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Sample records for characterization degradacao termica

  1. Thermodegradation of biodiesel: thermoanalytical and rheological characterization; Degradacao termica de biodiesel: caracterizacao termoanalitica e reologica

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    Silva, Everson L.; Carvalho, Laura H.; Araujo, Gilmar T.; Gadelha, Tatiana S. [Universidade Federal de Campina Grande (UFCG), PB (Brazil)

    2008-07-01

    Brazil is a country of extensive agricultural land and great oil consumption and these factors favor biodiesel production in this country. In order for diesel/biodiesel mixtures to be effectively employed in diesel engines, a rigid quality control of these mixtures is needed. Biodiesel and mixtures must have their quality monitored with respect to oxidative resistance, thermal stability, fluidity and volatility, properties which can be modified by the adverse transport and stock conditions prior to consumption. Oxidation is the main degradation mechanism of products under transport and stock conditions, which can lead to significant economical losses. In this work sought the thermal degradation of neat biodiesel, synthesized in our laboratories was monitored. Thermal aging was conducted at 210 deg C for up to 1000 h. Virgin and thermally degraded samples were characterized by rheological measurements (in different shear conditions); FTIR; density and by color changes. We concluded that the soy biodiesel was successfully synthesized and that thermal exposure caused thermal-oxidative degradation of the biodiesel sample, significantly changing its properties as a function of thermal exposure times. (author)

  2. Thermal degradation of a synthetic lube oil API SL/CF SAE 5W 40; Degradacao termica do oleo lubrificante sintetico API SL/CF SAE 5W 40

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    Lopes, Eddy H. de O.; Carvalho, Laura H. de; Silva, Everson de L. [Universidade Federal de Campina Grande (UFCG), PB (Brazil)

    2008-07-01

    This work deals with the thermal degradation to 210 deg C of lubricating oil synthetic API SL/CF SAE 5W 40 as received and on the presence of metallic particles, from engine parts (head and crankshaft). Samples were collected at various intervals of time. The metallic particles were spent in mesh sieve no. 200 (0.074 mm) and used both in the trials of characterization (EDX and SEM) as the thermal degradation of the oil. Changes in rheology, viscosity, density, color and FTIR were monitored over time of heat exposure. The results indicate that thermal exposure caused by thermal oxidation of synthetic oil and that the presence of metallic particles (10 ppm) accelerated this process, so it is suggested that during the exchange of oil are taken care to remove them from to prevent the premature deterioration of the new oil. The behaviour Newtonian was maintained throughout the period degradation and viscosity of the oil has not changed significantly even after long periods (1148 hours) of thermal exposure. Despite the density of oil also has not changed significantly with time of exposure, changes in color indicate that chemical changes occurred, which was detected by FTIR. (author)

  3. Characterization of a clay from Vitoria da Conquista, Bahia, Brazil, by thermal analysis; Caracterizacao de uma argila de Vitoria da Conquista, BA, por analise termica

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    Oliveira, O.M.; Zandonadi, A.R.; Martins, M.V. Surmani; Carrio, J.A.G.; Munhoz Junior, A.H. [Universidade Presbiteriana Mackenzie, Sao Paulo, SP (Brazil)

    2010-07-01

    Kaolinitic clays are vastly used in ceramic industry. Light coloration burned clays are very useful in the coatings production because of their aesthetic. In this work clay material from Vitoria da Conquista (south-west Bahia, Brazil) was characterized by various techniques. Differential Scanning Calorimetry (DSC) shows a kaolinite characteristic curve with an endothermic peak at 492 deg C, which corresponds to the kaolinite - metakaolinite transformation. Transformation alpha to beta quartz is characterized by a 573 deg C peak. The samples were also characterized by water absorption and x rays powder diffraction. The 1100 deg C burned samples were tested by rupture tension with acceptable results. (author)

  4. Thermal responses and its relation with the building outdoor conditions; Respuestas termicas y su relacion con la envolvente del edificio

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    Marincic, Irene [Universidad de Sonora, Hermosillo, Sonora (Mexico); Isalgue, Antoni [Universidad Politecnica de Cataluna, Barcelona (Spain)

    2000-07-01

    In order to understand and to control the indoor thermal behavior in buildings, it is necessary to know the origin of the energies coming into and outside the building, identifying the geometric factors and physical properties, that can modify the thermal balance of the system. In this work, we analyze the thermal behavior of a building experimentally, related with its exterior conditions. Specifically, we analyze the thermal response indoors at different distances from the building envelope, which implies different thermal insulation situations. Supported on temperature measurements in a residential building, which is representative of local construction styles (adjacent other buildings), we analyze the thermal response effects depending on the distances between the considered points and the envelope and on the insulation between both. Applying a methodology based on experimental transfer functions of buildings, the thermal behavior in the temporary and frequency domains is evaluated. With this methodology, it is possible to visualize certain phenomena and to obtain thermal parameters that characterize the dynamic aspects of the thermal response. The main scope is to extract information from the building analysis, in order to extrapolate the behavior conclusions to a proper thermal design of similar constructions. From the thermal responses analysis at different spatial localization, we conclude that the distance from the building envelope (and also its properties) has a great influence on thermal inertia effects, which can modify importantly the thermal response. This phenomena has a parallelism with the skin effect of the magnetic fields penetration in conductors. The spatial localization implies a certain thermal mass involved in each case, which controls the penetration of exterior thermal oscillation. [Spanish] Para poder entender y controlar los comportamientos termicos en el interior de los edificios, es necesario conocer el origen de las energias que

  5. Clay Characterization as Engineered Barrier to Contaminants Migration: Thermal, Hydraulic and Mechanical Properties; Caracterizacion de la Arcilla como Barrera de Ingenieria para la Migracion de Contaminantes: Propiedades Termicas, Hidraulicas y Mecanicas

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    Bru, A.; Casero, D. [CIEMAT: Madrid (Spain)

    2001-07-01

    In this work we characterize the structure of a clay, concretely bentonite. Our main aim is to stress the important role that plays the heterogeneity of the medium structure in transport processes. Randomness of pore sizes produces an anomalous transport of contaminants. We analyze mercuric porosimetry data with simulations finding that pore size distribution has a power-law behaviour. (Author) 6 refs.

  6. Application of the electrical characterization to the study of the hydrated phases of the cement with coal bottom ash; Aplicacion de la caracterizacion electrica al estudio de las fases hidratadas de cemento con adicion de escorias de centrales termicas

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    Menendez, E.; Frutos, J. de; Alvaro, A. M.

    2014-02-01

    The present paper investigates the influence of using Bottom and Fly Ash as partial replacement of cement in the hydration process. Through measurements of electrical impedance spectroscopy (EIS) and X -ray diffraction (XRD), we analyze from the early stages to the hydration process to the end. Values of EIS, XRD and its relation, are used to determine transformation of hydrated phases, and for each of the substitutions, is indicated as modified the hydrated phase as a function of time and compared it with the reference material. It also proves the relevance of using EIS measures in real time, and as non destructive testing to characterize the hydration process of these materials. (Author)

  7. Thermal activation and characterization of clay aiming their use as sorbent in fixed bed columns to remove cadmium; Ativacao termica e caracterizacao da argila visando sua utilizacao como adsorvente em colunas de leito fixo para a remocao de cadmio

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    Silva, M.M. da; Rodrigues, M.G.F. [Universidade Federal de Campina Grande (UFCG), PB (Brazil); Silva, M.L.P. [Universidade Federal Rural do Semi-Arido (UFERSA), RN (Brazil); Kleinübing, S.J.; Silva, M.G.C., E-mail: marciliomaximo@yahoo.com.br [Universidade Estadual de Campinas (UNICAMP), SP (Brazil)

    2011-07-01

    In this work we studied the removal of cadmium in a synthetic wastewater using clay of Pernambuco - Brazil, in systems of fixed bed column. Clay was thermally activated at 500 °C. The materials were characterized using X-ray Fluorescence (XRF), X-ray Diffraction (XRD) and nitrogen adsorption (BET method). For tests in fixed bed column, we applied a factorial design 2{sup 2} and found that increasing the flow adversely affects the process of removing cadmium concentration while acting positively. The studies showed these materials as promising for the removal of Cd{sup 2+} ions in synthetic wastewater containing low levels of this metal. (author)

  8. Characterization of new bioactive coatings of hydroxyapatite and TiO{sub 2} obtained by High-Velocity Oxy-Fuel; Caracterizacion de nuevos recubrimientos biocompatibles de hidroxiapatita-TiO{sub 2} obtenidos mediante Proyeccion Termica de Alta Velocidad

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    Melero, H.; Fernandez, J.; Dosta, S.; Guilemany, J. M.

    2011-07-01

    Hydroxyapatite (Hap: Ca{sub 1}0(PO{sub 4}){sub 6}OH{sub 2}) is a biocompatible and bioactive ceramic material widely used as a coating on metal surfaces (dental implants, hip replacements ...), but the low adhesion between Hap and the substrate, due to differences in thermal expansion coefficients of both (very important in thermal spraying because of the fast cooling of the coating, which can produce a lost of adherence), and the degradation of Hap, have been tried to be improved through the incorporation of TiO{sub 2} to get a good combination of mechanical properties. Therefore, the objective of this project is to produce coatings of Hap 80% TiO{sub 2} and 20% (by weight) on Ti6Al4V by High-Speed Thermal Spray (HVOF). The study of the microstructure has been carried out using scanning electron microscopy and characterization of the crystalline phases by X-ray diffraction and Raman spectrometry. The coatings adhesion has been measured by tensile tests according to ASTM C633-01 (2008), and their bioactivity also has been evaluated through its immersion in simulated body fluid (SBF), in order to measure their capacity to form an apatite layer on their surface. (Author) 26 refs.

  9. Characterization of the neutron flux in the Hohlraum of the thermal column of the TRIGA Mark III reactor of the ININ; Caracterizacion del flujo neutronico en el Hohlraum de la columna termica del reactor TRIGA Mark III del ININ

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    Delfin L, A.; Palacios, J.C.; Alonso, G. [ININ, 52045 Ocoyoacac, Estado de Mexico (Mexico)]. e-mail: adl@nuclear.inin.mx

    2006-07-01

    Knowing the magnitude of the neutron flux in the reactor irradiation facilities, is so much importance for the operation of the same one, like for the investigation developing. Particularly, knowing with certain precision the spectrum and the neutron flux in the different positions of irradiation of a reactor, it is essential for the evaluation of the results obtained for a certain irradiation experiment. The TRIGA Mark III reactor account with irradiation facilities designed to carry out experimentation, where the reactor is used like an intense neutron source and gamma radiation, what allows to make irradiations of samples or equipment in radiation fields with components and diverse levels in the different facilities, one of these irradiation facilities is the Thermal Column where the Hohlraum is. In this work it was carried out a characterization of the neutron flux inside the 'Hohlraum' of the irradiation facility Thermal Column of the TRIGA Mark III reactor of the Nuclear Center of Mexico to 1 MW of power. It was determined the sub cadmic neutron flux and the epi cadmic by means of the neutron activation technique of thin sheets of gold. The maps of the distribution of the neutron flux for both energy groups in three different positions inside the 'Hohlraum' are presented, these maps were obtained by means of the irradiation of undressed thin activation sheets of gold and covered with cadmium in arrangements of 10 x 12, located parallel to 11.5 cm, 40.5 cm and 70.5 cm to the internal wall of graphite of the installation in inverse address to the position of the reactor core. Starting from the obtained values of neutron flux it was found that, for the same position of the surface of irradiation of the experimental arrangement, the relative differences among the values of neutron flux can be of 80%, and that the differences among different positions of the irradiation surfaces can vary until in a one order of magnitude. (Author)

  10. Determination of the thermal conductivity of metallic coatings; Determinacion de la conductividad termica de recubrimientos metalicos

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    Uc Way, Manuel Eugenio

    1998-02-01

    Due to the corrosion by high temperature there is a serious problem of unavailability and efficiency of the steam generators in the thermoelectric power stations. One of the parts that is more affected by this phenomenon is the superheater tube banks. In order to diminish this problem it is intended to apply to these tubes a metallic coating nickel and chromium based (80Ni20Cr), the deposition of the coating is made by the method of thermal spraying of powders by flame. The coating thickness once it has been deposited is of the order of 500mm, it is doubtless that the thermal flow between gases of combustion and the fluid conducted in the tubes is affected. That is why it is important to know the thermal conductivity of the coating in order to evaluate the impact that it has in the operation of the steam generator. This necessity is the one that gives rise to the present thesis project, in which a technique that allows to measure the thermal conductivity of the coating is designed. The experimentation is carried out taking as departure point the ASTM norm E1225-87 and is adapted to the characteristics of the material to prove. A test piece of stainless steel 316 was designed to measure the thermal flow that traverses the coating. First the experimental installation was characterized in order to determine its reliability. Later the experimentation was made finding an average thermal conductivity of 2.09{+-}0.72 W/m K in the temperature interval of 110-180 Celsius degrees. This value is 12.3% inferior to the corresponding one of a solid metal of the same composition. If we consider that in the high temperature banks of the steam generators the thermal flow is in the interval from 15.000 to 100.000 W/m{sup 2} and a coating thickness of the order of 500mm it would cause that this material would introduce a temperature difference of 0.6 to 4 Celsius degrees, respectively. Please note that for the highest thermal flow a maximum affectation of 4 Celsuis degrees is

  11. Techniques of thermal energy conservation; Tecnicas de conservacion de la energia termica

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    Caltenco Estevez, Juan Luis; Roblez Lopez, Francisco; Ceballos Serna, Andres Alberto [Instituto Mexicano del Petroleo (Mexico)

    1996-07-01

    In modern industry the thermal energy is the energy more intensely used, which implies that in the processes and equipment that operate based on it, rely the greatest opportunities for saving . In this paper some saving and conservation techniques of thermal energy, which nowadays have been developed, are presented, whose application has helped to the successful attainment of the objectives of increased productivity of industrial plants, with the additional benefit of reducing the environmental impact of the production activities. [Spanish] En la industria moderna la energia termica es la forma de energia mas intensamente utilizada, lo cual implica que en los procesos y equipos que operan basandose en esta, residan las mayores oportunidades de ahorro. En este trabajo se presentan algunas de las tecnicas de ahorro y conservacion de energia termica, que hoy en dia se han desarrollado, cuya aplicacion ha coadyuvado a la consecucion exitosa de los objetivos de incremento de la productividad de plantas industriales, con el beneficio adicional de reducir el impacto ambiental de las actividades productivas.

  12. Application techniques of coatings by thermal projection; Tecnicas de aplicacion de recubrimientos por proyeccion termica

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    Porcayo Calderon, Jesus [Instituto de Investigaciones Electricas, Cuernavaca (Mexico)

    1995-12-31

    The coatings applied by thermal projection have an important number of applications in different industries (chemical, oil, electric, nuclear, etc.). The main purpose of the protection by means of coatings is to alter the surface characteristics of a component so as to resist corrosive environments, abrasion and erosion, among others. The coatings can be applied by different methods, but due to the fact that its characteristics appreciably differ from the base metal, it is important the knowledge of its properties when a coating is selected for a specific use. In this article the characteristics of the applied coatings by thermal projection, the factors that affect its performance and the principal application techniques, are described. [Espanol] Los recubrimientos aplicados por proyeccion termica tienen un numero importante de aplicaciones en diferentes industrias (quimica, petrolera, electrica, nuclear, etc.). El proposito principal de la proteccion por medio de recubrimientos es alterar las caracteristicas de la superficie de un componente de manera que resista ambientes corrosivos, abrasion y erosion, entre otros. Los recubrimientos pueden aplicarse por diferentes metodos, pero debido a que sus propiedades difieren apreciablemente de las del metal base, es importante el conocimiento de sus propiedades cuando se selecciona un recubrimiento para un uso especifico. En este articulo se describen las caracteristicas de los recubrimientos aplicados por proyeccion termica, los factores que afectan su desempeno y las principales tecnicas de aplicacion.

  13. Measurement of the thermal conductivity from construction materials; Medicion de conductividad termica de materiales de construccion

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    Lira Cortes, Leonel; Xaman Villasenor, Jesus P; Chavez Chena, Yvonne [CENIDET: Centro Nacional de Investigacion y Desarrollo Tecnologico, Cuernavaca, Morelos (Mexico)

    2000-07-01

    In order to improve the calculation of thermal loads that allows to model the thermal behavior of constructions with aims of energy saving, it is necessary to count on the thermophysical properties of the materials used in the construction industry. Nevertheless at present in Mexico do not exist reported data of the materials that are made and used in our country, reason why it is chosen to take the results reported in the literature, whose values in their majority do not correspond to Mexican materials. In order to cover this necessity, at the CENIDET an instrument was developed to determine the thermal conductivity of insulating and construction materials. To date they have come with studies of different materials, which are provided by the manufacturers, with the intention of obtaining real data of thermal conductivity and to apply them with whole confidence in simulations of calculations of thermal loads. In this paper the results of measurement of the apparent thermal conductivity of two different materials from construction are presented, pumice stone block and block of tezontle (a porous volcanic rock).The measurement was made with an absolute and primary instrument according to norm ANSI/ASTM C-177-97. The operation principle of the apparatus is based on the technique of heat transference by conduction in permanent state between two plates, the experiment is carried out using an apparatus of hot plate with guard (APCG). Given the geographic zone where the studied materials are to be used, it is concluded that the obtained results show better properties for both with respect to reported values of similar materials, by virtue that these materials are intended to be applied in a humid climate as it is in the state of Puebla, Mexico. [Spanish] Para mejorar el calculo de cargas termicas que permita modelar el comportamiento termico de edificaciones con fines de ahorro de energia, es necesario contar con las propiedades termofisicas de los materiales utilizados

  14. Clays as green catalysts in the cholesterol esterification: spectroscopic characterization and polymorphs identification by thermal analysis methods. An interdisciplinary laboratorial proposal for the undergraduate level; Argilas como catalisadores verdes na esterificacao do colesterol: caracterizacao espectroscopica e identificacao de polimorfos por metodos de analise termica. Uma proposta laboratorial interdisciplinar para o primeiro ciclo universitario

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    Maria, Teresa M R.; Nunes, Rui M. D.; Pereira, Mariette M.; Eusebio, M. Ermelinda S. [Universidade de Coimbra, Coimbra (Portugal). Dept. de Quimica], e-mail: troseiro@ci.uc.pt

    2009-07-01

    A laboratory experiment that enables the professor to introduce the problematic of sustainable development in pharmaceutical chemistry to undergraduate students is proposed, using a simple synthetic procedure. Cholesteryl acetate is prepared by the esterification of cholesterol using Montmorillonite K10 as heterogeneous catalyst. Cholesterol and cholesteryl acetate are characterized by spectroscopic ({sup 1}H RMN, {sup 13}C RMN, FTIR) and thermal analysis techniques. The thermal methods are used to introduce the concepts of polymorphism and the nature of mesophases. (author)

  15. Thermal, mechanics and electrical characterization of the Al-0,6%Mg-08%Si alloy refined and modified with different copper contents; Caracterizacao termica, mecanica e eletrica da liga Al-0,6% Mg-0,8% Si refinada e modificada com diferentes teores de cobre

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    Freitas, E.S. [Universidade Federal do Para (UFPA), Belem, PA (Brazil)], Email: mmanufreitas@gmail.com; Marques, P.R.R.; Santos, W.L.R.; Kamizono, K.A.; Quaresma, J. Maria V.

    2009-07-01

    The aluminum, magnesium and silicon alloys form a very important group, utilized as casted form and worked alloys, especially in 6201 alloy series. These alloys show applicability on cables and wires fabrication to electrical energy transmission. The present work analyzes the copper content variation and its influence in electrical conductivity, tensile strength and in studied alloy ductility. The refined Al-0,6% Mg-0,8% Si studied alloy was modified with the following contents: [0,05; 0,10; 0,20 e 0,30]% Cu and unidirectional solidified. The test specimen were machined to 10 mm diameter and rolled to 3,98 mm, whose deformation rate was 60,2%. The obtained wires were mechanical, electrical and structural characterized and the mechanical and electrical characterization results were associated to fractures of evaluated micro cavities. The highest observation was the Cu content in alloy increases the TS, decreases electrical conductivity and increases liquidus isotherm's velocity, forming micro cavities. (author)

  16. Multi-wall carbon nanotubes/epoxy resin composites characterization of the starting materials and evaluation of thermal and electrical conductivity;Compositos resina epoxi/nanotubos de carbonos de paredes multiplas: caracterizacao dos materiais de partida e avaliacao das condutividades eletrica e termica

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    Silva, Wellington Marcos da

    2009-07-01

    In this study we investigate the electrical and thermal properties of I) composite materials fabricated with O, I, 0,5 and I wt% of concentric multi-wall carbon nanotubes/epoxy resin (MWNT) dispersed randomly in the resin; 2) MWNT buckypaper/resin composite materials; 3) and neat MWNT buckypaper. Initially, we use the techniques of thermogravimetry, infrared spectroscopy, nuclear magnetic resonance, energy dispersive spectroscopy, x-ray fluorescence, scanning and transmission electron microscopy for a broadening characterization of the starting materials, to evaluate its morphology, purity, chemical composition and structure, in order to optimize the properties of crosslinked resin and, consequently, of the composite systems. Important parameters such as the average molecular mass and the equivalent weight of epoxy resin (DGEBA) were determined by {sup 1}H-NMR analysis and, after that, resin/curing agent relations with Phr 10, 15, 20 and 53,2 were elaborated and investigated by thermogravimetry, the resin/curing agent relation with Phr 10 showed to be the most thermally stable. This stoichiometric relation was used to elaborate the composites. We have evaluated that the effect of adding 10 wt% of the solvent acetone to the epoxy resin preparation does not alter its properties so we have adopted two routes to fabricate the composites. In the first route we used 10 wt% of acetone and, in the second the MWNT were dispersed in the matrix without using the solvent. However, no significant difference was observed for the dispersion of the bundle tubes in both systems. The electrical conductivity of the composites and buckypapers was evaluated by impedance spectroscopy and the thermal conductivity by the flash laser flash method. Only the buckypapers presented high values for electrical conductivity (10{sup 3} S.m{sup -1}). The composite systems presented values of 10{sup -3} S.m{sup -1}, only a bit different from the value of the crosslinked resin. For thermal

  17. Thermal analysis of the integration of an ammonia plant; Analisis de la integracion termica de una planta de amoniaco

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    Arriola Medellin, Alejandro M.; Huante Perez, Liborio; Rodriguez Martinez, J. Hugo; Alcaraz Calderon, A. Moises [Instituto de Investigaciones Electricas, Cuernavaca, Morelos (Mexico)]. E-mail: aarriola@iie.org.mx; lhp@iie.org.mx; jhrm@iie.org.mx; malcaraz@iie.org.mx

    2010-11-15

    In this paper the thermal integration of an existing ammonia plant is evaluated using the Pinch Analysis tools. It is shown the design criteria that would have to fulfill the heat recovery network to take advantage of process streams thermal potentials. It was identified the heat recovery equipment that induces energy losses by incorrect streams selection, and the economic implications. [Spanish] En este trabajo se evalua la integracion termica de una planta existente de amoniaco usando las herramientas del analisis Pinch. Se muestran los criterios de diseno que deberian de cumplir las redes de recuperacion de calor, para aprovechar al maximo el potencial termico de las corrientes del proceso. Tomando como base dichos criterios se analizo el diseno la red de recuperacion de calor de la planta existente, identificando los equipos de recuperacion de calor que generan perdidas de calor por la seleccion incorrecta de las corrientes. Se estiman las perdidas economicas derivadas del diseno ineficiente de la red.

  18. Analysis of the thermal and optical properties of some construction materials; Analisis de las propiedades termicas y opticas de algunos materiales de construccion

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    Marroquin Hernandez, Karla F. [Universidad Nacional Autonoma de Mexico, Huauchinango, Puebla (Mexico)

    2000-07-01

    In this paper the optical and thermal properties of some materials of construction of greater application in a region of the state of Puebla, are obtained and presented, with the purpose of extending the bibliography and at the same time to analyze the importance that these properties have in the field of energy saving and to know the normative aspects in Mexico, as well as the control that is held of the construction materials. The properties that were analyzed are: Optical (Transmittance, reflectance, absorbency and emittance), Thermal (Thermal conductivity). [Spanish] En este trabajo se obtienen y se presentan las propiedades opticas y termicas de algunos materiales de construccion de mayor aplicacion en una region del estado de Puebla, con el fin de ampliar la bibliografia y al mismo tiempo de analizar la importancia que dichas propiedades tienen en el campo del ahorro energetico y de conocer los aspectos de la normativa en Mexico, asi como el control que se tiene de los materiales de construccion. Las propiedades que se analizaron son: Opticas (Transmitancia, reflectancia, absortancia y emitancia) Termica (Conductividad termica).

  19. Study on the radiological Impact of Coal Fired Power Plants; Estudio del impacto radiologico de las centrales termicas de carbon sobre sus entornos. Unidad de produccion termica de litoral

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    Cancio, D.; Robles, B.; Mora, J. C.; Baeza, A.; Corbacho, J. A.; Vasco, J.; Guillen, J.

    2008-07-01

    The study is part of the goal set forth in Title VII of the European Basic Safety Standards and the Spanish regulations on radiation protection related to work activities that may involve a significant increase in exposure of workers and the public to natural radiation. Coal contains small quantities of radionuclides in the series of uranium, thorium and potassium which in the industrial process can lead to radiological exposure. This work presents the measurements and evaluations conducted in one of the power plants object of study: The Unidad Termica de Produccion de Litoral in the Almeria Province. The maximum dose assessed for workers are in the order of 0.14 mSv per year and in the order of 0.05 mSv per year for the public in the realistic scenarios considered. These values are well below the 1mSv per year reference levels, recommended in Europe to have some interest from the radiation protection point of view. (Author) 52 refs.

  20. The technical-economic potential of thermal energy saving in hospitals; El potencial tecnico-economico de ahorro de energia termica en hospitales

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    Herrera, A. [Universidad Nacional Autonoma de Mexico (Mexico); Islas, J [Universidad Nacional Autonoma de Mexico, Mexico, D.F. (Mexico); Arriola, A. [Instituto de Investigaciones Electricas, Cuernavaca, Morelos (Mexico)

    2001-07-01

    The hospitals are important consumers of energy. At the General Hospital of Zone (HGZ) N of the IMSS in Aguscalientes (HGZ N . IMSS Ags.), the diesel oil is the main fuel that is used to satisfy the requirements of thermal energy of the hospital. According to the data collected by this author, this fuel represented in 2001, 75% of its total energy consumption and the 67.9% of its total costs in energy that ascended to $396.131 (December 2001 Dollars) Since this last amount represents an important percentage of the total expenses of the hospital (29.367 million dollars) it is important to determine the technical-economic possibilities of thermal energy saving of the hospital. The HGZ N 1 IMSS Ags. is located in a ampler conglomerate where the IMSS units are located, such as, the regional laundry, the sport unit, the center of social security, the familiar medicine unit N 1 and the hospital. Nevertheless departing from the installation of the electrical systems and the provision of steam and hot water to the hospital, the electrical and thermal fluids of all this facilities are distributed. Due to this situation, in this work we will refer to the global consumption of the IMSS of Aguascalientes development where the hospital is the main consumer of thermal energy. In the present work we will calculate the technical-economic potential of thermal energy saving in the development of the IMSS through the thermodynamic technique of folding point or pinch technique. [Spanish] Los hospitales son importantes consumidores de energia. En el Hospital General de Zona N del IMSS en Aguscalientes (HGZ N - IMSS Ags.), el diesel es el principal combustible que se usa para satisfacer los requerimientos de energia termica del hospital. Segun los datos obtenidos por el autor anterior, este combustible represento en 2001 el 75% de su consumo total energetico y el 67.9% de sus costos totales en energeticos que ascendieron a $396,131 (dolares de diciembre de 2001). Dado que esta ultima

  1. Study of degradation polypropylene/organo clay mixtures during reprocessing in extrusion; Estudo da degradacao de misturas de polipropileno/argila organofilica durante o reprocesso na extrusao

    Energy Technology Data Exchange (ETDEWEB)

    Silvano, Josiane da R., E-mail: josianesilvano@hotmail.com, E-mail: lapinheiro@uepg.br [Programa de Pos Graduacao em Engenharia e Ciencia de Materiais, Universidade Estadual de Ponta Grossa - UEPG, Ponta Grossa, PR (Brazil); Canevarolo, Sebastiao V. [Universidade Federal de Sao Carlos . UFSCAR, Sao Carlos, SP (Brazil); Carvalho, Benjamim de M.; Pinheiro, Luis A. [Universidade Estadual de Ponta Grossa - UEPG, Ponta Grossa, PR (Brazil)

    2011-07-01

    The objective of this work is to prepare polypropylene/ organo clay montmorillonite mixtures, with Cloisite 15A and Cloisite 30B at concentrations of 1 and 3% and using polypropylene-co-maleic anhydride as compatibilizer through the technique of molten state intercalation using twin-screw extruder and performing 5 reprocessing to assess the level of degradation. The materials were characterized by X-ray diffraction and infrared spectroscopy. The results of X-ray diffraction indicated that there is no formation of nanocomposites. Through FTIR observed an increased degradation in all samples compared to pure polypropylene, whereas for the samples with clay Cloisite 30B were those with the highest level of degradation. (author)

  2. Equipment to evaluate in experimental form the thermal conductivity of the construction materials; Equipo para evaluar en forma experimental el coeficiente de conductividad termica de los materiales de construccion

    Energy Technology Data Exchange (ETDEWEB)

    Lopez C, Raymundo; Morales G, Juan R.; Diaz C, Alen; Lizardi R, Arturo [Universidad Autonoma Metropolitana-Azcapotzalco, Mexico, D. F. (Mexico); Vaca M, Mabel [Universidad Nacional Autonoma de Mexico, Mexico, D.F. (Mexico)

    2001-04-01

    An equipment meant to obtain the thermal conductivity coefficient was designed, constructed and evaluated. Convection losses in the experimental device were reduced by means of a vacuum chamber that wraps it. Conduction losses were minimized with the proper insulation. The tested materials are the most frequently used in the construction of buildings in Mexico, such as concrete, burnt brick, adobe and gypsum. Results observed are comparable to those reported in the literature. The essays done using the vacuum chamber produced values of thermal conductivity coefficient 3% lower than those obtained without using it. [Spanish] Se diseno, construyo y evaluo un equipo, con el cual se obtiene el coeficiente de conductividad termica en diversos materiales. En este se reducen las perdidas por conveccion, colocando una camara de vacio alrededor del conjunto de prueba. Las perdidas por conduccion se minimizan con un aislamiento adecuado. Los materiales evaluados son los que mas se utilizan en la construccion en Mexico, a saber, el concreto, el ladrillo cocido, el adobe y el yeso. Los valores obtenidos, sin considerar las perdidas por conveccion, se comparan con los de la literatura. Los ensayos utilizando la camara de vacio proporcionan valores del coeficiente de conductividad termica menores en 3% a los obtenidos sin dicha camara.

  3. Development and implementation of a methodology to simultaneously determine the thermal properties of rocks; Desarrollo e implantacion de una metodologia experimental para determinar simultaneamente las propiedades termicas de las rocas

    Energy Technology Data Exchange (ETDEWEB)

    Contreras Lopez, Enrique; Garcia Gutierrez, Alfonso [Instituto de Investigaciones Electricas, Cuernavaca (Mexico)

    1996-12-31

    In the frame of the experimental infrastructure development of the Reservoirs Laboratory of the Geothermal Department of the Instituto de Investigaciones Electricas (IIE), a methodology that allows the simultaneous determination of the thermal conductivity, thermal diffusivity and specific heat in rock samples and other solid materials of low and medium conductivity, was implemented. The methodology is based in the theoretical solution of temperature distribution around an ideal linear heat source immersed in an infinite medium. The three properties are derived from one relatively simple experiment, that essentially consists in recording the temporary temperature variation in a given point of the specimen during a short heating period. This methodology has special application in the geothermal area, as well as in other areas related to the development and exploitation of underground energy and mineral resources. [Espanol] En el marco de las actividades de desarrollo de infraestructura experimental del Laboratorio de Yacimientos del Departamento de Geotermia del Instituto de Investigaciones Electricas (IIE), se implemento una metodologia que permite determinar simultaneamente la conductividad termica, la difusividad termica y el calor especifico en muestras de rocas y otros materiales solidos de conductividad baja e intermedia. La metodologia se basa en la solucion teorica de la distribucion de temperatura alrededor de una fuente lineal ideal de calor inmersa en un medio infinito. Las tres propiedades se derivan de un solo experimento relativamente simple, que consiste esencialmente en registrar la variacion temporal de la temperatura en un punto dado del especimen durante un corto periodo de calentamiento. Esta metodologia tiene especial aplicacion en el ambito de la geotermia, asi como en otras areas relacionadas con el desarrollo y aprovechamiento de los recursos energeticos y minerales del subsuelo.

  4. Comparison of the thermal gain of the more commonly roofing systems used in Mexico`s social dwellings; Comparacion de la ganancia termica de los sistemas de techumbre mas comunmente utilizados en la vivienda social en Mexico

    Energy Technology Data Exchange (ETDEWEB)

    Fernandez, Alfredo [Division de Estudios de Posgrado de la Facultad de Arquitectura UNAM, Mexico, D. F. (Mexico); Morillon, David [Comision Nacional para el Ahorro de Energia (CONAE), Mexico, D. F. (Mexico)

    1996-12-31

    Under the frame of discussion of the Mexican Official Standard 008 (Integral Energy Efficiency in non-residential Buildings), and with the purpose of assessing its feasibility and possible extension to residential buildings, this paper, whose objective is to evaluate the roofing systems (opaque) more commonly utilized on the social dwellings in Mexico, is presented. To perform this evaluation the heat gains by conduction through the roofing in different cities were obtained. Later on these heat gains were compared against the energy consumption that would produce its removal in each one of the cases. Finally, thermal resistance values (R) that allow, in significant form diminishing such gains, are presented, producing in consequence, a thermally efficient building. [Espanol] Dentro del marco de discusion de la Norma Oficial Mexicana 008 (Eficiencia energetica integral en edificios no residenciales), y con el fin de evaluar su factibilidad y posible extension hacia las edificaciones residenciales, se presenta este trabajo que tiene como objetivo la evaluacion de los sistemas de techumbre (opacos) mas comunmente utilizados dentro de la vivienda social en Mexico. Para realizar esta evaluacion se obtuvieron las ganancias por conduccion a traves del techo para distintas ciudades. Posteriormente, se compararon dichas ganancias contra el consumo de energia que produciria la remocion de las mismas en cada uno de los casos. Finalmente, se proponen valores de Resistencia Termica (R) que permitan disminuir de manera importante dichas ganancias teniendo, en consecuencia, una edificacion energeticamente eficiente.

  5. Thickness calculation software of the thermal insulation in facilities using thermal solar energy; Software para el calculo de espesores del aislante termico en instalaciones de aprovechamiento de energia solar termica

    Energy Technology Data Exchange (ETDEWEB)

    Portillo Jimenez, Canek [Universidad Autonoma de Sinaloa, Culiacan, Sinaloa (Mexico)]. E-mail: cnk@uas.uasnet.mx

    2010-11-15

    It is presented a software application for calculating the thickness of the thermal insulation used in various facilities where there are thermal systems using solar energy. The software facilitates the calculation of the thermal cover thickness over components such as pipes (flat or round), storage and other devices that require thermal protection, installed in outdoors or indoors. The software was programmed in Visual Basic by following the technical specifications of the current regulations in the field. Application examples are performed, obtaining certain results that are discussed briefly. [Spanish] Se presenta un software de aplicacion para el calculo de los espesores de los aislantes termicos, utilizados en diferentes instalaciones donde existen sistemas de aprovechamiento termico de energia solar. El software facilita el calculo del grosor del recubrimiento termico en componentes tales como: tuberias (planas o circulares), depositos acumuladores y otros aparatos que necesiten proteccion termica, instalados en exteriores o en interiores. El software fue programado en Visual Basic siguiendo las especificaciones tecnicas de la normatividad vigente en la materia. Se realizan ejemplos de aplicacion, donde se obtienen ciertos resultados de los cuales se hace una breve discusion.

  6. Evaluation of environmental degradation effects in morphology of ultra-high molecular weight polyethylene (UHMWPE) fibers; Avaliacao dos efeitos da degradacao ambiental na morfologia das fibras de polietileno de ultra-alto peso molecular (PEUAPM)

    Energy Technology Data Exchange (ETDEWEB)

    Vivas, Viviane; Zylberberg, Marcel P.; Cardoso, Andre Luis V.; Pereira, Iaci M., E-mail: iacipere@gmail.com [Centro Tecnologico do Exercito (CTEx), RJ (Brazil); Weber, Ricardo P.; Suarez, Joao C. Miguez [Instituto Militar der Engenharia (IME), Rio de Janeiro, RJ (Brazil)

    2015-07-01

    This study aims to evaluate changes in the morphology of ultra-high molecular weight polyethylene fiber (UHMWPE), before and after exposure to environmental agents. Fibers produced by two different manufacturers were analyzed. To characterize the morphology, we used the technique of small angle x-ray scattering (SAXS). The results demonstrate that the original morphology of the fibers was UHMWPE affected by the defects caused by exposure to environmental agents. (author)

  7. Assessment of PWR fuel degradation by post-irradiation examinations and modeling in DEGRAD-1 code; Avaliacao da degradacao de combustivel PWR por exames pos-irradiacao e modelagem no codigo DEGRAD-1

    Energy Technology Data Exchange (ETDEWEB)

    Castanheira, Myrthes; Lucki, Georgi; Silva, Jose Eduardo Rosa da; Terremoto, Luis A.A.; Silva, Antonio Teixeira e; Teodoro, Celso A.; Damy, Margaret de A. [Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil). Centro de Engenharia Nuclear]. E-mail: myrthes@ipen

    2005-07-01

    On the majority of the cases, the inquiries on primary failures and secondary in PWR fuel rods are based on results of analysis were made use of the non-destructive examination results (coolant activities monitoring, sipping tests, visual examination). The complementary analysis methodology proposed in this work includes a modeling approach to characterization of the physical effects of the individual chemistry mechanisms that constitute the incubation phase of degradation phenomenon after primary failure that are integrated in the reactor operational history under stationary operational regime, and normal power transients. The computational program called DEGRAD-1 was developed based on this modeling approach. The practical outcome of the program is to predict cladding regions susceptible to massive hydriding. The applications presented demonstrate the validity of proposed method and models by actual cases simulation, which (primary and secondary) defects positions were known and formation time was estimated. By using the modeling approach, a relationship between the hydrogen concentration in the gap and the inner cladding oxide thickness has been identified which, when satisfied, will induce massive hydriding. The novelty in this work is the integrated methodology, which supplements the traditional analysis methods (using data from non-destructive techniques) with mathematical models for the hydrogen evolution, oxidation and hydriding that include refined approaches and criteria for PWR fuel, and using the FRAPCON-3 fuel performance code as the basic tool. (author)

  8. Use of ZnO:Mn particles for degradation of methylene blue by photocatalysis process; Utilizacao de particulas de ZnO:Mn para a degradacao do azul de metileno por processo de fotocatalise

    Energy Technology Data Exchange (ETDEWEB)

    Giraldi, T. R.; Swerts, J. P.; Vicente, M. A., E-mail: tania.giraldi@unifal-mg.edu.br, E-mail: jefersonps21@hotmail.com, E-mail: maquelyaspr@oi.com.br [Universidade Federal de Alfenas (UNIFAL), Pocos de Caldas, MG (Brazil). Instituto de Ciencia e Tecnologia; Mendonca, V.R. de, E-mail: vrm@ifsp.edu.br [Instituto Federal de Educacao, Ciencia e Tecnologia de Sao Paulo (IFSP), Itapetininga, SP (Brazil); Paris, E.C.; Ribeiro, C., E-mail: elaine.paris@embrapa.br, E-mail: caue.ribeiro@embrapa.br [Embrapa Instrumentacao, Sao Carlos, SP (Brazil)

    2016-10-15

    The management of water use in the agricultural environment is a key factor to build new environmentally sustainable productive methods. Photocatalysis is a promising method for water decontamination. This research paper aimed to evaluate the photocatalytic potential of pure and Mn-doped ZnO particles. The materials were obtained by the polymeric precursor method, and characterized by X-ray diffraction, N{sub 2} adsorption in low temperature, infrared and ultraviolet spectroscopy, and photoluminescence. In order to evaluate ZnO:Mn particles photo efficiency, experiments were carried out by applying the methylene blue dye solution to photodegradation under UVC exposure. The particles had ZnO single-phase, but low specific surface area. The sample ZnO:0.25% Mn presented higher efficiency in the methylene blue photocatalytic degradation test. This efficiency was related to a higher band gap energy value and a lower rate of electron recombination, which allows greater formation of hydroxyl radicals, which are responsible for dye degradation. (author)

  9. Pcm inclusion in gypsum boards for thermal energy storage through latent heat: thermal characterization with DSC; Incorporacion de materiales de cambio de fase en placas de yeso para almacenamiento de energia termica mediante calor latente: caracterizacion termica del material mediante la tecnica DSC

    Energy Technology Data Exchange (ETDEWEB)

    Oliver, A.; Neila, F. J.; Garcia, A.

    2011-07-01

    Differential Scanning Calorimetry (DSC) is a thermal analysis technique which has been used for more than three decades to measure the temperatures and heat flows associated with transitions in materials as a function of time. Other techniques, are Differential Thermal Analysis DTA and Conventional Calorimetry. There is great uncertainty in the values supplied by the manufacturers (because they are referred to pure substances) and the DSC should be used to get more accurate values. It will be analyzed the thermal storage capacity depending on temperature for several compound materials formed by some aggregates, mainly gypsum and phase change materials, in various proportions. The results have been compared with other building materials such as gypsum boards and brick layer. The suitability of the new construction material for thermal energy storage will be assessed in comparison with other materials traditionally used for this purpose. (Author) 21 refs.

  10. Analysis of thermal stability of ceramic engobes developed with marble reject; Analise da estabilidade termica de engobes ceramicos desenvolvidos com rejeito de marmore

    Energy Technology Data Exchange (ETDEWEB)

    Carlos, E.M.; Assis, R.B.; Sousa, R.F.; Galvao, A.C.P.; Mendes, J.U.L., E-mail: elionemoura@hotmail.com [Universidade Federal do Rio Grande do Norte (UFRN), RN (Brazil)

    2014-07-01

    Considering the technological growth and technical production in the ceramic industry, ceramic mass formulations were evaluated with addition of marble residue to substitute the quartz for obtaining of engobes. Five formulations were prepared varying the proportions of raw material, sieved at 200 mesh, ball mill homogenised, characterized by fluorescence (FRX) and X-ray diffraction (XRD). Samples were separated from the formulations for thermal analysis (TG / DSC) and dilatometry. The specimens were prepared in uniaxial press (25 Mpa). The FIII and FIV formulations presented satisfactory results, evidencing the potential of replacing quartz by the marble residue in ceramic formulation for engobes, minimizing the environmental impact by the undue discard of waste, reducing costs and increasing the range of raw materials for the coatings industry.

  11. Thermal and mechanical properties of polyamide 6/compatibilizer/clay nano composites; Propriedades termicas e mecanicas de nanocompositos de poliamida 6/compatibilizante/argila

    Energy Technology Data Exchange (ETDEWEB)

    Agrawal, P.; Brito, G.F.; Cunha, C.T.C.; Araujo, E.M.; Melo, T.J.A., E-mail: tomas@dema.ufcg.edu.b [Universidade Federal de Campina Grande (UFCG), PB (Brazil). Dept. de Engenharia de Materiais

    2010-07-01

    In this work, the thermal and mechanical properties of Polyamide 6 (PA6)/compatibilizer/clay (CL20A) nanocomposites were investigated. The nanocomposites were prepared in a counter-rotating twin screw extruder at 240 deg C and 50 rpm, and characterized by X-Ray Diffraction (XRD), Thermogravimetry (TG) and mechanical properties. XRD results showed that when the clay is mixed with PA6, the clay peak is shifted to lower 2{theta} angles, indicating that PA6 was intercalated between the clay platelets. For PA6/compatibilizer/clay system, the results indicated that a nanocomposite with exfoliated structure was formed. TG results showed that the thermal stability of PA6/CL20A and PA6/compatibilizer/CL20A was higher than that of neat PA6. The mechanical properties results showed that the addition of the compatibilizer to PA6/CL20A substantially increased the impact strength and decreased the stiffness. (author)

  12. Thermal stability of formulations of PVC irradiated with {gamma} of {sup 60}; Estabilidad termica de formulaciones de PVC irradiadas con {gamma} de {sup 60} Co

    Energy Technology Data Exchange (ETDEWEB)

    Martinez P, M.E.; Carrasco A, H. [ININ, A.P. 18-1027, 11801 Mexico D.F. (Mexico)]. E-mail: memp@nuclear.inin.mx; Castaneda F, A.; Benavides C, R.; Garcia R, S.P. [CIQA, 25100 Saltillo, Coahuila (Mexico)

    2004-07-01

    The industry of cables and wires frequently use cable isolations with base of formulations of PVC, in those that stabilizer has usually been used with the help of heavy metals, as the lead, which is toxic. To solve the problem, from the 2002 one has come studying in combined form in the National Institute of Nuclear Research ININ and the Center of Investigation in Applied Chemistry CIQA, the modifications induced by the radiation in formulations with the help of vinyl poly chloride PVC. In these formulations, prepared with cross linking agent, plastifying industrial grade, stuff and non toxic stabilizers of calcium estearate and zinc industrial grade, it is sought to replace the stabilizer of Pb. For this were irradiated it test tubes of PVC with gamma radiation of cobalt 60 to three different dose in atmospheres of air and argon. Later it was determined their thermal stability at different times of heating and it was measured the Young modulus by means of thermo mechanical analysis. Those results obtained together with other techniques of characterization suggest that the irradiated proposed formulation can substitute the one stabilized with lead. (Author)

  13. Prototype of thermal degradation for radioactive wastes of low and intermediate level; Prototipo de degradacion termica para desechos radiactivos de nivel bajo e intermedio

    Energy Technology Data Exchange (ETDEWEB)

    Diaz A, L.V.; Pacheco S, J.O.; Pacheco P, M.; Monroy G, F.; Emeterio H, M. [ININ, 52045 Ocoyoacac, Estado de Mexico (Mexico)]. e-mail: lauradiazarch@yahoo.com.mx

    2005-07-01

    At the present time, the scientific, academic, industrial and technological activities, generate great quantity of radioactive wastes of low and intermediate level (DRNBI). For to assure an appropriate final disposal of these, it is intended their treatment and vitrification by means of thermal plasma. This alternative offers multiple advantages in an only process: elevated energy density (105W/cm{sup 3}), high enthalpy (1400 kJ/mol), elevated chemical reactivity, quick quenching (106K/s) and operation temperatures of 4000 to 15000K; this allows the treatment of a great diversity of waste. Those reactors are compact and they work to atmospheric pressure and reduced thermal inertia. This technology allows to degrade DRNBI and to contain them in a vitreous matrix by means of a system made up of a reactor, canyon of plasma, of monitoring, of washing of gases and of control. Besides the design and general characteristics of the Prototype of Thermal Degradation of DRNBI, they are reported in this work the advances achieved in the selection of the ceramic material for the vitrification. Their characterization was carried out by means of SEM and XRD. With the preliminary results it can discern that the material but appropriate to be used as vitreous matrix is a ceramic clay. With the development of the proposed technology and the material for the vitreous matrix, it will be to treat DRNBI. (Author)

  14. Thermal and mechanical properties of PLA and PBAT/PLA systems; Propriedades mecanicas e termicas de sistemas de PLA e PBAT/PLA

    Energy Technology Data Exchange (ETDEWEB)

    Silva, M.C.; Oliveira, S.V. de; Araujo, E.M., E-mail: milecost@hotmail.com [Universidade Federal de Campina Grande (UFCG), PB (Brazil). Unidade Academica de Engenharia de Materiais

    2014-07-01

    Searches with biodegradable materials have grown every day, because they present a lower environmental impact compared to conventional polymers. In this work, biodegradable polymer matrices such as polylactide (PLA) and a poly(adipate butyleneco- terephthalate)/polylactide (PBAT/PLA) blend commercially known as Ecovio ® were used. It was also used a smectite clay from the Paraiba. It was modified with Praepagen surfactant and named as organoclay (OMMT). PLA and PBAT/PLA systems were prepared with organoclay in concentration of 3 wt.%. Initially, masters were produced in a high shear mixer. Subsequently, they were dispersed in the polymer matrix in a do-rotational twin screw extruder. The PLA/OMMT and PBAT/PLA/OMMT biocomposites were characterized by X-ray diffraction (XRD), tensile and impact mechanical properties and Differential Scanning Calorimetry (DSC). According to XRD patterns of PLA/OMMT and PBAT/PLA/OMMT systems, it was observed a probable formation of a microcomposite for both systems. It was noticed that they showed reduction in tensile mechanical properties, however there was an increase in impact strength for PLA/OMMT system. The DSC curves practically no change in the crystallinity of the systems. (author)

  15. Analysis of the temperature field of an instrument's guard to measure the thermal conductivity of insulating solid materials; Analisis del campo de temperatura de la guarda de un instrumento para medir la conductividad termica de materiales solidos aislantes

    Energy Technology Data Exchange (ETDEWEB)

    Lira Cortes, Leonel; Xaman Villasenor, Jesus P; Chavez Chena Yvonne [CENIDET: Centro Nacional de Investigacion y Desarrollo Tecnologico, Cuernavaca, Morelos(Mexico)

    2000-07-01

    In this paper the analysis of the temperature field of the guard of an instrument called hot plate apparatus with guard (APCG), is presented. The experimental results are compared against the ones that are obtained when solving the problem in analytical form. In the analytical solution the influence of taking into account more than one own value is analyzed and the results when truncating in the first term of sum that corresponds to the first own value and to truncate in the second term that includes the first and second root are compared. The instrument is a parallel flat plate apparatus with guards of 305 mm of diameter and operates in an interval of 10 to 80 of temperature and can measure insulating samples with a maximum thickness of 75 mm with a class of exactness of 4%. In applications of calculation of thermal loads, it is necessary to know the thermal conductivity of insulating and construction materials, when the applications are oriented to the use of renewable energies such as the solar, with the purpose of making an efficient use of this energy. [Spanish] En este trabajo se presenta el analisis del campo de temperatura de la guarda de un instrumento denominado aparato de placa caliente con guarda (APCG). Se comparan los resultados experimentales contra los que se obtienen al resolver el problema en forma analitica. En la solucion analitica se analiza la influencia de tomar en cuenta mas de un valor propio y se comparan los resultados al truncar en el primer termino de la sumatoria que corresponde al primer valor propio y truncar en el segundo termino que incluye la primera y segunda raiz. El instrumento es un aparato de platos planos paralelos con guardas de 305 mm de diametro y opera en un intervalo de 10 a 800 grados Celsius de temperatura y puede medir muestras aislantes con un maximo de espesor de 75 mm con una clase de exactitud del 4%. En aplicaciones del calculo de cargas termicas, es necesario conocer la conductividad termica de materiales

  16. Uranium dioxide thermal characterization by the flash laser method from 23 Celsius to 175 Celsius; Caraterizacao termica de dioxido de uranio pelo metodo flash laser de 23 Celsius a 175 Celsius

    Energy Technology Data Exchange (ETDEWEB)

    Faeda, K.C.M.; Lameiras, F.S.; Carneiro, L.S.S.; Camarano, D.M.; Ferreira, R.A.N. [Centro de Desenvolvimento da Tecnologia Nuclear (CDTN/CNEN-MG), Belo Horizonte, MG (Brazil)

    2010-07-01

    The Laser Flash Method has become one of the most common techniques for measuring thermal diffusivity and conductivity in solids and liquids. This method is recognized by INMETRO as standard to be used in Brazil for measuring thermophysical properties of materials, such as metals, carbon composites, ceramics, and also nuclear materials. This article describes the experimental bench of the LMPT-Laboratorio de Medicao de Propriedades Termofisicas de Combustiveis Nucleares e Materiais of the CDTN-Centro de Desenvolvimento da Tecnologia Nuclear, (LMPT), as well as the mathematical model developed based on this method. The obtained results for the thermal diffusivity and for the thermal conductivity of uranium dioxide (U0{sub 2}) pellets in the temperature range from 25 deg to 175 deg C, are discussed and compared with the literature data. The estimative of the input quantities uncertainty of the mathematical model was determined according to ISO - BIPM-Guide to the Expression of Uncertainty in Measurement and the Monte Carlo Method was used to estimate of the output quantities uncertainty (thermal diffusivity and thermal conductivity). Additionally the results of the x-rays of these pellets are presented. (author)

  17. Solar Thermal Energy; Energia Solar Termica

    Energy Technology Data Exchange (ETDEWEB)

    Perez-Martinez, M.; Cuesta-Santianes, M. J.; Cabrera Jimenez, J. A.

    2008-07-01

    Approximately, 50 % of worldwide primary energy consumption is done in the form of heat in applications with a temperature lower than 250 degree centigree (low-medium temperature heat). These data clearly demonstrate the great potential of solar thermal energy to substitute conventional fossil fuels, which are becoming more expensive and are responsible for global warming. Low-medium temperature solar thermal energy is mainly used to obtain domestic hot water and provide space heating. Active solar thermal systems are those related to the use of solar thermal collectors. This study is dealing with low temperature solar thermal applications, mainly focusing on active solar thermal systems. This kind of systems has been extensively growing worldwide during the last years. At the end of 2006, the collector capacity in operation worldwide equalled 127.8 GWth. The technology is considered to be already developed and actions should be aimed at favouring a greater market penetration: diffusion, financial support, regulations establishment, etc. China and USA are the leading countries with a technology based on evacuated tube collectors and unglazed collectors, respectively. The rest of the world markets are dominated by the flat glazed collectors technology. (Author) 15 refs.

  18. Estimation of consumption of the useful life in the nozzles of a gas turbine by the phenomenon of thermal fatigue; Estimacion de consumo de vida util en las toberas de una turbina de gas por el fenomeno de fatiga termica

    Energy Technology Data Exchange (ETDEWEB)

    Perez Hernandez, Efrain [Centro Nacional de Investigacion y Desarrollo Tecnologico (Cenidet), Cuernavaca, Morelos (Mexico); Mazur C, Zdzislaw; Garcia Illescas, R. [Instituto de Investigaciones Electricas, Cuernavaca, Morelos (Mexico)

    2007-11-15

    damage. [Spanish] La estimacion de vida util en los componentes calientes de las turbinas de gas como toberas y alabes es importante ya que sufren de cambios criticos de temperatura los cuales producen fatiga termomecanica durante los arranques, paros y cambios de fatiga para estimacion de vida util en las toberas de turbina de gas fabricados de aleacion base cobalto FSX-414 en las cuales se han desarrollado grietas durante la operacion. La inspeccion visual y metalografia de la tobera revelo muchas grietas por fatiga termomecanica en la superficie del alabe ademas de deterioracion de la aleacion. En los limites de grano se encontro una pelicula continua de carburos y tambien aumento de fraccion de carburos dentro de los granos. Esta densa y continua red de carburos reduce la ductilidad y aumenta la fragilidad, junto con la reduccion de energia de impacto (Charpy), facilita la iniciacion y propagacion de grietas. La iniciacion y propagacion de grieta en la aleacion fue debido a un mecanismo de fatiga termica y termofluencia que fue facilitado por fragilidad del material debido al deterioro previamente mencionado y a significativos niveles de esfuerzos termomecanicos. En el presente articulo se presentan los resultados de analisis de esfuerzos termicos a partir de los resultados de temperatura obtenidas de estudios previos de un analisis de transferencia de calor y flujo de fluidos mediante el programa Star-CD basado en volumen finito. Se muestra la metodologia empleada y las distribuciones de esfuerzos, los cuales se emplearon para el analisis de fatiga para la estimacion de vida util. Para eso se utilizo un modelo de elementos finitos en el programa NISA, asi como el programa de analisis de fatiga nCode. Para el conteo de ciclo de utilizo el metodo de Rainflow y se compararon los modelos de vida por fatiga de Manson-Coffin, Basquin, Morrow y Smih-Watson-Topper. La variacion de las propiedades mecanicas con la temperatura de la superaleacion empleada en esos componentes

  19. Analysis of the consumption of useful life by thermal fatigue in the gas turbine nozzles during the operation at continuous load and transients; Analisis de consumo de vida por fatiga termica en las toberas de turbina de gas durante operacion con carga continua y transitorios

    Energy Technology Data Exchange (ETDEWEB)

    Perez Hernandez, Efrain Betuel

    2007-08-15

    The gas turbines operate at extremely high temperatures, with high thermal and mechanical stresses, causing that the life of the involved components diminishes. In the present thesis the temperature distribution on the nozzle obtained in other investigation as a result of heat transfer and fluid flow analysis applying CDF code Star-CD was used. Next, the program NISA was used to perform the analysis of thermal stresses by means of finite element method. Finally, the results of stress analysis were introduced to the program nCode to accomplish the nozzle remaining useful life assessment due to thermal fatigue in critical location on the nozzle by means of the CLF module (Critical Location Fatigue). The full methodology used to determine the nozzle operational conditions, load history, material properties and the fatigue model used to determine the number of cycles to failure of the nozzle during constant load and transients operation is presented. [Spanish] Las turbinas de gas operan a temperaturas extremadamente altas, a elevados esfuerzos termicos y mecanicos, ocasionando que la vida de los componentes involucrados se reduzca. En la presente tesis se presentan los resultados realizados por otras investigaciones de temperaturas obtenidas a partir de un analisis de transferencia de calor y flujo de fluidos de la tobera mediante el programa Star-CD basado en volumenes finitos. Posteriormente, se utilizo el programa NISA para realizar el analisis de esfuerzos mediante elementos finitos. Finalmente, se llevaron los resultados al programa nCode para realizar la estimacion de vida util por fatiga termica en un punto critico de la tobera mediante el modulo CLF (Critical Location Fatigue). Se muestra la metodologia empleada para determinar las condiciones de operacion, historial de carga, propiedades del material y el modelo de dano por fatiga para determinar el numero de ciclo para falla de la tobera durante operacion con carga continua y transitorios.

