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Sample records for brazilian lnls synchrotron

  1. Multiple imaging radiography at LNLS

    Energy Technology Data Exchange (ETDEWEB)

    Hoennicke, M.G. [LORXI, Departamento de Fisica, Universidade Federal do Parana, Caixa Postal 19091, 81531-990 Curitiba (Brazil)], E-mail: marcelohonnicke@yahoo.com.br; Cusatis, C. [LORXI, Departamento de Fisica, Universidade Federal do Parana, Caixa Postal 19091, 81531-990 Curitiba(Brazil); Antunes, A. [Departamento de Fisica Aplicada, Instituto de Fisica, Universidade de Sao Paulo, Caixa Postal 66318, 05315-970 Sao Paulo (Brazil); Safatle, A.M.V.; Barros, P.S.M. [Laboratorio de Oftalmologia Experimental e Comparativa, Departamento de Cirurgia, Faculdade de Medicina Veterinaria, Universidade de Sao Paulo, 05508-900 Sao Paulo (Brazil); Morelhao, S.L. [Departamento de Fisica Aplicada, Instituto de Fisica, Universidade de Sao Paulo, Caixa Postal 66318, 05315-970 Sao Paulo (Brazil)

    2008-01-11

    An analyzer-based X-ray phase-contrast imaging (ABI) setup has been mounted at the Brazilian Synchrotron Light Laboratory (LNLS) for multiple imaging radiography (MIR) purposes. The algorithm employed for treating the MIR data collected at LNLS is described, and its reliability in extracting the distinct types of contrast that can be obtained with MIR is demonstrated by analyzing a test sample (thin polyamide wire). As a practical application, the possibility of studying ophthalmic tissues, corneal sequestra in this case, via MIR is investigated.

  2. XDS: a flexible beamline for X-ray diffraction and spectroscopy at the Brazilian synchrotron.

    Science.gov (United States)

    Lima, F A; Saleta, M E; Pagliuca, R J S; Eleotério, M A; Reis, R D; Fonseca Júnior, J; Meyer, B; Bittar, E M; Souza-Neto, N M; Granado, E

    2016-11-01

    The majority of the beamlines at the Brazilian Synchrotron Light Source Laboratory (LNLS) use radiation produced in the storage-ring bending magnets and are therefore currently limited in the flux that can be used in the harder part of the X-ray spectrum (above ∼10 keV). A 4 T superconducting multipolar wiggler (SCW) was recently installed at LNLS in order to improve the photon flux above 10 keV and fulfill the demands set by the materials science community. A new multi-purpose beamline was then installed at the LNLS using the SCW as a photon source. The XDS is a flexible beamline operating in the energy range between 5 and 30 keV, designed to perform experiments using absorption, diffraction and scattering techniques. Most of the work performed at the XDS beamline concentrates on X-ray absorption spectroscopy at energies above 18 keV and high-resolution diffraction experiments. More recently, new setups and photon-hungry experiments such as total X-ray scattering, X-ray diffraction under high pressures, resonant X-ray emission spectroscopy, among others, have started to become routine at XDS. Here, the XDS beamline characteristics, performance and a few new experimental possibilities are described.

  3. The Brazilian Synchrotron Light Source

    CERN Document Server

    Tavares, P F

    2005-01-01

    The Brazilian Synchrotron Radiation Laboratory has been operating the only light source in the southern hemisphere since July 1997. Over this 7 year period, approximately 22000 hours of beam time were delivered to users from all over Brazil as well as from 10 other countries. In this article, we report on the present configuration of the 1.37 GeV electron storage ring and associated instrumentation, describe recent improvements to the light source and analyze future prespectives including the installation of insertion devices and additional beamlines.

  4. The MX2 macromolecular crystallography beamline: a wiggler X-ray source at the LNLS.

    Science.gov (United States)

    Guimarães, Beatriz G; Sanfelici, Lucas; Neuenschwander, Regis T; Rodrigues, Flávio; Grizolli, Walan C; Raulik, Marco A; Piton, James R; Meyer, Bernd C; Nascimento, Alessandro S; Polikarpov, Igor

    2009-01-01

    The Brazilian Synchrotron Light Laboratory [Laboratório Nacional de Luz Síncrotron (LNLS), Campinas, SP, Brazil] is the first commissioned synchrotron light source in the southern hemisphere. The first wiggler macromolecular crystallography beamline (MX2) at the LNLS has been recently constructed and brought into operation. Here the technical design, experimental set-up, parameters of the beamline and the first experimental results obtained at MX2 are described. The beamline operates on a 2.0 T hybrid 30-pole wiggler, and its optical layout includes collimating mirror, Si(111) double-crystal monochromator and toroidal bendable mirror. The measured flux density at the sample position at 8.7 eV reaches 4.8 x 10(11) photons s(-1) mm(-2) (100 mA)(-1). The beamline is equipped with a MarResearch Desktop Beamline Goniostat (MarDTB) and 3 x 3 MarMosaic225 CCD detector, and is controlled by a customized version of the Blu-Ice software. A description of the first X-ray diffraction data sets collected at the MX2 LNLS beamline and used for macromolecular crystal structure solution is also provided.

  5. Commissioning of the LNLS 2 T Hybrid Wiggler

    CERN Document Server

    Farias, Ruy H A; Aparecida-Gouveia, Ana F; Cabral-Jahnel, Lucia; Citadini, James F; Ferreira, Marcelo J; Franco, J G; Liu, Lin; Neuenschwander, Regis; Resende, Ximenes R; Tavares, Pedro; Tosin, Giancarlo

    2005-01-01

    We present the results of the commissioning of a 28-pole 2 T Hybrid Wiggler at the 1.37 GeV electron storage ring of the Brazilian Synchrotron Light Source. The wiggler will be used mainly for protein crystallography and was optimized for the production of 12 keV photons. The very high field and relatively large gap (22 mm) of this insertion device led to a magnetic design that includes large main and side magnets and heavily saturated poles. We present the results of the commissioning with beam, with special attention to the correction of the large linear tune-shift perturbations produced by the wiggler as well as on the reduction of beam lifetime at full energy. Since the injection at the LNLS storage ring is performed at 500 MeV we also focus on the effects of non-linearities and their impact on injection efficiency.

  6. Orbit Stability at the Brazilian Synchrotron Light Source

    CERN Document Server

    Liu, Lin

    2005-01-01

    A task force has been implemented at the Brazilian Synchrotron Light Laboratory to improve the beam orbit stability in the 1.37 GeV electron storage ring. The main problems faced during this year (2004) were due to the installation of a second RF cavity in the machine. We describe the main problems and the solutions that were implemented.

  7. X-ray powder diffraction at the XRD1 beamline at LNLS.

    Science.gov (United States)

    Carvalho, A M G; Araújo, D H C; Canova, H F; Rodella, C B; Barrett, D H; Cuffini, S L; Costa, R N; Nunes, R S

    2016-11-01

    Various upgrades have been completed at the XRD1 beamline at the Brazilian synchrotron light source (LNLS). The upgrades are comprehensive, with changes to both hardware and software, now allowing users of the beamline to conduct X-ray powder diffraction experiments with faster data acquisition times and improved quality. The main beamline parameters and the results obtained for different standards are presented, showing the beamline ability of performing high-quality experiments in transmission geometry. XRD1 operates in the 5.5-14 keV range and has a photon flux of 7.8 × 109 photons s-1 (with 100 mA) at 12 keV, which is one of the typical working energies. At 8 keV (the other typical working energy) the photon flux at the sample position is 3.4 × 1010 photons s-1 and the energy resolution ΔE/E = 3 × 10-4.

  8. RF Phase Modulation at the LNLS Electron Storage Ring

    CERN Document Server

    Abreu, Natalia P; Tavares, Pedro

    2005-01-01

    In the Brazilian Electron Storage Ring, we observed that modulating the phase of accelerating fields at twice the synchrotron frequency suppressed remarkably well a longitudinal coupled-bunch mode of the beam driven by one of the RF cavities. We present results of a set of systematic measurements, in single and multi-bunch mode, aimed at characterizing the effects of the modulation on the beam. We also compare those experiments with the results of tracking simulations.

  9. Multielemental analysis of samples from patients with dermatological pathologies using synchrotron radiation

    Science.gov (United States)

    Soares, J. C. A. C. R.; Canellas, C. G. L.; Anjos, M. J.; Lopes, R. T.

    2014-02-01

    Using synchrotron radiation total X-ray fluorescence (SRTXRF) technique, the concentrations of trace elements were measured in four skin lesions: seborrheic keratosis, fibroepithelial polyp, cherry angioma and dermatosis papulosa nigra. The concentrations of P, S, K, Ca, Fe, Cu, Zn and Rb were evaluated in 62 pairs of lesions and healthy samples, each one having been collected from the same patient. The results revealed significant differences of P, Ca, K, Fe and Cu levels as well as a common trend in their variations between lesion and control samples among the skin diseases. This study revealed a powerful tool that can be useful for skin disorders research. The measurements were conducted at Brazilian National Synchrotron Light Laboratory (LNLS).

  10. Fish samples as bioindicator of environmental quality: synchrotron radiation total reflection X-ray fluorescence analysis (SR-TXRF)

    Energy Technology Data Exchange (ETDEWEB)

    Vives, Ana Elisa Sirito de [Universidade Metodista de Piracicaba (UNIMEP), Santa Barbara D' Oeste, SP (Brazil). Faculdade de Engenharia, Arquitetura e Urbanismo]. E-mail: aesvives@unimep.br; Moreira, Silvana [Universidade Estadual de Campinas, SP (Brazil). Faculdade de Engenharia, Arquitetura e Urbanismo]. E-mail: Silvana@fec.unicamp.br; Brienza, Sandra Maria Boscolo [Universidade Metodista de Piracicaba (UNIMEP), SP (Brazil). Faculdade de Ciencias Matematicas, da Natureza e de Tecnologia da Informacao]. E-mail: sbrienza@unimep.br; Zucchi, Orgheda Luiza Araujo Domingues [Sao Paulo Univ., Ribeirao Preto, SP (Brazil). Faculdade de Ciencias Farmaceuticas]. E-mail: olzucchi@fcfrp.usp.br; Nascimento Filho, Virgilio Franco do [Centro de Energia Nuclear na Agricultura (CENA), Piracicaba, SP (Brazil)]. E-mail: virgilio@cena.usp.br

    2005-07-01

    In this study fish were used as bioindicators of environmental contamination. The species were collected in Piracicaba River, Sao Paulo state, Brazil and the toxic elements concentrations were determined in muscle tissue and viscus (liver, intestine and stomach) by Synchrotron Radiation Total Reflection X-Ray Fluorescence Analysis (SR-TXRF). Were determined the elements Ti, Cr, Mn, Fe, Ni, Cu, Zn and Ba. The results were compared with values established by Brazilian Legislation for general food. The elements concentrations evidenced potential risk to human health and environmental quality alteration of the studied area. The measurements were realized at the 'Laboratorio Nacional de Luz Sincrotron' (LNLS) located in Campinas, Sao Paulo State, Brazil. (author)

  11. TXRF analysis of multielements in serum of patients with sickle cell anemia (SCA) by synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Canellas, Catarine G.L.; Jesus, Edgar F.O. de; Anjos, Marcelino J.; Lopes, Ricardo T., E-mail: catarine@lin.ufrj.b, E-mail: edgar@lin.ufrj.b, E-mail: marcelin@lin.ufrj.b, E-mail: ricardo@lin.ufrj.b [Federal University of Rio de Janeiro (UFRJ), RJ (Brazil). COPPE Technology Center. Nuclear Instrumentation Lab.; Carvalho, Silvia M.F., E-mail: silvia@hemorio.rj.gov.b [State Institute of Hematology Arthur de Siqueira Cavalcanti (HEMORIO), Rio de Janeiro, RJ (Brazil)

    2009-07-01

    The determination of trace elements levels in physiological fluids is of considerable interest in clinical chemistry. Since it has been established these levels in human serum can be utilized as indicators for several pathological conditions, diagnosis and treatment of various diseases. In this work, trace elements were analyzed in serum of patients with sickle cell anemia (SCA) by total reflection X-ray fluorescence using synchrotron radiation (SRTXRF). Sickle cell Anemia is a blood disorder that affects hemoglobin, the protein found in red blood cells that help carry oxygen throughout the body. SCA occurs when a person inherits two abnormal genes (one from each parent) that cause their red blood cells to change shape. These irregular-shaped blood cells die prematurely, resulting in a chronic shortage of red blood cells. We studied forty-three patients (15 males and 28 females) aged 18 to 50 years, suffering SCA and Sixty healthy volunteers (41 males and 19 females) aged 18 to 60 years. All the serum samples had been collected of people who live in the urban area of Rio de Janeiro City/Brazil. The measurements were performed at the X-ray fluorescence beam line at Brazilian National Synchrotron Light Laboratory (LNLS), in Campinas, Sao Paulo using a polychromatic beam. It was possible to determine the concentrations of the following elements: P, S, Cl, K, Ca, Cu, Zn, Br and Rb. (author)

  12. Synchrotron X-ray diffraction characterization of healthy and fluorotic human dental enamel

    Science.gov (United States)

    Colaço, M. V.; Barroso, R. C.; Porto, I. M.; Gerlach, R. F.; Costa, F. N.; Braz, D.; Droppa, R.; de Sousa, F. B.

    2012-10-01

    With the introduction of fluoride as the main anticaries agent used in preventive dentistry, and perhaps an increase in fluoride in our food chain, dental fluorosis has become an increasing world-wide problem. Visible signs of fluorosis begin to become obvious on the enamel surface as opacities, implying some porosity in the tissue. The mechanisms that conduct the formation of fluorotic enamel are unknown, but should involve modifications in the basic physical-chemistry reactions of demineralization and remineralisation of the enamel of the teeth, which is the same reaction of formation of the enamel's hydroxyapatite (HAp) in the maturation phase. The increase of the amount of fluoride inside of the apatite will result in gradual increase of the lattice parameters. The aim of this work is to characterize the healthy and fluorotic enamel in human tooth using Synchrotron X-ray diffraction. All the scattering profile measurements were carried out at the X-ray diffraction beamline (XRD1) at the Brazilian Synchrotron Light Laboratory—LNLS, Campinas, Brazil. X-ray diffraction experiments were performed both in powder samples and polished surfaces. The powder samples were analyzed to obtain the characterization of a typical healthy enamel pattern. The polished surfaces were analyzed in specific areas that have been identified as fluorotic ones. X-ray diffraction data were obtained for all samples and these data were compared with the control samples and also with the literature data.

  13. Phosphorus migration analysis using synchrotron radiation in soil treated with Brazilian granular fertilizers.

    Science.gov (United States)

    de Castro, Robson C; de Melo Benites, Vinícius; César Teixeira, Paulo; dos Anjos, Marcelino José; de Oliveira, Luis Fernando

    2015-11-01

    The aim of this study was to evaluate the phosphorus (P) mobility in a tropical Brazilian soil type red Oxisol treated with three different forms of granular fertilizer. Total Reflection X-Ray Fluorescence (TXRF) was applied to determine the concentration of P at different distances from granular fertilizer application point. The results showed that most of the P from fertilizers tends to concentrate in a region of up to 10mm around the place of the fertilizer deposition. Copyright © 2015. Published by Elsevier Ltd.

  14. Upgrades to the XRD1 beamline optics and endstation at the LNLS

    Science.gov (United States)

    Canova, H.; Fontoura, A.; Neuenschwander, R. T.; Diaz, B.; Rodella, C. B.

    2014-03-01

    XRD1 was the first X-ray diffraction beamline to be built at the LNLS and after approximately 12 years of operation it was substantially updated to improve beam stability, increase the reliability of the monochromator movement as well as provide an experimental hutch that would meet the demands of users. The improvements included the construction of an independent concrete slab below the mirror and monochromator to minimize the vibrations originating from the floor. In addition, the installation of new monochromator mechanisms as well as the replacement of the two Si(111) crystals were performed in order to attain higher precision, stability and reproducibility during operation. Moreover, the diffractometer was replaced by a 3-circle heavy duty diffractometer from Newport to collect XRD patterns primarily in capillary geometry. A robotic arm was installed for fast and automated replacement of samples as well as to secure a cryojet or a hot air blower in front of the sample during measurements. In addition, a housing equipped with 24 Mythen detectors was installed at the beamline allowing for extremely fast data acquisition. Another upgrade was the integration of motors and control systems from PXI National Instruments and Galil controllers with Phytron. These systems are crucial for the next upgrade that is underway at the beamline: enabling remote access for users to collect their measurements without the need to travel to the LNLS.

  15. Determination of Cu/Zn and Fe in human serum of patients with sickle cell anemia using radiation synchrotron

    Energy Technology Data Exchange (ETDEWEB)

    Canellas, C.G.L. [Nuclear Instrumentation Laboratory, COPPE/UFRJ, P.O. Box 68509, 21.941-972 Rio de Janeiro (Brazil); Carvalho, S.M.F. [State Institute of Hematology Arthur de Siqueira Cavalcanti, 20.211-030 Rio de Janeiro (Brazil); Anjos, M.J. [Nuclear Instrumentation Laboratory, COPPE/UFRJ, P.O. Box 68509, 21.941-972 Rio de Janeiro (Brazil); Physics Institute, State University of Rio de Janeiro, 20.559-900 Rio de Janeiro (Brazil); Lopes, R.T., E-mail: ricardo@lin.ufrj.br [Nuclear Instrumentation Laboratory, COPPE/UFRJ, P.O. Box 68509, 21.941-972 Rio de Janeiro (Brazil)

    2012-07-15

    In this work we analyzed serum samples from patients with Sickle Cell Anemia (SCA) using Total Reflection X-Ray Fluorescence using Synchrotron Radiation (SRTXRF). The SRTXRF measurements were performed at the X-Ray Fluorescence Beamline at the Brazilian National Synchrotron Light Laboratory (LNLS). We studied forty-three patients aged 18-50 suffering from SCA and sixty healthy volunteers aged 18-60. It was possible to determine the concentrations of the following elements: P, S, Cl, K, Ca, Fe, Cu, Zn, Br and Rb. Moreover, there are evidences of an association among Fe, Cu, Zn and Cu/Zn in the SCA pathogenesis process. The concentrations of Fe and Cu in the serum samples of patients with SCA were larger, 120% and 20%, respectively, when compared with the CG. The serum level Cu/Zn ratio was significantly higher (60%) in the serum samples from patients suffering from SCA than from the CG. Therefore, the Cu/Zn ratio can be used as an adjuvant index in enhancement for diagnosis of SCA. - Highlights: Black-Right-Pointing-Pointer Serum samples from patients with Sickle Cell Anemia (SCA) were analyzed by SRTXRF. Black-Right-Pointing-Pointer It was possible to determine the concentrations of the P, S, Cl, K, Ca, Fe, Cu, Zn, Br and Rb. Black-Right-Pointing-Pointer There are evidences of an association among Fe, Cu, Zn and Cu/Zn in the SCA process. Black-Right-Pointing-Pointer The results indicate that the Cu/Zn ratio can be used as an adjuvant index for diagnosis of SCA.

  16. X-ray diffraction microtomography using synchrotron radiation

    CERN Document Server

    Barroso, R C; Jesus, E F O; Oliveira, L F

    2001-01-01

    The X-ray diffraction computed tomography technique is based on the interference phenomena of the coherent scatter. For low-momentum transfer, it is most probable that the scattering interaction will be coherent. A selective discrimination of a given element in a scanned specimen can be realized by fixing the Bragg angle which produces an interference peak and then, to carry out the computed tomography in the standard mode. The image reconstructed exalts the presence of this element with respect to other ones in a sample. This work reports the feasibility of a non-destructive synchrotron radiation X-ray diffraction imaging technique. This research was performed at the X-ray Diffraction beam line of the National Synchrotron Light Laboratory (LNLS) in Brazil. The coherent scattering properties of different tissue and bone substitute materials were evaluated. Furthermore, diffraction patterns of some polycrystalline solids were studied due to industrial and environmental human exposure to these metals. The obtai...

