WorldWideScience

Sample records for calorimetry software calibration

  1. Simulating SiD Calorimetry: Software Calibration Procedures and Jet Energy Resolution

    International Nuclear Information System (INIS)

    Cassell, R.

    2009-01-01

    Simulated calorimeter performance in the SiD detector is examined. The software calibration procedures are described, as well as the perfect pattern recognition PFA reconstruction. Performance of the SiD calorimeters is summarized with jet energy resolutions from calorimetry only, perfect pattern recognition and the SiD PFA algorithm. Presented at LCWS08(1). Our objective is to simulate the calorimeter performance of the SiD detector, with and without a Particle Flow Algorithm (PFA). Full Geant4 simulations using SLIC(2) and the SiD simplified detector geometry (SiD02) are used. In this geometry, the calorimeters are represented as layered cylinders. The EM calorimeter is Si/W, with 20 layers of 2.5mm W and 10 layers of 5mm W, segmented in 3.5 x 3.5mm 2 cells. The HAD calorimeter is RPC/Fe, with 40 layers of 20mm Fe and a digital readout, segmented in 10 x 10mm 2 cells. The barrel detectors are layered in radius, while the endcap detectors are layered in z(along the beam axis)

  2. Hadronic calibration of D0 calorimetry

    International Nuclear Information System (INIS)

    Kehoe, R.

    1996-09-01

    The D null detector is used to study p anti p collisions at the 1.8 TeV center-of-momentum energies available at the Fermilab Tevatron. The heart of the detector is a hermetic calorimeter employing uranium absorber and liquid argon as the ionization sampling medium. Several analyses require a well-understood jet energy scale. This paper describes how this calibration is obtained

  3. ATLAS calorimetry. Trigger, simulation and jet calibration

    Energy Technology Data Exchange (ETDEWEB)

    Weber, P

    2007-02-06

    The Pre-Processor system of the ATLAS Level-1 Calorimeter Trigger performs complex processing of analog trigger tower signals from electromagnetic and hadronic calorimeters. The main processing block of the Pre-Processor System is the Multi-Chip Module (MCM). The first part of this thesis describes MCM quality assurance tests that have been developed, their use in the MCM large scale production and the results that have been obtained. In the second part of the thesis a validation of a shower parametrisation model for the ATLAS fast simulation package ATLFAST based on QCD dijet events is performed. A detailed comparison of jet response and jet energy resolution between the fast and the full simulation is presented. The uniformity of the calorimeter response has a significant impact on the accuracy of the jet energy measurement. A study of the calorimeter intercalibration using QCD dijet events is presented in the last part of the thesis. The intercalibration study is performed in azimuth angle {phi} and in pseudorapidity {eta}. The performance of the calibration methods including possible systematic and statistical effects is described. (orig.)

  4. An investigation of calibration methods for solution calorimetry.

    Science.gov (United States)

    Yff, Barbara T S; Royall, Paul G; Brown, Marc B; Martin, Gary P

    2004-01-28

    Solution calorimetry has been used in a number of varying applications within pharmaceutical research as a technique for the physical characterisation of pharmaceutical materials, such as quantifying small degrees of amorphous content, identifying polymorphs and investigating interactions between drugs and carbohydrates or proteins and carbohydrates. A calibration test procedure is necessary to validate the instrumentation; a few of the suggested calibration reactions are the enthalpies of solution associated with dissolving Tris in 0.1 M HCl or NaCl, KCl or propan-1-ol in water. In addition, there are a number of different methods available to determine enthalpies of solution from the experimental data provided by the calorimeter, for example, the Regnault-Pfaundler's method, a graphical extrapolation based on the Dickinson method, or a manual integration-based method. Thus, the aim of the study was to investigate how each of these methods influences the values for the enthalpy of solution. Experiments were performed according to the method outlined by Hogan and Buckton [Int. J. Pharm. 207 (2000) 57] using KCl (samples of 50, 100 and 200 mg), Tris and sucrose as calibrants. For all three materials the manual integration method was found to be the most consistent with the KCl in water (sample mass of 200 mg) being the most precise. Thus, this method is recommended for the validation of solution calorimeters.

  5. Calorimetry

    International Nuclear Information System (INIS)

    Pope, B.

    1983-01-01

    An overall review of properties of various types of calorimeters is given, with special attention given to the challenges of high luminosity and high energy. The calorimeters described include continuous calorimeters, scintillation sampling calorimetry, gas sampling calorimetry, and liquid ionization calorimeters. Next explored are some limiting factors involved in experiments at high luminosities (or at high energies), and some examples are offered of detectors capable of operating at the highest luminosities (energies). Specific areas where substantial research and development work is needed are itemized

  6. Calorimetry

    International Nuclear Information System (INIS)

    McDonald, J.C.

    1978-01-01

    The techniques and equipment currently employed for calorimetric dosimetry have been briefly surveyed and the status of some recent measurements presented. The problems which remain to be investigated are: the thermal defect, the suitability of A-150 plastic as a material for heavy charged particle calorimetry and calorimeter designs that are appropriate for specific radiation situations, including cryogenic calorimeters

  7. The Pandora Software Development Kit for Particle Flow Calorimetry

    International Nuclear Information System (INIS)

    Marshall, J S; Thomson, M A

    2012-01-01

    Pandora is a robust and efficient framework for developing and running pattern-recognition algorithms. It was designed to perform particle flow calorimetry, which requires many complex pattern-recognition techniques to reconstruct the paths of individual particles through fine granularity detectors. The Pandora C++ software development kit (SDK) consists of a single library and a number of carefully designed application programming interfaces (APIs). A client application can use the Pandora APIs to pass details of tracks and hits/cells to the Pandora framework, which then creates and manages named lists of self-describing objects. These objects can be accessed by Pandora algorithms, which perform the pattern-recognition reconstruction. Development with the Pandora SDK promotes the creation of small, re-usable algorithms containing just the kernel of a specific operation. The algorithms are configured via XML and can be nested to perform complex reconstruction tasks. As the algorithms only access the Pandora objects in a controlled manner, via the APIs, the framework can perform most book-keeping and memory-management operations. The Pandora SDK has been fully exploited in the implementation of PandoraPFA, which uses over 60 algorithms to provide the state of the art in particle flow calorimetry for ILC and CLIC.

  8. Calorimetry

    International Nuclear Information System (INIS)

    Anon.

    1982-01-01

    We have divided this study of calorimetry at the SLC into five topics: physics with calorimeters, readout geometries, performance of existing detectors, calorimeter technologies, and new calorimeter designs. The first topic is a review of the Z 0 physics in which calorimetry would be important. We discuss the Monte Carlo model and the general features of the events which it generates. We consider how the physics affects the design of the electromagnetic and hadron calorimeters in energy resolution, segmentation, solid angle coverage, and general performance. The two ways of reading out a calorimeter, strips and towers, are the basis of the second topic. We discuss a model which makes quantitative comparisons of these two schemes, with particular reference to electromagnetic calorimeters. These programs should be useful in other studies of calorimeter performance as well. There are six detectors at PEP and SPEAR with calorimetric elements. The third topic is a review of their performance at present energies and an evaluation of the problems which would arise at SLC energies. The new technologies which may be mature enough for use in an SLC detector are considered as the fourth topic. Some are now being built into anti pp detectors, others are in test beam stages, and others are still bright ideas. We review ten techniques and include references for further pursuit. The last section combines the physics goals, readout schemes, and present and future techniques into sensible calorimeter designs which sharpen the issues. Six models resulted. We discuss their strengths, weaknesses, feasibility, and rough costs

  9. An integrated calibration system for liquid argon calorimetry

    CERN Document Server

    Marschalkowski, E; Mense, T; Nürnberger, H A; Schäfer, U

    1999-01-01

    A novel technical solution for an integrated version of the pulse generator of a calibration system for liquid argon calorimeters is presented. It consists of a differential amplifier with automatic offset compensation, a current mirror and a switching logic. These components are integrated on an ASIC chip in CMOS technology. The technical realisation as well as results on the performance are presented. (author)

  10. Liquid Krypton Calorimeter Calibration Software

    CERN Document Server

    Hughes, Christina Lindsay

    2013-01-01

    Calibration of the liquid krypton calorimeter (LKr) of the NA62 experiment is managed by a set of standalone programs, or an online calibration driver. These programs are similar to those used by NA48, but have been updated to utilize classes and translated to C++ while maintaining a common functionality. A set of classes developed to handle communication with hardware was used to develop the three standalone programs as well as the main driver program for online calibration between bursts. The main calibration driver has been designed to respond to run control commands and receive burst data, both transmitted via DIM. In order to facilitate the process of reading in calibration parameters, a serializable class has been introduced, allowing the replacement of standard text files with XML configuration files.

  11. Application of TZERO calibrated modulated temperature differential scanning calorimetry to characterize model protein formulations.

    Science.gov (United States)

    Badkar, Aniket; Yohannes, Paulos; Banga, Ajay

    2006-02-17

    The objective of this study was to evaluate the feasibility of using T(ZERO) modulated temperature differential scanning calorimetry (MDSC) as a novel technique to characterize protein solutions using lysozyme as a model protein and IgG as a model monoclonal antibody. MDSC involves the application of modulated heating program, along with the standard heating program that enables the separation of overlapping thermal transitions. Although characterization of unfolding transitions for protein solutions requires the application of high sensitive DSC, separation of overlapping transitions like aggregation and other exothermic events may be possible only by use of MDSC. A newer T(ZERO) calibrated MDSC model from TA instruments that has improved sensitivity than previous models was used. MDSC analysis showed total, reversing and non-reversing heat flow signals. Total heat flow signals showed a combination of melting endotherms and overlapping exothermic events. Under the operating conditions used, the melting endotherms were seen in reversing heat flow signal while the exothermic events were seen in non-reversing heat flow signal. This enabled the separation of overlapping thermal transitions, improved data analysis and decreased baseline noise. MDSC was used here for characterization of lysozyme solutions, but its feasibility for characterizing therapeutic protein solutions needs further assessment.

  12. Improvement of gamma calibration procedures with commercial management software

    International Nuclear Information System (INIS)

    Lucena, Rodrigo F.; Potiens, Maria da Penha A.; Santos, Gelson P.; Vivolo, Vitor

    2007-01-01

    In this work, the gamma calibration procedure of the Instruments Calibration Laboratory (LCI) of the IPEN-CNEN-SP was improved with the use of the commercial management software Autolab TM from Automa Company. That software was adapted for our specific use in the calibration procedures. The evaluation of the uncertainties in gamma calibration protocol was improved by the LCI staff and yet the all worksheets and final calibration report lay-out was developed in commercial software like Excell TM and Word TM from Microsft TM . (author)

  13. Calibration Analysis Software for the ATLAS Pixel Detector

    CERN Document Server

    AUTHOR|(INSPIRE)INSPIRE-00372086; The ATLAS collaboration

    2016-01-01

    The calibration of the ATLAS Pixel detector at LHC fulfils two main purposes: to tune the front-end configuration parameters for establishing the best operational settings and to measure the tuning performance through a subset of scans. An analysis framework has been set up in order to take actions on the detector given the outcome of a calibration scan (e.g. to create a mask for disabling noisy pixels). The software framework to control all aspects of the Pixel detector scans and analyses is called Calibration Console. The introduction of a new layer, equipped with new Front End-I4 Chips, required an update the Console architecture. It now handles scans and scans analyses applied together to chips with different characteristics. An overview of the newly developed Calibration Analysis Software will be presented, together with some preliminary result.

  14. Calorimetry of energy-efficient glow discharge apparatus design and calibration

    International Nuclear Information System (INIS)

    Benson, Thomas B.; Passell, Thomas O.

    2006-01-01

    This work aims to develop a 'family' or low-powered calorimetrically accurate glow discharge units, similar to that reported by Dardik et al. at lCCF-10, and to use these to test a wide range or cathode materials, electrode coatings, gas types, gas pressures, and power input levels. We will describe the design and calibration of these units. The strategy is to use a large number of very similar units so that the calorimetric response does not vary significantly for a given power level. The design is metal or sealed glass cylindrical tubes, charged with 0.4 - 50 Torr mixtures of deuterium, hydrogen, argon, or helium gases. Units operate from 0.2 to >2 W power input. The units have low mass ( 1.2 with more than 95% certainty. It provides a valuable new platform for large-scale exploration of excess heat effects in the gas phase, using low-power inputs in the 0-3 W range, This method proves to be inexpensive, quick, accurate, and easy to perform once the basics are mastered. The authors are interested in testing electrode materials from other sources, especially those that have already been successful in a liquid (electrolytic) environment

  15. pytc: Open-Source Python Software for Global Analyses of Isothermal Titration Calorimetry Data.

    Science.gov (United States)

    Duvvuri, Hiranmayi; Wheeler, Lucas C; Harms, Michael J

    2018-05-08

    Here we describe pytc, an open-source Python package for global fits of thermodynamic models to multiple isothermal titration calorimetry experiments. Key features include simplicity, the ability to implement new thermodynamic models, a robust maximum likelihood fitter, a fast Bayesian Markov-Chain Monte Carlo sampler, rigorous implementation, extensive documentation, and full cross-platform compatibility. pytc fitting can be done using an application program interface or via a graphical user interface. It is available for download at https://github.com/harmslab/pytc .

  16. A Generic Software Framework for Data Assimilation and Model Calibration

    NARCIS (Netherlands)

    Van Velzen, N.

    2010-01-01

    The accuracy of dynamic simulation models can be increased by using observations in conjunction with a data assimilation or model calibration algorithm. However, implementing such algorithms usually increases the complexity of the model software significantly. By using concepts from object oriented

  17. ATLAS tile calorimeter cesium calibration control and analysis software

    International Nuclear Information System (INIS)

    Solovyanov, O; Solodkov, A; Starchenko, E; Karyukhin, A; Isaev, A; Shalanda, N

    2008-01-01

    An online control system to calibrate and monitor ATLAS Barrel hadronic calorimeter (TileCal) with a movable radioactive source, driven by liquid flow, is described. To read out and control the system an online software has been developed, using ATLAS TDAQ components like DVS (Diagnostic and Verification System) to verify the hardware before running, IS (Information Server) for data and status exchange between networked computers, and other components like DDC (DCS to DAQ Connection), to connect to PVSS-based slow control systems of Tile Calorimeter, high voltage and low voltage. A system of scripting facilities, based on Python language, is used to handle all the calibration and monitoring processes from hardware perspective to final data storage, including various abnormal situations. A QT based graphical user interface to display the status of the calibration system during the cesium source scan is described. The software for analysis of the detector response, using online data, is discussed. Performance of the system and first experience from the ATLAS pit are presented

  18. ATLAS tile calorimeter cesium calibration control and analysis software

    Energy Technology Data Exchange (ETDEWEB)

    Solovyanov, O; Solodkov, A; Starchenko, E; Karyukhin, A; Isaev, A; Shalanda, N [Institute for High Energy Physics, Protvino 142281 (Russian Federation)], E-mail: Oleg.Solovyanov@ihep.ru

    2008-07-01

    An online control system to calibrate and monitor ATLAS Barrel hadronic calorimeter (TileCal) with a movable radioactive source, driven by liquid flow, is described. To read out and control the system an online software has been developed, using ATLAS TDAQ components like DVS (Diagnostic and Verification System) to verify the hardware before running, IS (Information Server) for data and status exchange between networked computers, and other components like DDC (DCS to DAQ Connection), to connect to PVSS-based slow control systems of Tile Calorimeter, high voltage and low voltage. A system of scripting facilities, based on Python language, is used to handle all the calibration and monitoring processes from hardware perspective to final data storage, including various abnormal situations. A QT based graphical user interface to display the status of the calibration system during the cesium source scan is described. The software for analysis of the detector response, using online data, is discussed. Performance of the system and first experience from the ATLAS pit are presented.

  19. Software System for the Calibration of X-Ray Measuring Instruments

    International Nuclear Information System (INIS)

    Gaytan-Gallardo, E.; Tovar-Munoz, V. M.; Cruz-Estrada, P.; Vergara-Martinez, F. J.; Rivero-Gutierrez, T.

    2006-01-01

    A software system that facilities the calibration of X-ray measuring instruments used in medical applications is presented. The Secondary Standard Dosimetry Laboratory (SSDL) of the Nuclear Research National Institute in Mexico (ININ in Spanish), supports activities concerning with ionizing radiations in medical area. One of these activities is the calibration of X-ray measuring instruments, in terms of air kerma or exposure by substitution method in an X-ray beam at a point where the rate has been determined by means of a standard ionization chamber. To automatize this process, a software system has been developed, the calibration system is composed by an X-ray unit, a Dynalizer IIIU X-ray meter by RADCAL, a commercial data acquisition card, the software system and the units to be tested and calibrated. A quality control plan has been applied in the development of the software system, ensuring that quality assurance procedures and standards are being followed

  20. RORASC: Software for the rotated-random-scan calibration procedure

    NARCIS (Netherlands)

    Janssen PHM; CWM

    1995-01-01

    De release-versie 1.0 van het programma RORASC wordt gepresenteerd, tezamen met instructies en richtlijnen voor installatie en gebruik van de software. RORASC speelt een essentiele rol bij de 'rotated-random-scan' methode voor modelkalibratie. De software is geschreven in standaard

  1. Software Note: Using BILOG for Fixed-Anchor Item Calibration

    Science.gov (United States)

    DeMars, Christine E.; Jurich, Daniel P.

    2012-01-01

    The nonequivalent groups anchor test (NEAT) design is often used to scale item parameters from two different test forms. A subset of items, called the anchor items or common items, are administered as part of both test forms. These items are used to adjust the item calibrations for any differences in the ability distributions of the groups taking…

  2. Application of PHOTON simulation software on calibration of HPGe detectors

    Energy Technology Data Exchange (ETDEWEB)

    Nikolic, J., E-mail: jnikolic@vinca.rs [University of Belgrade Institute for Nuclear Sciences Vinča, Mike Petrovica Alasa 12-16, 11001 Belgrade (Serbia); Puzovic, J. [University of Belgrade Faculty of Physics, Studentski trg 6, 11000 Belgrade (Serbia); Todorovic, D.; Rajacic, M. [University of Belgrade Institute for Nuclear Sciences Vinča, Mike Petrovica Alasa 12-16, 11001 Belgrade (Serbia)

    2015-11-01

    One of the major difficulties in gamma spectrometry of voluminous environmental samples is the efficiency calibration of the detectors used for the measurement. The direct measurement of different calibration sources, containing isolated γ-ray emitters within the energy range of interest, and subsequent fitting to a parametric function, is the most accurate and at the same time most complicated and time consuming method of efficiency calibration. Many other methods are developed in time, some of them using Monte Carlo simulation. One of such methods is a dedicated and user-friendly program PHOTON, developed to simulate the passage of photons through different media with different geometries. This program was used for efficiency calibration of three HPGe detectors, readily used in Laboratory for Environment and Radiation Protection of the Institute for Nuclear Sciences Vinca, Belgrade, Serbia. The simulation produced the spectral response of the detectors for fixed energy and for different sample geometries and matrices. Thus obtained efficiencies were compared to the values obtained by the measurement of the secondary reference materials and to the results obtained by GEANT4 simulation, in order to establish whether the simulated values agree with the experimental ones. To further analyze the results, a realistic measurement of the materials provided by the IAEA within different interlaboratory proficiency tests, was performed. The activities obtained using simulated efficiencies were compared to the reference values provided by the organizer. A good agreement in the mid energy section of the spectrum was obtained, while for low energies the lack of some parameters in the simulation libraries proved to produce unacceptable discrepancies.

  3. Calibration of a dedicated software for 3D rendering

    International Nuclear Information System (INIS)

    Abrantes, Marcos E.S.; Felix, Warley F.; Veloso, Maria Auxiliadora F.; Universidade Federal de Minas Gerais

    2017-01-01

    With the increasing use of 3D reconstruction techniques, to assist in diagnosis, dedicated programs are being widely used. For this they must be calibrated in order to encounter the values of the real volumes of the human tissues. The purpose of this work is to indicate correction and calibration values for true volumes, read in a 3D reconstruction system dedicated, using DICOM images of Computed Tomography. This work utilized a PMMA thorax phantom associated with the DICOM image and the volume found by a program of a tomograph. The physical volume of the PMMA phantom found was 10359.0 cm³. For the volumes found according to the structures of interest, the values are 11005.5 cm³, 10249.3 cm³ and 10205.1 cm³ and the correction values are -6.2%, +1.1% e +1.5% respectively for tissues: pulmonary, bony and soft tissues. The procedure performed can be used for calibration in other 3D reconstruction programs, observing the necessary corrections and the methodology used. (author)

  4. Calibration of a dedicated software for 3D rendering

    Energy Technology Data Exchange (ETDEWEB)

    Abrantes, Marcos E.S.; Felix, Warley F.; Veloso, Maria Auxiliadora F., E-mail: marcos.nuclear@yahoo.com.br, E-mail: warleyferreirafelix@gmail.com, E-mail: mdora@nuclear.ufmg.br [Faculdade Ciencias Medicas de Minas Gerais (FCMMG), Belo Horizonte, MG (Brazil); Universidade Federal de Minas Gerais (UFMG), Belo Horizonte, MG (Brazil). Departamento de Engenharia Nuclear

    2017-11-01

    With the increasing use of 3D reconstruction techniques, to assist in diagnosis, dedicated programs are being widely used. For this they must be calibrated in order to encounter the values of the real volumes of the human tissues. The purpose of this work is to indicate correction and calibration values for true volumes, read in a 3D reconstruction system dedicated, using DICOM images of Computed Tomography. This work utilized a PMMA thorax phantom associated with the DICOM image and the volume found by a program of a tomograph. The physical volume of the PMMA phantom found was 10359.0 cm³. For the volumes found according to the structures of interest, the values are 11005.5 cm³, 10249.3 cm³ and 10205.1 cm³ and the correction values are -6.2%, +1.1% e +1.5% respectively for tissues: pulmonary, bony and soft tissues. The procedure performed can be used for calibration in other 3D reconstruction programs, observing the necessary corrections and the methodology used. (author)

  5. A Software module for pointwise calibration of free form objevts and for uncertainty representation

    DEFF Research Database (Denmark)

    Savio, Enrico; Farmer, A.F.; De Chiffre, Leonardo

    . The Centre for Geometrical Metrology (CGM) at the Technical University of Denmark takes care of free form measurements, in collaboration with DIMEG, University of Padova, Italy. The present report describes a software module, MULTICAL, to be used for the calibration of free form objects. The purpose...... of the software is to calculate the uncertainty of free form measurements according to the method described in the draft standard ISO/WD 15530-6....

  6. Designing a Signal Conditioning System with Software Calibration for Resistor-feedback Patch Clamp Amplifier.

    Science.gov (United States)

    Hu, Gang; Zhu, Quanhui; Qu, Anlian

    2005-01-01

    In this paper, a programmable signal conditioning system based on software calibration for resistor-feedback patch clamp amplifier (PCA) has been described, this system is mainly composed of frequency correction, programmable gain and filter whose parameters are configured by software automatically to minimize the errors, A lab-designed data acquisition system (DAQ) is used to implement data collections and communications with PC. The laboratory test results show good agreement with design specifications.

  7. Conceptual study of calibration software for large scale input accountancy tank

    International Nuclear Information System (INIS)

    Uchikoshi, Seiji; Yasu, Kan-ichi; Watanabe, Yuichi; Matsuda, Yuji; Kawai, Akio; Tamura, Toshiyuki; Shimizu, Hidehiko.

    1996-01-01

    Demonstration experiments for large scale input accountancy tank are going to be under way by Nuclear Material Control Center. Development of calibration software for accountancy system with dip-tube manometer is an important task in the experiments. A conceptual study of the software has been carried out to construct high precision accountancy system. And, the study was based on ANSI N15.19-1989. Items of the study are overall configuration, correction method for influence of bubble formation, function model of calibration, and fitting method for calibration curve. Following remarks are the results of this study. 1) Overall configuration of the software was constructed. 2) It was shown by numerical solution, that the influence of bubble formation can be corrected using period of pressure wave. 3) Two function models of calibration for well capacity and for inner structure volume were prepared from tank design, and good fitness of the model for net capacity (balance of both models) was confirmed by fitting to designed shape of the tank. 4) The necessity of further consideration about both-variables-in-error-model and cumulative-error-model was recognized. We are going to develop a practical software on the basis of the results, and to verify it by the demonstration experiments. (author)

  8. The issue of gamma spectral system sourceless object calibration software using in radioactive environment measurement

    International Nuclear Information System (INIS)

    Shen Ming; Zhu Yuelong; Zhao Yanzi

    2009-01-01

    The paper introduces the characteristic, based method of HPGe detector LabSOCS (Laboratory Sourceless Object Calibration Software). Compared measured efficiency and LabSOCS efficiency for different point sources, and the tolerance is about 6% at middle and high energy range. For cylinder samples of dirt, animal ash and plant ash, the results of verification is 7%-10%. (authors)

  9. Software framework and jet energy scale calibration in the ATLAS experiment

    International Nuclear Information System (INIS)

    Binet, Sebastien

    2006-01-01

    This thesis presents the work achieved to instrument the ATLAS software framework, ATHENA, with a library of tools and utensils for the physics analysis as well as the extraction of the jet energy scale using physics events (in-situ calibration). The software part presents the various components of the ATHENA framework which handles the simulated and reconstructed data flow as well as the different stages of this process, before and during the data taking. The building of a library of tools easing the reconstruction of physics objects, their association with Monte-Carlo particles and their API is then explained. The need for common language and collaboration-wide utensils is emphasised as it allows to share the workload of validating these tools and to get reproducible physics results. The analysis part deals with the implementation of a light jet energy scale calibration algorithm within the C++ framework. This calibration algorithm makes use of W bosons decaying into light jets within semileptonic t t-bar events. From the processing of fast and full simulation data with this algorithm, it seems possible to reach a percent level knowledge of the light jet energy scale. Finally, the feasibility study of the b-jet energy scale calibration using γZ 0 → γb b-bar events is presented. It is shown that a purely sequential approach is not sufficient to extract the signal nor to collect a sufficient amount of Z 0 to calibrate the b-jet energy scale. (author)

  10. Enhancing Seismic Calibration Research Through Software Automation and Scientific Information Management

    Energy Technology Data Exchange (ETDEWEB)

    Ruppert, S D; Dodge, D A; Ganzberger, M D; Harris, D B; Hauk, T F

    2009-07-07

    The National Nuclear Security Administration (NNSA) Ground-Based Nuclear Explosion Monitoring Research and Development (GNEMRD) Program at LLNL continues to make significant progress enhancing the process of deriving seismic calibrations and performing scientific integration, analysis, and information management with software automation tools. Our tool efforts address the problematic issues of very large datasets and varied formats encountered during seismic calibration research. New information management and analysis tools have resulted in demonstrated gains in efficiency of producing scientific data products and improved accuracy of derived seismic calibrations. In contrast to previous years, software development work this past year has emphasized development of automation at the data ingestion level. This change reflects a gradually-changing emphasis in our program from processing a few large data sets that result in a single integrated delivery, to processing many different data sets from a variety of sources. The increase in the number of sources had resulted in a large increase in the amount of metadata relative to the final volume of research products. Software developed this year addresses the problems of: (1) Efficient metadata ingestion and conflict resolution; (2) Automated ingestion of bulletin information; (3) Automated ingestion of waveform information from global data centers; and (4) Site Metadata and Response transformation required for certain products. This year, we also made a significant step forward in meeting a long-standing goal of developing and using a waveform correlation framework. Our objective for such a framework is to extract additional calibration data (e.g. mining blasts) and to study the extent to which correlated seismicity can be found in global and regional scale environments.

  11. Software development with two port calibration techniques for RHIC impedance measurements

    International Nuclear Information System (INIS)

    Mane, V.; Shea, T.

    1993-01-01

    The coupling impedance of accelerator devices is measured by simulating the beam with a central wire and measuring the scattering parameters of the system. The wire pipe system forms a mismatch with the 50 ohm transmission line. An integrated software environment has been developed in LabVIEW, for the Macintosh. The program measures the scattering parameters of some known standards, determines the connect scattering parameters of a device using TRL calibration technique and gives the impedance of the device. Its performance has been tested for some known microwave devices

  12. Calibration

    International Nuclear Information System (INIS)

    Greacen, E.L.; Correll, R.L.; Cunningham, R.B.; Johns, G.G.; Nicolls, K.D.

    1981-01-01

    Procedures common to different methods of calibration of neutron moisture meters are outlined and laboratory and field calibration methods compared. Gross errors which arise from faulty calibration techniques are described. The count rate can be affected by the dry bulk density of the soil, the volumetric content of constitutional hydrogen and other chemical components of the soil and soil solution. Calibration is further complicated by the fact that the neutron meter responds more strongly to the soil properties close to the detector and source. The differences in slope of calibration curves for different soils can be as much as 40%

  13. ENHANCING SEISMIC CALIBRATION RESEARCH THROUGH SOFTWARE AUTOMATION AND SCIENTIFIC INFORMATION MANAGEMENT

    Energy Technology Data Exchange (ETDEWEB)

    Ruppert, S; Dodge, D A; Ganzberger, M D; Hauk, T F; Matzel, E M

    2008-07-03

    The National Nuclear Security Administration (NNSA) Ground-Based Nuclear Explosion Monitoring Research and Development (GNEMRD) Program at LLNL continues to make significant progress enhancing the process of deriving seismic calibrations and performing scientific integration, analysis, and information management with software automation tools. Our tool efforts address the problematic issues of very large datasets and varied formats encountered during seismic calibration research. New information management and analysis tools have resulted in demonstrated gains in efficiency of producing scientific data products and improved accuracy of derived seismic calibrations. The foundation of a robust, efficient data development and processing environment is comprised of many components built upon engineered versatile libraries. We incorporate proven industry 'best practices' throughout our code and apply source code and bug tracking management as well as automatic generation and execution of unit tests for our experimental, development and production lines. Significant software engineering and development efforts have produced an object-oriented framework that provides database centric coordination between scientific tools, users, and data. Over a half billion parameters, signals, measurements, and metadata entries are all stored in a relational database accessed by an extensive object-oriented multi-technology software framework that includes stored procedures, real-time transactional database triggers and constraints, as well as coupled Java and C++ software libraries to handle the information interchange and validation requirements. Significant resources were applied to schema design to enable management of processing methods and station parameters, responses and metadata. This allowed for the development of merged ground-truth (GT) data sets compiled by the NNSA labs and AFTAC that include hundreds of thousands of events and tens of millions of arrivals. The

  14. A hardware-software system for the automation of verification and calibration of oil metering units secondary equipment

    Science.gov (United States)

    Boyarnikov, A. V.; Boyarnikova, L. V.; Kozhushko, A. A.; Sekachev, A. F.

    2017-08-01

    In the article the process of verification (calibration) of oil metering units secondary equipment is considered. The purpose of the work is to increase the reliability and reduce the complexity of this process by developing a software and hardware system that provides automated verification and calibration. The hardware part of this complex carries out the commutation of the measuring channels of the verified controller and the reference channels of the calibrator in accordance with the introduced algorithm. The developed software allows controlling the commutation of channels, setting values on the calibrator, reading the measured data from the controller, calculating errors and compiling protocols. This system can be used for checking the controllers of the secondary equipment of the oil metering units in the automatic verification mode (with the open communication protocol) or in the semi-automatic verification mode (without it). The peculiar feature of the approach used is the development of a universal signal switch operating under software control, which can be configured for various verification methods (calibration), which allows to cover the entire range of controllers of metering units secondary equipment. The use of automatic verification with the help of a hardware and software system allows to shorten the verification time by 5-10 times and to increase the reliability of measurements, excluding the influence of the human factor.

  15. Aplicaciones de Software Libre para automatizar servicios en una biblioteca: uso de software Calibre para la creación de un repositorio digital

    Directory of Open Access Journals (Sweden)

    Rolando Herrera Burgos

    2015-01-01

    Full Text Available Este artículo propone el uso de herramientas informáticas desarrolladas bajo el modelo de Software Libre para poder automatizar de forma sencilla distintos servicios que pueden brindar las bibliotecas. Se explora el uso de la aplicación Calibre para crear un repositorio digital que permita a los usuarios acceder a materiales en línea y a texto completo mediante el uso de Internet.

  16. Theory of calorimetry

    CERN Document Server

    Zielenkiewicz, Wojciech

    2004-01-01

    The purpose of this book is to give a comprehensive description of the theoretical fundamentals of calorimetry. The considerations are based on the relations deduced from the laws and general equations of heat exchange theory and steering theory.

  17. WE-D-9A-06: Open Source Monitor Calibration and Quality Control Software for Enterprise Display Management

    Energy Technology Data Exchange (ETDEWEB)

    Bevins, N; Vanderhoek, M; Lang, S; Flynn, M [Henry Ford Health System, Detroit, MI (United States)

    2014-06-15

    Purpose: Medical display monitor calibration and quality control present challenges to medical physicists. The purpose of this work is to demonstrate and share experiences with an open source package that allows for both initial monitor setup and routine performance evaluation. Methods: A software package, pacsDisplay, has been developed over the last decade to aid in the calibration of all monitors within the radiology group in our health system. The software is used to calibrate monitors to follow the DICOM Grayscale Standard Display Function (GSDF) via lookup tables installed on the workstation. Additional functionality facilitates periodic evaluations of both primary and secondary medical monitors to ensure satisfactory performance. This software is installed on all radiology workstations, and can also be run as a stand-alone tool from a USB disk. Recently, a database has been developed to store and centralize the monitor performance data and to provide long-term trends for compliance with internal standards and various accrediting organizations. Results: Implementation and utilization of pacsDisplay has resulted in improved monitor performance across the health system. Monitor testing is now performed at regular intervals and the software is being used across multiple imaging modalities. Monitor performance characteristics such as maximum and minimum luminance, ambient luminance and illuminance, color tracking, and GSDF conformity are loaded into a centralized database for system performance comparisons. Compliance reports for organizations such as MQSA, ACR, and TJC are generated automatically and stored in the same database. Conclusion: An open source software solution has simplified and improved the standardization of displays within our health system. This work serves as an example method for calibrating and testing monitors within an enterprise health system.

  18. WE-D-9A-06: Open Source Monitor Calibration and Quality Control Software for Enterprise Display Management

    International Nuclear Information System (INIS)

    Bevins, N; Vanderhoek, M; Lang, S; Flynn, M

    2014-01-01

    Purpose: Medical display monitor calibration and quality control present challenges to medical physicists. The purpose of this work is to demonstrate and share experiences with an open source package that allows for both initial monitor setup and routine performance evaluation. Methods: A software package, pacsDisplay, has been developed over the last decade to aid in the calibration of all monitors within the radiology group in our health system. The software is used to calibrate monitors to follow the DICOM Grayscale Standard Display Function (GSDF) via lookup tables installed on the workstation. Additional functionality facilitates periodic evaluations of both primary and secondary medical monitors to ensure satisfactory performance. This software is installed on all radiology workstations, and can also be run as a stand-alone tool from a USB disk. Recently, a database has been developed to store and centralize the monitor performance data and to provide long-term trends for compliance with internal standards and various accrediting organizations. Results: Implementation and utilization of pacsDisplay has resulted in improved monitor performance across the health system. Monitor testing is now performed at regular intervals and the software is being used across multiple imaging modalities. Monitor performance characteristics such as maximum and minimum luminance, ambient luminance and illuminance, color tracking, and GSDF conformity are loaded into a centralized database for system performance comparisons. Compliance reports for organizations such as MQSA, ACR, and TJC are generated automatically and stored in the same database. Conclusion: An open source software solution has simplified and improved the standardization of displays within our health system. This work serves as an example method for calibrating and testing monitors within an enterprise health system

  19. ATLAS calorimetry: Trigger, simulation and jet calibration

    CERN Document Server

    Weber, Pavel

    2008-01-01

    The Pre-Processor system of the ATLAS Level-1 Calorimeter Trigger performs complex processing of analog trigger tower signals from electromagnetic and hadronic calorimeters. The main processing block of the Pre-Processor System is the Multi-Chip Module (MCM). The first part of this thesis describes MCM quality assurance tests that have been developed, their use in the MCM large scale production and the results that have been obtained. In the second part of the thesis a validation of a shower parametrisation model for the ATLAS fast simulation package ATLFAST based on QCD dijet events is performed. A detailed comparison of jet response and jet energy resolution between the fast and the full simulation is presented. The uniformity of the calorimeter response has a significant impact on the accuracy of the jet energy measurement. A study of the calorimeter intercalibration using QCD dijet events is presented in the last part of the thesis. The intercalibration study is performed in azimuth angle phi and in pseud...

  20. Scintillator plate calorimetry

    International Nuclear Information System (INIS)

    Price, L.E.

    1990-01-01

    Calorimetry using scintillator plates or tiles alternated with sheets of (usually heavy) passive absorber has been proven over multiple generations of collider detectors. Recent detectors including UA1, CDF, and ZEUS have shown good results from such calorimeters. The advantages offered by scintillator calorimetry for the SSC environment, in particular, are speed (<10 nsec), excellent energy resolution, low noise, and ease of achieving compensation and hence linearity. On the negative side of the ledger can be placed the historical sensitivity of plastic scintillators to radiation damage, the possibility of nonuniform response because of light attenuation, and the presence of cracks for light collection via wavelength shifting plastic (traditionally in sheet form). This approach to calorimetry is being investigated for SSC use by a collaboration of Ames Laboratory/Iowa State University, Argonne National Laboratory, Bicron Corporation, Florida State University, Louisiana State University, University of Mississippi, Oak Ridge National Laboratory, Virginia Polytechnic Institute and State University, Westinghouse Electric Corporation, and University of Wisconsin

  1. Calorimetry for the SSC

    Energy Technology Data Exchange (ETDEWEB)

    Gordon, H.A.; Grannis, P.D.

    1984-01-01

    The activities related to calorimetry at Snowmass took place in three main areas. These were: (1) The performance criteria for SSC calorimetry, including the requirements on hermeticity, shower containment, segmentation and time resolution. The use of calorimetric means of particle identification was studied. (2) The study of triggering methods using calorimeter energy, angle and timing information. (3) A review of a wide variety of calorimeter materials for absorber and sampling, as well as several means of obtaining the readout of the energy deposits. 48 references, 10 figures, 1 table.

  2. Calorimetry for the SSC

    International Nuclear Information System (INIS)

    Gordon, H.A.; Grannis, P.D.

    1984-01-01

    The activities related to calorimetry at Snowmass took place in three main areas. These were: (1) The performance criteria for SSC calorimetry, including the requirements on hermeticity, shower containment, segmentation and time resolution. The use of calorimetric means of particle identification was studied. (2) The study of triggering methods using calorimeter energy, angle and timing information. (3) A review of a wide variety of calorimeter materials for absorber and sampling, as well as several means of obtaining the readout of the energy deposits. 48 references, 10 figures, 1 table

  3. Texas flexible pavements and overlays : calibration plans for M-E models and related software.

    Science.gov (United States)

    2013-06-01

    This five-year project was initiated to collect materials and pavement performance data on a minimum of 100 highway test sections around the State of Texas, incorporating flexible pavements and overlays. Besides being used to calibrate and validate m...

  4. Calorimetry at the SSC

    International Nuclear Information System (INIS)

    Wigmans, R.

    1988-01-01

    The state of the art, and the present understanding of the basic limitations in hadron calorimetry, are briefly described. The various options for SSC calorimeters are discussed, and the R ampersand D needed for the ones that look most promising is outlined. The most promising candidates are (1) lead/scintillating fibers and (2) lead (or uranium)/TMS (or other warm liquids)

  5. Calorimetry at the SSC

    International Nuclear Information System (INIS)

    Wigmans, R.

    1987-09-01

    The state of the art, and our present understanding of the basic limitations in hadron calorimetry, are briefly described. The various options for SSC calorimeters are discussed, and the R and D needed for the ones that look most promising is outlined. 13 refs.; 8 figs

  6. A guide to automation techniques in calorimetry

    International Nuclear Information System (INIS)

    Renz, D.P.; Wetzel, J.R.; Breakall, K.L.; James, S.J.; Kasperski, P.W.

    1992-01-01

    Many improvements occurring in calorimetry measurement technology in the past few years will help current users of calorimeters to achieve better use of their existing systems. These include a more user friendly operator computer interface, a more detailed printout at the end of each run, improved data processing to eliminate operator error, and improved system monitoring to detect system or environmental problems. In addition, an electrical calibration heater has been developed to replace plutonium-238 heat standards for calibrating calorimeters, and several automation systems allow for easier and safer system operation

  7. Recent developments in silicon calorimetry

    International Nuclear Information System (INIS)

    Brau, J.E.

    1990-11-01

    We present a survey of some of the recent calorimeter applications of silicon detectors. The numerous attractive features of silicon detectors are summarized, with an emphasis on those aspects important to calorimetry. Several of the uses of this technology are summarized and referenced. We consider applications for electromagnetic calorimetry, hadronic calorimetry, and proposals for the SSC

  8. APERO, AN OPEN SOURCE BUNDLE ADJUSMENT SOFTWARE FOR AUTOMATIC CALIBRATION AND ORIENTATION OF SET OF IMAGES

    Directory of Open Access Journals (Sweden)

    M. Pierrot Deseilligny

    2012-09-01

    Full Text Available IGN has developed a set of photogrammetric tools, APERO and MICMAC, for computing 3D models from set of images. This software, developed initially for its internal needs are now delivered as open source code. This paper focuses on the presentation of APERO the orientation software. Compared to some other free software initiatives, it is probably more complex but also more complete, its targeted user is rather professionals (architects, archaeologist, geomophologist than people. APERO uses both computer vision approach for estimation of initial solution and photogrammetry for a rigorous compensation of the total error; it has a large library of parametric model of distortion allowing a precise modelization of all the kind of pinhole camera we know, including several model of fish-eye; there is also several tools for geo-referencing the result. The results are illustrated on various application, including the data-set of 3D-Arch workshop.

  9. Tests of methods and software for set-valued model calibration and sensitivity analyses

    NARCIS (Netherlands)

    Janssen PHM; Sanders R; CWM

    1995-01-01

    Testen worden besproken die zijn uitgevoerd op methoden en software voor calibratie middels 'rotated-random-scanning', en voor gevoeligheidsanalyse op basis van de 'dominant direction analysis' en de 'generalized sensitivity analysis'. Deze technieken werden

  10. Scintillating-fibre calorimetry

    International Nuclear Information System (INIS)

    Livan, M.; Vercesi, V.; Wigmans, R.

    1995-01-01

    In the past decade, calorimetry based on scintillating plastic fibres as active elements was developed from a conceptual idea to a mature detector technology, which is nowadays widely applied in particle physics experiments. This development and the performance characteristics of representative calorimeters, both for the detection of electromagnetic and hadronic showers, are reviewed. We also discuss new information on shower development processes in dense matter and its application to calorimetric principles that has emerged from some very thorough studies that were performed in the framework of this development. (orig.)

  11. Laser-flash calorimetry

    International Nuclear Information System (INIS)

    Takahashi, Y.; Nakamura, J.-I.

    1982-01-01

    The heat capacity of vanadium has been measured by laser-flash calorimetry in the temperature region from 80 to 1000 K. The results are compared with available low- and high-temperature heat capacities, and revised thermodynamic values of vanadium are given. No heat-capacity anomaly has been found in the pure vanadium sample over the temperature range investigated, while a small heat-capacity discontinuity, less than 1.2 J.K -1 .mol -1 , has been observed at 220 to 230 K on the same sample but electropolished before measurement. This anomaly disappeared after annealing at 1000 K in vacuo for 1 h and is attributable to the introduction of a small amount of hydrogen during electropolishing. (author)

  12. Isothermal Titration Calorimetry Can Provide Critical Thinking Opportunities

    Science.gov (United States)

    Moore, Dale E.; Goode, David R.; Seney, Caryn S.; Boatwright, Jennifer M.

    2016-01-01

    College chemistry faculties might not have considered including isothermal titration calorimetry (ITC) in their majors' curriculum because experimental data from this instrumental method are often analyzed via automation (software). However, the software-based data analysis can be replaced with a spreadsheet-based analysis that is readily…

  13. Scintillating Fibre Calorimetry at the LHC

    CERN Multimedia

    2002-01-01

    Good electromagnetic and hadronic calorimetry will play a central role in an LHC detector. The lead/scintillating fibre calorimeter technique provides a fast signal response well matched to the LHC rate requirements. It can be made to give equal response for electrons and hadrons (compensation) with good electromagnetic and hadronic energy resolutions.\\\\ \\\\ The aim of this R&D proposal is to study in detail the aspects that are relevant for application of this type of calorimeter in an LHC environment, including its integration in a larger system of detectors, e.g.~projective geometry, radiation hardness, light detection, calibration and stability monitoring, electron/hadron separation.....

  14. Software

    Energy Technology Data Exchange (ETDEWEB)

    Macedo, R.; Budd, G.; Ross, E.; Wells, P.

    2010-07-15

    The software section of this journal presented new software programs that have been developed to help in the exploration and development of hydrocarbon resources. Software provider IHS Inc. has made additions to its geological and engineering analysis software tool, IHS PETRA, a product used by geoscientists and engineers to visualize, analyze and manage well production, well log, drilling, reservoir, seismic and other related information. IHS PETRA also includes a directional well module and a decline curve analysis module to improve analysis capabilities in unconventional reservoirs. Petris Technology Inc. has developed a software to help manage the large volumes of data. PetrisWinds Enterprise (PWE) helps users find and manage wellbore data, including conventional wireline and MWD core data; analysis core photos and images; waveforms and NMR; and external files documentation. Ottawa-based Ambercore Software Inc. has been collaborating with Nexen on the Petroleum iQ software for steam assisted gravity drainage (SAGD) producers. Petroleum iQ integrates geology and geophysics data with engineering data in 3D and 4D. Calgary-based Envirosoft Corporation has developed a software that reduces the costly and time-consuming effort required to comply with Directive 39 of the Alberta Energy Resources Conservation Board. The product includes an emissions modelling software. Houston-based Seismic Micro-Technology (SMT) has developed the Kingdom software that features the latest in seismic interpretation. Holland-based Joa Oil and Gas and Calgary-based Computer Modelling Group have both supplied the petroleum industry with advanced reservoir simulation software that enables reservoir interpretation. The 2010 software survey included a guide to new software applications designed to facilitate petroleum exploration, drilling and production activities. Oil and gas producers can use the products for a range of functions, including reservoir characterization and accounting. In

  15. The use of calorimetry for plutonium assay

    International Nuclear Information System (INIS)

    Mason, J.A.

    1982-12-01

    Calorimetry is a technique for measuring the thermal power of heat-producing substances. The technique may be applied to the measurement of plutonium-bearing materials which evolve heat as a result of alpha and beta decay. A calorimetric measurement of the thermal power of a plutonium sample, combined with a knowledge or measurement of the plutonium isotopic mass ratios of the sample provides a convenient and accurate, non-destructive measure of the total plutonium mass of the sample. The present report provides a description, and an assessment of the calorimetry technique applied to the assay of plutonium-bearing materials. Types and characteristics of plutonium calorimeters are considered, as well as calibration and operating procedures. The instrumentation used with plutonium calorimeters is described and the use of computer control for calorimeter automation is discussed. A critical review and assessment of plutonium calorimetry literature since 1970 is presented. Both fuel element and plutonium-bearing material calorimeters are considered. The different types of plutonium calorimeters are evaluated and their relative merits are discussed. A combined calorimeter and gamma-ray measurement assay system is considered. The design principles of plutonium assay calorimeters are considered. An automatic, computer-based calorimeter control system is proposed in conjunction with a general plutonium assay calorimeter design. (author)

  16. Calorimetry at the international linear collider. From simulation to reality

    Energy Technology Data Exchange (ETDEWEB)

    Wattimena, Nanda

    2010-02-15

    Calorimetry plays a crucial role in ongoing and upcoming high-energy physics experiments. To build a powerful calorimetric system with a performance tailored to the expected physics signatures, demands dedicated research and development of new readout technologies as well as dedicated reconstruction algorithms. The presented design of a calorimetric system which meets the high demands of precision physics at the future linear collider ILC, follows the paradigm of particle ow. Particle ow is a reconstruction principle that relies on a calorimetric system with high spatial granularity. In the detector optimisation process, the development of hardware and software are interlinked and cannot be judged independently. This thesis addresses two different aspects of detector optimisation, a test of the detector design against one example physics scenario and the development of a stable calibration procedure. In the rst part, a gauge-mediated Supersymmetry breaking scenario is used to test the design of the electromagnetic calorimeter in a full detector simulation study. The reconstruction of the neutralino properties, each decaying into a photon and a gravitino, requires a good energy resolution, as well as excellent position and angular resolution. The error bounds on the neutralino mass is strongly linked to the energy resolution, while the position and angular reconstruction of neutral particles is essential for the determination of the neutralino lifetime. The second part of this thesis focuses on the calibration procedure for a prototype of the hadron calorimeter. 7608 novel photodetectors are operated and tested in this prototype. They are exposed to beams of well de ned particle type and energy. The calibration is tested with a detailed study of electromagnetic showers inside the cubic-metre-sized prototype, with special attention paid towards the non-linearity correction. (orig.)

  17. Calorimetry at the international linear collider. From simulation to reality

    International Nuclear Information System (INIS)

    Wattimena, Nanda

    2010-02-01

    Calorimetry plays a crucial role in ongoing and upcoming high-energy physics experiments. To build a powerful calorimetric system with a performance tailored to the expected physics signatures, demands dedicated research and development of new readout technologies as well as dedicated reconstruction algorithms. The presented design of a calorimetric system which meets the high demands of precision physics at the future linear collider ILC, follows the paradigm of particle ow. Particle ow is a reconstruction principle that relies on a calorimetric system with high spatial granularity. In the detector optimisation process, the development of hardware and software are interlinked and cannot be judged independently. This thesis addresses two different aspects of detector optimisation, a test of the detector design against one example physics scenario and the development of a stable calibration procedure. In the rst part, a gauge-mediated Supersymmetry breaking scenario is used to test the design of the electromagnetic calorimeter in a full detector simulation study. The reconstruction of the neutralino properties, each decaying into a photon and a gravitino, requires a good energy resolution, as well as excellent position and angular resolution. The error bounds on the neutralino mass is strongly linked to the energy resolution, while the position and angular reconstruction of neutral particles is essential for the determination of the neutralino lifetime. The second part of this thesis focuses on the calibration procedure for a prototype of the hadron calorimeter. 7608 novel photodetectors are operated and tested in this prototype. They are exposed to beams of well de ned particle type and energy. The calibration is tested with a detailed study of electromagnetic showers inside the cubic-metre-sized prototype, with special attention paid towards the non-linearity correction. (orig.)

  18. An Introduction to ATLAS Pixel Detector DAQ and Calibration Software Based on a Year's Work at CERN for the Upgrade from 8 to 13 TeV

    CERN Document Server

    AUTHOR|(CDS)2094561

    An overview is presented of the ATLAS pixel detector Data Acquisition (DAQ) system obtained by the author during a year-long opportunity to work on calibration software for the 2015-16 Layer‑2 upgrade. It is hoped the document will function more generally as an easy entry point for future work on ATLAS pixel detector calibration systems. To begin with, the overall place of ATLAS pixel DAQ within the CERN Large Hadron Collider (LHC), the purpose of the Layer-2 upgrade and the fundamentals of pixel calibration are outlined. This is followed by a brief look at the high level structure and key features of the calibration software. The paper concludes by discussing some difficulties encountered in the upgrade project and how these led to unforeseen alternative enhancements, such as development of calibration “simulation” software allowing the soundness of the ongoing upgrade work to be verified while not all of the actual readout hardware was available for the most comprehensive testing.

  19. DAQ Software Contributions, Absolute Scale Energy Calibration and Background Evaluation for the NOvA Experiment at Fermilab

    Energy Technology Data Exchange (ETDEWEB)

    Flumerfelt, Eric Lewis [Univ. of Tennessee, Knoxville, TN (United States)

    2015-08-01

    The NOvA (NuMI Off-axis ve [nu_e] Appearance) Experiment is a long-baseline accelerator neutrino experiment currently in its second year of operations. NOvA uses the Neutrinos from the Main Injector (NuMI) beam at Fermilab, and there are two main off-axis detectors: a Near Detector at Fermilab and a Far Detector 810 km away at Ash River, MN. The work reported herein is in support of the NOvA Experiment, through contributions to the development of data acquisition software, providing an accurate, absolute-scale energy calibration for electromagnetic showers in NOvA detector elements, crucial to the primary electron neutrino search, and through an initial evaluation of the cosmic background rate in the NOvA Far Detector, which is situated on the surface without significant overburden. Additional support work for the NOvA Experiment is also detailed, including DAQ Server Administration duties and a study of NOvA’s sensitivity to neutrino oscillations into a “sterile” state.

  20. A Software Module for High-Accuracy Calibration of Rings and Cylinders on CMM using Multi-Orientation Techniques (Multi-Step and Reversal methods)

    DEFF Research Database (Denmark)

    Tosello, Guido; De Chiffre, Leonardo

    . The Centre for Geometrical Metrology (CGM) at the Technical University of Denmark takes care of free form measurements, in collaboration with DIMEG, University of Padova, Italy. The present report describes a software module, ROUNDCAL, to be used for high-accuracy calibration of rings and cylinders....... The purpose of the software is to calculate the form error and the least square circle of rings and cylinders by mean of average of pontwise measuring results becoming from so-called multi-orientation techniques (both reversal and multi-step methods) in order to eliminate systematic errors of CMM ....

  1. Liquid Argon Calorimetry with LHC-Performance Specifications

    CERN Multimedia

    2002-01-01

    % RD-3 Liquid Argon Calorimetry with LHC-Performance Specifications \\\\ \\\\Good electromagnetic and hadronic calorimetry will play a central role in an LHC detector. Among the techniques used so far, or under development, the liquid argon sampling calorimetry offers high radiation resistence, good energy resolution (electromagnetic and hadronic), excellent calibration stability and response uniformity. Its rate capabilities, however, do not yet match the requirements for LHC. \\\\ \\\\The aim of this proposal is to improve the technique in such a way that high granularity, good hermiticity and adequate rate capabilities are obtained, without compromising the above mentioned properties. To reach this goal, we propose to use a novel structure, the $^{\\prime\\prime}$accordion$^{\\prime\\prime}$, coupled to fast preamplifiers working at liquid argon temperature. Converter and readout electrodes are no longer planar and perpendicular to particles, as usual, but instead they are wiggled around a plane containing particles. ...

  2. An investigation into the long-term impact of the calibration of software estimation models using raw historical data

    OpenAIRE

    Shadle, Daryl Allen.

    1994-01-01

    Approved for public release, distribution unlimited The benefit of software cost estimation is universally recognized as one of the cornerstones of effective software project management and control. Despite the advances of computer-based estimation tools, their accuracy remains largely inadequate, and their utility among software development practitioners is limited. Consequently, the optimal estimation of software cost remains an elusive goal of most project managers. Central to this issu...

  3. Calorimetry at industrial electron accelerators

    DEFF Research Database (Denmark)

    Miller, Arne; Kovacs, A.

    1985-01-01

    Calorimetry is a convenient way to measure doses at industrial electron accelerators, where high absorbed doses (1-100 kGy) are delivered at dose rates of 102-105 Gy s-1 or even higher. Water calorimeters have been used for this purpose for several years, but recently other materials such as grap......Calorimetry is a convenient way to measure doses at industrial electron accelerators, where high absorbed doses (1-100 kGy) are delivered at dose rates of 102-105 Gy s-1 or even higher. Water calorimeters have been used for this purpose for several years, but recently other materials...

  4. Calorimetry end-point predictions

    International Nuclear Information System (INIS)

    Fox, M.A.

