WorldWideScience

Sample records for bulk plasma pressure

  1. Sheath and bulk expansion induced by RF bias in atmospheric pressure microwave plasma

    Science.gov (United States)

    Lee, Jimo; Nam, Woojin; Lee, Jae Koo; Yun, Gunsu

    2017-10-01

    A large axial volume expansion of microwave-driven plasma at atmospheric pressure is achieved by applying a low power radio frequency (RF) bias at an axial location well isolated from the original plasma bulk. The evolution of the plasma plume visualized by high speed ICCD imaging suggest that the free electrons drifting toward the bias electrode cause the prodigious expansion of the sheath, creating a stable plasma stream channel between the microwave and the RF electrodes. For argon plasma in ambient air, enhanced emissions of OH and N2 spectral lines are measured in the extended plume region, supporting the acceleration of electrons and subsequent generation of radical species. The coupling of RF bias with microwave provides an efficient way of enlarging the plasma volume and enhancing the production of radicals. Work supported by the National Research Foundation of Korea under BK21+ program and Grant No. 2015R1D1A1A01061556 (Ministry of Education).

  2. Low-pressure plasma-etching of bulk polymer materials using gas mixture of CF4 and O2

    Science.gov (United States)

    Nabesawa, Hirofumi; Hiruma, Takaharu; Hitobo, Takeshi; Wakabayashi, Suguru; Asaji, Toyohisa; Abe, Takashi; Seki, Minoru

    2013-11-01

    In this study, we have proposed a low-pressure reactive ion etching of bulk polymer materials with a gas mixture of CF4 and O2, and have achieved precise fabrication of poly(methyl methacrylate) (PMMA) and perfluoroalkoxy (PFA) bulk polymer plates with high-aspect-ratio and narrow gap array structures, such as, pillar, frustum, or cone, on a nano/micro scale. The effects of the etching conditions on the shape and size of each pillar were evaluated by changing etching duration and the size/material of etching mask. The fabricated PMMA array structures indicate possibilities of optical waveguide and nanofiber array. PFA cone array structures showed super-hydrophobicity without any chemical treatments. Also, polystyrene-coated silica spheres were used as an etching mask for the pillar array structure formation to control the gap between pillars.

  3. Negative ion extraction from hydrogen plasma bulk

    Energy Technology Data Exchange (ETDEWEB)

    Oudini, N. [Istituto di Metodologie Inorganiche e dei Plasmi, CNR, via Amendola 122/D, 70126 Bari (Italy); Laboratoire des plasma de décharges, Centre de Développement des Technologies Avancées, Cité du 20 Aout BP 17 Baba Hassen, 16081 Algiers (Algeria); Taccogna, F.; Minelli, P. [Istituto di Metodologie Inorganiche e dei Plasmi, CNR, via Amendola 122/D, 70126 Bari (Italy); Aanesland, A.; Raimbault, J.-L. [Laboratoire de Physique des Plasmas, École Polytechnique, 91128 Palaiseau Cedex (France)

    2013-10-15

    A two-dimensional particle-in-cell/Monte Carlo collision model has been developed and used to study low electronegative magnetized hydrogen plasma. A configuration characterized by four electrodes is used: the left electrode is biased at V{sub l} = −100 V, the right electrode is grounded, while the upper and lower transversal electrodes are biased at an intermediate voltage V{sub ud} between 0 and −100 V. A constant and homogeneous magnetic field is applied parallel to the lateral (left/right) electrodes. It is shown that in the magnetized case, the bulk plasma potential is close to the transversal electrodes bias inducing then a reversed sheath in front of the right electrode. The potential drop within the reversed sheath is controlled by the transversal electrodes bias allowing extraction of negative ions with a significant reduction of co-extracted electron current. Furthermore, introducing plasma electrodes, between the transversal electrodes and the right electrode, biased with a voltage just above the plasma bulk potential, increases the negative ion extracted current and decreases significantly the co-extracted electron current. The physical mechanism on basis of this phenomenon has been discussed.

  4. Partial pressure analysis of plasmas

    International Nuclear Information System (INIS)

    Dylla, H.F.

    1984-11-01

    The application of partial pressure analysis for plasma diagnostic measurements is reviewed. A comparison is made between the techniques of plasma flux analysis and partial pressure analysis for mass spectrometry of plasmas. Emphasis is given to the application of quadrupole mass spectrometers (QMS). The interface problems associated with the coupling of a QMS to a plasma device are discussed including: differential-pumping requirements, electromagnetic interferences from the plasma environment, the detection of surface-active species, ion source interactions, and calibration procedures. Example measurements are presented from process monitoring of glow discharge plasmas which are useful for cleaning and conditioning vacuum vessels

  5. Atmospheric-pressure plasma technology

    Science.gov (United States)

    Kogelschatz, U.

    2004-12-01

    Major industrial plasma processes operating close to atmospheric pressure are discussed. Applications of thermal plasmas include electric arc furnaces and plasma torches for generation of powders, for spraying refractory materials, for cutting and welding and for destruction of hazardous waste. Other applications include miniature circuit breakers and electrical discharge machining. Non-equilibrium cold plasmas at atmospheric pressure are obtained in corona discharges used in electrostatic precipitators and in dielectric-barrier discharges used for generation of ozone, for pollution control and for surface treatment. More recent applications include UV excimer lamps, mercury-free fluorescent lamps and flat plasma displays.

  6. Multifunctional bulk plasma source based on discharge with electron injection.

    Science.gov (United States)

    Klimov, A S; Medovnik, A V; Tyunkov, A V; Savkin, K P; Shandrikov, M V; Vizir, A V

    2013-01-01

    A bulk plasma source, based on a high-current dc glow discharge with electron injection, is described. Electron injection and some special design features of the plasma arc emitter provide a plasma source with very long periods between maintenance down-times and a long overall lifetime. The source uses a sectioned sputter-electrode array with six individual sputter targets, each of which can be independently biased. This discharge assembly configuration provides multifunctional operation, including plasma generation from different gases (argon, nitrogen, oxygen, acetylene) and deposition of composite metal nitride and oxide coatings.

  7. Atmospheric-pressure plasma jet

    Science.gov (United States)

    Selwyn, Gary S.

    1999-01-01

    Atmospheric-pressure plasma jet. A .gamma.-mode, resonant-cavity plasma discharge that can be operated at atmospheric pressure and near room temperature using 13.56 MHz rf power is described. Unlike plasma torches, the discharge produces a gas-phase effluent no hotter than 250.degree. C. at an applied power of about 300 W, and shows distinct non-thermal characteristics. In the simplest design, two concentric cylindrical electrodes are employed to generate a plasma in the annular region therebetween. A "jet" of long-lived metastable and reactive species that are capable of rapidly cleaning or etching metals and other materials is generated which extends up to 8 in. beyond the open end of the electrodes. Films and coatings may also be removed by these species. Arcing is prevented in the apparatus by using gas mixtures containing He, which limits ionization, by using high flow velocities, and by properly shaping the rf-powered electrode. Because of the atmospheric pressure operation, no ions survive for a sufficiently long distance beyond the active plasma discharge to bombard a workpiece, unlike low-pressure plasma sources and conventional plasma processing methods.

  8. Local and regular plasma oscillations in bulk donor type semiconductors

    OpenAIRE

    Kornyushin, Yuri

    2007-01-01

    Restoring force acts on the electronic cloud of the outer electrons of a neutral or charged impurity atom when it is shifted relative to the inner charged core. Because of this the dipole oscillation arises, which influences considerably the dispersion law of the plasma oscillation in bulk donor semiconductors. Assuming that only one transition of the outer electron from the ground state to the first excited state is essential, the dispersion law is calculated. It is shown that calculated dis...

  9. Bulk plasma properties in the pulsed glow discharge

    International Nuclear Information System (INIS)

    Jackson, Glen P.; King, Fred L.

    2003-01-01

    This work focuses on the spatial and temporal characteristics of a glow discharge plasma operated with power pulses of 5 ms in duration at 25% duty cycle. Interpretation of emission data provides insight into the nature of the plasma at each instant of a typical pulse cycle and at each position in space. Because the bulk plasma properties affect the distribution of excited energy levels of the sputtered atoms, an improved understanding of the plasma affords the ability to select conditions that enhance analytically important emission lines. Optical emission spectroscopy was used to determine the relative populations of excited states for atoms and ions during the initial breakdown, the steady state and the recombining periods of the discharge pulse cycle. The plasma is highly ionizing in nature at the time of breakdown--with lower excited states being overpopulated--before reaching the steady state, or plateau, period, also ionizing in nature. These behaviors arise from a loss of charged particles and photons to the surroundings that shifts the plasma away from Saha and Boltzmann balances during these periods. The post-pulse period typically displays recombining behavior, characterized by population inversion for selected species--except for regions close to the cathode, where electrons and ions are lost by diffusion and are not available for recombination. The sputtered analyte atom emissions closely mimic those of the plasma bath gas, except that their emissions persevere for longer in the recombining after-peak period than do the discharge gas species

  10. Bulk characterization of pharmaceutical powders by low-pressure compression

    DEFF Research Database (Denmark)

    Sørensen, A.H.; Sonnergaard, Jørn; Hovgaard, L.

    2005-01-01

    for characterization purposes. Significant correlation was demonstrated between several of the compression and tapping-derived parameters. The discriminative power of the low-pressure compression test was discussed using the compressed density at 0.2 MPa, correlated with the tapped density, and the relative Walker...... coefficient, correlated with the Compressibility Index, as examples. The compressed density at 0.2 MPa and the relative Walker coefficient demonstrated excellent discriminative power, superior to the discriminative power of the correlated tapping derived parameters. The low-pressure compression test......Low-pressure compression of pharmaceutical powders using small amounts of sample (50 mg) was evaluated as an alternative to traditional bulk powder characterization by tapping volumetry. Material parameters were extrapolated directly from the compression data and by fitting with the Walker...

  11. The Dawn of Atmospheric-pressure Plasma

    Science.gov (United States)

    Ono, Shigeru

    As never before, atmospheric-pressure plasma technology is poised to transform the world of plasma processing. Many corporate and academic researchers are betting that the future holds tremendous opportunity for atmospheric-pressure plasma, which offers low cost and sometimes surprisingly high performance. A recent example of research is presented.

  12. Atmospheric Pressure Plasma Process And Applications

    Energy Technology Data Exchange (ETDEWEB)

    Peter C. Kong; Myrtle

    2006-09-01

    This paper provides a general discussion of atmospheric-pressure plasma generation, processes, and applications. There are two distinct categories of atmospheric-pressure plasmas: thermal and nonthermal. Thermal atmospheric-pressure plasmas include those produced in high intensity arcs, plasma torches, or in high intensity, high frequency discharges. Although nonthermal plasmas are at room temperatures, they are extremely effective in producing activated species, e.g., free radicals and excited state atoms. Thus, both thermal and nonthermal atmosphericpressure plasmas are finding applications in a wide variety of industrial processes, e.g. waste destruction, material recovery, extractive metallurgy, powder synthesis, and energy conversion. A brief discussion of recent plasma technology research and development activities at the Idaho National Laboratory is included.

  13. Fabrication and properties of dense ex situ magnesium diboride bulk material synthesized using spark plasma sintering

    Energy Technology Data Exchange (ETDEWEB)

    Dancer, C E J; Todd, R I; Grovenor, C R M [Department of Materials, University of Oxford, Parks Road, Oxford OX1 3PH (United Kingdom); Prabhakaran, D [Department of Physics, Clarendon Laboratory, University of Oxford, Parks Road, Oxford OX1 3PU (United Kingdom); Basoglu, M; Yanmaz, E [Department of Physics, Faculty of Arts and Sciences, Karadeniz Technical University, 61080 Trabzon (Turkey); Yan, H; Reece, M, E-mail: claire.dancer@linacre.oxon.or [Department of Materials, Queen Mary, University of London, Mile End Road, London E1 4NS (United Kingdom)

    2009-09-15

    High density ex situ magnesium diboride bulks were synthesized from commercial MgB{sub 2} powder using spark plasma sintering under a range of applied uniaxial pressures between 16 and 80 MPa. The microstructure was characterized using x-ray diffraction, scanning electron microscopy, polarized optical microscopy, Vickers hardness measurements, and density measurements using the Archimedes method. By combining these data with those for other bulk samples we have developed a correlation curve for the hardness and density for magnesium diboride for relative densities of 60-100%. The superconducting properties were determined using magnetization measurements. Comparison to samples of significantly higher porosity indicates a positive correlation between magnetization critical current density and bulk density for magnesium diboride bulks up to around 90% density. Above this level other microstructural processes such as grain growth begin to influence the critical current density, suggesting that full elimination of porosity is not necessary to obtain high critical current density. We conclude that the best superconducting properties are likely to be obtained with a combination of small grain size and minimal porosity.

  14. High-pressure X-ray diffraction study of bulk- and nanocrystalline GaN

    DEFF Research Database (Denmark)

    Jorgensen, J.E.; Jakobsen, J.M.; Jiang, Jianzhong

    2003-01-01

    Bulk- and nanocrystalline GaN have been studied by high-pressure energy-dispersive X-ray diffraction. Pressure-induced structural phase transitions from the wurtzite to the NaCl phase were observed in both materials. The transition pressure was found to be 40 GPa for the bulk-crystalline GaN, whi...

  15. Seed disinfection effect of atmospheric pressure plasma and low pressure plasma on Rhizoctonia solani.

    Science.gov (United States)

    Nishioka, Terumi; Takai, Yuichiro; Kawaradani, Mitsuo; Okada, Kiyotsugu; Tanimoto, Hideo; Misawa, Tatsuya; Kusakari, Shinichi

    2014-01-01

    Gas plasma generated and applied under two different systems, atmospheric pressure plasma and low pressure plasma, was used to investigate the inactivation efficacy on the seedborne pathogenic fungus, Rhizoctonia solani, which had been artificially introduced to brassicaceous seeds. Treatment with atmospheric plasma for 10 min markedly reduced the R. solani survival rate from 100% to 3% but delayed seed germination. The low pressure plasma treatment reduced the fungal survival rate from 83% to 1.7% after 10 min and the inactivation effect was dependent on the treatment time. The seed germination rate after treatment with the low pressure plasma was not significantly different from that of untreated seeds. The air temperature around the seeds in the low pressure system was lower than that of the atmospheric system. These results suggested that gas plasma treatment under low pressure could be effective in disinfecting the seeds without damaging them.

  16. Quantum effects on propagation of bulk and surface waves in a thin quantum plasma film

    Energy Technology Data Exchange (ETDEWEB)

    Moradi, Afshin, E-mail: a.moradi@kut.ac.ir [Department of Engineering Physics, Kermanshah University of Technology, Kermanshah (Iran, Islamic Republic of); Department of Nano Sciences, Institute for Studies in Theoretical Physics and Mathematics (IPM), Tehran (Iran, Islamic Republic of)

    2015-06-19

    The propagation of bulk and surface plasma waves in a thin quantum plasma film is investigated, taking into account the quantum effects. The generalized bulk and surface plasma dispersion relation due to quantum effects is derived, using the quantum hydrodynamic dielectric function and applying appropriate additional boundary conditions. The quantum mechanical and film geometric effects on the bulk and surface modes are discussed. It is found that quantum effects become important for a thin film of small thickness. - Highlights: • New bulk and surface plasma dispersion relations due to quantum effects are derived, in a thin quantum plasma film. • It is found that quantum effects become important for a thin quantum film of small thickness.

  17. Cluster view of the plasma sheet boundary layer and bursty bulk flow connection

    Directory of Open Access Journals (Sweden)

    O. W. Lennartsson

    2009-04-01

    Full Text Available The high-latitude boundaries of the plasma sheet (PSBL are dynamic latitude zones of recurring and transient (minutes to tens of minutes earthward and magnetic field-aligned bursts of plasma, each being more or less confined in longitude as well, whose ionic component is dominated by protons with flux, energies and density that are consistent with a central plasma sheet (CPS source at varying distance (varying rates of energy time dispersion, sometimes as close as the ~19 RE Cluster apogees, or closer still. The arguably most plausible source consists of so called "bursty bulk flows" (BBFs, i.e. proton bulk flow events with large, positive and bursty GSE vx. Known mainly from CPS observations made at GSE x>−30 RE, the BBF type events probably take place much further downtail as well. What makes the BBFs an especially plausible source are (1 their earthward bulk flow, which helps explain the lack of distinctive latitudinal PSBL energy dispersion, and (2 their association with a transient strong increase of the local tail Bz component ("local dipolarization". The enhanced Bz provides intermittent access to higher latitudes for the CPS plasma, resulting in local density reductions in the tail midplane, as illustrated here by proton data from the Cluster CIS CODIF instruments. Another sign of kinship between the PSBL bursts and the BBFs is their similar spatial fine structure. The PSBL bursts have prominent filaments aligned along the magnetic field with transverse flux gradients that are often characterized by local ~10 keV proton gyroradii scale size (or even smaller, as evidenced by Cluster measurements. The same kind of fine structure is also found during Cluster near-apogee traversals of the tail midplane, as illustrated here and implied by recently published statistics on BBFs obtained with Cluster multipoint observations at varying satellite separations. Altogether, the Cluster observations described here mesh rather well with theories

  18. Large area atmospheric-pressure plasma jet

    Science.gov (United States)

    Selwyn, Gary S.; Henins, Ivars; Babayan, Steve E.; Hicks, Robert F.

    2001-01-01

    Large area atmospheric-pressure plasma jet. A plasma discharge that can be operated at atmospheric pressure and near room temperature using 13.56 MHz rf power is described. Unlike plasma torches, the discharge produces a gas-phase effluent no hotter than 250.degree. C. at an applied power of about 300 W, and shows distinct non-thermal characteristics. In the simplest design, two planar, parallel electrodes are employed to generate a plasma in the volume therebetween. A "jet" of long-lived metastable and reactive species that are capable of rapidly cleaning or etching metals and other materials is generated which extends up to 8 in. beyond the open end of the electrodes. Films and coatings may also be removed by these species. Arcing is prevented in the apparatus by using gas mixtures containing He, which limits ionization, by using high flow velocities, and by properly spacing the rf-powered electrode. Because of the atmospheric pressure operation, there is a negligible density of ions surviving for a sufficiently long distance beyond the active plasma discharge to bombard a workpiece, unlike the situation for low-pressure plasma sources and conventional plasma processing methods.

  19. Effects of pressure anisotropy on plasma transport

    International Nuclear Information System (INIS)

    Zawaideh, E.; Najmabadi, F.; Conn, R.W.

    1986-03-01

    In a recent paper a new set of generalized two-field equations is derived which describes plasma transport along the field lines of a space and time dependent magnetic field. These equations are valid for collisional to weakly collisional plasmas; they reduce to the conventional fluid equations of Braginskii for highly collisional plasmas. An important feature of these equations is that the anisotropy in the ion pressure is explicitly included. In this paper, these generalized transport equations are applied to a model problem of plasma flow through a magnetic mirror field. The profiles of the plasma parameters (density, flow speed, and pressures) are numerically calculated for plasma in different collisionality regimes. These profiles are explained by examining the competing terms in the transport equation. The pressure anisotropy is found to profoundly impact the plasma flow behavior. As a result, the new generalized equations predict flow behavior more accurately than the conventional transport equations. A large density and pressure drop is predicted as the flow passes through a magnetic mirror. Further, the new equations uniquely predict oscillations in the density profile, an effect missing in results from the conventional equations

  20. Diagnostics of atmospheric pressure air plasmas

    International Nuclear Information System (INIS)

    Laux, C.O.; Kruger, C.H.; Zare, R.N.

    2001-01-01

    Atmospheric pressure air plasmas are often thought to be in Local Thermodynamics Equilibrium (LTE) owing to fast interspecies collisional exchanges at high pressure. As will be seen here, this assumption cannot be relied upon, particularly with respect to optical diagnostics. Large velocity gradients in flowing plasmas and/or elevated electron temperatures created by electrical discharges can result in large departures from chemical and thermal equilibrium. Diagnostic techniques based on optical emission spectroscopy (OES) and Cavity Ring-Down Spectroscopy (CRDS) have been developed and applied at Stanford University to the investigation of atmospheric pressure plasmas under conditions ranging from thermal and chemical equilibrium to thermochemical nonequilibrium. This article presents a review of selected temperature and species concentration measurement techniques useful for the study of air and nitrogen plasmas

  1. Research on atmospheric pressure plasma processing sewage

    Science.gov (United States)

    Song, Gui-cai; Na, Yan-xiang; Dong, Xiao-long; Sun, Xiao-liang

    2013-08-01

    The water pollution has become more and more serious with the industrial progress and social development, so it become a worldwide leading environmental management problem to human survival and personal health, therefore, countries are looking for the best solution. Generally speaking, in this paper the work has the following main achievements and innovation: (1) Developed a new plasma device--Plasma Water Bed. (2) At atmospheric pressure condition, use oxygen, nitrogen, argon and helium as work gas respectively, use fiber spectrometer to atmospheric pressure plasma discharge the emission spectrum of measurement, due to the different work gas producing active particle is different, so can understand discharge, different particle activity, in the treatment of wastewater, has the different degradation effects. (3) Methyl violet solution treatment by plasma water bed. Using plasma drafting make active particles and waste leachate role, observe the decolorization, measurement of ammonia nitrogen removal.

  2. Simple microwave plasma source at atmospheric pressure

    International Nuclear Information System (INIS)

    Kim, Jeong H.; Hong, Yong C.; Kim, Hyoung S.; Uhm, Han S.

    2003-01-01

    We have developed a thermal plasma source operating without electrodes. One electrodeless torch is the microwave plasma-torch, which can produce plasmas in large quantities. We can generate plasma at an atmospheric pressure by marking use of the same magnetrons used as commercial microwave ovens. Most of the magnetrons are operated at the frequency of 2.45 GHz; the magnetron power microwave is about 1kW. Electromagnetic waves from the magnetrons propagate through a shorted waveguide. Plasma was generated under a resonant condition, by an auxiliary ignition system. The plasma is stabilized by vortex stabilization. Also, a high-power and high-efficiency microwave plasma-torch has been operated in air by combining two microwave plasma sources with 1kW, 2.45 GHz. They are arranged in series to generate a high-power plasma flame. The second torch adds all its power to the plasma flame of the first torch. Basically, electromagnetic waves in the waveguide were studied by a High Frequency Structure Simulator (HFSS) code and preliminary experiments were conducted

  3. Is the bulk mode conversion important in high density helicon plasma?

    International Nuclear Information System (INIS)

    Isayama, Shogo; Hada, Tohru; Shinohara, Shunjiro; Tanikawa, Takao

    2016-01-01

    In a high-density helicon plasma production process, a contribution of Trivelpiece-Gould (TG) wave for surface power deposition is widely accepted. The TG wave can be excited either due to an abrupt density gradient near the plasma edge (surface conversion) or due to linear mode conversion from the helicon wave in a density gradient in the bulk region (bulk mode conversion). By numerically solving the boundary value problem of linear coupling between the helicon and the TG waves in a background with density gradient, we show that the efficiency of the bulk mode conversion strongly depends on the dissipation included in the plasma, and the bulk mode conversion is important when the dissipation is small. Also, by performing FDTD simulation, we show the time evolution of energy flux associated with the helicon and the TG waves.

  4. Plasma Clouds and Snowplows: Bulk Plasma Escape from Mars Observed by MAVEN

    Science.gov (United States)

    Halekas, J. S.; Brain, D. A.; Ruhunusiri, S.; McFadden, J. P.; Mitchell, D. L.; Mazelle, C.; Connerney, J. E. P.; Harada, Y.; Hara, T.; Espley, J. R.; hide

    2016-01-01

    We present initial Mars Atmosphere and Volatile EvolutioN (MAVEN) observations and preliminary interpretation of bulk plasma loss from Mars. MAVEN particle and field measurements show that planetary heavy ions derived from the Martian atmosphere can escape in the form of discrete coherent structures or "clouds." The ions in these clouds are unmagnetized or weakly magnetized, have velocities well above the escape speed, and lie directly downstream from magnetic field amplifications, suggesting a "snowplow" effect. This postulated escape process, similar to that successfully used to explain the dynamics of active gas releases in the solar wind and terrestrial magnetosheath, relies on momentum transfer from the shocked solar wind protons to the planetary heavy ions, with the electrons and magnetic field acting as intermediaries. Fluxes of planetary ions on the order of 10(exp 7)/sq cm/s can escape by this process, and if it operates regularly, it could contribute 10-20% of the current ion escape from Mars.

  5. High-pressure X-ray diffraction study of bulk- and nanocrystalline GaN

    DEFF Research Database (Denmark)

    Jorgensen, J.E.; Jakobsen, J.M.; Jiang, Jianzhong

    2003-01-01

    Bulk- and nanocrystalline GaN have been studied by high-pressure energy-dispersive X-ray diffraction. Pressure-induced structural phase transitions from the wurtzite to the NaCl phase were observed in both materials. The transition pressure was found to be 40 GPa for the bulk-crystalline GaN, while...... the wurtzite phase was retained up to 60 GPa in the case of nanocrystalline GaN. The bulk moduli for the wurtzite phases were determined to be 187 ( 7) and 319 ( 10) GPa for the bulk- and nanocrystalline phases, respectively, while the respective NaCl phases were found to have very similar bulk moduli [ 208...... ( 28) and 206 ( 44) GPa]....

  6. Bulk plasma rotation in the presence of waves in the ion cyclotron range of frequencies

    International Nuclear Information System (INIS)

    Eriksson, L.G.; Noterdaeme, J.M.; Kirov, K.

    2003-01-01

    Experiments with directed ICRF waves have for the first time in JET demonstrated the influence of absorbed wave momentum on bulk plasma rotation. Resonating fast ions acted as an intermediary in this process, and the experiments therefore provided evidence for the effect of fast ions on the plasma rotation. Results from these experiments are reviewed together with results from ICRF heated plasmas with symmetric spectra in JET and Tore Supra. The relevance of different theoretical models is briefly considered. (author)

  7. Effect of plasma colloid osmotic pressure on intraocular pressure during haemodialysis

    OpenAIRE

    Tokuyama, T.; Ikeda, T.; Sato, K.

    1998-01-01

    BACKGROUND—In a previous case report, it was shown that an increase in plasma colloid osmotic pressure induced by the removal of fluid during haemodialysis was instrumental in decreasing intraocular pressure. The relation between changes in intraocular pressure, plasma osmolarity, plasma colloid osmotic pressure, and body weight before and after haemodialysis is evaluated.
METHODS—Intraocular pressure, plasma osmolarity, plasma colloid osmotic pressure, and body weight were evaluated before a...

  8. Superhard MgB sub 2 bulk material prepared by high-pressure sintering

    CERN Document Server

    Ma, H A; Chen, L X; Zhu, P W; Ren, G Z; Guo, W L; Fu, X Q; Zou Guang Tian; Ren, Z A; Che, G C; Zhao, Z X

    2002-01-01

    Superhard MgB sub 2 bulk material with a golden metallic shine was synthesized by high-pressure sintering for 8 h at 5.5 GPa and different temperatures. Appropriate pressure and temperature conditions for synthesizing polycrystalline MgB sub 2 with high hardness were investigated. The samples were characterized by means of atomic force microscopy and x-ray diffraction. The Vickers hardness, bulk density, and electrical resistivity were measured at room temperature.

  9. Diagnostics on an atmospheric pressure plasma jet

    International Nuclear Information System (INIS)

    Niemi, K; Reuter, St; Schaper, L; Knake, N; Gathen, V Schulz-von der; Gans, T

    2007-01-01

    The atmospheric pressure plasma jet (APPJ) is a homogeneous non-equilibrium discharge at ambient pressure. It operates with a noble base gas and a percentage-volume admixture of a molecular gas. Applications of the discharge are mainly based on reactive species in the effluent. The effluent region of a discharge operated in helium with an oxygen admixture has been investigated. The optical emission from atomic oxygen decreases with distance from the discharge but can still be observed several centimetres in the effluent. Ground state atomic oxygen, measured using absolutely calibrated two-photon laser induced fluorescence spectroscopy, shows a similar behaviour. Detailed understanding of energy transport mechanisms requires investigations of the discharge volume and the effluent region. An atmospheric pressure plasma jet has been designed providing excellent diagnostics access and a simple geometry ideally suited for modelling and simulation. Laser spectroscopy and optical emission spectroscopy can be applied in the discharge volume and the effluent region

  10. Enhanced bulk modulus and reduced transition pressure in gamma-Fe2O3 nanocrystals

    DEFF Research Database (Denmark)

    Jiang, Jianzhong; Olsen, J. Staun; Gerward, Leif

    1998-01-01

    GPa for the bulk material to 305 GPa for 9 nm size crystals. At the same time the transition pressure decreases from 35 to 27 GPa. The reduced transition pressure is explained in terms of nucleation and growth, the larger volume change upon transition in the nanocrystalline material being the main...

  11. Atmospheric Pressure Plasma Processing for Polymer Adhesion: A Review

    DEFF Research Database (Denmark)

    Kusano, Yukihiro

    2014-01-01

    Atmospheric pressure plasma processing has attracted significant interests over decades due to its usefulness and a variety of applications. Adhesion improvement of polymer surfaces is among the most important applications of atmospheric pressure plasma treatment. Reflecting recent significant...... development of the atmospheric pressure plasma processing, this work presents its fundamental aspects, applications, and characterization techniques relevant to adhesion....

  12. Atmospheric pressure microwave plasma system with ring waveguide

    International Nuclear Information System (INIS)

    Liu Liang; Zhang Guixin; Zhu Zhijie; Luo Chengmu

    2007-01-01

    Some scientists used waveguide as the cavity to produce a plasma jet, while large volume microwave plasma was relatively hard to get in atmospheric pressure. However, a few research institutes have already developed devices to generate large volume of atmospheric pressure microwave plasma, such as CYRANNUS and SLAN series, which can be widely applied. In this paper, present a microwave plasma system with ring waveguide to excite large volume of atmospheric pressure microwave plasma, plot curves on theoretical disruption electric field of some working gases, emulate the cavity through software, measure the power density to validate and show the appearance of microwave plasma. At present, large volume of argon and helium plasma have already been generated steadily by atmospheric pressure microwave plasma system. This research can build a theoretical basis of microwave plasma excitation under atmospheric pressure and will be useful in study of the device. (authors)

  13. MicroScale - Atmospheric Pressure Plasmas

    Energy Technology Data Exchange (ETDEWEB)

    Sankaran, Mohan [Case Western Reserve University

    2012-01-25

    Low-temperature plasmas play an essential role in the manufacturing of integrated circuits which are ubiquitous in modern society. In recent years, these top-down approaches to materials processing have reached a physical limit. As a result, alternative approaches to materials processing are being developed that will allow the fabrication of nanoscale materials from the bottom up. The aim of our research is to develop a new class of plasmas, termed “microplasmas” for nanomaterials synthesis. Microplasmas are a special class of plasmas formed in geometries where at least one dimension is less than 1 mm. Plasma confinement leads to several unique properties including high-pressure stability and non-equilibrium that make microplasams suitable for nanomaterials synthesis. Vapor-phase precursors can be dissociated to homogeneously nucleate nanometer-sized metal and alloyed nanoparticles. Alternatively, metal salts dispersed in liquids or polymer films can be electrochemically reduced to form metal nanoparticles. In this talk, I will discuss these topics in detail, highlighting the advantages of microplasma-based systems for the synthesis of well-defined nanomaterials.

  14. Structure and property evaluation of a vacuum plasma sprayed nanostructured tungsten-hafnium carbide bulk composite

    International Nuclear Information System (INIS)

    Rea, K.E.; Viswanathan, V.; Kruize, A.; Hosson, J.Th.M. de; O'Dell, S.; McKechnie, T.; Rajagopalan, S.; Vaidyanathan, R.; Seal, S.

    2008-01-01

    Vacuum plasma spray (VPS) forming of tungsten-based metal matrix nanocomposites (MMCs) has shown to be a cost effective and time saving method for the formation of bulk monolithic nanostructured thermo-mechanical components. Spray drying of powder feedstock appears to have a significant effect on the improved mechanical properties of the bulk nanocomposite. The reported elastic modulus of the nanocomposite nearly doubles due to the presence of HfC nano particulates in the W matrix. High resolution transmission electron microscopy (HRTEM) revealed the retention of nanostructures at the select process conditions and is correlated with the enhanced mechanical properties of the nanocomposite

  15. Ratio of bulk to shear viscosity in a quasigluon plasma: from weak to strong coupling

    CERN Document Server

    Bluhm, M; Redlich, K

    2012-01-01

    The ratio of bulk to shear viscosity is expected to exhibit a different behaviour in weakly and in strongly coupled systems. This can be expressed by the dependence of the ratio on the squared sound velocity. In the high temperature QCD plasma at small running coupling, the viscosity ratio is uniquely determined by a quadratic dependence on the conformality measure, whereas in certain strongly coupled and nearly conformal theories this dependence is linear. Employing an effective kinetic theory of quasiparticle excitations with medium-modified dispersion relation, we analyze the ratio of bulk to shear viscosity of the gluon plasma. We show that in this approach the viscosity ratio comprises both dependencies found by means of weak coupling perturbative and strong coupling holographic techniques.

  16. Growth of Rayleigh-Taylor and bulk convective instabilities in dynamics of plasma liners and pinches

    International Nuclear Information System (INIS)

    Bud'ko, A.B.; Velikovich, A.L.; Liberman, M.A.; Felber, F.S.

    1989-01-01

    Perturbation growth is studied for the initial, linear stage of an instability development in the course of a cylindrically-symmetric compression and expansion of plasma liners and Z-pinches with a sharp boundary. The hydrodynamic instabilities are Rayleigh-Taylor and bulk convective ones, the former being the most dengerous. Classification of the instability modes developing in accelerated plasmas, inclusing the local and global Rayleigh-Taylor modes, is given. The spectra of the instability growth rates are calculated for plasma liners and Z-pinches. The properties of the spectra appear to explain the filamentation and stratification of plasmas observed in the experiments with liners and Z-pinches. An axial magnetic field is shown to create a window of stability in the space of the flow parameters, where th Rayleigh-Taylor modes are fully suppressed by the magnetic shear, and the bulk convective ones - to a considerable extent. The axial magnetic field required to stabilize the implosion of a liner is estimated as B z0 =(10-30 kG)I(MA)/R 0 (cm), where I is the average current, R 0 - the initial radius of the liner

  17. Fluoropolymer coated alanine films treated by atmospheric pressure plasmas − In comparison with gamma irradiation

    DEFF Research Database (Denmark)

    Kusano, Yukihiro; Bardenshtein, Alexander; Morgen, Per

    2018-01-01

    Fluoropolymer coated alanine films are treated by a dielectric barrier discharge and a gliding arc at atmospheric pressure as well as with gamma irradiation. The film surfaces and the underlying bulk materials are characterized before and after each treatment. The fluorine content decreases...... and the oxygen content increases at the fluoropolymer surfaces, while deposition of specific plasma energies in the alanine films is detected by electron paramagnetic resonance spectroscopy, indicating that not only the fluoropolymer surfaces but also the bulk alanine materials are modified. Differences...

  18. Perspectives on atmospheric-pressure plasmas for nanofabrication

    International Nuclear Information System (INIS)

    Mariotti, Davide; Sankaran, R Mohan

    2011-01-01

    Low-pressure, low-temperature plasmas are widely used for materials applications in industries ranging from electronics to medicine. To avoid the high costs associated with vacuum equipment, there has always been a strong motivation to operate plasmas at higher pressures, up to atmospheric. However, high-pressure operation of plasmas often leads to instabilities and gas heating, conditions that are unsuitable for materials applications. The recent development of microscale plasmas (i.e. microplasmas) has helped realize the sustainment of stable, non-thermal plasmas at atmospheric pressure and enable low-cost materials applications. There has also been an unexpected benefit of atmospheric-pressure operation: the potential to fabricate nanoscale materials which is not possible by more conventional, low-pressure plasmas. For example, in a high-pressure environment, nanoparticles can be nucleated in the gas phase from vapour (or solid metal) precursors. Alternatively, non-thermal, atmospheric-pressure plasmas can be coupled with liquids such as water or ethanol to nucleate and modify solution-phase nanoparticles. In this perspective paper, we review some of these recent efforts and provide an outlook for the rapidly emerging field of atmospheric-pressure plasmas for nanofabrication.

  19. Formation and properties of two-phase bulk metallic glasses by spark plasma sintering

    Energy Technology Data Exchange (ETDEWEB)

    Xie Guoqiang, E-mail: xiegq@imr.tohoku.ac.jp [Institute for Materials Research, Tohoku University, 2-1-1 Katahira, Aoba-ku, Sendai 980-8577 (Japan); Louzguine-Luzgin, D.V. [WPI Advanced Institute for Materials Research, Tohoku University, Sendai 980-8577 (Japan); Inoue, Akihisa [Institute for Materials Research, Tohoku University, 2-1-1 Katahira, Aoba-ku, Sendai 980-8577 (Japan); WPI Advanced Institute for Materials Research, Tohoku University, Sendai 980-8577 (Japan)

    2011-06-15

    Research highlights: > Two-phase bulk metallic glasses with high strength and good soft magnetic properties as well as satisfying large-size requirements were produced by spark plasma sintering. > Effects of sintering temperature on thermal stability, microstructure, mechanical and magnetic properties were investigated. > Densified samples were obtained by the spark plasma sintering at above 773 K. - Abstract: Using a mixture of the gas-atomized Ni{sub 52.5}Nb{sub 10}Zr{sub 15}Ti{sub 15}Pt{sub 7.5} and Fe{sub 73}Si{sub 7}B{sub 17}Nb{sub 3} glassy alloy powders, we produced the two-phase bulk metallic glass (BMG) with high strength and good soft magnetic properties as well as satisfying large-size requirements by the spark plasma sintering (SPS) process. Two kinds of glassy particulates were homogeneously dispersed each other. With an increase in sintering temperature, density of the produced samples increased, and densified samples were obtained by the SPS process at above 773 K. Good bonding state among the Ni- and Fe-based glassy particulates was achieved.

  20. Properties of microwave plasma torch operating at a low pressure

    International Nuclear Information System (INIS)

    Cho, Soon C.; Uhm, Han S.; Hong, Yong C.; Kim, Jae H.

    2008-01-01

    A microwave plasma torch system is attached to a low-pressure chamber in this study. The electric field induced in a quartz discharge tube by microwave radiation breaks down the gas at a sufficiently low pressure, igniting the plasma, which is continuously sustained by the microwave radiation. The plasma profile at a very low pressure is shown to be asymmetric with higher density on the incoming side of the microwaves. The gas temperature at the bright spot of the torch plasma measured via the optical emission from hydroxide radicals is shown to increase drastically upon high-pressure operation as the microwave power increases. The electron density at the torch flame is measured by recording the Stark broadening of the hydrogen Balmer beta line. The plasma density increases as the microwave power increases. The typical argon plasma density of a plasma torch powered at 500 W under a pressure of 150 Torr is on the order of 10 14 /cm 3 . The electron temperature in the argon torch plasma was estimated to be 1.5 eV, thereby effectively exciting the molecules in the torch gas. Disintegration of nitrogen fluoride (NF 3 ) indicates that a microwave plasma torch operating at a low pressure can efficiently generate an abundant amount of chemical radicals.

  1. Biomedical applications and diagnostics of atmospheric pressure plasma

    International Nuclear Information System (INIS)

    Petrović, Z Lj; Puac, N; Lazović, S; Maletić, D; Spasić, K; Malović, G

    2012-01-01

    Numerous applications of non-equilibrium (cold, low temperature) plasmas require those plasmas to operate at atmospheric pressure. Achieving non-equilibrium at atmospheric pressure is difficult since the ionization growth is very fast at such a high pressure. High degree of ionization on the other hand enables transfer of energy between electrons and ions and further heating of the background neutral gas through collisions between ions and neutrals. Thus, all schemes to produce non-equilibrium plasmas revolve around some form of control of ionization growth. Diagnostics of atmospheric pressure plasmas is difficult and some of the techniques cannot be employed at all. The difficulties stem mostly from the small size. Optical emission spectroscopy and laser absorption spectroscopy require very high resolution in order to resolve the anatomy of the discharges. Mass analysis is not normally applicable for atmospheric pressure plasmas, but recently systems with triple differential pumping have been developed that allow analysis of plasma chemistry at atmospheric pressures which is essential for numerous applications. Application of such systems is, however, not free from problems. Applications in biomedicine require minimum heating of the ambient air. The gas temperature should not exceed 40 degrees C to avoid thermal damage to the living tissues. Thus, plasmas should operate at very low powers and power control is essential. We developed unique derivative probes that allow control of power well below 1 W and studied four different sources, including dielectric barrier discharges, plasma needle, atmospheric pressure jet and micro atmospheric pressure jet. The jet operates in plasma bullet regime if proper conditions are met. Finally, we cover results on treatment of bacteria and human cells as well as treatment of plants by plasmas. Localized delivery of active species by plasmas may lead to a number of medical procedures that may also involve removal of bacteria, fungi

  2. Direct depth distribution measurement of deuterium in bulk tungsten exposed to high-flux plasma

    Directory of Open Access Journals (Sweden)

    C. N. Taylor

    2017-05-01

    Full Text Available Understanding tritium retention and permeation in plasma-facing components is critical for fusion safety and fuel cycle control. Glow discharge optical emission spectroscopy (GD-OES is shown to be an effective tool to reveal the depth profile of deuterium in tungsten. Results confirm the detection of deuterium. A ∼46 μm depth profile revealed that the deuterium content decreased precipitously in the first 7 μm, and detectable amounts were observed to depths in excess of 20 μm. The large probing depth of GD-OES (up to 100s of μm enables studies not previously accessible to the more conventional techniques for investigating deuterium retention. Of particular applicability is the use of GD-OES to measure the depth profile for experiments where high deuterium concentration in the bulk material is expected: deuterium retention in neutron irradiated materials, and ultra-high deuterium fluences in burning plasma environment.

  3. Surface cleaning of metal wire by atmospheric pressure plasma

    International Nuclear Information System (INIS)

    Nakamura, T.; Buttapeng, C.; Furuya, S.; Harada, N.

    2009-01-01

    In this study, the possible application of atmospheric pressure dielectric barrier discharge plasma for the annealing of metallic wire is examined and presented. The main purpose of the current study is to examine the surface cleaning effect for a cylindrical object by atmospheric pressure plasma. The experimental setup consists of a gas tank, plasma reactor, and power supply with control panel. The gas assists in the generation of plasma. Copper wire was used as an experimental cylindrical object. This copper wire was irradiated with the plasma, and the cleaning effect was confirmed. The result showed that it is possible to remove the tarnish which exists on the copper wire surface. The experiment reveals that atmospheric pressure plasma is usable for the surface cleaning of metal wire. However, it is necessary to examine the method for preventing oxidization of the copper wire.

  4. Decomposition of Chemical Chain Molecules with Atmospheric Pressure Plasma

    Science.gov (United States)

    Tansli, Murat; Tasal, Erol

    2016-10-01

    Chemical chain molecules' decomposition is an interesting subject area for the atmospheric pressure plasma applications. The effects of the atmospheric pressure argon plasma on 4-((2-methoxyphenyl)Diazenyl)Benzene-1,3,-Diol molecule at room temperature are investigated. This molecule is one of the industrial dye molecules used widely. When considering the ecological life, this molecule will be very harmful and danger. We suggest a different, easy and useful decomposing method for such molecules. Atmospheric pressure plasma jet was principally treated for this decomposing of the molecule. Fourier transform infrared spectrometry (FT-IR) was used to characterization of the molecule after the plasma application to molecule in liquid phase with ethanol and methanol solvents. The atmospheric-pressure plasma jet of argon (Ar) as non-equilibrium has been formed by ac-power generator with frequency - 24 kHz and voltage - 12 kV. Characterizations for solutions prepared with ethanol and methanol solvents of molecule have been examined after applying (duration: 3 minutes) the atmospheric pressure plasma jet. The molecule was broken at 6C-7N =8N-9C stretching peak after the plasma treatment. The new plasma photo-products for ethanol and methanol solutions were produced as 6C-7N-8N =9C (strong, varying) and 12C =17O (strong, wide) stretching peaks.

  5. Modeling of low pressure plasma sources for microelectronics fabrication

    Science.gov (United States)

    Agarwal, Ankur; Bera, Kallol; Kenney, Jason; Likhanskii, Alexandre; Rauf, Shahid

    2017-10-01

    Chemically reactive plasmas operating in the 1 mTorr-10 Torr pressure range are widely used for thin film processing in the semiconductor industry. Plasma modeling has come to play an important role in the design of these plasma processing systems. A number of 3-dimensional (3D) fluid and hybrid plasma modeling examples are used to illustrate the role of computational investigations in design of plasma processing hardware for applications such as ion implantation, deposition, and etching. A model for a rectangular inductively coupled plasma (ICP) source is described, which is employed as an ion source for ion implantation. It is shown that gas pressure strongly influences ion flux uniformity, which is determined by the balance between the location of plasma production and diffusion. The effect of chamber dimensions on plasma uniformity in a rectangular capacitively coupled plasma (CCP) is examined using an electromagnetic plasma model. Due to high pressure and small gap in this system, plasma uniformity is found to be primarily determined by the electric field profile in the sheath/pre-sheath region. A 3D model is utilized to investigate the confinement properties of a mesh in a cylindrical CCP. Results highlight the role of hole topology and size on the formation of localized hot-spots. A 3D electromagnetic plasma model for a cylindrical ICP is used to study inductive versus capacitive power coupling and how placement of ground return wires influences it. Finally, a 3D hybrid plasma model for an electron beam generated magnetized plasma is used to understand the role of reactor geometry on plasma uniformity in the presence of E  ×  B drift.

  6. EFFECT OF LASER LIGHT ON LASER PLASMAS: Laser plasma at low air pressure

    Science.gov (United States)

    Vas'kovskiĭ, Yu M.; Moiseev, V. N.; Rovinskiĭ, R. E.; Tsenina, I. S.

    1993-01-01

    The dynamic and optical characteristics of the laser plasma produced during the application of a CO2 laser pulse to a target have been studied as a function of the ambient air pressure. The changes in the surface roughness of the sample after bombardment were studied as a function of the air pressure. It is concluded from the results that a transition from an air plasma to an erosion plasma occurs at a residual air pressure on the order of 1 torr. The experiment data support the existing picture of the process by which a plasma is produced near the surface of a target in air by laser pulses.

  7. Ultrasound enhanced plasma surface modification at atmospheric pressure

    DEFF Research Database (Denmark)

    Kusano, Yukihiro; Singh, Shailendra Vikram; Norrman, Kion

    2012-01-01

    Efficiency of atmospheric pressure plasma treatment can be highly enhanced by simultaneous high power ultrasonic irradiation onto the treating surface. It is because ultrasonic waves with a sound pressure level (SPL) above ∼140 dB can reduce the thickness of a boundary gas layer between the plasma...... arc at atmospheric pressure to study adhesion improvement. The effect of ultrasonic irradiation with the frequency diapason between 20 and 40 kHz at the SPL of ∼150 dB was investigated. After the plasma treatment without ultrasonic irradiation, the wettability was significantly improved....... The ultrasonic irradiation during the plasma treatment consistently enhanced the treatment efficiency. The principal effect of ultrasonic irradiation can be attributed to enhancing surface oxidation during plasma treatment. In addition, ultrasonic irradiation can suppress arcing, and the uniformity...

  8. Low-temperature atmospheric-pressure plasma sources for plasma medicine.

    Science.gov (United States)

    Setsuhara, Yuichi

    2016-09-01

    In this review paper, fundamental overviews of low-temperature atmospheric-pressure plasma generation are provided and various sources for plasma medicine are described in terms of operating conditions and plasma properties. Copyright © 2016 Elsevier Inc. All rights reserved.

  9. Non-equilbrium behavior of low-pressure plasma jets

    International Nuclear Information System (INIS)

    Chang, C.H.; Pfender, E.

    1989-01-01

    After establishing the basic equations, some sample calculations are presented to examine the thermodynamic state of the plasma from atmospheric to low pressures (80 mbar). These results indicate the validity of local thermodynamic equilibrium (LTE) at atmospheric pressure as well as strong deviations from LTE at lower pressures especially in terms of chemical equilibrium. Departures from kinetic equilibrium are not as severe as those from chemical equilibrium along the centerline of the jet. However, there are some departures from transitional equilibrium in the fringes of the jet. It is demonstrated that conventional methods based on the LTE assumption are not appropriate for describing low-pressure plasma jets

  10. Interaction of EM Waves with Atmospheric Pressure Plasmas

    National Research Council Canada - National Science Library

    Laroussi, Mounir

    2000-01-01

    .... The focus of the main activities is the generation of large volume, non-thermal, atmospheric pressure plasmas, their diagnostics, and their interactions with EM waves and with the cells of microorganism...

  11. Non-Thermal Sanitation By Atmospheric Pressure Plasma, Phase II

    Data.gov (United States)

    National Aeronautics and Space Administration — ORBITEC's Non-Thermal Sanitation by Atmospheric Pressure Plasma technology sanitizes fresh fruits and vegetables without the use of consumable chemicals and without...

  12. Non-Thermal Sanitation By Atmospheric Pressure Plasma, Phase I

    Data.gov (United States)

    National Aeronautics and Space Administration — ORBITEC proposes to develop a non-thermal technology based on atmospheric-pressure (AP) cold plasma to sanitize foods, food packaging materials, and other hardware...

  13. dc-Hydrogen plasma induced defects in bulk n-Ge

    Energy Technology Data Exchange (ETDEWEB)

    Nyamhere, C., E-mail: cloud.nyamhere@nmmu.ac.za [Department of Physics, Nelson Mandela Metropolitan University, PO Box 77000, Port Elizabeth 6031 (South Africa); Venter, A.; Murape, D.M. [Department of Physics, Nelson Mandela Metropolitan University, PO Box 77000, Port Elizabeth 6031 (South Africa); Auret, F.D.; Coelho, S.M.M. [Department of Physics, University of the Pretoria, Lynnwood Road, Pretoria 0002 (South Africa); Botha, J.R. [Department of Physics, Nelson Mandela Metropolitan University, PO Box 77000, Port Elizabeth 6031 (South Africa)

    2012-08-01

    Bulk antimony doped germanium (n-Ge) has been exposed to a dc-hydrogen plasma. Capacitance-voltage depth profiles revealed extensive near surface passivation of the shallow donors as evidenced by {approx}a 1.5 orders of magnitude reduction in the free carrier concentration up to depth of {approx}3.2 {mu}m. DLTS and Laplace-DLTS revealed a prominent electron trap 0.30 eV below the conduction (E{sub C} -0.30 eV). The concentration of this trap increased with plasma exposure time. The depth profile for this defect suggested a uniform distribution up to 1.2 {mu}m. Annealing studies show that this trap, attributed to a hydrogen-related complex, is stable up to 200 Degree-Sign C. Hole traps, or vacancy-antimony centers, common in this material after high energy particle irradiation, were not observed after plasma exposure, an indication that this process does not create Frenkel (V-I) pairs.

  14. Nanodiamonds in dusty low-pressure plasmas

    International Nuclear Information System (INIS)

    Vandenbulcke, L.; Gries, T.; Rouzaud, J. N.

    2009-01-01

    Dusty plasmas composed of carbon, hydrogen, and oxygen have been evidenced by optical emission spectroscopy and microwave interferometry, due to the increase in electron energy and the decrease in electron density. These plasmas allow homogeneous synthesis of nanodiamond grains composed of either pure diamond nanocrystals only (2-10 nm in size) or of diamond nanocrystals and some sp 2 -hybridized carbon entities. The control of their size and their microstructure could open ways for a wide range of fields. Their formation from a plasma-activated gaseous phase is also attractive because the formation of nanodiamonds in the universe is still a matter of controversy

  15. Ultrasound enhanced plasma surface modification at atmospheric pressure

    DEFF Research Database (Denmark)

    Kusano, Yukihiro; Singh, Shailendra Vikram; Norrman, Kion

    irradiation, the water contact angle dropped markedly, and tended to decrease furthermore at higher power. The ultrasonic irradiation during the plasma treatment consistently improved the wettability. Oxygen containing polar functional groups were introduced at the surface by the plasma treatment......Atmospheric pressure plasma treatment can be highly enhanced by simultaneous high-power ultrasonic irradiation onto the treating surface. It is because ultrasonic waves with a sound pressure level (SPL) above approximately 140 dB can reduce the thickness of a boundary gas layer between the plasma...... are separated using a polyethylene film. The gliding arc was extended by a high speed air flow into ambient air, directed the polyester surface at an angle of approximately 30o. The ultrasonic waves were introduced vertically to the surface. After the plasma treatment using each plasma source without ultrasonic...

  16. Low Temperature Atmospheric Pressure Plasma Sterilization Shower

    Data.gov (United States)

    National Aeronautics and Space Administration — The goal is to develop an atmospheric plasma jet that is capable of depositing a wide variety of materials on flexible substrates such as paper, plastic, cotton and...

  17. Spacecraft Sterilization Using Non-Equilibrium Atmospheric Pressure Plasma

    Science.gov (United States)

    Cooper, Moogega; Vaze, Nachiket; Anderson, Shawn; Fridman, Gregory; Vasilets, Victor N.; Gutsol, Alexander; Tsapin, Alexander; Fridman, Alexander

    2007-01-01

    As a solution to chemically and thermally destructive sterilization methods currently used for spacecraft, non-equilibrium atmospheric pressure plasmas are used to treat surfaces inoculated with Bacillus subtilis and Deinococcus radiodurans. Evidence of significant morphological changes and reduction in viability due to plasma exposure will be presented, including a 4-log reduction of B. subtilis after 2 minutes of dielectric barrier discharge treatment.

  18. Charge dependence of the plasma travel length in atmospheric-pressure plasma

    Energy Technology Data Exchange (ETDEWEB)

    Yambe, Kiyoyuki; Konda, Kohmei; Masuda, Seiya [Graduate School of Science and Technology, Niigata University, Niigata 950-2181 (Japan)

    2016-06-15

    Plasma plume is generated using a quartz tube, helium gas, and foil electrode by applying AC high voltage under the atmosphere. The plasma plume is released into the atmosphere from inside of the quartz tube and is seen as the continuous movement of the plasma bullet. The travel length of plasma bullet is defined from plasma energy and force due to electric field. The drift velocity of plasma bullet has the upper limit under atmospheric-pressure because the drift velocity is determined from the balance between electric field and resistive force due to collisions between plasma and air. The plasma plume charge depends on the drift velocity. Consequently, in the laminar flow of helium gas flow state, the travel length of the plasma plume logarithmically depends on the plasma plume charge which changes with both the electric field and the resistive force.

  19. Charge dependence of the plasma travel length in atmospheric-pressure plasma

    International Nuclear Information System (INIS)

    Yambe, Kiyoyuki; Konda, Kohmei; Masuda, Seiya

    2016-01-01

    Plasma plume is generated using a quartz tube, helium gas, and foil electrode by applying AC high voltage under the atmosphere. The plasma plume is released into the atmosphere from inside of the quartz tube and is seen as the continuous movement of the plasma bullet. The travel length of plasma bullet is defined from plasma energy and force due to electric field. The drift velocity of plasma bullet has the upper limit under atmospheric-pressure because the drift velocity is determined from the balance between electric field and resistive force due to collisions between plasma and air. The plasma plume charge depends on the drift velocity. Consequently, in the laminar flow of helium gas flow state, the travel length of the plasma plume logarithmically depends on the plasma plume charge which changes with both the electric field and the resistive force.

  20. Pressure-Dependent Electronic and Transport Properties of Bulk Platinum Oxide by Density Functional Theory

    Science.gov (United States)

    Kansara, Shivam; Gupta, Sanjeev K.; Sonvane, Yogesh; Nekrasov, Kirill A.; Kichigina, Natalia V.

    2018-02-01

    The structural, electronic, and vibrational properties of bulk platinum oxide (PtO) at compressive pressures in the interval from 0 GPa to 35 GPa are investigated using the density functional theory. The calculated electronic band structure of PtO shows poor metallicity at very low density of states on the Fermi level. However, the hybrid pseudopotential calculation yielded 0.78 eV and 1.30 eV direct band and indirect gap, respectively. Importantly, our results predict that PtO has a direct band gap within the framework of HSE06, and it prefers equally zero magnetic order at different pressures. In the Raman spectra, peaks are slightly shifted towards higher frequency with the decrease in pressure. We have also calculated the thermoelectric properties, namely the electronic thermal conductivity and electrical conductivity, with respect to temperature and thermodynamic properties such as entropy, specific heat at constant volume, enthalpy and Gibbs free energy with respect to pressure. The result shows that PtO is a promising candidate for use as a catalyst, in sensors, as a photo-cathode in water electrolysis, for thermal decomposition of inorganic salt and fuel cells.

  1. Atmospheric pressure H20 plasma treatment of polyester cord threads

    International Nuclear Information System (INIS)

    Simor, M.; Krump, H.; Hudec, I.; Rahel, J.; Brablec, A.; Cernak, M.

    2004-01-01

    Polyester cord threads, which are used as a reinforcing materials of rubber blend, have been treated in atmospheric-pressure H 2 0 plasma in order to enhance their adhesion to rubber. The atmospheric-pressure H 2 0 plasma was generated in an underwater diaphragm discharge. The plasma treatment resulted in approximately 100% improvement in the adhesion. Scanning electron microscopy investigation indicates that not only introduced surface polar groups but also increased surface area of the fibres due to a fibre surface roughening are responsible for the improved adhesive strength (Authors)

  2. Atmospheric pressure cold plasma as an antifungal therapy

    International Nuclear Information System (INIS)

    Sun Peng; Wu Haiyan; Sun Yi; Liu Wei; Li Ruoyu; Zhu Weidong; Lopez, Jose L.; Zhang Jue; Fang Jing

    2011-01-01

    A microhollow cathode based, direct-current, atmospheric pressure, He/O 2 (2%) cold plasma microjet was used to inactive antifungal resistants Candida albicans, Candida krusei, and Candida glabrata in air and in water. Effective inactivation (>90%) was achieved in 10 min in air and 1 min in water. Antifungal susceptibility tests showed drastic reduction of the minimum inhibitory concentration after plasma treatment. The inactivation was attributed to the reactive oxygen species generated in plasma or in water. Hydroxyl and singlet molecular oxygen radicals were detected in plasma-water system by electron spin resonance spectroscopy. This approach proposed a promising clinical dermatology therapy.

  3. Voltage-Current Characteristics of Plasma Pressure Sensor

    Science.gov (United States)

    Matlis, Eric; Corke, Thomas; Marshall, Curtis; Gogineni, Sivaram; University of Notre Dame Team; Spectral Energies Team

    2012-11-01

    A pressure sensor based on the use of plasma as the sensing element is being developed. This is an AC-driven, continuous-wave plasma which is encapsulated between two metallic bare electrodes with a small air gap on the order of 0.03 mm. The sensor uses a non-equilibrium discharge at less than 20 Watts of power. This devices features an amplitude modulated carrier to measure both mean and dynamic pressure. The frequency response is limited only by the carrier frequency which can be as high as 1 MHz. Glow-to-Arc transition is controlled with the use of a capacitive and resistive circuit in series with the discharge. A pressure chamber is used to document the plasma power characteristics as the ambient pressure is controlled from atmospheric to 100 psi. Plasma power is controlled so as to maintain the plasma in the normal and abnormal glow regimes. The phase angle between voltage and current is recorded as a function of pressure. This analysis will aid in the development of a feedback control and calibration of the pressure sensor. NavAir SBIR.

  4. Novel Approach in the Use of Plasma Spray: Preparation of Bulk Titanium for Bone Augmentations

    Directory of Open Access Journals (Sweden)

    Michaela Fousova

    2017-08-01

    Full Text Available Thermal plasma spray is a common, well-established technology used in various application fields. Nevertheless, in our work, this technology was employed in a completely new way; for the preparation of bulk titanium. The aim was to produce titanium with properties similar to human bone to be used for bone augmentations. Titanium rods sprayed on a thin substrate wire exerted a porosity of about 15%, which yielded a significant decrease of Young′s modulus to the bone range and provided rugged topography for enhanced biological fixation. For the first verification of the suitability of the selected approach, tests of the mechanical properties in terms of compression, bending, and impact were carried out, the surface was characterized, and its compatibility with bone cells was studied. While preserving a high enough compressive strength of 628 MPa, the elastic modulus reached 11.6 GPa, thus preventing a stress-shielding effect, a generally known problem of implantable metals. U-2 OS and Saos-2 cells derived from bone osteosarcoma grown on the plasma-sprayed surface showed good viability.

  5. The compact mirrors with high pressure plasmas

    International Nuclear Information System (INIS)

    Anikeev, A.V.; Bagryansky, P.A.; Ivanov, A.A.; Lizunov, A.A.; Murakhtin, S.V.; Prikhodko, V.V.; Collatz, S.; Noack, K.

    2004-01-01

    The gas dynamic trap (GDP) experimental facility at the Budker Institute Novosibirsk is a long axial-symmetric mirror system with a high mirror ratio variable in the range of 12.5 - 100 for the confinement of a two-component plasma. One component is a collisional plasma with ion and electron temperatures up to 100 eV and density up to 10 14 cm -3 . The second component is the population of high-energetic fast ions with energies of 2-18 keV and a density up to 10 13 cm -3 which is produced by neutral beam injection (NBI). GDP is currently undergoing an upgrade whose first stage is the achievement of the synthesized hot ion plasmoid experiment (SHIP). This experiment aims at the investigation of plasmas and at the knowledge of plasma parameters that have never been achieved before in magnetic mirrors. The paper presents the physical concept of the SHIP experiment, the results of numerical pre-calculations and draws conclusions regarding possible scenarios of experiments. The simulation of a maximal NBI power regime with hydrogen injection gave a fast ion density of 1.2*10 14 cm -3 with a mean energy of 14 keV. The calculation of the deuterium injection regime with 2 MW NBI power gave a maximal fast ion density of 1.9*10 14 cm -3 with a beam energy of 9 keV. The calculation of an experimental scenario with reduced magnetic field resulted in a maximal β-value of 62%, so this regime is recommended for the study of high-β effects in plasmas confined in axial-symmetric mirrors

  6. Characterization of non- equilibrium atmospheric pressure plasma jets

    International Nuclear Information System (INIS)

    Qurat-ul-Ain

    2012-01-01

    Low temperature atmospheric pressure plasmas have been recognized as a new paradigm in plasma physics with their potential, economic and technological impacts in many scientific disciplines. This is due to their lower costs, high productibility, continuous processing, and potentially novel applications, which cannot be attained by using expensive vacuum systems. They can be generated by a variety of techniques; one of them is the atmospheric pressure plasma jet (APPJ), which features a radio-frequency (RF) discharge between bare metallic electrodes. Usually APPJ is operated in the alpha mode at gap spacings in the range of 1 mm or even more. In this research work two APPJs (APPJ2, APPJ3) with different size are studied; the electrode area of the device APPJ3 is half than the area of APPJ2, and both are sandwiched structures. The RF capacitive coupled discharges were fundamentally characterized in helium there of by voltage-current measurements, macroscopic visualization and manipulation of the discharges and extensive spectroscopic measurements. APPJ3 is operated for gap spacing 1 mm down to 0.1 mm at a fixed gas flow rate. Uniform glow discharges can be generated for gap spacing 1 mm down to 0.1 mm. Plasma parameters were extracted using equivalent circuit models. It has been shown that at larger gaps discharge is present which exhibit a fully develop bulk plasma region with sheaths. At gap spacings 0.4 mm the discharge don't have a fully develop bulk plasma and sheaths starts occupying more space of the gap. At gap spacings 0.5 mm two regimes can be observed, a normal regime with partial coverage and an abnormal regime with full coverage of the electrodes, whereas for gaps 0.4 mm there is no partial coverage observed even at very low powers. In all cases impedance measurements have been performed and compared with equivalent circuit models. These equivalent circuit models capture the picture correctly at lager gaps. For smaller gaps using sheath only model and

  7. Sterilization of Turmeric by Atmospheric Pressure Dielectric Barrier Discharge Plasma

    International Nuclear Information System (INIS)

    Salarieh Setareh; Dorranian Davoud

    2013-01-01

    In this study atmospheric pressure dielectric barrier discharge (DBD) plasma has been employed for sterilizing dry turmeric powders. A 6 kV, 6 kHz frequency generator was used to generate plasma with Ar, Ar/O 2 , He, and He/O 2 gases between the 5 mm gap of two quartz covered electrodes. The complete sterilization time of samples due to plasma treatment was measured. The most important contaminant of turmeric is bacillus subtilis. The results show that the shortest sterilization time of 15 min is achieved by exposing the samples to Ar/O 2 plasma. Survival curves of samples are exponential functions of time and the addition of oxygen to plasma leads to a significant increase of the absolute value of time constant of the curves. Magnitudes of protein and DNA in treated samples were increased to a similar value for all samples. Taste, color, and solubility of samples were not changed after the plasma treatment

  8. Sterilization of Turmeric by Atmospheric Pressure Dielectric Barrier Discharge Plasma

    Science.gov (United States)

    Setareh, Salarieh; Davoud, Dorranian

    2013-11-01

    In this study atmospheric pressure dielectric barrier discharge (DBD) plasma has been employed for sterilizing dry turmeric powders. A 6 kV, 6 kHz frequency generator was used to generate plasma with Ar, Ar/O2, He, and He/O2 gases between the 5 mm gap of two quartz covered electrodes. The complete sterilization time of samples due to plasma treatment was measured. The most important contaminant of turmeric is bacillus subtilis. The results show that the shortest sterilization time of 15 min is achieved by exposing the samples to Ar/O2 plasma. Survival curves of samples are exponential functions of time and the addition of oxygen to plasma leads to a significant increase of the absolute value of time constant of the curves. Magnitudes of protein and DNA in treated samples were increased to a similar value for all samples. Taste, color, and solubility of samples were not changed after the plasma treatment.

  9. Free-floating atmospheric pressure ball plasmas

    Science.gov (United States)

    Wurden, G. A.; Ticos, C.; Wang, Z.; Wurden, C. J. V.

    2007-11-01

    A long-lived (0.3 second, 10-20 cm diameter) ball plasma floating in the air above a water surface has been formed and studied in the laboratory. A 0.4 - 1 mF capacitor is charged to 4-5 kV, and subsequently discharged (30-60 Amps, 20-50 msec duration) into central copper cathode held fixed just below the surface of a bucket of water (with a weak solution of various salts in distilled water, such as CuSO4 or CuCl2, LiCl or NaCl). An underwater ring anode completes the circuit. A bubble of hot vapor from the water surface rises up in the first few milliseconds, and changes from a mushroom cloud with stalk, to a detached quasi-spherical object, finally evolving into a vortex ring. The plasma consists of ionized water vapor, with positive salts and OH- radicals, as well as molecular species, and it completely excludes nitrogen or oxygen from the rising plasma structure. A fine boundary layer is visible in orange, in contrast to a green ball interior when using Cu/CuSO4, and filamentary structures are visible at late times. Finally, a whisp of smoke ring is observed as a residue. A variety of visible and infrared imaging (both video and still cameras) are used, along with 200-800 nm time & space resolved spectroscopy, to identify features of this laboratory analog to ball lightning. Possible applications include a windowless ball- plasma powered pulsed copper vapor laser operating at 510 nm.

  10. Stimulation of wound healing by helium atmospheric pressure plasma treatment

    Energy Technology Data Exchange (ETDEWEB)

    Nastuta, Andrei Vasile; Topala, Ionut; Pohoata, Valentin; Popa, Gheorghe [Faculty of Physics, Alexandru Ioan Cuza University, Bd. Carol No. 11, 700506, Iasi (Romania); Grigoras, Constantin, E-mail: andrei.nastuta@uaic.ro [Physiopathology Department, Grigore T. Popa University of Medicine and Pharmacy, 700115, Iasi (Romania)

    2011-03-16

    New experiments using atmospheric pressure plasma have found large application in treatment of living cells or tissues, wound healing, cancerous cell apoptosis, blood coagulation on wounds, bone tissue modification, sterilization and decontamination. In this study an atmospheric pressure plasma jet generated using a cylindrical dielectric-barrier discharge was applied for treatment of burned wounds on Wistar rats' skin. The low temperature plasma jet works in helium and is driven by high voltage pulses. Oxygen and nitrogen based impurities are identified in the jet by emission spectroscopy. This paper analyses the natural epithelization of the rats' skin wounds and two methods of assisted epithelization, a classical one using polyurethane wound dressing and a new one using daily atmospheric pressure plasma treatment of wounds. Systemic and local medical data, such as haematological, biochemical and histological parameters, were monitored during entire period of study. Increased oxidative stress was observed for plasma treated wound. This result can be related to the presence in the plasma volume of active species, such as O and OH radicals. Both methods, wound dressing and plasma-assisted epithelization, provided positive medical results related to the recovery process of burned wounds. The dynamics of the skin regeneration process was modified: the epidermis re-epitelization was accelerated, while the recovery of superficial dermis was slowed down.

  11. Stimulation of wound healing by helium atmospheric pressure plasma treatment

    International Nuclear Information System (INIS)

    Nastuta, Andrei Vasile; Topala, Ionut; Pohoata, Valentin; Popa, Gheorghe; Grigoras, Constantin

    2011-01-01

    New experiments using atmospheric pressure plasma have found large application in treatment of living cells or tissues, wound healing, cancerous cell apoptosis, blood coagulation on wounds, bone tissue modification, sterilization and decontamination. In this study an atmospheric pressure plasma jet generated using a cylindrical dielectric-barrier discharge was applied for treatment of burned wounds on Wistar rats' skin. The low temperature plasma jet works in helium and is driven by high voltage pulses. Oxygen and nitrogen based impurities are identified in the jet by emission spectroscopy. This paper analyses the natural epithelization of the rats' skin wounds and two methods of assisted epithelization, a classical one using polyurethane wound dressing and a new one using daily atmospheric pressure plasma treatment of wounds. Systemic and local medical data, such as haematological, biochemical and histological parameters, were monitored during entire period of study. Increased oxidative stress was observed for plasma treated wound. This result can be related to the presence in the plasma volume of active species, such as O and OH radicals. Both methods, wound dressing and plasma-assisted epithelization, provided positive medical results related to the recovery process of burned wounds. The dynamics of the skin regeneration process was modified: the epidermis re-epitelization was accelerated, while the recovery of superficial dermis was slowed down.

  12. Deviation from bulk in the pressure-temperature phase diagram of V2O3 thin films

    Science.gov (United States)

    Valmianski, I.; Ramirez, Juan Gabriel; Urban, C.; Batlle, X.; Schuller, Ivan K.

    2017-04-01

    We found atypical pressure dependence in the transport measurements of the metal to insulator transition (MIT) in epitaxial thin films of vanadium sesquioxide (V2O3 ). Three different crystallographic orientations and four thicknesses, ranging from 40 to 500 nm, were examined under hydrostatic pressures (Ph) of up to 1.5 GPa. All of the films at transition exhibited a four order of magnitude resistance change, with transition temperatures ranging from 140 to 165 K, depending on the orientation. This allowed us to build pressure-temperature phase diagrams of several orientations and film thicknesses. Interestingly, for pressures below 500 MPa, all samples deviate from bulk behavior and show a weak transition temperature (Tc) pressure dependence (d Tc/d Ph=1.2 ×10-2±0.3 ×10-2K /MPa ), which recovers to bulklike behavior (3.9 ×10-2±0.3 ×10-2K /MPa ) at higher pressures. Furthermore, we found that pressurization leads to morphological but not structural changes in the films. This indicates that the difference in the thin film and bulk pressure-temperature phase diagrams is most probably due to pressure-induced grain boundary relaxation, as well as both plastic and elastic deformations in the film microstructure. These results highlight the difference between bulk and thin films behaviors.

  13. In-package inhibition of E.coli 0157:H7 on bulk romaine lettuce using cold plasma

    Science.gov (United States)

    Dielectric barrier discharge atmospheric cold plasma (DACP) treatment was evaluated for the inactivation of Escherichia coli O157:H7, surface morphology, color, carbon dioxide generation, and weight loss of bulk Romaine lettuce in a commercial plastic clamshell container. The lettuce samples were pa...