  17. Atomic pair distribution function at the Brazilian Synchrotron Light Laboratory: application to the Pb1-xLaxZr0.40Ti0.60O3 ferroelectric system.

    Science.gov (United States)

    Saleta, M E; Eleotério, M; Mesquita, A; Mastelaro, V R; Granado, E

    2017-09-01

    This work reports the setting up of the X-ray diffraction and spectroscopy beamline at the Brazilian Synchrotron Light Laboratory for performing total scattering experiments to be analyzed by atomic pair distribution function (PDF) studies. The results of a PDF refinement for Al2O3 standard are presented and compared with data acquired at a beamline of the Advanced Photon Source, where it is common to perform this type of experiment. A preliminary characterization of the Pb1-xLaxZr0.40Ti0.60O3 ferroelectric system, with x = 0.11, 0.12 and 0.15, is also shown.

  18. Evaluation of Fe and Zn/Cu ratio in serum of patients with sickle cell anemia by total reflection X-ray fluorescence using synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Canellas, Catarine G.L.; Leitao, Roberta G.; Lopes, Ricardo T., E-mail: catarine@lin.ufrj.b, E-mail: ricardo@lin.ufrj.b [Universidade Federal do Rio de Janeiro (PEN/COPPE/UFRJ), RJ (Brazil). Coordenacao dos Programas de Pos-Graduacao de Engenharia. Programa de Engenharia Nuclear. Lab. de Instrumentaco Nuclear; Carvalho, Silvia M.F., E-mail: silvia@hemorio.rj.gov.b [State Institute of Hematology Arthur de Siqueira Cavalcanti (HEMORIO), Rio de Janeiro, RJ (Brazil); Bellido, Alfredo Victor B., E-mail: alfredo@ien.gov.b [Federal Fluminense University (UFF), Niteroi, RJ (Brazil). Chemistry Inst.; Anjos, Marcelino J., E-mail: marcelin@lin.ufrj.b [State University of Rio de Janeiro (UERJ), RJ (Brazil). Physics Inst.

    2011-07-01

    Sickle cell anemia (SCA) is a blood disorder that affects hemoglobin, the protein found in red blood cells that help carry oxygen throughout the body. In this work we have analyzed serum samples from patients with SCA by using total reflection X-ray fluorescence using synchrotron radiation (SRTXRF). The SRTXRF measurements were performed at the X-ray fluorescence beamline at Brazilian National Synchrotron Light Laboratory (LNLS), in Campinas, Sao Paulo using a polychromatic beam. We have studied forty-three patients aged 18-50 years old, suffering from SCA and Sixty healthy volunteers aged 18-60 years old. It was possible to determine the concentrations of the following elements: P, S, Cl, K, Ca, Fe, Cu, Zn, Br and Rb. Student's t-test was applied in order to check whether the two populations (CG x SCA) had the same mean values. It was observed that elemental concentration of P, Cl, K, Fe, Cu, Zn and Br differed significantly ({alpha} = 0.05) between groups of healthy subjects and SCA. The concentrations of K, Fe and Cu in the serum samples of patients with SCA were larger 15%, 120 % and 20 %, respectively, when compared with the CG. On the other hand, the concentrations of P (-20 %), Cl (-6 %), Zn (-25 %) and Br (-22 %) were smaller than the values determined for the control group. The serum level Cu/Zn ratio was significantly higher (60%) in the serum samples of patients with SCA group than the CG. So, the Cu/Zn ratio can be used as an adjuvant index in enhancement for diagnosis of SCA. There are evidences of an association among Fe, Cu, Zn and Cu/Zn in the SCA pathogenesis process. (author)

  19. Analyzing the mobility in granular forms of P fertilizer in Brazilians soils under laboratory conditions

    Energy Technology Data Exchange (ETDEWEB)

    Castro, Robson C. de; Oliveira, Davi Ferreira de; Oliveira, Luis Fernando de; Anjos, Marcelino Jose dos, E-mail: prof.robinho@gmail.com [Universidade do Estado do Rio de Janeiro (UERJ), Rio de Janeiro, RJ (Brazil). Inst. de Fisica Armando Dias Tavares; Teixeira, Paulo Cesar; Benites, Vinicius Melo, E-mail: paulo.c.teixeira@embrapa.br [Embrapa Solos, Rio de Janeiro, RJ (Brazil)

    2013-07-01

    Phosphorus is an essential nutrient for plant growth. Million of tones of P are applied to the soils annually. However, only a small fraction of the P applied with fertilizers is taken up by crops in the year of application, and the effectiveness of any residual P fertilizer declines with time. To improve our understanding of the mechanisms underlying this response to P in the field, we have studied the mobility of P from 3 different fertilizes: monoammonium phosphate (MAP), polymer coated monoammonium phosphate (MAPp) and Organomineral phosphate (OMP) applied on high weathered soil samples in a Petri dish experiment. Total Reflection X-Ray Fluorescence (TXRF) was used to determine the P diffusive flux at different distances (0 - 7.5, 7.5 – 13.5, 13.5 – 25.5 and 25.5 – 43 mm) from granular fertilizer. TXRF analyses were performed at the X-Ray Fluorescence Beamline D09B at Brazilian National Synchrotron Light Laboratory (LNLS), in Campinas, Sao Paulo, using a polychromatic beam with maximum energy of 20 keV for the excitation and an Ultra-LEGe detector with resolution of 148 eV at 5.9 keV. Besides that, the detections were performed in a high vacuum chamber (2.5 x 10-5 mbar) to avoid air absorption. After a period of five weeks, the total P concentration increased in the soil sampled 7.5 to 13.5 mm from the fertilizer showing a diffusive flux of P. About 20% (considering MAP and MAPp) of the total P applied diffused out of the central soil ring. Different sources showed differences in diffusive flux of P. Soil pH also influenced diffusive flux of P showing higher flux on lower pH soils. (author)

  20. Optimized IR synchrotron beamline design.

    Science.gov (United States)

    Moreno, Thierry

    2015-09-01

    Synchrotron infrared beamlines are powerful tools on which to perform spectroscopy on microscopic length scales but require working with large bending-magnet source apertures in order to provide intense photon beams to the experiments. Many infrared beamlines use a single toroidal-shaped mirror to focus the source emission which generates, for large apertures, beams with significant geometrical aberrations resulting from the shape of the source and the beamline optics. In this paper, an optical layout optimized for synchrotron infrared beamlines, that removes almost totally the geometrical aberrations of the source, is presented and analyzed. This layout is already operational on the IR beamline of the Brazilian synchrotron. An infrared beamline design based on a SOLEIL bending-magnet source is given as an example, which could be useful for future IR beamline improvements at this facility.

  1. Avaliação de multielementos em amostras de sangue humano usando SR-TXRF Evaluation of multielements in human blood samples using synchrotron radiation

    Directory of Open Access Journals (Sweden)

    Nivia Graciele V. Pinto

    2010-01-01

    Gammacell 220 Exce irradiator, and the second was irradiated with doses of from 2 to 100 cGy, using gamma radiation in a Theraton 780 C irradiator. After irradiation, all samples were lyophilized to remove the water and then submitted to standard chemical digestion by adding nitric acid. All the measurements were carried out by X-Ray Fluorescence beamline at the Brazilian Synchrotron Light Laboratory (LNLS in Campinas. While no positive association was found for variations in calcium, the variations in potassium were positively associated with the radiation dose for all analyzed samples. On the other hand, iron levels decreased for whole blood and plasma and zinc levels decreased only in whole blood as the dose increased.

  2. Synchrotron radiation X-ray microfluorescence techniques and ...

    Indian Academy of Sciences (India)

    Synchrotron X-ray imaging systems with fluorescence techniques was developed for biomedical researches in Brazilian Synchrotron Laboratory. An X-ray fluorescence microtomography system was implemented to analyse human prostate and breast samples and an X-ray microfluorescence system was implemented to ...

  3. Synchrotron SAXS Studies of Nanostructured Materials and Colloidal Solutions: A Review

    Directory of Open Access Journals (Sweden)

    Craievich A.F.

    2002-01-01

    Full Text Available Structural characterisations using the SAXS technique in a number of nanoheterogeneous materials and liquid solutions are reviewed. The studied systems are protein (lysozyme/water solutions, colloidal ZnO particles/water sols, nanoporous NiO-based xerogels, hybrid organic-inorganic siloxane-PEG and PPG nanocomposites and PbTe semiconductor nanocrystals embedded in a glass matrix. These investigations also focus on the transformations of time-varying structures and on structural changes related to variations in temperature and composition. The reviewed investigations aim at explaining the unusual and often interesting properties of nanostructured materials and solutions. Most of the reported studies were carried out using the SAXS beamline at the National Synchrotron Light Laboratory (LNLS, Campinas, Brazil.

  4. Atomic pair distribution function at the Brazilian Synchrotron Light Laboratory: application to the Pb1–x LaxZr 0.40Ti0.60O3 ferroelectric system

    Energy Technology Data Exchange (ETDEWEB)

    Saleta, M. E.; Eleotério, M.; Mesquita, A.; Mastelaro, V. R.; Granado, E.

    2017-07-29

    This work reports the setting up of the X-ray diffraction and spectroscopy beamline at the Brazilian Synchrotron Light Laboratory for performing total scattering experiments to be analyzed by atomic pair distribution function (PDF) studies. The results of a PDF refinement for Al2O3 standard are presented and compared with data acquired at a beamline of the Advanced Photon Source, where it is common to perform this type of experiment. A preliminary characterization of the Pb1–xLaxZr0.40Ti0.60O3 ferroelectric system, withx= 0.11, 0.12 and 0.15, is also shown.

  5. Synchrotron radiation facilities

    CERN Multimedia

    1972-01-01

    Particularly in the past few years, interest in using the synchrotron radiation emanating from high energy, circular electron machines has grown considerably. In our February issue we included an article on the synchrotron radiation facility at Frascati. This month we are spreading the net wider — saying something about the properties of the radiation, listing the centres where synchrotron radiation facilities exist, adding a brief description of three of them and mentioning areas of physics in which the facilities are used.

  6. Analysis of synchrotron X-ray diffraction patterns from fluorotic enamel samples

    Energy Technology Data Exchange (ETDEWEB)

    Almeida, Ana P.G.; Braz, Delson, E-mail: anapaulagalmeida@gmail.co [Coordenacao dos Programas de Pos-graduacao de Engenharia (COPPE/UFRJ), Rio de Janeiro, RJ (Brazil). Lab. de Instrumentacao Nuclear; Colaco, Marcos V.; Barroso, Regina C., E-mail: cely@uerj.b [Universidade do Estado do Rio de Janeiro (UERJ), RJ (Brazil). Inst. de Fisica; Porto, Isabel M., E-mail: belporto@ig.com.b [Universidade Estadual de Campinas (UNICAMP), Piracicaba, SP (Brazil). Faculdade de Odontologia; Gerlach, Raquel F., E-mail: rfgerlach@forp.usp.b [Universidade de Sao Paulo (USP), Ribeirao Preto, SP (Brazil). Faculdade de Odontologia; Droppa Junior, Roosevelt, E-mail: rdroppa@lnls.b [Associacao Brasileira de Tecnologia de Luz Sincrotron (ABTLuS), Campinas, SP (Brazil)

    2009-07-01

    With the introduction of fluoride as the main anticaries agent used in preventive dentistry, and perhaps an increase in fluoride in our food chain, dental fluorosis has become an increasing world-wide problem. Visible signs of fluorosis begin to become obvious on the enamel surface as opacities, implying some porosity in the tissue. The mechanisms that conduct the formation of fluorotic enamel are unknown, but should involve modifications in the basics physical-chemistry reactions of demineralisation and remineralisation of the enamel of the teeth, which is the same reaction of formation of the enamel's hydroxyapatite (HAp) in the maturation phase. The increase of the amount of fluoride inside of the apatite will result in gradual increase of the lattice parameters. The hexagonal symmetry seems to work well with the powder diffraction data, and the crystal structure of HAp is usually described in space group P63/m. The aim of this work is to characterize the healthy and fluorotic enamel in human tooth using technique Synchrotron X-ray diffraction in order to determine the crystal structure and crystallinity of on fluoroapatite (FAp) crystal present in fluoritic enamel. All the scattering profile measurements was carried out at the X-ray diffraction beamline (XRD1) at the National Synchrotron Light Laboratory - LNLS, Campinas, Brazil. (author)

  7. The World of Synchrotrons

    Indian Academy of Sciences (India)

    of Padova. He will be soon joining the Centro de Ciencias Fisicas,. Universidad Nacional. Autonoma de Mexico. Sameen Ahmed Khan. A summary of results on synchrotron radiation is presented along with notes on its properties and applications. Quantum aspects are briefly mentioned. Synchrotron radiation facilities are.

  8. Synchrotron radiation sources

    Energy Technology Data Exchange (ETDEWEB)

    van Steenbergen, A.

    1979-01-01

    As a result of the exponential growth of the utilization of synchrotron radiation for research in the domain of the material sciences, atomic and molecular physics, biology and technology, a major construction activity has been generated towards new dedicated electron storage rings, designed optimally for synchrotron radiation applications, also, expansion programs are underway at the existing facilities, such as DORIS, SPEAR, and VEPP. In this report the basic properties of synchrotron radiation will be discussed, a short overview will be given of the existing and new facilities, some aspects of the optimization of a structure for a synchrotron radiation source will be discussed and the addition of wigglers and undulators for spectrum enhancement will be described. Finally, some parameters of an optimized synchrotron radiation source will be given.

  9. Inauguration of Proton Synchrotron

    CERN Multimedia

    1960-01-01

    On 5 February 1960, the Proton Synchrotron (PS) was formally inaugurated. The great Danish physicist, Niels Bohr, releases a bottle of champagne against a shielding block to launch the PS on its voyage in physics.

  10. Future Synchrotron Radiation Sources

    CERN Document Server

    Winick, Herman

    2003-01-01

    Sources of synchrotron radiation (also called synchrotron light) and their associated research facilities have experienced a spectacular growth in number, performance, and breadth of application in the past two to three decades. In 1978 there were eleven electron storage rings used as light sources. Three of these were small rings, all below 500 mega-electron volts (MeV), dedicated to this purpose; the others, with energy up to 5 giga-electron volts (GeV), were used parasitically during the operation of the ring for high energy physics research. In addition, at that time synchrotron radiation from nine cyclic electron synchrotrons, with energy up to 5 GeV, was also used parasitically. At present no cyclic synchrotrons are used, while about 50 electron storage rings are in operation around the world as fully dedicated light sources for basic and applied research in a wide variety of fields. Among these fields are structural molecular biology, molecular environmental science, materials, analytic chemistry, micr...

  11. Elemental mapping by synchrotron radiation X-Ray microfluorescence in cellular spheroid of prostate tumor cells

    Energy Technology Data Exchange (ETDEWEB)

    Leitao, R.G.; Anjos, M.J.; Lopes, R.T., E-mail: roberta@lin.ufrj.br [Universidade Federal do Rio de Janeiro (UFRJ), RJ (Brazil). Lab. de Instrumentacao Nuclear; Santos, C.A.N. [Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMETRO), Duque de Caxias, RJ (Brazil). Lab. de Biotecnologia; Palumbo Junior, A.; Souza, P.A.V.R.; Nasciutti, L.E. [Universidade Federal do Rio de Janeiro (UFRJ), RJ (Brazil). Instituto de Ciencias Biomedicas; Pereira, G.R. [Universidade Federal do Rio de Janeiro (UFRJ), RJ (Brazil). Lab. de Ensaios Nao Destrutivos, Corrosao e Soldagem

    2013-08-15

    Prostate cancer is the sixth most common type of cancer and the third most common in males in Western industrialized countries. Cellular spheroid serves as excellent physiologic tumor models as they mimic avascular tumors and micrometastases. Trace elements play a significant role in biological processes. They are capable of affecting human health by competing with essential elements for available binding sites and by the activation or inhibition of reactions between metabolic enzymes. It is well known that zinc levels in the peripheral zone of dorsal and lateral lobes of the prostate are almost 10 times higher than in other soft tissues. Prostate tumor cells were isolated of the prostate tissue samples that were collected from patients submitted to surgery. The measurements were performed in XRF beam line at the Synchrotron Light National Laboratory (LNLS) in Campinas, Brazil. The results showed that all elements were heterogeneously distributed in different areas of the spheroids analyzed. P, S and Cl showed similar elemental distribution in all the samples analyzed while K, Ca, Fe, and Cu showed different elemental distribution. In all spheroids analyzed, Zn presented more intense distributions in the central region of the spheroid. The relationship between the function of Zn in the secretory epithelial cells and the carcinogenic process suggests that more studies on elemental mapping in spheroids are necessary. (author)

  12. Compact synchrotron light sources

    CERN Document Server

    Weihreter, Ernst

    1996-01-01

    This book covers a new niche in circular accelerator design, motivated by the promising industrial prospects of recent micromanufacturing methods - X-ray lithography, synchrotron radiation-based micromachining and microanalysis techniques. It describes the basic concepts and the essential challenges for the development of compact synchrotron radiation sources from an accelerator designer's point of view and gives an outline of the actual state of the art. The volume is intended as an introduction and as a reference for physicists, engineers and managers involved in this rapidly developing fiel

  13. Microfabrication using synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Tolfree, D.W.L. [CCLRC Daresbury Laboratory, Warrington, Cheshire (United Kingdom)

    1998-04-01

    The realization of precision deep microstructures requires high-energy, intense parallel beams of x-rays from synchrotron radiation sources and novel process technology. Deep x-ray lithography with synchrotron radiation is basically a shadow printing process in which a two-dimensional pattern is accurately transferred from a mask into a resist material by chemical changes induced by the radiation. Subsequent electroforming and moulding processes are used to manufacture microstructures from metals, plastics and ceramics. This process, known as LIGA (LIthographie, Galvanoformung, and Abformung), first developed in Germany, is based on a combination of lithography, electroforming and replication processes. The development of the LIGA process for the fabrication of a wide range of precision microstructures has been stimulated by the increasing use of synchrotron radiation sources for lithography. Applications for microstructures exist in many sectors of industry. These include chemical and process engineering, biomedical instrumentation, automotive and aerospace technology, environmental monitoring and information technology. Emphasis is placed on three main areas, micromechanics, micro-optics and microfluidics, which are emerging with the widest range of industrial applications. This paper reviews the progress being made in microfabrication technology using x-ray beam lithography and the LIGA process. It includes a description of synchrotron radiation, storage ring sources, the fabrication processes, applications and potential markets. Reference is also made to European networks and R and D activity worldwide. (author)

  14. Synchrotron X-ray Scattering from Self-organized Soft Nanostructures in Clays

    Science.gov (United States)

    Fossum, J. O.