    1981-01-01

    This paper describes a portion of the work presently in progress at Rocky Flats in the field of calorimetry. In particular, calorimetry end-point predictions are outlined. The problems associated with end-point predictions and the progress made in overcoming these obstacles are discussed. The two major problems, noise and an accurate description of the heat function, are dealt with to obtain the most accurate results. Data are taken from an actual calorimeter and are processed by means of three different noise reduction techniques. The processed data are then utilized by one to four algorithms, depending on the accuracy desired to determined the end-point

  5. Software framework and jet energy scale calibration in the ATLAS experiment; Environnement logiciel et etalonnage de l'echelle en energie des jets dans l'experience ATLAS

    Energy Technology Data Exchange (ETDEWEB)

    Binet, Sebastien [Laboratoire de Physique Corpusculaire, Universite Blaise Pascal - CNRS/IN2P3, 63000 Aubiere Cedex (France)

    2006-07-01

    This thesis presents the work achieved to instrument the ATLAS software framework, ATHENA, with a library of tools and utensils for the physics analysis as well as the extraction of the jet energy scale using physics events (in-situ calibration). The software part presents the various components of the ATHENA framework which handles the simulated and reconstructed data flow as well as the different stages of this process, before and during the data taking. The building of a library of tools easing the reconstruction of physics objects, their association with Monte-Carlo particles and their API is then explained. The need for common language and collaboration-wide utensils is emphasised as it allows to share the workload of validating these tools and to get reproducible physics results. The analysis part deals with the implementation of a light jet energy scale calibration algorithm within the C++ framework. This calibration algorithm makes use of W bosons decaying into light jets within semileptonic t t-bar events. From the processing of fast and full simulation data with this algorithm, it seems possible to reach a percent level knowledge of the light jet energy scale. Finally, the feasibility study of the b-jet energy scale calibration using {gamma}Z{sup 0} {yields} {gamma}b b-bar events is presented. It is shown that a purely sequential approach is not sufficient to extract the signal nor to collect a sufficient amount of Z{sup 0} to calibrate the b-jet energy scale. (author)

  6. Calorimetry of non-reacting systems

    CERN Document Server

    McCullough, John P

    2013-01-01

    Experimental Thermodynamics, Volume 1: Calorimetry of Non-Reacting Systems covers the heat capacity determinations for chemical substances in the solid, liquid, solution, and vapor states, at temperatures ranging from near the absolute zero to the highest at which calorimetry is feasible.This book is divided into 14 chapters. The first four chapters provide background information and general principles applicable to all types of calorimetry of non-reacting systems. The remaining 10 chapters deal with specific types of calorimetry. Most of the types of calorimetry treated are developed over a c

  7. Efficient multi-objective calibration of a computationally intensive hydrologic model with parallel computing software in Python

    Science.gov (United States)

    With enhanced data availability, distributed watershed models for large areas with high spatial and temporal resolution are increasingly used to understand water budgets and examine effects of human activities and climate change/variability on water resources. Developing parallel computing software...

  8. Water calorimetry: The heat defect

    International Nuclear Information System (INIS)

    Klassen, N.V.; Ross, C.K.

    1997-01-01

    Domen developed a sealed water calorimeter at NIST to measure absorbed dose to water from ionizing radiation. This calorimeter exhibited anomalous behavior using water saturated with gas mixtures of H 2 O 2 . Using computer simulations of the radiolysis of water, the authors show that the observed behavior can be explained if, in the gas mixtures, the amount-of-substance of H 2 and of O 2 differed significantly from 50%. The authors also report the results of simulations for other dilute aqueous solutions that are used for water calorimetry--pure water, air-saturated water, and H 2 -saturated water. The production of H 2 O 2 was measured for these aqueous solutions and compared to simulations. The results indicate that water saturated with a gas mixture containing an amount-of-substance of H 2 of 50% and of O 2 of 50% is suitable for water calorimetry if the water is stirred and is in contact with a gas space of similar volume. H 2 -saturated water does not require a gas space but O 2 contamination must be guarded against. The lack of a scavenger for OH radicals in pure water means that, depending on the water purity, some pure water might require a large priming dose to remove reactive impurities. The experimental and theoretical problems associated with air-saturated water and O 2 -saturated water in water calorimeters are discussed

  9. Development of Quartz Fiber Calorimetry

    CERN Multimedia

    2002-01-01

    % RD40 \\\\ \\\\ Very Forward Calorimeters (VFCs) in LHC detectors should cover the pseudorapidity range from $\\eta$~=~2.5 to at least $\\eta$~=~5 in order to compute missing transverse energy and for jet tagging. Operation at such high rapidity requires the use of a calorimetry technique that is very radiation resistant, fast and insensitive to radioactivity (especially to neutrons). This can be accomplished through the Quartz-Calorimeter~(Q-Cal) concept of embedding silica core fibers, that resist to the Gigarad radiation level, into an absorber. In this calorimeter the shower particles produce light through the Cherenkov effect generating a signal less than 10~ns in duration. Unique to this new technology the visible energy of hadronic showers has a transverse dimension nearly an order of magnitude smaller than that in conventional calorimeters, enabling precise spatial resolution, sharper isolation cuts and better jet recognition against the minimum bias events background. Last but not least, most radioactive ...

  10. Tritium inventory measurements using calorimetry

    International Nuclear Information System (INIS)

    Kapulla, H.; Kraemer, R.; Heine, R.

    1992-01-01

    In the past calorimetry has been developed as a powerful tool in radiometrology. Calorimetric methods have been applied for the determination of activities, half lives and mean energies released during the disintegration of radioactive isotopes. The fundamental factors and relations which determine the power output of radioactive samples are presented and some basic calorimeter principles are discussed in this paper. At the Kernforschungszentrum Karlsruhe (KfK) a family of 3 calorimeters has been developed to measure the energy release from radiative waste products arising from reprocessing operations. With these calorimeters, radiative samples with sizes from a few cm 3 to 2 ·10 5 cm 3 and heat ratings ranging from a few nW to kW can be measured. After modifications of tits inner part the most sensitive calorimeter among the three calorimeters mentioned above would be best suited for measuring the tritium inventory in T-getters of the Amersham-type

  11. Current status of tritium calorimetry at TLK

    Energy Technology Data Exchange (ETDEWEB)

    Buekki-Deme, A.; Alecu, C.G.; Kloppe, B.; Bornschein, B. [Institute of Technical Physics, Tritium Laboratory Karsruhe - TLK, Karlsruhe Institute of Technology - KIT, Karlsruhe (Germany)

    2015-03-15

    Inside a tritium facility, calorimetry is an important analytical method as it is the only reference method for accountancy (it is based on the measurement of the heat generated by the radioactive decay). Presently, at Tritium Laboratory Karlsruhe (TLK), 4 calorimeters are in operation, one of isothermal type and three of inertial guidance control type (IGC). The volume of the calorimeters varies between 0.5 and 20.6 liters. About two years ago we started an extensive work to improve our calorimeters with regard to reliability and precision. We were forced to upgrade 3 of our 4 calorimeters due to the outdated interfaces and software. This work involved creating new LabView programs driving the devices, re-tuning control loops and replacing obsolete hardware components. In this paper we give a review on the current performance of our calorimeters, comparing it to recently available devices from the market and in the literature. We also show some ideas for a next generation calorimeter based on experiences with our IGC calorimeters and other devices reported in the literature. (authors)

  12. Current status of tritium calorimetry at TLK

    International Nuclear Information System (INIS)

    Buekki-Deme, A.; Alecu, C.G.; Kloppe, B.; Bornschein, B.

    2015-01-01

    Inside a tritium facility, calorimetry is an important analytical method as it is the only reference method for accountancy (it is based on the measurement of the heat generated by the radioactive decay). Presently, at Tritium Laboratory Karlsruhe (TLK), 4 calorimeters are in operation, one of isothermal type and three of inertial guidance control type (IGC). The volume of the calorimeters varies between 0.5 and 20.6 liters. About two years ago we started an extensive work to improve our calorimeters with regard to reliability and precision. We were forced to upgrade 3 of our 4 calorimeters due to the outdated interfaces and software. This work involved creating new LabView programs driving the devices, re-tuning control loops and replacing obsolete hardware components. In this paper we give a review on the current performance of our calorimeters, comparing it to recently available devices from the market and in the literature. We also show some ideas for a next generation calorimeter based on experiences with our IGC calorimeters and other devices reported in the literature. (authors)

  13. Ultra-Fast Hadronic Calorimetry

    Energy Technology Data Exchange (ETDEWEB)

    Denisov, Dmitri [Fermilab; Lukić, Strahinja [VINCA Inst. Nucl. Sci., Belgrade; Mokhov, Nikolai [Fermilab; Striganov, Sergei [Fermilab; Ujić, Predrag [VINCA Inst. Nucl. Sci., Belgrade

    2017-12-18

    Calorimeters for particle physics experiments with integration time of a few ns will substantially improve the capability of the experiment to resolve event pileup and to reject backgrounds. In this paper time development of hadronic showers induced by 30 and 60 GeV positive pions and 120 GeV protons is studied using Monte Carlo simulation and beam tests with a prototype of a sampling steel-scintillator hadronic calorimeter. In the beam tests, scintillator signals induced by hadronic showers in steel are sampled with a period of 0.2 ns and precisely time-aligned in order to study the average signal waveform at various locations w.r.t. the beam particle impact. Simulations of the same setup are performed using the MARS15 code. Both simulation and test beam results suggest that energy deposition in steel calorimeters develop over a time shorter than 3 ns providing opportunity for ultra-fast calorimetry. Simulation results for an "ideal" calorimeter consisting exclusively of bulk tungsten or copper are presented to establish the lower limit of the signal integration window.

  14. WA80 BGO calorimetry electronics

    International Nuclear Information System (INIS)

    Wintenberg, A.L.; Britton, C.L. Jr.; Ericson, M.N.; Maples, R.A.; Young, G.R.; Awes, T.C.

    1991-01-01

    This paper describes instrumentation designed for BGO scintillator-based calorimetry of particles covering a very wide range of energies (from less than 50 MeV to 50 GeV). The instrumentation was designed to have a measurement accuracy of 0.1% over as much of the energy range as possible so the energy resolution of BGO would be the limiting factor. Two 1.5-cm 2 photodiodes were used per 2.5 cm x 2.5 cm x 25 cm BGO crystal. Both a charge-sensitive preamplifier and a pulse processor were developed specifically for the needs of the WA80 experiment. The preamplifier was designed for high detector capacitance (100 to 700 pF), low integral and differential non-linearity and low power consumption (200 mW). The pulse processor is a time-invariant shaping amplifier with integral peak-detect-and-hold and automatic gain selection circuits. The amplifier use quasi-triangular shaping with 4 μs peaking time, and the hold circuit is gated with a fast first level trigger. The system has more than 20 bits of effective resolution when used with an external 12-bit ADC. Results from beam tests at CERN are presented. 6 refs., 5 figs., 1 tab

  15. Differential scanning calorimetry of bacteria.

    Science.gov (United States)

    Miles, C A; Mackey, B M; Parsons, S E

    1986-04-01

    Thermograms obtained by differential scanning calorimetry of a range of bacteria of different heat resistances were compared. Equations were derived to calculate the rate at which the numbers of viable organisms in a calorimeter decline as the temperature is raised at a constant rate. Vegetative bacteria scanned at 10 degrees C min-1 showed multi-peaked thermograms with four major peaks (denoted m, n, p and q) occurring in the regions 68-73, 77-84, 89-99 and 105-110 degrees C respectively. Exceptions were that peak m (the largest peak) occurred at 79-82 degrees C in Bacillus stearothermophilus and an additional peak, r, was detected in Escherichia coli at 119 degrees C. At temperatures below the main peak m there were major differences in thermograms between species. There was a direct relationship between the onset of thermal denaturation and the thermoresistance of different organisms. Heat-sensitive organisms displayed thermogram features which were absent in the more heat-resistant types. When samples were cooled to 5 degrees C and re-heated, a small endothermic peak, pr, was observed at the same temperature as p. Peaks p and pr were identified as the melting endotherms of DNA. In all vegetative organisms examined, maximum death rates, computed from published D and z values, occurred at temperatures above the onset of thermal denaturation, i.e. cell death and irreversible denaturation of cell components occurred within the same temperature range.

  16. Liquid ionization calorimetry: review and preview

    International Nuclear Information System (INIS)

    Fabjan, C.W.

    1995-01-01

    The experimental requirements at existing and planned accelerators, and new facilities for underground or space-borne experimentation have stimulated a wide-ranging R and D programme in liquid ionization calorimetry. Precision sampling calorimetry is approaching ''crystal'' energy resolution whilst their rate capabilities will be able to cope with the highest LHC luminosities. (Quasi)-homogeneous noble-liquid calorimeters are under construction or in the planning stage to address some of the most fundamental physics questions. (orig.)

  17. Addressing the impact of environmental uncertainty in plankton model calibration with a dedicated software system: the Marine Model Optimization Testbed (MarMOT 1.1 alpha)

    Science.gov (United States)

    Hemmings, J. C. P.; Challenor, P. G.

    2012-04-01

    A wide variety of different plankton system models have been coupled with ocean circulation models, with the aim of understanding and predicting aspects of environmental change. However, an ability to make reliable inferences about real-world processes from the model behaviour demands a quantitative understanding of model error that remains elusive. Assessment of coupled model output is inhibited by relatively limited observing system coverage of biogeochemical components. Any direct assessment of the plankton model is further inhibited by uncertainty in the physical state. Furthermore, comparative evaluation of plankton models on the basis of their design is inhibited by the sensitivity of their dynamics to many adjustable parameters. Parameter uncertainty has been widely addressed by calibrating models at data-rich ocean sites. However, relatively little attention has been given to quantifying uncertainty in the physical fields required by the plankton models at these sites, and tendencies in the biogeochemical properties due to the effects of horizontal processes are often neglected. Here we use model twin experiments, in which synthetic data are assimilated to estimate a system's known "true" parameters, to investigate the impact of error in a plankton model's environmental input data. The experiments are supported by a new software tool, the Marine Model Optimization Testbed, designed for rigorous analysis of plankton models in a multi-site 1-D framework. Simulated errors are derived from statistical characterizations of the mixed layer depth, the horizontal flux divergence tendencies of the biogeochemical tracers and the initial state. Plausible patterns of uncertainty in these data are shown to produce strong temporal and spatial variability in the expected simulation error variance over an annual cycle, indicating variation in the significance attributable to individual model-data differences. An inverse scheme using ensemble-based estimates of the

  18. BES online calibration system

    International Nuclear Information System (INIS)

    Zhang Bingyun; Li Xiaonan; Zhu Kejun; Zhang Jiawen; Gong Mingyu

    2003-01-01

    We constructed BES (Beijing Spectrometer) online calibration system to ensure the coherence of readout electronic channels due to huge data volume in high energy physics experiment. This paper describes the structure of hardware and software, and its characteristic and function

  19. Calorimetry exchange program annual data report for 1992

    International Nuclear Information System (INIS)

    Barnett, T.M.

    1992-01-01

    The goals of the Calorimetry Sample Exchange Program are: discuss measurement differences; review and improve analytical measurements and methods; discuss new measurement capabilities; provide data to DOE on measurement capabilities to evaluate shipper-receiver differences; provide characterized or standard materials as necessary for exchange participants; and provide a measurement control program for plutonium analysis. A sample of PuO 2 powder is available at each participating site for NDA measurement, including either or both calorimetry and high-resolution gamma-ray spectroscopy, the elements which are typically combined to provide a calorimetric assay of plutonium. The facilities measure the sample as frequently and to the level of precision which they desire, and then submit the data to the Exchange for analysis. The data report includes summary tables for each measurement and charts showing the performance of each laboratory. Comparisons are made to the accepted values for the exchange sample and to data previously reported by that laboratory. This information is presented, in the form of quarterly and annual reports, intended for use by Exchange participants in measurement control programs, or to indicate when bias corrections may be appropriate. No attempt, however, has been made to standardize methods or frequency of data collection, calibration, or operating procedures. Direct comparisons between laboratories may, therefore, be misleading since data have not been collected to the same precision or for the same time periods. A meeting of the participants of the Calorimetry Exchange is held annually at EG ampersand G Mound Applied Technologies. The purposes of this meeting are to discuss measurement differences, problems, and new measurement capabilities, and to determine the additional activities needed to fulfill the goals of the Exchange. This document provides data for 1992

  20. Calorimetry energy measurement in particle physics

    CERN Document Server

    Wigmans, Richard

    2017-01-01

    Particle physics is the science that pursues the age-old quest for the innermost structure of matter and the fundamental interactions between its constituents. Modern experiments in this field rely increasingly on calorimetry, a detection technique in which the particles of interest are absorbed in the detector. Calorimeters are very intricate instruments. Their performance characteristics depend on subtle, sometimes counter-intuitive design details. This book, written by one of the world's foremost experts, is the first comprehensive text on this topic. It provides a fundamental and systematic introduction to calorimetry. It describes the state of the art in terms of both the fundamental understanding of calorimetric particle detection, and the actual detectors that have been or are being built and operated in experiments. The last chapter discusses landmark scientific discoveries in which calorimetry has played an important role. This book summarizes and puts into perspective the work described in some 900...

  1. Study of asphaltene precipitation by Calorimetry

    DEFF Research Database (Denmark)

    Verdier, Sylvain Charles Roland; Plantier, Frédéric; Bessières, David

    2007-01-01

    Can calorimetry bring new input to the Current understanding of asphaltene precipitation? In this work, two types of precipitation were studied by means of calorimetry: addition of n-heptane into asphaltene solutions and temperature/pressure variations on a recombined live oil. The first series...... of experiments showed that weak forces determine precipitation. Indeed, isothermal titration calorimetry could not detect any clear signal although this technique can detect low-energy transitions such as liquid-liquid equilibrium and rnicellization. The second series of tests proved that precipitation caused...... by T and P variations is exothermic for this system. Furthermore, the temperature-induced precipitation is accompanied by an increase in the apparent thermal expansivity. Therefore, it seems that these two phase transitions exhibit different calorimetric behaviours and they may not be as similar...

  2. Differential scanning calorimetry (DSC) of semicrystalline polymers.

    Science.gov (United States)

    Schick, C

    2009-11-01

    Differential scanning calorimetry (DSC) is an effective analytical tool to characterize the physical properties of a polymer. DSC enables determination of melting, crystallization, and mesomorphic transition temperatures, and the corresponding enthalpy and entropy changes, and characterization of glass transition and other effects that show either changes in heat capacity or a latent heat. Calorimetry takes a special place among other methods. In addition to its simplicity and universality, the energy characteristics (heat capacity C(P) and its integral over temperature T--enthalpy H), measured via calorimetry, have a clear physical meaning even though sometimes interpretation may be difficult. With introduction of differential scanning calorimeters (DSC) in the early 1960s calorimetry became a standard tool in polymer science. The advantage of DSC compared with other calorimetric techniques lies in the broad dynamic range regarding heating and cooling rates, including isothermal and temperature-modulated operation. Today 12 orders of magnitude in scanning rate can be covered by combining different types of DSCs. Rates as low as 1 microK s(-1) are possible and at the other extreme heating and cooling at 1 MK s(-1) and higher is possible. The broad dynamic range is especially of interest for semicrystalline polymers because they are commonly far from equilibrium and phase transitions are strongly time (rate) dependent. Nevertheless, there are still several unsolved problems regarding calorimetry of polymers. I try to address a few of these, for example determination of baseline heat capacity, which is related to the problem of crystallinity determination by DSC, or the occurrence of multiple melting peaks. Possible solutions by using advanced calorimetric techniques, for example fast scanning and high frequency AC (temperature-modulated) calorimetry are discussed.

  3. Calorimetry and thermal methods in catalysis

    CERN Document Server

    Auroux, Aline

    2013-01-01

    The book is about calorimetry and thermal analysis methods, alone or linked to other techniques, as applied to the characterization of catalysts, supports and adsorbents, and to the study of catalytic reactions in various domains: air and wastewater treatment, clean and renewable energies, refining of hydrocarbons, green chemistry, hydrogen production and storage. The book is intended to fill the gap between the basic thermodynamic and kinetics concepts acquired by students during their academic formation, and the use of experimental techniques such as thermal analysis and calorimetry to answ

  4. Prospects for and tests of hadron calorimetry with silicon

    International Nuclear Information System (INIS)

    Brau, J.E.; Gabriel, T.A.; Rancoita, P.G.

    1989-03-01

    Hadron calorimetry with silicon may provide crucial capabilities in experiments at the high luminosity, high energy colliders of the future, particularly due to silicon's fast intrinsic speed and absolute calibration. The important underlying processes of our understanding of hadron calorimeters are reviewed to set the framework for the presentation of recent calculations of the expected performance of silicon detector based hadron calorimeters. Such devices employing uranium are expected to achieve the compensation condition (that is, the ratio of the most probable electron signal to hadron signal (e/h) is ∼1.0) based on the understanding that has been derived from the uranium-liquid argon and uranium-plastic scintillator systems. In fact, even lead-silicon calorimeters are found to achieve the attractive value for the e/h ratio of 1.16 at 10 GeV. An experimental test of these predictions is underway at CERN by the SICAPO Collaboration. 64 refs., 19 figs

  5. New crystals for dual-readout calorimetry

    Czech Academy of Sciences Publication Activity Database

    Akchurin, N.; Bedeschi, F.; Cardini, A.; Carosi, R.; Ciapetti, G.; Ferrari, R.; Franchino, S.; Fraternali, M.; Gaudio, G.; Hauptman, J.; Incagli, M.; Korzhik, M.; Lacava, F.; La Rotonda, L.; Livan, M.; Meoni, E.; Nikl, Martin; Pinci, D.; Policicchio, A.; Popescu, S.; Scuri, F.; Sill, A.; Vandelli, W.; Vedda, A.; Venturelli, T.; Voena, C.; Volobouev, I.; Wigmans, R.

    2009-01-01

    Roč. 604, č. 3 (2009), s. 512-526 ISSN 0168-9002 Institutional research plan: CEZ:AV0Z10100521 Keywords : calorimetry * Cherenkov light * high-Z scintillating crystals Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 1.317, year: 2009

  6. Isothermal Titration Calorimetry in the Student Laboratory

    Science.gov (United States)

    Wadso, Lars; Li, Yujing; Li, Xi

    2011-01-01

    Isothermal titration calorimetry (ITC) is the measurement of the heat produced by the stepwise addition of one substance to another. It is a common experimental technique, for example, in pharmaceutical science, to measure equilibrium constants and reaction enthalpies. We describe a stirring device and an injection pump that can be used with a…

  7. Liquid argon calorimetry for the SSC

    International Nuclear Information System (INIS)

    Gordon, H.A.

    1990-01-01

    Liquid argon calorimetry is a mature technique. However, adapting it to the challenging environment of the SSC requires a large amount of R ampersand D. The advantages of the liquid argon approach are summarized and the issues being addressed by the R ampersand D program are described. 18 refs

  8. Monte Carlo studies of uranium calorimetry

    International Nuclear Information System (INIS)

    Brau, J.; Hargis, H.J.; Gabriel, T.A.; Bishop, B.L.

    1985-01-01

    Detailed Monte Carlo calculations of uranium calorimetry are presented which reveal a significant difference in the responses of liquid argon and plastic scintillator in uranium calorimeters. Due to saturation effects, neutrons from the uranium are found to contribute only weakly to the liquid argon signal. Electromagnetic sampling inefficiencies are significant and contribute substantially to compensation in both systems. 17 references

  9. Software framework and jet energy scale calibration in the ATLAS experiment; Environnement logiciel et etalonnage de l'echelle en energie des jets dans l'experience ATLAS

    Energy Technology Data Exchange (ETDEWEB)

    Binet, Sebastien [Laboratoire de Physique Corpusculaire, Universite Blaise Pascal - CNRS/IN2P3, 63000 Aubiere Cedex (France)

    2006-07-01

    This thesis presents the work achieved to instrument the ATLAS software framework, ATHENA, with a library of tools and utensils for the physics analysis as well as the extraction of the jet energy scale using physics events (in-situ calibration). The software part presents the various components of the ATHENA framework which handles the simulated and reconstructed data flow as well as the different stages of this process, before and during the data taking. The building of a library of tools easing the reconstruction of physics objects, their association with Monte-Carlo particles and their API is then explained. The need for common language and collaboration-wide utensils is emphasised as it allows to share the workload of validating these tools and to get reproducible physics results. The analysis part deals with the implementation of a light jet energy scale calibration algorithm within the C++ framework. This calibration algorithm makes use of W bosons decaying into light jets within semileptonic t t-bar events. From the processing of fast and full simulation data with this algorithm, it seems possible to reach a percent level knowledge of the light jet energy scale. Finally, the feasibility study of the b-jet energy scale calibration using {gamma}Z{sup 0} {yields} {gamma}b b-bar events is presented. It is shown that a purely sequential approach is not sufficient to extract the signal nor to collect a sufficient amount of Z{sup 0} to calibrate the b-jet energy scale. (author)

  10. Analyzing Protein Denaturation using Fast Differential Scanning Calorimetry

    NARCIS (Netherlands)

    Splinter, R.; Van Herwaarden, A.W.; Iervolino, E.; Vanden Poel, G.; Istrate, D.; Sarro, P.M.

    2012-01-01

    This paper investigates the possibility to measure protein denaturation with Fast Differential Scanning Calorimetry (FDSC). Cancer can be diagnosed by measuring protein denaturation in blood plasma using Differential Scanning Calorimetry (DSC). FDSC can reduce diagnosis time from hours to minutes,

  11. Calorimetry and thermodynamics of living systems

    International Nuclear Information System (INIS)

    Lamprecht, Ingolf

    2003-01-01

    Calorimetry of living systems and classical thermodynamics developed in parallel, from Lavoisier's early ice calorimeter experiments on guinea pigs, followed by Dubrunfaut's macrocalorimetric research of fermentation processes and Atwater-Rosa's whole-body calorimetry on humans and domestic animals, to the introduction of the famous Tian-Calvet instrument that found entrance into so many different fields of biology. In this work, six examples of living-system calorimetry and thermodynamics are presented. These are: (i) glycolytic oscillations far off the thermodynamic equilibrium; (ii) growth and energy balances in fermenting and respiring yeast cultures; (iii) direct and indirect calorimetric monitoring of electrically stimulated reptile metabolism; (iv) biologic and climatic factors influencing the temperature constancy and distribution in the mound of a wood ant colony as an example of a complex ecological system; (v) energetic considerations on the clustering of European honeybees in winter as a means to save energy and stored food as well as for their Japanese counterparts in defending against hornet predators; and (vi) energetic and evolutionary aspects of the mass specific entropy production rate, the so-called bound dissipation or psiu-function. The examples presented here are just a very personal selection of living systems from a broad spectrum at all levels of complexity. Common for all of them is that they were investigated calorimetrically on the background of classical and irreversible thermodynamics

  12. The importance of calorimetry for highly-boosted jet substructure

    Energy Technology Data Exchange (ETDEWEB)

    Coleman, Evan [Brown U.; Freytsis, Marat [Oregon U.; Hinzmann, Andreas [Hamburg U.; Narain, Meenakshi [Brown U.; Thaler, Jesse [MIT, Cambridge, CTP; Tran, Nhan [Fermilab; Vernieri, Caterina [Fermilab

    2017-09-25

    Jet substructure techniques are playing an essential role in exploring the TeV scale at the Large Hadron Collider (LHC), since they facilitate the efficient reconstruction and identification of highly-boosted objects. Both for the LHC and for future colliders, there is a growing interest in using jet substructure methods based only on charged-particle information. The reason is that silicon-based tracking detectors offer excellent granularity and precise vertexing, which can improve the angular resolution on highly-collimated jets and mitigate the impact of pileup. In this paper, we assess how much jet substructure performance degrades by using track-only information, and we demonstrate physics contexts in which calorimetry is most beneficial. Specifically, we consider five different hadronic final states - W bosons, Z bosons, top quarks, light quarks, gluons - and test the pairwise discrimination power with a multi-variate combination of substructure observables. In the idealized case of perfect reconstruction, we quantify the loss in discrimination performance when using just charged particles compared to using all detected particles. We also consider the intermediate case of using charged particles plus photons, which provides valuable information about neutral pions. In the more realistic case of a segmented calorimeter, we assess the potential performance gains from improving calorimeter granularity and resolution, comparing a CMS-like detector to more ambitious future detector concepts. Broadly speaking, we find large performance gains from neutral-particle information and from improved calorimetry in cases where jet mass resolution drives the discrimination power, whereas the gains are more modest if an absolute mass scale calibration is not required.

  13. Advanced ion beam calorimetry for the test facility ELISE

    International Nuclear Information System (INIS)

    Nocentini, R.; Fantz, U.; Franzen, P.; Fröschle, M.; Heinemann, B.; Riedl, R.; Ruf, B.; Wünderlich, D.; Bonomo, F.; Pimazzoni, A.; Pasqualotto, R.

    2015-01-01

    The negative ion source test facility ELISE (Extraction from a Large Ion Source Experiment) is in operation since beginning of 2013 at the Max-Planck-Institut für Plasmaphysik (IPP) in Garching bei München. The large radio frequency driven ion source of ELISE is about 1×1 m 2 in size (1/2 the ITER source) and can produce a plasma for up to 1 h. Negative ions can be extracted and accelerated by an ITER-like extraction system made of 3 grids with an area of 0.1 m 2 , for 10 s every 3 minutes. A total accelerating voltage of up to 60 kV is available, i.e. a maximum ion beam power of about 1.2 MW can be produced. ELISE is equipped with several beam diagnostic tools for the evaluation of the beam characteristics. In order to evaluate the beam properties with a high level of detail, a sophisticated diagnostic calorimeter has been installed in the test facility at the end of 2013, starting operation in January 2014. The diagnostic calorimeter is split into 4 copper plates with separate water calorimetry for each of the plates. Each calorimeter plate is made of 15×15 copper blocks, which act as many separate inertial calorimeters and are attached to a copper plate with an embedded cooling circuit. The block geometry and the connection with the cooling plate are optimized to accurately measure the time-averaged power of the 10 s ion beam. The surface of the blocks is covered with a black coating that allows infrared (IR) thermography which provides a 2D profile of the beam power density. In order to calibrate the IR thermography, 48 thermocouples are installed in as many blocks, arranged in two vertical and two horizontal rows. The paper describes the beam calorimetry in ELISE, including the methods used for the IR thermography, the water calorimetry and the analytical methods for beam profile evaluation. It is shown how the maximum beam inhomogeneity amounts to 13% in average. The beam divergence derived by IR thermography ranges between 1° and 4° and

  14. Calibration strategies for the Cherenkov Telescope Array

    NARCIS (Netherlands)

    Gaug, M.; Berge, D.; Daniel, M.; Doro, M.; Förster, A.; Hofmann, W.; Maccarone, M.C.; Parsons, D.; de los Reyes Lopez, R.; van Eldik, C.

    2014-01-01

    The Central Calibration Facilities workpackage of the Cherenkov Telescope Array (CTA) observatory for very high energy gamma ray astronomy defines the overall calibration strategy of the array, develops dedicated hardware and software for the overall array calibration and coordinates the calibration

  15. Fabrication of 12% 240Pu calorimetry standards

    International Nuclear Information System (INIS)

    Long, S.M.; Hildner, S.; Gutierrez, D.; Mills, C.; Garcia, W.; Gurule, C.

    1995-01-01

    Throughout the DOE complex, laboratories are performing calorimetric assays on items containing high burnup plutonium. These materials contain higher isotopic range and higher wattages than materials previously encountered in vault holdings. Currently, measurement control standards have been limited to utilizing 6% 240 Pu standards. The lower isotopic and wattage value standards do not complement the measurement of the higher burnup material. Participants of the Calorimetry Exchange (CALEX) Program have identified the need for new calorimetric assay standards with a higher wattage and isotopic range. This paper describes the fabrication and verification measurements of the new CALEX standard containing 12% 240 Pu oxide with a wattage of about 6 to 8 watts

  16. Isothermal calorimetry of enzymatic biodiesel reaction

    DEFF Research Database (Denmark)

    Fjerbæk Søtoft, Lene; Westh, Peter; Christensen, Knud Villy

    2010-01-01

      Isothermal calorimetry ITC has been used to investigate enzymatic biodiesel production. The transesterification of rapeseed oil with methanol and ethanol was catalyzed by the immobilized lipase Novozym 435 at 40°C. The ITC-experiments clearly demonstrate the possibilities of investigating complex...... and composition change in the system, the heat of reaction at 40°C for the two systems has been determined to -9.8 ± 0.9 kJ/mole biodiesel formed from rapeseed oil and methanol, and - 9.3 ± 0.7 kJ/mole when rapeseed oil and ethanol is used....

  17. The GERDA calibration system

    Energy Technology Data Exchange (ETDEWEB)

    Baudis, Laura; Froborg, Francis; Tarka, Michael; Bruch, Tobias; Ferella, Alfredo [Physik-Institut, Universitaet Zuerich (Switzerland); Collaboration: GERDA-Collaboration

    2012-07-01

    A system with three identical custom made units is used for the energy calibration of the GERDA Ge diodes. To perform a calibration the {sup 228}Th sources are lowered from the parking positions at the top of the cryostat. Their positions are measured by two independent modules. One, the incremental encoder, counts the holes in the perforated steel band holding the sources, the other measures the drive shaft's angular position even if not powered. The system can be controlled remotely by a Labview program. The calibration data is analyzed by an iterative calibration algorithm determining the calibration functions for different energy reconstruction algorithms and the resolution of several peaks in the {sup 228}Th spectrum is determined. A Monte Carlo simulation using the GERDA simulation software MAGE has been performed to determine the background induced by the sources in the parking positions.

  18. Development of Resistive Micromegas for Sampling Calorimetry

    Science.gov (United States)

    Geralis, T.; Fanourakis, G.; Kalamaris, A.; Nikas, D.; Psallidas, A.; Chefdeville, M.; Karyotakis, I.; Koletsou, I.; Titov, M.

    2018-02-01

    Resistive micromegas is proposed as an active element for sampling calorimetry. Future linear collider experiments or the HL-LHC experiments can profit from those developments for Particle Flow Calorimetry. Micromegas possesses remarkable properties concerning gain stability, reduced ion feedback, response linearity, adaptable sensitive element granularity, fast response and high rate capability. Recent developments on Micromegas with a protective resistive layer present excellent results, resolving the problem of discharges caused by local high charge deposition, thanks to its RC-slowed charge evacuation. Higher resistivity though, may cause loss of the response linearity at high rates. We have scanned a wide range of resistivities and performed laboratory tests with X-rays that demonstrate excellent response linearity up to rates of (a few) times 10MHz/cm2, with simultaneous mitigation of discharges. Beam test studies at SPS/CERN with hadrons have also shown a remarkable stability of the resistive Micromegas and low currents for rates up to 15MHz/cm2. We present results from the aforementioned studies confronted with MC simulation

  19. Radiation damage study for silicon calorimetry: Summary of first year's activity

    International Nuclear Information System (INIS)

    Russ, J.S.

    1988-01-01

    In the first contract year of this activity at Carnegie-Mellon we have had two major objectives. These were to devise and test a non-intrusive means to measure the energy and spatial profiles of the neutrons generated in a hadronic cascade at high energy; and to study the calibration systematics of silicon diode detectors as a prelude to their evaluation for SSC calorimetry. These objectives have been carried out, as are described in this paper. In addition we have recoded the ORNL detector simulation program HETC to operate on a VAX and are working on the conversion of the low energy neutron transport program MORSE. These programs are used heavily at Oak Ridge (Gabriel and coworkers) for cascade studies. For silicon calorimetry one wants to have more control over the energy deposition routines, especially in MORSE. Unfortunately, MORSE is heavily-laden with machine code, and its conversion is going slowly. 11 refs., 5 figs

  20. Applying fast calorimetry on a spent nuclear fuel calorimeter

    Energy Technology Data Exchange (ETDEWEB)

    Liljenfeldt, Henrik [Swedish Nuclear Fuel and Waste Management (Sweden); Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Uppsala Univ. (Sweden)

    2015-04-15

    Recently at Los Alamos National Laboratory, sophisticated prediction algorithms have been considered for the use of calorimetry for treaty verification. These algorithms aim to predict the equilibrium temperature based on early data and therefore be able to shorten the measurement time while maintaining good accuracy. The algorithms have been implemented in MATLAB and applied on existing equilibrium measurements from a spent nuclear fuel calorimeter located at the Swedish nuclear fuel interim storage facility. The results show significant improvements in measurement time in the order of 15 to 50 compared to equilibrium measurements, but cannot predict the heat accurately in less time than the currently used temperature increase method can. This Is both due to uncertainties in the calibration of the method as well as identified design features of the calorimeter that limits the usefulness of equilibrium type measurements. The conclusions of these findings are discussed, and suggestions of both improvements of the current calorimeter as well as what to keep in mind in a new design are given.

  1. Prospects for and tests of hadron calorimetry with silicon

    Energy Technology Data Exchange (ETDEWEB)

    Brau, James E. [Univ. of Oregon, OR (United States). Dept. of Physics; Gabriel, Tony A. [Oak Ridge National Lab., TN (United States); Rancoita, P. G. [INFN, Milan (Italy)

    1989-03-01

    Hadron calorimetry with silicon may provide crucial capabilities in experiments at the high luminosity, high energy colliders of the future, particularly due to silicon's fast intrinsic speed and absolute calibration. The important underlying processes of our understanding of hadron calorimeters are reviewed to set the framework for the presentation of recent calculations of the expected performance of silicon detector based hadron calorimeters. Such devices employing uranium are expected to achieve the compensation condition (that is, the ratio of the most probable electron signal to hadron signal (e/h) is approx.1.0) based on the understanding that has been derived from the uranium-liquid argon and uranium-plastic scintillator systems. In fact, even lead-silicon calorimeters are found to achieve the attractive value for the e/h ratio of 1.16 at 10 GeV. An experimental test of these predictions is underway at CERN by the SICAPO Collaboration. 64 refs., 19 figs.

  2. Characterization of pitches by differential scanning calorimetry

    Energy Technology Data Exchange (ETDEWEB)

    Ehrburger, P.; Martin, C.; Lahaye, J.; Saint-Romain, J.L.; Couderc, P.

    1988-12-01

    Pitch materials have generally a very complex composition with molecular mass ranging from a few hundred to several thousands units. In order to characterize these materials their properties related to the glassy transformation, in particular to enthalpy relaxation, have been investigated. Solvent soluble fractions have been characterized by differential scanning calorimetry (DSC). As with polymeric materials, enthalpy relaxation can provide information about pitches and the interactions occurring between the different types of molecules present in the pitch: mean molecular size, structural factor, molecular-size distribution. The determination of glass transition properties provides a useful means for the characterization of pitch and of their solvent extracts. It also permits insight into the complex reactions which occur when pitch materials are heat-treated. 7 refs., 2 figs., 3 tabs.

  3. Synergies between electromagnetic calorimetry and PET

    International Nuclear Information System (INIS)

    Moses, William W.

    2002-01-01

    The instrumentation used for the nuclear medical imaging technique of Positron Emission Tomography (PET) shares many features with the instrumentation used for electromagnetic calorimetry. Both fields can certainly benefit from technical advances in many common areas, and this paper discusses both the commonalties and the differences between the instrumentation needs for the two fields. The overall aim is to identify where synergistic development opportunities exist. While such opportunities exist in inorganic scintillators, photodetectors, amplification and readout electronics, and high-speed computing, it is important to recognize that while the requirements of the two fields are similar, they are not identical, and so it is unlikely that advances specific to one field can be transferred without modification to the other

  4. Silicon calorimetry for the SSC[ Superconducting Supercollider

    International Nuclear Information System (INIS)

    Bertrand, C.; Borchi, E.; Brau, J.E.

    1989-01-01

    SSC experiments will rely heavily on their calorimeters. Silicon calorimetry, which has been introduced in recent years as a useful technology, has many attractive characteristics which may make it a viable option for consideration. The many attractive properties of silicon detectors are reviewed. The relevant present day applications of large areas of silicon detectors are summarize to illustrate the emerging use. The troublesome issue of radiation damage in a high luminosity environment like the SSC is considered with a summary of much of the recent new measurements which help clarify this situation. A discussion of the electronics and a possible mechanical configuration is presented, followed by a summary of the outstanding R and D issues. 31 refs., 11 figs., 3 tabs

  5. Isothermal calorimetry on enzymatic biodiesel production

    DEFF Research Database (Denmark)

    Fjerbæk, Lene

    2008-01-01

    information about effects taking place when using lipases immobilized on an inert carrier for transesterification of a triglyceride and an alcohol as for biodiesel production. The biodiesel is produced by rapeseed oil and methanol as well as ethanol and a commercial biocatalyst Novozym 435 from Novozymes...... containing a Candida Antarctica B lipase immobilized on an acrylic resin. The reaction investigated is characterized by immiscible liquids (oil, methanol, glycerol and biodiesel) and enzymes imm. on an inert carrier during reaction, which allows several effects to take place that during normal reaction...... conditions can not be elucidated. These effects have been observed with isothermal calorimetry bringing forth new information about the reaction of enzymes catalyzing transesterification. Enzymatic biodiesel production has until now not been investigated with isothermal microcalorimetry, but the results...

  6. CMS Forward Calorimetry R&D

    Energy Technology Data Exchange (ETDEWEB)

    Bilki, Burak [Univ. of Iowa, Iowa City, IA (United States); Argonne National Lab. (ANL), Argonne, IL (United States)

    2013-11-11

    This is a technical scope of work (TSW) between the Fermi National Accelerator Laboratory (Fermilab) and the experimenters of the CMS Forward Calorimetry Taskforce (FCAL group) who have committed to participate in beam tests to be carried out during the 2013-2016 Fermilab Test Beam Facility program. The TSW is intended primarily for the purpose of recording expectations for budget estimates and work allocations for Fermilab, the funding agencies and the participating institutions. It reflects an arrangement that currently is satisfactory to the parties; however, it is recognized and anticipated that changing circumstances of the evolving research program will necessitate revisions. The parties agree to modify this scope of work to reflect such required adjustments. Actual contractual obligations will be set forth in separate documents.

  7. Front-End Electronics in calorimetry: from LHC to ILC

    International Nuclear Information System (INIS)

    De La Taille, Ch.

    2009-09-01

    This report summarizes the electronics developments for liquid argon calorimeter read-out at LHC and the development carried out in the framework of the CALICE collaboration for those of the future linear collider (ILC). It also includes chips designed for multi-anode photomultipliers (MaPMT) used in the OPERA experiment or on ATLAS luminometer, which also find applications in medical imaging. Started in the early 90's, the development for ATLAS calorimetry was extremely challenging in terms of readout speed, radiation tolerance and measurement accuracy. The high speed has required a new approach using current-sensitive preamplifiers instead of charge sensitive ones and the redefinition of noise performance in terms of ENI. The preamplifiers developed at Orsay and the monolithic shapers are described in Chapter 1, including considerations of digital filtering, which was a new technique in our field. Chapter 2 is dedicated to the calibration system, designed and built by Orsay, for which the high performance and accuracy necessitated in-depth studies. The 3. chapter closes the studies for ATLAS with a summary of the detector measurements which had to be carried out on the 200 000 channels in order to understand and model the detector and achieve everywhere the accuracy and uniformity at per-cent level. These developments for ATLAS ended in 2004, although parallel work was also carried out for the NA48 and DO calorimeters which are not detailed here. The next generation of collider will require a new generation of calorimeters, much more granular, referred to as 'imaging calorimetry' with embedded read-out electronics. The ASICs developed for this purpose in the framework of the CALICE collaboration are described in Chapter 4. They integrate all the functionalities of amplification, digitization and read-out making them complex 'System-On-Chip' circuits extremely efficient that find many other applications. A family of 3 chips reads out the Si-W electromagnetic

  8. Calibration uncertainty

    DEFF Research Database (Denmark)

    Heydorn, Kaj; Anglov, Thomas

    2002-01-01

    Methods recommended by the International Standardization Organisation and Eurachem are not satisfactory for the correct estimation of calibration uncertainty. A novel approach is introduced and tested on actual calibration data for the determination of Pb by ICP-AES. The improved calibration...

  9. Hierarchy of individual calibration levels for heart rate and accelerometry to measure physical activity

    DEFF Research Database (Denmark)

    Brage, Søren; Ekelund, Ulf; Brage, Niels

    2007-01-01

    , submaximal step and walk tests with and without calorimetry, and nonexercise calibration using sleeping HR and gender. Reference accelerometry and HR models explained >95% of the between-individual variance in PAI (P

  10. Differential scanning calorimetry techniques: applications in biology and nanoscience.

    Science.gov (United States)

    Gill, Pooria; Moghadam, Tahereh Tohidi; Ranjbar, Bijan

    2010-12-01

    This paper reviews the best-known differential scanning calorimetries (DSCs), such as conventional DSC, microelectromechanical systems-DSC, infrared-heated DSC, modulated-temperature DSC, gas flow-modulated DSC, parallel-nano DSC, pressure perturbation calorimetry, self-reference DSC, and high-performance DSC. Also, we describe here the most extensive applications of DSC in biology and nanoscience.

  11. Differential Scanning Calorimetry Techniques: Applications in Biology and Nanoscience

    OpenAIRE

    Gill, Pooria; Moghadam, Tahereh Tohidi; Ranjbar, Bijan

    2010-01-01

    This paper reviews the best-known differential scanning calorimetries (DSCs), such as conventional DSC, microelectromechanical systems-DSC, infrared-heated DSC, modulated-temperature DSC, gas flow-modulated DSC, parallel-nano DSC, pressure perturbation calorimetry, self-reference DSC, and high-performance DSC. Also, we describe here the most extensive applications of DSC in biology and nanoscience.

  12. Electron beam water calorimetry measurements to obtain beam quality conversion factors.

    Science.gov (United States)

    Muir, Bryan R; Cojocaru, Claudiu D; McEwen, Malcolm R; Ross, Carl K

    2017-10-01

    To provide results of water calorimetry and ion chamber measurements in high-energy electron beams carried out at the National Research Council Canada (NRC). There are three main aspects to this work: (a) investigation of the behavior of ionization chambers in electron beams of different energies with focus on long-term stability, (b) water calorimetry measurements to determine absorbed dose to water in high-energy beams for direct calibration of ion chambers, and (c) using measurements of chamber response relative to reference ion chambers, determination of beam quality conversion factors, k Q , for several ion chamber types. Measurements are made in electron beams with energies between 8 MeV and 22 MeV from the NRC Elekta Precise clinical linear accelerator. Ion chamber measurements are made as a function of depth for cylindrical and plane-parallel ion chambers over a period of five years to investigate the stability of ion chamber response and for indirect calibration. Water calorimetry measurements are made in 18 MeV and 22 MeV beams. An insulated enclosure with fine temperature control is used to maintain a constant temperature (drifts less than 0.1 mK/min) of the calorimeter phantom at 4°C to minimize effects from convection. Two vessels of different designs are used with calibrated thermistor probes to measure radiation induced temperature rise. The vessels are filled with high-purity water and saturated with H 2 or N 2 gas to minimize the effect of radiochemical reactions on the measured temperature rise. A set of secondary standard ion chambers are calibrated directly against the calorimeter. Finally, several other ion chambers are calibrated in the NRC 60 Co reference field and then cross-calibrated against the secondary standard chambers in electron beams to realize k Q factors. The long-term stability of the cylindrical ion chambers in electron beams is better (always <0.15%) than plane-parallel chambers (0.2% to 0.4%). Calorimetry measurements

  13. Calibration factor or calibration coefficient?

    International Nuclear Information System (INIS)

    Meghzifene, A.; Shortt, K.R.

    2002-01-01

    Full text: The IAEA/WHO network of SSDLs was set up in order to establish links between SSDL members and the international measurement system. At the end of 2001, there were 73 network members in 63 Member States. The SSDL network members provide calibration services to end-users at the national or regional level. The results of the calibrations are summarized in a document called calibration report or calibration certificate. The IAEA has been using the term calibration certificate and will continue using the same terminology. The most important information in a calibration certificate is a list of calibration factors and their related uncertainties that apply to the calibrated instrument for the well-defined irradiation and ambient conditions. The IAEA has recently decided to change the term calibration factor to calibration coefficient, to be fully in line with ISO [ISO 31-0], which recommends the use of the term coefficient when it links two quantities A and B (equation 1) that have different dimensions. The term factor should only be used for k when it is used to link the terms A and B that have the same dimensions A=k.B. However, in a typical calibration, an ion chamber is calibrated in terms of a physical quantity such as air kerma, dose to water, ambient dose equivalent, etc. If the chamber is calibrated together with its electrometer, then the calibration refers to the physical quantity to be measured per electrometer unit reading. In this case, the terms referred have different dimensions. The adoption by the Agency of the term coefficient to express the results of calibrations is consistent with the 'International vocabulary of basic and general terms in metrology' prepared jointly by the BIPM, IEC, ISO, OIML and other organizations. The BIPM has changed from factor to coefficient. The authors believe that this is more than just a matter of semantics and recommend that the SSDL network members adopt this change in terminology. (author)

  14. Electromagnetic Calorimeter Calibration with $\\pi^{0}$

    CERN Multimedia

    Puig Navarro, A

    2009-01-01

    Several methods can be used in order to achieve precise calibration of the LHCb Electromagnetic Calorimeter (ECAL) once reasonable cell equalization has been reached. At low transverse energy, the standard calibration procedure is an iterative method based on the fit of the $\\gamma\\gamma$ invariant mass distribution for each cell of the decay $\\pi^{0}\\to\\gamma\\gamma$ with resolved photons. A new technique for generating the combinatorial background of such decays directly from data has been developed. Knowledge of the background could allow an alternative calibration method based on a event by event fit of the same $\\gamma\\gamma$ invariant mass distribution where contributions from groups of cells are considered in a single fit. The background generation procedure and this possible new calibration method are presented in this poster, in addition to an overview of the LHCb Calorimetry system and ECAL calibration techniques.

  15. Calorimetry at the CMD-3 Detector

    CERN Document Server

    Razuvaev, G P; Anisenkov, A V; Aulchenko, V M; Bashtavoy, N S; Epifanov, D A; Epshteyn, L B; Erofeev, A L; Grebenuk, A A; Grigoriev, D N; Kazanin, V F; Kovalenko, O A; Kozyrev, A N; Kuzmenko, A E; Kuzmin, A S; Logashenko, I B; Mikhailov, K Yu; Okhapkin, V S; Ruban, A A; Shebalin, V E; Shwartz, B A; Talyshev, A A; Titov, V M; Yudin, Yu V

    2017-01-01

    The general purpose detector CMD-3 has been collecting data since 2010 in an energy range 0.32–2 GeV at the e+e- collider VEPP-2000 at the Budeker Institute of Nuclear Physics. The detector physics program includes the study of the e+e- annihilation into hadrons. To supply high registration efficiency for neutral particles the CMD-3 has an electromagnetic calorimeter consisted of three subsystems: BGO endcap calorimeter and barrel one with an inner part based on LXe and outer on CsI crystals. The main parameters of calorimeters, cluster reconstruction and calibration procedures with performance results are described.

  16. The CLEO-III Trigger: Calorimetry and tracking

    International Nuclear Information System (INIS)

    Bergfeld, T.J.; Gollin, G.D.; Haney, M.J.

    1996-01-01

    The CLEO-III Trigger provides a trigger decision every 42ns, with a latency of approximately 2.5μs. This paper describes the pipelined signal processing and pattern recognition schemes used by the calorimeter, and the axial and stereo portions of the drift chamber, to provide the information necessary to make these decisions. Field programmable gate arrays are used extensively to provide cluster filtering and location sorting for calorimetry, and path finding for tracking. Analog processing is also employed in the calorimetry to provide additional leverage on the problem. Timing information is extracted from both calorimetry and tracking

  17. Forward calorimetry in the upgraded UA1 experiment

    International Nuclear Information System (INIS)

    Alvarez-Taviel, F.J.; Diez-Hedo, F.; Doncel, P.; Marquina, M.A.; Rodrigo, T.; Bacci, C.; Petrolo, E.; Tusi, A.; Ferrando, A.; Givernaud, A.; Rubbia, C.; Vuillemin, V.

    1989-01-01

    The major improvement in the upgraded UA1 calorimetry at the Santi ppS is the general use of ionization chambers filled with tetramethylpentane (TMP) as a detection medium interspersed with uranium plates as absorber. To achieve overall uniformity of detection down to very small angles, an identical solution is proposed for the forward calorimetry. Forward calorimetry is essential for good total and missing energy measurement at high luminosity in view of the increasing rate of multiple collisions. Both designs for forward and very forward calorimeters are presented along with expected resolutions. (orig.)

  18. Continuing Studies on Lead/Scintillating Fibres Calorimetry (LFC)

    CERN Multimedia

    2002-01-01

    Starting from the results obtained in the framework of the LAA Project~2B, we propose a continuation of the R&D on lead/scintillating fibres calorimetry (``spaghetti calorimetry''), including further tests on the old calorimeter prototypes and the construction and testing of new prototypes. The main results we pursue concern the performances of a projective calorimeter built with new, cheaper, techniques and the radiation hardness of the scintillating fibres, the optimization of a preshower detector system is also studied.

  19. Vibration transducer calibration techniques

    Science.gov (United States)

    Brinkley, D. J.

    1980-09-01

    Techniques for the calibration of vibration transducers used in the Aeronautical Quality Assurance Directorate of the British Ministry of Defence are presented. Following a review of the types of measurements necessary in the calibration of vibration transducers, the performance requirements of vibration transducers, which can be used to measure acceleration, velocity or vibration amplitude, are discussed, with particular attention given to the piezoelectric accelerometer. Techniques for the accurate measurement of sinusoidal vibration amplitude in reference-grade transducers are then considered, including the use of a position sensitive photocell and the use of a Michelson laser interferometer. Means of comparing the output of working-grade accelerometers with that of previously calibrated reference-grade devices are then outlined, with attention given to a method employing a capacitance bridge technique and a method to be used at temperatures between -50 and 200 C. Automatic calibration procedures developed to speed up the calibration process are outlined, and future possible extensions of system software are indicated.

  20. Pressures Detector Calibration and Measurement

    CERN Document Server

    AUTHOR|(CDS)2156315

    2016-01-01

    This is report of my first and second projects (of 3) in NA61. I did data taking and analysis in order to do calibration of pressure detectors and verified it. I analyzed the data by ROOT software using the C ++ programming language. The first part of my project was determination of calibration factor of pressure sensors. Based on that result, I examined the relation between pressure drop, gas flow rate of in paper filter and its diameter.

  1. Topics in calorimetry for high energy physics

    International Nuclear Information System (INIS)

    Hollebeek, R.

    1992-01-01

    These lectures focus on a series of topics now of interest or which have been of interest to designes of calorimeters in the past few years. The examples concentrate on calorimeters from DESY because its focus this year is on e-P physics, and on CDF and SDC because they are best known to the author. Calorimeters are, broadly speaking, devices to measure the total energy of particles. In general, no one device will be optimal for all types of particles. The two broadest classes of calorimeters in high energy physics are the electromagnetic calorimeters used primarily for photons and electrons, and the hadronic calorimeters used for most charged mesons and baryons. Most operate by absorbing and thereby measuring a significant amount of the incoming particles energy directly. Some particles may require special devices for their interactions and observation. Modern calorimeters are characterized by energy and position resolution, and cost and size. Calorimeter cost is often a trade-off between performance desired and money available. The optimum cost will require a careful choice of materials, reduction of the overall size of the detector, elimination of labor intensive construction techniques, and careful consideration of the cost of calibration systems. Since at least some of these requirements which optimize cost and resolution are contradictory, the ideal calorimeter in seldom what one ends up building

  2. POLCAL - POLARIMETRIC RADAR CALIBRATION

    Science.gov (United States)

    Vanzyl, J.

    1994-01-01

    Calibration of polarimetric radar systems is a field of research in which great progress has been made over the last few years. POLCAL (Polarimetric Radar Calibration) is a software tool intended to assist in the calibration of Synthetic Aperture Radar (SAR) systems. In particular, POLCAL calibrates Stokes matrix format data produced as the standard product by the NASA/Jet Propulsion Laboratory (JPL) airborne imaging synthetic aperture radar (AIRSAR). POLCAL was designed to be used in conjunction with data collected by the NASA/JPL AIRSAR system. AIRSAR is a multifrequency (6 cm, 24 cm, and 68 cm wavelength), fully polarimetric SAR system which produces 12 x 12 km imagery at 10 m resolution. AIRSTAR was designed as a testbed for NASA's Spaceborne Imaging Radar program. While the images produced after 1991 are thought to be calibrated (phase calibrated, cross-talk removed, channel imbalance removed, and absolutely calibrated), POLCAL can and should still be used to check the accuracy of the calibration and to correct it if necessary. Version 4.0 of POLCAL is an upgrade of POLCAL version 2.0 released to AIRSAR investigators in June, 1990. New options in version 4.0 include automatic absolute calibration of 89/90 data, distributed target analysis, calibration of nearby scenes with calibration parameters from a scene with corner reflectors, altitude or roll angle corrections, and calibration of errors introduced by known topography. Many sources of error can lead to false conclusions about the nature of scatterers on the surface. Errors in the phase relationship between polarization channels result in incorrect synthesis of polarization states. Cross-talk, caused by imperfections in the radar antenna itself, can also lead to error. POLCAL reduces cross-talk and corrects phase calibration without the use of ground calibration equipment. Removing the antenna patterns during SAR processing also forms a very important part of the calibration of SAR data. Errors in the

  3. CEBAF beam viewer imaging software

    International Nuclear Information System (INIS)

    Bowling, B.A.; McDowell, C.