  20. Technical-economical diagnosis to schedule the maintenance shut downs of thermal power stations departing from behavior, economic engineering and thermo-economic tests; Diagnostico tecnico economico para programar las salidas a mantenimiento de centrales termicas a partir de pruebas de comportamiento, ingenieria economica y termo economia

    Energy Technology Data Exchange (ETDEWEB)

    Arreguin Arredondo, Antonio

    2002-08-01

    The thesis work develops a methodology to determine when it is convenient, technically and economically to provide maintenance to a thermal electric unit and the type of maintenance to be performed, all this sustained in an economic analysis taking into account the variation of the production costs, of the interest rates, of the fuel prices and of the electric energy prices, the maintenance costs and the degradation of the unit in the time. Once analyzed the previous matters a thermo-economic test model and reference (values provided by the manufacturer) is performed and they are compared to determine in what equipment or system of the process of electric energy generation is required to focus on the material resources as well as on the human resources, in order to obtain the best results from the maintenance and recover the greatest possible efficiency of the unit. [Spanish] El trabajo de tesis desarrolla una metodologia para determinar cuando conviene, tecnica y economicamente proporcionar mantenimiento a una unidad termica y el tiempo de mantenimiento a realizar, todo esto sustentado en un analisis economico tomando en cuenta la variacion de los costos de produccion de las tasas de interes, de los precios del combustible y de la energia electrica, el costo de mantenimiento y la degradacion de la unidad en el tiempo. Una vez analizado lo anterior se realiza un modelo termoeconomico de prueba y referencia (valores proporcionados por el fabricante) y se comparan para determinar en que equipos o sistema del proceso de generacion de energia electrica se requiere enfocar tanto los recursos materiales como humanos, con el fin de obtener mejores resultados del mantenimiento y recuperar lo mayor posible la eficiencia de la unidad.

  1. Evaluation of thermal properties of nanocomposites based on Ecobras matrix and vermiculite modified with alkyl phosphonium salt; Avaliacao das propriedades termicas dos nanocompositos de Ecobras e vermiculita modificada com sal alquil fosfonio

    Energy Technology Data Exchange (ETDEWEB)

    Oliveira, Marcelo F.L. de; Leite, Marcia C.A.M., E-mail: marceloilha@gmail.com [Universidade do Estado do Rio de Janeiro (UERJ), Rio de Janeiro, RJ (Brazil); Braga, Fernanda C.F.; Oliveira, Marcia G. [Instituto Nacional de Tecnologia (INT), Rio de Janeiro, RJ (Brazil)

    2015-07-01

    The use of biodegradable polymers for producing nanocomposites with mineral fillers fetch the production of new materials with low cost and reduced environmental impact, combined with improvements in the mechanical and thermal properties. Nanocomposites based on Ecobras and vermiculite (VMT) modified with hexadecyl tributyl phosphonium bromide (Ph-VMT) were prepared by melt intercalation. The intercalation of Ph-VMT in Ecobras was characterized by X-ray diffraction (XRD). The thermal properties of Ecobras and their compositions were characterized by differential scanning calorimetry (DSC) and thermal gravimetric analysis (TGA). The addition of VMT and Ph- VMT in Ecobras increases the crystallization temperature (Tc) and crystalline melting (Tm), as observed by DSC analysis. The result of the thermogravimetric analysis showed that the addition of Ph-VMT in Ecobras improved thermal stability of the nanocomposite. (author)

  2. Effect of chitosan content on morphology and thermal properties of poly (vinyl alcohol) / chitosan blends; Eefeito do teor de quitosana na morfologia e propriedades termicas das blendas de poli (alcool vinilico) / quitosana

    Energy Technology Data Exchange (ETDEWEB)

    Santos, Barbara Fernanda F. dos; Silva, Jessica Raquel M.B. da; Leite, Itamara Farias, E-mail: itamaraf@gmail.com [Universidade Federal da Paraiba (UFPB), Joao Pessoa, PB (Brazil). Centro de Tecnologia. Departamento de Engenharia de Materiais

    2015-07-01

    The objective of this work consists in the preparation and characterization of blends consisting of biodegradable polymers, chitosan (CS) and poly (vinyl alcohol) (PVA), to evaluate the effect of different chitosan content in morphology and thermal properties of PVA blends/CS, prepared by the solution method. Therefore, the blends were characterized by Infrared Spectroscopy Fourier Transform (FTIR), X-Ray Diffraction (XRD), Differential Scanning Calorimetry (DSC) and Thermogravimetry (TG). The results showed a good degree of interaction between the polymers of the blend constituents, suggesting certain degree of miscibility in the mixture. It was observed by XRD, that as the chitosan content in the mixture decreases PVA/CS, there is a slight increase in crystallinity. In comparative analysis, is observed that the composition PVA1/CS1 was the composition that showed improvement in thermal stability. (author)

  3. In situ synthesis and study of morphology and thermal properties of polyamide 6 nanocomposites reinforced with different layered compounds; Sintese in situ e estudo da morfologia e propriedades termicas de nanocompositos de poliamida 6 reforcados com diferentes compostos lamelares

    Energy Technology Data Exchange (ETDEWEB)

    Botan, Rodrigo; Sartor, Sabrina de B.; Moraes, Samara B. de; Lona, Liliane M.F., E-mail: botan.03@gmail.com [Universidade Estadual de Campinas (FEQ/UNICAMP), Campinas, SP (Brazil). Faculdade de Engenharia Quimica

    2015-07-01

    Presently the research and development of new polymer nanocomposites is a field of large interest and importance to the scientific and technological community. For the development and improvement in synthesis and properties of new nanocomposites, different reinforcement types have been explored. Thus, this work studies the in situ synthesis and, morphological and thermal characterization of new polyamide 6 (PA6) nanocomposites reinforced with two different types of layered compounds: layered double hydroxide (LDH) and layered hydroxide salt (LHS). These new synthesized nanocomposites were characterized by x-ray diffraction (XRD), infrared spectroscopy by Fourier transform (FTIR) and thermogravimetric analysis (TGA). The results demonstrate that the new nanocomposites showed strong evidence of exfoliated morphology with improvement in their thermal properties compared with the neat PA6. (author)

  4. Effect of gamma irradiation on mechanical and thermal properties of DGEBA/cycloaliphatic amine networks with potential for medical applications; Efeito da irradiacao gama nas propriedades mecanicas e termicas de redes DGEBA/amina cicloalifatica com potencial para aplicacoes medicas

    Energy Technology Data Exchange (ETDEWEB)

    Neves, Juliana C.; Silva, Glaura G., E-mail: glaura@qui.ufmg.br [Universidade Federal de Minas Gerais (UFMG), Belo Horizonte, MG (Brazil); Mendes, Marcio W. Duarte; Bressiani, Ana H.; Bressiani, Jose C. [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil); Garcia, Filiberto Gonzalez [Universidade Federal de Itajuba (UNIFEI), MG (Brazil)

    2013-07-01

    Two epoxy polymers based on diglycidyl ether of bisphenol A (DGEBA), cured with piperidine (Pip) and 4,4'-diamino-3,3'-dimethyldicyclohexylmethane (3DCM), were characterized before and after treatment with γ irradiation. The changes in the mechanical and thermal properties were studied by elastic modulus, glass transition temperature and degradation temperature measurements. A dose of 50 kGy of irradiation caused subtle variations in properties such as rigidity and stability, which are relevant from the fundamental point of view. The variations do not imply on negative impact when considering the stage of sterilization during the use of these systems as a biomaterial in the medical area. (author)

  5. Polymethyl methacrylate and polystyrene with layered double hydroxide nano composites: In situ synthesis, morphology and thermal properties; Nanocompositos de polimetacrilato de metila e poliestireno com hidroxido duplo lamelar: sintese in situ, morfologia e propriedades termicas

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2011-07-01

    Over the past decade, polymer nanocomposites have attracted interest, both in industry and in academia, because they often exhibit remarkable improvement in their properties when compared with pure polymer or conventional micro and macro-composites using low levels of reinforcements. In this work polymethyl methacrylate and polystyrene reinforced with layered double hydroxide, which was intercalated with sodium dodecyl sulfate were synthesized by in situ bulk polymerization. The nanocomposites were characterized and compared by X-ray diffraction, thermogravimetric analysis and flammability test. The X-ray diffraction demonstrated that synthesized nanocomposites showed a high global dispersion of layered double hydroxide, suggesting exfoliated morphology. The result of thermogravimetric analysis and flammability test for synthesized polystyrene/ layered double hydroxide nanocomposite presented a significant improvement in thermal stability and flammability property when compared with pure polymer. (author)

  6. Evaluation of compatibility and thermal properties of PP composites incorporated with Moringa oleifera fibers; Avaliacao das propriedades termicas e compatibilidade de compositos de PP incorporados com fibras de Moringa oleifera

    Energy Technology Data Exchange (ETDEWEB)

    Sa, Daniel M.; Novack, Katia M., E-mail: danielmirandaufop@yahoo.com.br, E-mail: knovack@iceb.ufop.br [Dept. de Quimica (DEQUI) - Universidade Federal de Ouro Preto (UFOP), Ouro Preto, MG (Brazil); Botaro, Vagner R., E-mail: vagner@ufscar.br [UFSCar/Sorocaba, SP (Brazil)

    2011-07-01

    The 70s, marked by the oil crisis led to knowledge about environmental problems due to indiscriminate use of nonrenewable resources. The automobile manufacturers have sought to obtain new materials for building more efficient cars, which favored the development of high-performance polymers. One alternative was the use of agents of natural reinforcements in composites manufacturing. In this work, composites were prepared using polypropylene as matrix and as a reinforcing agent of natural seed pods of Moringa oleifera in different proportions, treated with sodium hydroxide solution 10%. These composites were characterized by TGA, DSC, XRD, MEV and water absorption. It was found that increasing the amount of fiber in the polymer matrix did not change significantly the morphology and amount of water absorption of the samples. It was also observed that the addition of larger amounts of fibers decreases the degradation temperature of the samples and their melting temperatures shifts to lower temperatures, indicative of compatibility matrix / reinforcement agents. (author)

  7. Chemical structures and thermal properties of polyesters obtained from different samples of bio diesel epoxidized; Estruturas quimicas e propriedades termicas de poliesteres obtidos a partir de diferentes tipos de biodiesel epoxidado

    Energy Technology Data Exchange (ETDEWEB)

    Samios, Dimitrios; Reiznautt, Quelen B.; Nicolau, Aline; Martini, Denise D.; Chagas, Arthur L. das, E-mail: dsamios@iq.ufrgs.b [Universidade Federal do Rio Grande do Sul (IQ/UFRGS), Porto Alegre, RS (Brazil). Inst. de Quimica. Lab. de Instrumentacao e Dinamica Molecular

    2009-07-01

    In this work new structures from oligo esters and polyesters from different oils (olive oil, sunflower oil and linseed oil) were synthesized and characterized. Oligo esters and polyesters were synthesized from the reaction of fatty acid methyl epoxy-esters, obtained from different oils, with cis-1,2-cyclohexanedicarboxylic anhydride in the presence of triethylamine (TEA). Different amounts of the resin 1,4-butanediol diglycidyl ether (BDGE) were added in order to increase the capacity of crosslinking. The molar ratio of BDGE used in system was between 0 and 0.066. The intermediate structures, as well as the oligo esters and polyesters produced, were analyzed by using Fourier Transform Infrared Spectroscopy and Nuclear Magnetic Resonance ({sup 1}H - NMR). The thermal behavior of the products was realized through differential scanning calorimetry and Thermogravimetric analyses. The presence of BDGE in the materials chains increases the bonding capacity resulting in a higher molecular weight material which presents good thermal stability. (author)

  8. Effect of layered silicate content on the morphology and thermal properties of Poly(vinyl alcohol) films; Efeito do teor de silicato em camadas na morfologia e propriedades termicas de filmes de poli(alcool vinilico)

    Energy Technology Data Exchange (ETDEWEB)

    Silva, Jessica R.M.B. da; Santos, Barbara F.F. dos; Leite, Itamara F., E-mail: jraquell@homail.com [Universidade Federal da Paraiba (UFPB), Joao Pessoa, PB (Brazil). Centro de Tecnologia. Departamento de Engenharia de Materiais

    2015-07-01

    This study aims to evaluate the effect of layered silicate content on the morphology and thermal properties of PVA films. The PVA/layered silicate (AN) films were prepared by intercalation solution, using 1 to 2% of bentonite with respect to the PVA total weight. Then the films were characterized by Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), thermogravimetry (TG) and differential scanning calorimetry (DSC). Results of the FTIR revealed interaction between the functional groups of the PVA and the layered silicate. The XRD analysis showed that nanocomposites with intercalated and partially exfoliated morphology were obtained. The results of TG showed that the nanocomposite PVA/2%AN showed higher thermal stability compared to PVA/1%AN. The DSC results showed that the addition of AN to the PVA did not affect crystallization rate, as well as promoted a reduction in glass transition temperature and melting of the PVA. (author)

  9. Identification of market bags composition for biodegradable and oxo-biodegradable samples through thermal analysis in inert and oxidizer atmosphere; Identificacao da composicao de amostras de sacolas plasticas biodegradaveis e oxobiodegradaveis atraves de analises termicas em atmosfera inerte e oxidante

    Energy Technology Data Exchange (ETDEWEB)

    Finzi-Quintao, Cristiane M., E-mail: inzi@ufsj.edu.br [Universidade Federal de Sao Joao del-Rei (UFSJ), MG (Brazil); Novack, Katia M. [Universidade Federal de Ouro Preto (DEQUI/UFOP), MG (Brazil)

    2015-07-01

    Plastic films used to make market bags are based on polymers such as polyethylene, polystyrene and polypropylene, these materials require a long time to degrade in the environment. The alternative technologies of polymers have been developed to reduce the degradation time and the impact on the environment caused by the conventional materials, using pro-degrading additives or by the development biodegradable polymers. In Brazil, the laws of some municipalities require the use of biodegradable material in the production of market bags but the absence of specific surveillance policies makes its chemical composition unknown. In this paper, we analyzed 7 samples that was obtained from a a trading company and commercial market of Belo Horizonte . The samples were characterized by TGA / DTA , XRF , FTIR and MEV which allowed the identification and evaluation of the thermal behavior of the material in inert and oxidizing atmosphere. (author)

  10. Study of distillation and degradation of perfluoro polyether; Estudo da destilacao e degradacao do perfluoropolieter

    Energy Technology Data Exchange (ETDEWEB)

    Lopergolo, Lilian Cristine

    1997-07-01

    Perfluoro-polyethers, PFPE, were first synthesised by Sianesi and collaborators giving rise to a new lubricant oils and greases classes with several applications. Perfluoro polyethers have excellent properties, for instance: high chemical stability and thermal stability, high density, high radiation resistance and excellent lubricating properties. FOMBLIN-Y oil is one of the perfluoro polyethers used as a lubricant in vacuum systems applied in the UF{sub 6} enrichment installations. Due to its excellent properties and for its applications in the nuclear field, IPEN-CNEN/S P had the interest to dominate its production technology with the aim to substitute the commercial FOMBLIN-Y oil used in the national consumption. The FOMBLIN-Y oil synthesis method, adopted in IPEN-CNEN/S P, made by the photooxidation of the hexa fluoro propylene. In this work we study the fraction separation of the national available production with restricted an increased molecular weights which was obtained by fraction distillation in a vacuum according to the ASTM D-1160 norm. We also study the catalytic effect of metals on the thermal stability of perfluoro polyethers. The inertness of perfluoro polyethers at temperatures higher than 300 deg C is strongly affected by presence of some metals. Al and Ti alloys cause fluid degradation at 250 deg C. This degradation is very important because it has a yield increase of the perfluoro polyethers production. (author)

  11. Study of mechanical, rheological and thermal properties of nanocomposite HMSPP (high melt strength polypropylene) with Brazilian bentonite; Estudo das propriedades mecanicas, reologicas e termicas de nanocomposito de HMSPP (polipropileno com alta resistencia do fundido) com uma bentonita brasileira

    Energy Technology Data Exchange (ETDEWEB)

    Fermino, Danilo Marin

    2011-07-01

    This work concerns to the study of the mechanical, thermal and rheological behavior of the nano composite HMSPP - Polypropylene High Melt Strength (obtained at a dose of 12.5 kGy) and a bentonite clay Brazilian Paraiba, known as 'Chocolate' in concentrations of 5 and 10% by weight, comparison of to one American Clay, Cloisite 20A nanocomposite was done. Agent compatibilizer polypropylene-graft, known as maleic anhydride (PP-g-AM) was addict 3% concentration thought technique melt intercalation using a twin-screw extruder and the specimens were prepared by injection process. The mechanical behavior was evaluated by strength, flexural strength and impact tests. The thermal behavior was evaluated by the techniques of differential scanning calorimetry (DSC) and thermogravimetry (TGM). The rheological behavior was evaluated in rheometer. The morphology of the nanocomposites was studied by the technique of scanning electron microscopy (SEM). The organophilic bentonite and the nanocomposites were characterized by X-ray diffraction (XRD) and infrared (FTIR). (author)

  12. Multi-functional system of radiotherapy and thermal phototherapy for tumors that over-express receptors of the gastrin releasing peptide; Sistema multifuncional de radioterapia y fototerapia termica para tumores que sobre-expresan receptores del peptido liberador de gastrina

    Energy Technology Data Exchange (ETDEWEB)

    Jimenez M, N. P.

    2014-07-01

    The aim of this research was to prepare and characterize a multifunctional system of {sup 177}Lu and {sup 99m}Tc-labelled gold nanoparticles conjugated to Tat(49 57)-Lys{sup 3} bombesin ({sup 177}Lu/{sup 99m}Tc- AuNP-Tat-Bn) and to evaluate the radiation absorbed dose in GRP receptor positive PC3 tumours induced in mice (human prostate cancer cells), as well as to evaluate the thermal effect produced by the multifunctional system in PC3 cancer cells. The preparation of the system involved the conjugation of Bn-Tat, DOTA-GGC and HYNICTOC peptides to AuNP of 20 nm or 5 nm in diameter. The radiolabeling of the system with {sup 99m}Tc was carried out through the ligand HYNIC-TOC and with the {sup 177}Lu through DOTA-GGC. The functionalization of peptides to AuNP, was accomplished through a spontaneous reaction of thiol groups. The system was characterized by spectroscopic techniques while radiochemical purity was determined by size-exclusion molecular chromatography and ultrafiltration. Various internalization trials and non-specific binding were tested to demonstrate the affinity of the system to PC3 cells. The thermal effect was evaluated incubating the system into PC3 cells and irradiating it with a Nd:YAG pulsed laser beam and monitoring the temperature; after irradiation, cell viability was measured. In the evaluation of absorbed dose in mice with induced tumours, the system was administered intratumorally and later, mice were sacrificed, relevant organs and tumor were extracted, activity was quantified and radiopharmaceutical models were obtained for each organ and tumor to be used in the accumulated activity and absorbed dose calculation by the MIRD methodology. Finally, to establish the system location at cellular level, fluorescent images of the system incubated in PC3 cells were acquired with an epi fluorescent microscope. Tem, UV-Vis, XP S and Far-IR spectroscopy techniques demonstrated that AuNPs were functionalized with peptides through interactions with

  13. and characterization

    Directory of Open Access Journals (Sweden)

    Daniela L. Lamas

    2017-07-01

    Full Text Available Marine by-products contain valuable protein fractions. To ensure a profitable utilization of wastes from the fish industry, the knowledge about their quality and composition is necessary. Fish digestive proteolytic enzymes from cold-adapted ectothermic organisms have found applications in several industries because their temperature requirements and other characteristics differ from those of homologous proteases from warm-blooded animals. Herein, we describe detection, partial purification, and characterization of proteolytic enzymes from the viscera and heads of Engraulis anchoita. Enzymatic activities of the by-products were assayed using azocaseín as a substrate. To characterize the alkali protein fraction, the activity against inhibitors and their molecular weights were studied. The crude protein extract exhibited maximal activity at pH 8.0 and 60EC. Results relative to the substrate-specific Nabenzoyl-DL-arginine-p-nitroanilide and the 25 kDa molecular weight indicated that the recovered protease was trypsin. The activity showed an increment in presence of SDS and a slight decrease when it was incubated with EDTA. Increasing the concentration of NaCl up to 5% did not significantly decrease the protein’s activity. The results obtained suggest that by-products of anchovy industry could be used in the detergents industry.

  14. Elementi di trasmissione del calore

    CERN Document Server

    Guglielmini, Giovanni

    1990-01-01

    Introduzione ; concetti fondamentali di conduzione termica ; conduzione termica in regime stazionario ; conduzione termica in regime variabile ; analisi numerica nei problemi do conduzione ; concetti fondamentali di convezione termica ; convezione forzata ; convezione naturale ; scambio termico in ebollizione e condensazione ; concetti fondamentali di radiazione termica ; scambio termico per radiazione ; scambiatori di calore ; problemi termici negli edifici.

  15. Wear resistance of Fe-Nb-Cr-W, Nb, AISI 1020 and AISI 420 coatings produced by thermal spray wire arc; Resistencia al desgaste de recubrimientos Fe-Nb-Cr-W, Nb, AISI 1020 y AISI 420 producidos por proyeccion termica por arco electrico

    Energy Technology Data Exchange (ETDEWEB)

    Lopez-Covaleda, E. A.; Mercado-Veladia, J. L.; Olaya-Florez, J. J.

    2013-07-01

    The commercial materials 140MXC (with iron, tungsten, chrome, niobium), 530AS (AISI 1015 steel) and 560AS (AISI 420 steel) on AISI 4340 steel were deposited using thermal spray with arc. The aim of work was to evaluate the best strategy abrasive wear resistance of the system coating-substrate using the following combinations: (1) homogeneous coatings and (2) coatings depositing simultaneously 140MXC + 530AS and 140MXC + 560AS. The coatings microstructure was characterized using Optical microscopy, Scanning electron microscopy and Laser con focal microscopy. The wear resistance was evaluated through dry sand rubber wheel test (DSRW). We found that the wear resistance depends on the quantity of defects and the mechanical properties like hardness. For example, the softer coatings have the biggest wear rates and the failure mode was characterized by plastic deformation caused by particles indentation, and the other hand the failure mode at the harder materials was grooving. The details and wear mechanism of the coatings produced are described in this investigation. (Author)

  16. Influence of Y, Gd and Sm on the glass forming ability and thermal crystallization of aluminum based alloy; Efeito das terras raras Y, Gd e Sm na tendencia a formacao de amorfo e na cristalizacao termica em ligas a base de aluminio

    Energy Technology Data Exchange (ETDEWEB)

    Aliaga, L.C.R.; Bolfarini, C.; Kiminami, C.S.; Botta Filho, W.J., E-mail: aliaga@ufscar.b [Universidade Federal de Sao Carlos (DEMa/UFSCar), SP (Brazil). Dept. de Engenharia de Materiais; Danez, G.P. [Universidade Federal de Sao Carlos (PPG-CEMUFSCar), SP (Brazil). Programa de Pos-Graduacao em Ciencia e Engenharia de Materiais

    2010-07-01

    Al-based amorphous alloys represent an important family of metals and a great scientific activity has been devoted to determine the main features of both glass forming ability (GFA) and crystallization behavior in order to have a comprehensive framework aimed at potential technological applications. Nowadays, it is well known that the best Al-based amorphous alloys are formed in ternary systems such as Al- RE-TM, where RE is a rare earth and TM a transition metal. This paper presents results of research in Al{sub 85}Ni{sub 10}RE{sub 5} alloys (RE = Y, Gd and Sm). Amorphous ribbons were processed by melt-spinning under the same conditions and subsequently characterized by x-ray diffraction (XRD) and differential scanning calorimetry (DSC). Results show appreciable micro structural differences as function of the rare earth, thus crystal is obtained for Y, nano-glassy for Gd and, fully amorphous structure for Sm. (author)

  17. Effect of adding TiO{sub 2} to ethylene vinyl acetate copolymer on the latter's thermal properties and crystallinity; Efeito da adicao de TIO{sub 2} nas propriedades termicas e na cristalinidade do copolimero de etileno/acetato de vinila

    Energy Technology Data Exchange (ETDEWEB)

    Valentim, Ana Claudia S.; Tavares, Maria Ines Bruno; Silva, Emerson Oliveira da, E-mail: eos@ima.ufrj.br [Universidade Federal do Rio de Janeiro (UFRJ), RJ (Brazil). Instituto de Macromoleculas Professora Eloisa Mano

    2014-04-15

    We investigated the effect of adding titanium dioxide nanoparticles (TiO{sub 2}) to ethylene vinyl acetate (EVA) copolymer, containing 28% vinyl acetate groups, on the crystallinity and miscibility of the copolymer. Films of EVA/TiO{sub 2} containing 0.25%–1% TiO{sub 2}, relative to the total weight of EVA, were prepared from their solution. The obtained films were characterized by X-ray diffraction, low-field nuclear magnetic resonance, and differential scanning calorimetry. The addition of TiO{sub 2} to the EVA copolymer was proved to cause changes in the crystallinity and mobility of the polymer chains of EVA, due to new intermolecular interactions and nanostructure organization. (author)

  18. Materials characterization techniques

    National Research Council Canada - National Science Library

    Zhang, Sam; Li, L; Kumar, Ashok

    2009-01-01

    "With an emphasis on practical applications and real-world case studies, Materials Characterization Techniques presents the principles of widely used advanced surface and structural characterization...

  19. Nanotechnology Characterization Laboratory

    Data.gov (United States)

    Federal Laboratory Consortium — The Nanotechnology Characterization Laboratory (NCL) at the Frederick National Laboratory for Cancer Research performs preclinical characterization of nanomaterials...

  20. Nanotechnology Characterization Lab

    Data.gov (United States)

    Federal Laboratory Consortium — The Nanotechnology Characterization Laboratory (NCL) at the Frederick National Laboratory for Cancer Research performs preclinical characterization of nanomaterials...

  1. Modeling of the vapor cycle of Laguna Verde with the PEPSE code to conditions of thermal power licensed at present (2027 MWt); Modelado del ciclo de vapor de Laguna Verde con el codigo PEPSE a condiciones de potencia termica actualmente licenciada (2027 MWt)

    Energy Technology Data Exchange (ETDEWEB)

    Castaneda G, M. A.; Maya G, F.; Medel C, J. E.; Cardenas J, J. B.; Cruz B, H. J.; Mercado V, J. J., E-mail: miguel.castaneda01@cfe.gob.mx [Comision Federal de Electricidad, Central Nucleoelectrica Laguna Verde, Carretera Cardel-Nautla Km 42.5, Veracruz (Mexico)

    2011-11-15

    By means of the use of the performance evaluation of power system efficiencies (PEPSE) code was modeled the vapor cycle of the nuclear power station of Laguna Verde to reproduce the nuclear plant behavior to conditions of thermal power, licensed at present (2027 MWt); with the purpose of having a base line before the implementation of the project of extended power increase. The model of the gauged vapor cycle to reproduce the nuclear plant conditions makes use of the PEPSE model, design case of the vapor cycle of nuclear power station of Laguna Verde, which has as main components of the model the great equipment of the vapor cycle of Laguna Verde. The design case model makes use of information about the design requirements of each equipment for theoretically calculating the electric power of exit, besides thermodynamic conditions of the vapor cycle in different points. Starting from the design model and making use of data of the vapor cycle measured in the nuclear plant; the adjustment factors were calculated for the different equipment s of the vapor cycle, to reproduce with the PEPSE model the real vapor cycle of Laguna Verde. Once characterized the model of the vapor cycle of Laguna Verde, we can realize different sensibility studies to determine the effects macros to the vapor cycle by the variation of certain key parameters. (Author)

  2. Measurements and characterization - Electro-optical characterization

    Energy Technology Data Exchange (ETDEWEB)

    Cook, G.

    2000-03-16

    This brochure presents the capabilities that the Measurements and Characterization Division has in Electro-Optical Characterization, in which a variety of spectroscopy, ellipsometry, and capacitance techniques are used to probe the fundamental electrical and optical properties of solid-state materials.

  3. Practical materials characterization

    CERN Document Server

    2014-01-01

    Presents cross-comparison between materials characterization techniquesIncludes clear specifications of strengths and limitations of each technique for specific materials characterization problemFocuses on applications and clear data interpretation without extensive mathematics

  4. Waste Characterization Methods

    Energy Technology Data Exchange (ETDEWEB)

    Vigil-Holterman, Luciana R. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Naranjo, Felicia Danielle [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2016-02-02

    This report discusses ways to classify waste as outlined by LANL. Waste Generators must make a waste determination and characterize regulated waste by appropriate analytical testing or use of acceptable knowledge (AK). Use of AK for characterization requires several source documents. Waste characterization documentation must be accurate, sufficient, and current (i.e., updated); relevant and traceable to the waste stream’s generation, characterization, and management; and not merely a list of information sources.

  5. Detailed thermal simulation of fenestration; Simulacion termica detallada de una ventana

    Energy Technology Data Exchange (ETDEWEB)

    Fissore Sch, Adelqui; Tartari, Paula [Universidad de Concepcion (Chile). Facultad de Ingenieria. Dept. de Ingenieria Mecanica]. E-mail: afissore@udec.cl; ptartari@udec.cl; Hernandez C, Gaston [Universidad del Bio-Bio, Concepcion (Chile). Facultad de Ingenieria. Dept. de Ingenieria Mecanica]. E-mail: ghernand@ubiobio.cl

    2000-07-01

    In this paper a new model for heat balance of a window is proposed. The objective of the model is to solve accurately the heat balance on a single glass window in a moderate climate. This procedure will allow the designer to calculate the main parameters of a fenestration (surface, orientation, overhangs, etc.), minimizing the energy consumption for a specific enclosure (including heating, air conditioning and lighting). The present study is mainly focused on problems related with the internal long wave radiation calculations, and secondly on the effect of internal convection coefficient on the heat balance. A comparison between the results obtained using this model and those obtained with other current models is included in the second part of the paper. The importance of using the right internal convection coefficient on the heat balance of fenestration for this kind of application is also analyzed. (author)

  6. Thermal air contamination in urban environment. Contaminacion termica del aire en el medio ambiente urbano

    Energy Technology Data Exchange (ETDEWEB)

    Munoz Machado, A.

    1994-01-01

    This article summarizes the necessity of thermal contamination control. The principal contaminant is the loss of heat from buildings. There is not a regulation and the environmental regulation has not a special article to regulate this topic.

  7. Thermal recovery simulation at the pore-network level; Simulacao de recuperacao termica em escala microscopica

    Energy Technology Data Exchange (ETDEWEB)

    Oliveira, Claudio L.N.; Almeida, Murilo P.; Andrade Junior, Jose S. [Universidade Federal do Ceara (UFC), Fortaleza, CE (Brazil); Herrmann, Hans J. [Eidgenossische Technische Hochschule Zurich (ETHZ), Zurich (Switzerland)

    2008-07-01

    We have investigated the effect of temperature in penetration of an inviscid fluid into a porous media saturated with a very high viscous fluid. Gradient of temperature is applied across the medium. The viscosity of the defending fluid is considered as an exponential-like function with temperature. This scheme represents a small fraction of a heavy oil reservoir where steam injection is applied. The results show that the recovery of the viscous fluid is a hyperbolic tangent function with the difference of temperature, where it has a maximum recovery for high gradient. Our results show, also, that the recovery efficiency can increase substantially with the gradient of temperature. (author)

  8. Architecture's models: Integral thermal evaluation; Modelos en arquitectura: evaluacion termica integral

    Energy Technology Data Exchange (ETDEWEB)

    Roset, Jaume [Universidad Politecnica de Cataluna, Barcelona (Spain); Marincic, Irene; Ochoa, J. Manuel [Universidad de Sonora, Hermosillo, Sonora (Mexico)

    2000-07-01

    During the fist stages of a building design, considering energy conscious design, inhabitants needs and functionality, it is necessary to estimate and evaluate the buildings behavior and to know if it achieves the initial design objectives. Models are used to represent a description of objects and architectural concepts, as well as the hypothesis of its temporary and spatial behavior. The quantity and type of information needed as input of a model to be operative, has been, and still is, a controversial topic. The question is: how much useful are models that need a great quantity of inputs than other simpler ones? We consider as simple models those that habitually contain a certain quantity of empirical coefficients, which permit to reduce the number of inputs, solving the calculus as an approximation. In the other hand, in the architectural domain, information is usually presented in different type of supports (tables of numerical values, planes, physical models, ...). The information supplied in each type of support must necessary be combined, in order to maximize the information contained in the global system. In this paper, we present examples of thermal studies dealing with different ways to evaluate models, which involve variables of thermal behavior of buildings, the interaction between them and the environment and its influence on the indoor thermal comfort. As a general conclusion, we can say that a model should minimize the quantity of inputs required, which must be able to approach to the most relevant effects, that nearly represent the real behavior. The hypothesis and evaluation conditions of these effects must be understood and assumed by the user. [Spanish] Durante las etapas previas al diseno de un edificio eficiente energeticamente y coherente con las necesidades de sus usuarios y con su funcion, sera necesario estimar y evaluar su comportamiento para saber en que medida se estan logrando los objetivos de diseno planteados inicialmente. Con este fin, se utilizan modelos que representen tanto la descripcion de los objetos y conceptos arquitectonicos, como las hipotesis sobre su comportamiento espacio-temporal. La cantidad y tipo de informacion que es necesario suministrar a un modelo para hacerlo operativo ha sido, y es, objeto de grandes controversias. La cuestion es: hasta que punto son mas utiles modelos con gran cantidad de entradas que otros mas simples? Entendiendo por modelos simples aquellos que habitualmente contienen cierta cantidad de coeficientes empiricos, lo que reduce el numero de datos, llevando el calculo a una aproximacion. Por otro lado, en el dominio de la arquitectura la informacion se presenta de manera habitual, sobre soportes de diferente tipo (tablas de valores numericos, planos, maquetas, ...). Las informaciones suministradas en cada tipo de soporte deben, necesariamente, ser combinadas de manera que se maximice la informacion contenida sobre el sistema global. En este trabajo, presentamos ejemplos referentes a estudios termicos que hemos realizado sobre diferentes maneras de abordar la evaluacion de modelos variables relacionados con el comportamiento termico de los edificios, la interaccion de estos con el medio ambiente que los rodea y su influencia sobre el confort en el interior de los mismos. Como conclusion general, podriamos decir que un modelo deberia tener las minimas entradas posibles con las cuales abordar los efectos mas significativos, que puedan representar de la manera mas aproximada posible al comportamiento real. Las hipotesis y condiciones de evaluacion de estos efectos deben ser comprendidas y asumidas por el usuario.

  9. La teoria della radiazione termica dalla fisica classica alla fisica quantistica

    CERN Document Server

    Planck, Max

    1999-01-01

    La venuta alla luce, nella scienza fisica dei primi anni del Novecento, di elementi assolutamente nuovi prefiguranti il futuro mondo quantistico, è concordemente attribuita all'opera prevalente di Planck e di Einstein, secondo due linee di ricerca profondamente diverse, anche se non lontane risultano le loro concezioni del mondo fisico. Tuttavia, mentre del secondo è facilmente accessibile e sufficientemente nota la produzione scientifica, del primo risulta ancora scarsamente sconosciuta l'ingente produzione di quegli anni, anche perché reperibile, per la maggior parte, solo in lingua originale. Se si tiene presente, inoltre, la comparsa in tempi recenti, della ricostruzione storiografica non tradizionale di T. Kuhn, che ritiene di cogliere, negli scritti di Planck, la permanenza di una struttura integralmente classica fino ad anni successivi al 1906, data di pubblicazione delle Lezioni, risulta naturale convenire sull'opportunità di rendere più agevole l'accesso alle fonti planckiane di quegli anni. ...

  10. Propriedades mecanicas e termicas, morfologia e reologia de blendas de poliamida-6 e elastomeros

    OpenAIRE

    Edmir Carone Junior

    1999-01-01

    Resumo: Blendas de poliamida-6 (PA-6) e elastômeros é o tema central desta tese. O trabalho pode ser subdividido em três partes principais de acordo com o tipo de borracha utilizada, sendo que cada parte possui diferentes objetivos. Na primeira parte, foram exploradas as propriedades mecânicas e a morfologia de fases de blendas ternárias de poliamida-6 com borracha (copolímero aleatório de etileno e propileno modificado com anidrido maleico (EPR-g-MA) ou misturas do copolímero bloco de estire...

  11. Composito de poliuretano de mamona e residuo industrial para isolacao termica e absorcao sonora

    OpenAIRE

    Oliveira, Maria Cleide Ribeiro de

    2010-01-01

    Neste trabalho tratou-se do desenvolvimento de um material inovador constituído de matriz poliuretânica vegetal e carga de resíduo industrial, proveniente de recauchutagem de pneus, para fins de isolação térmica e conforto ambiental. Para tanto, são apresentados procedimentos e resultados experimentais obtidos da análise do desempenho térmico e acústico desse material compósito produzido a partir de resina expansiva derivada do óleo da semente de mamona e fibras de pneus ins...

  12. Evaluacion termica, mecanica y electrica de materiales compuestos cordierita-mullita

    Directory of Open Access Journals (Sweden)

    M.A. Camerucci

    2000-10-01

    Full Text Available Commercially available cordierite and mullite powders were used to obtain cordierite and cordierite-30wt% mullite materials by attrition milling, uniaxial pressing and sintering. Cordierite powders were the coarse (D50 = 1.82 mum, medium (D50 = 0.9 mum and fine (D50 = 0.45 mum single granulometric fractions and binary mixtures of them. Mullite powder employed in composites was the 7 h-attrition milled one (D50 = 1.3 mum. Hardness (H V and fracture toughness (K IC were measured by Vickers indentation techniques. Composites showed higher H V and K IC than cordierite matrices. In both materials, H V and K IC diminish with the increasing porosity. Dielectric constant (epsilon and losses (tan delta were determined at 1 MHz. An increase in epsilon and tan delta values was registered when mullite was present in composites with respect to cordierite material. Higher the porosity, epsilon was lower and tan delta increased. The thermal expansion coefficients (alpha were determined up to 1000 °C resulting the alpha of the composite close to that of the silicon.

  13. Zirconium titanate: stability and thermal expansion; Titanato de circonio: estabilidad termodinamica y expansion termica

    Energy Technology Data Exchange (ETDEWEB)

    Lopez-Lopez, E.; Moreno, R.; Baudin, C.

    2011-07-01

    Zirconium titanate is a well known compound in the field of electro ceramics, although it has also been used in catalyst and sensors applications. The crystallographic thermal expansion anisotropy of this compound makes it a potential candidate as constituent of structural components. In general, to assure the structural integrity and microstructural homogeneity of a ceramic piece, relatively low cooling rates from the fabrication temperature are required. This requirement is essential for zirconium titanate because thermal expansion as well as phase distribution is affected by small variations in the composition and cooling rate. This work reviews the available data on the phase equilibrium relationships in the systems ZrO{sub 2}-TiO{sub 2} and ZrO{sub 2}-TiO{sub 2}-Y{sub 2}O{sub 3}. The main discrepancies as well as the possible origins of them are discussed. Additionally, the crystallographic thermal expansion data in the current literature are reviewed. (Author) 56 refs.

  14. Detection of plastic explosives by thermic neutron radiography; Deteccao de explosivos plasticos por neutrongrafia termica

    Energy Technology Data Exchange (ETDEWEB)

    Hacidume, Leo R.; Crispim, Verginia R.; Silva, Ademir X. da [Universidade Federal, Rio de Janeiro, RJ (Brazil). Coordenacao dos Programas de Pos-graduacao de Engenharia. Programa de Engenharia Nuclear

    2000-07-01

    This work aims to demonstrate the potentiality of the neutron radiography technique, allied to the computerized tomography by transmission, to both detect and visualize plastic explosive samples in several hidden conditions, using a simple scanner as a digitalisation instrument. Each tomographic essay was obtained in the J-9 channel of the Argonauta Research Reactor of IEN/CNEN, in groups of six neutron radiographic projections, performed with an angular increment of 30 in a period of time of 30 minutes for each projection. Two groups of tomographic reconstructions were generated, distinguished by the digitalisation process of the interested lines in the reconstruction plane coming from the projection groups, utilizing a scanner and a microdensitometer, respectively. The reconstruction of the bi-dimensional image of the transverse section, in relation to this plane, was processed making use of the Image reconstruction algorithmic of an image based on the maximum entropy principle (ARIEM). From the qualitative analysis of the images, we conclude that the neutron radiographic system was able to detect the explosive sample in a satisfactory way while the quantitative analysis confirmed the application effectiveness of a scanner to acquire the projection dates whose objective is only a reconnaissance. (author)

  15. Detection of plastic explosives using thermal neutron radiography; Deteccao de explosivos plasticos por neutrongrafia termica

    Energy Technology Data Exchange (ETDEWEB)

    Hacidume, Leo Ryoske

    1999-12-01

    The work aims to demonstrate the potentiality of the neutron radiography technique, allied to the computerized tomography by transmission, to both detect and visualize plastic explosive samples in several hidden conditions, using a simple scanner as a digitalisation instrument. Each tomographic essay was obtained in the J-9 channel of the Argonauta Research Reactor of IEN/CNEN, in groups of six neutron radiographic projections, performed with an angular increment of 30 deg C, in a period of time of 30 minutes for each projection. Two groups of tomographic reconstructions were generated, distinguished by the digitalisation process of the interested lines in the reconstruction plane coming from the projection groups, utilization a scanner and a microdensitometer, respectively. The reconstruction of the bi-dimensional image of the transverse section, in relation to this plane, was processed making use of the Image Reconstruction Algorithmic of an Image based on the Maximum Entropy principle (ARIEM). From the qualitative analysis of the images, we conclude that the neutron radiographic system was able to detect the explosive sample in a satisfactory way while the quantitative analysis confirmed the application effectiveness of a scanner to acquire the projection dates whose objective is only a reconnaissance. (author)

  16. Dano cavitacional em revestimentos depositados por aspersão termica a chama

    OpenAIRE

    Paulo Villani Marques

    1996-01-01

    Resumo: Quantias elevadas são gastas anualmente na manutenção de turbinas hidráulicas usadas na geração de energia elétrica por causa do ataque cavitacional. Avaliou-se a aplicabilidade de revestimentos metálicos e cerâmicos depositados sobre aço carbono por aspersão térmica a chama na manutenção destes equipamentos em função de sua resistência à erosão por cavitação. Foram realizados ensaios de dureza, rugosidade, ensaio acelerado de cavitação induzida por vibração ultra-sônica, adesão (traç...

  17. Photovoltaic Characterization Laboratory

    Data.gov (United States)

    Federal Laboratory Consortium — NIST's PV characterization laboratory is used to measure the electrical performance and opto-electronic properties of solar cells and modules. This facility consists...

  18. Composites Characterization Laboratory

    Data.gov (United States)

    Federal Laboratory Consortium — The purpose of the Composites Characterization Laboratory is to investigate new and/or modified matrix materials and fibers for advanced composite applications both...

  19. Materials Characterization Facility

    Data.gov (United States)

    Federal Laboratory Consortium — The Materials Characterization Facility enables detailed measurements of the properties of ceramics, polymers, glasses, and composites. It features instrumentation...

  20. Characterization of solid surfaces

    National Research Council Canada - National Science Library

    Kane, Philip F; Larrabee, Graydon B

    1974-01-01

    .... A comprehensive review of surface analysis, this important volume surveys both principles and techniques of surface characterization, describes instrumentation, and suggests the course of future research...

  1. Characterization of revenue equivalence

    NARCIS (Netherlands)

    Heydenreich, B.; Müller, R.; Uetz, Marc Jochen; Vohra, R.

    2009-01-01

    The property of an allocation rule to be implementable in dominant strategies by a unique payment scheme is called revenue equivalence. We give a characterization of revenue equivalence based on a graph theoretic interpretation of the incentive compatibility constraints. The characterization holds

  2. Techniques for characterizing lignin

    Science.gov (United States)

    Nicole M. Stark; Daniel J. Yelle; Umesh P. Agarwal

    2016-01-01

    Many techniques are available to characterize lignin. The techniques presented in this chapter are considered nondegradative, which are commonly applied to lignin. A brief discussion of lignin structure is included with this chapter to aid the reader in understanding why the discussed characterization techniques are appropriate for the study of lignin. Because the...

  3. Implementation of ozonation process in degradation of the phenols present in petrochemistry effluents; Aplicacao do processo de ozonizacao na degradacao de fenois presentes em efluentes petroquimicos

    Energy Technology Data Exchange (ETDEWEB)

    Souza, Fernanda Batista de; Souza, Antonio Augusto Ulson de; Souza, Selene Maria Arruda Guelli Ulson de [Universidade Federal de Santa Catarina (UFSC), Florianopolis, SC (Brazil)

    2008-07-01

    The water contamination by the petrochemical pollutants with high toxicity, such as phenols, is a subject of interest of several researchers. The ozone is an alternative for the effluents treatment, being effective in environmental decontamination, reducing the COD and degrading the phenols. The ozone stability depends on the water pH, the type and content of organic matter. This study aimed to investigate in the phenol ozonation, evaluating the phenol and COD removal at different pHs. Ozone as injected in 5 L of phenol solution of 50 mg L-1 at pH = 2, 7 and 10, from 1 to 25 minutes, and then was measured the quantity of COD and phenol. It was found that in acid pH the ozone has increased the stability, because 82.19% of the ozone that enters in the column remains in solution. The phenol degradation was faster in alkaline solution (pH=10), where in 15 minutes of treatment, 99.7% of phenol was consumed. The COD removal increased from 7.3% in 6 minutes to 87.8% in 30 minutes, but the COD removal increases more slowly than that of phenol which was 53, 8% in 6 min, increasing to 99.2% at 25 min for pH=7. (author)

  4. Degradation of ion spent resin using the Fenton's reagent; Degradacao da resina de troca ionica utilizando o reagente de Fenton

    Energy Technology Data Exchange (ETDEWEB)

    Araujo, Leandro Goulart de

    2013-07-01

    The most common method for spent radioactive ion exchange resin treatment is its immobilization in cement, which reduces the radionuclides release into the environment. Although this method is efficient, it increases considerably the final volume of the waste due to the low incorporation capacity. The objective of this work was to develop a degradation method of spent resins arising from the nuclear research reactor located at the Nuclear and Energy Research Institute (IPEN-CNEN/SP), using an Advanced Oxidation Process (AOP) with Fenton's reagents. This method would allow a higher incorporation in cement. Three different resins were evaluated: cationic, anionic and a mixture of both resins. The reactions were conducted varying the catalyst concentration (25, 50, 100 and 150 mM), the volume of hydrogen peroxide (320 to 460 mL), and three different temperatures, 50, 60 and 70 deg C. Degradation of about 98% was achieved using a 50 mM catalyst solution and 330 mL of hydrogen peroxide solution. The most efficient temperature was 60 deg C. (author)

  5. Radiation degradation of biological waste (aflatoxins) produced in food laboratory; Degradacao por radiacao de residuos biologicos (aflatoxinas) produzidos em laboratorio de alimentos

    Energy Technology Data Exchange (ETDEWEB)

    Rogovschi, Vladimir Dias

    2009-07-01

    Many filamentous fungi can produce secondary metabolites, called mycotoxins, which can be found in food and agricultural products. One of the main genera of myco toxigenic fungi related to the food chain is the Aspergillus spp. There are over 400 mycotoxins described in the literature, the most common the aflatoxins B1, B2, G1 and G2. The mycotoxins are commonly found in foods and are considered one of the most dangerous contaminants. The aflatoxin B1 is classified in group one by the International Agency of Research on Cancer. Aflatoxins resisting for more than one hour in autoclave making it necessary to other means of degradation of these toxins. This work aimed to observe the effects of gamma radiation of {sup 60}Co and electron beams in the degradation of aflatoxins and compare the damage caused on the morphology of the Aspergillus flavus. The fungus was grown on potato dextrose agar (PDA) for 10 days and was subsequently transferred to coconut agar medium, and maintained for 14 days at 25 degree C. After this step the coconut agar was ground to become a homogeneous pasty and was irradiated with doses of 2.5, 5.0, 10 and 20 kGy. The samples used in scanning electron microscopy were irradiated with doses of 0, 2.5, 5.0, 10 and 20 kGy with sources of {sup 60}Co and electron beams. Irradiation with electron accelerator showed a slightly higher degradation to gamma radiation, reducing 29.93 %, 34.50 %, 52.63 % and 72.30 % for doses of 2.5, 5.0, 10 and 20 kGy, respectively. The Scanning Electron Microscopy showed that doses of 2.5 to 10 kGy did not cause damage to the fungus, but with a dose of 20 kGy it can be observed fungal damage to structures. (author)

  6. Study of oil diesel degradation in soil using oxidative advanced processes; Estudo da degradacao do oleo diesel em solo utilizando processos oxidativos avancados

    Energy Technology Data Exchange (ETDEWEB)

    Santos, Suenia S.; Silva, Valdinete L. da; Motta, Mauricio da [Universidade Federal de Pernambuco (UFPE), Recife, PE (Brazil). Dept. de Engenharia Quimica; Silva, Paula Tereza de S. e; Barros Neto, Benicio de [Universidade Federal de Pernambuco (UFPE), Recife, PE (Brazil). Dept. de Quimica Fundamental

    2004-07-01

    Recently it comes if observing several accidents during the exploration, refinement, transport and operation of storage of petroleum and yours derived, such as the diesel oil and the gasoline. In this paper We do a study of the degradation of the diesel oil in a characteristic soil of the state of Pernambuco using peroxide of hydrogen and Fenton reagent. Those two processes are based on the generation of the radical hydroxyl (OH.) that has to can oxidizer loud capable to promote the destruction of recalcitrant organic compositions. The studied soil has about 16,5{+-}0,3 g/kg of total organic carbon. A factorial planning was accomplished 2{sup 3} with 2 repetitions in the central point with the objective of finding the best conditions of degradation of the pollutant. The variables and the studied levels were: FeSO{sub 4} - 0,18 M (0, 4 and 8 Ml); pH (3; without adjustment and without adjustment) and Time of exhibition in the sun (8; 12 and 16:00). The volumes of H{sub 2}O{sub 2} used in the rehearsals were constant, being 80 mL. Soon afterwards it accomplished a fractional experimental planning 2{sup 3-1}, repeating the variables of the first planning, they put using a smaller volume of H{sub 2}O{sub 2}, 40 mL, to evaluate the influence of the amount of H{sub 2}O{sub 2} used about the degradation of the diesel oil. The mass of the soil used in each experiment was of 5 g. It was observed that there were not significant differences in the degradation in relation to the peroxide volume. The best found degradation was around 87% in the following conditions (4 mL of Faith, without pH adjustment, Time of exhibition in the sun of 12:00 and 80 ml of H{sub 2}O{sub 2}). That found degradation was quite satisfactory being still due to study more economical conditions. (author)

  7. Hydrolytic and photochemistry degradation of the amoxicillin in {beta}-cyclodextrin; Degradacao hidrolitica e fotoquimica da amoxicilina na presenca de {beta}-ciclodextrina

    Energy Technology Data Exchange (ETDEWEB)

    Bariccatti, R.A.; Silva, C.; Souza, M.L.; Lindino, C.A.; Rosa, M.F. [Universidade Estadual do Oeste do Parana, Toledo, PR (Brazil). Centro de Engenharias e Ciencias Exatas]. E-mail: reinaldo0207@brturbo.com.br

    2008-10-15

    This work has like purpose monitors the degradation of the drug amoxicillin in the presence and absence of {beta}-cyclodextrin, through techniques spectroscopy. For this, there was accompanied the hydrolysis of the drug protected of the light for around 400 hours. The results indicate that, initially, the cyclodextrin does not alter the hydrolysis of the amoxicillin, however, after 250 hours there is an increase of the hydrolysis of the amoxicillin when present at cyclodextrin. Another variable was the irradiation of the sample with radiation in the region of the UV, we see that the solutions containing {beta}- cyclodextrin suffer a slower phototransformation (26,8%) than the solutions without {beta}-cyclodextrin, when irradiated by UV radiation. (author)

  8. TRANGE: computer code to calculate the energy beam degradation in target stack; TRANGE: programa para calcular a degradacao de energia de particulas carregadas em alvos

    Energy Technology Data Exchange (ETDEWEB)

    Bellido, Luis F.

    1995-07-01

    A computer code to calculate the projectile energy degradation along a target stack was developed for an IBM or compatible personal microcomputer. A comparison of protons and deuterons bombarding uranium and aluminium targets was made. The results showed that the data obtained with TRANGE were in agreement with other computers code such as TRIM, EDP and also using Williamsom and Janni range and stopping power tables. TRANGE can be used for any charged particle ion, for energies between 1 to 100 MeV, in metal foils and solid compounds targets. (author). 8 refs., 2 tabs.

  9. Panel 3 - characterization

    Energy Technology Data Exchange (ETDEWEB)

    Erck, R.A.; Erdemir, A.; Janghsing Hsieh; Lee, R.H.; Xian Zheng Pan; Deming Shu [Argonne National Lab., IL (United States); Feldman, A. [National Inst. of Standards and Technology, Gaithersburg, MD (United States); Glass, J.T. [North Carolina State Univ., Raleigh (United States); Kleimer, R. [Coors Ceramics Co., Golden, CO (United States); Lawton, E.A. [JPL/Caltech, Pasadena, CA (United States); McHargue, C.J. [Univ. of Tennessee, Knoxville (United States)

    1993-01-01

    The task of this panel was to identify and prioritize needs in the area of characterization of diamond and diamond-like-carbon (DLC) films for use in the transportation industry. Until recent advances in production of inexpensive films of diamonds and DLC, it was not feasible that these materials could be mass produced. The Characterization Panel is restricting itself to identifying needs in areas that would be most useful to manufacturers and users in producing and utilizing diamond and DLC coatings in industry. These characterization needs include in-situ monitoring during growth, relation of structure to performance, and standards and definitions.

  10. SYNTHESIS, CHARACTERIZATION AND ANTIBACTERIAL ...

    African Journals Online (AJOL)

    Preferred Customer

    E-mail: a-ahmadi@kiau.ac.ir; ahmadikiau@yahoo.com. SYNTHESIS, CHARACTERIZATION AND ANTIBACTERIAL EVALUATION OF. SOME NOVEL DERIVATIVES OF 2-BROMOMETHYL-BENZIMIDAZOLE. Abbas Ahmadi*. Department of Medicinal Chemistry, Pharmaceutical Sciences Branch, Islamic Azad University,.

  11. Site characterization handbook

    Energy Technology Data Exchange (ETDEWEB)

    1988-06-01

    This Handbook discusses both management and technical elements that should be considered in developing a comprehensive site characterization program. Management elements typical of any project of a comparable magnitude and complexity are combined with a discussion of strategies specific to site characterization. Information specific to the technical elements involved in site characterization is based on guidance published by the Nuclear Regulatory Commission (NRC) with respect to licensing requirements for LLW disposal facilities. The objective of this Handbook is to provide a reference for both NRC Agreement States and non-Agreement States for use in developing a comprehensive site characterization program that meets the specific objectives of the State and/or site developer/licensee. Each site characterization program will vary depending on the objectives, licensing requirements, schedules/budgets, physical characteristics of the site, proposed facility design, and the specific concerns raised by government agencies and the public. Therefore, the Handbook is not a prescriptive guide to site characterization. 18 refs., 6 figs.

  12. Space Solar Cell Characterization Laboratory

    Data.gov (United States)

    Federal Laboratory Consortium — FUNCTION: Measures, characterizes, and analyzes photovoltaic materials and devices. The primary focus is the measurement and characterization of solar cell response...