    2009-04-01

    In the general context of self-organization of nanoparticles (in our case clay particles), and transitions in such structures, we study interconnected universal complex physical phenomena such as: (i) spontaneous gravitationally induced phase separation and nematic self-organization in systems of anisotropic clay nanoparticles in aqueous suspension, including studies of isotropic to nematic transitions [1,2] (ii) transitions from biaxial to uniaxial nematics by application of external magnetic field to self-organized systems of the same anisotropic (diamagnetic) clay nanoparticle systems [3,4] (iii) guided self-organization into chainlike structures of the same anisotropic clay nanoparticles in oil suspension when subjected to external electrical fields (electrorheological structures of polarized nanoparticles), and the stability of, and transitions of, such structures, when subjected to external mechanical stress [5,6] The experimental techniques used by us include synchrotron X-ray scattering, neutron scattering, rheometry. microscopy and magnetic resonance. We have demonstrated that clays may be used as good model systems for studies of universal physical phenomena and transitions in self-organized nanostructured soft and complex matter. Self-organization and related transitions in clay systems in particular, may have practical relevance for nano-patterning, properties of nanocomposites, and macroscopically anisotropic gels, among many other applications [7]. The synchrotron experiments have been performed at LNLS-Brazil, PLS- Korea, BNL-USA and ESRF-France. Acknowledgments: Collaborators, postdocs and students at NTNU-Norway, UiO-Norway, IFE-Norway, BNL-USA, LNLS-Brazil, UFPE-Brazil, UnB-Brazil, Univ. Amsterdam-Netherlands, Univ.Paris 7-France and other places. This research has been supported by the Research Council of Norway (RCN), through the NANOMAT, SUP and FRINAT Programs. References 1. J.O. Fossum, E. Gudding, D.d.M. Fonseca, Y. Meheust, E. DiMasi, T

  15. In situ hydration of sulphoaluminate cement mixtures monitored by synchrotron x-ray diffraction

    Energy Technology Data Exchange (ETDEWEB)

    Turrillas, X. [Institut de Ciencia de Materials de Barcelona (ICMAB-CSIC), Barcelona (Spain); Martinez, L.G.; Carvalho, A.M.; Carezzato, G.L. [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil); Rossetto, C.M. [Faculdade de Tecnologia de Sao Paulo (FATEC), SP (Brazil)

    2016-07-01

    Full text: The hydration of calcium sulpho-aluminate cement mixtures was studied in situ by synchrotron X-ray diffraction at the XRD1 beamline of the Laboratorio Nacional de Luz Sincrotron (LNLS) in Campinas, SP. The powder specimens were introduced in borosilicate glass capillary tubes of 0.7 mm of internal diameter and imbued with deionized water. As the hydration reaction is very fast the capillaries were placed on the goniometer and the data collection was started after two minutes of mixing with water. The X-ray energy chosen to get an adequate flux for these short time acquisitions was 12 keV or more precisely 1.033258 Å, determined with polycrystalline corundum standard. Diffraction patterns were collected sequentially every 35 seconds for several hours at temperatures ranging from 40 degC to 55 degC with an accuracy better than 0.1 degC attained with the help of a hot air blower. The diffracted signal was collected with an array of twenty-four Mythen detectors at 760 mm from the capillary tube. The diffraction patterns had appropriate statistics to determine the kinetics of the reaction either by quantitative Rietveld analysis or by fitting isolated diffraction peaks to Gaussian curves as a function of time. The most important phases involved in the hydration are Klein´s salt, also known as Ye’elimite, Ca4(AlO2)6SO4, and gypsum, CaSO4.2H2O to yield Ettringite, Ca6Al2(SO4)3(OH)12 - 26H2O, phase responsible for the mechanical properties. (author)

  16. The European Synchrotron Radiation Facility

    DEFF Research Database (Denmark)

    Buras, B.; Materlik, G.

    1986-01-01

    In recent years, X-ray synchrotron radiation became a powerful tool for studies of condensed matter, and in view of that a proposal for the construction of a European Synchrotron Radiation Facility (ESRF) was elaborated in some detail by the European Synchrotron Radiation Project. The heart...... by a great flexibility and a small emittance (7×10−9 rad m) leading to a very high brilliance (1019 photons/(s mm2 mrad2) in a relative bandwidth of 0.1% in case of a 1 Å undulator). The overview, as seen from the users point of view, gives a brief account of the storage ring, emitted radiation...

  17. Reshuffle lifts French synchrotron hopes

    CERN Multimedia

    McCabe, H

    2000-01-01

    The sacking of Claude Allegre as research minister has raised doubts over the level of France's promised participation in the construction of Diamond but reawakened French hopes that the synchrotron Soleil may now be built (1 page).

  18. Synchrotron radiation and structural proteomics

    CERN Document Server

    Pechkova, Eugenia

    2011-01-01

    This book presents an overview of the current state of research in both synchrotron radiation and structural proteomics from different laboratories worldwide. The book presents recent research results in the most advanced methods of synchrotron radiation analysis, protein micro- and nano crystallography, X-ray scattering and X-ray optics, coherent X-Ray diffraction, and laser cutting and contactless sample manipulation are described in details. The book focuses on biological applications and highlights important aspects such as radiation damage and molecular modeling.

  19. Brazilian Firms

    Directory of Open Access Journals (Sweden)

    Vicente Lima Crisóstomo

    2016-01-01

    Full Text Available This work makes an analysis of the determinants of Corporate Social Responsibility (CSR of Brazilian firms, as proxied by firm membership of the ISE Index of BM&FBOVESPA. Besides other proposed determinants of CSR present in the literature (firm size, profitability, growth opportunities, the work examines ownership concentration and the persistence on CSR status. Logit regression estimates have been run for a sample of 1649 firm-year observations in the period 2006-2011. The findings show that CSR of Brazilian firms is inversely correlated to its ownership concentration indicating that controlling voting shareholders may not see social concerns as a priority. Besides, firms tend to maintain their present CSR status. The results also indicate that leading CSR firms are larger, face more growth opportunities, and are persistent in their superior CSR situation.

  20. Synchrotron radiation is brighter than ever

    CERN Document Server

    Cornuejols, D

    2000-01-01

    What began life as an unwanted energy loss has become a major research industry. Dominique Cornuejols of the European Synchrotron Radiation Facility in Grenoble looks at the history and accomplishments of synchrotron radiation. (0 refs).

  1. PHOTOACOUSTIC SPECTROSCOPY USING A SYNCHROTRON LIGHT SOURCE.

    Energy Technology Data Exchange (ETDEWEB)

    JACKSON, R.S.; MICHAELIAN, K.H.; HOMES, C.C.

    2001-02-05

    We have investigated the use of a synchrotron as a source for infrared photoacoustic spectroscopy. A synchrotron has an intrinsically high radiance, which is beneficial when photoacoustic spectroscopy is applied to small samples, especially at long wavelengths.

  2. Brazilian energy

    Energy Technology Data Exchange (ETDEWEB)

    O`Shaughnessy, H.

    1997-04-01

    Brazilian Energy provides all the information necessary for energy companies to invest and operate in Brazil, including: a review of Brazil`s natural resources; an assessment of privatisation strategies at the federal, state and regional level; an analysis of the electricity industry and the future for Electrobras; an analysis of the oil industry and, in particular, Petrobras; a discussion of the fuel alcohol industry; the discovery of local natural gas, its prospects and the involvement of the auto industry; an assessment of the problems facing the coal industry and its future; a discussion of the regulatory framework for the newly privatised companies; the importance of intra-regional energy links and the booming membership of Mercosur; the difficulties experienced by foreign investors doing business in Brazil; brief profiles of the key energy companies; profiles of key people influencing the privatisation process in Brazil. Brazilian energy is essential reading for those wishing to advise and assist Brazil in this period of change and development, as well as those who wish to invest or become key players in the Brazilian energy sector. (author)

  3. DESY: Synchrotron and storage rings

    CERN Multimedia

    1972-01-01

    An improvement programme has been under way for several years at the 7.5 GeV électron synchrotron at DESY. In particular it has been designed to increase the accelerated beam intensity, to achieve better quality of the ejected électron beams and photon beams and to improve machine reliability.

  4. Biological physics and synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Filhol, J.M.; Chavanne, J. [European Synchrotron Radiation Facility, 38 - Grenoble (France); Weckert, E. [Hasylab at Desy, Hamburg (Germany)] [and others

    2001-07-01

    This conference deals with the applications of synchrotron radiation to current problems in biology and medicine. Seven sessions take stock on the subject: sources and detectors; inelastic scattering and dynamics; muscle diffraction; reaction mechanisms; macromolecular assemblies; medical applications; imaging and spectroscopy. The document presents the papers abstracts. (A.L.B.)

  5. Synchrotron Radiation and Faraday Rotation

    NARCIS (Netherlands)

    Heald, George

    2015-01-01

    Synchrotron radiation and its degree of linear polarization are powerful tracers of magnetic fields that are illuminated by cosmic ray electrons. Faraday rotation of the linearly polarized radiation is induced by intervening line-of-sight magnetic fields that are embedded in ionized plasmas. For

  6. Medical Applications of Synchrotron Radiation

    Science.gov (United States)

    Thomlinson, W.

    1991-10-01

    Ever since the first diagnostic x-ray was done in the United States on February 3, 1896, the application of ionizing radiation to the field of medicine has become increasingly important. Both in clinical medicine and basic research the use of x-rays for diagnostic imaging and radiotherapy is now widespread. Radiography, angiography, CAT and PETT scanning, mammography, and nuclear medicine are all examples of technologies developed to image the human anatomy. In therapeutic applications, both external and internal sources of radiation are applied to the battle against cancer. The development of dedicated synchrotron radiation sources has allowed exciting advances to take place in many of these applications. The new sources provide tunable, high-intensity monochromatic beams over a wide range of energies which can be tailored to specific programmatic needs. This paper surveys those areas of medical research in which synchrotron radiation facilities are actively involved.

  7. Medical applications of synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Thomlinson, W.

    1991-10-01

    Ever since the first diagnostic x-ray was done in the United States on February 3, 1896, the application of ionizing radiation to the field of medicine has become increasingly important. Both in clinical medicine and basic research the use of x-rays for diagnostic imaging and radiotherapy is now widespread. Radiography, angiography, CAT and PETT scanning, mammography, and nuclear medicine are all examples of technologies developed to image the human anatomy. In therapeutic applications, both external and internal sources of radiation are applied to the battle against cancer. The development of dedicated synchrotron radiation sources has allowed exciting advances to take place in many of these applications. The new sources provide tunable, high-intensity monochromatic beams over a wide range of energies which can be tailored to specific programmatic needs. This paper surveys those areas of medical research in which synchrotron radiation facilities are actively involved.

  8. Powder diffraction at ALBA synchrotron

    OpenAIRE

    Aranda, Miguel A. G.

    2017-01-01

    This talk is devoted to explain the uses of powder diffraction at MSPD (material science and powder diffraction) of ALBA synchrotron light source. General characteristics of the beamline are: Station 1 - High Pressure Diffraction on powders with diamond anvil cell (DAC) and CCD detector. Microdiffraction; and Station 2 - High Resolution Powder Diffraction with Multicrystal- and Silicon-Strip detector. Energy Range: 8-50keV; Typical beam size: 4x1mm; all typical sample geometries possible: cap...

  9. Synchrotron Radiation in Life Sciences

    Energy Technology Data Exchange (ETDEWEB)

    Stojanoff, Vivian; Northrup, Paul; Pietri, Ruth; Zhong, Zhong

    2012-05-01

    Synchrotron Radiation (SR) presents itself as a “play-ground” with a large range of methods and techniques suitable to unveil the mysteries of life. Here we attempt to present a few of these methods that complement those employed in the home laboratory. SR diffraction, spectroscopy and imaging methods relevant to the atomic structure determination and characterization of the properties and function of chemical compounds and macromolecules of biological relevance, are introduced.

  10. Synchrotron-driven spallation sources

    CERN Document Server

    Bryant, P J

    1996-01-01

    The use of synchrotrons for pulsed neutron spallation sources is an example of scientific and technological spin-off from the accelerator development for particle physics. Accelerator-driven sources provide an alternative to the continuous-flux, nuclear reactors that currently furnish the majority of neutrons for research and development. Although the present demand for neutrons can be adequately met by the existing reactors, this situation is unlikely to continue due to the increasing severity of safety regulations and the declared policies of many countries to close down their reactors within the next decade or so. Since the demand for neutrons as a research tool is, in any case,expected to grow, there has been a corresponding interest in sources that are synchrotron-driven or linac-driven with a pulse compression ring and currently several design studies are being made. These accelerator-driven sources also have the advantage of a time structure with a high peak neutron flux. The basic requirement is for a...

  11. Sirepo for Synchrotron Radiation Workshop

    Energy Technology Data Exchange (ETDEWEB)

    2016-10-25

    Sirepo is an open source framework for cloud computing. The graphical user interface (GUI) for Sirepo, also known as the client, executes in any HTML5 compliant web browser on any computing platform, including tablets. The client is built in JavaScript, making use of the following open source libraries: Bootstrap, which is fundamental for cross-platform web applications; AngularJS, which provides a model–view–controller (MVC) architecture and GUI components; and D3.js, which provides interactive plots and data-driven transformations. The Sirepo server is built on the following Python technologies: Flask, which is a lightweight framework for web development; Jinja, which is a secure and widely used templating language; and Werkzeug, a utility library that is compliant with the WSGI standard. We use Nginx as the HTTP server and proxy, which provides a scalable event-driven architecture. The physics codes supported by Sirepo execute inside a Docker container. One of the codes supported by Sirepo is the Synchrotron Radiation Workshop (SRW). SRW computes synchrotron radiation from relativistic electrons in arbitrary magnetic fields and propagates the radiation wavefronts through optical beamlines. SRW is open source and is primarily supported by Dr. Oleg Chubar of NSLS-II at Brookhaven National Laboratory.

  12. Compact IR synchrotron beamline design.

    Science.gov (United States)

    Moreno, Thierry

    2017-03-01

    Third-generation storage rings are massively evolving due to the very compact nature of the multi-bend achromat (MBA) lattice which allows amazing decreases of the horizontal electron beam emittance, but leaves very little place for infrared (IR) extraction mirrors to be placed, thus prohibiting traditional IR beamlines. In order to circumvent this apparent restriction, an optimized optical layout directly integrated inside a SOLEIL synchrotron dipole chamber that delivers intense and almost aberration-free beams in the near- to mid-IR domain (1-30 µm) is proposed and analyzed, and which can be integrated into space-restricted MBA rings. Since the optics and chamber are interdependent, the feasibility of this approach depends on a large part on the technical ability to assemble mechanically the optics inside the dipole chamber and control their resulting stability and thermo-mechanical deformation. Acquiring this expertise should allow dipole chambers to provide almost aberration-free IR synchrotron sources on current and `ultimate' MBA storage rings.

  13. Multielemental analysis in organic products and seed of linum by X-ray total reflection fluorescence with synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Serpa, Renata F.B.; Jesus, Edgar F.O. de; Lopes, Ricardo T. [Universidade Federal, Rio de Janeiro, RJ (Brazil). Coordenacao dos Programas de Pos-graduacao de Engenharia. Lab. de Instrumentacao Nuclear]. E-mail: renata@lin.ufrj.br; Carmo, Maria da Graca T. do [Universidade Federal, Rio de Janeiro, RJ (Brazil). Inst. de Nutricao; Moreira, Silvana [Universidade Estadual de Campinas, SP (Brazil). Faculdade de Engenharia Civil]. E-mail: silvana@fec.com.br

    2005-07-01

    The main goal of this study is to determining the trace and major elements levels in organic seeds samples, like soy, rice, bean and in Brazilian and Canadian linum seed by X-ray Total Reflection Fluorescence with Synchrotron Radiation (SR-TXRF). The measurements were carried out in the XRF beamline at the Light Synchrotron National Laboratory (Campinas, Brazil). The organic soy presented major concentrations of P, Ca, Ti, Fe, Ni, Cu, Zn, Br, Rb and Sr than organic bean and rice. Brazilian linum samples presented higher concentrations of S, P, Ca, Ni, Cu, Sr, Zr and Mo than Canadian one, even than organic samples. However potassium, iron and zinc were more pronounced in the Canadian seed of linum (author)

  14. High pressure and synchrotron radiation satellite workshop

    Energy Technology Data Exchange (ETDEWEB)

    Bass, J.; Guignot, N.; Morard, G.; Mezouar, M.; Andrault, D.; Bolfan-Casanova, N.; Sturhahn, W.; Daniel, I.; Reynard, B.; Simionovici, A.; Sanchez Valle, C.; Martinez, I.; Kantor, I.; Dubrovinsky, I.; Mccammon, C.; Dubrovinskaia, N.; Kurnosiv, A.; Kuznetsov, A.; Goncharenko, I.; Loubeyre, P.; Desgreniers, S.; Weck, G.; Yoo, C.S.; Iota, V.; Park, J.; Cynn, H.; Gorelli, F.; Toulemonde, P.; Machon, D.; Merlen, A.; San Miguel, A.; Amboage, M.; Aquilanti, G.; Mathon, O.; Pascarelli, S.; Itie, J.P.; Mcmillan, P.F.; Trapananti, A.; Di Cicco, A.; Panfilis, S. de; Filipponi, A.; Kreisel, J.; Bouvier, P.; Dkhil, B.; Chaabane, B.; Rosner, H.; Koudela, D.; Schwarz, U.; Handestein, A.; Hanfland, M.; Opahle, I.; Koepernik, K.; Kuzmin, M.; Mueller, K.H.; Mydosh, J.; Richter, M.; Hejny, C.; Falconi, S.; Lundegaard, L.F.; Mcmahon, M.I; Loa, I.; Syassen, K.; Wang, X.; Roth, H.; Lorenz, T.; Farber Daniel, I.; Antonangeli Daniele, I.; Krisch, M.; Badro, J.; Fiquet, G.; Occelli, F.; Mao, W.L.; Mao, H.K.; Eng, P.; Kao, C.C.; Shu, J.F.; Hemley, R.J.; Tse, J.S.; Yao, Y.; Deen, P.P.; Paolasini, I.; Braithwaite, D.; Kernavanois, N.; Lapertot, G.; Rupprecht, K.; Leupold, O.; Ponkratz, U.; Wortmann, G.; Beraud, A.; Krisch, M.; Farber, D.; Antonangeli, D.; Aracne, C.; Zarestky, J.L.; Mcqueeney, R.; Mathon, O.; Baudelet, F.; Decremps, F.; Itie, J.P.; Nataf, I.; Pascarelli, S.; Polian, A

    2006-07-01

    The workshop is dedicated to recent advances on science at high pressure at third generation synchrotron sources. A variety of experiments using synchrotron radiation techniques including X-ray diffraction, EXAFS (extended X-ray absorption fine structure), inelastic X-ray scattering, Compton scattering and Moessbauer spectroscopy of crystalline, liquid or amorphous samples, are reported. This document gathers the abstracts of the presentations.

  15. High-Intensity Synchrotron Radiation Effects

    CERN Document Server

    Suetsugu, Y.

    2016-01-01

    Various effects of intense synchrotron radiation on the performance of particle accelerators, especially for storage rings, are discussed. Following a brief introduction to synchrotron radiation, the basic concepts of heat load, gas load, electron emission, and the countermeasures against these effects are discussed.

  16. Funding problems threaten Middle East's synchrotron

    CERN Multimedia

    McCabe, H

    1999-01-01

    Scientists will tour the Middle East to try to raise support for the Synchrotron radiation for Experimental Science and Applications in the Middle East project. The plan is to dismantle and move a decommissioned synchrotron from Berlin to the Middle East where scientists of any nationality would be able to use it (3 paragraphs).