    1993-01-01

    This paper discusses the various software used in the analysis of beam viewer images at CEBAF. This software, developed at CEBAF, includes a three-dimensional viewscreen calibration code which takes into account such factors as multiple camera/viewscreen rotations and perspective imaging, and maintaining a calibration database for each unit. Additional software allows single-button beam spot detection, with determination of beam location, width, and quality, in less than three seconds. Software has also been implemented to assist in the determination of proper chopper RF control parameters from digitized chopper circles, providing excellent results

  4. Thin-film calorimetry. In-situ characterization of materials for lithium-ion batteries

    Energy Technology Data Exchange (ETDEWEB)

    Omelcenko, Alexander; Wulfmeier, Hendrik; Albrecht, Daniel; Fritze, Holger [Clausthal Univ. of Technology, Goslar (Germany). Inst. of Energy Research and Physical Technologies; El Mofid, Wassima; Ivanov, Svetlozar; Bund, Andreas [Ilmenau Univ. of Technology (Germany). Dept. of Electrochemistry

    2017-11-15

    Thin-film calorimetry allows for qualitative and quantitative in-situ analysis of thermodynamic properties of thin films and thin-film systems from room temperature up to 1000 C. It is based on highly sensitive piezoelectric langasite resonators which serve simultaneously as planar temperature sensors and substrates for the films of interest. Generation or consumption of heat during phase transformations of the films cause deviations from the regular course of the resonance frequency. Thermodynamic data such as phase transformation temperatures and enthalpies are extracted from these deviations. Thin-film calorimetry on Sn and Al thin films is performed to prove the concept. The results demonstrate high reproducibility of the measurement approach and are in agreement with literature data obtained by established calorimetric techniques. The calibration of the system is done in different atmospheres by application of defined heat pulses via heating structures. The latter replace the films of interest and simulate phase transformations to provide detailed analysis of the heat transfer mechanisms occurring in the measurement system. Based on this analysis, a data evaluation concept is developed. Application-relevant studies are performed on thin films of the lithium-ion battery materials NMC(A), NCA, LMO, and MoS{sub 2}. Their phase transformation temperatures and enthalpies are evaluated in oxidizing and reducing atmospheres. Furthermore, their thermodynamic stability ranges are presented. Finally, measurements on all-solid-state thin-film batteries during electrochemical cycling are performed. They demonstrate the suitability of the system for in-situ investigations.

  5. Instrumentation calibration

    International Nuclear Information System (INIS)

    Mack, D.A.

    1976-08-01

    Procedures for the calibration of different types of laboratory equipment are described. Provisions for maintaining the integrity of reference and working standards traceable back to a national standard are discussed. Methods of validation and certification methods are included. An appendix lists available publications and services of national standardizing agencies

  6. Automated Attitude Sensor Calibration: Progress and Plans

    Science.gov (United States)

    Sedlak, Joseph; Hashmall, Joseph

    2004-01-01

    This paper describes ongoing work a NASA/Goddard Space Flight Center to improve the quality of spacecraft attitude sensor calibration and reduce costs by automating parts of the calibration process. The new calibration software can autonomously preview data quality over a given time span, select a subset of the data for processing, perform the requested calibration, and output a report. This level of automation is currently being implemented for two specific applications: inertial reference unit (IRU) calibration and sensor alignment calibration. The IRU calibration utility makes use of a sequential version of the Davenport algorithm. This utility has been successfully tested with simulated and actual flight data. The alignment calibration is still in the early testing stage. Both utilities will be incorporated into the institutional attitude ground support system.

  7. Automated Calibration of Dosimeters for Diagnostic Radiology

    International Nuclear Information System (INIS)

    Romero Acosta, A.; Gutierrez Lores, S.

    2015-01-01

    Calibration of dosimeters for diagnostic radiology includes current and charge measurements, which are often repetitive. However, these measurements are usually done using modern electrometers, which are equipped with an RS-232 interface that enables instrument control from a computer. This paper presents an automated system aimed to the measurements for the calibration of dosimeters used in diagnostic radiology. A software application was developed, in order to achieve the acquisition of the electric charge readings, measured values of the monitor chamber, calculation of the calibration coefficient and issue of a calibration certificate. A primary data record file is filled and stored in the computer hard disk. The calibration method used was calibration by substitution. With this system, a better control over the calibration process is achieved and the need for human intervention is reduced. the automated system will be used in the calibration of dosimeters for diagnostic radiology at the Cuban Secondary Standard Dosimetry Laboratory of the Center for Radiation Protection and Hygiene. (Author)

  8. A water flow calorimeter calibration system

    International Nuclear Information System (INIS)

    Ullrich, F.T.

    1983-01-01

    Neutral beam systems are instrumented by several water flow calorimeter systems, and some means is needed to verify the accuracy of such systems and diagnose their failures. This report describes a calibration system for these calorimeters. The calibrator consists of two 24 kilowatt circulation water heaters, with associated controls and instrumentation. The unit can supply power from 0 to 48 kW in five coarse steps and one fine range. Energy is controlled by varying the power and the time of operation of the heaters. The power is measured by means of precision power transducers, and the energy is measured by integrating the power with respect to time. The accuracy of the energy measurement is better than 0.5% when the power supplied is near full scale, and the energy resolution is better than 1 kilojoule. The maximum energy delivered is approximately 50 megajoules. The calorimetry loop to be calibrated is opened, and the calibrator is put in series with the calorimeter heat source. The calorimeter is then operated in its normal fashion, with the calibrator used as the heat source. The calibrator can also be used in a stand alone mode to calibrate calorimeter sensors removed from systems

  9. Fast sampling calorimetry with solid argon ionization chambers

    International Nuclear Information System (INIS)

    Clark, E.; Linn, S.; Piekarz, H.; Wahl, H.; Womersley, J.; Hansen, S.; Hurh, P.; Rivetta, C.; Sanders, R.; Schmitt, R.; Stanek, R.; Stefanik, A.

    1992-01-01

    A proposal for the fast sampling calorimetry with solid argon as active medium and the preliminary results from the solid argon test cell are presented. The proposed test calorimeter module structure, the signal routing and the mechanical and cryogenic arrangements are also discussed

  10. Optimization of crystals for applications in dual-readout calorimetry

    Czech Academy of Sciences Publication Activity Database

    Akchurin, N.; Bedeschi, F.; Cardini, A.; Carosi, R.; Ciapetti, G.; Fasoli, M.; Ferrari, R.; Franchino, S.; Fraternali, M.; Gaudio, G.; Hauptman, J.; Incagli, M.; Lacava, F.; La Rotonda, L.; Lee, S.; Livan, M.; Meoni, E.; Nikl, Martin; Pinci, D.; Policicchio, A.; Popescu, S.; Scuri, F.; Sill, A.; Susinno, G.; Vandelli, W.; Vedda, A.; Venturelli, T.; Voena, C.; Volobouev, I.; Wigmans, R.

    2010-01-01

    Roč. 621, 1-3 (2010), 212-221 ISSN 0168-9002 Institutional research plan: CEZ:AV0Z10100521 Keywords : calorimetry * Cherenkov light * High-Z scintillating crystals Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 1.142, year: 2010

  11. Hadronic shower development in iron-scintillator tile calorimetry

    Czech Academy of Sciences Publication Activity Database

    Amaral, P.; Amorim, A.; Anderson, K.; Lokajíček, Miloš; Němeček, Stanislav

    2000-01-01

    Roč. 443, - (2000), s. 51-70 ISSN 0168-9002 R&D Projects: GA MPO RP-4210/69 Institutional research plan: CEZ:AV0Z1010920 Keywords : ATLAS Iron-Scintillator * hadron calorimeter * shower parametrisation * calorimetry * computer data analysis Subject RIV: BL - Plasma and Gas Discharge Physics Impact factor: 0.964, year: 2000

  12. Particle flow calorimetry at the international linear collider

    Indian Academy of Sciences (India)

    Particle flow calorimetry at the international linear ... It is widely believed that the most promising strategy for achieving a jet ... this level of performance for two main reasons. Firstly ... (i) Tracking: For the studies presented in this paper, the track pattern ... that particles propagating outward from the interaction region will cross ...

  13. Differential Binding Models for Direct and Reverse Isothermal Titration Calorimetry.

    Science.gov (United States)

    Herrera, Isaac; Winnik, Mitchell A

    2016-03-10

    Isothermal titration calorimetry (ITC) is a technique to measure the stoichiometry and thermodynamics from binding experiments. Identifying an appropriate mathematical model to evaluate titration curves of receptors with multiple sites is challenging, particularly when the stoichiometry or binding mechanism is not available. In a recent theoretical study, we presented a differential binding model (DBM) to study calorimetry titrations independently of the interaction among the binding sites (Herrera, I.; Winnik, M. A. J. Phys. Chem. B 2013, 117, 8659-8672). Here, we build upon our DBM and show its practical application to evaluate calorimetry titrations of receptors with multiple sites independently of the titration direction. Specifically, we present a set of ordinary differential equations (ODEs) with the general form d[S]/dV that can be integrated numerically to calculate the equilibrium concentrations of free and bound species S at every injection step and, subsequently, to evaluate the volume-normalized heat signal (δQ(V) = δq/dV) of direct and reverse calorimetry titrations. Additionally, we identify factors that influence the shape of the titration curve and can be used to optimize the initial concentrations of titrant and analyte. We demonstrate the flexibility of our updated DBM by applying these differentials and a global regression analysis to direct and reverse calorimetric titrations of gadolinium ions with multidentate ligands of increasing denticity, namely, diglycolic acid (DGA), citric acid (CIT), and nitrilotriacetic acid (NTA), and use statistical tests to validate the stoichiometries for the metal-ligand pairs studied.

  14. Indirect calorimetry: assessing animal response to heat and cold stress

    NARCIS (Netherlands)

    Gaughan, J.B.; Heetkamp, M.J.W.; Hendriks, P.

    2015-01-01

    Calorimetric thermal stress studies where indirect calorimetry is used as a tool to estimate energy expenditure have been undertaken since this technique was developed. Some examples of these studies are presented in this chapter. The measurement of gas exchange by means of an open-circuit

  15. What does calorimetry and thermodynamics of living cells tell us?

    Science.gov (United States)

    Maskow, Thomas; Paufler, Sven

    2015-04-01

    This article presents and compares several thermodynamic methods for the quantitative interpretation of data from calorimetric measurements. Heat generation and absorption are universal features of microbial growth and product formation as well as of cell cultures from animals, plants and insects. The heat production rate reflects metabolic changes in real time and is measurable on-line. The detection limit of commercially available calorimetric instruments can be low enough to measure the heat of 100,000 aerobically growing bacteria or of 100 myocardial cells. Heat can be monitored in reaction vessels ranging from a few nanoliters up to many cubic meters. Most important the heat flux measurement does not interfere with the biological process under investigation. The practical advantages of calorimetry include the waiver of labeling and reactants. It is further possible to assemble the thermal transducer in a protected way that reduces aging and thereby signal drifts. Calorimetry works with optically opaque solutions. All of these advantages make calorimetry an interesting method for many applications in medicine, environmental sciences, ecology, biochemistry and biotechnology, just to mention a few. However, in many cases the heat signal is merely used to monitor biological processes but only rarely to quantitatively interpret the data. Therefore, a significant proportion of the information potential of calorimetry remains unutilized. To fill this information gap and to motivate the reader using the full information potential of calorimetry, various methods for quantitative data interpretations are presented, evaluated and compared with each other. Possible errors of interpretation and limitations of quantitative data analysis are also discussed. Copyright © 2014 Elsevier Inc. All rights reserved.

  16. Dosimetry and Calibration Section

    International Nuclear Information System (INIS)

    Otto, T.

    1998-01-01

    The two tasks of the Dosimetry and Calibration Section at CERN are the Individual Dosimetry Service which assures the personal monitoring of about 5000 persons potentially exposed to ionizing radiation at CERN, and the Calibration Laboratory which verifies all the instruments and monitors. This equipment is used by the sections of the RP Group for assuring radiation protection around CERN's accelerators, and by the Environmental Section of TISTE. In addition, nearly 250 electronic and 300 quartz fibre dosimeters, employed in operational dosimetry, are calibrated at least once a year. The Individual Dosimetry Service uses an extended database (INDOS) which contains information about all the individual doses ever received at CERN. For most of 1997 it was operated without the support of a database administrator as the technician who had assured this work retired. The Software Support Section of TIS-TE took over the technical responsibility of the database, but in view of the many other tasks of this Section and the lack of personnel, only a few interventions for solving immediate problems were possible

  17. Integration and global analysis of isothermal titration calorimetry data for studying macromolecular interactions.

    Science.gov (United States)

    Brautigam, Chad A; Zhao, Huaying; Vargas, Carolyn; Keller, Sandro; Schuck, Peter

    2016-05-01

    Isothermal titration calorimetry (ITC) is a powerful and widely used method to measure the energetics of macromolecular interactions by recording a thermogram of differential heating power during a titration. However, traditional ITC analysis is limited by stochastic thermogram noise and by the limited information content of a single titration experiment. Here we present a protocol for bias-free thermogram integration based on automated shape analysis of the injection peaks, followed by combination of isotherms from different calorimetric titration experiments into a global analysis, statistical analysis of binding parameters and graphical presentation of the results. This is performed using the integrated public-domain software packages NITPIC, SEDPHAT and GUSSI. The recently developed low-noise thermogram integration approach and global analysis allow for more precise parameter estimates and more reliable quantification of multisite and multicomponent cooperative and competitive interactions. Titration experiments typically take 1-2.5 h each, and global analysis usually takes 10-20 min.

  18. Automation of dosimeters calibration for radiotherapy in secondary dosimetric calibration laboratory of the CPHR

    International Nuclear Information System (INIS)

    Acosta, Andy L. Romero; Lores, Stefan Gutierrez

    2013-01-01

    This paper presents the design and implementation of an automated system for measurements in the calibration of reference radiation dosimeters. It was made a software application that performs the acquisition of the measured values of electric charge, calculated calibration coefficient and automates the calibration certificate issuance. These values are stored in a log file on a PC. The use of the application improves control over the calibration process, helps to humanize the work and reduces personnel exposure. The tool developed has been applied to the calibration of dosimeters radiation patterns in the LSCD of the Centro de Proteccion e Higiene de las Radiaciones, Cuba

  19. Glass transition of anhydrous starch by fast scanning calorimetry.

    Science.gov (United States)

    Monnier, Xavier; Maigret, Jean-Eudes; Lourdin, Denis; Saiter, Allisson

    2017-10-01

    By means of fast scanning calorimetry, the glass transition of anhydrous amorphous starch has been measured. With a scanning rate of 2000Ks -1 , thermal degradation of starch prior to the glass transition has been inhibited. To certify the glass transition measurement, structural relaxation of the glassy state has been investigated through physical aging as well as the concept of limiting fictive temperature. In both cases, characteristic enthalpy recovery peaks related to the structural relaxation of the glass have been observed. Thermal lag corrections based on the comparison of glass transition temperatures measured by means of differential and fast scanning calorimetry have been proposed. The complementary investigations give an anhydrous amorphous starch glass transition temperature of 312±7°C. This estimation correlates with previous extrapolation performed on hydrated starches. Copyright © 2017 Elsevier Ltd. All rights reserved.

  20. Scintillating glasses for total absorption dual readout calorimetry

    Energy Technology Data Exchange (ETDEWEB)

    Bonvicini, V. [INFN, Trieste; Driutti, A. [Udine U.; Cauz, D. [Udine U.; Pauletta, G. [Udine U.; Rubinov, P. [Fermilab; Santi, L. [Udine U.; Wenzel, H. [Fermilab

    2012-01-01

    Scintillating glasses are a potentially cheaper alternative to crystal - based calorimetry with common problems related to light collection, detection and processing. As such, their use and development are part of more extensive R&D aimed at investigating the potential of total absorption, combined with the readout (DR) technique, for hadron calorimetry. A recent series of measurements, using cosmic and particle beams from the Fermilab test beam facility and scintillating glass with the characteristics required for application of the DR technique, serve to illustrate the problems addressed and the progress achieved by this R&D. Alternative solutions for light collection (conventional and silicon photomultipliers) and signal processing are compared, the separate contributions of scintillation and Cherenkov processes to the signal are evaluated and results are compared to simulation.

  1. Inherent limitations of fixed time servo-controlled radiometric calorimetry

    International Nuclear Information System (INIS)

    Wetzel, J.R.; Duff, M.F.; Lemming, J.F.

    1987-01-01

    There has been some interest in low precision, short run time calorimetry measurements. This type of calorimetry measurement has been proposed for use when high precision measurements are not required, for example, to screen scrap containers to determine if there is enough material to be measured more accurately of for confirmatory measurements that only require low precision results. The equipment needed to make these measurements is a servo-controlled calorimeter with a sample preequilibration bath. The preequilibration bath temperature is set to the internal temperature of the calorimeter running at a fixed servo-controlled wattage level. The sample power value is determined at a fixed time form the sample loading into the calorimeter. There are some limitations and areas of uncertainties in the use of data obtained by this method. Data collected under controlled conditions demonstrate the limitations. Sample packaging, preequilibration time, and item wattage were chosen as the variables most likely to be encountered in a plant environment

  2. Physicochemical characterization of pitches by differential scanning calorimetry

    Energy Technology Data Exchange (ETDEWEB)

    Lahaye, J.; Ehrburger, P.; Saint-Romain, J.L.; Couderc, P.

    1987-11-01

    The glass transition characterization of pitches has been studied by differential scanning calorimetry (d.s.c.). Experimental results and theoretical considerations indicate that: (1) the average molecular mass of pitches can be characterized by the apparent activation energy of the relaxation phenomenon of pitch molecules; (2) the molecular polydispersity is correlated with the width of the glass transition. Characterization of pitch by d.s.c. is well adapted to follow pitch transformation during heat treatment. 6 refs., 6 figs., 4 tabs.

  3. The upgraded CDF front end electronics for calorimetry

    Energy Technology Data Exchange (ETDEWEB)

    Drake, G.; Frei, D.; Hahn, S.R.; Nelson, C.A.; Segler, S.L.; Stuermer, W.

    1991-11-01

    The front end electronics used in the calorimetry of the CDF detector has been upgraded to meet system requirements for higher expected luminosity. A fast digitizer utilizing a 2 {mu}Sec, 16 bit ADC has been designed and built. Improvements to the front end trigger circuitry have been implemented, including the production of 900 new front end modules. Operational experience with the previous system is presented, with discussion of the problems and performance goals.

  4. The upgraded CDF front end electronics for calorimetry

    International Nuclear Information System (INIS)

    Drake, G.; Frei, D.; Hahn, S.R.; Nelson, C.A.; Segler, S.L.; Stuermer, W.

    1991-11-01

    The front end electronics used in the calorimetry of the CDF detector has been upgraded to meet system requirements for higher expected luminosity. A fast digitizer utilizing a 2 μSec, 16 bit ADC has been designed and built. Improvements to the front end trigger circuitry have been implemented, including the production of 900 new front end modules. Operational experience with the previous system is presented, with discussion of the problems and performance goals

  5. The Philosophy and Feasibility of Dual Readout Calorimetry

    International Nuclear Information System (INIS)

    Hauptman, John

    2006-01-01

    I will discuss the general physical ideas behind dual-readout calorimetry, their implementation in DREAM (Dual REAdout Module) with exact separation of scintillation and Cerenkov light, implementation with mixed light in DREAM fibers, anticipated implementation in PbWO4 crystals with applications to the 4th Concept detector and to CMS, use in high energy gamma-ray and cosmic ray astrophysics with Cerenkov and N2 fluorescent light, and implementation in the 4th Concept detector for muon identification

  6. Application of kinetic inductance thermometers to x-ray calorimetry

    International Nuclear Information System (INIS)

    Wai, Y.C.; Labov, S.E.; Silver, E.H.

    1990-01-01

    A kinetic inductance thermometer is applied to x-ray calorimetry, and its operation over a wide range of frequencies and geometries is discussed. Three amplifier configurations are described, one using a superconducting quantum interference device (SQUID) amplifier, another incorporating an FET amplifier in an amplitude modulated system, and the third, using a tunnel diode frequency modulated oscillator circuit. The predicted performance of each configuration is presented. 13 refs., 6 figs., 1 tab

  7. DEM Calibration Approach: design of experiment

    Science.gov (United States)

    Boikov, A. V.; Savelev, R. V.; Payor, V. A.

    2018-05-01

    The problem of DEM models calibration is considered in the article. It is proposed to divide models input parameters into those that require iterative calibration and those that are recommended to measure directly. A new method for model calibration based on the design of the experiment for iteratively calibrated parameters is proposed. The experiment is conducted using a specially designed stand. The results are processed with technical vision algorithms. Approximating functions are obtained and the error of the implemented software and hardware complex is estimated. The prospects of the obtained results are discussed.

  8. The KLOE online calibration system

    International Nuclear Information System (INIS)

    Pasqualucci, E.; Alexander, G.; Aloisio, A.

    2001-01-01

    Based on all the features of the KLOE online software, the online calibration system performs current calibration quality checking in real time and starts automatically new calibration procedures when needed. A calibration manager process controls the system, implementing the interface to the online system, receiving information from the run control and translating its state transitions to a separate state machine. It acts as a 'calibration run controller' and performs failure recovery when requested by a set of process checkers. The core of the system is a multi-threaded OO histogram server that receives histogramming commands by remote processes and operates on local ROOT histograms. A client library and C, fortran and C++ application interface libraries allow the user to connect and define his own histogram or read histograms owned by others using an book-like interface. Several calibration processes running in parallel in a distributed, multiplatform environment can fill the same histograms, allowing fast external information check. A monitor thread allow remote browsing for visual inspection. Pre-filtered data are read in non-privileged spy mode from the data acquisition system via the Kloe Integrated Dataflow. The main characteristics of the system are presented

  9. Software engineering

    CERN Document Server

    Sommerville, Ian

    2010-01-01

    The ninth edition of Software Engineering presents a broad perspective of software engineering, focusing on the processes and techniques fundamental to the creation of reliable, software systems. Increased coverage of agile methods and software reuse, along with coverage of 'traditional' plan-driven software engineering, gives readers the most up-to-date view of the field currently available. Practical case studies, a full set of easy-to-access supplements, and extensive web resources make teaching the course easier than ever.

  10. Calibration of the ZEUS forward calorimeter

    International Nuclear Information System (INIS)

    Kraemer, M.

    1990-10-01

    The physics at the ep-collider HERA requires high resolution calorimetry calibrated with an accuracy of better than 2%. The ZEUS detector meets these conditions by means of a compensating uranium scintillator sandwich calorimeter with an energy resolution of σ/E = 35%/√E + σ cal , where σ cal is the calibration error. One of the tools to minimize σ cal is the calibration with the signals of the radioactivity of the Uranium plates (UNO). Taking UNO data every 8 hours keeps the calibration stable within ≅ 1%. The muon calibration is done employing an algorithm, that determines the most probable energy loss with a precision of ≅ 1%. The channel-to-channel fluctuations of the ratio μ/UNO for a forward calorimeter (FCAL) prototype show a spread of 5.2% for the electromagnetic calorimeter and ≅ 2.5% for the hadronic sections. Improvements in the construction of the FCAL modules decreased these fluctuations to 2.0% and ≅ 1.8% respectively. The influence of the cracks between the calorimeter modules amounts to ≅ 1.7% on average for the ZEUS geometry, if a 2 mm thick Pb-sheet is introduced between the modules. We conclude that we are able to keep σ cal below 2%. (orig.)

  11. The STARLINK software collection

    Science.gov (United States)

    Penny, A. J.; Wallace, P. T.; Sherman, J. C.; Terret, D. L.

    1993-12-01

    A demonstration will be given of some recent Starlink software. STARLINK is: a network of computers used by UK astronomers; a collection of programs for the calibration and analysis of astronomical data; a team of people giving hardware, software and administrative support. The Starlink Project has been in operation since 1980 to provide UK astronomers with interactive image processing and data reduction facilities. There are now Starlink computer systems at 25 UK locations, serving about 1500 registered users. The Starlink software collection now has about 25 major packages covering a wide range of astronomical data reduction and analysis techniques, as well as many smaller programs and utilities. At the core of most of the packages is a common `software environment', which provides many of the functions which applications need and offers standardized methods of structuring and accessing data. The software environment simplifies programming and support, and makes it easy to use different packages for different stages of the data reduction. Users see a consistent style, and can mix applications without hitting problems of differing data formats. The Project group coordinates the writing and distribution of this software collection, which is Unix based. Outside the UK, Starlink is used at a large number of places, which range from installations at major UK telescopes, which are Starlink-compatible and managed like Starlink sites, to individuals who run only small parts of the Starlink software collection.

  12. Fast differential scanning calorimetry of liquid samples with chips

    DEFF Research Database (Denmark)

    Splinter, R.; van Herwaarden, A. W.; van Wetten, I. A.

    2015-01-01

    Based on a modified version of standard chips for fast differential scanning calorimetry, DSC of liquid samples has been performed at temperature scan rates of up to 1000 °C/s. This paper describes experimental results with the protein lysozyme, bovine serum, and olive oil. The heating and cooling....... The bovine serum measurements show two main peaks, in good agreement with standard DSC measurements. Olive oil has been measured, with good agreement for the cooling curve and qualitative agreement for the heater curve, compared to DSC measurements....

  13. Neutral-beam aiming and calorimetry for MFTF-B

    International Nuclear Information System (INIS)

    Goldner, A.I.; Margolies, D.

    1981-01-01

    The vessel for the Tandem Mirror Fusion Test Facility (MFTF-B) will have up to eleven 0.5-s-duration neutral-beam injectors for the initial heating of the MFTF-B plasma. Knowing the exact alignment of the beams and their total power is critical to the performance of the experiment. Using prototype aiming and calorimetry systems on the High Voltage Test Stand (HVTS) at Lawrence Livermore National Laboratory (LLNL), we hope to prove our ability to obtain an aiming accuracy of +-1 cm at the plasma and a calorimetric accuracy of +-5% of the actual total beam energy

  14. A custom floating point format ADC for LHC calorimetry

    International Nuclear Information System (INIS)

    Hermel, V.; Lecoq, J.; Bohner, G.

    1996-01-01

    Due to their large dynamic range (in excess of 16 bits) signals from LHC calorimetry poses severe problems to the shaping and digitizing circuits. We are investigating a solution for an ADC based on a custom floating point format. Since the calorimeter precision is limited, the full dynamic range can be split into 8 positive sub-ranges and 5 negative ones, each with an 8 bits dynamic. The reduced number of bits (8 for the mantissa, 4 for the exponent and 1 for the sign) translates itself into a reduction of the power consumption both of the ADC and of the following digital filtering stages. (authors)

  15. Evaluation of aluminosilicate glass sintering during differential scanning calorimetry

    International Nuclear Information System (INIS)

    Souza, Juliana Pereira de

    2015-01-01

    In this work a difference in the baseline in differential scanning calorimetry analyses, observed in a work where aluminosilicate glasses microspheres containing Ho were studied for application in selective internal radiotherapy as hepatocellular carcinoma treatment, was studied. The glasses with nominal composition 53,7 SiO 2 .10,5 Al 2 O 3 . 35,8 MgO in %mol were produced from traditional melting. The first obtained were milled and sieved in the range of 45 a 63 μm. The material was used to produce glass microspheres by the gravitational fall method. The glass powder and the microspheres were characterized by X ray fluorescence spectrometry, laser diffraction, X ray diffraction, differential scanning calorimetry, differential thermal analysis, thermogravimetry, mass spectrometry, and scanning electron microscopy. After the thermal analyses, pellets were formed in the crucibles and were analyzed by scanning electron microscopy, X ray diffraction, and He pycnometry. The difference in the baseline was associated to the viscous flow sintering process and happens because of the decrease in the detected heat flow due to the sample shrinkage. Other events as concurrent crystallization with the sintering process were also studied. (author)

  16. Tritium inventory measurements by 'in-bed' gas flowing calorimetry

    International Nuclear Information System (INIS)

    Hayashi, T.; Suzuki, T.; Yamada, M.; Okuno, K.

    1996-01-01

    In order to establish the 'in-bed' tritium accounting technology for the ITER scale tritium storage system, a gas flowing calorimetry has been studied using a scaled ZrCo bed (25 g tritium capacity). The basic calorimetric characteristics, steady state temperature raise of He gas stream flowing through a secondary coil line fixed in the ZrCo tritide, was measured and correlated with the stored tritium inventory. The results shows that about 4 degrees raise of He stream temperature can be detected for each gram of tritium storage. The sensitivity of this calorimetry is about 0.05 g of tritium, calculated by 0.2 degrees of temperature sensor error. The accuracy is better than 0.25 g of tritium on 25 g storage, evaluated by 2 times of standard deviation from the repeat measurements. This accuracy of < 1% on full storage capacity is satisfied the target accountability to measure ± 1 gram of tritium on 100 g storage for ITER. 13 refs., 7 figs

  17. SOFTWARE OPEN SOURCE, SOFTWARE GRATIS?

    Directory of Open Access Journals (Sweden)

    Nur Aini Rakhmawati

    2006-01-01

    Full Text Available Normal 0 false false false IN X-NONE X-NONE MicrosoftInternetExplorer4 Berlakunya Undang – undang Hak Atas Kekayaan Intelektual (HAKI, memunculkan suatu alternatif baru untuk menggunakan software open source. Penggunaan software open source menyebar seiring dengan isu global pada Information Communication Technology (ICT saat ini. Beberapa organisasi dan perusahaan mulai menjadikan software open source sebagai pertimbangan. Banyak konsep mengenai software open source ini. Mulai dari software yang gratis sampai software tidak berlisensi. Tidak sepenuhnya isu software open source benar, untuk itu perlu dikenalkan konsep software open source mulai dari sejarah, lisensi dan bagaimana cara memilih lisensi, serta pertimbangan dalam memilih software open source yang ada. Kata kunci :Lisensi, Open Source, HAKI

  18. Software Epistemology

    Science.gov (United States)

    2016-03-01

    in-vitro decision to incubate a startup, Lexumo [7], which is developing a commercial Software as a Service ( SaaS ) vulnerability assessment...LTS Label Transition System MUSE Mining and Understanding Software Enclaves RTEMS Real-Time Executive for Multi-processor Systems SaaS Software ...as a Service SSA Static Single Assignment SWE Software Epistemology UD/DU Def-Use/Use-Def Chains (Dataflow Graph)

  19. Computational integration of the phases and procedures of calibration processes for radioprotection

    International Nuclear Information System (INIS)

    Santos, Gleice R. dos; Thiago, Bibiana dos S.; Rocha, Felicia D.G.; Santos, Gelson P. dos; Potiens, Maria da Penha A.; Vivolo, Vitor

    2011-01-01

    This work proceed the computational integration of the processes phases by using only a single computational software, from the entrance of the instrument at the Instrument Calibration Laboratory (LCI-IPEN) to the conclusion of calibration procedures. So, the initial information such as trade mark, model, manufacturer, owner, and the calibration records are digitized once until the calibration certificate emission

  20. Software reliability

    CERN Document Server

    Bendell, A

    1986-01-01

    Software Reliability reviews some fundamental issues of software reliability as well as the techniques, models, and metrics used to predict the reliability of software. Topics covered include fault avoidance, fault removal, and fault tolerance, along with statistical methods for the objective assessment of predictive accuracy. Development cost models and life-cycle cost models are also discussed. This book is divided into eight sections and begins with a chapter on adaptive modeling used to predict software reliability, followed by a discussion on failure rate in software reliability growth mo

  1. Computer software.

    Science.gov (United States)

    Rosenthal, L E

    1986-10-01

    Software is the component in a computer system that permits the hardware to perform the various functions that a computer system is capable of doing. The history of software and its development can be traced to the early nineteenth century. All computer systems are designed to utilize the "stored program concept" as first developed by Charles Babbage in the 1850s. The concept was lost until the mid-1940s, when modern computers made their appearance. Today, because of the complex and myriad tasks that a computer system can perform, there has been a differentiation of types of software. There is software designed to perform specific business applications. There is software that controls the overall operation of a computer system. And there is software that is designed to carry out specialized tasks. Regardless of types, software is the most critical component of any computer system. Without it, all one has is a collection of circuits, transistors, and silicone chips.

  2. Bayesian calibration : past achievements and future challenges

    International Nuclear Information System (INIS)

    Christen, J.A.

    2001-01-01

    Due to variations of the radiocarbon content in the biosphere over time, radiocarbon determinations need to be calibrated to obtain calendar years. Over the past decade a series of researchers have investigated the possibility of using Bayesian statistics to calibrate radiocarbon determinations, the main feature being the inclusion of contextual information into the calibration process. This allows for a coherent calibration of groups of determinations arising from related contexts (stratigraphical layers, peat cores, cultural events, ect.). Moreover, the 'related contexts' are also dated, and not only the material radiocarbon dated itself. We review Bayesian Calibration and state some of its current challenges like: software development, prior specification, robustness, etc. (author). 14 refs., 4 figs

  3. Detectors for Linear Colliders: Calorimetry at a Future Electron-Positron Collider (3/4)

    CERN Multimedia

    CERN. Geneva

    2010-01-01

    Calorimetry will play a central role in determining the physics reach at a future e+e- collider. The requirements for calorimetry place the emphasis on achieving an excellent jet energy resolution. The currently favoured option for calorimetry at a future e+e- collider is the concept of high granularity particle flow calorimetry. Here granularity and a high pattern recognition capability is more important than the single particle calorimetric response. In this lecture I will describe the recent progress in understanding the reach of high granularity particle flow calorimetry and the related R&D efforts which concentrate on test beam demonstrations of the technological options for highly granular calorimeters. I will also discuss alternatives to particle flow, for example the technique of dual readout calorimetry.

  4. Hydroxylamine nitrate self-catalytic kinetics study with adiabatic calorimetry

    Energy Technology Data Exchange (ETDEWEB)

    Liu Lijun [Mary Kay O' Connor Process Safety Center, Artie McFerrin Department of Chemical Engineering, Texas A and M University System, College Station, TX 77843-3122 (United States); Wei Chunyang [BASF Corporation, Wyandotte, MI 48192 (United States); Guo Yuyan; Rogers, William J. [Mary Kay O' Connor Process Safety Center, Artie McFerrin Department of Chemical Engineering, Texas A and M University System, College Station, TX 77843-3122 (United States); Sam Mannan, M. [Mary Kay O' Connor Process Safety Center, Artie McFerrin Department of Chemical Engineering, Texas A and M University System, College Station, TX 77843-3122 (United States)], E-mail: mannan@tamu.edu

    2009-03-15

    Hydroxylamine nitrate (HAN) is an important member of the hydroxylamine compound family with applications that include equipment decontamination in the nuclear industry and aqueous or solid propellants. Due to its instability and autocatalytic behavior, HAN has been involved in several incidents at the Hanford and Savannah River Site (SRS) [Technical Report on Hydroxylamine Nitrate, US Department of Energy, 1998]. Much research has been conducted on HAN in different areas, such as combustion mechanism, decomposition mechanism, and runaway behavior. However, the autocatalytic decomposition behavior of HAN at runaway stage has not been fully addressed due to its highly exothermic and rapid decomposition behavior. This work is focused on extracting HAN autocatalytic kinetics and analyzing HAN critical behavior from adiabatic calorimetry measurements. A lumped autocatalytic kinetic model for HAN and associated model parameters are determined. Also the storage and handling critical conditions of diluted HAN solution without metal presence are quantified.

  5. Review of MEMS differential scanning calorimetry for biomolecular study

    Science.gov (United States)

    Yu, Shifeng; Wang, Shuyu; Lu, Ming; Zuo, Lei

    2017-12-01

    Differential scanning calorimetry (DSC) is one of the few techniques that allow direct determination of enthalpy values for binding reactions and conformational transitions in biomolecules. It provides the thermodynamics information of the biomolecules which consists of Gibbs free energy, enthalpy and entropy in a straightforward manner that enables deep understanding of the structure function relationship in biomolecules such as the folding/unfolding of protein and DNA, and ligand bindings. This review provides an up to date overview of the applications of DSC in biomolecular study such as the bovine serum albumin denaturation study, the relationship between the melting point of lysozyme and the scanning rate. We also introduce the recent advances of the development of micro-electro-mechanic-system (MEMS) based DSCs.

  6. On the Interpretation of Low Temperature Calorimetry Data

    DEFF Research Database (Denmark)

    Kjeldsen, Ane Mette; Geiker, Mette Rica

    2008-01-01

    The effect of selected factors and phenomena on Low Temperature Calorimetry (LTC) results has been investigated, in order to determine the possibilities and limitations of using LTC for characterisation of the porosity of cement-based materials. LTC was carried out on a model material with mono......-sized pores of approximately 14 nm saturated with either distilled water or a sodium chloride solution, as well as on water, the salt solution, and an artificial pore solution, alone. It was found that supercooling is unavoidable during the liquid-solid phase transition, and that even at low temperature...... to limit transport of liquid, whereas heating should be undertaken at a low rate to limit the effect of non-equilibrium....

  7. Probing Free-Energy Surfaces with Differential Scanning Calorimetry

    Science.gov (United States)

    Sanchez-Ruiz, Jose M.

    2011-05-01

    Many aspects of protein folding can be understood in terms of projections of the highly dimensional energy landscape onto a few (or even only one) particularly relevant coordinates. These free-energy surfaces can be probed conveniently from experimental differential scanning calorimetry (DSC) thermograms, as DSC provides a direct relation with the protein partition function. Free-energy surfaces thus obtained are consistent with two fundamental scenarios predicted by the energy-landscape perspective: (a) well-defined macrostates separated by significant free-energy barriers, in some cases, and, in many other cases, (b) marginal or even vanishingly small barriers, which furthermore show a good correlation with kinetics for fast- and ultrafast-folding proteins. Overall, the potential of DSC to assess free-energy surfaces for a wide variety of proteins makes it possible to address fundamental issues, such as the molecular basis of the barrier modulations produced by natural selection in response to functional requirements or to ensure kinetic stability.

  8. Hydroxylamine nitrate self-catalytic kinetics study with adiabatic calorimetry

    International Nuclear Information System (INIS)

    Liu Lijun; Wei Chunyang; Guo Yuyan; Rogers, William J.; Sam Mannan, M.

    2009-01-01

    Hydroxylamine nitrate (HAN) is an important member of the hydroxylamine compound family with applications that include equipment decontamination in the nuclear industry and aqueous or solid propellants. Due to its instability and autocatalytic behavior, HAN has been involved in several incidents at the Hanford and Savannah River Site (SRS) [Technical Report on Hydroxylamine Nitrate, US Department of Energy, 1998]. Much research has been conducted on HAN in different areas, such as combustion mechanism, decomposition mechanism, and runaway behavior. However, the autocatalytic decomposition behavior of HAN at runaway stage has not been fully addressed due to its highly exothermic and rapid decomposition behavior. This work is focused on extracting HAN autocatalytic kinetics and analyzing HAN critical behavior from adiabatic calorimetry measurements. A lumped autocatalytic kinetic model for HAN and associated model parameters are determined. Also the storage and handling critical conditions of diluted HAN solution without metal presence are quantified

  9. Novel investigation of enzymatic biodiesel reaction by isothermal calorimetry

    DEFF Research Database (Denmark)

    Søtoft, Lene Fjerbaek; Westh, Peter; Christensen, Knud V.

    2010-01-01

    Isothermal calorimetry (ITC) was used to investigate solvent-free enzymatic biodiesel production. The transesterification of rapeseed oil with methanol and ethanol was catalyzed by immobilized lipase Novozym 435 at 40 °C. The aim of the study was to determine reaction enthalpy for the enzymatic...... transesterification and to elucidate the mass transfer and energetic processes taking place. Based on the measured enthalpy and composition change in the system, the heat of reaction at 40 °C for the two systems was determined as −9.8 ± 0.9 kJ/mole biodiesel formed from rapeseed oil and methanol, and −9.3 ± 0.7 k...

  10. Local Measurement of Fuel Energy Deposition and Heat Transfer Environment During Fuel Lifetime Using Controlled Calorimetry

    International Nuclear Information System (INIS)

    Don W. Miller; Andrew Kauffmann; Eric Kreidler; Dongxu Li; Hanying Liu; Daniel Mills; Thomas D. Radcliff; Joseph Talnagi

    2001-01-01

    A comprehensive description of the accomplishments of the DOE grant titled, ''Local Measurement of Fuel Energy Deposition and Heat Transfer Environment During Fuel Lifetime using Controlled Calorimetry''

  11. SU-E-T-267: Development of the Compact Graphite Calorimetry System for the High Energy Photon Beam

    Energy Technology Data Exchange (ETDEWEB)

    Kim, B. C.; Kim, I. J.; Kim, J. H.; Yi, C. Y. [Korea Research Institute of Standards and Science, Daejeon (Korea, Republic of)

    2015-06-15

    Purpose: Graphite calorimeter systems are used for the absolute photon dosimetry. But many electronics are demanded in order to measure the tiny temperature changes. Minimizing the control system is needed to make a portable graphite calorimeter. Methods: A Domen-type graphite calorimetry system is constructing to measure the absorbed dose of the high energy photon beam. The graphite calorimeter divided into three parts, Core, Jacket, and Shield. In order to measure the temperature rising of the core due to the radiation accurately, the temperatures of the jacket and the shield should be controlled properly. A commercial temperature controller (Model 350, Lake Shore Cryogenics) was used to minimize the size of control system for making a portable graphite calorimetry system at the cost of the measurement uncertainty. The PID control of the jacket is conducted by the software (LabView) and Model 350 maintain the temperature of shield. Results: Our design value of the heat deposition power in the core is 0.04 mW for the dose rate of 3 Gy/min where the temperature sensitivity of the graphite is 1.4 mK/Gy. While the residuals of the Steinhart-hart equation fitting for the core thermistor were less than 0.1 mK, the temperature resolution of Model 350 is 1 mK. The temperature of the shield was kept within the 5 mK when the room temperature variation was about 0.5 K. Conclusion: The resolution of Model 350 for the temperature measurement and control is not good enough as the control system for the compact graphite calorimetry system. But The performance of Model 350 is good enough to maintain the temperature of the shield constantly. The Model 350 will be replaced by the AC resistance bridge (Model 372, Lake Shore Cryogenics) for the core temperature measurement and the jacket control.

  12. Infrared stereo calibration for unmanned ground vehicle navigation

    Science.gov (United States)

    Harguess, Josh; Strange, Shawn

    2014-06-01

    The problem of calibrating two color cameras as a stereo pair has been heavily researched and many off-the-shelf software packages, such as Robot Operating System and OpenCV, include calibration routines that work in most cases. However, the problem of calibrating two infrared (IR) cameras for the purposes of sensor fusion and point could generation is relatively new and many challenges exist. We present a comparison of color camera and IR camera stereo calibration using data from an unmanned ground vehicle. There are two main challenges in IR stereo calibration; the calibration board (material, design, etc.) and the accuracy of calibration pattern detection. We present our analysis of these challenges along with our IR stereo calibration methodology. Finally, we present our results both visually and analytically with computed reprojection errors.

  13. Calibration strategies for the Cherenkov Telescope Array

    Science.gov (United States)

    Gaug, Markus; Berge, David; Daniel, Michael; Doro, Michele; Förster, Andreas; Hofmann, Werner; Maccarone, Maria C.; Parsons, Dan; de los Reyes Lopez, Raquel; van Eldik, Christopher

    2014-08-01

    The Central Calibration Facilities workpackage of the Cherenkov Telescope Array (CTA) observatory for very high energy gamma ray astronomy defines the overall calibration strategy of the array, develops dedicated hardware and software for the overall array calibration and coordinates the calibration efforts of the different telescopes. The latter include LED-based light pulsers, and various methods and instruments to achieve a calibration of the overall optical throughput. On the array level, methods for the inter-telescope calibration and the absolute calibration of the entire observatory are being developed. Additionally, the atmosphere above the telescopes, used as a calorimeter, will be monitored constantly with state-of-the-art instruments to obtain a full molecular and aerosol profile up to the stratosphere. The aim is to provide a maximal uncertainty of 10% on the reconstructed energy-scale, obtained through various independent methods. Different types of LIDAR in combination with all-sky-cameras will provide the observatory with an online, intelligent scheduling system, which, if the sky is partially covered by clouds, gives preference to sources observable under good atmospheric conditions. Wide-field optical telescopes and Raman Lidars will provide online information about the height-resolved atmospheric extinction, throughout the field-of-view of the cameras, allowing for the correction of the reconstructed energy of each gamma-ray event. The aim is to maximize the duty cycle of the observatory, in terms of usable data, while reducing the dead time introduced by calibration activities to an absolute minimum.

  14. Hadronic energy resolution of a highly granular scintillator-steel hadron calorimeter using software compensation techniques

    Czech Academy of Sciences Publication Activity Database

    Adloff, C.; Blaha, J.; Blaising, J.J.; Cvach, Jaroslav; Gallus, Petr; Havránek, Miroslav; Janata, Milan; Kvasnička, Jiří; Lednický, Denis; Marčišovský, Michal; Polák, Ivo; Popule, Jiří; Tomášek, Lukáš; Tomášek, Michal; Růžička, Pavel; Šícho, Petr; Smolík, Jan; Vrba, Václav; Zálešák, Jaroslav

    2012-01-01

    Roč. 7, SEP (2012), 1-23 ISSN 1748-0221 R&D Projects: GA MŠk LA09042; GA MŠk LC527; GA ČR GA202/05/0653 Institutional research plan: CEZ:AV0Z10100502 Keywords : hadronic calorimetry * imaging calorimetry * software compensation Subject RIV: BF - Elementary Particles and High Energy Physics Impact factor: 1.869, year: 2011

  15. Software-based acoustical measurements

    CERN Document Server

    Miyara, Federico

    2017-01-01

    This textbook provides a detailed introduction to the use of software in combination with simple and economical hardware (a sound level meter with calibrated AC output and a digital recording system) to obtain sophisticated measurements usually requiring expensive equipment. It emphasizes the use of free, open source, and multiplatform software. Many commercial acoustical measurement systems use software algorithms as an integral component; however the methods are not disclosed. This book enables the reader to develop useful algorithms and provides insight into the use of digital audio editing tools to document features in the signal. Topics covered include acoustical measurement principles, in-depth critical study of uncertainty applied to acoustical measurements, digital signal processing from the basics, and metrologically-oriented spectral and statistical analysis of signals. The student will gain a deep understanding of the use of software for measurement purposes; the ability to implement software-based...

  16. Mechanics of log calibration

    International Nuclear Information System (INIS)

    Waller, W.C.; Cram, M.E.; Hall, J.E.

    1975-01-01

    For any measurement to have meaning, it must be related to generally accepted standard units by a valid and specified system of comparison. To calibrate well-logging tools, sensing systems are designed which produce consistent and repeatable indications over the range for which the tool was intended. The basics of calibration theory, procedures, and calibration record presentations are reviewed. Calibrations for induction, electrical, radioactivity, and sonic logging tools will be discussed. The authors' intent is to provide an understanding of the sources of errors, of the way errors are minimized in the calibration process, and of the significance of changes in recorded calibration data

  17. Software Innovation

    DEFF Research Database (Denmark)

    Rose, Jeremy

      Innovation is the forgotten key to modern systems development - the element that defines the enterprising engineer, the thriving software firm and the cutting edge software application.  Traditional forms of technical education pay little attention to creativity - often encouraging overly...

  18. A New Automated Instrument Calibration Facility at the Savannah River Site

    International Nuclear Information System (INIS)

    Polz, E.; Rushton, R.O.; Wilkie, W.H.; Hancock, R.C.

    1998-01-01

    The Health Physics Instrument Calibration Facility at the Savannah River Site in Aiken, SC was expressly designed and built to calibrate portable radiation survey instruments. The facility incorporates recent advances in automation technology, building layout and construction, and computer software to improve the calibration process. Nine new calibration systems automate instrument calibration and data collection. The building is laid out so that instruments are moved from one area to another in a logical, efficient manner. New software and hardware integrate all functions such as shipping/receiving, work flow, calibration, testing, and report generation. Benefits include a streamlined and integrated program, improved efficiency, reduced errors, and better accuracy

  19. Automation is an Effective Way to Improve Quality of Verification (Calibration) of Measuring Instruments

    Science.gov (United States)

    Golobokov, M.; Danilevich, S.

    2018-04-01

    In order to assess calibration reliability and automate such assessment, procedures for data collection and simulation study of thermal imager calibration procedure have been elaborated. The existing calibration techniques do not always provide high reliability. A new method for analyzing the existing calibration techniques and developing new efficient ones has been suggested and tested. A type of software has been studied that allows generating instrument calibration reports automatically, monitoring their proper configuration, processing measurement results and assessing instrument validity. The use of such software allows reducing man-hours spent on finalization of calibration data 2 to 5 times and eliminating a whole set of typical operator errors.

  20. Software engineering

    CERN Document Server

    Sommerville, Ian

    2016-01-01

    For courses in computer science and software engineering The Fundamental Practice of Software Engineering Software Engineering introduces readers to the overwhelmingly important subject of software programming and development. In the past few years, computer systems have come to dominate not just our technological growth, but the foundations of our world's major industries. This text seeks to lay out the fundamental concepts of this huge and continually growing subject area in a clear and comprehensive manner. The Tenth Edition contains new information that highlights various technological updates of recent years, providing readers with highly relevant and current information. Sommerville's experience in system dependability and systems engineering guides the text through a traditional plan-based approach that incorporates some novel agile methods. The text strives to teach the innovators of tomorrow how to create software that will make our world a better, safer, and more advanced place to live.

  1. Thermodynamics of biphasic lanthanide extraction by tripodal diglycolamide: a solution calorimetry study

    NARCIS (Netherlands)

    Ansari, S.A.; Mohapatra, P.K.; Verboom, Willem; Rao, L.

    2016-01-01

    Isothermal titration calorimetry was employed for the direct measurement of the enthalpy of extraction (ΔHextr) of Eu(NO3)3 by using a tripodal diglycolamide (T-DGA) ligand dissolved in n-dodecane containing 5% (v/v) 2-decanol. The enthalpy of extraction obtained by titration calorimetry was in good

  2. Isothermal reaction calorimetry as a tool for kinetic analysis

    International Nuclear Information System (INIS)

    Zogg, Andreas; Stoessel, Francis; Fischer, Ulrich; Hungerbuehler, Konrad

    2004-01-01

    Reaction calorimetry has found widespread application for thermal and kinetic analysis of chemical reactions in the context of thermal process safety as well as process development. This paper reviews the most important reaction calorimetric principles (heat-flow, heat-balance, power-compensation, and Peltier principle) and their applications in commercial or scientific devices. The discussion focuses on the different dynamic behavior of the main calorimetric principles during an isothermal reaction measurement. Examples of available reaction calorimeters are further compared considering their detection limit, time constant as well as temperature range. In a second part, different evaluation methods for the isothermally measured calorimetric data are reviewed and discussed. The methods will be compared, focusing especially on the fact that reaction calorimetric data always contains additional informations not directly related to the actual chemical reaction such as heat of mixing, heat of phase-transfer/change processes or simple measurement errors. Depending on the evaluation method applied such disturbances have a significant influence on the calculated reaction enthalpies or rate constants

  3. Thermodynamic properties of soddyite from solubility and calorimetry measurements

    International Nuclear Information System (INIS)

    Gorman-Lewis, Drew; Mazeina, Lena; Fein, Jeremy B.; Szymanowski, Jennifer E.S.; Burns, Peter C.; Navrotsky, Alexandra

    2007-01-01

    The release of uranium from geologic nuclear waste repositories under oxidizing conditions can only be modeled if the thermodynamic properties of the secondary uranyl minerals that form in the repository setting are known. Toward this end, we synthesized soddyite ((UO 2 ) 2 (SiO 4 )(H 2 O) 2 ), and performed solubility measurements from both undersaturation and supersaturation. The solubility measurements rigorously constrain the value of the solubility product of synthetic soddyite, and consequently its standard-state Gibbs free energy of formation. The log solubility product (lg K sp ) with its error (1σ) is (6.43 + 0.20/-0.37), and the standard-state Gibbs free energy of formation is (-3652.2 ± 4.2 (2σ)) kJ mol -1 . High-temperature drop solution calorimetry was conducted, yielding a calculated standard-state enthalpy of formation of soddyite of (-4045.4 ± 4.9 (2σ)) kJ . mol -1 . The standard-state Gibbs free energy and enthalpy of formation yield a calculated standard-state entropy of formation of soddyite of (-1318.7 ± 21.7 (2σ)) J . mol -1 . K -1 . The measurements and associated thermodynamic calculations not only describe the T = 298 K stability and solubility of soddyite, but they also can be used in predictions of repository performance through extrapolation of these properties to repository temperatures

  4. Test of calorimetry for high burn-up plutonium

    International Nuclear Information System (INIS)

    Beets, C.; Carchon, R.; Fettweis, P.

    1984-01-01

    In recent times, the interest of applying calorimetry for safeguards purpose is steadily increasing. Calorimetric measurements have been performed on a set of high burn-up (25000 MWd/t) Pu samples, ranging in mass between 60 g and 2.5 kg Pu, distributed as PuO 2 powder embedded in stainless steel containers. The powers produced by these containers ranged between 0.8 W and 36 W. The calorimeter used was the Mound 150 type, and the isotopics and the Am content have been determined earlier by mass spectroscopy, completed with α and γ counting, and were later verified by the same methods. Watts/gram measurements were made on twelve 60 g samples of the same plutonium lot to demonstrate the Pu elemental and isotopic homogeneity, and hence, its suitability for subsequent NDA experiments. These samples were also measured in a stacked way to fill up the mass and wattage gaps between 60 g (0.8W) and 1 kg (14W). Calorimetric assay values, obtained with both isotopic measurements are discussed

  5. Novel Technique for Quantitative Fast Scanning Calorimetry on Electrospun Fibers

    Science.gov (United States)

    Thomas, David; Govinna, Nelaka; Schick, Christoph; Cebe, Peggy

    Fast scanning chip calorimetry allows for the study of polymers which have rapid nucleation and/or crystallization kinetics, or degrade within their melting range. Heating rates used, up to 4000 K/s, allow studies of hetero and homogeneous nucleation at time scales inaccessible with conventional calorimeters, whose rates are typically alcohol (PVA) were chosen in the development of a new methodology to obtain quantitative fast scanning thermal data from electrospun nanofibers using a Flash DSC1. The structure of nanofibers requires special methods to load nanogram-sized samples onto a UFSC1 sensor. Fibers were directly spun onto TEM grids which provide a durable substrate to support bundles of nanofibers and possess excellent thermal conductivity allowing for a strong, repeatable signal and ensure good sample to sensor contact. As spun samples were held isothermally at temperatures ranging from Tg to Tm then heated at 2,000 K/s to assess as-spun crystallinity and cold crystallization behaviors. Above Tm the fibers break up into micro- and nano-droplets. On these samples, melt crystallization experiments were performed to study nucleation and crystallization of polymer confined to nanodroplet morphology. NSF DMR-1608125.

  6. Study of Liquid Argon Dopants for LHC Hadron Calorimetry

    CERN Multimedia

    2002-01-01

    Hadron calorimetry based on the Liquid Argon Ionisation Chamber technique is one of the choice techniques for LHC-experimentation. A systematic study of the effect of selected dopants on Liquid Argon (LAr) will be carried out with the aim to achieve an improvement on: \\item (i)~``Fast Liquid Argon'' search and study of dopants to increase the drift velocity. It has been already shown that CH&sub4. added at a fraction of one percent increases the drift velocity by a factor of two or more. \\item (ii)~``Compensated Liquid Argon'' search and study of dopants to increase the response to densely ionising particles, resulting in improved compensation, such as photosensitive dopants. \\end{enumerate}\\\\ \\\\ Monitoring of the parameters involved in understanding the response of a calorimeter is essential. In case of doped LAr, the charge yield, the non-saturated drift velocity and the electron lifetime in the liquid should be precisely and simultaneously monitored as they all vary with the level of dopant concentrati...

  7. Synthesis Polarimetry Calibration

    Science.gov (United States)

    Moellenbrock, George

    2017-10-01

    Synthesis instrumental polarization calibration fundamentals for both linear (ALMA) and circular (EVLA) feed bases are reviewed, with special attention to the calibration heuristics supported in CASA. Practical problems affecting modern instruments are also discussed.

  8. Thin-gap gas chambers for hadronic calorimetry

    Energy Technology Data Exchange (ETDEWEB)

    Mikenberg, G

    1988-03-01

    A new type of thin multiwire gas detector operating in a high gain mode has been developed. Its characteristics have been optimized for calorimetric use. The setup for mass production, quality control and calibration for the OPAL Pole Tip Calorimeter Chambers is presented as an application of such a device. Other possible applications as an electromagnetic presampler as well as its use in a high resolution calorimeter are also discussed.

  9. ORNL calibrations facility

    International Nuclear Information System (INIS)

    Berger, C.D.; Gupton, E.D.; Lane, B.H.; Miller, J.H.; Nichols, S.W.

