irradiated to very high dose

    Energy Technology Data Exchange (ETDEWEB)

    Chung, H. M.; Ruther, W. E.; Strain, R. V.; Shack, W. J.

    2001-09-01

    Certain safety-related core internal structural components of light water reactors, usually fabricated from Type 304 or 316 austenitic stainless steels (SSs), accumulate very high levels of irradiation damage (20--100 displacement per atom or dpa) by the end of life. The data bases and mechanistic understanding of, the degradation of such highly irradiated components, however, are not well established. A key question is the nature of irradiation-assisted intergranular cracking at very high dose, i.e., is it purely mechanical failure or is it stress-commotion cracking? In this work, hot-cell tests and microstructural characterization were performed on Type 304 SS from the hexagonal fuel can of the decommissioned EBR-11 reactor after irradiation to {approximately}50 dpa at {approximately}370 C. Slow-strain-rate tensile tests were conducted at 289 C in air and in water at several levels of electrochemical potential (ECP), and microstructural characteristics were analyzed by scanning and transmission electron microcopies. The material deformed significantly by twinning and exhibited surprisingly high ductility in air, but was susceptible to severe intergranular stress corrosion cracking (IGSCC) at high ECP. Low levels of dissolved O and ECP were effective in suppressing the susceptibility of the heavily irradiated material to IGSCC, indicating that the stress corrosion process associated with irradiation-induced grain-boundary Cr depletion, rather than purely mechanical separation of grain boundaries, plays the dominant role. However, although IGSCC was suppressed, the material was susceptible to dislocation channeling at low ECP, and this susceptibility led to poor work-hardening capability and low ductility.

  7. Stress corrosion cracking behavior of annealed and cold worked 316L stainless steel in supercritical water

    Energy Technology Data Exchange (ETDEWEB)

    Sáez-Maderuelo, A., E-mail: alberto.saez@ciemat.es; Gómez-Briceño, D.

    2016-10-15

    Highlights: • The alloy 316L is susceptible to stress corrosion cracking in supercritical water. • The susceptibility of alloy 316L increases with temperature and plastic deformation. • Dynamic strain ageing processes may be active in the material. - Abstract: The supercritical water reactor (SCWR) is one of the more promising designs considered by the Generation IV International Forum due to its high thermal efficiency and improving security. To build this reactor, standardized structural materials used in light water reactors (LWR), like austenitic stainless steels, have been proposed. These kind of materials have shown an optimum behavior to stress corrosion cracking (SCC) under LWR conditions except when they are cold worked. It is known that physicochemical properties of water change sharply with pressure and temperature inside of the supercritical region. Owing to this situation, there are several doubts about the behavior of candidate materials like austenitic stainless steel 316L to SCC in the SCWR conditions. In this work, alloy 316L was studied in deaerated SCW at two different temperatures (400 °C and 500 °C) and at 25 MPa in order to determine how changes in this variable influence the resistance of this material to SCC. The influence of plastic deformation in the behavior of alloy 316L to SCC in SCW was also studied at both temperatures. Results obtained from these tests have shown that alloy 316L is susceptible to SCC in supercritical water reactor conditions where the susceptibility of this alloy increases with temperature. Moreover, prior plastic deformation of 316L SS increased its susceptibility to environmental cracking in SCW.

  8. Simulated Service and Stress Corrosion Cracking Testing for Friction Stir Welded Spun Formed Domes

    Science.gov (United States)

    Stewart, Thomas J.; Torres, Pablo D.; Caratus, Andrei A.; Curreri, Peter A.

    2010-01-01

    Simulated service testing (SST) development was required to help qualify a new 2195 aluminum lithium (Al-Li) alloy spin forming dome fabrication process for the National Aeronautics and Space Administration (NASA) Exploration Development Technology Program. The application for the technology is to produce high strength low weight tank components for NASA s next generation launch vehicles. Since plate material is not currently manufactured large enough to fabricate these domes, two plates are joined by means of friction stir welding. The plates are then pre-contour machined to near final thicknesses allowing for a thicker weld land and anticipating the level of stretch induced by the spin forming process. The welded plates are then placed in a spin forming tool and hot stretched using a trace method producing incremental contours. Finally the dome receives a room temperature contour stretch to final dimensions, heat treatment, quenching, and artificial aging to emulate a T-8 condition of temper. Stress corrosion cracking (SCC) tests were also performed by alternate immersion in a sodium chloride (NaCl) solution using the typical double beam assembly and with 4-point loaded specimens and use of bent-beam stress-corrosion test specimens under alternate immersion conditions. In addition, experiments were conducted to determine the threshold stress intensity factor for SCC (K(sub ISCC)) which to our knowledge has not been determined previously for Al-Li 2195 alloy. The successful simulated service and stress corrosion testing helped to provide confidence to continue to Ares 1 scale dome fabrication

  9. Effects of microscale inertia on dynamic ductile crack growth

    Science.gov (United States)

    Jacques, N.; Mercier, S.; Molinari, A.

    2012-04-01

    The aim of this paper is to investigate the role of microscale inertia in dynamic ductile crack growth. A constitutive model for porous solids that accounts for dynamic effects due to void growth is proposed. The model has been implemented in a finite element code and simulations of crack growth in a notched bar and in an edge cracked specimen have been performed. Results are compared to predictions obtained via the Gurson-Tvergaard-Needleman (GTN) model where micro-inertia effects are not accounted for. It is found that microscale inertia has a significant influence on the crack growth. In particular, it is shown that micro-inertia plays an important role during the strain localisation process by impeding void growth. Therefore, the resulting damage accumulation occurs in a more progressive manner. For this reason, simulations based on the proposed modelling exhibit much less mesh sensitivity than those based on the viscoplastic GTN model. Microscale inertia is also found to lead to lower crack speeds. Effects of micro-inertia on fracture toughness are evaluated.

  10. Crack growth time dependence analysis of granite under compressive-shear stresses state

    Institute of Scientific and Technical Information of China (English)

    LI Jiang-teng; CAO Ping; Gu De-sheng; Wu Chao

    2008-01-01

    The curves of crack relative length //b and crack growth time t of granite were gained under compressive stresses state according to subcritical crack growth parameters and crack stability growth equation by double-torsion constant displacement load relaxa-tion method. The relations between crack relative length and the crack growth time were discussed under different stresses and different crack lengths. The results show that there is a turning point on curve of crack relative length //b and crack growth time of granite. The slope of curve is small when crack relative length is less than the vertical coordinate of the point, and crack grows stably in this case. Cracks grow, encounter and integrate catastro-phically when crack relative length is more than the vertical coordinate of the point, and there is not a gradual stage from crack stability growth to crack instability growth, i.e. rock mass instability is sudden. The curves of crack relative length //b and crack growth time t of granite move to right with decrease of stress σ1 or crack length a, which implies that limit time increases consequently. The results correspond to practicality.

  11. Stress corrosion cracking of austenitic weld deposits in a salt spray environment

    Science.gov (United States)

    Cai, J. B.; Yu, C.; Shiue, R. K.; Tsay, L. W.

    2015-10-01

    ER 308L and 309LMo were utilized as the filler metals for the groove and overlay welds of a 304L stainless steel substrate, which was prepared via a gas tungsten arc-welding process in multiple passes. U-bend and weight-loss tests were conducted by testing the welds in a salt spray containing 10 wt% NaCl at 120 °C. The dissolution of the skeletal structure in the fusion zone (FZ) caused the stress corrosion cracking (SCC) of the weld. The FZ in the cold-rolled condition showed the longest single crack length in the U-bend tests. Moreover, sensitization treatment at 650 °C for 10 h promoted the formation of numerous fine cracks, which resulted in a high SCC susceptibility. The weight loss of the deposits was consistent with the SCC susceptibility of the welds in a salt spray. The 309LMo deposit was superior to the 308L deposit in the salt spray.

  12. Public inquiry concerning stress corrosion cracking on Canadian oil and gas pipelines

    Energy Technology Data Exchange (ETDEWEB)

    Vollman, K.W.; Cote-Verhaaf, A.; Illing, R.

    1996-11-01

    An comprehensive inquiry was conducted into the serious problem of near-neutral pH stress corrosion cracking (SCC) in Canada`s buried oil and gas pipelines. The inquiry was prompted by evidence of the widespread nature of SCC and awareness that research was producing new insights into the problem. Two major ruptures and fires occurred on the TransCanada system in February and July of 1995. The July rupture was in a location where it was believed SCC could not occur. SCC on pipelines occurs when small cracks develop on the outside surface of the buried pipeline. With time the cracks grow large enough until the pipeline fails or ruptures. SCC results from an interaction of the following three conditions: a potent environment at the pipe surface, a susceptible pipe material, and a tensile stress. Recommendations to resolve the problem included implementation of an SCC management program by pipeline companies, changes to the design of the pipeline, continued research, establishment of an SCC database, improved emergency response practices, and information sharing. 84 refs., 8 tabs., 67 figs.

  13. Stress corrosion cracking of alloy 600 using the constant strain rate test

    Energy Technology Data Exchange (ETDEWEB)

    Bulischeck, T. S.; van Rooyen, D.

    1980-01-01

    The most recent corrosion problems experienced in nuclear steam generators tubed with Inconel alloy 600 is a phenomenon labeled ''denting''. Denting has been found in various degrees of severity in many operating pressurized water reactors. Laboratory investigations have shown that Inconel 600 exhibits intergranular SCC when subjected to high stresses and exposed to deoxygenated water at elevated temperatures. A research project was initiated at Brookhaven National Laboratory in an attempt to improve the qualitative and quantitative understanding of factors influencing SCC in high temperature service-related environments. An effort is also being made to develop an accelerated test method which could be used to predict the service life of tubes which have been deformed or are actively denting. Several heats of commercial Inconel 600 tubing were procured for testing in deaerated pure and primary water at temperatures from 290 to 365/sup 0/C. U-bend type specimens were used to determine crack initiation times which may be expected for tubes where denting has occurred but is arrested and provide baseline data for judging the accelerating effects of the slow strain rate method. Constant extension rate tests were employed to determine the crack velocities experienced in the crack propagation stage and predict failure times of tubes which are actively denting. 8 refs., 17 figs., 5 tabs.

  14. In vivo oxide-induced stress corrosion cracking of Ti-6Al-4V in a neck-stem modular taper: Emergent behavior in a new mechanism of in vivo corrosion.

    Science.gov (United States)

    Gilbert, Jeremy L; Mali, Sachin; Urban, Robert M; Silverton, Craig D; Jacobs, Joshua J

    2012-02-01

    In vivo modular taper corrosion in orthopedic total joint replacements has been documented to occur for head-neck tapers, modular-body tapers, and neck-stem tapers. While the fretting corrosion mechanism by which this corrosion occurs has been described in the literature, this report shows new and as yet unreported mechanisms at play. A retrieved Ti-6Al-4V/Ti-6Al-4V neck-stem taper interface, implanted for 6 years is subjected to failure analysis to document taper corrosion processes that lead to oxide driven crack formation on the medial side of the taper. Metallurgical sectioning techniques and scanning electron microscopy analysis are used to document the taper corrosion processes. The results show large penetrating pitting attack of both sides of the taper interface where corrosion selectively attacks the beta phase of the microstructure and eventually consumes the alpha phase. The pitting attack evolves into plunging pits that ultimately develop into cracks where the crack propagation process is one of corrosion resulting in oxide formation and subsequent reorganization. This process drives open the crack and advances the front by a combination of oxide-driven crack opening stresses and corrosion attack at the tip. The oxide that forms has a complex evolving structure including a network of transport channels that provide access of fluid to the crack tip. This emergent behavior does not appear to require continued fretting corrosion to propagate the pitting and cracking. This new mechanism is similar to stress corrosion cracking where the crack tip stresses arise from the oxide formation in the crack and not externally applied tensile stresses.

  15. POTENTIAL FOR STRESS CORROSION CRACKING OF A537 CARBON STEEL NUCLEAR WASTE TANKS CONTAINING HIGHLY CAUSTIC SOLUTIONS

    Energy Technology Data Exchange (ETDEWEB)

    Lam, P.; Stripling, C.; Fisher, D.; Elder, J.

    2010-04-26

    The evaporator recycle streams of nuclear waste tanks may contain waste in a chemistry and temperature regime that exceeds the current corrosion control program, which imposes temperature limits to mitigate caustic stress corrosion cracking (CSCC). A review of the recent service history found that two of these A537 carbon steel tanks were operated in highly concentrated hydroxide solution at high temperature. Visual inspections, experimental testing, and a review of the tank service history have shown that CSCC has occurred in uncooled/un-stress relieved tanks of similar construction. Therefore, it appears that the efficacy of stress relief of welding residual stress is the primary corrosion-limiting mechanism. The objective of this experimental program is to test A537 carbon steel small scale welded U-bend specimens and large welded plates (30.48 x 30.38 x 2.54 cm) in a caustic solution with upper bound chemistry (12 M hydroxide and 1 M each of nitrate, nitrite, and aluminate) and temperature (125 C). These conditions simulate worst-case situations in these nuclear waste tanks. Both as-welded and stress-relieved specimens have been tested. No evidence of stress corrosion cracking was found in the U-bend specimens after 21 days of testing. The large plate test was completed after 12 weeks of immersion in a similar solution at 125 C except that the aluminate concentration was reduced to 0.3 M. Visual inspection of the plate revealed that stress corrosion cracking had not initiated from the machined crack tips in the weld or in the heat affected zone. NDE ultrasonic testing also confirmed subsurface cracking did not occur. Based on these results, it can be concluded that the environmental condition of these tests was unable to develop stress corrosion cracking within the test periods for the small welded U-bends and for the large plates, which were welded with an identical procedure as used in the construction of the actual nuclear waste tanks in the 1960s. The

  16. Environmental stress cracking of PVC and PVC-CPE - Part III Crack growth

    NARCIS (Netherlands)

    Breen, J.

    1995-01-01

    The fracture toughness of Polyvinylchloride (PVC) and PVC modified with 10% chlorinated polyethylene (PVC-CPE) was studied in vapour and in liquid environments by crack growth measurements on single-edge notch specimens under three-point bending at 23°C. In addition, some results obtained in air at

  17. EFFECT OF OVERLOAD ON CRACK GROWTH IN FIBER REINFORCED METAL LAMINATES

    Institute of Scientific and Technical Information of China (English)

    1998-01-01

    This paper is concerned with fatigue behavior of glass fiber reinforced aluminium laminates (GLARE) under overload fatigue loading. The effect of single overload on the crack growth rates in GLARE was investigated, and the mechanism of the retardation of crack growth determined. Crack growth retardation by overload was observed in GLARE, but much smaller than monolithic metals. The retardation of crack growth in GLARE is only controlled by the effective stress intensity factor experienced by the constituent metals at crack tips.

  18. Corrosion of steel bars in cracked concrete made with ordinary portland, slag and fly ash cements

    Energy Technology Data Exchange (ETDEWEB)

    Mohammed, T.U.; Yamaji, T.; Hamada, H. [Port and Harbor Research Inst., Ministry of Land, Infrastructure and Transport (Japan); Aoyama, T. [PS Corp. (Japan)

    2001-07-01

    A study was conducted in which the marine durability of ordinary portland cement, slag and fly ash cement was examined using 15 year old plain and reinforced concrete cylindrical specimens. The performance of these cements was then examined for pre-cracked reinforced concrete prism samples. The process of manufacturing cement emits huge amounts of carbon dioxide into the global atmosphere. Replacing a portion of the cement with by-products from the steel industry and thermal power plants (which are both huge emitters of carbon dioxide) can lower carbon dioxide emissions and also solve the disposal issue of slag and fly ash while increasing the long-term durability of concrete structures. In this study, concrete cylindrical specimens were made of ordinary portland cement, slag and fly ash cements. The specimens were 100 x 100 x 600 mm prisms of different types of cement. Water-to-cement ratios were 0.45 and 0.55. Both tap water and seawater were used as mixing water. The samples were exposed in tidal pools for 15 years to evaluate the compressive strength of the concrete, corrosion of the steel bars, and chloride-ion concentrations in the concrete. It was shown that, with the exception of fly ash cements, the compressive strength of most cements increased after 15 years of exposure compared to its 28 day strength. Type C slag cement demonstrated the best performance against chloride-ion at the surface of concrete made with slag and fly ash. Voids in the steel-concrete interface make it possible for corrosion pits to develop. The use of seawater as mixing water results in earlier strength development at 28 days and does not cause to the strength of the concrete to regress after 15-years of exposure, but it causes more corrosion of steel bars at a lower cover depth. Corrosion of steel bars is not an issue at deeper cover depths. 15 refs., 19 tabs., 13 figs.

  19. The Effects of Load Ratio on Threshold Fatigue Crack Growth of Aluminum Alloys

    OpenAIRE

    Newman, John Andrew

    2000-01-01

    The integrity of nearly all engineering structures are threatened by the presence of cracks. Structural failure occurs if a crack larger than a critical size exists. Although most well designed structures initially contain no critical cracks, subcritical cracks can grow to failure under fatigue loading, called fatigue crack growth (FCG). Because it is impossible or impractical to prevent subcritical crack growth in most applications, a damage tolerant design philosophy was developed for cr...

  20. Deformation and crack growth response under cyclic creep conditions

    Energy Technology Data Exchange (ETDEWEB)

    Brust, F.W. Jr. [Battelle Memorial Institute, Columbus, OH (United States)

    1995-12-31

    To increase energy efficiency, new plants must operate at higher and higher temperatures. Moreover, power generation equipment continues to age and is being used far beyond its intended original design life. Some recent failures which unfortunately occurred with serious consequences have clearly illustrated that current methods for insuring safety and reliability of high temperature equipment is inadequate. Because of these concerns, an understanding of the high-temperature crack growth process is very important and has led to the following studies of the high temperature failure process. This effort summarizes the results of some recent studies which investigate the phenomenon of high temperature creep fatigue crack growth. Experimental results which detail the process of creep fatigue, analytical studies which investigate why current methods are ineffective, and finally, a new approach which is based on the T{sup *}-integral and its ability to characterize the creep-fatigue crack growth process are discussed. The potential validity of this new predictive methodology is illustrated.

  1. The influence of cracks on chloride-induced corrosion of reinforced concrete structures - development of the experimental set-up

    NARCIS (Netherlands)

    Blagojevic, A.; Koleva, D.A.; Walraven, J.C.

    2014-01-01

    Chloride-induced corrosion of steel reinforcement is one of the major threats to durability of reinforced concrete structures in aggressive environmental conditions. When the steel reinforcement starts to corrode, structures gradually lose integrity and service life is shortened. Cracks are inevitab

  2. Slow Crack Growth of Brittle Materials With Exponential Crack-Velocity Formulation. Part 1; Analysis

    Science.gov (United States)

    Choi, Sung R.; Nemeth, Noel N.; Gyekenyesi, John P.

    2002-01-01

    Extensive slow-crack-growth (SCG) analysis was made using a primary exponential crack-velocity formulation under three widely used load configurations: constant stress rate, constant stress, and cyclic stress. Although the use of the exponential formulation in determining SCG parameters of a material requires somewhat inconvenient numerical procedures, the resulting solutions presented gave almost the same degree of simplicity in both data analysis and experiments as did the power-law formulation. However, the fact that the inert strength of a material should be known in advance to determine the corresponding SCG parameters was a major drawback of the exponential formulation as compared with the power-law formulation.

  3. Fatigue crack growth rates of rotor steel at elevated temperatures

    Institute of Scientific and Technical Information of China (English)

    LIU Chang-hai; MA Li-juan; TANG Li-qiang

    2008-01-01

    Low fatigue samples were obtained from the outer edges of rotor steel (30CrlMolV) which had operated under different temperatures conditions.Based on this data,the effects of temperature on fatigue crack growth rates were investigated.This paper presents a derivation of the superposition expression of two natural logarithms governing crack growth rates and also discusses the relationship between a material's constants and temperature.These results can provide experimental and theoretical references for fatigue life design of root steel in steam turbines.

  4. Dynamic crack growth in a fiber-reinforced composite plate

    Institute of Scientific and Technical Information of China (English)

    LIU Kaixin; LIU Weifu; Zhang Jinxiang; LI Rong; ZHANG Guohua; FU Bin

    2005-01-01

    This paper reports an experiment on the failure of a precracked plate made of unidirectional glass-epoxy fiber-reinforced composites subjected to three-point bending impact load. In the experiment, the whole process of crack growth was recorded by using high-speed photographic technique, in which a transmitted light path was adopted. Moreover, a new phenomenon of dynamic fracture has been observed. Based on the results, some preliminary studies have been carried out on the rate and path of the crack growth, as well as the failure mode.

  5. Research of stress corrosion cracking of T225NG titanium alloy in loop water of high temperature and high pressure

    Institute of Scientific and Technical Information of China (English)

    Xu Jijin; Yan Keng; Chen Ligong; Jiang Chengyu

    2006-01-01

    Double cantilever beam (DCB) specimens were used to research the stress corrosion cracking of T225NG titanium alloy in loop water of high temperature and high pressure. DCB specimens were forced pre-stress, put into high pressure autoclave, and the stress corrosion and crack expansion of specimens were observed and measured in 500 h, 1 000 h and 2 000h respectively. The results show that small expansion occurred along the direction of pre-cracking. According to calculation,the speed of cracking expansion is lower than 10 -9 m/s in 500 h and the value of KIscc/KI is higher than 0. 75, which proves that T225NG has an excellent corrosion resistance in loop water. The main reason is that there is an oxide film on the surface of specimens. According to the analysis of energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD), the oxide film consists of TiO2. Therefore, the oxide film at the crack tip impedes the hydrogen separating out from the cathode to penetrate into titanium alloy and resists hydrogen embrittlement.

  6. Investigation into the stress corrosion cracking properties of AA2099, an aluminum-lithium-copper alloy

    Science.gov (United States)

    Padgett, Barbara Nicole

    Recently developed Al-Li-Cu alloys show great potential for implementation in the aerospace industry because of the attractive mix of good mechanical properties and low density. AA2099 is an Al-Li-Cu alloy with the following composition Al-2.69wt%Cu-1.8wt%Li-0.6wt%Zn-0.3wt%Mg-0.3wt%Mn-0.08wt%Zr. The environmental assisted cracking and localized corrosion behavior of the AA2099 was investigated in this thesis. The consequences of uncontrolled grain boundary precipitation via friction stir welding on the stress corrosion cracking (SCC) behavior of AA2099 was investigated first. Using constant extension rate testing, intergranular corrosion immersion experiments, and potentiodynamic scans, the heat-affected zone on the trailing edge of the weld (HTS) was determined to be most susceptible of the weld zones. The observed SCC behavior for the HTS was linked to the dissolution of an active phase (Al2CuLi, T1) populating the grain boundary. It should be stated that the SCC properties of AA2099 in the as-received condition were determined to be good. Focus was then given to the electrochemical behavior of precipitate phases that may occupy grain and sub-grain boundaries in AA2099. The grain boundary micro-chemistry and micro-electrochemistry have been alluded to within the literature as having significant influence on the SCC behavior of Al-Li-Cu alloys. Major precipitates found in this alloy system are T1 (Al 2CuLi), T2 (Al7.5Cu4Li), T B (Al6CuLi3), and theta (Al2 Cu). These phases were produced in bulk form so that the electrochemical nature of each phase could be characterized. It was determined T1 was most active electrochemically and theta was least. When present on grain boundaries in the alloy, electrochemical behavior of the individual precipitates aligned with the observed corrosion behavior of the alloy (e.g. TB was accompanied by general pitting corrosion and T 1 was accompanied by intergranular corrosion attack). In addition to the electrochemical behavior of

  7. Growth patterns and dynamics of mud cracks at different diagenetic stages and its geological significance

    Institute of Scientific and Technical Information of China (English)

    Zhen-yu ZHAO; Yan-ru GUO; Yan WANG; Hong LIU; Qing ZHANG

    2014-01-01

    This paper discusses the growth stages, spatial structures, quantitative fitting relationships among various parameters, growth patterns and influencing factors of mud cracks by field survey, core observation and SEM analysis. The study shows that:(1) Mud crack growth can go through three stages, i.e. the syndiagenetic stage, the burial diagenetic stage (including early diagenetic stage, middle-late diagenetic stage) and the epidiagenetic stage. (2) Quantitative fitting relationships among various parameters allow a great significance to describe the spatial structure, the regional distribution and the growth environment of mud cracks. (3) Mud crack growth has three models, such as the unilateral growth model including the linear growth pattern, the curvilinear growth pattern and the bifurcation growth pattern, the multilateral growth model including the intersectional growth pattern, the join growth pattern and the dispersed growth pattern, and the mixed growth model including the combination of any patterns listed above. (4) Modern mud crack growth usually undergoes four stages. Sand beds in sand-mud rhythmic strata can play a lubricative role on crack growth and provide enough sandy deposits for filling cracks. (5) Mud crack growth usually produces bifurcation and bifurcation angles which are mostly 120° or 90° that are related to sediment heterogeneity and released energy. (6) Factors affecting mud crack growth cover many aspects: clay content and salinity can control the number of mud cracks in different areas;terrain can control mud crack morphology;and different sedimentary cycles can control the growth patterns and filling models of mud cracks.

  8. Misunderstanding and Understanding of Primary Water Stress Corrosion Cracking of Structural Components in the Primary System of PWRs

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Young Suk; Kim, Sung Soo; Kim, Dae Whan [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2014-05-15

    All the structural components in the primary system of pressurized water reactors that are in contact with primary water are made of austenitic Ni-Cr-Fe alloys which are known to be corrosion resistant. Nevertheless, these Ni-Cr-Fe alloys such as Alloy 600, weld 182/82, austenitic stainless steels suffer from intergranular stress corrosion cracking (IGSCC) after their 10 year operation in reactors although the environment to which they have been exposed is almost pure water of pH 6.9 to 7.2, which is called primary water stress corrosion cracking (PWSCC). Given that the underlying mechanism of PWSCC remains unidentified so far, there are many misunderstandings related to PWSCC of the structural components, which may lead to unreasonable mitigation measures. The aim of this work is to highlight understanding and misunderstanding of PWSCC related to austenitic Ni-Cr-Fe alloys.

  9. A New Method of Retarding Fatigue Crack Growth on Pressure Vessels

    Institute of Scientific and Technical Information of China (English)

    Jianzhong YIN; Yanyan WANG; Xinwei DING

    2001-01-01

    An artificial wedge to retard fatigue crack growth in tension has been investigated. The results show that an artificial wedge can reduce the growth rate of fatigue crack on Surface fatigue crack and, the fatigue crack growth behavior is essentially similar in-depth and width directions. Based on a theoretical analysis, a model for the effective crack growth parameter △Keff is presented. It is shown that the relationships between the calculated △Keff value and crack speed are almost the same as those of cracked specimens without a wedge. Therefore this model can be applied to estimate retardation behavior.

  10. Modelling of iodine-induced stress corrosion cracking in CANDU fuel

    Science.gov (United States)

    Lewis, B. J.; Thompson, W. T.; Kleczek, M. R.; Shaheen, K.; Juhas, M.; Iglesias, F. C.

    2011-01-01

    Iodine-induced stress corrosion cracking (I-SCC) is a recognized factor for fuel-element failure in the operation of nuclear reactors requiring the implementation of mitigation measures. I-SCC is believed to depend on certain factors such as iodine concentration, oxide layer type and thickness on the fuel sheath, irradiation history, metallurgical parameters related to sheath like texture and microstructure, and the mechanical properties of zirconium alloys. This work details the development of a thermodynamics and mechanistic treatment accounting for the iodine chemistry and kinetics in the fuel-to-sheath gap and its influence on I-SCC phenomena. The governing transport equations for the model are solved with a finite-element technique using the COMSOL Multiphysics® commercial software platform. Based on this analysis, this study also proposes potential remedies for I-SCC.

  11. DEVELOPMENT OF SOFTWARE SYSTEM FOR MONITORING OF STRESS CORROSION CRACKING OF THE PIPELINE UNDER TENSION

    Directory of Open Access Journals (Sweden)

    Z. K. Abaev

    2016-01-01

    Full Text Available The software and hardware development tendency, providing the automated monitoring and control of basic and auxiliary technological processes of gas transportation via system of main gas pipelines has been revealed. The article discusses the stages of creation of the software of system of monitoring corrosion cracking under tension (SCC. The new useful adequate regression models development determining the risk level of LCC is shown. A ranking sections algorithm of main gas pipeline (MG on the propensity to SCC is presented. Adequate developed regression equation determining the LCC risk level has been developed. To count the main gas pipeline lifetime the variable rank of the danger of SCC (RSCC on the basis of methods of fuzzy logic is proposed to use. Implementation of the fuzzy model was carried out using the graphical tools developed in MATLAB using the expansion pack Fuzzy Logic Toolbox. The working algorithm of developed program and the screen forms are presented.

  12. Localized Deformation as a Primary Cause of Irradiation Assisted Stress Corrosion Cracking

    Energy Technology Data Exchange (ETDEWEB)

    Gary S. Was

    2009-03-31

    The objective of this project is to determine whether deformation mode is a primary factor in the mechanism of irradiation assisted intergranular stress corrosion cracking of austenitic alloys in light watert reactor core components. Deformation mode will be controlled by both the stacking fault energy of the alloy and the degree of irradiation. In order to establish that localized deformation is a major factor in IASCC, the stacking fault energies of the alloys selected for study must be measured. Second, it is completely unknown how dose and SFE trade-off in terms of promoting localized deformation. Finally, it must be established that it is the localized deformation, and not some other factor that drives IASCC.