  14. Atmospheric-Pressure Plasma Interaction with Soft Materials as Fundamental Processes in Plasma Medicine.

    Science.gov (United States)

    Takenaka, Kosuke; Miyazaki, Atsushi; Uchida, Giichiro; Setsuhara, Yuichi

    2015-03-01

    Molecular-structure variation of organic materials irradiated with atmospheric pressure He plasma jet have been investigated. Optical emission spectrum in the atmospheric-pressure He plasma jet has been measured. The spectrum shows considerable emissions of He lines, and the emission of O and N radicals attributed to air. Variation in molecular structure of Polyethylene terephthalate (PET) film surface irradiated with the atmospheric-pressure He plasma jet has been observed via X-ray photoelectron spectroscopy (XPS) and Fourier transform infrared spectroscopy (FT-IR). These results via XPS and FT-IR indicate that the PET surface irradiated with the atmospheric-pressure He plasma jet was oxidized by chemical and/or physical effect due to irradiation of active species.

  15. Laser-induced microexplosion confined in the bulk of a sapphire crystal: evidence of multimegabar pressures.

    Science.gov (United States)

    Juodkazis, S; Nishimura, K; Tanaka, S; Misawa, H; Gamaly, E G; Luther-Davies, B; Hallo, L; Nicolai, P; Tikhonchuk, V T

    2006-04-28

    Extremely high pressures (approximately 10 TPa) and temperatures (5 x 10(5) K) have been produced using a single laser pulse (100 nJ, 800 nm, 200 fs) focused inside a sapphire crystal. The laser pulse creates an intensity over 10(14) W/cm2 converting material within the absorbing volume of approximately 0.2 microm3 into plasma in a few fs. A pressure of approximately 10 TPa, far exceeding the strength of any material, is created generating strong shock and rarefaction waves. This results in the formation of a nanovoid surrounded by a shell of shock-affected material inside undamaged crystal. Analysis of the size of the void and the shock-affected zone versus the deposited energy shows that the experimental results can be understood on the basis of conservation laws and be modeled by plasma hydrodynamics. Matter subjected to record heating and cooling rates of 10(18) K/s can, thus, be studied in a well-controlled laboratory environment.

  16. Plasma pressure and anisotropy inferred from the Tsyganenkomagnetic field model

    Directory of Open Access Journals (Sweden)

    F. Cao

    Full Text Available A numerical procedure has been developed to deduce the plasma pressure and anisotropy from the Tsyganenko magnetic field model. The Tsyganenko empirical field model, which is based on vast satellite field data, provides a realistic description of magnetic field configuration in the magnetosphere. When the force balance under the static condition is assumed, the electromagnetic J×B force from the Tsyganenko field model can be used to infer the plasma pressure and anisotropy distributions consistent with the field model. It is found that the J×B force obtained from the Tsyganenko field model is not curl-free. The curl-free part of the J×B force in an empirical field model can be balanced by the gradient of the isotropic pressure, while the nonzero curl of the J×B force can only be associated with the pressure anisotropy. The plasma pressure and anisotropy in the near-Earth plasma sheet are numerically calculated to obtain a static equilibrium consistent with the Tsyganenko field model both in the noon-midnight meridian and in the equatorial plane. The plasma pressure distribution deduced from the Tsyganenko 1989 field model is highly anisotropic and shows this feature early in the substorm growth phase. The pressure anisotropy parameter αP, defined as αP=1-PVertP, is typically ~0.3 at x ≈ -4.5RE and gradually decreases to a small negative value with an increasing tailward distance. The pressure anisotropy from the Tsyganenko 1989 model accounts for 50% of the cross-tail current at maximum and only in a highly localized region near xsim-10RE. In comparison, the plasma pressure anisotropy inferred from the Tsyganenko 1987 model is much smaller. We also find that the boundary

  17. Mass analysis of an atmospheric pressure plasma needle discharge

    International Nuclear Information System (INIS)

    Malovic, G; Puac, N; Lazovic, S; Petrovic, Z

    2010-01-01

    Mass spectrometric measurements of a plasma needle (an example of atmospheric pressure non-equilibrium plasma source) were made for neutrals and ions. The measurements were performed for the same geometry as the standard plasma needles albeit for a somewhat increased gas flow. We discuss some of the problems of performing mass analysis at atmospheric pressures. The yields of N, O and NO radicals from the plasma needle were determined for different powers of the RF source and different flow rates of working gas. Positive ions generated by the plasma needle itself were measured for the first time. Significant conversion of feed gases (nitrogen and oxygen) into radicals and ions of N and O, and NO was observed as well as depletion of atomic radicals N and O which in chemical reactions form more complex molecules. Biomedical and nanotechnology applications of atmospheric pressure plasmas require a detailed understanding of the source, and mass analysis is perhaps the best technique to focus on chemical kinetics and in many ways interaction with surfaces.

  18. The main properties of microwave argon plasma at atmospheric pressure

    International Nuclear Information System (INIS)

    Benova, E; Pencheva, M

    2010-01-01

    Plasma torch sustained by surface wave at atmospheric pressure is theoretically studied by means of 1D model. A steady-state Boltzmann equation in an effective field approximation coupled with a collisional-radiative model for high-pressure argon discharge is numerically solved together with Maxwell's equations for an azimuthally symmetric TM surface wave. The axial dependences of the electrons, excited atoms, atomic and molecular ions densities as well as the electron temperature, the mean power per electron and the effective electron-neutral collision frequency are determined. A strong dependence of the plasma properties on the discharge conditions and the gas temperature is obtained.

  19. Atmospheric pressure plasma surface modification of carbon fibres

    DEFF Research Database (Denmark)

    Kusano, Yukihiro; Løgstrup Andersen, Tom; Michelsen, Poul

    2008-01-01

    Carbon fibres are continuously treated with dielectric barrier discharge plasma at atmospheric pressure in various gas conditions for adhesion improvement in mind. An x-ray photoelectron spectroscopic analysis indicated that oxygen is effectively introduced onto the carbon fibre surfaces by He, He....../O2 and Ar plasma treatments, mainly attributed to an increase in the density of the C-O single bond at the carbon fibre surfaces. The O/C ratio increased to 0.182 after 1-s He plasma treatment, and remained approximately constant after longer treatment. After exposure in an ambient air at room...

  20. HIPPO, the high-pressure preferred orientation diffractometer at LANSCE for characterization of bulk materials

    International Nuclear Information System (INIS)

    Bennett, K.; Dreele, R.B. von; Wenk, H.R.

    2001-01-01

    United States National Laboratory researchers and University of California faculty, representing a broad range of scientific disciplines, is building a novel time-of-flight (TOF) neutron diffractometer and associated in situ equipment at the Manuel Lujan Jr. Neutron Scattering Center (Lujan Center), under the auspices of the United States Department of Energy. The goal with the High-Pressure Preferred Orientation Instrument (HIPPO) is to investigate dynamic processes in heterogeneous bulk materials in a variety of environments. The instrument, which will become available in summer 2001, has the extremely high count-rates necessary to study time-dependent processes in small (1-mm diameter) and large (2-cm diameter) samples, and in a large variety of environmental conditions (10-2000 K cryostats and furnaces, 0-20 GPa pressure vessels, straining cells, goniometers, magnets, etc.). The 3-D arrangement of detectors allows direct measurements of crystal orientation distributions in polycrystalline materials. The analysis of TOF diffraction patterns with versatile Rietveld codes provides simultaneous information on crystal structure, texture, microstructure and phase proportions. While this instrument has many applications in materials science, it is also of great interest for geology and geophysics. Some applications include: kinetics of reactions, structure of silicate glasses and melts, high-pressure investigations of complex systems, evolution of texture and anisotropy during deformation and recrystallization. The Lujan Center aims at creating an instrument with high data through-put and easy access to researchers and students. While the HIPPO instrument will be part of the national user facility operated by the Lujan Center, the scientific program will be guided by the University of California consortium with the goal of satisfying national priorities and establishing an environment of scientific excellence. (author)

  1. HIPPO, the high-pressure preferred orientation diffractometer at LANSCE for characterization of bulk materials

    Energy Technology Data Exchange (ETDEWEB)

    Bennett, K.; Dreele, R.B. von [Manuel Lujan Jr. Neutron Scattering Center, Los Alamos, NM (United States); Wenk, H.R. [Department of Geology and Geophysics, Univ. of California, Berkely, CA (United States)

    2001-03-01

    United States National Laboratory researchers and University of California faculty, representing a broad range of scientific disciplines, is building a novel time-of-flight (TOF) neutron diffractometer and associated in situ equipment at the Manuel Lujan Jr. Neutron Scattering Center (Lujan Center), under the auspices of the United States Department of Energy. The goal with the High-Pressure Preferred Orientation Instrument (HIPPO) is to investigate dynamic processes in heterogeneous bulk materials in a variety of environments. The instrument, which will become available in summer 2001, has the extremely high count-rates necessary to study time-dependent processes in small (1-mm diameter) and large (2-cm diameter) samples, and in a large variety of environmental conditions (10-2000 K cryostats and furnaces, 0-20 GPa pressure vessels, straining cells, goniometers, magnets, etc.). The 3-D arrangement of detectors allows direct measurements of crystal orientation distributions in polycrystalline materials. The analysis of TOF diffraction patterns with versatile Rietveld codes provides simultaneous information on crystal structure, texture, microstructure and phase proportions. While this instrument has many applications in materials science, it is also of great interest for geology and geophysics. Some applications include: kinetics of reactions, structure of silicate glasses and melts, high-pressure investigations of complex systems, evolution of texture and anisotropy during deformation and recrystallization. The Lujan Center aims at creating an instrument with high data through-put and easy access to researchers and students. While the HIPPO instrument will be part of the national user facility operated by the Lujan Center, the scientific program will be guided by the University of California consortium with the goal of satisfying national priorities and establishing an environment of scientific excellence. (author)

  2. Atmospheric pressure plasma and electron cyclotron resonance plasma and their applications

    Science.gov (United States)

    Koretzky, Edward Van

    1999-03-01

    Based on a capacitively coupled electrical discharge scheme, an array of plasma torches is generated to form a dense plasma layer in the open air. In order to use a single power source to supply several torches simultaneously, capacitors are used as ballasting impedances coupling all the torches together. Several diagnostics are performed on a single plasma torch to find its temperature, dimensions, and plasma density. To ease constructing an atmospheric pressure plasma source, a modular system is then presented. The design and construction of the plasma torch module is described. The electrical characteristics of the module is studied for the case of a single module and two capacitively coupled modules. For understanding the plasma torch, each is represented by a parallel RC circuit, in which both R and C are time dependent due to the plasma. The dynamics of the plasma is described by the rate equations for the various plasma species. Numerical simulations have been performed to determine the parameter space for efficient generation of the plasma. Scattering (and absorption) of electromagnetic waves by the plasma torches in a rectangular waveguide is studied experimentally and theoretically. By changing the number of torches appearing in the waveguide, the dependence of the microwave power loss on the plasma volume is determined. ECR plasma-assisted chemical vapor deposition (PACVD) is a technique currently receiving much interest because the ECR plasma system offers a more complex parameter space than the conventional PACVD process. Moreover, a unique feature of the ECR plasma is the production of an energetic electron tail, establishing a large sheath potential on the substrate surface for energizing the bombarding ions, which enhances the nucleation rate. An ECR system for PACVD of diamond film on silicon substrates is designed and built. After surface treatment by the ECR produced energetic ions, the low pressure ECR plasma operation is switched, in situ, to a

  3. Using atmospheric pressure plasma treatment for treating grey cotton fabric.

    Science.gov (United States)

    Kan, Chi-Wai; Lam, Chui-Fung; Chan, Chee-Kooi; Ng, Sun-Pui

    2014-02-15

    Conventional wet treatment, desizing, scouring and bleaching, for grey cotton fabric involves the use of high water, chemical and energy consumption which may not be considered as a clean process. This study aims to investigate the efficiency of the atmospheric pressure plasma (APP) treatment on treating grey cotton fabric when compared with the conventional wet treatment. Grey cotton fabrics were treated with different combinations of plasma parameters with helium and oxygen gases and also through conventional desizing, scouring and bleaching processes in order to obtain comparable results. The results obtained from wicking and water drop tests showed that wettability of grey cotton fabrics was greatly improved after plasma treatment and yielded better results than conventional desizing and scouring. The weight reduction of plasma treated grey cotton fabrics revealed that plasma treatment can help remove sizing materials and impurities. Chemical and morphological changes in plasma treated samples were analysed by FTIR and SEM, respectively. Finally, dyeability of the plasma treated and conventional wet treated grey cotton fabrics was compared and the results showed that similar dyeing results were obtained. This can prove that plasma treatment would be another choice for treating grey cotton fabrics. Copyright © 2013 Elsevier Ltd. All rights reserved.

  4. Atmospheric pressure plasma jet treatment of Salmonella Enteritidis inoculated eggshells.

    Science.gov (United States)

    Moritz, Maike; Wiacek, Claudia; Koethe, Martin; Braun, Peggy G

    2017-03-20

    Contamination of eggshells with Salmonella Enteritidis remains a food safety concern. In many cases human salmonellosis within the EU can be traced back to raw or undercooked eggs and egg products. Atmospheric pressure plasma is a novel decontamination method that can reduce a wide range of pathogens. The aim of this work was to evaluate the possibility of using an effective short time cold plasma treatment to inactivate Salmonella Enteritidis on the eggshell. Therefore, artificially contaminated eggshells were treated with an atmospheric pressure plasma jet under different experimental settings with various exposure times (15-300s), distances from the plasma jet nozzle to the eggshell surface (5, 8 or 12mm), feed gas compositions (Ar, Ar with 0.2, 0.5 or 1.0% O 2 ), gas flow rates (5 and 7slm) and different inoculations of Salmonella Enteritidis (10 1 -10 6 CFU/cm 2 ). Atmospheric pressure plasma could reduce Salmonella Enteritidis on eggshells significantly. Reduction factors ranged between 0.22 and 2.27 log CFU (colony-forming units). Exposure time and, particularly at 10 4 CFU/cm 2 inoculation, feed gas had a major impact on Salmonella reduction. Precisely, longer exposure times led to higher reductions and Ar as feed gas was more effective than ArO 2 mixtures. Copyright © 2017 Elsevier B.V. All rights reserved.

  5. Generation of uniform atmospheric pressure argon glow plasma by ...

    Indian Academy of Sciences (India)

    Vol. 80, No. 3. — journal of. March 2013 physics pp. 507–517. Generation of uniform atmospheric pressure argon glow plasma by dielectric barrier discharge .... note that the change in current waveform is also due to the change in capacitance of the ... By taking the ratio of R1 and R2 we then obtain the expression: R1. R2.

  6. Changes in blood pressure and plasma urate induced by the ...

    African Journals Online (AJOL)

    ... as yet another risk factor for hypertension, known to be common amongst habitual ethanol drinkers. Further research is however, required to establish the mechanism (s) involved in such relationships. Key Words: Blood pressure, plasma urate, hypertension, alcohol. Global Jnl Medical Sciences Vol.2(2) 2003: 157-160 ...

  7. Exploration to generate atmospheric pressure glow discharge plasma in air

    Science.gov (United States)

    Wenzheng, LIU; Chuanlong, MA; Shuai, ZHAO; Xiaozhong, CHEN; Tahan, WANG; Luxiang, ZHAO; Zhiyi, LI; Jiangqi, NIU; Liying, ZHU; Maolin, CHAI

    2018-03-01

    Atmospheric pressure glow discharge (APGD) plasma in air has high application value. In this paper, the methods of generating APGD plasma in air are discussed, and the characteristics of dielectric barrier discharge (DBD) in non-uniform electric field are studied. It makes sure that APGD in air is formed by DBD in alternating current electric field with using the absorbing electron capacity of electret materials to provide initial electrons and to end the discharge progress. Through designing electric field to form two-dimensional space varying electric field and three-dimensional space varying electric field, the development of electron avalanches in air-gap is suppressed effectively and a large space of APGD plasma in air is generated. Further, through combining electrode structures, a large area of APGD plasma in air is generated. On the other hand, by using the method of increasing the density of initial electrons, millimeter-gap glow discharge in atmospheric pressure air is formed, and a maximum gap distance between electrodes is 8 mm. By using the APGD plasma surface treatment device composed of contact electrodes, the surface modification of high polymer materials such as aramid fiber and polyester are studied and good effect of modifications is obtained. The present paper provides references for the researchers of industrial applications of plasma.

  8. An investigation of transient pressures and plasma properties in a pinched plasma column. M.S. Thesis

    Science.gov (United States)

    Stover, E. K.; York, T. M.

    1971-01-01

    The transient pinched plasma column generated in a linear Z-pinch was studied experimentally and analytically. The plasma column was investigated experimentally with several plasma diagnostics; they were: a rapid response pressure transducer, a magnetic field probe, a voltage probe, and discharge luminosity. Axial pressure profiles on the discharge chamber axis were used to identify three characteristic regions of plasma column behavior: (1) strong axial pressure asymmetry noted early in plasma column lifetime, (2) followed by plasma heating in which there is a rapid rise in static pressure, and (3) a slight decrease static pressure before plasma column breakup. Plasma column lifetime was approximately 5 microseconds. The axial pressure asymmetry was attributed to nonsimultaneous pinching of the imploding current sheet along the discharge chamber axis. The rapid heating could be attributed in part to viscous effects introduced by radial gradients in the axial streaming velocity.

  9. Pulsed, atmospheric pressure plasma source for emission spectrometry

    Science.gov (United States)

    Duan, Yixiang; Jin, Zhe; Su, Yongxuan

    2004-05-11

    A low-power, plasma source-based, portable molecular light emission generator/detector employing an atmospheric pressure pulsed-plasma for molecular fragmentation and excitation is described. The average power required for the operation of the plasma is between 0.02 W and 5 W. The features of the optical emission spectra obtained with the pulsed plasma source are significantly different from those obtained with direct current (dc) discharge higher power; for example, strong CH emission at 431.2 nm which is only weakly observed with dc plasma sources was observed, and the intense CN emission observed at 383-388 nm using dc plasma sources was weak in most cases. Strong CN emission was only observed using the present apparatus when compounds containing nitrogen, such as aniline were employed as samples. The present apparatus detects dimethylsulfoxide at 200 ppb using helium as the plasma gas by observing the emission band of the CH radical. When coupled with a gas chromatograph for separating components present in a sample to be analyzed, the present invention provides an apparatus for detecting the arrival of a particular component in the sample at the end of the chromatographic column and the identity thereof.

  10. Development of Rayleigh-Taylor and bulk convection instabilities in the dynamics of plasma liners and pinches

    International Nuclear Information System (INIS)

    Bud'ko, A.B.; Velikovich, A.L.; Liberman, M.A.; Felber, F.S.

    1989-01-01

    A solution is derived for the problem of the initial, linear stage of the growth of small perturbations in the course of the cylindrically symmetric compression and expansion of a plasma liner and a Z-pinch with a sharp boundary. In these systems, Rayleigh-Taylor instabilities localized near the plasma boundaries are the most dangerous. Bulk convective instabilities develop in addition to these Rayleigh-Taylor instabilities. The various instability modes, including local and global Rayleigh-Taylor modes, which grown in an accelerated plasma with distributed profiles of hydrodynamic variables, are classified. The spectra of the instability growth rates are calculated for plasma liners and Z-pinches. The shape of these spectra reveals an explanation of the stratification and filamentation of the plasma observed experimentally in pinches and liners. The imposition of a longitudinal magnetic field gives rise to a stability window in the space of the flow parameters. In this window, the Rayleigh-Taylor modes are suppressed completely by magnetic shear, while the bulk convective modes are suppressed to a significant extent

  11. Production of high-strength Al85Y8Ni5Co2 bulk alloy by spark plasma sintering

    International Nuclear Information System (INIS)

    Surreddi, K B; Scudino, S; Sakaliyska, M; Eckert, J; Srivastava, V C; Uhlenwinkel, V; Kim, J S

    2010-01-01

    Highly dense bulk samples were produced by spark plasma sintering (SPS) through combined devitrification and consolidation of partially amorphous Al 85 Y 8 Ni 5 Co 2 gas atomized powders. The microstructure of the consolidated samples shows a mixed structure containing crystalline, ultrafine-grained and amorphous/nanocrystalline particles. The sintered sample exhibits a remarkable high strength of about 1050 MPa combined with 3.7 % fracture strain.

  12. Solvated electrons at the atmospheric pressure plasma-water anodic interface

    Science.gov (United States)

    Gopalakrishnan, R.; Kawamura, E.; Lichtenberg, A. J.; Lieberman, M. A.; Graves, D. B.

    2016-07-01

    We present results from a particle-in-cell/Monte Carlo model of a dc discharge in argon at atmospheric pressure coupled with a fluid model of an aqueous electrolyte acting as anode to the plasma. The coupled models reveal the structure of the plasma-electrolyte interface and near-surface region, with a special emphasis on solvated or hydrated electrons. Results from the coupled models are in generally good agreement with the experimental results of Rumbach et al (2016 Nat. Commun. 6 7248). Electrons injected from the plasma into the water are solvated, then lost by reaction with water within about 10-20 nm from the surface. The major reaction products are OH- and H2. The solvated electron density profile is controlled by the injected electron current density and subsequent reactions with water, and is relatively independent of the external plasma electric field and the salt concentration in the aqueous electrolyte. Simulations of the effects of added scavenger compounds (H2O2, \\text{NO}2- , \\text{NO}2- and H+) on near-surface solvated electron density generally match the experimental results. The generation of near-surface OH- following electron-water decomposition in the presence of bulk acid creates a highly basic region (pH ~ 11) very near the surface. In the presence of bulk solution acidity, pH can vary from a very acidic pH 2 away from the surface to a very basic pH 11 over a distance of ~200 nm. High near-surface gradients in aqueous solution properties could strongly affect plasma-liquid applications and challenge theoretical understanding of this complex region.

  13. Atmospheric Pressure Plasma Treatment for Grey Cotton Knitted Fabric

    Directory of Open Access Journals (Sweden)

    Chi-wai Kan

    2018-01-01

    Full Text Available 100% grey cotton knitted fabric contains impurities and yellowness and needs to be prepared for processing to make it suitable for coloration and finishing. Therefore, conventionally 100% grey cotton knitted fabric undergoes a process of scouring and bleaching, which involves the use of large amounts of water and chemicals, in order to remove impurities and yellowness. Due to increased environmental awareness, pursuing a reduction of water and chemicals is a current trend in textile processing. In this study, we explore the possibility of using atmospheric pressure plasma as a dry process to treat 100% grey cotton knitted fabric (single jersey and interlock before processing. Experimental results reveal that atmospheric pressure plasma treatment can effectively remove impurities from 100% grey cotton knitted fabrics and significantly improve its water absorption property. On the other hand, if 100% grey cotton knitted fabrics are pretreated with plasma and then undergo a normal scouring process, the treatment time is reduced. In addition, the surface morphological and chemical changes in plasma-treated fabrics were studied and compared with the conventionally treated fabrics using scanning electron microscope (SEM, Fourier-transform infrared spectroscopy-attenuated total reflection (FTIR-ATR and X-ray photoelectron spectroscopy (XPS. The decrease in carbon content, as shown in XPS, reveal the removal of surface impurities. The oxygen-to-carbon (O/C ratios of the plasma treated knitted fabrics reveal enhanced hydrophilicity.

  14. Application of atmospheric pressure plasma in polymer and composite adhesion

    Science.gov (United States)

    Yu, Hang

    An atmospheric pressure helium and oxygen plasma was used to investigate surface activation and bonding in polymer composites. This device was operated by passing 1.0-3.0 vol% of oxygen in helium through a pair of parallel plate metal electrodes powered by 13.56 or 27.12 MHz radio frequency power. The gases were partially ionized between the capacitors where plasma was generated. The reactive species in the plasma were carried downstream by the gas flow to treat the substrate surface. The temperature of the plasm gas reaching the surface of the substrate did not exceed 150 °C, which makes it suitable for polymer processing. The reactive species in the plasma downstream includes ~ 1016-1017 cm-3 atomic oxygen, ~ 1015 cm-3 ozone molecule, and ~ 10 16 cm-3 metastable oxygen molecule (O2 1Deltag). The substrates were treated at 2-5 mm distance from the exit of the plasma. Surface properties of the substrates were characterized using water contact angle (WCA), atomic force microscopy (AFM), infrared spectroscopy (IR), and X-ray photoelectron spectroscopy (XPS). Subsequently, the plasma treated samples were bonded adhesively or fabricated into composites. The increase in mechanical strength was correlated to changes in the material composition and structure after plasma treatment. The work presented hereafter establishes atmospheric pressure plasma as an effective method to activate and to clean the surfaces of polymers and composites for bonding. This application can be further expanded to the activation of carbon fibers for better fiber-resin interactions during the fabrication of composites. Treating electronic grade FR-4 and polyimide with the He/O2 plasma for a few seconds changed the substrate surface from hydrophobic to hydrophilic, which allowed complete wetting of the surface by epoxy in underfill applications. Characterization of the surface by X-ray photoelectron spectroscopy shows formation of oxygenated functional groups, including hydroxyl, carbonyl, and

  15. Sixteen-Day Bedrest Significantly Increases Plasma Colloid Osmotic Pressure

    Science.gov (United States)

    Hargens, Alan R.; Hsieh, S. T.; Murthy, G.; Ballard, R. E.; Convertino, V. A.; Wade, Charles E. (Technical Monitor)

    1994-01-01

    Upon exposure to microgravity, astronauts lose up to 10% of their total plasma volume, which may contribute to orthostatic intolerance after space flight. Because plasma colloid osmotic pressure (COP) is a primary factor maintaining plasma volume, our objective was to measure time course changes in COP during microgravity simulated by 6 deg. head-down tilt (HDT). Seven healthy male subjects (30-55 years of age) were placed in HDT for 16 days. For the purpose of another study, three of the seven subjects were chosen to exercise on a cycle ergometer on day 16. Blood samples were drawn immediately before bedrest on day 14 of bedrest, 18-24 hours following exercise while all subjects were still in HDT and 1 hour following bedrest termination. Plasma COP was measured in all 20 microliter EDTA-treated samples using an osmometer fitted with a PM 30 membrane. Data were analyzed with paired and unpaired t-tests. Plasma COP on day 14 of bedrest (29.9 +/- 0.69 mmHg) was significantly higher (p less than 0.005) than the control, pre-bedrest value (23.1 +/- 0.76 mmHg). At one hour of upright recovery after HDT, plasma COP remained significantly elevated (exercise: 26.9 +/- 0.87 mmHg; no exercise: 26.3 +/- 0.85 mmHg). Additionally, exercise had no significant effect on plasma COP 18-24 hours following exercise (exercise: 27.8 +/- 1.09 mmHg; no exercise: 27.1 +/- 0.78 mmHg). Our results demonstrate that plasma COP increases significantly with microgravity simulated by HDT. However, preliminary results indicate exercise during HDT does not significantly affect plasma COP.

  16. Blood pressure and plasma catecholamines in acute and prolonged hypoxia

    DEFF Research Database (Denmark)

    Kanstrup, I L; Poulsen, T D; Hansen, J M

    1999-01-01

    This study measured the pressor and plasma catecholamine response to local hypothermia during adaptation to hypobaric hypoxia. Eight healthy men were studied at rest and after 10 and 45 min of local cooling of one hand and forearm as well as after 30 min of rewarming at sea level and again 24 h...... and 5 days after rapid, passive transport to high altitude (4,559 m). Acute mountain sickness scores ranged from 5 to 16 (maximal attainable score: 20) on the first day but were reduced to 0-8 by the fifth day. Systolic blood pressure, heart rate, and plasma epinephrine increased on day 1 at altitude...

  17. Nanocapillary Atmospheric Pressure Plasma Jet: A Tool for Ultrafine Maskless Surface Modification at Atmospheric Pressure.

    Science.gov (United States)

    Motrescu, Iuliana; Nagatsu, Masaaki

    2016-05-18

    With respect to microsized surface functionalization techniques we proposed the use of a maskless, versatile, simple tool, represented by a nano- or microcapillary atmospheric pressure plasma jet for producing microsized controlled etching, chemical vapor deposition, and chemical modification patterns on polymeric surfaces. In this work we show the possibility of size-controlled surface amination, and we discuss it as a function of different processing parameters. Moreover, we prove the successful connection of labeled sugar chains on the functionalized microscale patterns, indicating the possibility to use ultrafine capillary atmospheric pressure plasma jets as versatile tools for biosensing, tissue engineering, and related biomedical applications.

  18. On non-equilibrium atmospheric pressure plasma jets and plasma bullet

    Science.gov (United States)

    Lu, Xinpei

    2012-10-01

    Because of the enhanced plasma chemistry, atmospheric pressure nonequilibrium plasmas (APNPs) have been widely studied for several emerging applications such as biomedical applications. For the biomedical applications, plasma jet devices, which generate plasma in open space (surrounding air) rather than in confined discharge gaps only, have lots of advantages over the traditional dielectric barrier discharge (DBD) devices. For example, it can be used for root canal disinfection, which can't be realized by the traditional plasma device. On the other hand, currently, the working gases of most of the plasma jet devices are noble gases or the mixtures of the noble gases with small amount of O2, or air. If ambient air is used as the working gas, several serious difficulties are encountered in the plasma generation process. Amongst these are high gas temperatures and disrupting instabilities. In this presentation, firstly, a brief review of the different cold plasma jets developed to date is presented. Secondly, several different plasma jet devices developed in our lab are reported. The effects of various parameters on the plasma jets are discussed. Finally, one of the most interesting phenomena of APNP-Js, the plasma bullet is discussed and its behavior is described. References: [1] X. Lu, M. Laroussi, V. Puech, Plasma Sources Sci. Technol. 21, 034005 (2012); [2] Y. Xian, X. Lu, S. Wu, P. Chu, and Y. Pan, Appl. Phys. Lett. 100, 123702 (2012); [3] X. Pei, X. Lu, J. Liu, D. Liu, Y. Yang, K. Ostrikov, P. Chu, and Y. Pan, J. Phys. D 45, 165205 (2012).

  19. Decomposition of tetrafluoromethane by water plasma generated under atmospheric pressure

    International Nuclear Information System (INIS)

    Narengerile,; Saito, Hironori; Watanabe, Takayuki

    2009-01-01

    Tetrafluoromethane (CF 4 ) decomposition by water plasma generated under atmospheric pressure was investigated by means of thermodynamic analyses and experiments. Thermodynamic equilibrium calculations were performed between 300 and 6000 K at atmospheric pressure. Experimental results indicated that CF 4 was completely decomposed by water plasma, and recovery of fluorine can be achieved more than 99%. Influence of factors such as arc current and additive flow rate of O 2 on CF 4 decomposition was determined. Furthermore, the decomposition mechanism of CF 4 was investigated from chemical kinetics consideration. CF x(x:1-4) was thermally decomposed above 4000 K, oxidized in the temperature range of 4000-2400 K, and removed by H radical at temperatures below 2400 K.

  20. Decomposition of tetrafluoromethane by water plasma generated under atmospheric pressure

    Energy Technology Data Exchange (ETDEWEB)

    Narengerile,; Saito, Hironori [Department of Environmental Chemistry and Engineering, Tokyo Institute of Technology, 4259 Nagatsuta, Yokohama, 226-8502 (Japan); Watanabe, Takayuki, E-mail: watanabe@chemenv.titech.ac.j [Department of Environmental Chemistry and Engineering, Tokyo Institute of Technology, 4259 Nagatsuta, Yokohama, 226-8502 (Japan)

    2009-12-01

    Tetrafluoromethane (CF{sub 4}) decomposition by water plasma generated under atmospheric pressure was investigated by means of thermodynamic analyses and experiments. Thermodynamic equilibrium calculations were performed between 300 and 6000 K at atmospheric pressure. Experimental results indicated that CF{sub 4} was completely decomposed by water plasma, and recovery of fluorine can be achieved more than 99%. Influence of factors such as arc current and additive flow rate of O{sub 2} on CF{sub 4} decomposition was determined. Furthermore, the decomposition mechanism of CF{sub 4} was investigated from chemical kinetics consideration. CF{sub x(x:1-4)} was thermally decomposed above 4000 K, oxidized in the temperature range of 4000-2400 K, and removed by H radical at temperatures below 2400 K.

  1. Surface wave propagation characteristics in atmospheric pressure plasma column

    International Nuclear Information System (INIS)

    Pencheva, M; Benova, E; Zhelyazkov, I

    2007-01-01

    In the typical experiments of surface wave sustained plasma columns at atmospheric pressure the ratio of collision to wave frequency (ν/ω) is much greater than unity. Therefore, one might expect that the usual analysis of the wave dispersion relation, performed under the assumption ν/ω = 0, cannot give adequate description of the wave propagation characteristics. In order to study these characteristics we have analyzed the wave dispersion relationship for arbitrary ν/ω. Our analysis includes phase and wave dispersion curves, attenuation coefficient, and wave phase and group velocities. The numerical results show that a turning back point appears in the phase diagram, after which a region of backward wave propagation exists. The experimentally observed plasma column is only in a region where wave propagation coefficient is higher than the attenuation coefficient. At the plasma column end the electron density is much higher than that corresponding to the turning back point and the resonance

  2. Plasmid DNA damage induced by helium atmospheric pressure plasma jet

    Science.gov (United States)

    Han, Xu; Cantrell, William A.; Escobar, Erika E.; Ptasinska, Sylwia

    2014-03-01

    A helium atmospheric pressure plasma jet (APPJ) is applied to induce damage to aqueous plasmid DNA. The resulting fractions of the DNA conformers, which indicate intact molecules or DNA with single- or double-strand breaks, are determined using agarose gel electrophoresis. The DNA strand breaks increase with a decrease in the distance between the APPJ and DNA samples under two working conditions of the plasma source with different parameters of applied electric pulses. The damage level induced in the plasmid DNA is also enhanced with increased plasma irradiation time. The reactive species generated in the APPJ are characterized by optical emission spectra, and their roles in possible DNA damage processes occurring in an aqueous environment are also discussed.

  3. Simulation of plasma loading of high-pressure RF cavities

    Energy Technology Data Exchange (ETDEWEB)

    Yu, K. [Brookhaven National Lab. (BNL), Upton, NY (United States). Computational Science Initiative; Samulyak, R. [Brookhaven National Lab. (BNL), Upton, NY (United States). Computational Science Initiative; Stony Brook Univ., NY (United States). Dept. of Applied Mathematics and Statistics; Yonehara, K. [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Freemire, B. [Northern Illinois Univ., DeKalb, IL (United States)

    2018-01-11

    Muon beam-induced plasma loading of radio-frequency (RF) cavities filled with high pressure hydrogen gas with 1% dry air dopant has been studied via numerical simulations. The electromagnetic code SPACE, that resolves relevant atomic physics processes, including ionization by the muon beam, electron attachment to dopant molecules, and electron-ion and ion-ion recombination, has been used. Simulations studies have also been performed in the range of parameters typical for practical muon cooling channels.

  4. Simulation of plasma loading of high-pressure RF cavities

    Science.gov (United States)

    Yu, K.; Samulyak, R.; Yonehara, K.; Freemire, B.

    2018-01-01

    Muon beam-induced plasma loading of radio-frequency (RF) cavities filled with high pressure hydrogen gas with 1% dry air dopant has been studied via numerical simulations. The electromagnetic code SPACE, that resolves relevant atomic physics processes, including ionization by the muon beam, electron attachment to dopant molecules, and electron-ion and ion-ion recombination, has been used. Simulations studies have been performed in the range of parameters typical for practical muon cooling channels.

  5. Avalanches driven by pressure gradients in a magnetized plasma

    Science.gov (United States)

    Van Compernolle, B.; Morales, G. J.

    2017-11-01

    The results are presented for a basic heat transport experiment involving an off-axis heat source in which avalanche events occur. The configuration consists of a long, hollow, cylindrical region of elevated electron temperature embedded in a colder plasma, and far from the device walls [Van Compernolle et al. Phys. Rev. E 91, 031102(R) (2015)]. The avalanche events are identified as sudden rearrangements of the pressure profile following the growth of fluctuations from ambient noise. The intermittent collapses of the plasma pressure profile are associated with unstable drift-Alfvén waves and exhibit both radial and poloidal dynamics. After each collapse, the plasma enters a quiescent phase in which the pressure profile slowly recovers and steepens until a threshold is exceeded, and the process repeats. The use of reference probes as time markers allows for the visualization of the 2D spatio-temporal evolution of the avalanche events. Avalanches are observed only for a limited combination of heating powers and magnetic fields. At higher heating powers, the system transits from the avalanche regime into a regime dominated by sustained drift-Alfvén wave activity. This manuscript focuses on new results that illustrate the individual contributions to the avalanche process from density and temperature gradients in the presence of zero-order, sheared flows.

  6. Plasma pressure in the discharge column of the Novillo Tokamak

    International Nuclear Information System (INIS)

    Gaytan G, E.

    1995-01-01

    The design and construction of an acquisition system for the measurement of the plasma pressure in the Novillo Tokamak is described in detail. The system includes a high voltage ramp generator, a hardware and a software interface with a personal computer. It is used to determine experimentally the variations of the pressure in the plasma column in the cleaning and main discharges. The measurement of the pressure is made with a Pirani sensor adapted to the acquisition hardware and synchronized with the discharge in the plasma. The software is made in object oriented programming as a graphic interface designed to be used easily. It controls the acquisition, records the data, displays in graphic form the results and save the measurements. The graphic interface is a building block that can be used in different acquisition tasks. The ramp generator can deliver a signal of 200 V peak to peak with a current of 200 m A and offset control. The acquisition time is 2.5 μ s for every measurement, 8192 measurements can be stored in the acquisition board for every discharge. (Author)

  7. Theory and simulation of anode spots in low pressure plasmas

    Science.gov (United States)

    Scheiner, Brett; Barnat, Edward V.; Baalrud, Scott D.; Hopkins, Matthew M.; Yee, Benjamin T.

    2017-11-01

    When electrodes are biased above the plasma potential, electrons accelerated through the associated electron sheath can dramatically increase the ionization rate of neutrals near the electrode surface. It has previously been observed that if the ionization rate is great enough, a double layer separates a luminous high-potential plasma attached to the electrode surface (called an anode spot or fireball) from the bulk plasma. Here, results of the first 2D particle-in-cell simulations of anode spot formation are presented along with a theoretical model describing the formation process. It is found that ionization leads to the build-up of an ion-rich layer adjacent to the electrode, forming a narrow potential well near the electrode surface that traps electrons born from ionization. It is shown that anode spot onset occurs when a quasineutral region is established in the potential well and the density in this region becomes large enough to violate the steady-state Langmuir condition, which is a balance between electron and ion fluxes across the double layer. A model for steady-state properties of the anode spot is also presented, which predicts values for the anode spot size, double layer potential drop, and form of the sheath at the electrode by considering particle, power, and current balance. These predictions are found to be consistent with the presented simulation and previous experiments.

  8. Crystallization of Pd40CU30Ni10P20 bulk metallic glass with and without pressure

    DEFF Research Database (Denmark)

    Yang, B.; Jiang, Jianzhong; Zhuang, Yanxin

    2007-01-01

    The glass-transition behavior of Pd40Cu30Ni10P20 bulk metallic glass was investigated by differential scanning calorimetry (DSC) and X-ray powder diffraction (XRD). The effect of pressure on the crystallization behavior of Pd40Cu30Ni10P20 bulk glass was studied by in situ high-pressure and high......-temperature X-ray powder diffraction using synchrotron radiation. Phase analyses show at least six crystalline phases in the crystallized sample, namely, monoclinic, tetragonal Cu3Pd-like, rhombohedral, fcc-Ni2Pd2P, fcc-(Ni, Pd) solid solution, and body-centered tetragonal (bct) Ni3P-like phases. The onset...

  9. Atmospheric pressure plasma accelerates tail regeneration in tadpoles Xenopus laevis

    Science.gov (United States)

    Rivie, A.; Martus, K.; Menon, J.

    2017-08-01

    Atmospheric pressure plasma is a partially ionized gas composed of neutral and charged particles, including electrons and ions, as well as reactive oxygen species (ROS). Recently, it is utilized as possible therapy in oncology, sterilization, skin diseases, wound healing and tissue regeneration. In this study we focused on effect of plasma exposure on tail regeneration of tadpoles, Xenopus leavis with special emphasis on role of ROS, antioxidant defenses and morphological features of the regenerate. When amputated region of the tail was exposed to the helium plasma it resulted in a faster rate of growth, elevated ROS and increase in antioxidant enzymes in the regenerate compared to that of untreated control. An increase in nitric oxide (free radical) as well as activity of nitric oxide synthase(s) were observed once the cells of the regeneration blastema - a mass of proliferating cells are ready for differentiation. Microscopically the cells of the regenerate of plasma treated tadpoles show altered morphology and characteristics of cellular hypoxia and oxidative stress. We summarize that plasma exposure accelerates the dynamics of wound healing and tail regeneration through its effects on cell proliferation and differentiation as well as angiogenesis mediated through ROS signaling.

  10. Non-equilibrium synergistic effects in atmospheric pressure plasmas.

    Science.gov (United States)

    Guo, Heng; Zhang, Xiao-Ning; Chen, Jian; Li, He-Ping; Ostrikov, Kostya Ken

    2018-03-19

    Non-equilibrium is one of the important features of an atmospheric gas discharge plasma. It involves complicated physical-chemical processes and plays a key role in various actual plasma processing. In this report, a novel complete non-equilibrium model is developed to reveal the non-equilibrium synergistic effects for the atmospheric-pressure low-temperature plasmas (AP-LTPs). It combines a thermal-chemical non-equilibrium fluid model for the quasi-neutral plasma region and a simplified sheath model for the electrode sheath region. The free-burning argon arc is selected as a model system because both the electrical-thermal-chemical equilibrium and non-equilibrium regions are involved simultaneously in this arc plasma system. The modeling results indicate for the first time that it is the strong and synergistic interactions among the mass, momentum and energy transfer processes that determine the self-consistent non-equilibrium characteristics of the AP-LTPs. An energy transfer process related to the non-uniform spatial distributions of the electron-to-heavy-particle temperature ratio has also been discovered for the first time. It has a significant influence for self-consistently predicting the transition region between the "hot" and "cold" equilibrium regions of an AP-LTP system. The modeling results would provide an instructive guidance for predicting and possibly controlling the non-equilibrium particle-energy transportation process in various AP-LTPs in future.

  11. Correlation between helium atmospheric pressure plasma jet (APPJ) variables and plasma induced DNA damage

    Science.gov (United States)

    Adhikari, Ek R.; Ptasinska, Sylwia

    2016-09-01

    A helium atmospheric pressure plasma jet (APPJ) source with a dielectric capillary and two tubular electrodes was used to induce damage in aqueous plasmid DNA. The fraction of different types of DNA damage (i.e., intact or undamaged, double strand breaks (DSBs), and single strand breaks (SSBs)) that occurred as the result of plasma irradiation was quantified through analysis of agarose gel electrophoresis images. The total DNA damage increased with an increase in both flow rate and duration of irradiation, but decreased with an increase in distance between the APPJ and sample. The average power of the plasma was calculated and the length of APPJ was measured for various flow rates and voltages applied. The possible effects of plasma power and reactive species on DNA damage are discussed.

  12. Sterilization of Surfaces with a Handheld Atmospheric Pressure Plasma

    Science.gov (United States)

    Hicks, Robert; Habib, Sara; Chan, Wai; Gonzalez, Eleazar; Tijerina, A.; Sloan, Mark

    2009-10-01

    Low temperature, atmospheric pressure plasmas have shown great promise for decontaminating the surfaces of materials and equipment. In this study, an atmospheric pressure, oxygen and argon plasma was investigated for the destruction of viruses, bacteria, and spores. The plasma was operated at an argon flow rate of 30 L/min, an oxygen flow rate of 20 mL/min, a power density of 101.0 W/cm^3 (beam area = 5.1 cm^2), and at a distance from the surface of 7.1 mm. An average 6log10 reduction of viable spores was obtained after only 45 seconds of exposure to the reactive gas. By contrast, it takes more than 35 minutes at 121^oC to sterilize anthrax in an autoclave. The plasma properties were investigated by numerical modeling and chemical titration with nitric oxide. The numerical model included a detailed reaction mechanism for the discharge as well as for the afterglow. It was predicted that at a delivered power density of 29.3 W/cm^3, 30 L/min argon, and 0.01 volume% O2, the plasma generated 1.9 x 10^14 cm-3 O atoms, 1.6 x 10^12 cm-3 ozone, 9.3 x 10^13 cm-3 O2(^1δg), and 2.9 x 10^12 cm-3 O2(^1σ^+g) at 1 cm downstream of the source. The O atom density measured by chemical titration with NO was 6.0 x 10^14 cm-3 at the same conditions. It is believe that the oxygen atoms and the O2(^1δg) metastables were responsible for killing the anthrax and other microorganisms.

  13. Pressure-induced switching in ferroelectrics: Phase-field modeling, electrochemistry, flexoelectric effect, and bulk vacancy dynamics

    Science.gov (United States)

    Cao, Ye; Morozovska, Anna; Kalinin, Sergei V.

    2017-11-01

    Pressure-induced polarization switching in ferroelectric thin films has emerged as a powerful method for domain patterning, allowing us to create predefined domain patterns on free surfaces and under thin conductive top electrodes. However, the mechanisms for pressure-induced polarization switching in ferroelectrics remain highly controversial, with flexoelectricity, polarization rotation and suppression, and bulk and surface electrochemical processes all being potentially relevant. Here we classify possible pressure-induced switching mechanisms, perform elementary estimates, and study in depth using phase-field modeling. We show that magnitudes of these effects are remarkably close and give rise to complex switching diagrams as a function of pressure and film thickness with nontrivial topology or switchable and nonswitchable regions.

  14. Bulk and shear viscosities of the gluon plasma in a quasiparticle description

    CERN Document Server

    Bluhm, M; Redlich, K

    2011-01-01

    Bulk and shear viscosities of deconfined gluonic matter are investigated within an effective kinetic theory by describing the strongly interacting medium phenomenologically in terms of quasiparticle excitations with medium-dependent self-energies. In this approach, local conservation of energy and momentum follows from a Boltzmann-Vlasov type kinetic equation and guarantees thermodynamic self-consistency. We show that the resulting transport coefficients reproduce the parametric dependencies on temperature and coupling obtained in perturbative QCD at large temperatures and small running coupling. The extrapolation into the non-perturbative regime results in a decreasing specific shear viscosity with decreasing temperature, exhibiting a minimum in the vicinity of the deconfinement transition temperature, while the specific bulk viscosity is sizeable in this region falling off rapidly with increasing temperature. The temperature dependence of specific bulk and shear viscosities found within this quasiparticle d...

  15. Atmospheric-pressure plasma decontamination/sterilization chamber

    Science.gov (United States)

    Herrmann, Hans W.; Selwyn, Gary S.

    2001-01-01

    An atmospheric-pressure plasma decontamination/sterilization chamber is described. The apparatus is useful for decontaminating sensitive equipment and materials, such as electronics, optics and national treasures, which have been contaminated with chemical and/or biological warfare agents, such as anthrax, mustard blistering agent, VX nerve gas, and the like. There is currently no acceptable procedure for decontaminating such equipment. The apparatus may also be used for sterilization in the medical and food industries. Items to be decontaminated or sterilized are supported inside the chamber. Reactive gases containing atomic and metastable oxygen species are generated by an atmospheric-pressure plasma discharge in a He/O.sub.2 mixture and directed into the region of these items resulting in chemical reaction between the reactive species and organic substances. This reaction typically kills and/or neutralizes the contamination without damaging most equipment and materials. The plasma gases are recirculated through a closed-loop system to minimize the loss of helium and the possibility of escape of aerosolized harmful substances.

  16. Development of atmospheric pressure plasma needle jet for sterilization applications

    Science.gov (United States)

    Elfa, Rizan Rizon; Ahmad, Mohd Khairul; Soon, Chin Fhong; Sahdan, Mohd Zainizan; Lias, Jais; Wibowo, Kusnanto Mukti; Bakar, Ahmad Shuhaimi Abu; Arshad, Mohd Khairuddin Md; Hashim, Uda; Nayan, Nafarizal

    2017-09-01

    Inactivation of bacteria or sterilization has been a major issue in the medical field, especially regarding of human safety, whereby, in a huge scenario fatality can be caused by hazardous bacteria. Often, E-coli as gram-negative bacteria are selected as a key indicator of proper sterilization process as E-coli is tough and dormant bacteria. The technology in sterilization has moved on from chemical, wet and irradiation sterilization to a high promising device such as atmospheric pressure plasma needle jet (APPNJ). It has been reported that atmospheric pressure plasma has provided bundle of advantages over earlier sterilization process. The APPNJ is developed in our lab using high frequency and high voltage neon transformer power supply connected to copper needle and copper sheet electrodes. The gas discharge is Ar gas flowing at 40 L/min through a quartz glass tube. The E-coli bacteria are self-cultured from waste water and then treated with APPNJ. The treatment processes are run into two difference gaps between the plasma orifice and sample with various treatment times. Only 40s is required by direct treatment to achieve 100% killing of E-coli. On the other hand, indirect treatment has inactivated 50% of the E-coli in 40s. In this study, direct and indirect effect of APPNJ to the E-coli can be observed which can be utilized into sterilization of bio-compatible material applications.

  17. Room-temperature atmospheric pressure plasma plume for biomedical applications

    International Nuclear Information System (INIS)

    Laroussi, M.; Lu, X.

    2005-01-01

    As low-temperature nonequilibrium plasmas come to play an increasing role in biomedical applications, reliable and user-friendly sources need to be developed. These plasma sources have to meet stringent requirements such as low temperature (at or near room temperature), no risk of arcing, operation at atmospheric pressure, preferably hand-held operation, low concentration of ozone generation, etc. In this letter, we present a device that meets exactly such requirements. This device is capable of generating a cold plasma plume several centimeters in length. It exhibits low power requirements as shown by its current-voltage characteristics. Using helium as a carrier gas, very little ozone is generated and the gas temperature, as measured by emission spectroscopy, remains at room temperature even after hours of operations. The plasma plume can be touched by bare hands and can be directed manually by a user to come in contact with delicate objects and materials including skin and dental gum without causing any heating or painful sensation

  18. Helium atmospheric pressure plasma jets touching dielectric and metal surfaces

    Science.gov (United States)

    Norberg, Seth A.; Johnsen, Eric; Kushner, Mark J.

    2015-07-01

    Atmospheric pressure plasma jets (APPJs) are being investigated in the context plasma medicine and biotechnology applications, and surface functionalization. The composition of the surface being treated ranges from plastics, liquids, and biological tissue, to metals. The dielectric constant of these materials ranges from as low as 1.5 for plastics to near 80 for liquids, and essentially infinite for metals. The electrical properties of the surface are not independent variables as the permittivity of the material being treated has an effect on the dynamics of the incident APPJ. In this paper, results are discussed from a computational investigation of the interaction of an APPJ incident onto materials of varying permittivity, and their impact on the discharge dynamics of the plasma jet. The computer model used in this investigation solves Poisson's equation, transport equations for charged and neutral species, the electron energy equation, and the Navier-Stokes equations for the neutral gas flow. The APPJ is sustained in He/O2 = 99.8/0.2 flowing into humid air, and is directed onto dielectric surfaces in contact with ground with dielectric constants ranging from 2 to 80, and a grounded metal surface. Low values of relative permittivity encourage propagation of the electric field into the treated material and formation and propagation of a surface ionization wave. High values of relative permittivity promote the restrike of the ionization wave and the formation of a conduction channel between the plasma discharge and the treated surface. The distribution of space charge surrounding the APPJ is discussed.

  19. Low-pressure rf plasmas: a versatile nitriding environment

    International Nuclear Information System (INIS)

    Priest, J.; Fewell, M.; Baldwin, M.

    1999-01-01

    Plasma nitriding is currently a widely used industrial process for increasing the surface hardness and load bearing capacity of steels. Commercial processes involve the use of an abnormal glow discharge with the workpiece as the cathode in nitrogen-hydrogen atmospheres at pressures between 10 to 1000 pa. The workpiece is heated during treatment, often entirely by energetic ion bombardment, to high temperatures, typically 500-560 deg C. Low-alloy and tool steels can be effectively treated in this way, but there are a range of steels, such as the austenitic grades of stainless steel, for which these process temperatures are too high. Although significant increases in the surface hardness are obtained, precipitation of CrN, which occurs at temperatures above 400 deg C, gives rise to a loss in the corrosion resistance. An advantage of low-pressure rf plasma nitriding lies in the straightforward control of process parameters such as treatment temperature and workpiece bias. The ion and neutral fluxes are generally lower than those at higher pressures so the process temperature can be kept low. Previously, we have explored this nitriding environment for the treatment of the austenitic grade of stainless steel AISI 316 for a wide range of process parameters using a treatment temperature of 400 deg C. In these investigations, a heated sample table was used, but this method of heating is not suitable for the treatment of large-scale or irregular shaped components, which are more suitably treated in a furnace environment. In this paper, we report on our recent efforts in scaling low-pressure rf plasma nitriding towards commercial exploitation through the development of a nest hot-wall nitriding reactor with features based on the design of an industrial heat-treatment furnace. Plasma-immersion ion implantation (PI 3 ), in which the workpiece is biased to high-voltage (20-50 kV), can also be conducted in this reactor. In the present work though, we deal with a negative bias

  20. Atmospheric pressure plasma treatment of glassy carbon for adhesion improvement

    DEFF Research Database (Denmark)

    Kusano, Yukihiro; Mortensen, Henrik Junge; Stenum, Bjarne

    2007-01-01

    Glassy carbon plates were treated with an atmospheric pressure dielectric barrier discharge (DBD). He gas, gas mixtures of He and reactive gases such as O2, CO2 and NH3, Ar gas and Ar/NH3 gas mixture were used as treatment gases. The oxygen and nitrogen contents on the surface as well as defect...... density increased with the plasma treatments. Adhesion test of the treated glassy carbon covered with cured epoxy showed cohesive failure, indicating strong bonding after the treatments. This is in contrast to the adhesion tests of untreated samples where the epoxy readily peeled off the glassy carbon....

  1. Study of pressure-volume relationships and higher derivatives of bulk modulus based on generalized equations of state

    International Nuclear Information System (INIS)

    Kushwah, S.S.; Shrivastava, H.C.; Singh, K.S.

    2007-01-01

    We have generalized the pressure-volume (P-V) relationships using simple polynomial and logarithmic expansions so as to make them consistent with the infinite pressure extrapolation according to the model of Stacey. The formulations are used to evaluate P-V relationships and pressure derivatives of bulk modulus upto third order (K', K'' and K''') for the earth core material taking input parameters based on the seismological data. The results based on the equations of state (EOS) generalized in the present study are found to yield good agreement with the Stacey EOS. The generalized logarithmic EOS due to Poirier and Tarantola deviates substantially from the seismic values for P, K and K'. The generalized Rydberg EOS gives almost identical results with the Birch-Murnaghan third-order EOS. Both of them yield deviations from the seismic data, which are in opposite direction as compared to those found from the generalized Poirier-Tarantola logarithmic EOS

  2. Bulk rock elastic moduli at high pressures, derived from the mineral textures and from extrapolated laboratory data

    International Nuclear Information System (INIS)

    Ullemeyer, K; Keppler, R; Lokajíček, T; Vasin, R N; Behrmann, J H

    2015-01-01

    The elastic anisotropy of bulk rock depends on the mineral textures, the crack fabric and external parameters like, e.g., confining pressure. The texture-related contribution to elastic anisotropy can be predicted from the mineral textures, the largely sample-dependent contribution of the other parameters must be determined experimentally. Laboratory measurements of the elastic wave velocities are mostly limited to pressures of the intermediate crust. We describe a method, how the elastic wave velocity trends and, by this means, the elastic constants can be extrapolated to the pressure conditions of the lower crust. The extrapolated elastic constants are compared to the texture-derived ones. Pronounced elastic anisotropy is evident for phyllosilicate minerals, hence, the approach is demonstrated for two phyllosilicate-rich gneisses with approximately identical volume fractions of the phyllosilicates but different texture types. (paper)

  3. Composites of amorphous and nanocrystalline Zr–Cu–Al–Nb bulk materials synthesized by spark plasma sintering

    Energy Technology Data Exchange (ETDEWEB)

    Drescher, P., E-mail: philipp.drescher@uni-rostock.de [Fluidic Technology and Microfluidics, Faculty of Mechanical Engineering and Marine Technology, University of Rostock, 18059 Rostock (Germany); Witte, K. [Physics of New Materials, Institute of Physics, University of Rostock, 18051 Rostock (Germany); Yang, B. [Polymer Physics, Institute of Physics, University of Rostock, 18051 Rostock (Germany); Steuer, R.; Kessler, O. [Chair of Materials Science, Faculty of Mechanical Engineering and Marine Technology, University of Rostock, 18059 Rostock (Germany); Burkel, E. [Physics of New Materials, Institute of Physics, University of Rostock, 18051 Rostock (Germany); Schick, C. [Polymer Physics, Institute of Physics, University of Rostock, 18051 Rostock (Germany); Seitz, H. [Fluidic Technology and Microfluidics, Faculty of Mechanical Engineering and Marine Technology, University of Rostock, 18059 Rostock (Germany)

    2016-05-15

    The fabrication of Zr{sub 70}Cu{sub 24}Al{sub 4}Nb{sub 2} bulk metallic glass composite samples by spark plasma sintering (SPS) process has been successfully realized. The unique characteristics of bulk metallic glasses could lead to the possibility of future applications as new structural and functional materials. The densification of an amorphous Zr{sub 70}Cu{sub 24}Al{sub 4}Nb{sub 2} powder was realized in a systematic study changing the sintering temperature in the SPS process leading to stable composites characteristic of amorphous and nanocrystalline structures. X-ray diffractometry (XRD) and differential scanning calorimetry (DSC) analysis, transmission electron microscopy (TEM) as well as hardness tests were applied to determine the structural and mechanical properties of the sintered materials. A stable amorphous bulk metallic glass based on Zr{sub 70}Cu{sub 24}Al{sub 4}Nb{sub 2} with a low fraction of crystallites could be fabricated applying a nominal sintering temperature of 400 °C. Higher sintering temperatures lead to composites with high fractions of nanocrystalline material with porosities below 0.5%.

  4. Development of dispersion interferometer for magnetic confinement plasmas and high-pressure plasmas

    Science.gov (United States)

    Akiyama, T.; Yasuhara, R.; Kawahata, K.; Nakayama, K.; Okajima, S.; Urabe, K.; Terashima, K.; Shirai, N.

    2015-09-01

    A CO2 laser dispersion interferometer (DI) has been developed for both magnetically fusion plasmas and high pressure industrial plasmas. The DI measures the phase shift caused by dispersion in a medium. Therefore, it is insensitive to the mechanical vibrations and changes in the neutral gas density, which degrade the resolution of the electron density measurement. We installed the DI on the Large Helical Device (LHD) and demonstrated a high density resolution of 2× 1017 m-3 without any vibration-free bench. The measured electron density with the DI shows good agreement with results of the existing far infrared laser (a wavelength of 119 μ m) interferometer. The DI system is also applied to the electron density measurement of high-pressure small-scale plasmas. The significant suppression of the phase shift caused by the neutral gas is proven. The achieved density resolution was 1.5× 1019 m-3 with a response time of 100 μ s. A shorter version of this contribution is due to be published in PoS at: 1st EPS conference on Plasma Diagnostics

  5. One-dimensional electromagnetic band gap plasma structure formed by atmospheric pressure plasma inhomogeneities

    Science.gov (United States)

    Babitski, V. S.; Callegari, Th.; Simonchik, L. V.; Sokoloff, J.; Usachonak, M. S.

    2017-08-01

    The ability to use plasma columns of pulse discharges in argon at atmospheric pressure to form a one-dimensional electromagnetic band gap structure (or electromagnetic crystal) in the X-band waveguide is demonstrated. We show that a plasma electromagnetic crystal attenuates a microwave propagation in the stopband more than by 4 orders of magnitude. In order to obtain an effective control of the transmission spectrum comparable with a metallic regular structure, the electron concentration in plasma inhomogeneities should vary within the range from 1014 cm-3 to 1016 cm-3, while gas temperature and mean electron energy must be in the range of 2000 K and 0.5 eV, respectively, to lower electron collision frequency around 1010 s-1. We analyze in detail the time evolution response of the electromagnetic crystal according to the plasma parameters for the duration of the discharge. The interest of using atmospheric pressure discharges is to increase the microwave breakdown threshold in discharge volumes, whereby it becomes possible to perform dynamic control of high power microwaves.

  6. Electrical studies and plasma characterization of an atmospheric pressure plasma jet operated at low frequency

    International Nuclear Information System (INIS)

    Giuliani, L.; Xaubet, M.; Grondona, D.; Minotti, F.; Kelly, H.

    2013-01-01

    Low-temperature, high-pressure plasma jets have an extensive use in medical and biological applications. Much work has been devoted to study these applications while comparatively fewer studies appear to be directed to the discharge itself. In this work, in order to better understand the kind of electrical discharge and the plasma states existing in those devices, a study of the electrical characteristics of a typical plasma jet, operated at atmospheric pressure, using either air or argon, is reported. It is found that the experimentally determined electrical characteristics are consistent with the model of a thermal arc discharge, with a highly collisional cathode sheet. The only exception is the case of argon at the smallest electrode separation studied, around 1 mm in which case the discharge is better modeled as either a non-thermal arc or a high-pressure glow. Also, variations of the electrical behavior at different gas flow rates are interpreted, consistently with the arc model, in terms of the development of fluid turbulence in the external jet

  7. Evaluation of Low-Pressure Cold Plasma for Disinfection of ISS Grown Produce and Metal Instruments

    Science.gov (United States)

    Hummerick, Mary E.; Hintze, Paul E.; Maloney, Philip R.; Spencer, Lashelle E.; Coutts, Janelle L.; Franco, Carolina

    2016-01-01

    Low pressure cold plasma, using breathing air as the plasma gas, has been shown to be effective at precision cleaning aerospace hardware at Kennedy Space Center.Both atmospheric and low pressure plasmas are relatively new technologies being investigated for disinfecting agricultural commodities and medical instruments.

  8. Thermal plasma synthesis of coated iron cobalt-iron cobalt vanadium nanoparticles as precursors for compacted nanocrystalline bulk magnets

    Science.gov (United States)

    Turgut, Zafer

    2000-12-01

    High temperature power applications such as starter and generator components of the aircraft engines require soft magnetic materials with optimum magnetic properties. Thus creep resistance and yield strength become important material properties due to the high temperatures and high rotational forces. FeCo based alloys are the only material that can meet desired magnetic properties but they exhibit poor creep resistance at temperatures up to 775 K. Eddy current losses, which are strong dependent on the materials' volume resistivity, are also one of the main concerns designing the aforementioned devices. Current technology utilizes stacks of ˜150 mum thick FeCo alloy laminates and limitations on dimensions arising from the eddy currents and skin depth issues. It is a well known fact that any improvement in mechanical properties through a secondary phase hardening will result in poor magnetic properties due to the domain wall pinning effect of the secondary phase. Engineering of fiber re-enforced structures to improve the mechanical properties also is not feasible due to the dimensions of the material. This indicates that any improvement on mechanical properties will interfere with the magnetic performance of the system. Coated nanoparticles eventually compacted in a bulk form, may offer a solution to poor mechanical properties thus magnetic properties can be further improved, i.e. lower coercivities and higher permeabilities, by tailoring the grain sizes to be smaller than the magnetic exchange length, Lex . Presence of a highly resistive coating phase can also reduce the eddy current losses and ease the limitations on the materials thickness. Oxide and carbon coated FeCo and FeCoV nanoparticles were synthesized through thermal plasma processing as precursors for the compacted bulk magnets. Their densification characteristics as well as the magnetic, structural and microstructural properties were studied before and after compaction. A hot isostatic pressing (HIP

  9. Contact angle analysis of low-temperature cyclonic atmospheric pressure plasma modified polyethylene terephthalate

    International Nuclear Information System (INIS)

    Huang, Chun; Chang, Ya-Chi; Wu, Shin-Yi

    2010-01-01

    Polyethylene terephthalate (PET) films are modified by cyclonic atmospheric pressure plasma. The experimentally measured gas phase temperature was around 30 o C to 90 o C, indicating that this cyclonic atmospheric pressure plasma can treat polymers without unfavorable thermal effects. The surface properties of cyclonic atmospheric pressure plasma-treated PET films were examined by the static contact angle measurements. The influences of plasma conditions such as treatment time, plasma power, nozzle distance, and gas flow rate on the PET surface properties were studied. It was found that such cyclonic atmospheric pressure plasma is very effective in PET surface modification, the reduced water contact angle was observed from 74 o to less than 37 o with only 10 s plasma treatment. The chemical composition of the PET films was analyzed by X-ray photoelectron spectroscopy (XPS). Atomic force microscopy (AFM) was used to study the changes in PET surface feature of the polymer surfaces due to plasma treatment. The photoemission plasma species in the continuous cyclone atmospheric pressure plasma was identified by optical emission spectroscopy (OES). From OES analysis, the plasma modification efficiency can be attributed to the interaction of oxygen-based plasma species in the plasma with PET surface. In this study, it shows a novel way for large scale polymeric surface modification by continuous cyclone atmospheric pressure plasma processing.

  10. Destruction of Bacillus subtilis cells using an atmospheric-pressure dielectric capillary electrode discharge plasma

    International Nuclear Information System (INIS)

    Panikov, N.S.; Paduraru, S.; Crowe, R.; Ricatto, P.J.; Christodoulatos, C.; Becker, K.

    2002-01-01

    The results of experiments aimed at the investigation of the destruction of spore-forming bacteria, which are believed to be among the most resistant microorganisms, using a novel atmospheric-pressure dielectric capillary electrode discharge plasma are reported. Various well-characterized cultures of Bacillus subtilis were prepared, subjected to atmospheric-pressure plasma jets emanating from a plasma shower reactor operated either in He or in air (N 2 /O 2 mixture) at various power levels and exposure times, and analyzed after plasma treatment. Reductions in colony-forming units ranged from 10 4 (He plasma) to 10 8 (air plasma) for plasma exposure times of less than 10 minutes. (author)

  11. Use of Atmospheric-Pressure Plasma Jet for Polymer Surface Modification: An Overview

    Energy Technology Data Exchange (ETDEWEB)

    Kuettner, Lindsey A. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-03-16

    Atmospheric-pressure plasma jets (APPJs) are playing an increasingly important role in materials processing procedures. Plasma treatment is a useful tool to modify surface properties of materials, especially polymers. Plasma reacts with polymer surfaces in numerous ways thus the type of process gas and plasma conditions must be explored for chosen substrates and materials to maximize desired properties. This report discusses plasma treatments and looks further into atmospheric-pressure plasma jets and the effects of gases and plasma conditions. Following the short literature review, a general overview of the future work and research at Los Alamos National Laboratory (LANL) is discussed.

  12. Surface chemical changes of atmospheric pressure plasma treated rabbit fibres important for felting process

    International Nuclear Information System (INIS)

    Štěpánová, Vlasta; Slavíček, Pavel; Stupavská, Monika; Jurmanová, Jana; Černák, Mirko

    2015-01-01

    Graphical abstract: - Highlights: • Rabbit fibres plasma treatment is an effective method for fibres modification. • Atmospheric pressure plasma treatment is able to affect fibres properties. • Surface changes on fibres after plasma treatment were analysed via SEM, ATR-FTIR, XPS. • Significant increase of fibres wettability after plasma treatment was observed. • Plasma treatment at atmospheric pressure can replace the chemical treatment of fibres. - Abstract: We introduce the atmospheric pressure plasma treatment as a suitable procedure for in-line industrial application of rabbit fibres pre-treatment. Changes of rabbit fibre properties due to the plasma treatment were studied in order to develop new technology of plasma-based treatment before felting. Diffuse Coplanar Surface Barrier Discharge (DCSBD) in ambient air at atmospheric pressure was used for plasma treatment. Scanning electron microscopy was used for determination of the fibres morphology before and after plasma treatment. X-ray photoelectron spectroscopy and attenuated total reflectance-Fourier transform infrared spectroscopy were used for evaluation of reactive groups. The concentration of carbon decreased and conversely the concentration of nitrogen and oxygen increased after plasma treatment. Aging effect of plasma treated fibres was also investigated. Using Washburn method the significant increase of fibres wettability was observed after plasma treatment. New approach of pre-treatment of fibres before felting using plasma was developed. Plasma treatment of fibres at atmospheric pressure can replace the chemical method which consists of application of strong acids on fibres.

  13. Surface chemical changes of atmospheric pressure plasma treated rabbit fibres important for felting process

    Energy Technology Data Exchange (ETDEWEB)

    Štěpánová, Vlasta, E-mail: vstepanova@mail.muni.cz [Department of Physical Electronics, Faculty of Science Masaryk University, Kotlářská 2, 611 37 Brno (Czech Republic); Slavíček, Pavel; Stupavská, Monika; Jurmanová, Jana [Department of Physical Electronics, Faculty of Science Masaryk University, Kotlářská 2, 611 37 Brno (Czech Republic); Černák, Mirko [Department of Physical Electronics, Faculty of Science Masaryk University, Kotlářská 2, 611 37 Brno (Czech Republic); Department of Experimental Physics, Faculty of Mathematics, Physics and Informatics, Comenius University, Mlynská dolina F2, 842 48 Bratislava (Slovakia)

    2015-11-15

    Graphical abstract: - Highlights: • Rabbit fibres plasma treatment is an effective method for fibres modification. • Atmospheric pressure plasma treatment is able to affect fibres properties. • Surface changes on fibres after plasma treatment were analysed via SEM, ATR-FTIR, XPS. • Significant increase of fibres wettability after plasma treatment was observed. • Plasma treatment at atmospheric pressure can replace the chemical treatment of fibres. - Abstract: We introduce the atmospheric pressure plasma treatment as a suitable procedure for in-line industrial application of rabbit fibres pre-treatment. Changes of rabbit fibre properties due to the plasma treatment were studied in order to develop new technology of plasma-based treatment before felting. Diffuse Coplanar Surface Barrier Discharge (DCSBD) in ambient air at atmospheric pressure was used for plasma treatment. Scanning electron microscopy was used for determination of the fibres morphology before and after plasma treatment. X-ray photoelectron spectroscopy and attenuated total reflectance-Fourier transform infrared spectroscopy were used for evaluation of reactive groups. The concentration of carbon decreased and conversely the concentration of nitrogen and oxygen increased after plasma treatment. Aging effect of plasma treated fibres was also investigated. Using Washburn method the significant increase of fibres wettability was observed after plasma treatment. New approach of pre-treatment of fibres before felting using plasma was developed. Plasma treatment of fibres at atmospheric pressure can replace the chemical method which consists of application of strong acids on fibres.

  14. The structural properties of Zr-based bulk metallic glasses subjected to high pressure torsion at different temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Boltynjuk, E. V., E-mail: boltynjuk@gmail.com; Ubyivovk, E. V.; Kshumanev, A. M. [Saint Petersburg State University, 28 Universitetskiy pr., Saint Petersburg, 198504 (Russian Federation); Gunderov, D. V.; Lukianov, A. V. [Ufa State Aviation Technical University, K. Marks 12, Ufa, 450000 (Russian Federation); Bednarz, A. [Faculty of Mechanical Engineering and Aeronautics, Department of Aircraft and Aircraft Engines, Rzeszow University of Technology, Al. Powstancow Warszawy 8, 35-959 Rzeszow (Poland); Valiev, R. Z. [Saint Petersburg State University, 28 Universitetskiy pr., Saint Petersburg, 198504 (Russian Federation); Ufa State Aviation Technical University, K. Marks 12, Ufa, 450000 (Russian Federation)

    2016-06-17

    The structural properties of a Zr{sub 62}Cu{sub 22}Al{sub 10}Fe{sub 5}Dy{sub 1} bulk metallic glasses were investigated. Cylindrical rods of the Zr{sub 62}Cu{sub 22}Al{sub 10}Fe{sub 5}Dy{sub 1} BMG were subjected to high pressure torsion at temperatures of 20°C and 150°C. X-ray diffraction, transmission electron microscopy were used to determine peculiarities of the modified structure. Analysis of fracture surfaces, nanohardness measurements were conducted to investigate the influence of structural changes on mechanical behavior of processed samples.