  13. Site characterization plan:

    International Nuclear Information System (INIS)

    1988-01-01

    The Yucca Mountain site in Nevada is one of three candidate sites for the first geologic repository for radioactive waste. On May 28, 1986, it was recommended for detailed study in a program of site characterization. This site characterization plan (SCP) has been prepared in accordance with the requirements of the Nuclear Waste Policy Act to summarize the information collected to date about the geologic conditions at the site;to describe the conceptual designs for the repository and the waste package;and to present the plans for obtaining the geologic information necessary to demonstrate the suitability of the site for repository, to design the repository and the waste package, to prepare an environmental impact statement, and to obtain from the US Nuclear Regulatory Commission (NRC) an authorization to construct the repository. This introduction begins with a brief section on the process for siting and developing a repository, followed by a discussion of the pertinent legislation and regulations. A description of site characterization is presented next;it describes the facilities to be constructed for the site characterization program and explains the principal activities to be conducted during the program. Finally, the purpose, content, organizing principles, and organization of this site characterization plan are outlined, and compliance with applicable regulations is discussed

  14. Site characterization plan:

    International Nuclear Information System (INIS)

    1988-01-01

    The Yucca Mountain site in Nevada is one of three candidate sites for the first geologic repository for radioactive waste. On May 28, 1986, it was recommended for detailed study in a program of site characterization. This site characterization plan (SCP) has been prepared in acordance with the requirements of the Nuclear Waste Policy Act to summarize the information collected to date about the geologic conditions at the site;to describe the conceptual designs for the repository and the waste package and to present the plans for obtaining the geologic information necessary to demonstrate the suitability of the site for a repository, to design the repository and the waste package, to prepare an environmental impact statement, and to obtain from the US Nuclear Regulatory Commission (NRC) an authorization to construct the repository. This introduction begins with a brief section on the process for siting and eveloping a repository, followed by a discussion of the pertinent legislation and regulations. A description of site characterization is presented next;it describes the facilities to be constructed for the site characterization program and explains the principal activities to be conducted during the program. Finally, the purpose, content, organizing prinicples, and organization of this site characterization plan are outlined, and compliance with applicable regulations is discussed. 880 refs., 130 figs., 25 tabs

  15. Tank characterization reference guide

    International Nuclear Information System (INIS)

    De Lorenzo, D.S.; DiCenso, A.T.; Hiller, D.B.; Johnson, K.W.; Rutherford, J.H.; Smith, D.J.; Simpson, B.C.

    1994-09-01

    Characterization of the Hanford Site high-level waste storage tanks supports safety issue resolution; operations and maintenance requirements; and retrieval, pretreatment, vitrification, and disposal technology development. Technical, historical, and programmatic information about the waste tanks is often scattered among many sources, if it is documented at all. This Tank Characterization Reference Guide, therefore, serves as a common location for much of the generic tank information that is otherwise contained in many documents. The report is intended to be an introduction to the issues and history surrounding the generation, storage, and management of the liquid process wastes, and a presentation of the sampling, analysis, and modeling activities that support the current waste characterization. This report should provide a basis upon which those unfamiliar with the Hanford Site tank farms can start their research

  16. Characterization of cellulose nanowhiskers

    International Nuclear Information System (INIS)

    Nascimento, Nayra R.; Pinheiro, Ivanei F.; Morales, Ana R.; Ravagnani, Sergio P.; Mei, Lucia

    2015-01-01

    Cellulose is the most abundant polymer earth. The cellulose nanowhiskers can be extracted from the cellulose. These have attracted attention for its use in nanostructured materials for various applications, such as nanocomposites, because they have peculiar characteristics, among them, high aspect ratio, biodegradability and excellent mechanical properties. This work aims to characterize cellulose nanowhiskers from microcrystalline cellulose. Therefore, these materials were characterized by X-ray diffraction (XRD) to assess the degree of crystallinity, infrared spectroscopy (FT-IR), transmission electron microscopy (TEM) to the morphology of nanowhiskers and thermal stability was evaluated by Thermogravimetric Analysis (TGA). (author)

  17. SHORT COMMUNICATION SYNTHESIS, CHARACTERIZATION ...

    African Journals Online (AJOL)

    Preferred Customer

    oxazine-. 2-ol methyl-2,3-diphenyl-2H-1,4-oxazine-2-ol (2). Characterization was performed using elemental analysis, UV-Vis and 1HNMR spectroscopy. The structure of this oxazine compound was determined by X-ray crystallography, and we ...

  18. Characterization of Revenue Equivalence

    NARCIS (Netherlands)

    Heydenreich, Birgit; Müller, Rudolf; Uetz, Marc Jochen; Vohra, Rakesh

    2008-01-01

    The property of an allocation rule to be implementable in dominant strategies by a unique payment scheme is called \\emph{revenue equivalence}. In this paper we give a characterization of revenue equivalence based on a graph theoretic interpretation of the incentive compatibility constraints. The

  19. Inhibin : purification and characterization

    NARCIS (Netherlands)

    S. van Dijk (Simon)

    1986-01-01

    textabstractThe aims of the studies described in this thesis were to purify and characterize inhibin from ovarian follicular fluids. The first objective was an extension of the studies by Jansen et al .. , (1981) who had partially purified inhibin from bovine ovarian follicular fluid (bFF) and made

  20. Cf-252 Characterization Documents

    Energy Technology Data Exchange (ETDEWEB)

    Feldman, Alexander [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2014-03-14

    Six documents were written by Vance and Associates under contract to the Off-Site Source Recovery Project of Los Alamos National Laboratory. These Six documents provided the basis for characterization of Californium-252 sealed sources and for the packaging and manifesting of this material for disposal at the Waste Isolation Pilot Project. The Six documents are: 1. VA-OSR-10, Development of radionuclide distributions for Cf-252 sealed sources. 2. VA-OSR-11, Uncertainty analysis for Cf-252 sealed sources. 3. VA-OSR-12, To determine the radionuclides in the waste drums containing Cf-252 sealed source waste that are required to be reported under the requirements of the WIPP WAC and the TRAMPAC. 4. VA-OSR-13, Development of the spreadsheet for the radiological calculations for the characterization of Cf-252 sources. 5. VA-OSR-14, Relative importance of neutron-induced fission in Cf-252 sources. 6. VA-OSR-15, Determine upper bound of decay product inventories from a drum of Cf-252 sources. These six documents provide the technical basis for the characterization of Cf-252 sources and will be part of the AK documentation required for submittal to the Central Characterization Project (CCP) of WIPP.

  1. PREPARATION, CHARACTERIZATION AND OPTICAL ...

    African Journals Online (AJOL)

    The prepared host-guest composite material shows luminescence. The material has the potentiality as luminescence material. KEY WORDS: Host-guest nanocomposite material, Nanometer MCM-41 molecular sieve host, Rhodamine B guest, Characterization, Luminescence Bull. Chem. Soc. Ethiop. 2009, 23(1), 145-150.

  2. Characterization of Bacillus cereus

    NARCIS (Netherlands)

    Wijnands LM; Dufrenne JB; Leusden FM; MGB

    2002-01-01

    Bacillus cereus is a ubiquitary microorganism that may cause food borne disease. Pathogenicity, however, depends on various characteristics such as the ability to form (entero)-toxin(s) that can not be detected by microbiological methods. Further characterization of pathogenic properties is not only

  3. Characterization of Photovoltaic Generators

    Science.gov (United States)

    Boitier, V.; Cressault, Y.

    2011-01-01

    This paper discusses photovoltaic panel systems and reviews their electrical properties and use in several industrial fields. We explain how different photovoltaic panels may be characterized by undergraduate students at university using simple methods to retrieve their electrical properties (power, current and voltage) and compare these values…

  4. Theoretical Characterization of Enclosures

    Czech Academy of Sciences Publication Activity Database

    Rohn, Jiří

    2016-01-01

    Roč. 21, October (2016), s. 140-145 ISSN 1573-1340 Institutional support: RVO:67985807 Keywords : interval linear equations * solution set * enclosure * component * characterization Subject RIV: BA - General Mathematics http://interval.louisiana.edu/reliable-computing-journal/volume-21/reliable-computing-21-pp-140-145.pdf

  5. Electro-Optical Characterization

    Energy Technology Data Exchange (ETDEWEB)

    2006-06-01

    In the Electro-Optical Characterization group, within the National Center for Photovoltaic's Measurements and Characterization Division, we use various electrical and optical experimental techniques to relate photovoltaic device performance to the methods and materials used to produce them. The types of information obtained by these techniques range from small-scale atomic-bonding information to large-scale macroscopic quantities such as optical constants and electron-transport properties. Accurate and timely measurement of the electro-optical properties as a function of device processing provides researchers and manufacturers with the knowledge needed to troubleshoot problems and develop the knowledge base necessary for reducing cost, maximizing efficiency, improving reliability, and enhancing manufacturability. We work collaboratively with you to solve materials- and device-related R&D problems. This sheet summarizes our primary techniques and capabilities.

  6. Capacitive skin characterization

    Science.gov (United States)

    McConnell, Robert; Manzo, Michael

    1992-10-01

    NASA is currently involved in research that utilizes a capacitive sensor that is used for proximity detection of objects. This sensor is sensitive to conductive and dielectric materials including metal objects and humans. The range of the sensor has been found to be about twelve inches. It is the goal of this research project to further characterize the sensor so that it can be tailored to specific requirements. The characterization of the sensor should be with respect to shield size, sensor size, object size, and object distance. The method of finite elements to calculate the capacitance of the sensor while varying different parameters was used. Each of the parameters was varied in turn, often by selecting data points from different runs. The plotted results are shown and an apparent functionality developed for each.

  7. Signal integrity characterization techniques

    CERN Document Server

    Bogatin, Eric

    2009-01-01

    "Signal Integrity Characterization Techniques" addresses the gap between traditional digital and microwave curricula all while focusing on a practical and intuitive understanding of signal integrity effects within the data transmission channel. High-speed interconnects such as connectors, PCBs, cables, IC packages, and backplanes are critical elements of differential channels that must be designed using today's most powerful analysis and characterization tools.Both measurements and simulation must be done on the device under test, and both activities must yield data that correlates with each other. Most of this book focuses on real-world applications of signal integrity measurements - from backplane for design challenges to error correction techniques to jitter measurement technologies. The authors' approach wisely addresses some of these new high-speed technologies, and it also provides valuable insight into its future direction and will teach the reader valuable lessons on the industry.

  8. A Characterization of Polynomials

    DEFF Research Database (Denmark)

    Andersen, Kurt Munk

    1996-01-01

    Given the problem:which functions f(x) are characterized by a relation of the form:f[x1,x2,...,xn]=h(x1+x2+...+xn), where n>1 and h(x) is a given function? Here f[x1,x2,...,xn] denotes the divided difference on n points x1,x2,...,xn of the function f(x).The answer is: f(x) is a polynomial of degr...

  9. Characterization of quantum logics

    International Nuclear Information System (INIS)

    Lahti, P.J.

    1980-01-01

    The quantum logic approach to axiomatic quantum mechanics is used to analyze the conceptual foundations of the traditional quantum theory. The universal quantum of action h>0 is incorporated into the theory by introducing the uncertainty principle, the complementarity principle, and the superposition principle into the framework. A characterization of those quantum logics (L,S) which may provide quantum descriptions is then given. (author)

  10. Probabilistic Logical Characterization

    DEFF Research Database (Denmark)

    Hermanns, Holger; Parma, Augusto; Segala, Roberto

    2011-01-01

    Probabilistic automata exhibit both probabilistic and non-deterministic choice. They are therefore a powerful semantic foundation for modeling concurrent systems with random phenomena arising in many applications ranging from artificial intelligence, security, systems biology to performance...... modeling. Several variations of bisimulation and simulation relations have proved to be useful as means to abstract and compare different automata. This paper develops a taxonomy of logical characterizations of these relations on image-finite and image-infinite probabilistic automata....

  11. On Characterizing Particle Shape

    Science.gov (United States)

    Ennis, Bryan J.; Rickman, Douglas; Rollins, A. Brent; Ennis, Brandon

    2014-01-01

    It is well known that particle shape affects flow characteristics of granular materials, as well as a variety of other solids processing issues such as compaction, rheology, filtration and other two-phase flow problems. The impact of shape crosses many diverse and commercially important applications, including pharmaceuticals, civil engineering, metallurgy, health, and food processing. Two applications studied here include the dry solids flow of lunar simulants (e.g. JSC-1, NU-LHT-2M, OB-1), and the flow properties of wet concrete, including final compressive strength. A multi-dimensional generalized, engineering method to quantitatively characterize particle shapes has been developed, applicable to both single particle orientation and multi-particle assemblies. The two-dimension, three dimension inversion problem is also treated, and the application of these methods to DEM model particles will be discussed. In the case of lunar simulants, flow properties of six lunar simulants have been measured, and the impact of particle shape on flowability - as characterized by the shape method developed here -- is discussed, especially in the context of three simulants of similar size range. In the context of concrete processing, concrete construction is a major contributor to greenhouse gas production, of which the major contributor is cement binding loading. Any optimization in concrete rheology and packing that can reduce cement loading and improve strength loading can also reduce currently required construction safety factors. The characterization approach here is also demonstrated for the impact of rock aggregate shape on concrete slump rheology and dry compressive strength.

  12. Characterization of shocked beryllium

    Science.gov (United States)

    Cady, Carl; Brown, Eric; Gray, George; Adams, Chris; Hull, Lawrence; Wynn, Thomas; Prime, Michael; Cooley, James; Bronkhorst, Curt; Addessio, Frank

    2013-06-01

    Explosively driven arrested beryllium experiments were performed with post mortem characterization to evaluate the microstructure and failure behaviors. The test samples were encapsulated in an aluminum assembly that was large relative to the sample, and the assembly features both axial and radial momentum traps. The sample carrier was inserted from the explosively loaded end and has features to lock the carrier to the surrounding cylinder using the induced plastic flow. Calculations with Lagrangian codes showed that the tensile stresses experienced by the Be sample were below the spall stress. Metallographic characterization of the arrested Be showed radial cracks present in the samples may have been caused by bending moments. Fractography showed the fractures propagated from the side of the sample closest to the explosives, the side with the highest tensile stress. There was evidence that the fractures may have propagated from the circumferential crack outward and downward radially. The EBSD results were the most informative of the characterization techniques used. EBSD provides information regarding texture, residual strain, and twinning. There was clear evidence of grain rotation as evidenced by the pole figures, the inverse pole figures and the Kernel Average Misorientation figures.

  13. Hypervelocity microparticle characterization

    Science.gov (United States)

    Idzorek, George C.

    1996-10-01

    To protect spacecraft from orbital debris requires a basic understanding of the processes involved in hypervelocity impacts and characterization of detectors to measure the space environment. Both require a source of well characterized hypervelocity particles. Electrostatic acceleration of charged microspheres provides such a source. Techniques refined at the Los Alamos National Laboratory provided information on hypervelocity impacts of particles of known mass and velocity ranging from 20 - 1000 nm diameter and 1 - 100 km/s. A Van De Graaff generator operating at 6 million volts was used to accelerate individual carbonyl iron microspheres produced by a specially designed particle source. Standard electrostatic lenses and steering were used to control the particle's flight path. Charge sensitive pickoff tubes measured the particle charge and velocity in-flight without disturbing the particle. This information coupled with the measured Van De Graaff terminal voltage allowed calculation of the particle energy, mass, momentum, and using an assumed density the size. Particles with the desired parameters were then electrostatically directed to a target chamber. Targets used in our experiments included cratering and foil puncture targets, microphone momentum enhancement detectors, triboluminescent detectors, and 'splash' charge detectors. In addition the system has been used to rapidly characterize size distributions of conductive plastic particles and potentially provide a method of easily sorting microscopic particles by size.

  14. Characterizing Black Hole Mergers

    Science.gov (United States)

    Baker, John; Boggs, William Darian; Kelly, Bernard

    2010-01-01

    Binary black hole mergers are a promising source of gravitational waves for interferometric gravitational wave detectors. Recent advances in numerical relativity have revealed the predictions of General Relativity for the strong burst of radiation generated in the final moments of binary coalescence. We explore features in the merger radiation which characterize the final moments of merger and ringdown. Interpreting the waveforms in terms of an rotating implicit radiation source allows a unified phenomenological description of the system from inspiral through ringdown. Common features in the waveforms allow quantitative description of the merger signal which may provide insights for observations large-mass black hole binaries.

  15. Characterization of Pixel Sensors

    CERN Document Server

    Oliveira, Felipe Ferraz

    2017-01-01

    It was commissioned at CERN ATLAS pixel group a fluorescence setup for characterization of pixel sensors. The idea is to measure the energies of different targets to calibrate your sensor. It was measured four matrices (80, 95, 98 and 106) of the Investigator1 sensor with different deep PW using copper, iron and titanium as target materials. The matrix 80 has a higher gain (0.065 ± 0.002) and matrix 106 has a better energy resolution (0.05 ± 0.04). The noise of the setup is around 3.6 mV .

  16. Characterization of clay minerals

    International Nuclear Information System (INIS)

    Diaz N, C.; Olguin, M.T.; Solache R, M.; Alarcon H, T.; Aguilar E, A.

    2002-01-01

    The natural clays are the more abundant minerals on the crust. They are used for making diverse industrial products. Due to the adsorption and ion exchange properties of these, a great interest for developing research directed toward the use of natural clays for the waste water treatment has been aroused. As part of such researches it is very important to carry out previously the characterization of the interest materials. In this work the results of the mineral and elemental chemical composition are presented as well as the morphological characteristics of clay minerals from different regions of the Mexican Republic. (Author)

  17. Characterization of solar cells

    Energy Technology Data Exchange (ETDEWEB)

    Haerkoenen, J.; Tuominen, E.; Nybergh, K.; Ezer, Y.; Yli-Koski, M.; Sinkkonen, J. [Helsinki Univ. of Technology, Otaniemi (Finland). Dept. of Electrical and Communications Engineering

    1998-10-01

    Photovoltaic research in the Electron Physics Laboratory started in 1993, when laboratory joined the national TEKES/NEMO 2 research program. Since the beginning of the project, characterization as well as experimentally orientated development of the fabrication process of the solar cells were carried out parallery. The process development research started by the initiatives of the Finnish industry. At the moment a large amount of the laboratory personnel works on solar cell research and the financing comes mainly from external projects. The funding for the research has come from TEKES, Ministry of Education, Finnish Academy, GETA graduate school, special equipment grants of the university, and from the laboratory

  18. Network Characterization Service (NCS)

    Energy Technology Data Exchange (ETDEWEB)

    Jin, Guojun [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Yang, George [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Crowley, Brian [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Agarwal, Deborah [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)

    2001-06-06

    Distributed applications require information to effectively utilize the network. Some of the information they require is the current and maximum bandwidth, current and minimum latency, bottlenecks, burst frequency, and congestion extent. This type of information allows applications to determine parameters like optimal TCP buffer size. In this paper, we present a cooperative information-gathering tool called the network characterization service (NCS). NCS runs in user space and is used to acquire network information. Its protocol is designed for scalable and distributed deployment, similar to DNS. Its algorithms provide efficient, speedy and accurate detection of bottlenecks, especially dynamic bottlenecks. On current and future networks, dynamic bottlenecks do and will affect network performance dramatically.

  19. Semiconductor characterization for optoelectronics

    Energy Technology Data Exchange (ETDEWEB)

    Miner, C.J. [Bell Northern Research Ltd., Ottawa, ON (Canada)

    1996-03-01

    Scanning reflectance spectroscopy, scanning photoluminescence, and double crystal x-ray diffraction mapping are all specialized non-destructive characterization tools which monitor the advanced materials used in the development of high speed optoelectronics. Each technology was described and their application in the assessment of III-V semiconductor composition, layer thickness and defect density was demonstrated. The new techniques have been optimized for speed, to make high spatial resolution mapping practical. Since the tests are non-destructive, frequent monitoring is possible. 11 refs., 7 figs.

  20. Characterizing Genuine Multilevel Entanglement

    Science.gov (United States)

    Kraft, Tristan; Ritz, Christina; Brunner, Nicolas; Huber, Marcus; Gühne, Otfried

    2018-02-01

    Entanglement of high-dimensional quantum systems has become increasingly important for quantum communication and experimental tests of nonlocality. However, many effects of high-dimensional entanglement can be simulated by using multiple copies of low-dimensional systems. We present a general theory to characterize those high-dimensional quantum states for which the correlations cannot simply be simulated by low-dimensional systems. Our approach leads to general criteria for detecting multilevel entanglement in multiparticle quantum states, which can be used to verify these phenomena experimentally.

  1. JANUS characterization report

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1996-07-01

    The JANUS Reactor was operated from 1965 to 1992. All of the fuel was removed and shipped offsite in 1993. To provide information for use in finalizing the planning for the decommissioning of the reactor, the Health Physics Section of Argonne National Laboratory performed a characterization of the facility in January and February 1996. The characterization included measurements for radioactivity, hazardous materials, lead in wall paint, and asbestos. Measurements and smear samples for surface contamination were collected from every wall, ceiling and floor of the facility. Samples to determine activity concentrations were collected from vertical and horizontal corings into the reactor shield and foundation, and from coring into walls of the high dose and low dose rooms. Soil samples were collected outdoors from two drill holes, one south and one north of the JANUS exhaust stack. The predominant radionuclides detected were {sup 60}Co, {sup 152}Eu, and {sup 154}Eu. The highest exposure rate was 175 mR/h at the center of the reactor core. No hazardous materials were found in pits or sumps. There are 20 identified areas with asbestos and 7 objects with lead based paint.

  2. JANUS characterization report

    International Nuclear Information System (INIS)

    1996-07-01

    The JANUS Reactor was operated from 1965 to 1992. All of the fuel was removed and shipped offsite in 1993. To provide information for use in finalizing the planning for the decommissioning of the reactor, the Health Physics Section of Argonne National Laboratory performed a characterization of the facility in January and February 1996. The characterization included measurements for radioactivity, hazardous materials, lead in wall paint, and asbestos. Measurements and smear samples for surface contamination were collected from every wall, ceiling and floor of the facility. Samples to determine activity concentrations were collected from vertical and horizontal corings into the reactor shield and foundation, and from coring into walls of the high dose and low dose rooms. Soil samples were collected outdoors from two drill holes, one south and one north of the JANUS exhaust stack. The predominant radionuclides detected were 60 Co, 152 Eu, and 154 Eu. The highest exposure rate was 175 mR/h at the center of the reactor core. No hazardous materials were found in pits or sumps. There are 20 identified areas with asbestos and 7 objects with lead based paint

  3. Carbon Characterization Laboratory Report

    Energy Technology Data Exchange (ETDEWEB)

    David Swank; William Windes; D.C. Haggard; David Rohrbaugh; Karen Moore

    2009-03-01

    The newly completed Idaho National Laboratory (INL) Carbon Characterization Laboratory (CCL) is located in Lab-C20 of the Idaho National Laboratory Research Center. This laboratory was established under the Next Generation Nuclear Plant (NGNP) Project to support graphite research and development activities. The CCL is designed to characterize and test carbon-based materials such as graphite, carbon-carbon composites, and silicon-carbide composite materials. The laboratory is fully prepared to measure material properties for nonirradiated carbon-based materials. Plans to establish the laboratory as a radiological facility within the next year are definitive. This laboratory will be modified to accommodate irradiated materials, after which it can be used to perform material property measurements on both irradiated and nonirradiated carbon-based material. Instruments, fixtures, and methods are in place for preirradiation measurements of bulk density, thermal diffusivity, coefficient of thermal expansion, elastic modulus, Young’s modulus, Shear modulus, Poisson ratio, and electrical resistivity. The measurement protocol consists of functional validation, calibration, and automated data acquisition.

  4. FRACTURING FLUID CHARACTERIZATION FACILITY

    Energy Technology Data Exchange (ETDEWEB)

    Subhash Shah

    2000-08-01

    Hydraulic fracturing technology has been successfully applied for well stimulation of low and high permeability reservoirs for numerous years. Treatment optimization and improved economics have always been the key to the success and it is more so when the reservoirs under consideration are marginal. Fluids are widely used for the stimulation of wells. The Fracturing Fluid Characterization Facility (FFCF) has been established to provide the accurate prediction of the behavior of complex fracturing fluids under downhole conditions. The primary focus of the facility is to provide valuable insight into the various mechanisms that govern the flow of fracturing fluids and slurries through hydraulically created fractures. During the time between September 30, 1992, and March 31, 2000, the research efforts were devoted to the areas of fluid rheology, proppant transport, proppant flowback, dynamic fluid loss, perforation pressure losses, and frictional pressure losses. In this regard, a unique above-the-ground fracture simulator was designed and constructed at the FFCF, labeled ''The High Pressure Simulator'' (HPS). The FFCF is now available to industry for characterizing and understanding the behavior of complex fluid systems. To better reflect and encompass the broad spectrum of the petroleum industry, the FFCF now operates under a new name of ''The Well Construction Technology Center'' (WCTC). This report documents the summary of the activities performed during 1992-2000 at the FFCF.

  5. Mound facility physical characterization

    Energy Technology Data Exchange (ETDEWEB)

    Tonne, W.R.; Alexander, B.M.; Cage, M.R.; Hase, E.H.; Schmidt, M.J.; Schneider, J.E.; Slusher, W.; Todd, J.E.

    1993-12-01

    The purpose of this report is to provide a baseline physical characterization of Mound`s facilities as of September 1993. The baseline characterizations are to be used in the development of long-term future use strategy development for the Mound site. This document describes the current missions and alternative future use scenarios for each building. Current mission descriptions cover facility capabilities, physical resources required to support operations, current safety envelope and current status of facilities. Future use scenarios identify potential alternative future uses, facility modifications required for likely use, facility modifications of other uses, changes to safety envelope for the likely use, cleanup criteria for each future use scenario, and disposition of surplus equipment. This Introductory Chapter includes an Executive Summary that contains narrative on the Functional Unit Material Condition, Current Facility Status, Listing of Buildings, Space Plans, Summary of Maintenance Program and Repair Backlog, Environmental Restoration, and Decontamination and Decommissioning Programs. Under Section B, Site Description, is a brief listing of the Site PS Development, as well as Current Utility Sources. Section C contains Site Assumptions. A Maintenance Program Overview, as well as Current Deficiencies, is contained within the Maintenance Program Chapter.

  6. TRU waste characterization chamber gloveboxes

    International Nuclear Information System (INIS)

    Duncan, D. S.

    1998-01-01

    Argonne National Laboratory-West (ANL-W) is participating in the Department of Energy's (DOE) National Transuranic Waste Program in support of the Waste Isolation Pilot Plant (WIPP). The Laboratory's support currently consists of intrusive characterization of a selected population of drums containing transuranic waste. This characterization is performed in a complex of alpha containment gloveboxes termed the Waste Characterization Gloveboxes. Made up of the Waste Characterization Chamber, Sample Preparation Glovebox, and the Equipment Repair Glovebox, they were designed as a small production characterization facility for support of the Idaho National Engineering and Environmental Laboratory (INEEL). This paper presents salient features of these gloveboxes

  7. Molybdenum Tube Characterization report

    Energy Technology Data Exchange (ETDEWEB)

    Beaux II, Miles Frank [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Usov, Igor Olegovich [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-02-07

    Chemical vapor deposition (CVD) techniques have been utilized to produce free-standing molybdenum tubes with the end goal of nuclear fuel clad applications. In order to produce tubes with properties desirable for this application, deposition rates were lowered requiring long deposition durations on the order of 50 hours. Standard CVD methods as well as fluidized-bed CVD (FBCVD) methods were applied towards these objectives. Characterization of the tubes produced in this manner revealed material suitable for fuel clad applications, but lacking necessary uniformity across the length of the tubes. The production of freestanding Mo tubes that possess the desired properties across their entire length represents an engineering challenge that can be overcome in a next iteration of the deposition system.

  8. EIGER characterization results

    International Nuclear Information System (INIS)

    Dinapoli, Roberto; Bergamaschi, Anna; Greiffenberg, Dominic; Henrich, Beat; Horisberger, Roland; Johnson, Ian; Mozzanica, Aldo; Radicci, Valeria; Schmitt, Bernd; Shi, Xintian; Tinti, Gemma

    2013-01-01

    Characterization and performance measurements have been done on several EIGER detector systems, produced with chips coming from two different lots, both with a lab X-ray source and at the Swiss Light Source (SLS). Results on the detector calibration, electronic noise, threshold dispersion, minimum achievable energy threshold, maximum detectable incoming photon flux and maximum frame rate are presented. An EIGER module is constructed from a ∼4×8cm 2 monolithic silicon sensor bump-bonded to 2 ×4 readout chips and contains 0.5 Mpixel. The first EIGER 500 K systems have been produced and images taken with these detectors are shown. Modules can be tiled together to form large area detectors; both a 9 Mpixel and a 16 Mpixel systems are at present under development for the coherent small angle X-ray scattering and protein crystallography beamlines of the SLS

  9. EIGER characterization results

    Energy Technology Data Exchange (ETDEWEB)

    Dinapoli, Roberto, E-mail: roberto.dinapoli@psi.ch [Paul Scherrer Institut, 5232 Villigen PSI (Switzerland); Bergamaschi, Anna; Greiffenberg, Dominic; Henrich, Beat; Horisberger, Roland; Johnson, Ian; Mozzanica, Aldo [Paul Scherrer Institut, 5232 Villigen PSI (Switzerland); Radicci, Valeria [Paul Scherrer Institut, 5232 Villigen PSI (Switzerland); ESRF, 6 Rue Horowitz, 38043 Grenoble (France); Schmitt, Bernd; Shi, Xintian [Paul Scherrer Institut, 5232 Villigen PSI (Switzerland); Tinti, Gemma [Paul Scherrer Institut, 5232 Villigen PSI (Switzerland); ESRF, 6 Rue Horowitz, 38043 Grenoble (France)

    2013-12-11

    Characterization and performance measurements have been done on several EIGER detector systems, produced with chips coming from two different lots, both with a lab X-ray source and at the Swiss Light Source (SLS). Results on the detector calibration, electronic noise, threshold dispersion, minimum achievable energy threshold, maximum detectable incoming photon flux and maximum frame rate are presented. An EIGER module is constructed from a ∼4×8cm{sup 2} monolithic silicon sensor bump-bonded to 2 ×4 readout chips and contains 0.5 Mpixel. The first EIGER 500 K systems have been produced and images taken with these detectors are shown. Modules can be tiled together to form large area detectors; both a 9 Mpixel and a 16 Mpixel systems are at present under development for the coherent small angle X-ray scattering and protein crystallography beamlines of the SLS.

  10. Characterization of graphene membranes

    Science.gov (United States)

    O'Hern, Sean; Lee, Jongho; Jain, Tarun; Karnik, Rohit; Idrobo, Juan; Laoui, Tahar; Atieh, Motaz

    2011-11-01

    Graphene, which exhibits very high breaking strength, atomistic thickness, and the ability to maintain stable nanometer-scale pores, has the potential to be a superior membrane material in both liquid- and gas-phase separation processes. We have recently demonstrated high-quality transfer of ~1 cm2 LPCVD graphene from copper foil to 200 nm polycarbonate track etch membranes with less than 0.3% of the area constituting holes or tears in the graphene, which is essential for characterizing transport through graphene. Through gallium ion bombardment we have introduced nanometer-scale pores in the transferred graphene and will report on the molecular and ionic transport through these membranes. Funded by the Center for Clean Energy and Water at MIT and KFUPM.

  11. Characterization of particulate amines

    International Nuclear Information System (INIS)

    Gundel, L.A.; Chang, S.G.; Clemenson, M.S.; Markowitz, S.S.; Novakov, T.

    1979-01-01

    The reduced nitrogen compounds associated with ambient particulate matter are chemically characterized by means of ESCA and proton activation analysis. Ambient particulate samples collected on silver filters in Berkeley, California were washed with water and organic solvents, and ESCA and proton activation analysis were performed in order to determine the composition of various nitrogen compounds and the total nitrogen content. It is found that 85% of the amines originally present in ambient particulate matter can be removed by water extraction, whereas the ammonium and nitrate are completely removed. An observed increase in ammonium ion in the extract, compared with its concentration in the original sample, coupled with the commensurate decrease in amine concentration, is attributed to the hydrolysis of amide groups, which may cause analytical methods based on extraction to yield erroneous results

  12. Characterization of dielectric materials

    Energy Technology Data Exchange (ETDEWEB)

    King, Danny J.; Babinec, Susan; Hagans, Patrick L.; Maxey, Lonnie C.; Payzant, Edward A.; Daniel, Claus; Sabau, Adrian S.; Dinwiddie, Ralph B.; Armstrong, Beth L.; Howe, Jane Y.; Wood, III, David L.; Nembhard, Nicole S.

    2017-06-27

    A system and a method for characterizing a dielectric material are provided. The system and method generally include applying an excitation signal to electrodes on opposing sides of the dielectric material to evaluate a property of the dielectric material. The method can further include measuring the capacitive impedance across the dielectric material, and determining a variation in the capacitive impedance with respect to either or both of a time domain and a frequency domain. The measured property can include pore size and surface imperfections. The method can still further include modifying a processing parameter as the dielectric material is formed in response to the detected variations in the capacitive impedance, which can correspond to a non-uniformity in the dielectric material.

  13. Radiation characterization summary :

    Energy Technology Data Exchange (ETDEWEB)

    Parma, Edward J.,; Quirk, Thomas J.; Lippert, Lance L.; Griffin, Patrick J; Naranjo, Gerald E.; Luker, Spencer Michael

    2013-04-01

    This document presents the facility-recommended characterization of the neutron, prompt gamma-ray, and delayed gamma-ray radiation fields in the Annular Core Research Reactor (ACRR) for the 44-inch-long lead-boron bucket in the central cavity on the 32-inch pedestal at the core centerline. The designation for this environment is ACRR-LB44-CC-32-cl. The neutron, prompt gamma-ray, and delayed gamma-ray energy spectra are presented as well as radial and axial neutron and gamma-ray flux profiles within the experiment area of the bucket. Recommended constants are given to facilitate the conversion of various dosimetry readings into radiation metrics desired by experimenters. Representative pulse and steady-state operations are presented with conversion examples.

  14. Photoelectronic characterization of heterointerfaces.

    Energy Technology Data Exchange (ETDEWEB)

    Brumbach, Michael Todd

    2012-02-01

    In many devices such as solar cells, light emitting diodes, transistors, etc., the performance relies on the electronic structure at interfaces between materials within the device. The objective of this work was to perform robust characterization of hybrid (organic/inorganic) interfaces by tailoring the interfacial region for photoelectron spectroscopy. Self-assembled monolayers (SAM) were utilized to induce dipoles of various magnitudes at the interface. Additionally, SAMs of molecules with varying dipolar characteristics were mixed into spatially organized structures to systematically vary the apparent work function. Polymer thin films were characterized by depositing films of varying thicknesses on numerous substrates with and without interfacial modifications. Hard X-ray photoelectron spectroscopy (HAXPES) was performed to evaluate a buried interface between indium tin oxide (ITO), treated under various conditions, and poly(3-hexylthiophene) (P3HT). Conducting polymer films were found to be sufficiently conducting such that no significant charge redistribution in the polymer films was observed. Consequently, a further departure from uniform substrates was taken whereby electrically disconnected regions of the substrate presented ideally insulating interfacial contacts. In order to accomplish this novel strategy, interdigitated electrodes were used as the substrate. Conducting fingers of one half of the electrodes were electrically grounded while the other set of electrodes were electronically floating. This allowed for the evaluation of substrate charging on photoelectron spectra (SCOPES) in the presence of overlying semiconducting thin films. Such an experiment has never before been reported. This concept was developed out of the previous experiments on interfacial modification and thin film depositions and presents new opportunities for understanding chemical and electronic changes in a multitude of materials and interfaces.

  15. Mixed waste characterization reference document

    International Nuclear Information System (INIS)

    1997-09-01

    Waste characterization and monitoring are major activities in the management of waste from generation through storage and treatment to disposal. Adequate waste characterization is necessary to ensure safe storage, selection of appropriate and effective treatment, and adherence to disposal standards. For some wastes characterization objectives can be difficult and costly to achieve. The purpose of this document is to evaluate costs of characterizing one such waste type, mixed (hazardous and radioactive) waste. For the purpose of this document, waste characterization includes treatment system monitoring, where monitoring is a supplement or substitute for waste characterization. This document establishes a cost baseline for mixed waste characterization and treatment system monitoring requirements from which to evaluate alternatives. The cost baseline established as part of this work includes costs for a thermal treatment technology (i.e., a rotary kiln incinerator), a nonthermal treatment process (i.e., waste sorting, macronencapsulation, and catalytic wet oxidation), and no treatment (i.e., disposal of waste at the Waste Isolation Pilot Plant (WIPP)). The analysis of improvement over the baseline includes assessment of promising areas for technology development in front-end waste characterization, process equipment, off gas controls, and monitoring. Based on this assessment, an ideal characterization and monitoring configuration is described that minimizes costs and optimizes resources required for waste characterization

  16. Mixed waste characterization reference document

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1997-09-01

    Waste characterization and monitoring are major activities in the management of waste from generation through storage and treatment to disposal. Adequate waste characterization is necessary to ensure safe storage, selection of appropriate and effective treatment, and adherence to disposal standards. For some wastes characterization objectives can be difficult and costly to achieve. The purpose of this document is to evaluate costs of characterizing one such waste type, mixed (hazardous and radioactive) waste. For the purpose of this document, waste characterization includes treatment system monitoring, where monitoring is a supplement or substitute for waste characterization. This document establishes a cost baseline for mixed waste characterization and treatment system monitoring requirements from which to evaluate alternatives. The cost baseline established as part of this work includes costs for a thermal treatment technology (i.e., a rotary kiln incinerator), a nonthermal treatment process (i.e., waste sorting, macronencapsulation, and catalytic wet oxidation), and no treatment (i.e., disposal of waste at the Waste Isolation Pilot Plant (WIPP)). The analysis of improvement over the baseline includes assessment of promising areas for technology development in front-end waste characterization, process equipment, off gas controls, and monitoring. Based on this assessment, an ideal characterization and monitoring configuration is described that minimizes costs and optimizes resources required for waste characterization.

  17. Characterization of organic thin films

    CERN Document Server

    Ulman, Abraham; Evans, Charles A

    2009-01-01

    Thin films based upon organic materials are at the heart of much of the revolution in modern technology, from advanced electronics, to optics to sensors to biomedical engineering. This volume in the Materials Characterization series introduces the major common types of analysis used in characterizing of thin films and the various appropriate characterization technologies for each. Materials such as Langmuir-Blodgett films and self-assembled monolayers are first introduced, followed by analysis of surface properties and the various characterization technologies used for such. Readers will find detailed information on: -Various spectroscopic approaches to characterization of organic thin films, including infrared spectroscopy and Raman spectroscopy -X-Ray diffraction techniques, High Resolution EELS studies, and X-Ray Photoelectron Spectroscopy -Concise Summaries of major characterization technologies for organic thin films, including Auger Electron Spectroscopy, Dynamic Secondary Ion Mass Spectrometry, and Tra...

  18. Risk characterization: principles and practice.

    Science.gov (United States)

    Williams, Pamela R D; Paustenbach, Dennis J

    2002-01-01

    In the field of risk assessment, characterizing the nature and magnitude of human health or environmental risks is arguably the most important step in the analytical process. In this step, data on the dose-response relationship of an agent are integrated with estimates of the degree of exposure in a population to characterize the likelihood and severity of risk. Although the purpose of risk characterizations is to make sense of the available data and describe what they mean to a broad audience, this step is often given insufficient attention in health risk evaluations. Too often, characterizations fail to interpret or summarize risk information in a meaningful way, or they present single numerical estimates of risk without an adequate discussion of the uncertainties inherent in key exposure parameters or the dose-response assessment, model assumptions, or analytical limitations. Consequently, many users of risk information have misinterpreted the findings of a risk assessment or have false impressions about the degree of accuracy (or the confidence of the scientist) in reported risk estimates. In this article we collected and integrated the published literature on conducting and reporting risk characterizations to provide a broad, yet comprehensive, analysis of the risk characterization process as practiced in the United States and some other countries. Specifically, the following eight topics are addressed: (1) objective of risk characterization, (2) guidance documents on risk characterization, (3) key components of risk characterizations, (4) toxicity criteria for evaluating health risks, (5) descriptors used to characterize health risks, (6) methods for quantifying human health risks, (7) key uncertainties in risk characterizations, and (8) the risk decision-making process. A brief discussion is also provided on international aspects of risk characterization. A number of examples are presented that illustrate key concepts, and citations are provided for

  19. 105-C Facility characterization plan

    International Nuclear Information System (INIS)

    Miller, R.L.

    1997-01-01

    This facility characterization plan is a site-specific document that describes how quantification and qualification of the radiological sources and the radioactive contamination in the 105-C Building will be accomplished. Characterization of hazardous materials will be addressed in a separate plan. This plan was developed from review of video tapes, photographs, and records. The purpose of this characterization plan is to provide an efficient and cost-effective method for determining the distribution of radioactive contamination at the 105-C Facility

  20. Characterization equipment essential drawing plan

    International Nuclear Information System (INIS)

    WILSON, G.W.

    1999-01-01

    The purpose of this document is to list the Characterization equipment drawings that are classified as Essential Drawings. Essential Drawings: Are those drawings identified by the facility staff as necessary to directly support the safe operation of the facility or equipment (HNF 1997a). The Characterization equipment drawings identified in this report are deemed essential drawings as defined in HNF-PRO-242, Engineering Drawing Requirements (HNF 1997a). These drawings will be prepared, revised, and maintained per HNF-PRO-440, Engineering Document Change Control (HNF 1997b). All other Characterization equipment drawings not identified in this document will be considered Support drawings until the Characterization Equipment Drawing Evaluation Report is completed

  1. MOLECULAR STRUCTURE AND MATERIALS CHARACTERIZATION

    Science.gov (United States)

    monocarboxylic acids and organosulfur compounds; solid state mass spectrometric studies; and the characterization of polyurethane elastomers with special reference to those used as binders for solid propellants.

  2. Nanometer Characterization/Manipulation Facility

    Data.gov (United States)

    Federal Laboratory Consortium — FUNCTION: Characterizes the nanometer scale of biological, chemical, physical, electronic, and mechanical properties of surfaces and thin films using scanning probe...

  3. Characterization of Hospital Residuals

    International Nuclear Information System (INIS)

    Blanco Meza, A.; Bonilla Jimenez, S.

    1997-01-01

    The main objective of this investigation is the characterization of the solid residuals. A description of the handling of the liquid and gassy waste generated in hospitals is also given, identifying the source where they originate. To achieve the proposed objective the work was divided in three stages: The first one was the planning and the coordination with each hospital center, in this way, to determine the schedule of gathering of the waste can be possible. In the second stage a fieldwork was made; it consisted in gathering the quantitative and qualitative information of the general state of the handling of residuals. In the third and last stage, the information previously obtained was organized to express the results as the production rate per day by bed, generation of solid residuals for sampled services, type of solid residuals and density of the same ones. With the obtained results, approaches are settled down to either determine design parameters for final disposition whether for incineration, trituration, sanitary filler or recycling of some materials, and storage politics of the solid residuals that allow to determine the gathering frequency. The study concludes that it is necessary to improve the conditions of the residuals handling in some aspects, to provide the cleaning personnel of the equipment for gathering disposition and of security, minimum to carry out this work efficiently, and to maintain a control of all the dangerous waste, like sharp or polluted materials. In this way, an appreciable reduction is guaranteed in the impact on the atmosphere. (Author) [es

  4. Characterization of acid tars

    Energy Technology Data Exchange (ETDEWEB)

    Leonard, Sunday A., E-mail: sunday.leonard@ucl.ac.uk [Department of Civil Environmental and Geomatic Engineering, University College London, Chadwick Building, Gower Street, London, WC1E 6BT (United Kingdom); Stegemann, Julia A. [Department of Civil Environmental and Geomatic Engineering, University College London, Chadwick Building, Gower Street, London, WC1E 6BT (United Kingdom); Roy, Amitava [J. Bennett Johnston, Sr., Centre for Advance Microstructures and Devices (CAMD), 6980 Jefferson Highway, Louisiana State University, Baton Rouge, LA, 70806 (United States)

    2010-03-15

    Acid tars from the processing of petroleum and petrochemicals using sulfuric acid were characterized by gas chromatography/mass spectrometry (GC/MS), inductively coupled plasma/optical emission spectrometry (ICP/OES), differential scanning calorimetry (DSC), Fourier transform infrared (FTIR) spectrometry, and scanning electron microscopy/energy dispersive X-ray (SEM/EDX) micro-analysis. Leaching of contaminants from the acid tars in 48 h batch tests with distilled water at a liquid-to-solid ratio 10:1 was also studied. GC/MS results show that the samples contained aliphatic hydrocarbons, cyclic hydrocarbons, up to 12 of the 16 USEPA priority polycyclic aromatic hydrocarbons (PAHs), and numerous other organic groups, including organic acids (sulfonic acids, carboxylic acids and aromatic acids), phenyl, nitrile, amide, furans, thiophenes, pyrroles, and phthalates, many of which are toxic. Metals analysis shows that Pb was present in significant concentration. DSC results show different transition peaks in the studied samples, demonstrating their complexity and variability. FTIR analysis further confirmed the presence of the organic groups detected by GC/MS. The SEM/EDX micro-analysis results provided insight on the surface characteristics of the samples and show that contaminants distribution was heterogeneous. The results provide useful data on the composition, complexity, and variability of acid tars; information which hitherto have been scarce in public domain.

  5. Plant Phenotype Characterization System

    Energy Technology Data Exchange (ETDEWEB)

    Daniel W McDonald; Ronald B Michaels

    2005-09-09

    This report is the final scientific report for the DOE Inventions and Innovations Project: Plant Phenotype Characterization System, DE-FG36-04GO14334. The period of performance was September 30, 2004 through July 15, 2005. The project objective is to demonstrate the viability of a new scientific instrument concept for the study of plant root systems. The root systems of plants are thought to be important in plant yield and thus important to DOE goals in renewable energy sources. The scientific study and understanding of plant root systems is hampered by the difficulty in observing root activity and the inadequacy of existing root study instrumentation options. We have demonstrated a high throughput, non-invasive, high resolution technique for visualizing plant root systems in-situ. Our approach is based upon low-energy x-ray radiography and the use of containers and substrates (artificial soil) which are virtually transparent to x-rays. The system allows us to germinate and grow plant specimens in our containers and substrates and to generate x-ray images of the developing root system over time. The same plant can be imaged at different times in its development. The system can be used for root studies in plant physiology, plant morphology, plant breeding, plant functional genomics and plant genotype screening.

  6. Characterizing European cultural landscapes

    DEFF Research Database (Denmark)

    Tieskens, Koen F.; Schulp, Catharina J E; Levers, Christian

    2017-01-01

    Almost all rural areas in Europe have been shaped or altered by humans and can be considered cultural landscapes, many of which now are considered to entail valuable cultural heritage. Current dynamics in land management have put cultural landscapes under a huge pressure of agricultural intensifi......Almost all rural areas in Europe have been shaped or altered by humans and can be considered cultural landscapes, many of which now are considered to entail valuable cultural heritage. Current dynamics in land management have put cultural landscapes under a huge pressure of agricultural...... intensification and land abandonment. To prevent the loss of cultural landscapes, knowledge on the location of different types of cultural landscapes is needed. In this paper, we present a characterization of European cultural landscapes based on the prevalence of three key dimensions of cultural landscapes......: landscape structure, management intensity, and value and meaning. We mapped these dimensions across Europe at a 1-km resolution by combining proxies on management intensity and landscape structure with new indicators such as social media usage and registered traditional food products. We integrated...

  7. Characterization of assembled MEMS

    Science.gov (United States)

    Jandric, Zoran; Randall, John N.; Saini, Rahul; Nolan, Michael; Skidmore, George

    2005-01-01

    Zyvex is developing a low-cost high-precision method for manufacturing MEMS-based three-dimensional structures/assemblies. The assembly process relies on compliant properties of the interconnecting components. The sockets and connectors are designed to benefit from their compliant nature by allowing the mechanical component to self-align, i.e. reposition themselves to their designed, stable position, independent of the initial placement of the part by the external robot. Thus, the self-aligning property guarantees the precision of the assembled structure to be very close to, or the same, as the precision of the lithography process itself. A three-dimensional (3D) structure is achieved by inserting the connectors into the sockets through the use of a passive end-effector. We have developed the automated, high-yield, assembly procedure which permits connectors to be picked up from any location within the same die, or a separate die. This general procedure allows for the possibility to assemble parts of dissimilar materials. We have built many 3D MEMS structures, including several 3D MEMS devices such as a scanning electron microscope (SEM) micro column, mass-spectrometer column, variable optical attenuator. For these 3D MEMS structures we characterize their mechanical strength through finite element simulation, dynamic properties by finite-element analysis and experimentally with UMECH"s MEMS motion analyzer (MMA), alignment accuracy by using an in-house developed dihedral angle measurement laser autocollimator, and impact properties by performing drop tests. The details of the experimental set-ups, the measurement procedures, and the experimental data are presented in this paper.

  8. Characterizing Decision Support Telemedicine Systems

    NARCIS (Netherlands)

    Nannings, B.; Abu-Hanna, A.

    2006-01-01

    OBJECTIVES: Decision Support Telemedicine Systems (DSTS) are at the intersection of two disciplines: tele-medicine and clinical decision support systems (CDSS). The objective of this paper is to provide a set of characterizing properties for DSTSs. This characterizing property set (CPS) can be used

  9. Characterizations of univariate continuous distributions

    CERN Document Server

    Ahsanullah, Mohammad

    2017-01-01

    Provides in an organized manner characterizations of univariate probability distributions with many new results published in this area since the 1978 work of Golambos & Kotz "Characterizations of Probability Distributions" (Springer), together with applications of the theory in model fitting and predictions.

  10. Characterization Of Robot Work Cell

    Science.gov (United States)

    Anderson, Ronald R.; Paternoster, Vincent Y.; Guthmiller, Wayne A.

    1990-01-01

    Iterative process of measurement and computation used to characterize work cell of robot, increasing accuracy of mathematical model of work cell. Characterization needed because model used in off-line programming (OLP) to compute paths to control motion of robot. Increases accuracies of model and paths.

  11. Protocol in NORM industries. Central thermal coal production; Protocolo de actuacion en industrial NORM. Centrales de produccion termica de carbon

    Energy Technology Data Exchange (ETDEWEB)

    Robles, B.; Mora, J. C.; Corbacho, J. A.; Baeza, A.; Cancio, D.

    2011-07-01

    This protocol arises from the execution of R and D project Study of the radiological impact of coal power plants on their environment, funded by the Nuclear Safety Council. Its main objective was to assess the radiological impact exerted on workers and their environments, the four coal-fired power more currently in Spain: As Pontes (A Coruna), Compostilla II (Leon ),Litoral (Almeria) and Andorra (Teruel). (Author)

  12. Electric power and thermal energy production using photovoltaic panels; Producao de eletricidade e energia termica usando paineis fotovoltaicos

    Energy Technology Data Exchange (ETDEWEB)

    Anon.

    2010-06-15

    Why should not be extracted the maximum of solar radiation, with the simultaneous obtention of electric power and thermal energy? This question has been the motivation of various projects which have in common the use of hybrid or refrigerated photovoltaic modules. They are closed panels, having circulating water, besides to refrigerate the photovoltaic cells, increasing the yield of the electricity conversion, and the water circulating being a source of thermal energy. (author)

  13. Thermal solar energy - application in industrial heat processes; Energia solar termica - aplicacion en procesos industriales de calor

    Energy Technology Data Exchange (ETDEWEB)

    Bonneschky, Alexis [Universidad Tecnica de Brandenburgo/Cottbus (Germany); Roth, Pedro; Cancino, Beatriz [Universidad Tecnica Federico Santa Maria, Valparaiso (Chile); Kanig, Thomas [Germany, (Georgia)

    2000-07-01

    The main objective of this paper is to show the use solar energy for water heating in industry, integrating the companies through some strategy that signifies a common purpose that benefits both of them. In this report a project made with two neighboring companies in the region of Branderburgo, Germany is presented, that mutually benefit with the solar energy installation, but which are independent as far as its intentions and capitals. The first company is the factory FK-Solartchnik Kleinkoschen that produces solar collectors for hot water and is interested in developing publicity in this sense, reason why it put at the disposition of the second industry the necessary area to install the solar collectors. The second company, is the FGT Glaswerk Kleinkoschen that produces high quality glass plates, but does not have facade available for the installation of any solar equipment. In this industry, for the manufacture of glass, hot water is used. The glass plates, already cut, go trough a process of washing and drying. The washing, requires a volume of 1 m{sup 3}/day of hot water, at 60 degrees Celsius and is made between 6:30 a.m. and 3:30 p.m. The water heating was carried out with two electrical heaters (around 12 kW each one). A solar equipment was designed that allows to diminish the energy losses in the accumulation in the hours following the process, where the water is warmed up, and additionally covers part of the requirements of the consumed water. This equipment has a collector with a surface of 27 m{sup 2}. With this system, plus the contribution made by the workers of the company, the water temperature for washing was diminished in 20 K, without affecting the product quality and in addition, the annual consumption of electrical energy of the company was reduced in 15,000 kWh, using the solar energy resources in about 50% of the total consumption. [Spanish] El objetivo principal de este trabajo es mostrar el uso de la energia solar para el calentamiento de agua en la industria, integrando a las empresas a traves de alguna estrategia que signifique una finalidad comun que beneficie a ambas. En este informe se presenta un proyecto realizado con dos empresas vecinas en la region de Branderburgo Alemania, que se benefician mutuamente por la instalacion de la energia solar, pero que son independientes en cuanto a sus propositos y capitales. La primera empresa es la fabrica FK-Solartchnik Kleinkoschen que produce colectores solares para agua caliente y le interesa desarrollar publicidad en este sentido, por lo que puso a disposicion de la segunda industria el area necesaria para instalar los colectores solares. La segunda empresa, es la FGT Glaswerk Kleinkoschen que produce planchas de vidrio de alta calidad, pero no cuenta con fachada disponible para la instalacion de ningun equipo solar. En esta industria, para la fabricacion del vidrio, se utiliza agua caliente. Las planchas de vidrio, ya cortadas, pasan a un proceso de lavado y secado. El lavado, requiere de un volumen de 1 m{sup 3}/dia agua caliente, a 600 grados Celsius y se realiza entre las 6:30 y las 15:30 h. El calentamiento del agua era efectuado con dos calentadores electricos (alrededor de 12 kW cada uno). Se diseno un equipo solar que permite disminuir las perdidas de energia en la acumulacion en las horas siguientes al proceso, donde se calienta el agua, y adicionalmente se cubre parte de los requerimientos del agua consumida. Este equipo tiene una superficie de colector de 27 m{sup 2}. Con este sistema, mas el aporte realizado por los trabajadores de la empresa, disminuyo la temperatura del agua de lavado en 20 K, sin afectar la calidad del producto y se redujo ademas el consumo anual de energia electrica de la empresa en 15,000 kWh, utilizando los recursos de la energia solar en un 50% del consumo total.

  14. Simulation of the fluctuations of hydraulic pressure in thermal power plants; Simulacion de golpe de ariete en centrales termicas

    Energy Technology Data Exchange (ETDEWEB)

    Calzada Mazeres, P. de la [INITEC (Spain)

    1995-07-01

    In this study the different equipments of the circulation waste system in thermal power plants are modellized (refrigeration water from the condenser). The purpose is to analyze the transient generated when the pump trip is produced at different shutting times of discharge valve. (Author)

  15. Thermal efficiency of low cost solar collectors - CSBC; Eficiencia termica de coletores solares de baixo custo - CSBC

    Energy Technology Data Exchange (ETDEWEB)

    Pereira, Renato C.; Shiota, Robson T.; Mello, Samuel F.; Assis Junior, Valdir; Bartoli, Julio R. [Universidade Estadual de Campinas (UNICAMP), SP (Brazil). Faculdade de Engenharia Quimica. Dept. de Tecnologia de Polimeros

    2006-07-01

    The thermal performance of a low cost flat panel solar collector was measured. This Low Cost Solar Collector is a novel concept for water heating using only thermoplastics materials, used on building: ceiling and tubes made of unplasticized PVC, but without transparent cover. The top side of the UPVC panel was black painted to be the solar radiation absorber surface. Prototypes were installed on two charity houses around Campinas and at the FEQ campus, being used without any trouble for one year. The thermal efficiency analysis followed ABNT NBR 10184 standard at the Green-Solar Laboratory, Brazilian Centre for Development of Solar Thermal Energy, PUC-Minas. It was measured a thermal efficiency of 67%, compared to the 75% usually found on conventional solar collectors made of copper tubes and with glass cover. (author)

  16. Typology of the Solar thermal facilities of low temperature; Tipologia de instalaciones solares termicas de baja temperatura

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2008-07-01

    The public interest by sustain ability and the governmental support are in the base of the great number of solar thermal collectors installed during the last years. In fact, the new 2006 Building Technical Code, Very responsible for this development on 2007, has provoked the appearance of new design instruments to guarantee in the collectors his energetic efficiency, his architectural integration, his durability and his maintenance. This article checks the different types of solar collectors of low temperate. (Author)

  17. Aumento da resistencia termica da borracha SIS atraves da adição de poli (oxido fenileno)

    OpenAIRE

    Anatoli Ivanov Junior

    2009-01-01

    Resumo: A utilização de borracha SIS (copolímero em bloco estireno/isopreno/estireno) em diversas aplicações tais como solados de sapatos, artefatos de vedação, adesivos com baixa resistência térmica (até 40º C). No entanto, neste trabalho apresentam -se os resultados obtidos com a incorporação de PPO (polioxidofenileno) a borracha SIS, o que resulta o aumento de resistência térmica da borracha, ampliando assim suas aplicações. Neste trabalho estudou-se a melhor condição em massa dos materiai...