  13. Characterization of the Resistance of Alloy 22 to Stress Corrosion Cracking

    Energy Technology Data Exchange (ETDEWEB)

    King, K J; Estill, J C; Rebak, R B

    2002-05-30

    In its current design, the high-level nuclear waste containers include an external layer of Alloy 22 (Ni-22Cr-13Mo-3W-3Fe). Since over their lifetime, the containers may be exposed to multi-ionic aqueous environments, a potential degradation mode of the outer layer could be environmentally assisted cracking (EAC). The objective of the current research was to characterize the effect of applied potential and temperature on the susceptibility of Alloy 22 to EAC in simulated concentrated water (SCW) using the slow strain rate test (SSRT). Results show that Alloy 22 may suffer EAC at applied potentials approximately 400 mV more anodic than the corrosion potential (E{sub corr}).

  14. Researches on corrosion cracking phenomenonthat occurs on welded of agricultural equipment

    Directory of Open Access Journals (Sweden)

    I. Sărăcin

    2015-04-01

    Full Text Available Welded construction equipments for agriculture are strongly stressed in terms of mechanics, but also in terms of environmental action and thus in many cases appears their wear by corrosion cracking phenomenon. After research it was noted that after a certain period of use of equipment, metallographic structure of welded steel structures has changed substantially and at the same time a change in the chemical composition of steel was also observed. In terms of chemical composition a reduction in carbon content was mainly observed, and an increase in sulfur content,determined mainly by the presence of large quantities of sulfur in the atmosphere. This sulfur in the atmosphere at the same time determines the acid action on metallic materials, by forming with water from precipitation of H2S.

  15. Numerical simulation of stable fatigue crack growth rate using a cohesive zone model

    NARCIS (Netherlands)

    Silitonga, S.; Maljaars, J.; Soetens, F.; Snijder, H.H.

    2012-01-01

    Predicting the remaining fatigue life of a structure with crack(s) is generally conducted by the fracture mechanics method. This method is aimed at predicting the crack growth and final fracture due to fluctuating loads. The crack growth curve required for these calculations is constructed on the ba

  16. Analysis of Fatigue Crack Growth in Ship Structural Details

    Directory of Open Access Journals (Sweden)

    Leheta Heba W.

    2016-04-01

    Full Text Available Fatigue failure avoidance is a goal that can be achieved only if the fatigue design is an integral part of the original design program. The purpose of fatigue design is to ensure that the structure has adequate fatigue life. Calculated fatigue life can form the basis for meaningful and efficient inspection programs during fabrication and throughout the life of the ship. The main objective of this paper is to develop an add-on program for the analysis of fatigue crack growth in ship structural details. The developed program will be an add-on script in a pre-existing package. A crack propagation in a tanker side connection is analyzed by using the developed program based on linear elastic fracture mechanics (LEFM and finite element method (FEM. The basic idea of the developed application is that a finite element model of this side connection will be first analyzed by using ABAQUS and from the results of this analysis the location of the highest stresses will be revealed. At this location, an initial crack will be introduced to the finite element model and from the results of the new crack model the direction of the crack propagation and the values of the stress intensity factors, will be known. By using the calculated direction of propagation a new segment will be added to the crack and then the model is analyzed again. The last step will be repeated until the calculated stress intensity factors reach the critical value.

  17. Crack Growth Modeling and Life Prediction of Pipeline Steels Exposed to Near-Neutral pH Environments: Dissolution Crack Growth and Occurrence of Crack Dormancy in Stage I

    Science.gov (United States)

    Zhao, Jiaxi; Chen, Weixing; Yu, Mengshan; Chevil, Karina; Eadie, Reg; Van Boven, Greg; Kania, Richard; Been, Jenny; Keane, Sean

    2017-04-01

    This investigation was initiated to provide governing equations for crack initiation, crack growth, and service life prediction of pipeline steels in near-neutral pH (NNpH) environments. This investigation has focused on the crack initiation and early-stage crack growth. The investigation considered a wide range of conditions that could lead to crack initiation, crack dormancy, and crack transition from a dormant state to active growth. It is concluded that premature rupture caused by stress cracking at a service life of about 20 to 30 years previously observed during field operation could take place only when the worst conditions responsible for crack initiation and growth have been realized concurrently at the site of rupture. This also explains the reason that over 95 pct of NNpH cracks remain harmless, while about 1 pct of them become a threat to the integrity of pipeline steels.

  18. Irradiation-assisted stress corrosion cracking behavior of austenitic stainless steels applicable to LWR core internals.

    Energy Technology Data Exchange (ETDEWEB)

    Chung, H. M.; Shack, W. J.; Energy Technology

    2006-01-31

    This report summarizes work performed at Argonne National Laboratory on irradiation-assisted stress corrosion cracking (IASCC) of austenitic stainless steels that were irradiated in the Halden reactor in simulation of irradiation-induced degradation of boiling water reactor (BWR) core internal components. Slow-strain-rate tensile tests in BWR-like oxidizing water were conducted on 27 austenitic stainless steel alloys that were irradiated at 288 C in helium to 0.4, 1.3, and 3.0 dpa. Fractographic analysis was conducted to determine the fracture surface morphology. Microchemical analysis by Auger electron spectroscopy was performed on BWR neutron absorber tubes to characterize grain-boundary segregation of important elements under BWR conditions. At 0.4 and 1.4 dpa, transgranular fracture was mixed with intergranular fracture. At 3 dpa, transgranular cracking was negligible, and fracture surface was either dominantly intergranular, as in field-cracked core internals, or dominantly ductile or mixed. This behavior indicates that percent intergranular stress corrosion cracking determined at {approx}3 dpa is a good measure of IASCC susceptibility. At {approx}1.4 dpa, a beneficial effect of a high concentration of Si (0.8-1.5 wt.%) was observed. At {approx}3 dpa, however, such effect was obscured by a deleterious effect of S. Excellent resistance to IASCC was observed up to {approx}3 dpa for eight heats of Types 304, 316, and 348 steel that contain very low concentrations of S. Susceptibility of Types 304 and 316 steels that contain >0.003 wt.% S increased drastically. This indicates that a sulfur related critical phenomenon plays an important role in IASCC. A sulfur content of <0.002 wt.% is the primary material factor necessary to ensure good resistance to IASCC. However, for Types 304L and 316L steel and their high-purity counterparts, a sulfur content of <0.002 wt.% alone is not a sufficient condition to ensure good resistance to IASCC. This is in distinct contrast to

  19. Irradiation-assisted stress corrosion cracking behavior of austenitic stainless steels applicable to LWR core internals.

    Energy Technology Data Exchange (ETDEWEB)

    Chung, H. M.; Shack, W. J.; Energy Technology

    2006-01-31

    This report summarizes work performed at Argonne National Laboratory on irradiation-assisted stress corrosion cracking (IASCC) of austenitic stainless steels that were irradiated in the Halden reactor in simulation of irradiation-induced degradation of boiling water reactor (BWR) core internal components. Slow-strain-rate tensile tests in BWR-like oxidizing water were conducted on 27 austenitic stainless steel alloys that were irradiated at 288 C in helium to 0.4, 1.3, and 3.0 dpa. Fractographic analysis was conducted to determine the fracture surface morphology. Microchemical analysis by Auger electron spectroscopy was performed on BWR neutron absorber tubes to characterize grain-boundary segregation of important elements under BWR conditions. At 0.4 and 1.4 dpa, transgranular fracture was mixed with intergranular fracture. At 3 dpa, transgranular cracking was negligible, and fracture surface was either dominantly intergranular, as in field-cracked core internals, or dominantly ductile or mixed. This behavior indicates that percent intergranular stress corrosion cracking determined at {approx}3 dpa is a good measure of IASCC susceptibility. At {approx}1.4 dpa, a beneficial effect of a high concentration of Si (0.8-1.5 wt.%) was observed. At {approx}3 dpa, however, such effect was obscured by a deleterious effect of S. Excellent resistance to IASCC was observed up to {approx}3 dpa for eight heats of Types 304, 316, and 348 steel that contain very low concentrations of S. Susceptibility of Types 304 and 316 steels that contain >0.003 wt.% S increased drastically. This indicates that a sulfur related critical phenomenon plays an important role in IASCC. A sulfur content of <0.002 wt.% is the primary material factor necessary to ensure good resistance to IASCC. However, for Types 304L and 316L steel and their high-purity counterparts, a sulfur content of <0.002 wt.% alone is not a sufficient condition to ensure good resistance to IASCC. This is in distinct contrast to

  20. Brittle-tough transitions during crack growth in toughened adhesives

    Science.gov (United States)

    Thoules, Michael

    2008-03-01

    The use of structural adhesives in automotive applications relies on an effective understanding of their performance under crash conditions. In particular, there is considerable potential for mechanics-based modeling of the interaction between an adhesive layer and the adherends, to replace current empirical approaches to design. Since energy dissipation during a crash, mediated by plastic deformation of the structure, is a primary consideration for automotive applications, traditional approaches of fracture mechanics are not appropriate. Cohesive-zone models that use two fracture parameters - cohesive strength and toughness - have been shown to provide a method for quantitative mechanics analysis. Combined numerical and experimental techniques have been developed to deduce the toughness and strength parameters of adhesive layers, allowing qualitative modeling of the performance of adhesive joints. These techniques have been used to study the failure of joints, formed from a toughened adhesive and sheet metal, over a wide range of loading rates. Two fracture modes are observed: quasi-static crack growth and dynamic crack growth. The quasi-static crack growth is associated with a toughened mode of failure; the dynamic crack growth is associated with a more brittle mode of failure. The results of the experiments and analyses indicate that the fracture parameters for quasi-static crack growth in this toughened system are essentially rate independent, and that quasi-static crack growth can occur even at the highest crack velocities. Effects of rate appear to be limited to the ease with which a transition to dynamic fracture could be triggered. This transition appears to be stochastic in nature, and it does not appear to be associated with the attainment of any critical value for crack velocity or loading rate. Fracture-mechanics models exist in the literature for brittle-ductile transitions in rate-dependent polymers, which rely on rate dependent values of toughness

  1. Dependence of crack growth kinetics on dendrite orientation and water chemistry for Alloy 182 weld metal in high-temperature water

    Energy Technology Data Exchange (ETDEWEB)

    Lu, Zhanpeng, E-mail: zplu@shu.edu.cn [Institute of Materials Science, School of Materials Science and Engineering, Shanghai University, Shanghai 200072 (China); New Industry Creation Hatchery Center, Tohoku University, Sendai 980-8579 (Japan); Chen, Junjie [Institute of Materials Science, School of Materials Science and Engineering, Shanghai University, Shanghai 200072 (China); Shoji, Tetsuo [New Industry Creation Hatchery Center, Tohoku University, Sendai 980-8579 (Japan); Meng, Fanjiang [Shanghai Nuclear Engineering Research & Design Institute, Shanghai 200233 (China)

    2015-03-15

    Highlights: • SCC paths along dendrite directions in both T–S and T–L specimens of Alloy 182. • Higher SCC growth rates in T–S orientation specimen than in T–L orientation specimen. • CGR increased with increasing dissolved oxygen. • Apparently negative da/dt curve by ACPD in hydrogen saturated water. - Abstract: Stress corrosion cracking growth rates of Alloy 182 weld metals in T–S and T–L orientations in 288 °C pure water with various dissolved oxygen and hydrogen concentrations were measured. Extensive inter-dendritic stress corrosion cracking paths on the side surfaces and fracture surfaces were observed. The crack growth path in the T–S orientation specimen was perpendicular to the applied loading direction, and parallel to the loading direction in the T–L specimen. Crack growth rates of the T–S specimen were significantly higher than those of the T–L specimen under the same test conditions. The crack growth rate decreased significantly with decreasing dissolved oxygen concentration. Adding dissolved hydrogen in water caused an apparent decrease of the alternating current potential drop signal during crack growth monitoring.

  2. Fracture model for predicting concrete cover-cracking induced by steel corrosion based on interface bond state

    Institute of Scientific and Technical Information of China (English)

    WANG Xian-li; ZHENG Jian-jun; WU Zhi-min

    2009-01-01

    Time-to-cracking of the concrete cover induced by the steel corrosion is one of the critical problems faced by engineers, operators and asset managers in making strategies for the maintenance and repairs of reinforced concrete (RC)structures affected by corrosion. In this paper, a theoretical model for predicting the time-to-cracking is derived by assuming the bond between the steel bar and the concrete as a linear combination of perfectly smooth and bonded. The model takes into account the characteristics of existing exiguous flaws and initial cracks in the concrete before the load acting on RC structures. The validity of the proposed model is preliminarily verified by comparing the obtained results with the available experimental results. A remarkable advantage of the proposed method is its application to the prediction of the service life of RC structures, made of the deformed steel bars as well as the round bars. By determining an experimental constant α, which is related to the interface bond state between the steel bar and the concrete, the service life of RC structures can be predicted using the proposed scheme. Analysis of major factors affecting the time-to-cracking demonstrates that the length of the initial crack affects the service life of RC structures significantly. Moreover, the larger cover thickness and the smaller diameter of the steel bar within a certain range are beneficial to prolonging the time-to-cracking.

  3. Stress-corrosion cracking of steels in ammonia with consideration given to OTEC design: a survey

    Energy Technology Data Exchange (ETDEWEB)

    Teel, R.B.

    1980-03-01

    Carbon steel, alloy steel, and high-strength, quenched and tempered steel, when under applied or residual stress and especially when cold formed and/or welded without subsequent thermal stress relief, are subject to failure by stress-corrosion cracking (SCC) in air-contaminated dry ammonia. Water as well as hydrazine when present in small amounts have been shown to be effective inhibitors in an all steel system. Galvanic corrosion between dissimilar metals and/or accelerated failure by SCC of stressed steel as a result of galvanic coupling may be of concern. Where water has proven effective as an inhibitor of SCC in an all steel system, it may not be adequate in a mixed metal system. With aluminum tubes, the tube sheet will either have to be solid aluminum, aluminum clad steel or some nonconductive coating will be necessary to effectively remove the cathodic alloy from the galvanic circuit. Research is required to determine the severity of the coupling effect between dissimilar alloys in ammonia under OTEC conditions; especially the possibility of accelerated SCC failures of stressed steel where the presence of an inhibitor in the ammonia may not be sufficient to override the galvanic coupling effect.

  4. Corrosion Behavior of Steel Reinforcement in Concrete with Recycled Aggregates, Fly Ash and Spent Cracking Catalyst

    Directory of Open Access Journals (Sweden)

    Hebé Gurdián

    2014-04-01

    Full Text Available The main strategy to reduce the environmental impact of the concrete industry is to reuse the waste materials. This research has considered the combination of cement replacement by industrial by-products, and natural coarse aggregate substitution by recycled aggregate. The aim is to evaluate the behavior of concretes with a reduced impact on the environment by replacing a 50% of cement by industrial by-products (15% of spent fluid catalytic cracking catalyst and 35% of fly ash and a 100% of natural coarse aggregate by recycled aggregate. The concretes prepared according to these considerations have been tested in terms of mechanical strengths and the protection offered against steel reinforcement corrosion under carbonation attack and chloride-contaminated environments. The proposed concrete combinations reduced the mechanical performance of concretes in terms of elastic modulus, compressive strength, and flexural strength. In addition, an increase in open porosity due to the presence of recycled aggregate was observed, which is coherent with the changes observed in mechanical tests. Regarding corrosion tests, no significant differences were observed in the case of the resistance of these types of concretes under a natural chloride attack. In the case of carbonation attack, although all concretes did not stand the highly aggressive conditions, those concretes with cement replacement behaved worse than Portland cement concretes.

  5. Corrosion resistance of a steel under an oxidizing atmosphere in a fluid catalytic cracking regenerator

    Directory of Open Access Journals (Sweden)

    Ieda Caminha

    2004-03-01

    Full Text Available In the present work, the corrosion resistance of an ASTM A 387 G11 steel was evaluated under two conditions: an oxidizing atmosphere in a fluid catalytic cracking regenerator of a petroleum processing unit and a simulated atmosphere in the laboratory, at temperatures of 650 °C and 700 °C. The characterization of the phases present in the oxidized layer was carried out by X-ray diffraction (XRD, optical microscopy (OM and scanning electron microscopy (SEM with X-ray energy dispersive analysis (EDS. Severe corrosion was observed after exposure to both the real and simulated conditions, with formation of several iron oxides (Fe2O3, Fe3O4 and FeO in the product scale layer, as well as a slight inner oxidation and sulfidation of chromium in the substrate. Internal nitridation of the silicon and the manganese was observed only in the real condition, probably related to the long-term exposure inside the regenerator.

  6. Analysis of hygral induced crack growth in multiphase materials

    NARCIS (Netherlands)

    Sadouki, H.; Van Mier, J.G.M.

    1996-01-01

    In this paper a numerical model for simulating crack growth processes caused by moisture movement in a porous multiphase material like concrete is proposed. In the model, the material is schematized as a regular triangular network of beam elements. The meso-material structure of the material is proj

  7. Probabilistic Model for Fatigue Crack Growth in Welded Bridge Details

    DEFF Research Database (Denmark)

    Toft, Henrik Stensgaard; Sørensen, John Dalsgaard; Yalamas, Thierry

    2013-01-01

    In the present paper a probabilistic model for fatigue crack growth in welded steel details in road bridges is presented. The probabilistic model takes the influence of bending stresses in the joints into account. The bending stresses can either be introduced by e.g. misalignment or redistributio...

  8. A computational study of the time dependent crack growth process

    Energy Technology Data Exchange (ETDEWEB)

    Brust, F.W.; Krishnaswamy, P.

    1992-01-01

    Universal studies of creep crack growth for (1) constant load and (2) variable load cases are presented. Results of the constant load cases is compared to experiment. The behavior of displacements and integral creep for fracture parameters are discussed for both load cases. The need for using a constitutive law which can handle cyclic creep is discussed.

  9. Status report: Intergranular stress corrosion cracking of BWR core shrouds and other internal components

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1996-03-01

    On July 25, 1994, the US Nuclear Regulatory Commission (NRC) issued Generic Letter (GL) 94-03 to obtain information needed to assess compliance with regulatory requirements regarding the structural integrity of core shrouds in domestic boiling water reactors (BWRs). This report begins with a brief description of the safety significance of intergranular stress corrosion cracking (IGSCC) as it relates to the design and function of BWR core shrouds and other internal components. It then presents a brief history of shroud cracking events both in the US and abroad, followed by an indepth summary of the industry actions to address the issue of IGSCC in BWR core shrouds and other internal components. This report summarizes the staff`s basis for issuing GL 94-03, as well as the staff`s assessment of plant-specific responses to GL 94-03. The staff is continually evaluating the licensee inspection programs and the results from examinations of BWR core shrouds and other internal components. This report is representative of submittals to and evaluations by the staff as of September 30, 1995. An update of this report will be issued at a later date.

  10. Effect of Nanostructure Changes on Stress Corrosion Cracking of Proton Irradiated Nuclear Energy Structural Materials

    Directory of Open Access Journals (Sweden)

    M.N. Lunika

    2011-01-01

    Full Text Available Austenitic stainless alloys are used extensively as structural materials in the internal components of light water reactor (LWR pressure vessels because of their relatively high strength, ductility, and fracture toughness. Irradiation-assisted stress corrosion cracking (IASCC is main degradation process that affects LWR internal components exposed to radiation. The existing data on proton irradiated austenitic alloys were reviewed to evaluate the effects of key parameters such as material composition, irradiation dose on IASCC susceptibility of these materials in LWR environments. The significance of deformation nanostructure and stacking fault energy (SFE changes in the material on IASCC susceptibility is also discussed. Results show that the IASCC susceptibility of the alloys increases with increasing irradiation dose and decreasing stacking fault energy. IASCC tends to initiate at locations where slip dislocation channels intersect grain boundaries. Localized deformation in the form of grain boundary sliding due to the interaction of slip channels and grain boundaries is likely the primary cause of the observed cracking initiation. It may play a key role in the underlying mechanism of IASCC in light water reactor core components.

  11. Reconstruction of stress corrosion cracks using signals of pulsed eddy current testing

    Science.gov (United States)

    Wang, Li; Xie, Shejuan; Chen, Zhenmao; Li, Yong; Wang, Xiaowei; Takagi, Toshiyuki

    2013-06-01

    A scheme to apply signals of pulsed eddy current testing (PECT) to reconstruct a deep stress corrosion crack (SCC) is proposed on the basis of a multi-layer and multi-frequency reconstruction strategy. First, a numerical method is introduced to extract conventional eddy current testing (ECT) signals of different frequencies from the PECT responses at different scanning points, which are necessary for multi-frequency ECT inversion. Second, the conventional fast forward solver for ECT signal simulation is upgraded to calculate the single-frequency pickup signal of a magnetic field by introducing a strategy that employs a tiny search coil. Using the multiple-frequency ECT signals and the upgraded fast signal simulator, we reconstructed the shape profiles and conductivity of an SCC at different depths layer-by-layer with a hybrid inversion scheme of the conjugate gradient and particle swarm optimisation. Several modelled SCCs of rectangular or stepwise shape in an SUS304 plate are reconstructed from simulated PECT signals with artificial noise. The reconstruction results show better precision in crack depth than the conventional ECT inversion method, which demonstrates the validity and efficiency of the proposed PECT inversion scheme.

  12. STRESS CORROSION CRACKING SUSCEPTIBILITY OF HIGH LEVEL WASTE TANKS DURING SLUDGE MASS REDUCTION

    Energy Technology Data Exchange (ETDEWEB)

    Subramanian, K

    2007-10-18

    Aluminum is a principal element in alkaline nuclear sludge waste stored in high level waste (HLW) tanks at the Savannah River Site. The mass of sludge in a HLW tank can be reduced through the caustic leaching of aluminum, i.e. converting aluminum oxides (gibbsite) and oxide-hydroxides (boehmite) into soluble hydroxides through reaction with a hot caustic solution. The temperature limits outlined by the chemistry control program for HLW tanks to prevent caustic stress corrosion cracking (CSCC) in concentrated hydroxide solutions will potentially be exceeded during the sludge mass reduction (SMR) campaign. Corrosion testing was performed to determine the potential for CSCC under expected conditions. The experimental test program, developed based upon previous test results and expected conditions during the current SMR campaign, consisted of electrochemical and mechanical testing to determine the susceptibility of ASTM A516 carbon steel to CSCC in the relevant environment. Anodic polarization test results indicated that anodic inhibition at the temperatures and concentrations of interest for SMR is not a viable, consistent technical basis for preventing CSCC. However, the mechanical testing concluded that CSCC will not occur under conditions expected during SMR for a minimum of 35 days. In addition, the stress relief for the Type III/IIIA tanks adds a level of conservatism to the estimates. The envelope for corrosion control is recommended during the SMR campaign is shown in Table 1. The underlying assumption is that solution time-in-tank is limited to the SMR campaign. The envelope recommends nitrate/aluminate intervals for discrete intervals of hydroxide concentrations, although it is recognized that a continuous interval may be developed. The limits also sets temperature limits.

  13. Numerical simulation of fatigue crack growth rate and crack retardation due to an overload using a cohesive zone model

    NARCIS (Netherlands)

    Silitonga, S.; Maljaars, J.; Soetens, F.; Snijder, H.H.

    2014-01-01

    In this work, a numerical method is pursued based on a cohesive zone model (CZM). The method is aimed at simulating fatigue crack growth as well as crack growth retardation due to an overload. In this cohesive zone model, the degradation of the material strength is represented by a variation of the

  14. Assessment of the Efficiency of HWCon IASCC Crack Growth Rate for High Fluence BWRMaterials

    Energy Technology Data Exchange (ETDEWEB)

    Teysseyre, Sebastien Paul [Idaho National Lab. (INL), Idaho Falls, ID (United States)

    2016-09-01

    This report describes the experimental study performed to assess the efficiency of hydrogen water chemistry on the propagation rate of cracks generated by irradiation assisted stress corrosion cracking in high fluence material. The selection of the material and the test procedures followed for this study are presented. The test results obtained with 8.6 dpa specimen are discussed.

  15. Sub-critical crack growth in silicate glasses: Role of network topology

    Energy Technology Data Exchange (ETDEWEB)

    Smedskjaer, Morten M., E-mail: mos@bio.aau.dk [Department of Chemistry and Bioscience, Aalborg University, 9220 Aalborg (Denmark); Bauchy, Mathieu [Department of Civil and Environmental Engineering, University of California, Los Angeles, California 90095 (United States)

    2015-10-05

    The presence of water in the surrounding atmosphere can cause sub-critical crack growth (SCCG) in glasses, a phenomenon known as fatigue or stress corrosion. Here, to facilitate the compositional design of more fatigue-resistant glasses, we investigate the composition dependence of SCCG by studying fourteen silicate glasses. The fatigue curves (V-K{sub I}) have been obtained by indentation experiments through measurements of the crack length as a function of post-indentation fatigue duration. Interestingly, we find that the fatigue resistance parameter N is generally improved by increasing the alumina content and is thereby found to exhibit a fairly linear dependence on the measured Vickers hardness H{sub V} for a wide range of N and H{sub V} values. This finding highlights the important role of network topology in governing the SCCG in silicate glasses, since hardness has been shown to scale linearly with the number of atomic constraints. Our results therefore suggest that glasses showing under-constrained flexible networks, which feature floppy internal modes of deformation, are more readily attacked by water molecules, thus promoting stress corrosion and reducing the fatigue resistance.

  16. INVESTIGATION OF THE POTENTIAL FOR CAUSTIC STRESS CORROSION CRACKING OF A537 CARBON STEEL NUCLEAR WASTE TANKS

    Energy Technology Data Exchange (ETDEWEB)

    Lam, P.

    2009-10-15

    The evaporator recycle streams contain waste in a chemistry and temperature regime that may be outside of the current waste tank corrosion control program, which imposes temperature limits to mitigate caustic stress corrosion cracking (CSCC). A review of the recent service history (1998-2008) of Tanks 30 and 32 showed that these tanks were operated in highly concentrated hydroxide solution at high temperature. Visual inspections, experimental testing, and a review of the tank service history have shown that CSCC has occurred in uncooled/un-stress relieved F-Area tanks. Therefore, for the Type III/IIIA waste tanks the efficacy of the stress relief of welding residual stress is the only corrosion-limiting mechanism. The objective of this experimental program is to test carbon steel small scale welded U-bend specimens and large welded plates (12 x 12 x 1 in.) in a caustic solution with upper bound chemistry (12 M hydroxide and 1 M each of nitrate, nitrite, and aluminate) and temperature (125 C). These conditions simulate worst-case situations in Tanks 30 and 32. Both as-welded and stress-relieved specimens have been tested. No evidence of stress corrosion cracking was found in the U-bend specimens after 21 days of testing. The large plate test is currently in progress, but no cracking has been observed after 9 weeks of immersion. Based on the preliminary results, it appears that the environmental conditions of the tests are unable to develop stress corrosion cracking within the duration of these tests.

  17. Crack growth through low-cycle fatigue loading of material ARMOX 500T

    Directory of Open Access Journals (Sweden)

    V. Pepel

    2016-10-01

    Full Text Available This paper presents microstructure analysis of the creation and growth of cracks in uniaxial load. Analyse were done for steel Armox 500T (armour sheet. Results show that cracks are present quit early in steel lifetime. First micro cracks occur before the 200th cycles, whereby crack growth is progressive during further loading. Also it can be seen that after a certain number of cycles there are more longer cracks then shorter ones.

  18. STUDY ON THE SURFACE CRACK GROWTH BEHAVIOR IN 14MnNbq BRIDGE STEEL

    Institute of Scientific and Technical Information of China (English)

    Yanping Liu; Chuanyao Chen; Guoqing Li

    2010-01-01

    Three-dimensional crack closure correction methods are investigated in this paper.The fatigue crack growth tests of surface cracks in 14MnNbq steel for bridge plate subjected to tensile and bending loadings are systematically conducted.The experimentally measured fatigue crack growth rates of surface cracks are compared with those of through-thickness cracks in detail.It is found that the crack growth rates of surface cracks are lower than those of through-thickness cracks.In order to correct their differences in fatigue crack growth rates,a dimensionless crack closure correction model is proposed.Although this correction model is determined only by the experimental data of surface cracks under tensile loading with a constant ratio R=0.05,it can correlate the surface crack growth rates with reasonable accuracy under tensile and bending loadings with various stress ratios ranging from 0 to 0.5.Furthermore,predictions of fatigue life and crack aspect ratio for surface cracks are discussed,and the predicted results are also compared with those obtained from other prediction approaches.Comparison results show that the proposed crack closure correction model gives better prediction of fatigue life than other models.