  15. Atmospheric Pressure Plasma Jet as an Accelerator of Tooth Bleaching.

    Science.gov (United States)

    Santak, Vedran; Zaplotnik, Rok; Milosevic, Slobodan; Klaric, Eva; Tarle, Zrinka

    2014-12-01

    To study the effect of atmospheric pressure plasma (APP) jet as a potential accelerator of the degradation of hydrogen peroxide in bleaching gels which could lead to better and faster bleaching. 25 pastilles of hydroxylapatite were colored in green tea for 8 hours and were randomly divided into five groups (n = 5). The bleaching process was performed with 30% and 40% hydrogen peroxide (HP) gel alone and in conjunction with helium APP jet. During the bleaching treatment, optical emission spectroscopy and non-contact surface temperature measurement using pyrometer were performed. Color of the pastilles was determined by a red-green-blue (RGB) colorimeter. PH values of bleaching gels were measured before and after the plasma treatment on additional 10 pastilles using a pH meter with contact pH electrode. The color measurements of pastilles before and after the treatment showed that treatment with APP jet improved the bleaching effect by 32% and 15% in the case of 30% and 40% HP gel. Better results were obtained approximately six times faster than with a procedure suggested by the bleaching gel manufacturer. Optical emission spectroscopy proved that plasma has a chemically active role on the gel. After the APP treatment, pH values of bleaching gels dropped to about 50-75% of their initial value while the surface temperature increased by 8-10˚C above baseline. The use of plasma jet provides more effective bleaching results in a shorter period of time without a significant temperature increase which may cause damage of the surrounding tissue.

  16. Ambulatory pulmonary arterial pressure in primary pulmonary hypertension: variability, relation to systemic arterial pressure, and plasma catecholamines.

    OpenAIRE

    Richards, A M; Ikram, H; Crozier, I G; Nicholls, M G; Jans, S

    1990-01-01

    The variability of pulmonary arterial pressure, the relation of pulmonary pressure to systemic pressure, pulmonary pressure responses to stimuli (exercise, hypoxia, smoking, free ambulation), and plasma catecholamine responses were assessed in five patients with primary pulmonary hypertension. Ambulatory monitoring techniques provided data for the computerised analysis of continuous, beat-to-beat, direct recordings of both pulmonary and systemic arterial pressures for 8 to 10 hours. The absol...

  17. Plasma diagnostics of low pressure high power impulse magnetron sputtering assisted by electron cyclotron wave resonance plasma

    Czech Academy of Sciences Publication Activity Database

    Straňák, V.; Herrendorf, A.-P.; Drache, S.; Čada, Martin; Hubička, Zdeněk; Bogdanowicz, R.; Tichý, M.; Hippler, R.

    2012-01-01

    Roč. 112, č. 9 (2012), "093305-1"-"093305-9" ISSN 0021-8979 R&D Projects: GA TA ČR TA01010517; GA ČR(CZ) GAP205/11/0386 Institutional research plan: CEZ:AV0Z10100522 Keywords : Langmuir probes * mass spectroscopy * plasma density * plasma diagnostics * plasma materials processing * plasma pressure * plasma radiofrequency heating Subject RIV: BL - Plasma and Gas Discharge Physics Impact factor: 2.210, year: 2012 http://jap.aip.org/resource/1/japiau/v112/i9/p093305_s1

  18. Modular Hybrid Plasma Reactor for Low Cost Bulk Production of Nanomaterials

    Energy Technology Data Exchange (ETDEWEB)

    Peter C. Kong

    2011-12-01

    INL developed a bench scale modular hybrid plasma system for gas phase nanomaterials synthesis. The system was being optimized for WO3 nanoparticles production and scale model projection to a 300 kW pilot system. During the course of technology development many modifications had been done to the system to resolve technical issues that had surfaced and also to improve the performance. All project tasks had been completed except 2 optimization subtasks. These 2 subtasks, a 4-hour and an 8-hour continuous powder production runs at 1 lb/hr powder feeding rate, were unable to complete due to technical issues developed with the reactor system. The 4-hour run had been attempted twice and both times the run was terminated prematurely. The modular electrode for the plasma system was significantly redesigned to address the technical issues. Fabrication of the redesigned modular electrodes and additional components had been completed at the end of the project life. However, not enough resource was available to perform tests to evaluate the performance of the new modifications. More development work would be needed to resolve these problems prior to scaling. The technology demonstrated a surprising capability of synthesizing a single phase of meta-stable delta-Al2O3 from pure alpha-phase large Al2O3 powder. The formation of delta-Al2O3 was surprising because this phase is meta-stable and only formed between 973-1073 K, and delta-Al2O3 is very difficult to synthesize as a single phase. Besides the specific temperature window to form this phase, this meta-stable phase may have been stabilized by nanoparticle size formed in a high temperature plasma process. This technology may possess the capability to produce unusual meta-stable nanophase materials that would be otherwise difficult to produce by conventional methods. A 300 kW INL modular hybrid plasma pilot scale model reactor had been projected using the experimental data from PPG Industries 300 kW hot wall plasma reactor. The

  19. Hydrophilic surface modification of coronary stent using an atmospheric pressure plasma jet for endothelialization.

    Science.gov (United States)

    Shim, Jae Won; Bae, In-Ho; Park, Dae Sung; Lee, So-Youn; Jang, Eun-Jae; Lim, Kyung-Seob; Park, Jun-Kyu; Kim, Ju Han; Jeong, Myung Ho

    2018-03-01

    The first two authors contributed equally to this study. Bioactivity and cell adhesion properties are major factors for fabricating medical devices such as coronary stents. The aim of this study was to evaluate the advantages of atmospheric-pressure plasma jet in enhancing the biocompatibility and endothelial cell-favorites. The experimental objects were divided into before and after atmospheric-pressure plasma jet treatment with the ratio of nitrogen:argon = 3:1, which is similar to air. The treated surfaces were basically characterized by means of a contact angle analyzer for the activation property on their surfaces. The effect of atmospheric-pressure plasma jet on cellular response was examined by endothelial cell adhesion and XTT analysis. It was difficult to detect any changeable morphology after atmospheric-pressure plasma jet treatment on the surface. The roughness was increased after atmospheric-pressure plasma jet treatment compared to nonatmospheric-pressure plasma jet treatment (86.781 and 7.964 nm, respectively). The X-ray photoelectron spectroscopy results showed that the surface concentration of the C-O groups increased slightly from 6% to 8% after plasma activation. The contact angle dramatically decreased in the atmospheric-pressure plasma jet treated group (22.6 ± 15.26°) compared to the nonatmospheric-pressure plasma jet treated group (72.4 ± 15.26°) ( n = 10, p atmospheric-pressure plasma jet on endothelial cell migration and proliferation was 85.2% ± 12.01% and 34.2% ± 2.68%, respectively, at 7 days, compared to the nonatmospheric-pressure plasma jet treated group (58.2% ± 11.44% in migration, n = 10, p atmospheric-pressure plasma jet method. Moreover, the atmospheric-pressure plasma jet might affect re-endothelialization after stenting.

  20. Atmospheric Pressure Plasma-Electrospin Hybrid Process for Protective Applications

    Science.gov (United States)

    Vitchuli Gangadharan, Narendiran

    2011-12-01

    -level aerosol chemical and biological threats. Polymer solution concentration, electrospinning voltage, and deposition areal density were varied to establish the relationship of processing-structure-filtration efficiency for electrospun fiber mats. A high barrier efficiency of greater than 99.5% was achieved on electrospun fiber mats without sacrificing air permeability and pressure drop. ii) Fabrication and Characterization of Multifunctional ZnO/Nylon 6 nanofibers ZnO/Nylon 6 nanofiber mats were prepared by an electrospinning-electrospraying hybrid process, The electrospinning of polymer solution and electrospraying of ZnO particles were carried out simultaneously such that the ZnO nanoparticles were dispersed on the surface of Nylon 6 nanofibers. The prepared ZnO/Nylon 6 nanofiber mats were tested for detoxifying characteristics against simulants of C-B agents. The results showed that ZnO/Nylon 6 functional nanofiber mats exhibited good detoxification action against paraoxon and have antibacterial efficiency over 99.99% against both the gram-negative E. coli and gram positive B. cereus bacteria. iii) Improving adhesion of electrospun nanofiber mat onto woven fabric by plasma pretreatment of substrate fabric and plasma-electrospinning hybrid process Electrospun nanofibers were deposited onto plasma-pretreated woven fabric to improve the adhesion. In addition, the plasma-electrospinning hybrid process was developed and used in which the nanofibers were subjected to in-situ plasma treatment during electrospinning. The effects of plasma treatement on substrate fabric and electrospun fibers were characterized by water contact angle test, XPS analyses. The improvement of nanofiber adhesive properties on fabric substrate was evaluated by peel test, flex resistance test and abrasion resistance test. The test results showed that the plasma treatment caused introduction of active chemical groups on substrate fabric and electrospun nanofibers. These active chemical assisted in possible

  1. Micro-electromechanical film bulk acoustic sensor for plasma and whole blood coagulation monitoring.

    Science.gov (United States)

    Chen, Da; Song, Shuren; Ma, Jilong; Zhang, Zhen; Wang, Peng; Liu, Weihui; Guo, Qiuquan

    2017-05-15

    Monitoring blood coagulation is an important issue in the surgeries and the treatment of cardiovascular diseases. In this work, we reported a novel strategy for the blood coagulation monitoring based on a micro-electromechanical film bulk acoustic resonator. The resonator was excited by a lateral electric field and operated under the shear mode with a frequency of 1.9GHz. According to the apparent step-ladder curves of the frequency response to the change of blood viscoelasticity, the coagulation time (prothrombin time) and the coagulation kinetics were measured with the sample consumption of only 1μl. The procoagulant activity of thromboplastin and the anticoagulant effect of heparin on the blood coagulation process were illustrated exemplarily. The measured prothrombin times showed a good linear correlation with R 2 =0.99969 and a consistency with the coefficient of variation less than 5% compared with the commercial coagulometer. The proposed film bulk acoustic sensor, which has the advantages of small size, light weight, low cost, simple operation and little sample consumption, is a promising device for miniaturized, online and automated analytical system for routine diagnostics of hemostatic status and personal health monitoring. Copyright © 2017 Elsevier B.V. All rights reserved.

  2. High Bulk Modulus of Nanocrystal γ-Fe2O3 with Chemical Dodecyl Benzene Sulfonic Decoration Under High Pressure

    Science.gov (United States)

    Jing, Zhao; Lin, Guo; Jing, Liu; Yang, Yang; Rong-Zheng, Che; Lei, Zhou

    2000-02-01

    Structural transformation in γ-Fe2O3 nanocrystals (about 10 nm) with dodecyl benzene sulfonic (DBS) coated is studied by using high-pressure energy dispersive x-ray diffraction of synchrotron radiation and high-resolution transmission electron microscopy (HRTEM). Relative to the bulk crystal, the transition pressure showed a decrease while the compressibility increases significantly up to 375 (±9 GPa). HRTEM picture confirmed that there is surface cladding surrounding nanocrystals due to DBS, which formed new special boundaries between nanocrystals and should be different from the ordinary grain boundaries. The experimental results imply that the surface layers of γ-Fe2O3 nanocrystals have strong effect on the compressibility.

  3. The effect of hydrostatic pressure on material parameters and electrical transport properties in bulk GaN

    Energy Technology Data Exchange (ETDEWEB)

    Eshghi, Hosein [Department of Physics, Shahrood University of Technology, Shahrood 316-36155 (Iran, Islamic Republic of)], E-mail: h_eshghi@shahroodut.ac.ir

    2009-04-27

    Experimental data for temperature dependence of electron transport properties in a bulk, low dislocation density, GaN sample at atmospheric pressure and 7.1 kbar have been presented. The data are representing a weak hydrostatic pressure dependence. Our quantitative analysis on its material parameters including: high and low dielectric constants ({epsilon}{sub {infinity}},{epsilon}{sub s}), longitudinal and transverse optical phonons ({omega}{sub LO},{omega}{sub TO}), and electronic effective mass (m{sub e}*) show a small fractional change of -0.12,-0.14,0.05,0.058 and 0.089 (percent/kbar), respectively. These results are confirmed by the Hall-effect data analysis on the basis of charge neutrality condition and various scattering mechanisms.

  4. An investigation of transient pressure and plasma properties in a pinched plasma column. M.S. Thesis

    Science.gov (United States)

    Stover, E. K.; York, T. M.

    1971-01-01

    The transient pinched plasma column generated in a linear Z-pinch was studied experimentally and analytically. The plasma column was investigated experimentally with the following plasma diagnostics: a special rapid response pressure transducer, a magnetic field probe, a voltage probe and discharge luminosity. Axial pressure profiles on the discharge chamber axis were used to identify three characteristic regions of plasma column behavior; they were in temporal sequence: strong axial pressure asymmetry noted early in plasma column lifetime followed by plasma heating in which there is a rapid rise in static pressure and a slight decrease static pressure before plasma column breakup. Plasma column lifetime was approximately 5 microseconds. The axial pressure asymmetry was attributed to nonsimultaneous pinching of the imploding current sheet along the discharge chamber axis. The rapid heating is attributed in part to viscous effects introduced by radial gradients in the axial streaming velocity. Turbulent heating arising from discharge current excitation of the ion acoustic wave instability is also considered a possible heating mechanism.

  5. Cancer therapy using non-thermal atmospheric pressure plasma with ultra-high electron density

    Energy Technology Data Exchange (ETDEWEB)

    Tanaka, Hiromasa [Institute of Innovation for Future Society, Nagoya University, Furo-cho, Chikusa-ku, Nagoya 464-8603 (Japan); Center for Advanced Medicine and Clinical Research, Nagoya University Graduate School of Medicine, Tsurumai-cho 65, Showa-ku, Nagoya 466-8550 (Japan); Mizuno, Masaaki [Center for Advanced Medicine and Clinical Research, Nagoya University Graduate School of Medicine, Tsurumai-cho 65, Showa-ku, Nagoya 466-8550 (Japan); Toyokuni, Shinya [Department of Pathology and Biological Responses, Nagoya University Graduate School of Medicine, Tsurumai-cho 65, Showa-ku, Nagoya 466-8550 (Japan); Maruyama, Shoichi [Department of Nephrology, Nagoya University Graduate School of Medicine, Tsurumai-cho 65, Showa-ku, Nagoya 466-8550 (Japan); Kodera, Yasuhiro [Department of Gastroenterological Surgery (Surgery II), Nagoya University Graduate School of Medicine, Tsurumai-cho 65, Showa-ku, Nagoya 466-8550 (Japan); Terasaki, Hiroko [Department of Ophthalmology, Nagoya University Graduate School of Medicine, Tsurumai-cho 65, Showa-ku, Nagoya 466-8550 (Japan); Adachi, Tetsuo [Laboratory of Clinical Pharmaceutics, Gifu Pharmaceutical University, 501-1196 Gifu (Japan); Kato, Masashi [Department of Occupational and Environmental Health, Nagoya University Graduate School of Medicine, Tsurumai-cho 65, Showa-ku, Nagoya 466-8550 (Japan); Kikkawa, Fumitaka [Department of Obstetrics and Gynecology, Nagoya University Graduate School of Medicine, Tsurumai-cho 65, Showa-ku, Nagoya 466-8550 (Japan); Hori, Masaru [Institute of Innovation for Future Society, Nagoya University, Furo-cho, Chikusa-ku, Nagoya 464-8603 (Japan)

    2015-12-15

    Cancer therapy using non-thermal atmospheric pressure plasma is a big challenge in plasma medicine. Reactive species generated from plasma are key factors for treating cancer cells, and thus, non-thermal atmospheric pressure plasma with high electron density has been developed and applied for cancer treatment. Various cancer cell lines have been treated with plasma, and non-thermal atmospheric plasma clearly has anti-tumor effects. Recent innovative studies suggest that plasma can both directly and indirectly affect cells and tissues, and this observation has widened the range of applications. Thus, cancer therapy using non-thermal atmospheric pressure plasma is promising. Animal experiments and understanding the mode of action are essential for clinical application in the future. A new academic field that combines plasma science, the biology of free radicals, and systems biology will be established.

  6. Cancer therapy using non-thermal atmospheric pressure plasma with ultra-high electron density

    International Nuclear Information System (INIS)

    Tanaka, Hiromasa; Mizuno, Masaaki; Toyokuni, Shinya; Maruyama, Shoichi; Kodera, Yasuhiro; Terasaki, Hiroko; Adachi, Tetsuo; Kato, Masashi; Kikkawa, Fumitaka; Hori, Masaru

    2015-01-01

    Cancer therapy using non-thermal atmospheric pressure plasma is a big challenge in plasma medicine. Reactive species generated from plasma are key factors for treating cancer cells, and thus, non-thermal atmospheric pressure plasma with high electron density has been developed and applied for cancer treatment. Various cancer cell lines have been treated with plasma, and non-thermal atmospheric plasma clearly has anti-tumor effects. Recent innovative studies suggest that plasma can both directly and indirectly affect cells and tissues, and this observation has widened the range of applications. Thus, cancer therapy using non-thermal atmospheric pressure plasma is promising. Animal experiments and understanding the mode of action are essential for clinical application in the future. A new academic field that combines plasma science, the biology of free radicals, and systems biology will be established

  7. Experimental determination of bulk modulus of 14Å tobermorite using high pressure synchrotron X-ray diffraction

    KAUST Repository

    Oh, Jae Eun

    2012-02-01

    Using a diamond anvil cell, 14 Å tobermorite, a structural analogue of calcium silicate hydrates (C-S-H), was examined by high-pressure synchrotron X-ray diffraction up to 4.8 GPa under hydrostatic conditions. The bulk modulus of 14 Å tobermorite was calculated, K o = 47 GPa. Comparison of the current results with previous high pressure studies on C-S-H(I) indicates that: (1) the compression behavior of the lattice parameters a and b of 14 Å tobermorite and C-S-H(I) are very similar, implying that both materials may have very similar Ca-O layers, and also implying that an introduction of structural defects into the Ca-O layers may not substantially change in-plane incompressibility of the ab plane of 14 Å tobermorite; and (2) the bulk modulus values of 14 Å tobermorite and C-S-H(I) are dominated by the incompressibility of the lattice parameter c, which is directly related to the interlayer spacing composed of dreierketten silicate chains, interlayer Ca, and water molecules. © 2011 Elsevier Ltd. All rights reserved.

  8. Calculation of high-pressure argon plasma parameters produced by excimer laser

    International Nuclear Information System (INIS)

    Tsuda, Norio; Yamada, Jun

    2000-01-01

    When a XeCl excimer laser light was focused in a high-pressure argon gas up to 150 atm, a dense plasma developed not only backward but also forward. It is important to study on the electron density and temperature of the laser-induced plasma in the high-pressure gas. The electron density and temperature in high-pressure argon plasma produced by XeCl excimer laser has been calculated and compared with the experimental data. (author)

  9. Thermal expansivity and bulk modulus of ZnO with NaCl-type cubic structure at high pressures and temperatures

    International Nuclear Information System (INIS)

    Sun Xiaowei; Liu Zijiang; Chen Qifeng; Chu Yandong; Wang Chengwei

    2006-01-01

    The thermal expansivity and bulk modulus of ZnO with NaCl-type cubic structure were estimated by using the constant temperature and pressure molecular dynamics technique with effective pair potentials which consist of the Coulomb, dispersion, and repulsion interaction at high pressures and temperatures. It is shown that the calculated thermodynamic parameters including linear thermal expansion coefficient, isothermal bulk modulus and its pressure derivative are in good agreement with the available experimental data and the latest theoretical results. At an extended pressure and temperature ranges, linear thermal expansion coefficient and isothermal bulk modus have also been predicted. The thermodynamic properties of ZnO with NaCl-type cubic structure are summarized in the pressure 0-150 GPa ranges and the temperature up to 3000 K

  10. Bulk characterization of pharmaceutical powders by low-pressure compression II

    DEFF Research Database (Denmark)

    Hagsten Sørensen, A.; Sonnergaard, Jørn; Hovgaard, L.

    2006-01-01

    was studied by compressing and tapping different grades of calcium carbonate, lactose, and microcrystalline cellulose. The low-pressure compression-derived parameters were compared to tapped densities and to Compressibility Indexes obtained by tapping volumetry. Even though the relationship between particle......The aim of the present study was to investigate the effect of punch and die diameter, sample size, compression speed, and particle size on two low-pressure compression-derived parameters; the compressed density and the Walker w parameter. The excellent repeatability of the low-pressure compression...... method allowed small effects of variations in punch and die diameter and sample size to be demonstrated on a high significance level. Changing the compression speed, however, did not cause a significant effect in the compressed density, whereas a decrease in w was seen. The effect of particle size...

  11. Pressure dependence of critical temperature of bulk FeSe from spin fluctuation theory

    Science.gov (United States)

    Hirschfeld, Peter; Kreisel, Andreas; Wang, Yan; Tomic, Milan; Jeschke, Harald; Jacko, Anthony; Valenti, Roser; Maier, Thomas; Scalapino, Douglas

    2013-03-01

    The critical temperature of the 8K superconductor FeSe is extremely sensitive to pressure, rising to a maximum of 40K at about 10GPa. We test the ability of the current generation of fluctuation exchange pairing theories to account for this effect, by downfolding the density functional theory electronic structure for each pressure to a tight binding model. The Fermi surface found in such a procedure is then used with fixed Hubbard parameters to determine the pairing strength using the random phase approximation for the spin singlet pairing vertex. We find that the evolution of the Fermi surface captured by such an approach is alone not sufficient to explain the observed pressure dependence, and discuss alternative approaches. PJH, YW, AK were supported by DOE DE-FG02-05ER46236, the financial support of MT, HJ, and RV from the DFG Schwerpunktprogramm 1458 is kindly acknowledged.

  12. Analytical calculations of the rotational transform angles in the torsatron systems with different plasma pressure profiles

    International Nuclear Information System (INIS)

    Kuznetsov, Yu.K.; Pinos, I.B.; Tyupa, V.I.

    1999-01-01

    With formulas for averaging over magnetic surfaces general analytical expressions are here deduced to determine the rotational transform angles in stellarator systems having different plasma pressure profiles

  13. Application of low pressure plasma technology in the field of environmental protection

    International Nuclear Information System (INIS)

    Sun Yabing

    2000-01-01

    The characteristics of low pressure plasma produced by a gas discharges lie in that the energy of the electrons are much higher than that of the heavy particles in the system. The low-pressure plasma treatment technology for the environmental contaminants was synthetically studied, and the reaction processing and mechanism between the low-pressure plasma and the environmental contaminants were theoretically analyzed. At last, the prospects and existing problems on the application of low-pressure plasma in the field of environmental protection were discussed

  14. Dry Sliding Wear Behavior of Spark Plasma Sintered Fe-Based Bulk Metallic Glass/Graphite Composites

    Directory of Open Access Journals (Sweden)

    Xiulin Ji

    2016-09-01

    Full Text Available Bulk metallic glass (BMG and BMG-graphite composites were fabricated using spark plasma sintering at the sintering temperature of 575 °C and holding time of 15 min. The sintered composites exhibited partial crystallization and the presence of distributed porosity and graphite particles. The effect of graphite reinforcement on the tribological properties of the BMG/graphite composites was investigated using dry ball-on-disc sliding wear tests. The reinforcement of graphite resulted in a reduction in both the wear rate and the coefficient of friction as compared to monolithic BMG samples. The wear surfaces of BMG/graphite composites showed regions of localized wear loss due to microcracking and fracture, as was also the case with the regions covered with graphite-rich protective film due to smearing of pulled off graphite particles.

  15. State of the art in medical applications using non-thermal atmospheric pressure plasma

    Science.gov (United States)

    Tanaka, Hiromasa; Ishikawa, Kenji; Mizuno, Masaaki; Toyokuni, Shinya; Kajiyama, Hiroaki; Kikkawa, Fumitaka; Metelmann, Hans-Robert; Hori, Masaru

    2017-12-01

    Plasma medical science is a novel interdisciplinary field that combines studies on plasma science and medical science, with the anticipation that understanding the scientific principles governing plasma medical science will lead to innovations in the field. Non-thermal atmospheric pressure plasma has been used for medical treatments, such as for cancer, blood coagulation, and wound healing. The interactions that occur between plasma and cells/tissues have been analyzed extensively. Direct and indirect treatment of cells with plasma has broadened the applications of non-thermal atmospheric pressure plasma in medicine. Examples of indirect treatment include plasma-assisted immune-therapy and plasma-activated medium. Controlling intracellular redox balance may be key in plasma cancer treatment. Animal studies are required to test the effectiveness and safety of these treatments for future clinical applications.

  16. Plasma-polymerized methyl methacrylate via intense and highly energetic atmospheric pressure micro-plasma for bio-medical applications

    Science.gov (United States)

    Park, Choon-Sang; Ballato, John; Kim, Sung-O.; Clemson University Team

    2013-09-01

    Poly (methyl methacrylate), PMMA, has been widely used as a biocompatible material in bone cement, dental fillings, and many other bio-related applications. Vacuum plasmas and radio frequency (RF) atmospheric plasmas are the most common methods for depositing plasma-derived thin films and nanoparticles. However, the necessary equipment is difficult to operate and maintain as well as being large and expensive. Here, we report the use of a novel intense and highly energetic atmospheric pressure plasma jet array using direct plasma jet-to-jet coupling effects to deposit high quality plasma-polymerized MMA (PPMMA) for bio-medical applications. The newly proposed atmospheric pressure micro-plasma jet array device can generate the intense plasma mode with a strong plasma emission and high plasma particle energy. PPMMA was successfully deposited on a variety of substrates and characterized by SEM, AFM, and FT-IR. The micro-plasma jet is obtained at a sinusoidal voltage with a peak value of 30 kV and frequency of 35 kHz. Argon gas was employed as the discharge gas for plasma generation and its flow rate was in the range of 2230 sccm, Methyl methacrylate (MMA) monomer was vaporized by means of a glass bubbler which was supplied by argon gas with flow rates in the range of 268 sccm from room temperature to 400°C. The deposited PPMMA thin films were flexible, transparent, thin, and strong on metal substrates.

  17. High pressure laser plasma studies. [energy pathways in He-Ar gas mixtures at low pressure

    Science.gov (United States)

    Wells, W. E.

    1980-01-01

    The operation of a nuclear pumped laser, operating at a wavelength of 1.79 micron m on the 3d(1/2-4p(3/2) transition in argon with helium-3 as the majority gas is discussed. The energy pathways in He-Ar gas were investigated by observing the effects of varying partial pressures on the emissions of levels lying above the 4p level in argon during a pulsed afterglow. An attempt is made to determine the population mechanisms of the 3d level in pure argon by observing emission from the same transition in a high pressure plasma excited by a high energy electron beam. Both collisional radiative and dissociative recombination are discussed.

  18. Selective cytotoxicity of indirect nonequilibrium atmospheric pressure plasma against ovarian clear-cell carcinoma.

    Science.gov (United States)

    Utsumi, Fumi; Kajiyama, Hiroaki; Nakamura, Kae; Tanaka, Hiromasa; Hori, Masaru; Kikkawa, Fumitaka

    2014-01-01

    Ovarian clear cell carcinoma (CCC) is a histological type of epithelial ovarian cancer that is less responsive to chemotherapy and associated with a poorer prognosis than serous and endometrioid carcinoma. Non-thermal atmospheric pressure plasma which produces reactive species has recently led to an explosion of research in plasma medicine. Plasma treatment can be applied to cancer treatment to induce apoptosis and tumor growth arrest. Furthermore, recent studies have shown that a medium exposed to plasma also has an anti-proliferative effect against cancer in the absence of direct exposure to plasma. In this study, we confirmed whether this indirect plasma has an anti-tumor effect against CCC, and investigated whether this efficacy is selective for cancer cells. Non-thermal atmospheric pressure plasma induced apoptosis in CCC cells, while human peritoneal mesothelial cells remained viable. Non-thermal atmospheric pressure plasma exhibits selective cytotoxicity against CCC cells which are resistant to chemotherapy.

  19. Crystallization in Zr41.2Ti13.8Cu12.5Ni10Be22.5 bulk metallic glass under pressure

    DEFF Research Database (Denmark)

    Jiang, Jianzhong; Zhou, T.J.; Rasmussen, Helge Kildahl

    2000-01-01

    The effect of pressure on the crystallization behavior of the bulk metallic glass-forming Zr41.2Ti13.8Cu12.5Ni10Be22.5 alloy with a wide supercooled liquid region has been investigated by in situ high-pressure and high-temperature x-ray powder diffraction measurements using synchrotron radiation....

  20. Atmospheric-pressure-plasma-enhanced fabrication of nonfouling nanocoatings for 316 stainless steel biomaterial interfaces

    Science.gov (United States)

    Huang, Chun; Lin, Jin-He; Li, Chi-Heng; Yu, I.-Chun; Chen, Ting-Lun

    2018-03-01

    Atmospheric-pressure plasma, which was generated with electrical RF power, was fed to a tetramethyldisiloxane/argon gas mixture to prepare bioinert organosilicon coatings for 316 stainless steel. The surface characteristics of atmospheric-pressure-plasma-deposited nanocoatings were evaluated as a function of RF plasma power, precursor gas flow, and plasma working distance. After surface deposition, the chemical features, elemental compositions, and surface morphologies of the organosilicon nanocoatings were examined. It was found that RF plasma power and plasma working distance are the essential factors that affect the formation of plasma-deposited nanocoatings. Fourier transform infrared spectroscopy spectra indicate that the atmospheric-pressure-plasma-deposited nanocoatings formed showed inorganic features. Atomic force microscopy analysis showed the surface roughness variation of the plasma-deposited nanocoating at different RF plasma powers and plasma working distances during surface treatment. From these surface analyses, it was found that the plasma-deposited organosilicon nanocoatings under specific operational conditions have relatively hydrophobic and inorganic characteristics, which are essential for producing an anti-biofouling interface on 316 stainless steel. The experimental results also show that atmospheric-pressure-plasma-deposited nanocoatings have potential use as a cell-resistant layer on 316 stainless steel.

  1. Competition of bulk trapping and surface erosion in the kinetics of tritium inventory and permeation in plasma protection metals

    International Nuclear Information System (INIS)

    Federici, G.; Holland, D.F.; Esser, B.

    1996-01-01

    A simplified transient model is presented to describe the migration of implanted tritium in the presence of trap sites across the bulk of metallic substrates whose thickness is decreasing with time due to erosion. The subject is relevant for quantifying the tritium inventory in - and permeation through -plasma facing armours in the next generation of D-T fuelled tokamak devices (i.e., the International Thermonuclear Experimental Reactor). This paper describes the equations of the physical model and the main assumptions used to simplify the complex analysis, and surveys the influence of several parameters such as the implantation flux, the erosion rate, the armour temperature, the armour thickness, the density and trapping energy of neutron-induced traps, etc., which are all expected to play a key role in the phenomena investigated. The examples presented to show the applicability of the model include the results of a study performed for beryllium armours exposed to heat and particle loads similar to those expected on the ITER divertor plasma facing components and comparison is made with cases where erosion does not play any role. (orig.)

  2. Characterization of atmospheric pressure plasma treated pure cashmere and wool/cashmere textiles: Treatment in air/water vapor mixture

    Energy Technology Data Exchange (ETDEWEB)

    Zanini, Stefano, E-mail: stefano.zanini@mib.infn.it [Università degli Studi di Milano-Bicocca, Dipartimento di Fisica “G. Occhialini”, p.za della Scienza, 3, I-20126 Milano (Italy); Grimoldi, Elisa [Università degli Studi di Milano-Bicocca, Dipartimento di Fisica “G. Occhialini”, p.za della Scienza, 3, I-20126 Milano (Italy); Citterio, Attilio [Politecnico di Milano, Dipartimento di Chimica, Materiali ed Ingegneria Chimica “G. Natta”, Via Mancinelli 7, I-20131 Milano (Italy); Riccardi, Claudia, E-mail: riccardi@mib.infn.it [Università degli Studi di Milano-Bicocca, Dipartimento di Fisica “G. Occhialini”, p.za della Scienza, 3, I-20126 Milano (Italy)

    2015-09-15

    Highlights: • We treated cashmere and wool/cashmere textiles with atmospheric pressure plasma. • Wettability of the fabrics was increased. • The increment in wettability derived from a surface oxidation of the fibers. • Only minor etching effects were observed with scanning electron microscopy. - Abstract: We performed atmospheric pressure plasma treatments of pure cashmere and wool/cashmere textiles with a dielectric barrier discharge (DBD) in humid air (air/water vapor mixtures). Treatment parameters have been optimized in order to enhance the wettability of the fabrics without changing their bulk properties as well as their touch. A deep characterization has been performed to study the wettability, the surface morphologies, the chemical composition and the mechanical properties of the plasma treated textiles. The chemical properties of the plasma treated samples were investigated with attenuated total reflectance Fourier transform infrared (FTIR/ATR) spectroscopy and X-ray photoelectron microscopy (XPS). The analyses reveal a surface oxidation of the treated fabrics, which enhances their surface wettability. Morphological characterization of the treated fibers with scanning electron microscopy (SEM) reveals minor etching effects, an essential feature for the maintenance of the textile softness.

  3. Collaborative Research: Atmospheric Pressure Plasma-Biomaterial Surface Interactions - Bridging Understanding of APP Sources to Rational Modification of Biomolecules

    Energy Technology Data Exchange (ETDEWEB)

    Graves, David Barry [Univ. of California, Berkeley, CA (United States)

    2017-11-24

    The overriding objective of this work is to bridge the gap between understanding of atmospheric pressure plasma (APP) sources and predictive chemical modifications of biomolecules. A key aspect of this problem is to understand what oxidizing species are created in water adjacent to APP jets that would ultimately affect aqueous biomolecules. We report the production of highly oxidative species in solutions exposed to a self-pulsed corona discharge in air. We examine how the properties of the target solution (pH, conductivity) and the discharge power affect the discharge stability and the production of H2O2. Indigo carmine, a common organic dye, is used as an indicator of oxidative strength and in particular, hydroxyl radical (OH•) production. The observed rate of indigo oxidation in contact with the discharge far exceeds that predicted from reactions based on concentrations of species measured in the bulk solution. The generation of H2O2 and the oxidation of indigo carmine indicate a high concentration of highly oxidizing species such as OH• at the plasma-liquid interface. These results indicate that reactions at the air plasma-liquid interface play a dominant role in species oxidation during direct non-equilibrium atmospheric pressure plasma (NE-APP) treatment.

  4. Influence of feeding pattern and hydraulic selection pressure to control filamentous bulking in biological treatment of dairy wastewaters.

    Science.gov (United States)

    Meunier, Christophe; Henriet, Olivier; Schoonbroodt, Bastien; Boeur, Jean-Marc; Mahillon, Jacques; Henry, Paul

    2016-12-01

    In sequencing batch reactors (SBRs) treating dairy wastewaters, the overgrowth of filamentous bacteria is a frequent cause of operational problems. The present study aimed at understanding to what extent the operating conditions of a SBR can be optimized to convert a bulking activated sludge into a well-settling biomass at low aeration velocity. The abundance of filament morphotypes and floc-formers able to store biopolymers were analysed by PCR-DGGE and 16S amplicon sequencing. The results indicated that a combination of an anaerobic-microaerated feeding pattern with a low selective pressure was beneficial to supress filamentous overgrowth and to form aerobic granules, while increasing the efficiency of suspended solid removal. Average removal efficiencies for total chemical oxygen demand (COD), total nitrogen (TN) and total phosphorus (TP) were 94±2%, 95±1% and 83±13%, respectively. Copyright © 2016 Elsevier Ltd. All rights reserved.

  5. Pressure and compressibility of a quantum plasma in a magnetic field

    NARCIS (Netherlands)

    Suttorp, L.G.

    1993-01-01

    The equilibrium pressure tensor that occurs in the momentum balance equation for a quantum plasma in a magnetic field is shown to be anisotropic. Its relation to the pressure that follows from thermodynamics is elucidated. A general proof of the compressibility rule for a magnetized quantum plasma

  6. Physico Chemical Characteristics of High Performance Polymer Modified by Low and Atmospheric Pressure Plasma1

    NARCIS (Netherlands)

    Bhatnagar, N.; Jha, S.; Bhowmik, S.; Gupta, G.; Moon, J.B.; Kim, C.G.

    2012-01-01

    In this work, the effect of low pressure plasma and atmospheric-pressure plasma treatment on surface properties and adhesion characteristics of high performance polymer, Polyether Ether Ketone (PEEK) are investigated in terms of Fourier Transform Infrared Spectroscopy (FTIR), X-ray photoelectron

  7. Analysis of Physics Processes in the AC Plasma Torch Discharge under High Pressure

    International Nuclear Information System (INIS)

    Safronov, A A; Vasilieva, O B; Dudnik, J D; Kuznetsov, V E; Kuchina, J A; Shiryaev, V N; Pavlov, A V

    2017-01-01

    The paper is devoted to investigation of electrophysical processes in the electric discharge generated by a three-phase AC plasma torch when using a high pressure inert working gas. AC plasma torch design with end electrodes intended for work on inert gases at pressures up to 81 bar is studied. Current-voltage characteristics for different gas flow rates and pressures are presented. Physical processes characteristics of the arising voltage ripples which depend on various working parameters of the plasma torch have been investigated. Arc burning processes in the electric discharge chamber of the three-phase AC plasma torch at various working parameters were photographed. (paper)

  8. Atmospheric pressure plasma surface modification of titanium for high temperature adhesive bonding

    NARCIS (Netherlands)

    Akram, M.; Jansen, K.M.B.; Ernst, L.J.; Bhowmik, S.

    2011-01-01

    In this investigation surface treatment of titanium is carried out by plasma ion implantation under atmospheric pressure plasma in order to increase the adhesive bond strength. Prior to the plasma treatment, titanium surfaces were mechanically treated by sand blasting. It is observed that the

  9. Biomedical Applications of Low Temperature Atmospheric Pressure Plasmas to Cancerous Cell Treatment and Tooth Bleaching

    Science.gov (United States)

    Lee, Jae Koo; Kim, Myoung Soo; Byun, June Ho; Kim, Kyong Tai; Kim, Gyoo Cheon; Park, Gan Young

    2011-08-01

    Low temperature atmospheric pressure plasmas have attracted great interests and they have been widely applied to biomedical applications to interact with living tissues, cells, and bacteria due to their non-thermal property. This paper reviews the biomedical applications of low temperature atmospheric pressure plasmas to cancerous cell treatment and tooth bleaching. Gold nanoparticles conjugated with cancer-specific antibodies have been introduced to cancerous cells to enhance selective killing of cells, and the mechanism of cell apoptosis induced by plasma has been investigated. Tooth exposed to helium plasma jet with hydrogen peroxide has become brighter and the productions of hydroxyl radicals from hydrogen peroxide have been enhanced by plasma exposure.

  10. Study on high pressure plasma produced by ArF laser

    OpenAIRE

    Tsuda, Norio; Yamada, Jun

    2004-01-01

    12th International Congress on Plasma Physics, 25-29 October 2004, Nice (France); When an ArF excimer laser beam was focused in a high pressure argon gas from 50 to 130 atm, the plasma development is observed by streak camera from side window of chamber. The high pressure ArF laser plasma develops symmetrically and the plasma produced by ArF excimer laser hardly develops as compared with the plasma produced by XeCl. The photon energy of ArF laser light is higher than the XeCl laser. The trans...

  11. Fluorination of poly(dimethylsiloxane surfaces by low pressure CF4 plasma – physicochemical and antifouling properties

    Directory of Open Access Journals (Sweden)

    2009-02-01

    Full Text Available Fluorinated surface groups were introduced into poly(dimethylsiloxane (PDMS coatings by plasma treatment using a low pressure radio frequency discharge operated with tetrafluoromethane. Substrates were placed in a remote position downstream the discharge. Discharge power and treatment time were tuned to alter the chemical composition of the plasma treated PDMS surface. The physicochemical properties and stability of the fluorine containing PDMS were characterized by X-ray photoelectron spectroscopy (XPS, atomic force microscopy (AFM and contact angle measurements. Smooth PDMS coatings with a fluorine content up to 47% were attainable. The CF4 plasma treatment generated a harder, non-brittle layer at the top-most surface of the PDMS. No changes of surface morphology were observed upon one week incubation in aqueous media. Surprisingly, the PDMS surface was more hydrophilic after the introduction of fluorine. This may be explained by an increased exposure of oxygen containing moieties towards the surface upon re-orientation of fluorinated groups towards the bulk, and/or be a consequence of oxidation effects associated with the plasma treatment. Experiments with strains of marine bacteria with different surface energies, Cobetia marina and Marinobacter hydrocarbonoclasticus, showed a significant decrease of bacteria attachment upon fluorination of the PDMS surface. Altogether, the CF4 plasma treatments successfully introduced fluorinated groups into the PDMS, being a robust and versatile surface modification technology that may find application where a minimization of bacterial adhesion is required.

  12. Stages of polymer transformation during remote plasma oxidation (RPO) at atmospheric pressure

    Science.gov (United States)

    Luan, P.; Oehrlein, G. S.

    2018-04-01

    The interaction of cold temperature plasma sources with materials can be separated into two types: ‘direct’ and ‘remote’ treatments. Compared to the ‘direct’ treatment which involves energetic charged species along with short-lived, strongly oxidative neutral species, ‘remote’ treatment by the long-lived weakly oxidative species is less invasive and better for producing uniformly treated surfaces. In this paper, we examine the prototypical case of remote plasma oxidation (RPO) of polymer materials by employing a surface micro-discharge (in a N2/O2 mixture environment) treatment on polystyrene. Using material characterization techniques including real-time ellipsometry, x-ray photoelectron spectroscopy, and Fourier-transform infrared spectroscopy, the time evolution of polymer film thickness, refractive index, surface, and bulk chemical composition were evaluated. These measurements revealed three consecutive stages of polymer transformation, i.e. surface adsorption and oxidation, bulk film permeation and thickness expansion followed by the material removal as a result of RPO. By correlating the observed film thickness changes with simultaneously obtained chemical information, we found that the three stages were due to the three effects of weakly oxidative species on polymers: (1) surface oxidation and nitrate (R-ONO2) chemisorption, (2) bulk oxidation, and (3) etching. Our results demonstrate that surface adsorption and oxidation, bulk oxidation, and etching can all happen during one continuous plasma treatment. We show that surface nitrate is only adsorbed on the top few nanometers of the polymer surface. The polymer film expansion also provided evidence for the diffusion and reaction of long-lived plasma species in the polymer bulk. Besides, we found that the remote plasma etched surface was relatively rich in O-C=O (ester or carboxylic acid). These findings clarify the roles of long-lived weakly oxidative plasma species on polymers and advance

  13. Selection of suitable diagnostic techniques for an RF atmospheric pressure plasma

    International Nuclear Information System (INIS)

    Kong, M.G.; Deng, X.T.

    2001-01-01

    As an early report of our study, this paper summaries the RF atmospheric pressure plasma system we intend to characterize and a number of diagnostic techniques presently under assessment for our plasma rig. By discussing the advantages and disadvantages of these diagnostic techniques at this meeting, we hope to gain feedback and comments to improve our choice of appropriate diagnostic techniques as well as our subsequent application of these techniques to nonthermal RF atmospheric pressure plasmas

  14. Dust acoustic waves in complex plasmas at elevated pressure

    International Nuclear Information System (INIS)

    Filippov, A.V.; Starostin, A.N.; Tkachenko, I.M.; Fortov, V.E.

    2011-01-01

    The bi-Yukawa effective interaction potential with different screening constants is employed to calculate dust static correlation functions in the hyper-netted chain approximation and to generalize the theory of dust acoustic waves within the non-perturbative moment approach complemented by hydrodynamic considerations. For the bi-Yukawa interaction potential the sound speed becomes significantly wavenumber-dependent, an additional soft diffusion-like mode is predicted, and the static dielectric function is shown to take negative values. The results can be applied to non-equilibrium dusty plasmas at elevated pressure. -- Highlights: ► Bi-Yukawa interaction potential of dust particles with different screening lengths. ► Dust static correlation functions in the hyper-netted chain approximation. ► The moment and hydrodynamic approaches are in a good agreement at weak non-ideality. ► The dust acoustic wave phase and group velocities depend on the wavenumber. ► The moment approach hints the appearance of the diffusion-like soft mode.

  15. Assessment of Atmospheric Pressure Plasma Treatment for Implant Osseointegration

    Directory of Open Access Journals (Sweden)

    Natalie R. Danna

    2015-01-01

    Full Text Available This study assessed the osseointegrative effects of atmospheric pressure plasma (APP surface treatment for implants in a canine model. Control surfaces were untreated textured titanium (Ti and calcium phosphate (CaP. Experimental surfaces were their 80-second air-based APP-treated counterparts. Physicochemical characterization was performed to assess topography, surface energy, and chemical composition. One implant from each control and experimental group (four in total was placed in one radius of each of the seven male beagles for three weeks, and one implant from each group was placed in the contralateral radius for six weeks. After sacrifice, bone-to-implant contact (BIC and bone area fraction occupancy (BAFO were assessed. X-ray photoelectron spectroscopy showed decreased surface levels of carbon and increased Ti and oxygen, and calcium and oxygen, posttreatment for Ti and CaP surfaces, respectively. There was a significant (P<0.001 increase in BIC for APP-treated textured Ti surfaces at six weeks but not at three weeks or for CaP surfaces. There were no significant (P=0.57 differences for BAFO between treated and untreated surfaces for either material at either time point. This suggests that air-based APP surface treatment may improve osseointegration of textured Ti surfaces but not CaP surfaces. Studies optimizing APP parameters and applications are warranted.

  16. Introduction of Atmospheric Pressure Plasma to Aqueous Detergent Processes.

    Science.gov (United States)

    Gotoh, Keiko; Kanasaki, Yu; Uchinomaru, Haruka

    2015-01-01

    The effects of exposure of polymer surfaces to atmospheric pressure plasma (APP) on detergency were investigated from the viewpoint of pretreatment to cleaning in aqueous systems using three PET substrates: film, mesh, and fabric. The PET substrates were soiled with stearic acid as a model oily contaminant, and were treated with the APP jet immediately before cleaning. Stir washing in aqueous solutions with and without alkali or anionic surfactant was performed, and then the detergency was evaluated from the microscopic image analysis or surface reflectance measurement. For all PET samples and detergent solutions, APP exposure was found to promote the removal of stearic acid. Contact angle measurements showed that APP exposure enhanced the hydrophilicity of PET and stearic acid. The increase in the surface oxygen concentration on PET and stearic acid due to the APP exposure was also observed by XPS analysis. The simultaneous oxidation of the PET substrate and stearic acid soil by the APP pretreatment resulted in detergency improvement via surface hydrophilization. Furthermore, microscopic observations suggested that the collapse of crystallized stearic acid deposited on the PET substrate by APP heating facilitated its removal. In situ detergency evaluation by a quartz crystal microbalance technique confirmed that the removal of stearic acid from the PET substrate was promoted by the APP exposure. The experimental findings of this study demonstrate the effectiveness of the APP exposure before cleaning in aqueous solutions.

  17. Assessment of Atmospheric Pressure Plasma Treatment for Implant Osseointegration.

    Science.gov (United States)

    Danna, Natalie R; Beutel, Bryan G; Tovar, Nick; Witek, Lukasz; Marin, Charles; Bonfante, Estevam A; Granato, Rodrigo; Suzuki, Marcelo; Coelho, Paulo G

    2015-01-01

    This study assessed the osseointegrative effects of atmospheric pressure plasma (APP) surface treatment for implants in a canine model. Control surfaces were untreated textured titanium (Ti) and calcium phosphate (CaP). Experimental surfaces were their 80-second air-based APP-treated counterparts. Physicochemical characterization was performed to assess topography, surface energy, and chemical composition. One implant from each control and experimental group (four in total) was placed in one radius of each of the seven male beagles for three weeks, and one implant from each group was placed in the contralateral radius for six weeks. After sacrifice, bone-to-implant contact (BIC) and bone area fraction occupancy (BAFO) were assessed. X-ray photoelectron spectroscopy showed decreased surface levels of carbon and increased Ti and oxygen, and calcium and oxygen, posttreatment for Ti and CaP surfaces, respectively. There was a significant (P < 0.001) increase in BIC for APP-treated textured Ti surfaces at six weeks but not at three weeks or for CaP surfaces. There were no significant (P = 0.57) differences for BAFO between treated and untreated surfaces for either material at either time point. This suggests that air-based APP surface treatment may improve osseointegration of textured Ti surfaces but not CaP surfaces. Studies optimizing APP parameters and applications are warranted.

  18. Measurement and analysis for optical radiation of glow discharge plasma at atmospheric pressure

    Science.gov (United States)

    Ren, Qinglei; Lin, Qi

    2006-02-01

    The optical radiation measurement and analysis to the glow discharge plasma at atmospheric pressure have been done in the paper. The low temperature plasma due to atmospheric pressure glow discharge (APGD) in air has been produced on the planar surface of designed electrode plate. The optical radiation spectra of the plasma produced in two kinds of electrode plats with different power values loaded have been measured and sampled with the minitype grating spectrograph system. The acquired spectra data are processed averagely and analyzed. The results of analysis indicate that the optical characteristic of the APGD plasma is related to the loaded power and layout of the electrode plate. This shows that it is feasible to describe the characteristic parameters of APGD plasma qualitatively and control the strength of the APGD plasma quantitatively by the obtained relationship, which provides a convenient approach for utilizing APGD plasma effectively and also establishes some foundation to investigate APGD plasma further.

  19. Atmospheric-pressure plasma activation and surface characterization on polyethylene membrane separator

    Science.gov (United States)

    Tseng, Yu-Chien; Li, Hsiao-Ling; Huang, Chun

    2017-01-01

    The surface hydrophilic activation of a polyethylene membrane separator was achieved using an atmospheric-pressure plasma jet. The surface of the atmospheric-pressure-plasma-treated membrane separator was found to be highly hydrophilic realized by adjusting the plasma power input. The variations in membrane separator chemical structure were confirmed by Fourier transform infrared spectroscopy and X-ray photoelectron spectroscopy. Chemical analysis showed newly formed carbonyl-containing groups and high surface concentrations of oxygen-containing species on the atmospheric-pressure-plasma-treated polymeric separator surface. It also showed that surface hydrophilicity primarily increased from the polar component after atmospheric-pressure plasma treatment. The surface and pore structures of the polyethylene membrane separator were examined by scanning electron microscopy, revealing a slight alteration in the pore structure. As a result of the incorporation of polar functionalities by atmospheric-pressure plasma activation, the electrolyte uptake and electrochemical impedance of the atmospheric-pressure-plasma-treated membrane separator improved. The investigational results show that the separator surface can be controlled by atmospheric-pressure plasma surface treatment to tailor the hydrophilicity and enhance the electrochemical performance of lithium ion batteries.

  20. Experimental validation of a Lyapunov-based controller for the plasma safety factor and plasma pressure in the TCV tokamak

    Science.gov (United States)

    Mavkov, B.; Witrant, E.; Prieur, C.; Maljaars, E.; Felici, F.; Sauter, O.; the TCV-Team

    2018-05-01

    In this paper, model-based closed-loop algorithms are derived for distributed control of the inverse of the safety factor profile and the plasma pressure parameter β of the TCV tokamak. The simultaneous control of the two plasma quantities is performed by combining two different control methods. The control design of the plasma safety factor is based on an infinite-dimensional setting using Lyapunov analysis for partial differential equations, while the control of the plasma pressure parameter is designed using control techniques for single-input and single-output systems. The performance and robustness of the proposed controller is analyzed in simulations using the fast plasma transport simulator RAPTOR. The control is then implemented and tested in experiments in TCV L-mode discharges using the RAPTOR model predicted estimates for the q-profile. The distributed control in TCV is performed using one co-current and one counter-current electron cyclotron heating actuation.

  1. Application of Langmuir Probe Method to the Atmospheric Pressure Discharge Plasma

    International Nuclear Information System (INIS)

    Matsuura, Hiroto; Matsumura, Yasuhiro; Nakano, Ken

    2008-01-01

    The heat balance model in the probe tip applied to atmospheric pressure plasma is constructed. Considering the natural convective heat loss, the limitation of plasma density for probe application to such a plasma is estimated. The rough limit is about n e = 10 18 m -3 . Four kind of materials (Cu, SUS, W, Al) are used for probe tips, and are tested in DC atmospheric pressure discharge. Heat conductivity is found to be a more important property than melting point in design of probes in high pressure discharge. DC atmospheric pressure discharge plasma parameters are obtained with our test probes. Obtained density is the order of 10 17 m -3 and does not contradict with the above density limitation. Change of space potential in air/Ar plasma is also confirmed.

  2. Theoretical Study of Plasma Parameters Dependence on Gas Temperature in an Atmospheric Pressure Argon Microwave Discharge

    International Nuclear Information System (INIS)

    Pencheva, M.; Benova, E.; Zhelyazkov, I.

    2008-01-01

    The gas temperature is an important parameter in many applications of atmospheric pressure microwave discharges (MW). That is why it is necessary to study the influence of that temperature on the plasma characteristics. Our investigation is based on a self-consistent model including the wave electrodynamics and gas-discharge kinetics. We adopt a blocks' energy structure of the argon excited atom. More specifically, we consider 7 different blocks of states, namely 4s, 4p, 3d, 5s, 5p, 4d, and 6s. Each block k is characterized by its effective energy uk (derived as an average energy of all levels in the block), as well as its effective g-factor and population. The argon dimmer, atomic and molecular ions are also taken into account in the model. We solve the Boltzmann equation in order to get the electron energy distribution function and the necessary rate constants of the elementary processes. The collisional-radiative part of the model is based on 87 processes. As a result we obtain the electron and ions' number densities, mean electron energy, mean power for sustaining an electron--ion pair in the discharge bulk, as well as the population of the excited blocks of states of the argon atom as functions of the gas temperature

  3. Perspective: The physics, diagnostics, and applications of atmospheric pressure low temperature plasma sources used in plasma medicine

    Science.gov (United States)

    Laroussi, M.; Lu, X.; Keidar, M.

    2017-07-01

    Low temperature plasmas have been used in various plasma processing applications for several decades. But it is only in the last thirty years or so that sources generating such plasmas at atmospheric pressure in reliable and stable ways have become more prevalent. First, in the late 1980s, the dielectric barrier discharge was used to generate relatively large volume diffuse plasmas at atmospheric pressure. Then, in the early 2000s, plasma jets that can launch cold plasma plumes in ambient air were developed. Extensive experimental and modeling work was carried out on both methods and much of the physics governing such sources was elucidated. Starting in the mid-1990s, low temperature plasma discharges have been used as sources of chemically reactive species that can be transported to interact with biological media, cells, and tissues and induce impactful biological effects. However, many of the biochemical pathways whereby plasma affects cells remain not well understood. This situation is changing rather quickly because the field, known today as "plasma medicine," has experienced exponential growth in the last few years thanks to a global research community that engaged in fundamental and applied research involving the use of cold plasma for the inactivation of bacteria, dental applications, wound healing, and the destruction of cancer cells/tumors. In this perspective, the authors first review the physics as well as the diagnostics of the principal plasma sources used in plasma medicine. Then, brief descriptions of their biomedical applications are presented. To conclude, the authors' personal assessment of the present status and future outlook of the field is given.

  4. Experimental investigation of gas heating and dissociation in a microwave plasma torch at atmospheric pressure

    International Nuclear Information System (INIS)

    Su, Liu; Kumar, Rajneesh; Ogungbesan, Babajide; Sassi, Mohamed

    2014-01-01

    Highlights: • Atmospheric-pressure microwave plasma torch. • Gas heating and dissociation. • Parametric studies of plasma operating conditions. • Local thermal equilibrium plasma. - Abstract: Experimental investigations are made to understand gas heating and dissociation in a microwave (MW) plasma torch at atmospheric pressure. The MW induced plasma torch operates at 2.45 GHz frequency and up to 2 kW power. Three different gas mixtures are injected in the form of axial flow and swirl flow in a quartz tube plasma torch to experimentally investigate the MW plasma to gas energy transfer. Air–argon, air–air and air–nitrogen plasmas are formed and their operational ranges are determined in terms of gas flow rates and MW power. Visual observations, optical emission spectroscopy and K-type thermocouple measurements are used to characterize the plasma. The study reveals that the plasma structure is highly dependent on the carrier gas type, gas flow rate, and MW power. However, the plasma gas temperature is shown not to vary much with these parameters. Further spectral and analytical analysis show that the plasma is in thermal equilibrium and presents very good energy coupling between the microwave power and gas heating and dissociation. The MW plasma torch outlet temperature is also measured and found to be suitable for many thermal heating and chemical dissociation applications

  5. Plasma properties and atomic processes at medium and high pressures

    International Nuclear Information System (INIS)

    Drawin, H.W.

    1979-01-01

    When the state of a plasma deviates from local thermodynamic equilibrium (L.T.E.) the equilibrium relations cannot be applied. The thermodynamic properties must then be described on the basis of models in which the individual atomic properties and elementary reactions intervene. The first part of the paper gives a schematic description of a plasma suffering power input, power losses and external constraints in the form of initial and boundary conditions. The rate equations for particle density, momentum and energy of open systems are summarized, including nuclear reactions. The second part gives a review of the progress made in understanding the properties of special types of non-L.T.E. plasmas such as glow discharge plasmas, negative ion plasmas (with application to the physics of SF 6 circuit-breakers) and Tokamak plasmas on the basis of these rate equations

  6. Intracellular effects of atmospheric-pressure plasmas on melanoma cancer cells

    Energy Technology Data Exchange (ETDEWEB)

    Ishaq, M., E-mail: ishaqmusarat@gmail.com [Peter MacCallum Cancer Centre, East Melbourne, VIC 3002 (Australia); Comonwealth Scientific and Industrial Research Organization, Sydney, New South Wales (Australia); Bazaka, K. [Institute for Health and Biomedical Innovation, School of Chemistry, Physics and Mechanical Engineering, Queensland University of Technology, Brisbane, QLD 4000 (Australia); Ostrikov, K. [Comonwealth Scientific and Industrial Research Organization, Sydney, New South Wales (Australia); Institute for Health and Biomedical Innovation, School of Chemistry, Physics and Mechanical Engineering, Queensland University of Technology, Brisbane, QLD 4000 (Australia)

    2015-12-15

    Gas discharge plasmas formed at atmospheric pressure and near room temperature have recently been shown as a promising tool for cancer treatment. The mechanism of the plasma action is attributed to generation of reactive oxygen and nitrogen species, electric fields, charges, and photons. The relative importance of different modes of action of atmospheric-pressure plasmas depends on the process parameters and specific treatment objects. Hence, an in-depth understanding of biological mechanisms that underpin plasma-induced death in cancer cells is required to optimise plasma processing conditions. Here, the intracellular factors involved in the observed anti-cancer activity in melanoma Mel007 cells are studied, focusing on the effect of the plasma treatment dose on the expression of tumour suppressor protein TP73. Over-expression of TP73 causes cell growth arrest and/or apoptosis, and hence can potentially be targeted to enhance killing efficacy and selectivity of the plasma treatment. It is shown that the plasma treatment induces dose-dependent up-regulation of TP73 gene expression, resulting in significantly elevated levels of TP73 RNA and protein in plasma-treated melanoma cells. Silencing of TP73 expression by means of RNA interference inhibited the anticancer effects of the plasma, similar to the effect of caspase inhibitor z-VAD or ROS scavenger N-acetyl cysteine. These results confirm the role of TP73 protein in dose-dependent regulation of anticancer activity of atmospheric-pressure plasmas.

  7. Intracellular effects of atmospheric-pressure plasmas on melanoma cancer cells

    Science.gov (United States)

    Ishaq, M.; Bazaka, K.; Ostrikov, K.

    2015-12-01

    Gas discharge plasmas formed at atmospheric pressure and near room temperature have recently been shown as a promising tool for cancer treatment. The mechanism of the plasma action is attributed to generation of reactive oxygen and nitrogen species, electric fields, charges, and photons. The relative importance of different modes of action of atmospheric-pressure plasmas depends on the process parameters and specific treatment objects. Hence, an in-depth understanding of biological mechanisms that underpin plasma-induced death in cancer cells is required to optimise plasma processing conditions. Here, the intracellular factors involved in the observed anti-cancer activity in melanoma Mel007 cells are studied, focusing on the effect of the plasma treatment dose on the expression of tumour suppressor protein TP73. Over-expression of TP73 causes cell growth arrest and/or apoptosis, and hence can potentially be targeted to enhance killing efficacy and selectivity of the plasma treatment. It is shown that the plasma treatment induces dose-dependent up-regulation of TP73 gene expression, resulting in significantly elevated levels of TP73 RNA and protein in plasma-treated melanoma cells. Silencing of TP73 expression by means of RNA interference inhibited the anticancer effects of the plasma, similar to the effect of caspase inhibitor z-VAD or ROS scavenger N-acetyl cysteine. These results confirm the role of TP73 protein in dose-dependent regulation of anticancer activity of atmospheric-pressure plasmas.

  8. Pressure effect on crystallization kinetics in Zr46.8Ti8.2Cu7.5Ni10Be27.5 bulk glass

    DEFF Research Database (Denmark)

    Jiang, Jianzhong; Gerward, Leif; Xu, Y.S.

    2002-01-01

    Crystallization kinetics of a Zr46.8Ti8.2Cu7.5Ni10Be27.5 bulk glass in the supercooled liquid region have been investigated by performing in situ high-temperature and high-pressure x-ray diffraction measurements using synchrotron radiation. A pressure-time-temperature-transformation diagram......, describing the onset of crystallization as a function of time during isothermal annealing under pressure, is presented. Different pressure dependences of crystallization kinetics in the temperature range for the glass have been observed and further be explained by a model of competing processes...

  9. Promoted cell and material interaction on atmospheric pressure plasma treated titanium

    International Nuclear Information System (INIS)

    Han, Inho; Vagaska, Barbora; Seo, Hyok Jin; Kang, Jae Kyeong; Kwon, Byeong-Ju; Lee, Mi Hee; Park, Jong-Chul

    2012-01-01

    Surface carbon contamination is a natural phenomenon. However, it interferes with cell-biomaterial interaction. In order to eliminate the interference, atmospheric pressure plasma treatment was employed. Dielectric barrier discharge treatment of titanium surface for less than 10 min turned titanium super-hydrophilic. Adsorption of fibronectin which is the major cell adhesive protein increased after plasma treatment. Cell attachment parameters of osteoblast cells such as population, cell area, perimeter, Feret's diameter and cytoskeleton development were also enhanced. Cell proliferation increased on the plasma treated titanium. In conclusion, dielectric barrier discharge type atmospheric pressure plasma system is effective to modify titanium surface and the modified titanium promotes cell and material interactions.

  10. Resistive internal kink modes in a tokamak with high-pressure plasma

    International Nuclear Information System (INIS)

    Kuvshinov, B.N.; Mikhajlovskij, A.B.; Tatarinov, E.G.

    1988-01-01

    Theory of resistive internal kink modes in a tokamak with high-pressure plasma is developed. Equation for Fourie-image of disturbed displacment in a resistive layer ie derived with regard to effects of the fourth order by plasma pressure within the framework of single-liquid approach. In its structure this equation coincides with a similar equation for resistive balloon modes and has an exact solution expressed by degenerated hypergeometric function. A general dispersion equation for resistive kink modes is derived with regard to the effects indicated. It is shown that plasma pressure finiteness leads to the reduction of reconnection and tyring-mode increments

  11. Non-equilibrium plasma chemistry at high pressure and its applications

    International Nuclear Information System (INIS)

    Bai Xiyao; Zhang Zhitao; Bai Mindong; Zhu Qiaoying

    2000-01-01

    A review is presented of research and development of gas discharge and non-equilibrium plasma including, new ideas of non-equilibrium plasma at high gas pressure. With special technology, strong electric fields (>400 Td) can be achieved by which electrons are accelerated suddenly, becoming high energy electrons (> 10 eV) at high pressure. On impact with the electrons, the gas molecules dissociate into ions, atomic ions, atoms and free radicals, and new substances or molecules can be synthesized through custom design. Chemical reaction difficult to achieve by conventional method can be realized or accelerated. Non-equilibrium plasma chemistry at high pressure has wide application prospects

  12. Surface-nitriding treatment of steels using microwave-induced nitrogen plasma at atmospheric pressure

    International Nuclear Information System (INIS)

    Sato, Shigeo; Arai, Yuuki; Yamashita, Noboru; Kojyo, Atsushi; Kodama, Kenji; Ohtsu, Naofumi; Okamoto, Yukio; Wagatsuma, Kazuaki

    2012-01-01

    A rapid surface-nitriding system using microwave-induced nitrogen plasma at atmospheric pressure was developed for modifying iron and steel surfaces. Since the conventional plasma nitriding technique requires a low-pressure atmosphere in the treatment chamber, the population of excited nitrogen molecules in the plasma is limited. Accordingly, several hours are required for nitriding treatment. By contrast, the developed nitriding system can use atmospheric-pressure plasma through application of the Okamoto cavity for excitation of nitrogen plasma. The high population of excited nitrogen molecules induced by the atmospheric-pressure plasma allowed the formation of a nitriding layer that was several micrometers thick within 1 min and produced an expanded austenite iron phase with a high nitrogen concentration close to the solubility limit on the iron substrate. In addition, the nitriding treatment on high-chromium steel was performed by introducing a reducing gas such as NH 3 and H 2 into the treatment chamber. While the nitriding reaction did not proceed in a simple N 2 atmosphere due to surface oxidation, the surface reduction induced by the NH 3 or H 2 gas promoted the nitriding reaction at the surface. These nitriding phenomena characteristics of the atmospheric-pressure plasma are discussed in this paper based on the effects of the specimen temperature and plasma atmosphere on the thickness, the chemical states, and the nitride compounds of the nitrided layer as investigated by X-ray diffraction, glow-discharge optical emission spectroscopy, and X-ray photoelectron spectroscopy.

  13. G-protein activity in Percoll-purified plasma membranes, bulk plasma membranes, and low-density plasma membranes isolated from rat cerebral cortex

    Czech Academy of Sciences Publication Activity Database

    Bouřová, Lenka; Stöhr, Jiří; Lisý, Václav; Rudajev, Vladimír; Novotný, Jiří; Svoboda, Petr

    2009-01-01

    Roč. 15, č. 4 (2009), BR111-BR122 ISSN 1234-1010 R&D Projects: GA MŠk(CZ) LC554; GA MŠk(CZ) LC06063; GA ČR(CZ) GA309/06/0121; GA AV ČR(CZ) IAA500110606 Institutional research plan: CEZ:AV0Z50110509 Keywords : rat cerebral cortex * plasma membrane * G-protein activity Subject RIV: CE - Biochemistry Impact factor: 1.543, year: 2009

  14. Cold plasma source for bacterial inactivation at atmospheric pressure

    DEFF Research Database (Denmark)

    Chen, Weifeng; Stamate, Eugen; Mejlholm, Ole

    A dielectric-barrier discharge system for cold plasma production was built for bacterial inactivation purpose. The eect of cold plasma treatment on sensory properties of seafood products was studied to establish how the sensory properties (e.g. appearance, texture) of seafood were aected by diere...

  15. Determination of the bulk modulus of hydroxycancrinite, a possible zeolitic precursor in geopolymers, by high-pressure synchrotron X-ray diffraction

    KAUST Repository

    Oh, Jae Eun

    2011-11-01

    Crystalline zeolitic materials, such as hydroxycancrinite, hydroxysodalite, herschelite and nepheline, are often synthesized from geopolymerization using fly-ash and solutions of NaOH at high temperatures. Comprised mainly of 6-membered aluminosilicate rings that act as basic building units, their crystal structures may provide insight into the reaction products formed in NaOH-activated fly ash-based geopolymers. Recent research indicates that the hydroxycancrinite and hydroxysodalite may play an important role as possible analogues of zeolitic precursor in geopolymers. Herein is reported a high pressure synchrotron study of the behavior of hydroxycancrinite exposed to pressures up to 6.1 GPa in order to obtain its bulk modulus. A refined equation of state for hydroxycancrinite yielded a bulk modulus of Ko = 46 ± 5 GPa (assuming Ko′ = 4.0) for a broad range of applied pressure. When low pressure values are excluded from the fit and only the range of 2.5 and 6.1 GPa is considered, the bulk modulus of hydroxycancrinite was found to be Ko = 46.9 ± 0.9 GPa (Ko′ = 4.0 ± 0.4, calculated). Comparison with the literature shows that all zeolitic materials possessing single 6-membered rings (i.e., hydroxycancrinite, sodalite and nepheline) have similar bulk moduli. © 2011 Elsevier Ltd. All rights reserved.

  16. A potential route to synthesize imporous MgB{sub 2} bulks by pretreatment of B powder at ambient pressure

    Energy Technology Data Exchange (ETDEWEB)

    Pan, X F; Zhou, J D; Zhao, Y [Key Laboratory of Magnetic Levitation and Maglev Trains (Ministry of Education of China), Superconductivity R and D Center (SRDC), Mail Stop 165, Southwest Jiaotong University, Chengdu, Sichuan 610031 (China); Cheng, C H [Superconductivity Research Group, School of Materials Science and Engineering, University of New South Wales, Sydney, 2052 NSW (Australia)], E-mail: yzhao@home.swjtu.edu.cn

    2009-04-15

    Imporous MgB{sub 2} bulks with a density of 1.82 g cm{sup -3} have been synthesized by pretreatment of B powder in an in situ solid-state reaction at ambient pressure. The results show that the MgB{sub 2} with B powder pretreatment has a significant improvement in J{sub c}, B{sub irr}, microstructure and intergranular coupling, but with no decrease of T{sub c}. At 20 K and 4 T, the J{sub c} is enhanced by 4 times by the pretreatment of the B powder. For the B pretreated MgB{sub 2}, the B{sub irr} at 20 K reaches 5 T and J{sub c} at 10 K and 6 T reaches 2200 A cm{sup -2}, compared to 4.2 T and 670 A cm{sup -2} for the B-not-pretreated MgB{sub 2}. It is argued that the small amounts of highly dispersed carbon in B powder may enhance the mobility of B particles during the reaction of B and Mg, which avoids the formation of voids in the positions of Mg particles.

  17. Study of Low Pressure Cold Plasma on Moisture Properties of Polyester Fabric

    Directory of Open Access Journals (Sweden)

    E. Masaeli

    2007-06-01

    Full Text Available Low temperature plasma technology is well established in surface modification of polymer materials on industrial scale. This method modifies surface properties of polymers without chemicals, manual work and reducing chemicals and energy consumption. In this study, low pressure plasma treatment was used to develop hydrophilic properties of polyethylene terephthalate (PET fabrics. It was found that, plasma treatment had a significant effect on the hydrophilicity properties of PET fibers. Plasma treatment increases wetting, wicking and electric conduction of fibers but the recovery of fibers was not affected by the plasma treatment. Also, scanning electron microscopy (SEM micrograph show some surface fibers etching that created some voids.

  18. Cellular and molecular responses of Neurospora crassa to non-thermal plasma at atmospheric pressure

    Science.gov (United States)

    Park, Gyungsoon; Ryu, Young H.; Hong, Young J.; Choi, Eun H.; Uhm, Han S.