  18. Thermal and hydraulic characteristics of the JEN-1 Reactor; Caracteristicas hidraulicas y termicas del Reactor JEN-1

    Energy Technology Data Exchange (ETDEWEB)

    Otra Otra, F.; Leira Rey, G.

    1971-07-01

    In this report an analysis is made of the thermal and hydraulic performances of the JEN-1 reactor operating steadily at 3 Mw of thermal power. The analysis is made separately for the core, main heat exchanger and cooling tower. A portion of the report is devoted to predict the performances of these three main components when and if the reactor was going to operate at a power higher than the maximum 3 Mw attainable today. Finally an study is made of the unsteady operation of the reactor, focusing the attention towards the pumping characteristics and the temperatures obtained in the fuel elements. Reference is made to several digital calculation programmes that nave been developed for such purpose. (Author) 21 refs.

  19. Notes for a procedure of certification of thermal solar facilities; Apuntes para un procedimiento de certificacion de instalaciones solares termicas

    Energy Technology Data Exchange (ETDEWEB)

    Prieto, J. I.; Garcia, D.

    2008-07-01

    A procedure to evaluate the quality of solar thermal installations is proposed, following some analogy to the Calificacion Energetica de Viviendas (C.E.V.) method. The steps required to develop the method are established, analysing with special detail the stage of design-based qualification. The proposed procedures of energy saving qualification, architectural qualification, and economical qualification, are justified. Moreover, the report suggests a list of previous data that must be provided and periodically updated by the Administration to guarantee both the objectivity and the transparency of the qualification procedure. The exposure of the method is complemented with numerical and graphical application to several case studies. (Author)

  20. Uruguayan tallow characterization

    Directory of Open Access Journals (Sweden)

    Cecilia Rodríguez

    2011-04-01

    Full Text Available Eatable tallow is the product  obtained fusing oily, from clean and  healthy tissues (included the fats of clippings, and from muscles or bones adherents of bovine animals (Bos tsurus,  lambs (Ovis aries in good conditions of health in the moment of its sacrifice and whose has been treated and therefore are considered suitable for the human consumption.To obtain fat from the raw, this material must surrender to a previous treatment that breaks the adipose cells, by  mechanical destruction, boiling or by treatment with alcáli. The easiest  way  consists of the mechanical disintegration (breakup under heat, using steam in direct or indirect form. This product can be obtained by one of the following : discontinuous merger, humid constant merger and  continues merger at low temperature. At present is used in the  cosmetic industry (production of soaps, for nutrition (raw material for margarine, ranching (for the manufacture of food concentrated for animals, for the self propelling industry (raw material for the production of biodiesel. The major purpose of this work is the tallow characterization from the determination of the following parameters :Moisture and Volatile Matter (g/100g of sample, Melting Point (1C, Free Acidity (g. Oleic acid /100g of sample, Colour (yellow and red and Insoluble Matter (g/100g.de shows of 15 samples of animal tallow from Uruguay, in order to provide useful information for the selection of the material. The Norm used as reference was the AOCS (American Oil Chemistry Society. With the obtained information it has been realized a statistical exploratory analysis. The preliminary results, due to the high variability of the studied factors, do not allow to establish with the current number of samples a  model who explains the above mentioned variability, neither at first, to reduce the quantity of factors to consider; in effect, the regression of the moisture against the rest of the factors determined the

  1. Characterizing Financial and Statistical Literacy

    DEFF Research Database (Denmark)

    Di Girolamo, Amalia; Harrison, Glenn W.; Lau, Morten

    We characterize the literacy of an individual in a domain by their elicited subjective belief distribution over the possible responses to a question posed in that domain. We consider literacy across several financial, economic and statistical domains. We find considerable demographic heterogeneity...... in the degree of literacy. We also characterize the degree of consistency within a sample about their knowledge, even when that knowledge is imperfect. We show how uncertainty aversion might be a normatively attractive behavior for individuals who have imperfect literacy. Finally, we discuss extensions of our...... approach to characterize financial capability, the consequences of non-literacy, social literacy, and the information content of hypothetical survey measures of literacy....

  2. 324 Building Baseline Radiological Characterization

    Energy Technology Data Exchange (ETDEWEB)

    R.J. Reeder, J.C. Cooper

    2010-06-24

    This report documents the analysis of radiological data collected as part of the characterization study performed in 1998. The study was performed to create a baseline of the radiological conditions in the 324 Building.

  3. Characterization of polyacrylonitrile ultrafiltration membranes

    NARCIS (Netherlands)

    Germic, J.; Germic, J.; Ebert, K.; Ebert, K.; Bouma, R.H.B.; Bouma, R.H.B.; Borneman, Zandrie; Mulder, M.H.V.; Strathmann, H.

    1997-01-01

    Various methods have been used to characterize ultrafiltration membranes, such as gas flux measurements, (field emission) scanning electron microscopy, permporometry and liquid-liquid displacement. Significant differences in the pore size distributions determined from permporometry and liquid-liquid

  4. Hanford site waste tank characterization

    International Nuclear Information System (INIS)

    De Lorenzo, D.S.; Simpson, B.C.

    1994-08-01

    This paper describes the on-going work in the characterization of the Hanford-Site high-level waste tanks. The waste in these tanks was produced as part of the nuclear weapons materials processing mission that occupied the Hanford Site for the first 40 years of its existence. Detailed and defensible characterization of the tank wastes is required to guide retrieval, pretreatment, and disposal technology development, to address waste stability and reactivity concerns, and to satisfy the compliance criteria for the various regulatory agencies overseeing activities at the Hanford Site. The resulting Tank Characterization Reports fulfill these needs, as well as satisfy the tank waste characterization milestones in the Hanford Federal Facility Agreement and Consent Order

  5. CHARACTERIZATION OF TRANSIENT PUFF EMISSIONS ...

    Science.gov (United States)

    Symposium Paper Transient puff emissions were characterized from burning carpet charges that were fed to a pilotscale rotary kiln combustor to assess the potential impact on emissions of using post-consumer carpet as an alternative fuel in cement kilns.

  6. Laser characterization of fine aggregate.

    Science.gov (United States)

    2012-12-01

    This report describes the results of a research effort to establish the feasibility of using a laser monitoring system to provide real-time data to characterize aggregate properties in a laboratory or field environment. This was accomplished by using...

  7. Hanford site waste tank characterization

    Energy Technology Data Exchange (ETDEWEB)

    De Lorenzo, D.S.; Simpson, B.C.

    1994-08-01

    This paper describes the on-going work in the characterization of the Hanford-Site high-level waste tanks. The waste in these tanks was produced as part of the nuclear weapons materials processing mission that occupied the Hanford Site for the first 40 years of its existence. Detailed and defensible characterization of the tank wastes is required to guide retrieval, pretreatment, and disposal technology development, to address waste stability and reactivity concerns, and to satisfy the compliance criteria for the various regulatory agencies overseeing activities at the Hanford Site. The resulting Tank Characterization Reports fulfill these needs, as well as satisfy the tank waste characterization milestones in the Hanford Federal Facility Agreement and Consent Order.

  8. CHARACTERIZING SITE HYDROLOGY (REGION 5)

    Science.gov (United States)

    Hydrogeology is the foundation of subsurface site characterization for evaluations of monitored natural attenuation (MNA). Three case studies are presented. Examples of the potentially detrimental effects of drilling additives on ground-water samples from monitoring wells are d...

  9. Magnetic Characterization of Organic Materials

    Science.gov (United States)

    2016-12-12

    AFRL-AFOSR-JP-TR-2017-0005 Magnetic Characterization of Organic Materials Dongho Kim YONSEI UNIVERSITY UNIVERSITY-INDUSTRY FOUNDATION Final Report 12...Final 3. DATES COVERED (From - To) 10 Sep 2015 to 09 Sep 2016 4. TITLE AND SUBTITLE Magnetic Characterization of Organic Materials 5a.  CONTRACT...DISTRIBUTION UNLIMITED: PB Public Release 13. SUPPLEMENTARY NOTES 14. ABSTRACT Organic materials show interesting phenomena called magnetic field effects (MFEs

  10. Dynamic Characterization of MEMS Scanners

    Directory of Open Access Journals (Sweden)

    Çağlar ATAMAN

    2009-09-01

    Full Text Available A simple yet precise optical characterization technique for beam scanning devices is proposed. The method uses a single photodetector to measure various dynamic characteristics of scanning devices, including frequency, scan angle, scan phase, and the mechanical quality factor, given that the scan waveform is known. A quantitative performance analysis and a set of experimental characterization results are presented. Experimentally 0.007 % scan angle measurement accuracy is demonstrated and it is shown that it can be improved.

  11. A PCP Characterization of AM

    OpenAIRE

    Drucker, Andrew

    2010-01-01

    We introduce a 2-round stochastic constraint-satisfaction problem, and show that its approximation version is complete for (the promise version of) the complexity class AM. This gives a `PCP characterization' of AM analogous to the PCP Theorem for NP. Similar characterizations have been given for higher levels of the Polynomial Hierarchy, and for PSPACE; however, we suggest that the result for AM might be of particular significance for attempts to derandomize this class. To test this notion, ...

  12. High Speed On-Wafer Characterization Laboratory

    Data.gov (United States)

    Federal Laboratory Consortium — At the High Speed On-Wafer Characterization Laboratory, researchers characterize and model devices operating at terahertz (THz) and millimeter-wave frequencies. The...

  13. SNF Site Characterization Data: C.Jarvis

    Data.gov (United States)

    National Aeronautics and Space Administration — Site characterization parameters (canopy density, litter components, soil characterization: color, moisture, components) for selected sites within the Superior...

  14. Characterization of Nonlinear Integrated Capacitors

    Directory of Open Access Journals (Sweden)

    Z. Kolka

    2008-12-01

    Full Text Available The paper deals with a modified CBCM (Charge-Based Capacitance Measurements method for nonlinear capacitance characterization. The method is characterized by high resolution although it is based on equipment found in any average laboratory. CBCM was originally developed for linear interconnect measurements. The proposed modification uses two DC swept sources to measure the whole nonlinear Q-v characteristic in both polarities without the necessity to switch the measured object. A test-chip implementing the method was designed and manufactured in the 0.35μm CMOS process. Verifica- tion against known capacitances proved the correctness and accuracy of the method. It was successfully used for MOSCAPs characterization.

  15. Design, construction and characterization of a rural solar furnace; Diseno, construccion y caracterizacion de un horno solar rural

    Energy Technology Data Exchange (ETDEWEB)

    Hernandez Luna, Gabriela

    2001-06-15

    This thesis presents the design, construction and characterization of a solar furnace, box type, for its use in rural communities in the inter-tropical zone. The work presented in this thesis departs from the opto-geometric design of a solar furnace, box type, proposed by an enthusiastic group of young students from the Centro de Investigacion de Energia (CIE) of the Universidad Nacional Autonoma de Mexico (UNAM). The contents of this thesis includes the systematization of the work previously made by these authors: the design and the optimization of geometry, the experimental evaluation of the same, as well as a theoretical model of the thermal behavior of the solar furnace based on a global balance of energy that assumes thermal states in cuasi-equilibrium of the internal components of the furnace. In this thesis a theoretical model of the solar concentration of energy by the reflectors of the furnace based on the model of Peres and Karsson (1993) is developed. The predictions of this model are satisfactorily compared with the experimental results of Jaramillo et al. (1999). Counting on the opto-geometric design of the furnace, the design is completed selecting the materials to be used in the different parts of the same, as well as defining constructive details. The material selected for the inner and outer boxes and the reflectors is stainless steel mirror finishing. Mineral wool is used As insulating mineral. The upper part of the furnace is protected by a glass that allows the entrance of the solar energy and diminishes the energy convective and radiation losses. For the thermal evaluation of the furnace an experimental methodology, based on the international procedures standardized for tests of furnaces and solar stoves is followed. Three tests for each one of the following operation conditions were performed: without load, with oil and with water. The maximum temperature registered in the inside air of the furnace, for the first condition was of 150

  16. Feedstock characterization and recommended procedures

    International Nuclear Information System (INIS)

    Chum, H.L.; Milne, T.A.; Johnson, D.K.; Agblevor, F.A.

    1993-01-01

    Using biomass for non-conventional applications such as feedstocks for fuels, chemicals, new materials, and electric power production requires knowledge of biomass characteristics important to these processes, and characterization techniques that are more appropriate than those employed today for conventional applications of food, feed, and fiber. This paper reviews feedstock characterization and standardization methodologies, and identifies research and development needs. It reviews the international cooperation involved in determining biomass characteristics and standards that has culminated in preparing four biomass samples currently available from the National Institute of Standards and Technology (NIST)

  17. CVD diamond metallization and characterization

    Science.gov (United States)

    Fraimovitch, D.; Adelberd, A.; Marunko, S.; Lefeuvre, G.; Ruzin, A.

    2017-02-01

    In this study we compared three diamond substrate grades: polycrystalline, optical grade single crystal, and electronic grade single crystal for detector application. Beside the bulk type, the choice of contact material, pre-treatment, and sputtering process details have shown to alter significantly the diamond detector performance. Characterization of diamond substrate permittivity and losses indicate grade and crystallinity related, characteristic differences for frequencies in 1 kHz-1 MHz range. Substantial grade related variations were also observed in surface electrostatic characterization performed by contact potential difference (CPD) mode of an atomic force microscope. Study of conductivity variations with temperature reveal that bulk trap energy levels are also dependent on the crystal grade.

  18. CVD diamond metallization and characterization

    Energy Technology Data Exchange (ETDEWEB)

    Fraimovitch, D., E-mail: dimitryf@mail.tau.ac.il [Faculty of Engineering, Tel Aviv University, 69978 Tel Aviv (Israel); Adelberd, A.; Marunko, S. [Faculty of Engineering, Tel Aviv University, 69978 Tel Aviv (Israel); Lefeuvre, G. [Micron Semiconductor Ltd. Royal Buildings, Marlborough Road, Lancing Business Park, BN15 8SJ (United Kingdom); Ruzin, A. [Faculty of Engineering, Tel Aviv University, 69978 Tel Aviv (Israel)

    2017-02-11

    In this study we compared three diamond substrate grades: polycrystalline, optical grade single crystal, and electronic grade single crystal for detector application. Beside the bulk type, the choice of contact material, pre-treatment, and sputtering process details have shown to alter significantly the diamond detector performance. Characterization of diamond substrate permittivity and losses indicate grade and crystallinity related, characteristic differences for frequencies in 1 kHz–1 MHz range. Substantial grade related variations were also observed in surface electrostatic characterization performed by contact potential difference (CPD) mode of an atomic force microscope. Study of conductivity variations with temperature reveal that bulk trap energy levels are also dependent on the crystal grade.

  19. Synthesis, characterization, photoluminescence and thermally ...

    Indian Academy of Sciences (India)

    Administrator

    Abstract. Sm3+-doped ZnAl2O4 phosphor was synthesized by citrate sol–gel method and characterized using. X-ray diffraction and scanning electron microscopy to identify the crystalline phase and determine the parti- cle size. Photoluminescence (PL) studies on the sample showed emission peaks at 563, 601, 646 and ...

  20. Characterization of Partial Intrinsic Symmetries

    NARCIS (Netherlands)

    Shehu, Aurela; Brunton, Alan; Wuhrer, Stefanie; Wand, Michael

    2014-01-01

    We present a mathematical framework and algorithm for characterizing and extracting partial intrinsic symmetries of surfaces, which is a fundamental building block for many modern geometry processing algorithms. Our goal is to compute all “significant” symmetry information of the shape, which we

  1. PRODUCTION AND CHARACTERIZATION OF LIQUID ...

    African Journals Online (AJOL)

    The aim of this work is to produce and characterized liquid detergents using potassium hydroxide obtained from waste of agricultural materials. The waste agricultural materials are cocoa pods, maize cobs and plantain peels. This was done by ashing these materials in a furnace at a temperature of 1050oC and dissolving ...

  2. Composite materials processing, applications, characterizations

    CERN Document Server

    2017-01-01

    Composite materials are used as substitutions of metals/traditional materials in aerospace, automotive, civil, mechanical and other industries. The present book collects the current knowledge and recent developments in the characterization and application of composite materials. To this purpose the volume describes the outstanding properties of this class of advanced material which recommend it for various industrial applications.

  3. Hydrothermal synthesis, characterization and luminescent ...

    Indian Academy of Sciences (India)

    Home; Journals; Bulletin of Materials Science; Volume 39; Issue 4. Hydrothermal synthesis, characterization and luminescent properties of lanthanide-doped NaLaF 4 nanoparticles. JIGMET LADOL HEENA KHAJURIA SONIKA KHAJURIA ... Keywords. Citric acid; X-ray diffraction; down-conversion emission; energy transfer.

  4. Material stabilization characterization management plan

    International Nuclear Information System (INIS)

    GIBSON, M.W.

    1999-01-01

    This document presents overall direction for characterization needs during stabilization of SNM at the Plutonium Finishing Plant (PFP). Technical issues for needed data and equipment are identified. Information on material categories and links to vulnerabilities are given. Comparison data on the material categories is discussed to assist in assessing the relative risks and desired processing priority

  5. Characterization of Injection Molded Structures

    DEFF Research Database (Denmark)

    Sun, Ling; Søgaard, Emil; Andersen, Nis Korsgaard

    and limitations. Therefore, it would be difficult to characterize complex, especially hierarchical structures by using only one method. Here we present a combined optical microscopy, scanning electron microscopy (SEM), and scanning probe microscopy study on injection molded structures. These structures are used......-properties relationship of the injection molded polymer samples. These results are very important in optimizing injection molding parameters....

  6. SYNTHESIS AND CHARACTERIZATION OF NANOCOMPOSITE ...

    African Journals Online (AJOL)

    ABSTRACT. In this work, nano ferrite spinel NiFe2O4 was synthesized by sol-gel method and characterized by. SEM, XRD, FT-IR, and VSM. In second step Schiff base made from salicylaldehyde and amino propyl triethoxy silane was used for modification of the synthesized nano ferrit. In the third step removal of Ni(II) was ...

  7. Semantic Characterizations of Navigational XPath

    NARCIS (Netherlands)

    Marx, M.J.; de Rijke, M.

    2005-01-01

    We give semantic characterizations of the expressive power of navigational XPath (a.k.a. Core XPath) in terms of first order logic. XPath can be used to specify sets of nodes and sets of paths in an XML document tree. We consider both uses. For sets of nodes, XPath is equally expressive as first

  8. Semantic characterizations of navigational XPath

    NARCIS (Netherlands)

    Marx, M.J.; de Rijke, M.; Mihajlovic, V.; Hiemstra, D.

    2004-01-01

    We give semantic characterizations of the expressive powerof navigational XPath (also called Core XPath) in terms offirst order logic. XPath can be used to specify sets of nodesand to specify sets of paths in a document tree. We considerboth uses. For sets of nodes, we show that first orderlogic in

  9. Waste characterization studies at CRNL

    International Nuclear Information System (INIS)

    Csullog, G.W.; Kupca, S.

    1984-01-01

    The strategy of the radioactive Waste Disposal Project at the Chalk River Nuclear Laboratories (CRNL) is to classify waste segments according to potentially hazardous lifetimes and to match these segment to disposal options selected for their abilities to isolate and contain these wastes. In support of this strategy the principal objective of the waste characterization program is to estimate the quantity and radiological characteristics of the CRNL wastes that will require disposal. The initial focus of the characterization program is the development of a practical, cost-effective waste assay system to estimate the radiological properties of solid wastes handled by the Waste Treatment Centre (WTC) where most of the volume of current solid wastes will be processed. The proposed system will characterize these wastes in a high-throughput, production environment, provide data in support of WTC process operation and maintain electronic data files for waste management purposes. This report summarizes the preliminary research effort to develop the assay system. Studies include the characterization of WTC incinerator ash and the nondestructive gamma-ray monitoring of the incinerator feed using sodium iodide and intrinsic germanium detectors. Additionally, specifications are given for demonstration, nondestructive, solid waste monitor for use at the WTC

  10. Structural characterization of electrodeposited boron

    Indian Academy of Sciences (India)

    Structural characterization of electrodeposited boron was carried out by using transmission electron microscopy and Raman spectroscopy. Electron diffraction and phase contrast imaging were carried out by using transmission electron microscopy. Phase identification was done based on the analysis of electron diffraction ...

  11. Magnetic characterization techniques for nanomaterials

    CERN Document Server

    2017-01-01

    Sixth volume of a 40 volume series on nanoscience and nanotechnology, edited by the renowned scientist Challa S.S.R. Kumar. This handbook gives a comprehensive overview about Magnetic Characterization Techniques for Nanomaterials. Modern applications and state-of-the-art techniques are covered and make this volume an essential reading for research scientists in academia and industry.

  12. CCD characterization and measurements automation

    Czech Academy of Sciences Publication Activity Database

    Kotov, I.V.; Frank, J.; Kotov, A.I.; Kubánek, Petr; O´Connor, P.; Prouza, Michael; Radeka, V.; Takacs, P.

    2012-01-01

    Roč. 695, Dec (2012), 188-192 ISSN 0168-9002 R&D Projects: GA MŠk ME09052 Institutional research plan: CEZ:AV0Z10100502 Keywords : CCD * characterization * test automation Subject RIV: BN - Astronomy, Celestial Mechanics, Astrophysics Impact factor: 1.142, year: 2012

  13. Synthesis, characterization, photoluminescence and thermally ...

    Indian Academy of Sciences (India)

    Administrator

    grinding and heating in (Ar + 10% H2) atmosphere. 2.2 Sample characterization. The as-synthesized ... with literature value of cell parameter a = 8⋅059 A. No impurity phase was observed. The XRD pattern was ..... are thankful to Dr N D Dahale, Fuel Chemistry Division,. BARC, Dr T K Seshagiri, former scientist, and Shri.

  14. Hydrothermal synthesis, characterization and luminescent ...

    Indian Academy of Sciences (India)

    Home; Journals; Bulletin of Materials Science; Volume 39; Issue 4. Hydrothermal synthesis, characterization and luminescent properties of lanthanide-doped NaLaF 4 nanoparticles. JIGMET LADOL HEENA KHAJURIA SONIKA KHAJURIA HAQ NAWAZ SHEIKH. Volume 39 Issue 4 August 2016 pp 943-952 ...

  15. Characterization technologies for environmental remediation

    Energy Technology Data Exchange (ETDEWEB)

    Pruett, J.G.

    1991-01-01

    Improved site characterization technologies are being developed at Martin Marietta Energy Systems for the US Department of Energy (DOE) Office of Technology Development (OTD) in support of environmental restoration activities throughout the DOE complex. Since site characterization is an expensive and time consuming process that must be performed prior to, during, and following remediation efforts, an obvious way to reduce the overall cost of remediation is to develop improved characterization methods. For example, the Derivative Ultraviolet Absorption Spectrometer (DUVAS), which is being field tested as part of the OTD program, is a fiberoptic device for in situ, real time measurement of aromatic organic compounds in groundwater. A transportable, direct sampling Ion Trap Mass Spectrometer (ITMS) is being developed for continuous monitoring of hazardous organic compounds in air. In areas where the environment is hazardous to human health, it is desirous to perform site characterization remotely; if robotics are to be employed, the Ultrasonic Ranging and Data System (USRADS) can be used to provide telemetry information on robot location as well as sensor measurements. Once fully developed, these technologies can be transferred to the private sector. 19 refs., 2 tabs.

  16. PREPARATION AND CHARACTERIZATION OF DIALDEHYDE ...

    African Journals Online (AJOL)

    User

    ABSTRACT. Dialdehyde starch urea (DASU) was prepared by the reaction of dialdehyde starch (DAS) from periodate oxidized cassava starch with urea, which was then used to adsorb Co(II), Pb(II) and. Zn(II) ions from aqueous solution. Starch modified starches and starch complexes were characterized by Fourier ...

  17. Analytical methods of radwaste characterization

    International Nuclear Information System (INIS)

    Garcia, C.M.

    1994-10-01

    In view of the need to carry out more extensive studies on the design of newly proposed methods for the treatment of radioactive wastes collected at PNRI, this study is aimed to provide a guide in the characterization of wastes which is a preparatory step for a well-planned waste processing. (auth.). 8 refs

  18. The Future of Subsurface Characterization

    Science.gov (United States)

    Yeh, T. J.

    2006-12-01

    Existing monitoring and characterization technologies can cover only a small fraction of the subsurface, and the information collected cannot be used to effectively manage current and future drought and other water- related problems. Subsurface sciences need a breakthrough "instrument" to greatly expand and deepen our ability to "see into the groundwater basin." The theme of this talk is to promote the idea of collecting data intelligently and analyzing data smartly for characterization of the subsurface at high resolutions beyond the capabilities of current technology. Specifically, we argue that tomographic surveying is a smart approach, which collects data more cost-effectively and less invasively than existing technologies to characterize the subsurface environments. Limitations of a single type (hydrologic, chemical or geophysical) of tomographic survey then motivate fusion of different types of tomographic surveys such that each survey takes advantage of others to overcome its weakness to reach its optimal capability in a reciprocal manner. A basin is an appropriate scale for the purpose of water resources management. Therefore, the field-scale data collection and fusion concept/technology is expanded to basin-scale characterizations. In order to facilitate these basin-scale tomographic surveys, fusion of passive basin-scale tomographys are suggested that exploit recurrent natural stimuli (e,g., lightning, earthquakes, storm events, barometric variations, river- stage variations, etc.) as sources of excitations, along with implementation of sensor networks that provide long-term and spatially distributed monitoring of signals on the land surface and in the subsurface. This vision for basin-scale subsurface characterization undoubtedly faces unprecedented technological challenges and requires interdisciplinary collaborations (e.g., surface and subsurface hydrology, geophysics, geology, geochemist, information technology, applied mathematics, atmospheric

  19. Characterization of grog of bricks

    International Nuclear Information System (INIS)

    Candido, V.S.; Pinheiro, R.M.; Monteiro, S.N.; Vieira, C.M.F.

    2010-01-01

    This work aims to characterize a waste of red ceramic, grog, generated from the milling of defective pieces of bricks fired in a Hoffmann type furnace by a industry from Campos dos Goytacazes-RJ. The grog was tested for X-ray diffraction, X-ray fluorescence, thermogravimetric and differential thermal analysis, dilatometry, sieving and sedimentation by gravity and optical microscopy. The results indicated that the grog is predominantly constituted of quartz, muscovite mica and hematite. The presence of kaolinite indicates that the bricks were fired at low temperatures, below 600 deg C. Finally, the characterization results indicated that the grog presents itself as an alternative non plastic material to be used in mixtures with clays for the production of red ceramics. (author)

  20. Ultrasonic techniques for fluids characterization

    CERN Document Server

    Povey, Malcolm J W

    1997-01-01

    This book is a comprehensive and practical guide to the use of ultrasonic techniques for the characterization of fluids. Focusing on ultrasonic velocimetry, the author covers the basic topics and techniques necessaryfor successful ultrasound measurements on emulsions, dispersions, multiphase media, and viscoelastic/viscoplastic materials. Advanced techniques such as scattering, particle sizing, and automation are also presented. As a handbook for industrial and scientific use, Ultrasonic Techniques for Fluids Characterization is an indispensable guide to chemists and chemical engineers using ultrasound for research or process monitoring in the chemical, food processing, pharmaceutical, cosmetic, biotechnology,and fuels industries. Key Features * Appeals to anyone using ultrasound to study fluids * Provides the first detailed description of the ultrasound profiling technique for dispersions * Describes new techniques for measuring phase transitions and nucleation, such as water/ice and oil/fat * Presents the l...

  1. Aerosol characterization during project POLINAT

    Energy Technology Data Exchange (ETDEWEB)

    Hagen, D.E.; Hopkins, A.R.; Paladino, J.D.; Whitefield, P.D. [Missouri Univ., Rolla, MO (United States). Cloud and Aerosol Sciences Lab.; Lilenfeld, H.V. [McDonnell Douglas Aerospace-East, St. Louis, MO (United States)

    1997-12-31

    The objectives of the aerosol/particulate characterization measurements of project POLINAT (POLlution from aircraft emissions In the North ATlantic flight corridor) are: to search for aerosol/particulate signatures of air traffic emissions in the region of the North Atlantic Flight Corridor; to search for the aerosol/particulate component of large scale enhancement (`corridor effects`) of air traffic related species in the North Atlantic region; to determine the effective emission indices for the aerosol/particulate component of engine exhaust in both the near and far field of aircraft exhaust plumes; to measure the dispersion and transformation of the aerosol/particulate component of aircraft emissions as a function of ambient condition; to characterize background levels of aerosol/particulate concentrations in the North Atlantic Region; and to determine effective emission indices for engine exhaust particulates for regimes beyond the jet phase of plume expansion. (author) 10 refs.

  2. Characterizing Ensembles of Superconducting Qubits

    Science.gov (United States)

    Sears, Adam; Birenbaum, Jeff; Hover, David; Rosenberg, Danna; Weber, Steven; Yoder, Jonilyn L.; Kerman, Jamie; Gustavsson, Simon; Kamal, Archana; Yan, Fei; Oliver, William

    We investigate ensembles of up to 48 superconducting qubits embedded within a superconducting cavity. Such arrays of qubits have been proposed for the experimental study of Ising Hamiltonians, and efficient methods to characterize and calibrate these types of systems are still under development. Here we leverage high qubit coherence (> 70 μs) to characterize individual devices as well as qubit-qubit interactions, utilizing the common resonator mode for a joint readout. This research was funded by the Office of the Director of National Intelligence (ODNI), Intelligence Advanced Research Projects Activity (IARPA) under Air Force Contract No. FA8721-05-C-0002. The views and conclusions contained herein are those of the authors and should not be interpreted as necessarily representing the official policies or endorsements, either expressed or implied, of ODNI, IARPA, or the US Government.

  3. Optical Particle Characterization in Flows

    Science.gov (United States)

    Tropea, Cameron

    2011-01-01

    Particle characterization in dispersed multiphase flows is important in quantifying transport processes both in fundamental and applied research: Examples include atomization and spray processes, cavitation and bubbly flows, and solid particle transport in gas and liquid carrier phases. Optical techniques of particle characterization are preferred owing to their nonintrusiveness, and they can yield information about size, velocity, composition, and to some extent the shape of individual particles. This review focuses on recent advances for measuring size, temperature, and the composition of particles, including several planar methods, various imaging techniques, laser-induced fluorescence, and the more recent use of femtosecond pulsed light sources. It emphasizes the main sources of uncertainty, the achievable accuracy, and the outlook for improvement of specific techniques and for specific applications. Some remarks are also directed toward the computational tools used to design and investigate the performance of optical particle diagnostic instruments.

  4. Imaging systems and materials characterization

    International Nuclear Information System (INIS)

    Murr, L.E.

    2009-01-01

    This paper provides a broad background for the historical development and modern applications of light optical metallography, scanning and transmission electron microscopy, field-ion microscopy and several forms of scanning probe microscopes. Numerous case examples illustrating especially synergistic applications of these imaging systems are provided to demonstrate materials characterization especially in the context of structure-property-performance issues which define materials science and engineering

  5. Characterization of MEMS FTIR spectrometer

    Science.gov (United States)

    Khalil, Diaa; Sabry, Yasser; Omran, Haitham; Medhat, Mostafa; Hafez, Amr; Saadany, Bassam

    2011-03-01

    In this work we present the full characterization of an optical MEMS Fourier Transform Infra Red FTIR spectrometer fabricated by Deep Reactive Ion Etching DRIE Technology on Silicon substrate. Both electrical and optical properties of the spectrometer are measured. The presented techniques allows to build an engineering model for the spectrometer and to predict its main specifications taking into account the specificity of the MEMS technology used in the spectrometer fabrication.

  6. Characterization of generalized Orlicz spaces

    KAUST Repository

    Ferreira, Rita

    2016-12-14

    The norm in classical Sobolev spaces can be expressed as a difference quotient. This expression can be used to generalize the space to the fractional smoothness case. Because the difference quotient is based on shifting the function, it cannot be used in generalized Orlicz spaces. In its place, we introduce a smoothed difference quotient and show that it can be used to characterize the generalized Orlicz-Sobolev space. Our results are new even in Orlicz spaces and variable exponent spaces.

  7. Parametric characterization of aggregation functions

    Czech Academy of Sciences Publication Activity Database

    Mesiar, Radko; Kolesárová, A.

    2009-01-01

    Roč. 160, č. 6 (2009), s. 816-831 ISSN 0165-0114 R&D Projects: GA ČR GA402/08/0618 Institutional research plan: CEZ:AV0Z10750506 Keywords : Aggregation function * Conjunction measure * Disjunction measure * Global/local parametric characterization * Idempotency measure Subject RIV: BA - General Mathematics Impact factor: 2.138, year: 2009 http://library.utia.cas.cz/separaty/2009/E/mesiar-parametriccharacterizationofaggregationfunctions.pdf

  8. Biophysical characterization of GPCR oligomerization

    DEFF Research Database (Denmark)

    Mathiasen, Signe

    The biophysical characterization of the fundamental molecular mechanisms behind G-protein coupled receptors (GPCRs) oligomerization is proposed to be paramount for understanding the pharmacological consequence of receptor self-association. Here we developed an in vitro assay that allowed a quanti......The biophysical characterization of the fundamental molecular mechanisms behind G-protein coupled receptors (GPCRs) oligomerization is proposed to be paramount for understanding the pharmacological consequence of receptor self-association. Here we developed an in vitro assay that allowed...... a quantitative characterization of GPCR oligomerization. The assay provided the first quantification of the association energy of the β2 Adrenergic Receptor (β2AR), a prototypical GPCR. Furthermore we directly observed the time-dependent dimerization of β2AR and Cannabinoid receptor 1 at the single molecule...... level, and revealed the existence of several dimerization interfaces, each with specific kinetics. Finally we investigated how a property of the membrane solubilizing GPCRs affected oligomerization. We observed a dramatic decrease in oligomer stability with increasing geometrical membrane curvature. We...

  9. Cross delay line sensor characterization

    Energy Technology Data Exchange (ETDEWEB)

    Owens, Israel J [Los Alamos National Laboratory; Remelius, Dennis K [Los Alamos National Laboratory; Tiee, Joe J [Los Alamos National Laboratory; Buck, Steven E [Los Alamos National Laboratory; Whittemore, Stephen R [Los Alamos National Laboratory; Thompson, David C [Los Alamos National Laboratory; Shirey, Robert [Los Alamos National Laboratory

    2010-01-01

    There exists a wealth of information in the scientific literature on the physical properties and device characterization procedures for complementary metal oxide semiconductor (CMOS), charge coupled device (CCD) and avalanche photodiode (APD) format detectors. Numerous papers and books have also treated photocathode operation in the context of photomultiplier tube (PMT) operation for either non imaging applications or limited night vision capability. However, much less information has been reported in the literature about the characterization procedures and properties of photocathode detectors with novel cross delay line (XDL) anode structures. These allow one to detect single photons and create images by recording space and time coordinate (X, Y & T) information. In this paper, we report on the physical characteristics and performance of a cross delay line anode sensor with an enhanced near infrared wavelength response photocathode and high dynamic range micro channel plate (MCP) gain (> 10{sup 6}) multiplier stage. Measurement procedures and results including the device dark event rate (DER), pulse height distribution, quantum and electronic device efficiency (QE & DQE) and spatial resolution per effective pixel region in a 25 mm sensor array are presented. The overall knowledge and information obtained from XDL sensor characterization allow us to optimize device performance and assess capability. These device performance properties and capabilities make XDL detectors ideal for remote sensing field applications that require single photon detection, imaging, sub nano-second timing response, high spatial resolution (10's of microns) and large effective image format.

  10. Characterization of ultrafine aluminum nanoparticles

    International Nuclear Information System (INIS)

    Sandstrom, Mary M.; Jorgensen, Betty S.; Mang, Joseph T.; Smith, Bettina L.; Son, Steven F.

    2004-01-01

    Aluminum nanopowders with particle sizes ranging from ∼25 nm to 80 nm were characterized by a variety of methods. We present and compare the results from common powder characterization techniques including transmission electron microscopy (TEM), high resolution transmission electron microscopy (HRTEM), BET gas adsorption surface area analysis, thermogravimetric analysis (TGA), photon correlation spectroscopy (PCS), and low angle laser light scattering (LALLS). Aluminum nanoparticles consist of an aluminum core with an aluminum oxide coating. HRTEM measurements of both the particle diameter and oxide layer thickness tend to be larger than those obtained from BET and TGA. LALLS measurements show a large degree of particle agglomeration in solution; therefore, primary particle sizes could not be determined. Furthermore, results from small-angle scattering techniques (SAS), including small-angle neutron (SANS) and x-ray (SAXS) scattering are presented and show excellent agreement with the BET, TGA, and HRTEM. The suite of analytical techniques presented in this paper can be used as a powerful tool in the characterization of many types of nanosized powders.

  11. Laboratory characterization of shale pores

    Science.gov (United States)

    Nur Listiyowati, Lina

    2018-02-01

    To estimate the potential of shale gas reservoir, one needs to understand the characteristics of pore structures. Characterization of shale gas reservoir microstructure is still a challenge due to ultra-fine grained micro-fabric and micro level heterogeneity of these sedimentary rocks. The sample used in the analysis is a small portion of any reservoir. Thus, each measurement technique has a different result. It raises the question which methods are suitable for characterizing pore shale. The goal of this paper is to summarize some of the microstructure analysis tools of shale rock to get near-real results. The two analyzing pore structure methods are indirect measurement (MIP, He, NMR, LTNA) and direct observation (SEM, TEM, Xray CT). Shale rocks have a high heterogeneity; thus, it needs multiscale quantification techniques to understand their pore structures. To describe the complex pore system of shale, several measurement techniques are needed to characterize the surface area and pore size distribution (LTNA, MIP), shapes, size and distribution of pore (FIB-SEM, TEM, Xray CT), and total porosity (He pycnometer, NMR). The choice of techniques and methods should take into account the purpose of the analysis and also the time and budget.

  12. Sofia Observatory Performance and Characterization

    Science.gov (United States)

    Temi, Pasquale; Miller, Walter; Dunham, Edward; McLean, Ian; Wolf, Jurgen; Becklin, Eric; Bida, Tom; Brewster, Rick; Casey, Sean; Collins, Peter; hide

    2012-01-01

    The Stratospheric Observatory for Infrared Astronomy (SOFIA) has recently concluded a set of engineering flights for Observatory performance evaluation. These in-flight opportunities have been viewed as a first comprehensive assessment of the Observatory's performance and will be used to address the development activity that is planned for 2012, as well as to identify additional Observatory upgrades. A series of 8 SOFIA Characterization And Integration (SCAI) flights have been conducted from June to December 2011. The HIPO science instrument in conjunction with the DSI Super Fast Diagnostic Camera (SFDC) have been used to evaluate pointing stability, including the image motion due to rigid-body and flexible-body telescope modes as well as possible aero-optical image motion. We report on recent improvements in pointing stability by using an Active Mass Damper system installed on Telescope Assembly. Measurements and characterization of the shear layer and cavity seeing, as well as image quality evaluation as a function of wavelength have been performed using the HIPO+FLITECAM Science Instrument configuration (FLIPO). A number of additional tests and measurements have targeted basic Observatory capabilities and requirements including, but not limited to, pointing accuracy, chopper evaluation and imager sensitivity. SCAI activities included in-flight partial Science Instrument commissioning prior to the use of the instruments as measuring engines. This paper reports on the data collected during the SCAI flights and presents current SOFIA Observatory performance and characterization.

  13. Ultrasonic Characterization of Aerospace Composites

    Science.gov (United States)

    Leckey, Cara; Johnston, Patrick; Haldren, Harold; Perey, Daniel

    2015-01-01

    Composite materials have seen an increased use in aerospace in recent years and it is expected that this trend will continue due to the benefits of reduced weight, increased strength, and other factors. Ongoing work at NASA involves the investigation of the large-scale use of composites for spacecraft structures (SLS components, Orion Composite Crew Module, etc). NASA is also involved in work to enable the use of composites in advanced aircraft structures through the Advanced Composites Project (ACP). In both areas (space and aeronautics) there is a need for new nondestructive evaluation and materials characterization techniques that are appropriate for characterizing composite materials. This paper will present an overview of NASA's needs for characterizing aerospace composites, including a description of planned and ongoing work under ACP for the detection of composite defects such as fiber waviness, reduced bond strength, delamination damage, and microcracking. The research approaches include investigation of angle array, guided wave, and phase sensitive ultrasonic methods. The use of ultrasonic simulation tools for optimizing and developing methods will also be discussed.

  14. Sustainability Characterization for Additive Manufacturing.

    Science.gov (United States)

    Mani, Mahesh; Lyons, Kevin W; Gupta, S K

    2014-01-01

    Additive manufacturing (AM) has the potential to create geometrically complex parts that require a high degree of customization, using less material and producing less waste. Recent studies have shown that AM can be an economically viable option for use by the industry, yet there are some inherent challenges associated with AM for wider acceptance. The lack of standards in AM impedes its use for parts production since industries primarily depend on established standards in processes and material selection to ensure the consistency and quality. Inability to compare AM performance against traditional manufacturing methods can be a barrier for implementing AM processes. AM process sustainability has become a driver due to growing environmental concerns for manufacturing. This has reinforced the importance to understand and characterize AM processes for sustainability. Process characterization for sustainability will help close the gaps for comparing AM performance to traditional manufacturing methods. Based on a literature review, this paper first examines the potential environmental impacts of AM. A methodology for sustainability characterization of AM is then proposed to serve as a resource for the community to benchmark AM processes for sustainability. Next, research perspectives are discussed along with relevant standardization efforts.

  15. Degradation of process water containing polymers UV/H{sub 2}O{sub 2} system; Degradacao de agua de processo contendo polimeros via sistema UV/H{sub 2}O{sub 2}

    Energy Technology Data Exchange (ETDEWEB)

    Will, Isabela B.S.; Telemaco, Emmanuelle P.; Chiavone-Filho, Osvaldo; Guardani, Roberto; Nascimento, Claudio A.O. do

    2004-07-01

    The water rationalization has been one of the goals of the petrochemical industry. Such goals in such a way demand technological innovations for new productive processes how much for new techniques of treatment and reuse of water in the production chain. The high industrial water costs in Brazil, particularly in the regions metropolitans, have stimulated the national industries to evaluate the possibilities of reuse. The objective of this work is the application of the process water treatment containing polypropylene using ultraviolet radiation and hydrogen peroxide, that is system UV/H{sub 2}O{sub 2}, aiming at to adjust them for reuses in the proper process, reducing the water capitation daily pay-treated and improving the water exploitation. Photochemical annular reactor with medium pressure mercury vapor lamp was used and the following parameters of process had been evaluated: radiation, temperature of reaction and hydrogen peroxide concentration. The monitoring of the experiments was based on the measurement of contents of dissolved organic carbon, total carbon and inorganic carbon. Additionally, experiments using solar radiation had been evaluated. The experimental results had indicated the viability of application of system UV/H{sub 2}O{sub 2} having used artificial and solar light sources. The quality of the water obtained in the treatment was adequate to reuse it. (author)

  16. Evaluation of natural and degradation by salt spray of red ceramics incorporated with ornamental rock waste; Avaliacao da degradacao natural e por nevoa salina de ceramica vermelha incorporadas com rejeito de rocha ornamental

    Energy Technology Data Exchange (ETDEWEB)

    Altoe, Larissa Machado; Xavier, Gustavo de Castro; Albuquerque, Fernando Saboya; Maia, Paulo Cesar de Almeida; Alexandre, Jonas, E-mail: daniellavrodrigues@hotmail.com, E-mail: gxavier@uenf.br [Universidade Estadual do Norte Fluminense Darcy Ribeiro (LECIV/UENF), Campos dos Goytacazes, RJ (Brazil)Laboratorio de Engenharia Civil

    2011-07-01

    To better study the mechanical behavior of red ceramic, the samples were degraded in salt spray equipment and exposed in environment. The salt spray equipment subjects the samples to conditions found by the sea, through the mix solutions of sodium chloride. The ceramic samples were prepared with up to 10% by mass of ornamental rock waste to dry and pressed into rectangular mold of steel. The materials were fired at temperatures of 650°C, 750° C and 850°C. After 90 days of degradation natural and 45 days in salt spray, ware analyzed the properties of ceramic material. The results of mechanical strength were compared using the Weibull distribution, before and after the degradation. Note that the material with ornamental rock waste raised the mechanical strength and did'nt significantly changes the material properties after degradation. (author)

  17. Degradation and formation of {sup 14} C-atrazine bound residues in soils of the Sao Paulo State; Degradacao e formacao de residuos ligados de {sup 14} C-atrazina em latossolo vermelho escuro e glei humico

    Energy Technology Data Exchange (ETDEWEB)

    Peixoto, Maria de Fatima da Silva Pinto [Bahia Univ., Cruz das Almas, BA (Brazil). Escola de Agronomia. Dept. de Quimica; Lavorenti, Arquimedes [Sao Paulo Univ., Piracicaba, SP (Brazil). Escola Superior de Agricultura Luiz de Queiroz. Dept. de Ciencias Exatas]. E-mail: alavoren@carpa.ciagri.usp.br; Regitano, Jussara Borges; Tornisielo, Valdemar Luiz [Centro de Energia Nuclear na Agricultura (CENA), Piracicaba, SP (Brazil). Secao de Ecotoxicologia

    2000-03-01

    The objective of this study was to evaluate the degradation and formation of {sup 14} C-atrazine bound residues in two soils of the Sao Paulo state, Brazil. Hapludox and Umbraquults soils were incubated for 63 days in 500 cm{sup 3} glass vessels with {sup 1}'4 C-atrazine at 10.38 {mu}g a.i.g{sup -1} of soil. The {sup 14} CO{sub 2} evolution was mensured weekly. Acetonitrile and water (4:1 v/v) was used as extractor solution of the herbicide residues and the organic matter fractionation was based on the solubility of the humic fractions of acids and bases. The extracted residue were analyzed for radioactivity by using the Thin Layer Chromatography (TLC) method. The mineralization process (0.1% at 63 days after incubation) was insignificant for the atrazine detoxification in the Umbraquults soil. Hidroxyatrazine was the main metabolite of atrazine found in both soils and bound residue formation was an important process in that molecule dissipation, especially in the Umbraquults soil. (author)

  18. Potential for photocatalytic degradation of the potassic diclofenac using scandium and silver modified titanium dioxide thin films; Potencial de degradacao fotocatalitica do diclofenaco potassico utilizando filmes finos de dioxido de titanio modificado com escandio e prata

    Energy Technology Data Exchange (ETDEWEB)

    Ciola, R.A.; Oliveira, C.T.; Lopes, S.A.; Cavalheiro, A.A., E-mail: rafaelciola@hotmail.com [Universidade Estadual de Mato Grosso do Sul (UFMS), Navirai, MS (Brazil). Centro de Pesquisas Tecnologicas em Recursos Naturais

    2011-07-01

    The potential for photocatalytic degradation of the potassic diclofenac drug was investigated using titanium dioxide thin films modified with two modifier types, scandium and silver, both prepared by Sol-Gel method. It was demonstrated by UVVis spectroscopy analysis of the solutions containing the drug, under UV-A light irradiation that the degradation efficiency of the titanium dioxide photocatalyst is dependent of the semiconductor nature and that the scandium accelerates the first step of the degradation when compared to the silver. This result seems to be related to the redox potential of the electron-hole pair, once the scandium modifying sample generates a p type semiconductor that reduces the band gap. The extra holes attract more strongly the chorine ion present in diclofenac and leading to the releasing more easily. However, after the first byproducts degradation the following steps are not facilitated, making the silver modifying more advantageous. (author)

  19. Cobalt-60 gamma radiation effects on degradation of pesticides used in stored rice and beans; Efeitos da radiacao gama do cobalto-60 na degradacao de inseticidas aplicados em arroz e feijao armazenados

    Energy Technology Data Exchange (ETDEWEB)

    Groppo, Gerson A.

    1988-02-01

    The present work, carried out at CENA, an agriculture nuclear energy center - University of Sao Paulo - Brazil, investigates the Cobalt-60 gamma radiation effects on insecticides applied to stored rice and beans. The radiation dose applied - 200 Gy - to the stored rice and beans treated with insecticides was not sufficient to cause a noticeable chemical degradation through insect mortality. (author). 31 refs., 23 tabs.

  20. Evaluation of parameters associated with UV/EB cured clearcoats degradation used in outdoor environment;Avaliacao da formacao e degradacao de filmes de vernizes curados por radiacao ultravioleta e feixe de eletrons e expostos ao envelhecimento acelerado

    Energy Technology Data Exchange (ETDEWEB)

    Ruiz, Carmen Silvia Bentivoglio, E-mail: brazilruiz@comcast.ne

    2009-07-01

    The materials curable by ultraviolet (UV) or electron beam (EB) radiation such as inks, adhesives and coatings are reactive compounds made up of resin, monomer, photoinitiator and additives which undergo polymerization and crosslinking under irradiation producing thermoset products. This technology has been used in a great variety of industrial applications, replacing the conventional curing process in the development of new products. One of the challenging applications has been to design weatherable radiation cured coating which maintain their desirable physical properties and aesthetic appearance. This research reports information about the behavior of four UV and EB curable clear coatings -with or without light stabilizer additives- under accelerated weathering. Thermogravimetry, differential scanning calorimetry, differential photocalorimetry, infrared and ultraviolet spectroscopy and tensile properties were used to evaluate these formulations. Clear coating 50 {mu}m thick films were cured with UV and EB radiation at different doses. The UV curing process was carried out at room temperature using an UV tunnel, with a medium pressure mercury lamp and a transport belt with variable speed. The ultraviolet radiation doses were in the range of 50 to 1500 mJ cm{sup -2}. The EB curing process was performed under N{sub 2} atmosphere, with doses in the range from 1,6 to 300 kGy using the IPEN-CNEN/SP Dynamitron electron beam accelerator with energy of 1.5 MeV. The cure degree was determined by means of the residual reaction heat of the undercured samples obtained from photo-DSC or DSC measurements. The accelerated aging tests were carried out using a Weather-Ometer chamber with exposition times in the range of 100 to 3000 hours. The experimental data obtained from the photo-aged samples were evaluated and correlated to the formulation composition, type of radiation - UV or EB, radiation dose and residence time in the aging chamber. The results have shown that the EB cured films have a better resistance to photoinduced weathering effects than UV cured ones. UV/EB films with light stabilizers have shown larger stability than those counterparts with no additives. The aging effects were evaluated by parameters such as hardness, gloss, surface roughness, yellowness index and changes in the FTIR absorption bands. (author)

  1. Inorganic elements and organic compounds degradation studies by gamma irradiation in used lubricating oils; Estudos de remocao de elementos inorganicos e degradacao de compostos organicos por radiacao gama em oleos lubrificantes usados

    Energy Technology Data Exchange (ETDEWEB)

    Scapin, Marcos Antonio

    2008-07-01

    The automotive lubricating oils have partial degradation of organic compounds and addition of undesirable inorganic elements, during its use. These substances classify the used lubricating oils as dangerous and highly toxic. According to global consensus, concerning the environmental conservation, the best is to perform a reuse treatment of these lubricating oils. For this purpose, the uses of an alternative and effective technology have been sought. In this work, the efficacy and technical feasibility of the advanced oxidation process (AOP), by gamma radiation, for used automotive lubricating oil treatment has been studied. Different quantities of hydrogen peroxide and water Milli-Q were added to oil samples. They were submitted to the Cobalt-60 irradiator, type Gammacell, with 100, 200 and 500 kGy absorbed doses. The inorganic analysis by X-ray fluorescence (WDXRF) showed inorganic elements removal, mainly to sulphur, calcium, iron and nickel elements at acceptable levels by environmental protection law for oils reusing. The gas chromatography (GC/MS) analysis showed that the advanced oxidation process promotes the organic compounds degradation. The main identified compounds were tridecane, 2-methyl-naphthalene, and trietilamina-tetramethyl urea, which have important industrial applications. The multivariate analysis, Cluster Analysis, showed that advanced oxidation process application is a viable and promising treatment for used lubricating oil reusing. (author)

  2. Hydrothermal degradation of tetragonal ZrO{sub 2} ceramic components used in dental applications; Efeito da degradacao em meio aquoso de componentes ceramicos a base de ZrO{sub 2} tetragonal para uso odontologico

    Energy Technology Data Exchange (ETDEWEB)

    Mukaeda, L.E.; Robin, A.; Taguchi, S.P. [Universidade de Sao Paulo (DEMAR/EEL/USP), Lorena, SP (Brazil). Escola de Engenharia de Lorena. Dept. de Engenharia de Materiais; Santos, C. [ProtMat Materiais Avancados, Guaratingueta, SP (Brazil)

    2009-07-01

    With the evolution of the dental restoration techniques, a considerable growth in the demand of ceramic products occurred. These materials present good strength associated to reliability. In this work, micrometric and nanometric scale tetragonal ZrO{sub 2} blocks were sintered at 1500 deg C-2h and 1350 deg C-2h, respectively, ground and polished. Ceramics with relative density higher than 98% were obtained. The specimens were immersed in hot water (150 deg C), for times ranging from 10h to 30h. The mass variation of the samples was measured and the crystalline phases present before and after the degradation tests were identified by X-ray diffractometry, in order to evaluate the capacity of these ceramics in resisting to aqueous medium exposure. Materials with nanometric structure present higher resistance to degradation than those with micrometric scale, and this interferes in structural stability after the test, and reduces the martensitic transformation. (author)

  3. Degradation of the insecticide ethyl parathion in different environmental matrices by gamma radiation from Cobalt-60; Degradacao do inseticida paration etilico em diversas matrizes ambientais por meio de radiacao ionizante gama do cobalto-60

    Energy Technology Data Exchange (ETDEWEB)

    Luchini, Luiz Carlos

    1995-07-01

    This work studies the use of gamma radiation from cobalt-60 to induce parathion degradation in different matrices, as well as, quantified GC-NPD and identified by GC-MS, the radiolysis resulting products. Results show that the insecticide was completely degraded in aqueous solution after treatment with 1.0 kGy dosis in a dosis rate of 3.12 kGy h{sup -1}. In methanol, parathion was completely degraded only with 30 kGy at 3.12 kGy h{sup -1}. The metabolites detected after radiolysis were the same formed by biological degradation, i.e, p-nitrophenol, p-aminophenol, paraoxon and aminoparathion. The gamma radiation also degraded paraoxon which is the most toxic metabolite of parathion. It was verified that, not only the total radiation, but also the dosis rate supplied to the aqueous solution had a significant effect on the insecticide degradation, and the formation of metabolites occurred in a selective way respecting the dosis and dosis rate. Otherwise, the gamma radiation did almost not degraded the parathion adsorbed in solid matrices as rice, moist and dry soil, even using dosis of 5,30 and 50 kGy, respectively. The parathion yield and the dosis of gamma radiation needed for 50% reduction of the insecticide initial concentration in aqueous solution were also calculated and presented. Thus, it was verified that irradiation of parathion besides to be an important instrument for environmental decontamination of this pesticide in aqueous matrix, it allows the production of parathion metabolites for ecotoxicological studies. (author)

  4. Gas characterization system software acceptance test report

    International Nuclear Information System (INIS)

    Vo, C.V.

    1996-01-01

    This document details the results of software acceptance testing of gas characterization systems. The gas characterization systems will be used to monitor the vapor spaces of waste tanks known to contain measurable concentrations of flammable gases

  5. Characterization of bridge foundations workshop report.

    Science.gov (United States)

    2013-11-01

    "In 2013, the Federal Highway Administration proposed a new research program for the characterization of bridge foundations. To narrow the focus and develop a research roadmap for the program, a workshop on Characterization of Bridge Foundations...

  6. Electrochemical characterization of liquid resistors

    International Nuclear Information System (INIS)

    Wilson, J.M.; Whiteley, R.V.

    1983-01-01

    During the first two years of operation of Sandia's Particle Beam Fusion Accelerator (PBFA I) the reliability of the CuSO 4 solution resistors in the Marx Generator Energy Storage System has been unsatisfactory. Resistor failure, which is characterized by a large increase in resistance, has been attributed to materials, production techniques, and operating parameters. The problems associated with materials and production techniques have been identified and solutions are proposed. Non-ideal operating parameters are shown to cause polarization of the cathode in the resistor. This initiates electrochemical reactions in the resistor. These reactions often lead to resistance changes and to eventual resistor failure

  7. Characterization of Microporous Insulation, Microsil

    Energy Technology Data Exchange (ETDEWEB)

    Thomas, R. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

    2017-06-15

    Microsil microporous insulation has been characterized by Lawrence Livermore National Laboratory for possible use in structural and thermal applications in the DPP-1 design. Qualitative test results have provided mechanical behavioral characteristics for DPP-1 design studies and focused on the material behavioral response to being crushed, cyclically loaded, and subjected to vibration for a confined material with an interference fit or a radial gap. Quantitative test results have provided data to support the DPP-1 FEA model analysis and verification and were used to determine mechanical property values for the material under a compression load. The test results are documented within this report.

  8. Neutron Characterization for Additive Manufacturing

    Science.gov (United States)

    Watkins, Thomas; Bilheux, Hassina; An, Ke; Payzant, Andrew; DeHoff, Ryan; Duty, Chad; Peter, William; Blue, Craig; Brice, Craig A.