  19. Effects of crack depth and specimen size on ductile crack growth of SENT and SENB specimens for fracture mechanics evaluation of pipeline steels

    Energy Technology Data Exchange (ETDEWEB)

    Xu, J. [Department of Structural Engineering, Norwegian University of Science and Technology (NTNU), Richard Birkelands vei 1a, N-7491 Trondheim (Norway); School of Materials Science and Engineering, University of Science and Technology Beijing (USTB), 100083 Beijing (China); Zhang, Z.L., E-mail: zhiliang.zhang@ntnu.n [Department of Structural Engineering, Norwegian University of Science and Technology (NTNU), Richard Birkelands vei 1a, N-7491 Trondheim (Norway); Ostby, E.; Nyhus, B. [SINTEF, Materials and Chemistry, N-7465 Trondheim (Norway); Sun, D.B. [School of Materials Science and Engineering, University of Science and Technology Beijing (USTB), 100083 Beijing (China)

    2009-12-15

    A strong geometry dependence of ductile crack growth resistance emerges under large scale yielding. The geometry dependence is associated with different levels of crack tip constraint conditions. However, in a recent attempt to identify appropriate fracture mechanics specimens for pipeline steels, an 'independent' relationship between the crack growth resistance curves and crack depths for SENT specimens has been observed experimentally. In this paper, we use the complete Gurson model to study the effects of crack depth and specimen size on ductile crack growth behavior. Crack growth resistance curves for plane strain, mode I crack growth under large scale yielding conditions have been computed. SENB and SENT specimens with three different specimen sizes, each specimen size with three different crack depths, have been selected. It has been found that crack tip constraint (Q-parameter) has a weak dependence on the crack depth for specimens in the low constraint regime.

  20. Stress corrosion cracking of welded joints of super-martensitic stainless steel in H{sub 2}S free environment

    Energy Technology Data Exchange (ETDEWEB)

    Hoerner, Bertrand; Bayle, Bernard; Delafosse, David [Centre Science des Materiaux et des Structures - URA CNRS 5146, ENS Mines de Saint-Etienne, 158 Cours Fauriel, 42023 Saint-Etienne cedex 02 (France); Ligier, Vincent [CRMC, INDUSTEEL Creusot, 56, rue Clemenceau, BP 56 - 71 202 Le Creusot Cedex (France)

    2004-07-01

    Due to their combination of good weldability and good mechanical properties, low carbon super-martensitic stainless steels are good candidates for oil and gas flow line applications. These alloys have already been used in slightly sour environments containing chlorides, CO{sub 2} and H{sub 2}S. The properties of a welded joint whose composition is matching or superduplex that of the base metal are investigated. The base material is the super-martensitic stainless steels medium alloy: 13Cr-4.5Ni-1.5Mo. The Heat Affected Zone (HAZ) of girth welds may be sensitive to stress corrosion cracking and presents distinct features intergranular cracking when tested in four-point bending in a sour deaerated environment at temperatures around 100 deg. C. The electrochemical properties of the medium alloy and the matching welded joint + HAZ were determined in a chloride-containing environment without H{sub 2}S. A passive film is formed on polished samples. This film is less protective for the welded joint + HAZ samples than in the base metal. Moreover, the pitting corrosion resistance is strongly decreased in the HAZ. Slow strain rate tensile tests were conducted in a de-aerated solution without H{sub 2}S. They reproduce the same type of cracking as was observed in four point bending tests in a sour environment: initiation in the HAZ and an intergranular crack with a very brittle aspect and no significant trace of corrosion. The presence H{sub 2}S is not the prevailing factor for the occurrence of cracking. Furthermore, it is not necessary to have a specific surface condition for crack initiation to occur in slow strain rate tension, as it is the case four point bend tests where initiation appears to be controlled by the surface condition (chemical and / or geometrical). Finally, a simulated PWHT strongly increase the resistance to SSC. (authors)

  1. Predictions for fatigue crack growth life of cracked pipes and pipe welds using RMS SIF approach and experimental validation

    Energy Technology Data Exchange (ETDEWEB)

    Arora, Punit, E-mail: punit@barc.gov.in [Bhabha Atomic Research Centre, Department of Atomic Energy, Maharashtra, Mumbai 400 085 (India); Singh, P.K.; Bhasin, Vivek; Vaze, K.K.; Ghosh, A.K. [Bhabha Atomic Research Centre, Department of Atomic Energy, Maharashtra, Mumbai 400 085 (India); Pukazhendhi, D.M.; Gandhi, P.; Raghava, G. [Structural Engineering Research Centre, Chennai 600 113 (India)

    2011-10-15

    The objective of the present study is to understand the fatigue crack growth behavior in austenitic stainless steel pipes and pipe welds by carrying out analysis/predictions and experiments. The Paris law has been used for the prediction of fatigue crack growth life. To carry out the analysis, Paris constants have been determined for pipe (base) and pipe weld materials by using Compact Tension (CT) specimens machined from the actual pipe/pipe weld. Analyses have been carried out to predict the fatigue crack growth life of the austenitic stainless steel pipes/pipes welds having part through cracks on the outer surface. In the analyses, Stress Intensity Factors (K) have been evaluated through two different schemes. The first scheme considers the 'K' evaluations at two points of the crack front i.e. maximum crack depth and crack tip at the outer surface. The second scheme accounts for the area averaged root mean square stress intensity factor (K{sub RMS}) at deepest and surface points. Crack growth and the crack shape with loading cycles have been evaluated. In order to validate the analytical procedure/results, experiments have been carried out on full scale pipe and pipe welds with part through circumferential crack. Fatigue crack growth life evaluated using both schemes have been compared with experimental results. Use of stress intensity factor (K{sub RMS}) evaluated using second scheme gives better fatigue crack growth life prediction compared to that of first scheme. Fatigue crack growth in pipe weld (Gas Tungsten Arc Welding) can be predicted well using Paris constants of base material but prediction is non-conservative for pipe weld (Shielded Metal Arc Welding). Further, predictions using fatigue crack growth rate curve of ASME produces conservative results for pipe and GTAW pipe welds and comparable results for SMAW pipe welds. - Highlights: > Predicting fatigue crack growth of Austenitic Stainless Steel pipes and pipe welds. > Use of RMS-SIF and

  2. Influence factors on stress corrosion cracking of P110 tubing steel under CO2 injection well annulus environment

    Institute of Scientific and Technical Information of China (English)

    刘然克; 贾静焕; 杜翠薇; 李晓刚

    2016-01-01

    Stress corrosion cracking (SCC) behavior of P110 tubing steel in simulated CO2 injection well annulus environments was investigated through three-point bent tests, potentiodynamic polarization and EIS measurements. The results demonstrate that SCC of P110 tubing steel could occur in acidulous simulated environment, and the sensitivity of SCC increases with the decrease of pH, as well as increase of sulfide concentration and total environmental pressure. Both anodic dissolution and hydrogen embrittlement make contributions to the SCC. Adequate concentration of corrosion inhibitor can inhibit the occurrence of SCC on account of the inhibition of localized anodic dissolution and cathodic hydrogen evolution.

  3. Improved stress corrosion cracking resistance of a novel biodegradable EW62 magnesium alloy by rapid solidification, in simulated electrolytes

    Energy Technology Data Exchange (ETDEWEB)

    Hakimi, O.; Aghion, E. [Department of Materials Engineering, Ben-Gurion University of the Negev, P.O. Box 653, Beer-Sheva 84105 (Israel); Goldman, J., E-mail: jgoldman@mtu.edu [Biomedical Engineering Department, Michigan Technological University, Houghton, MI, 49931 (United States)

    2015-06-01

    The high corrosion rate of magnesium (Mg) and Mg-alloys precludes their widespread acceptance as implantable biomaterials. Here, we investigated the potential for rapid solidification (RS) to increase the stress corrosion cracking (SCC) resistance of a novel Mg alloy, Mg–6%Nd–2%Y–0.5%Zr (EW62), in comparison to its conventionally cast (CC) counterpart. RS ribbons were extrusion consolidated in order to generate bioimplant-relevant geometries for testing and practical use. Microstructural characteristics were examined by SEM. Corrosion rates were calculated based upon hydrogen evolution during immersion testing. The surface layer of the tested alloys was analyzed by X-ray photoelectron spectroscopy (XPS). Stress corrosion resistance was assessed by slow strain rate testing and fractography. The results indicate that the corrosion resistance of the RS alloy is significantly improved relative to the CC alloy due to a supersaturated Nd enrichment that increases the Nd{sub 2}O{sub 3} content in the external oxide layer, as well as a more homogeneous structure and reduced grain size. These improvements contributed to the reduced formation of hydrogen gas and hydrogen embrittlement, which reduced the SCC sensitivity relative to the CC alloy. Therefore, EW62 in the form of a rapidly solidified extruded structure may serve as a biodegradable implant for biomedical applications. - Highlights: • Here we have evaluated the corrosion resistance of a novel Mg alloy (EW62). • Rapid solidification reduces the hydrogen gas evolution and hydrogen embrittlement. • Rapid solidification increases the stress corrosion cracking resistance of EW62. • Improvement is due to enrichment with supersaturated Nd in the external oxide film. • Rapidly solidified and extruded EW62 may serve as a biodegradable medical implant.

  4. Subcritical crack growth in a chemically reactive environment-implications for caprock integrity for CO2 storage

    Science.gov (United States)

    Fan, Z.; Eichhubl, P.; Callahan, O. A.; Major, J. R.; Chen, X.

    2015-12-01

    Seal integrity of cap-rock is a critical constraint on the long term performance of CO2 containment site. During fluid migration, the coupled geochemical reaction of minerals and geomechanical deformation of rock matrix may affect the seal integrity. The potential leakage of injected CO2 from cap-rock through preexisting fractures/faults represents a major concern associated with geological storage of CO2. To address the fundamental question of CO2 leakage through subcritical growth of fractures driven by chemically reactive fluid across caprocks, we build a Dugdale cohesive model. Ahead of the physical crack tip, a narrow band of cohesive zone is assumed to exist with the upper and lower cohesive surfaces held by the cohesive traction. In the vicinity of the crack tip, minerals dissolve due to the acidic environment and migrate from the physical crack tip into the cohesive zone causing damage of rock matrix in the form of a reduction of cohesive traction.Focusing on the dissolution of calcite and following the stress corrosion theory, we assume the degradation of cohesive traction is linearly proportional to the concentration of Ca2+whose evolution follows the reactive diffusion equation. Using a critical crack opening displacement criterion, the subcritical propagation behavior of crack due to stress corrosion is captured and the rate-limiting effects including the chemical reactions to produce the Ca2+ and the transport of minerals along the newly generated fracture cohesive zone are incorporated. Subcritical crack growth rate under different chemical environment conditions is examined and compared with the experimental fracture mechanics testing.

  5. Benefits of thread rolling process to the stress corrosion cracking and fatigue resistance of high strength fasteners

    Energy Technology Data Exchange (ETDEWEB)

    Kephart, A.R.; Hayden, S.Z.

    1993-05-01

    Stress corrosion cracking (SCC) behavior of cut (machined) vice thread rolled Alloy X-750 and Alloy 625 fasteners in a simulated high temperature primary water environment has been evaluated. SCC testing at 360 and 338C included 157 small and 40 large 60{degree} Vee thread studs. Thread rolled fasteners had improved resistance relative to cut fasteners. Tests of fatigue resistance in air at room temperature and both air and primary water at 315C were conducted on smaller studs with both cut and rolled threads. Results showed rolled threads can have significantly improved fatigue lives over those of cut threads in both air and primary water. Fasteners produced by two different thread rolling methods, in-feed (radial) and through-feed (axial), revealed similar SCC initiation test results. Testing of thread rolled fasteners revealed no significant SCC or fatigue growth of rolling induced thread crest laps typical of the thread rolling process. While fatigue resistance differed between the two rolled thread supplier`s studs, neither of the suppliers studs showed SCC initiation at exposure times beyond that of cut threads with SCC. In contrast to rolling at room temperature, warm rolled (427C) threads showed no improvement over cut threads in terms of fatigue resistance. The observed improved SCC and fatigue performance of rolled threads is postulated to be due to interactive factors, including beneficial residual stresses in critically stressed thread root region, reduction of plastic strains during loading and formation of favorable microstructure.

  6. Adaptation of Crack Growth Detection Techniques to US Material Test Reactors

    Energy Technology Data Exchange (ETDEWEB)

    A. Joseph Palmer; Sebastien P. Teysseyre; Kurt L. Davis; Joy L. Rempe; Gordon Kohse; Yakov Ostrovsky; David M. Carpenter

    2014-04-01

    A key component in evaluating the ability of Light Water Reactors to operate beyond 60 years is characterizing the degradation of materials exposed to radiation and various water chemistries. Of particular concern is the response of reactor materials to Irradiation Assisted Stress Corrosion Cracking (IASCC). Some materials testing reactors (MTRs) outside the U.S., such as the Halden Boiling Water Reactor (HBWR), have deployed a technique to measure crack growth propagation during irradiation. This technique incorporates a compact loading mechanism to stress the specimen during irradiation. A crack in the specimen is monitored using the Direct Current Potential Drop (DCPD) method. A project is underway to develop and demonstrate the performance of a similar type of test rig for use in U.S. MTRs. The first year of this three year project was devoted to designing, analyzing, fabricating, and bench top testing a mechanism capable of applying a controlled stress to specimens while they are irradiated in a pressurized water loop (simulating PWR reactor conditions). During the second year, the mechanism will be tested in autoclaves containing high pressure, high temperature water with representative water chemistries. In addition, necessary documentation and safety reviews for testing in a reactor environment will be completed. In the third year, the assembly will be tested in the Massachusetts Institute of Technology Reactor (MITR) and Post Irradiation Examinations (PIE) will be performed.

  7. Layer texture of hot-rolled BCC metals and its significance for stress-corrosion cracking of main gas pipelines

    Science.gov (United States)

    Perlovich, Yu. A.; Isaenkova, M. G.; Krymskaya, O. A.; Morozov, N. S.

    2016-10-01

    Based on data of X-ray texture analysis of hot-rolled BCC materials it was shown that the layerwise texture inhomogeneity of products is formed during their manufacturing. The effect can be explained by saturation with interstitial impurities of the surface layer, resulting in dynamical deformation aging (DDA). DDA prevents the dislocation slip under rolling and leads to an increase of lattice parameters in the external layer. The degree of arising inhomogeneity correlates with the tendency of hot-rolled sheets and obtained therefrom tubes to stress-corrosion cracking under exploitation, since internal layers have a compressive effect on external layers, and prevents opening of corrosion cracks at the tube surface.

  8. Stress corrosion cracking of X70 pipeline steel in near-neutral pH soil solution

    Energy Technology Data Exchange (ETDEWEB)

    Fang, B.Y.; Wang, J.Q.; Han, E.H.; Zhu, Z.Y.; Ke, W. [Chinese Academy of Sciences, Shenyang (China). State Key Laboratory for Corrosion and Protection, Inst. of Metal Research

    2004-07-01

    Near-neutral pH stress corrosion cracking (SCC) is characterized by wide transgranular cracks with quasi-cleavage on the fracture surface, and there is usually little evidence of general or lateral corrosion. Near-neutral pH SCC is related to dissolution and hydrogen ingress into steel pipes because discharged atomic hydrogen can enter the steel so that cracks are initiated or grown by a combination of dissolution and hydrogen-embrittlement. In this study, the SCC cracking behaviour of an X70 pipeline was investigated using slow strain rate tests (SSRT) and cyclic loading at high R and low frequency in a near-neutral pH soil solution saturated with 5 per cent carbon dioxide (CO{sub 2}) and 95 per cent nitrogen (N{sub 2}). Potentiodynamic polarization analyses and electrochemical impedance spectrum (EIS) analyses were also conducted in order to examine the effect of the concentration of bicarbonate, bubbled gas and the addition of chloride ions on polarization behaviour. Results of the SSRT tests showed that transgranular SCC occurred in the soil solution. Crack initiation was associated with pitting. The pipe's susceptibility to SCC increased with decreases in applied electrochemical potential and strain rate. Cyclic loading tests showed that crack propagation processes were dominated by SCC. At high R and low frequencies, SCC was observed on fatigued, pre-cracked specimens. Results of the electrochemical tests showed that polarization behaviours were influenced by the concentrations of bicarbonate, bubbled gas, and the addition of chloride ions. It was concluded that the addition of chloride ion can influence film stability on pipeline specimen surfaces. 22 refs., 2 tabs., 8 figs.

  9. Characteristics of Crack Growth in High Performance Concrete Subjected to Fire

    Institute of Scientific and Technical Information of China (English)

    Gaifei PENG; Sammy Yin Nin CHAN; Jianhua YAN; Yefeng LIU; Quanxin YI

    2005-01-01

    An experimental investigation was conducted to identify the characteristics of crack growth in high performance concrete (HPC) subjected to fire, including two parts of work, I.e. Crack growth resistance determinations and cracking observations, using concrete of three strength grades 40 Mpa, 70 Mpa, and 110 Mpa. The crack growth resistance curves (R-curves) of HPC subjected to high temperatures were determined using notched three-point bend beam specimens of 100 mm×100 mm×300 mm. The R-curve (crack growth resistance curve) flattening shows that the crack growth resistance has been significantly reduced by elevated temperature. Concrete with a higher strength grade has a steeper R-curve, with a higher fracture toughness but a shorter critical crack growth. The shorter critical crack growth means that concrete of a higher strength grade has a more brittle behavior. The concrete cracking observations reveal that the consequences of rapid heating are quite different from those of slow heating. For slow heating at a rate of 0.5℃/min, HPC suffered no obvious cracking below 600℃ even if it had a high moisture content. Explosive spalling is an extreme case of the internal cracking driven mainly by vapor pressure. All these results confirmed the vapor pressure mechanism for spalling behavior which should be more significant for denser concrete. The crack growth ranges obtained from the R-curve determination results are in good agreement with those measured in the concrete cracking observations.

  10. Empirical formulas for description of the fatigue crack growth rate

    Energy Technology Data Exchange (ETDEWEB)

    Rozumek, D. [Opole University of Technology, Faculty of Mechanical Engineering, Opole (Poland)

    2010-02-15

    The paper presents the test results obtained for fatigue crack growth in flat specimens subjected to bending. The tests were conducted for different loading amplitudes and different load ratios using the {delta}J parameter. Accuracy of description of the fatigue crack growth rate was tested with use of different empirical formulas. One-side restrained specimens made of 10HNAP steel were tested. In each tested specimen, there was the external notch 5 mm in depth, and the notch rounding radius was {rho}=0.2 mm. The tests were carried out at the fatigue test stand MZGS-100 under loading frequency 28.8 Hz. It has been found that the obtained results depend on the applied empirical formula. (Abstract Copyright [2010], Wiley Periodicals, Inc.)

  11. ADAPTATION OF CRACK GROWTH DETECTION TECHNIQUES TO US MATERIAL TEST REACTORS

    Energy Technology Data Exchange (ETDEWEB)

    A. Joseph Palmer; Sebastien P. Teysseyre; Kurt L. Davis; Gordon Kohse; Yakov Ostrovsky; David M. Carpenter; Joy L. Rempe

    2015-04-01

    A key component in evaluating the ability of Light Water Reactors to operate beyond 60 years is characterizing the degradation of materials exposed to radiation and various water chemistries. Of particular concern is the response of reactor materials to Irradiation Assisted Stress Corrosion Cracking (IASCC). Some test reactors outside the United States, such as the Halden Boiling Water Reactor (HBWR), have developed techniques to measure crack growth propagation during irradiation. The basic approach is to use a custom-designed compact loading mechanism to stress the specimen during irradiation, while the crack in the specimen is monitored in-situ using the Direct Current Potential Drop (DCPD) method. In 2012 the US Department of Energy commissioned the Idaho National Laboratory and the MIT Nuclear Reactor Laboratory (MIT NRL) to take the basic concepts developed at the HBWR and adapt them to a test rig capable of conducting in-pile IASCC tests in US Material Test Reactors. The first two and half years of the project consisted of designing and testing the loader mechanism, testing individual components of the in-pile rig and electronic support equipment, and autoclave testing of the rig design prior to insertion in the MIT Reactor. The load was applied to the specimen by means of a scissor like mechanism, actuated by a miniature metal bellows driven by pneumatic pressure and sized to fit within the small in-core irradiation volume. In addition to the loader design, technical challenges included developing robust connections to the specimen for the applied current and voltage measurements, appropriate ceramic insulating materials that can endure the LWR environment, dealing with the high electromagnetic noise environment of a reactor core at full power, and accommodating material property changes in the specimen, due primarily to fast neutron damage, which change the specimen resistance without additional crack growth. The project culminated with an in

  12. The susceptibility of 90Cu-10Ni alloy to stress corrosion cracking in seawater polluted by sulfide ions

    Science.gov (United States)

    Domiaty, A. El; Alhajji, J. N.

    1997-08-01

    Electrochemical polarization measurements and slow strain rate tests (SSRT) of a 90Cu-10Ni alloy in highly sulfide polluted seawater were conducted to investigate stress-corrosion cracking (SCC) behavior. The severity of the SCC depends on the sulfide concentration in the seawater. The severity increases as the concentration increases. Because the major time in SCC is spent in the initiation process of the propagating crack, the fracture toughness has only a minor effect in the component life failed by SCC. The SCC behavior of CDA706 is strictly linked to sulfide concentration in the range of 100 to 1000 ppm. The general corrosion of Cu-Ni alloys in low (100 ppm) sulfide polluted seawater increases due to the selective copper dissolution. Cyclic polarization measurements confirmed that the corrosion rate decreases slightly as the sulfide concentration increases. Pitting tendency was high in the low concentration range of sulfide and low in the high concentration range. The presence of stresses in SCC removes the protective layer as it increases during testing of the specimen or during the actual service of a component. The authors propose that film rupture occurred, and two proposed SCC mechanisms were operational, namely sulfide stress cracking associated with the anodic dissolution in the low sulfide concentration range and hydrogen embrittlement, which was dominant in the high sulfide concentration range. It was found that a synergism exists between sulfide and stress that enhances the effect of the latter.

  13. Crack growth sparse pursuit for wind turbine blade

    Science.gov (United States)

    Li, Xiang; Yang, Zhibo; Zhang, Han; Du, Zhaohui; Chen, Xuefeng

    2015-01-01

    One critical challenge to achieving reliable wind turbine blade structural health monitoring (SHM) is mainly caused by composite laminates with an anisotropy nature and a hard-to-access property. The typical pitch-catch PZTs approach generally detects structural damage with both measured and baseline signals. However, the accuracy of imaging or tomography by delay-and-sum approaches based on these signals requires improvement in practice. Via the model of Lamb wave propagation and the establishment of a dictionary that corresponds to scatters, a robust sparse reconstruction approach for structural health monitoring comes into view for its promising performance. This paper proposes a neighbor dictionary that identifies the first crack location through sparse reconstruction and then presents a growth sparse pursuit algorithm that can precisely pursue the extension of the crack. An experiment with the goal of diagnosing a composite wind turbine blade with an artificial crack is performed, and it validates the proposed approach. The results give competitively accurate crack detection with the correct locations and extension length.

  14. Subcritical crack growth of selected aerospace pressure vessel materials

    Science.gov (United States)

    Hall, L. R.; Bixler, W. D.

    1972-01-01

    This experimental program was undertaken to determine the effects of combined cyclic/sustained loads, stress level, and crack shape on the fatigue crack growth rate behavior of cracks subjected to plane strain conditions. Material/environment combinations tested included: 2219-T87 aluminum plate in gaseous helium, room air, and 3.5% NaCl solution at room temperature, liquid nitrogen, and liquid hydrogen; 5Al-2.5 Sn (ELI) titanium plate in liquid nitrogen and liquid hydrogen and 6AL-4V (ELI) STA titanium plate in gaseous helium and methanol at room temperature. Most testing was accomplished using surface flawed specimens instrumented with a clip gage to continuously monitor crack opening displacements at the specimen surface. Tapered double cantilever beam specimens were also tested. Static fracture and ten hour sustained load tests were conducted to determine fracture toughness and apparent threshold stress intensity values. Cyclic tests were performed using sinusoidal loading profiles at 333 MHz (20 cpm) and trapezoidal loading profiles at both 8.3 MHz (0.5 cpm) and 3.3 MHz (0.2 cpm). Data were evaluated using modified linear elastic fracture mechanics parameters.

  15. Fatigue Crack Growth Fundamentals in Shape Memory Alloys

    Science.gov (United States)

    Wu, Y.; Ojha, A.; Patriarca, L.; Sehitoglu, H.

    2015-03-01

    In this study, based on a regression of the crack tip displacements, the stress intensity range in fatigue is quantitatively determined for the shape memory alloy Ni2FeGa. The results are compared to the calculated stress intensity ranges with a micro-mechanical analysis accounting for the transformation-induced tractions. The effective stress intensity ranges obtained with both methods are in close agreement. Also, the fatigue crack closure levels were measured as 30 % of the maximum load using virtual extensometers along the crack flanks. This result is also in close agreement with the regression and micro-mechanical modeling findings. The current work pointed to the importance of elastic moduli changes and the residual transformation strains playing a role in the fatigue crack growth behavior. Additional simulations are conducted for two other important shape memory alloys, NiTi and CuZnAl, where the reductions in stress intensity range were found to be lower than Ni2FeGa.

  16. Equivalent Crack Size Modelling of Corrosion Pitting in an AA7050-T7451 Aluminium Alloy and its Implications for Aircraft Structural Integrity

    Science.gov (United States)

    2012-09-01

    provides a quantitative measurement of the spatial density of pits14 but there is no quantitative measurement of corrosion pit metrics without...and stress corrosion cracking in the 7075 T6 components of the RAAF C-130 Hercules...Post-Fracture Examination................................................................... 16 3.5.3 Surface Roughness Measurement

  17. Dynamical observations on the crack tip zone and stress corrosion of two-dimensional MoS2

    Science.gov (United States)

    Ly, Thuc Hue; Zhao, Jiong; Cichocka, Magdalena Ola; Li, Lain-Jong; Lee, Young Hee

    2017-01-01

    Whether and how fracture mechanics needs to be modified for small length scales and in systems of reduced dimensionality remains an open debate. Here, employing in situ transmission electron microscopy, atomic structures and dislocation dynamics in the crack tip zone of a propagating crack in two-dimensional (2D) monolayer MoS2 membrane are observed, and atom-to-atom displacement mapping is obtained. The electron beam is used to initiate the crack; during in situ observation of crack propagation the electron beam effect is minimized. The observed high-frequency emission of dislocations is beyond previous understanding of the fracture of brittle MoS2. Strain analysis reveals dislocation emission to be closely associated with the crack propagation path in nanoscale. The critical crack tip plastic zone size of nearly perfect 2D MoS2 is between 2 and 5 nm, although it can grow to 10 nm under corrosive conditions such as ultraviolet light exposure, showing enhanced dislocation activity via defect generation.

  18. Dynamical observations on the crack tip zone and stress corrosion of two-dimensional MoS2

    KAUST Repository

    Ly, Thuc Hue

    2017-01-18

    Whether and how fracture mechanics needs to be modified for small length scales and in systems of reduced dimensionality remains an open debate. Here, employing in situ transmission electron microscopy, atomic structures and dislocation dynamics in the crack tip zone of a propagating crack in two-dimensional (2D) monolayer MoS2 membrane are observed, and atom-to-atom displacement mapping is obtained. The electron beam is used to initiate the crack; during in situ observation of crack propagation the electron beam effect is minimized. The observed high-frequency emission of dislocations is beyond previous understanding of the fracture of brittle MoS2. Strain analysis reveals dislocation emission to be closely associated with the crack propagation path in nanoscale. The critical crack tip plastic zone size of nearly perfect 2D MoS2 is between 2 and 5 nm, although it can grow to 10 nm under corrosive conditions such as ultraviolet light exposure, showing enhanced dislocation activity via defect generation.

  19. A state of the art on primary side stress corrosion cracking in nuclear power plant

    Energy Technology Data Exchange (ETDEWEB)

    Kim, H. P.; Kim, J. S.; Han, J. H.; Lee, D. H.; Lim, Y. S.; Suh, J. H.; Hwang, S. S.; Hur, D. H

    1999-09-01

    A state of art on primary water stress corrosion cracking (PWSCC) of alloy 600 used as steam generator tubing of nuclear power plant and remedial action on the PWSCC were reviewed and analyzed. One of the major metallurgical factors which have effect on PWSCC is Cr carbide distribution. A semicontinuous intergranular Cr carbide distribution enhance PWSCC of alloy 600. PWSCC rate is reported to be reported to be proportional to exp(-50 cal/RT) {sigma}{sup 4}. PWSCC rate also increase with increase in hydrogen partial pressure from 0 to 150 ppm and then decreased with further increase in hydrogen partial pressure to 757 ppm. Development of PWSCC prediction technology which takes into account tubing material, fabrication process and operating history of steam generator is needed to manage PWSCC of domestic nuclear power plant. PWSCC has mainly occurred at expansion irregularities within tubesheet, expansion transitions, dented tube support plate intersections and transition and apex of U bend. Remedial actions to PWSCC are sleeving, plugging, temperature reduction, Ni plating, Ni sleeving, shot peening and steam generator replacement in worst case. Option to remedial actions depend on plant specific such as plant age, leak rate from primary to secondary, density and progression of PWSCC. Ni sleeving developed in Framatome seems to be a powerful method because it never subject to PWSCC. Remedial action should be developed and evaluated for possible PWSCC of domestic nuclear power plant. (author)

  20. Preparation Femtosecond Laser Prevention for the Cold-Worked Stress Corrosion Crackings on Reactor Grade Low Carbon Stainless Steel

    CERN Document Server

    John Minehara, Eisuke

    2004-01-01

    We report here that the femtosecond lasers like low average power Ti:Sapphire lasers, the JAERI high average power free-electron laser and others could peel off and remove two stress corrosion cracking (SCC) origins of the cold-worked and the cracking susceptible material, and residual tensile stress in hardened and stretched surface of low-carbon stainless steel cubic samples for nuclear reactor internals as a proof of principle experiment except for the third origin of corrosive environment. Because a 143 °C and 43% MgCl2 hot solution SCC test was performed for the samples to simulate the cold-worked SCC phenomena of the internals to show no crack at the laser-peered off strip on the cold-worked side and ten-thousands of cracks at the non-peeled off on the same side, it has been successfully demonstrated that the femtosecond lasers could clearly remove the two SCC origins and could resultantly prevent the cold-worked SCC.