    2012-02-01

    Filamentous fungi have been rarely explored in terms of plasma treatments. This letter presents the cellular and molecular responses of the filamentous fungus Neurospora crassa to an argon plasma jet at atmospheric pressure. The viability and cell morphology of N. crassa spores exposed to plasma were both significantly reduced depending on the exposure time when treated in water. The intracellular genomic DNA content was dramatically reduced in fungal tissues after a plasma treatment and the transcription factor tah-3 was found to be required for fungal tolerance to a harsh plasma environment.

  19. Atmospheric-Pressure Plasma Jet Surface Treatment for Use in Improving Adhesion

    Energy Technology Data Exchange (ETDEWEB)

    Kuettner, Lindsey Ann [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-09-06

    Atmospheric-pressure plasma jets (APPJs) are a method of plasma treatment that plays an important role in material processing and modifying surface properties of materials, especially polymers. Gas plasmas react with polymer surfaces in numerous ways such as oxidation, radical formation, degradation, and promotion of cross-linking. Because of this, gas and plasma conditions can be explored for chosen processes to maximize desired properties. The purpose of this study is to investigate plasma parameters in order to modify surface properties for improved adhesion between aluminum and epoxy substrates using two types of adhesives. The background, results to date, and future work will be discussed.

  20. Selective killing of ovarian cancer cells through induction of apoptosis by nonequilibrium atmospheric pressure plasma

    International Nuclear Information System (INIS)

    Iseki, Sachiko; Tanaka, Hiromasa; Kondo, Hiroki; Hori, Masaru; Nakamura, Kae; Hayashi, Moemi; Kajiyama, Hiroaki; Kikkawa, Fumitaka; Kano, Hiroyuki

    2012-01-01

    Two independent ovarian cancer cell lines and fibroblast controls were treated with nonequilibrium atmospheric pressure plasma (NEAPP). Most ovarian cancer cells were detached from the culture dish by continuous plasma treatment to a single spot on the dish. Next, the plasma source was applied over the whole dish using a robot arm. In vitro cell proliferation assays showed that plasma treatments significantly decreased proliferation rates of ovarian cancer cells compared to fibroblast cells. Flow cytometry and western blot analysis showed that plasma treatment of ovarian cancer cells induced apoptosis. NEAPP could be a promising tool for therapy for ovarian cancers.

  1. Optical Emission Spectroscopy of an Atmospheric Pressure Plasma Jet During Tooth Bleaching Gel Treatment.

    Science.gov (United States)

    Šantak, Vedran; Zaplotnik, Rok; Tarle, Zrinka; Milošević, Slobodan

    2015-11-01

    Optical emission spectroscopy was performed during atmospheric pressure plasma needle helium jet treatment of various tooth-bleaching gels. When the gel sample was inserted under the plasma plume, the intensity of all the spectral features increased approximately two times near the plasma needle tip and up to two orders of magnitude near the sample surface. The color change of the hydroxylapatite pastille treated with bleaching gels in conjunction with the atmospheric pressure plasma jet was found to be in correlation with the intensity of OH emission band (309 nm). Using argon as an additive to helium flow (2 L/min), a linear increase (up to four times) of OH intensity and, consequently, whitening (up to 10%) of the pastilles was achieved. An atmospheric pressure plasma jet activates bleaching gel, accelerates OH production, and accelerates tooth bleaching (up to six times faster).

  2. Surface modification of polylactic acid films by atmospheric pressure plasma treatment

    Science.gov (United States)

    Kudryavtseva, V. L.; Zhuravlev, M. V.; Tverdokhlebov, S. I.

    2017-09-01

    A new approach for the modification of polylactic acid (PLA) materials using atmospheric pressure plasma (APP) is described. PLA films plasma exposure time was 20, 60, 120 s. The surface morphology and wettability of the obtained PLA films were investigated by atomic force microscopy (AFM) and the sitting drop method. The atmospheric pressure plasma increased the roughness and surface energy of PLA film. The wettability of PLA has been improved with the application of an atmospheric plasma surface treatment. It was shown that it is possible to obtain PLA films with various surface relief and tunable wettability. Additionally, we demonstrated that the use of cold atmospheric pressure plasma for surface activation allows for the immobilization of bioactive compounds like hyaluronic acid (HA) on the surface of obtained films. It was shown that composite PLA-HA films have an increased long-term hydrophilicity of the films surface.

  3. Electron ranaway and ion-ion plasma formation in afterglow low-pressure plasma of oxygen-containing gas mixtures

    Science.gov (United States)

    Kudryavtsev, Anatoly; Bogdanov, Eugene; Kosykh, Nikolay; Gutsev, Sergey

    2012-10-01

    Experimental investigation of temporal evolution of charged plasma species in afterglow plasma of oxygen-containing mixtures have been investigated. The probe VAC and the time dependence of the saturation positive and negative particles currents to a probe in a fixed bias voltage were performed. The decay of afterglow low-pressure electronegative gas plasmas take place in two distinct stages (the electron-ion stage, and the ion-ion stage) as it was shown in [1] for pure oxygen. In the first stage, the negative ions are locked within a discharge volume and plasma is depleted of electrons and positive ions. The electron density decay is faster, than exponential, and practically all electrons leave plasma volume during finite time followed by the ion--ion (electron-free) plasma formation. The decay of the ion-ion plasma depends on the presence of detachment. With a large content of electronegative gas (oxygen) in a mixture, when there is a ``detachment particles,'' a small fraction of the electrons appearing as a result of the detachment continue to hold all negative ions in the discharge volume. In this case, the densities of all charged plasma components decay according to the same exponential law with a characteristic detachment time. At a low oxygen content in the gas mixture there is no detachment and plasma decays by an ion--ion ambipolar diffusion mechanism.[4pt][1]. S.A.Gutsev, A.A.Kudryavtsev, V.A.Romanenko. Tech.Phys. 40, 1131, (1995).

  4. Single channel atmospheric pressure transporting plasma and plasma stream demultiplexing: physical characterization and application to E. coli bacteria inactivation

    International Nuclear Information System (INIS)

    Valinataj Omran, A; Arefi-Khonsari, F; Sohbatzadeh, F; Siadati, S N; Hosseinzadeh Colagar, A; Akishev, Y

    2017-01-01

    In this article, we developed transporting plasma sources that operate at atmospheric pressure. The effect of electrode configuration on plasma transporting was investigated. In order to increase the transporting plasma cross-section, we converted a plasma stream into four plasma channels by a cylindrical housing. Electron excitation and rotational temperatures were estimated using optical emission spectroscopy. Furthermore, the electrical and temporal characteristics of the plasma, discharge power and charge deposition on the target were investigated. The propagation characteristics of single and multi-channel transporting plasma were compared with the same cross-sectional area. Two configurations for multi-channels were designed for this purpose. Escherichia coli bacteria were exposed to the single and multi-channel transporting discharge for different time durations. After exposure, the results indicated that the inactivation zones were significantly increased by a multi-channel transporting plasma. Finally, E. coli inactivation by those plasma apparatuses was compared with that of several standard antimicrobial test discs such as Gentamicin, Tetracycline, Amoxicillin and Cefixime. (paper)

  5. Design and experiment of high-current low-pressure plasma-cathode e-gun

    International Nuclear Information System (INIS)

    Xie Wenkai; Li Xiaoyun; Wang Bin; Meng Lin; Yan Yang; Gao Xinyan

    2006-01-01

    The preliminary design of a new high-power low pressure plasma-cathode e-gun is presented. Based on the hollow cathode effect and low-pressure glow discharge empirical formulas, the hollow cathode, the accelerating gap, and the working gas pressure region are given. The general experimental device of the low-pressure plasma cathode electron-gun generating high current density e-beam source is shown. Experiments has been done in continuous filled-in gases and gases-puff condition, and the discharging current of 150-200 A, the width of 60 μs and the collector current of 30-80 A, the width of 60 μs are obtained. The results show that the new plasma cathode e-gun can take the place of material cathode e-gun, especially in plasma filled microwave tubes. (authors)

  6. Plasma catecholamine level and portal venous pressure as guides to prognosis in patients with cirrhosis

    DEFF Research Database (Denmark)

    Tage-Jensen, U; Henriksen, Jens Henrik Sahl; Christensen, E

    1988-01-01

    , and the presence of ascites or cardiovascular disease were of significant prognostic value. In a multivariate analysis (Cox regression model), plasma noradrenaline concentration, portal pressure, serum bilirubin concentration, and the presence of ascites and cardiovascular disease remained significant independent...

  7. Fluorination of poly(dimethylsiloxane) surfaces by low pressure CF4 plasma : physicochemical and antifouling properties

    NARCIS (Netherlands)

    Cordeiro, A.L.; Nitschke, M.; Janke, A.; Helbig, R.; D'Souza, F.; Donnelly, G.T.; Willemsen, P.R.; Werner, C.

    2009-01-01

    Fluorinated surface groups were introduced into poly(dimethylsiloxane) (PDMS) coatings by plasma treatment using a low pressure radio frequency discharge operated with tetrafluoromethane. Substrates were placed in a remote position downstream the discharge. Discharge power and treatment time were

  8. Fructooligosaccharides integrity after atmospheric cold plasma and high-pressure processing of a functional orange juice.

    Science.gov (United States)

    Almeida, Francisca Diva Lima; Gomes, Wesley Faria; Cavalcante, Rosane Souza; Tiwari, Brijesh K; Cullen, Patrick J; Frias, Jesus Maria; Bourke, Paula; Fernandes, Fabiano A N; Rodrigues, Sueli

    2017-12-01

    In this study, the effect of atmospheric pressure cold plasma and high-pressure processing on the prebiotic orange juice was evaluated. Orange juice containing 7g/100g of commercial fructooligosaccharides (FOS) was directly and indirectly exposed to a plasma discharge at 70kV with processing times of 15, 30, 45 and 60s. For high-pressure processing, the juice containing the same concentration of FOS was treated at 450MPa for 5min at 11.5°C in an industrial equipment (Hyperbaric, model: 300). After the treatments, the fructooligosaccharides were qualified and quantified by thin layer chromatography. The organic acids and color analysis were also evaluated. The maximal overall fructooligosaccharides degradation was found after high-pressure processing. The total color difference was pressure and plasma processing. citric and ascorbic acid (Vitamin C) showed increased content after plasma and high-pressure treatment. Thus, atmospheric pressure cold plasma and high-pressure processing can be used as non-thermal alternatives to process prebiotic orange juice. Copyright © 2017 Elsevier Ltd. All rights reserved.

  9. Reactive species in non-equilibrium atmospheric-pressure plasmas: Generation, transport, and biological effects

    Energy Technology Data Exchange (ETDEWEB)

    Lu, X., E-mail: luxinpei@hotmail.com [State Key Laboratory of Advanced Electromagnetic Engineering and Technology, Huazhong University of Science and Technology, Wuhan, Hubei 430074 (China); IFSA Collaborative Innovation Center, Shanghai Jiao Tong University, Shanghai 200240 (China); Naidis, G.V. [Joint Institute for High Temperatures, Russian Academy of Sciences, Moscow 125412 (Russian Federation); Laroussi, M. [Plasma Engineering & Medicine Institute, Old Dominion University, Norfolk, VA 23529 (United States); Reuter, S. [Leibniz Institute for Plasma Science and Technology, Felix-Hausdorff-Strasse 2, 17489 Greifswald (Germany); Graves, D.B. [Department of Chemical and Biomolecular Engineering, University of California, Berkeley, CA 94720 (United States); Ostrikov, K. [Institute for Future Environments, Queensland University of Technology, Brisbane, QLD 4000 (Australia); School of Physics, Chemistry, and Mechanical Engineering, Queensland University of Technology, Brisbane, QLD 4000 (Australia); Commonwealth Scientific and Industrial Research Organization, P.O.Box 218, Lindfield, NSW 2070 (Australia); School of Physics, The University of Sydney, Sydney, NSW 2006 (Australia)

    2016-05-04

    Non-equilibrium atmospheric-pressure plasmas have recently become a topical area of research owing to their diverse applications in health care and medicine, environmental remediation and pollution control, materials processing, electrochemistry, nanotechnology and other fields. This review focuses on the reactive electrons and ionic, atomic, molecular, and radical species that are produced in these plasmas and then transported from the point of generation to the point of interaction with the material, medium, living cells or tissues being processed. The most important mechanisms of generation and transport of the key species in the plasmas of atmospheric-pressure plasma jets and other non-equilibrium atmospheric-pressure plasmas are introduced and examined from the viewpoint of their applications in plasma hygiene and medicine and other relevant fields. Sophisticated high-precision, time-resolved plasma diagnostics approaches and techniques are presented and their applications to monitor the reactive species and plasma dynamics in the plasma jets and other discharges, both in the gas phase and during the plasma interaction with liquid media, are critically reviewed. The large amount of experimental data is supported by the theoretical models of reactive species generation and transport in the plasmas, surrounding gaseous environments, and plasma interaction with liquid media. These models are presented and their limitations are discussed. Special attention is paid to biological effects of the plasma-generated reactive oxygen and nitrogen (and some other) species in basic biological processes such as cell metabolism, proliferation, survival, etc. as well as plasma applications in bacterial inactivation, wound healing, cancer treatment and some others. Challenges and opportunities for theoretical and experimental research are discussed and the authors’ vision for the emerging convergence trends across several disciplines and application domains is presented to

  10. Measurement of electron density in the atmospheric pressure helium plasma jet by using a dielectric probe

    International Nuclear Information System (INIS)

    Qi Bing; Zhou Qiujiao; Pan Lizhu; Zhang Mengdie; Huang Jianjun

    2014-01-01

    The electron densities in the atmospheric pressure helium plasma were calculated by means of electron drift velocity and the jet velocity respectively. The electron velocity and jet velocity can be calculated by means of helium plasma jet current measured by a dielectric probe and plasma discharge current signal measured by voltage probes. The results show that the estimated electron densities of the helium plasma jet calculated from electron drift velocity and the jet velocity are in the order of 10 11 cm -3 and they increase with applied voltage. There is a little fluctuation in the value of the electron density along the jet axis of the plasma. This result is the same as the measured electron density in atmospheric pressure helium non-thermal plasma jet by using a Rogowski coil and a Langmuir probe. This is in one order lower than the electron density measured by microwave antenna. (authors)

  11. Plasma spray formed near-net-shape MoSi2-Si3N4 bulk nanocomposites-structure property evaluation

    International Nuclear Information System (INIS)

    Hong, S.J.; Viswanathan, V.; Rea, K.; Patil, S.; Deshpande, S.; Georgieva, P.; McKechnie, T.; Seal, S.

    2005-01-01

    This article, for the first time, presents the challenges toward the successful consolidation of near-net-shape bulk MoSi 2 -Si 3 N 4 -SiC nanocomposite using plasma spray forming. A detailed characterization of the spray formed bulk nanocomponent has been performed using optical microscopy (OM), scanning electron microscopy (SEM), scanning transmission electron microscopy (STEM), and Vickers hardness testing. Vickers hardness (900 Hv) and fracture toughness (∼>5 MPa m 1/2 ) of the nanocomposite showed a little deviation from the expected, which might be due to the difference in the particle (Si 3 N 4 ) size and their distribution in the MoSi 2 matrix as a function of component thickness. Relatively higher hardness is attributed to the retention of the nanostructure in the composite. In addition, the as fabricated bulk nanocomposite showed enhanced oxidation resistance

  12. Characterization of an atmospheric pressure air plasma source for polymer surface modification

    Science.gov (United States)

    Yang, Shujun; Tang, Jiansheng

    2013-10-01

    An atmospheric pressure air plasma source was generated through dielectric barrier discharge (DBD). It was used to modify polyethyleneterephthalate (PET) surfaces with very high throughput. An equivalent circuit model was used to calculate the peak average electron density. The emission spectrum from the plasma was taken and the main peaks in the spectrum were identified. The ozone density in the down plasma region was estimated by Absorption Spectroscopy. NSF and ARC-ODU

  13. Second derivative Langmuir probe diagnostics of gas discharge plasma at intermediate pressures (review article)

    International Nuclear Information System (INIS)

    Popov, Tsv K; Dimitrova, M; Dias, F M; Tsaneva, V N; Stelmashenko, N A; Blamire, M G; Barber, Z H

    2006-01-01

    The second-derivative Langmuir probe method for precise determination of the plasma potential, the electron energy distribution function (respectively the electron temperature,) and the electron density of gas discharge plasma at intermediate pressures (100-1000 Pa) is reviewed. Results of applying the procedure proposed to different kinds of gas discharges are presented. Factors affecting the accuracy of the plasma characteristics evaluated are discussed

  14. Study of the low-pressure plasma effect on polypropylene nonwovens

    International Nuclear Information System (INIS)

    Lopez, R.; Pascual, M.; Calvo, O.; Boronat, T.; Balart, R.

    2010-01-01

    In this work we have used low-pressure plasma with a gas based on methane and oxygen mixture to improve wettability and durability of a PP nonwoven fabrics. The obtained results show good durability with the use of methane-oxygen plasma mixture gas. The effects of the plasma are similar to a plasmapolymerization process but in this case we obtain hydrophilic properties with high durability. The surface does not suffer important changes and the roughness of the material remains constant.

  15. Study of the low-pressure plasma effect on polypropylene nonwovens

    Science.gov (United States)

    López, R.; Boronat, T.; Pascual, M.; Calvo, O.; Balart, R.

    2010-06-01

    In this work we have used low-pressure plasma with a gas based on methane and oxygen mixture to improve wettability and durability of a PP nonwoven fabrics. The obtained results show good durability with the use of methane-oxygen plasma mixture gas. The effects of the plasma are similar to a plasmapolymerization process but in this case we obtain hydrophilic properties with high durability. The surface does not suffer important changes and the roughness of the material remains constant.

  16. Modified drug release using atmospheric pressure plasma deposited siloxane coatings

    International Nuclear Information System (INIS)

    Dowling, D P; Law, V J; Ardhaoui, M; Stallard, C; Maher, S; Keenan, A

    2016-01-01

    This pilot study evaluates the potential of atmospheric plasma polymerised coatings to modify the rate of drug release from polymeric substrates. The antibiotic rifampicin was deposited in a prototype multi-layer drug delivery system, consisting of a nebulized layer of active drug between a base layer of TEOS deposited on a plastic substrate (polystyrene) and an overlying layer of plasma polymerised PDMS. The polymerised TEOS and PDMS layers were deposited using a helium atmospheric plasma jet system. Elution of rifampicin was measured using UV–VIS spectroscopy, in addition to a antimicrobial well diffusion assay with an established indicator organism. The multi-layered plasma deposited coatings significantly extended the duration of release of the rifampicin from 24 h for the uncoated polymer to 144 h for the coated polymer. (paper)

  17. Cold atmospheric pressure plasma treatment of ready-to-eat meat

    DEFF Research Database (Denmark)

    Röd, Sara Katrine Solhøj; Hansen, Flemming; Leipold, Frank

    Sliced ready-to-eat (RTE) meat products are susceptible to growth of the foodborne pathogenic bacterium, Listeria monocytogenes. Cold atmospheric pressure plasma (CAPP) may be applicable for surface decontamination in sealed bags thus avoiding recontamination. Plasmas (Fig. 1), created in neutral...

  18. Effect of Atmospheric Pressure Plasma Modification on Polyimide and Adhesive Joining with Titanium

    NARCIS (Netherlands)

    Akram, M.; Jansen, K.M.B.; Ernst, L.J.; Bhowmik, S.; Ajeesh, G.; Ahmed, S.; Chakraborty, D.

    2015-01-01

    This investigation highlights the effect of surface modification on polyimide by atmospheric pressure plasma treatment with different exposure time. Surface modification of polymer by plasma treatment essentially creates physical and chemical changes such as cross-linking and formation of free

  19. Study of ion oscillations in a beam-plasma system in regimes of very low pressure

    Energy Technology Data Exchange (ETDEWEB)

    Silva, M.E.F.; Cabral, J.A.C.

    1982-03-01

    The ion oscillations that are excited with f approx. = f/sub ci/ in a beam-plasma system in very low pressure regimes were studied. The oscillations propagate in the azimuthal direction (k/sub z/=0) in the m=1 mode and are excited due to convection effects associated with a rotation of the plasma column.

  20. Influence of emitter temperature on the energy deposition in a low-pressure plasma

    International Nuclear Information System (INIS)

    Levko, Dmitry; Raja, Laxminarayan L.

    2016-01-01

    The influence of emitter temperature on the energy deposition into low-pressure plasma is studied by the self-consistent one-dimensional Particle-in-Cell Monte Carlo Collisions model. Depending on the emitter temperature, different modes of discharge operation are obtained. The mode type depends on the plasma frequency and does not depend on the ratio between the densities of beam and plasma electrons. Namely, plasma is stable when the plasma frequency is small. For this plasma, the energy transfer from emitted electrons to plasma electrons is inefficient. The increase in the plasma frequency results first in the excitation of two-stream electron instability. However, since the thermal velocity of plasma electrons is smaller than the electrostatic wave velocity, the resonant wave-particle interaction is inefficient for the energy deposition into the plasma. Further increase in the plasma frequency leads to the distortion of beam of emitted electrons. Then, the electrostatic wave generated due to two-stream instability decays into multiple slower waves. Phase velocities of these waves are comparable with the thermal velocity of plasma electrons which makes possible the resonant wave-particle interaction. This results in the efficient energy deposition from emitted electrons into the plasma.

  1. Dynamic behaviour of dc double anode plasma torch at atmospheric pressure

    International Nuclear Information System (INIS)

    Tu, X; Cheron, B G; Yan, J H; Cen, K F

    2007-01-01

    An original dc double anode plasma torch which provides a long-time and highly stable atmospheric plasma jet has been devised for the purpose of hazardous waste treatment. The arc fluctuations and dynamic behaviour of the argon and argon-nitrogen plasma jets under different operating conditions have been investigated by means of classical tools, such as the statistic method, fast Fourier transform (FFT) and correlation analysis. In our experiments, the takeover mode is identified as the fluctuation characteristic of the argon plasma jet while the restrike mode is typical in the argon-nitrogen plasma dynamic behaviour. In the case of pure argon, the FFT and correlation calculation results of electrical signals exhibit the only characteristic frequency of 150 Hz, which originates from the torch power and is independent of any change in the operating conditions. It indicates that the nature of fluctuations in an argon plasma jet is mainly induced by the undulation of the tri-phase rectified power supply. In contrast, besides the same low frequency bulk fluctuation, the dynamic behaviour of the argon-nitrogen plasma jet at high frequency (4.1 kHz) is ascribed to the rapid motion of both arc roots on the anode surface. In addition, it is found that each arc root attachment is rather diffused than located at a fixed position on the anode wall in the argon plasma jet, while constricted arc roots occur when nitrogen is added into argon as the plasma working gas

  2. Rare-gas liquids - Equation of state and reduced-pressure, reduced-bulk-modulus, and reduced-sound-velocity functions

    Science.gov (United States)

    Schlosser, Herbert

    1990-01-01

    This paper is concerned with verification of the applicability of the Vinet et al. (1987) universal equation of state to the liquid phase of the rare-gas elements under pressure. As previously observed in solids and liquids metals, to a good approximation, in the absence of phase transitions, plots of the logarithms of the reduced pressure function, of the reduced sound velocity, and of the reduced bulk modulus, are all linear functions of 1 - X over the entire experimental pressure range. The results obtained on the rare-gas liquids are comparable in accuracy to those obtained in previous work on solids and liquid metals.

  3. Generation of uniform atmospheric pressure argon glow plasma by ...

    Indian Academy of Sciences (India)

    In this paper, atmospheric pressure glow discharges (APGD) in argon generated in parallel plate dielectric barrier discharge ... Keywords. Atmospheric pressure glow discharge; argon glow discharge; electron density; hydrophobicity. PACS No. ... alcohol for 10 min and then dried in air. The effect of the treatment time on the ...

  4. Pressure effect of glass transition temperature in Zr46.8Ti8.2Cu7.5Ni10Be27.5 bulk metallic glass

    DEFF Research Database (Denmark)

    Jiang, Jianzhong; Roseker, W.; Sikorski, M.

    2004-01-01

    Pressure effects on glass transition temperature and supercooled liquid region of a Zr46.8Ti8.2Cu7.5Ni10Be27.5 bulk glass have been investigated by performing in situ high-temperature and high-pressure x-ray powder diffraction measurements using synchrotron radiation. The glass transition...... was detected from the change of the slope of peak position as a function of temperature. It is found that the glass transition temperature increases with pressure by 4.4 K/GPa for the Zr46.8Ti8.2Cu7.5Ni10Be27.5 bulk glass, and the supercooled liquid range decreases with pressure by 2.9 K/GPa in a pressure...... range of 0-2.2 GPa. This method opens a possibility to study the pressure effect of glass transition process in glassy systems under high pressures (>1 GPa). (C) 2004 American Institute of Physics....

  5. Nonlinear waves and solitons propagating perpendicular to the magnetic field in bi-ion plasma with finite plasma pressure

    Directory of Open Access Journals (Sweden)

    E. M. Dubinin

    2002-01-01

    Full Text Available We investigate the nature of nonlinear waves propagating transverse to the magnetic field in a bi-ion plasma including plasma pressure. By using the conservation laws derived from the multi-ion fluid equations the system may be described by a single order differential equation whose properties control the structure of the flow and the magnetic field. Compressive solitons exist in specific ranges of the characteristic Mach numbers. Various features of solitons differ in different existence "windows". For example, there are solitons that contain a strong proton rarefaction core embedded in the main compressional structure. Compressive solitons are found in a wide range of flow parameters. Finite ion pressure introduces critical Mach numbers. In contrast to a plasma consisting only of protons and electrons these singular points are reached where a specific combination of ion and electron speeds lies on particular locii, in multi-parameter space, which corresponds to the generalized "sonic point" of the compound system.

  6. plasmatis Center for Innovation Competence: Controlling reactive component output of atmospheric pressure plasmas in plasma medicine

    Science.gov (United States)

    Reuter, Stephan

    2012-10-01

    The novel approach of using plasmas in order to alter the local chemistry of cells and cell environment presents a significant development in biomedical applications. The plasmatis center for innovation competence at the INP Greifswald e.V. performs fundamental research in plasma medicine in two interdisciplinary research groups. The aim of our plasma physics research group ``Extracellular Effects'' is (a) quantitative space and time resolved diagnostics and modelling of plasmas and liquids to determine distribution and composition of reactive species (b) to control the plasma and apply differing plasma source concepts in order to produce a tailored output of reactive components and design the chemical composition of the liquids/cellular environment and (c) to identify and understand the interaction mechanisms of plasmas with liquids and biological systems. Methods to characterize the plasma generated reactive species from plasma-, gas- and liquid phase and their biological effects will be presented. The diagnostic spectrum ranges from absorption/emission/laser spectroscopy and molecular beam mass spectrometry to electron paramagnetic resonance spectroscopy and cell biological diagnostic techniques. Concluding, a presentation will be given of the comprehensive approach to plasma medicine in Greifswald where the applied and clinical research of the Campus PlasmaMed association is combined with the fundamental research at plasmatis center.

  7. On the physics of the pressure and temperature gradients in the edge of tokamak plasmas

    Science.gov (United States)

    Stacey, Weston M.

    2018-04-01

    An extended plasma fluid theory including atomic physics, radiation, electromagnetic and themodynamic forces, external sources of particles, momentum and energy, and kinetic ion orbit loss is employed to derive theoretical expressions that display the role of the various factors involved in the determination of the pressure and temperature gradients in the edge of tokamak plasmas. Calculations for current experiments are presented to illustrate the magnitudes of various effects including strong radiative and atomic physics edge cooling effects and strong reduction in ion particle and energy fluxes due to ion orbit loss in the plasma edge. An important new insight is the strong relation between rotation and the edge pressure gradient.

  8. The definition of the pressure of the classical one-component plasma

    International Nuclear Information System (INIS)

    Navet, Marcel; Jamin, Eric; Feix, M.R.

    1980-01-01

    A numerical simulation illustrates the 'virial' kinetic definition of the pressure of the classical one-component plasma introduced in a recent note. In spherical geometry it is found that this pressure, divided by kT, is equal to the density of particles on the wall, and a complete explanation of the discrepancy with the generally accepted thermodynamical definition is given [fr

  9. The conceptual design of high temporal resolution HCN interferometry for atmospheric pressure air plasmas

    Science.gov (United States)

    Zhang, J. B.; Liu, H. Q.; Jie, Y. X.; Wei, X. C.; Hu, L. Q.

    2018-01-01

    A heterodyne interferometer operating at the frequency f = 890 GHz has been designed for measuring the electron density of atmospheric pressure air plasmas, it's density range is from 1015 to 3×1019 m-3 and the pressure range is from 1 Pa to 20 kPa. The system is configured as a Mach\

  10. Atmospheric pressure plasma polymerization of 1,3-butadiene for hydrophobic finishing of textile substrates

    International Nuclear Information System (INIS)

    Samanta, Kartick K; Jassal, Manjeet; Agrawal, Ashwini K

    2010-01-01

    Atmospheric pressure plasma processing of textile has both ecological and economical advantages over the wet-chemical processing. However, reaction in atmospheric pressure plasma has important challenges to be overcome before it can be successfully used for finishing applications in textile. These challenges are (i) generating stable glow plasma in presence liquid/gaseous monomer, and (ii) keeping the generated radicals active in the presence of contaminants such as oxygen and air. In this study, a stable glow plasma was generated at atmospheric pressure in the mixture of gaseous reactive monomer-1,3-butadiene and He and was made to react with cellulosic textile substrate. After 12 min of plasma treatment, the hydrophilic surface of the cellulosic substrate turned into highly hydrophobic surface. The hydrophobic finish was found to be durable to soap washing. After soap washing, a water drop of 37 μl took around 250 s to get absorbed in the treated sample compared to 0 . Both top and bottom sides of the fabric showed similar hydrophobic results in terms of water absorbency and contact angle. The results may be attributed to chemical reaction of butadiene with the cellulosic textile substrate. The surface characterization of the plasma modified samples under SEM and AFM revealed modification of the surface under <100 nm. The results showed that atmospheric pressure plasma can be successfully used for carrying out reaction of 1,3-butadiene with cellulosic textile substrates for producing hydrophobic surface finish.

  11. An improved process for high nutrition of germinated brown rice production: Low-pressure plasma.

    Science.gov (United States)

    Chen, Hua Han; Chang, Hung Chia; Chen, Yu Kuo; Hung, Chien Lun; Lin, Su Yi; Chen, Yi Sheng

    2016-01-15

    Brown rice was exposed to low-pressure plasma ranging from 1 to 3kV for 10min. Treatment of brown rice in low-pressure plasma increases the germination percentage, seedling length, and water uptake in laboratory germination tests. Of the various treatments, 3-kV plasma exposure for 10min yielded the best results. In germinating brown rice, α-amylase activity was significantly higher in treated groups than in controls. The higher enzyme activity in plasma-treated brown rice likely triggers the rapid germination and earlier vigor of the seedlings. Low-pressure plasma also increased gamma-aminobutyric acid (GABA) levels from ∼19 to ∼28mg/100g. In addition, a marked increase in the antioxidant activity of brown rice was observed with plasma treatments compared to controls. The main finding of this study indicates that low-pressure plasma is effective at enhancing the growth and GABA accumulation of germinated brown rice, which can supply high nutrition to consumer. Copyright © 2015 Elsevier Ltd. All rights reserved.

  12. Experimental and simulation investigation of electrical and plasma parameters in a low pressure inductively coupled argon plasma

    Science.gov (United States)

    Jian, YANG; Angjian, WU; Xiaodong, LI; Yang, LIU; Fengsen, ZHU; Zhiliang, CHEN; Jianhua, YAN; Ruijuan, CHEN; Wangjun, SHEN

    2017-11-01

    The electrical and plasma parameters of a low pressure inductively coupled argon plasma are investigated over a wide range of parameters (RF power, flow rate and pressure) by diverse characterizations. The external antenna voltage and current increase with the augment of RF power, whereas decline with the enhancement of gas pressure and flow rate conversely. Compared with gas flow rate and pressure, the power transfer efficiency is significantly improved by RF power, and achieved its maximum value of 0.85 after RF power injected excess 125 W. Optical emission spectroscopy (OES) provides the local mean values of electron excited temperature and electron density in inductively coupled plasma (ICP) post regime, which vary in a range of 0.81 eV to 1.15 eV and 3.7× {10}16 {{{m}}}-3 to 8.7× {10}17 {{{m}}}-3, respectively. Numerical results of the average magnitudes of electron temperature and electron density in two-dimensional distribution exhibit similar variation trend with the experimental results under different operating condition by using COMSOL Multiphysics. By comprehensively understanding the characteristics in a low pressure ICP, optimized operating conditions could be anticipated aiming at different academic and industrial applications.

  13. Emission spectroscopy of argon ferrocene mixture jet in a low pressure plasma reactor

    International Nuclear Information System (INIS)

    Tiwari, N.; Tak, A.K.; Chakravarthy, Y.; Shukla, A.; Meher, K.C.; Ghorui, S.; Thiyagarajan, T.K.

    2015-01-01

    Emission spectroscopy is employed to measure the plasma temperature and species identification in a reactor used for studying homogenous nucleation and growth of iron nano particle. Reactor employs segmented non transferred plasma torch mounted on water cooled cylindrical chamber. The plasma jet passes through graphite nozzle and expands in low pressure reactor. Ferrocene is fed into the nozzle where it mixes with Argon plasma jet. A high resolution spectrograph (SHAMROCK 303i, resolution 0.06 nm) has been used to record the spectra over a wide range. Identification of different emission lines has been done using NIST database. Lines from (700 to 860nm) were considered for calculation of temperature. Spectra were recorded for different axial location, pressure and power. Temperature was calculated using Maxwell Boltzman plot method. Variation in temperature with pressure and location is presented and possible reasons for different behaviour are explored. (author)

  14. Two dimensional radial gas flows in atmospheric pressure plasma-enhanced chemical vapor deposition

    Science.gov (United States)

    Kim, Gwihyun; Park, Seran; Shin, Hyunsu; Song, Seungho; Oh, Hoon-Jung; Ko, Dae Hong; Choi, Jung-Il; Baik, Seung Jae

    2017-12-01

    Atmospheric pressure (AP) operation of plasma-enhanced chemical vapor deposition (PECVD) is one of promising concepts for high quality and low cost processing. Atmospheric plasma discharge requires narrow gap configuration, which causes an inherent feature of AP PECVD. Two dimensional radial gas flows in AP PECVD induces radial variation of mass-transport and that of substrate temperature. The opposite trend of these variations would be the key consideration in the development of uniform deposition process. Another inherent feature of AP PECVD is confined plasma discharge, from which volume power density concept is derived as a key parameter for the control of deposition rate. We investigated deposition rate as a function of volume power density, gas flux, source gas partial pressure, hydrogen partial pressure, plasma source frequency, and substrate temperature; and derived a design guideline of deposition tool and process development in terms of deposition rate and uniformity.

  15. Physico-chemical characteristics of high performance polymer modified by low and atmospheric pressure plasma

    International Nuclear Information System (INIS)

    Bhatnagar, Nitu; Sangeeta, Jha; Bhowmik, Shantanu; Gupta, Govind; Moon, J.B.; Kim, C.G.

    2012-01-01

    In this work, the effect of low pressure plasma and atmospheric p ressure plasma treatment on surface properties and adhesion characteristics of high performance polymer, Polyether Ether Ketone (PEEK) are investigated in terms of Fourier Transform Infrared Spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), and Atomic Force Microscopy (AFM). The experimental results show that the PEEK surface treated by atmospheric pressure plasma lead to an increase in the polar component of the surface energy, resulting in improving the adhesion characteristics of the PEEK/Epoxy adhesive system. Also, the roughness of the treated surfaces is largely increased as confirmed by AFM observation. These results can be explained by the fact that the atmospheric pressure plasma treatment of PEEK surface yields several oxygen functionalities on hydrophobic surface, which play an important role in increasing the surface polarity, wettability, and the adhesion characteristics of the PEEK/Epoxy adhesive system. (authors)

  16. Helically symmetric equilibria with pressure anisotropy and incompressible plasma flow

    Science.gov (United States)

    Evangelias, A.; Kuiroukidis, A.; Throumoulopoulos, G. N.

    2018-02-01

    We derive a generalized Grad-Shafranov equation governing helically symmetric equilibria with pressure anisotropy and incompressible flow of arbitrary direction. Through the most general linearizing ansatz for the various free surface functions involved therein, we construct equilibrium solutions and study their properties. It turns out that pressure anisotropy can act either paramegnetically or diamagnetically, the parallel flow has a paramagnetic effect, while the non-parallel component of the flow associated with the electric field has a diamagnetic one. Also, pressure anisotropy and flow affect noticeably the helical current density.

  17. Computational study of plasma-solid interaction in DC glow discharge in argon plasma at medium pressures

    International Nuclear Information System (INIS)

    Havlickova, E; Bartos, P; Hrach, R

    2007-01-01

    In the presented contribution two groups of techniques of computational physics-fluid modelling and non self-consistent particle technique were used to study plasma-solid interaction in argon plasma. We focused both on the physical processes taking place in the sheath at various pressures and on the problems of computational physics. The attention was given to preparation of two-dimensional fluid models with realistic assumptions about physical processes taking place in plasma during the plasma-solid interaction, further to improvement of the non self-consistent technique of particle modelling, where the external electric field was obtained either from the fluid model or directly from the trajectories of charged particles and finally to efficiency of individual algorithms

  18. Non-thermal atmospheric-pressure plasma possible application in wound healing.

    Science.gov (United States)

    Haertel, Beate; von Woedtke, Thomas; Weltmann, Klaus-Dieter; Lindequist, Ulrike

    2014-11-01

    Non-thermal atmospheric-pressure plasma, also named cold plasma, is defined as a partly ionized gas. Therefore, it cannot be equated with plasma from blood; it is not biological in nature. Non-thermal atmospheric-pressure plasma is a new innovative approach in medicine not only for the treatment of wounds, but with a wide-range of other applications, as e.g. topical treatment of other skin diseases with microbial involvement or treatment of cancer diseases. This review emphasizes plasma effects on wound healing. Non-thermal atmospheric-pressure plasma can support wound healing by its antiseptic effects, by stimulation of proliferation and migration of wound relating skin cells, by activation or inhibition of integrin receptors on the cell surface or by its pro-angiogenic effect. We summarize the effects of plasma on eukaryotic cells, especially on keratinocytes in terms of viability, proliferation, DNA, adhesion molecules and angiogenesis together with the role of reactive oxygen species and other components of plasma. The outcome of first clinical trials regarding wound healing is pointed out.

  19. Application of atmospheric pressure plasma on polyethylene for increased prosthesis adhesion

    Energy Technology Data Exchange (ETDEWEB)

    Van Vrekhem, S., E-mail: stijn.vanvrekhem@ugent.be [Research Unit Plasma Technology (RUPT), Department of Applied Physics, Faculty of Engineering and Architecture, Ghent University, Sint-Pietersnieuwstraat 41 B4, 9000 Ghent (Belgium); Cools, P. [Research Unit Plasma Technology (RUPT), Department of Applied Physics, Faculty of Engineering and Architecture, Ghent University, Sint-Pietersnieuwstraat 41 B4, 9000 Ghent (Belgium); Declercq, H. [Research Unit Plasma Technology (RUPT), Department of Applied Physics, Faculty of Engineering and Architecture, Ghent University, Sint-Pietersnieuwstraat 41 B4, 9000 Ghent (Belgium); Tissue Engineering Group, Department of Basic Medical Sciences, Faculty of Medicine and Health Sciences, Ghent University, De Pintelaan 185 6B3, 9000 Ghent (Belgium); Van Tongel, A. [Department of Orthopaedic Surgery and Traumatology, Ghent University Hospital, De Pintelaan 185 13K12, 9000 Ghent (Belgium); Vercruysse, C.; Cornelissen, M. [Tissue Engineering Group, Department of Basic Medical Sciences, Faculty of Medicine and Health Sciences, Ghent University, De Pintelaan 185 6B3, 9000 Ghent (Belgium); De Geyter, N.; Morent, R. [Research Unit Plasma Technology (RUPT), Department of Applied Physics, Faculty of Engineering and Architecture, Ghent University, Sint-Pietersnieuwstraat 41 B4, 9000 Ghent (Belgium)

    2015-12-01

    Biopolymers are often subjected to surface modification in order to improve their surface characteristics. The goal of this study is to show the use of plasma technology to enhance the adhesion of ultra-high molecular weight polyethylene (UHMWPE) shoulder prostheses. Two different plasma techniques (low pressure plasma activation and atmospheric pressure plasma polymerization) are performed on UHMWPE to increase the adhesion between (1) the polymer and polymethylmethacrylate (PMMA) bone cement and (2) the polymer and osteoblast cells. Both techniques are performed using a dielectric barrier discharge (DBD). A previous paper showed that low pressure plasma activation of UHMWPE results in the incorporation of oxygen-containing functional groups, which leads to an increased surface wettability. Atmospheric pressure plasma polymerization of methylmethacrylate (MMA) on UHMWPE results in a PMMA-like coating, which could be deposited with a high degree of control of chemical composition and layer thickness. The thin film also proved to be relatively stable upon incubation in a phosphate buffer solution (PBS). This paper discusses the next stage of the study, which includes testing the adhesion of the plasma-activated and plasma-polymerized samples to bone cement through pull-out tests and testing the cell adhesion and proliferation on the samples. In order to perform the pull-out tests, all samples were cut to standard dimensions and fixed in bone cement in a reproducible way with a sample holder specially designed for this purpose. The cell adhesion and proliferation were tested by means of an MTS assay and live/dead staining after culturing MC3T3 osteoblast cells on UHMWPE samples. The results show that both plasma activation and plasma polymerization significantly improve the adhesion to bone cement and enhance cell adhesion and proliferation. In conclusion, it can be stated that the use of plasma technology can lead to an implant with improved quality and a subsequent

  20. The influence of gas pressure on E↔H mode transition in argon inductively coupled plasmas

    OpenAIRE

    Xiao Zhang; Zhong-kai Zhang; Jin-xiang Cao; Yu Liu; Peng-cheng Yu

    2018-01-01

    Considering the gas pressure and radio frequency power change, the mode transition of E↔H were investigated in inductively coupled plasmas. It can be found that the transition power has almost the same trend decreasing with gas pressure, whether it is in H mode or E mode. However, the transition density increases slowly with gas pressure from E to H mode. The transition points of E to H mode can be understood by the propagation of electromagnetic wave in the plasma, while the H to E should be...

  1. The Healing Effect of Low-Temperature Atmospheric-Pressure Plasma in Pressure Ulcer: A Randomized Controlled Trial.

    Science.gov (United States)

    Chuangsuwanich, Apirag; Assadamongkol, Tananchai; Boonyawan, Dheerawan

    2016-12-01

    Pressure ulcers are difficult to treat. Recent reports of low-temperature atmospheric-pressure plasma (LTAPP) indicated its safe and effectiveness in chronic wound care management. It has been shown both in vitro and vivo studies that LTAPP not only helps facilitate wound healing but also has antimicrobial efficacy due to its composition of ion and electron, free radicals, and ultraviolet ray. We studied the beneficial effect of LTAPP specifically on pressure ulcers. In a prospective randomized study, 50 patients with pressure ulcers were divided into 2 groups: Control group received standard wound care and the study group was treated with LTAPP once every week for 8 consecutive weeks in addition to standard wound care. We found that the group treated with LTAPP had significantly better PUSH (Pressure Ulcer Scale for Healing) scores and exudate amount after 1 week of treatment. There was also a reduction in bacterial load after 1 treatment regardless of the species of bacteria identified.

  2. Pulmonary and heart diseases with inhalation of atmospheric pressure plasma flow

    Science.gov (United States)

    Hirata, Takamichi; Murata, Shigeru; Kishimoto, Takumi; Tsutsui, Chihiro; Kondo, Akane; Mori, Akira

    2012-10-01

    We examined blood pressure in the abdominal aorta of mini pig under plasma inhalation of atmospheric pressure plasma flow. The coaxial atmospheric pressure plasma source has a tungsten wire inside a glass capillary, that is surrounded by a grounded tubular electrode. Plasma was generated under the following conditions; applied voltage: 8 kVpp, frequency: 3 kHz, and helium (He) gas flow rate: 1 L/min. On the other hand, sphygmomanometry of a blood vessel proceeded using a device comprising a disposable force transducer, and a bedside monitor for simultaneous electrocardiography and signal pressure measurements. We directly measured Nitric oxide (NO) using a catheter-type NO sensor placed in the coronary sinus through an angiography catheter from the abdomen. Blood pressure decreased from 110/65 to 90/40 mm Hg in the animals in vivo under plasma inhalation. The NO concentration in the abdominal aorta like the blood pressure, reached a maximum value at about 40 s and then gradually decreased.

  3. Decay of femtosecond laser-induced plasma filaments in air, nitrogen, and argon for atmospheric and subatmospheric pressures.

    Science.gov (United States)

    Aleksandrov, N L; Bodrov, S B; Tsarev, M V; Murzanev, A A; Sergeev, Yu A; Malkov, Yu A; Stepanov, A N

    2016-07-01

    The temporal evolution of a plasma channel at the trail of a self-guided femtosecond laser pulse was studied experimentally and theoretically in air, nitrogen (with an admixture of ∼3% O_{2}), and argon in a wide range of gas pressures (from 2 to 760 Torr). Measurements by means of transverse optical interferometry and pulsed terahertz scattering techniques showed that plasma density in air and nitrogen at atmospheric pressure reduces by an order of magnitude within 3-4 ns and that the decay rate decreases with decreasing pressure. The argon plasma did not decay within several nanoseconds for pressures of 50-760 Torr. We extended our theoretical model previously applied for atmospheric pressure air plasma to explain the plasma decay in the gases under study and to show that allowance for plasma channel expansion affects plasma decay at low pressures.

  4. The Plasma Window: A Windowless High Pressure-Vacuum Interface for Various Accelerator Applications

    International Nuclear Information System (INIS)

    Hershcovitch, A. I.; Johnson, E. D.; Lanza, R. C.

    1999-01-01

    The Plasma Window is a stabilized plasma arc used as an interface between accelerator vacuum and pressurized targets. There is no solid material introduced into the beam and thus it is also capable of transmitting particle beams and electromagnetic radiation with low loss and of sustaining high beam currents without damage. Measurements on a prototype system with a 3 mm diameter opening have shown that pressure differences of more than 2.5 atmospheres can be sustained with an input pressure of ∼ 10 -6 Torr. The system is capable of scaling to higher-pressure differences and larger apertures. Various plasma window applications for synchrotron light sources, high power lasers, internal targets, high current accelerators such as the HAWK, ATW, APT, DARHT, spallation sources, as well as for a number of commercial applications, is discussed

  5. Treatment of Candida albicans biofilms with low-temperature plasma induced by dielectric barrier discharge and atmospheric pressure plasma jet

    Energy Technology Data Exchange (ETDEWEB)

    Koban, Ina; Welk, Alexander; Meisel, Peter; Holtfreter, Birte; Kocher, Thomas [Unit of Periodontology, Dental School, University of Greifswald, Rotgerberstr. 8, 17475 Greifswald (Germany); Matthes, Rutger; Huebner, Nils-Olaf; Kramer, Axel [Institute for Hygiene and Environmental Medicine, University of Greifswald, Walther-Rathenau-Str. 49 a, 17487 Greifswald (Germany); Sietmann, Rabea [Institute of Microbiology, University of Greifswald, Friedrich-Ludwig-Jahn-Str. 15, 17487 Greifswald (Germany); Kindel, Eckhard; Weltmann, Klaus-Dieter, E-mail: ina.koban@uni-greifswald.d [Leibniz Institute for Plasma Science and Technology (INP), Felix-Hausdorff-Str. 2, 17489 Greifswald (Germany)

    2010-07-15

    Because of some disadvantages of chemical disinfection in dental practice (especially denture cleaning), we investigated the effects of physical methods on Candida albicans biofilms. For this purpose, the antifungal efficacy of three different low-temperature plasma devices (an atmospheric pressure plasma jet and two different dielectric barrier discharges (DBDs)) on Candida albicans biofilms grown on titanium discs in vitro was investigated. As positive treatment controls, we used 0.1% chlorhexidine digluconate (CHX) and 0.6% sodium hypochlorite (NaOCl). The corresponding gas streams without plasma ignition served as negative treatment controls. The efficacy of the plasma treatment was determined evaluating the number of colony-forming units (CFU) recovered from titanium discs. The plasma treatment reduced the CFU significantly compared to chemical disinfectants. While 10 min CHX or NaOCl exposure led to a CFU log{sub 10} reduction factor of 1.5, the log{sub 10} reduction factor of DBD plasma was up to 5. In conclusion, the use of low-temperature plasma is a promising physical alternative to chemical antiseptics for dental practice.

  6. Treatment of Candida albicans biofilms with low-temperature plasma induced by dielectric barrier discharge and atmospheric pressure plasma jet

    International Nuclear Information System (INIS)

    Koban, Ina; Welk, Alexander; Meisel, Peter; Holtfreter, Birte; Kocher, Thomas; Matthes, Rutger; Huebner, Nils-Olaf; Kramer, Axel; Sietmann, Rabea; Kindel, Eckhard; Weltmann, Klaus-Dieter

    2010-01-01

    Because of some disadvantages of chemical disinfection in dental practice (especially denture cleaning), we investigated the effects of physical methods on Candida albicans biofilms. For this purpose, the antifungal efficacy of three different low-temperature plasma devices (an atmospheric pressure plasma jet and two different dielectric barrier discharges (DBDs)) on Candida albicans biofilms grown on titanium discs in vitro was investigated. As positive treatment controls, we used 0.1% chlorhexidine digluconate (CHX) and 0.6% sodium hypochlorite (NaOCl). The corresponding gas streams without plasma ignition served as negative treatment controls. The efficacy of the plasma treatment was determined evaluating the number of colony-forming units (CFU) recovered from titanium discs. The plasma treatment reduced the CFU significantly compared to chemical disinfectants. While 10 min CHX or NaOCl exposure led to a CFU log 10 reduction factor of 1.5, the log 10 reduction factor of DBD plasma was up to 5. In conclusion, the use of low-temperature plasma is a promising physical alternative to chemical antiseptics for dental practice.

  7. Oxygen Plasma Treatment of Rubber Surface by the Atmospheric Pressure Cold Plasma Torch

    DEFF Research Database (Denmark)

    Lee, Bong-ju; Kusano, Yukihiro; Kato, Nobuko

    1997-01-01

    adhesive. The adhesion property was improved by treatment of the rubber compound with plasma containing oxygen radicals. Physical and chemical changes of the rubber surface as a result of the plasma treatment were analyzed by field emission scanning electron microscopy (FE-SEM) and fourier transform......A new application of the atmospheric cold plasma torch has been investigated. Namely, the surface treatment of an air-exposed vulcanized rubber compound. The effect of plasma treatment was evaluated by the bondability of the treated rubber compound with another rubber compound using a polyurethane...

  8. Inactivation of Microorganisms in Model Biofilms by an Atmospheric Pressure Pulsed Non-thermal Plasma

    Science.gov (United States)

    Akishev, Yuri; Trushkin, N.; Grushin, M.; Petryakov, A.; Karal'nik, V.; Kobzev, E.; Kholodenko, V.; Chugunov, V.; Kireev, G.; Rakitsky, Yu.; Irkhina, I.

    Non-thermal plasma jet formed by self-running pulsed-periodical high-current spark generator (PPSG) was used for atmospheric pressure inactivation of microorganisms including biofilms. A distinctive feature of the PPSG is a formation of transient hot plasma clouds (plasma bullets) periodically flying out to the target. We experimented with model biofilms of E. coli and Bacillus subtilis monocultures which were grown on agar and surfaces of steel and polypropylene coupons. High efficiency of plasma inactivation was demonstrated. This effect is associated primarily with an interaction of transient hot plasma clouds with biofilms. Besides complete or partial degradation of the cell membrane, weakening of the cell wall of E.coli culture by active plasma was found.

  9. A battery-operated atmospheric-pressure plasma wand for biomedical applications

    Science.gov (United States)

    Pei, X.; Liu, J.; Xian, Y.; Lu, X.

    2014-04-01

    A handheld, battery-operated atmospheric-pressure plasma rod (named the plasma wand) which does not rely on an external power source (e.g. mains power or a power generator) or gas supply is reported. The plasma wand can be used for killing bacteria, fungi or viruses that are hidden in narrow channels such as the nasal cavity and ear canal, which are difficult to access using most currently available devices. Besides, the electrical characterization, plasma wand temperature, emission spectra of the plasma, ozone and OH radical concentration generated by the device, are investigated by different diagnostic methods. The ozone concentration reaches 120 ppm 1 mm away from the device and the OH concentration reaches 3.5 × 1014 cm-3 in the plasma. The preliminary bacteria inactivation experiment results show that all the bacteria samples on the microfiltration membrane are killed by this device within 30 s.

  10. The Research on Atmospheric Pressure Water Vapour Plasma Generation and Application for the Destruction of Wastes

    Directory of Open Access Journals (Sweden)

    Viktorija Grigaitiene

    2013-01-01

    Full Text Available In the Lithuanian Energy Institute an experimental atmospheric pressure Ar/water vapour plasma torch has been designed and tested. The power of plasma torch was estimated 40 ÷ 69 kW, the mean temperature of plasma jet at the exhaust nozzle was 2300÷2900K. The chemical compositionof water vapour plasma was established from the emission spectrum lines at 300 ÷ 800nm range. The main species observed in Ar/water vapour plasma were: Ar, OH, H, O, Cu. The experiments on water vapour steam reforming were performed. The results confirmed that water vapour plasma has the unique properties – high enthalpy and environmentally friendly conditions. It could be employed for environmental purposes such as destruction of wastes into simple molecules or conversion to synthetic gas.

  11. Electron dynamics and plasma jet formation in a helium atmospheric pressure dielectric barrier discharge jet

    Energy Technology Data Exchange (ETDEWEB)

    Algwari, Q. Th. [Centre for Plasma Physics, School of Maths and Physics, Queen' s University Belfast, University Road, Belfast, Northern Ireland BT7 1NN (United Kingdom); Electronic Department, College of Electronics Engineering, Mosul University, Mosul 41002 (Iraq); O' Connell, D. [Centre for Plasma Physics, School of Maths and Physics, Queen' s University Belfast, University Road, Belfast, Northern Ireland BT7 1NN (United Kingdom); York Plasma Institute, Department of Physics, University of York, York YO10 5DD (United Kingdom)

    2011-09-19

    The excitation dynamics within the main plasma production region and the plasma jets of a kHz atmospheric pressure dielectric barrier discharge (DBD) jet operated in helium was investigated. Within the dielectric tube, the plasma ignites as a streamer-type discharge. Plasma jets are emitted from both the powered and grounded electrode end; their dynamics are compared and contrasted. Ignition of these jets are quite different; the jet emitted from the powered electrode is ignited with a slight time delay to plasma ignition inside the dielectric tube, while breakdown of the jet at the grounded electrode end is from charging of the dielectric and is therefore dependent on plasma production and transport within the dielectric tube. Present streamer theories can explain these dynamics.

  12. Oxygen Plasma Treatment of Rubber Surface by the Atmospheric Pressure Cold Plasma Torch

    DEFF Research Database (Denmark)

    Lee, Bong-ju; Kusano, Yukihiro; Kato, Nobuko

    1997-01-01

    A new application of the atmospheric cold plasma torch has been investigated. Namely, the surface treatment of an air-exposed vulcanized rubber compound. The effect of plasma treatment was evaluated by the bondability of the treated rubber compound with another rubber compound using a polyurethane...

  13. Transient effects caused by pulsed gas and liquid injections into low pressure plasmas

    International Nuclear Information System (INIS)

    Ogawa, D; Goeckner, M; Overzet, L; Chung, C W

    2010-01-01

    The fast injection of liquid droplets into a glow discharge causes significant time variations in the pressure, the chemical composition of the gas and the phases present (liquid and/or solid along with gas). While the variations can be large and important, very few studies, especially kinetic studies, have been published. In this paper we examine the changes brought about in argon plasma by injecting Ar (gas), N 2 (gas) hexane (gas) and hexane (liquid droplets). The changes in the RF capacitively coupled power (forward and reflected), electron and ion density (n e , n i ), electron temperature (T e ) and optical emissions were monitored during the injections. It was found that the Ar injection (pressure change only) caused expected variations. The electron temperature reduced, the plasma density increased and the optical emission intensity remained nearly constant. The N 2 and hexane gas injections (chemical composition and pressure changes) also followed expected trends. The plasma densities increased and electron temperature decreased while the optical emissions changed from argon to the injected gas. These all serve to highlight the fact that the injection of evaporating hexane droplets in the plasma caused very little change. This is because the number of injected droplets is too small to noticeably affect the plasma, even though the shift in the chemical composition of the gas caused by evaporation from those same droplets can be very significant. The net conclusion is that using liquid droplets to inject precursors for low pressure plasmas is both feasible and controllable.

  14. Low-pressure water-cooled inductively coupled plasma torch

    Science.gov (United States)

    Seliskar, Carl J.; Warner, David K.

    1988-12-27

    An inductively coupled plasma torch is provided which comprises an inner tube, including a sample injection port to which the sample to be tested is supplied and comprising an enlarged central portion in which the plasma flame is confined; an outer tube surrounding the inner tube and containing water therein for cooling the inner tube, the outer tube including a water inlet port to which water is supplied and a water outlet port spaced from the water inlet port and from which water is removed after flowing through the outer tube; and an r.f. induction coil for inducing the plasma in the gas passing into the tube through the sample injection port. The sample injection port comprises a capillary tube including a reduced diameter orifice, projecting into the lower end of the inner tube. The water inlet is located at the lower end of the outer tube and the r.f. heating coil is disposed around the outer tube above and adjacent to the water inlet.

  15. Laser-Induced Graphite Plasma Kinetic Spectroscopy under Different Ambient Pressures

    International Nuclear Information System (INIS)

    Chaudhary, K.; Rosalan, S.; Aziz, M. S.; Bohadoran, M.; Ali, J; Bidin, N.; Saktioto; Yupapin, P. P.

    2015-01-01

    The laser induced plasma dynamics of graphite material are investigated by optical emission spectroscopy. Ablation and excitation of the graphite material is performed by using an 1064nm Nd:YAG laser in different ambient pressures. Characteristics of graphite spectra as line intensity variations and signal-to-noise ratio are presented with a main focus on the influence of the ambient pressure on the interaction of laser-induced graphite plasma with an ambient environment. Atomic emission lines are utilized to investigate the dynamical behavior of plasma, such as the excitation temperature and electron density, to describe emission differences under different ambient conditions. The excitation temperature and plasma electron density are the primary factors which contribute to the differences among the atomic carbon emission at different ambient pressures. Reactions between the plasma species and ambient gas, and the total molecular number are the main factors influencing molecular carbon emission. The influence of laser energy on the plasma interaction with environment is also investigated to demonstrate the dynamical behavior of carbon species so that it can be utilized to optimize plasma fluctuations. (paper)

  16. Atmospheric pressure plasma jet with high-voltage power supply based on piezoelectric transformer.

    Science.gov (United States)

    Babij, Michał; Kowalski, Zbigniew W; Nitsch, Karol; Silberring, Jerzy; Gotszalk, Teodor

    2014-05-01

    The dielectric barrier discharge plasma jet, an example of the nonthermal atmospheric pressure plasma jet (APPJ), generates low-temperature plasmas that are suitable for the atomization of volatile species and can also be served as an ionization source for ambient mass and ion mobility spectrometry. A new design of APPJ for mass spectrometry has been built in our group. In these plasma sources magnetic transformers (MTs) and inductors are typically used in power supplies but they present several drawbacks that are even more evident when dealing with high-voltage normally used in APPJs. To overcome these disadvantages, high frequency generators with the absence of MT are proposed in the literature. However, in the case of miniaturized APPJs these conventional power converters, built of ferromagnetic cores and inductors or by means of LC resonant tank circuits, are not so useful as piezoelectric transformer (PT) based power converters due to bulky components and small efficiency. We made and examined a novel atmospheric pressure plasma jet with PT supplier served as ionization source for ambient mass spectrometry, and especially mobile spectrometry where miniaturization, integration of components, and clean plasma are required. The objective of this paper is to describe the concept, design, and implementation of this miniaturized piezoelectric transformer-based atmospheric pressure plasma jet.

  17. Liquid alkali metals - Equation of state and reduced-pressure, bulk-modulus, sound-velocity, and specific-heat functions

    Science.gov (United States)

    Schlosser, Herbert; Ferrante, John

    1989-01-01

    The previous work of Schlosser and Ferrante (1988) on universality in solids is extended to the study of liquid metals. As in the case of solids, to a good approximation, in the absence of phase transitions, plots of the logarithm of the reduced-pressure function H, of the reduced-isothermal-bulk-modulus function b, and of the reduced-sound-velocity function v are all linear in 1-X. Finally, it is demonstrated that ln(Cp/C/v) is also linear in 1-X, where X = (V/V/0/)exp 1/3), and V(0) is the volume at zero pressure.

  18. Generation of uniform atmospheric pressure argon glow plasma by ...

    Indian Academy of Sciences (India)

    In this paper, atmospheric pressure glow discharges (APGD) in argon generated in parallel plate dielectric barrier discharge system is investigated by means of electrical and optical measurements. Using a high voltage (0–20 kV) power supply operating at 10–30 kHz, homogeneous and steady APGD has been observed ...

  19. Measurement of electric field distribution along the plasma column in Microwave jet discharges at atmospheric pressure

    International Nuclear Information System (INIS)

    Razzak, M. Abdur; Takamura, Shuichi; Tsujikawa, Takayuki; Shibata, Hideto; Hatakeyama, Yuto

    2009-01-01

    A new technique for the direct measurement of electric field distribution along the plasma column in microwave jet discharges is developed and employed. The technique is based on a servomotor-controlled reciprocating antenna moving along the nozzle axis and plasma column. The measurement technique is applied to a rectangular waveguide-based 2.45 GHz argon and helium plasma jets generated by using the modified TIAGO nozzle at atmospheric pressure with a microwave power of less than 500 W. The measurement has been done with and without igniting the plasma jet in order to investigate the standing wave propagation along the nozzle axis and plasma column. It is observed that the electric field decay occurs slowly in space with plasma ignition than that of without plasma, which indicates the surface electromagnetic wave propagation along the plasma column in order to sustain the plasma jet. This study enables one to design, determine and optimize the size and structure of launcher nozzle, which plays an important role for the stable and efficient microwave plasma generators. (author)

  20. Cold atmospheric-pressure plasma and bacteria: understanding the mode of action using vibrational microspectroscopy

    International Nuclear Information System (INIS)

    Kartaschew, Konstantin; Mischo, Meike; Bründermann, Erik; Havenith, Martina; Baldus, Sabrina; Awakowicz, Peter

    2016-01-01

    Cold atmospheric-pressure plasma show promising antimicrobial effects, however the detailed biochemical mechanism of the bacterial inactivation is still unknown. We investigated, for the first time, plasma-treated Gram-positive Bacillus subtilis and Gram-negative Escherichia coli bacteria with Raman and infrared microspectroscopy. A dielectric barrier discharge was used as a plasma source. We were able to detect several plasma-induced chemical modifications, which suggest a pronounced oxidative effect on the cell envelope, cellular proteins and nucleotides as well as a generation of organic nitrates in the treated bacteria. Vibrational microspectroscopy is used as a comprehensive and a powerful tool for the analysis of plasma interactions with whole organisms such as bacteria. Analysis of reaction kinetics of chemical modifications allow a time-dependent insight into the plasma-mediated impact. Investigating possible synergistic effects between the plasma-produced components, our observations strongly indicate that the detected plasma-mediated chemical alterations can be mainly explained by the particle effect of the generated reactive species. By changing the polarity of the applied voltage pulse, and hence the propagation mechanisms of streamers, no significant effect on the spectral results could be detected. This method allows the analysis of the individual impact of each plasma constituent for particular chemical modifications. Our approach shows great potential to contribute to a better understanding of plasma-cell interactions. (paper)

  1. Separated Type Atmospheric Pressure Plasma Microjets Array for Maskless Microscale Etching

    Directory of Open Access Journals (Sweden)

    Yichuan Dai

    2017-06-01

    Full Text Available Maskless etching approaches such as microdischarges and atmospheric pressure plasma jets (APPJs have been studied recently. Nonetheless, a simple, long lifetime, and efficient maskless etching method is still a challenge. In this work, a separated type maskless etching system based on atmospheric pressure He/O2 plasma jet and microfabricated Micro Electro Mechanical Systems (MEMS nozzle have been developed with advantages of simple-structure, flexibility, and parallel processing capacity. The plasma was generated in the glass tube, forming the micron level plasma jet between the nozzle and the surface of polymer. The plasma microjet was capable of removing photoresist without masks since it contains oxygen reactive species verified by spectra measurement. The experimental results illustrated that different features of microholes etched by plasma microjet could be achieved by controlling the distance between the nozzle and the substrate, additive oxygen ratio, and etch time, the result of which is consistent with the analysis result of plasma spectra. In addition, a parallel etching process was also realized by plasma microjets array.

  2. Effect of occupational lead-exposure on blood pressure, serum aldosterone level and plasma renin activity.

    Science.gov (United States)

    Shouman, A E; El-Safty, I A

    2000-01-01

    Numerous observations have indicated a relationship between lead exposure and elevated blood pressure. The present study aims to investigate the association between occupational lead-exposure and elevated blood pressure as well as serum aldosterone level and plasma renin activity as parameters affecting blood pressure. Fifty occupationally lead-exposed (16 males and 34 females) and 50 non-exposed (15 males and 34 females) workers were selected after application of certain exclusion criteria. All workers were admitted to complete clinical examination, including standard blood pressure measurement. Also, blood lead level, serum aldosterone concentration and plasma renin activity were estimated. The results of both occupationally lead-exposed males and females demonstrated no significant differences regarding age, work duration, systolic and diastolic blood pressures when compared to occupationally non-exposed males and females; respectively. In addition, occupationally lead-exposed males and females revealed a significant increase in blood lead level and serum aldosterone concentration in comparison to their controls. Moreover, plasma renin activity is significantly decreased among the lead-exposed male workers while it is significantly increased among the lead-exposed female workers in comparison to their controls. It is concluded that serum aldosterone level and plasma renin activity are affected by occupationally low-level of lead exposure, and the present study provide further support for the association between blood lead exposure and blood pressure related hormones.

  3. Measurements of Ion and Neutral Fluctuation Changes with Pressure in a Large-Scale Helicon Plasma

    Science.gov (United States)

    Dwyer, R. H.; Fisher, D. M.; Kelly, R. F.; Hatch, M. W.; Gilmore, M.

    2017-10-01

    Neutral particle dynamics may play an important role both in laboratory plasmas and in the edge of magnetic fusion devices. However, studies of neutral dynamics in these plasmas have been limited to date. Here we report on a basic study of ion and neutral fluctuations as a function of background neutral gas pressure. These experiments have been conducted in helicon discharges in the HelCat (Helicon-Cathode) dual-source plasma device at the University of New Mexico. The goal is to measure changes in ion and neutral density fluctuations with pressure and to gain an improved understanding of plasma-neutral interactions. Langmuir probe, Ar-I LIF, and high-speed imaging measurements of the fluctuations will be presented. Supported by U.S. National Science Foundation Award 1500423 and The University of New Mexico School of Engineering.

  4. International symposium on high pressure low temperature plasma chemistry. Contributed papers

    International Nuclear Information System (INIS)

    1998-01-01

    The proceedings contain the texts of 77 contributions, of which 31 contributions fall within the scope of the INIS database. The latter deal with various aspects of plasma behavior in pulsed electric discharges of various types, with the spectroscopic and probe diagnostics of a discharge plasma, and with the computer simulation of ionization and breakdown processes in the glow, corona, and arc discharges at atmospheric pressure. (J.U.)

  5. Modified quadrupole mass analyzer RGA-100 for beam plasma research in forevacuum pressure range

    Energy Technology Data Exchange (ETDEWEB)

    Zolotukhin, D. B.; Tyunkov, A. V. [Tomsk State University of Control Systems and Radioelectronics, 40 Lenin Ave., Tomsk 634050 (Russian Federation); Yushkov, Yu. G., E-mail: yuyushkov@gmail.com [Tomsk State University of Control Systems and Radioelectronics, 40 Lenin Ave., Tomsk 634050 (Russian Federation); Tomsk Polytechnic University, 30 Lenin Ave., Tomsk 634050 (Russian Federation); Oks, E. M. [Tomsk State University of Control Systems and Radioelectronics, 40 Lenin Ave., Tomsk 634050 (Russian Federation); Institute of High Current Electronics SB RAS, 2/3, Akademichesky Ave., Tomsk 634055 (Russian Federation)

    2015-12-15

    The industrial quadrupole RGA-100 residual gas analyzer was modified for the research of electron beam-generated plasma at forevacuum pressure range. The standard ionizer of the RGA-100 was replaced by three electrode extracting unit. We made the optimization of operation parameters in order to provide the maximum values of measured currents of any ion species. The modified analyzer was successfully tested with beam plasma of argon, nitrogen, oxygen, and hydrocarbons.

  6. Plasma catecholamine level and portal venous pressure as guides to prognosis in patients with cirrhosis

    DEFF Research Database (Denmark)

    Tage-Jensen, U; Henriksen, Jens Henrik; Christensen, E

    1988-01-01

    Circulating noradrenaline is increased in patients with cirrhosis, especially in decompensated patients with ascites. Eighty-one patients with alcoholic cirrhosis were followed for up to 8 years in order to establish a possible relationship between plasma catecholamines, haemodynamics, and routine...... clinical and biochemical variables and survival. Forty-seven (58%) of the patients died during the follow-up period. Univariate analysis showed that plasma noradrenaline and adrenaline concentrations, portal pressure, indocyanine green clearance, serum sodium, bilirubin, and albumin concentrations...

  7. Cleaning of niobium surface by plasma of diffuse discharge at atmospheric pressure

    Science.gov (United States)

    Tarasenko, V. F.; Erofeev, M. V.; Shulepov, M. A.; Ripenko, V. S.

    2017-07-01

    Elements composition of niobium surface before and after plasma treatment by runaway electron preionized diffuse discharge was investigated in atmospheric pressure nitrogen flow by means of an Auger electron spectroscopy. Surface characterizations obtained from Auger spectra show that plasma treatment by diffuse discharge after exposure of 120000 pulses provides ultrafine surface cleaning from carbon contamination. Moreover, the surface free energy of the treated specimens increased up to 3 times, that improve its adhesion property.

  8. HRTEM and Nanoindentation Studies of Bulk WC Nanocrystalline Materials Prepared by Spark Plasma Sintering of Ball-Milled Powders

    Science.gov (United States)

    Sherif El-Eskandarany, M.; Al-Hazza, Abdulsalam; Al-Hajji, L. A.

    2017-01-01

    In the present work, mechanical milling technique using a high-energy ball mill was employed for preparing of nanoscaled WC grains powders with an average grain size of 7 nm in diameters of WC. The present study demonstrates a successful consolidation process achieved at 1250 °C for sintering of ball-milled WC powders into full dense bulk buttons (above 99.6%), using SPS technique. The as-consolidated WC bulk nanocrystalline buttons revealed high hardness value ( 24 GPa) with low elastic modulus ( 332 GPa). Moreover, they possessed a high fracture toughness (15 MPa m1/2) that has never been reported for pure WC.