    2013-01-01

    Oak Ridge National Laboratory (ORNL) is leveraging decades of experience in neutron characterization of advanced materials together with resources such as the Spallation Neutron Source (SNS) and the High Flux Isotope Reactor (HFIR) shown in Fig. 1 to solve challenging problems in additive manufacturing (AM). Additive manufacturing, or three-dimensional (3-D) printing, is a rapidly maturing technology wherein components are built by selectively adding feedstock material at locations specified by a computer model. The majority of these technologies use thermally driven phase change mechanisms to convert the feedstock into functioning material. As the molten material cools and solidifies, the component is subjected to significant thermal gradients, generating significant internal stresses throughout the part (Fig. 2). As layers are added, inherent residual stresses cause warping and distortions that lead to geometrical differences between the final part and the original computer generated design. This effect also limits geometries that can be fabricated using AM, such as thin-walled, high-aspect- ratio, and overhanging structures. Distortion may be minimized by intelligent toolpath planning or strategic placement of support structures, but these approaches are not well understood and often "Edisonian" in nature. Residual stresses can also impact component performance during operation. For example, in a thermally cycled environment such as a high-pressure turbine engine, residual stresses can cause components to distort unpredictably. Different thermal treatments on as-fabricated AM components have been used to minimize residual stress, but components still retain a nonhomogeneous stress state and/or demonstrate a relaxation-derived geometric distortion. Industry, federal laboratory, and university collaboration is needed to address these challenges and enable the U.S. to compete in the global market. Work is currently being conducted on AM technologies at the ORNL

  9. Characterizing the Danish telemedicine ecosystem

    DEFF Research Database (Denmark)

    Manikas, Konstantinos; Hansen, Klaus Marius

    2013-01-01

    and interoperability issues, silo solutions, and lack of guidelines and standards. In this paper, we characterise the ecosystem evolved around the telemedicine services in Denmark and study the actors involved in this ecosystem. We establish a method for this study, where we define two actor roles and ways...... of characterizing actor contributions, and apply the method to the largest healthcare region of Denmark. Our findings reveal an ecosystem that is relatively closed to new actors, where the actors tend to be related to single telemedicine applications, the applications have low connectivity, and the most influential...... actors of the ecosystem can be characterised as both being beneficial and inhibitory to the ecosystem prosperity....

  10. Instrumentation for tropospheric aerosol characterization

    Energy Technology Data Exchange (ETDEWEB)

    Shi, Z.; Young, S.E.; Becker, C.H.; Coggiola, M.J. [SRI International, Menlo Park, CA (United States); Wollnik, H. [Giessen Univ. (Germany)

    1997-12-31

    A new instrument has been developed that determines the abundance, size distribution, and chemical composition of tropospheric and lower stratospheric aerosols with diameters down to 0.2 {mu}m. In addition to aerosol characterization, the instrument also monitors the chemical composition of the ambient gas. More than 25.000 aerosol particle mass spectra were recorded during the NASA-sponsored Subsonic Aircraft: Contrail and Cloud Effects Special Study (SUCCESS) field program using NASA`s DC-8 research aircraft. (author) 7 refs.

  11. Characterization of Mexican zeolite minerals

    International Nuclear Information System (INIS)

    Jimenez C, M.J.

    2005-01-01

    50% of the Mexican territory is formed by volcanic sequences of the Pliocene type, which appear extensively in the northwest states (Sonora, Sinaloa, Chihuahua, Durango) and west of Mexico (Jalisco and Nayarit), in central Mexico (Zacatecas, Guanajuato, San Luis Potosi, Queretaro, Hidalgo) and south of Mexico (Guerrero, Oaxaca); therefore, it is to be expected that in our country big locations of natural zeolites exist in its majority of the clinoptilolite type. The present study was focused toward the characterization of two Mexican natural zeolite rocks presumably of the clinoptilolite and filipsite types, one of them comes from the state of Chihuahua and the other of a trader company of non metallic minerals, due that these materials are not characterized, its are not known their properties completely and therefore, the uses that can be given to these materials. In this investigation work it was carried out the characterization of two Mexican zeolite rocks, one coming from the Arroyo zone, municipality of La Haciendita, in the state of Chihuahua; and the other one was bought to a trader company of non metallic minerals. The two zeolites so much in their natural form as conditioned with sodium; they were characterized by means of X-ray diffraction, scanning electron microscopy of high vacuum and elementary microanalysis (EDS), surface area analysis (BET), thermal gravimetric analysis. To differentiate the heulandite crystalline phase of the other clinoptilolite rock, its were carried out thermal treatments. The quantification of Al, Na, Ca, K, Mg, Fe was carried out in solution, by means of atomic absorption spectroscopy and the quantity of Si was determined by gravimetry. The zeolite rocks presented for the major part the crystalline heulandite and clinoptilolite phases for the most part, and it was found that the zeolite coming from the state of Chihuahua possesses a bigger content of heulandite and the denominated filipsite it is really a zeolite

  12. Advanced Fine Particulate Characterization Methods

    Energy Technology Data Exchange (ETDEWEB)

    Steven Benson; Lingbu Kong; Alexander Azenkeng; Jason Laumb; Robert Jensen; Edwin Olson; Jill MacKenzie; A.M. Rokanuzzaman

    2007-01-31

    The characterization and control of emissions from combustion sources are of significant importance in improving local and regional air quality. Such emissions include fine particulate matter, organic carbon compounds, and NO{sub x} and SO{sub 2} gases, along with mercury and other toxic metals. This project involved four activities including Further Development of Analytical Techniques for PM{sub 10} and PM{sub 2.5} Characterization and Source Apportionment and Management, Organic Carbonaceous Particulate and Metal Speciation for Source Apportionment Studies, Quantum Modeling, and High-Potassium Carbon Production with Biomass-Coal Blending. The key accomplishments included the development of improved automated methods to characterize the inorganic and organic components particulate matter. The methods involved the use of scanning electron microscopy and x-ray microanalysis for the inorganic fraction and a combination of extractive methods combined with near-edge x-ray absorption fine structure to characterize the organic fraction. These methods have direction application for source apportionment studies of PM because they provide detailed inorganic analysis along with total organic and elemental carbon (OC/EC) quantification. Quantum modeling using density functional theory (DFT) calculations was used to further elucidate a recently developed mechanistic model for mercury speciation in coal combustion systems and interactions on activated carbon. Reaction energies, enthalpies, free energies and binding energies of Hg species to the prototype molecules were derived from the data obtained in these calculations. Bimolecular rate constants for the various elementary steps in the mechanism have been estimated using the hard-sphere collision theory approximation, and the results seem to indicate that extremely fast kinetics could be involved in these surface reactions. Activated carbon was produced from a blend of lignite coal from the Center Mine in North Dakota and

  13. Characterization of retinaldehyde dehydrogenase 3

    OpenAIRE

    Graham, Caroline E.; Brocklehurst, Keith; Pickersgill, Richard W.; Warren, Martin J.

    2006-01-01

    RALDH3 (retinal dehydrogenase 3) was characterized by kinetic and binding studies, protein engineering, homology modelling, ligand docking and electrostatic-potential calculations. The major recognition determinant of an RALDH3 substrate was shown to be an eight-carbon chain bonded to the aldehyde group whose kinetic influence (kcat/Km at pH 8.5) decreases when shortened or lengthened. Surprisingly, the β-ionone ring of all-trans-retinal is not a major recognition site. The dissociation const...

  14. Digital Holographic Interferometry for Airborne Particle Characterization

    Science.gov (United States)

    2015-03-19

    Atmospheric and Energy Science, Center d’Energétique et de Thermique de Lyon, Lyon, France (2014). 3. Talk: Particle characterization with digital...Characterization, Journal of Quantitative Spectroscopy & Radiative Transfer (04 2014) Jing Wen, Matthew J. Berg, Matthew Steed. Scattering-based...Particulate-Systems Characterization, Journal of Quantitative Spectroscopy & Radiative Transfer (04 2013) Romain Ceolato, Matthew J. Berg, Nicolas

  15. Characterization system for resonant micro- and nanocantilevers

    DEFF Research Database (Denmark)

    Sandberg, Rasmus Kousholt; Boisen, Anja; Svendsen, Winnie Edith

    2005-01-01

    We present a system for characterization of the resonant properties of micro- and nanocantilever sensors. The system has been constructed as a vacuum chamber with capabilities for controlling environmental conditions such as pressure, temperature, and chemical constituents. Characterization can...... in resonant frequency determination, and demonstrating the importance of resonance characterization in a controlled environment. ©2005 American Institute of Physics...

  16. Genotypic identification and technological characterization of lactic ...

    African Journals Online (AJOL)

    enoh

    2012-04-05

    Apr 5, 2012 ... genotypic characterization, the dominant LAB were identified as Lactobacillus paracasei (43.3%), ... Lactobacillus brevis (5.2%), Enterococcus faecium (5.2%), Lactobacillus fermentum (4.1%) and ... Key words: Lactic acid bacteria, genotypic characterization, technological characterization, tulum cheese.

  17. Characterization and control of biological microrobots

    NARCIS (Netherlands)

    Khalil, I.S.M.; Pichel, Marc Philippe; Zondervan, L.; Abelmann, Leon; Misra, Sarthak; Desai, Jaydev P.; Dudek, Gregory; Khatib, Oussama; Kumar, Vijay

    2013-01-01

    This work addresses the characterization and control of Magnetotactic Bacterium (MTB) which can be considered as a biological microrobot. Magnetic dipole moment of the MTB and response to a field-with-alternating-direction are characterized. First, the magnetic dipole moment is characterized using

  18. Characterization and Control of Biological Microrobots

    NARCIS (Netherlands)

    Khalil, I.S.M.; Pichel, Marc Philippe; Pichel, M.P.; Zondervan, L.; Abelmann, Leon; Misra, Sarthak

    2012-01-01

    This work addresses the characterization and control of Magnetotactic Bacterium (MTB) which can be considered as a biological microrobot. Magnetic dipole moment of the MTB and response to a field-with-alternating-direction are characterized. First, the magnetic dipole moment is characterized using

  19. Portable system to luminaries characterization

    Science.gov (United States)

    Tecpoyotl-Torres, M.; Vera-Dimas, J. G.; Koshevaya, S.; Escobedo-Alatorre, J.; Cisneros-Villalobos, L.; Sanchez-Mondragon, J.

    2014-09-01

    For illumination sources designers is important to know the illumination distribution of their products. They can use several viewers of IES files (standard file format determined by Illuminating Engineering Society). This files are necessary not only know the distribution of illumination, but also to plain the construction of buildings by means of specialized softwares, such as Autodesk Revit. In this paper, a complete portable system for luminaries' characterization is given. The components of the systems are: Irradiance profile meter, which can generate photometry of luminaries of small sizes which covers indoor illumination requirements and luminaries for general areas. One of the meteŕs attributes is given by the color sensor implemented, which allows knowing the color temperature of luminary under analysis. The Graphic Unit Interface (GUI) has several characteristics: It can control the meter, acquires the data obtained by the sensor and graphs them in 2D under Cartesian and polar formats or 3D, in Cartesian format. The graph can be exported to png, jpg, or bmp formats, if necessary. These remarkable characteristics differentiate this GUI. This proposal can be considered as a viable option for enterprises of illumination design and manufacturing, due to the relatively low investment level and considering the complete illumination characterization provided.

  20. Characterization of Polymeric Nanofiltration Membranes

    Directory of Open Access Journals (Sweden)

    Simoncic, B.

    2007-11-01

    Full Text Available As membrane processes are increasingly used in industrial applications, there is a growing interest in methods of membrane characterization. Traditional membrane characteristics, such as cut-off value and pore size distribution, are being supplemented by membrane surface characteristics, such as charge density or zeta potential and hydrophobicity. This study, therefore, characterizes the three different polymeric membranes used (NFT-50, DL and DK. The molecular mass cut-off (MMCO value was determined using a set of reference solutes within the molecular range 150-600 Da, whereas streaming potential measurements enabled quantification of the surface charge characteristics. Hydrophobicity was studied using contact angle measurements. The results indicated that even though all three membranes had very similar layer compositions which consisted of poly(piperazneamide, as top layers they showed different values of measured quantitive. The NFT-50 membrane had the lowest MMCO value and the most hydrophilic membrane surface, followed by DK and DL. Membrane fouling as measured by flux reduction was determined by streaming potential measurements and accompanied by a positive change in zeta potential.

  1. BNFL Report Glass Formers Characterization

    International Nuclear Information System (INIS)

    Schumacher, R.F.

    2000-01-01

    The objective of this task was to obtain powder property data on candidate glass former materials, sufficient to guide conceptual design and estimate the cost of glass former handling facilities as requested under Part B1 of BNFL Technical and Development Support. Twenty-nine glass forming materials were selected and obtained from vendors for the characterization of their physical properties, durability in caustic solution, and powder flow characteristics. A glass former was selected based on the characterization for each of the ten oxide classes required for Envelope A, B, and C mixtures. Three blends (A, B, and C) were prepared based on formulations provided by Vitreous State Laboratory and evaluated with the same methods employed for the glass formers. The properties obtained are presented in a series of attached Tables. It was determined that five of the ten glass formers, (kyanite, iron oxide, titania, zircon, and zinc oxide) have the potential to cause some level of solids f low problems. In addition, all of the blends may require consideration for their handling. A number of engineering considerations and recommendations were prepared based on the experimental findings, experience, and other process considerations. Recommendations for future testing are included. In conjunction with future work, it is recommended that a professional consultant be engaged to guide and assist with testing and design input

  2. Optical metrology for DMD™ characterization

    Science.gov (United States)

    Miller, Seth A.; Mezenner, Rabah; Doane, Dennis

    2001-01-01

    The Digital Micromirror Device™ (DMD™) developed at Texas Instruments is a spatial light modulator composed of 500,000 to 1.3 million movable micromachined aluminum mirrors. The DMD™ serves as the engine for the current generation of computer-driven slide and video projectors, and for next generation devices in digital television and movie projectors. Because of the unique architecture and applications of the device, Texas Instruments has developed a series of customized optical testers for characterizing DMD™ performance. This paper provides a general overview of the MirrorMaster, a custom optical inspection tool. Particular attention is given to Bias Adhesion Mapping (BAM) as a device performance metric. BAM is an optical test that monitors the performance of the mirrors as a function of an applied voltage. This voltage drives the mirrors to the `on' or `off' position, and as the bias is stepped down the mirrors return to their neutral orientations. Important forces involved in this process include the electrostatic field applied, the compliance of the hinge, and static friction (stiction). BAM curves can help characterize device stiction and allow us to examine the efficacy of the lubrication system over the lifetime of the device.

  3. Solar Filament Extraction and Characterizing

    Science.gov (United States)

    Yuan, Yuan; Shih, F. Y.; Jing, J.; Wang, H.

    2010-05-01

    This paper presents a new method to extract and characterize solar filaments from H-alpha full-disk images produced by Big Bear Solar Observatory. A cascading Hough Transform method is designed to identify solar disk center location and radius. Solar disks are segmented from the background, and unbalanced illumination on the surface of solar disks is removed using polynomial surface fitting. And then a localized adaptive thresholding is employed to extract solar filament candidates. After the removal of small solar filament candidates, the remaining larger candidates are used as the seeds of region growing. The procedure of region growing not only connects broken filaments but also generate complete shape for each filament. Mathematical morphology thinning is adopted to produce the skeleton of each filament, and graph theory is used to prune branches and barbs to get the main skeleton. The length and the location of the main skeleton is characterized. The proposed method can help scientists and researches study the evolution of solar filament, for instance, to detect solar filament eruption. The presented method has already been used by Space Weather Research Lab of New Jersey Institute of Technology (http://swrl.njit.edu) to generate the solar filament online catalog using H-alpha full-disk images of Global H-alpha Network (http://swrl.njit.edu/ghn_web/).

  4. Immunohistochemical Characterization of Canine Lymphomas

    Directory of Open Access Journals (Sweden)

    Roxana CORA

    2017-11-01

    Full Text Available Lymphomas occur by clonal expansion of lymphoid cells and have distinctive morphological and immunophenotypic features. Determination of canine lymphoma immunophenotype is useful for accurate prognosis and further therapy. In the suggested study, we performed an immunohistochemical evaluation of some cases with canine lymphoma diagnosed in the Department of Pathology (Faculty of Veterinary Medicine, Cluj-Napoca, Romania, in order to characterize them. The investigation included 39 dogs diagnosed with different anatomical forms of lymphoma, following necropsy analysis or assessment of biopsies. The diagnosis of lymphoma was confirmed by necropsy and histopathology (Hematoxylin-eosin stain examinations. The collected specimens were analyzed by immunohistochemistry technique (automatic method using the following antibodies: CD3, CD20, CD21 and CD79a. The analyzed neoplasms were characterized as follows: about 64.10% of cases were diagnosed as B-cell lymphomas, 33.34% of cases as T-cell lymphomas, whereas 2.56% of cases were null cell type lymphomas (neither B nor T. Most of multicentric (80%, mediastinal (60% and primary central nervous system lymphomas (100% had B immunophenotype, while the majority of cutaneous (80% and digestive (100% lymphomas had T immunophenotype. Immunohistochemical description of canine lymphomas can deliver some major details concerning their behavior and malignancy. Additionally, vital prognosis and efficacy of some therapeutic protocols are relying on the immunohistochemical features of canine lymphoma.

  5. BNFL Report Glass Formers Characterization

    Energy Technology Data Exchange (ETDEWEB)

    Schumacher, R.F.

    2000-07-27

    The objective of this task was to obtain powder property data on candidate glass former materials, sufficient to guide conceptual design and estimate the cost of glass former handling facilities as requested under Part B1 of BNFL Technical and Development Support. Twenty-nine glass forming materials were selected and obtained from vendors for the characterization of their physical properties, durability in caustic solution, and powder flow characteristics. A glass former was selected based on the characterization for each of the ten oxide classes required for Envelope A, B, and C mixtures. Three blends (A, B, and C) were prepared based on formulations provided by Vitreous State Laboratory and evaluated with the same methods employed for the glass formers. The properties obtained are presented in a series of attached Tables. It was determined that five of the ten glass formers, (kyanite, iron oxide, titania, zircon, and zinc oxide) have the potential to cause some level of solids f low problems. The problems might include arching or ratholing in the silo/hopper. In addition, all of the blends may require consideration for their handling.

  6. Signal anomaly detection and characterization

    International Nuclear Information System (INIS)

    Morgenstern, V.M.; Upadhyaya, B.R.; Gloeckler, O.

    1988-08-01

    As part of a comprehensive signal validation system, we have developed a signal anomaly detector, without specifically establishing the cause of the anomaly. A signal recorded from process instrumentation is said to have an anomaly, if during steady-state operation, the deviation in the level of the signal, its root-mean-square (RMS) value, or its statistical distribution changes by a preset value. This deviation could be an unacceptable increase or a decrease in the quantity being monitored. An anomaly in a signal may be characterized by wideband or single-frequency noise, bias error, pulse-type error, nonsymmetric behavior, or a change in the signal bandwidth. Various signatures can be easily computed from data samples and compared against specified threshold values. We want to point out that in real processes, pulses can appear with different time widths, and at different rates of change of the signal. Thus, in characterizing an anomaly as a pulse-type, the fastest pulse width is constrained by the signal sampling interval. For example, if a signal is sampled at 100 Hz, we will not be able to detect pulses occurring at kHz rates. Discussion with utility and Combustion Engineering personnel indicated that it is not practical to detect pulses having a narrow time width. 9 refs., 11 figs., 8 tabs

  7. BNFL Report Glass Formers Characterization

    International Nuclear Information System (INIS)

    Schumacher, R.F.

    2000-01-01

    The objective of this task was to obtain powder property data on candidate glass former materials, sufficient to guide conceptual design and estimate the cost of glass former handling facilities as requested under Part B1 of BNFL Technical and Development Support. Twenty-nine glass forming materials were selected and obtained from vendors for the characterization of their physical properties, durability in caustic solution, and powder flow characteristics. A glass former was selected based on the characterization for each of the ten oxide classes required for Envelope A, B, and C mixtures. Three blends (A, B, and C) were prepared based on formulations provided by Vitreous State Laboratory and evaluated with the same methods employed for the glass formers. The properties obtained are presented in a series of attached Tables. It was determined that five of the ten glass formers, (kyanite, iron oxide, titania, zircon, and zinc oxide) have the potential to cause some level of solids f low problems. The problems might include arching or ratholing in the silo/hopper. In addition, all of the blends may require consideration for their handling

  8. Nanodosimetric characterization of ion beams

    International Nuclear Information System (INIS)

    Bug, M.U.; Hilgers, G.; Baek, W.Y.; Rabus, H.

    2014-01-01

    The characterization of particle track structure is essential for an estimation of radiobiological effects, particularly in the case of densely ionizing radiation. The particle track structure can be characterized by nano-dosimetric quantities which are measurable by means of a nano-dosimeter. Results obtained from experiments with the nano-dosimeter can be used to validate track structure simulations, which are essential for estimating track structure parameters in biological material. For this purpose, the dedicated Monte Carlo code PTra has been developed to simulate the nano-dosimeter setup as well as nano-metric targets consisting of water. Recently, electron-impact cross section data of DNA constituents measured at PTB were implemented into PTra. A calculation of nano-dosimetric quantities in DNA-analog media shows considerable differences to results obtained in water medium, particularly for electron energies lower than 200 eV. These discrepancies become more considerable when nano-dosimetric quantities are used to estimate biological effects. This paper aims to provide an overview of the present status of nano-dosimetry, focusing on the experimental and simulation work at PTB. Furthermore, the suitability of simple models directly linking nano-dosimetric track structure characteristics and radiobiological effectiveness is discussed. (authors)

  9. Quantitative Characterization of Nanostructured Materials

    Energy Technology Data Exchange (ETDEWEB)

    Dr. Frank (Bud) Bridges, University of California-Santa Cruz

    2010-08-05

    The two-and-a-half day symposium on the "Quantitative Characterization of Nanostructured Materials" will be the first comprehensive meeting on this topic held under the auspices of a major U.S. professional society. Spring MRS Meetings provide a natural venue for this symposium as they attract a broad audience of researchers that represents a cross-section of the state-of-the-art regarding synthesis, structure-property relations, and applications of nanostructured materials. Close interactions among the experts in local structure measurements and materials researchers will help both to identify measurement needs pertinent to real-world materials problems and to familiarize the materials research community with the state-of-the-art local structure measurement techniques. We have chosen invited speakers that reflect the multidisciplinary and international nature of this topic and the need to continually nurture productive interfaces among university, government and industrial laboratories. The intent of the symposium is to provide an interdisciplinary forum for discussion and exchange of ideas on the recent progress in quantitative characterization of structural order in nanomaterials using different experimental techniques and theory. The symposium is expected to facilitate discussions on optimal approaches for determining atomic structure at the nanoscale using combined inputs from multiple measurement techniques.

  10. Historical characterization of trigeminal neuralgia.

    Science.gov (United States)

    Eboli, Paula; Stone, James L; Aydin, Sabri; Slavin, Konstantin V

    2009-06-01

    TRIGEMINAL NEURALGIA IS a well known clinical entity characterized by agonizing, paroxysmal, and lancinating facial pain, often triggered by movements of the mouth or eating. Historical reviews of facial pain have attempted to describe this severe pain over the past 2.5 millennia. The ancient Greek physicians Hippocrates, Aretaeus, and Galen, described kephalalgias, but their accounts were vague and did not clearly correspond with what we now term trigeminal neuralgia. The first adequate description of trigeminal neuralgia was given in 1671, followed by a fuller description by physician John Locke in 1677. André described the convulsive-like condition in 1756, and named it tic douloureux; in 1773, Fothergill described it as "a painful affection of the face;" and in 1779, John Hunter more clearly characterized the entity as a form of "nervous disorder" with reference to pain of the teeth, gums, or tongue where the disease "does not reside." One hundred fifty years later, the neurological surgeon Walter Dandy equated neurovascular compression of the trigeminal nerve with trigeminal neuralgia.

  11. Impact-limiting materials characterization

    International Nuclear Information System (INIS)

    Glass, R.E.; Duffey, T.A.; McConnell, P.

    1993-01-01

    Three types of impact-limiting materials have been characterized which have applications in packages for the transport of radioactive materials. These materials are aluminum honeycombs, polyurethane foams, and aluminum foams. The results of the materials characterization have indicated strengths and weaknesses for each type of material. The polyurethane foams provide good impact limiting ability and excellent thermal insulation. However, they burn when subjected to the regulatory thermal event in the presence of air. The aluminum honeycombs provide excellent impact resistance in specific impact orientations. However, they provide relatively poor resistance to thermal assault. Finally, the aluminum foams exhibit relatively poor impact energy absorption capacities, significant variability in energy absorption, and limited thermal insulation. The development of the figures of merit examined the response of the materials to the impact event with the intent of maximizing the energy absorption of the materials with respect to either the volume or mass of the materials. Three figures of merit will be presented for the structural response. The figure of merit for the thermal event is based on minimizing the heat flux to the containment boundary. The paper presents a discussion of the test methods, a summary of the data and the figures of merit for each material. (J.P.N.)

  12. Characterization of Complex Colloidal Suspensions

    Science.gov (United States)

    Seaman, J. C.; Guerin, M.; Jackson, B. P.; Ranville, J. M.

    2003-04-01

    Surface chemical reactions play a major role in controlling contaminant fate and transport in the subsurface environment. Recent field and laboratory evidence suggests that mobile soil and groundwater colloids may facilitate the migration of sparingly soluble groundwater contaminants. Colloidal suspensions collected in the field or generated in laboratory column experiments tend to be fairly dilute in nature and comprised of relatively small particulates (reserved for studying ideal systems to the characterization of mobile colloids. However, many of these analytical techniques, including total/selective dissolution methods, dynamic light scattering, micro-electrophoresis, streaming potential, and even scanning electron microscopy (SEM), can be biased in of larger size fractions, and therefore, extremely sensitive to sampling, storage, and fractionation artifacts. In addition, surface modifiers such as sorbed oxides or organics can alter particulate appearance, composition, and behavior when compared to synthetic analogues or mineral standards. The current presentation will discuss the limitations and inherent biases associated with a number of analytical characterization techniques that are commonly applied to the study of mobile soil and groundwater colloids, including field flow fractionation (FFF) and acoustic based methods that have only recently become available.

  13. Characterization of minerals, metals and materials

    CERN Document Server

    Hwang, Jiann-Yang; Bai, Chengguang; Carpenter, John; Cai, Mingdong; Firrao, Donato; Kim, Byoung-Gon

    2012-01-01

    This state-of-the-art reference contains chapters on all aspects of the characterization of minerals, metals, and materials. The title presents papers from one of the largest yearly gatherings of materials scientists in the world and thoroughly discusses the characterization of minerals, metals, and materials The scope includes current industrial applications and research and developments in the following areas:  Characterization of Ferrous Metals Characterization of Non-Ferrous Materials Characterization of Minerals and Ceramics Character

  14. An ideal characterization of the Clifford operators

    Science.gov (United States)

    Farinholt, J. M.

    2014-08-01

    The Clifford operators are an important and well-studied subset of quantum operations, in both the qubit and higher-dimensional qudit cases. While there are many ways to characterize this set, this paper aims to provide an ideal characterization, in the sense that it has the same characterization in every finite dimension, is characterized by a minimal set of gates, is constructive, and does not make any assumptions about non-Clifford operations or resources (such as the use of ancillas or the ability to make measurements). While most characterizations satisfy some of these properties, this appears to be the first characterization satisfying all of the above. As an application, we use these results to briefly analyze characterizations of Clifford embeddings, that is, the action of logical Clifford operations acting on qunits embedded in higher-dimensional qudits, inside the qudit Clifford framework.

  15. Model characterizing sports game referees

    Directory of Open Access Journals (Sweden)

    Rudzitis A.

    2014-01-01

    Full Text Available The question concerning such a person who is forced to work in the conditions of increased stress and about work safety still is a psycho-physiological part of a broader problem. Referees of sports games can also be added to this group as this occupation has become their profession. Today, there is a situation that in order to enroll the most suitable individuals in this job position it is necessary to select the candidates for sports game referees according to strictly worked-out criteria. The aim of the study was to investigate the abilities characterizing high quality sports game referees. 18 international level referees of sports games in Latvia were selected as subjects of the research. To state the subjects' physical ability, functional state, psychological peculiarities the following were applied: a computerized testing device “Omega” was used to assess the functional state of the body; situation alertness, psycho-emotional stability, self-regulation ability and motivation were stated with the help of tests used in sport psychology; simple reactions and the quickness of alternative reaction were measured using the computer system Vienna Test System. 16 parameters of each subject were obtained, and they were processed using Factor analysis – closed variant of the main components with the following turning of the referent axis according to the Varimax criterion. With the Factor analysis nine main factors were obtained characterizing sports game referees. Their contribution in the common dispersion is 93.7%. Seven factors of higher value were interpreted, and they were as follows: choice reaction time, its contribution in the dispersion 30.31%; functional state of the body and readiness (17.92%; correctness of the answers in choice reaction time test (the quality of the decisions made 15.40%; the simple reaction time (9.02%; IQ coefficient (7.20%; psychological preparedness (5.01% and the ability to concentrate (4.80%. The quickness of

  16. Analysis of the Solar Resource Information Datasets for Thermal and/or electric Generation Using a Geographical Information System. Cases of Application: Central Cafeteria - University of the Valley, Cali Municipality and Farm {sup P}ozo Verde{sup ,} Jamundi Municipality , Cauca Valley, Colombia; Analisis de las Fuentes de Informacion sobre Recurso Solar para Generacion Termica y/o Electrica Empleando un Sistema de Informacion Geografica. Casos de Aplicacion: Cafeteria Central - Universidad del Valle, Municipio de Cali y Granja {sup P}ozo Verde{sup ,} Municipio de Jamundi, Valle del Cauca, Colombia

    Energy Technology Data Exchange (ETDEWEB)

    Dominguez, J.; Manrique, P. A.; Pinedo, I.

    2009-10-12

    In this report, two examples of renewable energy assessments based on Geographical Information Systems are presented. Several case studies have been carried out in the Valley of Cauca (Colombia), and one on them has been used to size a hybrid system. The results of this particular case study are presented in a second report. The aim of this document is analysing the different sources of data that could be used in the characterization of solar energy for electricity and electricity-heat use. With this purpose, data of two areas in Valley of Cauca obtained from the Atlas of Solar Radiation of Colombia, SWERA project and SSE-NASA have been compared. The data coming from these sources has been analysed using a Geographical Information System, and the conclusions are described along with cartographic and numeric products. These reports are the result of a collaboration established between Universidad del Valle (Colombia) and CIEMAT (Spain), and have been done by the author while his staying at our center included on his PhD program.

  17. Fuels characterization studies. [jet fuels

    Science.gov (United States)

    Seng, G. T.; Antoine, A. C.; Flores, F. J.

    1980-01-01

    Current analytical techniques used in the characterization of broadened properties fuels are briefly described. Included are liquid chromatography, gas chromatography, and nuclear magnetic resonance spectroscopy. High performance liquid chromatographic ground-type methods development is being approached from several directions, including aromatic fraction standards development and the elimination of standards through removal or partial removal of the alkene and aromatic fractions or through the use of whole fuel refractive index values. More sensitive methods for alkene determinations using an ultraviolet-visible detector are also being pursued. Some of the more successful gas chromatographic physical property determinations for petroleum derived fuels are the distillation curve (simulated distillation), heat of combustion, hydrogen content, API gravity, viscosity, flash point, and (to a lesser extent) freezing point.

  18. Technology characterization: liquified natural gas

    Energy Technology Data Exchange (ETDEWEB)

    None

    1976-12-01

    A technology characterization for liquefied natural gas (LNG) was made. The scope of work was confined to a literature review of LNG processes including natural gas production, liquefaction, and revaporization. The work was divided into five major categories as follows: (1) status of LNG projects, (2) general process description, (3) environmental aspects, (4) safety, and (5) economics. Each of these categories forms a major heading for this report. In addition, an LNG reference system of 250 million standard cubic feet per day (MMSCFD) is included in the report at Argonne National Laboratory's (Argonne) request. Information concerning this system was derived from other LNG systems in the literature. The report does not include an assessment of the market potential for the product gas or its end use. Published cost estimates in the literature have been identified but the original cost estimates have not been provided. Plant layouts, conceptual designs, and socioeconomic analysis are not provided.

  19. Aerosol Inlet Characterization Experiment Report

    Energy Technology Data Exchange (ETDEWEB)

    Bullard, Robert L. [Brookhaven National Lab. (BNL), Upton, NY (United States); Kuang, Chongai [Brookhaven National Lab. (BNL), Upton, NY (United States); Uin, Janek [Brookhaven National Lab. (BNL), Upton, NY (United States); Smith, Scott [Brookhaven National Lab. (BNL), Upton, NY (United States); Springston, Stephen R. [Brookhaven National Lab. (BNL), Upton, NY (United States)

    2017-05-01

    The U.S. Department of Energy (DOE) Atmospheric Radiation Measurement (ARM) Climate Research Facility Aerosol Observation System inlet stack was characterized for particle penetration efficiency from 10 nm to 20 μm in diameter using duplicate scanning mobility particle sizers (10 nm-450 nm), ultra-high-sensitivity aerosol spectrometers (60 nm-μm), and aerodynamic particle sizers (0.5 μm-20 μm). Results show good model-measurement agreement and unit transmission efficiency of aerosols from 10 nm to 4 μm in diameter. Large uncertainties in the measured transmission efficiency exist above 4 μm due to low ambient aerosol signal in that size range.

  20. Biopolymer chitin: extraction and characterization

    International Nuclear Information System (INIS)

    Andrade, Sania M.B. de; Ladchumananandasivam, Rasiah

    2011-01-01

    The biopolymers are materials made from renewable sources such as soybean, corn, cane sugar, cellulose and chitin. Chitin is the most abundant biopolymer found in nature, after cellulose. The chemical structure of chitin is distinguished by the hydroxyl group, of structure from cellulose, located at position C-2, which in the chitin is replaced by acetamine group. The objective of this study was to develop the chitin from exoskeletons of Litopenaeus vannamei shrimp, which are discarded as waste, causing pollutions, environmental problems and thus obtain better utilization of these raw materials. It also, show the extraction process and deacetylation of chitosan. The extraction of chitin followed steps of demineralization, desproteinization and deodorization. Chitin and chitosan were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD) and the thermals properties were analyzed by thermogravimetry (TG/DTG). (author)

  1. Hydraulic characterization of " Furcraea andina

    Science.gov (United States)

    Rivera-Velasquez, M. F.; Fallico, C.; Molinari, A.; Santillan, P.; Salazar, M.

    2012-04-01

    The present level of pollution, increasingly involving groundwaters, constitutes a serious risk for environment and human health. Therefore the remediation of saturated and unsaturated soils, removing pollutant materials through innovative and economic bio-remediation techniques is more frequently required. Recent studies on natural fiber development have shown the effectiveness of these fibers for removal of some heavy metals, due to the lignin content in the natural fibers which plays an important role in the adsorption of metal cations (Lee et al., 2004; Troisi et al., 2008; C. Fallico, 2010). In the context of remediation techniques for unsaturated and/or saturated zone, an experimental approach for the hydraulic characterization of the "Furcraea andina" (i.e., Cabuya Blanca) fiber was carried out. This fiber is native to Andean regions and grows easily in wild or cultivated form in the valleys and hillsides of Colombia, Ecuador, and Peru. Fibers of "Furcraea andina" were characterized by experimental tests to determine their hydraulic conductivity or permeability and porosity in order to use this medium for bioremediation of contaminated aquifer exploiting the physical, chemical and microbial capacity of natural fiber in heavy metal adsorption. To evaluate empirically the hydraulic conductivity, laboratory tests were carried out at constant head specifically on the fibers manually extracted. For these tests we used a flow cell (used as permeameter), containing the "Furcraea andina" fibers to be characterized, suitably connected by a tygon pipe to a Marriott's bottle, which had a plastic tube that allow the adjustment of the hydraulic head for different tests to a constant value. By this experiment it was also possible to identify relationships that enable the estimation of permeability as a function of density, i.e. of the compaction degree of the fibers. Our study was carried out for three values of hydraulic head (H), namely 10, 18, and 25 cm and for each

  2. Synthesis and characterization of Taurine

    Directory of Open Access Journals (Sweden)

    B Bayarmaa

    2014-10-01

    Full Text Available Have been obtained 2-aminoethanesulfonic acid (taurine from ethanolamine, sulfuric acid and sodium sulfite during the synthesis in laboratory condition. The process involves two steps of reactions, the first was esterification of ethanolamine with sulfuric acid to produce the intermediate product of 2-aminoethyl ester which than was extended to the second step by sulfonation with sodium sulfite to produce 2-aminoethanesulfonic acid. Resulting product was analyzed using 1H-NMR, IR, FAB-MS analysis and examined purity characterizations of the synthesized products. DOI: http://dx.doi.org/10.5564/mjc.v14i0.200 Mongolian Journal of Chemistry 14 (40, 2013, p57-60

  3. Materials characterization by photoelectron spectroscopy

    International Nuclear Information System (INIS)

    Nascente, P.A.P.

    2010-01-01

    Low energy electrons are suitable for investigating surfaces due to their low mean free path in solids, which correspond to a few atomic layers (0.5 to 3.0 nm), and could be used in one of the following ways: incident electrons cause the emission of backscattered and secondary electrons and the electrons are excited by irradiated photons. The first case includes the emission of Auger electrons, while photoemission corresponds to the second case. X-ray photoelectron spectroscopy (XPS) is one of the most used surface analysis techniques since it is able to identify not only the surface constituents but also their chemical states. XPS can be employed in several areas of science and engineering, but in this report it will be presented only few examples of its use in the characterization of metallic materials, with an emphasis on thin films of noble and transition metals. (author)

  4. Characterization of Czochralski Silicon Detectors

    CERN Document Server

    Luukka, Panja-Riina

    2012-01-01

    This thesis describes the characterization of irradiated and non-irradiated segmenteddetectors made of high-resistivity (>1 kΩcm) magnetic Czochralski (MCZ) silicon. It isshown that the radiation hardness (RH) of the protons of these detectors is higher thanthat of devices made of traditional materials such as Float Zone (FZ) silicon or DiffusionOxygenated Float Zone (DOFZ) silicon due to the presence of intrinsic oxygen (> 5 x1017 cm-3). The MCZ devices therefore present an interesting alternative for future highenergy physics experiments. In the large hadron collider (LHC), the RH of the detectorsis a critical issue due to the high luminosity (1034 cm-2s-1) corresponding to the expectedtotal fluencies of fast hadrons above 1015 cm-2. This RH improvement is important sinceradiation damage in the detector bulk material reduces the detector performance andbecause some of the devices produced from standard detector-grade silicon, e.g. FZsilicon with negligible oxygen concentration, might not survive the plann...

  5. Characterizing and Modeling Citation Dynamics

    Science.gov (United States)

    Eom, Young-Ho; Fortunato, Santo

    2011-01-01

    Citation distributions are crucial for the analysis and modeling of the activity of scientists. We investigated bibliometric data of papers published in journals of the American Physical Society, searching for the type of function which best describes the observed citation distributions. We used the goodness of fit with Kolmogorov-Smirnov statistics for three classes of functions: log-normal, simple power law and shifted power law. The shifted power law turns out to be the most reliable hypothesis for all citation networks we derived, which correspond to different time spans. We find that citation dynamics is characterized by bursts, usually occurring within a few years since publication of a paper, and the burst size spans several orders of magnitude. We also investigated the microscopic mechanisms for the evolution of citation networks, by proposing a linear preferential attachment with time dependent initial attractiveness. The model successfully reproduces the empirical citation distributions and accounts for the presence of citation bursts as well. PMID:21966387

  6. Solar Thermal Reactor Materials Characterization

    Energy Technology Data Exchange (ETDEWEB)

    Lichty, P. R.; Scott, A. M.; Perkins, C. M.; Bingham, C.; Weimer, A. W.

    2008-03-01

    Current research into hydrogen production through high temperature metal oxide water splitting cycles has created a need for robust high temperature materials. Such cycles are further enhanced by the use of concentrated solar energy as a power source. However, samples subjected to concentrated solar radiation exhibited lifetimes much shorter than expected. Characterization of the power and flux distributions representative of the High Flux Solar Furnace(HFSF) at the National Renewable Energy Laboratory(NREL) were compared to ray trace modeling of the facility. In addition, samples of candidate reactor materials were thermally cycled at the HFSF and tensile failure testing was performed to quantify material degradation. Thermal cycling tests have been completed on super alloy Haynes 214 samples and results indicate that maximum temperature plays a significant role in reduction of strength. The number of cycles was too small to establish long term failure trends for this material due to the high ductility of the material.

  7. Nano controllers characterization under radiation

    International Nuclear Information System (INIS)

    Bezerra, F.; Barde, S.; Carayon, J.L.; Sarthou, M.

    1999-01-01

    4 commercial nano-controllers (PIC16LC84, PIC16C73A, PIC16C76 and ST62E25) from MICROCHIP and SGS-Thomson have been characterized under heavy-ions, protons and total dose. The preliminary results show that PIC16LC84 has to be banned from the selection because it can not sustain high cumulated dose (its Idd begins to shift at 6 krads) and that its E 2 PROM code memory is too sensitive to SEU (single event upset). The 3 PICs have been tested with heavy-ions, the results show that they are sensible to upsets and latch-up, nevertheless no latch-up has been observed under proton irradiation. The sensitivity to latch-up does not matter a lot because PICs consume very little and it is planned to implement them in a tolerant design. (A.C.)

  8. Characterizing stellar and exoplanetary environments

    CERN Document Server

    Khodachenko, Maxim

    2015-01-01

    In this book an international group of specialists discusses studies of exoplanets subjected to extreme stellar radiation and plasma conditions. It is shown that such studies will help us to understand how terrestrial planets and their atmospheres, including the early Venus, Earth and Mars, evolved during the host star’s active early phase. The book presents an analysis of findings from Hubble Space Telescope observations of transiting exoplanets, as well as applications of advanced numerical models for characterizing the upper atmosphere structure and stellar environments of exoplanets. The authors also address detections of atoms and molecules in the atmosphere of “hot Jupiters” by NASA’s Spitzer telescope. The observational and theoretical investigations and discoveries presented are both timely and important in the context of the next generation of space telescopes. 
 The book is divided into four main parts, grouping chapters on exoplanet host star radiation and plasma environments, exoplanet u...

  9. Optical characterization of antirelaxation coatings

    Science.gov (United States)

    Tsvetkov, S.; Gateva, S.; Cartaleva, S.; Mariotti, E.; Nasyrov, K.

    2018-03-01

    Antirelaxation coatings (ARC) are used in optical cells containing alkali metal vapor to reduce the depolarization of alkali atoms after collisions with the cell walls. The long-lived ground state polarization is a basis for development of atomic clocks, magnetometers, quantum memory, slow light experiments, precision measurements of fundamental symmetries etc. In this work, a simple method for measuring the number of collisions of the alkali atoms with the cell walls without atomic spin randomization (Nasyrov et al., Proc. SPIE (2015)) was applied to characterize the AR properties of two PDMS coatings prepared from different solutions in ether (PDMS 2% and PDMS 5%). We observed influence of the light-induced atomic desorption (LIAD) on the AR properties of coatings.

  10. 324 Building Baseline Radiological Characterization

    International Nuclear Information System (INIS)

    Reeder, R.J.; Cooper, J.C.

    2010-01-01

    This report documents the analysis of radiological data collected as part of the characterization study performed in 1998. The study was performed to create a baseline of the radiological conditions in the 324 Building. A total of 85 technical (100 square centimeter (cm 2 )) smears were collected from the Room 147 hoods, the Shielded Materials Facility (SMF), and the Radiochemical Engineering Cells (REC). Exposure rate readings (window open and window closed) were taken at a distance of 2.5 centimeters (cm) and 30 cm from the surface of each smear. Gross beta-gamma and alpha counts of each smear were also performed. The smear samples were analyzed by gamma energy analysis (GEA). Alpha energy analysis (AEA) and strontium-90 analysis were also performed on selected smears. GEA results for one or more samples reported the presence of manganese-54, cobalt-60, silver-108m antimony-125, cesium-134, cesium-137, europium-154, europium-155, and americium-241. AEA results reported the presence of plutonium-239/240, plutonium-238/ 241 Am, curium-243/244, curium-242, and americium-243. Tables 5 through 9 present a summary by location of the estimated maximum removable and total contamination levels in the Room 147 hoods, the SMF, and the REC. The smear sample survey data and laboratory analytical results are presented in tabular form by sample in Appendix A. The Appendix A tables combine survey data documented in radiological survey reports found in Appendix B and laboratory analytical results reported in the 324 Building Physical and Radiological Characterization Study (Berk, Hill, and Landsman 1998), supplemented by the laboratory analytical results found in Appendix C.

  11. Characterization of NCPA Infrasound Sensors

    Science.gov (United States)

    Hart, D. M.; Jones, K. R.; Sauter, A.

    2011-12-01

    By adding NCPA (National Center for Physical Acoustics) Infrasound sensors to the eastern-half of the Transportable Array, the scientific community has gained another powerful tool for studying natural processes. In an effort to characterize the sensors, including the effect of the wind filter and acoustical porting, researchers at Sandia National Labs (SNL) FACT Site and IRIS PASSCAL have performed a series of tests that resulted in good agreement with the NCPA-provided response (20mV/Pa +-10%, .007Hz high-pass corner frequency). Through independent testing and verification we have gained confidence in the sensor's linearity over the pressure range tested, a measure of power usage, and a measure of the dynamic range the sensors are capable of delivering, indicating the instruments can measure signals well below the Bowman (2005) Acoustic Low Noise Model up to 8Hz. Researchers at the SNL Fact site have the capabilities not only to test the NCPA sensor in an acoustic pressure chamber, but also to test the equivalent of the entire infrasound system used in the TA stations: NCPA sensor, tubing, and wind reduction design (a PVC filter buried in a bag of pumice stone). SNL tests with this fully-ported infrasound system characterize the full system response. We found that the tubing used to port the sensor to the external wind reduction device adds a measurable 15Hz resonance to the response and influences the high-frequency roll-off point. At PASSCAL, we have performed an acceptance test on more than 350 NCPA sensors, and in the process, have collected statistics on their relative gains. The standard deviation of the relative gain for all measured sensors is 5.32%. For 59 repeated tests of the two NCPA sensors used as references, the standard deviation is .15%, which suggests that acceptance testing can be used to constrain the gain of individual NCPA sensors much tighter than the population deviation.

  12. Topological Characterization of Fractured Coal

    Science.gov (United States)

    Jing, Yu; Armstrong, Ryan T.; Ramandi, Hamed L.; Mostaghimi, Peyman

    2017-12-01

    Coal transport properties are highly dependent on the underlying fractured network, known as cleats, which are characterized by geometrical and topological properties. X-ray microcomputed tomography (micro-CT) has been widely applied to obtain 3-D digital representations of the cleat network. However, segmentation of 3-D data is often problematic due to image noise, which will result in inaccurate estimation of coal properties (e.g., porosity and specific surface area). To circumvent this issue, a discrete fracture network (DFN) model is proposed. We develop a characterization framework to determine if the developed DFN models can preserve the topological properties of the coal cleat network found in micro-CT data. We compute the Euler characteristic, fractal dimension, and percolation quantities to analyze the topology locally and globally and compare the results between micro-CT data (before denoising), filtered micro-CT data (after denoising), and the DFN model. We find that micro-CT data with noise have extensive connectivity while filtered micro-CT data and DFN models have similar topology both globally and locally. It is concluded that the topology of the DFN models are closer to that of the realistic cleat network that do not have segmentation-induced pores. In addition, micro-CT imaging always struggles with the trade-off between sample size and resolution, while the presented DFN models are not restricted by imaging resolution and thus can be constructed with extended domain size. Overall, the presented DFN model is a reliable alternative with realistic cleat topology, extended domain size and favorable data format for direct numerical simulations.

  13. NMR characterization of pituitary tumors

    International Nuclear Information System (INIS)

    Osbakken, M.; Gonzales, J.; Page, R.

    1984-01-01

    Twelve patients (5 male, 7 female, mean age 37.9 +- 20) with pituitary tumors were extensively evaluated with NMR imaging using a 1.5K gauss resistive magnet. Saturation recovery (SR), inversion recovery (IR) and spin echo (SE) pulse sequences were used for qualitative characterization of the lesions. T/sub 1/ calculations were also performed for brain and pituitary. Tumor histology and endocrine status were correlated with NMR data. All tumors were large with suprasellar extension (6 with prolactin secretion, 6 without). Pituitary T/sub 1/'s ranged from .2 to .64, the mean T/sub 1/ being longer than that of brain (Brain = .4 +- .04; Pit = .48 +- .14). 3 patients with histological evidence of homogeneous adenomas had long T/sub 1/'s (0.58 +- .05). 3 patients with evidence of recent or old hemorhage into the pituitary had much shorter T/sub 1/'s (0.29 +- .12). There was no relationship between prolactin secretion and T/sub 1/. Qualitative T/sub 1/ and T/sub 2/ information can be obtained by using a combination of SR, IR, and SE images. Using this method in the patients, homogeneous adenomas had similar T/sub 1/'s and longer T/sub 2/'s compared to the brain, while patients with bleeds had shorter T/sub 1/'s and T/sub 2/'s. Image T/sub 1/ characteristics correlated well with the calculated T/sub 1/ values. The range of T/sub 1/ (and potentially T/sub 2/) values which occur in apparently similar lesions are most likely due to anatomical and pathophysiological variations in these lesions. It may be ultimately possible to separate different types of pathological processes based on NMR image T/sub 1/ and T/sub 2/ characteristics after careful comparative studies of NMR and histological data are completed. The combination of calculated T/sub 1/ and T/sub 2/ with image T/sub 1/ and T/sub 2/ information may also be useful in further characterization of lesions

  14. Wellbore Microannulus Characterization and Modeling.

    Energy Technology Data Exchange (ETDEWEB)

    Matteo, Edward N; Sobolik, Steven R.; Stormont, John C.; Taha, Mahmoud Reda; Gomez, Steven Paul

    2016-05-01

    Subsurface geologic formations used for extracting resources such as oil and gas can subsequently be used as a storage reservoir for the common greenhouse gas CO2, a concept known as Carbon Capture and Storage (CCS). Pre-existing wellbores penetrate the reservoirs where supercritical CO2 is to be injected. These wellbores can potentially be a pathway for contamination if CO2 leaks through wellbore flaws to an overlying aquifer or the atmosphere. Characterizing wellbore integrity and providing zonal isolation by repairing these wellbore flaws is of critical importance to the long-term isolation of CO2 and success of CCS. This research aims to characterize the microannulus region of the cement sheath-steel casing interface in terms of its compressibility and permeability. A mock-up of a wellbore system was used for lab-scale testing. Specimens, consisting of a cement sheath cast on a steel casing with microannuli, were subjected to confining pressures and casing pressures in a pressure vessel that allows simultaneous measurement of gas flow along the axis of the specimen. The flow was interpreted as the hydraulic aperture of the microannuli. Numerical models are used to analyze stress and displacement conditions along the casing-cement interface. These numerical results provide good agreement with closed-form elastic solutions. Numerical models incorporating flaws of varying dimensions along the casing-cement interface were then developed to describe the microannulus region. A joint model is used to describe the hydraulic aperture of the microannulus region, whose mechanical stiffness is altered in response to the imposed stress state across the joint interface. The aperture-stress behavior is based upon laboratory measurements of hydraulic aperture as a function of imposed stress conditions. This investigation found that microannulus permeability can satisfactorily be described by a joint model and that the constitutive

  15. Characterization of Prototype LSST CCDs

    Energy Technology Data Exchange (ETDEWEB)

    OCONNOR,P.; FRANK, J.; GEARY, J.C.; GILMORE, D.K.; KOTOV, I.; RADEKA, V.; TAKACS, P.; TYSON, J.A.

    2008-06-23

    The ambitious science goals of the Large Synoptic Survey Telescope (LSST) will be achieved in part by a wide-field imager that will achieve a new level of performance in terms of area, speed, and sensitivity. The instrument performance is dominated by the focal plane sensors, which are now in development. These new-generation sensors will make use of advanced semiconductor technology and will be complemented by a highly integrated electronics package located inside the cryostat. A test laboratory has been set up at Brookhaven National Laboratory (BNL) to characterize prototype sensors and to develop test and assembly techniques for eventual integration of production sensors and electronics into modules that will form the final focal plane. As described in [1], the key requirements for LSST sensors are wideband quantum efficiency (QE) extending beyond lpm in the red, control of point spread function (PSF), and fast readout using multiple amplifiers per chip operated in parallel. In addition, LSST's fast optical system (f71.25) places severe constraints on focal plane flatness. At the chip level this involves packaging techniques to minimize warpage of the silicon die, and at the mosaic level careful assembly and metrology to achieve a high coplanarity of the sensor tiles. In view of the long lead time to develop the needed sensor technology, LSST undertook a study program with several vendors to fabricate and test devices which address the most critical performance features [2]. The remainder of this paper presents key results of this study program. Section 2 summarizes the sensor requirements and the results of design optimization studies, and Section 3 presents the sensor development plan. In Section 4 we describe the test bench at BNL. Section 5 reports measurement results obtained to date oh devices fabricated by several vendors. Section 6 presents a summary of the paper and an outlook for the future work. We present characterization methods and results on

  16. Performance characterization of edge detectors

    Science.gov (United States)

    Ramesh, Visvanathan; Haralick, Robert M.

    1992-03-01

    Edge detection is the most fundamental step in vision algorithms. A number of edge detectors have been discussed in the computer vision literature. Examples of classic edge detectors include the Marr-Hildreth edge operator, facet edge operator, and the Canny edge operator. Edge detection using morphological techniques are attractive because they can be efficiently implemented in near real time machine vision systems that have special hardware support. However, little performance characterization of edge detectors has been done. In general, performance characterization of edge detectors has been done mainly by plotting empirical curves of performance. Quantitative performance evaluation of edge detectors was first performed by Abdou and Pratt. It is the goal of this paper to perform a theoretical comparison of gradient based edge detectors and morphological edge detectors. By assuming that an ideal edge is corrupted with additive noise we derive theoretical expressions for the probability of misdetection (the probability of labeling of a true edge pixel as a nonedge pixel in the output). Further, we derive theoretical expressions for the probability of false alarm (the probability of labeling of a nonedge pixel as an output edge pixel) by assuming that the input to the operator is a region of flat graytone intensity corrupted with additive Gaussian noise of zero mean and variance (sigma) 2. Even though the blurring step in the morphological operator introduces correlation in the additive noise, we make an approximation that the output samples after blurring are i.i.d. Gaussian random variables with zero mean and variance (sigma) 2/M where M is the window size of the blurring kernel. The false alarm probabilities obtained by using this approximation can be shown to be upperbounds of the false alarm probabilities computed without the approximation. The theory indicates that the blur- min operator is clearly superior when a 3 X 3 window size is used. Since we only have

  17. Natural phenomena hazards site characterization criteria

    Energy Technology Data Exchange (ETDEWEB)

    1994-03-01

    The criteria and recommendations in this standard shall apply to site characterization for the purpose of mitigating Natural Phenomena Hazards (wind, floods, landslide, earthquake, volcano, etc.) in all DOE facilities covered by DOE Order 5480.28. Criteria for site characterization not related to NPH are not included unless necessary for clarification. General and detailed site characterization requirements are provided in areas of meteorology, hydrology, geology, seismology, and geotechnical studies.

  18. Poliovirus strain characterization: a WHO Memorandum*

    OpenAIRE

    1980-01-01

    Reliable laboratory techniques for the intratypic characterization of poliovirus types 1, 2, and 3 isolates have an important role in the epidemiological surveillance of poliomyelitis and in studies of the safety and efficacy of poliovirus vaccines. Of the techniques available for poliovirus strain characterization, those potentially most useful are intratypic serodifferentiation and the biochemical techniques. The value of strain-specific (absorbed) antisera for antigenic characterization of...

  19. Isolation and characterization of methanogenic bacteria from ...

    African Journals Online (AJOL)

    Isolation and characterization of methanogenic bacteria from brewery wastewater in Kenya. Sylvia Injete Murunga, Duncan Onyango Mbuge, Ayub Njoroge Gitau, Urbanus Ndungwa Mutwiwa, Ingrid Namae Wekesa ...

  20. High-G Thermal Characterization Centrifuge

    Data.gov (United States)

    Federal Laboratory Consortium — High-G testing of thermal components enables improved understanding of operating behavior under military-relevant environments. The High-G Thermal Characterization...

  1. Production of Elastomeric Polypeptides for Materials Characterizations

    National Research Council Canada - National Science Library

    Urry, Dan

    2004-01-01

    .... Specifically, this effort is to provide 100 gram quantities of six and 10 gram quantities of an additional nine elastomeric polypeptides for conventional and specialized materials characterizations...

  2. Characterization of genetic structure of Podophyllum hexandrum ...

    African Journals Online (AJOL)

    Characterization of genetic structure of Podophyllum hexandrum populations, an endangered medicinal herb of Northwestern Himalaya, using ISSR-PCR markers and its relatedness with podophyllotoxin content.