  1. Effect of T-stress on the cleavage crack growth resistance resulting from plastic flow

    DEFF Research Database (Denmark)

    Tvergaard, Viggo

    1998-01-01

    Crack growth is studied numerically for cases where fracture occurs by atomic separation, sc that the length scale of the fracture process is typically much smaller than the dislocation spacing. Thus, the crack growth mechanism is brittle, but due to plastic flow at some distance from the crack t...

  2. Comparison of Fatigue Properties and Fatigue Crack Growth Rates of Various Implantable Metals

    Directory of Open Access Journals (Sweden)

    Yoshimitsu Okazaki

    2012-12-01

    Full Text Available The fatigue strength, effects of a notch on the fatigue strength, and fatigue crack growth rate of Ti-15Zr-4Nb-4Ta alloy were compared with those of other implantable metals. Zr, Nb, and Ta are important alloying elements for Ti alloys for attaining superior long-term corrosion resistance and biocompatibility. The highly biocompatible Ti-15Zr-4Nb-4Ta alloy exhibited an excellent balance between strength and ductility. Its notched tensile strength was much higher than that of a smooth specimen. The strength of 20% cold-worked commercially pure (C.P. grade 4 Ti was close to that of Ti alloy. The tension-to-tension fatigue strength of an annealed Ti-15Zr-4Nb-4Ta rod at 107 cycles was approximately 740 MPa. The fatigue strength of this alloy was much improved by aging treatment after solution treatment. The fatigue strengths of C.P. grade 4 Ti and stainless steel were markedly improved by 20% cold working. The fatigue strength of Co-Cr-Mo alloy was markedly increased by hot forging. The notch fatigue strengths of 20% cold-worked C.P. grade 4 Ti, and annealed and aged Ti-15Zr-4Nb-4Ta, and annealed Ti-6Al-4V alloys were less than those of the smooth specimens. The fatigue crack growth rate of Ti-15Zr-4Nb-4Ta was the same as that of Ti-6Al-4V. The fatigue crack growth rate in 0.9% NaCl was the same as that in air. Stainless steel and Co-Cr-Mo-Ni-Fe alloy had a larger stress-intensity factor range (ΔK than Ti alloy.

  3. Standard test method for measurement of fatigue crack growth rates

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2015-01-01

    1.1 This test method covers the determination of fatigue crack growth rates from near-threshold to Kmax controlled instability. Results are expressed in terms of the crack-tip stress-intensity factor range (ΔK), defined by the theory of linear elasticity. 1.2 Several different test procedures are provided, the optimum test procedure being primarily dependent on the magnitude of the fatigue crack growth rate to be measured. 1.3 Materials that can be tested by this test method are not limited by thickness or by strength so long as specimens are of sufficient thickness to preclude buckling and of sufficient planar size to remain predominantly elastic during testing. 1.4 A range of specimen sizes with proportional planar dimensions is provided, but size is variable to be adjusted for yield strength and applied force. Specimen thickness may be varied independent of planar size. 1.5 The details of the various specimens and test configurations are shown in Annex A1-Annex A3. Specimen configurations other than t...

  4. Apparent activation energy of subcritical crack growth of SiC/SiC composites at elevated temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Chou, Y.S.; Stackpoole, M.M.; Bordia, R. [Univ. of Washington, Seattle, WA (United States)] [and others

    1995-04-01

    The purpose of this study is to investigate the environmental effect of oxygen-containing gases on the subcritical crack growth of continuous fiber (Nicalon {open_quotes}SiC{close_quotes}) reinforced ceramic matrix (SiC) composites at elevated temperatures. This is a continuing project and the primary goal for this time period is to obtain an apparent activation energy for SiC/SiC materials with two different interfaces: carbon and boron nitride coatings. In the past six months, the authors have conducted studies of subcritical crack growth on SiC/SiC composite materials in a corrosive (O{sub 2}) as well as an inert (Ar) atmosphere for temperatures ranging from 800 to 1100{degree}C.

  5. Fatigue crack growth characteristics of nitrogen-alloyed type 347 stainless under operating conditions of a pressurized water reactor

    Energy Technology Data Exchange (ETDEWEB)

    Min, Ki Deuk; Hong, Seok Min; Kim, Dae Whan; Lee, Bong Sang [Korea Atomic Energy Research Institute, Nuclear Materials Safety Research Division, Daejeon (Korea, Republic of); Kim, Seon Jin [Hanyang University, Division of materials science and engineering, Seoul (Korea, Republic of)

    2017-06-15

    The fatigue crack growth behavior of Type 347 (S347) and Type 347N (S347N) stainless steel was evaluated under the operating conditions of a pressurized water reactor (PWR). These two materials showed different fatigue crack growth rates (FCGRs) according to the changes in dissolved oxygen content and frequency. Under the simulated PWR conditions for normal operation, the FCGR of S347N was lower than that of S347 and insensitive to the changes in PWR water conditions. The higher yield strength and better corrosion resistance of the nitrogen-alloyed Type 347 stainless steel might be a main cause of slower FCGR and more stable properties against changes in environmental conditions.

  6. A review of irradiation effects on LWR core internal materials - IASCC susceptibility and crack growth rates of austenitic stainless steels

    Science.gov (United States)

    Chopra, O. K.; Rao, A. S.

    2011-02-01

    Austenitic stainless steels (SSs) are used extensively as structural alloys in the internal components of light water reactor (LWR) pressure vessels because of their relatively high strength, ductility, and fracture toughness. However, exposure to neutron irradiation for extended periods changes the microstructure (radiation hardening) and microchemistry (radiation-induced segregation) of these steels, and degrades their fracture properties. Irradiation-assisted stress corrosion cracking (IASCC) is another degradation process that affects LWR internal components exposed to neutron radiation. The existing data on irradiated austenitic SSs were reviewed to evaluate the effects of key parameters such as material composition, irradiation dose, and water chemistry on IASCC susceptibility and crack growth rates of these materials in LWR environments. The significance of microstructural and microchemistry changes in the material on IASCC susceptibility is also discussed. The results are used to determine (a) the threshold fluence for IASCC and (b) the disposition curves for cyclic and IASCC growth rates for irradiated SSs in LWR environments.

  7. Fatigue Crack Growth Rate Behavior of Type 347 Stainless Steel in Simulated PWR Water Environment

    Energy Technology Data Exchange (ETDEWEB)

    Min, Ki Deuk; Kim, Seon Jin [Hanyang University, Seoul (Korea, Republic of); Kim, Dae Whan; Lee, Bong Sang [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2012-05-15

    The pressurizer surge line of a Korean standard nuclear power plane uses Nb stabilized type 347 stainless steel. The pressurizer surge line is the pipe connecting the pressurizer and the hot leg line, and the path controlling the pressure and temperature of the cooling system of the nuclear reactor, operated at 316 .deg. C and in a 150atm. The pressurizer surge line operated at high temperature and high pressure receives thermal stress by a temperature change and mechanical stress by a pressure change at the same time, and by being exposed to the high temperature and high pressure cooling water environment of a nuclear power plant, environmental fatigue by stress and corrosion is the main damage instrument. As the effect of environmental fatigue has been reported, through low cycle fatigue, fatigue life evaluations of austenite stainless steel have been conducted, but evaluations of fatigue crack growth rate to evaluate the soundness are very poor. In this study, evaluated characteristics of fatigue crack growth rate base on a change of dissolved oxygen in a PWR environment

  8. Assessment of stress-corrosion cracking in a water-cooled ITER

    Energy Technology Data Exchange (ETDEWEB)

    Jones, R.H.; Bruemmer, S.M.

    1989-04-01

    Water-cooled, near-term reactors will operate under conditions at which SCC is possible; however, control of material purity and processing and coolant chemistry can either eliminate or greatly reduce the probability of this type of structural failure. This evaluation has focused on an assessment of water impurity effects on SCC of austenitic stainless steel at temperatures below 100{degree}C and on the conditions controlling sensitization in the fusion heat of Type 316 SS and the fusion materials heat of modified Type 316 SS designated as PCA. This assessment identifies the dominant effect of small concentrations of impurities in high-purity water on SCC such that crack growth rates at 25--75{degree}C in water with as little as 5--15 ppM Cl{sup {minus}} are equal to the crack growth rates at 200--300{degree}C in high-purity water. These effects are primarily for sensitized Type 304 SS, so analysis of sensitization behavior of fusion austenitic alloys was also undertaken. An SSDOS model developed at PNL was used to make these assessments, and correlation to experimental results for Type 316 SS was very good. Both the fusion heat of Type 316 SS and PCA can be severely sensitized but with proper thermal treatment it should be possible to avoid sensitization. 14 refs., 8 figs.

  9. Creep, Fatigue and Environmental Interactions and Their Effect on Crack Growth in Superalloys

    Science.gov (United States)

    Telesman, J.; Gabb, T. P.; Ghosn, L. J.; Smith, T.

    2017-01-01

    Complex interactions of creep/fatigue/environment control dwell fatigue crack growth (DFCG) in superalloys. Crack tip stress relaxation during dwells significantly changes the crack driving force and influence DFCG. Linear Elastic Fracture Mechanics, Kmax, parameter unsuitable for correlating DFCG behavior due to extensive visco-plastic deformation. Magnitude of remaining crack tip axial stresses controls DFCG resistance due to the brittle-intergranular nature of the crack growth process. Proposed a new empirical parameter, Ksrf, which incorporates visco-plastic evolution of the magnitude of remaining crack tip stresses. Previous work performed at 704C, extend the work to 760C.

  10. Fatigue Crack Growth Threshold Testing of Metallic Rotorcraft Materials

    Science.gov (United States)

    Newman, John A.; James, Mark A.; Johnson, William M.; Le, Dy D.

    2008-01-01

    Results are presented for a program to determine the near-threshold fatigue crack growth behavior appropriate for metallic rotorcraft alloys. Four alloys, all commonly used in the manufacture of rotorcraft, were selected for study: Aluminum alloy 7050, 4340 steel, AZ91E Magnesium, and Titanium alloy Ti-6Al-4V (beta-STOA). The Federal Aviation Administration (FAA) sponsored this research to advance efforts to incorporate damage tolerance design and analysis as requirements for rotorcraft certification. Rotorcraft components are subjected to high cycle fatigue and are typically subjected to higher stresses and more stress cycles per flight hour than fixed-wing aircraft components. Fatigue lives of rotorcraft components are generally spent initiating small fatigue cracks that propagate slowly under near-threshold cracktip loading conditions. For these components, the fatigue life is very sensitive to the near-threshold characteristics of the material.

  11. Recent progress to understand stress corrosion cracking in sodium borosilicate glasses: linking the chemical composition to structural, physical and fracture properties

    Science.gov (United States)

    Rountree, Cindy L.

    2017-08-01

    This topical review is dedicated to understanding stress corrosion cracking in oxide glasses and specifically the SiO_2{\\text-B_2O_3{\\text-}Na_2O} (SBN) ternary glass systems. Many review papers already exist on the topic of stress corrosion cracking in complex oxide glasses or overly simplified glasses (pure silica). These papers look at how systematically controlling environmental factors (pH, temperature...) alter stress corrosion cracking, while maintaining the same type of glass sample. Many questions still exist, including: What sets the environmental limit? What sets the velocity versus stress intensity factor in the slow stress corrosion regime (Region I)? Can researchers optimize these two effects to enhance a glass’ resistance to failure? To help answer these questions, this review takes a different approach. It looks at how systemically controlling the glass’ chemical composition alters the structure and physical properties. These changes are then compared and contrasted to the fracture toughness and the stress corrosion cracking properties. By taking this holistic approach, researchers can begin to understand the controlling factors in stress corrosion cracking and how to optimize glasses via the initial chemical composition.

  12. Electrochemical and Sulfide Stress Corrosion Cracking Behaviors of Tubing Steels in a H2S/CO2 Annular Environment

    Science.gov (United States)

    Liu, Z. Y.; Wang, X. Z.; Liu, R. K.; Du, C. W.; Li, X. G.

    2014-04-01

    The electrochemical and sulfide stress corrosion cracking (SSCC) behaviors of 13Cr stainless steel and P110 steel were investigated in a simulated acidic annular environment with low-temperature and high-pressure H2S/CO2 using electrochemical methods, U-bend immersion tests, and scanning electron microscopy. In the solution containing high pressure CO2, 13Cr, and P110 steels exhibited general corrosion and severe pitting, respectively. Compared with sweet corrosion, additional H2S in the solution enhanced the corrosion of 13Cr steel but inhibited the corrosion of P110 steel. By contrast, in a solution containing 4 MPa CO2 and different (0-0.3 MPa), the susceptibility of both 13Cr stainless steel and P110 steel toward SSCC was significantly promoted by increases in H2S partial pressure. The 13Cr stainless steel exhibited higher susceptibility toward SSCC than P110 steel under a H2S/CO2 environment but lower susceptibility under a pure CO2 environment.

  13. Improved stress corrosion cracking resistance of a novel biodegradable EW62 magnesium alloy by rapid solidification, in simulated electrolytes.

    Science.gov (United States)

    Hakimi, O; Aghion, E; Goldman, J

    2015-06-01

    The high corrosion rate of magnesium (Mg) and Mg-alloys precludes their widespread acceptance as implantable biomaterials. Here, we investigated the potential for rapid solidification (RS) to increase the stress corrosion cracking (SCC) resistance of a novel Mg alloy, Mg-6%Nd-2%Y-0.5%Zr (EW62), in comparison to its conventionally cast (CC) counterpart. RS ribbons were extrusion consolidated in order to generate bioimplant-relevant geometries for testing and practical use. Microstructural characteristics were examined by SEM. Corrosion rates were calculated based upon hydrogen evolution during immersion testing. The surface layer of the tested alloys was analyzed by X-ray photoelectron spectroscopy (XPS). Stress corrosion resistance was assessed by slow strain rate testing and fractography. The results indicate that the corrosion resistance of the RS alloy is significantly improved relative to the CC alloy due to a supersaturated Nd enrichment that increases the Nd2O3 content in the external oxide layer, as well as a more homogeneous structure and reduced grain size. These improvements contributed to the reduced formation of hydrogen gas and hydrogen embrittlement, which reduced the SCC sensitivity relative to the CC alloy. Therefore, EW62 in the form of a rapidly solidified extruded structure may serve as a biodegradable implant for biomedical applications.

  14. H2S Stress Corrosion Tests of Welded Joint for X65 Pipeline Steel and Finite Element Numerical Analysis of Crack Tip

    Institute of Scientific and Technical Information of China (English)

    金晓军; 霍立兴; 张玉凤; 白秉仁; 李小巍; 曹军

    2003-01-01

    The microstructure of welded joint is surveyed and the mechanical properties of X65 pipeline steel are studied in this paper, which provides experimental basis of performance effect on stress corrosion. H2S stress corrosion cracking (SCC) tests on the steel are carried out in the environment based on NACE TM-01-77 solution. The threshold stress intensity factor and crack propagation velocity for base metal and HAZ are obtained. The susceptibility of welded joint for X65 pipeline steel to H2S stress corrosion cracking is investigated. The programming package ANSYS of finite element model (FEM) is used to perform the three-dimensional elastic-plastic finite element analysis of WOL specimens. Stress field and concentration of hydrogen distribution property of the crack tip are obtained.

  15. Dissolution of copper in chloride/ammonia mixtures and the implications for the stress corrosion cracking of copper containers

    Energy Technology Data Exchange (ETDEWEB)

    King, F.; Greidanus, G.; Jobe, D.J

    1999-05-01

    Stress-corrosion cracking is a possible failure mechanism for copper nuclear fuel waste disposal containers. One species known to cause the stress corrosion of copper alloys is ammonia. It is conceivable that ammonia could be produced in a disposal vault under certain, very specific conditions. There are a number of conditions, however, that mitigate against container failure by stress corrosion, one of which is the presence of chloride ions in deep Canadian Shield groundwaters. There are a number of reports in the literature that suggest that Cl{sup -} has an inhibitive effect on the stress corrosion of Cu alloys in ammonia solutions. The electrochemical behaviour of Cu in Cl{sup -}/ammonia solutions has been studied as a function of ammonia concentration, pH, the rate of mass transport and electrochemical potential. In particular, the effects of these parameters on the formation Of Cu{sub 2}O films and the steady-state dissolution behaviour have been determined. All experiments were carried out in 0.1 mol{center_dot}dm{sup -3} NaC1 as a base solution. A series of aqueous speciation and equilibrium potential/pH diagrams are also presented for the quaternary system Cu-C1{sup -}NH{sub 3}/NH{sub 4{sup +}}H{sub 2}O. These diagrams are used to interpret the results of the electrochemical experiments reported here. In addition, it is demonstrated how these diagrams could be used to predict the time-dependence of the susceptibility to stress corrosion cracking of Cu containers in a disposal vault. (author)

  16. Crack Growth Monitoring in Harsh Environments by Electric Potential Measurements

    Energy Technology Data Exchange (ETDEWEB)

    Lloyd, Wilson Randolph; Reuter, Walter Graham; Weinberg, David Michael

    1999-09-01

    Electric potential measurement (EPM) technology offers an attractive alternative to conventional nondestructive evaluation (NDE) for monitoring crack growth in harsh environments. Where conventional NDE methods typically require localized human interaction, the EPM technique developed at the Idaho National Engineering and Environmental Laboratory (INEEL) can be operated remotely and automatically. Once a crack-like defect is discovered via conventional means, EPM can be applied to monitor local crack size changes. This is of particular interest in situations where an identified structural defect is not immediately rejectable from a fitness-for-service viewpoint, but due to operational and environmental conditions may grow to an unsafe size with continuing operation. If the location is in a harsh environment where periodic monitoring by normal means is either too costly or not possible, a very expensive repair may be immediately mandated. However, the proposed EPM methodology may offer a unique monitoring capability that would allow for continuing service. INEEL has developed this methodology, supporting equipment, and calibration information to apply EPM in a field environment for just this purpose. Laboratory and pilot scale tests on full-size engineering structures (pressure vessels and piping) have been successfully performed. The technique applicable is many severe environments because the sensitive equipment (electronics, operators) can be situated in a remote location, with only current and voltage probe electrical leads entering into the harsh environment. Experimental results showing the utility of the methodology are presented, and unique application concepts that have been examined by multiple experiments are discussed.

  17. Face/core debond fatigue crack growth characterization using the sandwich mixed mode bending specimen

    DEFF Research Database (Denmark)

    Manca, Marcello; Quispitupa, Amilcar; Berggreen, Christian;

    2012-01-01

    Face/core fatigue crack growth in foam-cored sandwich composites is examined using the mixed mode bending (MMB) test method. The mixed mode loading at the debond crack tip is controlled by changing the load application point in the MMB test fixture. Sandwich specimens were manufactured using H45...... critical load, at load ratios of R=0.1 and 0.2. The crack length was determined during fatigue testing using the analytical compliance expression and verified by visual measurements. Fatigue crack growth results revealed higher crack growth rates for mode I dominated loading. For specimens with H45 core...

  18. Development of Modified 304 Stainless Steel Resistant to Stress Corrosion Cracking in Chloride Environment

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    This was a feasibility study for a modified 304 steel resistant to stress corrosion cracking (SCC) in aqueous environment containing chloride. SCC tests were conducted potentiostaticaly with spot-welded specimens, which had both crevice and residual stress, mainly in 3 % NaCl solution at various temperatures to determine the critical temperature for SCC at and below which the steel would not suffer from SCC. The effects of individual alloying element of silicon, manganese and copper on SCC of 18Cr-14Ni steels which phosphor content is 0.002 % and molybdenum content is 0.01 % were examined. Addition of 1 or 2 % of copper has beneficial effect on resistance to SCC, while increasing silicon or manganese content has no significant effect. Critical temperature of the steel with 0.002 % of phosphor and 2 % of copper is 150 ℃, which is markedly higher than 50 ℃ of 304L steel. However, the beneficial effect of copper is reduced with increasing phosphor content. From practical viewpoint, the modified steel with good SCC resistance should have 0.01 %-0.015 % of phosphor and 0.3 % or more of molybdenum, because it is very difficult to reduce phosphor content below 0.008 % industrially and such molybdenum content is inevitably introduced through cost-saving melting process using return steel. Aluminium is to be added as another alloying element and 3 % of aluminium combined with 2 % of copper has been found to negate the deleterious effects of increased phosphor and molybdenum content. As a candidate steel at this stage, 14Cr-16Ni-0.013P-2Cu-1Al-(0.3-1)Mo steel has critical temperature of 110 ℃.

  19. Embrittlement and anodic process in stress corrosion cracking: study of the influent micro-mechanical parameters; Fragilisation et processus anodiques en corrosion sous contrainte: etude des parametres micro-mecaniques influents

    Energy Technology Data Exchange (ETDEWEB)

    Tinnes, J.Ph

    2006-11-15

    We study the influence of local mechanical parameters on crack propagation in Stress Corrosion Cracking, at the scale of the microstructure. Two systems are compared: the CuAl{sub 9}Ni{sub 3}Fe{sub 2} copper-aluminium alloy in synthetic sea water under cathodic polarization, where the crack propagation mechanism is related to strain-assisted anodic dissolution, and the 316L austenitic stainless steel in MgCl{sub 2} solution, where embrittlement mechanisms related to hydrogen effects prevail. We use micro-notched tensile specimen that allow to study isolated short cracks. These experiments are modelled by means of finite elements calculations, and further characterized by Electron Back scattered Diffraction (EBSD) in the case of the 316L alloy. In terms of the local mechanical parameters that control propagation, fundamental differences are outlined between the two systems. They are discussed from the viewpoint of the available models of Stress Corrosion Cracking. (author)

  20. Influence of nitrogen on the stress corrosion cracking resistance of austenitic stainless steels in chloride environment; Influence de l'azote sur la resistance a la corrosion sous contrainte d'aciers inoxydables austenitiques en milieu chlorure

    Energy Technology Data Exchange (ETDEWEB)

    Teysseyre, S

    2001-11-01

    The aim of this study is to investigate the influence of nitrogen additions on the Stress Corrosion Cracking (SSC) resistance of austenitic stainless steel in chloride environment. The investigation was carried out in two part: first, an experimental investigation with model industrial steels was carried out and secondly, numerical simulations based on the Corrosion Enhanced Plasticity Model were developed. Both slow strain rate tensile tests and constant load test of the different steels in boiling MgCl{sub 2} (153 deg C) at free potential show that, for a given plastic strain rate, nitrogen addition increases the critical stress for crack initiation without influencing the crack propagation rate. We observed that the creep rate under constant load was affected by the nitrogen content. As a consequence, the SCC behaviour (cracks density and propagation rate) depends on the nitrogen content. We thus confirm that the nitrogen content influences the corrosion - deformation interaction mechanisms via its positive contribution to the flow stress. These experimental results are reproduced semi-quantitatively by means of numerical simulations at the scale of crack. - dislocation interactions. The presence of nitrogen is modelled by an increased lattice friction stress, which in turn affects the dynamics of crack tip shielding by dislocation pile-ups. We conclude that nitrogen addition in austenitic stainless steels increases the SC crack initiation stress in proportion of the increased flow stress, without penalty in terms of SC crack propagation rate. (author)

  1. Crack growth rates and fracture toughness of irradiated austenitic stainless steels in BWR environments.

    Energy Technology Data Exchange (ETDEWEB)

    Chopra, O. K.; Shack, W. J.

    2008-01-21

    In light water reactors, austenitic stainless steels (SSs) are used extensively as structural alloys in reactor core internal components because of their high strength, ductility, and fracture toughness. However, exposure to high levels of neutron irradiation for extended periods degrades the fracture properties of these steels by changing the material microstructure (e.g., radiation hardening) and microchemistry (e.g., radiation-induced segregation). Experimental data are presented on the fracture toughness and crack growth rates (CGRs) of wrought and cast austenitic SSs, including weld heat-affected-zone materials, that were irradiated to fluence levels as high as {approx} 2x 10{sup 21} n/cm{sup 2} (E > 1 MeV) ({approx} 3 dpa) in a light water reactor at 288-300 C. The results are compared with the data available in the literature. The effects of material composition, irradiation dose, and water chemistry on CGRs under cyclic and stress corrosion cracking conditions were determined. A superposition model was used to represent the cyclic CGRs of austenitic SSs. The effects of neutron irradiation on the fracture toughness of these steels, as well as the effects of material and irradiation conditions and test temperature, have been evaluated. A fracture toughness trend curve that bounds the existing data has been defined. The synergistic effects of thermal and radiation embrittlement of cast austenitic SS internal components have also been evaluated.

  2. Evaluation of creep-fatigue crack growth for large-scale FBR reactor vessel and NDE assessment

    Energy Technology Data Exchange (ETDEWEB)

    Joo, Young Sang; Kim, Jong Bum; Kim, Seok Hun; Yoo, Bong

    2001-03-01

    Creep fatigue crack growth contributes to the failure of FRB reactor vessels in high temperature condition. In the design stage of reactor vessel, crack growth evaluation is very important to ensure the structural safety and setup the in-service inspection strategy. In this study, creep-fatigue crack growth evaluation has been performed for the semi-elliptical surface cracks subjected to thermal loading. The thermal stress analysis of a large-scale FBR reactor vessel has been carried out for the load conditions. The distributions of axial, radial, hoop, and Von Mises stresses were obtained for the loading conditions. At the maximum point of the axial and hoop stress, the longitudinal and circumferential surface cracks (i.e. PTS crack, NDE short crack and shallow long crack) were postulated. Using the maximum and minimum values of stresses, the creep-fatigue crack growth of the proposed cracks was simulated. The crack growth rate of circumferential cracks becomes greater than that of longitudinal cracks. The total crack growth of the largest PTS crack is very small after 427 cycles. The structural integrity of a large-scale reactor can be maintained for the plant life. The crack depth growth of the shallow long crack is faster than that of the NDE short crack. In the ISI of the large-scale FBR reactor vessel, the ultrasonic inspection is beneficial to detect the shallow circumferential cracks.

  3. Corrosion

    Science.gov (United States)

    Slabaugh, W. H.

    1974-01-01

    Presents some materials for use in demonstration and experimentation of corrosion processes, including corrosion stimulation and inhibition. Indicates that basic concepts of electrochemistry, crystal structure, and kinetics can be extended to practical chemistry through corrosion explanation. (CC)

  4. Corrosion

    Science.gov (United States)

    Slabaugh, W. H.

    1974-01-01

    Presents some materials for use in demonstration and experimentation of corrosion processes, including corrosion stimulation and inhibition. Indicates that basic concepts of electrochemistry, crystal structure, and kinetics can be extended to practical chemistry through corrosion explanation. (CC)

  5. Analysis of deterministic and statistical approaches to fatigue crack growth in pressure vessels

    Energy Technology Data Exchange (ETDEWEB)

    Francisco, Alexandre S.; Melo, P.F. Frutuoso e [Universidade Federal, Rio de Janeiro, RJ (Brazil). Coordenacao dos Programas de Pos-graduacao de Engenharia. Programa de Engenharia Nuclear. E-mail: frutuoso@lmn.con.ufrj.br

    2000-07-01

    This work presents three approaches to the fatigue crack growth process in steel pressure vessels as applied to failure probability calculation. In the Thomson's methodology, the crack growth is the term that represents the mechanical behavior which along the time will take the pressure vessel to a structural failure. The first result of failure probability will be obtained considering a deterministic approach, since the crack growth laws are of a deterministic nature. This approach will provide a reference value. Next, two statistical approaches will be performed based on the fact that fatigue crack growth is a random phenomenon. One of them takes into account only the variability of experimental data, proposing a distribution function to represent the failure process. The other, the stochastic approach, considers the random nature of crack growth along time, by performing the randomization of a crack growth law. The solution of this stochastic equation is a transition distribution function fitted to experimental data. (author)

  6. Mechanisms of dwell fatigue crack growth in an advanced nickel disc alloy RR1000

    Directory of Open Access Journals (Sweden)

    Yu S.Y.

    2014-01-01

    Full Text Available RR1000 is one of an advanced class of nickel-based superalloys developed for disc applications. Under one hour dwell fatigue loading, complex crack growth behaviour has been observed especially in a coarse grained version of this alloy. At a temperature of 700 ∘C in air an increase of nearly two orders of magnitude in crack growth rates compared to baseline fatigue crack growth rates may be seen. However for certain microstructural conditions, cracks can also demonstrate retardation following initial acceleration. When using a direct current potential difference (d.c.p.d technique for monitoring crack growth, a damage zone of a few hundred microns is often measured ahead of a fast growing crack. Advanced characterisation techniques including SEM, ECCI and X-ray tomography have been adopted in the current study to understand the observed damage zone and retardation phenomenon. It is found that damage zones measured by d.c.p.d reflect brittle and non-uniform advance of the crack resulting from continuous dynamic or quasi-dynamic fracture of an oxide intrusion ahead of the crack tip during the dwell period. In contrast, cracking of the oxide intrusion is less frequent or even prevented during dwell periods associated with a retarded and slow growing crack. Crack tip stress relaxation plays an important role in dictating whether or not dynamic cracking of the oxide intrusion can be avoided.