    1982-08-01

    The ORNL Calibrations Facility is operated by the Instrumentation Group of the Industrial Safety and Applied Health Physics Division. Its primary purpose is to maintain radiation calibration standards for calibration of ORNL health physics instruments and personnel dosimeters. This report includes a discussion of the radioactive sources and ancillary equipment in use and a step-by-step procedure for calibration of those survey instruments and personnel dosimeters in routine use at ORNL

  10. Software requirements

    CERN Document Server

    Wiegers, Karl E

    2003-01-01

    Without formal, verifiable software requirements-and an effective system for managing them-the programs that developers think they've agreed to build often will not be the same products their customers are expecting. In SOFTWARE REQUIREMENTS, Second Edition, requirements engineering authority Karl Wiegers amplifies the best practices presented in his original award-winning text?now a mainstay for anyone participating in the software development process. In this book, you'll discover effective techniques for managing the requirements engineering process all the way through the development cy

  11. The 2007 ESO Instrument Calibration Workshop

    CERN Document Server

    Kaufer, Andreas; ESO Workshop

    2008-01-01

    The 2007 ESO Instrument Calibration workshop brought together more than 120 participants with the objective to a) foster the sharing of information, experience and techniques between observers, instrument developers and instrument operation teams, b) review the actual precision and limitations of the applied instrument calibration plans, and c) collect the current and future requirements by the ESO users. These present proceedings include the majority of the workshop’s contributions and document the status quo of instrument calibration at ESO in large detail. Topics covered are: Optical Spectro-Imagers, Optical Multi-Object Spectrographs, NIR and MIR Spectro-Imagers, High-Resolution Spectrographs, Integral Field Spectrographs, Adaptive Optics Instruments, Polarimetric Instruments, Wide Field Imagers, Interferometric Instruments as well as other crucial aspects such as data flow, quality control, data reduction software and atmospheric effects. It was stated in the workshop that "calibration is a life-long l...

  12. Software Reviews.

    Science.gov (United States)

    Dwyer, Donna; And Others

    1989-01-01

    Reviewed are seven software packages for Apple and IBM computers. Included are: "Toxicology"; "Science Corner: Space Probe"; "Alcohol and Pregnancy"; "Science Tool Kit Plus"; Computer Investigations: Plant Growth"; "Climatrolls"; and "Animal Watch: Whales." (CW)

  13. Software Reviews.

    Science.gov (United States)

    Davis, Shelly J., Ed.; Knaupp, Jon, Ed.

    1984-01-01

    Reviewed is computer software on: (1) classification of living things, a tutorial program for grades 5-10; and (2) polynomial practice using tiles, a drill-and-practice program for algebra students. (MNS)

  14. Software Reviews.

    Science.gov (United States)

    Miller, Anne, Ed.; Radziemski, Cathy, Ed.

    1988-01-01

    Three pieces of computer software are described and reviewed: HyperCard, to build and use varied applications; Iggy's Gnees, for problem solving with shapes in grades kindergarten-two; and Algebra Shop, for practicing skills and problem solving. (MNS)

  15. PACMAN: PRIMA astrometric instrument software

    Science.gov (United States)

    Abuter, Roberto; Sahlmann, Johannes; Pozna, Eszter

    2010-07-01

    The dual feed astrometric instrument software of PRIMA (PACMAN) that is currently being integrated at the VLTI will use two spatially modulated fringe sensor units and a laser metrology system to carry out differential astrometry. Its software and hardware compromises a distributed system involving many real time computers and workstations operating in a synchronized manner. Its architecture has been designed to allow the construction of efficient and flexible calibration and observation procedures. In parallel, a novel scheme of integrating M-code (MATLAB/OCTAVE) with standard VLT (Very Large Telescope) control software applications had to be devised in order to support numerically intensive operations and to have the capacity of adapting to fast varying strategies and algorithms. This paper presents the instrument software, including the current operational sequences for the laboratory calibration and sky calibration. Finally, a detailed description of the algorithms with their implementation, both under M and C code, are shown together with a comparative analysis of their performance and maintainability.

  16. COMPARISON OF METHODS FOR GEOMETRIC CAMERA CALIBRATION

    Directory of Open Access Journals (Sweden)

    J. Hieronymus

    2012-09-01

    Full Text Available Methods for geometric calibration of cameras in close-range photogrammetry are established and well investigated. The most common one is based on test-fields with well-known pattern, which are observed from different directions. The parameters of a distortion model are calculated using bundle-block-adjustment-algorithms. This methods works well for short focal lengths, but is essentially more problematic to use with large focal lengths. Those would require very large test-fields and surrounding space. To overcome this problem, there is another common method for calibration used in remote sensing. It employs measurements using collimator and a goniometer. A third calibration method uses diffractive optical elements (DOE to project holograms of well known pattern. In this paper these three calibration methods are compared empirically, especially in terms of accuracy. A camera has been calibrated with those methods mentioned above. All methods provide a set of distortion correction parameters as used by the photogrammetric software Australis. The resulting parameter values are very similar for all investigated methods. The three sets of distortion parameters are crosscompared against all three calibration methods. This is achieved by inserting the gained distortion parameters as fixed input into the calibration algorithms and only adjusting the exterior orientation. The RMS (root mean square of the remaining image coordinate residuals are taken as a measure of distortion correction quality. There are differences resulting from the different calibration methods. Nevertheless the measure is small for every comparison, which means that all three calibration methods can be used for accurate geometric calibration.

  17. Silk I and Silk II studied by fast scanning calorimetry

    Energy Technology Data Exchange (ETDEWEB)

    Cebe, Peggy; Partlow, Benjamin P.; Kaplan, David L.; Wurm, Andreas; Zhuravlev, Evgeny; Schick, Christoph

    2017-06-01

    Using fast scanning calorimetry (FSC), we investigated the glass transition and crystal melting of samples of B. mori silk fibroin containing Silk I and/or Silk II crystals. Due to the very short residence times at high temperatures during such measurements, thermal decomposition of silk protein can be significantly suppressed. FSC was performed at 2000 K/s using the Mettler Flash DSC1 on fibroin films with masses around 130–270 ng. Films were prepared with different crystalline fractions (ranging from 0.26 to 0.50) and with different crystal structures (Silk I, Silk II, or mixed) by varying the processing conditions. These included water annealing at different temperatures, exposure to 50% MeOH in water, or autoclaving. The resulting crystal structure was examined using wide angle X-ray scattering. Degree of crystallinity was evaluated from Fourier transform infrared (FTIR) spectroscopy and from analysis of the heat capacity increment at the glass transition temperature. Silk fibroin films prepared by water annealing at 25 °C were the least crystalline and had Silk I structure. FTIR and FSC studies showed that films prepared by autoclaving or 50% MeOH exposure were the most crystalline and had Silk II structure. Intermediate crystalline fraction and mixed Silk I/Silk II structures were found in films prepared by water annealing at 37 °C. FSC results indicate that Silk II crystals exhibit endotherms of narrower width and have higher mean melting temperature Tm(II) = 351 ± 2.6 °C, compared to Silk I crystals which melt at Tm(I) = 292 ± 3.8 °C. Films containing mixed Silk I/Silk II structure showed two clearly separated endothermic peaks. Evidence suggests that the two types of crystals melt separately and do not thermally interconvert on the extremely short time scale (0.065 s between onset and end of melting) of the FSC experiment.

  18. Laser-Driven Calorimetry Measurements of Petroleum and Biodiesel Fuels.

    Science.gov (United States)

    Presser, Cary; Nazarian, Ashot; Millo, Amit

    2018-02-01

    Thermochemical characteristics were determined for several National Institute of Standards and Technology standard-reference-material petroleum and biodiesel fuels, using a novel laser-heating calorimetry technique. Measurements focused on the sample thermal behavior, specific heat release rate, and total specific heat release. The experimental apparatus consists of a copper sphere-shaped reactor mounted within a chamber, along with laser-beam-steering optical components, gas-supply manifold, and a computer-controlled data-acquisition system. At the center of the reactor, liquid sample is injected onto a copper pan substrate that rests and is in contact with a fine-wire thermocouple. A second thermocouple is in contact with the inner reactor sphere surface. The reactor is heated from opposing sides by a continuous-wave, near-infrared laser to achieve nearly uniform sample temperature. The change in temperature with time (thermogram) is recorded for both thermocouples, and compared to a baseline thermogram (without liquid in the pan). The thermograms are then processed (using an equation for thermal energy conservation) for the thermochemical information of interest. The results indicated that the energy reaching the pan is dominated by radiative heat transfer processes, while the dominant thermal process for the reactor sphere is the stored (internal) thermal energy within the sphere material. Sufficient laser power is necessary to detect the fuel thermal-related characteristics, and the required power can differ from one fuel to another. With sufficient laser power, one can detect the preferential vaporization of the lighter and heavier fuel fractions. The total specific heat release obtained for the different conventional and biodiesel fuels used in this investigation were similar to the expected values available in the literature.

  19. Application of calorimetry and thermodynamics to critical problems in materials science

    International Nuclear Information System (INIS)

    Atake, Tooru

    2009-01-01

    Calorimetry and thermodynamic studies have long been playing a very important role in the research fields of fundamental science and technology. Some topics and examples of thermodynamics studies are given, and the details are explained on the basis of the present author's experience, focusing attention to application of adiabatic calorimetry and thermodynamics to solve critical problems in materials science: (1) condensed gas calorimetry and third law entropy, (2) phase transition and polymorphism in simple molecular crystals, (3) incommensurate phase transitions, (4) particle size effects on the phase transitions in ferroelectric/ferroelastic crystals, (5) relaxor ferroelectrics and multi-ferroics, and some other topics in materials science and technology

  20. Application of prediction of equilibrium to servo-controlled calorimetry measurements

    International Nuclear Information System (INIS)

    Mayer, R.L. II

    1987-01-01

    Research was performed to develop an endpoint prediction algorithm for use with calorimeters operating in the digital servo-controlled mode. The purpose of this work was to reduce calorimetry measurement times while maintaining the high degree of precision and low bias expected from calorimetry measurements. Data from routine operation of two calorimeters were used to test predictive models at each stage of development against time savings, precision, and robustness criteria. The results of the study indicated that calorimetry measurement times can be significantly reduced using this technique. The time savings is, however, dependent on parameters in the digital servo-control algorithm and on packaging characteristics of measured items

  1. Software reengineering

    Science.gov (United States)

    Fridge, Ernest M., III

    1991-01-01

    Today's software systems generally use obsolete technology, are not integrated properly with other software systems, and are difficult and costly to maintain. The discipline of reverse engineering is becoming prominent as organizations try to move their systems up to more modern and maintainable technology in a cost effective manner. JSC created a significant set of tools to develop and maintain FORTRAN and C code during development of the Space Shuttle. This tool set forms the basis for an integrated environment to re-engineer existing code into modern software engineering structures which are then easier and less costly to maintain and which allow a fairly straightforward translation into other target languages. The environment will support these structures and practices even in areas where the language definition and compilers do not enforce good software engineering. The knowledge and data captured using the reverse engineering tools is passed to standard forward engineering tools to redesign or perform major upgrades to software systems in a much more cost effective manner than using older technologies. A beta vision of the environment was released in Mar. 1991. The commercial potential for such re-engineering tools is very great. CASE TRENDS magazine reported it to be the primary concern of over four hundred of the top MIS executives.

  2. Particle Size (Sieving) and Enthalpy (Acid Calorimetry) Analysis of Single-Pull K East Basin Floor and Pit Sludges

    International Nuclear Information System (INIS)

    Bredt, P.R.; Delegard, C.H.; Schmidt, A.J.; Silvers, K.L.; Thornton, B.M.; Gano, S.

    2000-01-01

    This report presents the results of particle size analyses and calorimetry testing performed on selected single-pull sludge samples collected from the Hanford K East Basin between December 1998 and June 1999. The samples were collected as isolated cores predominantly from areas that had not been previously sampled (e.g., North Loadout Pit, Dummy Elevator Pit, Tech View Pit), or from areas in which the sludge composition had been altered since the last sampling (e.g., Weasel Pit). Particle size analyses were performed by washing wet sludge samples through a series of four sieves with openings of 250, 500, 1410, and 4000 microm. The loaded sieves were weighed before and after drying to obtain wet and dry particle size distributions. Knowledge of the particle size distribution is needed to design and predict the performance of the systems that will be used to retrieve, transport, and recover sludge. Also, sieving provides an opportunity to observe the components in the sludge. For example, during sieving of the sludge sample from the North Loadout Pit, significant quantities of organic ion exchange beads were observed. The uranium metal content and the particle size of the uranium metal in the K Basin sludge will largely determine the chemical reactivity of the sludge. In turn, the designs for the sludge handling and storage systems must be compatible with the reactivity of the sludge. Therefore, acid calorimetry was performed to estimate the uranium metal content of the sludge. For this testing, sludge samples were dissolved in nitric acid within a calibrated adiabatic calorimeter. The resulting dissolution enthalpy data were then used to discriminate between metallic uranium (minus3750 J/g in nitric acid) and uranium oxide (minus394 J/g in nitric acid). Results from this testing showed that the single-pull sludge samples contained little or no uranium metal

  3. Software Authentication

    International Nuclear Information System (INIS)

    Wolford, J.K.; Geelhood, B.D.; Hamilton, V.A.; Ingraham, J.; MacArthur, D.W.; Mitchell, D.J.; Mullens, J.A.; Vanier, P. E.; White, G.K.; Whiteson, R.

    2001-01-01

    The effort to define guidance for authentication of software for arms control and nuclear material transparency measurements draws on a variety of disciplines and has involved synthesizing established criteria and practices with newer methods. Challenges include the need to protect classified information that the software manipulates as well as deal with the rapid pace of innovation in the technology of nuclear material monitoring. The resulting guidance will shape the design of future systems and inform the process of authentication of instruments now being developed. This paper explores the technical issues underlying the guidance and presents its major tenets

  4. Software engineering

    CERN Document Server

    Thorin, Marc

    1985-01-01

    Software Engineering describes the conceptual bases as well as the main methods and rules on computer programming. This book presents software engineering as a coherent and logically built synthesis and makes it possible to properly carry out an application of small or medium difficulty that can later be developed and adapted to more complex cases. This text is comprised of six chapters and begins by introducing the reader to the fundamental notions of entities, actions, and programming. The next two chapters elaborate on the concepts of information and consistency domains and show that a proc

  5. Software compensation in Particle Flow reconstruction

    CERN Document Server

    Lan Tran, Huong; Sefkow, Felix; Green, Steven; Marshall, John; Thomson, Mark; Simon, Frank

    2017-01-01

    The Particle Flow approach to calorimetry requires highly granular calorimeters and sophisticated software algorithms in order to reconstruct and identify individual particles in complex event topologies. The high spatial granularity, together with analog energy information, can be further exploited in software compensation. In this approach, the local energy density is used to discriminate electromagnetic and purely hadronic sub-showers within hadron showers in the detector to improve the energy resolution for single particles by correcting for the intrinsic non-compensation of the calorimeter system. This improvement in the single particle energy resolution also results in a better overall jet energy resolution by improving the energy measurement of identified neutral hadrons and improvements in the pattern recognition stage by a more accurate matching of calorimeter energies to tracker measurements. This paper describes the software compensation technique and its implementation in Particle Flow reconstruct...

  6. SU-E-T-749: Thorough Calibration of MOSFET Dosimeters

    International Nuclear Information System (INIS)

    Plenkovich, D; Thomas, J

    2015-01-01

    Purpose: To improve the accuracy of the MOSFET calibration procedure by performing the measurement several times and calculating the average value of the calibration factor for various photon and electron energies. Methods: The output of three photon and six electron beams of Varian Trilogy linear accelerator SN 5878 was calibrated. Five reinforced standard sensitivity MOSFET dosimeters were placed in the calibration jig and connected to the Reader Module. As the backscatter material was used 7 cm of Virtual Water. The MOSFET dosimeters were covered with 1.5 cm thick bolus for the regular and SRS 6 MV beams, 3 cm bolus for 15 MV beam, 1.5 cm bolus for 6 MeV electron beam, and 2 cm bolus for the electron energies of 9, 12, 15, 18, and 22 MeV. The dosimeters were exposed to 100 MU, and the calibration factor was determined using the mobileMOSFET software. To improve the accuracy of calibration, this procedure was repeated ten times and the calibration factors were averaged. Results: As the number of calibrations was increasing the variability of calibration factors of different dosimeters was decreasing. After ten calibrations, the calibration factors for all five dosimeters were within 1% of one another for all energies, except 6 MV SRS photons and 6 MeV electrons, for which the variability was 2%. Conclusions: The described process results in calibration factors which are almost independent of modality or energy. Once calibrated, the dosimeters may be used for in-vivo dosimetry or for daily verification of the beam output. Measurement of the radiation dose under bolus and scatter to the eye are examples of frequent use of calibrated MOSFET dosimeters. The calibration factor determined for full build-up is used under these circumstances. To the best of our knowledge, such thorough procedure for calibrating MOSFET dosimeters has not been reported previously. Best Medical Canada provided MOSFET dosimeters for this project

  7. Beam-based calibration system of BPM offset on BEPC

    International Nuclear Information System (INIS)

    Hu Chunliang

    2004-01-01

    The ever-increasing demand for better performance from circular accelerators requires improved methods to calibrate beam position monitors (BPM). A beam based calibration system has been established to locate the centers of the BPM with respect to the magnetic center of quadrupole magnets. Additional windings are applied to the quadrupole magnets to make the quadrupole magnetic strength individually adjustable and the number of the power supply of all 32 additional windings is only one. Software system has been finished to automatically measure the offsets of BPMs. The effect of the beam-based calibration system shows that the calibration of BPM has been more quickly and accurately

  8. Calibration of Flick standards

    International Nuclear Information System (INIS)

    Thalmann, Ruedi; Spiller, Jürg; Küng, Alain; Jusko, Otto

    2012-01-01

    Flick standards or magnification standards are widely used for an efficient and functional calibration of the sensitivity of form measuring instruments. The results of a recent measurement comparison have shown to be partially unsatisfactory and revealed problems related to the calibration of these standards. In this paper the influence factors for the calibration of Flick standards using roundness measurement instruments are discussed in detail, in particular the bandwidth of the measurement chain, residual form errors of the device under test, profile distortions due to the diameter of the probing element and questions related to the definition of the measurand. The different contributions are estimated using simulations and are experimentally verified. Also alternative methods to calibrate Flick standards are investigated. Finally the practical limitations of Flick standard calibration are shown and the usability of Flick standards both to calibrate the sensitivity of roundness instruments and to check the filter function of such instruments is analysed. (paper)

  9. ALMA software architecture

    Science.gov (United States)

    Schwarz, Joseph; Raffi, Gianni

    2002-12-01

    The Atacama Large Millimeter Array (ALMA) is a joint project involving astronomical organizations in Europe and North America. ALMA will consist of at least 64 12-meter antennas operating in the millimeter and sub-millimeter range. It will be located at an altitude of about 5000m in the Chilean Atacama desert. The primary challenge to the development of the software architecture is the fact that both its development and runtime environments will be distributed. Groups at different institutes will develop the key elements such as Proposal Preparation tools, Instrument operation, On-line calibration and reduction, and Archiving. The Proposal Preparation software will be used primarily at scientists' home institutions (or on their laptops), while Instrument Operations will execute on a set of networked computers at the ALMA Operations Support Facility. The ALMA Science Archive, itself to be replicated at several sites, will serve astronomers worldwide. Building upon the existing ALMA Common Software (ACS), the system architects will prepare a robust framework that will use XML-encoded entity objects to provide an effective solution to the persistence needs of this system, while remaining largely independent of any underlying DBMS technology. Independence of distributed subsystems will be facilitated by an XML- and CORBA-based pass-by-value mechanism for exchange of objects. Proof of concept (as well as a guide to subsystem developers) will come from a prototype whose details will be presented.

  10. Parallelism between gradient temperature raman spectroscopy and differential scanning calorimetry results

    Science.gov (United States)

    Temperature dependent Raman spectroscopy (TDR) applies the temperature gradients utilized in differential scanning calorimetry (DSC) to Raman spectroscopy, providing a straightforward technique to identify molecular rearrangements that occur just prior to phase transitions. Herein we apply TDR and D...

  11. Reviews, Software.

    Science.gov (United States)

    Science Teacher, 1988

    1988-01-01

    Reviews two computer software packages for use in physical science, physics, and chemistry classes. Includes "Physics of Model Rocketry" for Apple II, and "Black Box" for Apple II and IBM compatible computers. "Black Box" is designed to help students understand the concept of indirect evidence. (CW)

  12. Software Reviews.

    Science.gov (United States)

    Kinnaman, Daniel E.; And Others

    1988-01-01

    Reviews four educational software packages for Apple, IBM, and Tandy computers. Includes "How the West was One + Three x Four,""Mavis Beacon Teaches Typing,""Math and Me," and "Write On." Reviews list hardware requirements, emphasis, levels, publisher, purchase agreements, and price. Discusses the strengths…

  13. Software Review.

    Science.gov (United States)

    McGrath, Diane, Ed.

    1989-01-01

    Reviewed is a computer software package entitled "Audubon Wildlife Adventures: Grizzly Bears" for Apple II and IBM microcomputers. Included are availability, hardware requirements, cost, and a description of the program. The murder-mystery flavor of the program is stressed in this program that focuses on illegal hunting and game…

  14. Software Reviews.

    Science.gov (United States)

    Teles, Elizabeth, Ed.; And Others

    1990-01-01

    Reviewed are two computer software packages for Macintosh microcomputers including "Phase Portraits," an exploratory graphics tool for studying first-order planar systems; and "MacMath," a set of programs for exploring differential equations, linear algebra, and other mathematical topics. Features, ease of use, cost, availability, and hardware…

  15. MIAWARE Software

    DEFF Research Database (Denmark)

    Wilkowski, Bartlomiej; Pereira, Oscar N. M.; Dias, Paulo

    2008-01-01

    is automatically generated. Furthermore, MIAWARE software is accompanied with an intelligent search engine for medical reports, based on the relations between parts of the lungs. A logical structure of the lungs is introduced to the search algorithm through the specially developed ontology. As a result...

  16. Determination of Differential Enthalpy and Isotherm by Adsorption Calorimetry

    Directory of Open Access Journals (Sweden)

    V. Garcia-Cuello

    2008-01-01

    Full Text Available An adsorption microcalorimeter for the simultaneous determination of the differential heat of adsorption and the adsorption isotherm for gas-solid systems are designed, built, and tested. For this purpose, a Calvet heat-conducting microcalorimeter is developed and is connected to a gas volumetric unit built in stainless steel to record adsorption isotherms. The microcalorimeter is electrically calibrated to establish its sensitivity and reproducibility, obtaining K=154.34±0.23 WV−1. The adsorption microcalorimeter is used to obtain adsorption isotherms and the corresponding differential heats for the adsorption of CO2 on a reference solid, such as a NaZSM-5 type zeolite. Results for the behavior of this system are compared with those obtained with commercial equipment and with other studies in the literature.

  17. Characterization of indoor and outdoor pool fires with active calorimetry

    International Nuclear Information System (INIS)

    Koski, J.A.; Gill, W.; Gritzo, L.A.; Kent, L.A.; Wix, S.D.

    1994-01-01

    A water cooled, 1 m x 1 m, vertical calorimeter panel has been used in conjunction with other fire diagnostics to characterize a 6 m x 6 m outdoor and three 3 m x 3 m indoor JP-4 pool fires. Measurements reported include calorimeter surface heat flux and surface temperatures, flame temperatures, and gas flow velocities in the fire. From the data, effective radiative absorption coefficients for various zones in the fires have been estimated. The outdoor test was conducted at Sandia's Coyote Canyon test facility, while indoor tests were conducted at the indoor SMokE Reduction Facility (SMERF) at the same location. The measurements provide data useful in calibrating simple analytic fire models intended for the analysis of packages containing hazardous materials

  18. Micro-combustion calorimetry employing a Calvet heat flux calorimeter

    International Nuclear Information System (INIS)

    Rojas-Aguilar, Aaron; Valdes-Ordonez, Alejandro

    2004-01-01

    Two micro-combustion bombs developed from a high pressure stainless steel vessel have been adapted to a Setaram C80 Calvet calorimeter. The constant of each micro-bomb was determined by combustions with benzoic acid NIST 39j, giving for the micro-combustion bomb in the measurement sensor k m =(1.01112±0.00054) and for the micro-combustion bomb in the reference sensor k r =(1.00646±0.00059) which means an uncertainty of less than 0.06 per cent for calibration. The experimental methodology to get results of combustion energy of organic compounds with a precision also better than 0.06 per cent is described by applying this micro-combustion device to the measurement of the enthalpy of combustion of the succinic acid, giving Δ c H compfn m (cr, T=298.15 K)=-(1492.89 ± 0.77) kJ · mol -1

  19. RF impedance measurement calibration

    International Nuclear Information System (INIS)

    Matthews, P.J.; Song, J.J.

    1993-01-01

    The intent of this note is not to explain all of the available calibration methods in detail. Instead, we will focus on the calibration methods of interest for RF impedance coupling measurements and attempt to explain: (1). The standards and measurements necessary for the various calibration techniques. (2). The advantages and disadvantages of each technique. (3). The mathematical manipulations that need to be applied to the measured standards and devices. (4). An outline of the steps needed for writing a calibration routine that operated from a remote computer. For further details of the various techniques presented in this note, the reader should consult the references

  20. Enzyme-catalyzed and binding reaction kinetics determined by titration calorimetry.

    Science.gov (United States)

    Hansen, Lee D; Transtrum, Mark K; Quinn, Colette; Demarse, Neil

    2016-05-01

    Isothermal calorimetry allows monitoring of reaction rates via direct measurement of the rate of heat produced by the reaction. Calorimetry is one of very few techniques that can be used to measure rates without taking a derivative of the primary data. Because heat is a universal indicator of chemical reactions, calorimetry can be used to measure kinetics in opaque solutions, suspensions, and multiple phase systems and does not require chemical labeling. The only significant limitation of calorimetry for kinetic measurements is that the time constant of the reaction must be greater than the time constant of the calorimeter which can range from a few seconds to a few minutes. Calorimetry has the unique ability to provide both kinetic and thermodynamic data. This article describes the calorimetric methodology for determining reaction kinetics and reviews examples from recent literature that demonstrate applications of titration calorimetry to determine kinetics of enzyme-catalyzed and ligand binding reactions. A complete model for the temperature dependence of enzyme activity is presented. A previous method commonly used for blank corrections in determinations of equilibrium constants and enthalpy changes for binding reactions is shown to be subject to significant systematic error. Methods for determination of the kinetics of enzyme-catalyzed reactions and for simultaneous determination of thermodynamics and kinetics of ligand binding reactions are reviewed. Copyright © 2015 Elsevier B.V. All rights reserved.

  1. Development of a software for the curimeter model cdn102

    International Nuclear Information System (INIS)

    Dotres Llera, Armando

    2001-01-01

    The characteristics of the software for the Curimeter Model CD-N102 developed at CEADEN are presented. The software consists of two main parts: a basic software for the electrometer block and an application software for a P C. The basic software is totally independent of the Pc and performs all the basic functions of the process of measurement. The application software is optional and offers a friendlier interface and additional options to the user. Among these is the possibility to keep a statistical record of the measurements in a database, to create labels and to introduce new isotopes and calibrate them. A more detailed explanation of both software is given

  2. Effect of Body Position on Energy Expenditure of Preterm Infants as Determined by Simultaneous Direct and Indirect Calorimetry.

    Science.gov (United States)

    Bell, Edward F; Johnson, Karen J; Dove, Edwin L

    2017-04-01

    Background  Indirect calorimetry is the standard method for estimating energy expenditure in clinical research. Few studies have evaluated indirect calorimetry in infants by comparing it with simultaneous direct calorimetry. Our purpose was (1) to compare the energy expenditure of preterm infants determined by these two methods, direct calorimetry and indirect calorimetry; and (2) to examine the effect of body position, supine or prone, on energy expenditure. Study Design  We measured energy expenditure by simultaneous direct (heat loss by gradient-layer calorimeter corrected for heat storage) and indirect calorimetry (whole-body oxygen consumption and carbon dioxide production) in 15 growing preterm infants during two consecutive interfeeding intervals, once in the supine position and once in the prone position. Results  The mean energy expenditure for all measurements in both positions did not differ significantly by the method used: 2.82 (standard deviation [SD] 0.42) kcal/kg/h by direct calorimetry and 2.78 (SD 0.48) kcal/kg/h by indirect calorimetry. The energy expenditure was significantly lower, by 10%, in the prone than in the supine position, whether examined by direct calorimetry (2.67 vs. 2.97 kcal/kg/h, p  Direct calorimetry and indirect calorimetry gave similar estimates of energy expenditure. Energy expenditure was 10% lower in the prone position than in the supine position. Thieme Medical Publishers 333 Seventh Avenue, New York, NY 10001, USA.

  3. Search for the scalar partner of the top quark and contribution to the improvement of the calorimetry of the experiment D zero for the phase 2 of Tevatron; Recherche du partenaire supersymetrique du quark top et contribution a l'amelioration de la calorimetrie de l'experience D zero pour la phase 2 du tevatron

    Energy Technology Data Exchange (ETDEWEB)

    Olivier, B

    2001-04-01

    thus also describe in this thesis our contribution to the calorimeter upgrade, both on the on-line calibration system, and on the calorimeter reconstruction software. (authors)

  4. Picowatt Resolution Calorimetry for Micro and Nanoscale Energy Transport Studies

    Science.gov (United States)

    Sadat, Seid H.

    Precise quantification of energy transport is key to obtaining insights into a wide range of phenomena across various disciplines including physics, chemistry, biology and engineering. This thesis describes technical advancements into heat-flow calorimetry which enable measurement of energy transport at micro and nanoscales with picowatt resolution. I have developed two types of microfabricated calorimeter devices and demonstrated single digit picowatt resolution at room temperature. Both devices incorporate two distinct features; an active area isolated by a thermal conductance (GTh) of less than 1 microW/K and a high resolution thermometer with temperature resolution (DeltaTres) in the micro kelvin regime. These features enable measurements of heat currents (q) with picowatt resolution (q= Th xDeltaTres). In the first device the active area is suspended via silicon nitride beams with excellent thermal isolation (~600 nW/K) and a bimaterial cantilever (BMC) thermometer with temperature resolution of ~6 microK. Taken together this design enabled calorimetric measurements with 4 pW resolution. In the second device, the BMC thermometry technique is replaced by a high-resolution resistance thermometry scheme. A detailed noise analysis of resistance thermometers, confirmed by experimental data, enabled me to correctly predict the resolution of different measurement schemes and propose techniques to achieve an order of magnitude improvement in the resolution of resistive thermometers. By incorporating resistance thermometers with temperature resolution of ~30 microK, combined with a thermal isolation of ~150 nW/K, I demonstrated an all-electrical calorimeter device with a resolution of ~ 5 pW. Finally, I used these calorimeters to study Near-Field Radiative Heat Transfer (NF-RHT). Using these devices, we studied--for the first time--the effect of film thickness on the NF-RHT between two dielectric surfaces. We showed that even a very thin film (~50 nm) of silicon

  5. Silk I and Silk II studied by fast scanning calorimetry.

    Science.gov (United States)

    Cebe, Peggy; Partlow, Benjamin P; Kaplan, David L; Wurm, Andreas; Zhuravlev, Evgeny; Schick, Christoph

    2017-06-01

    Using fast scanning calorimetry (FSC), we investigated the glass transition and crystal melting of samples of B. mori silk fibroin containing Silk I and/or Silk II crystals. Due to the very short residence times at high temperatures during such measurements, thermal decomposition of silk protein can be significantly suppressed. FSC was performed at 2000K/s using the Mettler Flash DSC1 on fibroin films with masses around 130-270ng. Films were prepared with different crystalline fractions (ranging from 0.26 to 0.50) and with different crystal structures (Silk I, Silk II, or mixed) by varying the processing conditions. These included water annealing at different temperatures, exposure to 50%MeOH in water, or autoclaving. The resulting crystal structure was examined using wide angle X-ray scattering. Degree of crystallinity was evaluated from Fourier transform infrared (FTIR) spectroscopy and from analysis of the heat capacity increment at the glass transition temperature. Silk fibroin films prepared by water annealing at 25°C were the least crystalline and had Silk I structure. FTIR and FSC studies showed that films prepared by autoclaving or 50%MeOH exposure were the most crystalline and had Silk II structure. Intermediate crystalline fraction and mixed Silk I/Silk II structures were found in films prepared by water annealing at 37°C. FSC results indicate that Silk II crystals exhibit endotherms of narrower width and have higher mean melting temperature T m (II)=351±2.6°C, compared to Silk I crystals which melt at T m (I)=292±3.8°C. Films containing mixed Silk I/Silk II structure showed two clearly separated endothermic peaks. Evidence suggests that the two types of crystals melt separately and do not thermally interconvert on the extremely short time scale (0.065s between onset and end of melting) of the FSC experiment. Silkworm silk is a naturally occurring biomaterial. The fibroin component of silk forms two types of crystals. Silk properties depend upon the

  6. Software Tools for Software Maintenance

    Science.gov (United States)

    1988-10-01

    COMMUNICATIONS, AND COMPUTER SCIENCES I ,(AIRMICS) FO~SOFTWARE TOOLS (.o FOR SOF1 ’ARE MAINTENANCE (ASQBG-1-89-001) October, 1988 DTIC ELECTE -ifB...SUNWW~. B..c Program An~Iysw HA.c C-Tractr C Cobol Stncturing Facility VS Cobol 11 F-Scan Foctma Futbol Cobol Fortran Sltiuc Code Anaiyaer Fortran IS

  7. Calibration of moisture monitors

    International Nuclear Information System (INIS)

    Gutierrez, R.L.

    1979-02-01

    A method for calibrating an aluminum oxide hygrometer against an optical chilled mirror dew-point hygrometer has been established. A theoretical cross-point line of dew points from both hygrometers and a maximum moisture content of 10 ppM/sub v/ are used to define an area for calibrating the sensor probes of the aluminum oxide hygrometer

  8. Site Calibration report

    DEFF Research Database (Denmark)

    Yordanova, Ginka; Vesth, Allan

    The report describes site calibration measurements carried out on a site in Denmark. The measurements are carried out in accordance to Ref. [1]. The site calibration is carried out before a power performance measurement on a given turbine to clarify the influence from the terrain on the ratio...

  9. Topics in Statistical Calibration

    Science.gov (United States)

    2014-03-27

    Natural cubic spline speed di st 110 B.2 The calibrate function The most basic calibration problem, the one often encountered in more advanced ...0040-1706, 1537-2723. A. M. Mood, F. A. Graybill, and D. C. Boes. Introduction to the Theory of Statistics. McGraw-Hill, Auckland , U.A, 1974. ISBN

  10. EPIQR software

    Energy Technology Data Exchange (ETDEWEB)

    Flourentzos, F. [Federal Institute of Technology, Lausanne (Switzerland); Droutsa, K. [National Observatory of Athens, Athens (Greece); Wittchen, K.B. [Danish Building Research Institute, Hoersholm (Denmark)

    1999-11-01

    The support of the EPIQR method is a multimedia computer program. Several modules help the users of the method to treat the data collected during a diagnosis survey, to set up refurbishment scenario and calculate their cost or energy performance, and finally to visualize the results in a comprehensive way and to prepare quality reports. This article presents the structure and the main features of the software. (au)

  11. Software preservation

    Directory of Open Access Journals (Sweden)

    Tadej Vodopivec

    2011-01-01

    Full Text Available Comtrade Ltd. covers a wide range of activities related to information and communication technologies; its deliverables include web applications, locally installed programs,system software, drivers, embedded software (used e.g. in medical devices, auto parts,communication switchboards. Also the extensive knowledge and practical experience about digital long-term preservation technologies have been acquired. This wide spectrum of activities puts us in the position to discuss the often overlooked aspect of the digital preservation - preservation of software programs. There are many resources dedicated to digital preservation of digital data, documents and multimedia records,but not so many about how to preserve the functionalities and features of computer programs. Exactly these functionalities - dynamic response to inputs - render the computer programs rich compared to documents or linear multimedia. The article opens the questions on the beginning of the way to the permanent digital preservation. The purpose is to find a way in the right direction, where all relevant aspects will be covered in proper balance. The following questions are asked: why at all to preserve computer programs permanently, who should do this and for whom, when we should think about permanent program preservation, what should be persevered (such as source code, screenshots, documentation, and social context of the program - e.g. media response to it ..., where and how? To illustrate the theoretic concepts given the idea of virtual national museum of electronic banking is also presented.

  12. Sandia WIPP calibration traceability

    Energy Technology Data Exchange (ETDEWEB)

    Schuhen, M.D. [Sandia National Labs., Albuquerque, NM (United States); Dean, T.A. [RE/SPEC, Inc., Albuquerque, NM (United States)

    1996-05-01

    This report summarizes the work performed to establish calibration traceability for the instrumentation used by Sandia National Laboratories at the Waste Isolation Pilot Plant (WIPP) during testing from 1980-1985. Identifying the calibration traceability is an important part of establishing a pedigree for the data and is part of the qualification of existing data. In general, the requirement states that the calibration of Measuring and Test equipment must have a valid relationship to nationally recognized standards or the basis for the calibration must be documented. Sandia recognized that just establishing calibration traceability would not necessarily mean that all QA requirements were met during the certification of test instrumentation. To address this concern, the assessment was expanded to include various activities.

  13. Sandia WIPP calibration traceability

    International Nuclear Information System (INIS)

    Schuhen, M.D.; Dean, T.A.

    1996-05-01

    This report summarizes the work performed to establish calibration traceability for the instrumentation used by Sandia National Laboratories at the Waste Isolation Pilot Plant (WIPP) during testing from 1980-1985. Identifying the calibration traceability is an important part of establishing a pedigree for the data and is part of the qualification of existing data. In general, the requirement states that the calibration of Measuring and Test equipment must have a valid relationship to nationally recognized standards or the basis for the calibration must be documented. Sandia recognized that just establishing calibration traceability would not necessarily mean that all QA requirements were met during the certification of test instrumentation. To address this concern, the assessment was expanded to include various activities

  14. Differential Scanning Calorimetry and Thermodynamic Predictions—A Comparative Study of Al-Zn-Mg-Cu Alloys

    Directory of Open Access Journals (Sweden)

    Gernot K.-H. Kolb

    2016-08-01

    Full Text Available Al-Zn-Mg-Cu alloys are widely used in aircraft applications because of their superior mechanical properties and strength/weight ratios. Commercial Al-Zn-Mg-Cu alloys have been intensively studied over the last few decades. However, well-considered thermodynamic calculations, via the CALPHAD approach, on a variation of alloying elements can guide the fine-tuning of known alloy systems and the development of optimized heat treatments. In this study, a comparison was made of the solidus temperatures of different Al-Zn-Mg-Cu alloys determined from thermodynamic predictions and differential scanning calorimetry (DSC measurements. A variation of the main alloying elements Zn, Mg, and Cu generated 38 experimentally produced alloys. An experimental determination of the solidus temperature via DSC was carried out according to a user-defined method, because the broad melting interval present in Al-Zn-Mg-Cu alloys does not allow the use of the classical onset method for pure substances. The software algorithms implemented in FactSage®, Pandat™, and MatCalc with corresponding commercially available databases were deployed for thermodynamic predictions. Based on these investigations, the predictive power of the commercially available CALPHAD databases and software packages was critically reviewed.

  15. Calorimetry of the JET ITER-Like Wall components

    Energy Technology Data Exchange (ETDEWEB)

    Devaux, S., E-mail: stephane.devaux@ccfe.ac.uk [Max-Planck-Institut für Plasmaphysik, EURATOM-Assoziation, D-85748 Garching (Germany); Arnoux, G. [EURATOM/CCFE Association, Culham Science Center, Abingdon, Oxon OX14 3DB (United Kingdom); Corre, Y. [Association EURTATOM-CEA, CEA/DSM/IRFM, Cadarache, 13108 Saint Paul lez Durance (France); Gardarein, J-L.; Gaspar, J. [IUSTI UMR CNRS 7343, Aix-Marseille University Marseille (France); Jacquet, P. [Max-Planck-Institut für Plasmaphysik, EURATOM-Assoziation, D-85748 Garching (Germany); Marcotte, F. [EURATOM/CCFE Association, Culham Science Center, Abingdon, Oxon OX14 3DB (United Kingdom); Matthews, G.; Beaumont, P.; Cramp, S.; Dalley, S.; Kinna, D.; Horton, A.; Lomas, P. [Max-Planck-Institut für Plasmaphysik, EURATOM-Assoziation, D-85748 Garching (Germany); Mertens, Ph. [Institute of Energy and Climate Research IEK-4 (Plasma Physics), Forschungszentrum Jülich GmbH, Association EURATOM-FZJ, D-52425 Jülich (Germany); Riccardo, V. [Max-Planck-Institut für Plasmaphysik, EURATOM-Assoziation, D-85748 Garching (Germany); Valcàrcel, D. [Associação EURATOM/IST, Instituto de Plasmas e Fusão Nuclear, Instituto Superior Técnico, Universidade Técnica de Lisboa, P-1049-001 Lisboa (Portugal)

    2013-07-15

    As part of the ILW project, new diagnostics have been installed in order to protect the plasma-facing components (PFCs). Here we present the diagnostics used to monitor the PFC temperature, thermocouples and cameras, and assess the consistency of their measurements. In dedicated limited L-mode plasmas, the surface of the limiter tiles are heated up to 900 °C. The comparison of surface temperature measurements from IR and near IR cameras, which have been calibrated against a black-body source, leads to a Be emissivity of 0.18, comparable with the theoretical one. Energy calculation derived from thermocouples, which are embedded in both limiters and divertor target plates (W-coated CFC), is compared to a 1D model based on thermal quadrupole approach (benchmarked with an ANSYS model) associated to an inversion computation. The analysis of 20 pulses shows that a good energy balance is achieved within the error bar of the model, assessed to be of 30%.

  16. Calorimetry of the JET ITER-Like Wall components

    International Nuclear Information System (INIS)

    Devaux, S.; Arnoux, G.; Corre, Y.; Gardarein, J-L.; Gaspar, J.; Jacquet, P.; Marcotte, F.; Matthews, G.; Beaumont, P.; Cramp, S.; Dalley, S.; Kinna, D.; Horton, A.; Lomas, P.; Mertens, Ph.; Riccardo, V.; Valcàrcel, D.

    2013-01-01

    As part of the ILW project, new diagnostics have been installed in order to protect the plasma-facing components (PFCs). Here we present the diagnostics used to monitor the PFC temperature, thermocouples and cameras, and assess the consistency of their measurements. In dedicated limited L-mode plasmas, the surface of the limiter tiles are heated up to 900 °C. The comparison of surface temperature measurements from IR and near IR cameras, which have been calibrated against a black-body source, leads to a Be emissivity of 0.18, comparable with the theoretical one. Energy calculation derived from thermocouples, which are embedded in both limiters and divertor target plates (W-coated CFC), is compared to a 1D model based on thermal quadrupole approach (benchmarked with an ANSYS model) associated to an inversion computation. The analysis of 20 pulses shows that a good energy balance is achieved within the error bar of the model, assessed to be of 30%

  17. Enhanced thermal property measurement of a silver zinc battery cell using isothermal calorimetry

    Energy Technology Data Exchange (ETDEWEB)

    Ubelhor, Ryan, E-mail: ryan.ubelhor@navy.mil [Naval Surface Warfare Center, Crane Division, 300 Highway 361, Crane, IN 47522 (United States); Ellison, Daniel [Science Applications International Corporation, 300 Highway 361, Crane, IN 47522 (United States); Pierce, Cecilia [Naval Surface Warfare Center, Crane Division, 300 Highway 361, Crane, IN 47522 (United States)

    2015-04-20

    Highlights: • Design and construction of novel heat flow calorimeter for large battery cell. • Heat flow characterization of silver zinc battery under load. • Thermal efficiency determination of silver zinc battery under load. • Surface map of heat flow of silver zinc battery under load. - Abstract: The push for increased energy density of electrochemical cells highlights the need for novel electrochemical techniques as well as additional characterization methods for these cells in order to meet user needs and safety requirements. To achieve ever increasing energy densities and faster controlled release of that energy, all materials of construction must be constantly evaluated from electrode to casing and everything in-between. Increasing the energy density of the cell improves its utility, but it also increases the waste heat and maximum potential uncontrolled energy release. Design agents and system developers need new ways to monitor and classify the probability and severity of the catastrophic failures as well as the system characteristics during intended operation. To support optimization of these battery cells it is necessary to understand their thermal characteristics at rest as well as under prescribed charge and discharge cycles. One of the many calorimetric tools available to observe and record these characteristics is heat flow calorimetry. Typically, a heat flow calorimeter is operated isothermally and measures the sum heat released or consumed by a sample material inside of a calorimetric measuring cell. For this study an improved calorimetric measuring cell for a modified Hart 6209 precision temperature bath was designed and constructed to measure the heat flow of larger electrochemical cells (18 × 8 × 16 cm). This new calorimetric measuring cell is constructed to allow independent measurements of heat flow among each of the sample’s six sides in contrast to the typical one measurement of the average heat flow. Heat flows from 0.01 to 7

  18. Enhanced thermal property measurement of a silver zinc battery cell using isothermal calorimetry

    International Nuclear Information System (INIS)

    Ubelhor, Ryan; Ellison, Daniel; Pierce, Cecilia

    2015-01-01

    Highlights: • Design and construction of novel heat flow calorimeter for large battery cell. • Heat flow characterization of silver zinc battery under load. • Thermal efficiency determination of silver zinc battery under load. • Surface map of heat flow of silver zinc battery under load. - Abstract: The push for increased energy density of electrochemical cells highlights the need for novel electrochemical techniques as well as additional characterization methods for these cells in order to meet user needs and safety requirements. To achieve ever increasing energy densities and faster controlled release of that energy, all materials of construction must be constantly evaluated from electrode to casing and everything in-between. Increasing the energy density of the cell improves its utility, but it also increases the waste heat and maximum potential uncontrolled energy release. Design agents and system developers need new ways to monitor and classify the probability and severity of the catastrophic failures as well as the system characteristics during intended operation. To support optimization of these battery cells it is necessary to understand their thermal characteristics at rest as well as under prescribed charge and discharge cycles. One of the many calorimetric tools available to observe and record these characteristics is heat flow calorimetry. Typically, a heat flow calorimeter is operated isothermally and measures the sum heat released or consumed by a sample material inside of a calorimetric measuring cell. For this study an improved calorimetric measuring cell for a modified Hart 6209 precision temperature bath was designed and constructed to measure the heat flow of larger electrochemical cells (18 × 8 × 16 cm). This new calorimetric measuring cell is constructed to allow independent measurements of heat flow among each of the sample’s six sides in contrast to the typical one measurement of the average heat flow. Heat flows from 0.01 to 7

  19. MO-AB-BRA-03: Calorimetry-Based Absorbed Dose to Water Measurements Using Interferometry

    Energy Technology Data Exchange (ETDEWEB)

    Flores-Martinez, E; Malin, M; DeWerd, L [University of WI-Madison/ADCL, Madison, WI (United States)

    2015-06-15

    Purpose: Interferometry-based calorimetry is a novel technique to measure radiation-induced temperature changes allowing the measurement of absorbed dose to water (ADW). There are no mechanical components in the field. This technique also has the possibility of obtaining 2D dose distributions. The goal of this investigation is to calorimetrically-measure doses between 2.5 and 5 Gy over a single projection in a photon beam using interferometry and compare the results with doses calculated using the TG-51 linac calibration. Methods: ADW was determined by measuring radiation-induced phase shifts (PSs) of light passing through water irradiated with a 6 MV photon beam. A 9×9×9 cm{sup 3} glass phantom filled with water and placed in an arm of a Michelson interferometer was irradiated with 300, 400, 500 and 600 monitor units. The whole system was thermally insulated to achieve sufficient passive temperature control. The depth of measurement was 4.5 cm with a field size of 7×7 cm{sup 2}. The intensity of the fringe pattern was monitored with a photodiode and used to calculate the time-dependent PS curve. Data was acquired 60 s before and after the irradiation. The radiation-induced PS was calculated by taking the difference in the pre- and post-irradiation drifts extrapolated to the midpoint of the irradiation. Results were compared to computed doses. Results: Average comparison of calculated ADW values with interferometry-measured values showed an agreement to within 9.5%. k=1 uncertainties were 4.3% for calculations and 14.7% for measurements. The dominant source of uncertainty for the measurements was a temperature drift of about 30 µK/s caused by heat conduction from the interferometer’s surroundings. Conclusion: This work presented the first absolute ADW measurements using interferometry in the dose range of linac-based radiotherapy. Future work to improve measurements’ reproducibility includes the implementation of active thermal control techniques.

  20. Establishing software quality assurance

    International Nuclear Information System (INIS)

    Malsbury, J.

    1983-01-01

    This paper is concerned with four questions about establishing software QA: What is software QA. Why have software QA. What is the role of software QA. What is necessary to ensure the success of software QA

  1. Energy calibration of the barrel calorimeter of the CMD-3 detector

    International Nuclear Information System (INIS)

    Anisenkov, A.V.; Aulchenko, V.M.; Bashtovoy, N.S.; Bondar, A.E.; Grebenuk, A.A.; Epifanov, D.A.; Epshteyn, L.B.; Erofeev, A.L.; Kovalenko, O.A.; Kozyrev, A.N.; Kuzmin, A.S.; Mikhailov, K.Yu.; Logashenko, I.B.; Razuvaev, G.P.; Ruban, A.A.; Shebalin, V.E.; Shwartz, B.A.; Talyshev, A.A.; Titov, V.M.; Yudin, Yu.V.

    2017-01-01

    The VEPP-2000 e + e − collider has been operated in the Budker Institute of Nuclear Physics since 2010. Experiments are carried out with two detectors CMD-3 and SND. The calorimetry at the CMD-3 detector is based on three subsystems, two coaxial barrel calorimeters—Liquid Xenon calorimeter and crystal CsI calorimeter, and end cap calorimeter with BGO crystals. This paper describes the procedures of the energy calibration of the combined barrel calorimeter of the CMD-3 detector.

  2. INDIRECT CALORIMETRY DURING ULTRADISTANCE RUNNING: A CASE REPORT

    Directory of Open Access Journals (Sweden)

    Charles L. Dumke

    2006-12-01

    Full Text Available The purpose was to determine the energy expenditure during ultradistance trail running. A portable metabolic unit was carried by a male subject for the first 64.5 km portion of the Western States 100 running race. Calibrations were done with known gases and volumes at ambient temperature, humidity and pressure (23-40.5 °C and 16-40% respectively. Altitude averaged 1692.8 ± 210 m during data collection. The male subject (36 yrs, 75 kg, VO2max of 67.0 ml·kg-1·min-1 had an average (mean ± SD heart rate of 132 ± 9 bpm, oxygen consumption of 34.0 ± 6.8 ml·kg-1·min-1, RER of 0.91 ± 0.04, and VE of 86.0 ± 14.3 L·min-1 during the 21.7 km measuring period. This represented an average of 51% VO2max and 75% heart rate maximum. Energy expenditure was 12.6 ± 2.5 kcals·min-1, or 82.7 ± 16.6 kcals·km-1 (134 ± 27 kcals·mile-1 at 68.3 ± 12.5% carbohydrate. Extrapolation of this data would result in an energy expenditure of >13,000 kcals for the 160 km race, and an exogenous carbohydrate requirement of >250 kcal·hr-1. The energy cost of running for this subject on separate, noncompetitive occasions ranged from 64.9 ± 8.5 to 74.4 ± 5.5 kcals·km-1 (105 ± 14 to 120 ± 9 kcals·mile-1. Ultradistance trail running increases energy expenditure above that of running on nonundulating terrain, which may result in underestimating energy requirements during these events and subsequent undernourishment and suboptimal performance.

  3. Software Prototyping

    Science.gov (United States)

    Del Fiol, Guilherme; Hanseler, Haley; Crouch, Barbara Insley; Cummins, Mollie R.

    2016-01-01

    Summary Background Health information exchange (HIE) between Poison Control Centers (PCCs) and Emergency Departments (EDs) could improve care of poisoned patients. However, PCC information systems are not designed to facilitate HIE with EDs; therefore, we are developing specialized software to support HIE within the normal workflow of the PCC using user-centered design and rapid prototyping. Objective To describe the design of an HIE dashboard and the refinement of user requirements through rapid prototyping. Methods Using previously elicited user requirements, we designed low-fidelity sketches of designs on paper with iterative refinement. Next, we designed an interactive high-fidelity prototype and conducted scenario-based usability tests with end users. Users were asked to think aloud while accomplishing tasks related to a case vignette. After testing, the users provided feedback and evaluated the prototype using the System Usability Scale (SUS). Results Survey results from three users provided useful feedback that was then incorporated into the design. After achieving a stable design, we used the prototype itself as the specification for development of the actual software. Benefits of prototyping included having 1) subject-matter experts heavily involved with the design; 2) flexibility to make rapid changes, 3) the ability to minimize software development efforts early in the design stage; 4) rapid finalization of requirements; 5) early visualization of designs; 6) and a powerful vehicle for communication of the design to the programmers. Challenges included 1) time and effort to develop the prototypes and case scenarios; 2) no simulation of system performance; 3) not having all proposed functionality available in the final product; and 4) missing needed data elements in the PCC information system. PMID:27081404

  4. Automation of the Calibration of Reference Dosimeters Used in Radiotherapy

    International Nuclear Information System (INIS)

    Romero Acosta, A.; Gutierrez Lores, S.

    2013-01-01

    Traceability, accuracy and consistency of radiation measurements are essential in radiation dosimetry, particularly in radiotherapy, where the outcome of treatments is highly dependent on the radiation dose delivered to patients. The role of Secondary Standard Dosimetry Laboratories (SSDLs) is crucial in providing traceable calibrations to hospitals, since these laboratories disseminate calibrations at specific radiation qualities appropriate to the use of radiation measuring instruments. These laboratories follow IAEA/WHO guidelines for calibration procedures, often being current and charge measurements described in these guidelines a tedious task. However, these measurements are usually done using modern electrometers which are equipped with a RS-232 interface that allows instrument control from a PC. This paper presents the design and employment of an automated system aimed to the measurements of the radiotherapy dosimeters calibration process for Cobalt-60 gamma rays. A software was developed using Lab View, in order to achieve the acquisition of the charge values measured, calculation of the calibration coefficient and issue of a calibration certificate. A primary data report file is filled and stored in the PC's hard disk. By using this software tool, a better control over the calibration process is achieved, it reduces the need for human intervention and it also reduces the exposure of the laboratory staff. The automated system has been used for the calibration of reference dosimeters used in radiotherapy at the Cuban Secondary Standard Dosimetry Laboratory of the Center for Radiation Protection and Hygiene (Author)

  5. Compact radiometric microwave calibrator

    International Nuclear Information System (INIS)

    Fixsen, D. J.; Wollack, E. J.; Kogut, A.; Limon, M.; Mirel, P.; Singal, J.; Fixsen, S. M.

    2006-01-01

    The calibration methods for the ARCADE II instrument are described and the accuracy estimated. The Steelcast coated aluminum cones which comprise the calibrator have a low reflection while maintaining 94% of the absorber volume within 5 mK of the base temperature (modeled). The calibrator demonstrates an absorber with the active part less than one wavelength thick and only marginally larger than the mouth of the largest horn and yet black (less than -40 dB or 0.01% reflection) over five octaves in frequency

  6. Lidar to lidar calibration

    DEFF Research Database (Denmark)

    Fernandez Garcia, Sergio; Villanueva, Héctor

    This report presents the result of the lidar to lidar calibration performed for ground-based lidar. Calibration is here understood as the establishment of a relation between the reference lidar wind speed measurements with measurement uncertainties provided by measurement standard and corresponding...... lidar wind speed indications with associated measurement uncertainties. The lidar calibration concerns the 10 minute mean wind speed measurements. The comparison of the lidar measurements of the wind direction with that from the reference lidar measurements are given for information only....

  7. Study of Calorimeter Calibration with Tau's in CMS.

    CERN Document Server

    Denegri, Daniel; Nikitenko, Alexander

    1997-01-01

    We propose to calibrate in situ the CMS calorimetry using the single, isolated pions from tau-> pi nu in W -> tau nu and Z, gamma^* -> tau tau processes applying the p/E method. In case of pions non-interacting in the ECAL the method is straightforward, but for pions interacting in the ECAL care is needed to suppress and keep under control pi+- pi0's from tau's or QCS jets, which could vitiate the method. This can be achieved exploiting the ECAL granularity and tracker-calorimetry special matching. The momentum of the isolated high pt pion can be directly compared to the calorimeter measurement. Triggering of the W -> tau nu events is envisaged with a special tau-jet trigger combined with a missing transverse energy trigger. The Z gamma^* -> tau tau events could be triggered by lepton + tau-jet and double tau-jet trigger. The event rate for pt of pion > 15 GeV is e nough to calibrate each HCAL cell at a 1% precision after collection of 10^4 pb-1 of data.