  3. Axiomatic characterization of physical geometry

    International Nuclear Information System (INIS)

    Schmidt, H.J.

    1979-01-01

    This book deals with the foundations of a theory which can be considered as the most ancient part of physics, namely Euclidean geometry. It may be viewed as a partial realization of a program set up by G. Ludwig who suggested to formulate geometry explicity as a theory of possible operations with practically rigid bodies, using as basic concepts 'region', 'inclusion' and 'transport'. After an introduction to the problems, in which we sketch also the historical development, we develop a pre-theory with respect to the geometry with the aim to give an interpretation of the above-mentioned basic geometrical concepts in terms of notions which are closely related to experimental situations. The passage from a pure topological analysis of physical space to the differential geometrical view is made in the next section where we use the prerequisites established in the previous chapter to apply the Tits/Freudenthal solution of the Helmholtz-Lie problem. The main theorem of this book is stated in the last section by a characterization of Euclidean geometry. It turns out that two additional postulates are necessary whose empirical meaning we stress by referring to the axiom of dimension. The book might be of interest to scientist working in the field of axiomatics. Unfamiliar readers will be required to have a sound knowledge of topology and group theory. (HJ) 891 HJ/HJ 892 MB

  4. Laboratory characterization of rock joints

    Energy Technology Data Exchange (ETDEWEB)

    Hsiung, S.M.; Kana, D.D.; Ahola, M.P.; Chowdhury, A.H.; Ghosh, A. [Southwest Research Inst., San Antonio, TX (United States). Center for Nuclear Waste Regulatory Analyses

    1994-05-01

    A laboratory characterization of the Apache Leap tuff joints under cyclic pseudostatic and dynamic loads has been undertaken to obtain a better understanding of dynamic joint shear behavior and to generate a complete data set that can be used for validation of existing rock-joint models. Study has indicated that available methods for determining joint roughness coefficient (JRC) significantly underestimate the roughness coefficient of the Apache Leap tuff joints, that will lead to an underestimation of the joint shear strength. The results of the direct shear tests have indicated that both under cyclic pseudostatic and dynamic loadings the joint resistance upon reverse shearing is smaller than that of forward shearing and the joint dilation resulting from forward shearing recovers during reverse shearing. Within the range of variation of shearing velocity used in these tests, the shearing velocity effect on rock-joint behavior seems to be minor, and no noticeable effect on the peak joint shear strength and the joint shear strength for the reverse shearing is observed.

  5. Characterization of dry biopotential electrodes.

    Science.gov (United States)

    Xie, Li; Yang, Geng; Xu, Linlin; Seoane, Fernando; Chen, Qiang; Zheng, Lirong

    2013-01-01

    Driven by the increased interest in wearable long-term healthcare monitoring systems, varieties of dry electrodes are proposed based on different materials with different patterns and structures. Most of the studies reported in the literature focus on proposing new electrodes and comparing its performance with commercial electrodes. Few papers are about detailed comparison among different dry electrodes. In this paper, printed metal-plate electrodes, textile based electrodes, and spiked electrodes are for the first time evaluated and compared under the same experimental setup. The contact impedance and noise characterization are measured. The in-vivo electrocardiogram (ECG) measurement is applied to evaluate the overall performance of different electrodes. Textile electrodes and printed electrodes gain comparable high-quality ECG signals. The ECG signal obtained by spiked electrodes is noisier. However, a clear ECG envelope can be observed and the signal quality can be easily improved by backend signal processing. The features of each type of electrodes are analyzed and the suitable application scenario is addressed.

  6. Characterization of macrophage adhesion molecule

    International Nuclear Information System (INIS)

    Remold-O'Donnell, E.; Savage, B.

    1988-01-01

    Macrophage adhesion molecule (MAM), an abundant surface molecule which functions in the adhesion and spreading of guinea pig macrophages on surfaces, is characterized as a heterodimer of the trypsin- and plasmin-sensitive glycopeptide gp160 (MAM-α) and the glycopeptide gp93 (MAM-β). The density of MAM molecules is estimated at 630,000 per macrophage on the basis of quantitative binding of 125 I-labeled monoclonal antibody. The glycopeptide subunits display microheterogeneity on isoelectrofocusing; the pI is 5.8-6.3 for gp160 (MAM-α) and 6.4-7.0 for gp93 (MAM-β). A neutrophil gp160, gp93 molecule was shown to be indistinguishable from macrophage MAM on the basis of electrophoresis, isoelectrofocusing, and reactivity with 10 monoclonal antibodies. A related heterodimer of gp93 associated with a larger, antigenically different glycopeptide (gp180, gp93)was identified on circulating lymphocytes. Cumulative properties indicate that MAM is the guinea pig analog of human Mo1 and mouse Mac-1

  7. Geophysical characterization of subsurface barriers

    International Nuclear Information System (INIS)

    Borns, D.J.

    1995-08-01

    An option for controlling contaminant migration from plumes and buried waste sites is to construct a subsurface barrier of a low-permeability material. The successful application of subsurface barriers requires processes to verify the emplacement and effectiveness of barrier and to monitor the performance of a barrier after emplacement. Non destructive and remote sensing techniques, such as geophysical methods, are possible technologies to address these needs. The changes in mechanical, hydrologic and chemical properties associated with the emplacement of an engineered barrier will affect geophysical properties such a seismic velocity, electrical conductivity, and dielectric constant. Also, the barrier, once emplaced and interacting with the in situ geologic system, may affect the paths along which electrical current flows in the subsurface. These changes in properties and processes facilitate the detection and monitoring of the barrier. The approaches to characterizing and monitoring engineered barriers can be divided between (1) methods that directly image the barrier using the contrasts in physical properties between the barrier and the host soil or rock and (2) methods that reflect flow processes around or through the barrier. For example, seismic methods that delineate the changes in density and stiffness associated with the barrier represents a direct imaging method. Electrical self potential methods and flow probes based on heat flow methods represent techniques that can delineate the flow path or flow processes around and through a barrier

  8. Characterization of bioactive mixtures oligogalacturonidos

    International Nuclear Information System (INIS)

    Mederos Torres, Yuliem; Hormaza Montenegro, Josefa; Reynaldo Escobar, Ines; Montesino Sequi, Raquel

    2011-01-01

    Oligogalacturonides are pectic oligosaccharides composed of lineal chains of D-galacturonic acid, linked by α (1-4) glycosidic linkage. Oligogalacturonides' mixtures are obtained by enzymatic hydrolysis of pectins of diverse vegetal species. These oligosaccharides unchain a diverse biological activity in plants, which depends mainly on their polymerization degrees. The National Institute of Agricultural Science has a patent technology at national scale that lets to obtain a mixture of oligogalacturonides with different polymerization degree. In this work is presented the characterization of oligogalacturonides by spectrophotometric analysis attending to their uronic acids, reductor sugars, and neutral sugars content. Also the chromatographic profile of samples in study is obtained, using the derivatization with 2-aminobenzamide label and the separation by high pH anion exchange chromatography. It is achieved the separation of at least eight galacturonic acid oligomers with a variable degree of polymerization. On the other hand, the analysis by Fourier transform-infrared spectroscopy (FT-IR) showed that mixtures were composed by galacturonic acid salts. Results indicated that starting from two pectic acids with different characteristics, mixtures of oligogalacturonides of similar chemical composition could be obtained, but they differ in the proportion that they are presented

  9. Characterization of superconducting multilayers samples

    CERN Document Server

    Antoine, C Z; Berry, S; Bouat, S; Jacquot, J F; Villegier, J C; Lamura, G; Gurevich, A

    2009-01-01

    Best RF bulk niobium accelerating cavities have nearly reached their ultimate limits at rf equatorial magnetic field H  200 mT close to the thermodynamic critical field Hc. In 2006 Gurevich proposed to use nanoscale layers of superconducting materials with high values of Hc > HcNb for magnetic shielding of bulk niobium to increase the breakdown magnetic field inside SC RF cavities [1]. Depositing good quality layers inside a whole cavity is rather difficult but we have sputtered high quality samples by applying the technique used for the preparation of superconducting electronics circuits and characterized these samples by X-ray reflectivity, dc resistivity (PPMS) and dc magnetization (SQUID). Dc magnetization curves of a 250 nm thick Nb film have been measured, with and without a magnetron sputtered coating of a single or multiple stack of 15 nm MgO and 25 nm NbN layers. The Nb samples with/without the coating clearly exhibit different behaviors. Because SQUID measurements are influenced by edge an...

  10. Materials characterization at IMRE, Singapore

    International Nuclear Information System (INIS)

    Alfred Huan Cheng Hon

    2005-01-01

    Full text: This talk introduces the capabilities and work at the Materials Science and Characterisation Laboratory (MSCL) at the Institute of Materials Research and Engineering (IMRE), Singapore. The talk will illustrate how the characterization work augments the activities in materials research and provides crucial answers for key technological problems. Some work for industry will also be mentioned. Specifically, the discussion will centre upon the use of two surface analysis tools - namely, X-ray Photoelectron Spectroscopy (XPS) and Time-Of-Flight Secondary Ion Mass Spectroscopy (TOF-SIMS). The basic operating principles of these techniques will first be explained, followed by some details about instrumentation together with their comparative strengths, sensitivity and resolution limits. The interpretation and use of spectra for deriving information about the samples will be illustrated through examples from IMREs work. The key factors affecting the quality of the data obtained (including sample preparation) will also be highlighted. Finally, some comments on the outlook of new advances in instrumentation will be made. (Author)

  11. Mechanical Characterization of Mancos Shale

    Science.gov (United States)

    Broome, S.; Ingraham, M. D.; Dewers, T. A.

    2015-12-01

    A series of tests on Mancos shale have been undertaken to determine the failure surface and to characterize anisotropy. This work supports additional studies which are being performed on the same block of shale; fracture toughness, permeability, and chemical analysis. Mechanical tests are being conducted after specimens were conditioned for at least two weeks at 70% constant relative humidity conditions. Specimens are tested under drained conditions, with the constant relative humidity condition maintained on the downstream side of the specimen. The upstream is sealed. Anisotropy is determined through testing specimens that have been cored parallel and perpendicular to the bedding plane. Preliminary results show that when loaded parallel to bedding the shale is roughly 50% weaker. Test are run under constant mean stress conditions when possible (excepting indirect tension, unconfined compression, and hydrostatic). Tests are run in hydrostatic compaction to the desired mean stress, then differential stress is applied axially in displacement control to failure. The constant mean stress condition is maintained by decreasing the confining pressure by half of the increase in the axial stress. Results will be compared to typical failure criteria to investigate the effectiveness of capturing the behavior of the shale with traditional failure theory. Sandia National Laboratories is a multi-program laboratory managed and operated by Sandia Corporation, a wholly owned subsidiary of Lockheed Martin Corporation, for the U.S. Department of Energy's National Nuclear Security Administration under contract DE-AC04-94AL85000. SAND2015-6107 A.

  12. Multilayer Piezoelectric Stack Actuator Characterization

    Science.gov (United States)

    Sherrit, Stewart; Jones, Christopher M.; Aldrich, Jack B.; Blodget, Chad; Bao, Xioaqi; Badescu, Mircea; Bar-Cohen, Yoseph

    2008-01-01

    Future NASA missions are increasingly seeking to use actuators for precision positioning to accuracies of the order of fractions of a nanometer. For this purpose, multilayer piezoelectric stacks are being considered as actuators for driving these precision mechanisms. In this study, sets of commercial PZT stacks were tested in various AC and DC conditions at both nominal and extreme temperatures and voltages. AC signal testing included impedance, capacitance and dielectric loss factor of each actuator as a function of the small-signal driving sinusoidal frequency, and the ambient temperature. DC signal testing includes leakage current and displacement as a function of the applied DC voltage. The applied DC voltage was increased to over eight times the manufacturers' specifications to investigate the correlation between leakage current and breakdown voltage. Resonance characterization as a function of temperature was done over a temperature range of -180C to +200C which generally exceeded the manufacturers' specifications. In order to study the lifetime performance of these stacks, five actuators from one manufacturer were driven by a 60volt, 2 kHz sine-wave for ten billion cycles. The tests were performed using a Lab-View controlled automated data acquisition system that monitored the waveform of the stack electrical current and voltage. The measurements included the displacement, impedance, capacitance and leakage current and the analysis of the experimental results will be presented.

  13. Characterization of tinnitus in Nigeria.

    Science.gov (United States)

    Sogebi, Olusola Ayodele

    2013-08-01

    This study aimed to characterize tinnitus in middle aged and elderly out-patients attending a specialized clinic in a developing country. A cross sectional study of patients attending the ear, nose and throat (ENT) clinic of Olabisi Onabanjo University Teaching Hospital, OOUTH Sagamu, Nigeria. Data was collected with the use of a structured questionnaire. Data collected included socio demographics, medical history including experience of tinnitus, PTAs, BMI and BP. Data was analyzed using SPSS version 17.0. 79 patients had complaints of tinnitus thus making a crude prevalence of 14.5%, the prevalence increased steadily along the age groups. 51.9% of patients experienced tinnitus for a short period. 53.2% of the patients had symptoms referable to only one ear, while 54.4% had discrete as opposed to multiple types of tinnitus. Occurrence of intermittent symptoms was experienced by 75.9% of the patients and 70.9% were non-pulsatile in nature. Tinnitus was significantly associated with abnormal audiographic pattern, global increased hearing thresholds, high tone hearing loss, vertigo, hypertension and obesity. Tinnitus character was majorly short term, unilateral, discrete, intermittent, and non-pulsatile in nature, and it is associated with otological, audiological, anthropometric and cardiovascular anomalies. The characteristics of tinnitus in Nigerian patients were similar to those described in developed countries, but the major risk factors for tinnitus except hearing impairment, may be different from the latter. Copyright © 2012 Elsevier Ireland Ltd. All rights reserved.

  14. Dental imaging characterization of micropigs

    International Nuclear Information System (INIS)

    Lee, H.Y.; Choi, M.H.; Chang, J.H.; Jung, J.H.; Kim, M.E.; Lee, N.S.; Kim, J.Y.; Choi, M.C.

    2010-01-01

    Recently the micropig has been developed as human disease model. The dental and orofacial region of micropig is similar to that of humans, so it has been used for testing implant materials and techniques. The purpose of this study is on dental image at each age using radiography and computed tomography. Total twenty-two male micropigs, two or three animals of each 1, 3, 5, 7, 9, 12, 18 and 24 months old, were given radiographic examinations. After general anesthesia, extra- and intra-oral radiographic technique and computed tomographic scans were performed to assess the dental characterization of micropigs. The total deciduous dental formula comprised 28 teeth and was depicted as Di 3/3, Dc 1/1, Dp 3/3. The total permanent dental formula comprised 44 teeth and was depicted as I 3/3, C 1/1, P 4/4, M 3/3. Hypodontia of the first premolars was common in the micropig. The permanent teeth erupted from 3 to 24 month after birth. The sequence of eruption of the permanent teeth was M1, P1, I3, C, M2, I1 + P3 + P4, P2, I2, M3. Dental imaging enables visualization of the unerupted teeth and gives more information about the development of the teeth. The growth pattern of the teeth obtained through radiographic and computed tomographic examination provides basic data in the micropig as animal model for dental research

  15. Scattered light characterization of FORTIS

    Science.gov (United States)

    McCandliss, Stephan R.; Carter, Anna; Redwine, Keith; Teste, Stephane; Pelton, Russell; Hagopian, John; Kutyrev, Alexander; Li, Mary J.; Moseley, S. Harvey

    2017-08-01

    We describe our efforts to build a Wide-Field Lyman alpha Geocoronal simulator (WFLaGs) for characterizing the end-to-end sensitivity of FORTIS (Far-UV Off Rowland-circle Telescope for Imaging and Spectroscopy) to scattered Lyman α emission from outside of the nominal (1/2 degree)2 field-of-view. WFLaGs is a 50 mm diameter F/1 aluminum parabolic collimator fed by a hollow cathode discharge lamp with a 80 mm clear MgF2 window housed in a vacuum skin. It creates emission over a 10 degree FOV. WFLaGS will allow us to validate and refine a recently developed scattered light model and verify our scatter light mitigation strategies, which will incorporate low scatter baffle materials, and possibly 3-d printed light traps, covering exposed scatter centers. We present measurements of scattering intensity of Lyman alpha as a function of angle with respect to the specular reflectance direction for several candidate baffle materials. Initial testing of WFLaGs will be described.

  16. Characterizing and modeling citation dynamics.

    Directory of Open Access Journals (Sweden)

    Young-Ho Eom

    Full Text Available Citation distributions are crucial for the analysis and modeling of the activity of scientists. We investigated bibliometric data of papers published in journals of the American Physical Society, searching for the type of function which best describes the observed citation distributions. We used the goodness of fit with Kolmogorov-Smirnov statistics for three classes of functions: log-normal, simple power law and shifted power law. The shifted power law turns out to be the most reliable hypothesis for all citation networks we derived, which correspond to different time spans. We find that citation dynamics is characterized by bursts, usually occurring within a few years since publication of a paper, and the burst size spans several orders of magnitude. We also investigated the microscopic mechanisms for the evolution of citation networks, by proposing a linear preferential attachment with time dependent initial attractiveness. The model successfully reproduces the empirical citation distributions and accounts for the presence of citation bursts as well.

  17. Characterization of human septin interactions.

    Science.gov (United States)

    Sandrock, Kirstin; Bartsch, Ingrid; Bläser, Susanne; Busse, Anja; Busse, Eileen; Zieger, Barbara

    2011-08-01

    Septins constitute a group of GTP binding proteins that assemble into homo- and hetero-oligomeric complexes and filaments. These higher order septin structures are thought to function like scaffolds and/or diffusion barriers serving as spatial localizers for many proteins with key roles in cell polarity and cell cycle progression. In this study, we extensively characterized septin interaction partners using yeast two-hybrid and three-hybrid systems in addition to precipitation analyses in platelets. As a result, we identified human hetero-trimeric septin complexes on a large scale, which had been only postulated in the past. In addition, we illustrated roles of SEPT9 that might contribute to hetero-trimeric septin complex formation. SEPT9 can substitute for septins of the SEPT2 group and partially for SEPT7. Mutagenic analyses revealed that mutation of a potential phosphorylation site in SEPT7 (Y318) regulates the interaction with other septins. We identified several septin-septin interactions in platelets suggesting a regulatory role of diverse septin complexes in platelet function.

  18. Characterization of Vanadium Flow Battery

    DEFF Research Database (Denmark)

    Bindner, Henrik W.; Krog Ekman, Claus; Gehrke, Oliver

    This report summarizes the work done at Risø-DTU testing a vanadium flow battery as part of the project “Characterisation of Vanadium Batteries” (ForskEl project 6555) with the partners PA Energy A/S and OI Electric A/S under the Danish PSO energy research program. A 15kW/120kWh vanadium battery...... has been installed as part of the distributed energy systems experimental facility, SYSLAB, at Risø DTU. A test programme has been carried out to get hands-on experience with the technology, to characterize the battery from a power system point of view and to assess it with respect to integration...... of wind energy in the Danish power system. The battery has been in operation for 18 months. During time of operation the battery has not shown signs of degradation of performance. It has a round-trip efficiency at full load of approximately 60% (depending on temperature and SOC). The sources of the losses...

  19. Molecular characterization of opioid receptors

    Energy Technology Data Exchange (ETDEWEB)

    Howard, A.D.

    1986-01-01

    The aim of this research was to purify and characterize active opioid receptors and elucidate molecular aspects of opioid receptor heterogeneity. Purification to apparent homogeneity of an opioid binding protein from bovine caudate was achieved by solubilization in the non-ionic detergent, digitonin, followed by sequential chromatography on the opiate affinity matrix, ..beta..-naltrexylethylenediamine-CH-Sepharose 4B, and on the lectine affinity matrix, wheat germ agglutinin-agarose. Polyacrylamide gel electrophoresis in the presence of sodium dodecyl sulfate (SDS-PAGE) followed by autoradiography revealed that radioiodinated purified receptor gave a single band. Purified receptor preparations showed a specific activity of 12,000-15,000 fmol of opiate bound per mg of protein. Radioiodinated human beta-endorphin (/sup 125/I-beta-end/sub H/) was used as a probe to investigate the ligand binding subunits of mu and delta opioid receptors. /sup 125/I-beta-end/sub H/ was shown to bind to a variety of opioid receptor-containing tissues with high affinity and specificity with preference for mu and delta sites, and with little, if any, binding to kappa sites. Affinity crosslinking techniques were employed to covalently link /sup 125/I-beta-end/sub H/ to opioid receptors, utilizing derivatives of bis-succinimidyl esters that are bifunctional crosslinkers with specificities for amino and sulfhydryl groups. This, and competition experiments with high type-selective ligands, permitted the assignment of two labeled peptides to their receptor types, namely a peptide of M/sub r/ = 65,000 for mu receptors and one of M/sub r/ = 53,000 for delta receptors.

  20. Chemical characterization of marajoara ceramics

    International Nuclear Information System (INIS)

    Toyota, Rosimeiri Galbiati

    2009-01-01

    In this study the elemental concentration of Ce, Co, Cr, Cs, Eu, Fe, Hf, K, La, Lu, Na, Nd, Rb, Sc, Sm, Ta, Tb, Th, U, Yb and Zn were determined by instrumental neutron activation analysis (INAA) in 204 fragments of Marajoara archaeological ceramics, of which 156 were provided by the Archaeology and Ethnology Museum of Sao Paulo University (MAE) and 48 were provided by Dr. Denise Pahl Schaan, Marajo Museum curator. Also, 9 contemporary ceramics produced and marketed at Marajo Island were analyzed. Electron paramagnetic resonance (EPR) analyses were performed in 8 archaeological samples and 1 contemporary sample in order to identify the burning temperature of the samples. X-ray diffraction (XRD) analyses were performed in 13 archaeological samples and 2 contemporary samples for the investigation of their mineralogical composition. Mahalanobis distance was used for the study of outlier while modified filter was used for the study of the temper added to the ceramic paste. Result interpretation was performed using cluster analysis, principal components analysis and discriminant analysis. Procrustes analysis was used for variable selection and it showed that the Ce, Fe, Eu, Hf, K and Th variables are adequate for the characterization of the analyzed samples. The comparative study among the archaeological and contemporary ceramics showed the arrangement of two well-defined and close groups for the archaeological samples and a third, distant group for the contemporary ones. This result indicates that the archaeological and contemporary ceramics differ in their composition. EPR and XRD analysis were inconclusive for the differentiation of archaeological and contemporary ceramics. (author)

  1. Cytomorphological characterization of tea cultivars

    International Nuclear Information System (INIS)

    Rahman, H.; Khalil, I.H.; Shah, S.M.A.; Khanzada, T.Z.; Abbasi, F.M; Ahmad, H.; Shah, Z.

    2010-01-01

    Cytomorphological characterization was performed on tea cultivars, three each of Camellia sinensis and Camellia assamica species. For plant morphological study, one and a half year old healthy shoots were obtained from the selected mother bushes of the six tea cultivars. The field experiment conducted in randomized complete block design having four replications was aimed at evaluating plant height, number of leaves plant-l, number of branches plant-l, number of flowers plant-1, fresh and dry leaf weight plant-I. The data indicated significant difference between the two species with narrow leaved cultivars having increased plant height, number of leaves and branches plant-I than the broad leaved cultivars, but less number of flowers plant-l, fresh and dry leaf weight. Karyotype analysis indicated that both the groups are diploid with 2n = 30. On the basis of chromosome morphology, C. assamica had larger chromosomes (3-10.5 mu m) as compared to C. sinensis (3.9-8 mu m). C. assamica has relatively advanced features as compared to C. sinensis. However, both the groups possessed mostly median to sub-median centromeres with no secondary constrictions which possibly indicates that little or no evolutionary changes have taken place in tea and that the karyotype is still at a primitive stage, with C. sinensis being more primitive than C. assamica. Our results suggest that both the groups are different from each other in morphological as well as cytological attributes and could therefore generate more germplasm if the two species could be involved in tea breeding programs. (author)

  2. Characterize Human Forward Contamination Project

    Science.gov (United States)

    Rucker, Michelle

    2015-01-01

    Let's face it: wherever we go, we will inevitably carry along the little critters that live in and on us. Conventional wisdom has long held that it's unlikely those critters could survive the space environment, but in 2007 microscopic animals called Tardigrades survived exposure to space and in 2008 Cyanobacteria lived for 548 days outside the International Space Station (ISS). But what about the organisms we might reasonably expect a crewed spacecraft to leak or vent? Do we even know what they are? How long might our tiny hitch-hikers survive in close proximity to a warm spacecraft that periodically leaks/vents water or oxygen-and how might they mutate with long-duration exposure? Unlike the Mars rovers that we cleaned once and sent on their way, crew members will provide a constantly regenerating contaminant source. Are we prepared to certify that we can meet forward contamination protocols as we search for life at new destinations? This project has four technical objectives: 1. TEST: Develop a test plan to leverage existing equipment (i.e. ISS) to characterize the kinds of organisms we can reasonably expect pressurized, crewed volumes to vent or leak overboard; as part of testing, we'll need to develop an Extravehicular Activity (EVA)-compatible tool that can withstand the pressure and temperature extremes of space, as well as collect, separate, and store multiple samples; 2. ANALYSIS: Develop an analysis plan to study those organisms in relevant destination environments, including spacecraft-induced conditions; 3. MODEL: Develop a modeling plan to model organism transport mechanisms in relevant destination environments; 4. SHARE: Develop a plan to disseminate findings and integrate recommendations into exploration requirements & ops. In short, we propose a system engineering approach to roadmap the necessary experiments, analysis, and modeling up front--rather than try to knit together disparate chunks of data into a sensible conclusion after the fact.

  3. On characterizing terrain visibility graphs

    Directory of Open Access Journals (Sweden)

    William Evans

    2015-06-01

    Full Text Available A terrain is an $x$-monotone polygonal line in the $xy$-plane. Two vertices of a terrain are mutually visible if and only if there is no terrain vertex on or above the open line segment connecting them. A graph whose vertices represent terrain vertices and whose edges represent mutually visible pairs of terrain vertices is called a terrain visibility graph. We would like to find properties that are both necessary and sufficient for a graph to be a terrain visibility graph; that is, we would like to characterize terrain visibility graphs.Abello et al. [Discrete and Computational Geometry, 14(3:331--358, 1995] showed that all terrain visibility graphs are “persistent”. They showed that the visibility information of a terrain point set implies some ordering requirements on the slopes of the lines connecting pairs of points in any realization, and as a step towards showing sufficiency, they proved that for any persistent graph $M$ there is a total order on the slopes of the (pseudo lines in a generalized configuration of points whose visibility graph is $M$.We give a much simpler proof of this result by establishing an orientation to every triple of vertices, reflecting some slope ordering requirements that are consistent with $M$ being the visibility graph, and prove that these requirements form a partial order. We give a faster algorithm to construct a total order on the slopes. Our approach attempts to clarify the implications of the graph theoretic properties on the ordering of the slopes, and may be interpreted as defining properties on an underlying oriented matroid that we show is a restricted type of $3$-signotope.

  4. SHAPE CHARACTERIZATION OF CONCRETE AGGREGATE

    Directory of Open Access Journals (Sweden)

    Jing Hu

    2011-05-01

    Full Text Available As a composite material, the performance of concrete materials can be expected to depend on the properties of the interfaces between its two major components, aggregate and cement paste. The microstructure at the interfacial transition zone (ITZ is assumed to be different from the bulk material. In general, properties of conventional concrete have been found favoured by optimum packing density of the aggregate. Particle size is a common denominator in such studies. Size segregation in the ITZ among the binder particles in the fresh state, observed in simulation studies by concurrent algorithm-based SPACE system, additionally governs density as well as physical bonding capacity inside these shell-like zones around aggregate particles. These characteristics have been demonstrated qualitatively pertaining also after maturation of the concrete. Such properties of the ITZs have direct impact on composite properties. Despite experimental approaches revealed effects of aggregate grain shape on different features of material structure (among which density, and as a consequence on mechanical properties, it is still an underrated factor in laboratory studies, probably due to the general feeling that a suitable methodology for shape characterization is not available. A scientific argument hindering progress is the interconnected nature of size and shape. Presently, a practical problem preventing shape effects to be emphasized is the limitation of most computer simulation systems in concrete technology to spherical particles. New developments at Delft University of Technology will make it possible in the near future to generate jammed states, or other high-density fresh particle mixtures of non-spherical particles, which thereupon can be subjected to hydration algorithms. This paper will sketch the outlines of a methodological approach for shape assessment of loose (non-embedded aggregate grains, and demonstrate its use for two types of aggregate, allowing

  5. Characterization of ashes from biofuels

    Energy Technology Data Exchange (ETDEWEB)

    Frandsen, F.J.; Hansen, L.A. [Technical Univ. of Denmark. Dept. of Chemical Engineering (Denmark); Soerensen, H.S. [Geological Survey of Denmark and Greenland (Denmark); Hjuler, K. [dk-TEKNIK. Energy and Environment (Denmark)

    1998-02-01

    One motivation for initiating the present project was that the international standard method of estimating the deposit propensity of solid fuels, of which a number of variants exist (e.g. ISO, ASTM, SD, DIN), has shown to be unsuitable for biomass ashes. This goal was addressed by the development of two new methods for the detection of ash fusibility behaviour based on Simultaneous Thermal Analysis (STA) and High Temperature Light Microscopy (HTLM), respectively. The methods were developed specifically for ashes from biofuels, but are suitable for coal ashes as well. They have been tested using simple salt mixtures, geological standards and samples from straw CHP and coal-straw PF combustion plants. All samples were run in a nitrogen atmosphere at a heating rate of 10 deg. C/min. In comparison with the standard method, the new methods are objective and have superior repeatability and sensitivity. Furthermore, the two methods enable the melting behavior to be characterized by a continuous measurement of melt fraction versus temperature. Due to this two-dimensional resolution of the results, the STA and HTLM methods provide more information than the standard method. The study of bottom ash and fly ash as well as deposit samples from straw test firings at the Haslev and Slagelse Combined Heat and Power plants resulted in a better understanding of mineral behaviour during straw grate firing. In these tests a number of straws were fired which had been carefully selected for having different qualities with respect to sort and potassium and chlorine contents. By studying bottom ashes from Slagelse it was found that the melting behaviour correlated with the deposition rate on a probe situated at the outlet part of the combustion zone. (EG)

  6. Oil Slick Characterization with UAVSAR

    Science.gov (United States)

    Jones, C. E.; Holt, B.

    2017-12-01

    Although radar has long been used for mapping the spatial extent of oil slicks, its capability for characterizing oil, e.g., to discriminate thicker from thinner oil or mineral slicks from look-alikes, is far less well defined. In fact, the capability of SAR to quantify the oil-to-water ratio of emulsions within slicks on the open water was first demonstrated using UAVSAR data acquired over the 2010 Deepwater Horizon spill in the Gulf of Mexico [Minchew et al., 2012]. UAVSAR's capability was made possible by the airborne instrument's high signal-to-noise ratio, which enabled it to measure low backscatter signals from oil-smoothed water that are often near or below the noise floor of satellite SAR instruments. Since 2010, UAVSAR has been used to study oil slicks through experiments in Norway (2015) and the Gulf of Mexico. In November 2016, UAVSAR took part in a NOAA-led experiment to study remote sensing of oil slicks, which took place at the site of a persistent seep in the Gulf of Mexico. The goal was to use remote sensing to identify zones of thicker oil, which is the type of information that could direct emergency responders for more effective clean-up. The objectives of the experiment were to validate and compare different remote sensing methods' capabilities for measuring the thickness of oil within a slick on open water under environmental conditions typical of oil spills. In this presentation, we show the results from UAVSAR for determining oil thickness within a slick, and relate them to the standard method of oil slick classification, the Bonn Agreement oil appearance code used by trained observers in the field. This work was carried out in part at the Jet Propulsion Laboratory, California Institute of Technology, under contracts with the California Dept. of Water Resources and with the National Aeronautics and Space Administration.

  7. Rheological characterization of media containing Penicillium chrysogenum

    DEFF Research Database (Denmark)

    Pedersen, Annemarie Gade; Bundgaard-Nielsen, Mikael; Nielsen, Jens

    1993-01-01

    Samples from fed-batch fermentations of Penicillium chrysogenum on complex medium are rheologically characterized. The behavior is well described by a power law model for which the parameters are estimates. Furthermore, two types of model media are characterized and compared with the real...

  8. Material characterization of ancient Indian copper

    Indian Academy of Sciences (India)

    Keywords. Ancient Indian copper; material characterization; electrochemical behaviour; rust analysis; corrosion rate. Abstract. A chalcolithic (2350–1800 BC) copper chisel from Balathal has been characterized by X-ray diffraction, microstructural and electrochemical methods. The surface patina was composed of sulfates ...

  9. Synthesis and characterization of Trichloroisocyanouric acid ...

    Indian Academy of Sciences (India)

    Abstract. Trichloroisocyanouric acid (TCCA)-functionalized mesoporous silica nanocomposites (SBA/. TCCA) were synthesized and characterized for the acylation of indole. The uniform incorporation of TCCA inside the SBA-15 matrix was confirmed by standard characterization techniques (PXRD, Adsorption studies,. FT-IR ...

  10. Constant Width Planar Computation Characterizes ACC0

    DEFF Research Database (Denmark)

    Hansen, K.A.

    2004-01-01

    We obtain a characterization of ACC 0 in terms of a natural class of constant width circuits, namely in terms of constant width polynomial size planar circuits. This is shown via a characterization of the class of acyclic digraphs which can be embedded on a cylinder surface in such a way that all...

  11. Constant Width Planar Computation Characterizes ACC0

    DEFF Research Database (Denmark)

    Hansen, Kristoffer Arnsfelt

    2006-01-01

    We obtain a characterization of ACC0 in terms of a natural class of constant width circuits, namely in terms of constant width polynomial size planar circuits. This is shown via a characterization of the class of acyclic digraphs which can be embedded on a cylinder surface in such a way that all...

  12. Some Characterizations of Convex Interval Games

    NARCIS (Netherlands)

    Brânzei, R.; Tijs, S.H.; Alparslan-Gok, S.Z.

    2008-01-01

    This paper focuses on new characterizations of convex interval games using the notions of exactness and superadditivity. We also relate big boss interval games with concave interval games and obtain characterizations of big boss interval games in terms of exactness and subadditivity.

  13. Characterization of Geotechnical Properties of Lateritic Soil ...

    African Journals Online (AJOL)

    The purpose of this study was to characterize lateritic soil bentonite mixtures intended for use as low-permeability barrier in municipal waste disposal land ll. Characterization of the soil mixtures included measurement of Atterberg limits, compaction properties, hydraulic conductivity, shear strength, and desiccation shrinkage ...

  14. Physico-Chemical Characterization and Pollution Index ...

    African Journals Online (AJOL)

    Physico-Chemical Characterization and Pollution Index Determination of Leachates from Warri Waste Dumpsite, Southern Nigeria. ... This study characterizes the leachates quality of an active dumpsite in Warri, Delta State and also analyses its contamination or pollution potential. Leachate Pollution Index (LPI) - a tool for ...

  15. Axiomatic Characterizations of the Choquet Integral

    DEFF Research Database (Denmark)

    Groes, Ebbe; Whitta-Jacobsen, Hans Jørgen; Sloth, Birgitte

    The Choquet integral is an integral part of recent advances in decision theory involving non-additive measures. In this article we present two new axiomatic characterizations of this functional......The Choquet integral is an integral part of recent advances in decision theory involving non-additive measures. In this article we present two new axiomatic characterizations of this functional...

  16. Axiomatic Characterizations of the Choquet Integral

    DEFF Research Database (Denmark)

    Groes, Ebbe; Jacobsen, Hans Jørgen; Sloth, Birgitte

    1998-01-01

    The Choquet integral is an integral part of recent advances in decision theory involving non-additive measures. In this article we present two new axiomatic characterizations of this functional.......The Choquet integral is an integral part of recent advances in decision theory involving non-additive measures. In this article we present two new axiomatic characterizations of this functional....

  17. CHARACTERIZATION QUALITATIVE OF SOEL FOR A ...

    African Journals Online (AJOL)

    15 janv. 2015 ... ABSTRACT. The main objective of this study was to qualitatively characterize biomass of Solanum elaeagnifolium Cav. (or SOEL) to highlight the essential alternatives its valorization. At first, we studied the potential of composting biomass of this plant. The physico-chemical characterization of biomass ...

  18. Axiomatic Characterizations of IVF Rough Approximation Operators

    Directory of Open Access Journals (Sweden)

    Guangji Yu

    2014-01-01

    Full Text Available This paper is devoted to the study of axiomatic characterizations of IVF rough approximation operators. IVF approximation spaces are investigated. The fact that different IVF operators satisfy some axioms to guarantee the existence of different types of IVF relations which produce the same operators is proved and then IVF rough approximation operators are characterized by axioms.

  19. Morphological and molecular characterization of Amblyomma ...

    African Journals Online (AJOL)

    The association of most tick-borne pathogens with specific tick species has made it imperative that proper identification and characterization of such tick vectors is necessary for the purpose of developing effective tick and tick-borne control strategies. This study was undertaken to identify and characterize Amblyomma ...

  20. Processing and characterization of screen printing

    Indian Academy of Sciences (India)

    Home; Journals; Bulletin of Materials Science; Volume 39; Issue 2 ... Rheology; screen printing; perovskite-like material; oxygen membrane. ... were rheologically characterized, screen printed on three different porous alumina substrates and sintered at 1050 and 1150 ∘ C. The resulting membranes were characterized.

  1. Characterization monitoring & sensor technology crosscutting program

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1996-08-01

    The purpose of the Characterization, Monitoring, and Sensor Technology Crosscutting Program (CMST-CP) is to deliver appropriate characterization, monitoring, and sensor technology (CMST) to the OFfice of Waste Management (EM-30), the Office of Environmental Restoration (EM-40), and the Office of Facility Transition and Management (EM-60).

  2. 10 CFR 60.15 - Site characterization.

    Science.gov (United States)

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Site characterization. 60.15 Section 60.15 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) DISPOSAL OF HIGH-LEVEL RADIOACTIVE WASTES IN GEOLOGIC REPOSITORIES Licenses Preapplication Review § 60.15 Site characterization. (a) Prior to submittal of an application for a license to be...

  3. VLPC characterization for the Dzero upgrade

    International Nuclear Information System (INIS)

    1994-09-01

    The authors have studied the performance characteristics of approximately 4,000 Visible Light Photon Counters (VLPC) over a range of operating temperatures and biases. They will describe the characterization procedure and present the measured gain, noise, and relative quantum efficiency for the devices. They will also discuss the general operation of the devices and the significant problems encountered during the characterization

  4. Heavy truck rollover characterization (phase B).

    Science.gov (United States)

    2009-09-01

    The Heavy Truck Rollover Characterization Study - Phase-B builds on the results of prior phases of research. Phases 1 and 2 (Funded by Federal Highway Administration) involved heavy truck rollover characterization for a tractor and box-trailer; and P...

  5. Characterization of Exoplanet-Host Stars

    OpenAIRE

    Adibekyan, Vardan; Sousa, Sérgio G.; Santos, Nuno C.

    2017-01-01

    Precise and, if possible, accurate characterization of exoplanets cannot be dissociated from the characterization of their host stars. In this chapter we discuss different methods and techniques used to derive fundamental properties and atmospheric parameters of exoplanet-host stars. The main limitations, advantages and disadvantages, as well as corresponding typical measurement uncertainties of each method are presented.

  6. Characterization and intraspecific variation of Fusarium semitectum ...

    African Journals Online (AJOL)

    A total of 79 isolates of Fusarium semitectum were characterized by morphological and IGS-RFLP analysis to assess its intraspecific variation. Based on morphological characteristics, the isolates of F. semitectum were classified into 2 distinct groups, morphotypes I and II. Morphotype I was characterized by longer ...

  7. Purification, Characterization and Antibacterial Mechanism of ...

    African Journals Online (AJOL)

    Purpose: To carry out the extraction, purification and biological characterization, and assess the antibacterial activity of bacteriocin from Lactobacillus acidophilus XH1. Methods: Chloroform extraction method was used for bacteriocin extraction while characterization of bacteriocin was carried out by flat-dug well agar ...

  8. Characterization of radioactive waste forms and packages

    International Nuclear Information System (INIS)

    1997-01-01

    This publication provides a compendium of waste form, container and waste package properties which are potential importance for waste characterization to support approval for treatment/conditioning, storage and disposal methods and for predicting both short and long term waste behaviour in the repository environment. The properties to be characterized are defined in terms of the technical rationale for their control and characterization. Characterization methods for each property are described in general with reference to detailed discussions existing in the literature. Guidance as to the advantages and disadvantages of individual methods from a technical perspective is also provided where appropriate. This report deals with the characterization of all types of radioactive wastes except spent fuel intended for direct disposal. 115 refs, 17 figs, 12 tabs

  9. Characterization of MIPAS elevation pointing

    Directory of Open Access Journals (Sweden)

    M. Kiefer

    2007-01-01

    Full Text Available Sufficient knowledge of the pointing is essential for analyses of limb emission measurements. The scientific retrieval processor for MIPAS on ENVISAT operated at IMK allows the retrieval of pointing information in terms of tangent altitudes along with temperature. The retrieved tangent altitudes are independent of systematic offsets in the engineering Line-Of-Sight (LOS information delivered with the ESA Level 1b product. The difference of pointing retrieved from the reprocessed high resolution MIPAS spectra and the engineering pointing information was examined with respect to spatial/temporal behaviour. Among others the following characteristics of MIPAS pointing could be identified: Generally the engineering tangent altitudes are too high by 0–1.8 km with conspicuous variations in this range over time. Prior to December of 2003 there was a drift of about 50–100 m/h, which was due to a slow change in the satellite attitude. A correction of this attitude is done twice a day, which leads to discontinuities in the order of 1–1.5 km in the tangent altitudes. Occasionally discontinuities up to 2.5 km are found, as already reported from MIPAS and SCIAMACHY observations. After an update of the orbit position software in December 2003 values of drift and jumps are much reduced. There is a systematic difference in the mispointing between the poles which amounts to 1.5–2 km, i.e. there is a conspicuous orbit-periodic feature. The analysis of the correlation between the instrument's viewing angle azimuth and differential mispointing supports the hypotheses that a major part of this latter phenomenon can be attributed to an error in the roll angle of the satellite/instrument system of approximately 42 mdeg. One conclusion is that ESA level 2 data should be compared to other data exclusively on tangent pressure levels. Complementary to IMK data, ESA operational LOS calibration results were used to characterize MIPAS pointing. For this purpose

  10. Pretest characterization of WIPP experimental waste

    International Nuclear Information System (INIS)

    Johnson, J.; Davis, H.

    1991-01-01

    The Waste Isolation Pilot Plant (WIPP) near Carlsbad, New Mexico, is an underground repository designed for the storage and disposal of transuranic (TRU) wastes from US Department of Energy (DOE) facilities across the country. The Performance Assessment (PA) studies for WIPP address compliance of the repository with applicable regulations, and include full-scale experiments to be performed at the WIPP site. These experiments are the bin-scale and alcove tests to be conducted by Sandia National Laboratories (SNL). Prior to conducting these experiments, the waste to be used in these tests needs to be characterized to provide data on the initial conditions for these experiments. This characterization is referred to as the Pretest Characterization of WIPP Experimental Waste, and is also expected to provide input to other programmatic efforts related to waste characterization. The purpose of this paper is to describe the pretest waste characterization activities currently in progress for the WIPP bin-scale waste, and to discuss the program plan and specific analytical protocols being developed for this characterization. The relationship between different programs and documents related to waste characterization efforts is also highlighted in this paper

  11. Double tracks test site characterization report

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1996-05-01

    This report presents the results of site characterization activities performed at the Double Tracks Test Site, located on Range 71 North, of the Nellis Air Force Range (NAFR) in southern Nevada. Site characterization activities included reviewing historical data from the Double Tracks experiment, previous site investigation efforts, and recent site characterization data. The most recent site characterization activities were conducted in support of an interim corrective action to remediate the Double Tracks Test Site to an acceptable risk to human health and the environment. Site characterization was performed using a phased approach. First, previously collected data and historical records sere compiled and reviewed. Generalized scopes of work were then prepared to fill known data gaps. Field activities were conducted and the collected data were then reviewed to determine whether data gaps were filled and whether other areas needed to be investigated. Additional field efforts were then conducted, as required, to adequately characterize the site. Characterization of the Double Tracks Test Site was conducted in accordance with the US Department of Energy`s (DOE) Streamlined Approach for Environmental Restoration (SAFER).

  12. Characterization of amorphous and nanocrystalline carbon films

    International Nuclear Information System (INIS)

    Chu, Paul K.; Li Liuhe

    2006-01-01

    Amorphous and nanocrystalline carbon films possess special chemical and physical properties such as high chemical inertness, diamond-like properties, and favorable tribological proprieties. The materials usually consist of graphite and diamond microstructures and thus possess properties that lie between the two. Amorphous and nanocrystalline carbon films can exist in different kinds of matrices and are usually doped with a large amount of hydrogen. Thus, carbon films can be classified as polymer-like, diamond-like, or graphite-like based on the main binding framework. In order to characterize the structure, either direct bonding characterization methods or the indirect bonding characterization methods are employed. Examples of techniques utilized to identify the chemical bonds and microstructure of amorphous and nanocrystalline carbon films include optical characterization methods such as Raman spectroscopy, Ultra-violet (UV) Raman spectroscopy, and infrared spectroscopy, electron spectroscopic and microscopic methods such as scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS), Auger electron spectroscopy, transmission electron microscopy, and electron energy loss spectroscopy, surface morphology characterization techniques such as scanning probe microscopy (SPM) as well as other characterization methods such as X-ray reflectivity and nuclear magnetic resonance. In this review, the structures of various types of amorphous carbon films and common characterization techniques are described

  13. Exoplanet Characterization With Spitzer Eclipses

    Science.gov (United States)

    Harrington, Joseph

    We will analyze our existing Spitzer eclipse data for 11 exoplanets (GJ 436b, WASP-8b, WASP-29b, WASP-11b, TrES-1, WASP-34b, WASP-43b, HD 209458b, HAT-P-30b, HAT-P-13b, and WASP-12b) along with all other Spitzer eclipse and transit data for these systems (723 hours of total data). In combination with transit results, these measurements reveal the surface fluxes emitted by the planets' atmospheres in the six Spitzer bandpasses (3.6, 4.5, 5.8, 8.0, 16, and 24 1-4m), as well as orbital eccentricity and in a few cases possibly even precession rate. The fluxes, in turn, can constrain atmospheric composition and thermal profiles. We propose here to analyze data for these planets using Monte Carlo-driven, radiative-transfer, model-fitting codes; to conduct aggregate analyses; and to develop and share statistical modeling tools. Secondary eclipses provide us with a unique way to characterize exoplanetary atmospheres. Since other techniques like spectroscopy divide the planetary signal into many channels, they require very high signal-to-noise ratio (S/N) and are only possible for a few planets. Broadband eclipse photometry is thus the only technique that can measure dozens of atmospheres and identify the mechanisms that cause planets at a given irradiation level to behave so differently from one another. Until JWST becomes available, the broad variety of Spitzer data that we already have in hand, along with observations from the Hubble Space Telescope and possibly SOFIA, are our best way to understand the wide diversity of exoplanetary atmospheres. Since 2010, the team has produced six papers from a new, highly modular pipeline that implements optimal methods for analysis of Spitzer photometric time series, and our efficiency is increasing. The sensitivity needed for these measurements is up to 100 times better than Spitzer's design criteria, so careful treatment of systematic error is critically important and first-order approximations rarely work. The new pipeline

  14. Characterization of Cloud Water-Content Distribution

    Science.gov (United States)

    Lee, Seungwon

    2010-01-01

    The development of realistic cloud parameterizations for climate models requires accurate characterizations of subgrid distributions of thermodynamic variables. To this end, a software tool was developed to characterize cloud water-content distributions in climate-model sub-grid scales. This software characterizes distributions of cloud water content with respect to cloud phase, cloud type, precipitation occurrence, and geo-location using CloudSat radar measurements. It uses a statistical method called maximum likelihood estimation to estimate the probability density function of the cloud water content.

  15. Easy characterization of petroleum fractions: Part 1

    Energy Technology Data Exchange (ETDEWEB)

    Miquel, J. (Univ. Politecnica de Catalunya (Spain)); Castells, F. (Univ. Rovira i Virgili, Catalunya (Spain))

    1993-12-01

    A new method for characterizing petroleum fractions, based on pseudocomponent breakdown using the integral method has been developed. It requires only that one has an atmospheric true boiling point (tbp) distillation curve and known the entire fraction density. The proposed characterization procedure is valid for representing any oil fraction (light or heavy) with a boiling point range smaller than 300 K. It is based on the hypothesis of constant Watson's characterization factor, K[sub w], for all the pseudocomponents. Outside this range, it is less accurate (greater errors in material and molar balances). Therefore, a method considering the variable K[sub w] is best to treat these fractions.

  16. Plans for characterization of salt sites

    Energy Technology Data Exchange (ETDEWEB)

    Heim, G.E.; Matthews, S.C.; Kircher, J.F.; Kennedy, R.K.

    1983-01-01

    This basic salt site characterization program has been designed to provide the data required to support the design, performance assessment, and licensing of each of the principal project elements: the repository, the shafts, and the surface facilities. The work has been sequenced to meet the design and licensing schedule. It is anticipated that additional characterization activities will be performed to address site-specific considerations and to provide additional information to address questions which arise during the evaluation of characterization data. 3 figures, 3 tables.

  17. Characterization Well R-22 Geochemistry Report

    Energy Technology Data Exchange (ETDEWEB)

    Patrick Longmire

    2002-09-01

    This report provides analytical results for groundwater collected during four characterization-sampling rounds conducted at well R-22 from March 2001 through March 2002. Characterization well R-22 was sampled from March 6 through 13, 2001; June 19 through 26, 2001; November 30 through December 10, 2001; and February 27 through March 7, 2002. The goal of the characterization efforts was to assess the hydrochemistry and to determine whether or not contaminants are present in the regional aquifer in the vicinity of the well. A geochemical evaluation of the analytical results for the well is also presented in this report.

  18. Final Technical Report: Characterizing Emerging Technologies.

    Energy Technology Data Exchange (ETDEWEB)

    King, Bruce Hardison [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Hansen, Clifford [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Stein, Joshua [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Riley, Daniel [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Gonzalez, Sigifredo [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)

    2015-12-01

    The Characterizing Emerging Technologies project focuses on developing, improving and validating characterization methods for PV modules, inverters and embedded power electronics. Characterization methods and associated analysis techniques are at the heart of technology assessments and accurate component and system modeling. Outputs of the project include measurement and analysis procedures that industry can use to accurately model performance of PV system components, in order to better distinguish and understand the performance differences between competing products (module and inverters) and new component designs and technologies (e.g., new PV cell designs, inverter topologies, etc.).

  19. Nanoporous Gold: Fabrication, Characterization, and Applications

    Directory of Open Access Journals (Sweden)

    Michael L. Reed

    2009-12-01

    Full Text Available Nanoporous gold (np-Au has intriguing material properties that offer potential benefits for many applications due to its high specific surface area, well-characterized thiol-gold surface chemistry, high electrical conductivity, and reduced stiffness. The research on np-Au has taken place on various fronts, including advanced microfabrication and characterization techniques to probe unusual nanoscale properties and applications spanning from fuel cells to electrochemical sensors. Here, we provide a review of the recent advances in np-Au research, with special emphasis on microfabrication and characterization techniques. We conclude the paper with a brief outline of challenges to overcome in the study of nanoporous metals.

  20. Production, optimization, characterization and antifungal activity of ...

    African Journals Online (AJOL)

    SAM

    2014-04-02

    Apr 2, 2014 ... the present study, the antifungal activity of crude A. terrus chitinase was investigated against Apergillus niger, Aspergillus oryzae .... Chitinase activity was determined spectrophotometrically by estimating the amount of ..... characterization of two. Bifunctional chitinases lysozyme extracellularly produced by.

  1. Preparation and characterization of a novel benzimidazolium ...

    Indian Academy of Sciences (India)

    Hbbim] BF4) based on the benizimidazolium cation was synthesized and characterized. This new ionic liquid was successfully used as a suitable catalyst for the esterifications of carboxylic acids with aliphatic alcohols.

  2. THz characterization of hydrated and anhydrous materials

    Science.gov (United States)

    Sokolnikov, Andre

    2011-06-01

    The characterization of anhydrous and hydrated forms of materials is of great importance to science and industry. Water content poses difficulties for successful identification of the material structure by THz radiation. However, biological tissues and hydrated forms of nonorganic substances still may be investigated by THz radiation. This paper outlines the range of possibilities of the above characterization, as well as provides analysis of the physical mechanism that allows or prevents penetration of THz waves through the substance. THz-TDS is used to measure the parameters of the characterization of anhydrous and hydrated forms of organic and nonorganic samples. Mathematical methods (such as prediction models of time-series analysis) are used to help identifying the absorption coefficient and other parameters of interest. The discovered dependencies allow designing techniques for material identification/characterization (e.g. of drugs, explosives, etc. that may have water content). The results are provided.

  3. Characterization Of Glipizide-Loaded Polymethacrylate ...

    African Journals Online (AJOL)

    ® RS 100 and RL 100) by solvent evaporation method and characterized for their micromeritic properties and drug loading, as well as by Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy. In vitro release studies ...

  4. Synthesis and characterization of tetraethylammonium tetrachloro ...

    Indian Academy of Sciences (India)

    Unknown

    Synthesis and characterization of tetraethylammonium tetrachloro- cobaltate crystals. M A KANDHASWAMY and V SRINIVASAN*. Department of Physics, Sri Ramakrishna Mission Vidyalaya College of Arts and Science, Coimbatore 641 020, India. MS received 7 February 2000; revised 27 December 2001. Abstract.

  5. Laboratory Characterization of Solid Grade SW Brick

    National Research Council Canada - National Science Library

    Williams, Erin M; Akers, Stephen A; Reed, Paul A

    2007-01-01

    Personnel of the Geotechnical and Structures Laboratory, U.S. Army Engineer Research and Development Center, conducted a laboratory investigation to characterize the strength and constitutive property behavior of solid Grade SW brick...

  6. Biosynthesis, characterization and antimicrobial study of silver ...

    African Journals Online (AJOL)

    Both the characterization and antimicrobial activity test were very successful and could lead to significant economic viability, as well as being environmentally friendly for treatment of some infectious diseases. Keywords: Syzygium guineenses, Green Chemistry, Spectroscopy, Optoelectronics, Biomedical Sensors ...

  7. Biological synthesis and characterization of silver nanoparticles ...

    Indian Academy of Sciences (India)

    Biological synthesis and characterization of silver nanoparticles using. Eclipta alba leaf extract and evaluation of its cytotoxic and antimicrobial potential. PARAMASIVAM PREMASUDHA1, MUDILI VENKATARAMANA2,∗, MARRIAPPAN ABIRAMI3,. PERIYASAMY VANATHI4, KADIRVELU KRISHNA2 and RAMASAMY ...

  8. Optical characterization of epitaxial semiconductor layers

    CERN Document Server

    Richter, Wolfgang

    1996-01-01

    The last decade has witnessed an explosive development in the growth of expitaxial layers and structures with atomic-scale dimensions. This progress has created new demands for the characterization of those stuctures. Various methods have been refined and new ones developed with the main emphasis on non-destructive in-situ characterization. Among those, methods which rely on the interaction of electromagnetic radiation with matter are particularly valuable. In this book standard methods such as far-infrared spectroscopy, ellipsometry, Raman scattering, and high-resolution X-ray diffraction are presented, as well as new advanced techniques which provide the potential for better in-situ characterization of epitaxial structures (such as reflection anistropy spectroscopy, infrared reflection-absorption spectroscopy, second-harmonic generation, and others). This volume is intended for researchers working at universities or in industry, as well as for graduate students who are interested in the characterization of ...

  9. Synthesis and Characterization of Pyridine Functionalized ...

    African Journals Online (AJOL)

    picolyl) imidazolium salts (1). Treatment of the synthesized imidazolium salt with silver(I) oxide resulted in the formation of bis NHC silver(I) complex (2). The compound was characterized spectroscopically (NMR, mass spectrometry), by elemental ...

  10. Morphological characterization and evaluation of heat tolerance ...

    African Journals Online (AJOL)

    Morphological characterization and evaluation of heat tolerance traits in Nigerian goat breeds. M Wheto, BM Ilori, AJ Sanda, MA Adeleke, SO Durosaro, AS Adenaike, AO Adebambo, CON Ikeobi, OM Onagbesan, MO Ozoje, OA Adebambo ...

  11. Quantitative characterization of microstructure of asphalt mixtures

    Science.gov (United States)

    2010-10-01

    The microstructure of the fine aggregate matrix has a significant influence on the : mechanical properties and evolution of damage in an asphalt mixture. However, very little : work has been done to define and quantitatively characterize the microstr...