  7. FATIGUE GROWTH MODELING OF MIXED-MODE CRACK IN PLANE ELASTIC MEDIA

    Institute of Scientific and Technical Information of China (English)

    Yan Xiangqiao

    2005-01-01

    This paper presents an extension of a displacement discontinuity method with cracktip elements (a boundary element method) proposed by the author for fatigue crack growth analysis in plane elastic media under mixed-mode conditions. The boundary element method consists of the non-singular displacement discontinuity elements presented by Crouch and Starfield and the crack-tip displacement discontinuity elements due to the author. In the boundary element implementation the left or right crack-tip element is placed locally at the corresponding left or right crack tip on top of the non-singular displacement discontinuity elements that cover the entire crack surface and the other boundaries. Crack growth is simulated with an incremental crack extension analysis based on the maximum circumferential stress criterion. In the numerical simulation, for each increment of crack extension, remeshing of existing boundaries is not required because of an intrinsic feature of the numerical approach. Crack growth is modeled by adding new boundary elements on the incremental crack extension to the previous crack boundaries. At the same time, the element characteristics of some related elements are adjusted according to the manner in which the boundary element method is implemented. As an example, the fatigue growth process of cracks emanating from a circular hole in a plane elastic plate is simulated using the numerical simulation approach.

  8. Creep crack growth analysis using C{sub t}-parameter for internal circumferential and external axial surface cracks in a pressurized cylinder

    Energy Technology Data Exchange (ETDEWEB)

    Tun, Nwe Ni; Yang, Hee Seung; Yu, Jong Min; Yoon, Kee Bong [Dept. of Mechanical Engineering, Chung Ang University, Seoul (Korea, Republic of)

    2016-12-15

    Creep crack growth at elevated temperatures is a critical consideration in estimating the remaining life of high temperature structural components and in deciding their inspection interval. In this study, creep crack growth analyses for external radial-axial and internal radial-circumferential surface cracks in a pressurized cylinder were conducted by an analytical method. The effect of crack depth and crack length on the variations in Ct and remaining life predictions were investigated for surface cracks with various initial aspect ratios. It was observed that the remaining life of an internal radial-circumferential surface crack was approximately 53 times longer than that of an external radial-axial surface crack for the same crack size and loading conditions with 316 stainless steel material. It was also observed that the variations in remaining life, crack propagations, and the Ct values were considerably sensitive to the crack location and crack depth. Convergence of crack aspect ratio was not observed when the crack depth ratio was increased. Since the method is independent of material properties and location of the crack geometries, it can be extended to various material properties and various locations of the surface crack geometries.

  9. Development of a numerical procedure for mixed mode K-solutions and fatigue crack growth in FCC single crystal superalloys

    Science.gov (United States)

    Ranjan, Srikant

    2005-11-01

    Fatigue-induced failures in aircraft gas turbine and rocket engine turbopump blades and vanes are a pervasive problem. Turbine blades and vanes represent perhaps the most demanding structural applications due to the combination of high operating temperature, corrosive environment, high monotonic and cyclic stresses, long expected component lifetimes and the enormous consequence of structural failure. Single crystal nickel-base superalloy turbine blades are being utilized in rocket engine turbopumps and jet engines because of their superior creep, stress rupture, melt resistance, and thermomechanical fatigue capabilities over polycrystalline alloys. These materials have orthotropic properties making the position of the crystal lattice relative to the part geometry a significant factor in the overall analysis. Computation of stress intensity factors (SIFs) and the ability to model fatigue crack growth rate at single crystal cracks subject to mixed-mode loading conditions are important parts of developing a mechanistically based life prediction for these complex alloys. A general numerical procedure has been developed to calculate SIFs for a crack in a general anisotropic linear elastic material subject to mixed-mode loading conditions, using three-dimensional finite element analysis (FEA). The procedure does not require an a priori assumption of plane stress or plane strain conditions. The SIFs KI, KII, and KIII are shown to be a complex function of the coupled 3D crack tip displacement field. A comprehensive study of variation of SIFs as a function of crystallographic orientation, crack length, and mode-mixity ratios is presented, based on the 3D elastic orthotropic finite element modeling of tensile and Brazilian Disc (BD) specimens in specific crystal orientations. Variation of SIF through the thickness of the specimens is also analyzed. The resolved shear stress intensity coefficient or effective SIF, Krss, can be computed as a function of crack tip SIFs and the

  10. Effect of cracking and randomness of inputs on corrosion initiation of reinforced concrete bridge decks exposed to chlorides

    Directory of Open Access Journals (Sweden)

    P. Konecny

    2017-01-01

    Full Text Available The paper is aimed at the indicative evaluation of the effect of random scatter of input parameters in case of durability of reinforced concrete bridge deck. The time to onset of corrosion of steel reinforcement of concrete bridge deck exposed to chloride is evaluated. The effect of cracking in concrete onto chloride ingress is considered. The selected steel reinforcement protection strategies are: unprotected steel reinforcement, epoxy-coated steel reinforcement and water-proof barrier bellow asphalt overlay. The preliminary model for damage effect on chloride ion ingress through water proof membrane under penetrable asphalt overlay is used. 2-D finite element chloride ingress model is combined with Monte Carlo simulation technique. The innovative crack effect modeling via highly penetrable elements is applied. Deterministic and probabilistic calculations are compared.

  11. Complete Tangent Stiffness for eXtended Finite Element Method by including crack growth parameters

    DEFF Research Database (Denmark)

    Mougaard, J.F.; Poulsen, P.N.; Nielsen, L.O.

    2013-01-01

    The eXtended Finite Element Method (XFEM) is a useful tool for modeling the growth of discrete cracks in structures made of concrete and other quasi‐brittle and brittle materials. However, in a standard application of XFEM, the tangent stiffness is not complete. This is a result of not including...... the crack geometry parameters, such as the crack length and the crack direction directly in the virtual work formulation. For efficiency, it is essential to obtain a complete tangent stiffness. A new method in this work is presented to include an incremental form the crack growth parameters on equal terms...

  12. Stress corrosion cracking susceptibility of a high strength Mg-7%Gd-5%Y-1%Nd-0.5%Zr alloy

    Directory of Open Access Journals (Sweden)

    S.D. Wang

    2014-12-01

    Full Text Available Through performing the tensile tests with different strain rates in 3.5 wt.% NaCl solution, the stress corrosion cracking (SCC behavior and the effect of strain rate on the SCC susceptibility of an extruded Mg-7%Gd-5%Y-1%Nd-0.5%Zr (EW75 alloy have been investigated. Results demonstrate that the alloy is susceptible to SCC when the strain rate is lower than 5 × 10−6 s−1. At the strain rate of 1 × 10−6 s−1, the SCC susceptibility index (ISCC is 0.96 and the elongation-to-failure (εf is only 0.11%. Fractography indicates that the brittle quasi-cleavage feature is very obvious and become more pronounced with decreasing the strain rate. Further analysis confirms that the cracking mode is predominantly transgranular, but the partial intergranular cracking at some localized area can also occur. Meanwhile, it seems that the crack propagation path is unrelated to the existing phase particles.

  13. Thresholds of time dependent intergranular crack growth in a nickel disc alloy Alloy 720Li

    OpenAIRE

    Li Hangyue; Fisk Joe; Lim Lik-Beng; Williams Steve; Bowen Paul

    2014-01-01

    At high temperatures in air, introducing a dwell period at the peak stress of fatigue cycles promotes time dependent intergranular crack growth which can increase crack growth rates by upto a few orders of magnitude from the rates of transgranular fatigue crack growth in superalloys. It is expected that time dependent intergranular crack growth in nickel-based superalloys may not occur below a critical mechanical driving force, ΔKth−IG, analogous to a fatigue threshold (ΔKth) and a critical t...

  14. Crack Growth in Concrete Gravity Dams Based on Discrete Crack Method

    Directory of Open Access Journals (Sweden)

    A. R. Lohrasbi

    2008-01-01

    Full Text Available Seepage is the most parameter in water management safety and in stable agricultural. This seepage is passed through the cracks that are present to some degree in hydraulic structures. They may exist as basic defects in the constituent materials or may be induced in construction or during service life. To avoid such failure in concrete dams, safety would be an important factor. Over-design carries heavy penalty in terms of excess weight. So the fracture mechanics theory is a principal necessity of evaluating the stability of such crack propagation. For the process of crack propagation analysis in concrete structures, there are two general models: discrete crack and smeared crack. This study surveys the crack propagation in concrete gravity dams based on discrete crack methods. Moreover, we use a program provided specifically for this purpose.

  15. Subcritical Crack-Growth and Lifetime Behavior of Glass and SiC under Static Load

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    Crack initiation and subcritical crack growth in glass sheet and SiC bar specimen under static loading were investigated to study the failure process. It has been demonstrated that the lifetime process of brittle materials involves three possible forms of crack growth: subcritical crack growth,partly subcritical crack growth and instantaneous fracture without subcritical crack growth.Curves of v-K obtained in step-by-step static fatigue tests and in constant loading rate tests showed different trends for borosilicate glass sheet. α-SiC that is generally considered immune to mechanical fatigue effect and environmental attack was also tested under static loading and the lifetime was measured. The results showed that the threshold load to damage effect was over 80% of the initial strength for the SiC.

  16. A NOVEL PARAMETER FOR EVALUATING THE FATIGUE CRACK GROWTH RATE IN CARBON STEELS

    Institute of Scientific and Technical Information of China (English)

    X.S.Wang; S.Q.Zhu; N.Kawagoishi; H.Nisitani

    2001-01-01

    A novel parameter is suggested for evaluating the fatigue crack growth rate in carbonsteels.Fatigue crack propagation tests of an annealed 0.42% carbon steel were carriedout under different conditions to investigate the relationship between this dominatingparameter and the crack opening displacement (COD).A new equation of fatiguecrack growth rate is formulated in terms of the suggested parameter.The physicalmeanings of the material parameters in this equation are explored experimentally.Considering the relation of crack growth and deformation properties,a simple andapplicable method is proposed to evaluate the fatigue crack growth rate.It is alsoobserved that the material parameters in the fatigue crack growth rate equation ofcarbon steels are related linearly to the material strength.The results are in a goodagreement with experimental results.

  17. Thresholds of time dependent intergranular crack growth in a nickel disc alloy Alloy 720Li

    Directory of Open Access Journals (Sweden)

    Li Hangyue

    2014-01-01

    Full Text Available At high temperatures in air, introducing a dwell period at the peak stress of fatigue cycles promotes time dependent intergranular crack growth which can increase crack growth rates by upto a few orders of magnitude from the rates of transgranular fatigue crack growth in superalloys. It is expected that time dependent intergranular crack growth in nickel-based superalloys may not occur below a critical mechanical driving force, ΔKth−IG, analogous to a fatigue threshold (ΔKth and a critical temperature, Tth. In this study, dwell fatigue crack growth tests have been carefully designed and conducted on Alloy 720Li to examine such thresholds. Unlike a fatigue threshold, the threshold stress intensity factor range for intergranular crack growth is observed to be highly sensitive to microstructure, dwell time and test procedure. The near threshold crack growth behaviour is made complex by the interactions between grain boundary oxidation embrittlement and crack tip stress relaxation. In general, lower ΔKth−IG values are associated with finer grain size and/or shorter dwell times. Often a load increasing procedure promotes stress relaxation and tends to lead to higher ΔKth−IG. When there is limited stress relaxation at the crack tip, similar ΔKth−IG values are measured with load increasing and load shedding procedures. They are generally higher than the fatigue threshold (ΔKth despite faster crack growth rates (da/dN in the stable crack growth regime. Time dependent intergranular crack growth cannot be activated below a temperature of 500 ∘C.

  18. Fatigue of polycrystalline silicon for MEMS applications: Crack growth and stability under resonant loading conditions

    Energy Technology Data Exchange (ETDEWEB)

    Muhlstein, C.L.; Howe, R.T.; Ritchie, R.O.

    2001-12-05

    Although bulk silicon is not known to exhibit susceptibility to cyclic fatigue, micron-scale structures made from silicon films are known to be vulnerable to degradation by fatigue in ambient air environments, a phenomenon that has been recently modeled in terms of a mechanism of sequential oxidation and stress-corrosion cracking of the native oxide layer.

  19. Assessment of ultrasonic techniques for characterization of stress corrosion cracks in SG partition stubs

    Energy Technology Data Exchange (ETDEWEB)

    Sartre, B.; Banchet, J. [AREVA NP, Saint-Marcel (France); Moras, D.; Bastin, P. [Intercontrole, Rungis (France); Beroni, C. [EDF/CEIDRE, Saint-Denis (France)

    2006-07-01

    Studies by EDF and AREVA NP on Inconel zones have identified the Inconel 600 partition stubs of steam generators as potential areas of SCC, on the hot leg side. Decision was made to perform an expert assessment using ultrasonic testing (UT) techniques to be applied on the whole area of the stub showing penetrant testing (PT) techniques indications. UT techniques, probes and tools were then developed for that purpose. The aim is to size shallow defects, sizing capacity being maintained for defects propagated to a half-thickness. Although no formal qualification was required, the development was performed in view of a performance demonstration. Three mock-ups were manufactured by AREVA NP: two welded mock-ups with machined defects, surface condition and geometry representative of the ''envelope'' of situations likely to be found on the SG; one mock-up, with representative corrosion cracks Development was carried out in two phases: development of techniques and specification of probes and tooling, then development of tools, industrialization of probes, development of procedures, personnel training and performance demonstration. The basic inspection relied on TOFDT, with a contact probe; frequencies, PCS and dimensions were optimised using the results from the mock-ups. Three sets of transducers were defined: a HF transducer for flaw sizes close to the critical size, another HF transducer, with lower PCS for smaller defects, both transducers for material whose permeability was equivalent to that of the mock-ups; anticipating less permeable materials, a MF probe was added. Tests having shown that these transducers did not cover the whole plate thickness, a back-up phased-array probe was selected to scan the plate beyond halfthickness. For a better access under the TSP, a focused transducer was also added to complete the previous set. All of these transducers were operated in immersion, with the same tool: a COBRA type arm which positioned the probes

  20. Irradiation Programs and Test Plans to Assess High-Fluence Irradiation Assisted Stress Corrosion Cracking Susceptibility.

    Energy Technology Data Exchange (ETDEWEB)

    Teysseyre, Sebastien [Idaho National Lab. (INL), Idaho Falls, ID (United States)

    2015-03-01

    . Irradiation assisted stress corrosion cracking (IASCC) is a known issue in current reactors. In a 60 year lifetime, reactor core internals may experience fluence levels up to 15 dpa for boiling water reactors (BWR) and 100+ dpa for pressurized water reactors (PWR). To support a safe operation of our fleet of reactors and maintain their economic viability it is important to be able to predict any evolution of material behaviors as reactors age and therefore fluence accumulated by reactor core component increases. For PWR reactors, the difficulty to predict high fluence behavior comes from the fact that there is not a consensus of the mechanism of IASCC and that little data is available. It is however possible to use the current state of knowledge on the evolution of irradiated microstructure and on the processes that influences IASCC to emit hypotheses. This report identifies several potential changes in microstructure and proposes to identify their potential impact of IASCC. The susceptibility of a component to high fluence IASCC is considered to not only depends on the intrinsic IASCC susceptibility of the component due to radiation effects on the material but to also be related to the evolution of the loading history of the material and interaction with the environment as total fluence increases. Single variation type experiments are proposed to be performed with materials that are representative of PWR condition and with materials irradiated in other conditions. To address the lack of IASCC propagation and initiation data generated with material irradiated in PWR condition, it is proposed to investigate the effect of spectrum and flux rate on the evolution of microstructure. A long term irradiation, aimed to generate a well-controlled irradiation history on a set on selected materials is also proposed for consideration. For BWR, the study of available data permitted to identify an area of concern for long term performance of component. The efficiency of

  1. Crack shape developments and leak rates for circumferential complex-cracked pipes

    Energy Technology Data Exchange (ETDEWEB)

    Brickstad, B.; Bergman, M. [SAQ Inspection Ltd., Stockholm (Sweden)

    1997-04-01

    A computerized procedure has been developed that predicts the growth of an initial circumferential surface crack through a pipe and further on to failure. The crack growth mechanism can either be fatigue or stress corrosion. Consideration is taken to complex crack shapes and for the through-wall cracks, crack opening areas and leak rates are also calculated. The procedure is based on a large number of three-dimensional finite element calculations of cracked pipes. The results from these calculations are stored in a database from which the PC-program, denoted LBBPIPE, reads all necessary information. In this paper, a sensitivity analysis is presented for cracked pipes subjected to both stress corrosion and vibration fatigue.

  2. Slow Crack Growth of Brittle Materials With Exponential Crack-Velocity Formulation. Part 2; Constant Stress Rate Experiments

    Science.gov (United States)

    Choi, Sung R.; Nemeth, Noel N.; Gyekenyesi, John P.

    2002-01-01

    The previously determined life prediction analysis based on an exponential crack-velocity formulation was examined using a variety of experimental data on glass and advanced structural ceramics in constant stress rate and preload testing at ambient and elevated temperatures. The data fit to the relation of strength versus the log of the stress rate was very reasonable for most of the materials. Also, the preloading technique was determined equally applicable to the case of slow-crack-growth (SCG) parameter n greater than 30 for both the power-law and exponential formulations. The major limitation in the exponential crack-velocity formulation, however, was that the inert strength of a material must be known a priori to evaluate the important SCG parameter n, a significant drawback as compared with the conventional power-law crack-velocity formulation.

  3. Slow Crack Growth of Brittle Materials With Exponential Crack-Velocity Formulation. Part 3; Constant Stress and Cyclic Stress Experiments

    Science.gov (United States)

    Choi, Sung R.; Nemeth, Noel N.; Gyekenyesi, John P.

    2002-01-01

    The previously determined life prediction analysis based on an exponential crack-velocity formulation was examined using a variety of experimental data on advanced structural ceramics tested under constant stress and cyclic stress loading at ambient and elevated temperatures. The data fit to the relation between the time to failure and applied stress (or maximum applied stress in cyclic loading) was very reasonable for most of the materials studied. It was also found that life prediction for cyclic stress loading from data of constant stress loading in the exponential formulation was in good agreement with the experimental data, resulting in a similar degree of accuracy as compared with the power-law formulation. The major limitation in the exponential crack-velocity formulation, however, was that the inert strength of a material must be known a priori to evaluate the important slow-crack-growth (SCG) parameter n, a significant drawback as compared with the conventional power-law crack-velocity formulation.

  4. A study on fatigue crack growth in dual phase martensitic steel in air environment

    Indian Academy of Sciences (India)

    K V Sudhakar; E S Dwarakadasa

    2000-06-01

    Dual phase (DP) steel was intercritically annealed at different temperatures from fully martensitic state to achieve martensite plus ferrite, microstructures with martensite contents in the range of 32 to 76%. Fatigue crack growth (FCG) and fracture toughness tests were carried out as per ASTM standards E 647 and E 399, respectively to evaluate the potential of DP steels. The crack growth rates (/) at different stress intensity ranges ( ) were determined to obtain the threshold value of stress intensity range ( th). Crack path morphology was studied to determine the influence of microstructure on crack growth characteristics. After the examination of crack tortuosity, the compact tension (CT) specimens were pulled in static mode to determine fracture toughness values. FCG rates decreased and threshold values increased with increase in vol.% martensite in the DP steel. This is attributed to the lower carbon content in the martensite formed at higher intercritical annealing (ICA) temperatures, causing retardation of crack growth rate by crack tip blunting and/or deflection. Roughness induced crack closure was also found to contribute to the improved crack growth resistance at higher levels of martensite content. Scanning electron fractography of DP steel in the near threshold region revealed transgranular cleavage fracture with secondary cracking. Results indicate the possibility that the DP steels may be treated to obtain an excellent combination of strength and fatigue properties.

  5. A Study on the Residual Stress Improvement of PWSCC(Primary Water Stress Corrosion Cracking) in DMW(Dissimilar Metal Weld)

    Energy Technology Data Exchange (ETDEWEB)

    Kang, Sung Sik; Kim, Seok Hun; Lee, Seung Gun [Korea Institute of Nuclear Safety, Daejeon (Korea, Republic of); Park, Heung Bae [KEPCO Engineering and Construction Company, Daejeon (Korea, Republic of)

    2010-10-15

    Since 2000s, most of the cracks are found in welds, especially in (DMW) dissimilar metal welds such as pressurizer safety relief nozzle, reactor head penetration, reactor bottom mounted instrumentation (BMI), and reactor nozzles. Even the cracks are revealed as a primary water stress corrosion cracking (PWSCC), it is difficult to find the cracks by current non destructive examination. The PWSCC is occurred by three incident factors, such as susceptible material, environmental corrosive condition, and welding residual stress. If one of the three factors can be erased or decreased, the PWSCC could be prevented. In this study, we performed residual stress analysis for DMW and several residual stress improvement methods. As the preventive methods of PWSCC, we used laser peening(IP) method, inlay weld(IW) method, and induction heating stress improvement(IHSI) method. The effect of residual stress improvement for preventive methods was compared and discussed by finite element modeling and residual stress of repaired DMW

  6. The corrosion and corrosion mechanical properties evaluation for the LBB concept in VVERs

    Energy Technology Data Exchange (ETDEWEB)

    Ruscak, M.; Chvatal, P.; Karnik, D.

    1997-04-01

    One of the conditions required for Leak Before Break application is the verification that the influence of corrosion environment on the material of the component can be neglected. Both the general corrosion and/or the initiation and, growth of corrosion-mechanical cracks must not cause the degradation. The primary piping in the VVER nuclear power plant is made from austenitic steels (VVER 440) and low alloy steels protected with the austenitic cladding (VVER 1000). Inspection of the base metal and heterogeneous weldments from the VVER 440 showed that the crack growth rates are below 10 m/s if a low oxygen level is kept in the primary environment. No intergranular cracking was observed in low and high oxygen water after any type of testing, with constant or periodic loading. In the framework of the LBB assessment of the VVER 1000, the corrosion and corrosion mechanical properties were also evaluated. The corrosion and corrosion mechanical testing was oriented predominantly to three types of tests: stress corrosion cracking tests corrosion fatigue tests evaluation of the resistance against corrosion damage. In this paper, the methods used for these tests are described and the materials are compared from the point of view of response on static and periodic mechanical stress on the low alloyed steel 10GN2WA and weld metal exposed in the primary circuit environment. The slow strain rate tests and static loading of both C-rings and CT specimens were performed in order to assess the stress corrosion cracking characteristics. Cyclic loading of CT specimens was done to evaluate the kinetics of the crack growth under periodical loading. Results are shown to illustrate the approaches used. The data obtained were evaluated also from the point of view of comparison of the influence of different structure on the stress corrosion cracking appearance. The results obtained for the base metal and weld metal of the piping are presented here.

  7. Accelerated Near-Threshold Fatigue Crack Growth Behavior of an Aluminum Powder Metallurgy Alloy

    Science.gov (United States)

    Piascik, Robert S.; Newman, John A.

    2002-01-01

    Fatigue crack growth (FCG) research conducted in the near threshold regime has identified a room temperature creep crack growth damage mechanism for a fine grain powder metallurgy (PM) aluminum alloy (8009). At very low DK, an abrupt acceleration in room temperature FCG rate occurs at high stress ratio (R = Kmin/Kmax). The near threshold accelerated FCG rates are exacerbated by increased levels of Kmax (Kmax less than 0.4 KIC). Detailed fractographic analysis correlates accelerated FCG with the formation of crack-tip process zone micro-void damage. Experimental results show that the near threshold and Kmax influenced accelerated crack growth is time and temperature dependent.

  8. Microbial corrosion and cracking in steel. A concept for evaluation of hydrogen-assisted stress corrosion cracking in cathodically protected high-pressure gas transmission pipelines

    DEFF Research Database (Denmark)

    Nielsen, Lars Vendelbo

    of high-strength pipeline steel and the concentration of hydrogen present in the steel. B. Determine the degree hydrogen absorption by cathodically protected steel exposed in natural soil sediment, which include activity of sulphate-reducing bacteria (SRB). C. Compare the above points with fracture......An effort has been undertaken in order to develop a concept for evaluation of the risk of hydrogen-assisted cracking in cathodically protected gas transmission pipelines. The effort was divided into the following subtasks: A. Establish a correlation between the fracture mechanical properties...... in this steel....

  9. An investigation of environmental effects on fatigue crack growth in Q1N (HY80) steel

    Science.gov (United States)

    Soboyejo, W. O.; Knott, J. F.

    1990-11-01

    Fatigue threshold tests have been conducted on through-thickness and semielliptic cracks in laboratory air, vacuum, and salt water at stress ratios (R = Kmin/Kmax @#@) of 0.2 and 0.7. The effects of stress ratio are rationalized by crack closure concepts. Environmental effects are explained by considerations of the irreversibility of slip at the crack tip and the role of debris on the fracture surfaces. Differences in the fatigue crack growth rates in the three environments are attributed largely to the extent of the irreversibility of slip due to the chemisorption of water/ water vapor at the crack tip. Debris in saltwater solutions is also shown to significantly affect the near-threshold growth through its influence on crack closure and the transportation of environment to the crack tip.

  10. Subcritical crack growth under mode I, II, and III loading for Coconino sandstone

    Science.gov (United States)

    Ko, Tae Young

    In systems subjected to long-term loading, subcritical crack growth is the principal mechanism causing the time-dependent deformation and failure of rocks. Subcritical crack growth is environmentally-assisted crack growth, which can allow cracks to grow over a long period of time at stresses far smaller than their failure strength and at tectonic strain rates. The characteristics of subcritical crack growth can be described by a relationship between the stress intensity factor and the crack velocity. This study presents the results of studies conducted to validate the constant stress-rate test for determining subcritical crack growth parameters in Coconino sandstone, compared with the conventional testing method, the double torsion test. The results of the constant stress-rate test are in good agreement with the results of double torsion test. More importantly, the stress-rate tests can determine the parameter A with a much smaller standard deviation than the double torsion test. Thus the constant stress-rate test seems to be both a valid and preferred test method for determining the subcritical crack growth parameters in rocks. We investigated statistical aspects of the constant stress-rate test. The effects of the number of tests conducted on the subcritical crack growth parameters were examined and minimum specimen numbers were determined. The mean and standard deviation of the subcritical crack growth parameters were obtained by randomly selecting subsets from the original strength data. In addition, the distribution form of the subcritical crack growth parameters and the relation between the parameter n and A were determined. We extended the constant stress-rate test technique to modes II and III subcritical crack growth in rocks. The experimental results of the modes I, II and III tests show that the values of the subcritical crack growth parameters are similar to each other. The subcritical crack growth parameter n value for Coconino sandstone has the range

  11. Standard test method for measurement of creep crack growth times in metals

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2007-01-01

    1.1 This test method covers the determination of creep crack growth (CCG) in metals at elevated temperatures using pre-cracked specimens subjected to static or quasi-static loading conditions. The time (CCI), t0.2 to an initial crack extension δai = 0.2 mm from the onset of first applied force and creep crack growth rate, ˙a or da/dt is expressed in terms of the magnitude of creep crack growth relating parameters, C* or K. With C* defined as the steady state determination of the crack tip stresses derived in principal from C*(t) and Ct (1-14). The crack growth derived in this manner is identified as a material property which can be used in modeling and life assessment methods (15-25). 1.1.1 The choice of the crack growth correlating parameter C*, C*(t), Ct, or K depends on the material creep properties, geometry and size of the specimen. Two types of material behavior are generally observed during creep crack growth tests; creep-ductile (1-14) and creep-brittle (26-37). In creep ductile materials, where cr...

  12. Analysis of Cracking Mode of Anchor Structure of Underground Engineering Induced by Reinforcement Corrosion

    Directory of Open Access Journals (Sweden)

    Wantao Ding

    2014-02-01

    Full Text Available Based on elastic theory and assumption of maximum tensile-stress failure criterion, together with construction process of anchor structure and rust expansion critical process, this study proposed a simplified reinforcement rust expansion mechanical model of anchor structure system. Elastic criterion of different initial cracking mode was rewarded under different stress ratios. According to analysis of critical cracking mode of different medium, cracking order of mortar and surrounding rock depended on their material parameters, in-situ stress and thickness of mortar cover. Critical cracking conditions of different medium without effect of in-situ stress was the same as that of considering in-situ stress while k is equal to 3 or 1/3. And engineering example shows that three different cracking modes exist under different stress ratios. The result provides a useful reference for analysis of mechanical deterioration mechanism of anchor structure and design of support structure of underground engineering.