  8. Evaluation of the amorphous content of lactose by solution calorimetry and Raman spectroscopy.

    Science.gov (United States)

    Katainen, Erja; Niemelä, Pentti; Harjunen, Päivi; Suhonen, Janne; Järvinen, Kristiina

    2005-11-15

    Solution calorimetry can be used to determine the amorphous content of a compound when the solubility and dissolution rate of the compound in the chosen solvent are reasonably high. Sometimes, it can be difficult find a solvent in which a sample is freely soluble. The present study evaluated the use of solution calorimetry for the assessment of the amorphous content of a sample that is poorly soluble in a solvent. Physical mixtures of lactose and spray-dried lactose samples (the amorphous content varied from 0 to 100%) were analyzed by a solution calorimeter and the results were compared with Raman spectroscopy determinations. The heat of solvation of the samples was determined by solution calorimetry in organic solvents MeOH, EtOH, ACN, THF, acetone (400mg sample/100ml solvent). Lactose is virtually insoluble in ACN, THF and acetone and very slightly soluble in EtOH and MeOH. The amorphous content of the samples could not be determined by solution calorimetry in EtOH, ACN, THF or acetone. However, an excellent correlation was observed between the heat of solvation and the amorphous content of the samples in MeOH. Furthermore, the heat of solvation values of the samples in MeOH showed a linear correlation with the Raman quantifications. Therefore, our results demonstrate that solution calorimetry may represent a rapid and simple method for determining the amorphous content also in samples that are not freely soluble in the solvent.

  9. Mathematical Model for Localised and Surface Heat Flux of the Human Body Obtained from Measurements Performed with a Calorimetry Minisensor

    Science.gov (United States)

    Socorro, Fabiola; Rodríguez de Rivera, Pedro Jesús; Rodríguez de Rivera, Miriam

    2017-01-01

    The accuracy of the direct and local measurements of the heat power dissipated by the surface of the human body, using a calorimetry minisensor, is directly related to the calibration rigor of the sensor and the correct interpretation of the experimental results. For this, it is necessary to know the characteristics of the body’s local heat dissipation. When the sensor is placed on the surface of the human body, the body reacts until a steady state is reached. We propose a mathematical model that represents the rate of heat flow at a given location on the surface of a human body by the sum of a series of exponentials: W(t) = A0 + ∑Aiexp(−t/τi). In this way, transient and steady states of heat dissipation can be interpreted. This hypothesis has been tested by simulating the operation of the sensor. At the steady state, the power detected in the measurement area (4 cm2) varies depending on the sensor’s thermostat temperature, as well as the physical state of the subject. For instance, for a thermostat temperature of 24 °C, this power can vary between 100–250 mW in a healthy adult. In the transient state, two exponentials are sufficient to represent this dissipation, with 3 and 70 s being the mean values of its time constants. PMID:29182567

  10. Mathematical Model for Localised and Surface Heat Flux of the Human Body Obtained from Measurements Performed with a Calorimetry Minisensor.

    Science.gov (United States)

    Socorro, Fabiola; Rodríguez de Rivera, Pedro Jesús; Rodríguez de Rivera, Miriam; Rodríguez de Rivera, Manuel

    2017-11-28

    The accuracy of the direct and local measurements of the heat power dissipated by the surface of the human body, using a calorimetry minisensor, is directly related to the calibration rigor of the sensor and the correct interpretation of the experimental results. For this, it is necessary to know the characteristics of the body's local heat dissipation. When the sensor is placed on the surface of the human body, the body reacts until a steady state is reached. We propose a mathematical model that represents the rate of heat flow at a given location on the surface of a human body by the sum of a series of exponentials: W ( t ) = A ₀ + ∑A i exp( -t / τ i ). In this way, transient and steady states of heat dissipation can be interpreted. This hypothesis has been tested by simulating the operation of the sensor. At the steady state, the power detected in the measurement area (4 cm²) varies depending on the sensor's thermostat temperature, as well as the physical state of the subject. For instance, for a thermostat temperature of 24 °C, this power can vary between 100-250 mW in a healthy adult. In the transient state, two exponentials are sufficient to represent this dissipation, with 3 and 70 s being the mean values of its time constants.

  11. Calibration of areal surface topography measuring instruments

    Science.gov (United States)

    Seewig, J.; Eifler, M.

    2017-06-01

    The ISO standards which are related to the calibration of areal surface topography measuring instruments are the ISO 25178-6xx series which defines the relevant metrological characteristics for the calibration of different measuring principles and the ISO 25178-7xx series which defines the actual calibration procedures. As the field of areal measurement is however not yet fully standardized, there are still open questions to be addressed which are subject to current research. Based on this, selected research results of the authors in this area are presented. This includes the design and fabrication of areal material measures. For this topic, two examples are presented with the direct laser writing of a stepless material measure for the calibration of the height axis which is based on the Abbott- Curve and the manufacturing of a Siemens star for the determination of the lateral resolution limit. Based on these results, as well a new definition for the resolution criterion, the small scale fidelity, which is still under discussion, is presented. Additionally, a software solution for automated calibration procedures is outlined.

  12. Jagiellonian University Development of the LHCb VELO monitoring software platform

    CERN Document Server

    Majewski, Maciej

    2017-01-01

    One of the most important parts of the LHCb spectrometer is the VErtex LOcator (VELO), dedicated to the precise tracking close to the proton–proton interaction point. The quality of data produced by the VELO depends on the calibration process, which must be monitored to ensure its correctness. This work presents details on how the calibration monitoring is conducted and how it could be improved. It also includes information on monitoring software and data flow in the LHCb software framework.

  13. Air Data Calibration Facility

    Data.gov (United States)

    Federal Laboratory Consortium — This facility is for low altitude subsonic altimeter system calibrations of air vehicles. Mission is a direct support of the AFFTC mission. Postflight data merge is...

  14. SRHA calibration curve

    Data.gov (United States)

    U.S. Environmental Protection Agency — an UV calibration curve for SRHA quantitation. This dataset is associated with the following publication: Chang, X., and D. Bouchard. Surfactant-Wrapped Multiwalled...

  15. Calibrated Properties Model

    International Nuclear Information System (INIS)

    Ahlers, C.F.; Liu, H.H.

    2001-01-01

    The purpose of this Analysis/Model Report (AMR) is to document the Calibrated Properties Model that provides calibrated parameter sets for unsaturated zone (UZ) flow and transport process models for the Yucca Mountain Site Characterization Project (YMP). This work was performed in accordance with the AMR Development Plan for U0035 Calibrated Properties Model REV00 (CRWMS M and O 1999c). These calibrated property sets include matrix and fracture parameters for the UZ Flow and Transport Model (UZ Model), drift seepage models, drift-scale and mountain-scale coupled-processes models, and Total System Performance Assessment (TSPA) models as well as Performance Assessment (PA) and other participating national laboratories and government agencies. These process models provide the necessary framework to test conceptual hypotheses of flow and transport at different scales and predict flow and transport behavior under a variety of climatic and thermal-loading conditions

  16. Calibrated Properties Model

    International Nuclear Information System (INIS)

    Ahlers, C.; Liu, H.

    2000-01-01

    The purpose of this Analysis/Model Report (AMR) is to document the Calibrated Properties Model that provides calibrated parameter sets for unsaturated zone (UZ) flow and transport process models for the Yucca Mountain Site Characterization Project (YMP). This work was performed in accordance with the ''AMR Development Plan for U0035 Calibrated Properties Model REV00. These calibrated property sets include matrix and fracture parameters for the UZ Flow and Transport Model (UZ Model), drift seepage models, drift-scale and mountain-scale coupled-processes models, and Total System Performance Assessment (TSPA) models as well as Performance Assessment (PA) and other participating national laboratories and government agencies. These process models provide the necessary framework to test conceptual hypotheses of flow and transport at different scales and predict flow and transport behavior under a variety of climatic and thermal-loading conditions

  17. SPOTS Calibration Example

    Directory of Open Access Journals (Sweden)

    Patterson E.

    2010-06-01

    Full Text Available The results are presented using the procedure outlined by the Standardisation Project for Optical Techniques of Strain measurement to calibrate a digital image correlation system. The process involves comparing the experimental data obtained with the optical measurement system to the theoretical values for a specially designed specimen. The standard states the criteria which must be met in order to achieve successful calibration, in addition to quantifying the measurement uncertainty in the system. The system was evaluated at three different displacement load levels, generating strain ranges from 289 µstrain to 2110 µstrain. At the 289 µstrain range, the calibration uncertainty was found to be 14.1 µstrain, and at the 2110 µstrain range it was found to be 28.9 µstrain. This calibration procedure was performed without painting a speckle pattern on the surface of the metal. Instead, the specimen surface was prepared using different grades of grit paper to produce the desired texture.

  18. Global Software Engineering: A Software Process Approach

    Science.gov (United States)

    Richardson, Ita; Casey, Valentine; Burton, John; McCaffery, Fergal

    Our research has shown that many companies are struggling with the successful implementation of global software engineering, due to temporal, cultural and geographical distance, which causes a range of factors to come into play. For example, cultural, project managementproject management and communication difficulties continually cause problems for software engineers and project managers. While the implementation of efficient software processes can be used to improve the quality of the software product, published software process models do not cater explicitly for the recent growth in global software engineering. Our thesis is that global software engineering factors should be included in software process models to ensure their continued usefulness in global organisations. Based on extensive global software engineering research, we have developed a software process, Global Teaming, which includes specific practices and sub-practices. The purpose is to ensure that requirements for successful global software engineering are stipulated so that organisations can ensure successful implementation of global software engineering.

  19. Scanner calibration revisited

    Directory of Open Access Journals (Sweden)

    Pozhitkov Alexander E

    2010-07-01

    Full Text Available Abstract Background Calibration of a microarray scanner is critical for accurate interpretation of microarray results. Shi et al. (BMC Bioinformatics, 2005, 6, Art. No. S11 Suppl. 2. reported usage of a Full Moon BioSystems slide for calibration. Inspired by the Shi et al. work, we have calibrated microarray scanners in our previous research. We were puzzled however, that most of the signal intensities from a biological sample fell below the sensitivity threshold level determined by the calibration slide. This conundrum led us to re-investigate the quality of calibration provided by the Full Moon BioSystems slide as well as the accuracy of the analysis performed by Shi et al. Methods Signal intensities were recorded on three different microarray scanners at various photomultiplier gain levels using the same calibration slide from Full Moon BioSystems. Data analysis was conducted on raw signal intensities without normalization or transformation of any kind. Weighted least-squares method was used to fit the data. Results We found that initial analysis performed by Shi et al. did not take into account autofluorescence of the Full Moon BioSystems slide, which led to a grossly distorted microarray scanner response. Our analysis revealed that a power-law function, which is explicitly accounting for the slide autofluorescence, perfectly described a relationship between signal intensities and fluorophore quantities. Conclusions Microarray scanners respond in a much less distorted fashion than was reported by Shi et al. Full Moon BioSystems calibration slides are inadequate for performing calibration. We recommend against using these slides.

  20. Calibration of thermoluminiscent materials

    International Nuclear Information System (INIS)

    Bos, A.J.J.

    1989-07-01

    In this report the relation between exposure and absorbed radiation dose in various materials is represented, on the base of recent data. With the help of this a calibration procedure for thermoluminescent materials, adapted to the IRI radiation standard is still the exposure in rontgen. In switching to the air kerma standard the calibration procedure will have to be adapted. (author). 6 refs.; 4 tabs

  1. Software system safety

    Science.gov (United States)

    Uber, James G.

    1988-01-01

    Software itself is not hazardous, but since software and hardware share common interfaces there is an opportunity for software to create hazards. Further, these software systems are complex, and proven methods for the design, analysis, and measurement of software safety are not yet available. Some past software failures, future NASA software trends, software engineering methods, and tools and techniques for various software safety analyses are reviewed. Recommendations to NASA are made based on this review.

  2. Determination of the thermodynamic properties of complexation and extraction by micro-calorimetry

    International Nuclear Information System (INIS)

    Charbonnel, M.Ch.; Flandin, J.L.

    2000-01-01

    The CEA is currently developing the DIAMEX process, the first step in the strategy for the separation of minor actinides from high-level radioactive waste. The extractant belongs to the diamide family of molecules and is able to co-extract trivalent actinides and lanthanides. This study focuses on the thermodynamic properties (ΔH, ΔG, ΔS) of lanthanide extraction by malonamide in order to better understand the mechanisms involved and to account for differences in the behavior of various diamide extractants. The main technique used is microcalorimetric titration. The Thermal Activity Monitor (TAM) microcalorimeter is a modular system with a highly stable (± 0.1 mK) temperature-controlled bath containing up to four calorimetry vessel units. The sensor bulbs inserted in the reaction vessel can measure heat flows in static or dynamic conditions. Micro-calorimetry, and calorimetric titration in particular, is a fast growing field due to technical improvements in both hardware and software. In the case of an equilibrium reaction, titration allows both Δ r G and Δ r H (and thus Δ r S) to be determined simultaneously. It was decided to initiate this thermochemical investigation with a homogeneous phase reaction, and the first study concerned the aqueous phase complexation of a trivalent lanthanide ion by a water-soluble diamide, tetraethyl-malonamide (TEMA: (C 2 H 5 ) 2 NCO-CH 2 CON(C 2 H 5 ) 2 ). In the test system, the heat of dilution of the diamide in water is preponderant over the heat arising from the complexation reaction; the result is a positive value corresponding to an endothermic reaction. However, the equilibration constant K and Δ H are both very small, and cannot be calculated from the resulting Q v f(n TEMA ) curves. Moreover, in aqueous phase, the reactions involved are different from those observed when neodymium(III) is extracted into an organic phase, and the medium must be further characterized before the calorimetry data can be fully

  3. Calibrating nacelle lidars

    Energy Technology Data Exchange (ETDEWEB)

    Courtney, M.

    2013-01-15

    Nacelle mounted, forward looking wind lidars are beginning to be used to provide reference wind speed measurements for the power performance testing of wind turbines. In such applications, a formal calibration procedure with a corresponding uncertainty assessment will be necessary. This report presents four concepts for performing such a nacelle lidar calibration. Of the four methods, two are found to be immediately relevant and are pursued in some detail. The first of these is a line of sight calibration method in which both lines of sight (for a two beam lidar) are individually calibrated by accurately aligning the beam to pass close to a reference wind speed sensor. A testing procedure is presented, reporting requirements outlined and the uncertainty of the method analysed. It is seen that the main limitation of the line of sight calibration method is the time required to obtain a representative distribution of radial wind speeds. An alternative method is to place the nacelle lidar on the ground and incline the beams upwards to bisect a mast equipped with reference instrumentation at a known height and range. This method will be easier and faster to implement and execute but the beam inclination introduces extra uncertainties. A procedure for conducting such a calibration is presented and initial indications of the uncertainties given. A discussion of the merits and weaknesses of the two methods is given together with some proposals for the next important steps to be taken in this work. (Author)

  4. Absorbed dose to water determination with ionization chamber dosimetry and calorimetry in restricted neutron, photon, proton and heavy-ion radiation fields.

    Science.gov (United States)

    Brede, H J; Greif, K-D; Hecker, O; Heeg, P; Heese, J; Jones, D T L; Kluge, H; Schardt, D

    2006-08-07

    Absolute dose measurements with a transportable water calorimeter and ionization chambers were performed at a water depth of 20 mm in four different types of radiation fields, for a collimated (60)Co photon beam, for a collimated neutron beam with a fluence-averaged mean energy of 5.25 MeV, for collimated proton beams with mean energies of 36 MeV and 182 MeV at the measuring position, and for a (12)C ion beam in a scanned mode with an energy per atomic mass of 430 MeV u(-1). The ionization chambers actually used were calibrated in units of air kerma in the photon reference field of the PTB and in units of absorbed dose to water for a Farmer-type chamber at GSI. The absorbed dose to water inferred from calorimetry was compared with the dose derived from ionometry by applying the radiation-field-dependent parameters. For neutrons, the quantities of the ICRU Report 45, for protons the quantities of the ICRU Report 59 and for the (12)C ion beam, the recommended values of the International Atomic Energy Agency (IAEA) protocol (TRS 398) were applied. The mean values of the absolute absorbed dose to water obtained with these two independent methods agreed within the standard uncertainty (k = 1) of 1.8% for calorimetry and of 3.0% for ionometry for all types and energies of the radiation beams used in this comparison.

  5. Direct measurement of electron beam quality conversion factors using water calorimetry

    Energy Technology Data Exchange (ETDEWEB)

    Renaud, James, E-mail: james.renaud@mail.mcgill.ca; Seuntjens, Jan [Medical Physics Unit, McGill University, Montréal, Québec H3G 1A4 (Canada); Sarfehnia, Arman [Medical Physics Unit, McGill University, Montréal, Québec H3G 1A4, Canada and Department of Radiation Oncology, University of Toronto, Toronto, Ontario M5S 3E2 (Canada); Marchant, Kristin [Allan Blair Cancer Centre, Saskatchewan Cancer Agency, Regina, Saskatchewan S4T 7T1, Canada and Department of Oncology, University of Saskatchewan, Saskatoon, Saskatchewan S7N 5A1 (Canada); McEwen, Malcolm; Ross, Carl [Ionizing Radiation Standards, National Research Council of Canada, Ottawa, Ontario K1A 0R6 (Canada)

    2015-11-15

    Purpose: In this work, the authors describe an electron sealed water calorimeter (ESWcal) designed to directly measure absorbed dose to water in clinical electron beams and its use to derive electron beam quality conversion factors for two ionization chamber types. Methods: A functioning calorimeter prototype was constructed in-house and used to obtain reproducible measurements in clinical accelerator-based 6, 9, 12, 16, and 20 MeV electron beams. Corrections for the radiation field perturbation due to the presence of the glass calorimeter vessel were calculated using Monte Carlo (MC) simulations. The conductive heat transfer due to dose gradients and nonwater materials was also accounted for using a commercial finite element method software package. Results: The relative combined standard uncertainty on the ESWcal dose was estimated to be 0.50% for the 9–20 MeV beams and 1.00% for the 6 MeV beam, demonstrating that the development of a water calorimeter-based standard for electron beams over such a wide range of clinically relevant energies is feasible. The largest contributor to the uncertainty was the positioning (Type A, 0.10%–0.40%) and its influence on the perturbation correction (Type B, 0.10%–0.60%). As a preliminary validation, measurements performed with the ESWcal in a 6 MV photon beam were directly compared to results derived from the National Research Council of Canada (NRC) photon beam standard water calorimeter. These two independent devices were shown to agree well within the 0.43% combined relative uncertainty of the ESWcal for this beam type and quality. Absorbed dose electron beam quality conversion factors were measured using the ESWcal for the Exradin A12 and PTW Roos ionization chambers. The photon-electron conversion factor, k{sub ecal}, for the A12 was also experimentally determined. Nonstatistically significant differences of up to 0.7% were found when compared to the calculation-based factors listed in the AAPM’s TG-51 protocol

  6. Direct measurement of electron beam quality conversion factors using water calorimetry.

    Science.gov (United States)

    Renaud, James; Sarfehnia, Arman; Marchant, Kristin; McEwen, Malcolm; Ross, Carl; Seuntjens, Jan

    2015-11-01

    In this work, the authors describe an electron sealed water calorimeter (ESWcal) designed to directly measure absorbed dose to water in clinical electron beams and its use to derive electron beam quality conversion factors for two ionization chamber types. A functioning calorimeter prototype was constructed in-house and used to obtain reproducible measurements in clinical accelerator-based 6, 9, 12, 16, and 20 MeV electron beams. Corrections for the radiation field perturbation due to the presence of the glass calorimeter vessel were calculated using Monte Carlo (MC) simulations. The conductive heat transfer due to dose gradients and nonwater materials was also accounted for using a commercial finite element method software package. The relative combined standard uncertainty on the ESWcal dose was estimated to be 0.50% for the 9-20 MeV beams and 1.00% for the 6 MeV beam, demonstrating that the development of a water calorimeter-based standard for electron beams over such a wide range of clinically relevant energies is feasible. The largest contributor to the uncertainty was the positioning (Type A, 0.10%-0.40%) and its influence on the perturbation correction (Type B, 0.10%-0.60%). As a preliminary validation, measurements performed with the ESWcal in a 6 MV photon beam were directly compared to results derived from the National Research Council of Canada (NRC) photon beam standard water calorimeter. These two independent devices were shown to agree well within the 0.43% combined relative uncertainty of the ESWcal for this beam type and quality. Absorbed dose electron beam quality conversion factors were measured using the ESWcal for the Exradin A12 and PTW Roos ionization chambers. The photon-electron conversion factor, kecal, for the A12 was also experimentally determined. Nonstatistically significant differences of up to 0.7% were found when compared to the calculation-based factors listed in the AAPM's TG-51 protocol. General agreement between the relative

  7. The physics of compensating calorimetry and the new CALOR89 code system

    International Nuclear Information System (INIS)

    Gabriel, T.A.; Brau, J.E.; Bishop, B.L.

    1989-03-01

    Much of the understanding of the physics of calorimetry has come from the use of excellent radiation transport codes. A new understanding of compensating calorimetry was introduced four years ago following detailed studies with a new CALOR system. Now, the CALOR system has again been revised to reflect a better comprehension of high energy nuclear collisions by incorporating a modified high energy fragmentation model from FLUKA87. This revision will allow for the accurate analysis of calorimeters at energies of 100's of GeV. Presented in this paper is a discussion of compensating calorimetry, the new CALOR system, the revisions to HETC, and recently generated calorimeter related data on modes of energy deposition and secondary neutron production (E < 50 MeV) in infinite iron and uranium blocks. 38 refs., 5 figs., 5 tabs

  8. Application of prediction of equilibrium to servo-controlled calorimetry measurements

    International Nuclear Information System (INIS)

    Mayer, R.L. II.

    1987-01-01

    Research was performed to develop an endpoint prediction algorithm for use with calorimeters operating in the digital servo-controlled mode. The purpose of this work was to reduce calorimetry measurement times while maintaining the high degree of precision and low bias expected from calorimetry measurements. Data from routine operation of two calorimeters were used to test predictive models at each stage of development against time savings, precision, and robustness criteria. The results of the study indicated that calorimetry measurement times can be significantly reduced using this technique. The time savings is, however, dependent on parameters in the digital servo-control algorithm and on packaging characteristics of measured items. 7 refs., 4 figs., 1 tab

  9. Study of interactions between hyaluronan and cationic surfactants by means of calorimetry, turbidimetry, potentiometry and conductometry.

    Science.gov (United States)

    Krouská, J; Pekař, M; Klučáková, M; Šarac, B; Bešter-Rogač, M

    2017-02-10

    The thermodynamics of the micelle formation of the cationic surfactants tetradecyltrimethylammonium bromide (TTAB) and cetyltrimethylammonium bromide (CTAB) with and without the addition of hyaluronan of two molecular weights was studied in aqueous solution by titration calorimetry. Macroscopic phase separation, which was detected by calorimetry and also by conductometry, occurs when charges on the surfactant and hyaluronan are balanced. In contrast, turbidimetry and potentiometry showed hyaluronan-surfactant interactions at very low surfactant concentrations. The observed differences between systems prepared with CTAB and TTAB indicate that besides the electrostatic interactions, which probably predominate, hydrophobic effects also play a significant role in hyaluronan interactions with cationic surfactants. Copyright © 2016 Elsevier Ltd. All rights reserved.

  10. Optical fibre temperature sensor technology and potential application in absorbed dose calorimetry

    International Nuclear Information System (INIS)

    Allen, P.D.; Hargrave, N.J.

    1992-09-01

    Optical fibre based sensors are proposed as a potential alternative to the thermistors traditionally used as temperature sensors in absorbed dose calorimetry. The development of optical fibre temperature sensor technology over the last ten years is reviewed. The potential resolution of various optical techniques is assessed with particular reference to the requirements of absorbed dose calorimetry. Attention is drawn to other issues which would require investigation before the development of practical optical fibre sensors for this purpose could occur. 192 refs., 5 tabs., 4 figs

  11. Thermodynamics of Surfactants, Block Copolymers and Their Mixtures in Water: The Role of the Isothermal Calorimetry

    Science.gov (United States)

    De Lisi, Rosario; Milioto, Stefania; Muratore, Nicola

    2009-01-01

    The thermodynamics of conventional surfactants, block copolymers and their mixtures in water was described to the light of the enthalpy function. The two methodologies, i.e. the van’t Hoff approach and the isothermal calorimetry, used to determine the enthalpy of micellization of pure surfactants and block copolymers were described. The van’t Hoff method was critically discussed. The aqueous copolymer+surfactant mixtures were analyzed by means of the isothermal titration calorimetry and the enthalpy of transfer of the copolymer from the water to the aqueous surfactant solutions. Thermodynamic models were presented to show the procedure to extract straightforward molecular insights from the bulk properties. PMID:19742173

  12. Simbol-X Telescope Scientific Calibrations: Requirements and Plans

    International Nuclear Information System (INIS)

    Malaguti, G.; Raimondi, L.; Trifoglio, M.; Angelini, L.; Moretti, A.

    2009-01-01

    The Simbol-X telescope characteristics and the mission scientific requirements impose a challenging calibration plan with a number of unprecedented issues. The 20 m focal length implies for the incoming X-ray beam a divergence comparable to the incidence angle of the mirror surface also for 100 m-long facilities. Moreover this is the first time that a direct focussing X-ray telescope will be calibrated on an energy band covering about three decades, and with a complex focal plane. These problems require a careful plan and organization of the measurements, together with an evaluation of the calibration needs in terms of both hardware and software.

  13. Simbol-X Telescope Scientific Calibrations: Requirements and Plans

    Science.gov (United States)

    Malaguti, G.; Angelini, L.; Raimondi, L.; Moretti, A.; Trifoglio, M.

    2009-05-01

    The Simbol-X telescope characteristics and the mission scientific requirements impose a challenging calibration plan with a number of unprecedented issues. The 20 m focal length implies for the incoming X-ray beam a divergence comparable to the incidence angle of the mirror surface also for 100 m-long facilities. Moreover this is the first time that a direct focussing X-ray telescope will be calibrated on an energy band covering about three decades, and with a complex focal plane. These problems require a careful plan and organization of the measurements, together with an evaluation of the calibration needs in terms of both hardware and software.

  14. Traceable calibration of impedance heads and artificial mastoids

    International Nuclear Information System (INIS)

    Scott, D A; Dickinson, L P; Bell, T J

    2015-01-01

    Artificial mastoids are devices which simulate the mechanical characteristics of the human head, and in particular of the bony structure behind the ear. They are an essential tool in the calibration of bone-conduction hearing aids and audiometers. With the emergence of different types of artificial mastoids in the market, and the realisation that the visco-elastic part of these instruments changes over time, the development of a method of traceable calibration of these devices without relying on commercial software has become important for national metrology institutes. This paper describes commercially available calibration methods, and the development of a traceable calibration method including the traceable calibration of the impedance head used to measure the mechanical impedance of the artificial mastoid. (paper)

  15. Radiometer Calibration and Characterization (RCC) User's Manual: Windows Version 4.0

    Energy Technology Data Exchange (ETDEWEB)

    Andreas, Afshin M. [National Renewable Energy Lab. (NREL), Golden, CO (United States); Wilcox, Stephen M. [National Renewable Energy Lab. (NREL), Golden, CO (United States)

    2016-02-29

    The Radiometer Calibration and Characterization (RCC) software is a data acquisition and data archival system for performing Broadband Outdoor Radiometer Calibrations (BORCAL). RCC provides a unique method of calibrating broadband atmospheric longwave and solar shortwave radiometers using techniques that reduce measurement uncertainty and better characterize a radiometer's response profile. The RCC software automatically monitors and controls many of the components that contribute to uncertainty in an instrument's responsivity. This is a user's manual and guide to the RCC software.

  16. Sandia software guidelines: Software quality planning

    Energy Technology Data Exchange (ETDEWEB)

    1987-08-01

    This volume is one in a series of Sandia Software Guidelines intended for use in producing quality software within Sandia National Laboratories. In consonance with the IEEE Standard for Software Quality Assurance Plans, this volume identifies procedures to follow in producing a Software Quality Assurance Plan for an organization or a project, and provides an example project SQA plan. 2 figs., 4 tabs.

  17. Calibration Under Uncertainty.

    Energy Technology Data Exchange (ETDEWEB)

    Swiler, Laura Painton; Trucano, Timothy Guy

    2005-03-01

    This report is a white paper summarizing the literature and different approaches to the problem of calibrating computer model parameters in the face of model uncertainty. Model calibration is often formulated as finding the parameters that minimize the squared difference between the model-computed data (the predicted data) and the actual experimental data. This approach does not allow for explicit treatment of uncertainty or error in the model itself: the model is considered the %22true%22 deterministic representation of reality. While this approach does have utility, it is far from an accurate mathematical treatment of the true model calibration problem in which both the computed data and experimental data have error bars. This year, we examined methods to perform calibration accounting for the error in both the computer model and the data, as well as improving our understanding of its meaning for model predictability. We call this approach Calibration under Uncertainty (CUU). This talk presents our current thinking on CUU. We outline some current approaches in the literature, and discuss the Bayesian approach to CUU in detail.

  18. Avoidable Software Procurements

    Science.gov (United States)

    2012-09-01

    software license, software usage, ELA, Software as a Service , SaaS , Software Asset...PaaS Platform as a Service SaaS Software as a Service SAM Software Asset Management SMS System Management Server SEWP Solutions for Enterprise Wide...delivery of full Cloud Services , we will see the transition of the Cloud Computing service model from Iaas to SaaS , or Software as a Service . Software

  19. Calibration of Low Cost RGB and NIR Uav Cameras

    Science.gov (United States)

    Fryskowska, A.; Kedzierski, M.; Grochala, A.; Braula, A.

    2016-06-01

    Non-metric digital cameras are being widely used for photogrammetric studies. The increase in resolution and quality of images obtained by non-metric cameras, allows to use it in low-cost UAV and terrestrial photogrammetry. Imagery acquired with non-metric cameras can be used in 3D modeling of objects or landscapes, reconstructing of historical sites, generating digital elevation models (DTM), orthophotos, or in the assessment of accidents. Non-metric digital camcorders are characterized by instability and ignorance of the interior orientation parameters. Therefore, the use of these devices requires prior calibration. Calibration research was conducted using non-metric camera, different calibration tests and various software. The first part of the paper contains a brief theoretical introduction including the basic definitions, like the construction of non-metric cameras or description of different optical distortions. The second part of the paper contains cameras calibration process, details of the calibration methods and models that have been used. Sony Nex 5 camera calibration has been done using software: Image Master Calib, Matlab - Camera Calibrator application and Agisoft Lens. For the study 2D test fields has been used. As a part of the research a comparative analysis of the results have been done.

  20. Studies Concerning the ATLAS IBL Calibration Architecture

    CERN Document Server

    Kretz, Moritz; Kugel, Andreas

    With the commissioning of the Insertable B-Layer (IBL) in 2013 at the ATLAS experiment 12~million additional pixels will be added to the current Pixel Detector. While the idea of employing pairs of VME based Read-Out Driver (ROD) and Back of Crate (BOC) cards in the read-out chain remains unchanged, modifications regarding the IBL calibration procedure were introduced to overcome current hardware limitations. The analysis of calibration histograms will no longer be performed on the RODs, but on an external computing farm that is connected to the RODs via Ethernet. This thesis contributes to the new IBL calibration procedure and presents a concept for a scalable software and hardware architecture. An embedded system targeted to the ROD FPGAs is realized for sending data from the RODs to the fit farm servers and benchmarks are carried out with a Linux based networking stack, as well as a standalone software stack. Furthermore, the histogram fitting algorithm currently being employed on the Pixel Detector RODs i...

  1. Software engineering architecture-driven software development

    CERN Document Server

    Schmidt, Richard F

    2013-01-01

    Software Engineering: Architecture-driven Software Development is the first comprehensive guide to the underlying skills embodied in the IEEE's Software Engineering Body of Knowledge (SWEBOK) standard. Standards expert Richard Schmidt explains the traditional software engineering practices recognized for developing projects for government or corporate systems. Software engineering education often lacks standardization, with many institutions focusing on implementation rather than design as it impacts product architecture. Many graduates join the workforce with incomplete skil

  2. Ibis ground calibration

    International Nuclear Information System (INIS)

    Bird, A.J.; Barlow, E.J.; Tikkanen, T.; Bazzano, A.; Del Santo, M.; Ubertini, P.; Blondel, C.; Laurent, P.; Lebrun, F.; Di Cocco, G.; Malaguti, E.; Gabriele, M.; La Rosa, G.; Segreto, A.; Quadrini, E.; Volkmer, R.

    2003-01-01

    We present an overview of results obtained from IBIS ground calibrations. The spectral and spatial characteristics of the detector planes and surrounding passive materials have been determined through a series of calibration campaigns. Measurements of pixel gain, energy resolution, detection uniformity, efficiency and imaging capability are presented. The key results obtained from the ground calibration have been: - optimization of the instrument tunable parameters, - determination of energy linearity for all detection modes, - determination of energy resolution as a function of energy through the range 20 keV - 3 MeV, - demonstration of imaging capability in each mode, - measurement of intrinsic detector non-uniformity and understanding of the effects of passive materials surrounding the detector plane, and - discovery (and closure) of various leakage paths through the passive shielding system

  3. Gamma counter calibration system

    International Nuclear Information System (INIS)

    1977-01-01

    A method and apparatus are described for the calibration of a gamma radiation measurement instrument to be used over any of a number of different absolute energy ranges. The method includes the steps of adjusting the overall signal gain associated with pulses which are derived from detected gamma rays, until the instrument is calibrated for a particular absolute energy range; then storing parameter settings corresponding to the adjusted overall signal gain, and repeating the process for other desired absolute energy ranges. The stored settings can be subsequently retrieved and reapplied so that test measurements can be made using a selected one of the absolute energy ranges. Means are provided for adjusting the overall signal gain and a specific technique is disclosed for making coarse, then fine adjustments to the signal gain, for rapid convergence of the required calibration settings. (C.F.)

  4. Aqueous solutions of proline and NaCl studied by differential scanning calorimetry at subzero temperatures

    DEFF Research Database (Denmark)

    Rasmussen, Peter Have; Jørgensen, Bo; Nielsen, Jette

    1997-01-01

    The hydration properties of proline are studied by differential scanning calorimetry (DSC) in aqueous solutions during freezing to -60 degrees C and subsequent heating to +20 degrees C. The concentration of proline in the freeze concentrated solution was estimated to approximately 50 wt% (w/w) in...... plants and insects living under water stress conditions is discussed. (C) 1997 Elsevier Science B.V....

  5. Isothermal Titration Calorimetry and Macromolecular Visualization for the Interaction of Lysozyme and Its Inhibitors

    Science.gov (United States)

    Wei, Chin-Chuan; Jensen, Drake; Boyle, Tiffany; O'Brien, Leah C.; De Meo, Cristina; Shabestary, Nahid; Eder, Douglas J.

    2015-01-01

    To provide a research-like experience to upper-division undergraduate students in a biochemistry teaching laboratory, isothermal titration calorimetry (ITC) is employed to determine the binding constants of lysozyme and its inhibitors, N-acetyl glucosamine trimer (NAG[subscript 3]) and monomer (NAG). The extremely weak binding of lysozyme/NAG is…

  6. Subsite binding energies of an exo-polygalacturonase using isothermal titration calorimetry

    Science.gov (United States)

    Thermodynamic parameters for binding of a series of galacturonic acid oligomers to an exo-polygalacturonase, RPG16 from Rhizopus oryzae, were determined by isothermal titration calorimetry. Binding of oligomers varying in chain length from two to five galacturonic acid residues is an exothermic proc...

  7. Thermodynamic investigations of protein's behaviour with ionic liquids in aqueous medium studied by isothermal titration calorimetry.

    Science.gov (United States)

    Bharmoria, Pankaj; Kumar, Arvind

    2016-05-01

    While a number of reports appear on ionic liquids-proteins interactions, their thermodynamic behaviour using suitable technique like isothermal titration calorimetry is not systematically presented. Isothermal titration calorimetry (ITC) is a key technique which can directly measure the thermodynamic contribution of IL binding to protein, particularly the enthalpy, heat capacities and binding stoichiometry. Ionic liquids (ILs), owing to their unique and tunable physicochemical properties have been the central area of scientific research besides graphene in the last decade, and growing unabated. Their encounter with proteins in the biological system is inevitable considering their environmental discharge though most of them are recyclable for a number of cycles. In this article we will cover the thermodynamics of proteins upon interaction with ILs as osmolyte and surfactant. The up to date literature survey of IL-protein interactions using isothermal titration calorimetry will be discussed and parallel comparison with the results obtained for such studies with other techniques will be highlighted to demonstrate the accuracy of ITC technique. Net stability of proteins can be obtained from the difference in the free energy (ΔG) of the native (folded) and denatured (unfolded) state using the Gibbs-Helmholtz equation (ΔG=ΔH-TΔS). Isothermal titration calorimetry can directly measure the heat changes upon IL-protein interactions. Calculation of other thermodynamic parameters such as entropy, binding constant and free energy depends upon the proper fitting of the binding isotherms using various fitting models. Copyright © 2015 Elsevier B.V. All rights reserved.

  8. Monolithic front-end preamplifiers for a broad range of calorimetry applications

    Energy Technology Data Exchange (ETDEWEB)

    Radeka, V.; Rescia, S. [Brookhaven National Lab., Upton, NY (United States); Manfredi, P.F.; Speziali, V. [Pavia Univ. (Italy). Dipt. di Elettronica]|[INFN--Sezzione di Milano, Milano (Italy)

    1993-12-31

    The present paper summarizes the salient results of a research and development activity in the area of low noise preamplifiers for different applications in calorimetry. Design target for all circuits considered here are low noise, ability to cope with broad energy ranges and radiation hardness.

  9. Proton and Copper Binding to Humic Acids Analyzed by XAFS Spectroscopy and Isothermal Titration Calorimetry

    NARCIS (Netherlands)

    Xu, Jinling; Koopal, Luuk K.; Fang, Linchuan; Xiong, Juan; Tan, Wenfeng

    2018-01-01

    Proton and copper (Cu) binding to soil and lignite-based humic acid (HA) was investigated by combining X-ray absorption fine structure (XAFS) spectroscopy, isothermal titration calorimetry (ITC), and nonideal-competitive-adsorption (NICA) modeling. NICA model calculations and XAFS results showed

  10. Study of phase transition in hard microcrystalline waxes and wax blends by differential scanning calorimetry

    Czech Academy of Sciences Publication Activity Database

    Kumar, S.; Agrawal, K. M.; Khan, H. U.; Sikora, Antonín

    2004-01-01

    Roč. 22, 3 & 4 (2004), s. 337-345 ISSN 1091-6466 R&D Projects: GA AV ČR KSK4050111 Institutional research plan: CEZ:AV0Z4050913 Keywords : phase transition * hard microscrystalline waxes * differential scanning calorimetry Subject RIV: CD - Macromolecular Chemistry Impact factor: 0.312, year: 2004

  11. Monolithic junction field-effect transistor charge preamplifier for calorimetry at high luminosity hadron colliders

    International Nuclear Information System (INIS)

    Radeka, V.; Rescia, S.; Rehn, L.A.; Manfredi, P.F.; Speziali, V.

    1991-11-01

    The outstanding noise and radiation hardness characteristics of epitaxial-channel junction field-effect transistors (JFET) suggest that a monolithic preamplifier based upon them may be able to meet the strict specifications for calorimetry at high luminosity colliders. Results obtained so far with a buried layer planar technology, among them an entire monolithic charge-sensitive preamplifier, are described

  12. Detection of sunflower oil in extra virgin olive oil by fast differential scanning calorimetry

    NARCIS (Netherlands)

    Wetten, I.A.; Herwaarden, A.W.; Splinter, R.; Boerrigter-Eenling, R.; Ruth, van S.M.

    2015-01-01

    Extra virgin olive oil (EVOO) is an economically valuable product, due to its high quality and premium price. Therefore it is vulnerable for adulteration by means of the addition of cheaper vegetable oils. Differential scanning calorimetry (DSC) has been suggested as a fast technique for the

  13. Impact of sample saturation on the detected porosity of hardened concrete using low temperature calorimetry

    DEFF Research Database (Denmark)

    Wu, Min; Johannesson, Björn

    2014-01-01

    The present work studied the impact of sample saturation on the analysis of pore volume and pore size distribution by low temperature (micro-)calorimetry. The theoretical background was examined, which emphasizes that the freezing/melting temperature of water/ice confined in non-fully saturated p...

  14. Designing a compensating quartz fiber calorimeter for low angle calorimetry at LHC

    International Nuclear Information System (INIS)

    Ferrando, A.; Fouz, M.C.; Josa, M.I.; Khan, A.; Rosowsky, A.; Salicio, J.M.

    1996-01-01

    We present a design of a compensating quartz fiber calorimeter, made of a unique active section, and ment for the specific physics requirements of the low angle calorimetry in LHC experiments. The purposed calorimeter is exemplified for the case of the CMS experiment

  15. Coulometry and Calorimetry of Electric Double Layer Formation in Porous Electrodes

    NARCIS (Netherlands)

    Janssen, Mathijs; Griffioen, Elian; Biesheuvel, P. M.; Van Roij, René; Erné, Ben

    2017-01-01

    Coulometric measurements on salt-water-immersed nanoporous carbon electrodes reveal, at a fixed voltage, a charge decrease with increasing temperature. During far-out-of-equilibrium charging of these electrodes, calorimetry indicates the production of both irreversible Joule heat and reversible

  16. Thermodynamic profiling of Peptide membrane interactions by isothermal titration calorimetry: a search for pores and micelles

    DEFF Research Database (Denmark)

    Henriksen, Jonas Rosager; Andresen, Thomas Lars

    2011-01-01

    in mixed peptide-lipid micelles. We have investigated the mode of action of the antimicrobial peptide mastoparan-X using isothermal titration calorimetry (ITC) and cryo-transmission electron microscopy (cryo-TEM). The results show that mastoparan-X induces a range of structural transitions of POPC/POPG (3...

  17. Examination of water phase transitions in Loblolly pine and cell wall components by differential scanning calorimetry

    Science.gov (United States)

    Samuel L. Zelinka; Michael J. Lambrecht; Samuel V. Glass; Alex C. Wiedenhoeft; Daniel J. Yelle

    2012-01-01

    This paper examines phase transformations of water in wood and isolated wood cell wall components using differential scanning calorimetry with the purpose of better understanding "Type II water" or "freezable bound water" that has been reported for cellulose and other hydrophilic polymers. Solid loblolly pine (Pinus taeda...

  18. High Pressure Differential Scanning Calorimetry of poly(4-methyl-pentene-1)

    NARCIS (Netherlands)

    Hoehne, G.W.H.; Rastogi, S.; Wunderlich, B.

    2000-01-01

    The polymer poly(4-methyl pentene-1), P4MP1, displays an unusual pressure–temperature phase diagram. The previous exploration of this phase behavior through X-ray diffraction has been extended through high-pressure calorimetry. The resulting phase diagram displays a melt area, the common tetragonal

  19. Liquid Scintillation Counting - Packard Triple-Label Calibration

    Energy Technology Data Exchange (ETDEWEB)

    Torretto, P. A. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

    2017-03-23

    The Radiological Measurements Laboratory (RML) maintains and operates nine Packard Liquid Scintillation Counters (LSCs). These counters were obtained through various sources and were generally purchased as 2500, 2700 or 3100 series counters. In 2004/2005 the software and firmware on the counters were upgraded. The counters are now designated as 3100 series counters running the Quantasmart software package. Thus, a single procedure can be used to calibrate and operate the Packard LSCs.

  20. Individual dosimetry and calibration

    International Nuclear Information System (INIS)

    Hoefert, M.; Nielsen, M.

    1996-01-01

    In 1995 both the Individual Dosimetry and Calibration Sections worked under the condition of a status quo and concentrated fully on the routine part of their work. Nevertheless, the machine for printing the bar code which will be glued onto the film holder and hence identify the people when entering into high radiation areas was put into operation and most of the holders were equipped with the new identification. As far as the Calibration Section is concerned the project of the new source control system that is realized by the Technical Support Section was somewhat accelerated

  1. Radiation Calibration Measurements

    International Nuclear Information System (INIS)

    Omondi, C.

    2017-01-01

    KEBS Radiation Dosimetry mandate are: Custodian of Kenya Standards on Ionizing radiation, Ensure traceability to International System (SI ) and Calibration radiation equipment. RAF 8/040 on Radioisotope applications for troubleshooting and optimizing industrial process established Radiotracer Laboratory objective is to introduce and implement radiotracer technique for problem solving of industrial challenges. Gamma ray scanning technique applied is to Locate blockages, Locate liquid in vapor lines, Locate areas of lost refractory or lining in a pipe and Measure flowing densities. Equipment used for diagnostic and radiation protection must be calibrated to ensure Accuracy and Traceability

  2. Calibrating Legal Judgments

    Directory of Open Access Journals (Sweden)

    Frederick Schauer

    2017-09-01

    Full Text Available Objective to study the notion and essence of legal judgments calibration the possibilities of using it in the lawenforcement activity to explore the expenses and advantages of using it. Methods dialectic approach to the cognition of social phenomena which enables to analyze them in historical development and functioning in the context of the integrity of objective and subjective factors it determined the choice of the following research methods formallegal comparative legal sociological methods of cognitive psychology and philosophy. Results In ordinary life people who assess other peoplersaquos judgments typically take into account the other judgments of those they are assessing in order to calibrate the judgment presently being assessed. The restaurant and hotel rating website TripAdvisor is exemplary because it facilitates calibration by providing access to a raterrsaquos previous ratings. Such information allows a user to see whether a particular rating comes from a rater who is enthusiastic about every place she patronizes or instead from someone who is incessantly hard to please. And even when less systematized as in assessing a letter of recommendation or college transcript calibration by recourse to the decisional history of those whose judgments are being assessed is ubiquitous. Yet despite the ubiquity and utility of such calibration the legal system seems perversely to reject it. Appellate courts do not openly adjust their standard of review based on the previous judgments of the judge whose decision they are reviewing nor do judges in reviewing legislative or administrative decisions magistrates in evaluating search warrant representations or jurors in assessing witness perception. In most legal domains calibration by reference to the prior decisions of the reviewee is invisible either because it does not exist or because reviewing bodies are unwilling to admit using what they in fact know and employ. Scientific novelty for the first

  3. Calibration of scanning Lidar

    DEFF Research Database (Denmark)

    Gómez Arranz, Paula; Courtney, Michael

    This report describes the tests carried out on a scanning lidar at the DTU Test Station for large wind turbines, Høvsøre. The tests were divided in two parts. In the first part, the purpose was to obtain wind speed calibrations at two heights against two cup anemometers mounted on a mast. Additio......This report describes the tests carried out on a scanning lidar at the DTU Test Station for large wind turbines, Høvsøre. The tests were divided in two parts. In the first part, the purpose was to obtain wind speed calibrations at two heights against two cup anemometers mounted on a mast...

  4. Software for simulation of a computed tomography imaging spectrometer using optical design software

    Science.gov (United States)

    Spuhler, Peter T.; Willer, Mark R.; Volin, Curtis E.; Descour, Michael R.; Dereniak, Eustace L.

    2000-11-01

    Our Imaging Spectrometer Simulation Software known under the name Eikon should improve and speed up the design of a Computed Tomography Imaging Spectrometer (CTIS). Eikon uses existing raytracing software to simulate a virtual instrument. Eikon enables designers to virtually run through the design, calibration and data acquisition, saving significant cost and time when designing an instrument. We anticipate that Eikon simulations will improve future designs of CTIS by allowing engineers to explore more instrument options.

  5. The software life cycle

    CERN Document Server

    Ince, Darrel

    1990-01-01

    The Software Life Cycle deals with the software lifecycle, that is, what exactly happens when software is developed. Topics covered include aspects of software engineering, structured techniques of software development, and software project management. The use of mathematics to design and develop computer systems is also discussed. This book is comprised of 20 chapters divided into four sections and begins with an overview of software engineering and software development, paying particular attention to the birth of software engineering and the introduction of formal methods of software develop

  6. Chemical kinetics on thermal decompositions of cumene hydroperoxide in cumene studied by calorimetry: An overview

    Energy Technology Data Exchange (ETDEWEB)

    Duh, Yih-Shing, E-mail: yihshingduh@yahoo.com.tw [Department of Occupation Safety and Health, Jen-Teh Junior College of Medicine, Nursing and Management, Miaoli, 35664, Taiwan, ROC (China); Department of Safety, Health and Environmental Engineering, National United University, No. 1 Lien-Da, Miaoli, 36052, Taiwan, ROC (China)

    2016-08-10

    Highlights: • Chemical kinetics on thermal decompositions of CHP are conducted and summarized. • Kinetics agrees well between data from DSC and adiabatic calorimetry. • Ea is determined to be about 120 kJ mol{sup −1} by various calorimetry. • LogA (A in s{sup −1}) is determined to be about 11.8 by various calorimetry. - Abstract: Study on chemical kinetics related to the thermal decomposition of cumene hydoperoxide (CHP) in cumene is summarized in this work. It is of great importance to gather and compare the differences between these kinetic parameters for further substantial applications in the chemical industry and process safety. CHP has been verified to possess an autocatalytic behavior by using microcalorimetry (such as TAM and C-80) operated at isothermal mode in the temperature range from 70 °C to 120 °C. However, it exhibits a reaction of n-th order detected by non-isothermal DSC scanning and adiabatic calorimeter. By the isothermal aging tests, activation energy and frequency factor in logA(s{sup −1}) were averaged to be (117.3 ± 5.9) kJ mol{sup −1}and (11.4 ± 0.3), respectively. Kinetic parameters acquired from data of interlaboratories by using heat-flow calorimetry, the averaged activation energy and frequency factor in logA(s{sup −1}) were (119.3 ± 11.3) kJ mol{sup −1}and (12.0 ± 0.2), respectively. On the analogy of results from adiabatic calorimetry, the activation energy and frequency factor in logA(s{sup −1}) were respectively averaged to be (122.4 ± 9.2) kJ mol{sup −1}and (11.8 ± 0.8). Five sets of kinetic models in relation to autocatalytic reactions are collected and discussed as well.

  7. Direct calibration of PICKY-designed microarrays

    Directory of Open Access Journals (Sweden)

    Ronald Pamela C

    2009-10-01

    Full Text Available Abstract Background Few microarrays have been quantitatively calibrated to identify optimal hybridization conditions because it is difficult to precisely determine the hybridization characteristics of a microarray using biologically variable cDNA samples. Results Using synthesized samples with known concentrations of specific oligonucleotides, a series of microarray experiments was conducted to evaluate microarrays designed by PICKY, an oligo microarray design software tool, and to test a direct microarray calibration method based on the PICKY-predicted, thermodynamically closest nontarget information. The complete set of microarray experiment results is archived in the GEO database with series accession number GSE14717. Additional data files and Perl programs described in this paper can be obtained from the website http://www.complex.iastate.edu under the PICKY Download area. Conclusion PICKY-designed microarray probes are highly reliable over a wide range of hybridization temperatures and sample concentrations. The microarray calibration method reported here allows researchers to experimentally optimize their hybridization conditions. Because this method is straightforward, uses existing microarrays and relatively inexpensive synthesized samples, it can be used by any lab that uses microarrays designed by PICKY. In addition, other microarrays can be reanalyzed by PICKY to obtain the thermodynamically closest nontarget information for calibration.

  8. ECAL Energy Flow Calibration

    CERN Multimedia

    CERN. Geneva

    2015-01-01

    My talk will be covering my work as a whole over the course of the semester. The focus will be on using energy flow calibration in ECAL to check the precision of the corrections made by the light monitoring system used to account for transparency loss within ECAL crystals due to radiation damage over time.

  9. Calibration with Absolute Shrinkage

    DEFF Research Database (Denmark)

    Øjelund, Henrik; Madsen, Henrik; Thyregod, Poul

    2001-01-01

    In this paper, penalized regression using the L-1 norm on the estimated parameters is proposed for chemometric je calibration. The algorithm is of the lasso type, introduced by Tibshirani in 1996 as a linear regression method with bound on the absolute length of the parameters, but a modification...

  10. Calibration bench of flowmeters

    International Nuclear Information System (INIS)

    Bremond, J.; Da Costa, D.; Calvet, A.; Vieuxmaire, C.

    1966-01-01

    This equipment is devoted to the comparison of signals from two turbines installed in the Cabri experimental loop. The signal is compared to the standard turbine. The characteristics and the performance of the calibration bench are presented. (A.L.B.)

  11. Calibration of farmer dosemeters

    International Nuclear Information System (INIS)

    Ahmad, S.S.; Anwar, K.; Arshed, W.; Mubarak, M.A.; Orfi, S.D.

    1984-08-01

    The Farmer Dosemeters of Atomic Energy Medical Centre (AEMC) Jamshoro were calibrated in the Secondary Standard Dosimetry Laboratory (SSDL) at PINSTECH, using the NPL Secondary Standard Therapy level X-ray exposure meter. The results are presented in this report. (authors)

  12. Physiotherapy ultrasound calibrations

    International Nuclear Information System (INIS)

    Gledhill, M.

    1996-01-01

    Calibration of physiotherapy ultrasound equipment has long been a problem. Numerous surveys around the world over the past 20 years have all found that only a low percentage of the units tested had an output within 30% of that indicatd. In New Zealand, a survey carried out by the NRL in 1985 found that only 24% had an output, at the maximum setting, within + or - 20% of that indicated. The present performance Standard for new equipment (NZS 3200.2.5:1992) requires that the measured output should not deviate from that indicated by more than + or - 30 %. This may be tightened to + or - 20% in the next few years. Any calibration is only as good as the calibration equipment. Some force balances can be tested with small weights to simulate the force exerted by an ultrasound beam, but with others this is not possible. For such balances, testing may only be feasible with a calibrated source which could be used like a transfer standard. (author). 4 refs., 3 figs

  13. NVLAP calibration laboratory program

    Energy Technology Data Exchange (ETDEWEB)

    Cigler, J.L.

    1993-12-31

    This paper presents an overview of the progress up to April 1993 in the development of the Calibration Laboratories Accreditation Program within the framework of the National Voluntary Laboratory Accreditation Program (NVLAP) at the National Institute of Standards and Technology (NIST).

  14. NVLAP calibration laboratory program

    International Nuclear Information System (INIS)

    Cigler, J.L.

    1993-01-01

    This paper presents an overview of the progress up to April 1993 in the development of the Calibration Laboratories Accreditation Program within the framework of the National Voluntary Laboratory Accreditation Program (NVLAP) at the National Institute of Standards and Technology (NIST)

  15. Gamma ray calibration system

    International Nuclear Information System (INIS)

    Rosauer, P.J.; Flaherty, J.J.

    1981-01-01

    This invention is in the field of gamma ray inspection devices for tubular products and the like employing an improved calibrating block which prevents the sensing system from being overloaded when no tubular product is present, and also provides the operator with a means for visually detecting the presence of wall thicknesses which are less than a required minimum. (author)

  16. PLEIADES ABSOLUTE CALIBRATION : INFLIGHT CALIBRATION SITES AND METHODOLOGY

    Directory of Open Access Journals (Sweden)

    S. Lachérade

    2012-07-01

    Full Text Available In-flight calibration of space sensors once in orbit is a decisive step to be able to fulfil the mission objectives. This article presents the methods of the in-flight absolute calibration processed during the commissioning phase. Four In-flight calibration methods are used: absolute calibration, cross-calibration with reference sensors such as PARASOL or MERIS, multi-temporal monitoring and inter-bands calibration. These algorithms are based on acquisitions over natural targets such as African deserts, Antarctic sites, La Crau (Automatic calibration station and Oceans (Calibration over molecular scattering or also new extra-terrestrial sites such as the Moon and selected stars. After an overview of the instrument and a description of the calibration sites, it is pointed out how each method is able to address one or several aspects of the calibration. We focus on how these methods complete each other in their operational use, and how they help building a coherent set of information that addresses all aspects of in-orbit calibration. Finally, we present the perspectives that the high level of agility of PLEIADES offers for the improvement of its calibration and a better characterization of the calibration sites.