  17. Beer analysis by synchrotron radiation total reflection X-ray fluorescence (SR-TXRF)

    Energy Technology Data Exchange (ETDEWEB)

    Moreira, Silvana [Universidade Estadual de Campinas, SP (Brazil). Faculdade de Engenharia Civil, Arquitetura e Urbanismo. Dept. de Recursos Hidricos]. E-mail: silvana@fec.unicamp.br; Vives, Ana Elisa S. de [Universidade Metodista de Piracicaba (UNIMEP), Santa Barbara D' Oeste, SP (Brazil). Faculdade de Engenharia, Arquitetura e Urbanismo]. E-mail: aesvives@unimep.br; Nascimento Filho, Virgilio F. [Centro de Energia Nuclear na Agricultura (CENA), Piracicaba, SP (Brazil). Lab. de Instrumentacao Nuclear]. E-mail: virgilio@cena.usp.br; Zucchi, Orgheda L.D.A. [Sao Paulo Univ., Ribeirao Preto, SP (Brazil). Faculdade de Ciencias Farmaceuticas de Ribeirao Preto]. E-mail: olzucchi@fcfrp.usp.br

    2005-07-01

    In this work the concentrations of P, S, Cl, K, Ca, Mn, Fe, Zn and Br in twenty-nine brands of national and international beers were determined by Synchrotron Radiation Total Reflection X-Ray Fluorescence analysis (SR-TXRF). The results were compared with the limits established by the Brazilian Legislation and the nutritive values established by National Agricultural Library (NAL). The measurements were performed at the X-ray Fluorescence Beamline at Synchrotron Light Source Laboratory, in Campinas, Sao Paulo, Brazil, using a polychromatic beam for excitation. A small volume of 5 {mu}L of sample beers containing just an internal standard, used to correct geometry effects, were analyzed without any pre-treatment. The measuring time was 100 s and the detection limits obtained varied from 1{mu}g.L{sup -1} for Mn and Fe to 15{mu}g.L{sup -1} for P. (author)

  18. Investigation of mineral distribution in bone by synchrotron X-ray fluorescence microscopy after tibolone therapy

    Energy Technology Data Exchange (ETDEWEB)

    Lima, I. [Rio de Janeiro State Univ., Nova Friburgo, RJ (Brazil). Dept. of Mechanical Engineering and Energy; Federal Univ. of Rio de Janeiro, RJ (Brazil). Nuclear Instrumentation Lab. - COPPE; Carvalho, A.C.B.; Henriques, H.N.; Guzman-Silva, M.A. [Fluminense Federal Univ., Niteroi, RJ (Brazil). Lab. of Experimental Pathology; Sales, E.; Lopes, R.T. [Federal Univ. of Rio de Janeiro, RJ (Brazil). Nuclear Instrumentation Lab. - COPPE; Granjeiro, J.M. [Fluminense Federal Univ., Niteroi, RJ (Brazil). Dept. of Cellular and Molecular Biology

    2011-07-01

    Tibolone is a synthetic steroid with estrogenic, androgenic, and progestagenic properties used for the prevention of postmenopausal osteoporosis and treatment of climacteric symptoms. Tibolone shows almost no action on breast and endometrium, which are target-organs for estrogens and progesterone activity. The aim of this work was to investigate the spatial distribution of calcium and zinc minerals in the femoral head of ovariectomized rat in order to evaluate the effects of the long-term administration of tibolone. For that purpose X-ray microfluorescence was used with synchrotron radiation imaging technique which was performed at Brazilian Light Synchrotron Laboratory, Campinas, SP. Minerals were not homogeneously distributed in trabecular bone areas; a higher concentration of calcium in the trabecular regions at femoral heads was found in ovariectomized and tibolone-treated rats compared to ovariectomized and control groups. (orig.)

  19. Report of the Synchrotron Radiation Vacuum Workshop

    Energy Technology Data Exchange (ETDEWEB)

    Avery, R.T.

    1984-06-01

    The Synchrotron Radiation Vacuum Workshop was held to consider two vacuum-related problems that bear on the design of storage rings and beam lines for synchrotron radiation facilities. These problems are gas desorption from the vacuum chamber walls and carbon deposition on optical components. Participants surveyed existing knowledge on these topics and recommended studies that should be performed as soon as possible to provide more definitive experimental data on these topics. This data will permit optimization of the final design of the Advanced Light Source (ALS) and its associated beam lines. It also should prove useful for other synchrotron radiation facilities as well.

  20. Geological applications of synchrotron radiation

    Science.gov (United States)

    Henderson, C. M. B.; Cressey, G.; Redfern, S. A. T.

    1995-03-01

    Synchrotron-based, Earth sciences research carried out over the last 5 years is reviewed with special attention being given to X-ray absorption studies; X-ray diffraction and X-ray fluorescence microprobe applications are considered more briefly. A comprehensive bibliography is included. The main part of the paper summarizes recent work carried out at the Daresbury SRS. K-edge XAS studies of glasses as models for silicate melts provide information on the local structural environments of Si, Fe 2+ and Fe 3+. By analogy with synthetic "leucites" which contain Fe 2+ and Fe 3+ in tetrahedral framework sites, it seems that many model glasses also contain both oxidation states of Fe in the network, rather than as network modifiers. The structural sites occupied by the minor elements Mn, Zn and Ti in staurolite have been identified using XAFS; Mn and Zn substitute for Fe 2+ in the tetrahedral T2 site, while Ti occupies the distorted M2 octahedral site. L-edge spectroscopy is used to identify the valencies and electronic structures of Mn and Fe in minerals and the Fe 2+:Fe 3+ ratio in a natural spinel is determined. The polarized nature of the synchrotron beam is exploited in determining the Fe X-ray absorption anisotropy in single crystal tourmaline and epidote. XRD powder studies include Rietveld-refinement structure determination and compressibility studies. Synthetic "leucites" having the stoichiometry K 2MgSi 5O 12 have distinctly different structures. The dry-synthesized form is cubic Ia3d with Si and Mg fully disordered on tetrahedral framework sites, while the hydrothermally-synthesized polymorph is monoclinic P2 1/c with Si and Mg fully disordered on, respectively, 10 and 2 tetrahedral sites. The reversible tetragonal to orthorhombic phase transition in gillespite (BaFeSi 4O 10) has been studied in a diamond anvil cell using ED detection and found to occur at 1.2 ± 0.1 GPa. The anomalous compressibility observed has been interpreted in terms of ferroelastic and

  1. National Synchrotron Light Source annual report 1988

    Energy Technology Data Exchange (ETDEWEB)

    Hulbert, S.; Lazarz, N.; Williams, G. (eds.)

    1988-01-01

    This report discusses the experiment done at the National Synchrotron Light Source. Most experiments discussed involves the use of the x-ray beams to study physical properties of solid materials. (LSP)

  2. Molecular photoemission studies using synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Truesdale, C.M.

    1983-04-01

    The angular distributions of photoelectrons and Auger electrons were measured by electron spectroscopy using synchrotron radiation. The experimental results are compared with theoretical calculations to interpret the electronic behavior of photoionization for molecular systems.

  3. Stanford Synchrotron Radiation Light Source (SSRL)

    Data.gov (United States)

    Federal Laboratory Consortium — The SSRL at SLAC National Accelerator Laboratory was built in 1974 to take and use for synchrotron studies the intense x-ray beams from the SPEAR storage ring that...

  4. Synchrotron radiation applications in medical research

    Energy Technology Data Exchange (ETDEWEB)

    Thomlinson, W.

    1997-08-01

    Over the past two decades there has been a phenomenal growth in the number of dedicated synchrotron radiation facilities and a corresponding growth in the number of applications in both basic and applied sciences. The high flux and brightness, tunable beams, time structure and polarization of synchrotron radiation provide an ideal x- ray source for many applications in the medical sciences. There is a dual aspect to the field of medical applications of synchrotron radiation. First there are the important in-vitro programs such as structural biology, x-ray microscopy, and radiation cell biology. Second there are the programs that are ultimately targeted at in-vivo applications. The present status of synchrotron coronary angiography, bronchography, multiple energy computed tomography, mammography and radiation therapy programs at laboratories around the world is reviewed.

  5. Fiber structural analysis by synchrotron radiation

    CERN Document Server

    Kojima, J I; Kikutani, T

    2003-01-01

    Topics of fiber structural analysis by synchrotron radiation are explained. There are only three synchrotron radiation facilities in the world, SPring-8 (Super Photon ring-8) in Japan, APS (Advanced Photon Source) in U.S.A. and ESRF (European Synchrotron Radiation Facility) in France. Online measurement of melt spinning process of PET and Nylon6 is explained in detail. Polypropylene and PBO (poly-p-phenylenebenzobisoxazole) was measured by WAXD (Wide Angle X-ray Diffraction)/SAXS (Small Angle X-ray Scattering) at the same time. Some examples of measure of drawing process of fiber are described. The structure formation process of spider's thread was measured. Micro beam of X-ray of synchrotron facility was improved and it attained to 65nm small angle resolving power by 10 mu m beamsize. (S.Y.)

  6. Precision Calibration of Infrared Synchrotron Radiation Detectors

    CERN Document Server

    Maltsev, A A; Maslova, M V

    2003-01-01

    The technique of calibration of synchrotron radiation precision detectors on a tungsten source based on similarity (close similarity) of character of spectral distributions of synchrotron and thermal radiations is given. The characteristics of various commonly used lamps, used as "standard" ones, are given. The errors of measurements are analyzed. The detectors are intended for absolute measurements of the number of electrons in a ring-shaped bunch.

  7. Brazilian antidoping public policy.

    Science.gov (United States)

    Almeida, Claudio Bispo de; Rodrigues, Deyvis Nascimento

    2014-07-01

    Doping, used to improve sports performance, is legally prohibited. This paper describes Brazilian regulations, resolutions, and Federal laws addressing the issue of doping and antidoping which were collected in 2012 from official websites. We conclude that Brazilian laws have constrained doping, and have been updated over the years to conform to worldwide legal guidelines. Study limitations are noted.

  8. Synchrotron radiation applications in medical research

    Energy Technology Data Exchange (ETDEWEB)

    Thomlinson, W.

    1995-12-31

    The medical projects employing synchrotron radiation as discussed in this paper are, for the most part, still in their infancies and no one can predict the direction in which they will develop. Both the basic research and applied medical programs are sure to be advanced at the new facilities coming on line, especially the ESRF and Spring- 8. However, success is not guaranteed. There is a lot of competition from advances in conventional imaging with the development of digital angiography, computed tomography, functional magnetic resonance imaging and ultrasound. The synchrotron programs will have to provide significant advantages over these modalities in order to be accepted by the medical profession. Advances in image processing and potentially the development of compact sources will be required in order to move the synchrotron developed imaging technologies into the clinical world. In any event, it can be expected that the images produced by the synchrotron technologies will establish ``gold standards`` to be targeted by conventional modalities. A lot more work needs to be done in order to bring synchrotron radiation therapy and surgery to the level of human studies and, subsequently, to clinical applications.

  9. Single electrode electrochemical detection in hybrid poly(dimethylsiloxane)/glass multichannel micro devices

    Energy Technology Data Exchange (ETDEWEB)

    Moreira, Ney Henrique; Almeida, Andre Luis de Jesus de; Piazzeta, Maria Helena de Oliveira; Gobbia, Angelo Luiz [Laboratorio Nacional de Luz Sincrotron (LNLS), Campinas, SP (Brazil). Lab. de Microfabricacao; Jesus, Dosil Pereira de [Instituto Nacional de Ciencia e Tecnologia em Bioanalitica (INCTBio), Campinas, SP (Brazil); Deblire, Ariane; Silva, Jose Alberto Fracassi da [Universidade Estadual de Campinas (IQ/UNICAMP), SP (Brazil). Inst. de Quimica

    2009-07-01

    The fabrication process of a novel multichannel {mu}TAS based on PDMS and glass materials and with fully-integrated electrodes for amperometric detection has been described. Using the facilities of the Microfabrication Lab. (LMF) at Brazilian Synchrotron Light Laboratory (LNLS), soft-lithography, lift-off and O{sub 2} plasma surface activation sealing techniques were employed for rapid proto typing of cost effective PDMS/glass microchips. Fast calibration procedures were possible for the electro oxidation of hydroquinone, thiocyanate, and acetaminophen using Au and Cu electrodes. (author)

  10. Fifth school on Magnetism and Synchrotron Radiation

    CERN Document Server

    Beaurepaire, Eric; Scheurer, Fabrice; Kappler, Jean-Paul; Magnetism and Synchrotron Radiation : New Trends

    2010-01-01

    Advances in the synthesis of new materials with often complex, nano-scaled structures require increasingly sophisticated experimental techniques that can probe the electronic states, the atomic magnetic moments and the magnetic microstructures responsible for the properties of these materials. At the same time, progress in synchrotron radiation techniques has ensured that these light sources remain a key tool of investigation, e.g. synchrotron radiation sources of the third generation are able to support magnetic imaging on a sub-micrometer scale. With the Fifth Mittelwihr School on Magnetism and Synchrotron Radiation the tradition of teaching the state-of-the-art on modern research developments continues and is expressed through the present set of extensive lectures provided in this volume. While primarily aimed at postgraduate students and newcomers to the field, this volume will also benefit researchers and lecturers actively working in the field.

  11. Synchrotron emission from young and nearby pulsars

    Energy Technology Data Exchange (ETDEWEB)

    Kelso, Christopher M. [Department of Physics, University of Chicago, 5720 S. Ellis Ave., Chicago IL 60637 (United States); Hooper, Dan, E-mail: ckelso@uchicago.edu, E-mail: dhooper@fnal.gov [Department of Astronomy and Astrophysics, University of Chicago, 5640 S. Ellis Ave., Chicago IL 60637 (United States)

    2010-05-01

    The rising cosmic ray positron fraction reported by the PAMELA collaboration has lead to a great deal of interest in astrophysical sources of energetic electrons and positrons, including pulsars. In this paper, we calculate the spectrum of synchrotron emission from electrons and positrons injected from 366 young pulsars ( < 10{sup 6} years) contained in the ATNF catalog, and compare our results to observations. We find that if objects such as the Vela and Crab pulsars have injected ∼ 10{sup 48} erg or more in energetic electrons and/or positrons, they are expected to produce bright and distinctive features in the synchrotron sky. Intriguingly, we predict hard synchrotron emission from these regions of the sky which is qualitatively similar to that observed by WMAP.

  12. Synchrotron emission from young and nearby pulsars

    Science.gov (United States)

    Kelso, Christopher M.; Hooper, Dan

    2010-05-01

    The rising cosmic ray positron fraction reported by the PAMELA collaboration has lead to a great deal of interest in astrophysical sources of energetic electrons and positrons, including pulsars. In this paper, we calculate the spectrum of synchrotron emission from electrons and positrons injected from 366 young pulsars ( < 106 years) contained in the ATNF catalog, and compare our results to observations. We find that if objects such as the Vela and Crab pulsars have injected ~ 1048 erg or more in energetic electrons and/or positrons, they are expected to produce bright and distinctive features in the synchrotron sky. Intriguingly, we predict hard synchrotron emission from these regions of the sky which is qualitatively similar to that observed by WMAP.

  13. Chemical applications of synchrotron radiation: Workshop report

    Energy Technology Data Exchange (ETDEWEB)

    1989-04-01

    The most recent in a series of topical meetings for Advanced Photon Source user subgroups, the Workshop on Chemical Applications of Synchrotron Radiation (held at Argonne National Laboratory, October 3-4, 1988) dealt with surfaces and kinetics, spectroscopy, small-angle scattering, diffraction, and topography and imaging. The primary objectives were to provide an educational resource for the chemistry community on the scientific research being conducted at existing synchrotron sources and to indicate some of the unique opportunities that will be made available with the Advanced Photon Source. The workshop organizers were also interested in gauging the interest of chemists in the field of synchrotron radiation. Interest expressed at the meeting has led to initial steps toward formation of a Chemistry Users Group at the APS. Individual projects are processed separately for the data bases.

  14. Automation and Remote Synchrotron Data Collection

    Science.gov (United States)

    Gilski, M.

    2008-08-01

    X-ray crystallography is the natural choice for macromolecular structure determination by virtue of its accuracy, speed, and potential for further speed gains, while synchrotron radiation is indispensable because of its intensity and tuneability. Good X-ray crystallographic diffraction patterns are essential and frequently this is achievable through using the few large synchrotrons located worldwide. Beamline time on these facilities have long queues, and increasing the efficiency of utilization of these facilities will help in expediting the structure determination process. Automation and remote data collection are therefore essential steps in ensuring that macromolecular structure determination becomes a very high throughput process.

  15. 12 Experimental Techniques at Synchrotron Lightsource Beamlines

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Peter L [US Department of Energy Office of Science Office Basic Energy Sciences; Rhyne, James J [US Department of Energy Office of Science Office of Basic Energy Sciences

    2015-01-01

    The unique properties of synchrotron radiation are its continuous spectrum, high flux and brightness, and high coherence, which make it an indispensable tool in the exploration of matter. The wavelengths of the emitted photons span a range of dimensions from the atomic level to biological cells, thereby providing incisive probes for advanced research in materials science, physical and chemical sciences, metrology, geosciences, environmental sciences, biosciences, medical sciences, and pharmaceutical sciences. The features of synchrotron radiation are especially well matched to the needs of nanoscience.

  16. Synchrotron characterization of functional tin dioxide nanowires

    Energy Technology Data Exchange (ETDEWEB)

    Domashevskaya, E. P., E-mail: ftt@phys.vsu.ru; Chuvenkova, O. A.; Turishchev, S. Yu. [Voronezh State University, Voronezh (Russian Federation)

    2015-12-31

    Wire-like crystals of tin dioxide were synthesized by a gas-transport technique. The wires, of mainly nanometric diameters, were characterized by spectroscopy and microscopy techniques with the use of highly brilliant and intense synchrotron radiation. We studied the influence of the surface chemical state and the oxygen vacancies on the atomic and electronic structure of the nanowires. The surface of the nanowires is covered by a few nanometers of tin suboxides. The lack of oxygen over the surface layers leads to specific sub-zone formation in a gap, as shown by synchrotron studies.

  17. What is a synchrotron and why does Australia need one?

    CERN Document Server

    Nugent, K A

    2002-01-01

    Construction of a $157 million synchrotron will soon begin in Melbourne. The author describes what this facility means for Australian science. The Australian synchrotron is a third generation device. The facility would have the capacity to do a wide range of science and technology at the same time. A number of applications, which are the priority for the Australian synchrotron project are briefly described. The huge technological spin-offs of this knowledge have made synchrotrons an attractive proposition to state governments

  18. Wellcome Trust backs Rutherford to host synchrotron

    CERN Document Server

    Leder, N

    1999-01-01

    The Wellcome Trust has stated its preference for the site of the new Anglo-French synchrotron to be at RAL in Oxfordshire. But the statement coincides with an announcement from the UK government that a decision on the location of 'Diamond' will be delayed to allow two new reports on the canditate sites to be commissioned (1/2 page).

  19. Biological applications of synchrotron radiation infrared spectromicroscopy.

    Science.gov (United States)

    Marcelli, Augusto; Cricenti, Antonio; Kwiatek, Wojciech M; Petibois, Cyril

    2012-01-01

    Extremely brilliant infrared (IR) beams provided by synchrotron radiation sources are now routinely used in many facilities with available commercial spectrometers coupled to IR microscopes. Using these intense non-thermal sources, a brilliance two or three order of magnitude higher than a conventional source is achievable through small pinholes (infrared biological imaging covers a wide range of fundamental issues and applied researches such as cell imaging or tissue imaging. Molecular maps with a spatial resolution down to the diffraction limit may be now obtained with a synchrotron radiation IR source also on thick samples. Moreover, changes of the protein structure are detectable in an IR spectrum and cellular molecular markers can be identified and used to recognize a pathological status of a tissue. Molecular structure and functions are strongly correlated and this aspect is particularly relevant for imaging. We will show that the brilliance of synchrotron radiation IR sources may enhance the sensitivity of a molecular signal obtained from small biosamples, e.g., a single cell, containing extremely small amounts of organic matter. We will also show that SR IR sources allow to study chemical composition and to identify the distribution of organic molecules in cells at submicron resolution is possible with a high signal-to-noise ratio. Moreover, the recent availability of two-dimensional IR detectors promises to push forward imaging capabilities in the time domain. Indeed, with a high current synchrotron radiation facility and a Focal Plane Array the chemical imaging of individual cells can be obtained in a few minutes. Within this framework important results are expected in the next years using synchrotron radiation and Free Electron Laser (FEL) sources for spectro-microscopy and spectral-imaging, alone or in combination with Scanning Near-field Optical Microscopy methods to study the molecular composition and dynamic changes in samples of biomedical interest

  20. Brazilian Consensus on Photoprotection

    Science.gov (United States)

    Schalka, Sérgio; Steiner, Denise; Ravelli, Flávia Naranjo; Steiner, Tatiana; Terena, Aripuanã Cobério; Marçon, Carolina Reato; Ayres, Eloisa Leis; Addor, Flávia Alvim Sant'anna; Miot, Helio Amante; Ponzio, Humberto; Duarte, Ida; Neffá, Jane; da Cunha, José Antônio Jabur; Boza, Juliana Catucci; Samorano, Luciana de Paula; Corrêa, Marcelo de Paula; Maia, Marcus; Nasser, Nilton; Leite, Olga Maria Rodrigues Ribeiro; Lopes, Otávio Sergio; Oliveira, Pedro Dantas; Meyer, Renata Leal Bregunci; Cestari, Tânia; dos Reis, Vitor Manoel Silva; Rego, Vitória Regina Pedreira de Almeida

    2014-01-01

    Brazil is a country of continental dimensions with a large heterogeneity of climates and massive mixing of the population. Almost the entire national territory is located between the Equator and the Tropic of Capricorn, and the Earth axial tilt to the south certainly makes Brazil one of the countries of the world with greater extent of land in proximity to the sun. The Brazilian coastline, where most of its population lives, is more than 8,500 km long. Due to geographic characteristics and cultural trends, Brazilians are among the peoples with the highest annual exposure to the sun. Epidemiological data show a continuing increase in the incidence of non-melanoma and melanoma skin cancers. Photoprotection can be understood as a set of measures aimed at reducing sun exposure and at preventing the development of acute and chronic actinic damage. Due to the peculiarities of Brazilian territory and culture, it would not be advisable to replicate the concepts of photoprotection from other developed countries, places with completely different climates and populations. Thus the Brazilian Society of Dermatology has developed the Brazilian Consensus on Photoprotection, the first official document on photoprotection developed in Brazil for Brazilians, with recommendations on matters involving photoprotection. PMID:25761256

  1. Indigenous Brazilian Management Practices

    Directory of Open Access Journals (Sweden)

    Zandra Balbinot

    2012-12-01

    Full Text Available The present research seeks to understand to what extent companies in emerging countries, specifically, Brazilian, adopt dominant management practices, the so-called Euro-American practices, possess their one, or show a syncretism between the two. Methods: Mixed research. One phase was to collect data using a survey about cultural dimensions adopted from GLOBE (House 1998 management practices and also from Brazilian academy. Another was to collect data through interviews, which were analyzed in parallel. Results: Of the seven dominant cultural dimensions, indigenous practices influenced two. Another three were influenced by dominant management practices. Two of the local dimensions, even with internationalization, merged practices with Brazilian cultural traits. Even so, the practices derived from Jeitinho diminished relative to the international relations and experience of managers. Conclusions: The paper shows the existence of powerful Brazilian Indigenous Managerial Practices such as personalism and formalism. These practices have great influence on international business negotiations. On the other hand, it also shows that there are still dominant managerial practices specially in the case of more internationalized Brazilian managers

  2. Synchrotron Applications of High Magnetic Fields

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2006-07-01

    This workshop aims at discussing the scientific potential of X-ray diffraction and spectroscopy in magnetic fields above 30 T. Pulsed magnetic fields in the range of 30 to 40 T have recently become available at Spring-8 and the ESRF (European synchrotron radiation facility). This document gathers the transparencies of the 6 following presentations: 1) pulsed magnetic fields at ESRF: first results; 2) X-ray spectroscopy and diffraction experiments by using mini-coils: applications to valence state transition and frustrated magnet; 3) R{sub 5}(Si{sub x}Ge{sub 1-x}){sub 4}: an ideal system to be studied in X-ray under high magnetic field?; 4) high field studies at the Advanced Photon Source: present status and future plans; 5) synchrotron X-ray diffraction studies under extreme conditions; and 6) projects for pulsed and steady high magnetic fields at the ESRF.