  13. Slow Crack Growth and Fatigue Life Prediction of Ceramic Components Subjected to Variable Load History

    Science.gov (United States)

    Jadaan, Osama

    2001-01-01

    Present capabilities of the NASA CARES/Life (Ceramic Analysis and Reliability Evaluation of Structures/Life) code include probabilistic life prediction of ceramic components subjected to fast fracture, slow crack growth (stress corrosion), and cyclic fatigue failure modes. Currently, this code has the capability to compute the time-dependent reliability of ceramic structures subjected to simple time-dependent loading. For example, in slow crack growth (SCG) type failure conditions CARES/Life can handle the cases of sustained and linearly increasing time-dependent loads, while for cyclic fatigue applications various types of repetitive constant amplitude loads can be accounted for. In real applications applied loads are rarely that simple, but rather vary with time in more complex ways such as, for example, engine start up, shut down, and dynamic and vibrational loads. In addition, when a given component is subjected to transient environmental and or thermal conditions, the material properties also vary with time. The objective of this paper is to demonstrate a methodology capable of predicting the time-dependent reliability of components subjected to transient thermomechanical loads that takes into account the change in material response with time. In this paper, the dominant delayed failure mechanism is assumed to be SCG. This capability has been added to the NASA CARES/Life (Ceramic Analysis and Reliability Evaluation of Structures/Life) code, which has also been modified to have the ability of interfacing with commercially available FEA codes executed for transient load histories. An example involving a ceramic exhaust valve subjected to combustion cycle loads is presented to demonstrate the viability of this methodology and the CARES/Life program.

  14. Assessment of copper resistance to stress-corrosion cracking in nitrite solutions by means of joint analysis of acoustic emission measurements, deformation diagrams, qualitative and quantitative fractography, and non-linear fracture mechanics

    Energy Technology Data Exchange (ETDEWEB)

    Khanzhin, V.G.; Nikulin, S.A. [Moscow State Inst. of Steel and Alloys (Russian Federation)

    2005-06-01

    straining of MT specimens, the SCC crack front is found to shrink, due to crack tunneling between the shear lips extending from the specimen sides, and also to propagate by characteristic 'SCC lobes', which have a dark appearance and a rough surface morphology. At even higher loads on MT specimens, the SCC process becomes completely suppressed by the developed plastic deformation. The plastic crack opening proceeds by the usual mechanism of ductile fracture. The total crack advance in the CT specimen after 1,200 hours of testing (total time of SCC testing about 1,400 hours, minus the incubation period, 200 hours) was about 1.3 mm, which gives an estimate of the average crack growth rate of order of 3x10{sup -7} mm/s, for the conditions of continuous pumping of the corrosive solution through the crack. The fracture resistance of copper was estimated to be K{sub i} = 10.5 MPax{radical}m, J{sub i} = 114.6 kJ/m{sup 2} and K{sub i} = 29.3 MPax{radical}m, J{sub i} = 578 kJ/m{sup 2} for the first and the second stage of SCC kinetics, respectively. For the off-center loaded CT specimen, pre-embrittled after the static SCC test, the J-integral estimates were J{sub i} 98.3 kJ/m{sup 2} and J{sub i} = 380.4 kJ/m{sup 2}, for the first and the second kinetic stages of SCC fracture, respectively.

  15. Intergranular stress corrosion cracking of type 304 stainless steels treated with inhibitive chemicals in high temperature pure water

    Energy Technology Data Exchange (ETDEWEB)

    Yeh, T.K. [Nuclear Science and Technology Development Center, National Tsing-Hua Univ. Taiwan (China); Lee, M.Y.; Tsai, C.H. [Department of Engineering and System Science, National Tsing-Hua Univ. Taiwan (China)

    2002-07-01

    Electrochemical potentiodynamic polarizations, electrochemical corrosion potential (ECP) measurements and slow strain rate tensile (SSRT) tests were conducted to investigate the intergranular stress corrosion cracking (IGSCC) characteristics of Type 304 stainless steels treated with inhibitive chemicals in simulated boiling water reactor (BWR) environments. A number of thermally sensitized specimens were prepared and were pre-oxidized in a 288 C environment with the presence of 300 ppb dissolved oxygen for 360 hours. Most of the specimens were then treated with various chemicals including powdered zirconium oxide (ZrO{sub 2}), powdered titanium oxide (TiO{sub 2}), and zirconyl nitrate [ZrO(NO{sub 3}){sub 2}] via static immersion at 90 C, 150 C, and 200 C. Test environments were specifically designed in a circulation loop to create a dissolved oxygen concentration of 300 ppb. Test results showed that the corrosion current densities of all treated specimens were lower than that of the untreated, pre-oxidized specimen at ambient temperature in a solution mixed with 1 mM K{sub 3}Fe(CN){sub 6} and 1 mM K{sub 4}Fe(CN){sub 6}. The ECPs of the treated specimens could be lower or higher than that of the pre-oxidized one at 288 C, depending upon the type of treating chemical and the treating temperature. In addition, IGSCC was observed on all specimens (treated or untreated) in the same environment. However, the untreated specimen exhibited lower elongation, shorter failure time, and more secondary cracks on the side surfaces. It was therefore suggested that inhibitive chemicals such as ZrO{sub 2}, TiO{sub 2}, and ZrO(NO{sub 3}){sub 2} did provide a certain degree of enhancement in improving the mechanical behavior of the treated specimens and in prolonging the IGSCC initiation time. (authors)

  16. Effects of loading variables on fatigue-crack growth in liquid-metal environments

    CSIR Research Space (South Africa)

    Fernandes, PJL

    1995-10-01

    Full Text Available is examined using standard LEFM testing procedures. The effects of environment, load ratio, cyclic frequency and load waveform on the rate of crack growth are investigated. At Delta K > Delta K-th, crack growth rates are approximately an order of magnitude...

  17. Crack Growth Monitoring by Embedded Optical Fibre Bragg Grating Sensors: Fibre Reinforced Plastic Crack Growing Detection

    DEFF Research Database (Denmark)

    Pereira, Gilmar Ferreira; Mikkelsen, Lars Pilgaard; McGugan, Malcolm

    2015-01-01

    This article presents a novel method to asses a crack growing/damage event in fibre reinforced plastic, or adhesive using Fibre Bragg Grating (FBG) sensors embedded in a host material. Different features of the crack mechanism that induce a change in the FBG response were identified. Double Canti...

  18. Theoretical and numerical studies on morphological transitions in crack growth

    CERN Document Server

    Mühle, V

    1999-01-01

    This paper investigates the formation of crack patterns in stationary and transient temperature fields analytically with linear elastic fracture mechanics and numerically with the finite elements method (FEM). In particular, we consider the experimental situation of a narrow thin strip of hot glass slowly lowered into cold water, with temperature difference and velocity as variable parameters. The parameter regions of no crack, one straight crack and one oscillating crack are determined. The type of phase transition related to the borderline between straight and oscillating crack is characterized. The theoretical results are compared with those of other Similar investigations and comparisons are done for the propagation of multiple cracks. Quenching of a wide thin strip leads to a hierarchy of cracks whose scaling properties are analyzed. Without any fitting, theory and experiment agree surprisingly well.

  19. DEVELOPMENT OF AN EMAT IN-LINE INSPECTION SYSTEM FOR DETECTION, DISCRIMINATION, AND GRADING OF STRESS CORROSION CRACKING IN PIPELINES

    Energy Technology Data Exchange (ETDEWEB)

    Jeff Aron; Jon Gore, Roger Dalton; Stuart Eaton; Adrian Bowles; Owen Thomas; Tim Jarman

    2003-07-01

    This report describes progress, experiments, and results for a project to develop a pipeline inline inspection tool that uses electromagnetic acoustic transducers (EMATs) to detect and grade stress corrosion cracking (SCC). There is a brief introduction that gives background material about EMATs and relevant previous Tuboscope work toward a tool. This work left various choices about the modes and transducers for this project. The experimental section then describes the lab systems, improvements to these systems, and setups and techniques to narrow the choices. Improvements, which involved transducer matching networks, better magnetic biasing, and lower noise electronics, led to improved signal to noise (SNR) levels. The setups permitted transducer characterizations and interaction measurements in plates with man-made cracks, pipeline sections with SCC, and a full pipe with SCC. The latter were done with a moveable and compact EMAT setup, called a lab mouse, which is detailed. Next, the results section justifies the mode and transducer choices. These were for magnetostrictive EMATs and the use of EMAT launched modes: SH0 (at 2.1 MHz-mm) and SV1 (at 3.9 MHz-mm). This section then gives details of measurements on these modes. The measurements consisted of signal to noise ratio, insertion loss, magnetic biasing sensitivities crack reflection and transmission coefficients, beam width, standoff and tilt sensitivities. For most of the measurements the section presents analysis curves, such as reflection coefficient versus crack depth. Some notable results for the chosen modes are: that acceptable SNRs were generated in a pipe with magnetostrictive EMATs, that optimum bias for magnetostrictive transmitters and receivers is magnetic saturation, that crack reflection and transmission coefficients from crack interactions agree with 2 D simulations and seem workable for crack grading, and that the mouse has good waveform quality and so is ready for exhaustive measurement EMAT

  20. Stress Corrosion Cracking Behavior of Multipass TIG-Welded AA2219 Aluminum Alloy in 3.5 wt pct NaCl Solution

    Science.gov (United States)

    Venugopal, A.; Sreekumar, K.; Raja, V. S.

    2012-09-01

    The stress corrosion cracking (SCC) behavior of the AA2219 aluminum alloy in the single-pass (SP) and multipass (MP) welded conditions was examined and compared with that of the base metal (BM) in 3.5 wt pct NaCl solution using a slow-strain-rate technique (SSRT). The reduction in ductility was used as a parameter to evaluate the SCC susceptibility of both the BM and welded joints. The results showed that the ductility ratio ( ɛ NaCl/( ɛ air) was 0.97 and 0.96, respectively, for the BM and MP welded joint, and the same was marginally reduced to 0.9 for the SP welded joint. The fractographic examination of the failed samples revealed a typical ductile cracking morphology for all the base and welded joints, indicating the good environmental cracking resistance of this alloy under all welded conditions. To understand the decrease in the ductility of the SP welded joint, preexposure SSRT followed by microstructural observations were made, which showed that the decrease in ductility ratio of the SP welded joint was caused by the electrochemical pitting that assisted the nucleation of cracks in the form of corrosion induced mechanical cracking rather than true SCC failure of the alloy. The microstructural examination and polarization tests demonstrated a clear grain boundary (GB) sensitization of the PMZ, resulting in severe galvanic corrosion of the SP weld joint, which initiated the necessary conditions for the localized corrosion and cracking along the PMZ. The absence of PMZ and a refined fusion zone (FZ) structure because of the lesser heat input and postweld heating effect improved the galvanic corrosion resistance of the MP welded joint greatly, and thus, failure occurred along the FZ.

  1. Corrosion of steel in cracked concrete: Chloride microanalysis and service life predictions

    NARCIS (Netherlands)

    Pacheco Farias, J.

    2015-01-01

    Reinforcement corrosion is frequently considered as the predominant degradation mechanism affecting reinforced concrete structures. Reinforced concrete structures are commonly subject to harsh environmental and loading conditions in which aggressive species can penetrate. Chlorides, present in

  2. Corrosion of steel in cracked concrete: Chloride microanalysis and service life predictions

    NARCIS (Netherlands)

    Pacheco Farias, J.

    2015-01-01

    Reinforcement corrosion is frequently considered as the predominant degradation mechanism affecting reinforced concrete structures. Reinforced concrete structures are commonly subject to harsh environmental and loading conditions in which aggressive species can penetrate. Chlorides, present in seaw

  3. Stress Corrosion Cracking of X80 Pipeline Steel in Near-Neutral pH Environment under Constant Load Tests with and without Preload

    Institute of Scientific and Technical Information of China (English)

    Y.Z. Jia; J.Q. Wang; E.H. Han; W. Ke1

    2011-01-01

    Constant load tests in NS4 solution purged with N2-5%CO2 gas mixture were conducted on American Petroleum Institute (API) X80 pipeline steel applied in the 2nd West-East (;as Pipeline project with and without preload. The results show that cracks could initiate and propagate in X80 pipeline steel in near-neutral pH environment under a constant load condition. The life of crack initiation and propagation increased with decreasing applied stress. Preload did not change its corrosion behavior obviously. However, preload reduced the time for crack initiation.

  4. Laser Peening for Mitigation of Stress Corrosion Cracking at Welds in Marine Aluminum

    Science.gov (United States)

    2011-06-01

    Second Reader: Joseph C. Farmer THIS PAGE INTENTIONALLY LEFT BLANK i REPORT DOCUMENTATION PAGE Form Approved OMB No. 0704-0188 Public reporting burden...Advisor Joseph C. Farmer Second Reader Knox Millsaps Chair, Department of Mechanical and Aerospace Engineering iv THIS PAGE...Cruisers, in Defense News2010. p. 4. [4] K. N. Tran, M. R. Hill, et al., Welding Journal, 85 (2006) 28. [5] M. G. Fontana , Stress Corrosion, in Corrosion

  5. Allowing for surface preparation in stress corrosion cracking modelling; Prise en compte de l`etat de surface dans la modelisation de la fissuration par corrosion sous contrainte

    Energy Technology Data Exchange (ETDEWEB)

    Berge, P.; Buisine, D. [Electricite de France (EDF), 92 - Clamart (France); Gelpi, A. [FRAMATOME, 92 - Paris-La-Defence (France)

    1997-12-31

    When a 600 alloy component is significantly deformed during installation, by welding, rolling, bending, its stress corrosion cracking in Pressurized Water Nuclear Reactor`s primary coolant, is significantly changed by the initial surface treatment. Therefore, the crack initiated time may be reduced by several orders of magnitude for certain surfaces preparations. Allowing for cold working of the surface, for which modelling is proposed, depends less on the degree of cold work then on the depths of the hardened layers. Honing hardens the metal over depths of about one micron for vessel head penetrations, for example, and has little influence on subsequent behaviour after the part deforms. On the other hand, coarser turning treatment produces cold worked layers which can reach several tens of microns and can very significantly reduce the initiation time compared to fine honing. So evaluation after depths of hardening is vital on test pieces for interpreting laboratory results as well as on service components for estimating their service life. Suppression by mechanical or chemical treatment of these layers, after deformation, seems to be the most appropriate solution for reducing over-stressing connected with surface treatment carried out before deformation. (author). 14 refs.

  6. Elevated temperature crack growth in advanced powder metallurgy aluminum alloys

    Science.gov (United States)

    Porr, William C., Jr.; Gangloff, Richard P.

    1990-01-01

    Rapidly solidified Al-Fe-V-Si powder metallurgy alloy FVS0812 is among the most promising of the elevated temperature aluminum alloys developed in recent years. The ultra fine grain size and high volume fraction of thermally stable dispersoids enable the alloy to maintain tensile properties at elevated temperatures. In contrast, this alloy displays complex and potentially deleterious damage tolerant and time dependent fracture behavior that varies with temperature. J-Integral fracture mechanics were used to determine fracture toughness (K sub IC) and crack growth resistance (tearing modulus, T) of extruded FVS0812 as a function of temperature. The alloy exhibits high fracture properties at room temperature when tested in the LT orientation, due to extensive delamination of prior ribbon particle boundaries perpendicular to the crack front. Delamination results in a loss of through thickness constraint along the crack front, raising the critical stress intensity necessary for precrack initiation. The fracture toughness and tensile ductility of this alloy decrease with increasing temperature, with minima observed at 200 C. This behavior results from minima in the intrinsic toughness of the material, due to dynamic strain aging, and in the extent of prior particle boundary delaminations. At 200 C FVS0812 fails at K levels that are insufficient to cause through thickness delamination. As temperature increases beyond the minimum, strain aging is reduced and delamination returns. For the TL orientation, K (sub IC) decreased and T increased slightly with increasing temperature from 25 to 316 C. Fracture in the TL orientation is governed by prior particle boundary toughness; increased strain localization at these boundaries may result in lower toughness with increasing temperature. Preliminary results demonstrate a complex effect of loading rate on K (sub IC) and T at 175 C, and indicate that the combined effects of time dependent deformation, environment, and strain aging

  7. Influence of crack shielding on subcritical crack growth in zirconia ceramics; Influencia del apantallamientoen la propagacion subcritica de fisuras en materiales de circona

    Energy Technology Data Exchange (ETDEWEB)

    Casellas, D.; Feder, A.; Llanes, L.; Anglada, M.

    2001-07-01

    The increase in fatigue life under a constant applied load, due to the presence of crack shielding, was studied. Time to failure was estimated by using a mathematical function that describes the crack shielding developed during subcritical crack growth. Such results were compared with experimental fatigue lives obtained in Y-TZP/PSZ materials. From this it may be concluded that the initial slope of crack shielding curves greatly influences the rime to failure. (Author) 5 refs.

  8. Multifunctional Integrated Optic Sensor for Detection of Cracks and Corrosion Project

    Data.gov (United States)

    National Aeronautics and Space Administration — Los Gatos Research proposes to develop a new nondestructive inspection sensor system, capable of simultaneously measuring strain-based load and detecting crack,...

  9. Subcritical crack growth in oxide and non-oxide ceramics using the Constant Stress Rate Test

    Directory of Open Access Journals (Sweden)

    Agnieszka Wojteczko

    2015-12-01

    Full Text Available Fracture toughness is one of the most important parameters for ceramics description. In some cases, material failure occurs at lower stresses than described by KIc parameter. In these terms, determination of fracture toughness only, proves to be insufficient. This may be due to environmental factors, such as humidity, which might cause subcritical crack propagation in a material. Therefore, it is very important to estimate crack growth velocities to predict lifetime of ceramics used under specific conditions. Constant Stress Rate Test is an indirect method of subcritical crack growth parameters estimation. Calculations are made by using strength data, thus avoiding crack measurement. The expansion of flaws causes reduction of material strength. If subcritical crack growth phenomenon occurs, critical value of crack lengths increases with decreasing stress rate due to longer time for flaw to grow before the critical crack propagation at KIc takes place. Subcritical crack growth phenomenon is particularly dangerous for oxide ceramics due to chemical interactions occurring as a result of exposure to humidity. This paper presents results of Constant Stress Rate Test performed for alumina, zirconia, silicon carbide and silicon nitride in order to demonstrate the differences in subcritical crack propagation phenomenon course.

  10. The reduction in fatigue crack growth resistance of dentin with depth.

    Science.gov (United States)

    Ivancik, J; Neerchal, N K; Romberg, E; Arola, D

    2011-08-01

    The fatigue crack growth resistance of dentin was characterized as a function of depth from the dentino-enamel junction. Compact tension (CT) specimens were prepared from the crowns of third molars in the deep, middle, and peripheral dentin. The microstructure was quantified in terms of the average tubule dimensions and density. Fatigue cracks were grown in-plane with the tubules and characterized in terms of the initiation and growth responses. Deep dentin exhibited the lowest resistance to the initiation of fatigue crack growth, as indicated by the stress intensity threshold (ΔK(th) ≈ 0.8 MPa•m(0.5)) and the highest incremental fatigue crack growth rate (over 1000 times that in peripheral dentin). Cracks in deep dentin underwent incremental extension under cyclic stresses that were 40% lower than those required in peripheral dentin. The average fatigue crack growth rates increased significantly with tubule density, indicating the importance of microstructure on the potential for tooth fracture. Molars with deep restorations are more likely to suffer from the cracked-tooth syndrome, because of the lower fatigue crack growth resistance of deep dentin.

  11. Use of electrochemical potential noise to detect initiation and propagation of stress corrosion cracks in a 17-4 PH steel

    Energy Technology Data Exchange (ETDEWEB)

    Gonzalez-Rodriguez, J.G. [UAEM, Cuernavaca (Mexico); Salinas-Bravo, V.M.; Garcia-Ochoa, E. [Inst. de Investigaciones Electricas, Temixco (Mexico). Dept. de Fisicoquimica Aplicada; Diaz-Sanchez, A. [Inst. Nacional de Investigaciones Nucleares, Toluca (Mexico). Dept. de Materiales

    1997-09-01

    Corrosion potential transients were associated with nucleation and propagation of stress corrosion cracks in a 17-4 precipitation-hardenable (PH) martensitic stainless steel (SS) during slow strain rate tests (SSRT) at 90 C in deaerated sodium chloride (NaCl) solutions, Test solutions included 20 wt% NaCl at pH 3 and 7, similar to normal and faulted steam turbine environments, respectively. Time series were analyzed using the fast Fourier transform method. At the beginning of straining, the consistent noise behavior was perturbed with small potential transients, probably associated with rupture of the surface oxide layer. After yielding, these transients increased in intensity. At maximum load, the transients were still higher in intensity and frequency. These potential transients were related to crack nucleation and propagation. When the steel did not fail by stress corrosion cracking (SCC), such transients were found only at the beginning of the test. The power spectra showed some differences in all cases in roll-off slope and voltage magnitude, but these were not reliable tools to monitor the initiation and propagation of stress corrosion cracks.

  12. STOCHASTIC CRACKING AND HEALING BEHAVIORS OF THIN FILMS DURING REACTION-DIFFUSION GROWTH

    Institute of Scientific and Technical Information of China (English)

    S.L. Zhu; S.L. Yang; Y.M. Xiong; M.S. Li; S.J. Geng; C.S. Hu; Fuhui Wang; W. T. Wu

    2001-01-01

    The stochastic cracking and healing behaviors of reaction-diffusion growth of thin filmswere studied by means of Markov processes analysis. We chose the thermal growth ofoxide scales on metals as an example of reaction-diffusion growth. The thermal growthof oxide films follows power law when no cracking occurs. Our results showed that thegrowth kinetics under stochastic cracking and healing conditions was different fromthat without cracking. It might be altered to either pseudo-linear or pseudo-power lawsdependent upon the intensity and frequency of the cracking of the films. When thehoping items dominated, the growth followed pseudo-linear law; when the diffusionalitems dominated, it followed pseudo-power law with the exponentials lower than theintrinsical values. The numerical results were in good agreement with the meassuredkinetics of isothermal and cyclic oxidation of NiAl-0.1 Y (at. %) alloys in air at 1273K.

  13. Crack-growth behavior in thick welded plates of Inconel 718 at room and cryogenic temperatures

    Science.gov (United States)

    Forman, R. G.

    1974-01-01

    Results of mechanical-properties and axial-load fatigue and fracture tests performed on thick welded plates of Inconel 718 superalloy are presented. The test objectives were to determine the tensile strength properties and the crack-growth behavior in electron-beam, plasma-arc, and gas tungsten are welds for plates 1.90 cm (0.75 in) thick. Base-metal specimens were also tested to determine the flaw-growth behavior. The tests were performed in room-temperature-air and liquid nitrogen environments. The experimental crack-growth-rate data are correlated with theoretical crack-growth-rate predictions for semielliptical surface flaws.

  14. Interface debond crack growth in tension–tension cyclic loading of single fiber polymer composites

    DEFF Research Database (Denmark)

    Pupurs, Andrejs; Goutianos, Stergios; Brøndsted, Povl;

    2013-01-01

    Fiber/matrix interface debond crack growth from a fiber break is defined as one of the key mechanisms of fatigue damage in unidirectional composites. Considering debond as an interface crack its growth in cyclic loading is analyzed utilizing a power law, where the debond growth rate is a power...... for glass fiber/epoxy single fiber composites. Analytical method in the steady-state growth region and FEM for short debonds are combined for calculating the strain energy release rate of the growing debond crack. Interface failure parameters in fatigue are determined by fitting the modeling...

  15. Flaw growth of 7075, 7475, 7050 and 7049 aluminum alloy plate in stress corrosion environments

    Science.gov (United States)

    Dorward, R. C.; Hasse, K. R.

    1976-01-01

    Marine atmosphere and laboratory stress corrosion test results on smooth and precracked specimens from 7075, 7475, 7050, and 7049 alloy plates (1.25 and 3.0-in. thick) are presented. It is shown that for a given strength level, alloys 7050-T7X and 7049-T7X have superior short-transverse stress corrosion resistance (SCR) to 7X75-T7X. At typical strength levels above the minimum, for example, SCR of these alloys is considerably better than that of 7075-T76, and approaches that of 7075-T73. Alloy 7475 maintains an advantage in the area of fracture toughness, however, because it can be thermally processed to give particularly clean microstructures. Results from precracked specimens are in good qualitative agreement with those obtained from smooth specimens. Although both specimen types are capable of distinguishing between -T6, -T76 and -T73 tempers in relatively short time periods the precracked specimen provides more information about crack growth rates.

  16. Application of the cracked pipe element to creep crack growth prediction

    Energy Technology Data Exchange (ETDEWEB)

    Brochard, J.; Charras, T.

    1997-04-01

    The modification of a computer code for leak before break analysis is very briefly described. The CASTEM2000 code was developed for ductile fracture assessment of piping systems with postulated circumferential through-wall cracks under static or dynamic loading. The modification extends the capabilities of the cracked pipe element to the determination of fracture parameters under creep conditions (C*, {phi}c and {Delta}c). The model has the advantage of evaluating significant secondary effects, such as those from thermal loading.

  17. Effect of cold work hardening on stress corrosion cracking of stainless steels in primary water of pressurized water reactors

    Energy Technology Data Exchange (ETDEWEB)

    Raquet, O.; Herms, E. [CEA/Saclay, DEN/DPC, 91191 Gif sur Yvette Cedex (France); Vaillant, F.; Couvant, T.; Boursier, J.M. [EDF/Les Renardieres, R and D/MMC, 77250 Moret sur Loing (France)

    2004-07-01

    A R and D program is carried out in CEA and EDF laboratories to investigate separately the effects of factors which could contribute to IASCC mechanism. In the framework of this study, the influence of cold work on SCC of ASSs in primary water is studied to supply additional knowledge concerning the contribution of radiation hardening on IASCC of ASSs. Solution annealed ASSs, essentially of type AISI 304(L) and AISI 316(L), are generally considered very resistant to SCC in nominal primary water. However, Constant Extension Rate Tests (CERTs), performed on cold pressed humped specimens in nominal primary water at 360 deg. C, reveal that these materials can exhibit a high SCC susceptibility: deepest cracks reach 1 mm (mean crack growth rate about 1 {mu}m.h{sup -1}) and propagation is mainly intergranular for 304L and mainly transgranular for 316L. Indeed, work hardening in conjunction with high localized deformation can promote SCC. The influence of the nature of the cold work (shot peening, reaming, cold rolling, counter sinking, fatigue work hardening and tensile deformation) is investigated by means of screening CERTs performed with smooth specimens in 304L at 360 deg. C. For a given cold work hardening level, the susceptibility to crack initiation strongly depends on the cold working process, and no propagation is observed for a hardness level lower than 300 {+-}10 HV(0.49N). The propagation of cracks is observed only for dynamic loadings like CERT, traction/relaxation tests and crack growth rate tests performed with CT specimens under trapezoidal loading. Although crack initiation is observed for constant load and constant deformation tests, crack propagation do not seem to occur under these mechanical solicitations for 17000 hours of testing, even for hardness levels higher than 450 HV(0.49N). The mean crack growth rate increases when the hardness increases. An important R and D program is in progress to complement these results and to develop a SCC model for

  18. Crack growth in the through-thickness direction of hydrided thin-wall Zircaloy sheet

    Science.gov (United States)

    Raynaud, Patrick A.; Koss, Donald A.; Motta, Arthur T.

    2012-01-01

    In a reactivity-initiated accident, cladding failure may occur by crack initiation within a defect such as a hydride rim or blister and subsequent crack propagation through the thickness of the thin-wall cladding. In such a circumstance, determining the cladding resistance to crack propagation in the through-thickness direction is crucial to predicting cladding failure. To address this issue, through-thickness crack propagation in hydrided Zircaloy-4 sheet was analyzed at 25 °C, 300 °C, and 375 °C. At 25 °C, the fracture toughness decreased with increasing hydrogen content and with an increasing fraction of radial hydrides. Hydride particles fractured ahead of the crack tip, creating a path for crack growth. At both 300 °C and 375 °C, the resistance to crack-growth initiation was sufficiently high that crack extension was often caused by crack-tip blunting. There was no evidence of hydride particles fracturing near the crack tip, and no significant effect of hydrogen content on fracture toughness was observed at these elevated temperatures.

  19. Improvement of the extended finite element method for ductile crack growth

    Energy Technology Data Exchange (ETDEWEB)

    Pourmodheji, R. [Department of Mechanical Engineering, Isfahan University of Technology, Isfahan 84156-83111 (Iran, Islamic Republic of); Mashayekhi, M., E-mail: mashayekhi@cc.iut.ac.ir [Department of Mechanical Engineering, Isfahan University of Technology, Isfahan 84156-83111 (Iran, Islamic Republic of)

    2012-08-15

    The continuum damage mechanics (CDM) model is added to the extended finite element method (XFEM) to provide a model of ductile crack growth. In this model, the criterion for crack growth in the evaluation of ductile materials is the critical damage parameter obtained from continuum damage mechanics. Numerical implementation of the CDM-XFEM model was used to simulate crack growth modeling in comparison with experimental results, and the results are presented in this paper. The CDM-XFEM model was experimentally validated by the ductile damage evolution measured in A533B1 steel through three-point bending and compact tension tests. The identification of damage parameters was performed under various conditions. The critical load at crack growth initiation, the ductile behavior of cracks and the fracture toughness, J{sub Ic}, were also predicted with the CDM-XFEM model simulations. The results confirm the potential of the CDM-XFEM model for predicting crack growth in ductile materials. Using the proposed model, crack propagation has been simulated within two examples; center inclined crack and single edged notched beam for A533B1 steel.