  12. Production and characterization of biosurfactant from Pseudomonas ...

    African Journals Online (AJOL)

    Further characterization of biosurfactant using Fourier transform infrared spectroscopy (FTIR) revealed it as a rhamnolipid. Keywords: Mangrove ecosystems, Pseudomonas aeruginosa, biosurfactant, critical micelle concentration (CMC), FT-IR fourier transform infrared spectroscopy (FTIR). African Journal of Biotechnology, ...

  13. Production and characterization of pectinases obtained from ...

    African Journals Online (AJOL)

    Production and characterization of pectinases obtained from Aspergillus fumigatus in submerged fermentation system using pectin extracted from mango peels as carbon source. AL Ezugwu, SOO Eze, FC Chilaka, CU Anyanwu ...

  14. Laboratory Characterization of White Masonry Concrete

    National Research Council Canada - National Science Library

    Williams, Erin M; Akers, Stephen A; Reed, Paul A

    2006-01-01

    ... to characterize the strength and constitutive property behavior of a white masonry concrete (WMC). Forty-four mechanical property tests consisting of two hydrostatic compression tests, four unconfined compression...

  15. Aerococcus urinae: polyphasic characterization of the species

    DEFF Research Database (Denmark)

    Christensen, JJ; Kilian, Mogens; Fussing, V

    2005-01-01

    A polyphasic characterization of Aerococcus urinae is presented. In this study the intraspecies relationships between 26 strains of varying geographical origin were examined by phenotypic tests, ribotyping and multilocus enzyme electrophoresis. The results demonstrated two main phenotypic patterns...

  16. Coordinate Measuring Machine for Characterizing Conformal Optics

    National Research Council Canada - National Science Library

    Jacobs, Stephen

    2001-01-01

    ... Nanotech 150AG Aspharic Grinder and the Nanotecnnologv Systems Nanotech 5OOFG Freeform Generator. The unique and complex nature of these parts prevented them from being characterized with standard optical metrology instrumentation...

  17. A Characterization of Ordinal Potential Games

    NARCIS (Netherlands)

    Voorneveld, M.; Norde, H.W.

    1996-01-01

    This note characterizes ordinal potential games by the absence of weak improvement cycles and an order condition on the strategy space.This order condition is automatically satisfied if the strategy space is countable.

  18. Characterization Testing - A Predictive Maintenance Advantage

    National Research Council Canada - National Science Library

    Randolph, Russ

    1998-01-01

    Knowing that a traditional time directed preventive maintenance program is limited in its flexibility and effectiveness, the CHAR 921 characterization system software was developed as an open architecture design...

  19. Laser Diode Beam Basics, Manipulations and Characterizations

    CERN Document Server

    Sun, Haiyin

    2012-01-01

    Many optical design technical books are available for many years which mainly deal with image optics design based on geometric optics and using sequential raytracing technique. Some books slightly touched laser beam manipulation optics design. On the other hand many books on laser diodes have been published that extensively deal with laser diode physics with little touching on laser diode beam manipulations and characterizations. There are some internet resources dealing with laser diode beams. However, these internet resources have not covered enough materials with enough details on laser diode beam manipulations and characterizations. A technical book concentrated on laser diode beam manipulations and characterizations can fit in to the open and provide useful information to laser diode users. Laser Diode Beam Basics, Manipulations and  Characterizations is concentrated on the very practical side of the subject, it only discusses the basic physics and mathematics that are necessary for the readers in order...

  20. Generalized characterization theorem for quantum logics

    Energy Technology Data Exchange (ETDEWEB)

    Mukherjee, M.K. (Birkbeck Coll., London (UK). Dept. of Mathematics)

    1984-08-11

    In this paper the underlying methematical structure of a quantum logic is assumed to form a partially ordered set and not a lattice and a theorem which characterizes orthomodular partially ordered sets is proved.

  1. Characterization of nanoparticles as candidate reference materials

    International Nuclear Information System (INIS)

    Martins Ferreira, E.H.; Robertis, E. de; Landi, S.M.; Gouvea, C.P.; Archanjo, B.S.; Almeida, C.A.; Araujo, J.R. de; Kuznetsov, O.; Achete, C.A.

    2013-01-01

    We report the characterization of three different nanoparticles (silica, silver and multi-walled carbon nanotubes) as candidate reference material. We focus our analysis on the size distribution of those particles as measured by different microscopy techniques. (author)

  2. Molecular characterization of intestinal protozoan parasites from ...

    African Journals Online (AJOL)

    Koffi Mathurin

    2014-02-17

    AJEST. African Journal of Environmental Science and. Technology. Full Length Research Paper. Molecular characterization of intestinal protozoan parasites from children facing diarrheal disease and associated risk factors in ...

  3. Formulation and Characterization of Biodegradable Medicated ...

    African Journals Online (AJOL)

    PEG)-600, tributyl citrate, PEG-200, PEG-300, PEG-400, PEG-4000, triethyl citrate and castor oil. The gum formulations were characterized for the following parameters: texture profile analysis (TPA), biodegradation, in vitro drug release using a ...

  4. What characterizes persons with poor mental health?

    DEFF Research Database (Denmark)

    Christensen, Anne Illemann; Davidsen, Michael; Kjøller, Mette

    2014-01-01

    analysed by means of logistic regression models. Results: Men and women with poor mental health are characterized by being single, having a long-term illness, not being able to rely on help from others in case of illness and by feeling that family and friends demand too much of them. Men with poor mental...... health were further characterized by being a heavy smoker, and having a BMI below 25. Women with poor mental health were further characterized by being 16-44 years old and sedentary in leisure time. CONCLUSIONS THE PREVALENCE OF POOR MENTAL HEALTH IS HIGHER AMONG WOMEN THAN MEN, AND DIFFERENT FACTORS...... CHARACTERIZE MEN AND WOMEN WITH POOR MENTAL HEALTH THE PRESENT FINDINGS SUPPORT THE NOTION THAT BOTH SOCIO-DEMOGRAPHICS AND LIFESTYLE FACTORS ARE INDEPENDENTLY RELATED WITH POOR MENTAL HEALTH WE SUGGEST TAKING INTO ACCOUNT ALL THESE AREAS OF LIFE WHEN PLANNING ACTIVITIES TO PREVENT POOR MENTAL HEALTH AND WHEN...

  5. Characterization of asphaltenes by nonaqueous capillary electrophoresis

    NARCIS (Netherlands)

    Kok, W.T.; Tüdös, A.J.; Grutters, M.; Shepherd, A.G.

    2011-01-01

    Nonaqueous capillary electrophoresis was used for the separation and characterization of asphaltene samples from different sources. For the separation medium (background electrolyte), mixtures of tetrahydrofuran and a high-permittivity organic solvent could be used. The best results were obtained

  6. Waianae Ecological Characterization Oahu, Hawaii 2004

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — The Waianae Ecological Characterization is a digital synthesis of historical and current physical, ecological, and cultural information about the Waianae moku, which...

  7. Characterization of Tri-lab Tantalum Plate.

    Energy Technology Data Exchange (ETDEWEB)

    Buchheit, Thomas E.; Cerreta, Ellen K.; Deibler, Lisa Anne; Chen, Shu-Rong; Michael, Joseph R.

    2014-09-01

    This report provides a detailed characterization Tri-lab Tantalum (Ta) plate jointly purchased from HCStark Inc. by Sandia, Los Alamos and Lawrence Livermore National Laboratories. Data in this report was compiled from series of material and properties characterization experiments carried out at Sandia (SNL) and Los Alamos (LANL) Laboratories through a leveraged effort funded by the C2 campaign. Results include microstructure characterization detailing the crystallographic texture of the material and an increase in grain size near the end of the rolled plate. Mechanical properties evaluations include, compression cylinder, sub-scale tension specimen, micohardness and instrumented indentation testing. The plate was found to have vastly superior uniformity when compare with previously characterized wrought Ta material. Small but measurable variations in microstructure and properties were noted at the end, and at the top and bottom edges of the plate.

  8. CHARACTERIZING SITE HYDROLOGY (WORKSHOP MSA PRESENTATION)

    Science.gov (United States)

    Hydrogeology is the foundation of subsurface site characterization for evaluations of monitored natural attenuation (MNA). Three case studies are presented. Examples of the potentially detrimental effects of drilling additives on ground-water samples from monitoring wells are d...

  9. Characterizing Site Hydrology (Region 10, Seattle, WA)

    Science.gov (United States)

    Hydrogeology is the foundation of subsurface site characterization for evaluations of monitored natural attenuation (MNA). Three case studies are presented. Examples of the potentially detrimental effects of drilling additives on ground-water samples from monitoring wells are d...

  10. CHARACTERIZING SITE HYDROLOGY (REGION 8 WORKSHOP)

    Science.gov (United States)

    Hydrogeology is the foundation of subsurface site characterization for evaluations of monitored natural attenuation (MNA). Three case studies are presented. Examples of the potentially detrimental effects of drilling additives on ground-water samples from monitoring wells are d...

  11. Electrochemical synthesis and spectroscopic characterization of ...

    African Journals Online (AJOL)

    phenylpyrrole) coatings in an organic medium on iron and platinum electrodes. ... XPS measurements, infrared (FT-IR) and electronic absorption (UV-vis) spectroscopies were used to characterize the iron and platinum-coated electrodes. Finally the ...

  12. Characterization of Crushed Base Materials in Wyoming

    Science.gov (United States)

    2017-08-01

    To improve the pavement design and construction in Wyoming, the Wyoming Department of Transportation (WYDOT) is adopting the Mechanistic-Empirical Pavement Design Guide (MEPDG). A full implementation of MEPDG requires the characterization of local cr...

  13. Synthesis, characterization and electrochemistry of heterobimetallic ...

    African Journals Online (AJOL)

    dimethylpyrazolyl) borate with a series of manganese(II) Schiff bases have been synthesized. Characterization by UV, IR, MS and elemental analysis support their formulations. Cyclic and differential pulse voltammograms of manganese(II) Schiff base ...

  14. Characterization of 21 Strains of Bacillus Anthracis

    National Research Council Canada - National Science Library

    Kournikakis, B

    2000-01-01

    Twenty-one strains of Bacillus anthracis currently held in the culture collection at DRES were characterized by colonial morphology, antibiotic sensitivity and BiologTM metabolic identification profiles...

  15. Goniometric characterization of LED based greenhouse lighting

    DEFF Research Database (Denmark)

    Thorseth, Anders; Lindén, Johannes; Corell, Dennis Dan

    2015-01-01

    This paper describes a demonstration of goniospectroradiometry for characterizations of new light emitting diode (LED) based luminaries for enhanced photosynthesis in greenhouses. It highlights the differences between measurement of the traditional high pressure sodium (HPS) luminaries and the LED...

  16. Tank waste remediation system characterization project quality policies. Revision 1

    International Nuclear Information System (INIS)

    Trimble, D.J.

    1995-01-01

    These Quality Policies (QPs) describe the Quality Management System of the Tank Waste Characterization Project (hereafter referred to as the Characterization Project), Tank Waste Remediation System (TWRS), Westinghouse Hanford Company (WHC). The Quality Policies and quality requirements described herein are binding on all Characterization Project organizations. To achieve quality, the Characterization Project management team shall implement this Characterization Project Quality Management System

  17. Entropy Characterization of Random Network Models

    Directory of Open Access Journals (Sweden)

    Pedro J. Zufiria

    2017-06-01

    Full Text Available This paper elaborates on the Random Network Model (RNM as a mathematical framework for modelling and analyzing the generation of complex networks. Such framework allows the analysis of the relationship between several network characterizing features (link density, clustering coefficient, degree distribution, connectivity, etc. and entropy-based complexity measures, providing new insight on the generation and characterization of random networks. Some theoretical and computational results illustrate the utility of the proposed framework.

  18. Cloning and Biochemical Characterization of HIV Integrase

    Science.gov (United States)

    1989-12-15

    biochemical assays for the interaction of the HIV Intebration protein, IN, with a specific DNA target, the viral LTRs. The gene encoding IN has been subcloned ...FILE COPY CO CONTRACT NO.: DAMD7-88-C-8126 r TITLE: CLONING AND BIOCHEMICAL CHARACTERIZATION OF HIV INTEGRASE I- SPRINCIPAL INVESTIGATOR: ELLEN...ELEMENT No. NO. 392- NO. IACCESSION NO. 1 . TITLE (indude Security Classification)630A I315D49C08 (U) Cloning and Biochemical Characterization of the HIV

  19. Electric Propulsion System Characterization through Experiments

    OpenAIRE

    Hattenberger, Gautier; Drouin, Antoine; Bronz, Murat

    2016-01-01

    International audience; Electrical propulsion system characteristics are very important in UAV design, operation and control. This article presents the characterization of electric propulsion sets through experiments. A motor test bench have been build based on previous experience in order to improve the quality of the measurements. Moreover, the bench fits in a wind tunnel, allowing to perform a complete characterization over the full airspeed range of the considered mini and micro-UAVs. Aft...

  20. Characterizing changes in marine ecosystem services

    OpenAIRE

    Chan, Kai MA; Ruckelshaus, Mary

    2010-01-01

    The benefits of marine ecosystems for people are increasingly being characterized through the concept of ecosystem services, with the promise to aid decision making from marine spatial planning to ecosystem-based management. The characterization of changes in marine ecosystem services is central to the application of ecological science to policy contexts, and this field is quickly evolving with innovations in frameworks for integrating science, understanding of ecosystems and human benefits, ...

  1. In-situ characterization of heterogeneous catalysts

    CERN Document Server

    Rodriguez, Jose A; Chupas, Peter J

    2013-01-01

    Helps researchers develop new catalysts for sustainable fuel and chemical production Reviewing the latest developments in the field, this book explores the in-situ characterization of heterogeneous catalysts, enabling readers to take full advantage of the sophisticated techniques used to study heterogeneous catalysts and reaction mechanisms. In using these techniques, readers can learn to improve the selectivity and the performance of catalysts and how to prepare catalysts as efficiently as possible, with minimum waste. In-situ Characterization of Heterogeneous Catalysts feat

  2. A macroecological characterization of infectious disease transmission:

    DEFF Research Database (Denmark)

    Andersen-Ranberg, Emilie Ulrikka

    2017-01-01

    Presentation: Per M. Jensen*, Miguel L. Grilo, Christian B. Pipper, Emilie U. Andersen-Ranberg. A macroecological characterization of infectious disease transmission: the cases of Mycobacterium and Leptospira sp. The 2017 OIKOS meeting, 10th -11th March 2017, Copenhagen, Denmark......Presentation: Per M. Jensen*, Miguel L. Grilo, Christian B. Pipper, Emilie U. Andersen-Ranberg. A macroecological characterization of infectious disease transmission: the cases of Mycobacterium and Leptospira sp. The 2017 OIKOS meeting, 10th -11th March 2017, Copenhagen, Denmark...

  3. Synthesis and characterization of polypyrrole grafted chitin

    Science.gov (United States)

    Ramaprasad, A. T.; Latha, D.; Rao, Vijayalakshmi

    2017-05-01

    Synthesis and characterization of chitin grafted with polypyrrole (PPy) is reported in this paper. Chitin is soaked in pyrrole solution of various concentrations for different time intervals and polymerized using ammonium peroxy disulphate (APS) as an initiator. Grafting percentage of polypyrrole onto chitin is calculated from weight of chitin before and after grafting. Grafting of polymer is further verified by dissolution studies. The grafted polymer samples are characterized by FTIR, UV-Vis absorption spectrum, XRD, DSC, TGA, AFM, SEM and conductivity studies.

  4. Application of geophysical methods for fracture characterization

    International Nuclear Information System (INIS)

    Lee, K.H.; Majer, E.L.; McEvilly, T.V.; California Univ., Berkeley, CA; Morrison, H.F.; California Univ., Berkeley, CA

    1990-01-01

    One of the most crucial needs in the design and implementation of an underground waste isolation facility is a reliable method for the detection and characterization of fractures in zones away from boreholes or subsurface workings. Geophysical methods may represent a solution to this problem. If fractures represent anomalies in the elastic properties or conductive properties of the rocks, then the seismic and electrical techniques may be useful in detecting and characterizing fracture properties. 7 refs., 3 figs

  5. K Basin spent nuclear fuel characterization

    International Nuclear Information System (INIS)

    LAWRENCE, L.A.

    1999-01-01

    The results of the characterization efforts completed for the N Reactor fuel stored in the Hanford K Basins were Collected and summarized in this single referencable document. This summary provides a ''road map'' for what was done and the results obtained for the fuel characterization program initiated in 1994 and scheduled for completion in 1999 with the fuel oxidation rate measurement under moist inert atmospheres

  6. Radiological characterization of a relevant facility

    International Nuclear Information System (INIS)

    Barberis, Claudia M.; Madariaga, Marcelo

    2009-01-01

    The objective of this work is the radiological characterization of a Nuclear Installation, the RA-1 nuclear reactor. By means of this characterization all the information about amount, type and distribution of radionuclides in the installation will be available. Thus the order of magnitude of the activities that will be involved in the removal of the different materials, at the moment of the decommissioning, will be established. (author)

  7. K Basin spent nuclear fuel characterization

    Energy Technology Data Exchange (ETDEWEB)

    LAWRENCE, L.A.

    1999-02-10

    The results of the characterization efforts completed for the N Reactor fuel stored in the Hanford K Basins were Collected and summarized in this single referencable document. This summary provides a ''road map'' for what was done and the results obtained for the fuel characterization program initiated in 1994 and scheduled for completion in 1999 with the fuel oxidation rate measurement under moist inert atmospheres.

  8. Three dimensional characterization and archiving system

    International Nuclear Information System (INIS)

    Sebastian, R.L.; Clark, R.; Gallman, P.

    1995-01-01

    The Three Dimensional Characterization and Archiving System (3D-ICAS) is being developed as a remote system to perform rapid in situ analysis of hazardous organics and radionuclide contamination on structural materials. Coleman Research and its subcontractors, Thermedics Detection, Inc. (TD) and the University of Idaho (UI) are in the second phase of a three phase program to develop 3D-ICAS to support Decontamination and Decommissioning (D ampersand D) operations. Accurate physical characterization of surfaces and the radioactive and organic is a critical D ampersand D task. Surface characterization includes identification of potentially dangerous inorganic materials, such as asbestos and transite. Real-time remotely operable characterization instrumentation will significantly advance the analysis capabilities beyond those currently employed. Chemical analysis is a primary area where the characterization process will be improved. Chemical analysis plays a vital role throughout the process of decontamination. Before clean-up operations can begin the site must be characterized with respect to the type and concentration of contaminants, and detailed site mapping must clarify areas of both high and low risk. During remediation activities chemical analysis provides a means to measure progress and to adjust clean-up strategy. Once the clean-up process has been completed the results of chemical analysis will verify that the site is in compliance with federal and local regulations

  9. Readiness to proceed: Characterization planning basis

    International Nuclear Information System (INIS)

    Adams, M.R.

    1998-01-01

    This report summarizes characterization requirements, data availability, and data acquisition plans in support of the Phase 1 Waste Feed Readiness to Proceed Mid-Level Logic. It summarizes characterization requirements for the following program planning documents: Waste Feed Readiness Mid-Level Logic and Decomposition (in development); Master blue print (not available); Tank Waste Remediation System (TWRS) Operations and Utilization Plan and Privatization Contract; Enabling assumptions (not available); Privatization low-activity waste (LAW) Data Quality Objective (DQO); Privatization high-level waste (HLW) DQO (draft); Problem-specific DQOs (in development); Interface control documents (draft). Section 2.0 defines the primary objectives for this report, Section 3.0 discusses the scope and assumptions, and Section 4.0 identifies general characterization needs and analyte-specific characterization needs or potential needs included in program documents and charts. Section 4.0 also shows the analyses that have been conducted, and the archive samples that are available for additional analyses. Section 5.0 discusses current plans for obtaining additional samples and analyses to meet readiness-to-proceed requirements. Section 6.0 summarizes sampling needs based on preliminary requirements and discusses other potential characterization needs. Many requirements documents are preliminary. In many cases, problem-specific DQOs have not been drafted, and only general assumptions about the document contents could be obtained from the authors. As a result, the readiness-to-proceed characterization requirements provided in this document are evolving and may change

  10. Summary status of K Basins sludge characterization

    International Nuclear Information System (INIS)

    Baker, R.B.

    1995-01-01

    A number of activities are underway as part of the Spent Nuclear Fuels Project (SNFP) related to the processing and disposing of sludge in the 105-K Basins (K Basins). Efforts to rigorously define data requirements for these activities are being made using the Data Quality Objectives (DQO) process. Summaries of current sludge characterization data are required to both help support this DQO process and to allow continued progress with on-going engineering activities (e.g., evaluations of disposal alternatives). This document provides the status of K Basins sludge characterization data currently available to the Nuclear Fuel Evaluations group. This group is tasked by the SNFP to help develop and maintain the characterization baseline for the K Basins. The specific objectives of this document are to: (1) provide a current summary (and set of references) of sludge characterization data for use by SNFP initiatives, to avoid unnecessary duplication of effort and to support on-going initiatives; (2) submit these data to an open forum for review and comment, and identify additional sources of significant data that may be available; (3) provide a summary of current data to use as part of the basis to develop requirements for additional sludge characterization data through the DQO process; (4) provide an overview of the intended activities that will be used to develop and maintain the sludge characterization baseline

  11. Three dimensional characterization and archiving system

    Energy Technology Data Exchange (ETDEWEB)

    Sebastian, R.L.; Clark, R.; Gallman, P. [and others

    1995-12-01

    The Three Dimensional Characterization and Archiving System (3D-ICAS) is being developed as a remote system to perform rapid in situ analysis of hazardous organics and radionuclide contamination on structural materials. Coleman Research and its subcontractors, Thermedics Detection, Inc. (TD) and the University of Idaho (UI) are in the second phase of a three phase program to develop 3D-ICAS to support Decontamination and Decommissioning (D&D) operations. Accurate physical characterization of surfaces and the radioactive and organic is a critical D&D task. Surface characterization includes identification of potentially dangerous inorganic materials, such as asbestos and transite. Real-time remotely operable characterization instrumentation will significantly advance the analysis capabilities beyond those currently employed. Chemical analysis is a primary area where the characterization process will be improved. Chemical analysis plays a vital role throughout the process of decontamination. Before clean-up operations can begin the site must be characterized with respect to the type and concentration of contaminants, and detailed site mapping must clarify areas of both high and low risk. During remediation activities chemical analysis provides a means to measure progress and to adjust clean-up strategy. Once the clean-up process has been completed the results of chemical analysis will verify that the site is in compliance with federal and local regulations.

  12. Surface characterization protocol for precision aspheric optics

    Science.gov (United States)

    Sarepaka, RamaGopal V.; Sakthibalan, Siva; Doodala, Somaiah; Panwar, Rakesh S.; Kotaria, Rajendra

    2017-10-01

    In Advanced Optical Instrumentation, Aspherics provide an effective performance alternative. The aspheric fabrication and surface metrology, followed by aspheric design are complementary iterative processes for Precision Aspheric development. As in fabrication, a holistic approach of aspheric surface characterization is adopted to evaluate actual surface error and to aim at the deliverance of aspheric optics with desired surface quality. Precision optical surfaces are characterized by profilometry or by interferometry. Aspheric profiles are characterized by contact profilometers, through linear surface scans to analyze their Form, Figure and Finish errors. One must ensure that, the surface characterization procedure does not add to the resident profile errors (generated during the aspheric surface fabrication). This presentation examines the errors introduced post-surface generation and during profilometry of aspheric profiles. This effort is to identify sources of errors and is to optimize the metrology process. The sources of error during profilometry may be due to: profilometer settings, work-piece placement on the profilometer stage, selection of zenith/nadir points of aspheric profiles, metrology protocols, clear aperture - diameter analysis, computational limitations of the profiler and the software issues etc. At OPTICA, a PGI 1200 FTS contact profilometer (Taylor-Hobson make) is used for this study. Precision Optics of various profiles are studied, with due attention to possible sources of errors during characterization, with multi-directional scan approach for uniformity and repeatability of error estimation. This study provides an insight of aspheric surface characterization and helps in optimal aspheric surface production methodology.

  13. Characterization and modulation of femtosecond laser pulse

    International Nuclear Information System (INIS)

    Dorrer, Christophe

    1999-01-01

    This work brings some solutions to the characterization and control of femtosecond laser pulses. Spectral interferometry has been extensively studied; whereas this is a rather old technique, it has found new specific applications to short pulses. Several important points concerning the experimental implementation of this technique are treated. Sources of errors have been tracked and simple solutions have been found to enhance its reliability. A recently demonstrated technique for the complete characterization of short pulses has been used to characterize short pulses from Chirped Pulse Amplification Systems. This transposition of shearing interferometry to the optical frequency domain, known as Spectral Phase Interferometry for Direct Electric-field Reconstruction (SPlDER), is conceptually very interesting: for example, the inversion from the experimental data to the electric field to be characterized is completely algebraic. A reliable tool for the characterization and optimization of Chirped pulse amplification systems has been built on this principle. This is the first single-shot real-time characterization implementation of this technique. An improvement of the method has also allowed the first single-shot real-time characterization of a short pulse using a single mono-dimensional integrative detector and an algebraic inversion of the experimental data. The control of these pulses is also of prior interest. Through a collaboration with Thomson CSF-LCR, the demonstration of the use of an optically addressed light valve at the Fourier plane of a zero-dispersion line for spectral phase modulation has been made. This device allows a high-resolution control of the spectral phase of a short pulse. It is a well-adapted tool for the correction of the residual spectral phase, at the output of Chirped Pulse Amplification systems and the temporal synthesis of shaped pulses for specific experiments. (author) [fr

  14. Thermal analysis of Brazilian standards proposals for social residential buildings; Avaliacao termica das propostas de normas brasileiras para edificacoes de interesse social

    Energy Technology Data Exchange (ETDEWEB)

    Dilkin, Pedro [Universidade Regional do Noroeste do Estado do Rio Grande do Sul, Ijui, RSA (Brazil). Dept. de Fisica, Estatistica e Matematica]. E-mail: dilkin@main.unijui.tche.br; Schneider, Paulo Smith [Rio Grande do Sul Univ., Porto Alegre, RS (Brazil). Dept. de Engenharia Mecanica]. E-mail: pss@mecanica.ufrgs.br

    2000-07-01

    This work presents a critical analysis of national proposals of standards for the thermal performance of simple residential buildings. A review of some international standards is performed together with the description of the national proposals of standards, and a prototype of a house is assembled, following each one of the texts. Results are displayed and the prototypes are simulated using the TRNSYS environment, concerning winter and summer periods of Porto Alegre. Finally, the national proposal that achieved the best performance is improved by means new simulations. (author)

  15. Simplified model of the thermal evolution of the fuel dry storage; Modelo simplificado de la evolucion termica del combustible en almacenamiento en seco

    Energy Technology Data Exchange (ETDEWEB)

    Penalva, J.; Feria, F.; Herranz, L. E.

    2013-07-01

    The objective of this work is to establish a model that allows to determine easily temperature of the fuel burned and time out of reactor. The model will depend on the selected storage system, but the established methodology lays the groundwork for your application to any other case. to obtain the temperature has been used the FLUENT code, based on a model 3D itself and in the heat of decay at different burn (30-60 MWd/kgU) calculated with origin (information available in the literature). Of the different simulations carried out has developed a 3D map of temperature versus burned and time out of reactor, which has allowed to develop an equation simplified.

  16. Evaluation of thermal stability of paraffin wax by differential scanning calorimetry; Avaliacao da estabilidade termica de parafina por calorimetria diferencial de varredura

    Energy Technology Data Exchange (ETDEWEB)

    Godinho, K.O.; Silva, A.G.P.; Holanda, J.N.F. [Universidade Estadual do Norte Fluminense (LAMAV/UENF), Campos dos Goytacazes, RJ (Brazil). Grupo de Materiais Ceramicos], Email: holanda@uenf.br

    2010-07-01

    Phase change materials for heat storage are used as passive solar energy storage materials, which can be impregnated into construction materials. In this work the thermal stability (heating/cooling cycle) of the paraffin wax was investigated using differential scanning calorimetry. The latent heat and fusion temperature were determined for the following thermal cycles: 0, 30, 180 and 360. The thermal stability for paraffin wax infiltrated in support of gypsum was also determined. The experimental results showed that the paraffin wax showed good thermal stability in the states pure and infiltrated for up to 360 thermal cycles. (author)

  17. Development of method to chemical separation of gallium-67 by thermal diffusion technique; Desenvolvimento de metodo para separacao quimica de galio-67 pela tecnica de difusao termica

    Energy Technology Data Exchange (ETDEWEB)

    Martins, Patricia de Andrade

    2012-07-01

    Radioisotopes of gallium have been studied and evaluated for medical applications since 1949. Over the past 50 years {sup 67}Ga has been widely used in the diagnosis of various diseases, including acute and chronic inflammatory lesions, bacterial or sterile and several types of tumors. In Brazil 30% of clinics that provide services for Nuclear Medicine use {sup 67}Ga citrate and the demand for 67{sup G}a at IPEN-CNEN/SP is 37 GBq (1 Ci)/week. The {sup 67}Ga presents physical half-life of 3.26 days (78 hours) and decays 100% by electron capture to stable {sup 67}Zn. Its decay includes the emission of {gamma} rays with energies of 93.3 keV (37%), 184.6 keV (20.4%), 300.2 keV (16.6%) and 888 keV (26%). In the past {sup 67}Ga was produced by the reaction {sup 68}Zn (p, 2n) {sup 67}Ga at IPEN-CNEN/SP. After irradiation, the target was dissolved in concentrated HCl and the solution percolated through a cationic resin DOWEX 50W-X8, 200-400 mesh, conditioned with 10 mol L{sup -1} HCl. Zinc, nickel and copper were eluted in 10 mol L{sup -1} HCl and {sup 67}Ga 3.5 mol L{sup -1} HCl. The final product was obtained as {sup 67}Ga citrate. This work presents a new, fast, direct and efficient method for the chemical separation of 67{sup G}a by thermal diffusion (heating of the target) combined with concentrated acetic acid extraction. Purification was performed by ion exchange chromatography. Natural zinc electrodeposition was performed on nickel/copper plates as substrate and the zinc deposits were adherent to the substrate, slightly shiny and uniform. The targets were irradiated with 26 MeV protons and integrated current of 10 {mu}A.h. After irradiation, the targets were heated at 300 deg C for 2 hours and placed in contact with concentrated acetic acid for 1 hour. The average yield of extraction of {sup 67}Ga was (72 {+-} 10)%. This solution was evaporated and the residue was taken up in 0.5 mol L{sup -1} NH{sub 4}OH. The 67{sup G}a was purified on cationic resin Dowex 50WX8 in NH{sub 4}OH medium. The {sup 67}Ga recovery was (98 {+-} 2)%. This solution was evaporated and taken up in 0.1 mol L{sup -1} HCl. The chemical purity was evaluated by ICP-OES that resulted in (2 {+-} 1) {mu}g mL{sup -1} of zinc. The concentration of iron, copper and nickel was lower than the detection limits and also than the utilization limits for {sup 67}Ga. The radionuclidic purity was greater than (99.9%). This method showed to be suitable to obtain high purity {sup 67}Ga in less aggressive chemical conditions than before. (author)

  18. Thermal requirements of the coconut pest Atheloca subrufella (Hulst) (Lepidoptera: Phycitidae); Exigencias termicas da praga do coqueiro Atheloca subrufella (Hulst)(Lepidoptera: Phycitidae)

    Energy Technology Data Exchange (ETDEWEB)

    Santana, Suerda W.J. de; Barros, Reginaldo; Torres, Jorge B.; Gondim Junior, Manoel G.C. [Universidade Federal Rural de Pernambuco (UFRPE), Recife, PE (Brazil). Dept. de Agronomia/Entomologia

    2010-04-15

    Among the important pests of coconut, the coconut moth Atheloca subrufella (Hulst) is a significant pest of flowers and fruits, and is found across all coconut-producing regions in Brazil. We investigated the thermal requirements of A. subrufella and estimated the number of generations for two different growing coconut regions in Pernambuco State. The developmental time of all immature stages reduced as the temperature increased. The egg to adult period ranged from 19.3 to 59.8 days from 32 deg C to 18 deg C, respectively. The survival of the period from egg to adult was 25% at extreme temperatures (18 deg C and 32 deg C), while at the intermediate temperatures it was over 72%. Based on the thermal requirements determined for A. subrufella and the average temperatures determined for Zona da Mata and Sertao of Pernambuco State, it was estimated that A. subrufella is able to complete up to 13 generations per year in both areas. These results indicate that A. subrufella exhibited development and reproduction limited by temperatures higher than 32 deg C and lower than 18 deg C. However, based on the thermal requirements of A. subrufella and the mean temperatures of the Zona da Mata and Sertao of Pernambuco State, this pest can develop throughout the entire year. (author)

  19. Solar thermal plant of air tube for solar air conditioning; Planta Solar Termica de tubos de vacio para aire acondicionado solar

    Energy Technology Data Exchange (ETDEWEB)

    Bruno, J. C.; Lopez, J.; Coronas, A.

    2004-07-01

    The present implementation of refrigeration and air conditioning technologies driven by thermal solar energy is very limited although there is a great market demand for them for environmental reasons and security of energy supply. In this paper it is presented a detailed technical description of the solar plant installed at the technological Innovation Centre CREVER, and an example of a complete energy analysis of this plant working under the required conditions to be used for solar air conditioning applications. Also it is included a review of solar air conditioning systems state of the art. (Author)

  20. Study of electrical and thermal characteristics of inverters for grid-connected photovoltaic systems; Estudo de caracteristicas eletricas e termicas de inversores para sistemas fotovoltaicos conectados a rede

    Energy Technology Data Exchange (ETDEWEB)

    Rampinelli, Giuliano Arns

    2010-12-15

    Grid-connected photovoltaic systems directly convert solar energy into electrical energy delivering to the distribution grid a clean and renewable energy. These systems are basically formed by an array of photovoltaic modules and inverters. The inverters are responsible for converting direct current to alternating current. A study of electrical and thermal characteristics of inverters used in grid-connected photovoltaic systems from a theoretical and experimental analysis. The inverters tests were carried out in two stages: the first stage was performed at Solar Energy Lab. of the Federal University of Rio Grande do Sul (UFRGS), Brazil, where it was used a 4,8 kW{sub p} grid-connected photovoltaic system and ten inverters of different manufacturers. The inverters electrical characteristics measured and analyzed were: direct current to alternating current conversion efficiency, maximum power point tracker efficiency, power factor and harmonic distortion in current and voltage. Inverters thermal testing was also conducted and its results are presented ana analyzed. The second stage of the experimental tests was performed at Photovoltaic Solar Energy Lab. at CIEMAT in Spain. It was used 3 kW{sub p} photovoltaic system and seven inverters of different manufacturers. The inverters are single-phase, up to 5 kW and different topologies (high frequency transformer, low frequency transformer and transformerless). The influence of DC voltage input in the behavior of DC to AC conversion efficiency and power factor was analyzed. The results of the tests allowed the development of mathematical models that describe the electrical and thermal behavior of the inverters. The proposed mathematical models were inserted into computer simulation software developed at UFRGS named FVConect. The evolution of the simulation results compared to the experimental results validates the proposed models. The analysis of the behavior of the inverters improves the understanding of the operating os such equipment and their dynamic interaction with other grid-connected photovoltaic system components. (author)

  1. Composting as a source of thermal energy for water heating in aquaculture; Compostagem como fonte termica de energia para aquecimento de agua na agricultura

    Energy Technology Data Exchange (ETDEWEB)

    Souza, Samuel Nelson Melegari de; Neitzke, Guilherme; Hermes, Cesar Ademar [Universidade Estadual do Oeste do Parana (UNIOESTE/CCET), Cascavel, PR (Brazil). Centro de Ciencias Exatas. Programa Institucional de Bolsas de Iniciacao Cientifica], Emails: ssouza@unioeste.br, guilherme_neitzke@yahoo.com.br, cahermes@ibestvip.com.br

    2006-07-01

    The objective of the work is to use the composting as thermal energy source in the maintenance of aquatic organisms. The area of Toledo has annual medium temperature of the air of 20,5 deg C and average in the hottest quarter of 27 deg C and in the more cold of 16,5 deg C. The used experimental material consisted of boxes of water, pipes of aluminum, hay of grassy, manure of birds and swine, aquarium compressors, hoses and pipes, porous stones, fish lingers and thermometer. The temperatures of the air, the composition and the water without heating were monitored. The medium temperatures obtained were of 20,9 and 31,1 deg C, for the air and the composition, respectively. The averages of temperature of the water with heating and without heating were of 22,0 deg C and 20,0 deg C. The weight difference among the fish lingers was of 24,0 %. It is ended that the composting can be a thermal source of energy in the aquaculture. (author)

  2. Morphology and thermal properties of PLA films plasticized with aliphatic oligoesters; Morfologia e propriedades termicas de filmes de PLA plastificados com oligoesteres alifaticos

    Energy Technology Data Exchange (ETDEWEB)

    Inacio, Erika M.; Dias, Marcos L., E-mail: erika.minacio@ima.ufrj.br [Universidade Federal do Rio de Janeiro (UFRJ), Rio de Janeiro, RJ (Brazil); Lima, Maria Celiana P. [Instituto Federal do Rio de Janeiro (IFRJ), Duque de Caxias, RJ (Brazil)

    2015-07-01

    The addition of plasticizers to poly(lactic acid) (PLA) is one of the known ways of changing its ductility, making possible the modification of its mechanical and thermal properties. In this work, it was synthesized two biodegradable aliphatic oligoesters: oligo(trimethylene sebacate) (OST) and oligo(trimethylene malonate) (OMT), and these oligomers were used as plasticizer in cast films of commercial film grade PLA at concentrations of 1, 5 and 10 wt% of each plasticizer. X-ray diffraction (XRD) was used to investigate the morphology and differential scanning calorimetry (DSC) was also used aiming the evaluation of the thermal properties of these films. The PLA films containing no plasticizer showed an amorphous behavior, and the addition of PMT on the PLA films acted, simultaneously, decreasing the Tg, and rising the material's crystallinity. In contrast, the increased addition of OST to the PLA films did not change the Tg, and equally, did not have a significant changes in the material's crystallinity. Therefore, it was possible to observe the effect of the concentration of oligomers on the crystallinity of the films as well as the no plasticizer effect of the OST. (author)

  3. Dependence of the thermal neutron fluence at the size installations radiotherapy bunker; Dependencia de la fluencia termica de neutrones en el tamano del bunquer en instalaciones de radioterapia

    Energy Technology Data Exchange (ETDEWEB)

    Gonzalez-Soto, X.; Amgarou, K.; Langares, J. L.; Exposito, M. R.; Gomez, F.; Domingo, C.; Sanchez-Doblado, F.

    2011-07-01

    The project aims to infer the dose deposited by neutrons in the patient treated by radiation therapy, from a measurement of the thermal neutron fluence at a selected point within the treatment room. These thermal neutrons are created when fast neutrons produced in the linac head are moderate, mainly in the walls of the bunker, and its yield depends on both the volume of the room and its geometry.

  4. Study of corrosion in metallic coating in steel-carbon by thermal spray; Estudo de corrosao em revestimentos metalicos em aco-carbono obtidos por aspersao termica

    Energy Technology Data Exchange (ETDEWEB)

    Cruz, Maria C.P.; Cavalcanti, Eliane B.; Rambo, Elisabeth S.M.; Araujo, Paulo M.M. [Instituto de Tecnologia e Pesquisa (IPT), Aracaju, SE (Brazil); Santos, Anderson O. [PETROBRAS S.A., Rio de Janeiro, RJ (Brazil)

    2008-07-01

    The effect caused for constituent elements of the watery environment of production of the oil on metallic coverings was studied that simulate the artificial rise of the oil (connecting rods of pump mechanic). For in such a way, the techniques of electrochemical analysis had been used, as the method of linear polarization and the extrapolation of the straight line of Tafel of metallic coverings [alloy of Bronze and Aluminum; alloy of CrNi 80/20; NiCr 80/20; 95MXC (Cr: 26.5% - 31.5%, Cr: 26.5% - 31.5%, B: 3.35% - 4.15%, Mn: 1.1% - 2.2%, Itself: 1.1% -2.1%, Faith) and aluminum] on the substratum steel simulating covering in the connecting rods of pump. Oil well had been raised the resistance characteristics the polarization of the metal when submitted to the watery way surrounding it. They had been evaluated the resistance the covering polarization applied on the steel, with the objective to analyze its resistance the corrosion and to verify the possibility of its use as barrier against the problems originated for the degradation in connecting rods of pump. For the calculated Taxes of Corrosion, it can be concluded that the Aluminum coverings (0,003 mm/year) and NiCr 80/20 (0,179 mm/year) had been the ones that had presented a bigger resistance to the corrosive way. (author)

  5. The importance of equipment inspection in a thermometrical generation unit; A importancia da inspecao de equipamentos numa central de geracao termica

    Energy Technology Data Exchange (ETDEWEB)

    Dutra, Aldo C. [CEPEL, Rio de Janeiro, RJ (Brazil)

    1991-12-31

    This work comments the main aspects of equipment inspection and the main causes of deterioration and failures, the reasons for the systematic inspection and the already successful systematic used in the petroleum industry which may be applied to thermoelectric power plants

  6. Mechanical and thermal properties of polypropylene and layered double hydroxides nanocomposites; Propriedades mecanicas e termicas de nanocompositos de polipropileno e hidroxidos duplos lamelares

    Energy Technology Data Exchange (ETDEWEB)

    Duarte de Farias, A.M.; Fraga, M.A.; Oliveira, R.B.; Oliveira, M.G., E-mail: marcia.oliveira@int.gov.b [Instituto Nacional de Tecnologia (INT), Rio de Janeiro, RJ (Brazil)

    2010-07-01

    The recent interest in polymer nanocomposites involving layered double hydroxides (LDH) is due to improved thermal stability, flame resistance, mechanical and barrier properties. The LDHs are structurally described as the stacking of layers with positively charged hydrated anions intercalated between these lamellae. In this paper, polypropylene nanocomposites with Mg / Al-HDL unmodified and modified with sodium dodecyl sulfate (DS) were prepared in the internal mixing chamber equipped with roller rotors and heated to 190 deg C. The nanocomposites were injected molded and then morphology, mechanical and thermal properties were evaluated by X-ray diffraction, tensile tests and DSC, respectively. The results revealed that both LDH and LDH-DS reached a good degree of dispersion in the PP matrix, resulting in increased stiffness, but reduced capacity for deformation and toughness of nanocomposites. The crystallinity of the nanocomposites was higher compared to the PP matrix. (author)

  7. Training of solar energy applications in the Polytechnic School of Caceres; Docencia de las aplicaciones de la energia solar en la escuela politecnica de Caceres arquitectura termica

    Energy Technology Data Exchange (ETDEWEB)

    Tejeiro, C. Y.; Mendez, J. A. S.; Gutierrez, P. D. M.; Barrigon, J. M. M.

    2004-07-01

    In the Polytechnic School of Caceres, for the degree of Technical Architecture, the teaching of the installations of solar energy has been done by Final Projects. We have considered four basic points: 1st A diversified model of project, this means, a different building for each student, and a repeated typology of project. 2nd Teamwork, studying each student a part of the information, and explaining to the other. 3rd Internet as a forum and to obtain general information. 4th The Censolar course as calculus software and database in our laboratory. The result are 30 projects, some of them very completed, that resolve the general topic of the adaptation of the sport installations to be used with solar energy, besides of studying other topics as: maintenance of the installations, economic viability, integration in the landscape, etc. (Author)

  8. The PFBC Power Plant of Escatron; Proyecto de Demostracion de la Combustion en Lecho Fuido a Presion Central Termica de Escatron

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1998-12-31

    The Escatron Pressurized Fluidized Bed Combustion Demonstration Plant was led by ENDESA which set out on the Project with its own specific objectives, and also have involved contributions from designers and suppliers, as ABB and BWE. The project objectives may be defined as follows: To make progress in the development of clean and efficient technology applicable to a wide range of coal types, specially to the peculiar Spanish black lignites. To be able to design and manufacture a new technology in the contest of European Union, specially developing capacity in Spain. All this give rise to a framework which took shape in the Escatron Project Monitoring Committee. Sulphur retention in PFBC technology has proved to be efficient, with levels higher than 90%. The nitric oxides emissions fall within limits set by present regulations. It is likely that more restrictive regulations in the future, will require the consideration of injecting ammonium technic over free-chamber bed. The most significant problem is that the flue gas from the cyclones to the gas turbine, has a high dust content. The cleaning system for this gas should be improved, and the best option appear to be the introduction of ceramic filters. The new plants could be built at higher power, as should be 300-400 MWe, operating with higher pressure (16 bar). This option together with better steam conditions, gives rise to a better energy yields and competitive electric energy production. But we should not dimis more proved designs of 100-200 MWe, as an interesting modular solution. (Author)

  9. ACS production: optimal design of solar thermal power plants; Produccion de ACS. Optimizacion del dimensionado de instalaciones de energia solar termica

    Energy Technology Data Exchange (ETDEWEB)

    Platon Arias, L.; San Jose Alonso, F.

    2009-07-01

    The aim of this project is to develop a program to size solar thermal power plants for the production of the company ACS, which enable optimum value calculations of the different influence parameters (surface, inclination, orientation, energy input) advising diverse circumstances and requirements. The energy input calculation has been effected according to f-chart method. For the solar radiation on inclined and oriented surfaces calculation, has been applied the Klein Method. (Author) 14 refs.

  10. Development of the conductivity thermal logs based on electrical profiles; Desenvolvimento de perfil de condutividade termica a partir de perfis eletricos

    Energy Technology Data Exchange (ETDEWEB)

    Jesus, Carlos Luciano C. de; Lima, Olivar A.L. de; Argollo, Roberto M.; Romero, Pedro A. [Universidade Federal da Bahia, Salvador, BA (Brazil). Centro de Pesquisa em Geologia e Geofisica

    2004-07-01

    The thermal conductivity of the rocks is a necessary physical parameter for the calculation of the flow of heat in the terrestrial surface. The conventional methods to measure the thermal conductivity are developed in laboratory having used sample of certifications. However, these nor always are disposable by the industry of the oil, either because of difficulty operational either for its high cost. However, all the constructed wells of oil are stood geophysically, and, in the majority of the times the geophysical profiles are the only petrophysics registers of the wells, mainly when the same ones are not testified. A viable alternative for sedimentary rocks would be to determine the thermal conductivity through the electric conductivity, being this normally gotten in electric profiles of wells. As the electric conductivity and the thermal conductivity they depend on the porosity and of the texture of the rocks and these mathematically equivalents satisfy equations constituent, are intuitive to think that the same largeness can directly be correlated. Applying the same analytical theoretical procedure considered by Lima and Sharma (1990 and 1992) to describe the electric conductivity of clay-sand, we develop an expression to determine the thermal conductivity of clay-sandstone rocks. To test the applicability of this equation they had been used given of electric profile of five explore wells of the regions of Aracas and Miranga, both of the basin of Reconcavo. The results of the conversions are comparable with the ones of effected measures of thermal conductivity with the method of the bar for Carvalho (1981) in the terrigenous sequences of the Reconcavo. (author)

  11. Optimization of thermal efficiency of nuclear central power like as PWR; Otimizacao da eficiencia termica de uma usina nuclear do tipo PWR

    Energy Technology Data Exchange (ETDEWEB)

    Lapa, Nelbia da Silva

    2005-10-15

    The main purpose of this work is the definition of operational conditions for the steam and power conservation of Pressurized Water Reactor (PWR) plant in order to increase its system thermal efficiency without changing any component, based on the optimization of operational parameters of the plant. The thermal efficiency is calculated by a thermal balance program, based on conservation equations for homogeneous modeling. The circuit coefficients are estimated by an optimization tool, allowing a more realistic thermal balance for the plans under analysis, as well as others parameters necessary to some component models. With the operational parameter optimization, it is possible to get a level of thermal efficiency that increase capital gain, due to a better relationship between the electricity production and the amount of fuel used, without any need to change components plant. (author)

  12. Energy evaluation of using thermal covers on open refrigerated display cases; Avaliacao energetica do emprego de coberturas termicas em expositores refrigerados abertos

    Energy Technology Data Exchange (ETDEWEB)

    Mendes, Nathan [Pontificia Universidade Catolica do Parana, Curitiba (Brazil). Lab. de Sistemas Termicos]. E-mail: nmendes@ccet.pucpr.br; Mendes, Nivaldo E-mail: eliseeps@uol.com.br

    2000-07-01

    This is a sensitivity study to analyze the influence of using thermal covers on the energy efficiency of open refrigerated display cases in supermarkets. The study was accomplished during the summer in the city of Javelin, and it was observed a significant reduction of electric energy waste, among other benefits. (author)

  13. Hydrocarbons thermal maturation: Leopatin method applied to the Parana basin; Maturacao termica de hidrocarbonetos: aplicacao do metodo de Lopatin a Bacia do Parana

    Energy Technology Data Exchange (ETDEWEB)

    Eston, Sergio Medici de; Jardim, Niza S.

    1986-12-31

    One of the requirements for the existent of economic deposits of hydrocarbons is that the organic matter has undergone adequate thermal maturation. Several techniques have been proposed in order to quantity the catagenetic state of kerogen, and the Lopatin-Waples methodology permits quantification at any past time and does not require laboratory tests on samples of the material. For this reason it is an useful techniques for predicting mature zones using as basic information the thermal and subsidence histories of each stratum. Lopatin`s technique was applied to the Parana basin, with McKenzie`s crustal stretching model fitted to the data of 18 wells, and the areas predicted as mature for oil and/or gas were in good agreement with the field results. The technique predicted oil phone areas at the east border of the basin for the Ponta Grossa and Irati formation, and also that most of the thermal maturation occurred after the basalt flows of the Cretaceous period. (author) 41 refs., 6 figs., 6 tabs.

  14. Stress and thermal expansion numerical analysis of subsea buried pipelines; Analise numerica de tensoes e expansao termica de dutos submarinos enterrados

    Energy Technology Data Exchange (ETDEWEB)

    Souto, Marcio de S.; Vaz, Murilo A. [Universidade Federal, Rio de Janeiro, RJ (Brazil). Coordenacao dos Programas de Pos-graduacao de Engenharia; Solano, Rafael F. [PETROBRAS S.A., Rio de Janeiro, RJ (Brazil)

    2005-07-01

    The design of Capixaba North Terminal pipelines (TNC) became very complex, once the pipelines are exposed to elevated temperature variations. As the pipelines are buried, the interaction with the seabed can become critical with the thermal expansion development, since an axial compressive force arise, reaching critical values and then leading the pipeline to the thermo mechanical instability phenomenon. To minimize these effects, the pipeline will cross the shore approach through a horizontal directional drilling, and expansion loops and intermediate tie-ins took place on his route in order to permit pipeline displacements, working thermally. The objective of this present work is to develop a numerical model, able to analyze the entire pipeline stress, strain and displacements, considering different kinds of soil along of his route. The influence of expansion loops is evaluated and a comparative analysis in order to discover the minimum curvature radius at the directional drilling region is carried out. This study defines a methodology based on the developed numerical model which will be extended to future applications in subsea buried pipeline design. (author)

  15. Radiological Impact Study of the Coal-Fired Power Plant of Lada; Estudio del Impacto Radiologico de la Central Termica de Carbon de Lada

    Energy Technology Data Exchange (ETDEWEB)

    Robles, B.; Baeza, A.; Mora, J. C.; Corbacho, J. A.; Trueba, C.; Guillen, J.; Rodriguez, J.; Miralles, Y.

    2014-02-01

    Coal, fuel used in thermal power plants for electricity production, contains variable concentrations of naturally occurring radionuclides from natural disintegration series of 238{sup U}, 235{sup U}, 232{sup T}h and also the 40K, which are enhanced in the wastes and coproducts due to the industrial process. For this reason, natural radionuclides which are part of the noncombustible fraction of coal, except those volatiles which incorporate directly to the flue gases, concentrates and are partitioned between fly ashes and bottom ashes. This enhancement could cause, to the workers of the installation and to members of the public around the plant, an increase in the exposure which should be assessed under the radiation protection point of view. Present report collect the results obtained from a screening assessment of the radiological impact derived from the normal operation of the Lada coal-fired power plant. The project where this assessment was performed is part of a bigger project which is jointly developed by the Unit of Radiation Protection of the Public and the Environment (UPRPYMA) of CIEMAT and the Environmental Radioactivity Laboratory of the Extremadura University (LARUEX) in agreement with the Spanish Association of the Electrical Industry (ENUSA). (Author)

  16. Radiological Impact Study of the Coal-Fired Power Plant of Anllares; Estudio del Impacto Radiologico de la Central Termica de Carbon de Anllares

    Energy Technology Data Exchange (ETDEWEB)

    Robles, B.; Baeza, A.; Mora, J. C.; Corbacho, J. A.; Trueba, C.; Guillen, J.; Rodriguez, J.; Miralles, Y.

    2014-04-01

    Coal, fuel used in thermal power plants for electricity production, contains variable concentrations of naturally occurring radionuclides from natural disintegration series of {sup 2}38U, {sup 2}35U, {sup 2}32Th and also the 40K, which are enhanced in the wastes and coproducts due to the industrial process. For this reason, natural radionuclides which are part of the noncombustible fraction of coal, except those volatiles which incorporate directly to the flue gases, concentrates and are partitioned between fly ashes and bottom ashes. This enhancement could cause, to the workers of the installation and to members of the public around the plant, an increase in the exposure which should be assessed under the radiation protection point of view. Present report collect the results obtained from a screening assessment of the radiological impact derived from the normal operation of the Anllares coal-fired power plant. The project where this assessment was performed is part of a bigger project which is jointly developed by the Unit of Radiation Protection of the Public and the Environment (UPRPYMA) of CIEMAT and the Environmental Radioactivity Laboratory of the Extremadura University (LARUEX) in agreement with the Spanish Association of the Electrical Industry (ENUSA). (Author)

  17. Radiological Impact Study of the Coal-Fired Power Plant of Velilla; Estudio del Impacto Radiologico de la Central Termica de Carbon de Velilla

    Energy Technology Data Exchange (ETDEWEB)

    Robles, B.; Mora, J. c.; Trueba, C.; Rodriguez, J.; Baeza, A.; Corbacho, J. a.; Guillen, J.; Miralles, Y.

    2013-10-01

    Coal, fuel used in thermal power plants for electricity production, contains variable concentrations of naturally occurring radionuclides from natural disintegration series of 238U, 235U, 232Th and also the 40K, which are enhanced in the wastes and coproducts due to the industrial process. For this reason, natural radionuclides which are part of the non-combustible fraction of coal, except those volatiles which incorporate directly to the flue gases, concentrates and are partitioned between fly ashes and bottom ashes. This enhancement could cause, to the workers of the installation and to members of the public around the plant, an increase in the exposure which should be assessed under the radiation protection point of view. Present report collect the results obtained from a screening assessment of the radiological impact derived from the normal operation of the Velilla coal-fired power plant. The project where this assessment was performed is part of a bigger project which is jointly developed by the Unit of Radiation Protection of the Public and the Environment (UPRPYMA) of CIEMAT and the Environmental Radioactivity Laboratory of the Extremadura University (LARUEX) in agreement with the Spanish Association of the Electrical Industry (ENUSA). (Author)

  18. Radiological Impact Study of the Coal-Fired Power Plant of Meirama; Estudio del Impacto Radiologico de la Central Termica de Carbon de Meirama

    Energy Technology Data Exchange (ETDEWEB)

    Robles, B.; Baeza, A.; Mora, J. C.; Corbacho, J. A.; Trueba, C.; Guillen, J.; Rodriguez, J.; Miralles, Y.

    2014-04-01

    Coal, fuel used in thermal power plants for electricity production, contains variable concentrations of naturally occurring radionuclides from natural disintegration series of {sup 2}38U, {sup 2}35U, {sup 2}32Th and also the 40K, which are enhanced in the wastes and coproducts due to the industrial process. For this reason, natural radionuclides which are part of the noncombustible fraction of coal, except those volatiles which incorporate directly to the flue gases, concentrates and are partitioned between fly ashes and bottom ashes. This enhancement could cause, to the workers of the installation and to members of the public around the plant, an increase in the exposure which should be assessed under the radiation protection point of view. Present report collect the results obtained from a screening assessment of the radiological impact derived from the normal operation of the Meirama coal-fired power plant. The project where this assessment was performed is part of a bigger project which is jointly developed by the Unit of Radiation Protection of the Public and the Environment (UPRPYMA) of CIEMAT and the Environmental Radioactivity Laboratory of the Extremadura University (LARUEX) in agreement with the Spanish Association of the Electrical Industry (ENUSA). (Author)

  19. Radiological Impact Study of the Coal-Fired Power Plant of La Robla; Estudio del Impacto Radiologico de la Central Termica de Carbon de La Robla

    Energy Technology Data Exchange (ETDEWEB)

    Robles, B.; Baeza, A.; Mora, J. C.; Corbacho, J. A.; Trueba, C.; Guillen, J.; Rodriguez, J.; Miralles, Y.