  17. Mercury CEM Calibration

    Energy Technology Data Exchange (ETDEWEB)

    John F. Schabron; Joseph F. Rovani; Susan S. Sorini

    2007-03-31

    The Clean Air Mercury Rule (CAMR) which was published in the Federal Register on May 18, 2005, requires that calibration of mercury continuous emissions monitors (CEMs) be performed with NIST-traceable standards. Western Research Institute (WRI) is working closely with the Electric Power Research Institute (EPRI), the National Institute of Standards and Technology (NIST), and the Environmental Protection Agency (EPA) to facilitate the development of the experimental criteria for a NIST traceability protocol for dynamic elemental mercury vapor generators. The traceability protocol will be written by EPA. Traceability will be based on the actual analysis of the output of each calibration unit at several concentration levels ranging from about 2-40 ug/m{sup 3}, and this analysis will be directly traceable to analyses by NIST using isotope dilution inductively coupled plasma/mass spectrometry (ID ICP/MS) through a chain of analyses linking the calibration unit in the power plant to the NIST ID ICP/MS. Prior to this project, NIST did not provide a recommended mercury vapor pressure equation or list mercury vapor pressure in its vapor pressure database. The NIST Physical and Chemical Properties Division in Boulder, Colorado was subcontracted under this project to study the issue in detail and to recommend a mercury vapor pressure equation that the vendors of mercury vapor pressure calibration units can use to calculate the elemental mercury vapor concentration in an equilibrium chamber at a particular temperature. As part of this study, a preliminary evaluation of calibration units from five vendors was made. The work was performed by NIST in Gaithersburg, MD and Joe Rovani from WRI who traveled to NIST as a Visiting Scientist.

  18. Savannah River Plant Californium-252 Shuffler software manual

    International Nuclear Information System (INIS)

    Johnson, S.S.; Crane, T.W.; Eccleston, G.W.

    1979-03-01

    A software manual for operating the Savannah River Plant Shuffler nondestructive assay instrument is presented. The procedures for starting up the instrument, making assays, calibrating, and checking the performance of the hardware units are described. A list of the error messages with an explanation of the circumstances prompting the message and possible corrective measures is given. A summary of the software package is included showing the names and contents of the files and subroutines. The procedure for modifying the software package is outlined

  19. Software compensation in particle flow reconstruction

    Energy Technology Data Exchange (ETDEWEB)

    Tran, Huong Lan; Krueger, Katja; Sefkow, Felix [Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany); Green, Steven; Marshall, John; Thomson, Mark [Cavendish Laboratory, Cambridge (United Kingdom); Simon, Frank [Max-Planck-Institut fuer Physik, Muenchen (Germany)

    2017-10-15

    The particle flow approach to calorimetry benefits from highly granular calorimeters and sophisticated software algorithms in order to reconstruct and identify individual particles in complex event topologies. The high spatial granularity, together with analogue energy information, can be further exploited in software compensation. In this approach, the local energy density is used to discriminate electromagnetic and purely hadronic sub-showers within hadron showers in the detector to improve the energy resolution for single particles by correcting for the intrinsic non-compensation of the calorimeter system. This improvement in the single particle energy resolution also results in a better overall jet energy resolution by improving the energy measurement of identified neutral hadrons and improvements in the pattern recognition stage by a more accurate matching of calorimeter energies to tracker measurements. This paper describes the software compensation technique and its implementation in particle flow reconstruction with the Pandora Particle Flow Algorithm (PandoraPFA). The impact of software compensation on the choice of optimal transverse granularity for the analogue hadronic calorimeter option of the International Large Detector (ILD) concept is also discussed.

  20. Software compensation in particle flow reconstruction

    Energy Technology Data Exchange (ETDEWEB)

    Tran, Huong Lan; Krueger, Katja; Sefkow, Felix [Deutsches Elektronen-Synchrotron DESY, Hamburg (Germany); Green, Steven; Marshall, John; Thomson, Mark [Cavendish Laboratory, Cambridge (United Kingdom); Simon, Frank [Max-Planck-Institut fuer Physik, Muenchen (Germany)

    2017-10-15

    The particle flow approach to calorimetry benefits from highly granular calorimeters and sophisticated software algorithms in order to reconstruct and identify individual particles in complex event topologies. The high spatial granularity, together with analogue energy information, can be further exploited in software compensation. In this approach, the local energy density is used to discriminate electromagnetic and purely hadronic sub-showers within hadron showers in the detector to improve the energy resolution for single particles by correcting for the intrinsic non-compensation of the calorimeter system. This improvement in the single particle energy resolution also results in a better overall jet energy resolution by improving the energy measurement of identified neutral hadrons and improvements in the pattern recognition stage by a more accurate matching of calorimeter energies to tracker measurements. This paper describes the software compensation technique and its implementation in particle flow reconstruction with the Pandora Particle Flow Algorithm (PandoraPFA). The impact of software compensation on the choice of optimal transverse granularity for the analogue hadronic calorimeter option of the International Large Detector (ILD) concept is also discussed. (orig.)

  1. Software compensation in particle flow reconstruction

    International Nuclear Information System (INIS)

    Tran, Huong Lan; Krueger, Katja; Sefkow, Felix; Green, Steven; Marshall, John; Thomson, Mark; Simon, Frank

    2017-10-01

    The particle flow approach to calorimetry benefits from highly granular calorimeters and sophisticated software algorithms in order to reconstruct and identify individual particles in complex event topologies. The high spatial granularity, together with analogue energy information, can be further exploited in software compensation. In this approach, the local energy density is used to discriminate electromagnetic and purely hadronic sub-showers within hadron showers in the detector to improve the energy resolution for single particles by correcting for the intrinsic non-compensation of the calorimeter system. This improvement in the single particle energy resolution also results in a better overall jet energy resolution by improving the energy measurement of identified neutral hadrons and improvements in the pattern recognition stage by a more accurate matching of calorimeter energies to tracker measurements. This paper describes the software compensation technique and its implementation in particle flow reconstruction with the Pandora Particle Flow Algorithm (PandoraPFA). The impact of software compensation on the choice of optimal transverse granularity for the analogue hadronic calorimeter option of the International Large Detector (ILD) concept is also discussed.

  2. CAX a software for automated spectrum analysis

    International Nuclear Information System (INIS)

    Zahn, Guilherme S.; Genezini, Frederico A.

    2017-01-01

    In this work, the scripting capabilities of Genie-2000 were used to develop a software that automatically analyses all spectrum files in either Ortec's CHN or Canberra's MCA or CNF formats in a folder, generating two output files: a print-ready text le (.DAT) and a Comma-Separated Values (.CSV) le which can be easily imported in any major spreadsheet software. This software, named CAX ('Convert and Analyse for eXcel'), uses Genie-2000's functions to import spectrum files into Genie's native CNF format and analyze the converted spectra. The software can also, if requested, import energy and FWHM calibrations from a stored calibrated spectrum. The print-ready output le (.DAT) is generated by Genie-2000 using a customized script, and the CSV le is generated by a custom-built DAT2CSV software which generates a CSV le that complies to the Brazilian standards, with commas as a decimal indicator and semicolons as eld separators. This software is already used in the daily routines in IPEN's Neutron Activation Laboratory, greatly reducing the time required for sample analyses, as well as reducing the possibility of transcription errors. (author)

  3. CAX a software for automated spectrum analysis

    Energy Technology Data Exchange (ETDEWEB)

    Zahn, Guilherme S.; Genezini, Frederico A., E-mail: gzahn@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (CRPq/IPEN/CNEN-SP), Sao Paulo, SP (Brazil). Centro do Reator de Pesquisas

    2017-11-01

    In this work, the scripting capabilities of Genie-2000 were used to develop a software that automatically analyses all spectrum files in either Ortec's CHN or Canberra's MCA or CNF formats in a folder, generating two output files: a print-ready text le (.DAT) and a Comma-Separated Values (.CSV) le which can be easily imported in any major spreadsheet software. This software, named CAX ('Convert and Analyse for eXcel'), uses Genie-2000's functions to import spectrum files into Genie's native CNF format and analyze the converted spectra. The software can also, if requested, import energy and FWHM calibrations from a stored calibrated spectrum. The print-ready output le (.DAT) is generated by Genie-2000 using a customized script, and the CSV le is generated by a custom-built DAT2CSV software which generates a CSV le that complies to the Brazilian standards, with commas as a decimal indicator and semicolons as eld separators. This software is already used in the daily routines in IPEN's Neutron Activation Laboratory, greatly reducing the time required for sample analyses, as well as reducing the possibility of transcription errors. (author)

  4. Field calibration of cup anemometers

    DEFF Research Database (Denmark)

    Schmidt Paulsen, Uwe; Mortensen, Niels Gylling; Hansen, Jens Carsten

    2007-01-01

    A field calibration method and results are described along with the experience gained with the method. The cup anemometers to be calibrated are mounted in a row on a 10-m high rig and calibrated in the free wind against a reference cup anemometer. The method has been reported [1] to improve...... the statistical bias on the data relative to calibrations carried out in a wind tunnel. The methodology is sufficiently accurate for calibration of cup anemometers used for wind resource assessments and provides a simple, reliable and cost-effective solution to cup anemometer calibration, especially suited...

  5. Automatic component calibration and error diagnostics for model-based accelerator control. Phase I final report

    International Nuclear Information System (INIS)

    Carl Stern; Martin Lee

    1999-01-01

    Phase I work studied the feasibility of developing software for automatic component calibration and error correction in beamline optics models. A prototype application was developed that corrects quadrupole field strength errors in beamline models

  6. Automatic component calibration and error diagnostics for model-based accelerator control. Phase I final report

    CERN Document Server

    Carl-Stern

    1999-01-01

    Phase I work studied the feasibility of developing software for automatic component calibration and error correction in beamline optics models. A prototype application was developed that corrects quadrupole field strength errors in beamline models.

  7. A single model procedure for estimating tank calibration equations

    International Nuclear Information System (INIS)

    Liebetrau, A.M.

    1997-10-01

    A fundamental component of any accountability system for nuclear materials is a tank calibration equation that relates the height of liquid in a tank to its volume. Tank volume calibration equations are typically determined from pairs of height and volume measurements taken in a series of calibration runs. After raw calibration data are standardized to a fixed set of reference conditions, the calibration equation is typically fit by dividing the data into several segments--corresponding to regions in the tank--and independently fitting the data for each segment. The estimates obtained for individual segments must then be combined to obtain an estimate of the entire calibration function. This process is tedious and time-consuming. Moreover, uncertainty estimates may be misleading because it is difficult to properly model run-to-run variability and between-segment correlation. In this paper, the authors describe a model whose parameters can be estimated simultaneously for all segments of the calibration data, thereby eliminating the need for segment-by-segment estimation. The essence of the proposed model is to define a suitable polynomial to fit to each segment and then extend its definition to the domain of the entire calibration function, so that it (the entire calibration function) can be expressed as the sum of these extended polynomials. The model provides defensible estimates of between-run variability and yields a proper treatment of between-segment correlations. A portable software package, called TANCS, has been developed to facilitate the acquisition, standardization, and analysis of tank calibration data. The TANCS package was used for the calculations in an example presented to illustrate the unified modeling approach described in this paper. With TANCS, a trial calibration function can be estimated and evaluated in a matter of minutes

  8. ESTSC - Software Best Practices

    Science.gov (United States)

    DOE Scientific and Technical Software Best Practices December 2010 Table of Contents 1.0 Introduction 2.0 Responsibilities 2.1 OSTI/ESTSC 2.2 SIACs 2.3 Software Submitting Sites/Creators 2.4 Software Sensitivity Review 3.0 Software Announcement and Submission 3.1 STI Software Appropriate for Announcement 3.2

  9. Software Assurance Competency Model

    Science.gov (United States)

    2013-03-01

    COTS) software , and software as a service ( SaaS ). L2: Define and analyze risks in the acquisition of contracted software , COTS software , and SaaS ...2010a]: Application of technologies and processes to achieve a required level of confidence that software systems and services function in the...

  10. Software attribute visualization for high integrity software

    Energy Technology Data Exchange (ETDEWEB)

    Pollock, G.M.

    1998-03-01

    This report documents a prototype tool developed to investigate the use of visualization and virtual reality technologies for improving software surety confidence. The tool is utilized within the execution phase of the software life cycle. It provides a capability to monitor an executing program against prespecified requirements constraints provided in a program written in the requirements specification language SAGE. The resulting Software Attribute Visual Analysis Tool (SAVAnT) also provides a technique to assess the completeness of a software specification.

  11. Individual dosimetry and calibration

    International Nuclear Information System (INIS)

    Otto, T.

    1997-01-01

    In 1996, the Dosimetry and Calibration Section was, as in previous years, mainly engaged in routine tasks: the distribution of over 6000 dosimeters (with a total of more than 10,000 films) every two months and the calibration of about 900 fixed and mobile instruments used in the radiation survey sections of RP group. These tasks were, thanks to an experienced team, well mastered. Special efforts had to be made in a number of areas to modernize the service or to keep it in line with new prescriptions. The Individual Dosimetry Service had to assure that CERN's contracting firms comply with the prescriptions in the Radiation Safety Manual (1996) that had been inspired by the Swiss Ordinance of 1994: Companies must file for authorizations with the Swiss Federal Office for Public Health requiring that in every company an 'Expert in Radiation Protection' be nominated and subsequently trained. CERN's Individual Dosimetry Service is accredited by the Swiss Federal Authorities and works closely together with other, similar services on a rigorous quality assurance programme. Within this framework, CERN was mandated to organize this year the annual Swiss 'Intercomparison of Dosimeters'. All ten accredited dosimetry services - among others those of the Paul Scherrer Institute (PSI) in Villigen and of the four Swiss nuclear power stations - sent dosimeters to CERN, where they were irradiated in CERN's calibration facility with precise photon doses. After return to their origin they were processed and evaluated. The results were communicated to CERN and were compared with the originally given doses. A report on the results was subsequently prepared and submitted to the Swiss 'Group of Experts on Personal Dosimetry'. Reference monitors for photon and neutron radiation were brought to standard laboratories to assure the traceability of CERN's calibration service to the fundamental quantities. For photon radiation, a set of ionization chambers was calibrated in the reference field

  12. New approach for calibration the efficiency of HPGe detectors

    International Nuclear Information System (INIS)

    Alnour, I.A.; Wagiran, H.; Suhaimi Hamzah; Siong, W.B.; Mohd Suhaimi Elias

    2013-01-01

    Full-text: This work evaluates the efficiency calibrating of HPGe detector coupled with Canberra GC3018 with Genie 2000 software and Ortec GEM25-76-XLB-C with Gamma Vision software; available at Neutron activation analysis laboratory in Malaysian Nuclear Agency (NM). The efficiency calibration curve was constructed from measurement of an IAEA, standard gamma point sources set composed by 214 Am, 57 Co, 133 Ba, 152 Eu, 137 Cs and 60 Co. The efficiency calibrations were performed for three different geometries: 5, 10 and 15 cm distances from the end cap detector. The polynomial parameters functions were simulated through a computer program, MATLAB in order to find an accurate fit to the experimental data points. The efficiency equation was established from the known fitted parameters which allow for the efficiency evaluation at particular energy of interest. The study shows that significant deviations in the efficiency, depending on the source-detector distance and photon energy. (author)

  13. The contribution to the calibration of LAr calorimeters at the ATLAS experiment

    International Nuclear Information System (INIS)

    Pecsy, M.

    2011-01-01

    The presented thesis brings various contributions to the testing and validation of the ATLAS detector calorimeter calibration. Since the ATLAS calorimeter is non-compensating, the sophisticated software calibration of the calorimeter response is needed. One of the ATLAS official calibration methods is the local hadron calibration. This method is based on detailed simulations providing information about the true deposited energy in calorimeter. Such calibration consists of several independent steps, starting with the basic electromagnetic scale signal calibration and proceeding to the particle energy calibration. Calibration starts from the topological clusters reconstruction and calibration at EM scale. These clusters are classified as EM or hadronic and the hadronic ones receive weights to correct for the invisible energy deposits of hadrons. To get the nal reconstructed energy the out-of-cluster and dead material corrections are applied in next steps. The tests of calorimeter response with the rst real data from cosmic-ray muons and the LHC collisions data are presented in the thesis. The detailed studies of the full hadronic calibration performance in the special combined end-cap calorimeter beam test 2004 are presented as well. To optimise the performance of the calibration, the Monte-Carlo based studies are necessary. Two alternative methods of cluster classification are discussed, and the software tool of particle track extrapolation has been developed. (author)

  14. Quantifying low amorphous or crystalline amounts of alpha-lactose-monohydrate using X-ray powder diffraction, near-infrared spectroscopy, and differential scanning calorimetry.

    Science.gov (United States)

    Fix, I; Steffens, K J

    2004-05-01

    Efficient and accurate quantification of low amorphous and crystalline contents within pharmaceutical materials still remains a challenging task in the pharmaceutical industry. Since X-ray powder diffraction (XRPD) equipment has improved in recent years, our aim was 1) to investigate the possibility of substantially lowering the detection limits of amorphous or crystalline material to about 1% or 0.5% w/w respectively by applying conventional Bragg Brentano optics, combined with a fast and simple evaluation technique; 2) to perform these measurements within a short time to make it suitable for routine analysis; and 3) to subject the same data sets to a partial least squares regression (PLSR) in order to investigate whether it is possible to improve accuracy and precision compared to the standard integration method. Near-infrared spectroscopy (NIRS) and differential scanning calorimetry (DSC) were chosen as reference method. As model substance, alpha lactose monohydrate was chosen to create calibration curves based on predetermined mixtures of highly crystalline and amorphous substance. In contrast to DSC, XRPD and NIRS revealed an excellent linearity, precision, and accuracy with the percent of crystalline amount and a detectability down to about 0.5% w/w. Chemometric evaluation (partial least squares regression) applied to the XRPD data further improved the quality of our calibration.

  15. Calibration of a complex activated sludge model for the full-scale wastewater treatment plant

    OpenAIRE

    Liwarska-Bizukojc, Ewa; Olejnik, Dorota; Biernacki, Rafal; Ledakowicz, Stanislaw

    2011-01-01

    In this study, the results of the calibration of the complex activated sludge model implemented in BioWin software for the full-scale wastewater treatment plant are presented. Within the calibration of the model, sensitivity analysis of its parameters and the fractions of carbonaceous substrate were performed. In the steady-state and dynamic calibrations, a successful agreement between the measured and simulated values of the output variables was achieved. Sensitivity analysis revealed that u...

  16. MAVEN SEP Calibrated Data Bundle

    Data.gov (United States)

    National Aeronautics and Space Administration — The maven.sep.calibrated Level 2 Science Data Bundle contains fully calibrated SEP data, as well as the raw count data from which they are derived, and ancillary...

  17. Ultrasonic calibration assembly

    International Nuclear Information System (INIS)

    1981-01-01

    Ultrasonic transducers for in-service inspection of nuclear reactor vessels have several problems associated with them which this invention seeks to overcome. The first is that of calibration or referencing a zero start point for the vertical axis of transducer movement to locate a weld defect. The second is that of verifying the positioning (vertically or at a predetermined angle). Thirdly there is the problem of ascertaining the speed per unit distance in the operating medium of the transducer beam prior to the actual inspection. The apparatus described is a calibration assembly which includes a fixed, generally spherical body having a surface for reflecting an ultrasonic beam from one of the transducers which can be moved until the reflection from the spherical body is the highest amplitude return signal indicating radial alignment from the body. (U.K.)

  18. Travelling gradient thermocouple calibration

    International Nuclear Information System (INIS)

    Broomfield, G.H.

    1975-01-01

    A short discussion of the origins of the thermocouple EMF is used to re-introduce the idea that the Peltier and Thompson effects are indistinguishable from one another. Thermocouples may be viewed as devices which generate an EMF at junctions or as integrators of EMF's developed in thermal gradients. The thermal gradient view is considered the more appropriate, because of its better accord with theory and behaviour, the correct approach to calibration, and investigation of service effects is immediately obvious. Inhomogeneities arise in thermocouples during manufacture and in service. The results of travelling gradient measurements are used to show that such effects are revealed with a resolution which depends on the length of the gradient although they may be masked during simple immersion calibration. Proposed tests on thermocouples irradiated in a nuclear reactor are discussed

  19. Picosecond calorimetry

    DEFF Research Database (Denmark)

    Georgiou, Panayiotis; Vincent, Jonathan; Andersson, Magnus

    2006-01-01

    to rapidly heat liquid C H2 Cl2 using UV pulses of 100 fs duration. A significant x-ray diffraction signal is visible prior to the onset of thermal expansion, which characterizes a highly compressed superheated liquid. Liquid C H2 Cl2 then expands as a shock wave propagates through the sample...

  20. Mesoscale hybrid calibration artifact

    Science.gov (United States)

    Tran, Hy D.; Claudet, Andre A.; Oliver, Andrew D.

    2010-09-07

    A mesoscale calibration artifact, also called a hybrid artifact, suitable for hybrid dimensional measurement and the method for make the artifact. The hybrid artifact has structural characteristics that make it suitable for dimensional measurement in both vision-based systems and touch-probe-based systems. The hybrid artifact employs the intersection of bulk-micromachined planes to fabricate edges that are sharp to the nanometer level and intersecting planes with crystal-lattice-defined angles.

  1. Calibration of germanium detectors

    International Nuclear Information System (INIS)

    Bjurman, B.; Erlandsson, B.

    1985-01-01

    This paper describes problems concerning the calibration of germanium detectors for the measurement of gamma-radiation from environmental samples. It also contains a brief description of some ways of reducing the uncertainties concerning the activity determination. These uncertainties have many sources, such as counting statistics, full energy peak efficiency determination, density correction and radionuclide specific-coincidence effects, when environmental samples are investigated at close source-to-detector distances

  2. Calibration of hydrometers

    Science.gov (United States)

    Lorefice, Salvatore; Malengo, Andrea

    2006-10-01

    After a brief description of the different methods employed in periodic calibration of hydrometers used in most cases to measure the density of liquids in the range between 500 kg m-3 and 2000 kg m-3, particular emphasis is given to the multipoint procedure based on hydrostatic weighing, known as well as Cuckow's method. The features of the calibration apparatus and the procedure used at the INRiM (formerly IMGC-CNR) density laboratory have been considered to assess all relevant contributions involved in the calibration of different kinds of hydrometers. The uncertainty is strongly dependent on the kind of hydrometer; in particular, the results highlight the importance of the density of the reference buoyant liquid, the temperature of calibration and the skill of operator in the reading of the scale in the whole assessment of the uncertainty. It is also interesting to realize that for high-resolution hydrometers (division of 0.1 kg m-3), the uncertainty contribution of the density of the reference liquid is the main source of the total uncertainty, but its importance falls under about 50% for hydrometers with a division of 0.5 kg m-3 and becomes somewhat negligible for hydrometers with a division of 1 kg m-3, for which the reading uncertainty is the predominant part of the total uncertainty. At present the best INRiM result is obtained with commercially available hydrometers having a scale division of 0.1 kg m-3, for which the relative uncertainty is about 12 × 10-6.

  3. Calibration of high resolution digital camera based on different photogrammetric methods

    International Nuclear Information System (INIS)

    Hamid, N F A; Ahmad, A

    2014-01-01

    This paper presents method of calibrating high-resolution digital camera based on different configuration which comprised of stereo and convergent. Both methods are performed in the laboratory and in the field calibration. Laboratory calibration is based on a 3D test field where a calibration plate of dimension 0.4 m × 0.4 m with grid of targets at different height is used. For field calibration, it uses the same concept of 3D test field which comprised of 81 target points located on a flat ground and the dimension is 9 m × 9 m. In this study, a non-metric high resolution digital camera called Canon Power Shot SX230 HS was calibrated in the laboratory and in the field using different configuration for data acquisition. The aim of the calibration is to investigate the behavior of the internal digital camera whether all the digital camera parameters such as focal length, principal point and other parameters remain the same or vice-versa. In the laboratory, a scale bar is placed in the test field for scaling the image and approximate coordinates were used for calibration process. Similar method is utilized in the field calibration. For both test fields, the digital images were acquired within short period using stereo and convergent configuration. For field calibration, aerial digital images were acquired using unmanned aerial vehicle (UAV) system. All the images were processed using photogrammetric calibration software. Different calibration results were obtained for both laboratory and field calibrations. The accuracy of the results is evaluated based on standard deviation. In general, for photogrammetric applications and other applications the digital camera must be calibrated for obtaining accurate measurement or results. The best method of calibration depends on the type of applications. Finally, for most applications the digital camera is calibrated on site, hence, field calibration is the best method of calibration and could be employed for obtaining accurate

  4. Reliability of software

    International Nuclear Information System (INIS)

    Kopetz, H.

    1980-01-01

    Common factors and differences in the reliability of hardware and software; reliability increase by means of methods of software redundancy. Maintenance of software for long term operating behavior. (HP) [de

  5. Observation models in radiocarbon calibration

    International Nuclear Information System (INIS)

    Jones, M.D.; Nicholls, G.K.

    2001-01-01

    The observation model underlying any calibration process dictates the precise mathematical details of the calibration calculations. Accordingly it is important that an appropriate observation model is used. Here this is illustrated with reference to the use of reservoir offsets where the standard calibration approach is based on a different model to that which the practitioners clearly believe is being applied. This sort of error can give rise to significantly erroneous calibration results. (author). 12 refs., 1 fig

  6. Self consistently calibrated photopyroelectric calorimeter for the high resolution simultaneous absolute measurement of the specific heat and of the thermal conductivity

    Directory of Open Access Journals (Sweden)

    U. Zammit

    2012-03-01

    Full Text Available High temperature resolution study of the specific heat and of the thermal conductivity over the smecticA-nematic and nematic-isotropic phase transitions in octylcynobephenyl liquid crystal using a new photopyroelectric calorimetry configuration are reported, where, unlike previously adopted ones, no calibration is required other than the procedure used during the actual measurement. This makes photopyroelectric calorimetry suitable for “absolute” measurements of the thermal parameters like most other existing conventional calorimetric techniques where, however, the thermal conductivity cannot be measured.

  7. Calibrated Properties Model

    International Nuclear Information System (INIS)

    Ghezzehej, T.

    2004-01-01

    The purpose of this model report is to document the calibrated properties model that provides calibrated property sets for unsaturated zone (UZ) flow and transport process models (UZ models). The calibration of the property sets is performed through inverse modeling. This work followed, and was planned in, ''Technical Work Plan (TWP) for: Unsaturated Zone Flow Analysis and Model Report Integration'' (BSC 2004 [DIRS 169654], Sections 1.2.6 and 2.1.1.6). Direct inputs to this model report were derived from the following upstream analysis and model reports: ''Analysis of Hydrologic Properties Data'' (BSC 2004 [DIRS 170038]); ''Development of Numerical Grids for UZ Flow and Transport Modeling'' (BSC 2004 [DIRS 169855]); ''Simulation of Net Infiltration for Present-Day and Potential Future Climates'' (BSC 2004 [DIRS 170007]); ''Geologic Framework Model'' (GFM2000) (BSC 2004 [DIRS 170029]). Additionally, this model report incorporates errata of the previous version and closure of the Key Technical Issue agreement TSPAI 3.26 (Section 6.2.2 and Appendix B), and it is revised for improved transparency

  8. Comparison of calorimetry and destructive analytical measurement techniques for excess plutonium powders

    International Nuclear Information System (INIS)

    Welsh, T.L.

    1996-01-01

    In Dec. 1994, IAEA safeguards were initiated on inventory of Pu- bearing materials, originating from the US nuclear weapons complex, at vault 3 of DOE's Plutonium Finishing Plant at Hanford. Because of the diversity and heterogeneity of the Pu, plant operators have increasingly used calorimetry for accountability measurements. During the recent commencement of IAEA safeguards at vault 3, destructive (electrochemical titration) methods were used to determine Pu concentrations in subsamples of inventory items with widely ranging chemical purities. The Pu concentrations in the subsamples were determined and contribution of heterogeneity to total variability was identified. Measurement results, gathered by PFP and IAEA laboratories, showed total measurement variability for calorimetry to be comparable with or lower than those of sampling and chemical analyses

  9. Application of isothermal calorimetry and uv spectroscopy for stability monitoring of pentaerythritol tetranitrate

    International Nuclear Information System (INIS)

    Dosser, L.R.; Pickard, J.M.

    1992-01-01

    Thermal stabilities for a series of pentaerythritol-tetranitrate (PETN) samples with variable surf ace areas were monitored by isothermal calorimetry and UV spectroscopy over the temperature range of 363 to 408 K. Isothermal induction times measured with constant volume calorimetry under an air atmosphere and No evolution rates monitored by UV absorbance at 213 nm under vacuum correlated with the PETN surface area at temperatures equal to or exceeding 383 K. Rate data measured at 383 K are in accord with predictions based on detailed kinetic modeling. Below 383 K, NO evolution data suggested that additional geometric factors may be significant in controlling PETN stability. Mechanisms for influencing surface area upon the rate-determining step are addressed

  10. Laser Calorimetry Spectroscopy for ppm-level Dissolved Gas Detection and Analysis.

    Science.gov (United States)

    K S, Nagapriya; Sinha, Shashank; R, Prashanth; Poonacha, Samhitha; Chaudhry, Gunaranjan; Bhattacharya, Anandaroop; Choudhury, Niloy; Mahalik, Saroj; Maity, Sandip

    2017-02-20

    In this paper we report a newly developed technique - laser calorimetry spectroscopy (LCS), which is a combination of laser absorption spectroscopy and calorimetry - for the detection of gases dissolved in liquids. The technique involves determination of concentration of a dissolved gas by irradiating the liquid with light of a wavelength where the gas absorbs, and measuring the temperature change caused by the absorbance. Conventionally, detection of dissolved gases with sufficient sensitivity and specificity was done by first extracting the gases from the liquid and then analyzing the gases using techniques such as gas chromatography. Using LCS, we have been able to detect ppm levels of dissolved gases without extracting them from the liquid. In this paper, we show the detection of dissolved acetylene in transformer oil in the mid infrared (MIR) wavelength (3021 nm) region.

  11. Modulated Temperature Differential Scanning Calorimetry Theoretical and Practical Applications in Polymer Characterisation

    CERN Document Server

    Reading, Mike

    2006-01-01

    MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure ...

  12. Characterization of the phase transformations in shape-memory alloys by modulated differential scanning calorimetry

    International Nuclear Information System (INIS)

    Wei, Z.G.; Sandstroem, R.

    1999-01-01

    Modulated differential scanning calorimetry (MDSC) is a recently developed calorimetric technique, which has demonstrated some significant advantages over the conventional differential scanning calorimetry (DSC). By separating the reversing quantity from the non-reversing component in the total thermal events, it provides some new information that can not be obtained from the conventional DSC. The technique has been applied to various polycrystalline and single crystalline shape-memory alloys, including Cu-Zn-Al, Cu-Al-Ni, Ti-Ni(Cu), Ni-Mn-Ga and Fe-Mn-Si, to characterize the martensitic transformations, bainitic transformation, chemical and magnetic ordering transitions, atomic reordering and other kinetic relaxation processes in the alloys. The preliminary results of the MDSC measurements are summarized and the interpretation of the MDSC results and some factors affecting the results are discussed. (orig.)

  13. Inherent limitations of fixed-time, servo-controlled radiometric calorimetry

    International Nuclear Information System (INIS)

    Wetzel, J.R.; Lemming, J.F.; Duff, M.F.

    1987-01-01

    Interest has been shown in using fixed-time, servo-controlled calorimetry to shorten the measurement times for certain samples that require low precision values (3 to 5%). This type of calorimeter measurement could be particularly useful for screening scrap samples to determine whether there is a need for a more accurate measurement or for certain confirmatory measurements for which low precision numbers are sufficient. The equipment required for this type of measurement is a servo-controlled calorimeter and a preconditioning unit. Samples to be measured are placed in the preconditioning unit, which is maintained at the internal temperature of the calorimeter. The power value for the sample is determined at a fixed time after loading into the calorimeter, for example, 30 min. When a calorimeter is operated using a fixed cutoff time, there are additional sources of uncertainty that need to be considered. The major factors affecting the uncertainty of the calorimetry power values are discussed. 2 refs., 4 figs

  14. Space Flight Software Development Software for Intelligent System Health Management

    Science.gov (United States)

    Trevino, Luis C.; Crumbley, Tim

    2004-01-01

    The slide presentation examines the Marshall Space Flight Center Flight Software Branch, including software development projects, mission critical space flight software development, software technical insight, advanced software development technologies, and continuous improvement in the software development processes and methods.

  15. Precision tracking and electromagnetic calorimetry towards a measurement of the pion polarisabilities at COMPASS

    Energy Technology Data Exchange (ETDEWEB)

    Dinkelbach, Anna-Maria Elisabeth

    2010-07-20

    In 2004 the COMPASS experiment at CERN SPS measured soft reactions with a beam of negatively charged pions on various nuclear targets. For this measurement, a silicon micro-strip telescope was installed in the target region. For the first time 5 silicon detector stations were operated simultaneously in the COMPASS experiment. A novel method of time calibration, with a clustering algorithm accordingly adapted, and refined alignment corrections were implemented in the analysis software. The spatial resolution of a silicon detector was determined to be 5 - 14 {mu}m and the time resolution 2 - 3 ns. Combining the time information of all stations, a track time resolution of 530 ps from the silicon telescope could be reached. One of the key points of this experiment was the observation of Primakoff events, namely pions scattering off quasi-real photons in the Coulomb field of a heavy nucleus. The production of real photons corresponds to pion Compton scattering in inverse kinematics which is sensitive to the pion polarisabilities {alpha}{sub {pi}} and {beta}{sub {pi}}. Key ingredient for such measurements is a precise knowledge of the performance of the electromagnetic calorimeter. This includes a study of the instabilities of calorimeter cells and an improved reconstruction algorithm. A data-driven shower model was developed, which was used for a timedependent recalibration of the calorimeter. A new cluster refitting method was used to recover position and energy of clusters containing passive or saturated cells and detects double-hit clusters. The latter are important, as the main background to the Primakoff Compton events stems from neutral pions misinterpreted as single-photon hits. The physics analysis comprised the selection of Primakoff events and the necessary steps to obtain the pionic polarisabilities. The measurement was limited by systematic effects of the apparatus also determined within this thesis. (orig.)

  16. Software Engineering Guidebook

    Science.gov (United States)

    Connell, John; Wenneson, Greg

    1993-01-01

    The Software Engineering Guidebook describes SEPG (Software Engineering Process Group) supported processes and techniques for engineering quality software in NASA environments. Three process models are supported: structured, object-oriented, and evolutionary rapid-prototyping. The guidebook covers software life-cycles, engineering, assurance, and configuration management. The guidebook is written for managers and engineers who manage, develop, enhance, and/or maintain software under the Computer Software Services Contract.

  17. Immersion Calorimetry for the Characterization of PD Catalysts Supported on Activated Carbon

    Directory of Open Access Journals (Sweden)

    Liliana Giraldo

    2009-01-01

    Full Text Available Activated carbons obtained from coconut peel were oxidized using hydrogen peroxide. Superficial characteristics of these carbons were determined through N2 and CO2 isotherms and functional groups were characterized by TPD. Finally, the microcalorimetry technique was used in order to obtain the immersion enthalpies in diverse liquids and established the relation between them and the results obtained by the other characterization techniques. The results suggested that the immersion calorimetry allow establishing the difference between the supports and the catalysts.

  18. Monitoring of an RNA Multistep Folding Pathway by Isothermal Titration Calorimetry

    OpenAIRE

    Reymond, Cédric; Bisaillon, Martin; Perreault, Jean-Pierre

    2009-01-01

    Isothermal titration calorimetry was used to monitor the energetic landscape of a catalytic RNA, specifically that of the hepatitis delta virus ribozyme. Using mutants that isolated various tertiary interactions, the thermodynamic parameters of several ribozyme-substrate intermediates were determined. The results shed light on the impact of several tertiary interactions on the global structure of the ribozyme. In addition, the data indicate that the formation of the P1.1 pseudoknot is the lim...

  19. Low-temperature heat capacity of small Nb3Sn polycrystals by ac calorimetry

    International Nuclear Information System (INIS)

    Viswanathan, R.; Johnston, D.C.

    1976-01-01

    It is shown by an ac calorimetry technique that the multiple heat capacity anomalies which occur below the superconducting transition temperature for small polycrystalline Nb 3 Sn samples are intrinsic to these samples. The recent suggestions that shear stresses can account for these results are analyzed for their validity. The dependence of the occurrence of these multiple anomalies upon the thermal history of the samples was investigated

  20. A survey of the year 2007 literature on applications of isothermal titration calorimetry

    OpenAIRE

    Bjelic, S; Jelesarov, I

    2008-01-01

    Elucidation of the energetic principles of binding affinity and specificity is a central task in many branches of current sciences: biology, medicine, pharmacology, chemistry, material sciences, etc. In biomedical research, integral approaches combining structural information with in-solution biophysical data have proved to be a powerful way toward understanding the physical basis of vital cellular phenomena. Isothermal titration calorimetry (ITC) is a valuable experimental tool facilitating ...

  1. Photothermal beam deflection calorimetry in solution photochemistry: recent progress and future prospects.

    Science.gov (United States)

    Falvey, D E

    1997-01-01

    Photothermal beam deflection (PBD) calorimetry is a technique that measures changes in the solvent's refractive index that accompanies photothermal heating. This method is capable of extracting both kinetic and thermodynamic information from photochemical reactions. A qualitative description of physical basis of time-resolved PBD is presented. Several recent examples of its application to photochemical and photobiological problems are discussed. Finally, the advantages and limitations of PBD are described.

  2. Application of calorimetry in evaluation of phase transformations in the selected hypoeutectic silumins

    Directory of Open Access Journals (Sweden)

    J. Szymszal

    2009-04-01

    Full Text Available The investigations of phase transformations described in this study were carried out on hypoeutectic alloys from the Al-Si during heating and cooling. The determination and analysis of characteristic temperature values from the solidification range was made by the DSC method in calorimetric investigations carried out on a high-temperature multi HTC Setaram scanning calorimeter. Applying the lever rule, the phase composition of the examined slumins was calculated and compared with the results of DSC calorimetry.

  3. A bipolar monolithic preamplifier for high-capacitance SSC [Superconducting Super Collider] silicon calorimetry

    International Nuclear Information System (INIS)

    Britton, C.L. Jr.; Kennedy, E.J.; Bugg, W.M.

    1990-01-01

    This paper describes a preamplifier designed and fabricated specifically to address the requirements of silicon calorimetry for the Superconducting Super Collider (SSC). The topology and its features are discussed in addition to the design methodology employed. The simulated and measured results for noise, power consumption, and speed are presented. Simulated an measured data for radiation damage effects as well as data for post-damage annealing are also presented. 8 refs., 7 figs., 2 tabs

  4. Advanced forward calorimetry for the SSC and TeVatron collider

    International Nuclear Information System (INIS)

    DiBitonto, D.; Van Peteghem, P.M.; Geiger, R.L.; McIntyre, P.M.; Pang, Y.; Thane, J.M.; White, J.T.; Atac, M.

    1989-01-01

    We describe a project to develop fast, radiation hardened forward calorimetry for the SSC and TeVatron collider. Detector technologies discussed are based on gas and warm liquid media. In particular, we present the design of an ultrasensitive hybrid charge preamplifier for liquid technology capable of operating at 0.1-1 GHz. The actual detector bandwidth will depend on the choice of detector media used and the maximum allowable operating high voltage. (orig.)

  5. Recent advances and potential applications of modulated differential scanning calorimetry (mDSC) in drug development

    DEFF Research Database (Denmark)

    Knopp, Matthias Manne; Löbmann, Korbinian; Elder, David P.

    2016-01-01

    Differential scanning calorimetry (DSC) is frequently the thermal analysis technique of choice within preformulation and formulation sciences because of its ability to provide detailed information about both the physical and energetic properties of a substance and/or formulation. However, convent......-dried formulations. However, as discussed in the present review, a number of other potential applications could also be relevant for the pharmaceutical scientist....

  6. Determination of the aggregation number for micelles by isothermal titration calorimetry

    DEFF Research Database (Denmark)

    Olesen, Niels Erik; Holm, Rene; Westh, Peter

    2014-01-01

    Isothermal titration calorimetry (ITC) has previously been applied to estimate the aggregation number (n), Gibbs free energy (ΔG), enthalpy (ΔH) and entropy (ΔS) of micellization. However, some difficulties of micelle characterization by ITC still remain; most micelles have aggregation numbers...... insight into optimal design of titration protocols for micelle characterization. By applying the new method, the aggregation number of sodium dodecyl sulphate and glycochenodeoxycholate was determined at concentrations around their critical micelle concentration (CMC)...

  7. Trigger Algorithms for Alignment and Calibration at the CMS Experiment

    CERN Document Server

    Fernandez Perez Tomei, Thiago Rafael

    2017-01-01

    The data needs of the Alignment and Calibration group at the CMS experiment are reasonably different from those of the physics studies groups. Data are taken at CMS through the online event selection system, which is implemented in two steps. The Level-1 Trigger is implemented on custom-made electronics and dedicated to analyse the detector information at a coarse-grained scale, while the High Level Trigger (HLT) is implemented as a series of software algorithms, running in a computing farm, that have access to the full detector information. In this paper we describe the set of trigger algorithms that is deployed to address the needs of the Alignment and Calibration group, how it fits in the general infrastructure of the HLT, and how it feeds the Prompt Calibration Loop (PCL), allowing for a fast turnaround for the alignment and calibration constants.

  8. Indirect calorimetry in nutritional therapy. A position paper by the ICALIC study group.

    Science.gov (United States)

    Oshima, Taku; Berger, Mette M; De Waele, Elisabeth; Guttormsen, Anne Berit; Heidegger, Claudia-Paula; Hiesmayr, Michael; Singer, Pierre; Wernerman, Jan; Pichard, Claude

    2017-06-01

    This review aims to clarify the use of indirect calorimetry (IC) in nutritional therapy for critically ill and other patient populations. It features a comprehensive overview of the technical concepts, the practical application and current developments of IC. Pubmed-referenced publications were analyzed to generate an overview about the basic knowledge of IC, to describe advantages and disadvantages of the current technology, to clarify technical issues and provide pragmatic solutions for clinical practice and metabolic research. The International Multicentric Study Group for Indirect Calorimetry (ICALIC) has generated this position paper. IC can be performed in in- and out-patients, including those in the intensive care unit, to measure energy expenditure (EE). Optimal nutritional therapy, defined as energy prescription based on measured EE by IC has been associated with better clinical outcome. Equations based on simple anthropometric measurements to predict EE are inaccurate when applied to individual patients. An ongoing international academic initiative to develop a new indirect calorimeter aims at providing innovative and affordable technical solutions for many of the current limitations of IC. Indirect calorimetry is a tool of paramount importance, necessary to optimize the nutrition therapy of patients with various pathologies and conditions. Recent technical developments allow broader use of IC for in- and out-patients. Copyright © 2016 Elsevier Ltd and European Society for Clinical Nutrition and Metabolism. All rights reserved.

  9. CALOR2012 XVth International Conference on Calorimetry in High Energy Physics

    Energy Technology Data Exchange (ETDEWEB)

    Akchurin, Nural .

    2015-05-04

    The International Conferences on Calorimetry in High Energy Physics, or the CALOR series, have always been where the calorimeter experts come together to review the state of calorimetry and bring forth new ideas every two years. The fteenth conference, CALOR2012, in Santa Fe was no exception. Although they were built roughly a decade ago, we are now witnessing the exceptional power of the LHC calorimeters and the crucial role they have been playing in the discovery of the 125 GeV Higgs-like boson. As we ruminate on the coming generation of experiments at the next (linear) collider and on the upgrades at the LHC, we are heartened by the substantial advances we made in calorimetry in the last decade. These advances will certainly help uncover new physics in the years to come, not only at colliders but also in astroparticle experiments that take advantage of natural elements such as air, water, and ice. The proceedings were published by the IOP in Journal of Physics, Vol 404 2011. The conference web site is calor2012.ttu.edu.

  10. Recent DIII-D neutral beam calibration results

    International Nuclear Information System (INIS)

    Wight, J.; Hong, R.M.; Phillips, J.

    1991-10-01

    Injected DIII-D neutral beam power is estimated based on three principle quantities: the fraction of ion beam that is neutralized in the neutralizer gas cell, the beamline transmission efficiency, and the fraction of beam reionized in the drift duct. System changes in the past few years have included a new gradient grid voltage operating point, ion source arc regulation, routine deuterium operations and new neutralizer gas flow controllers. Additionally, beam diagnostics have been improved and better calibrated. To properly characterize the beams the principle quantities have been re-measured. Two diagnostics are primarily used to measure the quantities. The beamline waterflow calorimetry system measures the neutralization efficiency and the beamline transmission efficiency, and the target tile thermocouples measure the reionization loss. An additional diagnostic, the target tile pyrometer, confirmed the reionization loss measurement. Descriptions and results of these measurements will be presented. 4 refs., 5 figs., 2 tabs

  11. Ionic liquids. Combination of combustion calorimetry with high-level quantum chemical calculations for deriving vaporization enthalpies.

    Science.gov (United States)

    Emel'yanenko, Vladimir N; Verevkin, Sergey P; Heintz, Andreas; Schick, Christoph

    2008-07-10

    In this work, the molar enthalpies of formation of the ionic liquids [C2MIM][NO3] and [C4MIM][NO3] were measured by means of combustion calorimetry. The molar enthalpy of fusion of [C2MIM][NO3] was measured using differential scanning calorimetry. Ab initio calculations of the enthalpy of formation in the gaseous phase have been performed for the ionic species using the G3MP2 theory. We have used a combination of traditional combustion calorimetry with modern high-level ab initio calculations in order to obtain the molar enthalpies of vaporization of a series of the ionic liquids under study.

  12. The Chandra Source Catalog 2.0: Calibrations

    Science.gov (United States)

    Graessle, Dale E.; Evans, Ian N.; Rots, Arnold H.; Allen, Christopher E.; Anderson, Craig S.; Budynkiewicz, Jamie A.; Burke, Douglas; Chen, Judy C.; Civano, Francesca Maria; D'Abrusco, Raffaele; Doe, Stephen M.; Evans, Janet D.; Fabbiano, Giuseppina; Gibbs, Danny G., II; Glotfelty, Kenny J.; Grier, John D.; Hain, Roger; Hall, Diane M.; Harbo, Peter N.; Houck, John C.; Lauer, Jennifer L.; Laurino, Omar; Lee, Nicholas P.; Martínez-Galarza, Juan Rafael; McCollough, Michael L.; McDowell, Jonathan C.; Miller, Joseph; McLaughlin, Warren; Morgan, Douglas L.; Mossman, Amy E.; Nguyen, Dan T.; Nichols, Joy S.; Nowak, Michael A.; Paxson, Charles; Plummer, David A.; Primini, Francis Anthony; Siemiginowska, Aneta; Sundheim, Beth A.; Tibbetts, Michael; Van Stone, David W.; Zografou, Panagoula

    2018-01-01

    Among the many enhancements implemented for the release of Chandra Source Catalog (CSC) 2.0 are improvements in the processing calibration database (CalDB). We have included a thorough overhaul of the CalDB software used in the processing. The software system upgrade, called "CalDB version 4," allows for a more rational and consistent specification of flight configurations and calibration boundary conditions. Numerous improvements in the specific calibrations applied have also been added. Chandra's radiometric and detector response calibrations vary considerably with time, detector operating temperature, and position on the detector. The CalDB has been enhanced to provide the best calibrations possible to each observation over the fifteen-year period included in CSC 2.0. Calibration updates include an improved ACIS contamination model, as well as updated time-varying gain (i.e., photon energy) and quantum efficiency maps for ACIS and HRC-I. Additionally, improved corrections for the ACIS quantum efficiency losses due to CCD charge transfer inefficiency (CTI) have been added for each of the ten ACIS detectors. These CTI corrections are now time and temperature-dependent, allowing ACIS to maintain a 0.3% energy calibration accuracy over the 0.5-7.0 keV range for any ACIS source in the catalog. Radiometric calibration (effective area) accuracy is estimated at ~4% over that range. We include a few examples where improvements in the Chandra CalDB allow for improved data reduction and modeling for the new CSC.This work has been supported by NASA under contract NAS 8-03060 to the Smithsonian Astrophysical Observatory for operation of the Chandra X-ray Center.

  13. CALIBRATION PROCEDURES ON OBLIQUE CAMERA SETUPS

    Directory of Open Access Journals (Sweden)

    G. Kemper

    2016-06-01

    Full Text Available Beside the creation of virtual animated 3D City models, analysis for homeland security and city planning, the accurately determination of geometric features out of oblique imagery is an important task today. Due to the huge number of single images the reduction of control points force to make use of direct referencing devices. This causes a precise camera-calibration and additional adjustment procedures. This paper aims to show the workflow of the various calibration steps and will present examples of the calibration flight with the final 3D City model. In difference to most other software, the oblique cameras are used not as co-registered sensors in relation to the nadir one, all camera images enter the AT process as single pre-oriented data. This enables a better post calibration in order to detect variations in the single camera calibration and other mechanical effects. The shown sensor (Oblique Imager is based o 5 Phase One cameras were the nadir one has 80 MPIX equipped with a 50 mm lens while the oblique ones capture images with 50 MPix using 80 mm lenses. The cameras are mounted robust inside a housing to protect this against physical and thermal deformations. The sensor head hosts also an IMU which is connected to a POS AV GNSS Receiver. The sensor is stabilized by a gyro-mount which creates floating Antenna –IMU lever arms. They had to be registered together with the Raw GNSS-IMU Data. The camera calibration procedure was performed based on a special calibration flight with 351 shoots of all 5 cameras and registered the GPS/IMU data. This specific mission was designed in two different altitudes with additional cross lines on each flying heights. The five images from each exposure positions have no overlaps but in the block there are many overlaps resulting in up to 200 measurements per points. On each photo there were in average 110 well distributed measured points which is a satisfying number for the camera calibration. In a first

  14. Calibration of triaxial fluxgate gradiometer

    International Nuclear Information System (INIS)

    Vcelak, Jan

    2006-01-01

    The description of simple and fast calibration procedures used for double-probe triaxial fluxgate gradiometer is provided in this paper. The calibration procedure consists of three basic steps. In the first step both probes are calibrated independently in order to reach constant total field reading in every position. Both probes are numerically aligned in the second step in order that the gradient reading is zero in homogenous magnetic field. The third step consists of periodic drift calibration during measurement. The results and detailed description of each calibration step are presented and discussed in the paper. The gradiometer is finally verified during the detection of the metal object in the measuring grid

  15. Primary calibration in acoustics metrology

    International Nuclear Information System (INIS)

    Milhomem, T A Bacelar; Soares, Z M Defilippo

    2015-01-01

    SI unit in acoustics is realized by the reciprocity calibrations of laboratory standard microphones in pressure field, free field and diffuse field. Calibrations in pressure field and in free field are already consolidated and the Inmetro already done them. Calibration in diffuse field is not yet consolidated, however, some national metrology institutes, including Inmetro, are conducting researches on this subject. This paper presents the reciprocity calibration, the results of Inmetro in recent key comparisons and the research that is being developed for the implementation of reciprocity calibration in diffuse field

  16. Mercury CEM Calibration

    Energy Technology Data Exchange (ETDEWEB)

    John Schabron; Joseph Rovani; Mark Sanderson

    2008-02-29

    Mercury continuous emissions monitoring systems (CEMS) are being implemented in over 800 coal-fired power plant stacks. The power industry desires to conduct at least a full year of monitoring before the formal monitoring and reporting requirement begins on January 1, 2009. It is important for the industry to have available reliable, turnkey equipment from CEM vendors. Western Research Institute (WRI) is working closely with the Electric Power Research Institute (EPRI), the National Institute of Standards and Technology (NIST), and the Environmental Protection Agency (EPA) to facilitate the development of the experimental criteria for a NIST traceability protocol for dynamic elemental mercury vapor generators. The generators are used to calibrate mercury CEMs at power plant sites. The Clean Air Mercury Rule (CAMR) which was published in the Federal Register on May 18, 2005 requires that calibration be performed with NIST-traceable standards (Federal Register 2007). Traceability procedures will be defined by EPA. An initial draft traceability protocol was issued by EPA in May 2007 for comment. In August 2007, EPA issued an interim traceability protocol for elemental mercury generators (EPA 2007). The protocol is based on the actual analysis of the output of each calibration unit at several concentration levels ranging initially from about 2-40 {micro}g/m{sup 3} elemental mercury, and in the future down to 0.2 {micro}g/m{sup 3}, and this analysis will be directly traceable to analyses by NIST. The document is divided into two separate sections. The first deals with the qualification of generators by the vendors for use in mercury CEM calibration. The second describes the procedure that the vendors must use to certify the generator models that meet the qualification specifications. The NIST traceable certification is performance based, traceable to analysis using isotope dilution inductively coupled plasma/mass spectrometry performed by NIST in Gaithersburg, MD. The

  17. The CHEOPS calibration bench

    Science.gov (United States)

    Wildi, F.; Chazelas, B.; Deline, A.; Sarajlic, M.; Sordet, M.

    2017-09-01

    CHEOPS is an ESA Class S Mission aiming at the characterization of exoplanets through the precise measurement of their radius, using the transit method [1]. To achieve this goal, the payload is designed to be a high precision "absolute" photometer, looking at one star at a time. It will be able to cover la large fraction of the sky by repointing. Its launch is expected at the end of 2017 [2, this conference]. CHEOPS' main science is the measure of the transit of exoplanets of radius ranging from 1 to 6 Earth radii orbiting bright stars. The required photometric stability to reach this goal is of 20 ppm in 6 hours for a 9th magnitude star. The CHEOPS' only instrument is a Ritchey-Chretien style telescope with 300 mm effective aperture diameter, which provides a defocussed image of the target star on a single frame-transfer backside illuminated CCD detector cooled to -40°C and stabilized within 10 mK [2]. CHEOPS being in a LEO, it is equipped with a high performance baffle. The spacecraft platform provides a pointing stability of < 2 arcsec rms. This relatively modest pointing performance makes high quality flat-fielding necessary In the rest of this article we will refer to the only CHEOPS instrument simply as "CHEOP" Its behavior will be calibrated thoroughly on the ground and only a small subset of the calibrations can be redone in flight. The main focuses of the calibrations are the photonic gain stability and sensibility to the environment variations and the Flat field that has to be known at a precision better than 0.1%.

  18. CALIBRATED HYDRODYNAMIC MODEL

    Directory of Open Access Journals (Sweden)

    Sezar Gülbaz

    2015-01-01

    Full Text Available The land development and increase in urbanization in a watershed affect water quantityand water quality. On one hand, urbanization provokes the adjustment of geomorphicstructure of the streams, ultimately raises peak flow rate which causes flood; on theother hand, it diminishes water quality which results in an increase in Total SuspendedSolid (TSS. Consequently, sediment accumulation in downstream of urban areas isobserved which is not preferred for longer life of dams. In order to overcome thesediment accumulation problem in dams, the amount of TSS in streams and inwatersheds should be taken under control. Low Impact Development (LID is a BestManagement Practice (BMP which may be used for this purpose. It is a land planningand engineering design method which is applied in managing storm water runoff inorder to reduce flooding as well as simultaneously improve water quality. LID includestechniques to predict suspended solid loads in surface runoff generated over imperviousurban surfaces. In this study, the impact of LID-BMPs on surface runoff and TSS isinvestigated by employing a calibrated hydrodynamic model for Sazlidere Watershedwhich is located in Istanbul, Turkey. For this purpose, a calibrated hydrodynamicmodel was developed by using Environmental Protection Agency Storm WaterManagement Model (EPA SWMM. For model calibration and validation, we set up arain gauge and a flow meter into the field and obtain rainfall and flow rate data. Andthen, we select several LID types such as retention basins, vegetative swales andpermeable pavement and we obtain their influence on peak flow rate and pollutantbuildup and washoff for TSS. Consequently, we observe the possible effects ofLID on surface runoff and TSS in Sazlidere Watershed.

  19. Radionuclide calibrators performance evaluation

    International Nuclear Information System (INIS)

    Mora Ramirez, E.; Zeledon Fonseca, P.; Jimenez Cordero, M.

    2008-01-01

    Radionuclide calibrators are used to estimate accurately activity prior to administration to a patient, so it is very important that this equipment meets its performance requirements. The purpose of this paper is to compare the commercially available 'Calicheck' (Calcorp. Inc), used to assess linearity, versus the well-known source decay method, and also to show our results after performing several recommended quality control tests. The parameters that we wanted to evaluate were carried on using the Capintec CRC-15R and CRC-15 β radionuclide calibrators. The evaluated tests were: high voltage, display, zero adjust, background, reproducibility, source constancy, accuracy, precision and linearity. The first six tests were evaluated on the daily practice, here we analyzed the 2007 recorded data; and the last three were evaluated once a year. During the daily evaluation both calibrators performance were satisfactory comparing with the manufacture's requirements. The accuracy test show result within the ± 10% allowed for a field instrument. Precision performance is within the ± 1 % allowed. On the other hand, the linearity test shows that using the source decay method the relative coefficient is 0.9998, for both equipment and using the Calicheck the relative coefficient is 0.997. However, looking the percentage of error, during the 'Calicheck' test, its range goes from 0.0 % up to -25.35%, and using the source decay method, the range goes from 0.0 % up to -31.05 %, taking into account both instruments. Checking the 'Calicheck' results we can see that the results varying randomly, but using the source decay method the percentage of error increase as the source activity decrease. We conclude that both devices meet its manufactures requirements, in the case of the linearity using the decay method, decreasing the activity source, increasing the percentage of error, this may happen because of the equipment age. (author)

  20. Self-calibrating interferometer

    International Nuclear Information System (INIS)

    Nussmeier, T.A.