  20. Effects of microstructure and crystallography on crack path and intrinsic resistance to shear-mode fatigue crack growth

    Directory of Open Access Journals (Sweden)

    J. Pokluda

    2015-10-01

    Full Text Available The paper focuses on the effective resistance and the near-threshold growth mechanisms in the ferritic-pearlitic and the pure pearlitic steel. The influence of microstructure on the shear-mode fatigue crack growth is divided here into two factors: the crystal lattice type and the presence of different phases. Experiments were done on ferritic-pearlitic steel and pearlitic steel using three different specimens, for which the effective mode II and mode III threshold values were measured and fracture surfaces were reconstructed in three dimensions using stereophotogrammetry in scanning electron microscope. The ferritic-pearlitic and pearlitic steels showed a much different behaviour of modes II and III cracks than that of the ARMCO iron. Both the deflection angle and the mode II threshold were much higher and comparable to the austenitic steel. Mechanism of shear-mode crack behaviour in the ARMCO iron, titanium and nickel were described by the model of emission of dislocations from the crack tip under a dominant mode II loading. In other tested materials the cracks propagated under a dominance of the local mode I. In the ferritic-pearlitic and pearlitic steels, the reason for such behaviour was the presence of the secondary-phase particles (cementite lamellas, unlike in the previously austenitic steel, where the fcc structure and the low stacking fault energy were the main factors. A criterion for mode I deflection from the mode II crack-tip loading, which uses values of the effective mode I and mode II thresholds, was in agreement with fractographical observations.

  1. Fatigue crack growth behavior of the simulated HAZ of 800 MPa grade high-performance steel

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Sanghoon [Division of Materials Science and Engineering, Hanyang University, 17 Haengdang-dong, Seongdong-gu, Seoul 133-791 (Korea, Republic of); Kang, Donghwan; Kim, Tae-Won [School of Mechanical Engineering, Hanyang University, 17 Haengdang-dong, Seongdong-gu, Seoul 133-791 (Korea, Republic of); Lee, Jongkwan [Research Institute of Industrial Science and Technology, 75-9, Youngcheon, Dongtan, Hwaseong, Gyeonggi-do 445-813 (Korea, Republic of); Lee, Changhee, E-mail: chlee@hanyang.ac.kr [Division of Materials Science and Engineering, Hanyang University, 17 Haengdang-dong, Seongdong-gu, Seoul 133-791 (Korea, Republic of)

    2011-03-15

    Research highlights: {yields} Fatigue crack resistances of HSB800 base steel and HAZs: Base steel > FGHAZ > CGHAZ > ICCGHAZ. {yields} In the case of ICCGHAZ, fatigue cracks are rapidly initiated and propagated through massive M-A constituents. {yields} Fatigue crack growth rate of CGHAZ was faster than that of FGHAZ, mainly due to the coarsened prior austenite grain and martensite packet. - Abstract: The present study focuses on the fatigue properties in the weld heat-affected zone (HAZ) of 800 MPa grade high-performance steel, which is commonly used in bridges and buildings. Single- and multi-pass HAZs were simulated by the Gleeble system. Fatigue properties were estimated using a crack propagation test under a 0.3 stress ratio and 0.1 load frequencies. The microstructures and fracture surfaces were analyzed by optical microscopy, scanning electron microscopy, and transmission electron microscopy. The results of the crack propagation test showed that the fatigue crack growth rate of coarse-grained HAZ (CGHAZ) was faster than fine-grained HAZ (FGHAZ), although both regions have identical fully martensite microstructures, because FGHAZ has smaller prior austenite grain and martensite packet sizes, which can act as effective barriers to crack propagation. The fatigue crack growth rate of intercritically reheated CGHAZ (ICCGHAZ) was the fastest among local zones in the HAZ, due to rapid crack initiation and propagation via the massive martensite-austenite (M-A) constituent.

  2. Effect of a novel three-step aging on strength, stress corrosion cracking and microstructure of AA7085

    Institute of Scientific and Technical Information of China (English)

    陈送义; 陈康华; 董朋轩; 叶升平; 黄兰萍; 阳代军

    2016-01-01

    The influence of a novel three-step aging on strength, stress corrosion cracking (SCC) and microstructure of AA7085 was investigated by tensile testing and slow strain rate testing combined with transmission electron microscopy (TEM). The results indicate that with the increase of second-step aging time of two-step aging, the mechanical properties increase first and then decrease, while the SCC resistance increases. Compared with two-step aging, three-step aging treatment improves SCC resistance and the strength increases by about 5%. The effects of novel three-step aging on strength and SCC resistance are explained by the role of matrix precipitates and grain boundary precipitates, respectively.

  3. Effects of cold work on stress corrosion cracking of type 316L stainless steel in hot lithium hydroxide solution

    Energy Technology Data Exchange (ETDEWEB)

    Zheng, J.H.; Bogaerts, W.F. (Univ. of Leuven (Belgium). Dept. of Metallurgy and Materials Engineering)

    1993-07-01

    Lithium hydroxide (LiOH) has ben chose as the lithium compound to be used in the Aqueous Lithium Salt Blanket (ALSB) concept that has been proposed as a possible driver blanket for the Next European Torus (NET), the next generation of fusion testing devices in Europe, as well as for the International Thermonuclear Experimental Reactor program (ITER). The stress corrosion cracking (SCC) behavior of cold-worked AISI type 316L stainless steel (SS) in a concentrated lithium salt solution at elevated temperature was investigated. Using the slow strain rate technique, SCC experiments were carried out on 20% and 40% cold-worked materials in a solution of 10g lithium hydroxide and 100 cm[sup 3]H[sub 2]O at 95C under conditions with controlled electrochemical potential. Observation of the fracture surfaces by scanning electron microscope indicated the SCC behavior of the cold-worked steel was essentially different from that of the solution-annealed steel. A ductile fracture of cold-worked samples occurred under open-circuit conditions ([approximately][minus]280 mV) and at 200 mV. Slight intergranular attack was found in the region near the surface of cold-worked specimens when the electrochemical potential was controlled at [minus]120 mV. SCC was observed when the experiments were conducted at +100mV. Intergranular stress corrosion cracking (IGSCC) of solution-annealed material changed into a mixed SCC mode, or a dominant transgranular SCC (TGSCC) with an increase of cold work to 20% and 40%. Compared to the SCC behavior of the solution-annealed 316L, the results showed cold work improved significantly the resistance of 316L SS to IGSCC in the hot LiOH environment. Susceptibility to TGSCC of cold-worked 316L SS increased with increasing extent of cold working. These effects were reviewed with respect to electrochemical and microstructural phenomena.

  4. Fatigue crack growth monitoring of idealized gearbox spline component using acoustic emission

    Science.gov (United States)

    Zhang, Lu; Ozevin, Didem; Hardman, William; Kessler, Seth; Timmons, Alan

    2016-04-01

    The spline component of gearbox structure is a non-redundant element that requires early detection of flaws for preventing catastrophic failures. The acoustic emission (AE) method is a direct way of detecting active flaws; however, the method suffers from the influence of background noise and location/sensor based pattern recognition method. It is important to identify the source mechanism and adapt it to different test conditions and sensors. In this paper, the fatigue crack growth of a notched and flattened gearbox spline component is monitored using the AE method in a laboratory environment. The test sample has the major details of the spline component on a flattened geometry. The AE data is continuously collected together with strain gauges strategically positions on the structure. The fatigue test characteristics are 4 Hz frequency and 0.1 as the ratio of minimum to maximum loading in tensile regime. It is observed that there are significant amount of continuous emissions released from the notch tip due to the formation of plastic deformation and slow crack growth. The frequency spectra of continuous emissions and burst emissions are compared to understand the difference of sudden crack growth and gradual crack growth. The predicted crack growth rate is compared with the AE data using the cumulative AE events at the notch tip. The source mechanism of sudden crack growth is obtained solving the inverse mathematical problem from output signal to input signal. The spline component of gearbox structure is a non-redundant element that requires early detection of flaws for preventing catastrophic failures. In this paper, the fatigue crack growth of a notched and flattened gearbox spline component is monitored using the AE method The AE data is continuously collected together with strain gauges. There are significant amount of continuous emissions released from the notch tip due to the formation of plastic deformation and slow crack growth. The source mechanism of

  5. An investigation of fracture and fatigue crack growth behavior of cast niobium aluminide intermetallics

    Energy Technology Data Exchange (ETDEWEB)

    Ye, F.; Soboyejo, W.O. [Ohio State Univ., Columbus, OH (United States). Dept. of Materials Science and Engineering; Farkas, D. [Department of Materials Science and Engineering, Virginia Polytechnic Institute and State University, 213 Holden Hall, Blacksburg, VA 24061-0237 (United States)

    1999-05-31

    This paper presents the results of a combined experimental and theoretical study of fracture toughness and fatigue crack growth in cast Nb-15Al-xTi (x=10, 25 and 40 at%) niobium aluminide-based intermetallics. Fracture toughness and fatigue crack growth resistance are shown to improve significantly in the cast alloy containing 40 at% Ti. The improvements in the fracture toughness of the 40Ti alloy are shown to be due to the combined effects of ligament toughening, crack-tip plasticity and crack-tip blunting. The atomistic simulations show that the increased plasticity in these alloys is associated with their higher Ti content. The micromechanisms of fatigue crack growth are also elucidated. The implications of the results are discussed for potential structural application of niobium aluminide intermetallics. (orig.) 19 refs.

  6. 7075-T6 and 2024-T351 Aluminum Alloy Fatigue Crack Growth Rate Data

    Science.gov (United States)

    Forth, Scott C.; Wright, Christopher W.; Johnston, William M., Jr.

    2005-01-01

    Experimental test procedures for the development of fatigue crack growth rate data has been standardized by the American Society for Testing and Materials. Over the past 30 years several gradual changes have been made to the standard without rigorous assessment of the affect these changes have on the precision or variability of the data generated. Therefore, the ASTM committee on fatigue crack growth has initiated an international round robin test program to assess the precision and variability of test results generated using the standard E647-00. Crack growth rate data presented in this report, in support of the ASTM roundrobin, shows excellent precision and repeatability.

  7. The Effect of Sensitization on the Stress Corrosion Cracking of Aluminum Alloy 5456

    Science.gov (United States)

    2012-06-01

    electrochemically active particles. (From Jones, [26]) ....................................23 Figure 16. Illustration of corrosion tunnel model. (a) Schematic of...46 Table 6. Grinding and Polishing Conditions...approaches continuity along grain boundaries. The β phase is more anodic than the surrounding material matrix and therefore is electrochemically more

  8. Effect of pH Value on Stress Corrosion Cracking of X70 Pipeline Steel in Acidic Soil Environment

    Institute of Scientific and Technical Information of China (English)

    Zhiyong LIU; Cuiwei DU; Xin ZHANG; Fuming WANG; Xiaogang LI

    2013-01-01

    The effect of pH value on the stress corrosion cracking (SCC) of API X70 pipeline steel in simulated acidic soil solutions was investigated by using slow strain rate test,electrochemical polarization curves,electrochemical impedance spectroscopy,and scanning electron microscopy.pH plays an important role in the susceptibility and electrochemical mechanism of SCC.The pH higher than 5 has no significant effect on electrochemical processes.By contrast,the pH lower than 5 intensifies cathodic hydrogen evolution reactions,thus increasing the cathodic current and corrosion potential.Under different pH values,the SCC mechanism of X70 pipeline steel varies among anodic dissolution (AD),hydrogen embrittlement (HE),and the combination of AD and HE (AD + HE) with variations of applied potential.At-850 mVSCE,the SCC mechanism is HE if pH is less than 4 or AD + HE if pH value is more positive.

  9. Fatigue crack growth from handling surface anomalies in a Nickel based superalloy at high temperature

    Directory of Open Access Journals (Sweden)

    Gourdin Stéphane

    2014-06-01

    Full Text Available Aircraft engine manufacturers have to demonstrate that handling surface anomalies in sensible areas of discs are not critical for in-service life of a component. Currently, the models used consider anomalies as long cracks propagating from the first cycle, which introduce a certain degree of conservatism when calculating the fatigue life of surface flaws. Preliminary studies have shown that the first stages of crack propagation from surface anomalies are responsible for the conservative results. Thus, the aim of the study is to characterize the crack propagation from typical surface anomalies and to establish a new crack growth model, which can account for the micro-propagation stage.

  10. Finite element simulation of stress intensity factors in elastic-plastic crack growth

    Institute of Scientific and Technical Information of China (English)

    ALSHOAIBI Abdulnaser M.; ARIFFIN Ahmad Kamal

    2006-01-01

    A finite element program developed elastic-plastic crack propagation simulation using Fortran language. At each propagation step, the adaptive mesh is automatically refined based on a posteriori h-type refinement using norm stress error estimator. A rosette of quarter-point elements is then constructed around the crack tip to facilitate the prediction of crack growth based on the maximum normal stress criterion and to calculate stress intensity factors under plane stress and plane strain conditions.Crack was modelled to propagate through the inter-element in the mesh. Some examples are presented to show the results of the implementation.

  11. The role of grain boundary structure and crystal orientation on crack growth asymmetry in aluminum

    Energy Technology Data Exchange (ETDEWEB)

    Adlakha, I. [School for Engineering of Matter, Transport, and Energy, Arizona State University, Tempe, AZ 85287 (United States); Tschopp, M.A. [U.S. Army Research Laboratory, Aberdeen Proving Ground, MD 21005 (United States); Solanki, K.N., E-mail: kiran.solanki@asu.edu [School for Engineering of Matter, Transport, and Energy, Arizona State University, Tempe, AZ 85287 (United States)

    2014-11-17

    Atomistic simulations have shown that the grain boundary (GB) structure affects a number of physical, mechanical, thermal, and chemical properties, which can have a profound effect on macroscopic properties of polycrystalline materials. The research objective herein is to use atomistic simulations to explore the role that GB structure and the adjacent crystallographic orientations have on the directional asymmetry of an intergranular crack (i.e. cleavage behavior is favored along one direction, while ductile behavior along the other direction of the interface) for aluminum grain boundaries. Simulation results from seven 〈110〉 symmetric tilt grain boundaries (STGBs) show that the GB structure and the associated free volume directly influence the stress–strain response, crack growth rate, and crack tip plasticity mechanisms for middle-tension (M(T)) crack propagation specimens. In particular, the structural units present within the GB promote whether a dislocation or twinning-based mechanism operates at the crack tip during intergranular fracture along certain GBs (e.g., the ‘E’ structural unit promotes twinning at the crack tip in Al). Furthermore, the crystallography of the adjacent grains, and therefore the available slip planes, can significantly affect the crack growth rates in both directions of the crack – this creates a strong directional asymmetry in the crack growth rate in the Σ11 (113) and the Σ27 (552) STGBs. Upon comparing these results with the theoretical Rice criterion, it was found that certain GBs in this study (Σ9 (221), Σ11 (332) and Σ33 (441)) show an absence of directional asymmetry in the observed crack growth behavior, in conflict with the Rice criterion. The significance of the present research is that it provides a physical basis for the role of GB character and crystallographic orientation on intergranular crack tip deformation behavior.

  12. An evaluation of microbial growth and corrosion of 316L SS in glycol/seawater mixtures

    Science.gov (United States)

    Lee, Jason S.; Ray, Richard I.; Lowe, Kristine L.; Jones-Meehan, Joanne; Little, Brenda J.

    2003-01-01

    Glycol/seawater mixtures containing > 50% glycol inhibit corrosion of 316L stainless steel and do not support bacterial growth. The results indicate bacteria are able to use low concentrations of glycol (10%) as a growth medium, but bacterial growth decreased with increasing glycol concentration. Pitting potential, determined by anodic polarization, was used to evaluate susceptibility of 316L SS to corrosion in seawater-contaminated glycol. Mixture containing a minimum concentration of 50% propylene glycol-based coolant inhibited pitting corrosion. A slightly higher minimum concentration (55%) was needed for corrosion protection in ethylene glycol mixtures.

  13. Effect of fracture surface roughness on shear crack growth

    Energy Technology Data Exchange (ETDEWEB)

    Gross, T.S.; Watt, D.W. (New Hampshire Univ., Durham, NH (United States). Dept. of Mechanical Engineering); Mendelsohn, D.A. (Ohio State Univ., Columbus, OH (United States). Dept. of Engineering Mechanics)

    1992-12-01

    A model of fracture surface interference for Mode I fatigue crack profiles was developed and evaluated. Force required to open the crack faces is estimated from point contact expressions for Mode I stress intensity factor. Force transfer across contacting asperities is estimated and used to calculate Mode II resistance stress intensity factor (applied factor is sum of effective and resistance factors). Electro-optic holographic interferometry was used to measure 3-D displacement field around a Mode I fatigue pre-crack in Al loaded in Mode II shear. Induced Mode I crack face displacements were greater than Mode II displacements. Plane stress shear lip caused displacement normal to surface as the crack faces are displaced. Algorithms are being developed to track the displacements associated with the original coordinate system in the camera. A 2-D boundary element method code for mixed mode I and II loading of a rough crack (sawtooth asperity model) has been completed. Addition of small-scale crack tip yielding and a wear model are completed and underway, respectively.

  14. Crack Growth Monitoring by Embedded Optical Fibre Bragg Grating Sensors: Fibre Reinforced Plastic Crack Growing Detection

    DEFF Research Database (Denmark)

    Pereira, Gilmar Ferreira; Mikkelsen, Lars Pilgaard; McGugan, Malcolm

    2015-01-01

    This article presents a novel method to asses a crack growing/damage event in fibre reinforced plastic, or adhesive using Fibre Bragg Grating (FBG) sensors embedded in a host material. Different features of the crack mechanism that induce a change in the FBG response were identified. Double...... Cantilever Beams specimens made with glass fibre glued with structural adhesive, were instrumented with an array of FBG sensors embedded in the material and tested using an experimental fracture procedure. A digital image correlation technique was used to determine the presence of the specific phenomena...

  15. Application of the cracked pipe element to creep crack growth prediction

    Energy Technology Data Exchange (ETDEWEB)

    Brochard, J.; Charras, T. [C.E.A.-C.E.-Saclay DRN/DMT, Gif Sur Yvette (France); Ghoudi, M. [C.E.A.-C.E.-Saclay, Gif Sur Yvette (France)

    1997-04-01

    Modifications to a computer code for ductile fracture assessment of piping systems with postulated circumferential through-wall cracks under static or dynamic loading are very briefly described. The modifications extend the capabilities of the CASTEM2000 code to the determination of fracture parameters under creep conditions. The main advantage of the approach is that thermal loads can be evaluated as secondary stresses. The code is applicable to piping systems for which crack propagation predictions differ significantly depending on whether thermal stresses are considered as primary or secondary stresses.

  16. Stress corrosion cracking behavior of Alloy 600 in high temperature water

    Energy Technology Data Exchange (ETDEWEB)

    Webb, G.L.; Burke, M.G.

    1995-07-01

    SCC susceptibility of Alloy 600 in deaerated water at 360 C (statically loaded U-bend specimens) is dependent on microstructure and whether the material was cold-worked and annealed (CWA) or hot-worked and annealed (HWA). All cracking was intergranular, and materials lacking grain boundary carbides were most susceptible to SCC initiation. CWA tubing materials are more susceptible to SCC initiation than HWA ring-rolled forging materials with similar microstructures (optical metallography). In CWA tubing materials, one crack dominated and grew to a visible size. HWA materials with a low hot-working finishing temperature (<925 C) and final anneals at 1010-1065 C developed both large cracks (similar to those in CWA materials) and small intergranular microcracks detectable only by destructive metallography. HWA materials with a high hot-working finishing temperature (>980 C) and a high-temperature final anneal (>1040 C), with grain boundaries that are fully decorated, developed only microcracks in all specimens. These materials did not develop large, visually detectable cracks, even after more than 300 weeks exposure. A low-temperature thermal treatment (610 C for 7h), which reduces or eliminates SCC in Alloy 600, did not eliminate microcrack formation in high temperature processed HWA materials. Conventional metallographic and analytical electron microscopy (AEM) were done on selected materials to identify the factors responsible for the observed differences in cracking behavior. Major difference between high-temperature HWA and low-temperature HWA and CWA materials was that the high temperature processing and final annealing produced predominantly ``semi-continuous`` dendritic M{sub 7}C{sub 3} carbides along grain boundaries with a minimal amount of intragranular carbides. Lower temperature processing produced intragranular M7C3 carbides, with less intergranular carbides.

  17. Stress-induced martensitic transformation in metastable austenitic stainless steels: Effect on fatigue crack growth rate

    Science.gov (United States)

    Khan, Z.; Ahmed, M.

    1996-04-01

    This paper addresses the influence of cyclic stress-induced martensitic transformation on fatigue crack growth rates in metastable austenitic stainless steels. At low applied stress and mean stress values in AISI type 301 stainless steel, fatigue crack growth rate is substantially retarded due to a cyclic stress-induced γ-α' and γ-ɛ martensitic transformation occurring at the crack-tip plastic zone. It is suggested that the transformation products produce a compressive residual stress at the tip of the fatigue crack, which essentially lowers the effective stress intensity and hence retards the fatigue crack growth rate. At high applied stress or mean stress values, fatigue crack growth rates in AISI type 301 steels become almost equal to those of stable AISI type 302 alloy. As the amount of transformed products increases (with an increase in applied or mean stress), the strain-hardening effect brought about by the transformed martensite phase appears to accelerate fatigue crack growth, offsetting the contribution from the compressive residual stress produced by the positive volume change of γ → α' or ɛ transformation.

  18. Measurement and simulation of crack growth rate and direction under non-proportional loadings

    Directory of Open Access Journals (Sweden)

    Y. Hos

    2015-10-01

    Full Text Available A series of fatigue experiments on thin-walled tubes under tension and torsion, the experimental results – crack path and crack growth life – are measured and compared. It is observed that the cracks follow a curvature from a tensile to a shear dominated growth with increasing crack length. The results are enforced by the high amplitudes applied to the specimens causing large cyclic plastic deformations and crack growth rates in the order of 10-3 mm/cycle. The non-linear nature of the cyclic deformation has been taken into account by applying a cyclic plasticity model, and plasticity-induced crack closure is captured by a contact formulation. Already for the uniaxial reference case the current limitations in modelling plasticity induced crack closure – a prerequisite for achieving realistic simulation results – have become obvious. Measurements have shown that friction and roughness induced closure processes come up, especially for non-planar crack surfaces, challenge to be met in the future.

  19. An ultrasonic method for dynamic monitoring of fatigue crack initiation and growth.

    Science.gov (United States)

    Mi, Bao; Michaels, Jennifer E; Michaels, Thomas E

    2006-01-01

    Attached ultrasonic sensors can detect changes caused by crack initiation and growth if the wave path is directed through the area of critical crack formation. Dynamics of cracks opening and closing under load cause nonlinear modulation of received ultrasonic signals, enabling small cracks to be detected by stationary sensors. A methodology is presented based upon the behavior of ultrasonic signals versus applied load to detect and monitor formation and growth of cracks originating from fastener holes. Shear wave angle beam transducers operating in through transmission mode are mounted on either side of the hole such that the transmitted wave travels through the area of expected cracking. Time shift is linear with respect to load, and is well explained by path changes due to strain combined with wave speed changes due to acoustoelasticity. During subsequent in situ monitoring with unknown loads, the measured time of flight is used to estimate the load, and behavior of the received energy as a function of load is the basis for crack detection. Results are presented from low cycle fatigue tests of several aluminum specimens and illustrate the efficacy of the method in both determining the applied load and monitoring crack initiation and growth.

  20. Numerical simulation of the detection of crack in reinforced concrete structures of NPP due to expansion of reinforcing corrosive products using Impact-Echo method

    Directory of Open Access Journals (Sweden)

    Morávka Š.

    2008-12-01

    Full Text Available Nuclear energy boom is starting nowadays. But also current nuclear power plants (NPP are duty to certify their security for regular renewal of their operating licenses. NPP security can be significantly affected by defects of large amount of ageing reinforced concrete structures. Advanced Impact-Echo method seams to be very hopeful to cooperate at performing in-service inspections such structures. Just these in-service inspections are included in the first priority group of specific technical issues according to the recommendations of OECD-Nuclear Energy Agency, Commission on Safety of Nuclear Installation in the field of ageing management.This paper continues of extensive project dealing with Impact-Echo method application. It will present method description and main results of numerical modeling of detection and localization of crack caused by corrosive product expansion. Steel reinforcing rods are subjected to corrosion due to diffusion of corrosive agents from structure surface. Corrosive products have up to 7-times larger volume than pure steel. Raised strain can cad lead up to concrete failure and crack development. We investigate whether it is possible to detect these growing cracks by Impact-Echo method in time.Experimental verification of our numerical predictions is prepared on Civil Faculty in Brno.

  1. Effect of band-overload on fatigue crack growth rate of HSLA steel

    Science.gov (United States)

    Abhinay, S. V.; Tenduwe, Om Prakash; Kumar, Ajit; Dutta, K.; Verma, B. B.; Ray, P. K.

    2015-02-01

    Fatigue crack growth behavior is important parameter of structural materials. This parameters can be used to predict their life, service reliability and operational safety in different conditions. The material used in this investigation is an HSLA steel. In this investigation effect of single overload and band-overload on fatigue crack growth of same steel are studied using compact tension (CT) specimens under mode-I condition and R=0.3. It is observed that overload and band-overload applications resulted retardation on the fatigue crack growth rate in most of the cases. It is also noticed that maximum retardation took place on application of seven successive overload cycles. Application of ten and more overload cycles caused no crack growth retardation.

  2. Stress-Corrosion Cracking in High Strength Steels and in Titanium and Aluminum Alloys

    Science.gov (United States)

    1972-01-01

    widely throughout the technical community and is not available in collected form, the authors of the chapter on titanium have included a much higher...Elements................ 22 Derivation of KI by Specimen Compliance.............. 23 Experiental Determination of Comll-!hlncc........... 24 Theoretical...101. R. T. Ault, Republic Steel Corp., private communication . 102. S. R. Novak and S. T. Rolfe, Kt, Stress-Corrosion Tests of l2Ni-5Cr-3Mo and l8Ni

  3. The Role of Stress in the Corrosion Cracking of Aluminum Alloys

    Science.gov (United States)

    2013-03-01

    orthogonal to the other two directions. This system is used for sheet, extrusions , and forgings with nonsymmetrical grain flow [18]. All testing...around the constituent particles and then spreads to the grain boundaries. It is not possible to determine from the present results if the IGC...International, 2011, pp.1-8. [30] J. R. Scully et al., " Spreading of intergranular corrosion on the surface of sensitized Al-4.4Mg alloys: A general finding

  4. Fatigue Crack Growth Rate of Ti-6Al-4V Considering the Effects of Fracture Toughness and Crack Closure

    Institute of Scientific and Technical Information of China (English)

    ZHANG Junhong; YANG Shuo; LIN Jiewei

    2015-01-01

    Fatigue fracture is one of the main failure modes of Ti-6Al-4V alloy, fracture toughness and crack closure have strong effects on the fatigue crack growth(FCG) rate of Ti-6Al-4V alloy. The FCG rate of Ti-6Al-4V is investigated by using experimental and analytical methods. The effects of stress ratio, crack closure and fracture toughness on the FCG rate are studied and discussed. A modified prediction model of the FCG rate is proposed, and the relationship between the fracture toughness and the stress intensity factor(SIF) range is redefined by introducing a correcting coefficient. Notched plate fatigue tests (including the fracture toughness test and the FCG rate test) are conducted to investigate the influence of affecting factors on the FCG rate. Comparisons between the predicted results of the proposed model, the Paris model, the Walker model, the Sadananda model, and the experimental data show that the proposed model gives the best agreement with the test data particularly in the near–threshold region and the Paris region, and the corresponding calculated fatigue life is also accurate in the same regions. By considering the effects of fracture toughness and crack closure, the novel FCG rate prediction model not only improves the estimating accuracy, but also extends the adaptability of the FCG rate prediction model in engineering.

  5. Fatigue crack growth rate of Ti-6Al-4V considering the effects of fracture toughness and crack closure

    Science.gov (United States)

    Zhang, Junhong; Yang, Shuo; Lin, Jiewei

    2015-03-01

    Fatigue fracture is one of the main failure modes of Ti-6Al-4V alloy, fracture toughness and crack closure have strong effects on the fatigue crack growth(FCG) rate of Ti-6Al-4V alloy. The FCG rate of Ti-6Al-4V is investigated by using experimental and analytical methods. The effects of stress ratio, crack closure and fracture toughness on the FCG rate are studied and discussed. A modified prediction model of the FCG rate is proposed, and the relationship between the fracture toughness and the stress intensity factor(SIF) range is redefined by introducing a correcting coefficient. Notched plate fatigue tests (including the fracture toughness test and the FCG rate test) are conducted to investigate the influence of affecting factors on the FCG rate. Comparisons between the predicted results of the proposed model, the Paris model, the Walker model, the Sadananda model, and the experimental data show that the proposed model gives the best agreement with the test data particularly in the near-threshold region and the Paris region, and the corresponding calculated fatigue life is also accurate in the same regions. By considering the effects of fracture toughness and crack closure, the novel FCG rate prediction model not only improves the estimating accuracy, but also extends the adaptability of the FCG rate prediction model in engineering.

  6. Fatigue Crack Growth Rate of Inconel 718 Sheet at Cryogenic Temperatures

    Science.gov (United States)

    Wells, Douglas; Wright, Jonathan; Hastings, Keith

    2005-01-01

    Inconel 718 sheet material was tested to determine fatigue crack growth rate (FCGR) at cryogenic conditions representative of a liquid hydrogen (LH2) environment at -423 degree F. Tests utilized M(T) and ESE(T) specimen geometries and environments were either cold gaseous helium or submersion in LH2. The test results support a significant improvement in the fatigue crack growth threshold at -423 degree F compared to -320 degree F or 70 degree F.