    2014-04-01

    Coal, fuel used in thermal power plants for electricity production, contains variable concentrations of naturally occurring radionuclides from natural disintegration series of {sup 2}38U, {sup 2}35U, {sup 2}32Th and also the 40K, which are enhanced in the wastes and coproducts due to the industrial process. For this reason, natural radionuclides which are part of the noncombustible fraction of coal, except those volatiles which incorporate directly to the flue gases, concentrates and are partitioned between fly ashes and bottom ashes. This enhancement could cause, to the workers of the installation and to members of the public around the plant, an increase in the exposure which should be assessed under the radiation protection point of view. Present report collect the results obtained from a screening assessment of the radiological impact derived from the normal operation of the La Robla coal-fired power plant. The project where this assessment was performed is part of a bigger project which is jointly developed by the Unit of Radiation Protection of the Public and the Environment (UPRPYMA) of CIEMAT and the Environmental Radioactivity Laboratory of the Extremadura University (LARUEX) in agreement with the Spanish Association of the Electrical Industry (ENUSA). (Author)

  20. Radiological Impact Study of the Coal-Fired Power Plant of La Robla; Estudio del Impacto Radiologico de la Central Termica de Carbon de La Robla

    Energy Technology Data Exchange (ETDEWEB)

    Robles, B.; Mora, J. C.; Trueba, C.; Rodriguez, J.; Baeza, A.; Corbacho, J. A.; Guillen, J.; Miralles, Y.

    2013-07-01

    Coal, fuel used in thermal power plants for electricity production, contains variable concentrations of naturally occurring radionuclides from natural disintegration series of 238{sup U}, 235{sup U}, 232{sup T}h and also the 40{sup K}, which are enhanced in the wastes and coproducts due to the industrial process. For this reason, natural radionuclides which are part of the non-combustible fraction of coal, except those volatiles which incorporate directly to the flue gases, concentrates and are partitioned between fly ashes and bottom ashes. This enhancement could cause, to the workers of the installation and to members of the public around the plant, an increase in the exposure which should be assessed under the radiation protection point of view. Present report collect the results obtained from a screening assessment of the radiological impact derived from the normal operation of the La Robla coal-fired power plant. The project where this assessment was performed is part of a bigger project which is jointly developed by the Unit of Radiation Protection of the Public and the Environment (UPRPYMA) of CIEMAT and the Environmental Radioactivity Laboratory of the Extremadura University (LARUEX) in agreement with the Spanish Association of the Electrical Industry (ENUSA). (Author)

  1. Radiological Impact Study of the Coal-Fired Power Plant of Abono; Estudio del Impacto Radiologico de la Central Termica de Carbon de Abono

    Energy Technology Data Exchange (ETDEWEB)

    Robles, B.; Baeza, A.; Mora, J. C.; Corbacho, J. A.; Trueba, C.; Guillen, J.; Rodriguez, J.; Miralles, Y.

    2014-04-01

    Coal, fuel used in thermal power plants for electricity production, contains variable concentrations of naturally occurring radionuclides from natural disintegration series of {sup 2}38U, {sup 2}35U, {sup 2}32Th and also the {sup 4}0K, which are enhanced in the wastes and coproducts due to the industrial process. For this reason, natural radionuclides which are part of the noncombustible fraction of coal, except those volatiles which incorporate directly to the flue gases, concentrates and are partitioned between fly ashes and bottom ashes. This enhancement could cause, to the workers of the installation and to members of the public around the plant, an increase in the exposure which should be assessed under the radiation protection point of view. Present report collect the results obtained from a screening assessment of the radiological impact derived from the normal operation of the Abono coal-fired power plant. The project where this assessment was performed is part of a bigger project which is jointly developed by the Unit of Radiation Protection of the Public and the Environment (UPRPYMA) of CIEMAT and the Environmental Radioactivity Laboratory of the Extremadura University (LARUEX) in agreement with the Spanish Association of the Electrical Industry (ENUSA). (Author)

  2. Thermal efficiency of a non-transferred thermal plasma cannon; Eficiencia termica de un canon de plasma termico no-transferido

    Energy Technology Data Exchange (ETDEWEB)

    Mercado, A.; Cota, G.; Merlo, L.; Pacheco, J.; Pena, R.; Cruz, A. [Instituto nacional de Investigaciones Nucleares, A.P. 18-1027, 11801 Mexico D.F. (Mexico)

    1997-07-01

    This work shows a thermal efficiency research ({nu}) for a plasma torch in d.c. which was carried out through the realization of an energy balance around the system under consideration. The plasma torch is manufactured in copper with a tungsten incrustations in cathode. The gas used was argon and the gas fluxes were at the rank of 10 and 40 lt/min to the total pressure of 1.2 bar (1.1 atm). With these conditions it was worked with electric currents at the rank of 40 and 180 A. The data were collected through a data acquisition card which was programmed in Windows environment. (Author)

  3. 3D simulation of the thermal and chemical plumes using open source software; Simulacion 3D de las plumas termica y quimica mediante software de codigo libre

    Energy Technology Data Exchange (ETDEWEB)

    Saenz Temino, J. L.; Lerones Martin, J.; Gonzalez Delgado, J.

    2013-07-01

    The interaction of thermal and chemical plumes in the region of the Irish Sea near the site has been simulated using a finite element model representative of the local hydrodynamic regime, concluding how the method of selected cooling, open cycle, is physically and environmentally feasible. Furthermore, tunnel lengths required for each scenario under discussion have been preliminarily defined, varying in a range from 1800 to 2300 meters for a unit (1 tunnel), 4400-6300 meters of two units (2 tunnels) and 8000 meters to three units (2 tunnels), depending on the chosen technology.

  4. Thermal analysis of a solar collector consisting of V cavities for water heating; Analise termica de um coletor solar composto de cavidades V para aquecimento de agua

    Energy Technology Data Exchange (ETDEWEB)

    Moreira, Michel Fabio de Souza

    2009-03-15

    The solar water heating is carried through, in Brazil, by means of solar heaters compound for collectors flat plate of the type plate-and-pipes, devices that operate in stationary position and they do not require tracking of the sun. A compound collector for some formed V-trough concentrators can be an alternative to the conventional solar collectors flat plate. This compound collector for V-trough is considered, each one, for side-walls which are specularly reflecting surfaces associates in V (equivalent to a triangular gutter). Next to the vertex to each V-trough concentrators an absorber tube is fixed, for flow of the fluid to be heated. Interconnection of the absorbers tubes forms a similar tubular network existing in solar collectors of the type the plate and pipe. V-trough concentrators with the absorbers tubes are made use in series in the interior a prismatic box, which have one of its faces consisting by a glass covering and directed toward incidence of the solar radiation. An analysis of thermal performance of these devices operating stationary and without tracking of the sun is researched. A mathematical model for the computational simulation of the optical and thermal performance of these concentrative devices is elaborated, whose implementation was carried through software EES (Engineering Equation Solver). The efficiency optics of V-trough concentrators with cylindrical absorbers is calculated from the adaptation of the methodology used for Fraidenraich (1994), proposal for Hollands (1971) for V-trough cavities with plain absorbers. The thermal analysis of the considered collector was based on the applied methodology the CPC for Hsieh (1981) and Leao (1989). Relative results to the thermal performance of V-trough concentrators suggest that these configurations are not competitive, technique and economically, with the conventional plain collectors. Although some geometric configurations presented next thermal efficiencies to the conventional plain collectors, it's raised unitary costs, however, make impracticable, at a first moment, for the domestic water heating. (author)

  5. Simulação e integração termica SRV em colunas de destilação extrativa

    OpenAIRE

    Eduardo Augusto Caldas Batista

    1995-01-01

    Resumo: Neste trabalho estudou-se a aplicação da integração térmica SRV ("Secondary Reflux and Vaporization") à destilação extrativa para misturas com solvente de baixa volatilidade, etanol/água/etileno glicol, e para misturas com solvente que se vaporiza, acetona/metanol/água. Esta integração térmica, que consiste principalmente da transferência de calor da seção de enriquecimento para a seção de esgotamento, pode fazer uso de um gradiente de temperatura natural existente entre as seções da ...

  6. Evaluation of visual impact of solar hermal systems on urban landscape; Metodo de evaluacion del impacto visual de las instalaciones de energia solar termica en el paisaje urbano

    Energy Technology Data Exchange (ETDEWEB)

    Lopez, G.; Martinez, J.

    2004-07-01

    This article proposes a methodology and systematics for the valuation and evaluation of the visual impact produced by solar thermal systems on urban landscapes. On the one hand, from the characteristics of solar thermal systems capable of producing a visual impact and, on the second hand, from the analysis of the urban landscape (character and perception; classification in three subtypes), an interrelationship of the system and the urban landscape parameters is established by means of matrixes. The result shall be the visual impact of a solar thermal system on an urban landscape, which may range from a minimum (Nonexistent) to a maximum (Unacceptable), including other categories like Acceptable, Compatible, Compatible with Corrections, and Incompatible. (Author)

  7. Thermal requirements of Galleria mellonella L. (Lepidoptera: Pyralidae) immature stages; Exigencias termicas de estagios imaturos de Galleria mellonella L. (Lepidoptera: Pyralidae)

    Energy Technology Data Exchange (ETDEWEB)

    Cardoso, Aline C.; Prezoto, Fabio [Universidade Federal de Juiz de Fora (UFJF), MG (Brazil). Programa de Pos-Graduacao em Ciencias Biologicas]. E-mail: ac-bio@bol.com.br; fprezoto@icb.ufjf.br; Prata, Marcia C. de A.; Furlong, John [EMBRAPA Gado de Leite, Juiz de Fora, MG (Brazil)]. E-mail: mprata@cnpgl.embrapa.br, john@cnpgl.embrapa.br

    2007-09-15

    The rearing of Galleria mellonella L. in laboratory is important for multiplication of entomopathogenic nematodes, mandatory for biological control studies. The objective of this study was to evaluate the effect of three thermal profiles on development stages of this insect, allowing synchronization of cycle production. Two distinct rearing phases were done: firstly, using nucleous of incubation for development of eggs and, secondly, using circular-aluminum manifolds for development of larvae and pupae. The time necessary for development of the immature stages decreased with higher temperatures. Incubation periods lasted 13.4 days at 22 deg C, 8.3 at 27 deg C and 6.8 days at 32 deg C, while periods for larvae development lasted 40.4, 27.2, and 23.4 days, respectively, for the same temperatures. Development to pupal stage was observed 18.2, 15.0, and 12.2 days, respectively, for the same temperatures. Larval survival was higher at 32 deg C, however embryonic stages and pupae survival were higher at 27 deg C and 22 deg C, respectively. The threshold temperature was 11.209167 deg C for the embryonic development stage, 7.695869 deg C for larval stage, and 1.943050 deg C for pupal stage of G. mellonella. Thermal constants were 138.380533 DG (degree day) for egg, 554.968830 DG for larvae, and 369.054080 DG for pupae. (author)

  8. Strategy and methodology for radioactive waste characterization

    International Nuclear Information System (INIS)

    2007-03-01

    Over the past decade, significant progress has been achieved in the development of waste characterization as well as control procedures and equipment. This has been as a direct response to ever-increasing requirements for quality and reliability of information on waste characteristics. Failure in control procedures at any step can have important, adverse consequences and may result in producing waste packages which are not compliant with the waste acceptance criteria for disposal, thereby adversely impacting the repository. The information and guidance included in this publication corresponds to recent achievements and reflects the optimum approaches, thereby reducing the potential for error and enhancing the quality of the end product. This publication discusses the strategy and methodology to be adopted in conceiving a characterization programme for the various kinds of radioactive waste fluxes or packages. No international publications have dealt with this topic in such depth. The strategy elaborated here takes into account the international State of the art in the different characterization methodologies. The strategy and methodology of the characterization programme will depend on the type of radioactive waste. In addition, the accuracy and quality of the characterization programme very much depends on the requirements to demonstrate compliance with the waste acceptance criteria. This publication presents a new subdivision of radioactive waste based on its physicochemical composition and its time dependence: simple/stable, complex/stable, simple/variable and complex/variable. Decommissioning and historical waste deserve special attention in this publication, and they can belong to any of the four categories. Identifying the life cycle of the radioactive waste is a cornerstone in defining the strategy for radioactive waste characterization. The waste acceptance criteria and the performance assessment of the repository are other key factors in the strategy and

  9. WRAP Module 1 waste characterization plan

    International Nuclear Information System (INIS)

    Mayancsik, B.A.

    1995-01-01

    The purpose of this document is to present the characterization methodology for waste generated, processed, or otherwise the responsibility of the Waste Receiving and Processing (WRAP) Module 1 facility. The scope of this document includes all solid low level waste (LLW), transuranic (TRU), mixed waste (MW), and dangerous waste. This document is not meant to be all-inclusive of the waste processed or generated within WRAP Module 1, but to present a methodology for characterization. As other streams are identified, the method of characterization will be consistent with the other streams identified in this plan. The WRAP Module 1 facility is located in the 200 West Area of the Hanford Site. The facility's function is two-fold. The first is to verify/characterize, treat and repackage contact handled (CH) waste currently in retrievable storage in the LLW Burial Grounds, Hanford Central Waste Complex, and the Transuranic Storage and Assay Facility (TRUSAF). The second is to verify newly generated CH TRU waste and LLW, including MW. The WRAP Module 1 facility provides NDE and NDA of the waste for both drums and boxes. The NDE is used to identify the physical contents of the waste containers to support waste characterization and processing, verification, or certification. The NDA results determine the radioactive content and distribution of the waste

  10. Glycan characterization of biopharmaceuticals: Updates and perspectives

    International Nuclear Information System (INIS)

    Planinc, Ana; Bones, Jonathan; Dejaegher, Bieke; Van Antwerpen, Pierre; Delporte, Cédric

    2016-01-01

    Therapeutic proteins are rapidly becoming the most promising class of pharmaceuticals on the market due to their successful treatment of a vast array of serious diseases, such as cancers and immune disorders. Therapeutic proteins are produced using recombinant DNA technology. More than 60% of therapeutic proteins are posttranslationally modified following biosynthesis by the addition of N- or O-linked glycans. Glycosylation is the most common posttranslational modifications of proteins. However, it is also the most demanding and complex posttranslational modification from the analytical point of view. Moreover, research has shown that glycosylation significantly impacts stability, half-life, mechanism of action and safety of a therapeutic protein. Considering the exponential growth of biotherapeutics, this present review of the literature (2009–2015) focuses on the characterization of protein glycosylation, which has witnessed an improvement in methodology. Furthermore, it discusses current issues in the fields of production and characterization of therapeutic proteins. This review also highlights the problem of non-standard requirements for the approval of biosimilars with regard to their glycosylation and discusses recent developments and perspectives for improved glycan characterization. - Highlights: • Biopharmaceuticals have emerged as the new class of blockbuster drugs in the pharmaceutical industry. • More than 60% of the approved biopharmaceuticals are glycosylated. • Glycosylation has an effect on the efficacy and the safety of therapeutic glycoproteins. • N-glycosylation characterization of therapeutic glycoproteins is a regulatory requirement. • Biosimilar releases are increasing and demonstration of comparability poses challenges for N-glycosylation characterization.

  11. Three dimensional characterization and archiving system

    International Nuclear Information System (INIS)

    Sebastian, R.L.; Clark, R.; Gallman, P.

    1996-01-01

    The Three Dimensional Characterization and Archiving System (3D-ICAS) is being developed as a remote system to perform rapid in situ analysis of hazardous organics and radionuclide contamination on structural materials. Coleman Research and its subcontractors, Thermedics Detection, Inc. (TD) and the University of Idaho (UI) are in the second phase of a three phase program to develop 3D-ICAS to support Decontamination and Decommissioning (D and D) operations. Accurate physical characterization of surfaces and the radioactive and organic is a critical D and D task. Surface characterization includes identification of potentially dangerous inorganic materials, such as asbestos and transite. Real-time remotely operable characterization instrumentation will significantly advance the analysis capabilities beyond those currently employed. Chemical analysis is a primary area where the characterization process will be improved. The 3D-ICAS system robotically conveys a multisensor probe near the surfaces to be inspected. The sensor position and orientation are monitored and controlled using coherent laser radar (CLR) tracking. The CLR also provides 3D facility maps which establish a 3D world view within which the robotic sensor system can operate

  12. X-ray Characterization of Materials

    Science.gov (United States)

    Lifshin, Eric

    1999-09-01

    Linking of materials properties with microstructures is a fundamental theme in materials science, for which a detailed knowledge of the modern characterization techniques is essential. Since modern materials such as high-temperature alloys, engineering thermoplastics and multilayer semiconductor films have many elemental constituents distributed in more than one phase, characterization is essential to the systematic development of such new materials and understanding how they behave in practical applications. X-ray techniques play a major role in providing information on the elemental composition and crystal and grain structures of all types of materials. The challenge to the materials characterization expert is to understand how specific instruments and analytical techniques can provide detailed information about what makes each material unique. The challenge to the materials scientist, chemist, or engineer is to know what information is needed to fully characterize each material and how to use this information to explain its behavior, develop new and improved properties, reduce costs, or ensure compliance with regulatory requirements. This comprehensive handbook presents all the necessary background to understand the applications of X-ray analysis to materials characterization with particular attention to the modern approach to these methods.

  13. Glycan characterization of biopharmaceuticals: Updates and perspectives

    Energy Technology Data Exchange (ETDEWEB)

    Planinc, Ana [Analytical Platform of the Faculty of Pharmacy and Laboratory of Pharmaceutical Chemistry, Faculty of Pharmacy, Universite Libre de Bruxelles (ULB), Brussels (Belgium); Bones, Jonathan [Characterisation and Comparability Laboratory, NIBRT – The National Institute for Bioprocessing Research and Training, Foster Avenue, Mount Merrion, Blackrock, Co. Dublin (Ireland); Dejaegher, Bieke [Laboratory of Instrumental Analysis and Bioelectrochemistry, Faculty of Pharmacy, Université Libre de Bruxelles (ULB), Boulevard du Triomphe, B-1050 Brussels (Belgium); Department of Analytical Chemistry and Pharmaceutical Technology (FABI), Center for Pharmaceutical Research (CePhaR), Faculty of Medicines and Pharmacy, Vrije Universiteit Brussel - VUB, Laarbeeklaan 103, B-1090 Brussels (Belgium); Van Antwerpen, Pierre [Analytical Platform of the Faculty of Pharmacy and Laboratory of Pharmaceutical Chemistry, Faculty of Pharmacy, Universite Libre de Bruxelles (ULB), Brussels (Belgium); Delporte, Cédric, E-mail: cedric.delporte@ulb.ac.be [Analytical Platform of the Faculty of Pharmacy and Laboratory of Pharmaceutical Chemistry, Faculty of Pharmacy, Universite Libre de Bruxelles (ULB), Brussels (Belgium)

    2016-05-19

    Therapeutic proteins are rapidly becoming the most promising class of pharmaceuticals on the market due to their successful treatment of a vast array of serious diseases, such as cancers and immune disorders. Therapeutic proteins are produced using recombinant DNA technology. More than 60% of therapeutic proteins are posttranslationally modified following biosynthesis by the addition of N- or O-linked glycans. Glycosylation is the most common posttranslational modifications of proteins. However, it is also the most demanding and complex posttranslational modification from the analytical point of view. Moreover, research has shown that glycosylation significantly impacts stability, half-life, mechanism of action and safety of a therapeutic protein. Considering the exponential growth of biotherapeutics, this present review of the literature (2009–2015) focuses on the characterization of protein glycosylation, which has witnessed an improvement in methodology. Furthermore, it discusses current issues in the fields of production and characterization of therapeutic proteins. This review also highlights the problem of non-standard requirements for the approval of biosimilars with regard to their glycosylation and discusses recent developments and perspectives for improved glycan characterization. - Highlights: • Biopharmaceuticals have emerged as the new class of blockbuster drugs in the pharmaceutical industry. • More than 60% of the approved biopharmaceuticals are glycosylated. • Glycosylation has an effect on the efficacy and the safety of therapeutic glycoproteins. • N-glycosylation characterization of therapeutic glycoproteins is a regulatory requirement. • Biosimilar releases are increasing and demonstration of comparability poses challenges for N-glycosylation characterization.

  14. Status of Gulf Coast salt dome characterization

    International Nuclear Information System (INIS)

    Swanson, O.E.; Gibbons, M.G.; Deyling, M.A.; McPherson, R.B.

    1982-01-01

    Screening and characterization for a potential nuclear waste repository have progressed through the area phase in these Gulf Coast Salt Basins. The domes studied during the area phase are described briefly. The area characterization studies are outlined, and the resulting reports are listed. Geologic and environmental studies resulted in elimination of four domes from further consideration. The remaining domes were judged acceptable and were classified as to their favorability to license. Site characterization planning for location phase activities deals primarily with technical, environmental, and socioeconomic issues of concern to the states and/or to the Office of Nuclear Waste Isolation (ONWI), Department of Energy (DOE). These issues are listed and discussed. 16 references, 9 figures

  15. Properties and characterization of modern materials

    CERN Document Server

    Altenbach, Holm

    2017-01-01

    This book focuses on robust characterization and prediction methods for materials in technical applications as well as the materials’ safety features during operation. In particular, it presents methods for reliably predicting material properties, an aspect that is becoming increasingly important as engineering materials are pushed closer and closer to their limits to boost the performance of machines and structures. To increase their engineering value, components are now designed under the consideration of their multiphysical properties and functions, which requires much more intensive investigation and characterization of these materials. The materials covered in this monograph range from metal-based groups such as lightweight alloys, to advanced high-strength steels and modern titanium alloys. Furthermore, a wide range of polymers and composite materials (e.g. with micro- and nanoparticles or fibres) is covered. The book explores methods for property prediction from classical mechanical characterization-...

  16. Oromucosal film preparations: classification and characterization methods.

    Science.gov (United States)

    Preis, Maren; Woertz, Christina; Kleinebudde, Peter; Breitkreutz, Jörg

    2013-09-01

    Recently, the regulatory authorities have enlarged the variety of 'oromucosal preparations' by buccal films and orodispersible films. Various film preparations have entered the market and pharmacopoeias. Due to the novelty of the official monographs, no standardized characterization methods and quality specifications are included. This review reports the methods of choice to characterize oromucosal film preparations with respect to biorelevant characterization and quality control. Commonly used dissolution tests for other dosage forms are not transferable for films in all cases. Alternatives and guidance on decision, which methods are favorable for film preparations are discussed. Furthermore, issues about requirements for film dosage forms are reflected. Oromucosal film preparations offer a wide spectrum of opportunities. There are a lot of suggestions in the literature on how to control the quality of these innovative products, but no standardized tests are available. Regulatory authorities need to define the standards and quality requirements more precisely.

  17. Towards an integrated materials characterization toolbox

    DEFF Research Database (Denmark)

    Robertson, Ian M.; Schuh, Christopher A.; Vetrano, John S.

    2011-01-01

    The material characterization toolbox has recently experienced a number of parallel revolutionary advances, foreshadowing a time in the near future when material scientists can quantify material structure evolution across spatial and temporal space simultaneously. This will provide insight...... development. Electron microscopy; atom probe tomography; x-ray, neutron and electron tomography; serial sectioning tomography; and diffraction-based analysis methods are reviewed, and opportunities for their future development are highlighted. Advances in surface probe microscopy have been reviewed recently...... the state-of-the-art in characterization and suggest a trajectory for the continued development of the field. Based on this review, a set of grand challenges for characterization science is identified, including suggestions for instrumentation advances, scientific problems in microstructure analysis...

  18. Quantitative Characterization of Boundary Roughness in Metals

    DEFF Research Database (Denmark)

    Sun, Jun

    variable to obtain information of local structural variations such as protrusions and retrusions formed on recrystallization boundaries. The AII value is directionindependent allowing unbiased characterization of morphological irregularities with both closed and non-closed boundary profiles. The length...... structural aspects into account, a detailed characterization is essential of partly recrystallized microstructures focusing on the local shapes of the boundaries, in particular on whether protrusions and retrusions are formed or not. Quantification of the “amount” of boundary roughness in the form...... scale at which the rough features are characterized is determined by a parameter termed sampling radius used to measure the AII values. A number of roughness parameters are developed based on the AII dataset for a boundary or boundary segment, whose local morphological characteristics are represented...

  19. Characterization of DWPF recycle condensate materials

    Energy Technology Data Exchange (ETDEWEB)

    Bannochie, C. J. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL); Adamson, D. J. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL); King, W. D. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL)

    2015-04-01

    A Defense Waste Processing Facility (DWPF) Recycle Condensate Tank (RCT) sample was delivered to the Savannah River National Laboratory (SRNL) for characterization with particular interest in the concentration of I-129, U-233, U-235, total U, and total Pu. Since a portion of Salt Batch 8 will contain DWPF recycle materials, the concentration of I-129 is important to understand for salt batch planning purposes. The chemical and physical characterizations are also needed as input to the interpretation of future work aimed at determining the propensity of the RCT material to foam, and methods to remediate any foaming potential. According to DWPF the Tank Farm 2H evaporator has experienced foaming while processing DWPF recycle materials. The characterization work on the RCT samples has been completed and is reported here.

  20. Characterizing Cool Giant Planets in Reflected Light

    Science.gov (United States)

    Marley, Mark

    2016-01-01

    While the James Webb Space Telescope will detect and characterize extrasolar planets by transit and direct imaging, a new generation of telescopes will be required to detect and characterize extrasolar planets by reflected light imaging. NASA's WFIRST space telescope, now in development, will image dozens of cool giant planets at optical wavelengths and will obtain spectra for several of the best and brightest targets. This mission will pave the way for the detection and characterization of terrestrial planets by the planned LUVOIR or HabEx space telescopes. In my presentation I will discuss the challenges that arise in the interpretation of direct imaging data and present the results of our group's effort to develop methods for maximizing the science yield from these planned missions.

  1. Biological tracer for waste site characterization

    International Nuclear Information System (INIS)

    Strong-Gunderson, J.

    1995-01-01

    Remediating hazardous waste sites requires detailed site characterization. In groundwater remediation, characterizing the flow paths and velocity is a major objective. Various tracers have been used for measuring groundwater velocity and transport of contaminants, colloidal particles, and bacteria and nutrients. The conventional techniques use dissolved solutes, dyes. and gases to estimate subsurface transport pathways. These tracers can provide information on transport and diffusion into the matrix, but their estimates for groundwater flow through fractured regions are very conservative. Also, they do not have the same transport characteristics as bacteria and suspended colloid tracers, both of which must be characterized for effective in-place remediation. Bioremediation requires understanding bacterial transport and nutrient distribution throughout the acquifer, knowledge of contaminants s mobile colloidal particles is just essential

  2. Characterizing popularity dynamics of online videos

    Science.gov (United States)

    Ren, Zhuo-Ming; Shi, Yu-Qiang; Liao, Hao

    2016-07-01

    Online popularity has a major impact on videos, music, news and other contexts in online systems. Characterizing online popularity dynamics is nature to explain the observed properties in terms of the already acquired popularity of each individual. In this paper, we provide a quantitative, large scale, temporal analysis of the popularity dynamics in two online video-provided websites, namely MovieLens and Netflix. The two collected data sets contain over 100 million records and even span a decade. We characterize that the popularity dynamics of online videos evolve over time, and find that the dynamics of the online video popularity can be characterized by the burst behaviors, typically occurring in the early life span of a video, and later restricting to the classic preferential popularity increase mechanism.

  3. Automated clustering-based workload characterization

    Science.gov (United States)

    Pentakalos, Odysseas I.; Menasce, Daniel A.; Yesha, Yelena

    1996-01-01

    The demands placed on the mass storage systems at various federal agencies and national laboratories are continuously increasing in intensity. This forces system managers to constantly monitor the system, evaluate the demand placed on it, and tune it appropriately using either heuristics based on experience or analytic models. Performance models require an accurate workload characterization. This can be a laborious and time consuming process. It became evident from our experience that a tool is necessary to automate the workload characterization process. This paper presents the design and discusses the implementation of a tool for workload characterization of mass storage systems. The main features of the tool discussed here are: (1)Automatic support for peak-period determination. Histograms of system activity are generated and presented to the user for peak-period determination; (2) Automatic clustering analysis. The data collected from the mass storage system logs is clustered using clustering algorithms and tightness measures to limit the number of generated clusters; (3) Reporting of varied file statistics. The tool computes several statistics on file sizes such as average, standard deviation, minimum, maximum, frequency, as well as average transfer time. These statistics are given on a per cluster basis; (4) Portability. The tool can easily be used to characterize the workload in mass storage systems of different vendors. The user needs to specify through a simple log description language how the a specific log should be interpreted. The rest of this paper is organized as follows. Section two presents basic concepts in workload characterization as they apply to mass storage systems. Section three describes clustering algorithms and tightness measures. The following section presents the architecture of the tool. Section five presents some results of workload characterization using the tool.Finally, section six presents some concluding remarks.

  4. Characterization of Stock Blu-ray diodes

    Science.gov (United States)

    Cunningham, Mark; Archibald, James; Erickson, Christopher; Durfee, Dallin

    2010-10-01

    I am developing a process to test and characterize diodes of unknown wavelengths. using a B&WTEK Spectrometer we are characterizing the wavelength of 405 nm blu-ray diodes purchased in bulk. With the known error in production of the Diode Lasers we are hoping to find a diode at 408 nm to use in driving a raman transition between hyperfine states of strontium 87 ions. The bulk of the project is a java program that communicates with the spectrometer and graphically displays the intensities of the wavelengths from the laser diodes.

  5. OCCIMA: Optical Channel Characterization in Maritime Atmospheres

    Science.gov (United States)

    Hammel, Steve; Tsintikidis, Dimitri; deGrassie, John; Reinhardt, Colin; McBryde, Kevin; Hallenborg, Eric; Wayne, David; Gibson, Kristofor; Cauble, Galen; Ascencio, Ana; Rudiger, Joshua

    2015-05-01

    The Navy is actively developing diverse optical application areas, including high-energy laser weapons and free- space optical communications, which depend on an accurate and timely knowledge of the state of the atmospheric channel. The Optical Channel Characterization in Maritime Atmospheres (OCCIMA) project is a comprehensive program to coalesce and extend the current capability to characterize the maritime atmosphere for all optical and infrared wavelengths. The program goal is the development of a unified and validated analysis toolbox. The foundational design for this program coordinates the development of sensors, measurement protocols, analytical models, and basic physics necessary to fulfill this goal.

  6. Physical Characterization of Florida International University Simulants

    Energy Technology Data Exchange (ETDEWEB)

    HANSEN, ERICHK.

    2004-08-19

    Florida International University shipped Laponite, clay (bentonite and kaolin blend), and Quality Assurance Requirements Document AZ-101 simulants to the Savannah River Technology Center for physical characterization and to report the results. The objectives of the task were to measure the physical properties of the fluids provided by FIU and to report the results. The physical properties were measured using the approved River Protection Project Waste Treatment Plant characterization procedure [Ref. 1]. This task was conducted in response to the work outlined in CCN066794 [Ref. 2], authored by Gary Smith and William Graves of RPP-WTP.

  7. Characterization of in vitro translation products

    International Nuclear Information System (INIS)

    Jagus, R.

    1987-01-01

    This chapter describes the characterization of in vitro translation products by the most commonly used techniques. The methods include SDS-polyacrylamide gel electrophoresis (SDS-PAGE), combined with immunoprecipitation and/or fluorography of [ 35 S]methionine-labeled translation products. The other frequently used characterization tool, translation of hybrid-selected mRNA or hybrid-arrested translation, is treated separately in this volume. Methods are also given for the recognition of mRNAs coding for secreted or membrane proteins

  8. Characterization of potassium dichromate solutions for spectrophotometercalibration

    Science.gov (United States)

    Conceição, F. C.; Silva, E. M.; Gomes, J. F. S.; Borges, P. P.

    2018-03-01

    Spectrophotometric analysis in the ultraviolet (UV) region is used in the determination of several quantitative and qualitative parameters. For ensuring reliability of the analyses performed on the spectrophotometers, verification / calibration of the equipment must be performed periodically using certified reference materials (CRMs). This work presents the characterization stage needed for producing this CRM. The property value characterized was the absorbance for the wavelengths in the UV spectral regions. This CRM will contribute to guarantee the accuracy and linearity of the absorbance scale to the spectrophotometers, through which analytical measurement results will be provided with metrological traceability.

  9. Source characterization of Purnima Neutron Generator (PNG)

    International Nuclear Information System (INIS)

    Bishnoi, Saroj; Patel, T.; Paul, Ram K.; Sarkar, P.S.; Adhikari, P.S.; Sinha, Amar

    2011-01-01

    The use of 14.1 MeV neutron generators for the applications such as elemental analysis, Accelerated Driven System (ADS) study, fast neutron radiography requires the characterization of neutron source i.e neutron yield (emission rate in n/sec), neutron dose, beam spot size and energy spectrum. In this paper, a series of experiments carried out to characterize this neutron source. The neutron source has been quantified with neutron emission rate, neutron dose at various source strength and beam spot size at target position

  10. On characterizations of quasi-metric completeness

    Energy Technology Data Exchange (ETDEWEB)

    Dag, H.; Romaguera, S.; Tirado, P.

    2017-07-01

    Hu proved in [4] that a metric space (X, d) is complete if and only if for any closed subspace C of (X, d), every Banach contraction on C has fixed point. Since then several authors have investigated the problem of characterizing the metric completeness by means of fixed point theorems. Recently this problem has been studied in the more general context of quasi-metric spaces for different notions of completeness. Here we present a characterization of a kind of completeness for quasi-metric spaces by means of a quasi-metric versions of Hu’s theorem. (Author)

  11. Characterizing R-duality in Banach spaces

    DEFF Research Database (Denmark)

    Christensen, Ole; Xiao, Xiang Chun; Zhu, Yu Can

    2013-01-01

    R-duals of certain sequences in Hilbert spaces were introduced by Casazza, Kutyniok and Lammers in 2004 and later generalized to Banach spaces by Xiao and Zhu. In this paper we provide some characterizations of R-dual sequences in Banach spaces.......R-duals of certain sequences in Hilbert spaces were introduced by Casazza, Kutyniok and Lammers in 2004 and later generalized to Banach spaces by Xiao and Zhu. In this paper we provide some characterizations of R-dual sequences in Banach spaces....

  12. Characterization of Nanoparticles by Scattering Techniques

    International Nuclear Information System (INIS)

    Chu, Benjamin; Liu Tianbo

    2000-01-01

    Basic principles and applications of different scattering techniques (including static and dynamic light scattering (SLS and DLS), small-angle X-ray scattering (SAXS), wide-angle X-ray diffraction (WAXD) and small-angle neutron scattering (SANS)) on the characterization of nanoparticles are reviewed in this paper. By choosing a suitable scattering technique or a combination of different techniques for nanoparticle characterization, the particles' molecular weight, radius of gyration, hydrodynamic radius, size distribution, shape and internal structure as well as interparticle interactions of nanoparticles, can be determined. Examples including some sophisticated colloidal systems are presented

  13. 4. International reservoir characterization technical conference

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1997-04-01

    This volume contains the Proceedings of the Fourth International Reservoir Characterization Technical Conference held March 2-4, 1997 in Houston, Texas. The theme for the conference was Advances in Reservoir Characterization for Effective Reservoir Management. On March 2, 1997, the DOE Class Workshop kicked off with tutorials by Dr. Steve Begg (BP Exploration) and Dr. Ganesh Thakur (Chevron). Tutorial presentations are not included in these Proceedings but may be available from the authors. The conference consisted of the following topics: data acquisition; reservoir modeling; scaling reservoir properties; and managing uncertainty. Selected papers have been processed separately for inclusion in the Energy Science and Technology database.

  14. Concretes characterization for spent radioactive sources

    International Nuclear Information System (INIS)

    Martinez B, J.; Monroy G, F. P.

    2013-10-01

    The present work includes the preparation and characterization of the concrete used as conditioning matrix of spent radioactive sources in the Treatment Plant of Radioactive Wastes of the Instituto Nacional de Investigaciones Nucleares (ININ). The concrete tests tubes were subjected to resistance assays to the compression, leaching, resistance to the radiation and porosity, and later on characterized by means of X rays diffraction, scanning electron microscopy and infrared spectrometry, with the purpose of evaluating if this concrete accredits the established tests by the NOM-019-Nucl-1995. The results show that the concrete use in the Treatment Plant fulfills the requirements established by the NOM-019-Nucl-1995. (author)

  15. Characterization of Fernald Silo 3 Waste

    Energy Technology Data Exchange (ETDEWEB)

    Langton, C.A.

    2001-04-04

    This report summarizes characterization results for uranium residues from the Fernald Environmental Management Project (FEMP) Operable Unit (OU-4). These residues are currently stored in a one-million-gallon concrete silo, Silo 3, at the DOE Fernald Site, Ohio. Characterization of the Silo 3 waste is the first part of a three part study requested by Rocky Mountain Remedial Services (RMRS) through a Work for others Agreement, WFO-00-007, between the Westinghouse Savannah River Company (WSRC) and RMRS. Parts 2 and 3 of this effort include bench- and pilot-scale testing.

  16. Characterization of oil and gas reservoir heterogeneity

    Energy Technology Data Exchange (ETDEWEB)

    1991-01-01

    The objective of the cooperative research program is to characterize Alaskan reservoirs in terms of their reserves, physical and chemical properties, geologic configuration and structure, and the development potential. The tasks completed during this period include: (1) geologic reservoir description of Endicott Field; (2) petrographic characterization of core samples taken from selected stratigraphic horizons of the West Sak and Ugnu (Brookian) wells; (3) development of a polydispersed thermodynamic model for predicting asphaltene equilibria and asphaltene precipitation from crude oil-solvent mixtures, and (4) preliminary geologic description of the Milne Point Unit.

  17. Preparation, characterization and mechanical properties of k ...

    Indian Academy of Sciences (India)

    Structural characterizations of the prepared nanocomposite films were carried out by Fourier transform infrared, scanning electron microscope (SEM) andtransmission electron microscope (TEM) techniques. SEM and TEM showed homogeneous dispersion of SiO 2 nanoparticles in the KCG matrix. The tensile strength ...

  18. Purification and characterization of extracellular amylolytic enzyme ...

    African Journals Online (AJOL)

    DOSS

    2012-10-16

    Oct 16, 2012 ... Sephadex G-50 column chromatography and the enzyme activity was measured by using synthetic substrate starch. ... Key words: Aspergillus species, Sephadex G-50, column chromatography, diethyl amino ethyl (DEAE) cellulose. ... chemical properties characterized (Ravan et al., 2009). Although ...

  19. Characterization of potential probiotic bacteria isolated from ...

    African Journals Online (AJOL)

    Characterization of potential probiotic bacteria isolated from sorghum and pearl millet of the semi-arid tropics. ... A total of nine probiotic bacterial isolates were short listed based on these traits. The sequences of 16s rDNA gene ... probiotic foods. Key words: Probiotics, prebiotics, sorghum, pearl millet, product development.

  20. Characterization and antitumor activity of camptothecin from ...

    African Journals Online (AJOL)

    Xueqin Ran1, Gen Zhang2, Sheng Li2, Jiafu Wang2,3. 1. College of Animal Science, ... Cite as: Ran X, Zhang G, Li S, Wang J. Characterization and antitumor activity of camptothecin from endophytic fungus Fusarium solani isolated from Camptotheca ... Camptotheca acuminata has been used as tradition- ally Chinese ...

  1. Synthesis and characterization of saturated polyester and ...

    Indian Academy of Sciences (India)

    Synthesis and characterization of saturated polyester and nanocomposites derived from glycolyzed PET waste ... construction industries. PET is widely used in the packaging of beverages and drugs. ... ing the synthesis of saturated polyester (from GPET waste). This has been done for the estimation of the maximum. 277 ...

  2. Sub classification and targeted characterization of prophage ...

    Indian Academy of Sciences (India)

    2007-06-21

    Jun 21, 2007 ... The construct of ybcS has been over expressed in E. coli and the purified protein was functional, exhibiting lytic activity against E. coli and Salmonella typhi cell wall substrate. Such targeted sequence-structure-function characterization of proteins encoded by cryptic prophages will help understand the ...

  3. Clinical characterization of familial isolated pituitary adenomas

    NARCIS (Netherlands)

    A.F. Daly (Adrian); M-L. Jaffrain-Rea (Marie-Lise); E. Ciccarelli (Enrica); H. Valdes-Socin (H.); V. Rohmer (Vincent); G. Tamburrano (Guido); F. Borson-Chazot (Francoise); B. Estour (Bruno); E. Ciccarelli (Enrica); T. Brue (Thierry); P. Ferolla (Piero); P. Emy (Philippe); A. Colao (Annamaria); E. de Menis (Ernesto); P. Lecomte (Pierre); A. Penfornis (Alfred); B. Delemer (B.); J. Bertherat (Jerome); J.L. Wémeau; W.W. de Herder (Wouter); F. Archambeaud (Françoise); A. Stevenaert (A.); A. Calender (Alain); A. Murat (Arnaud); F. Cavagnini (Francesco); A. Beckers (Albert)

    2006-01-01

    textabstractContext: Familial pituitary adenomas occur rarely in the absence of multiple endocrine neoplasia type 1(MEN1)and Carney complex (CNC). Objective: Our objective was to characterize the clinical and genealogical features of non-MEN1/CNC familial isolated pituitary adenomas (FIPA). Design

  4. Seismic and Geophysical Characterization of Northern Asia

    Science.gov (United States)

    2010-09-01

    SEISMIC AND GEOPHYSICAL CHARACTERIZATION OF NORTHERN ASIA Kevin Mackey1, Hans Hartse2, Kazuya Fujita1, Michael Pasyanos3, and Michael Begnaud2...improve the calibration of northern Asia for nuclear explosion monitoring purposes. This project builds off previous work, and is a cooperative...propagation characteristics in northern Asia . Our work will further improve location and detection and discrimination capabilities, crustal and upper

  5. Molecular characterization and expression analysis of chalcone ...

    African Journals Online (AJOL)

    Chalcone synthase (CHS, EC: 2.3.1.74) is a key enzyme in the flavonoid and anthocyanin biosynthesis pathway. In order to investigate the role of CHS in tree peony flower coloration mechanism, we isolated and characterized the CHS gene from Paeonia suffruticosa cv. Yu Ji Yan Zhuang and analyzed its spatial and ...

  6. Phenotypic and Genotypic Characterization of Pasteurella Multocida ...

    African Journals Online (AJOL)

    Pasteurella multocida causes fowl cholera in domestic poultry and pasteurellosis in other avian species. This study was carried out due to paucity of information on the isolation and characterization of the organism from poultry in Nigeria. In the present study, 512 poultry were cultured at necropsy for the organism from the ...

  7. Biological synthesis and characterization of intracellular gold ...

    Indian Academy of Sciences (India)

    Nanoparticles are produced by various methods like physical, chemical, mechanical and biological. Biological me- thods of ... Stable nanoparticles were produced when an aqueous solution of chloroauric acid (HAuCl4) was reduced ... for the biomimetic synthesis and characterization of protein capped silver nanoparticles.

  8. Shape memory alloys–characterization techniques

    Indian Academy of Sciences (India)

    The former transformation has been widely used in the applications like antenna deployment of satellite, aerospace couplings, orthodontic arch wires, medical guide wires for diagnostic and therapeutic catheters and other industrial applications. Our group has been giving emphasis to the characterization techniques for R ...

  9. Complement component 3: characterization and association with ...

    Indian Academy of Sciences (India)

    Complement component C3 plays a major role as a central molecule of the complement cascade involving in killing ofmicroorganisms, either directly or in cooperation with phagocytic cells. C3 cDNA were isolated, from Egyptian buffalo and cattle, sequenced and characterized. The C3 cDNA sequences of buffalo and cattle ...

  10. Formulation and characterization of caffeine biodegradable chewing ...

    African Journals Online (AJOL)

    ) is a test for analysing the textural properties of food, in which the samples are ..... Food Technol 1978;. 32: 62-66. 16. Mehta FM, Trivedi P. Formulation and characterization of biodegradable medicated chewing gum delivery system for motion ...

  11. Molecular characterization and differential expression of two ...

    Indian Academy of Sciences (India)

    Here, we identified a pair of duplicated Or genes, AcerOr1 and AcerOr3, from the antennae of the Asian honeybee, Apis cerana cerana, and reported their molecular characterization and temporal expression profiles. The results showed that these two genes shared high similarity both in sequence and the gene structure.

  12. Synthesis, characterization and photophysical studies of ...

    Indian Academy of Sciences (India)

    These novel zinc(II) porphyrin-benzo--pyrone dyads successfully underwent demetallation in the presence of concentrated hydrochloric acid in chloroform at 25°C to form the corresponding free-base porphyrin analogues in good yields. The newly synthesized products were characterized on the basis of spectral data and ...

  13. Characterizing all models in infinite cardinalities

    NARCIS (Netherlands)

    Keskinen, L.

    2011-01-01

    Fix a cardinal κ. We can ask the question what kind of a logic L is needed to characterize all models of cardinality κ (in a finite vocabulary) up to isomorphism by their L-theories. In other words: for which logics L it is true that if any models A and B satisfy the same L-theory then they are

  14. Electrokinetic characterization of whey protein separation

    DEFF Research Database (Denmark)

    Keiding, Kristian; Stougård, Anders; Christensen, Morten Lykkegaard

    Cross flow filtration of whey protein has been performed on 3 different membranes. The rejections have been determined by HPLC analysis of the feed and permeate. The pure membranes as well as the fouled membranes have been characterized by measurements of the streaming potential along the membrane...

  15. Zeolite from fly ash: synthesis and characterization

    Indian Academy of Sciences (India)

    Coal fly ash was used to synthesize X-type zeolite by alkali fusion followed by hydrothermal treatment. The synthesized zeolite was characterized using various techniques such as X-ray diffraction, scanning electron microscopy, Fourier transform infrared spectroscopy, BET method for surface area measurement etc.

  16. Synthesis and optical characterization of copper nanoparticles ...

    Indian Academy of Sciences (India)

    Home; Journals; Bulletin of Materials Science; Volume 40; Issue 1. Synthesis and optical characterization of copper nanoparticles prepared by laser ablation. SAMIRA MONIRI MAHMOOD GHORANNEVISS MOHAMMAD REZA HANTEHZADEH MOHSEN ASADI ASADABAD. Volume 40 Issue 1 February 2017 pp 37-43 ...

  17. Characterization of P2P Systems

    Science.gov (United States)

    Stutzbach, Daniel; Rejaie, Reza

    The combination of large scale and geographically distributed nature of P2P system has led to their significant impact on the Internet. It is essential to characterize deployed P2P system for at least three reasons: (1) Accurately assessing their impact on the Internet, (2) identifying any performance bottleneck as well as any opportunity for performance improvement, (3) understanding user-driven dynamics in P2P systems. To characterize a P2P system, one needs to accurately capture snapshots of the resulting P2P overlay. This is challenging because the overlay is often large and dynamic. While the overlay is discovered by a crawler, it is changing which leads to a distorted view of the system. Capturing unbiased view of the traffic in the overlay is equally challenging because it is difficult to show that the captured behavior represent the observed behavior by all peers. In this chapter, we describe some of the fundamental problems in empirical characterization of widely deployed P2P systems. We present several examples to illustrate the effect of ad-hoc measurement/data collection on the resulting analysis/characterization. We then present two sampling techniques as a powerful approach to capture unbiased view of peer properties in a scalable fashion.

  18. Expression, purification and characterization of the interferon ...

    Indian Academy of Sciences (India)

    2012-01-19

    Jan 19, 2012 ... utilizing a single-step affinity purification with an appreciable yield of the highly purified protein. Recombinant RNase L was characterized by SDS-PAGE, immunoblotting and MALDI-TOF analysis. A semi-quantitative agarose-gel-based ribonuclease assay was developed for measuring its 2-5A-dependent ...

  19. Polyphasic taxonomic characterization of lactic acid bacteria ...

    African Journals Online (AJOL)

    Polyphasic taxonomic characterization of lactic acid bacteria isolated from spontaneous sorghum fermentations used to produce ting, a traditional South African food. ... The results of these analyses showed that ting fermentation involved at least three different species of LAB, i.e. Lactobacillus fermentum, L. plantarum

  20. Niosomal Delivery of Isoniazid - Development and Characterization ...

    African Journals Online (AJOL)

    Drug entrapment efficiency in the niosomes was determined spectrophotometrically. The niosomes were further characterized for their particle size, polydispersity index (PI) and zeta potential as well as by scanning electron microscopy and stability studies. Furthermore, in vitro drug release and cellular uptake studies on the ...

  1. Piezoelectric paint: characterization for further applications

    International Nuclear Information System (INIS)

    Yang, C; Fritzen, C-P

    2012-01-01

    Piezoelectric paint is a very attractive piezoelectric composite in many fields, such as non-destructive testing, or structural health monitoring. However, there are still many obstacles which restrict the real application of it. One of the main problems is that piezoelectric paint lacks a standard fabrication procedure, thus characterization is needed before use. The work presented here explores the characterization of piezoelectric paint. It starts with fabrication of samples with certain piezoelectric powder weight percentages. The microstructures of the samples are investigated by a scanning electron microscope; the results indicate that the fabrication method can produce high quality samples. This is followed by measurements of Young’s modulus and sensitivity. The piezoelectric charge constant d 31 is then deduced from the experimental data; the results agree well with a published result, which validates the effectiveness of the fabrication and characterization method. The characterized piezoelectric paint can expand its applications into different fields and therefore becomes a more promising and competitive smart material. (paper)

  2. Development and characterization of ten polymorphic microsatellites ...

    Indian Academy of Sciences (India)

    2000;. Webster and Reichart 2004). To this end, we developed 10 autosomal microsatellite markers for this species. To eval- uate the usefulness and variability of each marker, 43 indi- viduals were characterized along the Chilean coast. Seven- teen loci were originally isolated. Two failed to amplify using labelled primers.

  3. Molecular Characterization of the Resistance of Mycobacterium ...

    African Journals Online (AJOL)

    Purpose: To characterize the resistance of Mycobacterium tuberculosis to second line drugs using a line probe assay. Methods: Multi-drug resistant strains of Mycobacterium tuberculosis isolated between December 2008 and December 2009 were tested for resistance to fluoroquinolones and second-line injectable drugs ...

  4. Isolation and characterization of thirteen polymorphic microsatellite ...

    Indian Academy of Sciences (India)

    perfect repeat motifs, 36 of these were suitable for design- ing locus-specific primers using the Primer3 web interface program (Rozen and Skaletsky 2000). The characterization of microsatellites was ..... eral users and for biologist programmers. In Bioinformatics meth- ods and protocols (ed. S. Krawetz and S. Misener), pp.

  5. Characterization of Carbamazepine-Loaded Solid Lipid ...

    African Journals Online (AJOL)

    The formulations were characterized by infrared spectroscopy (IR), scanning electron microscopy (SEM) and ultraviolet spectrophotometry (UV). Results: Application of RESS to pure stearic acid yielded spherical particles in the range 40 to 200 nm which was about 600 times smaller than the unprocessed powder based on ...

  6. Synthesis and characterization of fluorophore attached silver ...

    Indian Academy of Sciences (India)

    Silver nanoparticles stabilized by soluble starch were synthesized and characterized. in vivo studies in rats showed no toxicity and revealed their distribution in various tissues and permeability across BBB. This starch stabilized silver nanoparticles have good biological characteristics to act as a potential promising vector for ...

  7. Synthesis and characterization of gold nanoparticles incorporated ...

    Indian Academy of Sciences (India)

    Synthesis and characterization of gold nanoparticles incorporated bentonite clay for electrocatalytic sensing of arsenic(III). Pankaj Kumar Rastogi Dharmendra Kumar Yadav Shruti Pandey Vellaichamy Ganesan Piyush Kumar Sonkar Rupali Gupta. Regular Articles Volume 128 Issue 3 March 2016 pp 349-356 ...

  8. Characterization of sugar beet pulp derived oligosaccharides

    NARCIS (Netherlands)

    Leijdekkers, M.

    2015-01-01

    Abstract This thesis aimed at characterizing complex mixtures of sugar beet pulp derived oligosaccharides, in order to be able to monitor and optimize the enzymatic saccharification of sugar beet pulp. Hydrophilic interaction chromatography with on-line evaporative light scattering

  9. Isolation, molecular and biochemical characterization of oil ...

    African Journals Online (AJOL)

    Biochemical and physiological characterization performed on the 34 bacterial isolates, revealed the presence of oil biodegrading bacterial genera and species of Pseudomonas Acidovorans, P. aerugi-nosa, P. alcaligenes, P. fluorescens, P. cepacia, P. mallei, P. maltophilia, P. oleovorans, P. putida, P. stutzeri P. vesicularis, ...

  10. NMR characterization of polymers: Review and update

    Science.gov (United States)

    NMR spectroscopy is a major technique for the characterization and analysis of polymers. A large number of methodologies have been developed in both the liquid and the solid state, and the literature has grown considerably (1-5). The field now covers a broad spectrum of activities, including polym...

  11. Preparation and Characterization of Poloxamer 188 solid ...

    African Journals Online (AJOL)

    Poloxamer 188 (PXM 188) was employed as a hydrophilic carrier at various IMC: PXM 188 ratios to prepare IMC-loaded solid dispersions (SDs) using the fusion method. Characterization based on surface morphology, particle size, absolute drug content and moisture sorption properties were carried out on the SDs. The in ...

  12. Organic fragments from graphene oxide: Isolation, characterization ...

    Indian Academy of Sciences (India)

    As-prepared graphene oxide (GO) contains oxidative debris which can be washed using basic solutions. We present the isolation and characterization of these debris. Dynamic light scattering (DLS) is used to monitor the separation of the debris in various solvents in the presence of different protic and aprotic alkylamino ...

  13. Grafted hydroxypropyl guargum: Development, characterization and ...

    Indian Academy of Sciences (India)

    Synthesis of hydroxypropyl guargum--polyacrylamide was carried out by ceric ion induced redox polymerization technique at 28 ± 1°C. The graft copolymer was characterized by IR and thermal analysis. The flocculation performance of graft copolymer was tested in 1 wt% coal suspension.

  14. A fuzzy expert system for soil characterization.

    Science.gov (United States)

    López, Eva M; García, Miriam; Schuhmacher, Marta; Domingo, José L

    2008-10-01

    As soil is a natural resource not always renewable, the risk characterization of contaminated soils is an issue of great interest. Artificial Intelligence (AI), based on Decision Support Systems (DSSs), has been developed for a wide range of applications in contaminated soil management. Decision trees have already shown to be easy to interpret and able to treat large scale applications. Fuzzy logic gives an improvement in the perturbations and the variance of the training data, due to the elasticity of fuzzy set formalism. In this study, we have developed a classificatory tool applied to characterize contaminated soil in function of human and environmental risks. Knowledge engineering for constructing the Soil Risk Characterization Decision Support System (SRC-DSS) involves three stages: knowledge acquisition, conceptual design and system implementation. A total of 26 parameters were divided into three groups to facilitate the configuration of the expert system: source attributes, transfer vector attributes, and local properties. Sixteen case studies were evaluated with the SRC-DSS. In comparison with other techniques, the results of the current study have shown that SRC-DDS is an excellent tool to classify and characterize soils according to the associated risk.

  15. Preliminary Phytochemical and Physicochemical Characterization of ...

    African Journals Online (AJOL)

    ethanol. Thin layer chromatography (TLC) analysis indicates the presence of rutin in the methanol extract of. G. segetum and this was supported by high performance liquid chromatography (HPLC) studies. Conclusion: Useful quantitative and descriptive data essential for identifying and characterizing the plant for.

  16. Taxonomic Identification and Characterization of African ...

    African Journals Online (AJOL)

    Nijmegen, the Netherlands. A descriptor list with 48 vegetative and reproductive characters was developed and used to characterize flowering and fruiting plants. Counting of chromosome was done on root squash preparations from one weekold seedlings, aided by digital enhancement of microscopic images. Nine species ...

  17. Laser characterization with advanced digital signal processing

    DEFF Research Database (Denmark)

    Piels, Molly; Tafur Monroy, Idelfonso; Zibar, Darko

    2015-01-01

    The use of machine learning techniques to characterize lasers with low output power is reviewed. Optimized phase tracking algorithms that can produce accurate noise spectra are discussed, and a method for inferring the amplitude noise spectrum and rate equation model of the laser under test is pr...

  18. Molecular Characterization of the Resistance of Mycobacterium ...

    African Journals Online (AJOL)

    Abstract. Purpose: To characterize the resistance of Mycobacterium tuberculosis to second line drugs using a line probe assay. Methods: ... Marne-la-Coquette,. France). Bacterial isolates contained in 500 µl of liquid culture were heat- inactivated at 95 °C for 30 min and then sonicated for 12 min. Finally, the suspension was ...

  19. Synthesis, characterization and photocatalytic reactions of ...

    Indian Academy of Sciences (India)

    Titanium dioxide is one of the most extensively investigated photocatalyst and is the subject of extensive .... with commercial titania powder from Merck. 2.2 Characterization. X-ray diffraction patterns of the ..... Bickley R I and Navio J A 1985 Photocatalytic production of energy-rich compounds (eds) G Grassi and D O Hall ...

  20. Laser beam characterization with digital holograms

    CSIR Research Space (South Africa)

    Forbes, A

    2013-04-01

    Full Text Available We show how laser beam characterization may be done in real-time with digital holograms. We illustrate the power of the techniques by applying them to a variety of laser sources, from fibers to solid-state....