    1982-01-01

    A self-calibrating interferometer is disclosed which forms therein a pair of Michelson interferometers with one beam length of each Michelson interferometer being controlled by a common phase shifter. The transfer function measured from the phase shifter to either of a pair of detectors is sinusoidal with a full cycle for each half wavelength of phase shifter travel. The phase difference between these two sinusoidal detector outputs represents the optical phase difference between a path of known distance and a path of unknown distance

  1. Calibration and performance testing of the IAEA Aquila Active Well Coincidence Counter (Unit 1)

    International Nuclear Information System (INIS)

    Menlove, H.O..; Siebelist, R.; Wenz, T.R.

    1996-01-01

    An Active Well Coincidence Counter (AWCC) and a portable shift register (PSR-B) produced by Aquila Technologies Group, Inc., have been tested and cross-calibrated with existing AWCCs used by the International Atomic Energy Agency (IAEA). This report summarizes the results of these tests and the cross-calibration of the detector. In addition, updated tables summarizing the cross-calibration of existing AWCCs and AmLi sources are also included. Using the Aquila PSR-B with existing IAEA software requires secondary software also supplied by Aquila to set up the PSR-B with the appropriate measurement parameters

  2. Ensuring Software IP Cleanliness

    Directory of Open Access Journals (Sweden)

    Mahshad Koohgoli

    2007-12-01

    Full Text Available At many points in the life of a software enterprise, determination of intellectual property (IP cleanliness becomes critical. The value of an enterprise that develops and sells software may depend on how clean the software is from the IP perspective. This article examines various methods of ensuring software IP cleanliness and discusses some of the benefits and shortcomings of current solutions.

  3. Commercial Literacy Software.

    Science.gov (United States)

    Balajthy, Ernest

    1997-01-01

    Presents the first year's results of a continuing project to monitor the availability of software of relevance for literacy education purposes. Concludes there is an enormous amount of software available for use by teachers of reading and literacy--whereas drill-and-practice software is the largest category of software available, large numbers of…

  4. Ensuring Software IP Cleanliness

    OpenAIRE

    Mahshad Koohgoli; Richard Mayer

    2007-01-01

    At many points in the life of a software enterprise, determination of intellectual property (IP) cleanliness becomes critical. The value of an enterprise that develops and sells software may depend on how clean the software is from the IP perspective. This article examines various methods of ensuring software IP cleanliness and discusses some of the benefits and shortcomings of current solutions.

  5. Statistical Software Engineering

    Science.gov (United States)

    1998-04-13

    multiversion software subject to coincident errors. IEEE Trans. Software Eng. SE-11:1511-1517. Eckhardt, D.E., A.K Caglayan, J.C. Knight, L.D. Lee, D.F...J.C. and N.G. Leveson. 1986. Experimental evaluation of the assumption of independence in multiversion software. IEEE Trans. Software

  6. Agile Software Development

    Science.gov (United States)

    Biju, Soly Mathew

    2008-01-01

    Many software development firms are now adopting the agile software development method. This method involves the customer at every level of software development, thus reducing the impact of change in the requirement at a later stage. In this article, the principles of the agile method for software development are explored and there is a focus on…

  7. Improving Software Developer's Competence

    DEFF Research Database (Denmark)

    Abrahamsson, Pekka; Kautz, Karlheinz; Sieppi, Heikki

    2002-01-01

    Emerging agile software development methods are people oriented development approaches to be used by the software industry. The personal software process (PSP) is an accepted method for improving the capabilities of a single software engineer. Five original hypotheses regarding the impact...

  8. Software - Naval Oceanography Portal

    Science.gov (United States)

    are here: Home › USNO › Earth Orientation › Software USNO Logo USNO Navigation Earth Orientation Products GPS-based Products VLBI-based Products EO Information Center Publications about Products Software Search databases Auxiliary Software Supporting Software Form Folder Earth Orientation Matrix Calculator

  9. Software Engineering Education Directory

    Science.gov (United States)

    1990-04-01

    and Engineering (CMSC 735) Codes: GPEV2 * Textiooks: IEEE Tutoria on Models and Metrics for Software Management and Engameeing by Basi, Victor R...Software Engineering (Comp 227) Codes: GPRY5 Textbooks: IEEE Tutoria on Software Design Techniques by Freeman, Peter and Wasserman, Anthony 1. Software

  10. SOFTWARE Manual for VMM3 Slow Control

    CERN Document Server

    Guth, Manuel

    2017-01-01

    For the New Small Wheel upgrade of the ATLAS detector a new readout chip, called VMM3(a), was developed. In order to provide this new technology to a larger community, the RD51 collaboration is integrating the VMM3 in their scalable readout system (SRS). For this purpose, a new slow control and calibration tool is necessary. This new software was developed and improved within a CERN Summer Student project.

  11. Great software debates

    CERN Document Server

    Davis, A

    2004-01-01

    The industry’s most outspoken and insightful critic explains how the software industry REALLY works. In Great Software Debates, Al Davis, shares what he has learned about the difference between the theory and the realities of business and encourages you to question and think about software engineering in ways that will help you succeed where others fail. In short, provocative essays, Davis fearlessly reveals the truth about process improvement, productivity, software quality, metrics, agile development, requirements documentation, modeling, software marketing and sales, empiricism, start-up financing, software research, requirements triage, software estimation, and entrepreneurship.

  12. Immersion calorimetry as a tool to evaluate the catalytic performance of titanosilicate materials in the epoxidation of cyclohexene.

    Science.gov (United States)

    Vernimmen, Jarian; Guidotti, Matteo; Silvestre-Albero, Joaquin; Jardim, Erika O; Mertens, Myrjam; Lebedev, Oleg I; Van Tendeloo, Gustaaf; Psaro, Rinaldo; Rodríguez-Reinoso, Francisco; Meynen, Vera; Cool, Pegie

    2011-04-05

    Different types of titanosilicates are synthesized, structurally characterized, and subsequently catalytically tested in the liquid-phase epoxidation of cyclohexene. The performance of three types of combined zeolitic/mesoporous materials is compared with that of widely studied Ti-grafted-MCM-41 molecular sieve and the TS-1 microporous titanosilicate. The catalytic test results are correlated with the structural characteristics of the different catalysts. Moreover, for the first time, immersion calorimetry with the same substrate molecule as in the catalytic test reaction is applied as an extra means to interpret the catalytic results. A good correlation between catalytic performance and immersion calorimetry results is found. This work points out that the combination of catalytic testing and immersion calorimetry can lead to important insights into the influence of the materials structural characteristics on catalysis. Moreover, the potential of using immersion calorimetry as a screening tool for catalysts in epoxidation reactions is shown.

  13. Dosimetry and Calibration Section

    International Nuclear Information System (INIS)

    Otto, T.

    1999-01-01

    The Dosimetry and Calibration Section fulfils two tasks within CERN's Radiation Protection Group: the Individual Dosimetry Service monitors more than 5000 persons potentially exposed to ionizing radiation on the CERN sites, and the Calibration Laboratory verifies throughout the year, at regular intervals, over 1000 instruments, monitors, and electronic dosimeters used by RP Group. The establishment of a Quality Assurance System for the Individual Dosimetry Service, a requirement of the new Swiss Ordinance for personal dosimetry, put a considerable workload on the section. Together with an external consultant it was decided to identify and then describe the different 'processes' of the routine work performed in the dosimetry service. The resulting Quality Manual was submitted to the Federal Office for Public Health in Bern in autumn. The CERN Individual Dosimetry Service will eventually be officially endorsed after a successful technical test in March 1999. On the technical side, the introduction of an automatic development machine for gamma films was very successful. It processes the dosimetric films without an operator being present, and its built-in regeneration mechanism keeps the concentration of the processing chemicals at a constant level

  14. Piezoelectric trace vapor calibrator

    International Nuclear Information System (INIS)

    Verkouteren, R. Michael; Gillen, Greg; Taylor, David W.

    2006-01-01

    The design and performance of a vapor generator for calibration and testing of trace chemical sensors are described. The device utilizes piezoelectric ink-jet nozzles to dispense and vaporize precisely known amounts of analyte solutions as monodisperse droplets onto a hot ceramic surface, where the generated vapors are mixed with air before exiting the device. Injected droplets are monitored by microscope with strobed illumination, and the reproducibility of droplet volumes is optimized by adjustment of piezoelectric wave form parameters. Complete vaporization of the droplets occurs only across a 10 deg. C window within the transition boiling regime of the solvent, and the minimum and maximum rates of trace analyte that may be injected and evaporated are determined by thermodynamic principles and empirical observations of droplet formation and stability. By varying solution concentrations, droplet injection rates, air flow, and the number of active nozzles, the system is designed to deliver--on demand--continuous vapor concentrations across more than six orders of magnitude (nominally 290 fg/l to 1.05 μg/l). Vapor pulses containing femtogram to microgram quantities of analyte may also be generated. Calibrated ranges of three explosive vapors at ng/l levels were generated by the device and directly measured by ion mobility spectrometry (IMS). These data demonstrate expected linear trends within the limited working range of the IMS detector and also exhibit subtle nonlinear behavior from the IMS measurement process

  15. A Simple Accelerometer Calibrator

    International Nuclear Information System (INIS)

    Salam, R A; Islamy, M R F; Khairurrijal; Munir, M M; Latief, H; Irsyam, M

    2016-01-01

    High possibility of earthquake could lead to the high number of victims caused by it. It also can cause other hazards such as tsunami, landslide, etc. In that case it requires a system that can examine the earthquake occurrence. Some possible system to detect earthquake is by creating a vibration sensor system using accelerometer. However, the output of the system is usually put in the form of acceleration data. Therefore, a calibrator system for accelerometer to sense the vibration is needed. In this study, a simple accelerometer calibrator has been developed using 12 V DC motor, optocoupler, Liquid Crystal Display (LCD) and AVR 328 microcontroller as controller system. The system uses the Pulse Wave Modulation (PWM) form microcontroller to control the motor rotational speed as response to vibration frequency. The frequency of vibration was read by optocoupler and then those data was used as feedback to the system. The results show that the systems could control the rotational speed and the vibration frequencies in accordance with the defined PWM. (paper)

  16. Views on Software Testability

    OpenAIRE

    Shimeall, Timothy; Friedman, Michael; Chilenski, John; Voas, Jeffrey

    1994-01-01

    The field of testability is an active, well-established part of engineering of modern computer systems. However, only recently have technologies for software testability began to be developed. These technologies focus on accessing the aspects of software that improve or depreciate the ease of testing. As both the size of implemented software and the amount of effort required to test that software increase, so will the important of software testability technologies in influencing the softwa...

  17. Agile software assessment

    OpenAIRE

    Nierstrasz Oscar; Lungu Mircea

    2012-01-01

    Informed decision making is a critical activity in software development but it is poorly supported by common development environments which focus mainly on low level programming tasks. We posit the need for agile software assessment which aims to support decision making by enabling rapid and effective construction of software models and custom analyses. Agile software assessment entails gathering and exploiting the broader context of software information related to the system at hand as well ...

  18. Software component quality evaluation

    Science.gov (United States)

    Clough, A. J.

    1991-01-01

    The paper describes a software inspection process that can be used to evaluate the quality of software components. Quality criteria, process application, independent testing of the process and proposed associated tool support are covered. Early results indicate that this technique is well suited for assessing software component quality in a standardized fashion. With automated machine assistance to facilitate both the evaluation and selection of software components, such a technique should promote effective reuse of software components.

  19. Photometric Calibration of Consumer Video Cameras

    Science.gov (United States)

    Suggs, Robert; Swift, Wesley, Jr.

    2007-01-01

    analyze. The light source used to generate the calibration images is an artificial variable star comprising a Newtonian collimator illuminated by a light source modulated by a rotating variable neutral- density filter. This source acts as a point source, the brightness of which varies at a known rate. A video camera to be calibrated is aimed at this source. Fixed neutral-density filters are inserted in or removed from the light path as needed to make the video image of the source appear to fluctuate between dark and saturated bright. The resulting video-image data are analyzed by use of custom software that determines the integrated signal in each video frame and determines the system response curve (measured output signal versus input brightness). These determinations constitute the calibration, which is thereafter used in automatic, frame-by-frame processing of the data from the video images to be analyzed.

  20. Temperature calibration procedure for thin film substrates for thermo-ellipsometric analysis using melting point standards

    International Nuclear Information System (INIS)

    Kappert, Emiel J.; Raaijmakers, Michiel J.T.; Ogieglo, Wojciech; Nijmeijer, Arian; Huiskes, Cindy; Benes, Nieck E.

    2015-01-01

    Highlights: • Facile temperature calibration method for thermo-ellipsometric analysis. • The melting point of thin films of indium, lead, zinc, and water can be detected by ellipsometry. • In-situ calibration of ellipsometry hot stage, without using any external equipment. • High-accuracy temperature calibration (±1.3 °C). - Abstract: Precise and accurate temperature control is pertinent to studying thermally activated processes in thin films. Here, we present a calibration method for the substrate–film interface temperature using spectroscopic ellipsometry. The method is adapted from temperature calibration methods that are well developed for thermogravimetric analysis and differential scanning calorimetry instruments, and is based on probing a transition temperature. Indium, lead, and zinc could be spread on a substrate, and the phase transition of these metals could be detected by a change in the Ψ signal of the ellipsometer. For water, the phase transition could be detected by a loss of signal intensity as a result of light scattering by the ice crystals. The combined approach allowed for construction of a linear calibration curve with an accuracy of 1.3 °C or lower over the full temperature range

  1. Assuring Software Cost Estimates: Is it an Oxymoron?

    Science.gov (United States)

    Hihn, Jarius; Tregre, Grant

    2013-01-01

    The software industry repeatedly observes cost growth of well over 100% even after decades of cost estimation research and well-known best practices, so "What's the problem?" In this paper we will provide an overview of the current state oj software cost estimation best practice. We then explore whether applying some of the methods used in software assurance might improve the quality of software cost estimates. This paper especially focuses on issues associated with model calibration, estimate review, and the development and documentation of estimates as part alan integrated plan.

  2. Specific heat capacities of different clayey samples obtained by differential scanning calorimetry

    International Nuclear Information System (INIS)

    Fernandez, A.M.

    2012-01-01

    Document available in extended abstract form only. The thermo-physical properties allow to calculate heat flows and to determine the thermal behaviour of the materials. Temperature influences the rates of the physical, chemical and biological reactions and processes in the soil or a material. Variations in temperature and water content in thermal, hydraulic, mechanical and geochemical processes affect the thermal properties such as density, specific heat, thermal conductivity and thermal diffusivity. Therefore, mathematical models that describe the dependence of the thermal properties on temperature and concentration are of interest to be used in computational programs applied to the modelling of coupled thermo-mechanical-hydraulic and chemical (THMC) processes. In this work, the specific heat capacity of different clayey international reference materials was determined. Differential Scanning Calorimetry (DSC) was used for such purpose. DSC is the main tool for determining the specific heat capacities of materials as a function of temperature. The specific heat capacity, c p (J/Kg.K), is a measurement of the amount of heat required to raise the temperature of a unit mass of a substance by one unit of temperature. A change in temperature, caused by a gain or a loss of heat from a material, depends on the specific heat capacity of the material. Thus, the specific heat capacity is a key and characteristic property of a material and/or substance, which should be determine accurately. The specific heat capacity is an intensive property and, unlike the thermal conductivity and thermal diffusivity, is independent of the dry density of the material. C p of the solid samples was determined by using a SETSYS Evolution 16 thermal analyser coupled to a differential scanning calorimeter (TG-DSC-DTA) from SETARAM Instrumentation. The thermal analyser system can use a heating rate from 0.01 to 100 C/min under a dynamic argon atmosphere and temperatures ranging from ambient to

  3. Automated ECU software tests on hardware-in-the-loop test benches; Automatisierte ECU-Software-Tests an Hardware-in-the-Loop-Pruefstaenden

    Energy Technology Data Exchange (ETDEWEB)

    Voegl, R. [AVL List GmbH, Graz (Austria). Abteilung Kalibrierung Ottomotoren; Duerager, Ch. [AVL List GmbH, Graz (Austria). Abteilung Kalibriermethodik; Beer, W.; Martini, E. [AVL List GmbH, Graz (Austria)

    2005-08-01

    Due to the continuous increase in complexity of engine application, AVL List decided to develop methods for automated ECU software commissioning on HiL test benches. This required the intensive co-operation of the departments for calibration methodology, calibration and electrical/electronic engineering. The result is a practical orientated collection of methods that significantly increase the test coverage for a new software version without extending the commissioning time. (orig.)

  4. Software Quality Assurance Metrics

    Science.gov (United States)

    McRae, Kalindra A.

    2004-01-01

    Software Quality Assurance (SQA) is a planned and systematic set of activities that ensures conformance of software life cycle processes and products conform to requirements, standards and procedures. In software development, software quality means meeting requirements and a degree of excellence and refinement of a project or product. Software Quality is a set of attributes of a software product by which its quality is described and evaluated. The set of attributes includes functionality, reliability, usability, efficiency, maintainability, and portability. Software Metrics help us understand the technical process that is used to develop a product. The process is measured to improve it and the product is measured to increase quality throughout the life cycle of software. Software Metrics are measurements of the quality of software. Software is measured to indicate the quality of the product, to assess the productivity of the people who produce the product, to assess the benefits derived from new software engineering methods and tools, to form a baseline for estimation, and to help justify requests for new tools or additional training. Any part of the software development can be measured. If Software Metrics are implemented in software development, it can save time, money, and allow the organization to identify the caused of defects which have the greatest effect on software development. The summer of 2004, I worked with Cynthia Calhoun and Frank Robinson in the Software Assurance/Risk Management department. My task was to research and collect, compile, and analyze SQA Metrics that have been used in other projects that are not currently being used by the SA team and report them to the Software Assurance team to see if any metrics can be implemented in their software assurance life cycle process.

  5. Calibration Procedures in Mid Format Camera Setups

    Science.gov (United States)

    Pivnicka, F.; Kemper, G.; Geissler, S.

    2012-07-01

    A growing number of mid-format cameras are used for aerial surveying projects. To achieve a reliable and geometrically precise result also in the photogrammetric workflow, awareness on the sensitive parts is important. The use of direct referencing systems (GPS/IMU), the mounting on a stabilizing camera platform and the specific values of the mid format camera make a professional setup with various calibration and misalignment operations necessary. An important part is to have a proper camera calibration. Using aerial images over a well designed test field with 3D structures and/or different flight altitudes enable the determination of calibration values in Bingo software. It will be demonstrated how such a calibration can be performed. The direct referencing device must be mounted in a solid and reliable way to the camera. Beside the mechanical work especially in mounting the camera beside the IMU, 2 lever arms have to be measured in mm accuracy. Important are the lever arms from the GPS Antenna to the IMU's calibrated centre and also the lever arm from the IMU centre to the Camera projection centre. In fact, the measurement with a total station is not a difficult task but the definition of the right centres and the need for using rotation matrices can cause serious accuracy problems. The benefit of small and medium format cameras is that also smaller aircrafts can be used. Like that, a gyro bases stabilized platform is recommended. This causes, that the IMU must be mounted beside the camera on the stabilizer. The advantage is, that the IMU can be used to control the platform, the problematic thing is, that the IMU to GPS antenna lever arm is floating. In fact we have to deal with an additional data stream, the values of the movement of the stabiliser to correct the floating lever arm distances. If the post-processing of the GPS-IMU data by taking the floating levers into account, delivers an expected result, the lever arms between IMU and camera can be applied

  6. CALIBRATION PROCEDURES IN MID FORMAT CAMERA SETUPS

    Directory of Open Access Journals (Sweden)

    F. Pivnicka

    2012-07-01

    Full Text Available A growing number of mid-format cameras are used for aerial surveying projects. To achieve a reliable and geometrically precise result also in the photogrammetric workflow, awareness on the sensitive parts is important. The use of direct referencing systems (GPS/IMU, the mounting on a stabilizing camera platform and the specific values of the mid format camera make a professional setup with various calibration and misalignment operations necessary. An important part is to have a proper camera calibration. Using aerial images over a well designed test field with 3D structures and/or different flight altitudes enable the determination of calibration values in Bingo software. It will be demonstrated how such a calibration can be performed. The direct referencing device must be mounted in a solid and reliable way to the camera. Beside the mechanical work especially in mounting the camera beside the IMU, 2 lever arms have to be measured in mm accuracy. Important are the lever arms from the GPS Antenna to the IMU's calibrated centre and also the lever arm from the IMU centre to the Camera projection centre. In fact, the measurement with a total station is not a difficult task but the definition of the right centres and the need for using rotation matrices can cause serious accuracy problems. The benefit of small and medium format cameras is that also smaller aircrafts can be used. Like that, a gyro bases stabilized platform is recommended. This causes, that the IMU must be mounted beside the camera on the stabilizer. The advantage is, that the IMU can be used to control the platform, the problematic thing is, that the IMU to GPS antenna lever arm is floating. In fact we have to deal with an additional data stream, the values of the movement of the stabiliser to correct the floating lever arm distances. If the post-processing of the GPS-IMU data by taking the floating levers into account, delivers an expected result, the lever arms between IMU and

  7. Using LabVIEW to facilitate calibration and verification for respiratory impedance plethysmography.

    Science.gov (United States)

    Ellis, W S; Jones, R T

    1991-12-01

    A system for calibrating the Respitrace impedance plethysmograph was developed with the capacity to quantitatively verify the accuracy of calibration. LabVIEW software was used on a Macintosh II computer to create a user-friendly environment, with the added benefit of reducing development time. The system developed enabled a research assistant to calibrate the Respitrace within 15 min while achieving an accuracy within the normally accepted 10% deviation when the Respitrace output is compared to a water spirometer standard. The system and methods described were successfully used in a study of 10 subjects smoking cigarettes containing marijuana or cocaine under four conditions, calibrating all subjects to 10% accuracy within 15 min.

  8. Software Engineering Program: Software Process Improvement Guidebook

    Science.gov (United States)

    1996-01-01

    The purpose of this document is to provide experience-based guidance in implementing a software process improvement program in any NASA software development or maintenance community. This guidebook details how to define, operate, and implement a working software process improvement program. It describes the concept of the software process improvement program and its basic organizational components. It then describes the structure, organization, and operation of the software process improvement program, illustrating all these concepts with specific NASA examples. The information presented in the document is derived from the experiences of several NASA software organizations, including the SEL, the SEAL, and the SORCE. Their experiences reflect many of the elements of software process improvement within NASA. This guidebook presents lessons learned in a form usable by anyone considering establishing a software process improvement program within his or her own environment. This guidebook attempts to balance general and detailed information. It provides material general enough to be usable by NASA organizations whose characteristics do not directly match those of the sources of the information and models presented herein. It also keeps the ideas sufficiently close to the sources of the practical experiences that have generated the models and information.

  9. From Software Development to Software Assembly

    NARCIS (Netherlands)

    Sneed, Harry M.; Verhoef, Chris

    2016-01-01

    The lack of skilled programming personnel and the growing burden of maintaining customized software are forcing organizations to quit producing their own software. It's high time they turned to ready-made, standard components to fulfill their business requirements. Cloud services might be one way to

  10. On chromatic and geometrical calibration

    DEFF Research Database (Denmark)

    Folm-Hansen, Jørgen

    1999-01-01

    The main subject of the present thesis is different methods for the geometrical and chromatic calibration of cameras in various environments. For the monochromatic issues of the calibration we present the acquisition of monochrome images, the classic monochrome aberrations and the various sources...... the correct interpolation method is described. For the chromatic issues of calibration we present the acquisition of colour and multi-spectral images, the chromatic aberrations and the various lens/camera based non-uniformities of the illumination of the image plane. It is described how the monochromatic...... to design calibration targets for both geometrical and chromatic calibration are described. We present some possible systematical errors on the detection of the objects in the calibration targets, if viewed in a non orthogonal angle, if the intensities are uneven or if the image blurring is uneven. Finally...

  11. Development of portable flow calibrator

    International Nuclear Information System (INIS)

    Akiyama, Kiyomitsu; Iijima, Nobuo

    1995-01-01

    In the nuclear facilities, air sniffer system is often utilized to evaluate atmospheric concentration of radioactivity in the working environment. The system collects airborne dust on the filter during some sampling period. In this method, total air flow during the sampling period is an important parameter to evaluate the radioactivity concentration correctly. Therefore, calibration for the flow meter of air sniffer system must be done periodically according to Japan Industry Standards (JIS). As we have had to available device to calibrate the flow meter in the working area, we had to remove the flow meters from the installed place and carry them to another place where calibration can be made. This work required a great deal of labor. Now we have developed a portable flow calibrator for air sniffer system which enables us to make in-site calibration of the flow meter in the working area more easily. This report describes the outline of portable flow calibrator and it's experimental results. (author)

  12. Percent relative cumulative frequency analysis in indirect calorimetry: application to studies of transgenic mice.

    Science.gov (United States)

    Riachi, Marc; Himms-Hagen, Jean; Harper, Mary-Ellen

    2004-12-01

    Indirect calorimetry is commonly used in research and clinical settings to assess characteristics of energy expenditure. Respiration chambers in indirect calorimetry allow measurements over long periods of time (e.g., hours to days) and thus the collection of large sets of data. Current methods of data analysis usually involve the extraction of only a selected small proportion of data, most commonly the data that reflects resting metabolic rate. Here, we describe a simple quantitative approach for the analysis of large data sets that is capable of detecting small differences in energy metabolism. We refer to it as the percent relative cumulative frequency (PRCF) approach and have applied it to the study of uncoupling protein-1 (UCP1) deficient and control mice. The approach involves sorting data in ascending order, calculating their cumulative frequency, and expressing the frequencies in the form of percentile curves. Results demonstrate the sensitivity of the PRCF approach for analyses of oxygen consumption (.VO2) as well as respiratory exchange ratio data. Statistical comparisons of PRCF curves are based on the 50th percentile values and curve slopes (H values). The application of the PRCF approach revealed that energy expenditure in UCP1-deficient mice housed and studied at room temperature (24 degrees C) is on average 10% lower (p lower environmental temperature, there were no differences in .VO2 between groups. The latter is likely due to augmented shivering thermogenesis in UCP1-deficient mice compared with controls. With the increased availability of murine models of metabolic disease, indirect calorimetry is increasingly used, and the PRCF approach provides a novel and powerful means for data analysis.

  13. Water calorimetry and ionization chamber dosimetry in an 85-MeV clinical proton beam.

    Science.gov (United States)

    Palmans, H; Seuntjens, J; Verhaegen, F; Denis, J M; Vynckier, S; Thierens, H

    1996-05-01

    In recent years, the increased use of proton beams for clinical purposes has enhanced the demand for accurate absolute dosimetry for protons. As calorimetry is the most direct way to establish the absorbed dose and because water has recently been accepted as standard material for this type of beam, the importance of water calorimetry is obvious. In this work we report water calorimeter operation in an 85-MeV proton beam and a comparison of the absorbed dose to water measured by ionometry with the dose resulting from water calorimetric measurements. To ensure a proper understanding of the heat defect for defined impurities in water for this type of radiation, a relative response study was first done in comparison with theoretical calculations of the heat defect. The results showed that pure hypoxic water and hydrogen-saturated water yielded the same response with practically zero heat defect, in agreement with the model calculations. The absorbed dose inferred from these measurements was then compared with the dose derived from ionometry by applying the European Charged Heavy Particle Dosimetry (ECHED) protocol. Restricting the comparison to chambers recommended in the protocol, the calorimeter dose was found to be 2.6% +/- 0.9% lower than the average ionometry dose. In order to estimate the significance of chamber-dependent effects in this deviation, measurements were performed using a set of ten ionization chambers of five different types. The maximum internal deviation in the ionometry results amounted to 1.1%. We detected no systematic chamber volume dependence, but observed a small but systematic effect of the chamber wall thickness. The observed deviation between calorimetry and ionometry can be attributed to a combination of the value of (Wair/e)p for protons, adopted in the ECHED protocol, the mass stopping power ratios of water to air for protons, and possibly small ionization chamber wall effects.

  14. Determination of magnetic characteristics of nanoparticles by low-temperature calorimetry methods

    Energy Technology Data Exchange (ETDEWEB)

    Ugulava, A.; Toklikishvili, Z. [Department of Physics, I.Javakhishvili Tbilisi State University,I.Chavchavadze av. 3, 0179 Tbilisi, Georgia (United States); Chkhaidze, S., E-mail: simon.chkhaidze@tsu.ge [Department of Physics, I.Javakhishvili Tbilisi State University,I.Chavchavadze av. 3, 0179 Tbilisi, Georgia (United States); Kekutia, Sh. [V. Chavchanidze Institute of Cybernetics, at the Technical State University, S. Euli str. 5, 0186 Tbilisi, Georgia (United States)

    2017-05-15

    At low temperatures, the heat capacity of a superparamagnetic “ideal gas” determined by magnetic degrees of freedom can greatly exceed the lattice heat capacity. It is shown that in the presence of an external magnetic field, the temperature dependence of the magnetic part of the heat capacity has two maxima. The relations between the temperature at which these maxima are achieved, the magnetic moment of the nanoparticles and the magnetic anisotropy constant have been obtained. Measuring the heat capacity maxima temperatures by low-temperature calorimetry methods and using the obtained relations, we can obtain the numerical values both of the magnetic moment of nanoparticles and the magnetic anisotropy constants.

  15. Physico-chemical changes in heavy ions irradiated polymer foils by differential scanning calorimetry

    International Nuclear Information System (INIS)

    Ciesla, K.; Trautmann, Ch.; Vansant, E.F.

    1994-01-01

    The sample of commercial PETP (Hostaphan) and very heavy ions irradiated products were investigated by differential scanning calorimetry in nitrogen flow. Irradiation were performed with Dy ions of 13 MeV/u with fluences 5 x 10 10 ions/cm 2 . Differences were observed in melting behaviour of unirradiated and irradiated foils. The influence of irradiation conditions on the results was noticed. Moreover the samples of polyimide (Kapton) and polycarbonate (Macrofol) irradiated in similar conditions were examined by DSC. The DSC traces have been compared with those of unirradiated reference samples. (author). 8 refs, 5 figs

  16. Test in a beam of large-area Micromegas chambers for sampling calorimetry

    CERN Document Server

    Adloff, C.; Dalmaz, A.; Drancourt, C.; Gaglione, R.; Geffroy, N.; Jacquemier, J.; Karyotakis, Y.; Koletsou, I.; Peltier, F.; Samarati, J.; Vouters, G.

    2014-06-11

    Application of Micromegas for sampling calorimetry puts specific constraints on the design and performance of this gaseous detector. In particular, uniform and linear response, low noise and stability against high ionisation density deposits are prerequisites to achieving good energy resolution. A Micromegas-based hadronic calorimeter was proposed for an application at a future linear collider experiment and three technologically advanced prototypes of 1$\\times$1 m$^{2}$ were constructed. Their merits relative to the above-mentioned criteria are discussed on the basis of measurements performed at the CERN SPS test-beam facility.

  17. Calorimetry of Pu in the context of fuel fabrication follow-up

    International Nuclear Information System (INIS)

    Sanson, C.; Arnal, Thierry

    1979-01-01

    Calorimetry appears to be a particularly attractive method for obtaining balances within the context of fuel fabrication follow-up. Under this method the heat released by any plutonium sample is determined with calorimeters fitted with thermocouples, thereby ensuring perfect stability in time response. The first results achieved with two inexpensive prototype calorimeters are as follows, so far: response time, six hours approximately; sensitivity greater than 4 mv.W -1 and repeatability in the order 1%. It will no doubt be possible to improve this performance to a notable extent in the near future [fr

  18. Insights into glass transition and relaxation behavior using temperature-modulated differential scanning calorimetry

    DEFF Research Database (Denmark)

    Guo, Xiaoju; Mauro, J.C.; Allan, D.C.

    Temperature-modulated differential scanning calorimetry (TMDSC) is based on conventional DSC but with a sinusoidally modulated temperature path. Our simulations of TMDSC signals prove that the frequency correction of non-reversing heat flow can give a master curve within a certain range...... of frequencies. This frequency range is dependent not only on the measurement parameters such as linear heating/cooling rate and frequency and amplitude of the modulation, but also on the previous thermal history before the TMDSC measurement. The frequency correction for the reversing heat flow gives more...

  19. On the Frequency Correction in Temperature-Modulated Differential Scanning Calorimetry of Glass Transition

    DEFF Research Database (Denmark)

    Guo, Xiaoju; Mauro, J.C.; Allan, D.C.

    2012-01-01

    Temperature-modulated differential scanning calorimetry (TMDSC) is based on conventional DSC but with a sinusoidally modulated temperature path. Simulations of TMDSC signals were performed for Corning EAGLE XG® glass over a wide range of modulation frequencies. Our results reveal that the frequency...... correction commonly used in the interpretation of TMDSC signals leads to a master nonreversing heat flow curve independent of modulation frequency, provided that sufficiently high frequencies are employed in the TMDSC measurement. A master reversing heat flow curve can also be generated through the frequency...

  20. A novel calorimetry technique for monitoring electron beam curing of polymer resins

    International Nuclear Information System (INIS)

    Chen, J.H.; Johnston, A.; Petrescue, L.; Hojjati, M.

    2006-01-01

    This paper describes the development of a calorimetry-based technique for monitoring of the curing of electron beam (EB) curable resins, including design of the calorimeter hardware and the development of an analytical model for calculating resin cure rates and radiation dose. Factors affecting the performance of the calorimeter were investigated. Experimental trials monitoring the curing of epoxy resin were conducted under single pass and multiple passes of EB irradiation. Results show that the developed calorimeter is a simple, inexpensive and reasonably accurate technique for monitoring the EB curing of cationic epoxies

  1. Conductivity, calorimetry and phase diagram of the NaHSO4–KHSO4 system

    DEFF Research Database (Denmark)

    Hind, Hamma-Cugny; Rasmussen, Søren Birk; Rogez, J.

    2006-01-01

    to polynomials of the form κ(X)=A(X)+B(X)(T-Tm)+C(X)(T-Tm)2, where Tm is the intermediate temperature of the measured temperature range and X, the mole fraction of KHSO4. The possible role of this binary system as a catalyst solvent is also discussed. (C) 2005 Elsevier B.V. All rights reserved.......Physico-chemical properties of the binary system NaHSO4-KHSO4 were studied by calorimetry and conductivity, The enthalpy of mixing has been measured at 505 K in the full composition range and the phase diagram calculated. The phase diagram has also been constructed from phase transition...

  2. Quality Management and Calibration

    Science.gov (United States)

    Merkus, Henk G.

    Good specification of a product’s performance requires adequate characterization of relevant properties. Particulate products are usually characterized by some PSD, shape or porosity parameter(s). For proper characterization, adequate sampling, dispersion, and measurement procedures should be available or developed and skilful personnel should use appropriate, well-calibrated/qualified equipment. The characterization should be executed, in agreement with customers, in a wellorganized laboratory. All related aspects should be laid down in a quality handbook. The laboratory should provide proof for its capability to perform the characterization of stated products and/or reference materials within stated confidence limits. This can be done either by internal validation and audits or by external GLP accreditation.

  3. SURF Model Calibration Strategy

    Energy Technology Data Exchange (ETDEWEB)

    Menikoff, Ralph [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-03-10

    SURF and SURFplus are high explosive reactive burn models for shock initiation and propagation of detonation waves. They are engineering models motivated by the ignition & growth concept of high spots and for SURFplus a second slow reaction for the energy release from carbon clustering. A key feature of the SURF model is that there is a partial decoupling between model parameters and detonation properties. This enables reduced sets of independent parameters to be calibrated sequentially for the initiation and propagation regimes. Here we focus on a methodology for tting the initiation parameters to Pop plot data based on 1-D simulations to compute a numerical Pop plot. In addition, the strategy for tting the remaining parameters for the propagation regime and failure diameter is discussed.

  4. Calibration of Nanopositioning Stages

    Directory of Open Access Journals (Sweden)

    Ning Tan

    2015-12-01

    Full Text Available Accuracy is one of the most important criteria for the performance evaluation of micro- and nanorobots or systems. Nanopositioning stages are used to achieve the high positioning resolution and accuracy for a wide and growing scope of applications. However, their positioning accuracy and repeatability are not well known and difficult to guarantee, which induces many drawbacks for many applications. For example, in the mechanical characterisation of biological samples, it is difficult to perform several cycles in a repeatable way so as not to induce negative influences on the study. It also prevents one from controlling accurately a tool with respect to a sample without adding additional sensors for closed loop control. This paper aims at quantifying the positioning repeatability and accuracy based on the ISO 9283:1998 standard, and analyzing factors influencing positioning accuracy onto a case study of 1-DoF (Degree-of-Freedom nanopositioning stage. The influence of thermal drift is notably quantified. Performances improvement of the nanopositioning stage are then investigated through robot calibration (i.e., open-loop approach. Two models (static and adaptive models are proposed to compensate for both geometric errors and thermal drift. Validation experiments are conducted over a long period (several days showing that the accuracy of the stage is improved from typical micrometer range to 400 nm using the static model and even down to 100 nm using the adaptive model. In addition, we extend the 1-DoF calibration to multi-DoF with a case study of a 2-DoF nanopositioning robot. Results demonstrate that the model efficiently improved the 2D accuracy from 1400 nm to 200 nm.

  5. Automatic calibration and signal switching system for the particle beam fusion research data acquisition facility

    Energy Technology Data Exchange (ETDEWEB)

    Boyer, W.B.

    1979-09-01

    This report describes both the hardware and software components of an automatic calibration and signal system (Autocal) for the data acquisition system for the Sandia particle beam fusion research accelerators Hydra, Proto I, and Proto II. The Autocal hardware consists of off-the-shelf commercial equipment. The various hardware components, special modifications and overall system configuration are described. Special software has been developed to support the Autocal hardware. Software operation and maintenance are described.

  6. Automatic calibration and signal switching system for the particle beam fusion research data acquisition facility

    International Nuclear Information System (INIS)

    Boyer, W.B.

    1979-09-01

    This report describes both the hardware and software components of an automatic calibration and signal system (Autocal) for the data acquisition system for the Sandia particle beam fusion research accelerators Hydra, Proto I, and Proto II. The Autocal hardware consists of off-the-shelf commercial equipment. The various hardware components, special modifications and overall system configuration are described. Special software has been developed to support the Autocal hardware. Software operation and maintenance are described

  7. Radiological Calibration and Standards Facility

    Data.gov (United States)

    Federal Laboratory Consortium — PNNL maintains a state-of-the-art Radiological Calibration and Standards Laboratory on the Hanford Site at Richland, Washington. Laboratory staff provide expertise...

  8. Portable compact multifunction IR calibrator

    International Nuclear Information System (INIS)

    Wyatt, C.L.; Jacobsen, L.; Steed, A.

    1988-01-01

    A compact portable multifunction calibrator designed for future sensor systems is described which enables a linearity calibration for all detectors simultaneously using a near small-area source, a high-resolution mapping of the focal plane with 10 microrad setability and with a blur of less than 100 microrad, system spectral response calibration (radiometer) using a Michelson interferometer source, relative spectral response (spectrometer) using high-temperature external commercial blackbody simulators, and an absolute calibration using an internal low-temperature extended-area source. 5 references

  9. Bias in segmented gamma scans arising from size differences between calibration standards and assay samples

    International Nuclear Information System (INIS)

    Sampson, T.E.

    1991-01-01

    Recent advances in segmented gamma scanning have emphasized software corrections for gamma-ray self-adsorption in particulates or lumps of special nuclear material in the sample. another feature of this software is an attenuation correction factor formalism that explicitly accounts for differences in sample container size and composition between the calibration standards and the individual items being measured. Software without this container-size correction produces biases when the unknowns are not packaged in the same containers as the calibration standards. This new software allows the use of different size and composition containers for standards and unknowns, as enormous savings considering the expense of multiple calibration standard sets otherwise needed. This paper presents calculations of the bias resulting from not using this new formalism. These calculations may be used to estimate bias corrections for segmented gamma scanners that do not incorporate these advanced concepts

  10. BXS Re-calibration

    International Nuclear Information System (INIS)

    Welch, J.

    2010-01-01

    Early in the commissioning it was noticed by Cecile Limborg that the calibration of the BXS spectrometer magnet seemed to be different from the strength of the BX01/BX02 magnets. First the BX01/BX02 currents were adjusted to 135 MeV and the beam energy was adjusted to make the horizontal orbit flat. Then BX01/BX02 magnets were switched off and BXS was adjusted to make the horizontal orbit in the spectrometer line flat, without changing the energy of the beam. The result was that about 140-141 MeV were required on the BXS magnet. This measurement was repeated several times by others with the same results. It was not clear what was causing the error: magnet strength or layout. A position error of about 19 mm of the BXS magnet could explain the difference. Because there was a significant misalignment of the vacuum chamber in the BXS line, the alignment of the whole spectrometer line was checked. The vacuum chamber was corrected, but the magnets were found to be in the proper alignment. So we were left with one (or conceivably two) magnet calibration errors. Because BXS is a wedged shaped magnet, the bend angle depends on the horizontal position of the incoming beam. As mentioned, an offset of the beam position of 19 mm would increase or decrease the bend angle roughly by the ratio of 135/141. The figure of 19 mm is special and caused a considerable confusion during the design and measurement of the BXS magnet. This is best illustrated in Figure 1 which was taken out of the BXS Traveler document. The distance between the horizontal midplanes of the poles and the apex of the beam path was chosen to be 19 mm so the beam is close to the good field region throughout its entire path. Thus it seemed possible that there was an error that resulted in the beam not being on this trajectory, or conversely, that the magnetic measurements were done on the wrong trajectory and the magnet was then mis-calibrated. Mechanical measurements of the vacuum chamber made in the tunnel

  11. Automation of dosimeters calibration for radiotherapy in secondary dosimetric calibration laboratory of the CPHR; Automatizacion de la calibracion de dosimetros de radioterapia en el laboratorio secundario de calibracion dosimetrica del CPHR

    Energy Technology Data Exchange (ETDEWEB)

    Acosta, Andy L. Romero; Lores, Stefan Gutierrez, E-mail: c19btm@frcuba.co.cu [Centro de Proteccion e Higiene de las Radiaciones (CPHR), La Habana (Cuba)

    2013-11-01

    This paper presents the design and implementation of an automated system for measurements in the calibration of reference radiation dosimeters. It was made a software application that performs the acquisition of the measured values of electric charge, calculated calibration coefficient and automates the calibration certificate issuance. These values are stored in a log file on a PC. The use of the application improves control over the calibration process, helps to humanize the work and reduces personnel exposure. The tool developed has been applied to the calibration of dosimeters radiation patterns in the LSCD of the Centro de Proteccion e Higiene de las Radiaciones, Cuba.

  12. Efficient mass calibration of magnetic sector mass spectrometers

    International Nuclear Information System (INIS)

    Roddick, J.C.

    1996-01-01

    Magnetic sector mass spectrometers used for automatic acquisition of precise isotopic data are usually controlled with Hall probes and software that uses polynomial equations to define and calibrate the mass-field relations required for mass focusing. This procedure requires a number of reference masses and careful tuning to define and maintain an accurate mass calibration. A simplified equation is presented and applied to several different magnetically controlled mass spectrometers. The equation accounts for nonlinearity in typical Hall probe controlled mass-field relations, reduces calibration to a linear fitting procedure, and is sufficiently accurate to permit calibration over a mass range of 2 to 200 amu with only two defining masses. Procedures developed can quickly correct for normal drift in calibrations and compensate for drift during isotopic analysis over a limited mass range such as a single element. The equation is: Field A·Mass 1/2 + B·(Mass) p where A, B, and p are constants. The power value p has a characteristic value for a Hall probe/controller and is insensitive to changing conditions, thus reducing calibration to a linear regression to determine optimum A and B. (author). 1 ref., 1 tab., 6 figs

  13. CAMAC-controlled calibration system for nuclear reactor instruments

    International Nuclear Information System (INIS)

    McDowell, W.P.; Cornella, R.J.

    1977-01-01

    The hardware and the software which have been developed to implement a nuclear instrument calibration system for the Argonne National Laboratory ZPR-VI and ZPR-IX reactor complex are described. The system is implemented using an SEL-840 computer with its associated CAMAC crates and a hardware interface to generate input parameters and measure the required outputs on the instrument under test. Both linear and logarithmic instruments can be calibrated by the system and output parameters can be measured at various automatically selected values of ac line voltage. A complete report on each instrument is printed as a result of the calibration and out-of-tolerance readings are flagged. Operator interface is provided by a CAMAC-controlled Hazeltine terminal. The terminal display leads the operator through the complete calibration procedure. This computer-controlled system is a significant improvement over previously used methods of calibrating nuclear instruments since it reduces reactor downtime and allows rapid detection of long-term changes in instrument calibration

  14. Efficient mass calibration of magnetic sector mass spectrometers

    Energy Technology Data Exchange (ETDEWEB)

    Roddick, J C

    1997-12-31

    Magnetic sector mass spectrometers used for automatic acquisition of precise isotopic data are usually controlled with Hall probes and software that uses polynomial equations to define and calibrate the mass-field relations required for mass focusing. This procedure requires a number of reference masses and careful tuning to define and maintain an accurate mass calibration. A simplified equation is presented and applied to several different magnetically controlled mass spectrometers. The equation accounts for nonlinearity in typical Hall probe controlled mass-field relations, reduces calibration to a linear fitting procedure, and is sufficiently accurate to permit calibration over a mass range of 2 to 200 amu with only two defining masses. Procedures developed can quickly correct for normal drift in calibrations and compensate for drift during isotopic analysis over a limited mass range such as a single element. The equation is: Field A{center_dot}Mass{sup 1/2} + B{center_dot}(Mass){sup p} where A, B, and p are constants. The power value p has a characteristic value for a Hall probe/controller and is insensitive to changing conditions, thus reducing calibration to a linear regression to determine optimum A and B. (author). 1 ref., 1 tab., 6 figs.

  15. Color calibration and color-managed medical displays: does the calibration method matter?

    Science.gov (United States)

    Roehrig, Hans; Rehm, Kelly; Silverstein, Louis D.; Dallas, William J.; Fan, Jiahua; Krupinski, Elizabeth A.

    2010-02-01

    Our laboratory has investigated the efficacy of a suite of color calibration and monitor profiling packages which employ a variety of color measurement sensors. Each of the methods computes gamma correction tables for the red, green and blue color channels of a monitor that attempt to: a) match a desired luminance range and tone reproduction curve; and b) maintain a target neutral point across the range of grey values. All of the methods examined here produce International Color Consortium (ICC) profiles that describe the color rendering capabilities of the monitor after calibration. Color profiles incorporate a transfer matrix that establishes the relationship between RGB driving levels and the International Commission on Illumination (CIE) XYZ (tristimulus) values of the resulting on-screen color; the matrix is developed by displaying color patches of known RGB values on the monitor and measuring the tristimulus values with a sensor. The number and chromatic distribution of color patches varies across methods and is usually not under user control. In this work we examine the effect of employing differing calibration and profiling methods on rendition of color images. A series of color patches encoded in sRGB color space were presented on the monitor using color-management software that utilized the ICC profile produced by each method. The patches were displayed on the calibrated monitor and measured with a Minolta CS200 colorimeter. Differences in intended and achieved luminance and chromaticity were computed using the CIE DE2000 color-difference metric, in which a value of ▵E = 1 is generally considered to be approximately one just noticeable difference (JND) in color. We observed between one and 17 JND's for individual colors, depending on calibration method and target.

  16. Exposure-rate calibration using large-area calibration pads

    International Nuclear Information System (INIS)

    Novak, E.F.

    1988-09-01

    The US Department of Energy (DOE) Office of Remedial Action and Waste Technology established the Technical Measurements Center (TMC) at the DOE Grand Junction Projects Office (GJPO) in Grand Junction, Colorado, to standardize, calibrate, and compare measurements made in support of DOE remedial action programs. A set of large-area, radioelement-enriched concrete pads was constructed by the DOE in 1978 at the Walker Field Airport in Grand Junction for use as calibration standards for airborne gamma-ray spectrometer systems. The use of these pads was investigated by the TMC as potential calibration standards for portable scintillometers employed in measuring gamma-ray exposure rates at Uranium Mill Tailings Remedial Action (UMTRA) project sites. Data acquired on the pads using a pressurized ionization chamber (PIC) and three scintillometers are presented as an illustration of an instrumental calibration. Conclusions and recommended calibration procedures are discussed, based on the results of these data

  17. Calibration of LOFAR data on the cloud

    Science.gov (United States)

    Sabater, J.; Sánchez-Expósito, S.; Best, P.; Garrido, J.; Verdes-Montenegro, L.; Lezzi, D.

    2017-04-01

    New scientific instruments are starting to generate an unprecedented amount of data. The Low Frequency Array (LOFAR), one of the Square Kilometre Array (SKA) pathfinders, is already producing data on a petabyte scale. The calibration of these data presents a huge challenge for final users: (a) extensive storage and computing resources are required; (b) the installation and maintenance of the software required for the processing is not trivial; and (c) the requirements of calibration pipelines, which are experimental and under development, are quickly evolving. After encountering some limitations in classical infrastructures like dedicated clusters, we investigated the viability of cloud infrastructures as a solution. We found that the installation and operation of LOFAR data calibration pipelines is not only possible, but can also be efficient in cloud infrastructures. The main advantages were: (1) the ease of software installation and maintenance, and the availability of standard APIs and tools, widely used in the industry; this reduces the requirement for significant manual intervention, which can have a highly negative impact in some infrastructures; (2) the flexibility to adapt the infrastructure to the needs of the problem, especially as those demands change over time; (3) the on-demand consumption of (shared) resources. We found that a critical factor (also in other infrastructures) is the availability of scratch storage areas of an appropriate size. We found no significant impediments associated with the speed of data transfer, the use of virtualization, the use of external block storage, or the memory available (provided a minimum threshold is reached). Finally, we considered the cost-effectiveness of a commercial cloud like Amazon Web Services. While a cloud solution is more expensive than the operation of a large, fully-utilized cluster completely dedicated to LOFAR data reduction, we found that its costs are competitive if the number of datasets to be

  18. Offline software for the DAMPE experiment

    Science.gov (United States)

    Wang, Chi; Liu, Dong; Wei, Yifeng; Zhang, Zhiyong; Zhang, Yunlong; Wang, Xiaolian; Xu, Zizong; Huang, Guangshun; Tykhonov, Andrii; Wu, Xin; Zang, Jingjing; Liu, Yang; Jiang, Wei; Wen, Sicheng; Wu, Jian; Chang, Jin

    2017-10-01

    A software system has been developed for the DArk Matter Particle Explorer (DAMPE) mission, a satellite-based experiment. The DAMPE software is mainly written in C++ and steered using a Python script. This article presents an overview of the DAMPE offline software, including the major architecture design and specific implementation for simulation, calibration and reconstruction. The whole system has been successfully applied to DAMPE data analysis. Some results obtained using the system, from simulation and beam test experiments, are presented. Supported by Chinese 973 Program (2010CB833002), the Strategic Priority Research Program on Space Science of the Chinese Academy of Science (CAS) (XDA04040202-4), the Joint Research Fund in Astronomy under cooperative agreement between the National Natural Science Foundation of China (NSFC) and CAS (U1531126) and 100 Talents Program of the Chinese Academy of Science

  19. Software Engineering Improvement Plan

    Science.gov (United States)

    2006-01-01

    In performance of this task order, bd Systems personnel provided support to the Flight Software Branch and the Software Working Group through multiple tasks related to software engineering improvement and to activities of the independent Technical Authority (iTA) Discipline Technical Warrant Holder (DTWH) for software engineering. To ensure that the products, comments, and recommendations complied with customer requirements and the statement of work, bd Systems personnel maintained close coordination with the customer. These personnel performed work in areas such as update of agency requirements and directives database, software effort estimation, software problem reports, a web-based process asset library, miscellaneous documentation review, software system requirements, issue tracking software survey, systems engineering NPR, and project-related reviews. This report contains a summary of the work performed and the accomplishments in each of these areas.

  20. Spotting software errors sooner

    International Nuclear Information System (INIS)

    Munro, D.

    1989-01-01

    Static analysis is helping to identify software errors at an earlier stage and more cheaply than conventional methods of testing. RTP Software's MALPAS system also has the ability to check that a code conforms to its original specification. (author)

  1. Avionics and Software Project

    Data.gov (United States)

    National Aeronautics and Space Administration — The goal of the AES Avionics and Software (A&S) project is to develop a reference avionics and software architecture that is based on standards and that can be...

  2. Paladin Software Support Lab

    Data.gov (United States)

    Federal Laboratory Consortium — The Paladin Software Support Environment (SSE) occupies 2,241 square-feet. It contains the hardware and software tools required to support the Paladin Automatic Fire...

  3. Pragmatic Software Innovation

    DEFF Research Database (Denmark)

    Aaen, Ivan; Jensen, Rikke Hagensby

    2014-01-01

    We understand software innovation as concerned with introducing innovation into the development of software intensive systems, i.e. systems in which software development and/or integration are dominant considerations. Innovation is key in almost any strategy for competitiveness in existing markets......, for creating new markets, or for curbing rising public expenses, and software intensive systems are core elements in most such strategies. Software innovation therefore is vital for about every sector of the economy. Changes in software technologies over the last decades have opened up for experimentation......, learning, and flexibility in ongoing software projects, but how can this change be used to facilitate software innovation? How can a team systematically identify and pursue opportunities to create added value in ongoing projects? In this paper, we describe Deweyan pragmatism as the philosophical foundation...

  4. Process mining software repositories

    NARCIS (Netherlands)

    Poncin, W.; Serebrenik, A.; Brand, van den M.G.J.

    2011-01-01

    Software developers' activities are in general recorded in software repositories such as version control systems, bug trackers and mail archives. While abundant information is usually present in such repositories, successful information extraction is often challenged by the necessity to

  5. Direct calorimetry of free-moving eels with manipulated thyroid status

    Science.gov (United States)

    van Ginneken, Vincent; Ballieux, Bart; Antonissen, Erik; van der Linden, Rob; Gluvers, Ab; van den Thillart, Guido

    2007-02-01

    In birds and mammals, the thyroid gland secretes the iodothyronine hormones of which tetraiodothyronine (T4) is less active than triiodothyronine (T3). The action of T3 and T4 is calorigenic and is involved in the control of metabolic rate. Across all vertebrates, thyroid hormones also play a major role in differentiation, development and growth. Although the fish thyroidal system has been researched extensively, its role in thermogenesis is unclear. In this study, we measured overall heat production to an accuracy of 0.1 mW by direct calorimetry in a free-moving European eel ( Anguilla anguilla L.) with different thyroid status. Hyperthyroidism was induced by injection of T3 and T4, and hypothyroidism was induced with phenylthiourea. The results show for the first time at the organismal level, using direct calorimetry, that neither overall heat production nor overall oxygen consumption in eels is affected by hyperthyroidism. Therefore, we conclude that the thermogenic metabolism-stimulating effect of thyroid hormones (TH) is not present with a cold-blooded fish species like the European eel. This supports the concept that TH does not stimulate thermogenesis in poikilothermic species.

  6. Resting energy expenditure and body composition in children with cancer: indirect calorimetry and bioimpedance analysis

    Directory of Open Access Journals (Sweden)

    M. V. Konovalova

    2014-07-01

    Full Text Available Resting energy expenditure (REE by indirect calorimetry and body composition by bioimpedance analysis are studied in three groups of children aged 5–18 years. Group 1 (n = 181 – patients in remission of cancer, group 2 (n = 55 – children with oncology diseases receiving chemotherapy or who are in the early period after hematopoietic stem cell transplantation, group 3 (n = 63 – children with non-malignant diseases of the gastrointestinal tract. To eliminate the influence of age and gender on the intergroup comparisons, body composition parameters were expressed as standardized values (z-scores relative to a reference group of healthy Russian children (n = 138,191. Group 1 was characterized by excess fat content with intact lean body mass, and groups 2 and 3 by protein depletion, more pronounced in Group 2 with a higher percentage of body fat. All used conventional formulas (WHO, Harris–Benedict and others in groups 1 and 3 underestimated REE as compared with indirect calorimetry. A new formula for REE, giving an unbiased estimate in the group 1 was proposed: REE (kcal/day = 28.7 × BCM (kg +10.5 × Height (cm – 38.6 × Age (years – 134, where BCM – body cell mass according to bioimpedance analysis (R2 = 0.67, the standard deviation of 196 kcal/day.

  7. Titration calorimetry of surfactant–drug interactions: Micelle formation and saturation studies

    International Nuclear Information System (INIS)

    Waters, Laura J.; Hussain, Talib; Parkes, Gareth M.B.