  7. Simple Predicting Method for Fatigue Crack Growth Rate Based on Tensile Strength of Carbon Steel

    Institute of Scientific and Technical Information of China (English)

    2003-01-01

    Three types of fatigue tests for an annealed carbon steel containing carbon of 0.42 % were carried out on smooth specimens and specimens with a small blind hole in order to investigate the fatigue crack growth law. A simple predicting method for crack growth rates has been proposed involving strength σb and the relation between cyclic stress and strain. The validity of proposed method has been confirmed by experiments on several carbon steels with different loadings.

  8. High Temperature Fatigue Crack Growth Rate of G91 Steel with Applying 30 Seconds Hold Time

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Jong Bum; Park, Chang Gyu; Koo, Gyeong Hoi [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of); Lee, Jong Hoon [Sungkyunkwan University, Suwon (Korea, Republic of); Kim, Bum Joon [Osan Univ., Osan (Korea, Republic of)

    2015-05-15

    Subsection NH since 2004. The database of creep and creep-fatigue crack growth rate of G91 steel is necessary for the structural integrity evaluation of the SFR structures because the database of these properties of materials is insufficient through the world. Moreover, it is difficult to use the database which is gained by the research center of advanced countries because it is not to be opened. Therefore, it is necessary to make an effort to get the database of material properties. Creep-fatigue crack initiation and growth tests for a G91 tubular specimen, including a machined defect, have been performed by Kim and it attempted to assess a high temperature crack behavior of G91 side plate specimen by Lee. Creep-fatigue crack growth rate were compared in terms of different temperature range. Tests were performed at temperatures of 500, 550 and 600, respectively. Stress ratio was set to 0.1 and trapezoidal shape of stress condition was applied to the specimens to perform the creep-fatigue crack growth rate tests. Each specimen's surface was polished and fatigue pre-crack was manufactured by fatigue test before the high temperature test. And DCPD method was adopted to measure the crack length in the high temperature.

  9. Online fatigue crack growth monitoring with clip gauge and direct current potential drop

    OpenAIRE

    De Tender, Steven; Micone, Nahuel; De Waele, Wim

    2016-01-01

    Fatigue is a well-known failure phenomenon which has been and still is extensively studied. Often structures are designed according to the safe-life principle so no crack initiation occurs. Nowadays there is a high emphasis on cost-efficiency, and one might rather opt for a fail-safe design. Therefore a certain amount of crack growth can be allowed in structures, but then a good knowledge of stresses and related crack growth rates is needed. To this end, extensive studies are done to obtain a...

  10. Growth of long fatigue cracks under non-proportional loadings – experiment and simulation

    Directory of Open Access Journals (Sweden)

    Y. Hos

    2016-07-01

    Full Text Available An experimental campaign was carried out on thin-walled tubes under tension and torsion. The results from experiments are measured and compared. It is observed that cracks follow a shear-dominated growth pattern with increasing crack length, instead of a tension-dominated one. The experiments are performed with high amplitudes applied to the specimens, resulting in large cyclic plastic deformations and crack growth rates up to 10-3 mm/cycle. Stress intensity factors were calculated for the proportional loading case.

  11. Simulation Analysis of Whole Cracking Process due to Reinforcement Corrosion in Concrete Structures%钢筋混凝土结构锈胀开裂全过程仿真分析

    Institute of Scientific and Technical Information of China (English)

    徐港; 徐可; 王青; 王谊敏

    2012-01-01

    利用大型有限元软件DIANA,详细分析了绣蚀导致混凝土保护层开裂的全过程.仿真分析表明:混凝土保护层的锈胀开裂过程可分为内裂、扩展、外裂和内外裂缝贯通4个阶段;锈蚀产物膨胀率一定时,混凝土保护层内侧裂缝的产生主要与混凝土抗拉强度相关,其他因素影响甚微;混凝土保护层表面锈胀开裂及其裂缝贯通主要与相对保护层厚度有关,该值越大,裂缝越不容易发展;提高混凝土抗拉强度,能有效延缓锈胀裂缝的产生和发展;在相同条件下,混凝土保护层非均匀锈胀开裂时的钢筋锈蚀率较均匀锈胀开裂时低;混凝土保护层剥落的特征主要与钢筋净间距和保护层厚度的比值相关,当该值较大(>3)时,仅角区保护层发生局部剥落,否则保护层将整体剥落.%By the large-scale finite element software DIANA, the whole splitting process of concrete protective cover layer due to reinforcement corrosion was analyzed in detail. The simulation analysis shows that the whole cracking process can be divided into four steps, that is, internal cracking, crack growth, external cracking, and penetration cracking. At a certain level of the volumetric expansion ratio of corroded products, the internal cracks initiation at internal side of the concrete protective layer around the steel bar is mainly related to the tensile strength of concrete, and other factors have little effect on it. External cracking as well as penetration cracking are related to the ratio of protective layer thickness to bar diameter. The larger the ratio is, the more difficultly the crack propagation occurs. It is effective to improve the tensile strength of concrete by delaying crack initiation and propagation) under the same conditions, the critical corrosion ratio of reinforcing bar at cracking in non-uniform corrosion is lower than thBt in uniform corrosioni the spalling patterns of concrete protective layer are mainly

  12. Kinetics of fatigue crack growth and crack paths in the old puddled steel after 100-years operating time

    Directory of Open Access Journals (Sweden)

    G. Lesiuk

    2015-10-01

    Full Text Available The goal of the authors’ investigations was determination of the fatigue crack growth in fragments of steel structures (of the puddled steel and its cyclic behavior. Tested steel elements coming from the turn of the 19th and 20th were gained from still operating ancient steel construction (a main hall of Railway Station, bridges etc.. This work is a part of investigations devoted to the phenomenon of microstructural degradation and its potential influence on their strength properties. The analysis of the obtained results indicated that those long operating steels subject to microstructure degradation processes consisting mainly in precipitation of carbides and nitrides inside ferrite grains, precipitation of carbides at ferrite grain boundaries and degeneration of pearlite areas [1, 2]. It is worth noticing that resistance of the puddled steel to fatigue crack propagation in the normalized state was higher. The authors proposed the new kinetic equation of fatigue crack growth rate in such a steel. Thus the relationship between the kinetics of degradation processes and the fatigue crack growth rate also have been shown. It is also confirmed by the materials research of the viaduct from 1885, which has not shown any significant changes in microstructure. The non-classical kinetic fatigue fracture diagrams (KFFD based on deformation ( or energy (W approach was also considered. In conjunction with the results of low- and high-cycle fatigue and gradual loss of ductility as a consequence (due to the microstructural degradation processes - it seems to be a promising construction of the new kinetics fatigue fracture diagrams with the energy approach.

  13. Testing study of subcritical crack growth rate and fracture toughness in different rocks

    Institute of Scientific and Technical Information of China (English)

    CAO Ping; LI Jiang-teng; YUAN Hai-ping

    2006-01-01

    Subcritical crack growth of double torsion specimens made of ore, lherzolite, marble and granite was studied using Instron1342 type electro hydraulic servo test machine. The relations of the mode-Ⅰ stress intensity factor KI versus the subcritical crack growth velocity v and the fracture toughness KIC were obtained by the double torsion constant displacement load relaxation method. The behavior of subcritical crack growth was analyzed for different rocks. The results show that lgKI-lgv relations of four kinds of rocks measured by this method accord with linear rule, i.e. the relations between subcritical crack growth velocity and stress intensity factor have a power law, which is in good agreement with CHARLES theory. lgKI-lgv curves move to top left corner with the decrease of the elastic modulus, which implies that the subcritical crack growth velocity speeds up. The maximum subcritical crack growth velocity exhibits negative exponential increase, and mode-Ⅰ fracture toughness KIC decreases with the decrease of elastic modulus. The testing results provide a basis for time-dependence of rock engineering stability.

  14. Influence of chemical liquids on the fatigue crack growth of the AZ31 magnesium alloy

    Science.gov (United States)

    Wang, Zhang-Zhong; He, Xian-Cong; Bai, Yun-Qiang; Ba, Zhi-Xin; Dai, Yu-Ming; Zhou, Heng-Zhi

    2012-03-01

    The fatigue crack growth behavior of an AZ31 magnesium alloy was investigated by comparing the effect of zirconate and phosphate chemical liquids. The morphology, components, and phase compositions of the chemical depositions at the fatigue crack tip were analyzed by employing scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), and X-ray diffraction (XRD), respectively. For samples with and without the chemical liquids, their stress-intensity factor values at the fatigue crack tip were compared by using a stress-strain gauge. The results demonstrated that a zirconate film (Zr x O y ·Zn x O y ) and a phosphate film (Zn3(PO4)2·4H2O and MgZnP2O7) could be formed on the fatigue crack-surface at the fatigue crack tip. The stress distribution was changed because of the chemical depositions and the causticity of the chemical liquids. This could decrease the stress-intensity factor value and thus effectively cause fatigue crack closure, which reduces the fatigue crack growth rate. Moreover, it was found that the fatigue crack closure effect of zirconates was more positive than that of phosphates.

  15. Study of alloy 600`S stress corrosion cracking mechanisms in high temperature water; Etude des mecanismes de corrosion sous contrainte de l`alliage 600 dans l`eau a haute temperature

    Energy Technology Data Exchange (ETDEWEB)

    Rios, R.

    1994-06-01

    In order to better understand the mechanisms involved in Alloy 600`s stress corrosion cracking in PWR environment, laboratory tests were performed. The influence of parameters pertinent to the mechanisms was studies : hydrogen and oxygen overpressures, local chemical composition, microstructure. The results show that neither hydrogen nor dissolution/oxidation, despite their respective roles in the process, are sufficient to account for experimental facts. SEM observation of micro-cleavage facets on specimens` fracture surfaces leads to pay attention to a new mechanism of corrosion/plasticity interactions. (author). 113 refs., 73 figs., 15 tabs., 4 annexes.

  16. Influences of gaseous environment on low growth-rate fatigue crack propagation in steels. Annual report No. 1, January 1980. Report No. FPL/R/80/1030

    Energy Technology Data Exchange (ETDEWEB)

    Ritchie, R.O.; Suresh, S.; Toplosky, J.

    1980-01-01

    The influence of gaseous environment is examined on fatigue crack propagation behavior in steels. Specifically, a fully martensitic 300-M ultrahigh strength steel and a fully bainitic 2-1/4Cr-1Mo lower strength steel are investigated in environments of ambient temperature moist air and low pressure dehumidified hydrogen and argon gases over a wide range of growth rates from 10/sup -8/ to 10/sup -2/ mm/cycle, with particular emphasis given to behavior near the crack propagation threshold ..delta..K/sub 0/. It is found that two distinct growth rate regimes exist where hydrogen can markedly accelerate crack propagation rates compared to air, (1) at near-threshold levels below (5 x 10/sup -6/ mm/cycle) and (2) at higher growth rates, typically around 10/sup -5/ mm/cycle above a critical maximum stress intensity K/sub max//sup T/. Hydrogen-assisted crack propagation at higher growth rates is attributed to a hydrogen embrittlement mechanism, with K/sub max//sup T/ nominally equal to K/sub Iscc/ (the sustained load stress corrosion threshold) in high strength steels, and far below K/sub Iscc/ in the strain-rate sensitive lower strength steels. Hydrogen-assisted crack propagation at near-threshold levels is attributed to a new mechanism involving fretting-oxide-induced crack closure generated in moist (or oxygenated) environments. The absence of hydrogen embrittlement mechanisms at near-threshold levels is supported by tests showing that ..delta..K/sub 0/ values in dry gaseous argon are similar to ..delta..K/sub 0/ values in hydrogen. The potential ramifications of these results are examined in detail.

  17. Creep crack growth in a reactor pressure vessel steel at 360 deg C

    Energy Technology Data Exchange (ETDEWEB)

    Rui Wu; Seitisleam, F.; Sandstroem, R. [Swedish Institute for Metals Research, Stockholm (Sweden)

    1998-12-31

    Plain creep (PC) and creep crack growth (CCG) tests at 360 deg C and post metallography were carried out on a low alloy reactor pressure vessel steel (ASTM A508 class 2) with different microstructures. Lives for the CCG tests were shorter than those for the PC tests and this is more pronounced for simulated heat affected zone microstructure than for the parent metal at longer lives. For the CCG tests, after initiation, the cracks grew constantly and intergranularly before they accelerated to approach rupture. The creep crack growth rate is well described by C*. The relations between reference stress, failure time and steady crack growth rate are presented for the CCG tests. It is demonstrated that the failure stress due to CCG is considerably lower than the yield stress at 360 deg C. Consequently, the CCG will control the static strength of a reactor vessel. (orig.) 17 refs.

  18. Accelerated Threshold Fatigue Crack Growth Effect-Powder Metallurgy Aluminum Alloy

    Science.gov (United States)

    Piascik, R. S.; Newman, J. A.

    2002-01-01

    Fatigue crack growth (FCG) research conducted in the near threshold regime has identified a room temperature creep crack growth damage mechanism for a fine grain powder metallurgy (PM) aluminum alloy (8009). At very low (Delta) K, an abrupt acceleration in room temperature FCG rate occurs at high stress ratio (R = K(sub min)/K(sub max)). The near threshold accelerated FCG rates are exacerbated by increased levels of K(sub max) (K(sub max) = 0.4 K(sub IC)). Detailed fractographic analysis correlates accelerated FCG with the formation of crack-tip process zone micro-void damage. Experimental results show that the near threshold and K(sub max) influenced accelerated crack growth is time and temperature dependent.

  19. Fracture resistance and fatigue crack growth characteristics of two Al-Cu-Mg-Zr alloys

    Science.gov (United States)

    Sarkar, Bhaskar; Lisagor, W. B.

    1992-01-01

    The dependence of strength, fracture resistance, and fatigue crack growth rate on the aging conditions of two alloy compositions based on Al-3.7Cu-1.85Mg-0.2Mn is investigated. Mechanical properties were evaluated in two heat treatment conditions and in two orientations (longitudinal and transverse). Compact tension specimens were used to determine fatigue crack growth characteristics and fracture resistance. The aging response was monitored on coupons using hardness measurements determined with a standard Rockwell hardness tester. Fracture resistance is found to increase with increasing yield strength during artificial aging of age-hardenable 2124-Zr alloys processed by powder metallurgy techniques. Fatigue crack growth rate increases with increasing strength. It is argued that these changes are related to deformation modes of the alloys; a homogeneous deformation mode tends to increase fracture resistance and to decrease the resistance to the fatigue crack propagation rate.

  20. An Effective Fem-Based Approach for Discrete 3D Crack Growth

    DEFF Research Database (Denmark)

    Nielsen, Morten Eggert; Lambertsen, Søren Heide; Pedersen, Erik B.

    2015-01-01

    A new geometric approach for discrete crack growth modeling is proposed and implemented in a commercial FEM software. The basic idea is to model the crack growth by removing volumes of material as the crack front advances. Thereby, adaptive meshing techniques, found in commercial software, is well......-suited for relatively fast and reasonable meshing of the updated geometry. Influence on structural stiffness is negligible, as the amount of removed material is kept insignificant. The approach is automatized in ANSYS APDL and demonstrated by means of energy-based mixed mode stress intensity factors and the crack...... growth direction criterion by Richard. The applicability of the implemented approach is validated against a previously published experimental result, which tests a mixed mode I + III fatigue loading of a modified CT specimen. The proposed approach may be used as a computational framework for modeling...

  1. Creep-Fatigue Crack Growth Interaction in Nickel Base Supper Alloy

    Directory of Open Access Journals (Sweden)

    F. Djavanroodi

    2008-01-01

    Full Text Available Most engineering components which operate at elevated temperatures are subjected to non-steady loading during service. This paper describes the current fracture mechanics concepts that are employed to predict cracking of Nickel base supper alloy materials at high temperatures under low and high frequency cyclic loading. A model for predicting creep crack growth in terms of C* and the creep uniaxial ductility is presented at low frequency and at high frequency power law relation is used to predict the crack growth rate. When dealing with creep/fatigue interaction a simple cumulative damage concept with fractography evidence is used to predict the crack growth rate. It is shown that these models give good agreement with the experimental results.

  2. Fatigue crack growth study of SCS6/Ti-15-3 composite

    Science.gov (United States)

    Kantzos, P.; Telesman, J.

    1990-01-01

    A study was performed to determine the fatigue crack growth (FCG) behavior and the associated fatigue damage processes in a (0)8- and (90)8-oriented SCS6/Ti-15-3 composite. Companion testing was also done on identically processed Ti-15-3 unreinforced material. The active fatigue crack growth failure processes were very similar for both composite orientations tested. For both orientations, fatigue crack growth was along the fiber direction. It was found that the composite constituent most susceptible to fatigue damage was the interface region and, in particular, the carbon coating surrounding the fiber. The failure of the interface region led to crack initiation and also strongly influenced the FCG behavior in this composite. The failure of the interface region was apparently driven by normal stresses perpendicular to the fiber direction. The FCG rates were considerably higher for the (90)8-oriented CT specimens in comparison to the unreinforced material.

  3. Estimation of Crack Growth Properties of High Strength Metallic Materials by a Novel Technique

    Directory of Open Access Journals (Sweden)

    P R Sadananda Rao

    2010-12-01

    Full Text Available This research work proposes a novel technique based on fracture mechanics approach for the quick determination of fatigue crack growth rate and threshold stress intensity factor range (ΔKth of metallic materials using circumferentially cracked round bar (CCRBspecimen geometry. The literature survey indicates that the fatigue crack growth rate data generated using ASTM E-647 standard test specimens were strongly dependent on specimen size and its configuration. Also the standard test procedure is more cumbersome and time consuming requires costly instrumentation. Aluminum 2014T6 alloy is used as the test specimen because of its wide applicationin automobiles and aero plane industry. It is found that the test procedure is simple, reliable, less time consuming and uses simple instrumentation. The obtained fatigue crack growth rate is found to be very close to the values obtained by using standard specimens. This methodology can be widely applied in industries for rapid determination of ΔKth any metallic materials.

  4. Influence of high pressure hydrogen on cyclic load crack growth in metals

    Science.gov (United States)

    Jewett, R. P.; Walter, R. J.; Chandler, W. T.

    1978-01-01

    The effect of high pressure hydrogen on the crack growth rate of various nickel-base alloys was studied at ambient temperature. Considerable enhancement of the cyclic flaw growth rate was observed for Inconel 718, wrought and cast, and Waspaloy, a nickel-base alloy similar to Inconel 718. Only slight enhancement of the flaw growth rate for Alloy 903 was observed.

  5. Intrinsic fatigue crack growth rates for Al-Li-Cu-Mg alloys in vacuum

    Science.gov (United States)

    Slavik, D. C.; Blankenship, C. P., Jr.; Starke, E. A., Jr.; Gangloff, R. P.

    1993-01-01

    The influences of microstructure and deformation mode on inert environment intrinsic fatigue crack propagation were investigated for Al-Li-Cu-Mg alloys AA2090, AA8090, and X2095 compared to AA2024. The amount of coherent shearable delta-prime (Al3Li) precipitates and extent of localized planar slip deformation were reduced by composition (increased Cu/Li in X2095) and heat treatment (double aging of AA8090). Intrinsic growth rates, obtained at high constant K(max) to minimize crack closure and in vacuum to eliminate any environmental effect, were alloy dependent; da/dN varied up to tenfold based on applied Delta-K or Delta-K/E. When compared based on a crack tip cyclic strain or opening displacement parameter, growth rates were equivalent for all alloys except X2095-T8, which exhibited unique fatigue crack growth resistance. Tortuous fatigue crack profiles and large fracture surface facets were observed for each Al-Li alloy independent of the precipitates present, particularly delta-prime, and the localized slip deformation structure. Reduced fatigue crack propagation rates for X2095 in vacuum are not explained by either residual crack closure or slip reversibility arguments; the origin of apparent slip band facets in a homogeneous slip alloy is unclear.

  6. Evaluation of Stress Corrosion Cracking Susceptibility Using Fracture Mechanics Techniques, Part 1. [environmental tests of aluminum alloys, stainless steels, and titanium alloys

    Science.gov (United States)

    Sprowls, D. O.; Shumaker, M. B.; Walsh, J. D.; Coursen, J. W.

    1973-01-01

    Stress corrosion cracking (SSC) tests were performed on 13 aluminum alloys, 13 precipitation hardening stainless steels, and two titanium 6Al-4V alloy forgings to compare fracture mechanics techniques with the conventional smooth specimen procedures. Commercially fabricated plate and rolled or forged bars 2 to 2.5-in. thick were tested. Exposures were conducted outdoors in a seacoast atmosphere and in an inland industrial atmosphere to relate the accelerated tests with service type environments. With the fracture mechanics technique tests were made chiefly on bolt loaded fatigue precracked compact tension specimens of the type used for plane-strain fracture toughness tests. Additional tests of the aluminum alloy were performed on ring loaded compact tension specimens and on bolt loaded double cantilever beams. For the smooth specimen procedure 0.125-in. dia. tensile specimens were loaded axially in constant deformation type frames. For both aluminum and steel alloys comparative SCC growth rates obtained from tests of precracked specimens provide an additional useful characterization of the SCC behavior of an alloy.

  7. Critical issues in De-alloying and transcrystalline stress-corrosion cracking

    Energy Technology Data Exchange (ETDEWEB)

    Sieradzki, K.; Wagner, J.W.

    1992-03-01

    This report describes our progress since the last reporting reporting period (March 1991) and details the third year research plans on the program. The three major components of the program relate to (1) kinetic aspects of the selective dissolution in alloys and the coarsening of de-alloyed layers, (2) measurements of crack dynamics during film induced cleavage processes, and (3) mechanical properties of the intrinsic de-alloyed layers responsible for film-induced cleavage events. We discuss progress in each of these areas below.

  8. Estimation of elastic modulus of reinforcement corrosion products using inverse analysis of digital image correlation measurements for input in corrosion-induced cracking model

    DEFF Research Database (Denmark)

    Pease, Bradley Justin; Michel, Alexander; Thybo, Anna Emilie A.;

    2012-01-01

    A combined experimental and numerical approach for estimating the elastic modulus of reinforcement corrosion products is presented. Deformations between steel and mortar were measured using digital image correlation during accelerated corrosion testing at 100 μA/cm2 (~1.16 mm/year). Measured...... deformations were compared to a numerical corrosion model that considers electrochemical, transport, and mechanical processes, including penetration of corrosion products into a ‘corrosion-accommodating region,’ provided by the mortar’s capillary porosity, directly surrounding the steel. Comparing model...... and experimental results provides an order-of-magnitude approximation of corrosion product stiffness of 2.0 GPa....

  9. Short fatigue cracks nucleation and growth in lean duplex stainless steel LDX 2101

    Energy Technology Data Exchange (ETDEWEB)

    Strubbia, R., E-mail: strubbia@ifir-conicet.gov.ar [Instituto de Física Rosario – CONICET, Universidad Nacional de Rosario (Argentina); Hereñú, S.; Alvarez-Armas, I. [Instituto de Física Rosario – CONICET, Universidad Nacional de Rosario (Argentina); Krupp, U. [Faculty of Engineering and Computer Science, University of Applied Sciences Osnabrück (Germany)

    2014-10-06

    This work is focused on the fatigue damage of lean duplex stainless steels (LDSSs) LDX 2101. Special interest is placed on analyzing short fatigue crack behavior. In this sense, short crack initiation and growth during low cycle fatigue (LCF) and short crack nucleation during high cycle fatigue (HCF) of this LDSS have been studied. The active slip systems and their associated Schmid factors (SF) are determined using electron backscattered diffraction (EBSD). Additionally, the dislocation structure developed during cycling is observed by transmission electron microscopy (TEM). Regardless of the fatigue regime, LCF and HCF, short cracks nucleate along intrusion/extrusions in ferritic grains. Moreover, during the LCF phase boundaries decelerate short crack propagation. These results are rationalized by the hardness of the constitutive phases and the dependence of screw dislocation mobility in the ferrite phase on strain rate and stress amplitude.

  10. Crack growth through the thickness of thin-sheet Hydrided Zircaloy-4

    Science.gov (United States)

    Raynaud, Patrick A. C.

    In recent years, the limits on fuel burnup have been increased to allow an increase in the amount of energy produced by a nuclear fuel assembly thus reducing waste volume and allowing greater capacity factors. As a result, it is paramount to ensure safety after longer reactor exposure times in the case of design-basis accidents, such as reactivity-initiated accidents (RIA). Previously proposed failure criteria do not directly address the particular cladding failure mechanism during a RIA, in which crack initiation in brittle outer-layers is immediately followed by crack growth through the thickness of the thin-wall tubing. In such a case, the fracture toughness of hydrided thin-wall cladding material must be known for the conditions of through-thickness crack growth in order to predict the failure of high-burnup cladding. The fracture toughness of hydrided Zircaloy-4 in the form of thin-sheet has been examined for the condition of through-thickness crack growth as a function of hydride content and distribution at 25°C, 300°C, and 375°C. To achieve this goal, an experimental procedure was developed in which a linear hydride blister formed across the width of a four-point bend specimen was used to inject a sharp crack that was subsequently extended by fatigue pre-cracking. The electrical potential drop method was used to monitor the crack length during fracture toughness testing, thus allowing for correlation of the load-displacement record with the crack length. Elastic-plastic fracture mechanics were used to interpret the experimental test results in terms of fracture toughness, and J-R crack growth resistance curves were generated. Finite element modeling was performed to adapt the classic theories of fracture mechanics applicable to thick-plate specimens to the case of through-thickness crack growth in thin-sheet materials, and to account for non-uniform crack fronts. Finally, the hydride microstructure was characterized in the vicinity of the crack tip by

  11. Fatigue Crack Growth Behavior of Nickel-base Superalloy Haynes 282 at 550-750 °C

    Science.gov (United States)

    Rozman, K. A.; Kruzic, J. J.; Hawk, J. A.

    2015-08-01

    The fatigue crack growth rates for nickel-based superalloy Haynes 282 were measured at temperatures of 550, 650, and 750 °C using compact tension specimens with a load ratio of 0.1 and cyclic loading frequencies of 25 Hz and 0.25 Hz. Increasing the temperature from 550 to 750 °C caused the fatigue crack growth rates to increase from ~20 to 60% depending upon the applied stress intensity level. The effect of reducing the applied loading frequency increased the fatigue crack growth rates from ~20 to 70%, also depending upon the applied stress intensity range. The crack path was observed to be transgranular for the temperatures and frequencies used during fatigue crack growth rate testing. At 750 °C, there were some indications of limited intergranular cracking excursions at both loading frequencies; however, the extent of intergranular crack growth was limited and the cause is not understood at this time.

  12. Environmental Degradation of Materials: Surface Chemistry Related to Stress Corrosion Cracking

    Science.gov (United States)

    Schwarz, J. A.

    1985-01-01

    Parallel experiments have been performed in order to develop a comprehensive model for stress cracking (SCC) in structural materials. The central objective is to determine the relationship between the activity and selectivity of the microstructure of structural materials to their dissolution kinetics and experimentally measured SCC kinetics. Zinc was chosen as a prototype metal system. The SCC behavior of two oriented single-crystal disks of zinc in a chromic oxide/sodium sulfate solution (Palmerton solution) were determined. It was found that: (1) the dissolution rate is strongly (hkil)-dependent and proportional to the exposure time in the aggressive environment; and (2) a specific slip system is selectively active to dissolution under applied stress and this slip line controls crack initiation and propagation. As a precursor to potential microgrvity experiments, electrophoretic mobility measurements of zinc particles were obtained in solutions of sodium sulfate (0.0033 M) with concentrations of dissolved oxygen from 2 to 8 ppm. The equilibrium distribution of exposed oriented planes as well as their correlation will determine the particle mobility.

  13. Environmental Degradation of Materials: Surface Chemistry Related to Stress Corrosion Cracking

    Science.gov (United States)

    Schwarz, J. A.

    1985-01-01

    Parallel experiments have been performed in order to develop a comprehensive model for stress cracking (SCC) in structural materials. The central objective is to determine the relationship between the activity and selectivity of the microstructure of structural materials to their dissolution kinetics and experimentally measured SCC kinetics. Zinc was chosen as a prototype metal system. The SCC behavior of two oriented single-crystal disks of zinc in a chromic oxide/sodium sulfate solution (Palmerton solution) were determined. It was found that: (1) the dissolution rate is strongly (hkil)-dependent and proportional to the exposure time in the aggressive environment; and (2) a specific slip system is selectively active to dissolution under applied stress and this slip line controls crack initiation and propagation. As a precursor to potential microgrvity experiments, electrophoretic mobility measurements of zinc particles were obtained in solutions of sodium sulfate (0.0033 M) with concentrations of dissolved oxygen from 2 to 8 ppm. The equilibrium distribution of exposed oriented planes as well as their correlation will determine the particle mobility.

  14. Growth model for large branched three-dimensional hydraulic crack system in gas or oil shale.

    Science.gov (United States)

    Chau, Viet T; Bažant, Zdeněk P; Su, Yewang

    2016-10-13

    Recent analysis of gas outflow histories at wellheads shows that the hydraulic crack