  9. Shock Formation by Plasma Filaments of Microwave Discharge under Atmospheric Pressure

    International Nuclear Information System (INIS)

    Takahashi, Masayuki; Ohnishi, Naofumi

    2016-01-01

    A one-dimensional compressible fluid calculation was coupled with a finite- difference time-domain code and a particle-in-cell code with collision to reproduce propagation of electromagnetic wave, ionization process of plasma, and shock wave formation in atmospheric microwave discharge. Plasma filaments are driven toward the microwave source at 1 atm, and the distance between each filament is one-fifth of the wavelength of the incident microwave. The strong shock wave is generated due to the high plasma density at the atmospheric pressure. A simple analysis of the microwave propagation into the plasma shows that cut-off density of the microwave becomes smaller with the pressure decrease in a collisional plasma. At the lower pressure, the smaller density plasma is obtained with a diffusive pattern because of the smaller cut-off density and the larger diffusion effect. In contrast with the 1-atm case, the weak shock wave is generated at a rarefied condition, which lowers performance of microwave thruster. (paper)

  10. Effect of feed-gas humidity on nitrogen atmospheric-pressure plasma jet for biological applications.

    Science.gov (United States)

    Stephan, Karl D; McLean, Robert J C; DeLeon, Gian; Melnikov, Vadim

    2016-11-14

    We investigate the effect of feed-gas humidity on the oxidative properties of an atmospheric-pressure plasma jet using nitrogen gas. Plasma jets operating at atmospheric pressure are finding uses in medical and biological settings for sterilization and other applications involving oxidative stress applied to organisms. Most jets use noble gases, but some researchers use less expensive nitrogen gas. The feed-gas water content (humidity) has been found to influence the performance of noble-gas plasma jets, but has not yet been systematically investigated for jets using nitrogen gas. Low-humidity and high-humidity feed gases were used in a nitrogen plasma jet, and the oxidation effect of the jet was measured quantitatively using a chemical dosimeter known as FBX (ferrous sulfate-benzoic acid-xylenol orange). The plasma jet using high humidity was found to have about ten times the oxidation effect of the low-humidity jet, as measured by comparison with the addition of measured amounts of hydrogen peroxide to the FBX dosimeter. Atmospheric-pressure plasma jets using nitrogen as a feed gas have a greater oxidizing effect with a high level of humidity added to the feed gas.

  11. [Investigation on the gas temperature of a plasma jet at atmospheric pressure by emission spectrum].

    Science.gov (United States)

    Li, Xue-chen; Yuan, Ning; Jia, Peng-ying; Niu, Dong-ying

    2010-11-01

    A plasma jet of a dielectric barrier discharge in coaxial electrode was used to produce plasma plume in atmospheric pressure argon. Spatially and temporally resolved measurement was carried out by photomultiplier tubes. The light emission signals both from the dielectric barrier discharge and from the plasma plume were analyzed. Furthermore, emission spectrum from the plasma plume was collected by high-resolution optical spectrometer. The emission spectra of OH (A 2sigma + --> X2 II, 307.7-308.9 nm) and the first negative band of N2+ (B2 sigma u+ --> X2 IIg+, 390-391.6 nm) were used to estimate the rotational temperature of the plasma plume by fitting the experimental spectra to the simulated spectra. The rotational temperature obtained is about 443 K by fitting the emission spectrum from the OH, and that from the first negative band of N2+ is about 450 K. The rotational temperatures obtained by the two method are consistent within 5% error band. The gas temperature of the plasma plume at atmospheric pressure was obtained because rotational temperature equals to gas temperature approximately in gas discharge at atmospheric pressure. Results show that gas temperature increases with increasing the applied voltage.

  12. Spectral measurement of atmospheric pressure plasma by means of digital camera

    International Nuclear Information System (INIS)

    Ge Yuanjing; Zhang Guangqiu; Liu Yimin; Zhao Zhifa

    2002-01-01

    A digital camera measuring system has been used successfully to measure the space fluctuation behaviors of Induced Dielectric Barrier Discharge (IDBD) plasma at atmospheric pressure. The experimental results showed that: (1) The uniformity of electron temperature in space depends on discharge condition and structure of web electrode. For a certain web electrode the higher the discharge voltage is, the more uniform distribution of electron temperature in space will be. For a certain discharge the finer and denser the holes on web electrode are, the more uniform distribution of electron temperature in space will be. (2) Digital camera is an available equipment to measure some behaviors of the plasma working at atmospheric pressure

  13. Decontamination of objects in a sealed container by means of atmospheric pressure plasmas

    DEFF Research Database (Denmark)

    Leipold, Frank; Schultz-Jensen, Nadja; Kusano, Yukihiro

    2011-01-01

    The decontamination of objects (food) in a sealed container by means of atmospheric pressure plasmas is investigated. The target is Listeria monocytogenes, a bacterium which causes listeriosis and can be found in plants and food. The non-pathogenic species, Listeria innocua, is used....... The ambient atmosphere was air at atmospheric pressure. A plasma is generated inside the bag forming ozone from the oxygen. The maximum ozone concentration in the bag was found to be 140 ppm. A log 6 reduction of L. innocua is obtained after 15 min of exposure time. The temperature of the slides after...

  14. Plasma chemistry in an atmospheric pressure Ar/NH3 dielectric barrier discharge

    DEFF Research Database (Denmark)

    Fateev, A.; Leipold, F.; Kusano, Y.

    2005-01-01

    An atmospheric pressure dielectric barrier discharge (DBD) in Ar/NH3 (0.1 - 10%) mixtures with a parallel plate electrode geometry was studied. The plasma was investigated by emission and absorption spectroscopy in the UV spectral range. Discharge current and voltage were measured as well. UV...... of an atmospheric pressure Ar/NH3 DBD are H-2, N-2 and N2H4. The hydrazine (N2H4) concentration in the plasma and in the exhaust gases at various ammonia concentrations and different discharge powers was measured. Thermal N2H4 decomposition into NH2 radicals may be used for NOx reduction processes....

  15. Stability of Atmospheric-Pressure Plasma Induced Changes on Polycarbonate Surfaces

    Science.gov (United States)

    Sharma, Rajesh; Holcomb, Edward; Trigwell, Steve

    2006-01-01

    Polycarbonate films are subjected to plasma treatment in a number of applications such as improving adhesion between polycarbonate and silicon alloy in protective and optical coatings. The changes in surface chemistry due to plasma treatment have tendency to revert back. Thus stability of the plasma induced changes on polymer surfaces over desired time period is very important. The objective of this study was to examine the effect of ageing on atmospheric pressure helium-plasma treated polycarbonate (PC) sample as a function of treatment time. The ageing effects were studied over a period of 10 days. The samples were plasma treated for 0.5, 2, 5 and 10 minutes. Contact angle measurements were made to study surface energy changes. Modification of surface chemical structure was examined using, X-ray Photoelectron Spectroscopy (XPS). Contact angle measurements on untreated and plasma treated surfaces were made immediately, 24, 48, 72 and 96 hrs after treatment. Contact angle decreased from 93 deg for untreated sample to 30 deg for sample plasma treated for 10 minutes. After 10 days the contact angles for the 10 minute plasma treated sample increased to 67 deg, but it never reverted back to that of untreated surface. Similarly the O/C ratio increased from 0.136 for untreated sample to 0.321 for 10 minute plasma treated sample indication increase in surface energy.

  16. Atmospheric pressure plasma: a high-performance tool for the efficient removal of biofilms.

    Directory of Open Access Journals (Sweden)

    Katja Fricke

    Full Text Available INTRODUCTION: The medical use of non-thermal physical plasmas is intensively investigated for sterilization and surface modification of biomedical materials. A further promising application is the removal or etching of organic substances, e.g., biofilms, from surfaces, because remnants of biofilms after conventional cleaning procedures are capable to entertain inflammatory processes in the adjacent tissues. In general, contamination of surfaces by micro-organisms is a major source of problems in health care. Especially biofilms are the most common type of microbial growth in the human body and therefore, the complete removal of pathogens is mandatory for the prevention of inflammatory infiltrate. Physical plasmas offer a huge potential to inactivate micro-organisms and to remove organic materials through plasma-generated highly reactive agents. METHOD: In this study a Candida albicans biofilm, formed on polystyrene (PS wafers, as a prototypic biofilm was used to verify the etching capability of the atmospheric pressure plasma jet operating with two different process gases (argon and argon/oxygen mixture. The capability of plasma-assisted biofilm removal was assessed by microscopic imaging. RESULTS: The Candida albicans biofilm, with a thickness of 10 to 20 µm, was removed within 300 s plasma treatment when oxygen was added to the argon gas discharge, whereas argon plasma alone was practically not sufficient in biofilm removal. The impact of plasma etching on biofilms is localized due to the limited presence of reactive plasma species validated by optical emission spectroscopy.

  17. Nanoparticle formation in a low pressure argon/aniline RF plasma

    Science.gov (United States)

    Pattyn, C.; Kovacevic, E.; Hussain, S.; Dias, A.; Lecas, T.; Berndt, J.

    2018-01-01

    The formation of nanoparticles in low temperature plasmas is of high importance for different fields: from astrophysics to microelectronics. The plasma based synthesis of nanoparticles is a complex multi-scale process that involves a great variety of different species and comprises timescales ranging from milliseconds to several minutes. This contribution focuses on the synthesis of nanoparticles in a low temperature, low pressure capacitively coupled plasma containing mixtures of argon and aniline. Aniline is commonly used for the production of polyaniline, a material that belongs to the family of conductive polymers, which has attracted increasing interest in the last few years due to the large number of potential applications. The nanoparticles which are formed in the plasma volume and levitate there due to the collection of negative charges are investigated in this contribution by means of in-situ FTIR spectroscopy. In addition, the plasma is analyzed by means of plasma (ion) mass spectroscopy. The experiments reveal the possibility to synthesize nanoparticles both in continuous wave and in pulsed discharges. The formation of particles in the plasma volume can be suppressed by pulsing the plasma in a specific frequency range. The in-situ FTIR analysis also reveals the influence of the argon plasma on the characteristics of the nanoparticles.

  18. Fourier transform infrared absorption spectroscopy characterization of gaseous atmospheric pressure plasmas with 2 mm spatial resolution

    Energy Technology Data Exchange (ETDEWEB)

    Laroche, G. [Laboratoire d' Ingenierie de Surface, Centre de Recherche sur les Materiaux Avances, Departement de genie des mines, de la metallurgie et des materiaux, Universite Laval, 1065, avenue de la Medecine, Quebec G1V 0A6 (Canada); Centre de recherche du CHUQ, Hopital St Francois d' Assise, 10, rue de l' Espinay, local E0-165, Quebec G1L 3L5 (Canada); Vallade, J. [Laboratoire Procedes, Materiaux et Energie Solaire, PROMES, CNRS, Technosud, Rambla de la Thermodynamique, F-66100 Perpignan (France); Agence de l' environnement et de la Ma Latin-Small-Letter-Dotless-I -carettrise de l' Energie, 20, avenue du Gresille, BP 90406, F-49004 Angers Cedex 01 (France); Bazinette, R.; Hernandez, E.; Hernandez, G.; Massines, F. [Laboratoire Procedes, Materiaux et Energie Solaire, PROMES, CNRS, Technosud, Rambla de la Thermodynamique, F-66100 Perpignan (France); Nijnatten, P. van [OMT Solutions bv, High Tech Campus 9, 5656AE Eindhoven (Netherlands)

    2012-10-15

    This paper describes an optical setup built to record Fourier transform infrared (FTIR) absorption spectra in an atmospheric pressure plasma with a spatial resolution of 2 mm. The overall system consisted of three basic parts: (1) optical components located within the FTIR sample compartment, making it possible to define the size of the infrared beam (2 mm Multiplication-Sign 2 mm over a path length of 50 mm) imaged at the site of the plasma by (2) an optical interface positioned between the spectrometer and the plasma reactor. Once through the plasma region, (3) a retro-reflector module, located behind the plasma reactor, redirected the infrared beam coincident to the incident path up to a 45 Degree-Sign beamsplitter to reflect the beam toward a narrow-band mercury-cadmium-telluride detector. The antireflective plasma-coating experiments performed with ammonia and silane demonstrated that it was possible to quantify 42 and 2 ppm of these species in argon, respectively. In the case of ammonia, this was approximately three times less than this gas concentration typically used in plasma coating experiments while the silane limit of quantification was 35 times lower. Moreover, 70% of the incoming infrared radiation was focused within a 2 mm width at the site of the plasma, in reasonable agreement with the expected spatial resolution. The possibility of reaching this spatial resolution thus enabled us to measure the gaseous precursor consumption as a function of their residence time in the plasma.

  19. Adhesion improvement of fibres by continuous plasma treatment at atmospheric pressure

    DEFF Research Database (Denmark)

    Kusano, Yukihiro; Løgstrup Andersen, Tom; Sørensen, Bent F.

    2013-01-01

    Carbon fibres and ultra-high-molecular-weight polyethylene (UHMWPE) fibres were continuously treated by a dielectric barrier discharge plasma at atmospheric pressure for adhesion improvement with epoxy resins. The plasma treatment improved wettability, increased the oxygen containing polar...... functional groups at the surface, and subsequently improved adhesion to the epoxy and fracture resistance of epoxy composites. Hansen solubility parameters (HSP), quantitatively describing physical interactions among molecules, were measured for the UHMWPE fibre surfaces. The result identifies two distinct...... types of surfaces in both the plasma treated and the untreated fibres. One type is typical of polyethylene polymers while the other is characteristic of the oxygenated surface at much higher values of HSP....

  20. Characterization of atmospheric pressure plasma treated wool/cashmere textiles: Treatment in nitrogen

    Science.gov (United States)

    Zanini, Stefano; Citterio, Attilio; Leonardi, Gabriella; Riccardi, Claudia

    2018-01-01

    We performed atmospheric pressure plasma treatments of wool/cashmere (15/85%) textiles with a dielectric barrier discharge (DBD) in nitrogen. The chemical properties of the plasma treated samples were investigated with attenuated total reflectance Fourier transform infrared (FTIR/ATR) spectroscopy, X-ray photoelectron microscopy (XPS), and fatty acid gas chromatographic analysis. Changes in mechanical properties and tactile performance of textiles after the plasma treatment were determined using the KES-F system. The analyses reveal significant surface modification of the treated fabrics, which enhances their surface wettability.

  1. Diagnostics of surface wave driven low pressure plasmas based on indium monoiodide-argon system

    International Nuclear Information System (INIS)

    Ögün, C M; Kaiser, C; Kling, R; Heering, W

    2015-01-01

    Indium monoiodide is proposed as a suitable alternative to hazardous mercury, i.e. the emitting component inside the compact fluorescent lamps (CFL), with comparable luminous efficacy. Indium monoiodide-argon low pressure lamps are electrodelessly driven with surface waves, which are launched and coupled into the lamp by the ‘surfatron’, a microwave coupler optimized for an efficient operation at a frequency of 2.45 GHz. A non intrusive diagnostic method based on spatially resolved optical emission spectroscopy is employed to characterize the plasma parameters. The line emission coefficients of the plasma are derived by means of Abel’s inversion from the measured spectral radiance data. The characteristic plasma parameters, e.g. electron temperature and density are determined by comparing the experimentally obtained line emission coefficients with simulated ones from a collisional-radiative model. Additionally, a method to determine the absolute plasma efficiency via irradiance measurements without any goniometric setup is presented. In this way, the relationship between the plasma efficiency and the plasma parameters can be investigated systematically for different operating configurations, e.g. electrical input power, buffer gas pressure and cold spot temperature. The performance of indium monoiodide-argon plasma is compared with that of conventional CFLs. (paper)

  2. Glass transition, crystallization kinetics and pressure effect on crystallization of ZrNbCuNiBe bulk metallic glass

    DEFF Research Database (Denmark)

    Xing, P.F.; Zhuang, Yanxin; Wang, W.H.

    2002-01-01

    The glass transition behavior and crystallization kinetics of Zr48Nb8Cu14Ni12Be18 bulk metallic glass have been investigated by differential scanning calorimetry and x-ray powder diffraction (XRD). The activation energies of both glass transition and crystallization events have been obtained usin...

  3. Ionization instability induced striations in low frequency and pulsed He/H2O atmospheric pressure plasmas

    Science.gov (United States)

    Kawamura, E.; Lieberman, M. A.; Lichtenberg, A. J.

    2018-01-01

    In previous work [Kawamura et al., Plasma Sources Sci. Technol. 25, 054009 (2016)] and [Kawamura et al., J. Phys. D: Appl. Phys. 50, 145204 (2017)], 1D kinetic particle-in-cell (PIC) simulations of narrow gap (1 to 4 mm), high frequency (27 MHz) or dc-driven, He/2%H2O atmospheric pressure plasmas (APPs) showed an ionization instability resulting in standing striations (spatial oscillations) in the bulk plasma. We developed a steady-state striation theory which showed that the striations are due to non-local electron kinetics. In both the high frequency and dc-driven cases, the equilibrium electron density n0 in the plasma bulk was stationary. In this work, we first conduct 1D PIC simulations of a 1 mm gap He/2%H2O APP, driven by a sinusoidal current at a low frequency of f = 50 kHz such that ω = 2πf is well below the ionization frequency νiz. In this case, n0 varies with time, and we observe a time-varying instability which quasistatically depends on n0(t). At each phase of the rf cycle, the discharge resembles a dc discharge at the same n0. At higher frequencies (200 kHz-1 MHz), ω approaches νiz, and quasistatic equilibrium at each phase breaks down. The discharge is also driven with a 200 kHz, 50% duty cycle square wave pulse with a short rise and fall time of 0.1 μs in an attempt to directly measure the striation growth rate s during the on-cycle before it saturated. However, the spike in current during the rise time leads to a spike in electron temperature Te and hence νiz and s at the beginning of the rise which saturated during the beginning of the on-cycle. To predict the instability growth rate and saturation during and after the current spike, we extend our striation theory to include time-varying n0, Te, νiz, as well as terms for the nonlinear saturation and noise floor of the striation amplitude. The time-varying global model predictions are compared to the PIC simulations, showing reasonable agreement.

  4. Induction of proliferation of basal epidermal keratinocytes by cold atmospheric-pressure plasma.

    Science.gov (United States)

    Hasse, S; Duong Tran, T; Hahn, O; Kindler, S; Metelmann, H-R; von Woedtke, T; Masur, K

    2016-03-01

    Over the past few decades, new cold plasma sources have been developed that have the great advantage of operating at atmospheric pressure and at temperatures tolerable by biological material. New applications for these have emerged, especially in the field of dermatology. Recently it was demonstrated that cold atmospheric-pressure plasma positively influences healing of chronic wounds. The potential of cold plasma lies in its capacity to reduce bacterial load in the wound while at the same time stimulating skin cells and therefore promoting wound closure. In recent years, there have been great advances in the understanding of the molecular mechanisms triggered by cold plasma involving signalling pathways and gene regulation in cell culture. To investigate cold plasma-induced effects in ex vivo treated human skin biopsies. Human skin tissue was exposed to cold plasma for different lengths of time, and analysed by immunofluorescence with respect to DNA damage, apoptosis, proliferation and differentiation markers. After cold plasma treatment, the epidermal integrity and keratin expression pattern remained unchanged. As expected, the results revealed an increase in apoptotic cells after 3 and 5 min of treatment. Strikingly, an induction of proliferating basal keratinocytes was detected after cold plasma exposure for 1 and 3 min. As these are the cells that regenerate the epidermis, this could indeed be beneficial for wound closure. We investigated the effect of cold plasma on human skin by detecting molecules for growth and apoptosis, and found that both processes are dependent on treatment time. Therefore, this approach offers promising results for further applications of cold plasma in clinical dermatology. © 2015 British Association of Dermatologists.

  5. Meter-Scale Atmospheric-Pressure Microwave Plasma Using Sub-Millimeter-Gap Slot

    Science.gov (United States)

    Toyoda, Hirotaka

    2013-09-01

    Atmospheric-pressure pulsed plasmas have been given much attention because of its various possibilities for industrial applications such as surface wettability control, sterilization and so on. Among various atmospheric-pressure plasma sources, microwave plasma that is produced inside waveguide-slots is attractive because high-density plasma up to 1015 cm-3 can be easily produced along very long waveguide with light-weight and rather simple antenna configuration. So far, we have investigated plasma production inside slot of the waveguide and in this talk, elongation of the plasma up to meter-scale with newly-designed plasma source will be presented. In this study, two types of antennas are proposed to elongate the atmospheric-pressure microwave plasma. Firstly, array-structured slot design with a closed-end waveguide is adopted using X-band microwave (10 GHz). In this structure, slot antennas with a total number of more than 40 are positioned with λg/2-pitch along ~1m waveguide so as to utilize standing wave inside the waveguide and to increase the electric field inside the slot. By optimizing the antenna design, arrayed microwave plasmas are successfully produced along ~1m-length waveguide. The arrayed-slot structure, however, the plasma is not completely uniform along the waveguide and plasma density drastically decreases between two adjacent slots. To solve this, an alternative type of antenna that is free from the standing wave effect is designed. In this new-type antenna, travelling wave inside the waveguide with no reflection wave is realized by a combination of a microwave circulator and a ring-structured waveguide. By this transmission line, microwave power flows only to one direction and the average microwave power becomes spatially uniform along the waveguide. By using a single but very long slot up to several tens cm, very uniform plasma is produced along the slot. The result strongly suggests easy scale-up of the plasma source more than one meter that

  6. How to Ignite an Atmospheric Pressure Microwave Plasma Torch without Any Additional Igniters.

    Science.gov (United States)

    Leins, Martina; Gaiser, Sandra; Schulz, Andreas; Walker, Matthias; Schumacher, Uwe; Hirth, Thomas

    2015-04-16

    This movie shows how an atmospheric pressure plasma torch can be ignited by microwave power with no additional igniters. After ignition of the plasma, a stable and continuous operation of the plasma is possible and the plasma torch can be used for many different applications. On one hand, the hot (3,600 K gas temperature) plasma can be used for chemical processes and on the other hand the cold afterglow (temperatures down to almost RT) can be applied for surface processes. For example chemical syntheses are interesting volume processes. Here the microwave plasma torch can be used for the decomposition of waste gases which are harmful and contribute to the global warming but are needed as etching gases in growing industry sectors like the semiconductor branch. Another application is the dissociation of CO2. Surplus electrical energy from renewable energy sources can be used to dissociate CO2 to CO and O2. The CO can be further processed to gaseous or liquid higher hydrocarbons thereby providing chemical storage of the energy, synthetic fuels or platform chemicals for the chemical industry. Applications of the afterglow of the plasma torch are the treatment of surfaces to increase the adhesion of lacquer, glue or paint, and the sterilization or decontamination of different kind of surfaces. The movie will explain how to ignite the plasma solely by microwave power without any additional igniters, e.g., electric sparks. The microwave plasma torch is based on a combination of two resonators - a coaxial one which provides the ignition of the plasma and a cylindrical one which guarantees a continuous and stable operation of the plasma after ignition. The plasma can be operated in a long microwave transparent tube for volume processes or shaped by orifices for surface treatment purposes.

  7. How to Ignite an Atmospheric Pressure Microwave Plasma Torch without Any Additional Igniters

    Science.gov (United States)

    Leins, Martina; Gaiser, Sandra; Schulz, Andreas; Walker, Matthias; Schumacher, Uwe; Hirth, Thomas

    2015-01-01

    This movie shows how an atmospheric pressure plasma torch can be ignited by microwave power with no additional igniters. After ignition of the plasma, a stable and continuous operation of the plasma is possible and the plasma torch can be used for many different applications. On one hand, the hot (3,600 K gas temperature) plasma can be used for chemical processes and on the other hand the cold afterglow (temperatures down to almost RT) can be applied for surface processes. For example chemical syntheses are interesting volume processes. Here the microwave plasma torch can be used for the decomposition of waste gases which are harmful and contribute to the global warming but are needed as etching gases in growing industry sectors like the semiconductor branch. Another application is the dissociation of CO2. Surplus electrical energy from renewable energy sources can be used to dissociate CO2 to CO and O2. The CO can be further processed to gaseous or liquid higher hydrocarbons thereby providing chemical storage of the energy, synthetic fuels or platform chemicals for the chemical industry. Applications of the afterglow of the plasma torch are the treatment of surfaces to increase the adhesion of lacquer, glue or paint, and the sterilization or decontamination of different kind of surfaces. The movie will explain how to ignite the plasma solely by microwave power without any additional igniters, e.g., electric sparks. The microwave plasma torch is based on a combination of two resonators — a coaxial one which provides the ignition of the plasma and a cylindrical one which guarantees a continuous and stable operation of the plasma after ignition. The plasma can be operated in a long microwave transparent tube for volume processes or shaped by orifices for surface treatment purposes. PMID:25938699

  8. In-Package atmospheric cold plasma treatment of bulk grape tomatoes for their microbiological safety and preservation

    Science.gov (United States)

    Effects of dielectric barrier discharge atmospheric cold plasma (DACP) treatment on the inactivation of Salmonella and the storability of grape tomato were investigated. Grape tomatoes, with or without inoculation with Salmonella, were packaged in a polyethylene terephthalate (PET) commercial clamsh...

  9. Elimination of Aspergillus parasiticus from nut surface with low pressure cold plasma (LPCP) treatment.

    Science.gov (United States)

    Basaran, Pervin; Basaran-Akgul, Nese; Oksuz, Lutfi

    2008-06-01

    Low pressure cold plasma (LPCP) using air gases and sulfur hexafluoride (SF(6)) was developed and tested for anti-fungal efficacy against Aspergillus parasiticus on various nut samples. Artificially A. parasiticus contaminated hazelnuts, peanuts, and pistachio nuts were treated with air gases plasma and SF(6) plasma for up to 20 min duration. The sterilizing effect of LPCP on A. parasiticus was higher during the early treatment period than the later treatment period. Air gases plasma treatment for 5 min resulted in 1-log reduction of A. parasiticus and a further 5 min treatment resulted in additional 1-log reduction. SF(6) plasma application was more effective resulting in approximately a 5-log decrease in fungal population for the same duration. When effectiveness of plasma treatment against aflatoxins were tested, 20 min air gases plasma treatment resulted in a 50% reduction in total aflatoxins (AFB1, AFB2, AFG1, and AFG2), while only a 20% reduction in total aflatoxin was observed after 20 min SF(6) plasma treatment. In this study, a rapid, functional clean-up method for the elimination of aflatoxin producing fungus from shelled and unshelled nuts was investigated as a suitable fungal decontamination method.

  10. Effect of atmospheric pressure plasma treatment condition on adhesion of ramie fibers to polypropylene for composite

    International Nuclear Information System (INIS)

    Li, Ying; Manolache, Sorin; Qiu, Yiping; Sarmadi, Majid

    2016-01-01

    Graphical abstract: - Highlights: • The continuous ethanol flow technique can successfully modify ramie fiber surface with an increase in IFSS value up to 50%. • Response surface methodology was applied to design the plasma treatment parameters for ramie fiber modification. • The ethanol flow rate was the most influential treatment parameter in plasma modification process. - Abstract: In order to improve the interfacial adhesion between hydrophilic ramie fibers and hydrophobic polypropylene (PP) matrices, ramie fibers are modified by atmospheric pressure dielectric barrier discharge (DBD) plasma with our continuous ethanol flow technique in helium environment. A central composite design of experiments with different plasma processing parameter combinations (treatment current, treatment time and ethanol flow rate) is applied to find the most influential parameter and to obtain the best modification effect. Field emission scanning electron microscope (SEM) shows the roughened surfaces of ramie fibers from the treated groups due to plasma etching effect. Dynamic contact angle analysis (DCAA) demonstrates that the wettability of the treated fibers drastically decreases. Microbond pullout test shows that the interfacial shear strength (IFSS) between treated ramie fibers and PP matrices increases significantly. Residual gas analysis (RGA) confirms the creation of ethyl groups during plasma treatment. This study shows that our continuous ethanol flow technique is effective in the plasma modification process, during which the ethanol flow rate is the most influential parameter but all parameters have simultaneous influence on plasma modification effect of ramie fibers.

  11. Effect of atmospheric pressure plasma treatment condition on adhesion of ramie fibers to polypropylene for composite

    Energy Technology Data Exchange (ETDEWEB)

    Li, Ying [College of Material and Textile Engineering, Jiaxing University, Jiaxing 314033 (China); Center for Plasma-Aided Manufacturing, Madison, WI 53706 (United States); School of Human Ecology, University of Wisconsin-Madison, Madison, WI 53706 (United States); Manolache, Sorin [Center for Plasma-Aided Manufacturing, Madison, WI 53706 (United States); US Forest Products Laboratory, Madison, WI 53726 (United States); Qiu, Yiping, E-mail: ypqiu@dhu.edu.cn [College of Textiles, Donghua University, Shanghai 201620 (China); Sarmadi, Majid, E-mail: majidsar@wisc.edu [Center for Plasma-Aided Manufacturing, Madison, WI 53706 (United States); School of Human Ecology, University of Wisconsin-Madison, Madison, WI 53706 (United States); Materials Science Program, University of Wisconsin-Madison, Madison, WI 53706 (United States)

    2016-02-28

    Graphical abstract: - Highlights: • The continuous ethanol flow technique can successfully modify ramie fiber surface with an increase in IFSS value up to 50%. • Response surface methodology was applied to design the plasma treatment parameters for ramie fiber modification. • The ethanol flow rate was the most influential treatment parameter in plasma modification process. - Abstract: In order to improve the interfacial adhesion between hydrophilic ramie fibers and hydrophobic polypropylene (PP) matrices, ramie fibers are modified by atmospheric pressure dielectric barrier discharge (DBD) plasma with our continuous ethanol flow technique in helium environment. A central composite design of experiments with different plasma processing parameter combinations (treatment current, treatment time and ethanol flow rate) is applied to find the most influential parameter and to obtain the best modification effect. Field emission scanning electron microscope (SEM) shows the roughened surfaces of ramie fibers from the treated groups due to plasma etching effect. Dynamic contact angle analysis (DCAA) demonstrates that the wettability of the treated fibers drastically decreases. Microbond pullout test shows that the interfacial shear strength (IFSS) between treated ramie fibers and PP matrices increases significantly. Residual gas analysis (RGA) confirms the creation of ethyl groups during plasma treatment. This study shows that our continuous ethanol flow technique is effective in the plasma modification process, during which the ethanol flow rate is the most influential parameter but all parameters have simultaneous influence on plasma modification effect of ramie fibers.

  12. Elimination of diazinon insecticide from cucumber surface by atmospheric pressure air-dielectric barrier discharge plasma.

    Science.gov (United States)

    Dorraki, Naghme; Mahdavi, Vahideh; Ghomi, Hamid; Ghasempour, Alireza

    2016-12-06

    The food industry is in a constant search for new technologies to improve the commercial sterilization process of agricultural commodities. Plasma treatment may offer a novel and efficient method for pesticide removal from agricultural product surfaces. To study the proposed technique of plasma food treatment, the degradation behavior of diazinon insecticide by air-dielectric barrier discharge (DBD) plasma was investigated. The authors studied the effect of different plasma powers and treatment times on pesticide concentration in liquid form and coated on the surface of cucumbers, where the diazinon residue was analyzed with mass spectroscopy gas chromatography. Our results suggest that atmospheric pressure air-DBD plasma is potentially effective for the degradation of diazinon insecticide, and mainly depends on related operating parameters, including plasma treatment time, discharge power, and pesticide concentrations. Based on the interaction between reactive oxygen species and electrons in the plasma with the diazinon molecule, two degradation pathway of diazinon during plasma treatment are proposed. It was also found that produced organophosphate pesticides are harmless and less hazardous compounds than diazinon.

  13. Sterilization effect of atmospheric pressure non-thermal air plasma on dental instruments.

    Science.gov (United States)

    Sung, Su-Jin; Huh, Jung-Bo; Yun, Mi-Jung; Chang, Brian Myung W; Jeong, Chang-Mo; Jeon, Young-Chan

    2013-02-01

    Autoclaves and UV sterilizers have been commonly used to prevent cross-infections between dental patients and dental instruments or materials contaminated by saliva and blood. To develop a dental sterilizer which can sterilize most materials, such as metals, rubbers, and plastics, the sterilization effect of an atmospheric pressure non-thermal air plasma device was evaluated. After inoculating E. coli and B. subtilis the diamond burs and polyvinyl siloxane materials were sterilized by exposing them to the plasma for different lengths of time (30, 60, 90, 120, 180 and, 240 seconds). The diamond burs and polyvinyl siloxane materials were immersed in PBS solutions, cultured on agar plates and quantified by counting the colony forming units. The data were analyzed using one-way ANOVA and significance was assessed by the LSD post hoc test (α=0.05). The device was effective in killing E. coli contained in the plasma device compared with the UV sterilizer. The atmospheric pressure non-thermal air plasma device contributed greatly to the sterilization of diamond burs and polyvinyl siloxane materials inoculated with E. coli and B. subtilis. Diamond burs and polyvinyl siloxane materials inoculated with E. coli was effective after 60 and 90 seconds. The diamond burs and polyvinyl siloxane materials inoculated with B. subtilis was effective after 120 and 180 seconds. The atmospheric pressure non-thermal air plasma device was effective in killing both E. coli and B. subtilis, and was more effective in killing E. coli than the UV sterilizer.

  14. Attenuation Effects of Plasma on Ka-Band Wave Propagation in Various Gas and Pressure Environments

    Directory of Open Access Journals (Sweden)

    Joo Hwan Lee

    2018-01-01

    Full Text Available This work demonstrates attenuation effects of plasma on waves propagating in the 26.5–40 GHz range. The effect is investigated via experiments measuring the transmission between two Ka-band horn antennas set 30 cm apart. A dielectric-barrier-discharge (DBD plasma generator with a size of 200 mm × 100 mm × 70 mm and consisting of 20 layers of electrodes is placed between the two antennas. The DBD generator is placed in a 400 mm × 300 mm × 400 mm acrylic chamber so that the experiments can be performed for plasma generated under various conditions of gas and pressure, for instance, in air, Ar, and He environments at 0.001, 0.05, and 1 atm of pressure. Attenuation is calculated by the difference in the transmission level, with and without plasma, which is generated with a bias voltage of 20 kV in the 0.1–1.4 kHz range. Results show that the attenuation varies from 0.05 dB/m to 9.0 dB/m depending on the environment. Noble gas environments show higher levels of attenuation than air, and He is lossier than Ar. In all gas environments, attenuation increases as pressure increases. Finally, electromagnetic models of plasmas generated in various conditions are provided.

  15. Studies of air, water, and ethanol vapor atmospheric pressure plasmas for antimicrobial applications.

    Science.gov (United States)

    Ferrell, James R; Bogovich, Erinn R; Lee, Nicholas R; Gray, Robert L; Pappas, Daphne D

    2015-06-25

    The generation of air-based plasmas under atmospheric plasma conditions was studied to assess their antimicrobial efficacy against commonly found pathogenic bacteria. The mixture of initial gases supplied to the plasma was found to be critical for the formation of bactericidal actives. The optimal gas ratio for bactericidal effect was determined to be 99% nitrogen and 1% oxygen, which led to a 99.999% reduction of a pathogenic strain of Escherichia coli on stainless steel surfaces. The experimental substrate, soil load on the substrate, flow rate of the gases, and addition of ethanol vapor all were found to affect antimicrobial efficacy of studied plasmas. Optical emission spectroscopy was used to identify the species that were present in the plasma bulk phase for multiple concentrations of nitrogen and oxygen ratios. The collected spectra indicate a unique series of bands present in the ultraviolet region of the electromagnetic spectrum that can be attributed to nitric oxide species known to be highly antimicrobial. This intense spectral profile dramatically changes as the concentration of nitrogen decreases.

  16. Influence of atmospheric pressure plasma treatment on surface properties of PBO fiber

    International Nuclear Information System (INIS)

    Zhang Ruiyun; Pan Xianlin; Jiang Muwen; Peng Shujing; Qiu Yiping

    2012-01-01

    Highlights: ► PBO fibers were treated with atmospheric pressure plasmas. ► When 1% of oxygen was added to the plasma, IFSS increased 130%. ► Increased moisture regain could enhance plasma treatment effect on improving IFSS with long treatment time. - Abstract: In order to improve the interfacial adhesion property between PBO fiber and epoxy, the surface modification effects of PBO fiber treated by atmospheric pressure plasma jet (APPJ) in different time, atmosphere and moisture regain (MR) were investigated. The fiber surface morphology, functional groups, surface wettability for control and plasma treated samples were analyzed by scanning electron microscope (SEM), X-ray photoelectron spectroscopy (XPS) and water contact angle measurements, respectively. Meanwhile, the fiber interfacial shear strength (IFSS), representing adhesion property in epoxy, was tested using micro-bond pull-out test, and single fiber tensile strength was also tested to evaluate the mechanical performance loss of fibers caused by plasma treatment. The results indicated that the fiber surface was etched during the plasma treatments, the fiber surface wettability and the IFSS between fiber and epoxy had much improvement due to the increasing of surface energy after plasma treatment, the contact angle decreased with the treatment time increasing, and the IFSS was improved by about 130%. The processing atmosphere could influence IFSS significantly, and moisture regains (MR) of fibers also played a positive role on improving IFSS but not so markedly. XPS analysis showed that the oxygen content on fiber surface increased after treatment, and C=O, O-C=O groups were introduced on fiber surface. On the other hand, the observed loss of fiber tensile strength caused by plasma treatment was not so remarkable to affect the overall performance of composite materials.

  17. Calculation of the net emission coefficient of an air thermal plasma at very high pressure

    International Nuclear Information System (INIS)

    Billoux, T; Cressault, Y; Teulet, Ph; Gleizes, A

    2012-01-01

    The aim of this paper is to present an accurate evaluation of the phenomena appearing for high pressure air plasmas supposed to be in local thermodynamic equilibrium (LTE). In the past, we already calculated the net emission coefficient for air mixtures at atmospheric pressure and for temperatures up to 30kK (molecular contribution being restricted to 10kK). Unfortunately, the existence of high pressures does not allow us to use this database due to the non-ideality of the plasma (Viriel and Debye corrections, energy cut-off ...), and due to the significant shifts of molecular reactions towards upper temperatures. Consequently, this paper proposes an improvement of our previous works with a consideration of high pressure corrections in the composition algorithm in order to take into account the pressure effects, and with a new calculation of all the contributions of the plasma radiation (atomic lines and continuum, molecular continuum, and molecular bands) using an updated database. A particular attention is paid to calculate the contribution of all the major molecular band systems to the radiation: O 2 (Schumann–Runge), N 2 (VUV, 1st and 2nd positive), NO (IR, β, γ, δ, element of ) and N 2 + (1st negative and Meinel). The discrete atomic lines and molecular bands radiation including the overlapping are calculated by a line-by-line method up to 30kK and 100 bar. This updated database is validated in the case of optically thin plasmas and pressure of 1bar by the comparison of our integrated emission strength with the published results. Finally, this work shows the necessity to extend the molecular radiation database up to 15kK at high pressure (bands and continuum) since their corresponding contributions could not be neglected at high temperature.

  18. Sterilization of packed matter by means of low temperature atmospheric pressure plasmas

    DEFF Research Database (Denmark)

    Leipold, Frank

    2010-01-01

    Summary form only given. The decontamination of material in closed containers by means of atmospheric pressure plasmas is investigated. The target is Listeria monocytogenes, a bacterium which causes listeriosis and can be found in plants and food. The non-pathogenic species, Listeria innocua...

  19. Effect of pressure on behavior of anode attachment of dc arc plasma torch

    Czech Academy of Sciences Publication Activity Database

    Chumak, Oleksiy; Kopecký, Vladimír; Konrád, Miloš; Kavka, Tetyana; Hrabovský, Milan

    2005-01-01

    Roč. 9, č. 3 (2005), s. 391-400 ISSN 1093-3611 R&D Projects: GA ČR GA202/05/0669 Institutional research plan: CEZ:AV0Z20430508 Keywords : arc anode * dc arc jet * anode restrike * low pressure Subject RIV: BL - Plasma and Gas Discharge Physics Impact factor: 0.136, year: 2005

  20. Power-law scaling of plasma pressure on laser-ablated tin microdroplets

    NARCIS (Netherlands)

    Kurilovich, Dmitry; Basko, Mikhail M.; Kim, Dmitrii A.; Torretti, Francesco; Schupp, Ruben; Visschers, Jim C.; Scheers, Joris; Hoekstra, Ronnie; Ubachs, Wim; Versolato, Oscar O.

    The measurement of the propulsion of metallic microdroplets exposed to nanosecond laser pulses provides an elegant method for probing the ablation pressure in a dense laser-produced plasma. We present the measurements of the propulsion velocity over three decades in the driving Nd:YAG laser pulse

  1. Conversion of high-pressure carbon dioxide by laser-induced plasma

    Science.gov (United States)

    Goto, Taku; Suzuki, Hirotaka; Koizumi, Masato; Ito, Tsuyohito

    2016-09-01

    In the conversion process of CO2 ->CO + 1/2 O2 by means of plasma, an atomic oxygen is often observed as the intermediate state. As the following reaction forming 1/2 O2 from O is exothermic, unless the energy is reused, the existence of O atoms results in a lower conversion efficiency of the process. Thus, we are trying to find a pathway which forms 1/2 O2 directly, by contribution of the high pressure, which hopefully boosts the conversion efficiency. In this study, we produce plasma by nanosecond-pulsed laser focused on various metallic targets (Sn, Zn and Cu) in pressurized CO2 environments. The results indicate that the energy conversion efficiency depends on the pressure. In addition, applying a target results in a higher energy conversion efficiency than that without targets, and the efficiency depends on the target materials. We currently believe that the target materials modify the initial density of plasma and the pressure controls the following plasma dynamics. The details will be presented at the conference.

  2. Application of atmospheric pressure nonthermal plasma for the in vitro eradication of bacterial biofilms.

    Science.gov (United States)

    Alkawareek, Mahmoud Y; Algwari, Qais T; Gorman, Sean P; Graham, William G; O'Connell, Deborah; Gilmore, Brendan F

    2012-07-01

    The use of atmospheric pressure nonthermal plasma represents an interesting and novel approach for the decontamination of surfaces colonized with microbial biofilms that exhibit enhanced tolerance to antimicrobial challenge. In this study, the influence of an atmospheric pressure nonthermal plasma jet, operated in a helium and oxygen gas mixture under ambient pressure, was evaluated against biofilms of Bacillus cereus, Staphylococcus aureus, Escherichia coli and Pseudomonas aeruginosa. Within < 4 min of plasma exposure, complete eradication of the two gram-positive bacterial biofilms was achieved. Although gram-negative biofilms required longer treatment time, their complete eradication was still possible with 10 min of exposure. Whilst this study provides useful proof of concept data on the use of atmospheric pressure plasmas for the eradication of bacterial biofilms in vitro, it also demonstrates the critical need for improved understanding of the mechanisms and kinetics related to such a potentially significant approach. © 2012 Federation of European Microbiological Societies. Published by Blackwell Publishing Ltd. All rights reserved.

  3. Effects of atmospheric pressure plasma jet with floating electrode on murine melanoma and fibroblast cells

    Science.gov (United States)

    Xu, G.; Liu, J.; Yao, C.; Chen, S.; Lin, F.; Li, P.; Shi, X.; Zhang, Guan-Jun

    2017-08-01

    Atmospheric pressure cold plasma jets have been recently shown as a highly promising tool in certain cancer therapies. In this paper, an atmospheric pressure plasma jet (APPJ) with a one inner floating and two outer electrode configuration using helium gas for medical applications is developed. Subjected to a range of applied voltages with a frequency of 19.8 kHz at a fixed rate of gas flow (i.e., 3 l/min), electrical and optical characteristics of the APPJ are investigated. Compared with the device only with two outer electrodes, higher discharge current, longer jet, and more active species in the plasma plume at the same applied voltage together with the lower gas breakdown voltage can be achieved through embedding a floating inner electrode. Employing the APPJ with a floating electrode, the effects of identical plasma treatment time durations on murine melanoma cancer and normal fibroblast cells cultured in vitro are evaluated. The results of cell viability, cell apoptosis, and DNA damage detection show that the plasma can inactivate melanoma cells in a time-dependent manner from 10 s to 60 s compared with the control group (p treatment time from 30 s to 60 s can induce significant changes (p melanoma cells at the same treatment time. The different basal reactive oxygen species level and antioxidant superoxide dismutase level of two kinds of cells may account for their different responses towards the identical plasma exposure.

  4. Sterilization by negative and positive DC plasma with a micro discharge gap at atmospheric pressure

    Science.gov (United States)

    Li, Hua; Jiang, Lin-Xiu; Jiang, Yong-Rong; Zhu, Jian-Min; Chen, Zhen-Cheng

    2017-11-01

    A new needle-to-droplet electrode structure with a micro discharge gap (2 mm) was designed to achieve direct current (DC) discharge plasma in ambient air with the aim of using the plasma to sterilize liquids. Without using noble gases or an external air flow, we succeeded in generating both a negative and positive DC plasma at atmospheric pressure. The plasma was driven by a 0 to ‑20,000 V, 100 W DC power supply. A stainless steel needle with a tip diameter of ˜ 50μm and a 200-μL droplet of bacteria-containing liquid served as the electrodes. At atmospheric pressure and room temperature (23∘C), utilizing the negative DC plasma, the discharge time lasted 10 s; the results showed that the higher the discharge voltage, the more efficient the sterilization effect. Conversely, when we applied a voltage of ‑5.5 kV, we found that the sterilization effect was more efficient for longer discharge times. Our findings demonstrate that Escherichia coli (E. coli) and Bacillus subtilis (B. subtilis) can be killed in about 30 s. Our experiments show that our sterilization method required less time and was more efficient for positive than for negative DC plasma under the same conditions.

  5. Electron density measurement of non-equilibrium atmospheric pressure plasma using dispersion interferometer

    Science.gov (United States)

    Yoshimura, Shinji; Kasahara, Hiroshi; Akiyama, Tsuyoshi

    2017-10-01

    Medical applications of non-equilibrium atmospheric plasmas have recently been attracting a great deal of attention, where many types of plasma sources have been developed to meet the purposes. For example, plasma-activated medium (PAM), which is now being studied for cancer treatment, has been produced by irradiating non-equilibrium atmospheric pressure plasma with ultrahigh electron density to a culture medium. Meanwhile, in order to measure electron density in magnetic confinement plasmas, a CO2 laser dispersion interferometer has been developed and installed on the Large Helical Device (LHD) at the National Institute for Fusion Science, Japan. The dispersion interferometer has advantages that the measurement is insensitive to mechanical vibrations and changes in neutral gas density. Taking advantage of these properties, we applied the dispersion interferometer to electron density diagnostics of atmospheric pressure plasmas produced by the NU-Global HUMAP-WSAP-50 device, which is used for producing PAM. This study was supported by the Grant of Joint Research by the National Institutes of Natural Sciences (NINS).

  6. Synergistic effects of atmospheric pressure plasma-emitted components on DNA oligomers: a Raman spectroscopic study.

    Science.gov (United States)

    Edengeiser, Eugen; Lackmann, Jan-Wilm; Bründermann, Erik; Schneider, Simon; Benedikt, Jan; Bandow, Julia E; Havenith, Martina

    2015-11-01

    Cold atmospheric-pressure plasmas have become of increasing importance in sterilization processes especially with the growing prevalence of multi-resistant bacteria. Albeit the potential for technological application is obvious, much less is known about the molecular mechanisms underlying bacterial inactivation. X-jet technology separates plasma-generated reactive particles and photons, thus allowing the investigation of their individual and joint effects on DNA. Raman spectroscopy shows that particles and photons cause different modifications in DNA single and double strands. The treatment with the combination of particles and photons does not only result in cumulative, but in synergistic effects. Profilometry confirms that etching is a minor contributor to the observed DNA damage in vitro. Schematics of DNA oligomer treatment with cold atmospheric-pressure plasma. © 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  7. Simulation of propagation of the HPM in the low-pressure argon plasma

    Science.gov (United States)

    Zhigang, LI; Zhongcai, YUAN; Jiachun, WANG; Jiaming, SHI

    2018-02-01

    The propagation of the high-power microwave (HPM) with a frequency of 6 GHz in the low-pressure argon plasma was studied by the method of fluid approximation. The two-dimensional transmission model was built based on the wave equation, the electron drift-diffusion equations and the heavy species transport equations, which were solved by means of COMSOL Multiphysics software. The simulation results showed that the propagation characteristic of the HPM was closely related to the average electron density of the plasma. The attenuation of the transmitted wave increased nonlinearly with the electron density. Specifically, the growth of the attenuation slowed down as the electron density increased uniformly. In addition, the concrete transmission process of the HPM wave in the low-pressure argon plasma was given.

  8. Atmospheric pressure plasma jets: an overview of devices and new directions

    Science.gov (United States)

    Winter, J.; Brandenburg, R.; Weltmann, K.-D.

    2015-12-01

    Atmospheric pressure plasma jets have a long history of more than 50 years. During this time their design and plasma generation mechanism has been developed and adapted to various fields of applications. This review aims at giving an overview of jet devices by starting with a brief history of their development. This is followed by an overview of commonly used terms and definitions as well as a survey of different classification schemes (e.g. geometry, excition frequency or specific energy input) described in literature. A selective update of new designs and novel research achievments on atmospheric pressure plasma jets published in 2012 or later shows the impressive variety and rapid development of the field. Finally, a brief outlook on the future trends and directions is given.

  9. The effect of sheared toroidal rotation on pressure driven magnetic islands in toroidal plasmas

    Energy Technology Data Exchange (ETDEWEB)

    Hegna, C. C. [Departments of Engineering Physics and Physics, University of Wisconsin-Madison, Madison, Wisconsin 53706 (United States)

    2016-05-15

    The impact of sheared toroidal rotation on the evolution of pressure driven magnetic islands in tokamak plasmas is investigated using a resistive magnetohydrodynamics model augmented by a neoclassical Ohm's law. Particular attention is paid to the asymptotic matching data as the Mercier indices are altered in the presence of sheared flow. Analysis of the nonlinear island Grad-Shafranov equation shows that sheared flows tend to amplify the stabilizing pressure/curvature contribution to pressure driven islands in toroidal tokamaks relative to the island bootstrap current contribution. As such, sheared toroidal rotation tends to reduce saturated magnetic island widths.

  10. Characterizations of atmospheric pressure low temperature plasma jets and their applications

    Science.gov (United States)

    Karakas, Erdinc

    2011-12-01

    Atmospheric pressure low temperature plasma jets (APLTPJs) driven by short pulses have recently received great attention because of their potential in biomedical and environmental applications. This potential is due to their user-friendly features, such as low temperature, low risk of arcing, operation at atmospheric pressure, easy handheld operation, and low concentration of ozone generation. Recent experimental observations indicate that an ionization wave exists and propagates along the plasma jet. The plasma jet created by this ionization wave is not a continuous medium but rather consists of a bullet-like-structure known as "Plasma Bullet". More interestingly, these plasma bullets actually have a donut-shaped makeup. The nature of the plasma bullet is especially interesting because it propagates in the ambient air at supersonic velocities without any externally applied electric field. In this dissertation, experimental insights are reported regarding the physical and chemical characteristics of the APLTPJs. The dynamics of the plasma bullet are investigated by means of a high-speed ICCD camera. A plasma bullet propagation model based on the streamer theory is confirmed with adequate explanations. It is also found that a secondary discharge, ignited by the charge accumulation on the dielectric electrode surfaces at the end of the applied voltage, interrupts the plasma bullet propagation due to an opposing current along the ionization channel. The reason for this interesting phenomenon is explained in detail. The plasma bullet comes to an end when the helium mole fraction along the ionization channel, or applied voltage, or both, are less than some critical values. The presence of an inert gas channel in the surrounding air, such as helium or argon, has a critical role in plasma bullet formation and propagation. For this reason, a fluid dynamics study is employed by a commercially available simulation software, COMSOL, based on finite element method. Spatio

  11. Development of bio/blood compatible polypropylene through low pressure nitrogen plasma surface modification

    Energy Technology Data Exchange (ETDEWEB)

    Gomathi, N., E-mail: gomathi@iist.ac.in [Department of Chemistry, Indian Institute of Space Science and Technology, Department of Space, Trivandrum, 695547 (India); Department of Chemical Engineering, Indian Institute of Technology, Kharagpur, 721302 (India); Rajasekar, R. [Materials Science Center, Indian Institute of Technology, Kharagpur, 721302 (India); Department of BIN Fusion Technology, Chonbuk National University, Jeonju, Jeonbuk, 561-756 (Korea, Republic of); Babu, R. Rajesh [Rubber Technology Center, Indian Institute of Technology, Kharagpur, 721302 (India); Advanced Tyre Research, Apollo Tyres, Baroda, 391750 (India); Mishra, Debasish [Department of Biotechnolgy, Indian Institute of Technology, Kharagpur, 721302 (India); Neogi, S. [Department of Chemical Engineering, Indian Institute of Technology, Kharagpur, 721302 (India)

    2012-10-01

    Surface modification of polypropylene by nitrogen containing plasma was performed in this work in order to improve the wettability which resulted in enhanced biocompatibility and blood compatibility. Various nitrogen containing functional groups as well as oxygen containing functional groups were found to be incorporated to the polymer surface during plasma treatment and post plasma reaction respectively. Wettability of the polymers was evaluated by static contact angle measurement to show the improvement in hydrophilicity of plasma treated polypropylene. Cross linking and surface modification were reported to be dominating in the case of nitrogen plasma treatment compared to degradation. The effect of various process variables namely power, pressure, flow rate and treatment time on surface energy and weight loss was studied at various levels according to the central composite design of response surface methodology (RSM). Except pressure the other variables resulted in increased weight loss due to etching whereas with increasing pressure weight loss was found to increase and then decrease. The effect of process variables on surface morphology of polymers was evaluated by Scanning Electron Microscopy (SEM) and Atomic Force Microscopy (AFM). Well spread fibroblast cells on nitrogen plasma treated polypropylene due to the presence of CO, NH{sup 2+} and NH{sup +} was observed. Reduced platelet adhesion and increased partial thromboplastin time evidenced the increased blood compatibility. - Highlights: Black-Right-Pointing-Pointer Improved biocompatibility and blood compatibility of polypropylene. Black-Right-Pointing-Pointer Nitrogen plasma surface modification. Black-Right-Pointing-Pointer Maintaining a balance between polar group incorporation and weight loss due to etching. Black-Right-Pointing-Pointer Optimization of process conditions by response surface methodology.

  12. Development of bio/blood compatible polypropylene through low pressure nitrogen plasma surface modification

    International Nuclear Information System (INIS)

    Gomathi, N.; Rajasekar, R.; Babu, R. Rajesh; Mishra, Debasish; Neogi, S.

    2012-01-01

    Surface modification of polypropylene by nitrogen containing plasma was performed in this work in order to improve the wettability which resulted in enhanced biocompatibility and blood compatibility. Various nitrogen containing functional groups as well as oxygen containing functional groups were found to be incorporated to the polymer surface during plasma treatment and post plasma reaction respectively. Wettability of the polymers was evaluated by static contact angle measurement to show the improvement in hydrophilicity of plasma treated polypropylene. Cross linking and surface modification were reported to be dominating in the case of nitrogen plasma treatment compared to degradation. The effect of various process variables namely power, pressure, flow rate and treatment time on surface energy and weight loss was studied at various levels according to the central composite design of response surface methodology (RSM). Except pressure the other variables resulted in increased weight loss due to etching whereas with increasing pressure weight loss was found to increase and then decrease. The effect of process variables on surface morphology of polymers was evaluated by Scanning Electron Microscopy (SEM) and Atomic Force Microscopy (AFM). Well spread fibroblast cells on nitrogen plasma treated polypropylene due to the presence of CO, NH 2+ and NH + was observed. Reduced platelet adhesion and increased partial thromboplastin time evidenced the increased blood compatibility. - Highlights: ► Improved biocompatibility and blood compatibility of polypropylene. ► Nitrogen plasma surface modification. ► Maintaining a balance between polar group incorporation and weight loss due to etching. ► Optimization of process conditions by response surface methodology.

  13. Theory of mass-discrimination effects in ion extraction from a plasma of wide pressure range

    International Nuclear Information System (INIS)

    Chang, J.-S.; Kodera, K.

    1979-01-01

    Mass-discrimination effects in stagnation-point ion extraction are treated for a plasma with a wide range of Knudsen number, i.e. when the charged particle's mean free path 3 , ion Schmidt numbers, from 0 to 10 4 , the effective Knudsen number K from 0 to infinity, and the Debye ratio Rsub(p)/lambdasub(D) from 0 to 10 -1 . Numerical results show that: (1) for a non-flowing plasma, mass-discrimination effects increase with increasing effective Knudsen number (or gas pressure) and decreasing sampling potential; (2) for a non-flowing plasma, no significant effect of the Debye ratio on mass-discrimination was found; (3) for a flowing plasma, mass-discrimination effects decrease with increasing Reynolds number (or flow velocity) and ion Schmidt number, and with decreasing sampling potential and effective Knudsen number. (Auth.)

  14. Application of a novel atmospheric pressure plasma fluidized bed in the powder surface modification

    International Nuclear Information System (INIS)

    Chen Guangliang; Chen Shihua; Zhou Mingyan; Feng Wenran; Gu Weichao; Yang Size

    2006-01-01

    A novel atmospheric pressure plasma fluidized bed (APPFB) with one liquid electrode was designed, and its preliminary discharge characteristics were studied. The glow discharge in the APPFB was generated by applying a low power with helium (He) gas, and the plasma gas temperature was no higher than 320 K when the applied power was lower than 11 W. The plasma optical emission spectrum (OES) of the gas mixture consisting of He and hexamethyldisiloxane (HMDSO) was recorded by a UV-visible monochromator. The calcium carbonate powders were modified by APPFB using HMDSO in the He plasma. The powder surface energy was decreased greatly by coating an organosilicon polymer onto the powder surface. This surface modification process changed the wettability of the powder from super-hydrophilicity to super-hydrophobicity, and the contact angle of water on the modified powders surface was greater than 160 0

  15. Effect of cold atmospheric pressure He-plasma jet on DNA change and mutation

    Science.gov (United States)

    Yaopromsiri, C.; Yu, L. D.; Sarapirom, S.; Thopan, P.; Boonyawan, D.

    2015-12-01

    Cold atmospheric pressure plasma jet (CAPPJ) effect on DNA change was studied for assessment of its safety. The experiment utilized a home-developed CAPPJ using 100% helium to directly treat naked DNA plasmid pGFP (plasmid green fluorescent protein). A traversal electric field was applied to separate the plasma components and both dry and wet sample conditions were adopted to investigate various factor roles in changing DNA. Plasma species were measured by using optical emission spectroscopy. DNA topological form change was analyzed by gel electrophoresis. The plasma jet treated DNA was transferred into bacterial Escherichia coli cells for observing mutation. The results show that the He-CAPPJ could break DNA strands due to actions from charge, radicals and neutrals and potentially cause genetic modification of living cells.

  16. Experimental and numerical investigations of microwave return loss of aircraft inlets with low-pressure plasma

    Science.gov (United States)

    Zhang, Yachun; He, Xiang; Chen, Jianping; Chen, Hongqing; Chen, Li; Zhang, Hongchao; Ni, Xiaowu; Lu, Jian; Shen, Zhonghua

    2018-03-01

    The relationships between return losses of the cylindrical inlet and plasma discharge parameters are investigated experimentally and numerically. The return losses are measured using a high dynamic range measurement system and simulated by COMSOL Multiphysics when the frequency band of the microwaves is in the range 1-4 GHz. The profiles of the plasma density are estimated using Epstein and Bessel functions. Results show that the incident microwaves can be absorbed by plasma efficaciously. The maximal return loss can reach -13.84 dB when the microwave frequency is 2.3 GHz. The increase of applied power implies augmentation of the return loss, which behaves conversely for gas pressure. The experimental and numerical results display reasonable agreement on return loss, suggesting that the use of plasma is effective in the radar cross section reduction of aircraft inlets.

  17. Influence of processing parameters on atmospheric pressure plasma etching of polyamide 6 films

    Science.gov (United States)

    Gao, Zhiqiang; Peng, Shujing; Sun, Jie; Yao, Lan; Qiu, Yiping

    2009-06-01

    This study is designed to systematically investigate how various factors, such as treatment duration, output power, oxygen gas flux, jet to substrate distance, and moisture regain, influence atmospheric pressure plasma etching rate of polyamide 6 (PA 6) films. The etching rate increased as the output power, oxygen gas flux, and moisture regain increased. As the treatment time increased, the etching rate increased first and then decreased. When the substrate was too close or too far from the nozzle, the etching rate was almost not measurable. Scanning electron microscopy (SEM) and atomic force microscopy (AFM) show an increased surface roughness after the plasma treatment. X-ray photoelectron spectroscopy (XPS) shows a decreased carbon content and an increased oxygen content after the plasma treatment. T-peel strength shows an improved bonding strength between the PA 6 films and an adhesive tape after the plasma treatment.

  18. Effect of cold atmospheric pressure He-plasma jet on DNA change and mutation

    Energy Technology Data Exchange (ETDEWEB)

    Yaopromsiri, C. [Plasma and Beam Physics Research Facility, Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand); Yu, L.D., E-mail: yuld@thep-center.org [Plasma and Beam Physics Research Facility, Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand); Thailand Center of Excellence in Physics, Commission on Higher Education, 328 Si Ayutthaya Road, Bangkok 10400 (Thailand); Sarapirom, S. [Plasma and Beam Physics Research Facility, Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand); Faculty of Science, Maejo University, Bang Khen, Chiang Mai 50290 (Thailand); Thopan, P.; Boonyawan, D. [Plasma and Beam Physics Research Facility, Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand)

    2015-12-15

    Cold atmospheric pressure plasma jet (CAPPJ) effect on DNA change was studied for assessment of its safety. The experiment utilized a home-developed CAPPJ using 100% helium to directly treat naked DNA plasmid pGFP (plasmid green fluorescent protein). A traversal electric field was applied to separate the plasma components and both dry and wet sample conditions were adopted to investigate various factor roles in changing DNA. Plasma species were measured by using optical emission spectroscopy. DNA topological form change was analyzed by gel electrophoresis. The plasma jet treated DNA was transferred into bacterial Escherichia coli cells for observing mutation. The results show that the He-CAPPJ could break DNA strands due to actions from charge, radicals and neutrals and potentially cause genetic modification of living cells.

  19. Acetylcysteine reduces plasma homocysteine concentration and improves pulse pressure and endothelial function in patients with end-stage renal failure

    DEFF Research Database (Denmark)

    Scholze, Alexandra; Rinder, Christiane; Beige, Joachim

    2004-01-01

    Increased oxidative stress, elevated plasma homocysteine concentration, increased pulse pressure, and impaired endothelial function constitute risk factors for increased mortality in patients with end-stage renal failure.......Increased oxidative stress, elevated plasma homocysteine concentration, increased pulse pressure, and impaired endothelial function constitute risk factors for increased mortality in patients with end-stage renal failure....

  20. Surface modification with a remote atmospheric pressure plasma: dc glow discharge and surface streamer regime

    International Nuclear Information System (INIS)

    Temmerman, Eef; Akishev, Yuri; Trushkin, Nikolay; Leys, Christophe; Verschuren, Jo

    2005-01-01

    A remote atmospheric pressure discharge working with ambient air is used for the near room temperature treatment of polymer foils and textiles of varying thickness. The envisaged plasma effect is an increase in the surface energy of the treated material, leading, e.g., to a better wettability or adhesion. Changes in wettability are examined by measuring the contact angle or the liquid absorptive capacity. Two regimes of the remote atmospheric pressure discharge are investigated: the glow regime and the streamer regime. These regimes differ mainly in power density and in the details of the electrode design. The results show that this kind of discharge makes up a convenient non-thermal plasma source to be integrated into a treatment installation working at atmospheric pressure

  1. Atmospheric pressure plasma jets interacting with liquid covered tissue: touching and not-touching the liquid

    International Nuclear Information System (INIS)

    Norberg, Seth A; Johnsen, Eric; Tian, Wei; Kushner, Mark J

    2014-01-01

    In the use of atmospheric pressure plasma jets in biological applications, the plasma-produced charged and neutral species in the plume of the jet often interact with a thin layer of liquid covering the tissue being treated. The plasma-produced reactivity must then penetrate through the liquid layer to reach the tissue. In this computational investigation, a plasma jet created by a single discharge pulse at three different voltages was directed onto a 200 µm water layer covering tissue followed by a 10 s afterglow. The magnitude of the voltage and its pulse length determined if the ionization wave producing the plasma plume reached the surface of the liquid. When the ionization wave touches the surface, significantly more charged species were created in the water layer with H 3 O + aq , O 3 − aq , and O 2 − aq being the dominant terminal species. More aqueous OH aq , H 2 O 2aq , and O 3aq were also formed when the plasma plume touches the surface. The single pulse examined here corresponds to a low repetition rate plasma jet where reactive species would be blown out of the volume between pulses and there is not recirculation of flow or turbulence. For these conditions, N x O y species do not accumulate in the volume. As a result, aqueous nitrites, nitrates, and peroxynitrite, and the HNO 3aq and HOONO aq , which trace their origin to solvated N x O y , have low densities. (paper)

  2. Development of an Organosilicon-Based Superhydrophobic/Icephobic Surface Using an Atmospheric Pressure Plasma Jet =

    Science.gov (United States)

    Asadollahi, Siavash

    During the past few decades, plasma-based surface treatment methods have gained a lot of interest in various applications such as thin film deposition, surface etching, surface activation and/or cleaning, etc. Generally, in plasma-based surface treatment methods, high-energy plasma-generated species are utilized to modify the surface structure or the chemical composition of a substrate. Unique physical and chemical characteristics of the plasma along with the high controllability of the process makes plasma treatment approaches very attractive in several industries. Plasma-based treatment methods are currently being used or investigated for a number of practical applications, such as adhesion promotion in auto industry, wound management and cancer treatment in biomedical industry, and coating development in aerospace industry. In this study, a two-step procedure is proposed for the development of superhydrophobic/icephobic coatings based on atmospheric-pressure plasma treatment of aluminum substrates using air and nitrogen plasma. The effects of plasma parameters on various surface properties are studied in order to identify the optimum conditions for maximum coating efficiency against icing and wetting. In the first step, the interactions between air or nitrogen plasma and the aluminum surface are studied. It is shown that by reducing jet-to-substrate distance, air plasma treatment, unlike nitrogen plasma treatment, is capable of creating micro-porous micro-roughened structures on the surface, some of which bear a significant resemblance to the features observed in laser ablation of metals with short and ultra-short laser pulses. The formation of such structures in plasma treatment is attributed to a transportation of energy from the jet to the surface over a very short period of time, in the range of picoseconds to microseconds. This energy transfer is shown to occur through a streamer discharge from the rotating arc source in the jet body to a close proximity of

  3. Variability of hydrostatic hepatic vein and ascitic fluid pressure, and of plasma and ascitic fluid colloid osmotic pressure in patients with liver cirrhosis

    DEFF Research Database (Denmark)

    Henriksen, Jens Henrik Sahl

    1980-01-01

    The variability of hydrostatic hepatic vein and ascitic fluid pressures and of plasma and ascitic fluid colloid osmotic (oncotic) pressures was assessed during hepatic venous catheterization by repeated measurements on different days and at different locations in patients with cirrhosis...... during catheterization give a good reproducibility in determination of the hydrostatic pressures in hepatic vein and ascitic fluid and of the colloid osmotic (oncotic) pressure in plasma and ascitic fluid in the resting supine patient with cirrhosis, which substantiates the use of measurements during...... of the liver. Furthermore, calculation of oncotic pressure from protein determinations was compared to the directly measured value of plasma and ascitic fluid samples. Repeated measurements of hydrostatic pressure in the same hepatic vein within 15 min showed a standard deviation (SD) below 1 mm...

  4. High-strength bulk nano-crystalline silver prepared by selective leaching combined with spark plasma sintering

    Czech Academy of Sciences Publication Activity Database

    Marek, I.; Vojtěch, D.; Michalcová, A.; Kubatík, Tomáš František

    2015-01-01

    Roč. 627, March (2015), s. 326-332 ISSN 0921-5093 Institutional support: RVO:61389021 Keywords : Nano-crystalline material * Selective leaching * Silver * Spark plasma sintering * Strength Subject RIV: JK - Corrosion ; Surface Treatment of Materials Impact factor: 2.647, year: 2015 http://dx.doi.org/10.1016/j.msea.2015.01.014

  5. Radiative heat transfer in plasma of pulsed high pressure caesium discharge

    Science.gov (United States)

    Lapshin, V. F.

    2016-01-01

    Two-temperature many component gas dynamic model is used for the analysis of features of radiative heat transfer in pulsed high pressure caesium discharge plasma. It is shown that at a sufficiently high pressure the radial optical thickness of arc column is close to unit (τR (λ) ∼ 1) in most part of spectrum. In this case radiative heat transfer has not local character. In these conditions the photons which are emitted in any point of plasma volume are absorbed in other point remote from an emission point on considerable distance. As a result, the most part of the electric energy put in the discharge mainly near its axis is almost instantly redistributed on all volume of discharge column. In such discharge radial profiles of temperature are smooth. In case of low pressure, when discharge plasma is optically transparent for own radiation in the most part of a spectrum (τR(λ) << 1), the emission of radiation without reabsorption takes place. Radiative heat transfer in plasma has local character and profiles of temperature have considerable gradient.

  6. Spectrum response and analysis of 77 GHz band collective Thomson scattering diagnostic for bulk and fast ions in LHD plasmas

    DEFF Research Database (Denmark)

    Nishiura, M.; Kubo, S.; Tanaka, K.

    2014-01-01

    A collective Thomson scattering (CTS) diagnostic was developed and used to measure the bulk and fast ions originating from 180 keV neutral beams in the Large Helical Device (LHD). Electromagnetic waves from a gyrotron at 77 GHz with 1 MW power output function as both the probe and electron......, a stray radiation component was observed in the CTS spectrum whereas it was negligibly small at low density. The CTS spectrum was measured and analysed after the in situ beam alignment using a beam scan. Qualitatively, the CTS spectrogram shows consistent response to ion temperatures of 1–2 ke......V for electron densities of (1–2) × 1019 m−3 and electron temperatures of 2–4 keV. The measured CTS spectrum shows an asymmetric shape at the foot of the bulk-ion region during the injection of 180 keV fast ions. This shape is explained by the fast-ion distribution in the velocity space (v‖, v⊥) based on Monte...

  7. High-pressure pyrolysis study of C sub 3 N sub 6 H sub 6 : a route to preparing bulk C sub 3 N sub 4

    CERN Document Server

    Ma, H A; Chen, L X; Zhu, P W; Guo, W L; Guo, X B; Wang, Y D; Li, S Q; Zou Guang Tian; Zhang, G; Bex, P

    2002-01-01

    In order to prepare bulk C sub 3 N sub 4 , high-pressure pyrolysis of melamine (C sub 3 N sub 6 H sub 6) at different temperatures was carried out. The products were characterized by C, N, H element analysis, Fourier transform infrared spectroscopy, x-ray photoelectron spectroscopy, and x-ray diffractometry. The results of the analysis reveal that graphitic phase C sub 3 N sub 4 has been synthesized. It provides a novel route to synthesis of the theoretical superhard cubic C sub 3 N sub 4 and other C sub 3 N sub 4 phases from organic compounds by a high-pressure and high-temperature method.

  8. Synthesis and Characterization of Nanofibrous Polyaniline Thin Film Prepared by Novel Atmospheric Pressure Plasma Polymerization Technique

    Directory of Open Access Journals (Sweden)

    Choon-Sang Park

    2016-01-01

    Full Text Available This work presents a study on the preparation of plasma-polymerized aniline (pPANI nanofibers and nanoparticles by an intense plasma cloud type atmospheric pressure plasma jets (iPC-APPJ device with a single bundle of three glass tubes. The nano size polymer was obtained at a sinusoidal wave with a peak value of 8 kV and a frequency of 26 kHz under ambient air. Discharge currents, photo-sensor amplifier, and optical emission spectrometer (OES techniques were used to analyze the plasma produced from the iPC-APPJ device. Field emission scanning electron microscopy (FE-SEM, transmission electron microscopy (TEM, Fourier transform infrared spectroscopy (FT-IR, gas chromatography-mass spectrometry (GC-MS, and gel permeation chromatography (GPC techniques were used to analyze the pPANI. FE-SEM and TEM results show that pPANI has nanofibers, nanoparticles morphology, and polycrystalline characteristics. The FT-IR and GC-MS analysis show the characteristic polyaniline peaks with evidence that some quinone and benzene rings are broken by the discharge energy. GPC results show that pPANI has high molecular weight (Mw, about 533 kDa with 1.9 polydispersity index (PDI. This study contributes to a better understanding on the novel growth process and synthesis of uniform polyaniline nanofibers and nanoparticles with high molecular weights using the simple atmospheric pressure plasma polymerization technique.