  3. Acceleration by synchrotron absorption and superluminal sources

    Energy Technology Data Exchange (ETDEWEB)

    Ghisellini, G.; Bodo, G.; Trussoni, E.; Rees, M.J. (Torino Osservatorio Astronomico, Turin (Italy) Cambridge Univ. (England))

    1990-10-01

    A magnetized blob, containing relativistic electrons, can absorb, by the synchrotron process, low-frequency photons emitted by an underlying source. The momentum of the adsorbed photons can accelerate the blob to relativistic velocities. The final bulk Lorentz factor can be as large as required by observations of superluminal sources even if only the low-frequency part of the spectrum of a sub-Eddington central source is used for the acceleration process, and even if the blob contains an equal number of protons and electrons. This is mainly due to the large absorption cross section of the synchrotron process with respect to the electron scattering cross section, but partly because strongly aberrated photons are seen blueshifted in the rest frame of the blob and are less efficiently absorbed, reducing the importance of the braking force due to the radiation drag. 12 refs.

  4. Calculation of coherent synchrotron radiation using mesh

    Directory of Open Access Journals (Sweden)

    T. Agoh

    2004-05-01

    Full Text Available We develop a new method to simulate coherent synchrotron radiation numerically. It is based on the mesh calculation of the electromagnetic field in the frequency domain. We make an approximation in the Maxwell equation which allows a mesh size much larger than the relevant wavelength so that the computing time is tolerable. Using the equation, we can perform a mesh calculation of coherent synchrotron radiation in transient states with shielding effects by the vacuum chamber. The simulation results obtained by this method are compared with analytic solutions. Though, for the comparison with theories, we adopt simplifications such as longitudinal Gaussian distribution, zero-width transverse distribution, horizontal uniform bend, and a vacuum chamber with rectangular cross section, the method is applicable to general cases.

  5. Single-mode coherent synchrotron radiation instability

    Directory of Open Access Journals (Sweden)

    S. Heifets

    2003-06-01

    Full Text Available The microwave instability driven by the coherent synchrotron radiation (CSR has been previously studied [S. Heifets and G. V. Stupakov, Phys. Rev. ST Accel. Beams 5, 054402 (2002] neglecting effect of the shielding caused by the finite beam pipe aperture. In practice, the unstable mode can be close to the shielding threshold where the spectrum of the radiation in a toroidal beam pipe is discrete. In this paper, the CSR instability is studied in the case when it is driven by a single synchronous mode. A system of equations for the beam-wave interaction is derived and its similarity to the 1D free-electron laser theory is demonstrated. In the linear regime, the growth rate of the instability is obtained and a transition to the case of continuous spectrum is discussed. The nonlinear evolution of the single-mode instability, both with and without synchrotron damping and quantum diffusion, is also studied.

  6. The Prototype Synchrotron Radiation Detector (PSRD)

    CERN Document Server

    Anderhub, H; Baumgartner, S; Biland, A; Camps, C; Capell, M; Commichau, V; Djambazov, L; Fanchiang, Y J; Flügge, G; Grimm, O; Gunten, H P V; Hangarter, K; Hofer, H; Kan, R; Kenney, G; Koutsenko, V F; Kraeber, M; Kuipers, J; Lebedev, A; Lee, S C; Ren, D; Ren, Z L; Röser, U; Ting, Samuel C C; Tiwari, A; Viertel, Gert M; Waldmeier-Wicki, S; Wang, T S; Zimmermann, B

    2002-01-01

    The components of the PSRD, a detector to study the flux of X-rays and charged particles in the keV-MeV energy range in outer space, are described. The device is a precursor for the Synchrotron Radiation Detector, which is one of the detector components of the Alpha Magnetic Spectrometer (AMS02). The AMS02 will be operated for several years on the International Space Station.

  7. The Prototype Synchrotron Radiation Detector (PSRD)

    Energy Technology Data Exchange (ETDEWEB)

    Anderhub, H.; Baetzner, D.; Baumgartner, S.; Biland, A.; Camps, C.; Capell, M.; Commichau, V.; Djambazov, L.; Fanchiang, Y.-J.; Fluegge, G.; Grimm, O.; Hangarter, K.; Hofer, H.; Kan, R.; Kenney, G.; Koutsenko, V.; Kraeber, M.; Kuipers, J.; Lebedev, A.; Lee, S.-C.; Ren, D.; Ren, Z.L.; Roeser, U.; Ting, Samuel C.C.; Tiwari, A.; Viertel, G.M. E-mail: gert.viertel@cern.ch; Gunten, H.P. von; Waldmeier Wicki, S.; Wang, T.-S.; Zimmermann, B

    2002-02-01

    The components of the PSRD, a detector to study the flux of X-rays and charged particles in the keV-MeV energy range in outer space, are described. The device is a precursor for the Synchrotron Radiation Detector, which is one of the detector components of the Alpha Magnetic Spectrometer (AMS02). The AMS02 will be operated for several years on the International Space Station.

  8. Structural analysis with high brilliance synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Ohno, Hideo [Japan Atomic Energy Research Inst., Kamigori, Hyogo (Japan). Kansai Research Establishment

    1997-11-01

    The research subjects in diffraction and scattering of materials with high brilliance synchrotron radiation such as SPring-8 (Super Photon ring 8 GeV) are summarized. The SPring-8 project is going well and 10 public beamlines will be opened for all users in October, 1997. Three JAERI beamlines are also under construction for researches of heavy element science, physical and structural properties under extreme conditions such as high temperature and high pressure. (author)

  9. Synchrotron Imaging Assessment of Bone Quality.

    Science.gov (United States)

    Ma, Shaocheng; Boughton, Oliver; Karunaratne, Angelo; Jin, Andi; Cobb, Justin; Hansen, Ulrich; Abel, Richard

    Bone is a complex hierarchical structure, and its principal function is to resist mechanical forces and fracture. Bone strength depends not only on the quantity of bone tissue but also on the shape and hierarchical structure. The hierarchical levels are interrelated, especially the micro-architecture, collagen and mineral components; hence, analysis of their specific roles in bone strength and stiffness is difficult. Synchrotron imaging technologies including micro-CT and small/wide angle X-ray scattering/diffraction are becoming increasingly popular for studying bone because the images can resolve deformations in the micro-architecture and collagen-mineral matrix under in situ mechanical loading. Synchrotron cannot be directly applied in vivo due to the high radiation dose but will allow researchers to carry out systematic multifaceted studies of bone ex vivo. Identifying characteristics of aging and disease will underpin future efforts to generate novel devices and interventional therapies for assessing and promoting healthy aging. With our own research work as examples, this paper introduces how synchrotron imaging technology can be used with in situ testing in bone research.

  10. Synchrotron radiation: its characteristics and applications

    Energy Technology Data Exchange (ETDEWEB)

    Blewett, J. P.; Chasman, R.; Green, G. K.

    1977-01-01

    It has been known for a century that charged particles radiate when accelerated and that relativistic electrons in the energy range between 100 MeV and several GeV and constrained to travel in circular orbits emit concentrated, intense beams with broad continuous spectra that can cover the electromagnetic spectrum from infrared through hard X-rays. Recently the possible applications of this radiation have been appreciated and electron synchrotrons and electron storage rings are now being used in many centers for studies of the properties of matter in the solid, liquid and gaseous states. A brief history is presented of ''synchrotron radiation'' as it is now called. The basic properties of this radiation are described and the world-wide distribution is indicated of facilities for its production. Particular attention is given to the proposed facility at Brookhaven which will be the first major installation to be dedicated only to the production and use of synchrotron radiation. Finally, typical examples are given of applications in the areas of radiation absorption studies, techniques based on scattering of radiation, and advances based on X-ray lithography.

  11. MICROANALYSIS OF MATERIALS USING SYNCHROTRON RADIATION.

    Energy Technology Data Exchange (ETDEWEB)

    JONES,K.W.; FENG,H.

    2000-12-01

    High intensity synchrotron radiation produces photons with wavelengths that extend from the infrared to hard x rays with energies of hundreds of keV with uniquely high photon intensities that can be used to determine the composition and properties of materials using a variety of techniques. Most of these techniques represent extensions of earlier work performed with ordinary tube-type x-ray sources. The properties of the synchrotron source such as the continuous range of energy, high degree of photon polarization, pulsed beams, and photon flux many orders of magnitude higher than from x-ray tubes have made possible major advances in the possible chemical applications. We describe here ways that materials analyses can be made using the high intensity beams for measurements with small beam sizes and/or high detection sensitivity. The relevant characteristics of synchrotron x-ray sources are briefly summarized to give an idea of the x-ray parameters to be exploited. The experimental techniques considered include x-ray fluorescence, absorption, and diffraction. Examples of typical experimental apparatus used in these experiments are considered together with descriptions of actual applications.

  12. Tabletop synchrotron and its unique features

    CERN Document Server

    Yamada, H

    2002-01-01

    Two synchrotrons, AURORA and MIRRORCLE, were built in Ritsumeikan University. MIRRORCLE-20 is the smallest normal conduction synchrotron (15 cm orbit radius and 1.2 m outer diameter) in the world. It uses 2/3 resonance method for electron beam incidence but is not optimized for X-ray generation. MIRRORCLE-6 shall be optimized for X-ray generation. X-ray generated by MIRRORCLE shows very flat white light, rich in hard X-ray, pulse with width changeable from a few mu s to a few ms , wide radiation angle of 25 mrad at MIRRORCLE-20 and 80 mrad at MIRRORCLE-8 and high coherence. The feature such as pulsed light and high coherence is expected to new application which photon radiation cannot practice. Imaging experiments by MIRRORCLE were carried out by Cu plate, Al plate, Teflon and acryl plate. We took a photograph of insect, electric lamp, connector, and cyclotron. New X-ray generation mechanism, X-ray strength, development of tabletop synchrotron and features of X-ray beam are explained. (S.Y.)

  13. 50 Years of synchrotrons Adams' Memorial lecture

    CERN Document Server

    Lawson, J D; CERN. Geneva

    1996-01-01

    Fifty years ago Frank Goward of the Atomic Energy Research Establishment Group at Malvern converted a small American betatron to make the worldÕs first synchrotron. At the same time Marcus Oliphant was planning to build at Birmingham a large proton machine with a ring magnet and variable magnetic field. Ideas for this had come to him during night-shifts tending the electromagnetic separators at Oak Ridge during the war. Some seven years later, in 1953, a group gathered together in Geneva to build the PS. A major contributor to the design work which had made this possible was John Adams. An account of some of the achievements in these eventful years will be presented. CERN has built nine synchrotrons/colliders and two temporary test rings. Eight machines are still running. The review will start with the PS, the first proton synchrotron based on the alternating gradient principle invented in 1952 at BNL. The design work of the PS team, under the enlightened leadership of J.B. Adams, and the construction of the...

  14. A novel approach to synchrotron radiation simulation

    CERN Document Server

    Trad, G; Goldblatt, A; Mazzoni, S; Roncarolo, F

    2014-01-01

    At the Large Hadron Collider (LHC) at CERN, synchrotron radiation (SR) is used to continuously monitor the transverse properties of the beams. Unfortunately the machine and beam parameters are such that the useful radiation emitted inside a separation dipole, chosen as source, is diffraction limited heavily affecting the accuracy of the measurement. In order to deconvolve the diffraction effects from the acquired beam images and in order to design an alternative monitor based on a double slit interferometer an extensive study of the synchrotron light source and of the optical propagation has been made. This study is based on simulations combining together several existing tools: SRW for the source, ZEMAX for the transport and MATLAB for the “glue” and analysis of the results. The resulting tool is very powerful and can be easily adapted to other synchrotron radiation problems. In this paper the simulation package and the way it is used will be described as well as the results obtained for the LHC and SPS.

  15. New synchrotron radiation facility project. Panel on new synchrotron radiation facility project

    CERN Document Server

    Sato, S; Kimura, Y

    2003-01-01

    The project for constructing a new synchrotron radiation facility dedicated to the science in VUV (or EUV) and Soft X-ray (SX) region has been discussed for these two years at the Panel on New Synchrotron Radiation Facility Project. The Panel together with the Accelerator Design Working Group (WG), Beamline Design WG and Research Program WG suggested to the Ministry of Education, Science, Culture and Sports the construction of a 1.8 GeV electron storage ring suitable for 'Top-Up' operation and beamlines and monochromators designed for undulator radiation. The scientific programs proposed by nationwide scientists are summarized with their requirements of the characteristics of the beam. (author)

  16. Evaluation of osteoporotic bone structure through synchrotron radiation X-ray microfluorescence images

    Energy Technology Data Exchange (ETDEWEB)

    Lima, I. [Nuclear Engineering Program/COPPE/UFRJ, P.O. Box 68509, Av. Horacio Macedo 2030, Sala I-133, Cidade Universitaria, 21941-914 Rio de Janeiro, RJ (Brazil)], E-mail: inaya@lin.ufrj.br; Anjos, M.J. [Nuclear Engineering Program/COPPE/UFRJ, P.O. Box 68509, Av. Horacio Macedo 2030, Sala I-133, Cidade Universitaria, 21941-914 Rio de Janeiro, RJ (Brazil); Physics Institute, UERJ (Brazil); Farias, M.L.F. [University Hospital, UFRJ (Brazil); Pantaleao, T.U.; Correa da Costa, V.M. [Biophysics Institute, UFRJ (Brazil); Lopes, R.T. [Nuclear Engineering Program/COPPE/UFRJ, P.O. Box 68509, Av. Horacio Macedo 2030, Sala I-133, Cidade Universitaria, 21941-914 Rio de Janeiro, RJ (Brazil)

    2008-12-15

    The abnormal accumulation or deficiency of trace elements may theoretically impair the formation of bone and contribute to osteoporosis. In this context, the knowledge of major and trace elements is very important in order to clarify many issues regarding diseases of the bone, such as osteoporosis, that remain unresolved. Several kinds of imaging techniques can be useful to access morphology and the minerals present in osteoporotic bones. In this work, synchrotron radiation X-ray microfluorescence was used as an X-ray imaging technique to investigate bone structures. Therefore, this research aims to improve the knowledge about some aspects of bone quality. The measurements were carried out at the Brazilian Synchrotron Laboratory Light Laboratory, in Brazil. A white beam with an energy range of 4-23 keV, a 45 deg./45 deg. geometry and a capillary optics were used. It was demonstrated that bone quality can and must be evaluated not only by considering the architecture of bones but also by taking into account the concentration and the distribution of minerals. Our results showed that the elemental distributions in bone zones on a micron scale were very helpful to understand functions in those structures.

  17. Atomic photoelectron-spectroscopy studies using synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Kobrin, P.H.

    1983-02-01

    Photoelectron spectroscopy combined with tunable synchrotron radiation has been used to study the photoionization process in several atomic systems. The time structure of the synchrotron radiation source at the Stanford Synchrotron Radiation Laboratory (SSRL) was used to record time-of-flight (TOF) photoelectron spectra of gaseous Cd, Hg, Ne, Ar, Ba, and Mn. The use of two TOF analyzers made possible the measurement of photoelectron angular distributions as well as branching ratios and partial cross sections.

  18. Synchrotron radiation photoionization mass spectrometry of laser ablated species

    OpenAIRE

    Alvarez Ruiz, Jesus; Casu, A.; Coreno, M.; De Simone, M.; Hoyos Campos, L.M.; Juarez-Reyes, A.M.; Kivimäki, A.; Orlando, S.; Sanz, M.; Spezzani, C.; Stankiewicz, M; Trucchi, D. M.

    2010-01-01

    The present paper describes an experimental apparatus suitable to create and study free clusters by combining laser ablation and synchrotron radiation. First tests on sulfur samples, S, showed the production, through laser ablation, of neutral Sn clusters (n = 1–8). These clusters were ionized using synchrotron radiation at photon energies from 160 eV to 175 eV, across the S 2p core edge. The feasibility of such combined ablation–synchrotron radiation experiments is demonstrated, opening new ...

  19. Bystander Effects During Synchrotron Imaging Procedures?

    Science.gov (United States)

    Schültke, Elisabeth; Bewer, Brian; Wysokinski, Tomasz; Chapman, Dean; Nikkhah, Guido

    2010-07-01

    Using monochromatic beam and synchrotron phase-contrast technique at the biomedical beamline of the Italian synchrotron facility Elettra (SYRMEP), we have shown in a small animal model of malignant brain tumor that it is possible to obtain high-resolution images of very small tumors when they have developed from implanted tumor cells loaded with colloidal gold nanoparticles (GNP). All previous experiments were conducted in post-mortem samples. We have now designed a cell culture experiment to investigate the effects of synchrotron radiation with an energy and dose profile similar to that expected in our first in vivo imaging studies according to the protocol developed at SYRMEP. Materials and Methods: Culture flasks containing either gold-loaded or naïve C6 glioma cells were exposed to a dose of 0.5 Gy at 24 keV. The irradiated medium was aspirated and replaced with fresh growth medium. Twenty-four hours later this non-irradiated medium exposed to irradiated cells was aspirated, then added to non-irradiated C6 cells in order to investigate whether bystander effects are seen under the conditions of our image acquisition protocol. The irradiated medium was added to a number of other non-irradiated cell cultures. Cell counts were followed until 72 hrs after irradiation. Western blots were conducted with H2AX antibodies. This experiment was one of the first biomedical experiments conducted at BMIT, the new biomedical imaging and therapy beamline of the Canadian Light Source. Results: No significant differences in proliferation were seen between cells that were directly irradiated, exposed to irradiated medium or exposed to the non-irradiated 24-hr-medium from the irradiated cells. However, there was a tendency towards a higher number of double strand breaks in previously irradiated cells when they were exposed to non-irradiated medium that had been in contact with irradiated cells for 24 hrs.