    2012-01-01

    Highlights: ► Isothermal titration calorimetry can be used to monitor the saturation of micelles with pharmaceutical compounds. ► The number of drug molecules per micelle varies depending on the drug used and the temperature of the calorimeter. ► The change in enthalpy for the saturation of micelles with drugs can be endothermic or exothermic. ► The critical micellar concentration of an anionic surfactant (SDS) does not appear to vary in the presence of drugs. - Abstract: Isothermal titration calorimetry (ITC) was employed to monitor the addition of five model drugs to anionic surfactant based micelles, composed of sodium dodecyl sulfate (SDS), through to the point at which they were saturated with drug. Analysis of the resultant data using this newly developed method has confirmed the suitability of the technique to acquire such data with saturation limits established in all cases. Values for the point at which saturation occurred ranged from 17 molecules of theophylline per micelle at T = 298 K up to 63 molecules of caffeine per micelle at 310 K. Micellar systems can be disrupted by the presence of additional chemicals, such as the drugs used in this study, therefore a separate investigation was undertaken to determine the critical micellar concentration (CMC) for SDS in the presence of each drug at T = 298 K and 310 K using ITC. In the majority of cases, there was no appreciable alteration to the CMC of SDS with drug present.

  8. Kinetics of enzymatic high-solid hydrolysis of lignocellulosic biomass studied by calorimetry.

    Science.gov (United States)

    Olsen, Søren N; Lumby, Erik; McFarland, Kc; Borch, Kim; Westh, Peter

    2011-03-01

    Enzymatic hydrolysis of high-solid biomass (>10% w/w dry mass) has become increasingly important as a key step in the production of second-generation bioethanol. To this end, development of quantitative real-time assays is desirable both for empirical optimization and for detailed kinetic analysis. In the current work, we have investigated the application of isothermal calorimetry to study the kinetics of enzymatic hydrolysis of two substrates (pretreated corn stover and Avicel) at high-solid contents (up to 29% w/w). It was found that the calorimetric heat flow provided a true measure of the hydrolysis rate with a detection limit of about 500 pmol glucose s(-1). Hence, calorimetry is shown to be a highly sensitive real-time method, applicable for high solids, and independent on the complexity of the substrate. Dose-response experiments with a typical cellulase cocktail enabled a multidimensional analysis of the interrelationships of enzyme load and the rate, time, and extent of the reaction. The results suggest that the hydrolysis rate of pretreated corn stover is limited initially by available attack points on the substrate surface (conversion) but becomes proportional to enzyme dosage (excess of attack points) at later stages (>10% conversion). This kinetic profile is interpreted as an increase in polymer end concentration (substrate for CBH) as the hydrolysis progresses, probably due to EG activity in the enzyme cocktail. Finally, irreversible enzyme inactivation did not appear to be the source of reduced hydrolysis rate over time.

  9. Study of gamma irradiated polyethylenes by temperature modulated differential scanning calorimetry

    International Nuclear Information System (INIS)

    Secerov, B.; Galovic, S.; Trifunovic, S.; Milicevic, D.; Suljovrujic, E.

    2011-01-01

    Complete text of publication follows. The various polyethylenes (PEs) and effects of high energy radiation on theirs structures were widely studied in the past using conventional Differential Scanning Calorimetry (DSC) measurements. In this work, we applied the Temperature Modulated Differential Scanning Calorimetry (TMDSC) technique in order to obtain more information about the influence of initial structural differences and gamma radiation on the evolution in structure and thermal properties of different polyethylenes. For this reason, low density polyethylene (LDPE), linear low density polyethylene (LLDPE) and high density polyethylene (HDPE) samples were exposed to gamma radiation, in air, to a wide range of absorbed doses (up to 2400 kGy). The separation of the total heat flow TMDSC signal into a reversing and nonreversing part enabled to observed the low temperature enthalpy relaxation (related to the existence of the 'rigid amorphous phase') and recrystallization processes as well as to follow their and/or radiation-induced evolution of melting in a more revealing manner compared to the case of the conventional DSC. Consequently, our results indicate that TMDSC could improve the understanding of radiation-induced effects in polymers.

  10. A study of gamma-irradiated polyethylenes by temperature modulated differential scanning calorimetry

    Science.gov (United States)

    Galovic, S.; Secerov, B.; Trifunovic, S.; Milicevic, D.; Suljovrujic, E.

    2012-09-01

    Various polyethylenes (PEs) and the effects of high-energy radiation on their structures were widely studied in the past using conventional Differential Scanning Calorimetry (DSC) measurements. In this work, we used the Temperature Modulated Differential Scanning Calorimetry (TMDSC) technique in order to obtain more information about the influence of the initial structural differences and gamma radiation on the evolution in structure and thermal properties of different polyethylenes. For this reason, low density polyethylene (LDPE), linear low density polyethylene (LLDPE) and high density polyethylene (HDPE) samples were exposed to gamma radiation, in air, to a wide range of absorbed doses (up to 2400 kGy). The separation of the total heat flow TMDSC signal into a reversing and non-reversing part enabled us to observe the low-temperature enthalpy relaxation (related to the existence of the "rigid amorphous phase") and recrystallisation processes, as well as to follow their radiation-induced evolution and/or that of melting in a more revealing manner compared to the case of the conventional DSC. Consequently, our results indicate that TMDSC could improve the understanding of radiation-induced effects in polymers.

  11. Thermal behavior and phase identification of Valsartan by standard and temperature-modulated differential scanning calorimetry.

    Science.gov (United States)

    Skotnicki, Marcin; Gaweł, Agnieszka; Cebe, Peggy; Pyda, Marek

    2013-10-01

    Thermal behavior of angiotensin II type 1 (AT1) receptor antagonist, Valsartan (VAL), was examined employing thermogravimetric analysis (TGA), standard differential scanning calorimetry (DSC) and temperature-modulated differential scanning calorimetry (TMDSC). The stability of VAL was measured by TGA from 25 to 600°C. Decomposition of Valsartan starts around 160°C. The DSC curve shows two endotherms, occurring around 80°C and 100°C, related to evaporation of water and enthalpy relaxation, respectively. Valsartan was identified by DSC as an amorphous material and it was confirmed by X-ray powder diffraction. The glass transition of fresh Valsartan appears around 76°C (fictive temperature). TMDSC allows separation of the total heat flow rate into reversing and nonreversing parts. The nonreversing curve corresponds to the enthalpy relaxation and the reversing curve shows changes of heat capacity around 94°C. In the second run, TMDSC curve shows the glass transition process occurring at around 74°C. Results from standard DSC and TMDSC of Valsartan were compared over the whole range of temperature.

  12. The heat capacity of polyethylene fibers measured by multi-frequency temperature-modulated calorimetry

    International Nuclear Information System (INIS)

    Pyda, M.; Nowak-Pyda, E.; Wunderlich, B.

    2006-01-01

    The apparent heat capacity of polyethylene fibers in the melting region was measured by quasi-isothermal, temperature-modulated differential scanning calorimetry (TMDSC) and compared with results from standard differential scanning calorimetry (DSC) and the solid and liquid thermodynamic heat capacity as references from the ATHAS Data Bank. Using a multi-frequency, complex sawtooth modulation in the quasi-isothermal mode disclosed for the first time that the uncorrected apparent heat capacity C p =A Φ /(A T s ω) of the liquid polyethylene fiber increases with increasing frequency (A Φ is the differential heat-flow rate and A T s is the sample temperature). The frequency-dependent heat capacity cannot be represented by the expression: C p =A Φ /(A T s νω)[1+(τνω) 2 ] 0.5 because of a negative τ 2 . The results were later confirmed by independent measurements on single sinusoidal quasi-isothermal TMDSC on the same material. The error is caused by shrinking of the fiber, which deforms the sample pan

  13. Chip calorimetry for evaluation of biofilm treatment with biocides, antibiotics, and biological agents.

    Science.gov (United States)

    Morais, Frida Mariana; Buchholz, Friederike; Maskow, Thomas

    2014-01-01

    Any growth or bioconversion in biofilms is accompanied by the release of heat. The heat (in J) is tightly related to the stoichiometry of the respective process via law of Hess, and the heat production rate (in W or J/s) is additionally related to the process kinetics. This heat and the heat production rate can nowadays be measured by modern calorimetry with extremely high sensitivity. Flow-through calorimetry allows the measurement of bioprocesses in biofilms in real time, without the need of invasive sample preparation and disturbing of biofilm processes. Furthermore, it can be applied for long-term measurements and is even applicable to turbid media. Chip or miniaturized calorimeters have the additional advantages of extremely short thermal equilibration times and the requirement of very small amounts of media and chemicals. The precision of flow-through chip calorimeters (about 3 mW/L) allows the detection of early stages of biofilm development (about 10(5) bacteria cm(-2)).

  14. A High-Throughput Biological Calorimetry Core: Steps to Startup, Run, and Maintain a Multiuser Facility.

    Science.gov (United States)

    Yennawar, Neela H; Fecko, Julia A; Showalter, Scott A; Bevilacqua, Philip C

    2016-01-01

    Many labs have conventional calorimeters where denaturation and binding experiments are setup and run one at a time. While these systems are highly informative to biopolymer folding and ligand interaction, they require considerable manual intervention for cleaning and setup. As such, the throughput for such setups is limited typically to a few runs a day. With a large number of experimental parameters to explore including different buffers, macromolecule concentrations, temperatures, ligands, mutants, controls, replicates, and instrument tests, the need for high-throughput automated calorimeters is on the rise. Lower sample volume requirements and reduced user intervention time compared to the manual instruments have improved turnover of calorimetry experiments in a high-throughput format where 25 or more runs can be conducted per day. The cost and efforts to maintain high-throughput equipment typically demands that these instruments be housed in a multiuser core facility. We describe here the steps taken to successfully start and run an automated biological calorimetry facility at Pennsylvania State University. Scientists from various departments at Penn State including Chemistry, Biochemistry and Molecular Biology, Bioengineering, Biology, Food Science, and Chemical Engineering are benefiting from this core facility. Samples studied include proteins, nucleic acids, sugars, lipids, synthetic polymers, small molecules, natural products, and virus capsids. This facility has led to higher throughput of data, which has been leveraged into grant support, attracting new faculty hire and has led to some exciting publications. © 2016 Elsevier Inc. All rights reserved.

  15. Applications of isothermal titration calorimetry - the research and technical developments from 2011 to 2015.

    Science.gov (United States)

    Falconer, Robert J

    2016-10-01

    Isothermal titration calorimetry is a widely used biophysical technique for studying the formation or dissociation of molecular complexes. Over the last 5 years, much work has been published on the interpretation of isothermal titration calorimetry (ITC) data for single binding and multiple binding sites. As over 80% of ITC papers are on macromolecules of biological origin, this interpretation is challenging. Some researchers have attempted to link the thermodynamics constants to events at the molecular level. This review highlights work carried out using binding sites characterized using x-ray crystallography techniques that allow speculation about individual bond formation and the displacement of individual water molecules during ligand binding and link these events to the thermodynamic constants for binding. The review also considers research conducted with synthetic binding partners where specific binding events like anion-π and π-π interactions were studied. The revival of assays that enable both thermodynamic and kinetic information to be collected from ITC data is highlighted. Lastly, published criticism of ITC research from a physical chemistry perspective is appraised and practical advice provided for researchers unfamiliar with thermodynamics and its interpretation. Copyright © 2016 John Wiley & Sons, Ltd. Copyright © 2016 John Wiley & Sons, Ltd.

  16. Thermochemistry of some binary lead and transition metal compounds by high temperature direct synthesis calorimetry

    Energy Technology Data Exchange (ETDEWEB)

    Meschel, S.V., E-mail: meschel@jfi.uchicago.edu [Illinois Institute of Technology,Thermal Processing Technology Center, 10 W. 32nd Street, Chicago, Illinois 60615 (United States); Gordon Center for Integrated Science, 929 E. 57th Street, Chicago, Illinois 60637 (United States); Nash, P. [Illinois Institute of Technology,Thermal Processing Technology Center, 10 W. 32nd Street, Chicago, Illinois 60615 (United States); Chen, X.Q.; Wei, P. [Materials processing Modeling Division, Shenyang National Laboratory for Materials Science, Institute of Metals Research, 72 Wenhua Road, Shenyang City (China)

    2015-06-05

    Highlights: • Studied binary lead-transition metal alloys by high temperature calorimetry. • Determined the enthalpies of formation of 8 alloys. • Compared the measurements with predictions by the model of Miedema and by the ab initio method. - Abstract: The standard enthalpies of formation of some binary lead and transition metal compounds have been measured by high temperature direct synthesis calorimetry. The reported results are: Pb{sub 3}Sc{sub 5}(−61.3 ± 2.9); PbTi{sub 4}(−16.6 ± 2.4); Pb{sub 3}Y{sub 5}(−64.8 ± 3.6); Pb{sub 3}Zr{sub 5}(−50.6 ± 3.1); PbNb{sub 3}(−10.4 ± 3.4); PbRh(−16.5 ± 3.3); PbPd{sub 3}(−29.6 ± 3.1); PbPt(−34.7 ± 3.3) kJ/mole of atoms. We will compare our results with previously published measurements. We will also compare the experimental measurements with enthalpies of formation of transition metal compounds with elements in the same vertical column in the periodic table. We will compare our measurements with predicted values on the basis of the semi empirical model of Miedema and coworkers and with ab initio values when available.

  17. Methodology of hot nucleus calorimetry and thermometry produced by nuclear reactions around Fermi energies; Methodologie de la calorimetrie et de la thermometrie des noyaux chauds formes lors de collisions nucleaires aux energies de Fermi

    Energy Technology Data Exchange (ETDEWEB)

    Vient, E

    2006-12-15

    This work deals with the calorimetry and thermometry of hot nuclei produced in collisions Xe + Sn between 25 and 100 MeV/u. The apparatus for hot nucleus physical characterization is the 4{pi} detector array Indra. This study was made by using the event generators Gemini, Simon and Hipse and a data-processing filter simulating the complete operation of the multi-detector. The first chapter presents the different ways of producing hot nuclei. In the second and third chapters, the author presents a critical methodological study of calorimetry and thermometry applied to hot nuclei, different methods are reviewed, their accuracy and application range are assessed. All the calorimetry methods rely on the assumption that we are able to discriminate decay products of the hot nucleus from evaporated particles. In the fourth chapter, the author gives some ways of improving calorimetry characterization of the hot nucleus. An alternative method of calorimetry is proposed in the fifth chapter, this method is based on the experimental determination of an evaporation probability that is deduced from the physical characteristics of the particles present in a restricted domain of the space of velocities.

  18. Optimization of Antivirus Software

    OpenAIRE

    Catalin BOJA; Adrian VISOIU

    2007-01-01

    The paper describes the main techniques used in development of computer antivirus software applications. For this particular category of software, are identified and defined optimum criteria that helps determine which solution is better and what are the objectives of the optimization process. From the general viewpoint of software optimization are presented methods and techniques that are applied at code development level. Regarding the particularities of antivirus software, the paper analyze...

  19. Open Source Software Development

    Science.gov (United States)

    2011-01-01

    appropriate to refer to FOSS or FLOSS (L for Libre , where the alternative term “ libre software ” has popularity in some parts of the world) in order...Applying Social Network Analysis to Community-Drive Libre Software Projects, Intern. J. Info. Tech. and Web Engineering, 2006, 1(3), 27-28. 17...Open Source Software Development* Walt Scacchi Institute for Software Researcher University of California, Irvine Irvine, CA 92697-3455 USA Abstract

  20. Gammasphere software development

    International Nuclear Information System (INIS)

    Piercey, R.B.

    1994-01-01

    This report describes the activities of the nuclear physics group at Mississippi State University which were performed during 1993. Significant progress has been made in the focus areas: chairing the Gammasphere Software Working Group (SWG); assisting with the porting and enhancement of the ORNL UPAK histogramming software package; and developing standard formats for Gammasphere data products. In addition, they have established a new public ftp archive to distribute software and software development tools and information

  1. Software engineer's pocket book

    CERN Document Server

    Tooley, Michael

    2013-01-01

    Software Engineer's Pocket Book provides a concise discussion on various aspects of software engineering. The book is comprised of six chapters that tackle various areas of concerns in software engineering. Chapter 1 discusses software development, and Chapter 2 covers programming languages. Chapter 3 deals with operating systems. The book also tackles discrete mathematics and numerical computation. Data structures and algorithms are also explained. The text will be of great use to individuals involved in the specification, design, development, implementation, testing, maintenance, and qualit

  2. Software Testing Requires Variability

    DEFF Research Database (Denmark)

    Christensen, Henrik Bærbak

    2003-01-01

    Software variability is the ability of a software system or artefact to be changed, customized or configured for use in a particular context. Variability in software systems is important from a number of perspectives. Some perspectives rightly receive much attention due to their direct economic...... impact in software production. As is also apparent from the call for papers these perspectives focus on qualities such as reuse, adaptability, and maintainability....

  3. LANL MTI calibration team experience

    Science.gov (United States)

    Bender, Steven C.; Atkins, William H.; Clodius, William B.; Little, Cynthia K.; Christensen, R. Wynn

    2004-01-01

    The Multispectral Thermal Imager (MTI) was designed as an imaging radiometer with absolute calibration requirements established by Department of Energy (DOE) mission goals. Particular emphasis was given to water surface temperature retrieval using two mid wave and three long wave infrared spectral bands, the fundamental requirement was a surface temperature determination of 1K at the 68% confidence level. For the ten solar reflective bands a one-sigma radiometric performance goal of 3% was established. In order to address these technical challenges a calibration facility was constructed containing newly designed sources that were calibrated at NIST. Additionally, the design of the payload and its onboard calibration system supported post launch maintenance and update of the ground calibration. The on-orbit calibration philosophy also included vicarious techniques using ocean buoys, playas and other instrumented sites; these became increasingly important subsequent to an electrical failure which disabled the onboard calibration system. This paper offers various relevant lessons learned in the eight-year process of reducing to practice the calibration capability required by the scientific mission. The discussion presented will include observations pertinent to operational and procedural issues as well as hardware experiences; the validity of some of the initial assumptions will also be explored.

  4. Field calibration of cup anemometers

    DEFF Research Database (Denmark)

    Kristensen, L.; Jensen, G.; Hansen, A.

    2001-01-01

    An outdoor calibration facility for cup anemometers, where the signals from 10 anemometers of which at least one is a reference can be can be recorded simultaneously, has been established. The results are discussed with special emphasis on the statisticalsignificance of the calibration expressions...

  5. Cobalt source calibration

    International Nuclear Information System (INIS)

    Rizvi, H.M.

    1999-01-01

    The data obtained from these tests determine the dose rate of the two cobalt sources in SRTC. Building 774-A houses one of these sources while the other resides in room C-067 of Building 773-A. The data from this experiment shows the following: (1) The dose rate of the No.2 cobalt source in Building 774-A measured 1.073 x 10 5 rad/h (June 17, 1999). The dose rate of the Shepherd Model 109 Gamma cobalt source in Building 773-A measured 9.27 x 10 5 rad/h (June 25, 1999). These rates come from placing the graduated cylinder containing the dosimeter solution in the center of the irradiation chamber. (2) Two calibration tests in the 774-A source placed the graduated cylinder with the dosimeter solution approximately 1.5 inches off center in the axial direction. This movement of the sample reduced the measured dose rate 0.92% from 1.083 x 10 5 rad/h to 1.073 x 10 5 rad/h. and (3) A similar test in the cobalt source in 773-A placed the graduated cylinder approximately 2.0 inches off center in the axial direction. This change in position reduced the measured dose rate by 10.34% from 1.036 x 10 6 to 9.27 x 10 5 . This testing used chemical dosimetry to measure the dose rate of a radioactive source. In this method, one determines the dose by the chemical change that takes place in the dosimeter. For this calibration experiment, the author used a Fricke (ferrous ammonium sulfate) dosimeter. This solution works well for dose rates to 10 7 rad/h. During irradiation of the Fricke dosimeter solution the Fe 2+ ions ionize to Fe 3+ . When this occurs, the solution acquires a slightly darker tint (not visible to the human eye). To determine the magnitude of the change in Fe ions, one places the solution in an UV-VIS Spectrophotometer. The UV-VIS Spectrophotometer measures the absorbency of the solution. Dividing the absorbency by the total time (in minutes) of exposure yields the dose rate

  6. Computer software quality assurance

    International Nuclear Information System (INIS)

    Ives, K.A.

    1986-06-01

    The author defines some criteria for the evaluation of software quality assurance elements for applicability to the regulation of the nuclear industry. The author then analyses a number of software quality assurance (SQA) standards. The major extracted SQA elements are then discussed, and finally specific software quality assurance recommendations are made for the nuclear industry

  7. Software Architecture Evolution

    Science.gov (United States)

    Barnes, Jeffrey M.

    2013-01-01

    Many software systems eventually undergo changes to their basic architectural structure. Such changes may be prompted by new feature requests, new quality attribute requirements, changing technology, or other reasons. Whatever the causes, architecture evolution is commonplace in real-world software projects. Today's software architects, however,…

  8. XES Software Communication Extension

    NARCIS (Netherlands)

    Leemans, M.; Liu, C.

    2017-01-01

    During the execution of software, execution data can be recorded. With the development of process mining techniques on the one hand, and the growing availability of software execution data on the other hand, a new form of software analytics comes into reach. That is, applying process mining

  9. Neutron Scattering Software

    Science.gov (United States)

    Home Page | Facilities | Reference | Software | Conferences | Announcements | Mailing Lists Neutron Scattering Banner Neutron Scattering Software A new portal for neutron scattering has just been established sets KUPLOT: data plotting and fitting software ILL/TAS: Matlab probrams for analyzing triple axis data

  10. XES Software Event Extension

    NARCIS (Netherlands)

    Leemans, M.; Liu, C.

    2017-01-01

    During the execution of software, execution data can be recorded. With the development of process mining techniques on the one hand, and the growing availability of software execution data on the other hand, a new form of software analytics comes into reach. That is, applying process mining

  11. ARC Software and Models

    Science.gov (United States)

    Archives RESEARCH ▼ Research Areas Ongoing Projects Completed Projects SOFTWARE CONTACT ▼ Primary Contacts Researchers External Link MLibrary Deep Blue Software Archive Most research conducted at the ARC produce software code and methodologies that are transferred to TARDEC and industry partners. These

  12. XES Software Telemetry Extension

    NARCIS (Netherlands)

    Leemans, M.; Liu, C.

    2017-01-01

    During the execution of software, execution data can be recorded. With the development of process mining techniques on the one hand, and the growing availability of software execution data on the other hand, a new form of software analytics comes into reach. That is, applying process mining

  13. Specifications in software prototyping

    OpenAIRE

    Luqi; Chang, Carl K.; Zhu, Hong

    1998-01-01

    We explore the use of software speci®cations for software prototyping. This paper describes a process model for software prototyping, and shows how specifications can be used to support such a process via a cellular mobile phone switch example.

  14. Software Engineering for Portability.

    Science.gov (United States)

    Stanchev, Ivan

    1990-01-01

    Discussion of the portability of educational software focuses on the software design and development process. Topics discussed include levels of portability; the user-computer dialog; software engineering principles; design techniques for student performance records; techniques of courseware programing; and suggestions for further research and…

  15. Software Acquisition and Software Engineering Best Practices

    National Research Council Canada - National Science Library

    Eslinger, S

    1999-01-01

    The purpose of this white paper is to address the issues raised in the recently published Senate Armed Services Committee Report 106-50 concerning Software Management Improvements for the Department of Defense (DoD...

  16. Calibration and compensation of deflections and compliances in remote handling equipment configurations

    International Nuclear Information System (INIS)

    Kivelae, Tuomo; Saarinen, H.; Mattila, J.; Haemaelaeinen, V.; Siuko, M.; Semeraro, L.

    2011-01-01

    This paper presents a generic method of calibrating and compensating remote handling system configurations subject to manufacturing and assembly tolerances, deflections and compliances. A method consists of kinematic part and non-kinematic part. A kinematic calibration algorithm is presented for finding the values of kinematic model errors by measuring the end-effector Cartesian position. This is a conventional way to calibrate industrial robots. However, in this case the kinematic calibration is not able to compensate flaws fully due to large deflections and compliances caused by a massive Cassette payload (approx. 9 ton). Positioning error at the furthest point of the cassette before any compensation was 80 mm. Therefore, extra compensation must be introduced in addition to a kinematic calibration. A kinematic calibration together with an extra compensation is a demanding task to carry out. The resulting complex compensation function has to be such that it can be implemented in real-time Cassette Multifunctional Mover (CMM) control system software.

  17. Bench calibration of INDUS-2 beam position indicators

    International Nuclear Information System (INIS)

    Tyagi, Y.; Banerji, Anil; Kotaiah, S.

    2005-01-01

    A third generation synchrotron radiation source of energy 2.5 GeV named INDUS-2 at Centre for Advanced Technology (C.A.T), Indore (M.P) is in the advanced stage of construction. Accurate determination and correction of beam closed orbit in INDUS-2 machine within 100 of microns is a very desirable goal. Bench based calibration of Beam Position Indicators (BPI) play a very important and useful role during initial commissioning of electron machines. To precisely measure transverse position of electron beam in the Indus-2 storage ring, 56 Beam Position Indicators (BPI) will be installed in INDUS-2 machine. Out of 56 Beam Position Indicators 40 are of individual type whereas 16 are integrated with dipole vacuum chamber. The Beam Position Indicators are required to be calibrated before they can be installed. The calibration is done to determine electrical offset with respect to defined mechanical centre, to determine displacement sensitivities as well as non linearity's of BPI. Ideally when beam passes through the geometrical center of BPI's, all electrodes should have same signal strength. However due to different capacitance of electrodes and offset and drift in electronics, the electrical centre (mechanical x, y where all electrodes shows same signal strength) differs from mechanical centre of BPI. A fully automatic calibration system has been developed to carry out the calibration of Beam Position Indicators. A calibration software has been developed which has necessary utilities to process and display calibration data and results. This paper describes the calibration results of Indus-2 BPM. (author)

  18. Permanently calibrated interpolating time counter

    International Nuclear Information System (INIS)

    Jachna, Z; Szplet, R; Kwiatkowski, P; Różyc, K

    2015-01-01

    We propose a new architecture of an integrated time interval counter that provides its permanent calibration in the background. Time interval measurement and the calibration procedure are based on the use of a two-stage interpolation method and parallel processing of measurement and calibration data. The parallel processing is achieved by a doubling of two-stage interpolators in measurement channels of the counter, and by an appropriate extension of control logic. Such modification allows the updating of transfer characteristics of interpolators without the need to break a theoretically infinite measurement session. We describe the principle of permanent calibration, its implementation and influence on the quality of the counter. The precision of the presented counter is kept at a constant level (below 20 ps) despite significant changes in the ambient temperature (from −10 to 60 °C), which can cause a sevenfold decrease in the precision of the counter with a traditional calibration procedure. (paper)

  19. TIME CALIBRATED OSCILLOSCOPE SWEEP CIRCUIT

    Science.gov (United States)

    Smith, V.L.; Carstensen, H.K.

    1959-11-24

    An improved time calibrated sweep circuit is presented, which extends the range of usefulness of conventional oscilloscopes as utilized for time calibrated display applications in accordance with U. S. Patent No. 2,832,002. Principal novelty resides in the provision of a pair of separate signal paths, each of which is phase and amplitude adjustable, to connect a high-frequency calibration oscillator to the output of a sawtooth generator also connected to the respective horizontal deflection plates of an oscilloscope cathode ray tube. The amplitude and phase of the calibration oscillator signals in the two signal paths are adjusted to balance out feedthrough currents capacitively coupled at high frequencies of the calibration oscillator from each horizontal deflection plate to the vertical plates of the cathode ray tube.

  20. Software Quality Assurance in Software Projects: A Study of Pakistan

    OpenAIRE

    Faisal Shafique Butt; Sundus Shaukat; M. Wasif Nisar; Ehsan Ullah Munir; Muhammad Waseem; Kashif Ayyub

    2013-01-01

    Software quality is specific property which tells what kind of standard software should have. In a software project, quality is the key factor of success and decline of software related organization. Many researches have been done regarding software quality. Software related organization follows standards introduced by Capability Maturity Model Integration (CMMI) to achieve good quality software. Quality is divided into three main layers which are Software Quality Assurance (SQA), Software Qu...

  1. Model calibration and beam control systems for storage rings

    International Nuclear Information System (INIS)

    Corbett, W.J.; Lee, M.J.; Ziemann, V.

    1993-04-01

    Electron beam storage rings and linear accelerators are rapidly gaining worldwide popularity as scientific devices for the production of high-brightness synchrotron radiation. Today, everybody agrees that there is a premium on calibrating the storage ring model and determining errors in the machine as soon as possible after the beam is injected. In addition, the accurate optics model enables machine operators to predictably adjust key performance parameters, and allows reliable identification of new errors that occur during operation of the machine. Since the need for model calibration and beam control systems is common to all storage rings, software packages should be made that are portable between different machines. In this paper, we report on work directed toward achieving in-situ calibration of the optics model, detection of alignment errors, and orbit control techniques, with an emphasis on developing a portable system incorporating these tools

  2. Reliably detectable flaw size for NDE methods that use calibration

    Science.gov (United States)

    Koshti, Ajay M.

    2017-04-01

    Probability of detection (POD) analysis is used in assessing reliably detectable flaw size in nondestructive evaluation (NDE). MIL-HDBK-1823 and associated mh18232 POD software gives most common methods of POD analysis. In this paper, POD analysis is applied to an NDE method, such as eddy current testing, where calibration is used. NDE calibration standards have known size artificial flaws such as electro-discharge machined (EDM) notches and flat bottom hole (FBH) reflectors which are used to set instrument sensitivity for detection of real flaws. Real flaws such as cracks and crack-like flaws are desired to be detected using these NDE methods. A reliably detectable crack size is required for safe life analysis of fracture critical parts. Therefore, it is important to correlate signal responses from real flaws with signal responses form artificial flaws used in calibration process to determine reliably detectable flaw size.

  3. Calibrating the Cryogenian

    Science.gov (United States)

    MacDonald, F. A.; Schmitz, M. D.; Crowley, J. L.; Haam, E.; Huybers, P.; Cohen, P. A.; Johnston, D. T.

    2009-12-01

    The IGCP 512 sub-commission on the Neoproterozoic is currently discussing criteria for the definition of the Cryogenian period. Herein we provide new U/Pb ID-TIMS ages and carbon and oxygen isotope data from Fifteenmile and Mt. Harper Groups in the Yukon Territory that inform the basis for the placement of the basal Cryogenian “golden spike”. Our U/Pb ages are from volcanic tuffs interbedded within glaciogenic, fossiliferous, and carbonate strata. With the current lack of Neoproterozoic index fossils and the paucity of radiogenic age constraints, chemo-stratigraphic correlations are particularly important for tuning the Neoproterozoic timescale. In an effort to move beyond conventional 'wiggle matching', chemostratigraphic correlations are determined using a new statistical method1, which indicates that the resulting chemo-stratigraphic correlations are statistically significant. These results permit us to refine and integrate Neoproterozoic climate, microfossil, and geochemical proxy records both regionally and globally. The newly calibrated microfossil record points to a eukaryotic radiation roughly coincident with the Bitter Springs isotopic stage and a barren interval between the Sturtian and Marinoan glaciations. 1 Haam, E. & Huybers, P., 2009, A test for the presence of covariance between time-uncertain series of data with applications to the Dongge Cave speleothem and atmospheric radiocarbon records, Paleoceanography, in press.

  4. Licensing safety critical software

    International Nuclear Information System (INIS)

    Archinoff, G.H.; Brown, R.A.

    1990-01-01

    Licensing difficulties with the shutdown system software at the Darlington Nuclear Generating Station contributed to delays in starting up the station. Even though the station has now been given approval by the Atomic Energy Control Board (AECB) to operate, the software issue has not disappeared - Ontario Hydro has been instructed by the AECB to redesign the software. This article attempts to explain why software based shutdown systems were chosen for Darlington, why there was so much difficulty licensing them, and what the implications are for other safety related software based applications

  5. Determination of absorbed dose to water in a clinical carbon ion beam by means of fluorescent nuclear track detectors, ionization chambers, and water calorimetry

    Energy Technology Data Exchange (ETDEWEB)

    Osinga-Blaettermann, Julia-Maria

    2016-12-20

    Until now, dosimetry of carbon ions with ionization chambers has not reached the same level of accuracy as of high-energy photons. This is mainly caused by the threefold higher uncertainty of the k{sub Q,Q{sub 0}}-factor of ionization chambers, which is derived by calculations due to a lack of experimental data. The current thesis comprises two major aims with respect to the dosimetry of carbon ion beams: first, the investigation of the potential of fluorescent nuclear track detectors for fluence-based dosimetry and second, the experimental determination of the k{sub Q,Q{sub 0}}-factor. The direct comparison of fluence- and ionization-based measurements has shown a significant discrepancy of 4.5 %, which re-opened the discussion on the accuracy of calculated k{sub Q,Q{sub 0}}-factors. Therefore, absorbed dose to water measurements by means of water calorimetry have been performed allowing for the direct calibration of ionization chambers and thus for the experimental determination of k{sub Q,Q{sub 0}}. For the first time it could be shown that the experimental determination of k{sub Q,Q{sub 0}} for carbon ion beams is achievable with a standard measurement uncertainty of 0.8 %. This corresponds to a threefold reduction of the uncertainty compared to calculated values and therefore enables to significantly decrease the overall uncertainty related to ionization-based dosimetry of clinical carbon ion beams.

  6. HAZARD ANALYSIS SOFTWARE

    International Nuclear Information System (INIS)

    Sommer, S; Tinh Tran, T.

    2008-01-01

    Washington Safety Management Solutions, LLC developed web-based software to improve the efficiency and consistency of hazard identification and analysis, control selection and classification, and to standardize analysis reporting at Savannah River Site. In the new nuclear age, information technology provides methods to improve the efficiency of the documented safety analysis development process which includes hazard analysis activities. This software provides a web interface that interacts with a relational database to support analysis, record data, and to ensure reporting consistency. A team of subject matter experts participated in a series of meetings to review the associated processes and procedures for requirements and standard practices. Through these meetings, a set of software requirements were developed and compiled into a requirements traceability matrix from which software could be developed. The software was tested to ensure compliance with the requirements. Training was provided to the hazard analysis leads. Hazard analysis teams using the software have verified its operability. The software has been classified as NQA-1, Level D, as it supports the analysis team but does not perform the analysis. The software can be transported to other sites with alternate risk schemes. The software is being used to support the development of 14 hazard analyses. User responses have been positive with a number of suggestions for improvement which are being incorporated as time permits. The software has enforced a uniform implementation of the site procedures. The software has significantly improved the efficiency and standardization of the hazard analysis process

  7. Mercury Continuous Emmission Monitor Calibration

    Energy Technology Data Exchange (ETDEWEB)

    John Schabron; Eric Kalberer; Ryan Boysen; William Schuster; Joseph Rovani

    2009-03-12

    Mercury continuous emissions monitoring systems (CEMs) are being implemented in over 800 coal-fired power plant stacks throughput the U.S. Western Research Institute (WRI) is working closely with the Electric Power Research Institute (EPRI), the National Institute of Standards and Technology (NIST), and the Environmental Protection Agency (EPA) to facilitate the development of the experimental criteria for a NIST traceability protocol for dynamic elemental mercury vapor calibrators/generators. These devices are used to calibrate mercury CEMs at power plant sites. The Clean Air Mercury Rule (CAMR) which was published in the Federal Register on May 18, 2005 and vacated by a Federal appeals court in early 2008 required that calibration be performed with NIST-traceable standards. Despite the vacature, mercury emissions regulations in the future will require NIST traceable calibration standards, and EPA does not want to interrupt the effort towards developing NIST traceability protocols. The traceability procedures will be defined by EPA. An initial draft traceability protocol was issued by EPA in May 2007 for comment. In August 2007, EPA issued a conceptual interim traceability protocol for elemental mercury calibrators. The protocol is based on the actual analysis of the output of each calibration unit at several concentration levels ranging initially from about 2-40 {micro}g/m{sup 3} elemental mercury, and in the future down to 0.2 {micro}g/m{sup 3}, and this analysis will be directly traceable to analyses by NIST. The EPA traceability protocol document is divided into two separate sections. The first deals with the qualification of calibrator models by the vendors for use in mercury CEM calibration. The second describes the procedure that the vendors must use to certify the calibrators that meet the qualification specifications. The NIST traceable certification is performance based, traceable to analysis using isotope dilution inductively coupled plasma

  8. Software Validation in ATLAS

    International Nuclear Information System (INIS)

    Hodgkinson, Mark; Seuster, Rolf; Simmons, Brinick; Sherwood, Peter; Rousseau, David

    2012-01-01

    The ATLAS collaboration operates an extensive set of protocols to validate the quality of the offline software in a timely manner. This is essential in order to process the large amounts of data being collected by the ATLAS detector in 2011 without complications on the offline software side. We will discuss a number of different strategies used to validate the ATLAS offline software; running the ATLAS framework software, Athena, in a variety of configurations daily on each nightly build via the ATLAS Nightly System (ATN) and Run Time Tester (RTT) systems; the monitoring of these tests and checking the compilation of the software via distributed teams of rotating shifters; monitoring of and follow up on bug reports by the shifter teams and periodic software cleaning weeks to improve the quality of the offline software further.

  9. Comparing Single-Point and Multi-point Calibration Methods in Modulated DSC

    Energy Technology Data Exchange (ETDEWEB)

    Van Buskirk, Caleb Griffith [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-06-14

    Heat capacity measurements for High Density Polyethylene (HDPE) and Ultra-high Molecular Weight Polyethylene (UHMWPE) were performed using Modulated Differential Scanning Calorimetry (mDSC) over a wide temperature range, -70 to 115 °C, with a TA Instruments Q2000 mDSC. The default calibration method for this instrument involves measuring the heat capacity of a sapphire standard at a single temperature near the middle of the temperature range of interest. However, this method often fails for temperature ranges that exceed a 50 °C interval, likely because of drift or non-linearity in the instrument's heat capacity readings over time or over the temperature range. Therefore, in this study a method was developed to calibrate the instrument using multiple temperatures and the same sapphire standard.

  10. Calibration and test of an aneroid mini-bomb combustion calorimeter

    International Nuclear Information System (INIS)

    Ribeiro da Silva, Manuel A.V.; Pilcher, Geoffrey; Santos, Luis M.N.B.F.; Lima, Luis M. Spencer S.

    2007-01-01

    A new mini-bomb combustion calorimeter designed at the University of Lund was improved, installed and calibrated at the University of Porto. This calorimeter is suitable for high precision combustion calorimetry with samples of mass about (10 to 40)mg. The energy equivalent of the calorimeter, ε cal =(1946.45+/-0.11)J.K -1 , was obtained from 15 independent calibration experiments with benzoic acid SRM 39i. Anthracene, succinic acid, acetanilide, and 1,2,4-triazole were used as test compounds, with excellent agreement with the literature values. -Δ c H m o Δ f H m o (cr)kJ.mol -1 kJ.mol -1 Anthracene7062.6+/-2.1124.3+/-2.8Succinic acid1490.2+/-0.7-941.3+/-0.9Acetanilide4226.2+/-1.1-208.2+/-1.61,2, 4-Triazole1326.1+/-0.4110.3+/-0.5

  11. Online neural trigger for optimizing data acquisition during particle beam calibration tests with calorimeters

    International Nuclear Information System (INIS)

    Silva, P.V.M. da; Seixas, J.M. de; Damazio, D.O.; Ferreira, B.C.

    2004-01-01

    For LHC, the hadronic calorimetry of the ATLAS detector is performed by Tilecal, a scintillating tile calorimeter. For calibration purposes, a fraction of the Tilecal modules is placed in particle beam lines. Despite beam high quality, experimental beam contamination is observed and this masks the actual performance of the calorimeter. For optimizing the calibration task, an online neural particle classifier was developed for Tilecal. Envisaging a neural trigger for incoming particles, a neural process runs integrated to the data acquisition task and performs online training for particle identification. The neural classification performance is evaluated by correlating the neural response to classical methodology, confirming an ability for outsider identification at levels as high as 99.3%

  12. Online neural trigger for optimizing data acquisition during particle beam calibration tests with calorimeters

    CERN Document Server

    Da Silva, P V M; De Seixas, J M; Ferreira, B C

    2004-01-01

    For LHC, the hadronic calorimetry of the ATLAS detector is performed by Tilecal, a scintillating tile calorimeter. For calibration purposes, a fraction of the Tilecal modules is placed in particle beam lines. Despite beam high quality, experimental beam contamination is observed and this masks the actual performance of the calorimeter. For optimizing the calibration task, an online neural particle classifier was developed for Tilecal. Envisaging a neural trigger for incoming particles, a neural process runs integrated to the data acquisition task and performs online training for particle identification. The neural classification performance is evaluated by correlating the neural response to classical methodology, confirming an ability for outsider identification at levels as high as 99.3%.

  13. The Mars Science Laboratory APXS calibration target: Comparison of Martian measurements with the terrestrial calibration

    International Nuclear Information System (INIS)

    Campbell, J.L.; King, P.L.; Burkemper, L.; Berger, J.A.; Gellert, R.; Boyd, N.I.; Perrett, G.M.; Pradler, I.; Thompson, L.; Edgett, K.S.; Yingst, R.A.

    2014-01-01

    The Mars Science Laboratory Curiosity rover carries a basalt calibration target for monitoring the performance of the alpha particle X-ray spectrometer. The spectrum acquired on Sol 34 shows increased contributions from Mg, S, Cl and Fe relative to laboratory spectra recorded before launch. Mars Hand Lens Imager images confirm changes in the appearance of the surface. Spectra taken on Sols 179 and 411 indicate some loss of the deposited material. The observations suggest deposition of a surface film likely consisting of dust mobilized by impingement of the sky crane’s terminal descent engine plumes with surface fines during Curiosity’s landing. New APXS software has been used to model the thin film that coated the calibration target on landing. The results suggest that a film of about 100 nm thickness, and containing predominantly MgO, Fe 2 O 3 , SO 3 , Cl and Na 2 O could give rise to the observed spectral changes. If this film is also present on the alpha particle sources within the APXS, then its effect is negligible and the terrestrial calibration remains appropriate

  14. The Mars Science Laboratory APXS calibration target: Comparison of Martian measurements with the terrestrial calibration

    Energy Technology Data Exchange (ETDEWEB)

    Campbell, J.L., E-mail: icampbel@uoguelph.ca [Guelph-Waterloo Physics Institute, University of Guelph, Ontario N1G2W1 (Canada); King, P.L. [Guelph-Waterloo Physics Institute, University of Guelph, Ontario N1G2W1 (Canada); Institute of Meteoritics, University of New Mexico, NM 87131 (United States); Department of Earth Sciences, Western University, London, Ontario N6A3K7 (Canada); Burkemper, L. [Institute of Meteoritics, University of New Mexico, NM 87131 (United States); Berger, J.A. [Institute of Meteoritics, University of New Mexico, NM 87131 (United States); Department of Earth Sciences, Western University, London, Ontario N6A3K7 (Canada); Gellert, R.; Boyd, N.I.; Perrett, G.M.; Pradler, I. [Guelph-Waterloo Physics Institute, University of Guelph, Ontario N1G2W1 (Canada); Thompson, L. [Planetary and Space Science Centre, University of New Brunswick, Fredericton, NB E3B5A3 (Canada); Edgett, K.S. [Malin Space Science Systems, San Diego, CA 92191-0148 (United States); Yingst, R.A. [Planetary Science Institute, Tucson, AZ 85719-2395 (United States)

    2014-03-15

    The Mars Science Laboratory Curiosity rover carries a basalt calibration target for monitoring the performance of the alpha particle X-ray spectrometer. The spectrum acquired on Sol 34 shows increased contributions from Mg, S, Cl and Fe relative to laboratory spectra recorded before launch. Mars Hand Lens Imager images confirm changes in the appearance of the surface. Spectra taken on Sols 179 and 411 indicate some loss of the deposited material. The observations suggest deposition of a surface film likely consisting of dust mobilized by impingement of the sky crane’s terminal descent engine plumes with surface fines during Curiosity’s landing. New APXS software has been used to model the thin film that coated the calibration target on landing. The results suggest that a film of about 100 nm thickness, and containing predominantly MgO, Fe{sub 2}O{sub 3}, SO{sub 3}, Cl and Na{sub 2}O could give rise to the observed spectral changes. If this film is also present on the alpha particle sources within the APXS, then its effect is negligible and the terrestrial calibration remains appropriate.

  15. Kinect Fusion improvement using depth camera calibration

    Science.gov (United States)

    Pagliari, D.; Menna, F.; Roncella, R.; Remondino, F.; Pinto, L.

    2014-06-01

    Scene's 3D modelling, gesture recognition and motion tracking are fields in rapid and continuous development which have caused growing demand on interactivity in video-game and e-entertainment market. Starting from the idea of creating a sensor that allows users to play without having to hold any remote controller, the Microsoft Kinect device was created. The Kinect has always attract researchers in different fields, from robotics to Computer Vision (CV) and biomedical engineering as well as third-party communities that have released several Software Development Kit (SDK) versions for Kinect in order to use it not only as a game device but as measurement system. Microsoft Kinect Fusion control libraries (firstly released in March 2013) allow using the device as a 3D scanning and produce meshed polygonal of a static scene just moving the Kinect around. A drawback of this sensor is the geometric quality of the delivered data and the low repeatability. For this reason the authors carried out some investigation in order to evaluate the accuracy and repeatability of the depth measured delivered by the Kinect. The paper will present a throughout calibration analysis of the Kinect imaging sensor, with the aim of establishing the accuracy and precision of the delivered information: a straightforward calibration of the depth sensor in presented and then the 3D data are correct accordingly. Integrating the depth correction algorithm and correcting the IR camera interior and exterior orientation parameters, the Fusion Libraries are corrected and a new reconstruction software is created to produce more accurate models.

  16. Kinect Fusion improvement using depth camera calibration

    Directory of Open Access Journals (Sweden)

    D. Pagliari

    2014-06-01

    Full Text Available Scene's 3D modelling, gesture recognition and motion tracking are fields in rapid and continuous development which have caused growing demand on interactivity in video-game and e-entertainment market. Starting from the idea of creating a sensor that allows users to play without having to hold any remote controller, the Microsoft Kinect device was created. The Kinect has always attract researchers in different fields, from robotics to Computer Vision (CV and biomedical engineering as well as third-party communities that have released several Software Development Kit (SDK versions for Kinect in order to use it not only as a game device but as measurement system. Microsoft Kinect Fusion control libraries (firstly released in March 2013 allow using the device as a 3D scanning and produce meshed polygonal of a static scene just moving the Kinect around. A drawback of this sensor is the geometric quality of the delivered data and the low repeatability. For this reason the authors carried out some investigation in order to evaluate the accuracy and repeatability of the depth measured delivered by the Kinect. The paper will present a throughout calibration analysis of the Kinect imaging sensor, with the aim of establishing the accuracy and precision of the delivered information: a straightforward calibration of the depth sensor in presented and then the 3D data are correct accordingly. Integrating the depth correction algorithm and correcting the IR camera interior and exterior orientation parameters, the Fusion Libraries are corrected and a new reconstruction software is created to produce more accurate models.

  17. Thermodynamically consistent model calibration in chemical kinetics

    Directory of Open Access Journals (Sweden)

    Goutsias John

    2011-05-01

    Full Text Available Abstract Background The dynamics of biochemical reaction systems are constrained by the fundamental laws of thermodynamics, which impose well-defined relationships among the reaction rate constants characterizing these systems. Constructing biochemical reaction systems from experimental observations often leads to parameter values that do not satisfy the necessary thermodynamic constraints. This can result in models that are not physically realizable and may lead to inaccurate, or even erroneous, descriptions of cellular function. Results We introduce a thermodynamically consistent model calibration (TCMC method that can be effectively used to provide thermodynamically feasible values for the parameters of an open biochemical reaction system. The proposed method formulates the model calibration problem as a constrained optimization problem that takes thermodynamic constraints (and, if desired, additional non-thermodynamic constraints into account. By calculating thermodynamically feasible values for the kinetic parameters of a well-known model of the EGF/ERK signaling cascade, we demonstrate the qualitative and quantitative significance of imposing thermodynamic constraints on these parameters and the effectiveness of our method for accomplishing this important task. MATLAB software, using the Systems Biology Toolbox 2.1, can be accessed from http://www.cis.jhu.edu/~goutsias/CSS lab/software.html. An SBML file containing the thermodynamically feasible EGF/ERK signaling cascade model can be found in the BioModels database. Conclusions TCMC is a simple and flexible method for obtaining physically plausible values for the kinetic parameters of open biochemical reaction systems. It can be effectively used to recalculate a thermodynamically consistent set of parameter values for existing thermodynamically infeasible biochemical reaction models of cellular function as well as to estimate thermodynamically feasible values for the parameters of new

  18. Heat capacity and transition behavior of sucrose by standard, fast scanning and temperature-modulated calorimetry

    Energy Technology Data Exchange (ETDEWEB)

    Magoń, A. [Department of Chemistry, University of Technology, 35-959 Rzeszów (Poland); Wurm, A.; Schick, C. [Department of Physics, University of Rostock, 18057 Rostock (Germany); Pangloli, Ph.; Zivanovic, S. [Department of Food Science and Technology, University of Tennessee, Knoxville, TN 37996 (United States); Skotnicki, M. [Department of Pharmaceutical Technology, Poznan University of Medical Sciences, 60-780 Poznań (Poland); Pyda, M., E-mail: mpyda@utk.edu [Department of Chemistry, University of Technology, 35-959 Rzeszów (Poland)

    2014-08-10

    Highlights: • Experimental, apparent heat capacity of sucrose was investigated by advanced thermal analysis. • Vibrational heat capacity of solid state was linked with a low temperature experimental heat capacity of sucrose. • Equilibrium melting parameters of sucrose were determined. • Decomposition, superheating of crystalline sucrose during melting process were presented. • TGA, DSC, TMDSC, and FSC are useful tools for characterization of sucrose. - Abstract: The heat capacity (C{sub p}) of crystalline and amorphous sucrose was determined using standard and quasi-isothermal temperature modulated differential scanning calorimetry. The results were combined with the published data determined by adiabatic calorimetry, and the C{sub p} values are now reported for the wide 5–600 K range. The experimental C{sub p} of solid sucrose at 5–300 K was used to calculate the vibrational, solid C{sub p} based on the vibrational molecular motions. The calculated solid and liquid C{sub p} together with the transition parameters for equilibrium conditions were used as references for detailed quantitative thermal analysis of crystalline and amorphous sucrose. Melting temperature (T{sub m}) of the crystalline sucrose was identified in a broad 442–465 K range with a heat of fusion of 40–46 J/mol determined at heating rates 0.5–20 K/min, respectively. The equilibrium T{sub m} and heat of fusion of crystalline sucrose were estimated at zero heating rate as T{sup o}{sub m} = 424.4 K and ΔH{sup o}{sub f} = 32 kJ/mol, respectively. The glass transition temperature (T{sub g}) of amorphous sucrose was at 331 K with a change in C{sub p} of 267 J/(mol K) as it was estimated from reversing heat capacity by quasi-isothermal TMDSC on cooling. At heating rates less than 30 K/min, thermal decomposition occurred during melting, while at extreme rate of 1000 K/s, degradation was not observed. Data obtained by fast scanning calorimetry (FSC) at 1000 K/s, showed that T{sub m} was

  19. LHCb calorimeter electronics. Photon identification. Calorimeter calibration

    International Nuclear Information System (INIS)

    Machefert, F.

    2011-01-01

    LHCb is one of the four large experiments installed on the LHC accelerator ring. The aim of the detector is to precisely measure CP violation observables and rare decays in the B meson sector. The calorimeter system of LHCb is made of four sub-systems: the scintillating pad detector, the pre-shower, the electromagnetic (ECAL) and hadronic (HCAL) calorimeters. It is essential to reconstruct B decays, to efficiently trigger on interesting events and to identify electrons and photons. After a review of the LHCb detector sub-systems, the first part of this document describes the calorimeter electronics. First, the front-end electronics in charge of measuring the ECAL and HCAL signals from the photomultipliers is presented, then the following section is an overview of the control card of the four calorimeters. The chapters three and four concern the test software of this electronics and the technological choices making it tolerant to radiations in the LHCb cavern environment. The measurements performed to ensure this tolerance are also given. The second part of this document concerns both the identification of the photons with LHCb and the calibration of the calorimeters. The photon identification method is presented and the performances given. Finally, the absolute energy calibration of the PRS and ECAL, based on the data stored in 2010 is explained. (author)

  20. The ATLAS Inner Detector commissioning and calibration

    CERN Document Server

    Aad, G.; Abdallah, J.; Abdelalim, A.A.; Abdesselam, A.; Abdinov, O.; Abi, B.; Abolins, M.; Abramowicz, H.; Abreu, H.; Acharya, B.S.; Adams, D.L.; Addy, T.N.; Adelman, J.; Adorisio, C.; Adragna, P.; Adye, T.; Aefsky, S.; Aguilar-Saavedra, J.A.; Aharrouche, M.; Ahlen, S.P.; Ahles, F.; Ahmad, A.; Ahsan, M.; Aielli, G.; Akdogan, T.; Akesson, T.P.A.; Akimoto, G.; Akimov, A.V.; Aktas, A.; Alam, M.S.; Alam, M.A.; Albert, J.; Albrand, S.; Aleksa, M.; Aleksandrov, I.N.; Alexa, C.; Alexander, G.; Alexandre, G.; Alexopoulos, T.; Alhroob, M.; Aliev, M.; Alimonti, G.; Alison, J.; Aliyev, M.; Allport, P.P.; Allwood-Spiers, S.E.; Almond, J.; Aloisio, A.; Alon, R.; Alonso, A.; Alviggi, M.G.; Amako, K.; Amelung, C.; Amorim, A.; Amoros, G.; Amram, N.; Anastopoulos, C.; Andeen, T.; Anders, C.F.; Anderson, K.J.; Andreazza, A.; Andrei, V.; Anduaga, X.S.; Angerami, A.; Anghinolfi, F.; Anjos, N.; Annovi, A.; Antonaki, A.; Antonelli, M.; Antonelli, S.; Antos, J.; Antunovic, B.; Anulli, F.; Aoun, S.; Arabidze, G.; Aracena, I.; Arai, Y.; Arce, A.T.H.; Archambault, J.P.; Arfaoui, S.; Arguin, J-F.; Argyropoulos, T.; Arik, M.; Armbruster, A.J.; Arnaez, O.; Arnault, C.; Artamonov, A.; Arutinov, D.; Asai, M.; Asai, S.; Asfandiyarov, R.; Ask, S.; Asman, B.; Asner, D.; Asquith, L.; Assamagan, K.; Astbury, A.; Astvatsatourov, A.; Atoian, G.; Auerbach, B.; Augsten, K.; Aurousseau, M.; Austin, N.; Avolio, G.; Avramidou, R.; Axen, D.; Ay, C.; Azuelos, G.; Azuma, Y.; Baak, M.A.; Bach, A.M.; Bachacou, H.; Bachas, K.; Backes, M.; Badescu, E.; Bagnaia, P.; Bai, Y.; Bain, T.; Baines, J.T.; Baker, O.K.; Baker, M.D.; Baker, S.; Baltasar Dos, F.Santos Pedrosa; Banas, E.; Banerjee, P.; Banerjee, S.; Banfi, D.; Bangert, A.; Bansal, V.; Baranov, S.P.; Baranov, S.; Barashkou, A.; Barber, T.; Barberio, E.L.; Barberis, D.; Barbero, M.; Bardin, D.Y.; Barillari, T.; Barisonzi, M.; Barklow, T.; Barlow, N.; Barnett, B.M.; Barnett, R.M.; Baroncelli, A.; Barr, A.J.; Barreiro, F.; Guimara, J.Barreiro; Barrillon, P.; Bartoldus, R.; 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    2010-01-01

    The ATLAS Inner Detector is a composite tracking system consisting of silicon pixels, silicon strips and straw tubes in a 2 T magnetic field. Its installation was completed in August 2008 and the detector took part in data- taking with single LHC beams and cosmic rays. The initial detector operation, hardware commissioning and in-situ calibrations are described. Tracking performance has been measured with 7.6 million cosmic-ray events, collected using a tracking trigger and reconstructed with modular pattern-recognition and fitting software. The intrinsic hit efficiency and tracking trigger efficiencies are close to 100%. Lorentz angle measurements for both electrons and holes, specific energy-loss calibration and transition radiation turn-on measurements have been performed. Different alignment techniques have been used to reconstruct the detector geometry. After the initial alignment, a transverse impact parameter resolution of 22.1+/-0.9 {\\mu}m and a relative momentum resolution {\\sigma}p/p = (4.83+/-0.16)...