  9. Synthesis and Characterization of Nanofibrous Polyaniline Thin Film Prepared by Novel Atmospheric Pressure Plasma Polymerization Technique.

    Science.gov (United States)

    Park, Choon-Sang; Kim, Dong Ha; Shin, Bhum Jae; Tae, Heung-Sik

    2016-01-11

    This work presents a study on the preparation of plasma-polymerized aniline (pPANI) nanofibers and nanoparticles by an intense plasma cloud type atmospheric pressure plasma jets (iPC-APPJ) device with a single bundle of three glass tubes. The nano size polymer was obtained at a sinusoidal wave with a peak value of 8 kV and a frequency of 26 kHz under ambient air. Discharge currents, photo-sensor amplifier, and optical emission spectrometer (OES) techniques were used to analyze the plasma produced from the iPC-APPJ device. Field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FT-IR), gas chromatography-mass spectrometry (GC-MS), and gel permeation chromatography (GPC) techniques were used to analyze the pPANI. FE-SEM and TEM results show that pPANI has nanofibers, nanoparticles morphology, and polycrystalline characteristics. The FT-IR and GC-MS analysis show the characteristic polyaniline peaks with evidence that some quinone and benzene rings are broken by the discharge energy. GPC results show that pPANI has high molecular weight ( M w ), about 533 kDa with 1.9 polydispersity index (PDI). This study contributes to a better understanding on the novel growth process and synthesis of uniform polyaniline nanofibers and nanoparticles with high molecular weights using the simple atmospheric pressure plasma polymerization technique.

  10. Diffuse plasma treatment of polyamide 66 fabric in atmospheric pressure air

    Energy Technology Data Exchange (ETDEWEB)

    Li, Lee, E-mail: leeli@mail.hust.edu.cn; Peng, Ming-yang; Teng, Yun; Gao, Guozhen

    2016-01-30

    Graphical abstract: - Highlights: • A cylindrical-electrode nanosecond-pulse diffuse-discharge reactor is presented. • Large-scale non-thermal plasmas were generated steadily in atmospheric air. • Treated PA66 fabric is etched with oxygen-containing group increases. • The hydrophily of treated PA66 fabric improves effectively. • Extending the treatment time is a method to reduce the treatment frequency. - Abstract: The polyamide 66 (PA66) fabrics are hard to be colored or glued in industrial production due to the poor hydrophily. Diffuse plasma is a kind of non-thermal plasma generated at atmospheric pressure in air. This paper proposes that large-scale diffuse plasma generated between wire electrodes can be employed for improving the hydrophily of PA66 fabrics. A repetitive nanosecond-pulse diffuse-discharge reactor using a cylindrical wire electrode configuration is presented, which can generate large-scale non-thermal plasmas steadily at atmospheric pressure without any barrier dielectric. Then the reactor is used to treat PA66 fabrics in different discharge conditions. The hydrophilicity property of modified PA66 is measured by wicking test method. The modified PA66 is also analyzed by atomic force microscopy (AFM) and X-ray photoelectron spectroscopy (XPS) to prove the surface changes in physical microstructure and chemical functional groups, respectively. What's more, the effects of treatment time and treatment frequency on surface modification are investigated and discussed.

  11. Diffuse plasma treatment of polyamide 66 fabric in atmospheric pressure air

    International Nuclear Information System (INIS)

    Li, Lee; Peng, Ming-yang; Teng, Yun; Gao, Guozhen

    2016-01-01

    Graphical abstract: - Highlights: • A cylindrical-electrode nanosecond-pulse diffuse-discharge reactor is presented. • Large-scale non-thermal plasmas were generated steadily in atmospheric air. • Treated PA66 fabric is etched with oxygen-containing group increases. • The hydrophily of treated PA66 fabric improves effectively. • Extending the treatment time is a method to reduce the treatment frequency. - Abstract: The polyamide 66 (PA66) fabrics are hard to be colored or glued in industrial production due to the poor hydrophily. Diffuse plasma is a kind of non-thermal plasma generated at atmospheric pressure in air. This paper proposes that large-scale diffuse plasma generated between wire electrodes can be employed for improving the hydrophily of PA66 fabrics. A repetitive nanosecond-pulse diffuse-discharge reactor using a cylindrical wire electrode configuration is presented, which can generate large-scale non-thermal plasmas steadily at atmospheric pressure without any barrier dielectric. Then the reactor is used to treat PA66 fabrics in different discharge conditions. The hydrophilicity property of modified PA66 is measured by wicking test method. The modified PA66 is also analyzed by atomic force microscopy (AFM) and X-ray photoelectron spectroscopy (XPS) to prove the surface changes in physical microstructure and chemical functional groups, respectively. What's more, the effects of treatment time and treatment frequency on surface modification are investigated and discussed.

  12. Surface modification of polyester synthetic leather with tetramethylsilane by atmospheric pressure plasma

    International Nuclear Information System (INIS)

    Kan, C.W.; Kwong, C.H.; Ng, S.P.

    2015-01-01

    Highlights: • Atmospheric pressure plasma treatment improved surface performance of polyester synthetic leather with tetramethylsilane. • XPS and FTIR confirmed the deposition of organosilanes on the sample's surface. • Contact angle increases to 138° after plasma treatment. - Abstract: Much works have been done on synthetic materials but scarcely on synthetic leather owing to its surface structures in terms of porosity and roughness. This paper examines the use of atmospheric pressure plasma (APP) treatment for improving the surface performance of polyester synthetic leather by use of a precursor, tetramethylsilane (TMS). Plasma deposition is regarded as an effective, simple and single-step method with low pollution. Scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS) and Fourier transform infrared spectroscopy (FTIR) confirm the deposition of organosilanes on the sample's surface. The results showed that under a particular combination of treatment parameters, a hydrophobic surface was achieved on the APP treated sample with sessile drop static contact angle of 138°. The hydrophobic surface is stable without hydrophilic recovery 30 days after plasma treatment

  13. Decontamination of chemical and biological warfare (CBW) agents using an atmospheric pressure plasma jet (APPJ)

    International Nuclear Information System (INIS)

    Herrmann, H.W.; Henins, I.; Park, J.; Selwyn, G.S.

    1999-01-01

    The atmospheric pressure plasma jet (APPJ) [A. Schuetze et al., IEEE Trans. Plasma Sci. 26, 1685 (1998)] is a nonthermal, high pressure, uniform glow plasma discharge that produces a high velocity effluent stream of highly reactive chemical species. The discharge operates on a feedstock gas (e.g., He/O 2 /H 2 O), which flows between an outer, grounded, cylindrical electrode and an inner, coaxial electrode powered at 13.56 MHz rf. While passing through the plasma, the feedgas becomes excited, dissociated or ionized by electron impact. Once the gas exits the discharge volume, ions and electrons are rapidly lost by recombination, but the fast-flowing effluent still contains neutral metastable species (e.g., O 2 * , He * ) and radicals (e.g., O, OH). This reactive effluent has been shown to be an effective neutralizer of surrogates for anthrax spores and mustard blister agent. Unlike conventional wet decontamination methods, the plasma effluent does not cause corrosion and it does not destroy wiring, electronics, or most plastics, making it highly suitable for decontamination of sensitive equipment and interior spaces. Furthermore, the reactive species in the effluent rapidly degrade into harmless products leaving no lingering residue or harmful by-products. copyright 1999 American Institute of Physics

  14. Hydrophobic and superhydrophobic surfaces fabricated using atmospheric pressure cold plasma technology: A review.

    Science.gov (United States)

    Dimitrakellis, Panagiotis; Gogolides, Evangelos

    2018-03-29

    Hydrophobic surfaces are often used to reduce wetting of surfaces by water. In particular, superhydrophobic surfaces are highly desired for several applications due to their exceptional properties such as self-cleaning, anti-icing, anti-friction and others. Such surfaces can be prepared via numerous methods including plasma technology, a dry technique with low environmental impact. Atmospheric pressure plasma (APP) has recently attracted significant attention as lower-cost alternative to low-pressure plasmas, and as a candidate for continuous rather than batch processing. Although there are many reviews on water-repellent surfaces, and a few reviews on APP technology, there are hardly any review works on APP processing for hydrophobic and superhydrohobic surface fabrication, a topic of high importance in nanotechnology and interface science. Herein, we critically review the advances on hydrophobic and superhydrophobic surface fabrication using APP technology, trying also to give some perspectives in the field. After a short introduction to superhydrophobicity of nanostructured surfaces and to APPs we focus this review on three different aspects: (1) The atmospheric plasma reactor technology used for fabrication of (super)hydrophobic surfaces. (2) The APP process for hydrophobic surface preparation. The hydrophobic surface preparation processes are categorized methodologically as: a) activation, b) grafting, c) polymerization, d) roughening and hydrophobization. Each category includes subcategories related to different precursors used. (3) One of the most important sections of this review concerns superhydrophobic surfaces fabricated using APP. These are methodologically characterized as follows: a) single step processes where micro-nano textured topography and low surface energy coating are created at the same time, or b) multiple step processes, where these steps occur sequentially in or out of the plasma. We end the review with some perspectives in the field. We

  15. Atmospheric Pressure Plasma Jet as a Dry Alternative to Inkjet Printing in Flexible Electronics

    Science.gov (United States)

    Gandhiraman, Ram Prasad; Lopez, Arlene; Koehne, Jessica; Meyyappan, M.

    2016-01-01

    We have developed an atmospheric pressure plasma jet printing system that works at room temperature to 50 deg C unlike conventional aerosol assisted techniques which require a high temperature sintering step to obtain desired thin films. Multiple jets can be configured to increase throughput or to deposit multiple materials, and the jet(s) can be moved across large areas using a x-y stage. The plasma jet has been used to deposit carbon nanotubes, graphene, silver nanowires, copper nanoparticles and other materials on substrates such as paper, cotton, plastic and thin metal foils.

  16. Highly ionized physical vapor deposition plasma source working at very low pressure

    Czech Academy of Sciences Publication Activity Database

    Straňák, V.; Herrendorf, A.-P.; Drache, S.; Čada, Martin; Hubička, Zdeněk; Tichý, M.; Hippler, R.

    2012-01-01

    Roč. 100, č. 14 (2012), "141604-1"-"141604-3" ISSN 0003-6951 R&D Projects: GA TA ČR TA01010517; GA ČR(CZ) GAP205/11/0386; GA ČR GAP108/12/1941 Institutional research plan: CEZ:AV0Z10100522 Keywords : magnetron * ECWR * low-pressure * sputtering * plasma diagnostics Subject RIV: BL - Plasma and Gas Discharge Physics Impact factor: 3.794, year: 2012 http://dx.doi.org/10.1063/1.3699229

  17. Elevated Plasma Endothelin-1 and Pulmonary Arterial Pressure in Children Exposed to Air Pollution

    Science.gov (United States)

    Calderón-Garcidueñas, Lilian; Vincent, Renaud; Mora-Tiscareño, Antonieta; Franco-Lira, Maricela; Henríquez-Roldán, Carlos; Barragán-Mejía, Gerardo; Garrido-García, Luis; Camacho-Reyes, Laura; Valencia-Salazar, Gildardo; Paredes, Rogelio; Romero, Lina; Osnaya, Hector; Villarreal-Calderón, Rafael; Torres-Jardón, Ricardo; Hazucha, Milan J.; Reed, William

    2007-01-01

    Background Controlled exposures of animals and humans to particulate matter (PM) or ozone air pollution cause an increase in plasma levels of endothelin-1, a potent vasoconstrictor that regulates pulmonary arterial pressure. Objectives The primary objective of this field study was to determine whether Mexico City children, who are chronically exposed to levels of PM and O3 that exceed the United States air quality standards, have elevated plasma endothelin-1 levels and pulmonary arterial pressures. Methods We conducted a study of 81 children, 7.9 ± 1.3 years of age, lifelong residents of either northeast (n = 19) or southwest (n = 40) Mexico City or Polotitlán (n = 22), a control city with PM and O3 levels below the U.S. air quality standards. Clinical histories, physical examinations, and complete blood counts were done. Plasma endothelin-1 concentrations were determined by immunoassay, and pulmonary arterial pressures were measured by Doppler echocardiography. Results Mexico City children had higher plasma endothelin-1 concentrations compared with controls (p < 0.001). Mean pulmonary arterial pressure was elevated in children from both northeast (p < 0.001) and southwest (p < 0.05) Mexico City compared with controls. Endothelin-1 levels in Mexico City children were positively correlated with daily outdoor hours (p = 0.012), and 7-day cumulative levels of PM air pollution < 2.5 μm in aerodynamic diameter (PM2.5) before endothelin-1 measurement (p = 0.03). Conclusions Chronic exposure of children to PM2.5 is associated with increased levels of circulating endothelin-1 and elevated mean pulmonary arterial pressure. PMID:17687455

  18. Effect of shock pressure on the structure and superconducting properties of Y-Ba-Cu-O in explosively fabricated bulk metal-matrix composites

    Science.gov (United States)

    Murr, L. E.; Niou, C. S.; Pradhan-Advani, M.

    1991-01-01

    While it is now well established that copper-oxide-based power, or virtually any other ceramic superconductor powder, can be consolidated and encapsulated within a metal matrix by explosive consolidation, the erratic superconductivity following fabrication has posed a major problem for bulk applications. The nature of this behavior was found to arise from microstructural damage created in the shock wave front, and the residual degradation in superconductivity was demonstrated to be directly related to the peak shock pressure. The explosively fabricated or shock loaded YBa2Cu3Ox examples exhibit drastically altered rho (or R) - T curves. The deterioration in superconductivity is even more noticeable in the measurement of ac magnetic susceptibility and flux exclusion or shielding fraction which is also reduced in proportion to increasing peak shock pressure. The high frequency surface resistance (in the GHz range) is also correspondingly compromised in explosively fabricated, bulk metal-matrix composites based on YBa2Cu3O7. Transmission electron microscopy (including lattice imaging techniques) is being applied in an effort to elucidate the fundamental (microstructural) nature of the shock-induced degradation of superconductivity and normal state conductivity. One focus of TEM observations has assumed that oxygen displaced from b-chains rather than oxygen-vacancy disorder in the basal plane of oxygen deficient YBa2Cu3Ox may be a prime mechanism. Shock-wave displaced oxygen may also be locked into new positions or interstitial clusters or chemically bound to displaced metal (possibly copper) atoms to form precipitates, or such displacements may cause the equivalent of local lattice cell changes as a result of stoichiometric changes. While the shock-induced suppression of T(sub c) is not desirable in the explosive fabrication of bulk metal-matrix superconductors, it may be turned into an advantage if the atomic-scale distortion can be understood and controlled as local

  19. Surface modification of polyimide (PI) film using water cathode atmospheric pressure glow discharge plasma

    International Nuclear Information System (INIS)

    Zheng Peichao; Liu Keming; Wang Jinmei; Dai Yu; Yu Bin; Zhou Xianju; Hao Honggang; Luo Yuan

    2012-01-01

    Highlights: ► Equipment called water cathode atmospheric pressure glow discharge was used to improve the hydrophilicity of polyimide films. ► The data shows good homogeneity and the variation trends of contact angles are different for polar and non-polar testing liquids. ► The thickness of liquid layer plays an important role in plasma processing and directly affects the treatment effect. ► Surface hydrophilicity after plasma treatment is improved partly due to the increase in the roughness. ► The hydrophilicity of polyimide films is still better than untreated ones after long-term storage. - Abstract: The industrial use of polyimide film is limited because of undesirable properties such as poor wettability. In the present paper, a new kind of equipment called water cathode atmospheric pressure glow discharge was used to improve the surface properties of polyimide films and made them useful to technical applications. The changes in hydrophilicity of modified polyimide film surfaces were investigated by contact angle, surface energy and water content measurements as a function of treatment time. The results obtained show good treatment homogeneity and that the variation trends of contact angles are different for polar and non-polar testing liquids, while surface energy and water content are significantly enhanced with the increase of treatment time until they achieve saturated values after 60 s plasma treatment. Also, the thickness of liquid layer plays an important role in plasma processing and directly affects the treatment effect. Changes in morphology of polyimide films were analyzed by atomic force microscope and the results indicate that surface hydrophilicity after plasma treatment are improved partly due to the increase in the roughness. In addition, polyimide films treated by plasma are subjected to an ageing process to determine the durability of plasma treatment. It is found that the hydrophilicity is still better than untreated ones though the

  20. Comparison of the characteristics of atmospheric pressure plasma jets using different working gases and applications to plasma-cancer cell interactions

    Directory of Open Access Journals (Sweden)

    Hea Min Joh

    2013-09-01

    Full Text Available Atmospheric pressure plasma jets employing nitrogen, helium, or argon gases driven by low-frequency (several tens of kilohertz ac voltage and pulsed dc voltage were fabricated and characterized. The changes in discharge current, optical emission intensities from reactive radicals, gas temperature, and plume length of plasma jets with the control parameters were measured and compared. The control parameters include applied voltage, working gas, and gas flow rate. As an application to plasma-cancer cell interactions, the effects of atmospheric pressure plasma jet on the morphology and intracellular reactive oxygen species (ROS level of human lung adenocarcinoma cell (A549 and human bladder cancer cell (EJ were explored. The experimental results show that the plasma can effectively control the intracellular concentrations of ROS. Although there exist slight differences in the production of ROS, helium, argon, or nitrogen plasma jets are found to be useful in enhancing the intracellular ROS concentrations in cancer cells.

  1. Effect of porosity on thermal and electrical properties of polycrystalline bulk ZrN prepared by spark plasma sintering

    International Nuclear Information System (INIS)

    Adachi, Jun; Kurosaki, Ken; Uno, Masayoshi; Yamanaka, Shinsuke

    2007-01-01

    Two kinds of polycrystalline zirconium nitride (ZrN) pellets were prepared by a spark plasma sintering (SPS). Thermal and electrical properties were measured from room temperature to 1473 and 1000 K, respectively. Thermal expansion is almost independent of porosity. On the other hand, electrical and thermal conductivities systematically decreased with increasing porosity. Porosity dependences of electrical and thermal conductivities are studied through the Maxwell-Eucken's equation

  2. Influence of air pressure on the performance of plasma synthetic jet actuator

    International Nuclear Information System (INIS)

    Li Yang; Jia Min; Li Ying-hong; Song Hui-min; Liang Hua; Wu Yun; Zong Hao-hua

    2016-01-01

    Plasma synthetic jet actuator (PSJA) has a wide application prospect in the high-speed flow control field for its high jet velocity. In this paper, the influence of the air pressure on the performance of a two-electrode PSJA is investigated by the schlieren method in a large range from 7 kPa to 100 kPa. The energy consumed by the PSJA is roughly the same for all the pressure levels. Traces of the precursor shock wave velocity and the jet front velocity vary a lot for different pressures. The precursor shock wave velocity first decreases gradually and then remains at 345 m/s as the air pressure increases. The peak jet front velocity always appears at the first appearance of a jet, and it decreases gradually with the increase of the air pressure. A maximum precursor shock wave velocity of 520 m/s and a maximum jet front velocity of 440 m/s are observed at the pressure of 7 kPa. The averaged jet velocity in one period ranges from 44 m/s to 54 m/s for all air pressures, and it drops with the rising of the air pressure. High velocities of the precursor shock wave and the jet front indicate that this type of PSJA can still be used to influence the high-speed flow field at 7 kPa. (paper)

  3. Surface treatment of a titanium implant using low temperature atmospheric pressure plasmas

    Science.gov (United States)

    Lee, Hyun-Young; Tang, Tianyu; Ok, Jung-Woo; Kim, Dong-Hyun; Lee, Ho-Jun; Lee, Hae June

    2015-09-01

    During the last two decades, atmospheric pressure plasmas(APP) are widely used in diverse fields of biomedical applications, reduction of pollutants, and surface treatment of materials. Applications of APP to titanium surface of dental implants is steadily increasing as it renders surfaces wettability and modifies the oxide layer of titanium that hinders the interaction with cells and proteins. In this study, we have treated the titanium surfaces of screw-shaped implant samples using a plasma jet which is composed of a ceramic coaxial tube of dielectrics, a stainless steel inner electrode, and a coper tube outer electrode. The plasma ignition occurred with Ar gas flow between two coaxial metal electrodes and a sinusoidal bias voltage of 3 kV with a frequency of 20 kHz. Titanium materials used in this study are screw-shaped implants of which diameter and length are 5 mm and 13 mm, respectively. Samples were mounted at a distance of 5 mm below the plasma source, and the plasma treatment time was set to 3 min. The wettability of titanium surface was measured by the moving speed of water on its surface, which is enhanced by plasma treatment. The surface roughness was also measured by atomic force microscopy. The optimal condition for wettability change is discussed.

  4. Multi-electrodes Atmospheric Pressure Plasma Jet Aiming Bio-applications

    Science.gov (United States)

    Han, Jeon G.; Sahu, B. B.; Shin, K. S.; Lee, J. S.; Hori, M.

    2015-09-01

    For the recent advancement in the field of plasma medicine, there is growing demand for the atmospheric-pressure plasma (APP) jet sources with desired plasma characteristics. In this study, a stable non-thermal low-voltage APP jet device was designed and developed for optical and electrical characterizations. The jet was operated at very low frequency in the range 10-40 KHz, which enabled the generation of low power (~ 7W) plasma with a plasma column diameter of about 5 mm. The jet has a visible radial diameter of approximately 10 mm. Optical emission spectroscopy was used as a diagnostic tool to investigate the generation of plasmas and radical species. Discharge parameters are also measured to evaluate the different operating conditions. The gas temperature measured at the substrate location varies from 300 to 315 K for different gases where the electrical input power ranged from 1 to 7 W. The highly reactive species like OH, O, N2, N2 + and along with the trace of NO are characterized with respect to the different gas flow rate of Ar/He/O2/N2, applied voltages, duty cycles and frequencies to evaluate the capability of the APP jet for future bio-applications.

  5. Reduction in lateral lipid mobility of lipid bilayer membrane by atmospheric pressure plasma irradiation

    Science.gov (United States)

    Suda, Yoshiyuki; Tero, Ryugo; Yamashita, Ryuma; Yusa, Kota; Takikawa, Hirofumi

    2016-03-01

    Plasma medicine is an emerging research field in which various applications of electrical discharge, especially in the form of nonequilibrium plasma at atmospheric pressure, are examined, for example, the application of plasma to biological targets for various purposes such as selective killing of tumor cells and blood stanching. We have focused on the behavior of an artificial cell membrane system at the solid-liquid interface. To evaluate the lateral lipid mobility, we measured the diffusion coefficient of the supported lipid bilayer (SLB) composed of dioleoylphosphatidylcholine with fluorescence recovery after photobleaching by confocal laser scanning microscopy. It was found that the diffusion coefficient was decreased by plasma irradiation and that the diffusion coefficient decreasing rate proceeded with increasing plasma power. We investigated the effects of stimulation with an equilibrium chemical, H2O2, on the SLB and confirmed that the diffusion coefficient did not change at least up to a H2O2 concentration of 5 mM. These results indicate that transient active species generated by plasma play critical roles in the reduction in SLB fluidity. The effects of the two generated major oxidized lipid species, hydroxyl- or hydroperoxy-phosphatidylcholine (PC) and acyl-chain-truncated PCs terminated with aldehyde or carboxyl group, on lateral lipid mobility are discussed.

  6. Dust ion acoustic solitary waves in a magnetized dusty plasma with anisotropic ion pressure

    International Nuclear Information System (INIS)

    Choi, Cheong Rim; Ryu, Chang-Mo; Lee, D.-Y.; Lee, Nam C.; Kim, Y.-H.

    2007-01-01

    The influence of anisotropic ion pressure on the dust ion acoustic solitary wave (DIASW) and the double layer (DL) obliquely propagating to a magnetic field are investigated by using the Sagdeev potential. The anisotropic ion pressure is defined by applying the Chew-Goldberger-Low (CGL) theory, p-perpendicular=p-perpendicular 0 n and p-parallel=p-parallel 0 n 3 , where n is the normalized ion density. The solutions of DIASWs and DLs obliquely propagating to an external magnetic field are obtained in the small amplitude limit. It is found that the perpendicular component of anisotropic ion pressure works differently from that of the parallel component on the DIASWs in a magnetized dusty plasma, deviating from a straight extension of the isotropic pressure effect

  7. Nonlinear dynamics of collapse phenomena in heliotron plasma with large pressure gradient

    International Nuclear Information System (INIS)

    Mizuguchi, N.; Suzuki, Y.; Ohyabu, N.

    2008-10-01

    We have executed nonlinear magnetohydrodynamic (MHD) simulations in a heliotron-type configuration with a large pressure gradient to reveal the nonlinear dynamics of collapse phenomena. The simulation results reproduce the qualitative characteristics of the experimental observation on the so-called core density collapse (CDC) events in the Large Helical Device (LHD) plasma with the super dense core (SDC) profile. A long-term nonlinear behavior on the event, including the flushing mechanism of the core pressure, is clarified. The simulation result shows the linear growth of the ballooning-like resistive instability modes with the intermediate poloidal wavenumbers. The growth of the modes are saturated soon, and the system experiences the energy relaxation in about 1 msec. It should be noted that the linear mode structures are localized in the edge region, whereas the core pressure rapidly falls as the system reaches the relaxed state. The co-existence of the edge perturbation and the core collapse is consistent with the experimental observations. The lost pressure forms a wider tail in the peripheral region. The core pressure is remarkably reduced at a certain period, while it had withstood the disturbance before it. The most salient feature on this period is the disordering of the magnetic field structure. The system keeps the nested-flux-surface structure well in the beginnings, whereas part of them are abruptly lost at this period. Such a situation can induce a flattening of the pressure profile along the reconnected field lines. By checking the place where the plasma loss due to this mechanism occurs, such plasma outlets are found to be located mainly on the disordered region. Thus, one can conclude that the core collapse can be caused by the disturbance of the magnetic field. (author)

  8. Variability of hydrostatic hepatic vein and ascitic fluid pressure, and of plasma and ascitic fluid colloid osmotic pressure in patients with liver cirrhosis

    DEFF Research Database (Denmark)

    Henriksen, Jens Henrik Sahl

    1980-01-01

    The variability of hydrostatic hepatic vein and ascitic fluid pressures and of plasma and ascitic fluid colloid osmotic (oncotic) pressures was assessed during hepatic venous catheterization by repeated measurements on different days and at different locations in patients with cirrhosis...... of the liver. Furthermore, calculation of oncotic pressure from protein determinations was compared to the directly measured value of plasma and ascitic fluid samples. Repeated measurements of hydrostatic pressure in the same hepatic vein within 15 min showed a standard deviation (SD) below 1 mm......Hg. The variation in hydrostatic hepatic vein pressures, pressure differences and ascitic fluid pressures (when measured at different locations within the liver and peritoneal space during a single examination) was 1.5, 1.0 and 1.0 mmHg (SD), respectively. When measured on different days, the variation...

  9. A Brief Study on the Ignition of the Non-Thermal Atmospheric Pressure Plasma Jet from a Double Dielectric Barrier Configured Plasma Pencil

    International Nuclear Information System (INIS)

    Begum, Asma; Laroussi, Mounir; Pervez, M. R.

    2013-01-01

    To understand the self sustained propagation of the plasma jet/bullet in air under atmospheric pressure, the ignition of the plasma jet/bullet, the plasma jet/bullet ignition point in the plasma pencil, the formation time and the formation criteria from a dielectric barrier configured plasma pencil were investigated in this study. The results were confirmed by comparing these results with the plasma jet ignition process in the plasma pencil without a dielectric barrier. Electrical, optical, and imaging techniques were used to study the formation of the plasma jet from the ignition of discharge in a double dielectric barrier configured plasma pencil. The investigation results show that the plasma jet forms at the outlet of the plasma pencil as a donut shaped discharge front because of the electric field line along the outlet's surface. It is shown that the required time for the formation of the plasma jet changes with the input voltage of the discharge. The input power calculation for the gap discharge and for the whole system shows that 56% of the average input power is used by the first gap discharge. The estimated electron density inside the gap discharge is in the order of 10 11 cm −3 . If helium is used as a feeding gas, a minimum 1.48×10 −8 C charge is required per pulse in the gap discharge to generate a plasma jet

  10. Mechanism for heating of nitrogen plasmas in an electrodeless rf capacitive discharge at medium pressures

    International Nuclear Information System (INIS)

    Berdichevskii, M.G.; Marusin, V.V.

    1979-01-01

    The possible contributions of several processes to the experimentally observed heating of nitrogen plasmas in an electarodeless rf capacitive discharge at pressures of p=2.7-67 kPa are discussed. These processes are electron-rotational, vibrational--translational (V--T), and nonresonance vibrational--vibrational (V--V) energy exchange and effects due to O 2 , H 2 O, and NO impurities in the gas. It is shown that as the pressure is decreased the heating mechanism changes from quasiequilibrium to nonequilibrium V--T heating caused by overpopulation of high vibrational levels in the ground state of the nitrogen molecule

  11. Effects of imipramine of the orthostatic changes in blood pressure, heart rate and plasma catecholamines

    DEFF Research Database (Denmark)

    Nielsen, J R; Johansen, Torben; Arentoft, A

    1983-01-01

    The effect of imipramine on the orthostatic changes in heart rate, blood pressure and plasma catecholamines were examined in six healthy male subjects on two occasions on high sodium balance (Na+ excretion greater than 120 mmol per day) and on low sodium balance (Na+ excretion less than 110 mmol...... per day), respectively. Orthostatic tests were carried out before and 2 h after ingestion of 150 mg imipramine hydrochloride. Imipramine caused a moderate increase in supine systolic blood pressure, and a pronounced increase in the rise in heart rate, when the subjects assumed erect position...

  12. Gas Diffusion Barriers Prepared by Spatial Atmospheric Pressure Plasma Enhanced ALD.

    Science.gov (United States)

    Hoffmann, Lukas; Theirich, Detlef; Pack, Sven; Kocak, Firat; Schlamm, Daniel; Hasselmann, Tim; Fahl, Henry; Räupke, André; Gargouri, Hassan; Riedl, Thomas

    2017-02-01

    In this work, we report on aluminum oxide (Al 2 O 3 ) gas permeation barriers prepared by spatial ALD (SALD) at atmospheric pressure. We compare the growth characteristics and layer properties using trimethylaluminum (TMA) in combination with an Ar/O 2 remote atmospheric pressure plasma for different substrate velocities and different temperatures. The resulting Al 2 O 3 films show ultralow water vapor transmission rates (WVTR) on the order of 10 -6 gm -2 d -1 . In notable contrast, plasma based layers already show good barrier properties at low deposition temperatures (75 °C), while water based processes require a growth temperature above 100 °C to achieve equally low WVTRs. The activation energy for the water permeation mechanism was determined to be 62 kJ/mol.

  13. Mycotoxin Decontamination of Food: Cold Atmospheric Pressure Plasma versus "Classic" Decontamination.

    Science.gov (United States)

    Hojnik, Nataša; Cvelbar, Uroš; Tavčar-Kalcher, Gabrijela; Walsh, James L; Križaj, Igor

    2017-04-28

    Mycotoxins are secondary metabolites produced by several filamentous fungi, which frequently contaminate our food, and can result in human diseases affecting vital systems such as the nervous and immune systems. They can also trigger various forms of cancer. Intensive food production is contributing to incorrect handling, transport and storage of the food, resulting in increased levels of mycotoxin contamination. Mycotoxins are structurally very diverse molecules necessitating versatile food decontamination approaches, which are grouped into physical, chemical and biological techniques. In this review, a new and promising approach involving the use of cold atmospheric pressure plasma is considered, which may overcome multiple weaknesses associated with the classical methods. In addition to its mycotoxin destruction efficiency, cold atmospheric pressure plasma is cost effective, ecologically neutral and has a negligible effect on the quality of food products following treatment in comparison to classical methods.

  14. Mycotoxin Decontamination of Food: Cold Atmospheric Pressure Plasma versus “Classic” Decontamination

    Science.gov (United States)

    Hojnik, Nataša; Cvelbar, Uroš; Tavčar-Kalcher, Gabrijela; Walsh, James L.; Križaj, Igor

    2017-01-01

    Mycotoxins are secondary metabolites produced by several filamentous fungi, which frequently contaminate our food, and can result in human diseases affecting vital systems such as the nervous and immune systems. They can also trigger various forms of cancer. Intensive food production is contributing to incorrect handling, transport and storage of the food, resulting in increased levels of mycotoxin contamination. Mycotoxins are structurally very diverse molecules necessitating versatile food decontamination approaches, which are grouped into physical, chemical and biological techniques. In this review, a new and promising approach involving the use of cold atmospheric pressure plasma is considered, which may overcome multiple weaknesses associated with the classical methods. In addition to its mycotoxin destruction efficiency, cold atmospheric pressure plasma is cost effective, ecologically neutral and has a negligible effect on the quality of food products following treatment in comparison to classical methods. PMID:28452957

  15. Decontamination of a rotating cutting tool during operation by means of atmospheric pressure plasmas

    DEFF Research Database (Denmark)

    Leipold, Frank; Kusano, Yukihiro; Hansen, F.

    2010-01-01

    The decontamination of a rotating cutting tool used for slicing in the meat industry by means of atmospheric pressure plasmas is investigated. The target is Listeria monocytogenes, a bacterium which causes listeriosis and can be found in plants and food. The non-pathogenic species, Listeria innocua......, is used for the experiments. A rotating knife was inoculated with L. innocua. The surface of the rotating knife was partly exposed to an atmospheric pressure dielectric barrier discharge operated in air, where the knife itself served as a ground electrode. The rotation of the knife ensures a treatment...... of the whole cutting tool. A log 5 reduction of L. innocua is obtained after 340 s of plasma operation. The temperature of the knife after treatment was found to be below 30 °C. The design of the setup allows a decontamination during slicing operation....

  16. Ultrasound enhanced 50 Hz plasma treatment of glass-fiber-reinforced polyester at atmospheric pressure

    DEFF Research Database (Denmark)

    Kusano, Yukihiro; Norrman, Kion; Singh, Shailendra Vikram

    2013-01-01

    approximately from 20 up to 80 mJm2 with ultrasonic irradiation. The plasma treatment with ultrasonic irradiation also introduced oxygen- and nitrogen-containing functional groups at the GFRP surface. These changes would improve the adhesion properties of the GFRP plates....... of around 30 kHz with the sound pressure level of approximately 155 dB were introduced vertically to the GFRP surface through a cylindrical waveguide. The polar component of the surface energy was almost unchanged after the plasma treatment without ultrasonic irradiation, but drastically increased......Glass-fiber-reinforced polyester (GFRP) plates are treated using a 50Hz dielectric barrier discharge at a peak-to-peak voltage of 30 kV in helium at atmospheric pressure with and without ultrasonic irradiation to study adhesion improvement. The ultrasonic waves at the fundamental frequency...

  17. Prediction of Pressure and Temperature Gradients in the Tokamak Plasma Edge

    Science.gov (United States)

    Stacey, W. M.

    2017-10-01

    An extended plasma fluid theory that takes into account kinetic ion orbit loss and electromagnetic forces in the continuity, momentum and energy balances, as well as atomic physics and radiation, has been used to reveal the explicit dependence of the temperature and pressure gradients in the tokamak edge plasma on these various factors. Combining the ion radial momentum balance and the Ohm's Law expression for Er reveals the dependence of the radial ion pressure gradient on VxB forces driven by radial particle fluxes, which depend on ion orbit loss, and other factors. The strong temperature gradients measured in the H-mode edge pedestal could certainly be associated with radiative and atomic physics edge cooling effects and the strong reduction in ion and energy fluxes due to ion orbit loss, as well as to the possible reductions in thermal diffusivities that is usually assumed to be the cause. Work supported by USDOE under DE-FC02-04ER54698.

  18. Heterogenization of Ketone Catalyst for Epoxidation by Low Pressure Plasma Fluorination of Silica Gel Supports.

    Science.gov (United States)

    D'Accolti, Lucia; De Vietro, Nicoletta; Fanelli, Fiorenza; Fusco, Caterina; Nacci, Angelo; Fracassi, Francesco

    2017-11-30

    Low pressure plasma was used for preparing heterogeneous organocatalysts 2 -( A )-( C ) suitable for dioxirane-mediated epoxidations. Heterogenization was accomplished by adsorption of the methyl perfluoroheptyl ketone ( 2 ) on fluorinated supports ( A )-( C ) deriving from the treatment of commercial C₈-silica gel in low pressure plasma fed with fluorocarbons. Catalyst 2 -( C ) proved to be the most efficient one, promoting epoxidation of an array of alkenes, including unsaturated fatty esters like methyl oleate ( 10 ) and the triglyceride soybean oil ( 11 ), with the cheap potassium peroxymonosulfate KHSO₅ (caroate) as a green oxidant. Notably, the perfluorinated matrix gives rise to the activation of caroate, generating singlet oxygen. Materials were characterized by infrared Attenuated Total Reflectance spectroscopy (ATR-FTIR), X-ray Photoelectron Spectroscopy (XPS ) and Emission Scanning Electron Microscope (FESEM).

  19. Atmospheric-pressure plasma jet characterization and applications on melanoma cancer treatment (B/16-F10)

    Science.gov (United States)

    Mashayekh, Shahriar; Rajaee, Hajar; Akhlaghi, Morteza; Shokri, Babak; Hassan, Zuhir M.

    2015-09-01

    A new approach in medicine is the use of cold plasma for various applications such as sterilization blood coagulation and cancer cell treatment. In this paper, a pin-to-hole plasma jet for biological applications has been designed and manufactured and characterized. The characterization includes power consumption via Lissajous method, thermal behavior of atmospheric-pressure plasma jet by using Infra-red camera as a novel method and using Speicair software to determine vibrational and transitional temperatures, and optical emission spectroscopy to determine the generated species. Treatment of Melanoma cancer cells (B16/F10) was also implemented, and tetrazolium salt dye (MTT assay) and flow cytometry were used to evaluate viability. Effect of ultraviolet photons on cancerous cells was also observed using an MgF2 crystal with MTT assay. Finally, in-vivo studies on C57 type mice were also done in order to have a better understanding of the effects in real conditions.

  20. Atmospheric-pressure plasma jet characterization and applications on melanoma cancer treatment (B/16-F10)

    Energy Technology Data Exchange (ETDEWEB)

    Mashayekh, Shahriar [Physics Department, Shahid Beheshti University, G.C., Evin, 19839-63113 Tehran, Islamic Republic of Iran (Iran, Islamic Republic of); Rajaee, Hajar; Hassan, Zuhir M. [Imonology Department, Faculty of Medical Science, Tarbiat Modarres University, Tehran (Iran, Islamic Republic of); Akhlaghi, Morteza [Laser-Plasma Research Institute, Shahid Beheshti University, G.C., Evin, 19839-63113 Tehran, Islamic Republic of Iran (Iran, Islamic Republic of); Shokri, Babak [Physics Department and Laser-Plasma Research Institute, Shahid Beheshti University, G.C., Evin, 19839-63113 Tehran, Islamic Republic of Iran (Iran, Islamic Republic of)

    2015-09-15

    A new approach in medicine is the use of cold plasma for various applications such as sterilization blood coagulation and cancer cell treatment. In this paper, a pin-to-hole plasma jet for biological applications has been designed and manufactured and characterized. The characterization includes power consumption via Lissajous method, thermal behavior of atmospheric-pressure plasma jet by using Infra-red camera as a novel method and using Speicair software to determine vibrational and transitional temperatures, and optical emission spectroscopy to determine the generated species. Treatment of Melanoma cancer cells (B16/F10) was also implemented, and tetrazolium salt dye (MTT assay) and flow cytometry were used to evaluate viability. Effect of ultraviolet photons on cancerous cells was also observed using an MgF{sub 2} crystal with MTT assay. Finally, in-vivo studies on C57 type mice were also done in order to have a better understanding of the effects in real conditions.

  1. Low pressure plasma discharges for the sterilization and decontamination of surfaces

    International Nuclear Information System (INIS)

    Rossi, F; Rauscher, H; Hasiwa, M; Gilliland, D; Kylian, O

    2009-01-01

    The mechanisms of sterilization and decontamination of surfaces are compared in direct and post discharge plasma treatments in two low-pressure reactors, microwave and inductively coupled plasma. It is shown that the removal of various biomolecules, such as proteins, pyrogens or peptides, can be obtained at high rates and low temperatures in the inductively coupled plasma (ICP) by using Ar/O 2 mixtures. Similar efficiency is obtained for bacterial spores. Analysis of the discharge conditions illustrates the role of ion bombardment associated with O radicals, leading to a fast etching of organic matter. By contrast, the conditions obtained in the post discharge lead to much lower etching rates but also to a chemical modification of pyrogens, leading to their de-activation. The advantages of the two processes are discussed for the application to the practical case of decontamination of medical devices and reduction of hospital infections, illustrating the advantages and drawbacks of the two approaches.

  2. Low pressure plasma discharges for the sterilization and decontamination of surfaces

    Energy Technology Data Exchange (ETDEWEB)

    Rossi, F; Rauscher, H; Hasiwa, M; Gilliland, D [European Commission, Joint Research Centre, Institute for Health and Consumer Protection, Via E. Fermi 2749, 21027 Ispra (Vatican City State, Holy See) (Italy); Kylian, O [Faculty of Mathematics and Physics, Charles University, V Holesovickach 2, Prague 8, 180 00 (Czech Republic)], E-mail: francois.rossi@jrc.ec.europa.eu

    2009-11-15

    The mechanisms of sterilization and decontamination of surfaces are compared in direct and post discharge plasma treatments in two low-pressure reactors, microwave and inductively coupled plasma. It is shown that the removal of various biomolecules, such as proteins, pyrogens or peptides, can be obtained at high rates and low temperatures in the inductively coupled plasma (ICP) by using Ar/O{sub 2} mixtures. Similar efficiency is obtained for bacterial spores. Analysis of the discharge conditions illustrates the role of ion bombardment associated with O radicals, leading to a fast etching of organic matter. By contrast, the conditions obtained in the post discharge lead to much lower etching rates but also to a chemical modification of pyrogens, leading to their de-activation. The advantages of the two processes are discussed for the application to the practical case of decontamination of medical devices and reduction of hospital infections, illustrating the advantages and drawbacks of the two approaches.

  3. Apparatus and method for atmospheric pressure reactive atom plasma processing for shaping of damage free surfaces

    Science.gov (United States)

    Carr,; Jeffrey, W [Livermore, CA

    2009-03-31

    Fabrication apparatus and methods are disclosed for shaping and finishing difficult materials with no subsurface damage. The apparatus and methods use an atmospheric pressure mixed gas plasma discharge as a sub-aperture polisher of, for example, fused silica and single crystal silicon, silicon carbide and other materials. In one example, workpiece material is removed at the atomic level through reaction with fluorine atoms. In this example, these reactive species are produced by a noble gas plasma from trace constituent fluorocarbons or other fluorine containing gases added to the host argon matrix. The products of the reaction are gas phase compounds that flow from the surface of the workpiece, exposing fresh material to the etchant without condensation and redeposition on the newly created surface. The discharge provides a stable and predictable distribution of reactive species permitting the generation of a predetermined surface by translating the plasma across the workpiece along a calculated path.

  4. Synthesis and characterization of carbon coated nanoparticles produced by a continuous low-pressure plasma process

    Energy Technology Data Exchange (ETDEWEB)

    Panchal, Vineet; Neergat, Manoj [Indian Institute of Technology Bombay, Department of Energy Science and Engineering (India); Bhandarkar, Upendra, E-mail: bhandarkar@iitb.ac.in [Indian Institute of Technology Bombay, Department of Mechanical Engineering (India)

    2011-09-15

    Core-shell nanoparticles coated with carbon have been synthesized in a single chamber using a continuous and entirely low-pressure plasma-based process. Nanoparticles are formed in an argon plasma using iron pentacarbonyl Fe(CO){sub 5} as a precursor. These particles are trapped in a pure argon plasma by shutting off the precursor and then coated with carbon by passing acetylene along with argon as the main background gas. Characterization of the particles was carried out using TEM for morphology, XPS for elemental composition and PPMS for magnetic properties. Iron nanoparticles obtained were a mixture of FeO and Fe{sub 3}O{sub 4}. TEM analysis shows an average size of 7-14 nm for uncoated particles and 15-24 nm for coated particles. The effect of the carbon coating on magnetic properties of the nanoparticles is studied in detail.

  5. Feasibility, strategy, methodology, and analysis of probe measurements in plasma under high gas pressure

    Science.gov (United States)

    Demidov, V. I.; Koepke, M. E.; Kurlyandskaya, I. P.; Malkov, M. A.

    2018-02-01

    This paper reviews existing theories for interpreting probe measurements of electron distribution functions (EDF) at high gas pressure when collisions of electrons with atoms and/or molecules near the probe are pervasive. An explanation of whether or not the measurements are realizable and reliable, an enumeration of the most common sources of measurement error, and an outline of proper probe-experiment design elements that inherently limit or avoid error is presented. Additionally, we describe recent expanded plasma-condition compatibility for EDF measurement, including in applications of large wall probe plasma diagnostics. This summary of the authors’ experiences gained over decades of practicing and developing probe diagnostics is intended to inform, guide, suggest, and detail the advantages and disadvantages of probe application in plasma research.

  6. "Virtual IED sensor" at an rf-biased electrode in low-pressure plasma

    Science.gov (United States)

    Bogdanova, M. A.; Lopaev, D. V.; Zyryanov, S. M.; Rakhimov, A. T.

    2016-07-01

    Energy distribution and the flux of the ions coming on a surface are considered as the key-parameters in anisotropic plasma etching. Since direct ion energy distribution (IED) measurements at the treated surface during plasma processing are often hardly possible, there is an opportunity for virtual ones. This work is devoted to the possibility of such indirect IED and ion flux measurements at an rf-biased electrode in low-pressure rf plasma by using a "virtual IED sensor" which represents "in-situ" IED calculations on the absolute scale in accordance with a plasma sheath model containing a set of measurable external parameters. The "virtual IED sensor" should also involve some external calibration procedure. Applicability and accuracy of the "virtual IED sensor" are validated for a dual-frequency reactive ion etching (RIE) inductively coupled plasma (ICP) reactor with a capacitively coupled rf-biased electrode. The validation is carried out for heavy (Ar) and light (H2) gases under different discharge conditions (different ICP powers, rf-bias frequencies, and voltages). An EQP mass-spectrometer and an rf-compensated Langmuir probe (LP) are used to characterize plasma, while an rf-compensated retarded field energy analyzer (RFEA) is applied to measure IED and ion flux at the rf-biased electrode. Besides, the pulsed selfbias method is used as an external calibration procedure for ion flux estimating at the rf-biased electrode. It is shown that pulsed selfbias method allows calibrating the IED absolute scale quite accurately. It is also shown that the "virtual IED sensor" based on the simplest collisionless sheath model allows reproducing well enough the experimental IEDs at the pressures when the sheath thickness s is less than the ion mean free path λi (s λi), the difference between calculated and experimental IEDs due to ion collisions in the sheath is observed in the low energy range. The effect of electron impact ionization in the sheath on the origin and

  7. Theory of ballooning-mirror instabilities for anisotropic pressure plasmas in the magnetosphere

    Energy Technology Data Exchange (ETDEWEB)

    Cheng, C.Z.; Qian, Q.

    1993-09-01

    This paper deals with a kinetic-MHD eigenmode stability analysis of low frequency ballooning-mirror instabilities for anisotropic pressure plasmas in the magnetosphere. The ballooning mode is a dominant transverse wave driven unstable by pressure gradient in the bad curvature region. The mirror mode with a dominant compressional magnetic field perturbation is excited when the product of plasma beta and pressure anisotropy is large. The field-aligned eigenmode equations take into account the coupling of the transverse and compressional components of the perturbed magnetic field and describe the coupled ballooning-mirror mode. Because the energetic trapped ions precess very rapidly across the {rvec B} field, their motion becomes very rigid with respect to low frequency MHD perturbations with symmetric structure of parallel perturbed magnetic field {delta}B{sub {parallel}} and electrostatic potential {Phi} along the north-south ambient magnetic field, and the symmetric ballooning-mirror mode is shown to be stable. On the other hand, the ballooning-mirror mode with antisymmetric {delta}B{sub {parallel}}, and {Phi} structure along the north-south ambient magnetic field is only weakly influenced by energetic trapped particle kinetic effects due to rapid trapped particle bounce motion and has the lowest instability threshold determined by MHD theory. With large plasma beta ({beta}{sub {parallel}} {ge} O(1)) and pressure anisotropy (P{sub {perpendicular}}/P{sub {parallel}} > 1) at equator the antisymmetric ballooning-mirror mode structures resemble the field-aligned wave structures of the multisatellite observations of a long lasting compressional Pc 5 wave event during November 14--15, 1979 [Takahashi et al.]. The study provides the theoretical basis for identifying the internal excitation mechanism of ULF (Pc 4-5) waves by comparing the plasma stability parameters computed from the satellite particle data with the theoretical values.

  8. Eradication of Pseudomonas aeruginosa biofilms by atmospheric pressure non-thermal plasma.

    Science.gov (United States)

    Alkawareek, Mahmoud Y; Algwari, Qais Th; Laverty, Garry; Gorman, Sean P; Graham, William G; O'Connell, Deborah; Gilmore, Brendan F

    2012-01-01

    Bacteria exist, in most environments, as complex, organised communities of sessile cells embedded within a matrix of self-produced, hydrated extracellular polymeric substances known as biofilms. Bacterial biofilms represent a ubiquitous and predominant cause of both chronic infections and infections associated with the use of indwelling medical devices such as catheters and prostheses. Such infections typically exhibit significantly enhanced tolerance to antimicrobial, biocidal and immunological challenge. This renders them difficult, sometimes impossible, to treat using conventional chemotherapeutic agents. Effective alternative approaches for prevention and eradication of biofilm associated chronic and device-associated infections are therefore urgently required. Atmospheric pressure non-thermal plasmas are gaining increasing attention as a potential approach for the eradication and control of bacterial infection and contamination. To date, however, the majority of studies have been conducted with reference to planktonic bacteria and rather less attention has been directed towards bacteria in the biofilm mode of growth. In this study, the activity of a kilohertz-driven atmospheric pressure non-thermal plasma jet, operated in a helium oxygen mixture, against Pseudomonas aeruginosa in vitro biofilms was evaluated. Pseudomonas aeruginosa biofilms exhibit marked susceptibility to exposure of the plasma jet effluent, following even relatively short (≈ 10's s) exposure times. Manipulation of plasma operating conditions, for example, plasma operating frequency, had a significant effect on the bacterial inactivation rate. Survival curves exhibit a rapid decline in the number of surviving cells in the first 60 seconds followed by slower rate of cell number reduction. Excellent anti-biofilm activity of the plasma jet was also demonstrated by both confocal scanning laser microscopy and metabolism of the tetrazolium salt, XTT, a measure of bactericidal activity.

  9. Eradication of Pseudomonas aeruginosa biofilms by atmospheric pressure non-thermal plasma.

    Directory of Open Access Journals (Sweden)

    Mahmoud Y Alkawareek

    Full Text Available Bacteria exist, in most environments, as complex, organised communities of sessile cells embedded within a matrix of self-produced, hydrated extracellular polymeric substances known as biofilms. Bacterial biofilms represent a ubiquitous and predominant cause of both chronic infections and infections associated with the use of indwelling medical devices such as catheters and prostheses. Such infections typically exhibit significantly enhanced tolerance to antimicrobial, biocidal and immunological challenge. This renders them difficult, sometimes impossible, to treat using conventional chemotherapeutic agents. Effective alternative approaches for prevention and eradication of biofilm associated chronic and device-associated infections are therefore urgently required. Atmospheric pressure non-thermal plasmas are gaining increasing attention as a potential approach for the eradication and control of bacterial infection and contamination. To date, however, the majority of studies have been conducted with reference to planktonic bacteria and rather less attention has been directed towards bacteria in the biofilm mode of growth. In this study, the activity of a kilohertz-driven atmospheric pressure non-thermal plasma jet, operated in a helium oxygen mixture, against Pseudomonas aeruginosa in vitro biofilms was evaluated. Pseudomonas aeruginosa biofilms exhibit marked susceptibility to exposure of the plasma jet effluent, following even relatively short (≈ 10's s exposure times. Manipulation of plasma operating conditions, for example, plasma operating frequency, had a significant effect on the bacterial inactivation rate. Survival curves exhibit a rapid decline in the number of surviving cells in the first 60 seconds followed by slower rate of cell number reduction. Excellent anti-biofilm activity of the plasma jet was also demonstrated by both confocal scanning laser microscopy and metabolism of the tetrazolium salt, XTT, a measure of bactericidal

  10. Atmospheric pressure plasma polymers for tuned QCM detection of protein adhesion.

    Science.gov (United States)

    Rusu, G B; Asandulesa, M; Topala, I; Pohoata, V; Dumitrascu, N; Barboiu, M

    2014-03-15

    Our efforts have been concentrated in preparing plasma polymeric thin layers at atmospheric pressure grown on Quartz Crystal Microbalance-QCM electrodes for which the non-specific absorption of proteins can be efficiently modulated, tuned and used for QCM biosensing and quantification. Plasma polymerization reaction at atmospheric pressure has been used as a simple and viable method for the preparation of QCM bioactive surfaces, featuring variable protein binding properties. Polyethyleneglycol (ppEG), polystyrene (ppST) and poly(ethyleneglycol-styrene) (ppST-EG) thin-layers have been grown on QCM electrodes. These layers were characterized by Atomic Force Microscopy (AFM), Contact angle measurements, Fourier transform infrared (FTIR) and X-ray photoelectron spectroscopy (XPS). The plasma ppST QCM electrodes present a higher adsorption of Concanavalin A (ConA) and Bovine Serum Albumin (BSA) proteins when compared with the commercial coated polystyrene (ppST) ones. The minimum adsorption was found for ppEG, surface, known by their protein anti-fouling properties. The amount of adsorbed proteins can be tuned by the introduction of PEG precursors in the plasma discharge during the preparation of ppST polymers. © 2013 Elsevier B.V. All rights reserved.

  11. Electrical and optical characteristics of atmospheric pressure plasma needle jet driven by neon trasformer

    Science.gov (United States)

    Elfa, Rizan Rizon; Ahmad, Mohd Khairul; Soon, Chin Fhong; Sahdan, Mohd Zainizan; Lias, Jais; Mamat, Mohamad Hafiz; Rusop, Mohamad; Nayan, Nafarizal

    2017-09-01

    The atmospheric pressure plasma needle jet driven by double sinusoidal waveform of neon transformer is reported in this paper. The commercial neon transformer produces about 5 kV of peak sinusoidal voltages and 35 kHz of frequency. Argon gas has been used as discharge gas for this system since the discharge was easily developed rather than using helium gas. In addition, argon gas is three times cheaper than helium gas. The electrical property of the argon discharge has been analyzed in details by measuring its voltage, current and power during the discharge process. Interestingly, it has been found that the total power on the inner needle electrode was slightly lower than that of outer electrode. This may be due to the polarization charges that occurred at inner needle electrode. Then, further investigation to understand the discharge properties was carried out using optical emission spectroscopy (OES) analysis. During OES measurements, two positions of plasma discharge are measured by aligning the quartz optical lens and spectrometer fiber. The OH emission intensity was found higher than that of N2 at the plasma orifice. However, OH emission intensity was lower at 1.5 cm distance from orifice which may be due to penning ionization effect. These results and understanding are essential for surface modification and biomedical applications of atmospheric pressure plasma needle jet.

  12. Theoretical and experimental investigation of plasma and wave characteristics of coaxial discharges at low pressures

    International Nuclear Information System (INIS)

    Neichev, Z; Benova, E; Gamero, A; Sola, A

    2006-01-01

    The paper discusses a new configuration of the surface-wave sustained plasma - 'the coaxial structure'. The coaxial structure is investigated on the base of one-dimensional axial fluid model. That model is adequate enough for low pressure plasma, when the main process for charged particles production is the direct ionization from the ground state and the loss of electrons is due to diffusion to the wall. The role of the geometric factors is evaluated and discussed, varying the discharge conditions in the theoretical model. The main equations of the model - the local dispersion relation and the wave energy balance equation are obtained from Maxwell's equations with appropriate boundary conditions. The phase diagrams, the radial profiles of the electric field and the axial profiles of dimensionless electron number density, wave number, wave power are obtained at various plasma radii and dielectric tube thickness. The results are compared with those for the typical cylindrical plasma column at similar conditions. For the purpose of modelling at low pressure of a coaxial discharge sustained by a travelling electromagnetic wave, some important characteristics of the propagation of surface waves have been investigated experimentally. The axial profiles of the propagation coefficient and radial profiles of the electric field at different experimental conditions have been obtained and discussed

  13. Amine Enrichment of Thin-Film Composite Membranes via Low Pressure Plasma Polymerization for Antimicrobial Adhesion.

    Science.gov (United States)

    Reis, Rackel; Dumée, Ludovic F; He, Li; She, Fenghua; Orbell, John D; Winther-Jensen, Bjorn; Duke, Mikel C

    2015-07-15

    Thin-film composite membranes, primarily based on poly(amide) (PA) semipermeable materials, are nowadays the dominant technology used in pressure driven water desalination systems. Despite offering superior water permeation and salt selectivity, their surface properties, such as their charge and roughness, cannot be extensively tuned due to the intrinsic fabrication process of the membranes by interfacial polymerization. The alteration of these properties would lead to a better control of the materials surface zeta potential, which is critical to finely tune selectivity and enhance the membrane materials stability when exposed to complex industrial waste streams. Low pressure plasma was employed to introduce amine functionalities onto the PA surface of commercially available thin-film composite (TFC) membranes. Morphological changes after plasma polymerization were analyzed by SEM and AFM, and average surface roughness decreased by 29%. Amine enrichment provided isoelectric point changes from pH 3.7 to 5.2 for 5 to 15 min of plasma polymerization time. Synchrotron FTIR mappings of the amine-modified surface indicated the addition of a discrete 60 nm film to the PA layer. Furthermore, metal affinity was confirmed by the enhanced binding of silver to the modified surface, supported by an increased antimicrobial functionality with demonstrable elimination of E. coli growth. Essential salt rejection was shown minimally compromised for faster polymerization processes. Plasma polymerization is therefore a viable route to producing functional amine enriched thin-film composite PA membrane surfaces.

  14. Measurement of the non-thermal properties of a low pressure spraying plasma by electric and spectroscopic methods

    International Nuclear Information System (INIS)

    Jung, Yong Ho

    2003-02-01

    For the case of an atmospheric plasma, the local thermodynamic equilibrium (LTE) model can be applied to plasmas at a nozzle entrance and to those on the axis of the plasma flame, but it is not easy to justify applying the LTE model to off-center plasma and to a low-pressure spraying plasma. Although the energy distribution of the electrons is assumed to be Maxwellian for the most of spraying plasmas, the non-Maxwellian distribution is possible for the case of low-pressure spaying plasma and edge plasma of atmospheric spraying plasma. In this work, the non-Maxwellian distribution of electrons was measured by using an electric probe installed on the fast scanning probe system, and non-LTE effects were measured by using the optical emission spectroscopy system. Distribution of the electrons of a low-pressure spraying plasma is observed not as Maxwellian but as bi-Maxwellian by the measurement of the single probe. Bi-Maxwellian distribution appears in the edge of a low pressure spraying plasma and seems to be due to the reduction of the collisonality by the drastic variation of the plasma density. Non-LTE characteristics of a low-pressure spraying plasma can be deuced from the measured results of the optical emission spectroscopy and is analyzed by the collisional radiative equilibrium (CRE) model, where the Maxwellian and the non-Maxwellian distributions are assumed for comparison. For the electron temperature, the results from optical emission spectroscopy were similar to the results from the single probe (3∼5 % in error)

  15. Equilibrium separation in a high pressure helium plasma and its application to the determination of temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Rodero, A.; Garcia, M.C.; Gamero, A. [Universidad de Cordoba (Spain)

    1995-12-31

    The spectroscopy method based on the Boltzmann-plot of emission lines has been usually employed for measuring the excitation temperature (T{sub exc}) in high pressure plasmas. In the present work, it is shown that this method can produce great errors in the temperature determination when equilibrium separation exists. In this way, the suitability of this determination is tested comparing with other alternative methods in a high pressure helium plasma and also studying its separation from the equilibrium situation, via the absolute population measurements of atomic levels and the estimation of its atomic state distribution function (ASDF). We have made this study using a new excitation structure, the axial injection torch (Torche A Injection Axiale or T.I.A.), which produces a high power microwave plasma at atmospheric pressure. The measurements were carried out at the beginning of the flame (the highest line intensity zone) for a 300-900 W power range at 2.45 GHz and 71/min. of helium gas flow.

  16. Analytical interpretation of arc instabilities in a DC plasma spray torch: the role of pressure

    International Nuclear Information System (INIS)

    Rat, V; Coudert, J F

    2016-01-01

    Arc instabilities in a plasma spray torch are investigated experimentally and theoretically thanks to a linear simplified analytical model. The different parameters that determine the useful properties of the plasma jet at the torch exit, such as specific enthalpy and speed, but also pressure inside the torch and time variations of the flow rate are studied. The work is particularly focused on the link between the recorded arc voltage and the pressure in the cathode cavity. A frequency analysis of the recorded voltage and pressure allows the separation of different contributions following their spectral characteristics and highlights a resonance effect due to Helmholtz oscillations; these oscillations are responsible for the large amplitude fluctuations of all the parameters investigated. The influence of heat transfer, friction forces and residence time of the plasma in the nozzle are taken into account, thanks to different characteristics’ times. The volume of the cathode cavity in which the cold gas is stored before entering the arc region appears to be of prime importance for the dynamics of instabilities, particularly for the non-intuitive effect that induces flow-rate fluctuations in spite of the fact that the torch is fed at a constant flow rate. (paper)

  17. Effects of the finite pressure of plasma on internal kink mode

    International Nuclear Information System (INIS)

    Oliveira, G.M.G. de.

    1980-01-01

    The objective of this work is to study the stability of the Internal Kink and Central Kink modes in ideal MHD cylindrical plasma due to the pressure variations and the different current profiles. It was used the σ Euler equation derived by Goedbloed and Sakanaka. Its analysis is based on the boundary layer method, where the effects due to the plasma inertia are only considered in a boundary layer in the neighborhood of the surface where the perturbation is parallel to the field lines. For the internal Kink mode a numerical analysis is also done by integrating the Euler equation. It was calculated the growth rate of the two modes for the different pressure ans current profiles. It was verified that for both, the Internal Kink and Central Kink modes, the growth rate becomes larger as the derivative of these profiles increases. However, for the Internal Kink mode, one obtains a reduction of up to 50% in the growth rate calculated by Rosenbluth et al. For the Central Kink mode, one notices that the growth rate is proportional to β of the plasma and to the derivatives of the pressure and current. (author) [pt

  18. Spectroscopic diagnosis of an atmospheric-pressure waveguide-based microwave N2–Ar plasma torch

    International Nuclear Information System (INIS)

    Li, Shou-Zhe; Chen, Chuan-Jie; Zhang, Xin; Zhang, Jialiang; Wang, Yong-Xing

    2015-01-01

    An atmospheric-pressure N 2 –Ar plasma is investigated by means of optical emission spectroscopic diagnosis concerning the variation of its fundamental parameters, electron density and plasma temperature, and concentrations of ionized molecular nitrogen, atomic nitrogen, and excited argon with the tuning variables, such as the input power and the ratio of N 2 in N 2 –Ar mixture gas, in the discharge region of the plasma torch. Moreover, qualitative discussions are delivered with respect to the mechanisms for nitrogen dissociation and influence of the Ar component on the N 2 plasma discharge at atmospheric pressure. (paper)

  19. Generation of ultra-high-pressure shocks by collision of a fast plasma projectile driven in the laser-induced cavity pressure acceleration scheme with a solid target

    Czech Academy of Sciences Publication Activity Database

    Badziak, J.; Rosinski, M.; Krouský, Eduard; Kucharik, M.; Liska, R.; Ullschmied, Jiří

    2015-01-01

    Roč. 22, č. 3 (2015), s. 1-11, č. článku 032709. ISSN 1070-664X R&D Projects: GA MŠk(CZ) LD14089; GA MŠk LM2010014 EU Projects: European Commission(XE) 284464 - LASERLAB-EUROPE Institutional support: RVO:68378271 ; RVO:61389021 Keywords : laser-produced plasma * ultra-high-pressure shocks * laser-induced cavity pressure acceleration Subject RIV: BL - Plasma and Gas Discharge Physics OBOR OECD: Fluids and plasma physics (including surface physics) Impact factor: 2.207, year: 2015

  20. Microstructure and mechanical properties of bulk and plasma-sprayed y2O3-partially stabilized zirconia

    Science.gov (United States)

    Valentine, P. G.; Maier, R. D.

    1980-01-01

    Bulk 8.0 weight percent yttria partially stabilied zirconia (PSZ) was studied by light microscopy, transmission electron microscopy, X-ray analysis, microhardness testing, and fracture toughness testing. The as received PSZ contained spheroidal and grain boundary precipitates up to 4 micrometers in size. Spheroids up to 1.26 micrometers were metastable tetragonal; large spheroids were monoclinic. Grinding the PSZ into powder did not cause a significant amount of tetragonal to transform to monoclinic. This indicates that transformation toughness is not a significant mechanism in PSZ. Aging the PSZ at 1500 C caused the fine tetragonal precipitates to grow from 0.06 to 0.12 micrometers, in 250 minutes. A peak hardness of 1400 kg/sq mm was attained after 50 minutes. Solution annealing and quenching the as received PSZ eliminated the large precipitates, but fine tetragonal precipitates reformed on quenching. Aging at 1500 C caused the fine 0.02 micrometers tetragonal precipitates to grow into plates about 0.10 by 0.50 micrometers. A peak hardness of 1517 kg/sq mm was obtained after 250 minutes. On further aging, monoclinic percipitates formed along grain boundaries. The fracture toughness of the aged and unaged solution annealed and quenched PSZ was found to be between 2 and 3 MN /square root of m cubed. This range of fracture toughness is consistent with PSZ's that do not undergo transformation toughening.

  1. A Development of Atmospheric Pressure Plasma Equipment and Its Applications for Treatment of Ag Films Formed from Nano-Particle Ink

    International Nuclear Information System (INIS)

    Itoh, H; Kubota, Y; Kashiwagi, Y; Takeda, K; Ishikawa, K; Kondo, H; Sekine, M; Toyoda, H; Hori, M

    2013-01-01

    We have developed an equipment of atmospheric pressure plasma with two microwave guide antennas, which have a discharge line with 41 slots. The antennas are set against a stage with a heater in a process chamber. A process gas, which is a 1 % H 2 gas diluted by Ar gas and its flow rate is 20 standard litter per minute (slm), flows into the micro-wave guide and goes to a process chamber through each slots. A micro-wave is introduced to the micro-wave guide and the atmospheric pressure plasma grows at each slots. We obtained the electron density of 1×10 15 cm −3 and the H radical density of 1×10 −16 cm −3 at the slot on the condition of a 10 GHz, 1.5 kWatt, pulsed micro-wave with 2.5 pulsed voltage, 4 kHz pulsed frequency, and a duty ratio of 0.16. We applied this system to improve the quality of the spin-coated Ag firm formed from Ag nano-particle ink. This Ag film showed a resistivity of 32 μΩ cm after annealing on the condition of 180 °C for 30 minutes recommended by the maker (The bulk resistivity of Ag is 1.6 μΩ cm). In order to make the annealing time shorter, we studied the effect of atmospheric plasma treatment of Ag film. We obtained the Ag film of the 5.7 μΩ cm resistivity after the atmospheric pressure plasma treatment under 180 °C for 5 min.

  2. Cold plasma synthesis of high quality organic nanoparticles at atmospheric pressure

    Energy Technology Data Exchange (ETDEWEB)

    Radacsi, N., E-mail: kefehu@gmail.com; Heijden, A. E. D. M. van der; Stankiewicz, A. I.; Horst, J. H. ter [Delft University of Technology, Process and Energy Department (Netherlands)

    2013-02-15

    Atmospheric pressure cold surface dielectric barrier discharge (SDBD) plasma was used for the first time to produce nano-sized organic crystals. Nano-sized particles can have beneficial product properties, such as improved internal quality and dissolution rate, compared to conventionally sized crystalline products. In cold plasma crystallization a nebulizer system sprays the solution aerosol into the plasma with the help of a carrier gas. The plasma heats and charges the droplets causing solvent evaporation and coulomb fission to occur, after which nucleation and crystal growth commence within the small, confined volume offered by the small droplets. As a result nano-sized crystals are produced. The operation conditions of SDBD plasma to produce nano-sized crystals of the energetic material RDX were determined by scanning electron microscopy, and the product was investigated with X-ray powder diffraction and sensitivity tests. The sensitivity tests indicated that the nano-sized product had reduced sensitivity for friction, indicating a higher internal quality of the crystalline product.

  3. Atmospheric pressure He-air plasma jet: Breakdown process and propagation phenomenon

    International Nuclear Information System (INIS)

    Begum, Asma; Laroussi, Mounir; Pervez, Mohammad Rasel

    2013-01-01

    In this paper He-discharge (plasma jet/bullet) in atmospheric pressure air and its progression phenomenon has been studied experimentally using ICCD camera, optical emission spectroscopy (OES) and calibrated dielectric probe measurements. The repetitive nanosecond pulse has applied to a plasma pencil to generate discharge in the helium gas channel. The discharge propagation speed was measured from the ICCD images. The axial electric field distribution in the plasma jet is inferred from the optical emission spectroscopic data and from the probe measurement. The correlation between the jet velocities, jet length with the pulse duration is established. It shows that the plasma jet is not isolated from the input voltage along its propagation path. The discharge propagation speed, the electron density and the local and average electric field distribution along the plasma jet axis predicted from the experimental results are in good agreement with the data predicted by numerical simulation of the streamer propagation presented in different literatures. The ionization phenomenon of the discharge predicts the key ionization parameters, such as speed, peak electric field in the front, and electron density. The maximum local electric field measured by OES is 95 kV/cm at 1.3 cm of the jet axis, and average EF measured by probe is 24 kV/cm at the same place of the jet. The average and local electron density estimated are in the order of 10 11 cm -3 and it reaches to the maximum of 10 12 cm -3 .

  4. Application of microwave air plasma in the destruction of trichloroethylene and carbon tetrachloride at atmospheric pressure.

    Science.gov (United States)

    Rubio, S J; Quintero, M C; Rodero, A

    2011-02-15

    In this study, the destruction rate of a volatile waste destruction system based on a microwave plasma torch operating at atmospheric pressure was investigated. Atmospheric air was used to maintain the plasma and was introduced by a compressor, which resulted in lower operating costs compared to other gases such as argon and helium. To isolate the output gases and control the plasma discharge atmosphere, the plasma was coupled to a reactor. The effect of the gas flow rate, microwave power and initial concentration of compound on the destruction efficiency of the system was evaluated. In this study, trichloroethylene and carbon tetrachloride were used as representative volatile organic compounds to determine the destruction rate of the system. Based on the experimental results, at an applied microwave power less than 1000 W, the proposed system can reduce input concentrations in the ppmv range to output concentrations at the ppbv level. High air flow rates and initial concentrations produced energy efficiency values greater than 1000 g/kW h. The output gases and species present in the plasma were analysed by gas chromatography and optical emission spectroscopy, respectively, and negligible amounts of halogenated compounds resulting from the cleavage of C(2)HCl(3) and CCl(4) were observed. The gaseous byproducts of decomposition consisted mainly of CO(2), NO and N(2)O, as well as trace amounts of Cl(2) and solid CuCl. Copyright © 2010 Elsevier B.V. All rights reserved.