  20. Laser synchrotron radiation and beam cooling

    Energy Technology Data Exchange (ETDEWEB)

    Esarey, E.; Sprangle, P.; Ting, A. [Naval Research Lab., Washington, DC (United States)] [and others

    1995-12-31

    The interaction of intense {approx_gt} 10{sup 18} W/cm{sup 2}, short pulse ({approx_lt} 1 ps) lasers with electron beams and plasmas can lead to the generation of harmonic radiation by several mechanisms. Laser synchrotron radiation may provide a practical method for generating tunable, near monochromatic, well collimated, short pulse x-rays in compact, relatively inexpensive source. The mechanism for the generation of laser synchrotron radiation is nonlinear Thomson scattering. Short wavelengths can be generated via Thomson scattering by two methods, (i) backscattering from relativistic electron beams, in which the radiation frequency is upshifted by the relativistic factor 4{gamma}{sup 2}, and (ii) harmonic scattering, in which a multitude of harmonics are generated with harmonic numbers extending out to the critical harmonic number nc{approx_equal}a{sub 0}{sup 3} {much_gt} 1, where a{sub 0} {approx_equal}10{sup -9}{lambda}I{sup 1/2}, {lambda} is the laser wavelength in {mu}m and I is the laser intensity in W/cm{sup 2}. Laser synchrotron sources are capable of generating short ({approx_lt} ps) x-ray pulses with high peak flux ({approx_gt} 10{sup 21} photons/s) and brightness ({approx_gt}{sup 19} photons/s-mm{sup 2}-mrad{sup 2} 0.1%BW. As the electron beam radiates via Thomson scattering, it can subsequently be cooled, i.e., the beam emittance and energy spread can be reduced. This cooling can occur on rapid ({approximately} ps) time scales. In addition, electron distributions with sufficiently small axial energy spreads can be used to generate coherent XUV radiation via a laser-pumped FEL mechanism.

  1. Synchrotron light and its uses. [Historical review

    Energy Technology Data Exchange (ETDEWEB)

    Blewett, J P

    1978-01-01

    It was known for a century that charged particles radiate when accelerated and that relativistic electrons in the energy range between 100 MeV and several GeV and constrained to travel in circular orbits emit concentrated, intense beams with broad continuous spectra that can cover the electromagnetic spectrum from infrared through hard x-rays. Recently the possible applications of this radiation were appreciated and electron synchrotrons and electron storage rings are now being used in many centers for studies of the properties of matter in the solid, liquid and gaseous states. 10 references.

  2. Ampicillin Trihydrate from Synchrotron Powder Diffraction Data

    Energy Technology Data Exchange (ETDEWEB)

    Burley,J.; van de Streek, J.; Stephens, P.

    2006-01-01

    The crystal structure of ampicillin trihydrate {l_brace}systematic name: 6-[D(-)-{alpha}-aminophenylacetamido]penicillanic acid trihydrate{r_brace}, C{sub 16}H{sub 19}N{sub 3}O{sub 4}S{center_dot}3H{sub 2}O, a broad-spectrum {beta}-lactam antibiotic of the aminopenicillin type, has been determined from synchrotron X-ray powder diffraction data. The three water molecules form an infinite hydrogen-bonded chain through the crystal structure, with hydrogen bonds to the NH{sub 3}{sup +}, COO{sup -}, C{double_bond}O and NH groups of the ampicillin molecules.

  3. Handbook on synchrotron radiation, v.2

    CERN Document Server

    1987-01-01

    Volume 2 of this series concentrates on the use of synchrotron radiation which covers that region of the electromagnetic spectrum which extends from about 10eV to 3keV in photon energy and is essentially the region where the radiation is strongly absorbed by atmospheric gases. It therefore has to make extensive use of a high vacuum to transport the radiation to the workstation where the presence of hard X-rays can cause extensive damage to both the optics and the targets used in the experimental rigs. The topics chosen for this volume have been limited to the disciplines of physics and chemi

  4. Variable-Period Undulators For Synchrotron Radiation

    Energy Technology Data Exchange (ETDEWEB)

    Shenoy, Gopal (Naperville, IL); Lewellen, John (Plainfield, IL); Shu, Deming (Darien, IL); Vinokurov, Nikolai (Novosibirsk, RU)

    2005-02-22

    A new and improved undulator design is provided that enables a variable period length for the production of synchrotron radiation from both medium-energy and high-energy storage rings. The variable period length is achieved using a staggered array of pole pieces made up of high permeability material, permanent magnet material, or an electromagnetic structure. The pole pieces are separated by a variable width space. The sum of the variable width space and the pole width would therefore define the period of the undulator. Features and advantages of the invention include broad photon energy tunability, constant power operation and constant brilliance operation.

  5. Variable-Period Undulators for Synchrotron Radiation

    Energy Technology Data Exchange (ETDEWEB)

    Shenoy, Gopal; Lewellen, John; Shu, Deming; Vinokurov, Nikolai

    2005-02-22

    A new and improved undulator design is provided that enables a variable period length for the production of synchrotron radiation from both medium-energy and high energy storage rings. The variable period length is achieved using a staggered array of pole pieces made up of high permeability material, permanent magnet material, or an electromagnetic structure. The pole pieces are separated by a variable width space. The sum of the variable width space and the pole width would therefore define the period of the undulator. Features and advantages of the invention include broad photon energy tunability, constant power operation and constant brilliance operation.

  6. Glancing angle synchrotron X-ray diffraction

    Energy Technology Data Exchange (ETDEWEB)

    Cernik, R.J. [Daresbury Lab., Warrington, WA (United States)

    1996-09-01

    This paper describes in basic detail some of the techniques that can be used to study thin films and surfaces. These are all in the X-ray region and cover reflectivity, diffraction form polycrystalline films, textured films and single crystal films. Other effects such as fluorescence and diffuse scattering are mentioned but not discussed in detail. Two examples of the reflectivity from multilayers and the diffraction from iron oxide films are discussed. The advantages of the synchrotron for these studies is stressed and the experimental geometries that can be employed are described i detail. A brief bibliography is provided at the end to accompany this part of the 1996 Frascati school.

  7. The synchrotron radiation angiography program at the national synchrotron light source

    Energy Technology Data Exchange (ETDEWEB)

    Thomlinson, W.; Gmuer, N.

    1987-01-01

    The National Synchrotron Light Source (NSLS) angiography program is under development. The program is a collaboration between the Stanford University Angiography Project and the NSLS. A 180 m/sup 2/ clinical facility has been built. A beam line is being constructed to utilize a superconducting wiggler radiation source. Projected start-up date for the NSLS program is Summer 1988.

  8. Cold Collisions in a Molecular Synchrotron

    Science.gov (United States)

    van der Poel, Aernout P. P.; Zieger, Peter C.; van de Meerakker, Sebastiaan Y. T.; Loreau, Jérôme; van der Avoird, Ad; Bethlem, Hendrick L.

    2018-01-01

    We study collisions between neutral, deuterated ammonia molecules (ND3 ) stored in a 50 cm diameter synchrotron and argon atoms in copropagating supersonic beams. The advantages of using a synchrotron in collision studies are twofold: (i) By storing ammonia molecules many round-trips, the sensitivity to collisions is greatly enhanced; (ii) the collision partners move in the same direction as the stored molecules, resulting in low collision energies. We tune the collision energy in three different ways: by varying the velocity of the stored ammonia packets, by varying the temperature of the pulsed valve that releases the argon atoms, and by varying the timing between the supersonic argon beam and the stored ammonia packets. These give consistent results. We determine the relative, total, integrated cross section for ND3+Ar collisions in the energy range of 40 - 140 cm-1 , with a resolution of 5 - 10 cm-1 and an uncertainty of 7%-15%. Our measurements are in good agreement with theoretical scattering calculations.

  9. Undulators as sources of synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Krinsky, S.

    1983-01-01

    At the present time the first generation of facilities having electron storage rings designed for and dedicated to synchrotron radiation research are beginning operations in the US, Europe and Japan. The use of wigglers and undulators as enhanced sources of synchrotron radiation plays an important role at all these facilities. Moreover, recently there has been much activity in the design of the next generation machines, which will place even greater, and perhaps exclusive, emphasis on the use of wigglers and undulators. The operation of these insertion devices has been made even more attractive by advances in the design and construction of permanent magnet wigglers and undulators. This reliable and economical technology eliminates the need for more complex superconducting magnets, except to achieve very high magnetic fields for the production of hard photons from relatively low energy rings. We review the spectral properties of the radiation, emphasizing the complementary aspects of time- and frequency-domain analyses. We next study the brightness of the undulator source. Finally, we consider some limitations associated with operating an undulator in a storage ring.

  10. Infrared synchrotron radiation instrumentation and applications

    Science.gov (United States)

    Hirschmugl, Carol

    1992-08-01

    Infrared synchrotron radiation (IRSR) is a blossoming field which has three working beamlines, U41R at the National Synchrotron Light Source, Brookhaven National Laboratory, USA, and two at the Institute of Molecular Sciences in Okasaki, Japan, with extensive research projects. There are also several new beamlines in the planning and development stages, both in the United States and abroad. IRSR offers a unique way to access the far infrared (30 μm to ˜ 1mm), which is a notoriously difficult region to work in. In particular, experiments that demand high brightness are well suited to IRSR just as they are in the X-ray region. The central issue in all of the experiments to date has been good signal to noise, which has been the focus of the instrumentation improvements at the U41R beamline. A commercial Fourier transform instrument was the chosen spectrometer. Then modifications were made in order to expand the usable region of the existing experiments, in both the far and near infrared. As an example of the performance of this beamline, I will focus on the reflection absorption spectroscopy results for adsorbates on clean surfaces in ultrahigh vacuum.

  11. Beam halo collimation in heavy ion synchrotrons

    Directory of Open Access Journals (Sweden)

    I. Strašík

    2015-08-01

    Full Text Available This paper presents a systematic study of the halo collimation of ion beams from proton up to uranium in synchrotrons. The projected Facility for Antiproton and Ion Research synchrotron SIS100 is used as a reference case. The concepts are separated into fully stripped (e.g., ^{238}U^{92+} and partially stripped (e.g., ^{238}U^{28+} ion collimation. An application of the two-stage betatron collimation system, well established for proton accelerators, is intended also for fully stripped ions. The two-stage system consists of a primary collimator (a scattering foil and secondary collimators (bulky absorbers. Interaction of the particles with the primary collimator (scattering, momentum losses, and nuclear interactions was simulated by using fluka. Particle-tracking simulations were performed by using mad-x. Finally, the dependence of the collimation efficiency on the primary ion species was determined. The influence of the collimation system adjustment, lattice imperfections, and beam parameters was estimated. The concept for the collimation of partially stripped ions employs a thin stripping foil in order to change their charge state. These ions are subsequently deflected towards a dump location using a beam optical element. The charge state distribution after the stripping foil was obtained from global. The ions were tracked by using mad–x.

  12. Mapping prehistoric ghosts in the synchrotron

    Energy Technology Data Exchange (ETDEWEB)

    Edwards, N.P.; Wogelius, R.A. [University of Manchester, School of Earth, Atmospheric, and Environmental Sciences, Manchester (United Kingdom); University of Manchester, Williamson Research Centre for Molecular Environmental Science, Manchester (United Kingdom); Bergmann, U. [SLAC National Accelerator Laboratory, Linac Coherent Light Source, Menlo Park, CA (United States); Larson, P. [Black Hills Institute of Geological Research, Inc., Hill City, SD (United States); Sellers, W.I. [University of Manchester, Faculty of Life Sciences, Manchester (United Kingdom); Manning, P.L. [University of Manchester, School of Earth, Atmospheric, and Environmental Sciences, Manchester (United Kingdom); University of Manchester, Williamson Research Centre for Molecular Environmental Science, Manchester (United Kingdom); University of Pennsylvania, Department of Earth and Environmental Science, Philadelphia, PA (United States)

    2013-04-15

    The detailed chemical analysis of fossils has the potential to reveal great insight to the composition, preservation and biochemistry of ancient life. Such analyses would ideally identify, quantify, and spatially resolve the chemical composition of preserved bone and soft tissue structures, but also the embedding matrix. Mapping the chemistry of a fossil in situ can place constraints on mass transfer between the enclosing matrix and the preserved organism(s), and therefore aid in distinguishing taphonomic processes from original chemical zonation remnant within the fossils themselves. Conventional analytical methods, such as scanning electron microscopy (SEM) and pyrolysis-gas chromatography/mass spectrometry (Py-GC/MS) have serious limitations in this case, primarily, an inability to provide large (i.e., decimeter) scale chemical maps. Additionally, vacuum chamber size and the need for destructive sampling preclude analysis of large and precious fossil specimens. However, the recent development of Synchrotron Rapid Scanning X-ray Fluorescence (SRS-XRF) at the Stanford Synchrotron Radiation Lightsource (SSRL) allows the non-destructive chemical analysis and imaging of major, minor, and trace element concentrations of large paleontological and archeological specimens in rapid scanning times. Here we present elemental maps of a fossil reptile produced using the new SRS-XRF method. Our results unequivocally show that preserved biological structures are not simply impressions or carbonized remains, but possess a remnant of the original organismal biochemistry. We show that SRS-XRF is a powerful new tool for the study of paleontological and archaeological samples. (orig.)

  13. Synchrotrons for hadron therapy: Part I

    CERN Document Server

    Badano, L; Bryant, P; Crescenti, M; Holy, P; Knaus, P; Maier, A; Pullia, M; Rossi, S

    1999-01-01

    The treatment of cancer with accelerator beams has a long history with betatrons, linacs, cyclotrons and now synchrotrons being exploited for this purpose. Treatment techniques can be broadly divided into the use of spread-out beams and scanned 'pencil' beams. The Bragg-peak behaviour of hadrons makes them ideal candidates for the latter. The combination of precisely focused 'pencil' beams with controllable penetration (Bragg peak) and high, radio-biological efficiency (light ions) opens the way to treating the more awkward tumours that are radio-resistant, complex in shape and lodged against critical organs. To accelerate light ions (probably carbon) with pulse-to-pulse energy variation, a synchrotron is the natural choice. The beam scanning system is controlled via an on-line measurement of the particle flux entering the patient and, for this reason, the beam spill must be extended in time (seconds) by a slow-extraction scheme. The quality of the dose intensity profile ultimately depends on the uniformity o...

  14. Synchrotrons for hadron therapy, part 1

    CERN Document Server

    Badano, L; Bryant, P J; Crescenti, M; Holy, P; Knaus, P; Maier, A T; Pullia, M; Rossi, S

    1999-01-01

    The treatment of cancer with accelerator beams has a long history with linacs, cyclotrons and now synchrotrons being exploited for this purpose. Treatment techniques can be broadly divided into the use of spread-out beams and scanned 'pencil' beams. The Bragg-peak behaviour of hadrons makes them ideal candidates for the latter. The combination of precisely focused 'pencil' beams with controllable penetration (Bragg peak) and high, radio-biological efficiency (light ions) opens the way to treating the more awkward tumours that are radio-resistant, complex in shape and lodged against critical organs. To accelerate light ions (probably carbon) with pulse-to-pulse energy variation, a synchrotron is the natural choice. The beam scanning system is controlled via an on-line measurement of the particle flux entering the patient and, for this reason, the beam spill must be extended in time (seconds) by a slow-extraction scheme. The quality of the dose intensity profile ultimately depends on the uniformity of the beam ...

  15. Ferroelectrics under the Synchrotron Light: A Review

    Science.gov (United States)

    Fuentes-Cobas, Luis E.; Montero-Cabrera, María E.; Pardo, Lorena; Fuentes-Montero, Luis

    2015-01-01

    Currently, an intensive search for high-performance lead-free ferroelectric materials is taking place. ABO3 perovskites (A = Ba, Bi, Ca, K and Na; B = Fe, Nb, Ti, and Zr) appear as promising candidates. Understanding the structure–function relationship is mandatory, and, in this field, the roles of long- and short-range crystal orders and interactions are decisive. In this review, recent advances in the global and local characterization of ferroelectric materials by synchrotron light diffraction, scattering and absorption are analyzed. Single- and poly-crystal synchrotron diffraction studies allow high-resolution investigations regarding the long-range average position of ions and subtle global symmetry break-downs. Ferroelectric materials, under the action of electric fields, undergo crystal symmetry, crystallite/domain orientation distribution and strain condition transformations. Methodological aspects of monitoring these processes are discussed. Two-dimensional diffraction clarify larger scale ordering: polycrystal texture is measured from the intensities distribution along the Debye rings. Local order is investigated by diffuse scattering (DS) and X-ray absorption fine structure (XAFS) experiments. DS provides information about thermal, chemical and displacive low-dimensional disorders. XAFS investigation of ferroelectrics reveals local B-cation off-centering and oxidation state. This technique has the advantage of being element-selective. Representative reports of the mentioned studies are described. PMID:28787814

  16. Ferroelectrics under the Synchrotron Light: A Review

    Directory of Open Access Journals (Sweden)

    Luis E. Fuentes-Cobas

    2015-12-01

    Full Text Available Currently, an intensive search for high-performance lead-free ferroelectric materials is taking place. ABO3 perovskites (A = Ba, Bi, Ca, K and Na; B = Fe, Nb, Ti, and Zr appear as promising candidates. Understanding the structure–function relationship is mandatory, and, in this field, the roles of long- and short-range crystal orders and interactions are decisive. In this review, recent advances in the global and local characterization of ferroelectric materials by synchrotron light diffraction, scattering and absorption are analyzed. Single- and poly-crystal synchrotron diffraction studies allow high-resolution investigations regarding the long-range average position of ions and subtle global symmetry break-downs. Ferroelectric materials, under the action of electric fields, undergo crystal symmetry, crystallite/domain orientation distribution and strain condition transformations. Methodological aspects of monitoring these processes are discussed. Two-dimensional diffraction clarify larger scale ordering: polycrystal texture is measured from the intensities distribution along the Debye rings. Local order is investigated by diffuse scattering (DS and X-ray absorption fine structure (XAFS experiments. DS provides information about thermal, chemical and displacive low-dimensional disorders. XAFS investigation of ferroelectrics reveals local B-cation off-centering and oxidation state. This technique has the advantage of being element-selective. Representative reports of the mentioned studies are described.

  17. Synchrotron radiation in art and archaeology SRA 2005

    Energy Technology Data Exchange (ETDEWEB)

    Pollard, A.M.; Janssens, K.; Artioli, G.; Young, M.L.; Casadio, F.; Schnepp, S.; Marvin, J.; Dunand, D.C.; Almer, J.; Fezzaa, K.; Lee, W.K.; Haeffner, D.R.; Reguer, S.; Dillmann, Ph.; Mirambet, F.; Susini, J.; Lagarde, P.; Pradell, T.; Molera, J.; Brunetti, B.; D' acapito, F.; Maurizio, C.; Mazzoldi, P.; Padovani, S.; Sgamellotti, A.; Garges, F.; Etcheverry, M.P.; Flank, A.M.; Lagarde, P.; Marcus, M.A.; Scheidegger, A.M.; Grolimund, D.; Pallot-Frossard, I.; Smith, A.D.; Jones, M.; Gliozzo, E.; Memmi-Turbanti, I.; Molera, J.; Vendrell, M.; Mcconachie, G.; Skinner, T.; Kirkman, I.W.; Pantos, E.; Wallert, A.; Kanngiesser, B.; Hahn, O.; Wilke, M.; NekaT, B.; Malzer, W.; Erko, A.; Chalmin, E.; Vignaud, C.; Farges, F.; Susini, J.; Menu, M.; Sandstrom, M.; Cotte, M.; Kennedy, C.J.; Wess, T.J.; Muller, M.; Murphy, B.; Roberts, M.A.; Burghammer, M.; Riekel, C.; Gunneweg, J.; Pantos, E.; Dik, J.; Tafforeau, P.; Boistel, R.; Boller, E.; Bravin, A.; Brunet, M.; Chaimanee, Y.; Cloetens, P.; Feist, M.; Hoszowska, J.; Jaeger, J.J.; Kay, R.F.; Lazzari, V.; Marivaux, L.; Nel, A.; Nemoz, C.; Thibault, X.; Vignaud, P.; Zabler, S.; Sciau, P.; Goudeau, P.; Tamura, N.; Doormee, E.; Kockelmann, W.; Adriaens, A.; Ryck, I. de; Leyssens, K.; Hochleitner, B.; Schreiner, M.; Drakopoulos, M.; Snigireva, I.; Snigirev, A.; Sanchez Del Rio, M.; Martinetto, P.; Dooryhee, E.; Suarez, M.; Sodo, A.; Reyes-Valerio, C.; Haro Poniatowski, E.; Picquart, M.; Lima, E.; Reguera, E.; Gunneweg, J.; Reiche, I.; Berger, A.; Bevers, H.; Duval, A

    2005-07-01

    Materials - bones, artifacts, artwork,.... - lie at the heart of both archaeology and art conservation. Synchrotron radiation techniques provide powerful ways to interrogate these records of our physical and cultural past. In this workshop we will discuss and explore the current and potential applications of synchrotron radiation science to problems in archaeology and art conservation. This document gathers the abstracts of the presentations.