  5. Surface treatment of aramid fiber by air dielectric barrier discharge plasma at atmospheric pressure

    International Nuclear Information System (INIS)

    Jia Caixia; Chen Ping; Liu Wei; Li Bin; Wang Qian

    2011-01-01

    Aramid fiber samples are treated by air dielectric barrier discharge (DBD) plasma at atmospheric pressure; the plasma treatment time is investigated as the major parameter. The effects of this treatment on the fiber surface physical and chemical properties are studied by using surface characterization techniques. Scanning electron microscopy (SEM) is performed to determine the surface morphology changes, X-ray photoelectron spectroscopy (XPS) is analyzed to reveal the surface chemical composition variations and dynamic contact angle analysis (DCAA) is used to examine the changes of the fiber surface wettability. In addition, the wetting behavior of a kind of thermoplastic resin, poly(phthalazinone ether sulfone ketone) (PPESK), on aramid fiber surface is also observed by SEM photos. The study shows that there seems to be an optimum treatment condition for surface modification of aramid fiber by the air DBD plasma. In this paper, after the 12 s, 27.6 W/cm 3 plasma treatment the aramid fiber surface roughness is significantly improved, some new oxygen-containing groups such as C-O, C=O and O=C-O are generated on the fiber surface and the fiber surface wettability is greatly enhanced, which results in the better wetting behavior of PPESK resin on the plasma-treated aramid fiber.

  6. DNA damage in oral cancer and normal cells induced by nitrogen atmospheric pressure plasma jets

    Science.gov (United States)

    Han, Xu; Kapaldo, James; Liu, Yueying; Stack, M. Sharon; Ptasinska, Sylwia

    2015-09-01

    Nitrogen atmospheric pressure plasma jets (APPJs) have been shown to effectively induce DNA double strand breaks in SCC25 oral cancer cells. The APPJ source constructed in our laboratory operates based on dielectric barrier discharge. It consists of two copper electrodes alternatively wrapping around a fused silica tube with nitrogen as a feed gas. It is generally more challenging to ignite plasma in N2 atmosphere than in noble gases. However, N2 provides additional advantages such as lower costs compared to noble gases, thus this design can be beneficial for the future long-term clinical use. To compare the effects of plasma on cancer cells (SCC25) and normal cells (OKF), the cells from both types were treated at the same experimental condition for various treatment times. The effective area with different damage levels after the treatment was visualized as 3D maps. The delayed damage effects were also explored by varying the incubation times after the treatment. All of these studies are critical for a better understanding of the damage responses of cellular systems exposed to the plasma radiation, thus are useful for the development of the advanced plasma cancer therapy. The research described herein was supported by the Division of Chemical Sciences, Geosciences and Biosciences, Basic Energy Sciences, Office of Science, United States Department of Energy through Grant No. DE-FC02-04ER15533.

  7. Inactivation of virus in solution by cold atmospheric pressure plasma: identification of chemical inactivation pathways

    Science.gov (United States)

    Aboubakr, Hamada A.; Gangal, Urvashi; Youssef, Mohammed M.; Goyal, Sagar M.; Bruggeman, Peter J.

    2016-05-01

    Cold atmospheric pressure plasma (CAP) inactivates bacteria and virus through in situ production of reactive oxygen and nitrogen species (RONS). While the bactericidal and virucidal efficiency of plasmas is well established, there is limited knowledge about the chemistry leading to the pathogen inactivation. This article describes a chemical analysis of the CAP reactive chemistry involved in the inactivation of feline calicivirus. We used a remote radio frequency CAP produced in varying gas mixtures leading to different plasma-induced chemistries. A study of the effects of selected scavengers complemented with positive control measurements of relevant RONS reveal two distinctive pathways based on singlet oxygen and peroxynitrous acid. The first mechanism is favored in the presence of oxygen and the second in the presence of air when a significant pH reduction is induced in the solution by the plasma. Additionally, smaller effects of the H2O2, O3 and \\text{NO}2- produced were also found. Identification of singlet oxygen-mediated 2-imidazolone/2-oxo-His (His  +14 Da)—an oxidative modification of His 262 comprising the capsid protein of feline calicivirus links the plasma induced singlet oxygen chemistry to viral inactivation.

  8. Radio frequency energy coupling to high-pressure optically pumped nonequilibrium plasmas

    International Nuclear Information System (INIS)

    Plonjes, Elke; Palm, Peter; Lee, Wonchul; Lempert, Walter R.; Adamovich, Igor V.

    2001-01-01

    This article presents an experimental demonstration of a high-pressure unconditionally stable nonequilibrium molecular plasma sustained by a combination of a continuous wave CO laser and a sub-breakdown radio frequency (rf) electric field. The plasma is sustained in a CO/N 2 mixture containing trace amounts of NO or O 2 at pressures of P=0.4 - 1.2atm. The initial ionization of the gases is produced by an associative ionization mechanism in collisions of two CO molecules excited to high vibrational levels by resonance absorption of the CO laser radiation with subsequent vibration-vibration (V-V) pumping. Further vibrational excitation of both CO and N 2 is produced by free electrons heated by the applied rf field, which in turn produces additional ionization of these species by the associative ionization mechanism. In the present experiments, the reduced electric field, E/N, is sufficiently low to preclude field-induced electron impact ionization. Unconditional stability of the resultant cold molecular plasma is enabled by the negative feedback between gas heating and the associative ionization rate. Trace amounts of nitric oxide or oxygen added to the baseline CO/N 2 gas mixture considerably reduce the electron - ion dissociative recombination rate and thereby significantly increase the initial electron density. This allows triggering of the rf power coupling to the vibrational energy modes of the gas mixture. Vibrational level populations of CO and N 2 are monitored by infrared emission spectroscopy and spontaneous Raman spectroscopy. The experiments demonstrate that the use of a sub-breakdown rf field in addition to the CO laser allows an increase of the plasma volume by about an order of magnitude. Also, CO infrared emission spectra show that with the rf voltage turned on the number of vibrationally excited CO molecules along the line of sight increase by a factor of 3 - 7. Finally, spontaneous Raman spectra of N 2 show that with the rf voltage the vibrational

  9. Bulk nanocrystalline Al85Ni10La5 alloy fabricated by spark plasma sintering of atomized amorphous powders

    International Nuclear Information System (INIS)

    Sasaki, T.T.; Hono, K.; Vierke, J.; Wollgarten, M.; Banhart, J.

    2008-01-01

    Amorphous Al 85 Ni 10 La 5 powders were consolidated to cylindrical samples by spark plasma sintering (SPS), and their microstructures and mechanical properties were investigated. When the powders were consolidated below the crystallization temperature, an amorphous phase was retained in the consolidated sample. Sintering above the crystallization temperature caused full crystallization. The Vickers hardness of the amorphous-containing sample was about 350 HV in the as-sintered state and increased up to 450 HV by a subsequent heat treatment just below the crystallization temperature. The highest hardness was achieved in a nanocrystalline microstructure. Compression tests revealed the brittle nature of the consolidated samples although the fracture and yield strength was higher than 1 GPa. The brittleness is due to the low relative density of the amorphous-containing samples and the presence of a large amount of intermetallic compounds in the fully crystallized sample

  10. Atmospheric pressure plasma jet for bacterial decontamination and property improvement of fruit and vegetable processing wastewater

    Science.gov (United States)

    Mohamed, Abdel-Aleam H.; Shariff, Samir M. Al; Ouf, Salama A.; Benghanem, Mohamed

    2016-05-01

    An atmospheric pressure plasma jet was tested for decontaminating and improving the characteristics of wastewater derived from blackberry, date palm, tomato and beetroot processing industries. The jet was generated by blowing argon gas through a cylindrical alumina tube while a high voltage was applied between two electrodes surrounding the tube. Oxygen gas was mixed with argon at the rate of 0.2% and the argon mass flow was fixed at 4.5 slm. Images show that the generated plasma jet penetrated the treated wastewater samples. Plasma emission spectra show the presence of O and OH radicals as well as excited molecular nitrogen and argon. Complete decontamination of wastewater derived from date palm and tomato processing was achieved after 120 and 150 s exposure to the plasma jet, respectively. The bacterial count of wastewater from blackberry and beetroot was reduced by 0.41 and 2.24 log10 colony-forming units (CFU) per ml, respectively, after 180 s. Escherichia coli was the most susceptible bacterial species to the cold plasma while Shigella boydii had the minimum susceptibility, recording 1.30 and 3.34 log10 CFU ml-1, respectively, as compared to the 7.00 log10 initial count. The chemical oxygen demands of wastewater were improved by 57.5-93.3% after 180 s exposure to the plasma jet being tested. The endotoxins in the wastewater were reduced by up to 90.22%. The variation in plasma effectiveness is probably related to the antioxidant concentration of the different investigated wastewaters.

  11. Limits of deuterium pressure range with neutron production in plasma focus devices

    International Nuclear Information System (INIS)

    Pouzo, J.; Milanese, M.; Piriz, R.; Cortazar, D.; Moroso, R.

    1988-01-01

    In this work we present the experimental curves of neutron yield (Y) respect to the deuterium filling pressure (p) obtained in our plasma focuses device PACO. Y increases with the focus current (I f ) according with the scaling law Y ∼I 4-5 f , but it presents a limited range of p beyond which Y drastically decreases. The higher pressure limit is coincident with recently reported limit due to the energy available to maintain the ionization rate of the neutral gas during the roll-off stage. The lower pressure limit is here explained, through experimental evidences, in terms of a phenomenon connected with the dynamics of the current sheath (cs) during the roll-off stage. (author). 8 refs, 11 figs

  12. Effects of imipramine of the orthostatic changes in blood pressure, heart rate and plasma catecholamines

    DEFF Research Database (Denmark)

    Nielsen, J R; Johansen, Torben; Arentoft, A

    1983-01-01

    The effect of imipramine on the orthostatic changes in heart rate, blood pressure and plasma catecholamines were examined in six healthy male subjects on two occasions on high sodium balance (Na+ excretion greater than 120 mmol per day) and on low sodium balance (Na+ excretion less than 110 mmol...... per day), respectively. Orthostatic tests were carried out before and 2 h after ingestion of 150 mg imipramine hydrochloride. Imipramine caused a moderate increase in supine systolic blood pressure, and a pronounced increase in the rise in heart rate, when the subjects assumed erect position....... The orthostatic drop in systolic blood pressure was in most cases only moderately increased after ingestion of imipramine, but in three subjects pronounced orthostatic hypotension developed when the sodium balance was low, whereas no clinical symptoms were seen in the same subjects when tested after imipramine...

  13. Fish oil affects blood pressure and the plasma lipid profile in healthy Danish infants

    DEFF Research Database (Denmark)

    Damsgaard, C.T.; Schack-Nielsen, L.; Michaelsen, K.F.

    2006-01-01

    Animal and epidemiologic studies indicate that early nutrition has lasting effects on metabolism and cardiovascular disease risk. In adults, (n-3) long-chain PUFA (LCPUFA) from fish oils improve blood pressure, the lipid profile, and possibly cardiovascular disease mortality. This randomized trial...... is the first to investigate the effects of fish oil on blood pressure and the lipid profile in infancy. Healthy term 9-mo old infants In 83) were randomly assigned to 5 mL fish oil daily or no fish oil for 3 mo and to 2 different milk types. Before and after the intervention, blood pressure was measured...... with an oscillometric device, and blood was sampled for analysis of erythrocyte fatty acid composition and the plasma lipid profile. This paper examines the effects of the fish oil supplement, with adjustment for the effects of the milk intervention when relevant. The fish oil intervention increased erythrocyte (n-3...

  14. Shear-induced pressure anisotropization and correlation with fluid vorticity in a low collisionality plasma

    Science.gov (United States)

    Del Sarto, Daniele; Pegoraro, Francesco

    2018-03-01

    The momentum anisotropy contained in a sheared flow may be transferred to a pressure anisotropy, both gyrotropic and non-gyrotropic, via the action of the fluid strain on the pressure tensor components. In particular, it is the traceless symmetric part of the strain tensor (i.e. the so-called shear tensor) that drives the mechanism, the fluid vorticity just inducing rotations of the pressure tensor components. This possible mechanism of anisotropy generation from an initially isotropic pressure is purely dynamical and can be described in a fluid framework where the full pressure tensor evolution is retained. Here, we interpret the correlation between vorticity and anisotropy, often observed in numerical simulations of solar wind turbulence, as due to the correlation between shear rate tensor and fluid vorticity. We then discuss some implications of this analysis for the onset of the Kelvin-Helmholtz instability in collisionless plasmas where a full pressure tensor evolution is allowed, and for the modelling of secondary reconnection in turbulence.

  15. The influence of gas pressure on E↔H mode transition in argon inductively coupled plasmas

    Science.gov (United States)

    Zhang, Xiao; Zhang, Zhong-kai; Cao, Jin-xiang; Liu, Yu; Yu, Peng-cheng

    2018-03-01

    Considering the gas pressure and radio frequency power change, the mode transition of E↔H were investigated in inductively coupled plasmas. It can be found that the transition power has almost the same trend decreasing with gas pressure, whether it is in H mode or E mode. However, the transition density increases slowly with gas pressure from E to H mode. The transition points of E to H mode can be understood by the propagation of electromagnetic wave in the plasma, while the H to E should be illustrated by the electric field strength. Moreover, the electron density, increasing with the pressure and power, can be attributed to the multiple ionization, which changes the energy loss per electron-ion pair created. In addition, the optical emission characteristics in E and H mode is also shown. The line ratio of I750.4 and I811.5, taken as a proxy of the density of metastable state atoms, was used to illustrate the hysteresis. The 750.4 nm line intensity, which has almost the same trend with the 811.5 nm line intensity in H mode, both of them increases with power but decreases with gas pressure. The line ratio of 811.5/750.4 has a different change rule in E mode and H mode, and at the transition point of H to E, it can be one significant factor that results in the hysteresis as the gas pressure change. And compared with the 811.5 nm intensity, it seems like a similar change rule with RF power in E mode. Moreover, some emitted lines with lower rate constants don't turn up in E mode, while can be seen in H mode because the excited state atom density increasing with the electron density.

  16. Roles of bulk viscosity on Rayleigh-Taylor instability: Non-equilibrium thermodynamics due to spatio-temporal pressure fronts

    Energy Technology Data Exchange (ETDEWEB)

    Sengupta, Tapan K., E-mail: tksen@iitk.ac.in; Bhole, Ashish; Shruti, K. S. [HPCL, Department of Aerospace Engineering, IIT Kanpur, Kanpur, UP (India); Sengupta, Aditi [Department of Engineering, University of Cambridge, Cambridge (United Kingdom); Sharma, Nidhi [Graduate Student, HPCL, Department of Aerospace Engineering, IIT Kanpur, Kanpur, UP (India); Sengupta, Soumyo [Department of Mechanical and Aerospace Engineering, Ohio State University, Columbus, Ohio 43210 (United States)

    2016-09-15

    Direct numerical simulations of Rayleigh-Taylor instability (RTI) between two air masses with a temperature difference of 70 K is presented using compressible Navier-Stokes formulation in a non-equilibrium thermodynamic framework. The two-dimensional flow is studied in an isolated box with non-periodic walls in both vertical and horizontal directions. The non-conducting interface separating the two air masses is impulsively removed at t = 0 (depicting a heaviside function). No external perturbation has been used at the interface to instigate the instability at the onset. Computations have been carried out for rectangular and square cross sections. The formulation is free of Boussinesq approximation commonly used in many Navier-Stokes formulations for RTI. Effect of Stokes’ hypothesis is quantified, by using models from acoustic attenuation measurement for the second coefficient of viscosity from two experiments. Effects of Stokes’ hypothesis on growth of mixing layer and evolution of total entropy for the Rayleigh-Taylor system are reported. The initial rate of growth is observed to be independent of Stokes’ hypothesis and the geometry of the box. Following this stage, growth rate is dependent on the geometry of the box and is sensitive to the model used. As a consequence of compressible formulation, we capture pressure wave-packets with associated reflection and rarefaction from the non-periodic walls. The pattern and frequency of reflections of pressure waves noted specifically at the initial stages are reflected in entropy variation of the system.

  17. Direct Simulation Monte Carlo Simulations of Low Pressure Semiconductor Plasma Processing

    International Nuclear Information System (INIS)

    Gochberg, L. A.; Ozawa, T.; Deng, H.; Levin, D. A.

    2008-01-01

    The two widely used plasma deposition tools for semiconductor processing are Ionized Metal Physical Vapor Deposition (IMPVD) of metals using either planar or hollow cathode magnetrons (HCM), and inductively-coupled plasma (ICP) deposition of dielectrics in High Density Plasma Chemical Vapor Deposition (HDP-CVD) reactors. In these systems, the injected neutral gas flows are generally in the transonic to supersonic flow regime. The Hybrid Plasma Equipment Model (HPEM) has been developed and is strategically and beneficially applied to the design of these tools and their processes. For the most part, the model uses continuum-based techniques, and thus, as pressures decrease below 10 mTorr, the continuum approaches in the model become questionable. Modifications have been previously made to the HPEM to significantly improve its accuracy in this pressure regime. In particular, the Ion Monte Carlo Simulation (IMCS) was added, wherein a Monte Carlo simulation is used to obtain ion and neutral velocity distributions in much the same way as in direct simulation Monte Carlo (DSMC). As a further refinement, this work presents the first steps towards the adaptation of full DSMC calculations to replace part of the flow module within the HPEM. Six species (Ar, Cu, Ar*, Cu*, Ar + , and Cu + ) are modeled in DSMC. To couple SMILE as a module to the HPEM, source functions for species, momentum and energy from plasma sources will be provided by the HPEM. The DSMC module will then compute a quasi-converged flow field that will provide neutral and ion species densities, momenta and temperatures. In this work, the HPEM results for a hollow cathode magnetron (HCM) IMPVD process using the Boltzmann distribution are compared with DSMC results using portions of those HPEM computations as an initial condition.

  18. Improvement of field emission from screen-printed carbon nanotubes by He/(N2,Ar) atmospheric pressure plasma treatment

    International Nuclear Information System (INIS)

    Kyung, S. J.; Park, J. B.; Lee, J. H.; Yeom, G. Y.

    2006-01-01

    A screen-printed carbon nanotube (CNT) paste for applications to field emission emitters was treated with He, He/Ar, and He/N 2 atmospheric pressure plasmas. The effect of the different plasma treatments on the field emission characteristics of the screen-printed CNTs was investigated. The atmospheric pressure plasma applied to the screen-printed CNT paste for 10 s resulted in a reduction in the turn-on electric field. In particular, the application of a He/N 2 plasma treatment decreased the turn-on electric field from 3.13 to 1.29 V/μm and increased the field enhancement factor from 737 to 2775 after the treatment. These results suggest that an adequate atmospheric pressure plasma treatment of screen-printed CNTs can be effective in enhancing the field emission properties

  19. The effect of quercetin on plasma oxidative status, C-reactive protein and blood pressure in women with rheumatoid arthritis

    Directory of Open Access Journals (Sweden)

    Fatemeh Javadi

    2014-01-01

    Conclusions: In this study, quercetin had no effect on oxidative and inflammatory status of plasma and blood pressure in patients with RA. Further studies are needed to ensure the effect of quercetin on oxidative stress and inflammation in human.

  20. Sterilization and Decontamination of Surfaces Contaminated With Biological and Chemical Warfare Agents Using Atmospheric Pressure Plasma Discharges

    National Research Council Canada - National Science Library

    Garate, Eusebio

    1999-01-01

    ... based on the application of an atmospheric pressure plasma. We used both a DC corona and dielectric barrier discharge for the sterilization tests which were conducted on a variety of substrates including metals and chemically resistant fabrics...

  1. Nonequilibrium atmospheric pressure plasma jet using a combination of 50 kHz/2 MHz dual-frequency power sources

    International Nuclear Information System (INIS)

    Zhou, Yong-Jie; Yuan, Qiang-Hua; Li, Fei; Wang, Xiao-Min; Yin, Gui-Qin; Dong, Chen-Zhong

    2013-01-01

    An atmospheric pressure plasma jet is generated by dual sinusoidal wave (50 kHz and 2 MHz). The dual-frequency plasma jet exhibits the advantages of both low frequency and radio frequency plasmas, namely, the long plasma plume and the high electron density. The radio frequency ignition voltage can be reduced significantly by using dual-frequency excitation compared to the conventional radio frequency without the aid of the low frequency excitation source. A larger operating range of α mode discharge can be obtained using dual-frequency excitation which is important to obtain homogeneous and low-temperature plasma. A larger controllable range of the gas temperature of atmospheric pressure plasma could also be obtained using dual-frequency excitation

  2. LIF diagnostics of hydroxyl radical in a methanol containing atmospheric-pressure plasma jet

    Science.gov (United States)

    Qian, Mu-Yang; Liu, San-Qiu; Pei, Xue-Kai; Lu, Xin-Pei; Zhang, Jia-Liang; Wang, De-Zhen

    2016-10-01

    In this paper, a pulsed-dc CH3OH/Ar plasma jet generated at atmospheric pressure is studied by laser-induced fluorescence (LIF) and optical emission spectroscopy (OES). A gas-liquid bubbler system is proposed to introduce the methanol vapor into the argon gas, and the CH3OH/Ar volume ratio is kept constant at about 0.1%. Discharge occurs in a 6-mm needle-to-ring gap in an atmospheric-pressure CH3OH/Ar mixture. The space-resolved distributions of OH LIF inside and outside the nozzle exhibit distinctly different behaviors. And, different production mechanisms of OH radicals in the needle-to-ring discharge gap and afterglow of plasma jet are discussed. Besides, the optical emission lines of carbonaceous species, such as CH, CN, and C2 radicals, are identified in the CH3OH/Ar plasma jet. Finally, the influences of operating parameters (applied voltage magnitude, pulse frequency, pulsewidth) on the OH radical density are also presented and analyzed. Project supported by the National Natural Science Foundation of China (Grant Nos. 11465013 and 11375041), the Natural Science Foundation of Jiangxi Province, China (Grant Nos. 20151BAB212012 and 20161BAB201013), and the International Science and Technology Cooperation Program of China (Grant No. 2015DFA61800).

  3. Atomic hydrogen determination in medium-pressure microwave discharge hydrogen plasmas via emission actinometry

    International Nuclear Information System (INIS)

    Geng Zicai; Xu Yong; Yang Xuefeng; Wang Weiguo; Zhu Aimin

    2005-01-01

    Atomic hydrogen plays an important role in the chemical vapour deposition of functional materials, plasma etching and new approaches to the chemical synthesis of hydrogen-containing compounds. This work reports experimental determinations of atomic hydrogen in microwave discharge hydrogen plasmas formed from the TM 01 microwave mode in an ASTeX-type reactor, via optical emission spectroscopy using Ar as an actinometer. The relative intensities of the H atom Balmer lines and Ar-750.4 nm emissions as functions of input power and gas pressure have been investigated. At an input microwave power density of 13.5 W cm -3 , the approximate hydrogen dissociation fractions calculated from electron-impact excitation and quenching cross sections in the literature, decreased from ∼0.08 to ∼0.03 as the gas pressure was increased from 5 to 25 Torr. The influences of the above cross sections, and the electron and gas temperatures of the plasmas on the determination of the hydrogen dissociation fraction data have been discussed

  4. Superhydrophobic treatment using atmospheric-pressure He/C4F8 plasma for buoyancy improvement

    Science.gov (United States)

    Noh, Sooryun; Moon, A.-Young; Moon, Se Youn

    2015-04-01

    A superhydrophobic miniature boat was fabricated with aluminum alloy plates treated with atmospheric-pressure helium (He)/octafluorocyclobutane (C4F8) plasma using 13.56 MHz rf power. When only 0.13% C4F8 was added to He gas, the contact angle of the surface increased to 140° and the surface showed superhydrophobic properties. On the basis of chemical and morphological analyses, fluorinated functional groups (CF, CF2, and CF3) and nano-/micro-sized particles were detected on the Al surface. These features brought about superhydrophobicity similar to the lotus effect. While the miniature boat, assembled with plasma-treated plates, was immersed in water, a layer of air (i.e., a plastron) surrounded the superhydrophobic surfaces. This effect contributed to the development of a 4.7% increase in buoyancy. In addition, the superhydrophobic properties lasted for two months under the submerged condition. These results demonstrate that treatment with atmospheric-pressure He/C4F8 plasma is a promising method of improving the load capacity and antifouling properties, and reducing the friction of marine ships through a fast and low-cost superhydrophobic treatment process.

  5. An Evaluation of Atmospheric-pressure Plasma for the Cost-Effective Deposition of Antireflection Coatings

    Energy Technology Data Exchange (ETDEWEB)

    Rob Sailer; Guruvenket Srinivasan; Kyle W. Johnson; Douglas L. Schulz

    2010-04-01

    Atmospheric-pressure plasma deposition (APPD) has previously been used to deposit various functional materials including polymeric surface modification layers, transparent conducting oxides, and photo catalytic materials. For many plasma polymerized coatings, reaction occurs via free radical mechanism where the high energy electrons from the plasma activate the olefinic carbon-carbon double bonds - a typical functional group in such precursors. The precursors for such systems are typically inexpensive and readily available and have been used in vacuum PECVD previously. The objectives are to investigate: (1) the effect of plasma power, gas composition and substrate temperature on the Si-based film properties using triethylsilane(TES) as the precursor; and (2) the chemical, mechanical, and optical properties of several experimental matrices based on Design of Experiment (DOE) principals. A simple APPD route has been utilized to deposit Si based films from an inexpensive precursor - Triethylsilane (TES). Preliminary results indicates formation of Si-C & Si-O and Si-O, Si-C & Si-N bonds with oxygen and nitrogen plasmas respectively. N{sub 2}-O{sub 2} plasma showed mixed trend; however oxygen remains a significant portion of all films, despite attempts to minimize exposure to atmosphere. SiN, SiC, and SiO ratios can be modified by the reaction conditions resulting in differing film properties. SE studies revealed that films with SiN bond possess refractive index higher than coatings with Si-O/Si-C bonds. Variable angle reflectance studies showed that SiOCN coatings offer AR properties; however thickness and refractive index optimization of these coatings remains necessary for application as potential AR coatings.

  6. Degeneration of amyloid-ß fibrils caused by exposure to low-temperature atmospheric-pressure plasma in aqueous solution

    OpenAIRE

    Takai, Eisuke; Ohashi, Gai; Yoshida, Tomonori; Sörgjerd, Karin Margareta; Zako, Tamotsu; Maeda, Mizuo; Kitano, Katsuhisa; Shiraki, Kentaro

    2014-01-01

    Low-temperature atmospheric-pressure plasma was applied to degenerate amyloid-ß (Aß) fibrils, which are a major component of neuritic plaque associated with Alzheimer's disease (AD). We showed that an Aß fibril exposed to a low-frequency (LF) plasma jet in aqueous solution retained its morphology, molecular weight, and cytotoxicity, but, intriguingly, decreased in protease resistance and ß-sheet content. These results suggested that an LF plasma jet could be utilized for the treatment of AD t...

  7. Atmospheric pressure plasma deposition of antimicrobial coatings on non-woven textiles

    Science.gov (United States)

    Nikiforov, Anton Yu.; Deng, Xiaolong; Onyshchenko, Iuliia; Vujosevic, Danijela; Vuksanovic, Vineta; Cvelbar, Uros; De Geyter, Nathalie; Morent, Rino; Leys, Christophe

    2016-08-01

    A simple method for preparation of nanoparticle incorporated non-woven fabric with high antibacterial efficiency has been proposed based on atmospheric pressure plasma process. In this work direct current plasma jet stabilized by fast nitrogen flow was used as a plasma deposition source. Three different types of the nanoparticles (silver, copper and zinc oxide nanoparticles) were employed as antimicrobial agents. X-ray photoelectron spectroscopy (XPS) measurements have shown a positive chemical shift observed for Ag 3d 5/2 (at 368.1 eV) suggests that silver nanoparticles (AgNPs) are partly oxidized during the deposition. The surface chemistry and the antibacterial activity of the samples against Staphylococcus aureus and Escherichia coli were investigated and analyzed. It is shown that the samples loaded with nanoparticles of Ag and Cu and having the barrier layer of 10 nm characterized by almost 97% of bacterial reduction whereas the samples with ZnO nanoparticles provide 86% reduction of Staphylococcus aureus. Contribution to the topical issue "6th Central European Symposium on Plasma Chemistry (CESPC-6)", edited by Nicolas Gherardi, Ester Marotta and Cristina Paradisi

  8. Surface Decontamination of Chemical Agent Surrogates Using an Atmospheric Pressure Air Flow Plasma Jet

    Science.gov (United States)

    Li, Zhanguo; Li, Ying; Cao, Peng; Zhao, Hongjie

    2013-07-01

    An atmospheric pressure dielectric barrier discharge (DBD) plasma jet generator using air flow as the feedstock gas was applied to decontaminate the chemical agent surrogates on the surface of aluminum, stainless steel or iron plate painted with alkyd or PVC. The experimental results of material decontamination show that the residual chemical agent on the material is lower than the permissible value of the National Military Standard of China. In order to test the corrosion effect of the plasma jet on different material surfaces in the decontamination process, corrosion tests for the materials of polymethyl methacrylate, neoprene, polyvinyl chloride (PVC), polyethylene (PE), phenolic resin, iron plate painted with alkyd, stainless steel, aluminum, etc. were carried out, and relevant parameters were examined, including etiolation index, chromatism, loss of gloss, corrosion form, etc. The results show that the plasma jet is slightly corrosive for part of the materials, but their performances are not affected. A portable calculator, computer display, mainboard, circuit board of radiogram, and a hygrometer could work normally after being treated by the plasma jet.

  9. Surface Decontamination of Chemical Agent Surrogates Using an Atmospheric Pressure Air Flow Plasma Jet

    International Nuclear Information System (INIS)

    Li Zhanguo; Li Ying; Cao Peng; Zhao Hongjie

    2013-01-01

    An atmospheric pressure dielectric barrier discharge (DBD) plasma jet generator using air flow as the feedstock gas was applied to decontaminate the chemical agent surrogates on the surface of aluminum, stainless steel or iron plate painted with alkyd or PVC. The experimental results of material decontamination show that the residual chemical agent on the material is lower than the permissible value of the National Military Standard of China. In order to test the corrosion effect of the plasma jet on different material surfaces in the decontamination process, corrosion tests for the materials of polymethyl methacrylate, neoprene, polyvinyl chloride (PVC), polyethylene (PE), phenolic resin, iron plate painted with alkyd, stainless steel, aluminum, etc. were carried out, and relevant parameters were examined, including etiolation index, chromatism, loss of gloss, corrosion form, etc. The results show that the plasma jet is slightly corrosive for part of the materials, but their performances are not affected. A portable calculator, computer display, mainboard, circuit board of radiogram, and a hygrometer could work normally after being treated by the plasma jet

  10. Microwave atmospheric pressure plasma jets for wastewater treatment: Degradation of methylene blue as a model dye.

    Science.gov (United States)

    García, María C; Mora, Manuel; Esquivel, Dolores; Foster, John E; Rodero, Antonio; Jiménez-Sanchidrián, César; Romero-Salguero, Francisco J

    2017-08-01

    The degradation of methylene blue in aqueous solution as a model dye using a non thermal microwave (2.45 GHz) plasma jet at atmospheric pressure has been investigated. Argon has been used as feed gas and aqueous solutions with different concentrations of the dye were treated using the effluent from plasma jet in a remote exposure. The removal efficiency increased as the dye concentration decreased from 250 to 5 ppm. Methylene blue degrades after different treatment times, depending on the experimental plasma conditions. Thus, kinetic constants up to 0.177 min -1 were obtained. The higher the Ar flow, the faster the degradation rate. Optical emission spectroscopy (OES) was used to gather information about the species present in the gas phase, specifically excited argon atoms. Argon excited species and hydrogen peroxide play an important role in the degradation of the dye. In fact, the conversion of methylene blue was directly related to the density of argon excited species in the gas phase and the concentration of hydrogen peroxide in the aqueous liquid phase. Values of energy yield at 50% dye conversion of 0.296 g/kWh were achieved. Also, the use of two plasma applicators in parallel has been proven to improve energy efficiency. Copyright © 2017 Elsevier Ltd. All rights reserved.

  11. Investigation of the gas flow effect on an atmospheric pressure RF plasma torch

    International Nuclear Information System (INIS)

    Atanasova, M; Degrez, G; Mihailova, D; Carbone, E; Van Dijk, J; Van der Mullen, J J A M; Benova, E

    2011-01-01

    A cool atmospheric pressure non-thermal capactively-coupled RF discharge is studied. It is created between two parallel electrodes - a powered one supplied by 13.56 MHz, and a grounded one. The feed gas argon flows via holes between the electrodes where it is ionized. The plasma torch is studied by means of a time dependent two-dimensional fluid model. A simplified kinetic scheme with four active species is considered, namely argon excited atoms (Ar*), atomic (Ar + ) ions, molecular (Ar 2+ ) ions and electrons (e). The plasma dynamics in the space between the electrodes as well as in the extended region behind the grounded electrode is studied. The effect of the gas flow on the plasma is examined. Constriction of the plasma is induced by the field sustaining the discharge due to the sieve-like structure of the electrodes. As a result of the stationary gas flow the filaments extend beyond the electrodes ensuring a flow of active species in the afterglow.

  12. A collisional-radiative model for low-pressure weakly magnetized Ar plasmas

    Science.gov (United States)

    Zhu, Xi-Ming; Tsankov, Tsanko; Czarnetzki, Uwe; Marchuk, Oleksandr

    2016-09-01

    Collisional-radiative (CR) models are widely investigated in plasma physics for describing the kinetics of reactive species and for optical emission spectroscopy. This work reports a new Ar CR model used in low-pressure (0.01-10 Pa) weakly magnetized (Tesla) plasmas, including ECR, helicon, and NLD discharges. In this model 108 realistic levels are individually studied, i.e. 51 lowest levels of the Ar atom and 57 lowest levels of the Ar ion. We abandon the concept of an ``effective level'' usually adopted in previous models for glow discharges. Only in this way the model can correctly predict the non-equilibrium population distribution of close energy levels. In addition to studying atomic metastable and radiative levels, this model describes the kinetic processes of ionic metastable and radiative levels in detail for the first time. This is important for investigation of plasma-surface interaction and for optical diagnostics using atomic and ionic line-ratios. This model could also be used for studying Ar impurities in tokamaks and astrophysical plasmas.

  13. Cold atmospheric pressure plasma and decontamination. Can it contribute to preventing hospital-acquired infections?

    Science.gov (United States)

    O'Connor, N; Cahill, O; Daniels, S; Galvin, S; Humphreys, H

    2014-10-01

    Healthcare-associated infections (HCAIs) affect ∼4.5 million patients in Europe alone annually. With the ever-increasing number of 'multi-resistant' micro-organisms, alternative and more effective methods of environmental decontamination are being sought as an important component of infection prevention and control. One of these is the use of cold atmospheric pressure plasma (CAPP) systems with clinical applications in healthcare facilities. CAPPs have been shown to demonstrate antimicrobial, antifungal and antiviral properties and have been adopted for other uses in clinical medicine over the past decade. CAPPs vary in their physical and chemical nature depending on the plasma-generating mechanism (e.g. plasma jet, dielectric barrier discharge, etc.). CAPP systems produce a 'cocktail' of species including positive and negative ions, reactive atoms and molecules (e.g. atomic oxygen, ozone, superoxide and oxides of nitrogen), intense electric fields, and ultraviolet radiation (UV). The effects of these ions have been studied on micro-organisms, skin, blood, and DNA; thus, a range of possible applications of CAPPs has been identified, including surface decontamination, wound healing, biofilm removal, and even cancer therapy. Here we evaluate plasma devices, their applications, mode of action and their potential role specifically in combating HCAIs on clinical surfaces. Copyright © 2014 The Healthcare Infection Society. Published by Elsevier Ltd. All rights reserved.

  14. Liquid sampling-atmospheric pressure glow discharge as a secondary excitation source: Assessment of plasma characteristics

    Science.gov (United States)

    Manard, Benjamin T.; Gonzalez, Jhanis J.; Sarkar, Arnab; Dong, Meirong; Chirinos, Jose; Mao, Xianglei; Russo, Richard E.; Marcus, R. Kenneth

    The liquid sampling-atmospheric pressure glow discharge (LS-APGD) has been assessed as a secondary excitation source with a parametric evaluation regarding carrier gas flow rate, applied current, and electrode distance. With this parametric evaluation, plasma optical emission was monitored in order to obtain a fundamental understanding with regards to rotational temperature (Trot), excitation temperature (Texc), electron number density (ne), and plasma robustness. Incentive for these studies is not only for a greater overall fundamental knowledge of the APGD, but also in instrumenting a secondary excitation/ionization source following laser ablation (LA). Rotational temperatures were determined through experimentally fitting of the N2 and OH molecular emission bands while atomic excitation temperatures were calculated using a Boltzmann distribution of He and Mg atomic lines. The rotational and excitation temperatures were determined to be ~ 1000 K and ~ 2700 K respectively. Electron number density was calculated to be on the order of ~ 3 × 1015 cm- 3 utilizing Stark broadening effects of the Hα line of the Balmer series and a He I transition. In addition, those diagnostics were performed introducing magnesium (by solution feed and laser ablation) into the plasma in order to determine any perturbation under heavy matrix sampling. The so-called plasma robustness factor, derived by monitoring Mg II/Mg I emission ratios, is also employed as a reflection of potential perturbations in microplasma energetics across the various operation conditions and sample loadings. While truly a miniaturized source (laser ablation sample introduction.

  15. Characterization of Atmospheric Pressure Plasma Jet (APPJ) and Its Effect on Plasmid DNA

    Science.gov (United States)

    Adhikari, Ek; Ptasinska, Sylwia

    2015-09-01

    A helium atmospheric pressure plasma jet (APPJ) source was constructed and then characterized by monitoring a deflected current on a high voltage electrode and a potential difference between two electrodes. The deflected current was also monitored for the APPJ source with varied electrical and fed gas composition e.g. admixtures of He and water vapor. The deflected power per cycle for gas admixtures was decreased with the increase in fraction of water vapor. In addition, this APPJ source was used to induce damage to aqueous plasmid DNA. The fraction of supercoiled, single-strand breaks and double-strand breaks in DNA were quantified by using agarose gel electrophoresis. The number of DNA strand breaks increased as a function of plasma irradiation time and decrease as a distance between APPJ and DNA sample increased. The APPJ with the gas admixture, in which the fraction of water vapor was varied, was also used to induce damage to aqueous DNA samples. The damage level decreased with the increase in a fraction of water vapor under specific experimental conditions. The change in numbers of DNA strand breaks irradiated by a pure He plasma and a plasma with a gas admixture is predicted by different physical and chemical process in the APPJ. This material is based upon work supported by the U.S. Department of Energy Office of Science, Office of Basic Energy Sciences under Award Number DE-FC02-04ER15533.

  16. Inactivation of Gram-positive biofilms by low-temperature plasma jet at atmospheric pressure

    Science.gov (United States)

    Marchal, F.; Robert, H.; Merbahi, N.; Fontagné-Faucher, C.; Yousfi, M.; Romain, C. E.; Eichwald, O.; Rondel, C.; Gabriel, B.

    2012-08-01

    This work is devoted to the evaluation of the efficiency of a new low-temperature plasma jet driven in ambient air by a dc-corona discharge to inactivate adherent cells and biofilms of Gram-positive bacteria. The selected microorganisms were lactic acid bacteria, a Weissella confusa strain which has the particularity to excrete a polysaccharide polymer (dextran) when sucrose is present. Both adherent cells and biofilms were treated with the low-temperature plasma jet for different exposure times. The antimicrobial efficiency of the plasma was tested against adherent cells and 48 h-old biofilms grown with or without sucrose. Bacterial survival was estimated using both colony-forming unit counts and fluorescence-based assays for bacterial cell viability. The experiments show the ability of the low-temperature plasma jet at atmospheric pressure to inactivate the bacteria. An increased resistance of bacteria embedded within biofilms is clearly observed. The resistance is also significantly higher with biofilm in the presence of sucrose, which indicates that dextran could play a protective role.

  17. Characteristics of atmospheric pressure plasma jets emerging into ambient air and helium

    International Nuclear Information System (INIS)

    Zhu Wenchao; Li Qing; Zhu Ximing; Pu Yikang

    2009-01-01

    An investigation of atmospheric pressure helium plasma jets emerging into ambient air and helium was carried out with the aim of shedding light on the mechanism for the formation of extended plasma plumes. By electron multiplying charge coupled device imaging, it is shown that the geometrical shape of the jet in ambient helium is not an arrow-like shape as that in ambient air, but a diffusive one. In ambient helium, the jet length increased continuously with the applied voltage. For ambient air, the jet length was determined by both the helium flow rate and the applied voltage. In addition, the N 2 (C-B) band and the N 2 + lines dominate the emission spectra of the jet in ambient air. The Penning ionization between metastable He atoms and N 2 molecular may be the main source of N 2 + . (fast track communication)

  18. Gas mixing enhanced by power modulations in atmospheric pressure microwave plasma jet

    Science.gov (United States)

    Voráč, J.; Potočňáková, L.; Synek, P.; Hnilica, J.; Kudrle, V.

    2016-04-01

    Microwave plasma jet operating in atmospheric pressure argon was power modulated by audio frequency sine envelope in the 102 W power range. Its effluent was imaged using interference filters and ICCD camera for several different phases of the modulating signal. The combination of this fast imaging with spatially resolved optical emission spectroscopy provides useful insights into the plasmachemical processes involved. Phase-resolved schlieren photography was performed to visualize the gas dynamics. The results show that for higher modulation frequencies the plasma chemistry is strongly influenced by formation of transient flow perturbation resembling a vortex during each period. The perturbation formation and speed are strongly influenced by the frequency and power variations while they depend only weakly on the working gas flow rate. From application point of view, the perturbation presence significantly broadened lateral distribution of active species, effectively increasing cross-sectional area suitable for applications.

  19. Counter-propagating streamers in an atmospheric-pressure helium plasma jet

    Science.gov (United States)

    Hasan, M. I.; Cvelbar, U.; Bradley, J. W.; Walsh, J. L.

    2017-05-01

    This study explores an atmospheric pressure plasma jet impinging on a downstream dielectric surface using a 2D numerical plasma fluid model. It is demonstrated that a counter-propagating discharge ignites at the exposed dielectric surface when the discharge is ignited using negative polarity voltage pulses with fall times in the microsecond range. Two distinct streamer discharges are created, a cathode-directed streamer propagating upstream toward the cathode, and an anode-directed streamer propagating parallel to the dielectric surface facing the gas flow. The surface discharge propagating parallel to the dielectric surface deposits negative surface charge. It is also shown that driving an APPJ with a negative applied potential significantly increases the \\text{O}\\text{2}- time-averaged flux to the dielectric surface while decreasing the \\text{O}\\text{2}+ time-averaged flux.

  20. A model for plasma modification of polypropylene using atmospheric pressure discharges

    CERN Document Server

    Dorai, R

    2003-01-01

    Atmospheric pressure plasmas are commonly used to improve the wetting and adhesion properties of polymers. In spite of their use, the mechanisms for achieving these properties are unclear. In this regard, we report on a computational investigation of the gas phase and surface kinetics during humid-air corona treatment of polypropylene (PP) and the resulting modification of its surface properties while varying energy deposition, relative humidity (RH), web speed, and gas temperature. Using results from a global plasma chemistry model validated against experiments, we found that increasing energy deposition increased the densities of alcohol, carbonyl, acid, and peroxy radicals on the PP surface. In doing so, significant amounts of gas phase O sub 3 and N sub x O sub y are produced. Increasing the RH increased the production of peroxy and acid groups, while decreasing those of alcohol and carbonyl groups. Production of O sub 3 decreased while that of HNO sub 3 increased. Increasing the temperature decreased the...

  1. Reel-to-Reel Atmospheric Pressure Dielectric Barrier Discharge (DBD Plasma Treatment of Polypropylene Films

    Directory of Open Access Journals (Sweden)

    Lukas JW Seidelmann

    2017-03-01

    Full Text Available Atmospheric pressure plasma treatment of the surface of a polypropylene film can significantly increase its surface energy and, thereby improve the printability of the film. A laboratory-scale dielectric barrier discharge (DBD system has therefore been developed, which simulates the electrode configuration and reel-to-reel web transport mechanism used in a typical industrial-scale system. By treating the polypropylene in a nitrogen discharge, we have shown that the water contact angle could be reduced by as much as 40° compared to the untreated film, corresponding to an increase in surface energy of 14 mNm−1. Ink pull-off tests showed that the DBD plasma treatment resulted in excellent adhesion of solvent-based inks to the polypropylene film.

  2. Atmospheric-pressure plasma jet system for silicon etching without fluorocarbon gas feed

    Science.gov (United States)

    Ohtsu, Yasunori; Nagamatsu, Kenta

    2018-01-01

    We developed an atmospheric-pressure plasma jet (APPJ) system with a tungsten rod electrode coated with C2F4 particles of approximately 0.3 µm diameter for the surface treatment of a silicon wafer. The APPJ was generated by dielectric barrier discharge with a driving frequency of 22 kHz using a He gas flow. The characteristics of the APPJ were examined under various experimental conditions. The plasma jet length increased proportionally to the electric field. It was found that the treatment area of the silicon wafer was approximately 1 mm in diameter. By atomic force microscopy analysis, minute irregularities with a maximum length of about 600 nm and part of a ring-shaped trench were observed. A Si etching rate of approximately 400 nm/min was attained at a low power of 6 W and a He flow rate of 1 L/min without introducing molecular gas including F atoms.

  3. Fish oil affects blood pressure and the plasma lipid profile in healthy Danish infants

    DEFF Research Database (Denmark)

    Damsgaard, C.T.; Schack-Nielsen, L.; Michaelsen, K.F.

    2006-01-01

    with an oscillometric device, and blood was sampled for analysis of erythrocyte fatty acid composition and the plasma lipid profile. This paper examines the effects of the fish oil supplement, with adjustment for the effects of the milk intervention when relevant. The fish oil intervention increased erythrocyte (n-3.......04) than infants not administered fish oil. Plasma triacylglycerol was inversely associated with the erythrocyte content of eicosapentaenoic acid (r = 0.34, P dose. The observed effects of fish oil are in accordance with findings in adults. The long-term health implications......Animal and epidemiologic studies indicate that early nutrition has lasting effects on metabolism and cardiovascular disease risk. In adults, (n-3) long-chain PUFA (LCPUFA) from fish oils improve blood pressure, the lipid profile, and possibly cardiovascular disease mortality. This randomized trial...

  4. Parametric Study of Effects of Atmospheric Pressure Plasma Treatment on the Wettability of Cotton Fabric

    Directory of Open Access Journals (Sweden)

    Chi-Wai Kan

    2018-02-01

    Full Text Available In textiles processing, wettability of fabric plays a very important role in enhancing processes such as dyeing and printing. Although well-prepared cotton fabric has very good wettability, further enhancement of its wettability can effectively improve the subsequent dyeing and printing processes. Plasma treatment, especially atmospheric pressure plasma treatment (APPT, a continuous process, is now drawing attention of the industry. In this study, we investigated the effect of APPT under four operational parameters: (1 discharge power; (2 flow rate of oxygen; (3 jet travelling speed; and (4 jet-to-substrate distance on wettability (in terms of wickability and wetting area of cotton fabric. Experimental results revealed that the four parameters interact with each other in affecting the wettability of the cotton fabric. The results are discussed comprehensively.

  5. Langmuir probe diagnostics of an atmospheric pressure, vortex-stabilized nitrogen plasma jet

    Energy Technology Data Exchange (ETDEWEB)

    Prevosto, L.; Mancinelli, B. R. [Grupo de Descargas Electricas, Departamento Ingenieria Electromecanica, Facultad Regional Venado Tuerto (UTN), Laprida 651, (2600) Venado Tuerto, Santa Fe (Argentina); Kelly, H. [Grupo de Descargas Electricas, Departamento Ingenieria Electromecanica, Facultad Regional Venado Tuerto (UTN), Laprida 651, (2600) Venado Tuerto, Santa Fe (Argentina) and Instituto de Fisica del Plasma (CONICET), Departamento de Fisica, Facultad de Ciencias Exactas y Naturales UBA Ciudad Universitaria Pab. I, (1428) Buenos Aires (Argentina)

    2012-09-15

    Langmuir probe measurements in an atmospheric pressure direct current (dc) plasma jet are reported. Sweeping probes were used. The experiment was carried out using a dc non-transferred arc torch with a rod-type cathode and an anode of 5 mm diameter. The torch was operated at a nominal power level of 15 kW with a nitrogen flow rate of 25 Nl min{sup -1}. A flat ion saturation region was found in the current-voltage curve of the probe. The ion saturation current to a cylindrical probe in a high-pressure non local thermal equilibrium (LTE) plasma was modeled. Thermal effects and ionization/recombination processes inside the probe perturbed region were taken into account. Averaged radial profiles of the electron and heavy particle temperatures as well as the electron density were obtained. An electron temperature around 11 000 K, a heavy particle temperature around 9500 K and an electron density of about 4 Multiplication-Sign 10{sup 22} m{sup -3}, were found at the jet centre at 3.5 mm downstream from the torch exit. Large deviations from kinetic equilibrium were found throughout the plasma jet. The electron and heavy particle temperature profiles showed good agreement with those reported in the literature by using spectroscopic techniques. It was also found that the temperature radial profile based on LTE was very close to that of the electrons. The calculations have shown that this method is particularly useful for studying spraying-type plasma jets characterized by electron temperatures in the range 9000-14 000 K.

  6. Polydiagnostic calibration performed on a low pressure surface wave sustained argon plasma

    Science.gov (United States)

    de Vries, N.; Palomares, J. M.; Iordanova, E. I.; van Veldhuizen, E. M.; van der Mullen, J. J. A. M.

    2008-10-01

    The electron density and electron temperature of a low pressure surface wave sustained argon plasma have been determined using passive and active (laser) spectroscopic methods simultaneously. In this way the validity of the various techniques is established while the plasma properties are determined more precisely. The electron density, ne, is determined with Thomson scattering (TS), absolute continuum measurements, Stark broadening and an extrapolation of the atomic state distribution function (ASDF). The electron temperature, Te, is obtained using TS and absolute line intensity (ALI) measurements combined with a collisional-radiative (CR) model for argon. At an argon pressure of 15 mbar, the ne values obtained with TS and Stark broadening agree with each other within the error bars and are equal to (4 ± 0.5) × 1019 m-3, whereas the ne value (2 ± 0.5) × 1019 m-3 obtained from the continuum is about 30% lower. This suggests that the used formula and cross-section values for the continuum method have to be reconsidered. The electron density determined by means of extrapolation of the ASDF to the continuum is too high (~1020 m-3). This is most probably related to the fact that the plasma is strongly ionizing so that the extrapolation method is not justified. At 15 mbar, the Te values obtained with TS are equal to 13 400 ± 1100 K while the ALI/CR-model yields an electron temperature that is about 10% lower. It can be concluded that the passive results are in good or fair agreement with the active results. Therefore, the calibrated passive methods can be applied to other plasmas in a similar regime for which active diagnostic techniques cannot be used.

  7. Polydiagnostic calibration performed on a low pressure surface wave sustained argon plasma

    Energy Technology Data Exchange (ETDEWEB)

    Vries, N de; Iordanova, E I; Van Veldhuizen, E M; Mullen, J J A M van der [Department of Applied Physics, Eindhoven University of Technology, PO Box 513, 5600 MB Eindhoven (Netherlands); Palomares, J M [Departamento de Fisica, Universidad de Cordoba, Campus de Rabanales, ed. C-2, 14071 Cordoba (Spain)], E-mail: j.j.a.m.v.d.Mullen@tue.nl

    2008-10-21

    The electron density and electron temperature of a low pressure surface wave sustained argon plasma have been determined using passive and active (laser) spectroscopic methods simultaneously. In this way the validity of the various techniques is established while the plasma properties are determined more precisely. The electron density, n{sub e}, is determined with Thomson scattering (TS), absolute continuum measurements, Stark broadening and an extrapolation of the atomic state distribution function (ASDF). The electron temperature, T{sub e}, is obtained using TS and absolute line intensity (ALI) measurements combined with a collisional-radiative (CR) model for argon. At an argon pressure of 15 mbar, the n{sub e} values obtained with TS and Stark broadening agree with each other within the error bars and are equal to (4 {+-} 0.5) x 10{sup 19} m{sup -3}, whereas the n{sub e} value (2 {+-} 0.5) x 10{sup 19} m{sup -3} obtained from the continuum is about 30% lower. This suggests that the used formula and cross-section values for the continuum method have to be reconsidered. The electron density determined by means of extrapolation of the ASDF to the continuum is too high ({approx}10{sup 20} m{sup -3}). This is most probably related to the fact that the plasma is strongly ionizing so that the extrapolation method is not justified. At 15 mbar, the T{sub e} values obtained with TS are equal to 13 400 {+-} 1100 K while the ALI/CR-model yields an electron temperature that is about 10% lower. It can be concluded that the passive results are in good or fair agreement with the active results. Therefore, the calibrated passive methods can be applied to other plasmas in a similar regime for which active diagnostic techniques cannot be used.

  8. Expansion Rate Measurements at Moderate Pressure of Nonneutral Electron Plasmas in the Electron Diffusion Gauge (EDG) Experiment

    International Nuclear Information System (INIS)

    Morrison, Kyle A.; Davidson, Ronald C.; Paul, Stephen F.; Belli, Emily A.; Chao, Edward H.

    2001-01-01

    Measurements of the expansion rate of pure-electron plasmas have been performed on the Electron Diffusion Gauge (EDG) device at background helium gas pressures in the 5 x 10(superscript -8) Torr to 1 x 10(superscript -5) Torr range, where plasma expansion due to electron-neutral collisions dominates over plasma expansion due to trap asymmetries. It is found that the expansion rate, defined as the time rate of change of the particles' mean-square radius, scales approximately linearly with pressure and inversely as the square of the magnetic field strength in this regime, in agreement with classical predictions

  9. Measurements of Pfirsch-Schlueter current and pressure profile for the high density ECH plasmas in Heliotron DR

    International Nuclear Information System (INIS)

    Morimoto, S.; Yanagi, N.; Nakasuga, M.; Obiki, T.; Iiyoshi, A.; Uo, K.

    1988-01-01

    The Pfirsch-Schlueter current and pressure profiles are estimated from magnetic measurements for high density electron cyclotron heating (ECH) plasmas (n-bar e =(2-3)x10 13 cm -3 , T e0 =200-400 eV, (β) 0 (1-(r/a) 2 ) s , is about two in macroscopically stable plasmas. A fast loss of plasma energy from the centre to the periphery is observed during the onset of the MHD instability. This method of measuring the pressure profile shape is simple and useful for heliotron type devices. (author). 20 refs, 8 figs, 1 tab

  10. Rapid Atmospheric-Pressure-Plasma-Jet Processed Porous Materials for Energy Harvesting and Storage Devices

    Directory of Open Access Journals (Sweden)

    Jian-Zhang Chen

    2015-01-01

    Full Text Available Atmospheric pressure plasma jet (APPJ technology is a versatile technology that has been applied in many energy harvesting and storage devices. This feature article provides an overview of the advances in APPJ technology and its application to solar cells and batteries. The ultrafast APPJ sintering of nanoporous oxides and 3D reduced graphene oxide nanosheets with accompanying optical emission spectroscopy analyses are described in detail. The applications of these nanoporous materials to photoanodes and counter electrodes of dye-sensitized solar cells are described. An ultrashort treatment (1 min on graphite felt electrodes of flow batteries also significantly improves the energy efficiency.

  11. Control, pressure perturbations, displacements, and disruptions in highly elongated tokamak plasmas

    International Nuclear Information System (INIS)

    Marcus, F.B.; Hofmann, F.; Tonetti, G.; Jardin, S.C.; Noll, P.

    1989-06-01

    The control and evolution of highly elongated tokamak plasmas with large growth rates are simulated with the axisymmetric, resistive MHD code TSC in the geometry of the TCV tokamak. Pressure perturbations such as sawteeth and externally programmed displacements create initial velocity perturbations which may be stabilized by low power, rapid response coils inside the passively stabilizing vacuum vessel, together with slower shaping coils outside the vessel. Vertical disruption induced voltages and forces on the rapid coils and vessel are investigated, and a model is proposed for an additional vertical force due to poloidal currents. (author) 6 figs., 1 tab., 26 refs

  12. Atmospheric pressure plasma treatment of glass fibre composite for adhesion improvement

    DEFF Research Database (Denmark)

    Kusano, Yukihiro; Mortensen, H.; Stenum, Bjarne

    2007-01-01

    Glass-fibre-reinforced polyester composite plates were treated with an atmospheric pressure dielectric barrier discharge. Synthetic air was used as the treatment gas. The water contact angle dropped markedly from 84 to 22° after a 2-s treatment, and decreased to 0° when the composite plates were...... treated for more than 30 s. X-Ray photoelectron spectroscopic analysis showed that the contents of aluminium and oxygen on the surface increased with the plasma treatment. The adhesion strength of the 2-s treated surface was comparable to or higher than that achieved by conventional mechanical surface...

  13. Fluctuation-Coupling of Cathode Cavity Pressure and Arc Voltage in a dc Plasma Torch with a Long Inter-Electrode Channel at Reduced Pressure

    International Nuclear Information System (INIS)

    Cao Jin-Wen; Huang He-Ji; Pan Wen-Xia

    2014-01-01

    Fluctuations of cathode cavity pressure and arc voltage are observed experimentally in a dc plasma torch with a long inter-electrode channel. The results show that they have the same frequency of around 4 kHz under typical experimental conditions. The observed phase difference between the pressure and the voltage, which is influenced by the path length between the pressure sensor and the cathode cavity, varies with different input powers. Combined with numerical simulation, the position of the pressure perturbation origin is estimated, and the results show that it is located at 0.01–0.05 m upstream of the inter-electrode channel outlet

  14. Fabrication of Al doped ZnO films using atmospheric pressure cold plasma

    International Nuclear Information System (INIS)

    Suzaki, Yoshifumi; Miyagawa, Hayato; Yamaguchi, Kenzo; Kim, Yoon-Kee

    2012-01-01

    Under atmospheric pressure, homogeneous non-equilibrium cold plasma was generated stably by high voltage pulsed power (1 kV, 20 kHz, 38 W) excitation of a mixture of He and O 2 gases produced by a dielectric barrier discharge setup. By feeding Bis (2 methoxy‐6-methyl‐3, 5-heptanedione) Zn (Zn-MOPD, C 18 H 3 O 6 Zn) and Tris (2-methoxy‐6‐methy l‐3, 5-heptanedione) Al (Al-MOPD, C 27 H 45 O 9 Al) into this plasma with He carrier gas, transparent flat Al-doped ZnO (ZnO:Al) films about 120–240 nm thick were prepared on glass substrates directly under the slit made into the cathode. Deposition rates of the films were about 20–40 nm/min. The concentration of Al was measured by inductively coupled plasma atomic emission spectroscopy. The composition ratio of Al to Zn was 7.8 mol% when the carrier He gas flow rate of Al-MOPD was 30 cm 3 . The average transmittance of all films was more than 85% in the wavelength range from 400 to 800 nm. When the composition ratio of Al/Zn was between 1.1 and 7.8 mol%, the optical band gap of the film increased from 3.28 to 3.40 eV. The resistivity of ZnO:Al film was 2.96 Ω cm at 1.3 mol% of Al/Zn. In addition, the microstructure of the films was studied by X-ray diffraction measurement and field emission scanning electron microscope observation. It was revealed that doped Al is substituted onto the Zn site of the ZnO crystalline structure in ZnO:Al films. - Highlights: ► An atmospheric pressure cold plasma generator generated stable glow discharge. ► We fabricated Al doped ZnO films on glass substrates using cold plasma. ► Al concentration measured by inductively coupled plasma atomic emission spectroscopy. ► The transmission spectrum and the resistivity of the films were measured. ► The microstructure of the films was studied.

  15. Crystalline and amorphous phases in carbon nitride films produced by intense high-pressure plasma

    Energy Technology Data Exchange (ETDEWEB)

    Gurarie, V.N.; Orlov, A.V.; Bursill, L.A.; JuLin, P.; Nugent, K.W.; Chon, J.W.; Prawer, S

    1997-12-31

    Carbon-nitride films are prepared using a high-intensity pulsed plasma deposition technique. A wide range of nitrogen pressure and discharge intensity are used to investigate their effect on the morphology, nitrogen content, structure, bonding, phase composition and mechanical characteristics of the CN films deposited. Increasing the nitrogen pressure from 0.1 atm to 10 atm results in an increase of nitrogen incorporation into CN films to maximum of 45 at %. Under the high-energy density deposition conditions which involve ablation of the quartz substrate the CN films are found to incorporate in excess of 60 at %N. Raman spectra of these films contain sharp peaks characteristic of a distinct crystalline CN phase. TEM diffraction patterns for the films deposited below 1 atm unambiguously show the presence of micron-sized crystals displaying a cubic symmetry. (authors). 12 refs., 4 figs.

  16. Modelling of indium(I) iodide-argon low pressure plasma

    International Nuclear Information System (INIS)

    Ögün, C M; Truong, W; Kaiser, C; Kling, R; Heering, W

    2014-01-01

    A new collisional-radiative model for a mercury-free low pressure plasma based on an indium(I) iodide-argon system is presented. The electron impact cross sections and rate coefficients for ionization, excitation and dissociation, as well as de-excitation, three-body recombination and dissociative recombination, of studied fillings have been calculated. Additionally, the coefficients for free and ambipolar diffusion were determined. The rate balance equations for individual generation and loss processes have been created. Densities of ions, electrons and neutral particles (ground or metastable state) are presented as a function of electron temperature for varied lamp parameters, such as argon buffer gas pressure and cold spot temperature (coldest point of discharge vessel). With the help of the presented model, the line emission coefficients of essential emission lines of indium for given electron temperatures and densities can be predicted. (paper)

  17. Novel diagnostics for direct measurements of radical densities in atmospheric pressure plasma jets

    Science.gov (United States)

    Wagenaars, Erik

    2017-10-01

    Atmospheric-pressure plasma jets (APPJs) are widely studied for potential applications in industry and healthcare, e.g. surface modification of plastics, plasma medicine and photoresist removal. These plasmas can operate in open air, remain at room temperature and still have a non-equilibrium chemistry. Even though the exact mechanisms through which APPJs affect target surfaces remain largely unknown, it is clear that reactive species play a pivotal role in the success of APPJs. Therefore, reactive species diagnostics of APPJs play an important role in further developing our understanding of the plasma chemistry and will enable increases in treatment efficacy. Two-photon Absorption Laser Induced Fluorescence (TALIF) is a well-known technique for the measurement of absolute densities of atomic radicals such as O, N and H. Unfortunately, application of this technique on APPJs that are operating under realistic conditions for applications, i.e. in open air and with complex admixtures, is not straightforward. The highly collisional environment of APPJs means that collisional quenching of the laser-excited state becomes significant and needs to be taken into account. For well-controlled atmospheres and simple admixtures the effect can be estimated using quenching coefficients, however under realistic operating conditions the identity and density of the quenching partners is unknown due to the complexity of the plasma chemistry. I will present a picosecond TALIF diagnostic which uses a sub-nanosecond laser and iCCD camera that allows the measurement of the quenching-affected fluorescence decay rate directly, enabling absolute measurements of O and N density maps in the open-air effluent of an APPJ. The author acknowledges his collaborators at UoY, A. West, J. Bredin, S. Schroeter, K. Niemi, T. Gans, J. Dedrick and D. O'Connell and support from the UK EPSRC (EP/K018388/1 & EP/H003797/1).

  18. Atmospheric pressure He-air plasma jet: Breakdown process and propagation phenomenon

    Energy Technology Data Exchange (ETDEWEB)

    Begum, Asma [Independent University, Bangladesh, School of Engineering and Computer Science, Bashundhara, Dhaka (Bangladesh); Laroussi, Mounir [Old Dominion University, Department of Electrical and Computer Engineering, Norfolk, Virginia (United States); Pervez, Mohammad Rasel [Master Mind College, Department of Physics, Dhanmondi, Dhaka (Bangladesh)

    2013-06-15

    In this paper He-discharge (plasma jet/bullet) in atmospheric pressure air and its progression phenomenon has been studied experimentally using ICCD camera, optical emission spectroscopy (OES) and calibrated dielectric probe measurements. The repetitive nanosecond pulse has applied to a plasma pencil to generate discharge in the helium gas channel. The discharge propagation speed was measured from the ICCD images. The axial electric field distribution in the plasma jet is inferred from the optical emission spectroscopic data and from the probe measurement. The correlation between the jet velocities, jet length with the pulse duration is established. It shows that the plasma jet is not isolated from the input voltage along its propagation path. The discharge propagation speed, the electron density and the local and average electric field distribution along the plasma jet axis predicted from the experimental results are in good agreement with the data predicted by numerical simulation of the streamer propagation presented in different literatures. The ionization phenomenon of the discharge predicts the key ionization parameters, such as speed, peak electric field in the front, and electron density. The maximum local electric field measured by OES is 95 kV/cm at 1.3 cm of the jet axis, and average EF measured by probe is 24 kV/cm at the same place of the jet. The average and local electron density estimated are in the order of 10{sup 11} cm{sup -3} and it reaches to the maximum of 10{sup 12} cm{sup -3}.

  19. Plasma pressure tensor effects on reconnection: Hybrid and Hall-magnetohydrodynamics simulations

    International Nuclear Information System (INIS)

    Yin Lin; Winske, Dan

    2003-01-01

    Collisionless reconnection is studied using two-dimensional (2-D) hybrid (particle ions, massless fluid electrons) and Hall-magnetohydrodynamics (Hall-MHD) simulations. Both use the full electron pressure tensor instead of a localized resistivity in Ohm's law to initiate reconnection; an initial perturbation or boundary driving to the equilibrium is used. The initial configurations include one-dimensional (1-D) and 2-D current sheets both with and without a guide field. Electron dynamics from the two calculations are compared, and overall agreement is found between the calculations in both reconnection rate and global configuration [L. Yin et al., J. Geophys. Res. 106, 10761 (2001)]. It is shown that the electron drifts in the small-transverse-scale fields near the X point cause the electron motion to decouple from the ion motion, and that reconnection occurs due to electron viscous effects contained in the off-diagonal terms of the electron pressure tensor. Comparing the hybrid and Hall-MHD simulations shows that effects of the off-diagonal terms in the ion pressure tensor, i.e., the ion gyro-radius effects, are necessary in order to model correctly the ion out-of-plane motion. It is shown that these effects can be modeled efficiently in a particle Hall-MHD simulation in which particle ions are used in a predictor/corrector manner to implement ion gyro-radius corrections [L. Yin et al., Phys. Plasmas 9, 2575 (2002)]. For modeling reconnection in large systems, a new integrated approach is examined in which Hall-MHD calculations using a full electron pressure tensor model is embedded inside a MHD simulation. The embedded simulation of current sheet thinning and reconnection dynamics in a realistic 2-D magnetotail equilibrium exhibits smooth transitions of plasma and field quantities between the two regions, with small-scale physics represented well in the compressed current sheet and in the near-X-point region

  20. Optical and Structural Properties of ZnO Nanoparticles Synthesized by CO2 Microwave Plasma at Atmospheric Pressure

    OpenAIRE

    Chun, Se Min; Choi, Dae Hyun; Park, Jong Bae; Hong, Yong Cheol

    2014-01-01

    The results of carbon-doped zinc oxide nanoparticles synthesized by CO2 microwave plasma at atmospheric pressure are presented. The 2.45-GHz microwave plasma torch and feeder for injecting Zn granules are used in the synthesis of zinc oxide nanoparticles. The Zn granules (13.5 g/min) were introduced into the microwave plasma by CO2 (5 l/min) swirl gas. The microwave power delivered to the CO2 microwave plasma was 1 kW. The synthesis of carbon-doped zinc oxide nanoparticles was carried out in ...

  1. Magnetic diagnostics: general principles and the problem of reconstruction of plasma current and pressure profiles in toroidal systems

    International Nuclear Information System (INIS)

    Pustovitov, V.D.

    2000-04-01

    The restrictions of the magnetic diagnostics are discussed. Being related to the integral nature of the measurable quantities, they follow from the fundamental laws of electromagnetism. A series of particular examples demonstrating the strength of these restrictions is given and analyzed. A general rule is emphasized that the information obtained from external magnetic measurements is obviously insufficient for the reliable evaluation of plasma current and pressure profiles in tokamaks or in stellarators. The underlying reason is that outside the plasma the own field of the equilibrium plasma currents is determined by the boundary conditions on the plasma surface only. (author)

  2. The multipole resonance probe: A concept for simultaneous determination of plasma density, electron temperature, and collision rate in low-pressure plasmas

    International Nuclear Information System (INIS)

    Lapke, M.; Mussenbrock, T.; Brinkmann, R. P.

    2008-01-01

    A diagnostic concept is presented which enables the simultaneous determination of plasma density, electron temperature, and collision rate in low-pressure gas discharges. The proposed method utilizes a radio-frequency driven probe of particular spherical design which is immersed in the plasma to excite a family of spatially bounded surface resonances. An analysis of the measured absorption spectrum S(ω) of the probe provides information on the distribution of the plasma in its vicinity, from which the values of the plasma parameters can be inferred. In its simplest realization, the probe consists of two dielectrically shielded, conducting hemispheres, which are symmetrically driven by an radio-frequency source, and the excited resonances can be classified as multipole fields, which allows an analytical evaluation of the measured signal. The proposed method is robust, calibration free, economical, and can be used for ideal and reactive plasmas alike

  3. Plasma assisted measurements of alkali metal concentrations in pressurized combustion processes

    Energy Technology Data Exchange (ETDEWEB)

    Hernberg, R.; Haeyrinen, V. [Tampere Univ. of Technology (Finland). Dept. of Physics

    1996-12-01

    The plasma assisted method for continuous measurement of alkali concentrations in product gas flows of pressurized energy processes will be tested and applied at the 1.6 MW PFBC/G facility at Delft University of Technology in the Netherlands. During the reporting period the alkali measuring device has been tested under pressurized conditions at VTT Energy, DMT, Foster-Wheeler Energia and ABB Carbon. Measurements in Delft will be performed during 1996 after installation of the hot gas filter. The original plan for measurements in Delft has been postponed due to schedule delays in Delft. The results are expected to give information about the influence of different process conditions on the generation of alkali vapours, the comparison of different methods for alkali measurement and the specific performance of our system. This will be the first test of the plasma assisted measurement method in a gasification process. The project belongs to the Joule II extension program under contract JOU2-CT93-0431. (author)

  4. The role of magnetic energy on plasma localization during the glow discharge under reduced pressure

    Directory of Open Access Journals (Sweden)

    Chodun Rafal

    2016-06-01

    Full Text Available In this work, we present the first results of our research on the synergy of fields, electric and magnetic, in the initiation and development of glow discharge under reduced pressure. In the two-electrode system under reduced pressure, the breakdown voltage characterizes a minimum energy input of the electric field to initiate and sustain the glow discharge. The glow discharge enhanced by the magnetic field applied just above the surface of the cathode influences the breakdown voltage decreasing its value. The idea of the experiment was to verify whether the contribution of potential energy of the magnetic field applied around the cathode is sufficiently effective to locate the plasma of glow discharge to the grounded cathode, which, in fact, is the part of a vacuum chamber wall (the anode is positively biased in this case. In our studies, we used the grounded magnetron unit with positively biased anode in order to achieve favorable conditions for the deposition of thin films on fibrous substrates such as fabrics for metallization, assuming that locally applied magnetic field can effectively locate plasma. The results of our studies (Paschen curve with the participation of the magnetic field seem to confirm the validity of the research assumption. What is the most spectacular - the glow discharge was initiated between introduced into the chamber anode and the grounded cathode of magnetron ‘assisted’ by the magnetic field (discharge did not include the area of the anode, which is a part of the magnetron construction.