  18. Enhancing the accelerated beam current in the booster synchrotron ...

    Indian Academy of Sciences (India)

    Based on these measured beam parameters, beam optics of a transport line was optimized and its results are alsodiscussed in this paper. This beam transport line is used to transport the electron beam from the 20MeV microtron to the booster synchrotron. The booster synchrotron works as a main injector for Indus-1 and ...

  19. Low frequency interference between short synchrotron radiation sources

    Directory of Open Access Journals (Sweden)

    F. Méot

    2001-06-01

    Full Text Available A recently developed analytical formalism describing low frequency far-field synchrotron radiation (SR is applied to the calculation of spectral angular radiation densities from interfering short sources (edge, short magnet. This is illustrated by analytical calculation of synchrotron radiation from various assemblies of short dipoles, including an “isolated” highest density infrared SR source.

  20. Current status and perspectives of synchrotron radiation in medicine

    Energy Technology Data Exchange (ETDEWEB)

    Thomlinson, W.

    1996-11-01

    The high flux and brightness, tunable beams, time structure and polarization of synchrotron radiation provide an ideal x-ray source for many medical applications. The present status of synchrotron angiography, multiple energy computed tomography, mammography and radiation therapy at laboratories around the world is reviewed and some future projections for these applications are addressed.

  1. A comparative study of the spectra recorded at RRCAT synchrotron ...

    Indian Academy of Sciences (India)

    The aim of the present work is to make a comparative study of the EXAFS spectra recorded at the BL-8 dispersive EXAFS beamline at 2 GeV Indus-2 synchrotron source at RRCAT, Indore (India) with those recorded at other synchrotron EXAFS beamlines, viz., X-19A at NSLS, BNL (USA), EXAFS wiggler beamline 4-1 at the ...

  2. A synchrotron radiation facility for x-ray astronomy

    DEFF Research Database (Denmark)

    Hall, C.J.; Lewis, R.A.; Christensen, Finn Erland

    1997-01-01

    A proposal for an x-ray optics test facility based at a synchrotron radiation source is presented. The facility would incorporate a clean preparation area, and a large evacuable test area. The advantages of using a synchrotron as the source of the test radiation are discussed. These include the a...

  3. Third generation synchrotron radiation applied to materials science

    Energy Technology Data Exchange (ETDEWEB)

    Kaufmann, E.N.; Yun, W.

    1993-11-01

    Utility of synchrotron radiation for characterization of materials and ramifications of availability of new third-generation, high-energy, high-intensity sources of synchrotron radiation are discussed. Examples are given of power of x-ray analysis techniques to be expected with these new machines.

  4. The Brazilian School Principals

    Directory of Open Access Journals (Sweden)

    Ângelo Ricardo de Souza

    2007-09-01

    Full Text Available This article discusses the policy nature of school principal, considering the thoughts of many authors about school administration and the debate about politics, power and burocracy. The study still presents a profile of Brazilian school principals with the data of Basic Education Evaluation System – SAEB, of 2003, specially comparing elements about gender, experience and formation of school principals, and aspects linked with methodology to provide/indicate the school principal and its possible democratic vocation.

  5. Brazilian Trichoptera Checklist II

    Directory of Open Access Journals (Sweden)

    Henrique Paprocki

    2014-10-01

    Full Text Available A second assessment of Brazilian Trichoptera species records is presented here. A total of 625 species were recorded for Brazil. This represents an increase of 65.34% new species recorded during the last decade. The Hydropsychidae (124 spp., followed by the Hydroptilidae (102 spp. and Polycentropodidae (97 spp., are the families with the greatest richness recorded for Brazil. The knowledge on Trichoptera biodiversity in Brazil is geographically unequal. The majority of the species is recorded for the southeastern region.

  6. BRAZILIAN NEWS PORTALS CHARACTERISTICS

    Directory of Open Access Journals (Sweden)

    Heloiza G. Herckovitz

    2011-02-01

    Full Text Available A content analysis of four Brazilian news media portals found that economic news dominated the top headlines with little attention paid to education, the environment and welfare. Other trends included a focus on local events and national news sources, reliance on few sources, mostly official ones, and a low percentage of news that fitted the concept of newsworthiness (a combination of both social significance and deviance concepts. Other findings of a study of 432 top news stories published by UOL, Estadão, iG and Terra during a 15-day period between February and March 2008 indicate that the top portions of the portals’ front pages carry news that lacks story depth, editorial branding, and multimedia applications. The results suggest that online news portals are in their infancy although Brazil has the largest online population of Latin America. This study hopes to shed light on the gatekeeping process in Brazilian news portals. Brazilian media portals have yet to become a significant editorial force able to provide knowledge about social issues and public affairs in a socially responsible fashione.

  7. Comments on Landau damping due to synchrotron frequency spread

    Energy Technology Data Exchange (ETDEWEB)

    Ng, K.Y.; /Fermilab

    2005-01-01

    An inductive/space-charge impedance shifts the synchrotron frequency downwards above/below transition, but it is often said that the coherent synchrotron frequency of the bunch is not shifted in the rigid-dipole mode. On the other hand, the incoherent synchrotron frequency due to the sinusoidal rf always spreads in the downward direction. This spread will therefore not be able to cover the coherent synchrotron frequency, implying that there will not be any Landau damping no matter how large the frequency spread is. By studying the dispersion relation, it is shown that the above argument is incorrect, and there will be Landau damping if there is sufficient frequency spread. The main reason is that the coherent frequency of the rigid-dipole mode will no longer remain unshifted in the presence of a synchrotron frequency spread.

  8. Illuminating magma shearing processes via synchrotron imaging

    Science.gov (United States)

    Lavallée, Yan; Cai, Biao; Coats, Rebecca; Kendrick, Jackie E.; von Aulock, Felix W.; Wallace, Paul A.; Le Gall, Nolwenn; Godinho, Jose; Dobson, Katherine; Atwood, Robert; Holness, Marian; Lee, Peter D.

    2017-04-01

    Our understanding of geomaterial behaviour and processes has long fallen short due to inaccessibility into material as "something" happens. In volcanology, research strategies have increasingly sought to illuminate the subsurface of materials at all scales, from the use of muon tomography to image the inside of volcanoes to the use of seismic tomography to image magmatic bodies in the crust, and most recently, we have added synchrotron-based x-ray tomography to image the inside of material as we test it under controlled conditions. Here, we will explore some of the novel findings made on the evolution of magma during shearing. These will include observations and discussions of magma flow and failure as well as petrological reaction kinetics.

  9. 3D Detectors for Synchrotron Applications

    CERN Document Server

    Pennicard, D

    2009-01-01

    3D detectors are a novel variety of photodiode radiation detector, invented by Parker, Kenney and Segal (1997). Instead of having n- and p-type contacts on the front and back surfaces of a silicon substrate, like a standard photodiode, they have columns of doped material passing through the thickness of the silicon. This structure means that the detector can combine a reasonable substrate thickness with a very small electrode spacing, resulting in a low depletion voltage, fast charge collection and low charge sharing. These detectors have a couple of promising applications. Their fast charge collection and low depletion voltage should make them very radiation-tolerant. So, they could be used for future particle physics experiments at the Super Large Hadron Collider (SLHC), where high levels of radiation damage are expected. Also, their low charge sharing means they could potentially improve X-ray diffraction measurements at synchrotrons such as Diamond Light Source. This would allow these experiments, for exa...

  10. Galactic synchrotron emission from astrophysical electrons

    Science.gov (United States)

    Lineros, Roberto A.; Bringmann, Torsten; Donato, Fiorenza

    2012-07-01

    The interaction between the galactic magnetic field and the non-thermal population of electrons is responsible for a large part of the radio sky from 10 MHz up to several GHz. This population is mostly composed of electrons with primary and secondary origin. Cosmic ray propagation models describe their evolution in space and energy, and allow to study the impact on the radio sky in intensity and morphology at different frequencies. We consider different propagation models and test their compatibility with available radio maps. We find models highly consistent both with B/C data, the local electron flux and synchrotron emission observations. The resulting constraints on propagation models could significantly improve prospects for indirect dark matter searches in these channels and, even more so, in antiprotons.

  11. The tomography beamline ANATOMIX at Synchrotron SOLEIL

    Science.gov (United States)

    Weitkamp, T.; Scheel, M.; Giorgetta, JL; Joyet, V.; Le Roux, V.; Cauchon, G.; Moreno, T.; Polack, F.; Thompson, A.; Samama, JP

    2017-06-01

    ANATOMIX is a 200-m-long undulator beamline for full-field tomography techniques at photon energies from 5 to 25 keV. It is currently under construction at Synchrotron SOLEIL, the French national light source near Paris. ANATOMIX will feature experimental stations both for parallel-beam microtomography (with a beam of up to 40 mm width) and for zone-plate transmission X-ray microscopy (down to pixel sizes of 30 nm) in absorption and phase contrast. The location of ANATOMIX on a canted straight section of the SOLEIL storage ring implies specific challenges for the design and operation conditions of the beamline. In this paper we present general design aspects and the status of construction.

  12. Optical substrate materials for synchrotron radiation beamlines

    Energy Technology Data Exchange (ETDEWEB)

    Howells, M.R. [Lawrence Berkeley National Lab., CA (United States). Advanced Light Source; Paquin, R.A. [Univ. of Arizona, Tucson, AZ (United States). Optical Sciences Center

    1997-06-01

    The authors consider the materials choices available for making optical substrates for synchrotron radiation beam lines. They find that currently the optical surfaces can only be polished to the required finish in fused silica and other glasses, silicon, CVD silicon carbide, electroless nickel and 17-4 PH stainless steel. Substrates must therefore be made of one of these materials or of a metal that can be coated with electroless nickel. In the context of material choices for mirrors they explore the issues of dimensional stability, polishing, bending, cooling, and manufacturing strategy. They conclude that metals are best from an engineering and cost standpoint while the ceramics are best from a polishing standpoint. They then give discussions of specific materials as follows: silicon carbide, silicon, electroless nickel, Glidcop{trademark}, aluminum, precipitation-hardening stainless steel, mild steel, invar and superinvar. Finally they summarize conclusions and propose ideas for further research.

  13. A guide to synchrotron radiation science

    CERN Document Server

    Sato, Shigeru; Munro, Ian; Lodha, G S

    2015-01-01

    Synchrotron Radiation (SR), as a light source is now in use around the world to provide brilliant radiation from the infrared into the soft and hard X-ray regions. It is an indispensible and essential tool to establish the physic-chemical characteristics of materials and surfaces from an atomic and molecular view point. It is being applied to topics which range from mineralogy to protein crystallography, embracing research in areas from the physical to the life sciences. This new guide is a concise yet comprehensive and easily readable introduction to an expanding area of science. It presents in a readily assimilable form the basic concepts of SR science from its generation principles, through source design and operation to the principles of instruments for SR exploitation followed by a survey of its actual applications in selected research fields, including spectroscopy, diffractometry, microanalysis and chemical processing.

  14. Quadrupole magnet for a rapid cycling synchrotron

    Energy Technology Data Exchange (ETDEWEB)

    Witte, H. [Brookhaven National Lab. (BNL), Upton, NY (United States); Berg, J. S. [Brookhaven National Lab. (BNL), Upton, NY (United States)

    2015-05-03

    Rapid Cycling Synchrotrons (RCS) feature interleaved warm and cold dipole magnets; the field of the warm magnets is used to modulate the average bending field depending on the particle energy. It has been shown that RCS can be an attractive option for fast acceleration of particles, for example, muons, which decay quickly. In previous studies it was demonstrated that in principle warm dipole magnets can be designed which can provide the required ramp rates, which are equivalent to frequencies of about 1 kHz. To reduce the losses it is beneficial to employ two separate materials for the yoke; it was also shown that by employing an optimized excitation coil geometry the eddy current losses are acceptable. In this paper we show that the same principles can be applied to quadrupole magnets targeting 30 T/m with a repetition rate of 1kHz and good field quality.

  15. The Alba synchrotron; El sincrotron Alba

    Energy Technology Data Exchange (ETDEWEB)

    Bolufer-Mayans, P.

    2009-07-01

    ALBA is a giant microscope, that will be formally open in 2010, Cerdanyola del Valles, Barcelona. It has a cost of 201 millions of Euros and it belongs to the third generation of synchrotrons. Thermal stability is guarantied by not going beyond 0, 5 degree centigrade. The light is produced by intensive electrons up to ultra relative speeds. ALBA will be able to get more than 30 independent light lines for experimentation. Each line characteristic is defined by different variables; font's nature (a bending magnet) and the optic (focus, chromates, energetic level). ALBA's light is polarized by different states: lineal polarization horizontal or vertical type, circular and intermediate geometric. The generated light will allow precise observations upon atomic and molecular structures. It will also improve pure and applied science in the molecular biology branch (protein and virus structure). (Author)

  16. Helical magnetized wiggler for synchrotron radiation laser

    CERN Document Server

    Wang Mei; Hirshfield, J L

    1999-01-01

    A helical magnetized iron wiggler has been built for a novel infrared synchrotron radiation laser (SRL) experiment. The wiggler consists of four periods of helical iron structure immersed in a solenoid field. This wiggler is to impart transverse velocity to a prebunched 6 MeV electron beam, and thus to obtain a desired high orbit pitch ratio for the SRL. Field tapering at beam entrance is considered and tested on a similar wiggler. Analytic and simulated characteristics of wigglers of this type are discussed and the performance of the fabricated wigglers is demonstrated experimentally. A 4.7 kG peak field was measured for a 6.4 mm air gap and a 5.4 cm wiggler period at a 20 kG solenoid field. The measured helical fields compare favorably with the analytical solution. This type of helical iron wigglers has the potential to be scaled to small periods with strong field amplitude.

  17. Silicon Pixel Detectors for Synchrotron Applications

    CERN Document Server

    Stewart, Graeme Douglas

    Recent advances in particle accelerators have increased the demands being placed on detectors. Novel detector designs are being implemented in many different areas including, for example, high luminosity experiments at the LHC or at next generation synchrotrons. The purpose of this thesis was to characterise some of these novel detectors. The first of the new detector types is called a 3D detector. This design was first proposed by Parker, Kenney and Segal (1997). In this design, doped electrodes are created that extend through the silicon substrate. When compared to a traditional photodiode with electrodes on the opposing surfaces, the 3D design can combine a reasonable detector thickness with a small electrode spacing resulting in fast charge collection and limited charge sharing. The small electrode spacing leads to the detectors having lower depletion voltages. This, combined with the fast collection time, makes 3D detectors a candidate for radiation hard applications. These applications include the upgra...

  18. Further notes on Brazilian Conidae

    NARCIS (Netherlands)

    Mol, van J.-J.; Tursch, B.; Kempf, M.

    1971-01-01

    Since the publication of a survey of brazilian Conidae (Van Moll et al., 1967) new extensive dredgings effected by one of us (M.K.) along considerable portions of the Brazilian coast have brought a rich material allowing us to add to the previous work and to correct certain opinions therein

  19. 3 GeV Booster Synchrotron Conceptual Design Report

    Energy Technology Data Exchange (ETDEWEB)

    Wiedemann, Helmut

    2009-06-02

    Synchrotron light cna be produced from a relativistic particle beam circulating in a storage ring at extremely high intensity and brilliance over a large spectral region reaching from the far infrared regime to hard x-rays. The particles, either electrons or positrons, radiate as they are deflected in the fields of the storage ring bending magnets or of magnets specially optimized for the production of synchrotron light. The synchrotron light being very intense and well collimated in the forward direction has become a major tool in a large variety of research fields in physics, chemistry, material science, biology, and medicine.

  20. Longitudinal emittance control in high intensity proton synchrotrons

    Energy Technology Data Exchange (ETDEWEB)

    Shinto, K.; Takagi, A.; Machida, S.; Yoshii, M.; Mori, Y.; Koba, K. [High Energy Accelerator Research Organization, Tsukuba, Ibaraki (Japan)

    1998-11-01

    Experiments of synchrotron injection using the direct fast chopped H{sup -} beam extracted from a surface-plasma-type H{sup -} ion source has been successfully achieved. The injection phase of the fast chopped beam from linac into the booster synchrotron is adjustable to the center of rf bucket by using this beam. It was obtained that the longitudinal emittance was controlled at the extraction of the booster synchrotron, and that the beam loss during the injection into main ring of the KEK-PS was reduced by this fast chopped beam. (author)

  1. X-ray microfluorescence analysis of pigments in decorative paintings from the sarcophagus cartonnage of an Egyptian mummy

    Science.gov (United States)

    Calza, C.; Anjos, M. J.; de Souza, S. M. F. Mendonça; Brancaglion, A.; Lopes, R. T.

    2007-10-01

    This work characterized the elemental composition of the pigments used in decorative paintings from the sarcophagus cartonnage fragments of an Egyptian mummy, using μXRF with Synchrotron Radiation. This female mummy (n.158) is considered one of the most important pieces of the National Museum (Rio de Janeiro, Brazil) because of its unconventional embalming with legs and arms swathed separately. The measurements were performed at the XRF beamline D09B of the Brazilian Synchrotron Light Laboratory (LNLS), using white beam and a Si(Li) detector with resolution of 165 eV at 5.9 keV. The elements found in the samples were: Si, S, Cl, K, Ca, Ti, Cr, Mn, Fe, Ni, Cu, Zn, As, Sr, Hg and Pb.

  2. X-ray microfluorescence analysis of pigments in decorative paintings from the sarcophagus cartonnage of an Egyptian mummy

    Energy Technology Data Exchange (ETDEWEB)

    Calza, C. [Nuclear Instrumentation Laboratory, COPPE/UFRJ, P.O. Box 68509, 21941-972 Rio de Janeiro (Brazil)], E-mail: ccalza@lin.ufrj.br; Anjos, M.J. [Nuclear Instrumentation Laboratory, COPPE/UFRJ, P.O. Box 68509, 21941-972 Rio de Janeiro (Brazil); Physics Institute, UERJ, Rio de Janeiro (Brazil); Mendonca de Souza, S.M.F. [National Museum, UFRJ, Rio de Janeiro (Brazil); Oswaldo Cruz Foundation, ENSP, Rio de Janeiro (Brazil); Brancaglion, A. [National Museum, UFRJ, Rio de Janeiro (Brazil); Lopes, R.T. [Nuclear Instrumentation Laboratory, COPPE/UFRJ, P.O. Box 68509, 21941-972 Rio de Janeiro (Brazil)

    2007-10-15

    This work characterized the elemental composition of the pigments used in decorative paintings from the sarcophagus cartonnage fragments of an Egyptian mummy, using {mu}XRF with Synchrotron Radiation. This female mummy (n.158) is considered one of the most important pieces of the National Museum (Rio de Janeiro, Brazil) because of its unconventional embalming with legs and arms swathed separately. The measurements were performed at the XRF beamline D09B of the Brazilian Synchrotron Light Laboratory (LNLS), using white beam and a Si(Li) detector with resolution of 165 eV at 5.9 keV. The elements found in the samples were: Si, S, Cl, K, Ca, Ti, Cr, Mn, Fe, Ni, Cu, Zn, As, Sr, Hg and Pb.