  5. Bullet-shaped ionization front of plasma jet plumes driven by microwave pulses at atmospheric gas pressure

    Science.gov (United States)

    Chen, Zhaoquan; Xia, Guangqing; Zou, Changlin; Liu, Xiaodong; Feng, Deren; Li, Ping; Hu, Yelin; Stepanova, Olga; Kudryavtsev, A. A.

    2017-09-01

    Ionization waves (propagating bullet-shaped plasma) are always present in atmospheric-pressure plasma jets generated by a pulsed DC power supply or low-frequency voltages. Nevertheless, whether these ionization waves exist for pulsed microwave plasma jets remains unclear. In this paper, a coaxial transmission line resonator driven by microwave pulses is capable of generating atmospheric pressure plasma jet plumes. Depending on the discharges, these plasma jet plumes exhibit distinctive characteristics, such as bullet-shaped ionization fronts for argon plasma and ball-shaped for helium plasma. Fast images show argon plasma plumes generating several small branches but only one dominant ionization front travels more distance along the jet axis. Both ionization-wave images and electromagnetic simulation results indicate that the bullet-shaped ionization front forms a plasma jet plume immediately. The dominant ionization wave is resonantly excited by the local enhanced electric field, which originates from the local net charge of the streamer plus surface plasmon polariton located at the open end of the resonator.

  6. Pressure-controlled nucleation and growth in Zr41Ti14Cu12.5Ni10Be22.5 bulk metallic glass close to and beyond glass transition temperature

    International Nuclear Information System (INIS)

    Pan Mingxiang; Yao Yushu; Zhao Deqian; Zhuang Yanxin; Wang Weihua

    2002-01-01

    By high-pressure annealing close to and beyond glass transition temperature, the behavior of nucleation and growth of crystals in Zr 41 Ti 14 Cu 12.5 Ni 10 Be 22.5 bulk metallic glass (BMG) is investigated. The experimental results indicate that exerting a high pressure during annealing can markedly decrease the nucleation temperature of the BMG. The growth rate of crystals first increases and then decreases with increase of annealing pressure. The effect of pressure on nucleation and growth of crystals is phenomenologically explained

  7. Stability study of polyacrylic acid films plasma-polymerized on polypropylene substrates at medium pressure

    Energy Technology Data Exchange (ETDEWEB)

    Morent, Rino, E-mail: Rino.Morent@Ugent.be [Department of Applied Physics, Research Unit Plasma Technology, Faculty of Engineering, Ghent University, Jozef Plateaustraat 22, 9000 Ghent (Belgium); De Geyter, Nathalie [Department of Applied Physics, Research Unit Plasma Technology, Faculty of Engineering, Ghent University, Jozef Plateaustraat 22, 9000 Ghent (Belgium); Trentesaux, Martine; Gengembre, Leon [Unite de Catalyse et Chimie du Solide, UMR CNRS 8181, Universite des Sciences et Technologies de Lille, Bat. C3, Cite Scientifique, 59655 Villeneuve d' Ascq (France); Dubruel, Peter [Department of Organic Chemistry, Polymer Chemistry and Biomaterials Research Group, Faculty of Sciences, Ghent University, Krijgslaan 281, 9000 Ghent (Belgium); Leys, Christophe [Department of Applied Physics, Research Unit Plasma Technology, Faculty of Engineering, Ghent University, Jozef Plateaustraat 22, 9000 Ghent (Belgium); Payen, Edmond [Unite de Catalyse et Chimie du Solide, UMR CNRS 8181, Universite des Sciences et Technologies de Lille, Bat. C3, Cite Scientifique, 59655 Villeneuve d' Ascq (France)

    2010-11-01

    Plasma polymerization of acrylic acid has become an interesting research subject, since these coatings are expected to be beneficial for biomedical applications due to their high surface density of carboxylic acid functional groups. However, the application of these monomers is counteracted by their low stability in humid environments, since a high stability is a required characteristic for almost any biological application. The present work investigates whether it is possible to obtain stable deposits with a high retention of carboxylic acid functions by performing plasma polymerization on polypropylene substrates with a dielectric barrier discharge operating at medium pressure. In order to obtain coatings with the desired properties, the plasma parameters need to be optimized. Therefore, in this paper, the influence of discharge power and location of the substrate in the discharge chamber is examined in detail. The properties of the deposited films are studied using contact angle measurements, X-ray photoelectron spectroscopy, atomic force microscopy and Fourier transform infrared spectroscopy. Moreover, to determine whether the obtained deposits are soluble in water, the coatings are once again analyzed after rinsing in water. This paper will clearly show that stable COOH-rich surfaces can be obtained at high discharge power and close to the monomer inlet, which might open perspectives for future biomedical applications.

  8. A radio-frequency nonequilibrium atmospheric pressure plasma operating with argon and oxygen

    International Nuclear Information System (INIS)

    Moravej, M.; Yang, X.; Hicks, R.F.; Penelon, J.; Babayan, S.E.

    2006-01-01

    A capacitively coupled, atmospheric pressure plasma has been developed that produces a high concentration of reactive species at a gas temperature below 300 deg. C. The concentration of ground-state oxygen atoms produced by the discharge was measured by NO titration, and found to equal 1.2 vol %, or 1.2±0.4x10 17 cm -3 , using 6.0 vol % O 2 in argon at 150 W/cm 3 . The ozone concentration determined at the same conditions was 4.3±0.5x10 14 cm -3 . A model of the gas phase reactions was developed and yielded O atom and O 3 concentrations in agreement with experiment. This plasma source etched Kapton registered at 5.0 μm/s at 280 deg. C and an electrode-to-sample spacing of 1.5 cm. This fast etch rate is attributed to the high O atom flux generated by the plasma source

  9. Spectroscopic study of atmospheric pressure 915 MHz microwave plasma at high argon flow rate

    International Nuclear Information System (INIS)

    Miotk, R; Hrycak, B; Jasinski, M; Mizeraczyk, J

    2012-01-01

    In this paper results of optical emission spectroscopic (OES) study of atmospheric pressure microwave 915 MHz argon plasma are presented. The plasma was generated in microwave plasma source (MPS) cavity-resonant type. The aim of research was determination of electron excitation temperature T exc gas temperature Tg and electron number density n e . All experimental tests were performed with a gas flow rate of 100 and 200 l/min and absorbed microwave power PA from 0.25 to 0.9 kW. The emission spectra at the range of 300 – 600 nm were recorded. Boltzmann plot method for argon 5p – 4s and 5d – 4p transition lines allowed to determine T exc at level of 7000 K. Gas temperature was determined by comparing the measured and simulated spectra using LIFBASE program and by analyzing intensities of two groups of unresolved rotational lines of the OH band. Gas temperature ranged 600 – 800 K. The electron number density was determined using the method based on the Stark broadening of hydrogen H β line. The measured n e rang ed 2 × 10 15 − 3.5×10 15 cm −3 , depending on the absorbed microwave power. The described MPS works very stable with various working gases at high flow rates, that makes it an attractive tool for different gas processing.

  10. Decomposition of water-insoluble organic waste by water plasma at atmospheric pressure

    International Nuclear Information System (INIS)

    Choi, S; Watanabe, T

    2012-01-01

    The water plasma was generated in atmospheric pressure with the emulsion state of 1-decanol which is a source of soil and ground water pollution. In order to investigate effects of operating conditions on the decomposition of 1-decanol, generated gas and liquid from the water plasma treatment were analysed in different arc current and 1-decanol concentration. The 1-decanol was completely decomposed generating hydrogen, carbon monoxide, carbon dioxide, methane, treated liquid and solid carbon in all experimental conditions. The feeding rate of 1- decanol emulsion was increased with increasing the arc current in virtue of enhanced input power. The generation rate of gas and the ratio of carbon dioxide to carbon monoxide were increased in the high arc current, while the generation rate of solid carbon was decreased due to enhanced oxygen radicals in the high input power. Generation rates of gas and solid carbon were increased at the same time with increasing the concentration of 1-decanol, because carbon radicals were increased without enhancement of oxygen radicals in a constant power level. In addition, the ratio of carbon dioxide to carbon monoxide was increased along with the concentration of 1-decanol due to enhanced carbon radicals in the water plasma flame.

  11. Causes of plasma column contraction in surface-wave-driven discharges in argon at atmospheric pressure

    Science.gov (United States)

    Ridenti, Marco Antonio; de Amorim, Jayr; Dal Pino, Arnaldo; Guerra, Vasco; Petrov, George

    2018-01-01

    In this work we compute the main features of a surface-wave-driven plasma in argon at atmospheric pressure in view of a better understanding of the contraction phenomenon. We include the detailed chemical kinetics dynamics of Ar and solve the mass conservation equations of the relevant neutral excited and charged species. The gas temperature radial profile is calculated by means of the thermal diffusion equation. The electric field radial profile is calculated directly from the numerical solution of the Maxwell equations assuming the surface wave to be propagating in the TM00 mode. The problem is considered to be radially symmetrical, the axial variations are neglected, and the equations are solved in a self-consistent fashion. We probe the model results considering three scenarios: (i) the electron energy distribution function (EEDF) is calculated by means of the Boltzmann equation; (ii) the EEDF is considered to be Maxwellian; (iii) the dissociative recombination is excluded from the chemical kinetics dynamics, but the nonequilibrium EEDF is preserved. From this analysis, the dissociative recombination is shown to be the leading mechanism in the constriction of surface-wave plasmas. The results are compared with mass spectrometry measurements of the radial density profile of the ions Ar+ and Ar2+. An explanation is proposed for the trends seen by Thomson scattering diagnostics that shows a substantial increase of electron temperature towards the plasma borders where the electron density is small.

  12. Cell treatment and surface functionalization using a miniature atmospheric pressure glow discharge plasma torch

    International Nuclear Information System (INIS)

    Yonson, S; Coulombe, S; Leveille, V; Leask, R L

    2006-01-01

    A miniature atmospheric pressure glow discharge plasma torch was used to detach cells from a polystyrene Petri dish. The detached cells were successfully transplanted to a second dish and a proliferation assay showed the transplanted cells continued to grow. Propidium iodide diffused into the cells, suggesting that the cell membrane had been permeabilized, yet the cells remained viable 24 h after treatment. In separate experiments, hydrophobic, bacteriological grade polystyrene Petri dishes were functionalized. The plasma treatment reduced the contact angle from 93 0 to 35 0 , and promoted cell adhesion. Two different torch nozzles, 500 μm and 150 μm in internal diameter, were used in the surface functionalization experiments. The width of the tracks functionalized by the torch, as visualized by cell adhesion, was approximately twice the inside diameter of the nozzle. These results indicate that the miniature plasma torch could be used in biological micropatterning, as it does not use chemicals like the present photolithographic techniques. Due to its small size and manouvrability, the torch also has the ability to pattern complex 3D surfaces

  13. Dealcoholized red wine decreases systolic and diastolic blood pressure and increases plasma nitric oxide: short communication.

    Science.gov (United States)

    Chiva-Blanch, Gemma; Urpi-Sarda, Mireia; Ros, Emilio; Arranz, Sara; Valderas-Martínez, Palmira; Casas, Rosa; Sacanella, Emilio; Llorach, Rafael; Lamuela-Raventos, Rosa M; Andres-Lacueva, Cristina; Estruch, Ramon

    2012-09-28

    Experimental studies have shown a potential blood pressure (BP) lowering effect of red wine polyphenols, whereas the effects of ethanol and polyphenols on BP in humans are not yet clear. The aim of the present work was to evaluate the effects of red wine fractions (alcoholic and nonalcoholic) on BP and plasma nitric oxide (NO) in subjects at high cardiovascular risk. Sixty-seven men at high cardiovascular risk were studied. After a 2-week run-in period, subjects were randomized into 3 treatment periods in a crossover clinical trial, with a common background diet plus red wine (30g alcohol/day), the equivalent amount of dealcoholized red wine, or gin (30g alcohol/day), lasting 4 weeks each intervention. At baseline and after each intervention, anthropometrical parameters, BP and plasma NO were measured. Systolic and diastolic BP decreased significantly after the dealcoholized red wine intervention and these changes correlated with increases in plasma NO. Dealcoholized red wine decreases systolic and diastolic BP. Our results point out through an NO-mediated mechanism. The daily consumption of dealcoholized red wine could be useful for the prevention of low to moderate hypertension. Trial registered at controlled-trials.com: ISRCTN88720134.

  14. Molecular Effects of Atmospheric Pressure Plasma Jet on the Double-Stranded DNA

    Directory of Open Access Journals (Sweden)

    Abasalt Hosseinzadeh Colagar

    2017-03-01

    Full Text Available Introduction The aim of this study was toinvestigate the sterilization potential of atmospheric pressure plasma jet (APPJ and interactions of this technology with double-stranded DNA using the polymerase chain reaction (PCR and single-strand conformation polymorphism (SSCP techniques. Materials and Methods The plasma jet was produced through a high voltage sinusoidal power supplyusing a mixture of argon and oxygen gases with theflow rate of 1 L/min. Escherichia coli cells and double-stranded DNA (dsDNA fragments were amplified by T7 universal primer through the PCR technique and treated with argon/oxygen APPJ at different exposure times. The data were analyzed by the agarose and polyacrylamide gel electrophoresis, SSCP and renewed PCR techniques. Results According to the results of the study, the APPJ could serve as an effective instrument for sterilization at > 30 sec discharge. The destruction of DNA was detectable by different techniques after 120 sec from APPJ discharge. Conclusion Our findings revealed that the active species of plasma can lead to cell death. These species may break or nick the dsDNA, exchange DNA nucleotides, and lead to transition and transversion mutations. These mutagenesis effects of APPJ might be the reason of microorganism cell death after the treatment in addition to other destructive effects of APPJ on macromolecules.

  15. Application of atmospheric-pressure argon plasma jet for bread mold decontamination

    Science.gov (United States)

    Thonglor, P.; Amnuaycheewa, P.

    2017-09-01

    Atmospheric-pressure argon plasma (APAP) is a promising non-thermal technology for microbial control and prevention minimally affecting quality of foods. Effect of APAP jet on the growth of bread molds, including two Aspergillus sp., Rhizopus stolonifer, and Penicillium roqueforti, isolated from white bread were investigated. The molds were isolated, verified, cultured to fully grown on potato dextrose agar (PDA), and subsequently treated with APAP jet using plasma generating power at 24 W for 5, 10, and 20 min, respectively. The inhibition of mold growth was investigated by comparing fungal dry weights and the effect on fungal cell structure was observed using compound light microscope. The results indicated that the 20-min treatment time is most effective in retarding the growth of the three bread molds. However, this level of generating power did not lead to destruction of the cellular structures for all the four fungi. Plasma generating power and treatment time are significant parameters determining the success of bread mold decontamination and further investigation on real bread matrix is needed.

  16. Oxidative modification and electrochemical inactivation of Escherichia coli upon cold atmospheric pressure plasma exposure.

    Directory of Open Access Journals (Sweden)

    Marlène Dezest

    Full Text Available Cold atmospheric pressure plasmas (CAPPs are known to have bactericidal effects but the mechanism of their interaction with microorganisms remains poorly understood. In this study the bacteria Escherichia coli were used as a model and were exposed to CAPPs. Different gas compositions, helium with or without adjunctions of nitrogen or oxygen, were used. Our results indicated that CAPP induced bacterial death at decontamination levels depend on the duration, post-treatment storage and the gas mixture composition used for the treatment. The plasma containing O2 in the feeding gas was the most aggressive and showed faster bactericidal effects. Structural modifications of treated bacteria were observed, especially significant was membrane leakage and morphological changes. Oxidative stress caused by plasma treatment led to significant damage of E. coli. Biochemical analyses of bacterial macromolecules indicated massive intracellular protein oxidation. However, reactive oxygen and nitrogen species (RONS are not the only actors involved in E. coli's death, electrical field and charged particles could play a significant role especially for He-O2 CAPP.

  17. Effects of Background Fluid on the Efficiency of Inactivating Yeast with Non-Thermal Atmospheric Pressure Plasma

    Science.gov (United States)

    Ryu, Young-Hyo; Kim, Yong-Hee; Lee, Jin-Young; Shim, Gun-Bo; Uhm, Han-Sup; Park, Gyungsoon; Choi, Eun Ha

    2013-01-01

    Non-thermal plasma at atmospheric pressure has been actively applied to sterilization. However, its efficiency for inactivating microorganisms often varies depending on microbial species and environments surrounding the microorganisms. We investigated the influence of environmental factors (surrounding media) on the efficiency of microbial inactivation by plasma using an eukaryotic model microbe, Saccharomyces cerevisiae, to elucidate the mechanisms for differential efficiency of sterilization by plasma. Yeast cells treated with plasma in water showed the most severe damage in viability and cell morphology as well as damage to membrane lipids, and genomic DNA. Cells in saline were less damaged compared to those in water, and those in YPD (Yeast extract, Peptone, Dextrose) were least impaired. HOG1 mitogen activated protein kinase was activated in cells exposed to plasma in water and saline. Inactivation of yeast cells in water and saline was due to the acidification of the solutions by plasma, but higher survival of yeast cells treated in saline may have resulted from the additional effect related to salt strength. Levels of hydroxyl radical (OH.) produced by plasma were the highest in water and the lowest in YPD. This may have resulted in differential inactivation of yeast cells in water, saline, and YPD by plasma. Taken together, our data suggest that the surrounding media (environment) can crucially affect the outcomes of yeast cell plasma treatment because plasma modulates vital properties of media, and the toxic nature of plasma can also be altered by the surrounding media. PMID:23799081

  18. Liquid sampling-atmospheric pressure glow discharge as a secondary excitation source: Assessment of plasma characteristics

    International Nuclear Information System (INIS)

    Manard, Benjamin T.; Gonzalez, Jhanis J.; Sarkar, Arnab; Dong, Meirong; Chirinos, Jose; Mao, Xianglei; Russo, Richard E.; Marcus, R. Kenneth

    2014-01-01

    The liquid sampling-atmospheric pressure glow discharge (LS-APGD) has been assessed as a secondary excitation source with a parametric evaluation regarding carrier gas flow rate, applied current, and electrode distance. With this parametric evaluation, plasma optical emission was monitored in order to obtain a fundamental understanding with regards to rotational temperature (T rot ), excitation temperature (T exc ), electron number density (n e ), and plasma robustness. Incentive for these studies is not only for a greater overall fundamental knowledge of the APGD, but also in instrumenting a secondary excitation/ionization source following laser ablation (LA). Rotational temperatures were determined through experimentally fitting of the N 2 and OH molecular emission bands while atomic excitation temperatures were calculated using a Boltzmann distribution of He and Mg atomic lines. The rotational and excitation temperatures were determined to be ∼ 1000 K and ∼ 2700 K respectively. Electron number density was calculated to be on the order of ∼ 3 × 10 15 cm −3 utilizing Stark broadening effects of the Hα line of the Balmer series and a He I transition. In addition, those diagnostics were performed introducing magnesium (by solution feed and laser ablation) into the plasma in order to determine any perturbation under heavy matrix sampling. The so-called plasma robustness factor, derived by monitoring Mg II/Mg I emission ratios, is also employed as a reflection of potential perturbations in microplasma energetics across the various operation conditions and sample loadings. While truly a miniaturized source ( 3 volume), the LS-APGD is shown to be quite robust with plasma characteristics and temperatures being unaffected upon introduction of metal species, whether by liquid or laser ablation sample introduction. - Highlights: • Liquid sampling-atmospheric pressure glow discharge (LS-APGD) • LS-APGD as a secondary excitation source for laser-ablated (LA

  19. Surface conductivity dependent dynamic behaviour of an ultrafine atmospheric pressure plasma jet for microscale surface processing

    Energy Technology Data Exchange (ETDEWEB)

    Abuzairi, Tomy [Graduate School of Science and Technology, Shizuoka University, Hamamatsu 432-8561 (Japan); Department of Electrical Engineering, Faculty of Engineering, Universitas Indonesia, Depok 16424 (Indonesia); Okada, Mitsuru [Department of Engineering, Shizuoka University, Hamamatsu 432-8561 (Japan); Bhattacharjee, Sudeep [Department of Physics, Indian Institute of Technology, Kanpur 208016 (India); Nagatsu, Masaaki, E-mail: nagatsu.masaaki@shizuoka.ac.jp [Graduate School of Science and Technology, Shizuoka University, Hamamatsu 432-8561 (Japan); Department of Engineering, Shizuoka University, Hamamatsu 432-8561 (Japan); Research Institute of Electronics, Shizuoka University, Hamamatsu 432-8561 (Japan)

    2016-12-30

    Highlights: • Spatio-temporal behaviors of capillary APPJs are studied for various substrates. • Plasma irradiation area depended on the substrate conductivity and permittivity. • Surface irradiation area was significantly broadened in polymer-like substrate. • Effect of applying a substrate bias on the APPJ irradiation area was investigated. - Abstract: An experimental study on the dynamic behaviour of microcapillary atmospheric pressure plasma jets (APPJs) with 5 μm tip size for surfaces of different conductivity is reported. Electrical and spatio-temporal characteristics of the APPJs are monitored using high voltage probe, current monitor and high speed intensified charge couple device camera. From these experimental results, we presented a simple model to understand the electrical discharge characteristics of the capillary APPJs with double electrodes, and estimated the velocity of the ionization fronts in the jet and the electron density to be 3.5–4.2 km/s and 2–7 × 10{sup 17} m{sup −3}. By analyzing the dynamics of the microcapillary APPJs for different substrate materials, it was found that the surface irradiation area strongly depended on the substrate conductivity and permittivity, especially in the case of polymer-like substrate, surface irradiation area was significantly broadened probably due to the repelling behaviour of the plasma jets from the accumulated electrical charges on the polymer surface. The effect of applying a substrate bias in the range from −900 V to +900 V on the plasma irradiation onto the substrates was also investigated. From the knowledge of the present results, it is helpful for choosing the substrate materials for microscale surface modification.

  20. Dual effects of atmospheric pressure plasma jet on skin wound healing of mice.

    Science.gov (United States)

    Xu, Gui-Min; Shi, Xing-Min; Cai, Jing-Fen; Chen, Si-Le; Li, Ping; Yao, Cong-Wei; Chang, Zheng-Shi; Zhang, Guan-Jun

    2015-01-01

    Cold plasma has become an attractive tool for promoting wound healing and treating skin diseases. This article presents an atmospheric pressure plasma jet (APPJ) generated in argon gas through dielectric barrier discharge, which was applied to superficial skin wounds in BALB/c mice. The mice (n = 50) were assigned randomly into five groups (named A, B, C, D, E) with 10 animals in each group. Natural wound healing was compared with stimulated wound healing treated daily with APPJ for different time spans (10, 20, 30, 40, and 50 seconds) on 14 consecutive days. APPJ emission spectra, morphological changes in animal wounds, and tissue histological parameters were analyzed. Statistical results revealed that wound size changed over the duration of the experimental period and there was a significant interaction between experimental day and group. Differences between group C and other groups at day 7 were statistically significant (p wounds at day 14. The wounds treated with APPJ for 10, 20, 30, and 40 seconds showed significantly enhanced daily improvement compared with the control and almost complete closure at day 12, 10, 7, and 13, respectively. The optimal results of epidermal cell regeneration, granulation tissue hyperplasia, and collagen deposition in histological aspect were observed at day 7. However, the wounds treated for 50 seconds were less well healed at day 14 than those of the control. It was concluded that appropriate doses of cold plasma could inactivate bacteria around the wound, activate fibroblast proliferation in wound tissue, and eventually promote wound healing. Whereas, over doses of plasma suppressed wound healing due to causing cell death by apoptosis or necrosis. Both positive and negative effects may be related to the existence of reactive oxygen and nitrogen species (ROS and RNS) in APPJ. © 2015 by the Wound Healing Society.

  1. On the induction of homogeneous bulk crystallization in Eu-doped calcium aluminosilicate glass by applying simultaneous high pressure and temperature

    Energy Technology Data Exchange (ETDEWEB)

    Muniz, R. F., E-mail: robsonfmuniz@yahoo.com.br [Institut Lumière Matière, UMR 5306 CNRS-Université Lyon 1, Université de Lyon, 69622 Villeurbanne (France); Departamento de Física, Universidade Estadual de Maringá, 87020900, Maringá, PR (Brazil); Ligny, D. de [Department of Materials Science, Glass and Ceramics, University of Erlangen Nürnberg, Martensstr. 5, 91058 Erlangen (Germany); Le Floch, S.; Martinet, C.; Guyot, Y. [Institut Lumière Matière, UMR 5306 CNRS-Université Lyon 1, Université de Lyon, 69622 Villeurbanne (France); Rohling, J. H.; Medina, A. N.; Sandrini, M.; Baesso, M. L. [Departamento de Física, Universidade Estadual de Maringá, 87020900, Maringá, PR (Brazil); Andrade, L. H. C.; Lima, S. M. [Grupo de Espectroscopia Óptica e Fototérmica, Universidade Estadual de Mato Grosso do Sul, C.P. 351, Dourados, MS (Brazil)

    2016-06-28

    From initial calcium aluminosilicate glass, transparent glass-ceramics have been successfully synthesized under simultaneous high pressure and temperature (SHPT). Possible homogeneous volumetric crystallization of this glassy system, which was not achieved previously by means of conventional heat treatment, has been put in evidence with a SHPT procedure. Structural, mechanical, and optical properties of glass and glass-ceramic obtained were investigated. Raman spectroscopy and X-ray diffraction allowed to identify two main crystalline phases: merwinite [Ca{sub 3}Mg(SiO{sub 4}){sub 2}] and diopside [CaMgSi{sub 2}O{sub 6}]. A Raman scanning profile showed that the formation of merwinite is quite homogeneous over the bulk sample. However, the sample surface also contains significant diopside crystals. Instrumented Berkovich nanoindentation was applied to determine the effect of SHPT on hardness from glass to glass-ceramic. For Eu-doped samples, the broadband emission due to 4f{sup 6}5d{sup 1} → 4f{sup 7} transition of Eu{sup 2+} was studied in both host systems. Additionally, the {sup 5}D{sub 0} → {sup 7}F{sub J} transition of Eu{sup 3+} was used as an environment probe in the pristine glass and the glass-ceramic.

  2. Evidence for plasma phase transition in high pressure hydrogen from ab-initio simulations

    Energy Technology Data Exchange (ETDEWEB)

    Morales, M; Pierleoni, C; Schwegler, E; Ceperley, D

    2010-02-08

    We have performed a detailed study of molecular dissociation in liquid hydrogen using both Born-Oppenheimer molecular dynamics with Density Functional Theory and Coupled Electron-Ion Monte Carlo simulations. We observe a range of densities where (dP/d{rho}){sub T} = 0 that coincides with sharp discontinuities in the electronic conductivity, which is clear evidence of the plasma phase transition for temperatures 600K {le} T {le} 1500K. Both levels of theory exhibit the transition, although Quantum Monte Carlo predicts higher transition pressures. Based on the temperature dependence of the discontinuity in the electronic conductivity, we estimate the critical point of the transition at temperatures slightly below 2000 K. We examine the influence of proton zero point motion by using Path Integral Molecular Dynamics with Density Functional Theory; the main effect is to shift the transition to lower pressures. Furthermore, we calculate the melting curve of molecular hydrogen up to pressures of 200 GPa, finding a reentrant melting line in good agreement with previous calculations. The melting line crosses the metalization line at 700 K and 220 GPa using density functional energetics and at 550 K and 290 GPa using Quantum Monte Carlo energetics.

  3. Atmospheric pressure plasma enhanced chemical vapor deposition of zinc oxide and aluminum zinc oxide

    International Nuclear Information System (INIS)

    Johnson, Kyle W.; Guruvenket, Srinivasan; Sailer, Robert A.; Ahrenkiel, S. Phillip; Schulz, Douglas L.

    2013-01-01

    Zinc oxide (ZnO) and aluminum-doped zinc oxide (AZO) thin films were deposited via atmospheric pressure plasma enhanced chemical vapor deposition. A second-generation precursor, bis(1,1,1,5,5,5-hexafluoro-2,4-pentanedionato)(N,N′-diethylethylenediamine) zinc, exhibited significant vapor pressure and good stability at one atmosphere where a vaporization temperature of 110 °C gave flux ∼ 7 μmol/min. Auger electron spectroscopy confirmed that addition of H 2 O to the carrier gas stream mitigated F contamination giving nearly 1:1 metal:oxide stoichiometries for both ZnO and AZO with little precursor-derived C contamination. ZnO and AZO thin film resistivities ranged from 14 to 28 Ω·cm for the former and 1.1 to 2.7 Ω·cm for the latter. - Highlights: • A second generation precursor was utilized for atmospheric pressure film growth. • Addition of water vapor to the carrier gas stream led to a marked reduction of ZnF 2 . • Carbonaceous contamination from the precursor was minimal

  4. Physical and chemical interactions at the interface between atmospheric pressure plasmas and aqueous solutions

    Science.gov (United States)

    Lindsay, Alexander; Byrns, Brandon; Knappe, Detlef; Graves, David; Shannon, Steven

    2014-10-01

    Transport and reactions of charged species, neutrals, and photons at the interface between plasmas and liquids must be better quantified. The work presented here combines theoretical and experimental investigations of conditions in the gas and liquid phases in proximity to the interface for various discharges. OES is used to determine rotational and vibrational temperatures of OH, NO, and N2+; the relationship between these temperatures that characterize the distribution of internal energy states and gas and electron kinetic temperatures is considered. The deviation of OH rotational states from equilibrium under high humidity conditions is also presented. In contradiction with findings of other groups, high energy rotational states appear to become underpopulated with increasing humidity. In the aqueous phase, concentrations of longer-lived species such as nitrate, nitrite, hydrogen peroxide, and ozone are determined using ion chromatography and colorimetric methods. Spin-traps and electron paramagnetic resonance (EPR) are investigated for characterization of short-lived aqueous radicals like OH, O2-, NO, and ONOO-. Finally, experimental results are compared to a numerical model which couples transport and reactions within and between the bulk gas and liquid phases.

  5. Promotion of adhesive penetration and resin bond strength to dentin using non-thermal atmospheric pressure plasma.

    Science.gov (United States)

    Kim, Jae-Hoon; Han, Geum-Jun; Kim, Chang-Keun; Oh, Kyu-Hwan; Chung, Sung-No; Chun, Bae-Hyeock; Cho, Byeong-Hoon

    2016-02-01

    Non-thermal atmospheric pressure plasmas (NT-APPs) have been shown to improve the bond strength of resin composites to demineralized dentin surfaces. Based on a wet-bonding philosophy, it is believed that a rewetting procedure is necessary after treatment with NT-APP because of its air-drying effect. This study investigated the effect of 'plasma-drying' on the bond strength of an etch-and-rinse adhesive to dentin by comparison with the wet-bonding technique. Dentin surfaces of human third molars were acid-etched and divided into four groups according to the adhesion procedure: wet bonding, plasma-drying, plasma-drying/rewetting, and dry bonding. In plasma treatment groups, the demineralized dentin surfaces were treated with a plasma plume generated using a pencil-type low-power plasma torch. After the adhesion procedures, resin composite/dentin-bonded specimens were subjected to a microtensile bond-strength test. The hybrid layer formation was characterized by micro-Raman spectroscopy and scanning electron microscopy. The plasma-drying group presented significantly higher bond strength than the wet-bonding and dry-bonding groups. Micro-Raman spectral analysis indicated that plasma-drying improved the penetration and polymerization efficacy of the adhesive. Plasma-drying could be a promising method to control the moisture of demineralized dentin surfaces and improve the penetration of adhesive and the mechanical property of the adhesive/dentin interface. © 2015 Eur J Oral Sci.

  6. An experimental study on discharge characteristics in a pulsed-dc atmospheric pressure CH3OH/Ar plasma jet

    Science.gov (United States)

    Qian, Muyang; Liu, Sanqiu; Yang, Congying; Pei, Xuekai; Lu, Xinpei; Zhang, Jialiang; Wang, Dezhen

    2016-10-01

    Recently, C/H/Ar plasma discharges found enormous potential and possibility in carbonaceous compounds conversion and production. In this work, a pulsed-dc CH3OH/Ar plasma jet generated at atmospheric pressure is investigated by means of optical and electrical diagnosis concerning the variation of its basic parameters, absolute concentration of OH radicals, and plasma temperature with different CH3OH/Ar volume ratios, in the core region of discharge with needle-to-ring electrode configuration. The voltage-current characteristics are also measured at different CH3OH/Ar ratios. Laser-induced fluorescence (LIF) results here show that only small amounts of added methanol vapor to argon plasma (about 0.05% CH3OH/Ar volume ratio) is favorable for the production of OH radicals. The optical emission lines of CH, CN, and C2 radicals have been detected in the CH3OH/Ar plasma. And, the plasma temperatures increase with successive amount of added methanol vapor to the growth plasma. Moreover, qualitative discussions are presented regarding the mechanisms for methanol dissociation and effect of the CH3OH component on the Ar plasma discharge at atmospheric pressure.

  7. Investigation of working pressure on the surface roughness controlling technology of glow discharge polymer films based on the diagnosed plasma

    Science.gov (United States)

    Zhang, Ling; Chen, Guo; He, Zhibing; Ai, Xing; Huang, Jinglin; Liu, Lei; Tang, Yongjian; He, Xiaoshan

    2017-07-01

    The effects of working pressure on the component, surface morphology, surface roughness, and deposition rate of glow discharge polymer (GDP) films by a trans-2-butene/hydrogen gas mixture were investigated based on plasma characteristics diagnosis. The composition and ion energy distributions of a multi-carbon (C4H8/H2) plasma mixture at different working pressures were diagnosed by an energy-resolved mass spectrometer (MS) during the GDP film deposition process. The Fourier transform infrared spectroscopy (FT-IR), field emission scanning electron microscope (SEM) and white-light interferometer (WLI) results were obtained to investigate the structure, morphology and roughness characterization of the deposited films, respectively. It was found that the degree of ionization of the C4H8/H2 plasma reduces with an increase in the working pressure. At a low working pressure, the C-H fragments exhibited small-mass and high ion energy in plasma. In this case, the film had a low CH3/CH2 ratio, and displayed a smooth surface without any holes, cracks or asperities. While the working pressure increased to 15 Pa, the largest number of large-mass fragments led to the deposition rate reaching a maximum of 2.11 μm h-1, and to hole defects on the film surface. However, continuing to increase the working pressure, the film surface became smooth again, and the interface between clusters became inconspicuous without etching pits.

  8. Effect of chronic elevation of plasma calcium concentration by PTH or vitamin D3on blood pressure and hypotensive activity of nifedipine in rats

    NARCIS (Netherlands)

    Jonkman, F.A.M.; Thoolen, M.J.M.C.; Wilffert, B.

    1984-01-01

    The influence of a chronically elevated total plasma calcium concentration on blood pressure and heart rate was investigated in conscious normotensive rats. The plasma calcium concentration was elevated by continuous subcutaneous infusion with parathormone (PTH) after parathyreoidectomy, and by oral

  9. Effect of non-thermal air atmospheric pressure plasma jet treatment on gingival wound healing

    Science.gov (United States)

    Lee, Jung-Hwan; Choi, Eun-Ha; Kim, Kwang-Mahn; Kim, Kyoung-Nam

    2016-02-01

    Non-thermal atmospheric pressure plasmas have been applied in the biomedical field for the improvement of various cellular activities. In dentistry, the healing of gingival soft tissue plays an important role in health and aesthetic outcomes. While the biomedical application of plasma has been thoroughly studied in dentistry, a detailed investigation of plasma-mediated human gingival fibroblast (HGF) migration for wound healing and its underlying biological mechanism is still pending. Therefore, the aim of this study is to apply a non-thermal air atmospheric pressure plasma jet (NTAAPPJ) to HGF to measure the migration and to reveal the underlying biological mechanisms involved in the migration. After the characterization of NTAAPPJ by optical emission spectroscopy, the adherent HGF was treated with NTAAPPJ or air with a different flow rate. Cell viability, lipid peroxidation, migration, intracellular reactive oxygen species (ROS), and the expression of migration-related genes (EGFR, PAK1, and MAPK3) were investigated. The level of statistical significance was set at 0.05. NTAAPPJ and air treatment with a flow rate of 250-1000 standard cubic centimetres per minute (sccm) for up to 30 s did not induce significant decreases in cell viability or membrane damage. A significant increase in the migration of mitomycin C-treated HGF was observed after 30 s of NTAAPPJ treatment compared to 30 s air-only treatment, which was induced by high levels of intracellular reactive oxygen species (ROS). An increase in migration-related gene expression and EGFR activation was observed following NTAAPPJ treatment in an air flow rate-dependent manner. This is the first report that NTAAPPJ treatment induces an increase in HGF migration without changing cell viability or causing membrane damage. HGF migration was related to an increase in intracellular ROS, changes in the expression of three of the migration-related genes (EGFR, PAK1, and MAPK1), and EGFR activation. Therefore

  10. Effect of non-thermal air atmospheric pressure plasma jet treatment on gingival wound healing

    International Nuclear Information System (INIS)

    Lee, Jung-Hwan; Choi, Eun-Ha; Kim, Kwang-Mahn; Kim, Kyoung-Nam

    2016-01-01

    Non-thermal atmospheric pressure plasmas have been applied in the biomedical field for the improvement of various cellular activities. In dentistry, the healing of gingival soft tissue plays an important role in health and aesthetic outcomes. While the biomedical application of plasma has been thoroughly studied in dentistry, a detailed investigation of plasma-mediated human gingival fibroblast (HGF) migration for wound healing and its underlying biological mechanism is still pending. Therefore, the aim of this study is to apply a non-thermal air atmospheric pressure plasma jet (NTAAPPJ) to HGF to measure the migration and to reveal the underlying biological mechanisms involved in the migration. After the characterization of NTAAPPJ by optical emission spectroscopy, the adherent HGF was treated with NTAAPPJ or air with a different flow rate. Cell viability, lipid peroxidation, migration, intracellular reactive oxygen species (ROS), and the expression of migration-related genes (EGFR, PAK1, and MAPK3) were investigated. The level of statistical significance was set at 0.05. NTAAPPJ and air treatment with a flow rate of 250–1000 standard cubic centimetres per minute (sccm) for up to 30 s did not induce significant decreases in cell viability or membrane damage. A significant increase in the migration of mitomycin C-treated HGF was observed after 30 s of NTAAPPJ treatment compared to 30 s air-only treatment, which was induced by high levels of intracellular reactive oxygen species (ROS). An increase in migration-related gene expression and EGFR activation was observed following NTAAPPJ treatment in an air flow rate-dependent manner. This is the first report that NTAAPPJ treatment induces an increase in HGF migration without changing cell viability or causing membrane damage. HGF migration was related to an increase in intracellular ROS, changes in the expression of three of the migration-related genes (EGFR, PAK1, and MAPK1), and EGFR activation. Therefore

  11. The influence of electrode configuration on light emission profiles and electrical characteristics of an atmospheric-pressure plasma jet

    Science.gov (United States)

    Maletić, Dejan; Puač, Nevena; Malović, Gordana; Đorđević, Antonije; Petrović, Zoran Lj

    2017-04-01

    In this paper we focus on the influence of the type of electrodes, their dimensions and inter-electrode gap on the formation of a helium plasma jet. Plasma emission profiles are recorded by an ICCD camera simultaneously with volt-ampere characteristics for three different copper electrode configurations. The delivered power was up to 6.5 W, but it may be set and controlled to 0.1 W. This study shows how the electrode configuration shapes and controls temporal and spatial plasma development as well as electrical characteristics of an atmospheric pressure plasma jet. It is shown that, in our system, the width of the grounded electrode has no significant influence on the formation and properties of pulsed atmospheric-pressure streamers (PAPS) outside the tube, while the width of the powered electrode is crucial in their formation.

  12. Plasma treatment of carbon fibres and glass-fibre-reinforced polyesters at atmospheric pressure for adhesion improvement

    DEFF Research Database (Denmark)

    Kusano, Yukihiro; Løgstrup Andersen, Tom; Toftegaard, Helmuth Langmaack

    2014-01-01

    Atmospheric pressure plasma treatment is useful for adhesion improvement, because cleaning, roughening and addition of polar functional groups can be expected at the surfaces. Its possible applications in the wind energy industry include plasma treatment of fibres and fibre-reinforced polymer....... The plasma treatment improved fracture toughness, indicating that adhesion between the fibres and the epoxy was enhanced by the treatment. In addition, glass-fibre-reinforced polyester plates are treated using a gliding arc and an ultrasound enhanced dielectric barrier discharge, improving the wettability...... composites before assembling them to build wind turbine blades. In the present work, unsized carbon fibres are continuously treated using a dielectric barrier discharge plasma in helium at atmospheric pressure, and carbon fibre reinforced epoxy composite plates are manufactured for the mechanical test...

  13. Internal helical modes with m > 1 in a tokamak with a small shear and high plasma pressure

    International Nuclear Information System (INIS)

    Mikha lovskij, A.B.; Aburdzhaniya, G.D.; Krymskij, A.M.

    1979-01-01

    Internal helical modes with m>1 in a circular cross-section tokamak with a small shear and large value of the parameter β (β is the ratio between the mean plasma pressure and the mean pressure of the poloidal magnetic field) are investigated. The equations obtained are used to study the destabilizing effects leading to helical instabilities. The role of destabilizing effects is regarded both in local and in a nonlocal approximations on the assumption that the radial plasma pressure is distributed parabolically and that the radial current distribution is also parabolic though slightly varying. It has been established that the profiling of current may lead to the tokamak plasma stability with respect to the modes under investigation. A tokamak with a small shear has been shown to be more stable relative to these modes than that with a large shear

  14. Probe measurements of electron energy spectrum and plasma-wall interaction in Helium/air micro-plasma at atmospheric pressure

    Science.gov (United States)

    Adams, S. F.; Demidov, V. I.; Hensley, A. L.; Koepke, M. E.; Kurlyandskaya, I. P.; Miles, J. A.; Tolson, B. A.

    2018-02-01

    It is experimentally demonstrated that a wall probe may be a useful instrument for measurement of electron energy spectrum (EES) and the plasma-boundary interaction in a micro-plasma with a nonlocal electron distribution function at atmospheric pressure. The measurements of the EES have been conducted in the plasma of several micro-hollow cathode discharges of differing sizes. The discharges with a flow of Helium gas were exposed to air. Typical results of measurements demonstrate signature of energetic electrons arising due to plasma-chemical reactions. It is experimentally shown that wall probe potential is associated with energetic electrons rather than the ambient electron kinetic energy. The devices may be applicable for developing analytical sensors for extreme environments, including high radiation and high temperatures.

  15. Cold atmospheric-pressure air plasma treatment of C6 glioma cells: effects of reactive oxygen species in the medium produced by the plasma on cell death

    Science.gov (United States)

    Wang, Yuyang; Cheng, Cheng; Gao, Peng; Li, Shaopeng; Shen, Jie; Lan, Yan; Yu, Yongqiang; Chu, Paul K.

    2017-02-01

    An atmospheric-pressure air plasma is employed to treat C6 glioma cells in vitro. To elucidate on the mechanism causing cell death and role of reactive species (RS) in the medium produced by the plasma, the concentration of the long-lived RS such as hydrogen peroxide, nitrate, and ozone in the plasma-treated liquid (phosphate-buffered saline solution) is measured. When vitamin C is added to the medium as a ROS quencher, the viability of C6 glioma cells after the plasma treatment is different from that without vitamin C. The results demonstrate that reactive oxygen species (ROS) such as H2O2, and O3 constitute the main factors for inactivation of C6 glioma cells and the reactive nitrogen species (RNS) may only play an auxiliary role in cell death.

  16. An Alternative to Annealing TiO2 Nanotubes for Morphology Preservation: Atmospheric Pressure Plasma Jet Treatment.

    Science.gov (United States)

    Seo, Sang-Hee; Uhm, Soo-Hyuk; Kwon, Jae-Sung; Choi, Eun Ha; Kim, Kwang-Mahn; Kim, Kyoung-Nam

    2015-03-01

    Titanium oxide nanotube layer formed by plasma electrolytic oxidation (PEO) is known to be excellent in biomaterial applications. However, the annealing process which is commonly performed on the TiO2 nanotubes cause defects in the nanotubular structure. The purpose of this work was to apply a non-thermal atmospheric pressure plasma jet on diameter-controlled TiO2 nanotubes to mimic the effects of annealing while maintaining the tubular structure for use as biomaterial. Diameter-controlled nanotube samples fabricated by plasma electrolytic oxidation were dried and prepared under three different conditions: untreated, annealed at 450 °C for 1 h in air with a heating rate of 10 °C/min, and treated with an air-based non-thermal atmospheric pressure plasma jet for 5 minutes. The contact angle measurement was investigated to confirm the enhanced hydrophilicity of the TiO2 nanotubes. The chemical composition of the surface was studied using X-ray photoelectron spectroscopy, and the morphology of TiO2 nanotubes was examined by field emission scanning electron microscopy. For the viability of the cell, the attachment of the osteoblastic cell line MC3T3-E1 was determined using the water-soluble tetrazolium salt assay. We found that there are no morphological changes in the TiO2 nanotubular structure after the plasma treatment. Also, we investigated a change in the chemical composition and enhanced hydrophilicity which result in improved cell behavior. The results of this study indicated that the non-thermal atmospheric pressure plasma jet results in osteoblast functionality that is comparable to annealed samples while maintaining the tubular structure of the TiO2 nanotubes. Therefore, this study concluded that the use of a non-thermal atmospheric pressure plasma jet on nanotube surfaces may replace the annealing process following plasma electrolytic oxidation.

  17. Tribological Characterization of SiC and B4C Manufactured by Plasma Pressure Compaction

    Science.gov (United States)

    Rubino, Felice; Pisaturo, Mario; Senatore, Adolfo; Carlone, Pierpaolo; Sudarshan, Tirumalai S.

    2017-11-01

    The objective of the present study was to assess the tribological properties and the wear behavior of silicon carbide and boron carbide ceramics, produced by the plasma pressure compaction sintering process. Reciprocating sliding tests were executed to evaluate the tribological behavior of silicon carbide and boron carbide. Samples of each material with distinct values of surface roughness Ra were tested. Wear mass loss, coefficients of friction and wear mechanism of the boron carbide and silicon carbide were evaluated by means of microscopes and an energy-dispersive spectroscopy probe. The coefficient of friction of the evaluated boron carbide was found to be 0.8, and the surface roughness affects only the starting transient, while for silicon carbide the steady-state value ranges from 0.5 to 0.8 depending on the roughness value Ra.

  18. Effects of reactor pressure on two-dimensional radio-frequency methane plasma: a numerical study

    Science.gov (United States)

    Bera, K.; Farouk, B.; Lee, Y. H.

    1999-08-01

    A self-consistent two-dimensional radio-frequency glow discharge model has been developed for methane gas using a fluid model. The objective of the study is to provide insights into charged-species dynamics and investigate their effects on deposition in a polyatomic gas discharge. Swarm data as a function of electron energy are provided as input to the model. The necessary dc bias for the discharge is also predicted consistently such that the cycle-averaged current to the powered electrode becomes zero. The predictions provide a comprehensive understanding of the various processes in methane discharges found in plasma-assisted chemical vapour deposition (PACVD) reactors for the deposition of carbon films. The effects of discharge pressure on discharge variables are identified and presented in the paper.

  19. Study of structural modification of sugarcane bagasse employing hydrothermal treatment followed by atmospheric pressure plasmas treatment

    Science.gov (United States)

    Amorim, Jayr; Pimenta, Maria Teresa; Gurgel, Leandro; Squina, Fabio; Souza-Correa, Jorge; Curvelo, Antonio

    2009-10-01

    Nowadays, the cellulosic ethanol is an important alternative way to many liquid biofuels using renewable biomass rich in polysaccharides. To be used as feedstock for ethanol production, the bagasse needs to be pretreated in order to expose its main constitutive. The present work proposes the use of different pretreatment processes to better expose the cellulose for hydrolysis and fermentation. In the present paper the sugarcane bagasse was submitted to a hydrothermal pretreatment followed by atmospheric pressure plasmas (APPs). An RF microplasma torch was employed as APPs in Ar and Ar/O2 mixing. The bagasse was treated in discharge and post-discharge regions. The position and time of treatment was varied as well as the gas mixture. The quantity of polysaccharides was determined by using high performance liquid chromatography. It was observed the release of a fraction of the hemicelluloses in the sugarcane bagasse. Modifications in the surface of the sugarcane fibers were monitored by employing scanning electron microscopy.

  20. The use of atmospheric pressure plasma as a curing process for canned ground ham.

    Science.gov (United States)

    Lee, Juri; Jo, Kyung; Lim, Yubong; Jeon, Hee Joon; Choe, Jun Ho; Jo, Cheorun; Jung, Samooel

    2018-02-01

    This study investigated the potential use of atmospheric pressure plasma (APP) treatment as a curing process for canned ground ham. APP treatment for 60min while mixing increased the nitrite content in the meat batters from 0.64 to 60.50mgkg -1 while the pH and the total content of aerobic bacteria in the meat batters were unchanged. The canned ground hams cured by the APP treatment for 30min displayed no difference in their physicochemical qualities, such as nitrosyl hemochrome, color, residual nitrite, texture, lipid oxidation, and protein oxidation, compared with those of canned ground hams cured with sodium nitrite or celery powder at 42mgkg -1 of nitrite. The canned ground hams cured by the APP treatment received a higher score in taste and overall acceptability than those cured with sodium nitrite. Canned ground ham can be cured by the APP treatment without nitrite additives. Copyright © 2017 Elsevier Ltd. All rights reserved.

  1. Low pressure water vapour plasma treatment of surfaces for biomolecules decontamination

    DEFF Research Database (Denmark)

    Fumagalli, F; Kylian, O; Amato, Letizia

    2012-01-01

    Decontamination treatments of surfaces are performed on bacterial spores, albumin and brain homogenate used as models of biological contaminations in a low-pressure, inductively coupled plasma reactor operated with water-vapour-based gas mixtures. It is shown that removal of contamination can...... be achieved using pure H2O or Ar/H2O mixtures at low temperatures with removal rates comparable to oxygen-based mixtures. Particle fluxes (Ar+ ions, O and H atomic radicals and OH molecular radicals) from water vapour discharge are measured by optical emission spectroscopy and Langmuir probe under several...... operating conditions. Analysis of particle fluxes and removal rates measurements illustrates the role of ion bombardment associated with O radicals, governing the removal rates of organic matter. Auxiliary role of hydroxyl radicals is discussed on the basis of experimental data. The advantages of a water...

  2. Plasma discharge in N2 + CH4 at low pressures - Experimental results and applications to Titan

    Science.gov (United States)

    Thompson, W. Reid; Henry, Todd J.; Schwartz, Joel M.; Khare, B. N.; Sagan, Carl

    1991-01-01

    Results are reported from laboratory continuous-flow plasma-discharge experiments designed to simulate the formation of hydrocarbons and nitriles from N2 and CH4 in the atmosphere of Titan. Gas-chromatography and mass-spectrometry data were obtained in experiments lasting up to 100 h at temperature 295 K and pressure 17 or 0.24 mbar, modeling (1) cosmic-ray-induced processes in the Titan troposphere and (2) processes related to stratospheric aurorae excited by energetic electrons and ions from the Saturn magnetosphere, respectively. The results are presented in extensive tables and graphs, and the 0.24-mbar yields are incorporated into an eddy-mixing model to give stratospheric column abundances and mole fractions in good agreement with Voyager IRIS observations.

  3. Effects of regional hemoconcentration during LBNP on plasma volume determinations. [Lower Body Negative Pressure

    Science.gov (United States)

    Loeppky, J. A.; Kobayashi, Y.; Venters, M. D.; Luft, U. C.

    1979-01-01

    Blood samples were obtained from forearm vein or artery with indwelling cannula (1) before, (2) during the last min, and (3) about 2 min after lower body negative pressure (LBNP) in 16 experiments to determine whether plasma volume (PV) estimates were affected by regional hemoconcentration in the lower body. Total hemoglobin (THb) was estimated with the CO method prior to LBNP. Hemoglobin (Hb) and hematocrit (Hct) values from (2) gave only a 3% (87 ml) loss in PV due to LBNP, assuming no change in THb. However, Hb and Hct values from (3) showed an 11% loss in PV (313 ml). This 72% underestimation of PV loss with (2) must have resulted from the sequestration of blood and subsequent hemoconcentration in the lower body during LBNP. The effects of LBNP on PV should be estimated 1-3 min after exposure, after mixing but before extravascular fluid returns to the circulation.

  4. Magnetic Ignition of Pulsed Gas Discharges in Air of Low Pressure in a Coaxial Plasma Gun

    Science.gov (United States)

    Thom, Karlheinz; Norwood, Joseph, Jr.

    1961-01-01

    The effect of an axial magnetic field on the breakdown voltage of a coaxial system of electrodes has been investigated by earlier workers. For low values of gas pressure times electrode spacing, the breakdown voltage is decreased by the application of the magnetic field. The electron cyclotron radius now assumes the role held by the mean free path in nonmagnetic discharges and the breakdown voltage becomes a function of the magnetic flux density. In this paper the dependence of the formative time lag as a function of the magnetic flux density is established and the feasibility of using a magnetic field for igniting high-voltage, high-current discharges is shown through theory and experiment. With a 36 microfarad capacitor bank charged to 48,000 volts, a peak current of 1.3 x 10( exp 6) amperes in a coaxial type of plasma gun was achieved with a current rise time of only 2 microseconds.

  5. Fabrication of a Silicon Nanowire on a Bulk Substrate by Use of a Plasma Etching and Total Ionizing Dose Effects on a Gate-All-Around Field-Effect Transistor

    Science.gov (United States)

    Moon, Dong-Il; Han, Jin-Woo; Meyyappan, Meyya

    2016-01-01

    The gate all around transistor is investigated through experiment. The suspended silicon nanowire for the next generation is fabricated on bulk substrate by plasma etching method. The scallop pattern generated by Bosch process is utilized to form a floating silicon nanowire. By combining anisotropic and istropic silicon etch process, the shape of nanowire is accurately controlled. From the suspended nanowire, the gate all around transistor is demonstrated. As the silicon nanowire is fully surrounded by the gate, the device shows excellent electrostatic characteristics.

  6. Tailoring electron energy distribution functions through energy confinement in dual radio-frequency driven atmospheric pressure plasmas

    Energy Technology Data Exchange (ETDEWEB)

    O' Neill, C.; Waskoenig, J. [Centre for Plasma Physics, School of Maths and Physics, Queen' s University Belfast, Belfast BT7 1NN (United Kingdom); Gans, T. [Centre for Plasma Physics, School of Maths and Physics, Queen' s University Belfast, Belfast BT7 1NN (United Kingdom); York Plasma Institute, Department of Physics, University of York, York YO10 5DD (United Kingdom)

    2012-10-08

    A multi-scale numerical model based on hydrodynamic equations with semi-kinetic treatment of electrons is used to investigate the influence of dual frequency excitation on the effective electron energy distribution function (EEDF) in a radio-frequency driven atmospheric pressure plasma. It is found that variations of power density, voltage ratio, and phase relationship provide separate control over the electron density and the mean electron energy. This is exploited to directly influence both the phase dependent and time averaged effective EEDF. This enables tailoring the EEDF for enhanced control of non-equilibrium plasma chemical kinetics at ambient pressure and temperature.

  7. Atmospheric Pressure Plasma Enhanced Spatial ALD of ZrO2 for Low-Temperature, Large-Area Applications

    OpenAIRE

    Mione, M.A.; Katsouras, I.; Creyghton, Y.; Boekel, W. van; Maas, J.; Gelinck, G.; Roozeboom, F.; Illiberi, A.

    2017-01-01

    High permittivity (high-k) materials have received considerable attention as alternatives to SiO2 for CMOS and low-power flexible electronics applications. In this study, we have grown high-quality ZrO2 by using atmospheric-pressure plasma-enhanced spatial ALD (PE-sALD), which, compared to temporal ALD, offers higher effective deposition rates and uses atmospheric-pressure plasma to activate surface reactions at lower temperatures. We used tetrakis(ethylmethylamino)zirconium (TEMAZ) as precur...

  8. Aluminum metal surface cleaning and activation by atmospheric-pressure remote plasma

    Energy Technology Data Exchange (ETDEWEB)

    Muñoz, J., E-mail: jmespadero@uco.es; Bravo, J.A.; Calzada, M.D.

    2017-06-15

    Highlights: • Atmospheric-pressure postdischarges have been applied on aluminium surfaces. • The outer hydrocarbon layer is reduced by the action of the postdischarge. • The treatment promotes the appearance of hydrophilic OH radicals in the surface. • Effectivity for distances up to 5 cm allows for treating irregular surfaces. • Ageing in air due to the disappearance of OH radicals has been reported. - Abstract: The use of the remote plasma (postdischarge) of argon and argon-nitrogen microwave plasmas for cleaning and activating the surface of metallic commercial aluminum samples has been studied. The influence of the nitrogen content and the distance between the treated samples and the end of the discharge on the hydrophilicity and the surface energy has been analyzed by means of the sessile drop technique and the Owens-Wendt method. A significant increase in the hydrophilicity has been noted in the treated samples, together with an increase in the surface energy from values around 37 mJ/m{sup 2} to 77 mJ/m{sup 2}. Such increase weakly depends on the nitrogen content of the discharge, and the effectivity of the treatment extends to distances up to 5 cm from the end of the discharge, much longer than those reported in other plasma-based treatments. The analysis of the treated samples using X-ray photoelectron spectroscopy reveals that such increase in the surface energy takes place due to a reduction of the carbon content and an increase in the amount of OH radicals in the surface. These radicals tend to disappear within 24–48 h after the treatment when the samples are stored in contact with ambient air, resulting in the ageing of the treated surface and a partial retrieval of the hydrophobicity of the surface.

  9. Two-resonance probe for measuring electron density in low-pressure plasmas

    Science.gov (United States)

    Kim, D. W.; You, S. J.; Kim, S. J.; Kim, J. H.; Oh, W. Y.

    2017-04-01

    A technique for measuring double-checked electron density using two types of microwave resonance is presented. Simultaneous measurement of the resonances (plasma and quarter-wavelength resonator resonances), which were used for the cutoff probe (CP) and hairpin probe (HP), was achieved by the proposed microwave resonance probe. The developed two-resonance probe (TRP) consists of parallel separated coaxial cables exposing the radiation and detection tips. The structure resembles that of the CP, except the gapped coaxial cables operate not only as a microwave feeder for the CP but also as a U- shaped quarter-wavelength resonator for the HP. By virtue of this structure, the microwave resonances that have typically been used for measuring the electron density for the CP and HP were clearly identified on the microwave transmission spectrum of the TRP. The two types of resonances were measured experimentally under various power and pressure conditions for the plasma. A three-dimensional full-wave simulation model for the TRP is also presented and used to investigate and reproduce the resonances. The electron densities inferred from the resonances were compared and showed good agreement. Quantitative differences between the densities were attributed to the effects of the sheath width and spatial density gradient on the resonances. This accessible technique of using the TRP to obtain double-checked electron densities may be useful for comparative study and provides complementary uses for the CP and HP.

  10. Pressure dependence of electron temperature using rf-floated electrostatic probes in rf plasmas

    International Nuclear Information System (INIS)

    Cantin, A.; Gagne, R.R.J.

    1977-01-01

    A new technique, which eliminates ac between probe and plasma by means of a ''follower'', permits electrostatic probes to be used in rf plasmas with a degree of confidence and accuracy which is equal, if not better, to that for a dc discharge. Measurements in argon, using this technique, have shown that electron temperature (T/sub e/) in an rf discharge is not higher than in dc discharge. Moreover the values of T/sub e/ do not agree with von Engel's law, but are in close agreement with a theory based on free diffusion and extrapolated up to values of pR=20 Torr cm (pressure times tube radius). These results are in contradiction with published electrostatic probe results for a positive column, but agree with published results as determined by microwave radiometry and optical spectroscopy. The hypothesis is made that the supporting evidence in favor of von Engel's law, afforded by published electrostatic probe results, could be due to an artifact

  11. Simulations of planar non-thermal plasma assisted ignition at atmospheric pressure

    KAUST Repository

    Casey, Tiernan A.

    2016-10-21

    The opportunity for ignition assistance by a pulsed applied voltage is investigated in a canonical one-dimensional configuration. An incipient ignition kernel, formed by localized energy deposition into a lean mixture of methane and air at atmospheric pressure, is subjected to sub-breakdown electric fields (E/N ≈ 100 Td) by a DC potential applied across the domain, resulting in non-thermal behavior of the plasma formed during the discharge. A two-fluid approach is employed to couple thermal neutrals and ions to the non-thermal electrons. A two-temperature plasma mechanism describing gas phase combustion, excitation of neutral species, and high-energy electron kinetics is employed to account for non-thermal effects. Charged species transported from the ignition zone drift rapidly through the domain, augmenting the magnitude of the electric field in the fresh gas during the pulse through a dynamic-electrode effect, which results in an increase in the energy of the electrons in the fresh mixture with increasing time. Enhanced fuel and oxidizer decomposition due to electron impact dissociation and interaction with excited neutrals generate a pool of radicals, mostly O and H, in the fresh gas ahead of the flame\\'s preheat zone. In the configuration considered, the effect of the nanosecond pulse is to increase the mass of fuel burned at equivalent times relative to the unsupported ignition through enhanced radical generation, resulting in an increased heat release rate in the immediate aftermath of the pulse.

  12. Investigation of surface treatment of conductive wire in cylindrical atmospheric pressure plasmas

    International Nuclear Information System (INIS)

    Ye Rubin; Kagohashi, Tsutomu; Zheng Wei

    2009-01-01

    Polyethylene insulated electric wire was treated in He and Ar dielectric barrier discharge atmospheric pressure plasmas generated in a quartz tube wound with tubular electrodes. The wire was put penetrating through the high voltage and the grounded electrodes, improving the discharge and facilitating uniform surface treatment. In this work, the influences of conductivity of the wire on the effects of surface treatment and discharge behavior were investigated. Surface properties of the wire samples were analyzed by means of surface energy measurement and X-ray photoelectron spectroscopy. In order to reveal the mechanism for treating the conductive wire, I-V discharge waveforms were measured and time-resolved plasma images were taken. It was demonstrated that the conductive wire was involved in the discharge process, reducing the breakdown voltage significantly and enhancing the discharge. It shows that the discharge mode was strongly dependent on the conductivity of a wire. Intensive surface discharges developed along the conductive wire were found to be mainly responsible for noticeable improvement in the treatment effect.

  13. Hydrophilic film polymerized on the inner surface of PMMA tube by an atmospheric pressure plasma jet

    Science.gov (United States)

    Yin, Mengmeng; Huang, Jun; Yu, Jinsong; Chen, Guangliang; Qu, Shanqing

    2017-07-01

    Polymethyl methacrylate (PMMA) tube is widely used in biomedical and mechanical engineering fields. However, it is hampered for some special applications as the inner surface of PMMA tube exhibts a hydrophobic characteristic. The aim of this work is to explore the hydrophilic modification of the inner surface of the PMMA tubes using an atmospheric pressure plasma jet (APPJ) system that incorporates the acylic acid monomer (AA). Polar groups were grafted onto the inner surface of PMMA tube via the reactive radicals (•OH, •H, •O) generated in the Ar/O2/AA plasma, which were observed by the optical emission spectroscopy (OES). The deposition of the PAA thin layer on the PMMA surface was verified through the ATR-FTIR spectra, which clearly showed the strengthened stretching vibration of the carbonyl group (C=O) at 1700 cm-1. The XPS data show that the carbon ratios of C-OH/R and COOH/R groups increased from 9.50% and 0.07% to 13.49% and 17.07% respectively when a discharge power of 50 W was used in the APPJ system. As a result, the static water contat angle (WCA) of the modified inner surface of PMMA tube decreased from 100° to 48°. Furthermore, the biocompatibility of the APP modified PMMA tubes was illustrated by the study of the adhesion of the cultured MC3T3-E1 osteocyte cells, which exhibted a significantly enhanced adhesion density.

  14. Atmospheric-pressure plasma-irradiation inhibits mouse embryonic stem cell differentiation to mesoderm and endoderm but promotes ectoderm differentiation

    Science.gov (United States)

    Miura, Taichi; Hamaguchi, Satoshi; Nishihara, Shoko

    2016-04-01

    Recently, various effects of low-temperature atmospheric-pressure plasma irradiation on living cells have been demonstrated, such as tissue sterilization, blood coagulation, angiogenesis, wound healing, and tumor elimination. However, the effect of plasma-irradiation on the differentiation of mouse embryonic stem cells (mESCs) has not yet been clarified. A large number of reactive species are generated by plasma-irradiation in medium, of which hydrogen peroxide (H2O2) is one of the main species generated. Here, we investigated the effect of plasma-irradiation on the differentiation of mESCs using an embryoid body (EB) formation assay with plasma-irradiated medium or H2O2-supplemented non-irradiated medium. Our findings demonstrated that plasma-irradiated medium potently inhibits the differentiation from mESCs to mesoderm and endoderm by inhibiting Wnt signaling as determined by quantitative polymerase chain reaction and immunoblotting analyses. In contrast, both the plasma-irradiated medium and H2O2-supplemented non-irradiated medium enhanced the differentiation to epiblastoid, ectodermal, and neuronal lineages by activation of fibroblast growth factor 4 (FGF4) signaling, suggesting that these effects are caused by the H2O2 generated by plasma-irradiation in medium. However, in each case, the differentiation to glial cells remained unaffected. This study is the first demonstration that plasma-irradiation affects the differentiation of mESCs by the regulation of Wnt and FGF4 signaling pathways.

  15. Investigation of Atmospheric Pressure Plasma Discharge and Its Application to Surface Modification of Blood-Filtering Material

    Science.gov (United States)

    Tang, Xiaoliang; Feng, Xianping; Qiu, Gao; Yan, Yonghui; Shi, Yuncheng

    2004-10-01

    Melt-blown polybutylene terephthalate (PBT) nonwoven materials treated by using plasma is regarded as one of the excellent materials to filter white blood cells (WBC) from blood. In this paper, dielectric barrier discharge (DBD) plasma source at an improved quasi-stable atmospheric pressure is achieved when discharge voltage, discharge current, and gap between the electrodes are carefully controlled. This plasma source has been used to modify the surface of PBT melt-blown nonwoven materials. Experimental results indicate that both the wettability and permeation of treated PBT melt-blown nonwoven materials are greatly improved.

  16. Investigation of atmospheric pressure plasma discharge and its application to surface modification of blood-filtering material

    International Nuclear Information System (INIS)

    Tang Xiaoliang; Qiu Gao; Yan Yonghui; Shi Yuncheng

    2004-01-01

    Melt-blown polybutylene terephthalate (PBT) nonwoven materials treated by using plasma is regarded as one of the excellent materials to filter white blood cells (WBC) from blood. In this paper, dielectric barrier discharge (DBD) plasma source at an improved quasi-stable atmospheric pressure is achieved when discharge voltage, discharge current, and gap between the electrodes are carefully controlled. This plasma source has been used to modify the surface of PBT melt-blown nonwoven materials. Experimental results indicate that both the wettability and permeation of treated PBT melt-blown nonwoven materials are greatly improved. (authors)

  17. Cold atmospheric pressure plasma treatment of ready-to-eat meat: Inactivation of Listeria innocua and changes in product quality

    DEFF Research Database (Denmark)

    Rød, Sara Katrine; Hansen, Flemming; Leipold, Frank

    2012-01-01

    The application of cold atmospheric pressure plasma for decontamination of a sliced ready-to-eat (RTE) meat product (bresaola) inoculated with Listeria innocua was investigated. Inoculated samples were treated at 15.5, 31, and 62 W for 2–60 s inside sealed linear-low-density-polyethylene bags...... the sensory threshold level. Surface colour changes included loss of redness of ∼40% and 70% after 1 and 14 days of storage, respectively, regardless of plasma treatment. The results indicate that plasma may be applicable in surface decontamination of pre-packed RTE food products. However, oxidation may...... constitute an issue in some products....

  18. Design and simulation of a three-electrode atmospheric pressure plasma jet device for its potential application in actinide decontamination

    International Nuclear Information System (INIS)

    Arundhati Bute; Kar, Rajib; Chand, Naresh; Sinha, Sucharita; Chandra, Romesh; Sharma, Archana

    2015-01-01

    The design of a three electrode plasma torch for microwave Atmospheric Pressure Plasma Jet (APPJ) experiments was simulated using Microwave Studio (MWS) software, to match its line impedance throughout the length of the torch. Electric field was simulated to be maximum at the tip of each electrode for plasma jet formation. Length of the torch was kept equal to the wavelength of the microwave signal. The plasma torch can be subdivided into three parts namely N-type connector, Teflon stud and three pin electrode section. Line impedance between each of these parts was matched. Impedance variation throughout the length of the torch was kept within 48.5 ohm to 51.3 ohm. The torch was tested in laboratory with Argon plasma. Microwave power at 2.45 GHz was fed to the torch through RG 214 microwave cable. This torch exhibited good efficiency with only 7% reflection of the input power. (author)

  19. Simultaneous and long-lasting hydrophilization of inner and outer wall surfaces of polytetrafluoroethylene tubes by transferring atmospheric pressure plasmas

    International Nuclear Information System (INIS)

    Chen, Faze; Song, Jinlong; Huang, Shuai; Xu, Wenji; Sun, Jing; Liu, Xin; Xu, Sihao; Xia, Guangqing; Yang, Dezheng

    2016-01-01

    Plasma hydrophilization is a general method to increase the surface free energy of materials. However, only a few works about plasma modification focus on the hydrophilization of tube inner and outer walls. In this paper, we realize simultaneous and long-lasting plasma hydrophilization on the inner and outer walls of polytetrafluoroethylene (PTFE) tubes by atmospheric pressure plasmas (APPs). Specifically, an Ar atmospheric pressure plasma jet (APPJ) is used to modify the PTFE tube’s outer wall and meanwhile to induce transferred He APP inside the PTFE tube to modify its inner wall surface. The optical emission spectrum (OES) shows that the plasmas contain many chemically active species, which are known as enablers for various applications. Water contact angle (WCA) measurements, x-ray photoelectron spectroscopy (XPS) and atomic force microscopy (AFM) are used to characterize the plasma hydrophilization. Results demonstrate that the wettability of the tube walls are well improved due to the replacement of the surface fluorine by oxygen and the change of surface roughness. The obtained hydrophilicity decreases slowly during more than 180 d aging, indicating a long-lasting hydrophilization. The results presented here clearly demonstrate the great potential of transferring APPs for surface modification of the tube’s inner and outer walls simultaneously. (paper)

  20. Changes in the biomechanical properties of a single cell induced by nonthermal atmospheric pressure micro-dielectric barrier discharge plasma.

    Science.gov (United States)

    Choi, Hyeongwon; Choi, Eun Ha; Kim, Kyung Sook

    2017-10-01

    Mechanical properties of a single cell are closely related to the fate and functions of the cell. Changes in mechanical properties may cause diseases or cell apoptosis. Selective cytotoxic effects of nonthermal atmospheric pressure micro-dielectric barrier discharge (DBD) plasma have been demonstrated on cancer cells. In this work, changes in the mechanical properties of a single cell induced by nonthermal atmospheric pressure micro-DBD plasma were investigated using atomic force microscopy (AFM). Two cervical cancer cell lines (HeLa and SiHa) and normal human fibroblast cells (HFBs) were exposed to micro-DBD plasma for various exposure times. The elasticity of a single cell was determined by force-distance curve measurement using AFM. Young's modulus was decreased by plasma treatment for all cells. The Young's modulus of plasma-treated HeLa cells was decreased by 75% compared to nontreated HeLa cells. In SiHa cells and HFBs, elasticity was decreased slightly. Chemical changes induced by the plasma treatment, which were observed by Raman spectroscopy, were also significant in HeLa cells compared to SiHa cells and HFBs. These results suggested that the molecular changes induced by micro-DBD plasma were related to cell mechanical changes. © 2017 Wiley Periodicals, Inc.