  3. SYNCHROTRON HEATING BY A FAST RADIO BURST IN A SELF-ABSORBED SYNCHROTRON NEBULA AND ITS OBSERVATIONAL SIGNATURE

    Energy Technology Data Exchange (ETDEWEB)

    Yang, Yuan-Pei; Dai, Zi-Gao [School of Astronomy and Space Science, Nanjing University, Nanjing 210093 (China); Zhang, Bing, E-mail: zhang@physics.unlv.edu [Department of Physics and Astronomy, University of Nevada, Las Vegas, NV 89154 (United States)

    2016-03-01

    Fast radio bursts (FRBs) are mysterious transient sources. If extragalactic, as suggested by their relative large dispersion measures, their brightness temperatures must be extremely high. Some FRB models (e.g., young pulsar model, magnetar giant flare model, or supra-massive neutron star collapse model) suggest that they may be associated with a synchrotron nebula. Here we study a synchrotron-heating process by an FRB in a self-absorbed synchrotron nebula. If the FRB frequency is below the synchrotron self-absorption frequency of the nebula, electrons in the nebula would absorb FRB photons, leading to a harder electron spectrum and enhanced self-absorbed synchrotron emission. In the meantime, the FRB flux is absorbed by the nebula electrons. We calculate the spectra of FRB-heated synchrotron nebulae, and show that the nebula spectra would show a significant hump in several decades near the self-absorption frequency. Identifying such a spectral feature would reveal an embedded FRB in a synchrotron nebula.

  4. Brazilian Nanotechnology Initiative

    Science.gov (United States)

    Fazzio, Adalberto

    2015-03-01

    In Brazil there is intense research activity in nanotechnology, most of these developed in universities and research institutes. The Brazilian Nanotechnology Initiative (BNI) aims to integrate government actions to promote the competitiveness of the Brazilian industry. This initiative is founded on support for research and development in the laboratories of the National Laboratories for Nanotechnology (SisNANO), starting from an improvement in infrastructure and opening of laboratories for users of academia and business, promoting interaction and transfer knowledge between academia and business. Country currently has 26 thematic networks of nanotechnology, 16 -Virtual-National Institutes of Technology, seven National- Laboratories and 18 Associate Laboratories, which comprise the SisNANO. Seeking to expand and share governance with other government actors, the Interministries Committee for Nanotechnology was set up, composed of 10 ministries, and has the task of coordinating the entire program of the Federal Government Nanotechnology.Cooperation activities are an important part of BNI. Currently Brazil has cooperation programs with U.S., China, Canada and European Union among others. Recently, Brazil decided to join the European NanoReg program where 60 research groups are joining efforts to provide protocols and standards that can help regulatory agencies and governments.

  5. Multiple energy synchrotron biomedical imaging system.

    Science.gov (United States)

    Bassey, B; Martinson, M; Samadi, N; Belev, G; Karanfil, C; Qi, P; Chapman, D

    2016-12-07

    A multiple energy imaging system that can extract multiple endogenous or induced contrast materials as well as water and bone images would be ideal for imaging of biological subjects. The continuous spectrum available from synchrotron light facilities provides a nearly perfect source for multiple energy x-ray imaging. A novel multiple energy x-ray imaging system, which prepares a horizontally focused polychromatic x-ray beam, has been developed at the BioMedical Imaging and Therapy bend magnet beamline at the Canadian Light Source. The imaging system is made up of a cylindrically bent Laue single silicon (5,1,1) crystal monochromator, scanning and positioning stages for the subjects, flat panel (area) detector, and a data acquisition and control system. Depending on the crystal's bent radius, reflection type, and the horizontal beam width of the filtered synchrotron radiation (20-50 keV) used, the size and spectral energy range of the focused beam prepared varied. For example, with a bent radius of 95 cm, a (1,1,1) type reflection and a 50 mm wide beam, a 0.5 mm wide focused beam of spectral energy range 27 keV-43 keV was obtained. This spectral energy range covers the K-edges of iodine (33.17 keV), xenon (34.56 keV), cesium (35.99 keV), and barium (37.44 keV); some of these elements are used as biomedical and clinical contrast agents. Using the developed imaging system, a test subject composed of iodine, xenon, cesium, and barium along with water and bone were imaged and their projected concentrations successfully extracted. The estimated dose rate to test subjects imaged at a ring current of 200 mA is 8.7 mGy s -1 , corresponding to a cumulative dose of 1.3 Gy and a dose of 26.1 mGy per image. Potential biomedical applications of the imaging system will include projection imaging that requires any of the extracted elements as a contrast agent and multi-contrast K-edge imaging.

  6. Clash over demand for more synchrotron sources in Europe

    CERN Multimedia

    Butler, D

    1998-01-01

    French synchrotron staff accused the science minister, Claude Allegre, of misleading the National Assembly over the need to replace LURE, Paris. Allegre believes all big science facilities should be European with national facilities the exception (1 page).

  7. Aerial view of the 28 GeV Protron Synchrotron

    CERN Multimedia

    CERN PhotoLab

    1965-01-01

    The underground ring of the 28 GeV proton synchrotron in 1965. Left, the South and North experimental halls. Top right, part of the East hall. Bottom right, the main generator room and the cooling condensers.

  8. Staff accuse bosses of secrecy over British synchrotron plans

    CERN Multimedia

    Loder, N

    1999-01-01

    Scientific staff at Daresbury who have worked on the Diamond project for many years, believe senior management has kept them in the dark over discussions about the possible siting of the synchrotron at RAL (1 page).

  9. Daresbury senses victory in battle for UK synchrotron

    CERN Document Server

    Loder, N

    1999-01-01

    Scientists campaigning for the future synchrotron source, Diamond, to be sited at Daresbury rather than RAL, believe they have won their case following a meeting between the Office of Science & Technology and the director of the Welcome Trust (1 pg).

  10. CERN PSB Beam Tests of CNAO Synchrotron's Digital LLRF

    CERN Document Server

    Angoletta, M E; De Martinis, C; Falbo, L; Findlay, A; Foglio, R; Hunt, S; Tourres, D; Vescovi, C

    2008-01-01

    The Italian National Centre for Oncological hAdrontherapy (CNAO), in its final construction phase, uses proton and carbon ion beams to treat patients affected by solid tumours. At the heart of CNAO is a 78- meter circumference synchrotron that accelerates particles to up to 400 MeV/u. The synchrotron relies on a digital LLRF system based upon Digital Signal Processors (DSPs) and Field Programmable Gate Array (FPGA). This system implements cavity servoing and beam control capabilities, such as phase and radial loops. Beam tests of the CNAO synchrotron LLRF system were carried out at CERN's Proton Synchrotron Booster (PSB) in autumn 2007, to verify the combined DSP/FPGA architecture and the beam control capabilities. For this, a prototype version of CNAO's LLRF system was adapted to the PSB requirements. This paper outlines the prototype system layout and describes the tests carried out and their results. In particular, system architecture and beam control capabilities were successfully proven by comparison wit...

  11. The use of slow-cycling synchrotrons in injection systems

    CERN Multimedia

    1966-01-01

    The PS improvement programme is concerned with increasing the potential of the PS for high energy physics. It involves developing the performance of the proton synchrotron itself and providing major items of experimental equipment to be used on the machine.

  12. Pharmacogenetics in the Brazilian population

    Directory of Open Access Journals (Sweden)

    Guilherme eSuarez-Kurtz

    2010-10-01

    Full Text Available Brazil is the 5th largest country in the world and its present population, in excess of 190 million, is highly heterogeneous, as a result of centuries of admixture between Amerindians, Europeans and Sub-Saharan Africans. The estimated individual proportions of biogeographical ancestry vary widely and continuously among Brazilians, most individuals - irrespective of self-identification as White, Brown or Black, the major categories of the Brazilian Census race/color system - having significant degrees of European and African ancestry, while a sizeable number display also Amerindian ancestry. These features have important pharmacogenetic (PGx implications: first, extrapolation of PGx data from relatively well-defined ethnic groups is clearly not applicable to the majority of Brazilians; second, the frequency distribution of polymorphisms in pharmacogenes (e.g. CYP3A5, CYP2C9, GSTM1, ABCB1, GSTM3, VKORC, etc varies continuously among Brazilians and is not captured by race/color self-identification; third, the intrinsic heterogeneity of the Brazilian population must be acknowledged in the design and interpretation of PGx studies in order to avoid spurious conclusions based on improper matching of study cohorts. The peculiarities of PGx in Brazilians are illustrated with data for different therapeutic groups, such as anticoagulants, HIV-protease inhibitors and nonsteroidal antinflammatory drugs, and the challenges and advantages created by population admixture for the study and implementation of PGx are discussed. PGx data for Amerindian groups and Brazilian-born, first generation Japanese are presented to illustrate the rich diversity of the Brazilian population. Finally, I introduce the reader to the Brazilian Pharmacogenetic Network or Refargen (www.refargen.org.br, a nationwide consortium of research groups, with the mission to provide leadership in PGx research and education in Brazil, with a population health impact.

  13. Study of complex molecules of biological interest with synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Prince, K.C. [Elettra-Sincrotrone Trieste, Strada Statale 14–km 163,5 in AREA Science Park, I-34149 Trieste (Italy); Istituto Officina dei Materiali, Consiglio Nazionale delle Ricerche, in Area Science Park, I-34149 Trieste (Italy); Molecular Model Discovery Laboratory, Faculty of Science, Engineering and Technology, Swinburne University of Technology, Hawthorn, Melbourne, Victoria, 3122 (Australia); Bolognesi, P., E-mail: paola.bolognesi@cnr.it [CNR-ISM, Area della Ricerca di Roma 1, Via Salaria Km. 29,300, Monterotondo (Roma) (Italy); Feyer, V. [Elettra-Sincrotrone Trieste, Strada Statale 14–km 163,5 in AREA Science Park, I-34149 Trieste (Italy); Research Center Jülich, Peter Grünberg Institute (PGI-6), 52425 Jülich (Germany); Plekan, O. [Elettra-Sincrotrone Trieste, Strada Statale 14–km 163,5 in AREA Science Park, I-34149 Trieste (Italy); Avaldi, L. [CNR-ISM, Area della Ricerca di Roma 1, Via Salaria Km. 29,300, Monterotondo (Roma) (Italy)

    2015-10-15

    Synchrotron radiation and synchrotron based spectroscopic techniques have found important applications in the study of isolated molecular species of biological interest. In this paper, some examples of spectroscopic and dynamic studies of amino acids and small peptides, nucleobases and pharmaceuticals are reviewed. Opportunities offered by the advent of new radiation sources combined with novel methods for the production of beams of these molecules are also discussed.

  14. An introduction to synchrotron radiation techniques and applications

    CERN Document Server

    Willmott, Philip

    2011-01-01

    This book introduces the reader to the basic concepts of the generation and manipulation of synchrotron light, its interaction with matter, and the application of synchrotron light in the “classical” techniques, while including some of the most modern technological developments. As much as possible, complicated mathematical derivations and formulas are avoided. A more heuristic approach is adopted, whereby the general physical reasoning behind the equations is highlighted.

  15. Golden Jubilee photos: The Proton Synchrotron

    CERN Multimedia

    2004-01-01

    Energy record Standing before the CERN personnel in the Main Auditorium on 25 November 1959, John Adams held not a bottle of champagne but a bottle of vodka. It had been presented to him a few months earlier during a visit to Dubna in the Soviet Union, where the world's most powerful accelerator had just been commissioned. He had been given strict instructions not to open the bottle until Dubna's energy record of 10 GeV had been broken. On 24 November, the record was smashed by CERN's brand new machine, the Proton Synchrotron, which accelerated protons at 24 GeV, over twice the energy of the Dubna machine. Before sending the empty bottle back to the Soviet Union, John Adams, who had headed the accelerator's construction, placed the recording of the signal in it as proof of the record. More than 40 years later, the PS is still going strong, delivering beams with particle densities a thousand times greater than when it first started operation. Over the years, other accelerators have grown up around it and the...

  16. Imaging using synchrotron radiation for forensic science

    Science.gov (United States)

    Cervelli, F.; Carrato, S.; Mattei, A.; Jerian, M.; Benevoli, L.; Mancini, L.; Zanini, F.; Vaccari, L.; Perucchi, A.; Aquilanti, G.

    2011-03-01

    Forensic science is already taking benefits from synchrotron radiation (SR) sources in trace evidence analysis. In this contribution we show a multi-technique approach to study fingerprints from the morphological and chemical point of view using SR based techniques such as Fourier transform infrared microspectroscopy (FTIRMS), X-ray fluorescence (XRF), X-ray absorption structure (XAS), and phase contrast microradiography. Both uncontaminated and gunshot residue contaminated human fingerprints were deposited on lightly doped silicon wafers and on poly-ethylene-terephthalate foils. For the uncontaminated fingerprints an univariate approach of functional groups mapping to model FT-IRMS data was used to get the morphology and the organic compounds map. For the gunshot residue contaminated fingerprints, after a preliminary elemental analysis using XRF, microradiography just below and above the absorption edge of the elements of interest has been used to map the contaminants within the fingerprint. Finally, XAS allowed us to determine the chemical state of the different elements. The next step will be fusing the above information in order to produce an exhaustive and easily understandable evidence.

  17. Coronary angiography in rats using synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Matsushita, S. [Department of Cardiovascular Surgery, University of Tsukuba, Tsukuba (Japan)]. E-mail: shomatsu@md.tsukuba.ac.jp; Hyodo, K. [Instutute of Medical Science, High Energy Accelerator Research Organization, Tsukuba (Japan); Akishima, S. [Department of Cardiovascular Surgery, University of Tsukuba, Tsukuba (Japan); Sato, F. [Department of Cardiovascular Surgery, University of Tsukuba, Tsukuba (Japan); Imazuru, T. [Department of Cardiovascular Surgery, University of Tsukuba, Tsukuba (Japan); Noma, M. [Department of Cardiovascular Surgery, University of Tsukuba, Tsukuba (Japan); Hiramatsu, Y. [Department of Cardiovascular Surgery, University of Tsukuba, Tsukuba (Japan); Shigeta, O. [Department of Cardiovascular Surgery, University of Tsukuba, Tsukuba (Japan); Sakakibara, Y. [Department of Cardiovascular Surgery, University of Tsukuba, Tsukuba (Japan)

    2005-08-11

    Monochromatic X-rays obtained from synchrotron radiation (SR), provide a high-quality tool for medical imaging including, coronary angiography. To pursue higher resolution in experimental coronary angiography, a smaller visual field had seemed to be inevitable. However, there are cases in which whole coronary angiography is preferable in order to investigate such vasomotor activities as coronary vasospasm. To meet these requirements, we are trying to develop a new type of SR coronary angiography using Langendorff excised rat hearts. Experiments were performed at Photon Factory Accelerator Ring (PF-AR), High Energy Accelerator Research Organization (KEK), Japan. SR was obtained from a 6.5 GeV electron beam. The energy of the monochromatic X-rays was 33.3 keV, which is just above the K-edge energy of iodine. Iodine (35%) was infused as a contrast material to the aorta at the rate of 1 ml/min for 1 s. In the image obtained from coronary angiography, the resolution was 13 {mu}m and the width of the visual field 26 mmx26 mm. Whole heart coronary vasculature identifying small arteries down to those 100 {mu}m in diameter was obtained in beating hearts. Arteries as small as 50 {mu}m were identified in arrested hearts. This method of SR coronary angiography is useful for the investigation of whole coronary configurations simultaneously in one visual field to the level of microvasculature.

  18. Topography measurement of nanometer synchrotron optics

    Science.gov (United States)

    Illemann, Jens; Geckeler, Ralf D.; Weingartner, Ingolf; Schlewitt, Carsten; Grubert, Bernd; Schnabel, Olaf

    2002-12-01

    The technological limit on the beam quality when modern synchrotron radiation sources are used is determined by the geometrical accuracy of the optical components. This in turn is limited by the accuracy of the measuring technique which is within the range of up to 0.05 arcsec rms for one meter mirror length, which corresponds (in the absence of waviness) to an uncertainty of the topography of 5 nm rms. If the topography can be measured with higher accuracy, modern methods of ion beam processing allow the surface to be postprocessed with a high resolution of depth. We will present first tests with a novel measuring device which allows deflectometric measurements by the ESAD principle (Extended Shear Angle Difference) to be carried out. The basic item of this device is a commercial electronic autocollimator (AC) whose exit aperture is tripartite. By suitable evaluation one is in consequence able to simultaneously determine the angle information belonging to three surface points situated next to one another. According to the ESAD method, the angular topography can be completely reconstructed from two sets of angular difference data. The uncertainty of measurements of angular difference is transferred with a factor close to 1 to that of the set of reconstructed angle. First measurements show a reproducibility of about 25 milli-arcsec rms at a time of integration of 0.4 seconds per point. With this set-up, in the first order, no guide errors, vibrations or air turbulences enter.

  19. Synchrotron powder diffraction on Aztec blue pigments

    Energy Technology Data Exchange (ETDEWEB)

    Sanchez del Rio, M. [European Synchrotron Radiation Facility, B.P. 220, Grenoble Cedex (France); Gutierrez-Leon, A.; Castro, G.R.; Rubio-Zuazo, J. [Spanish CRG Beamline at the European Synchrotron Radiation Facility, SpLine, B.P. 220, Grenoble Cedex (France); Solis, C. [Universidad Nacional Autonoma de Mexico, Instituto de Fisica, Mexico, D.F. (Mexico); Sanchez-Hernandez, R. [INAH Subdireccion de Laboratorios y Apoyo Academico, Mexico, D.F. (Mexico); Robles-Camacho, J. [INAH Centro Regional Michoacan, Morelia, Michoacan (Mexico); Rojas-Gaytan, J. [INAH Direccion de Salvamento Arqueologico, Naucalpan de Juarez (Mexico)

    2008-01-15

    Some samples of raw blue pigments coming from an archaeological rescue mission in downtown Mexico City have been characterized using different techniques. The samples, some recovered as a part of a ritual offering, could be assigned to the late Aztec period (XVth century). The striking characteristic of these samples is that they seem to be raw pigments prior to any use in artworks, and it was possible to collect a few {mu}g of pigment after manual grain selection under a microscopy monitoring. All pigments are made of indigo, an organic colorant locally known as anil or xiuhquilitl. The colorant is always found in combination with an inorganic matrix, studied by powder diffraction. In one case the mineral base is palygorskite, a rare clay mineral featuring micro-channels in its structure, well known as the main ingredient of the Maya blue pigment. However, other samples present the minerals sepiolite (a clay mineral of the palygorskite family) and calcite. Another sample contains barite, a mineral never reported in prehispanic paints. We present the results of characterization using high resolution powder diffraction recorded at the European Synchrotron Radiation Facility (BM25A, SpLine beamline) complemented with other techniques. All of them gave consistent results on the composition. A chemical test on resistance to acids was done, showing a high resistance for the palygorskite and eventually sepiolite compounds, in good agreement with the excellent resistance of the Maya blue. (orig.)

  20. Characterization of Medipix3 With Synchrotron Radiation

    CERN Document Server

    Gimenez, E N; Marchal, J; Turecek, D; Ballabriga, R; Tartoni, N; Campbell, M; Llopart, X; Sawhney, K J S

    2011-01-01

    Medipix3 is the latest generation of photon counting readout chips of the Medipix family. With the same dimensions as Medipix2 (256 x 256 pixels of 55 mu m x 55 mu m pitch each), Medipix3 is however implemented in an 8-layer metallization 0.13 mu m CMOS technology which leads to an increase in the functionality associated with each pixel over Medipix2. One of the new operational modes implemented in the front-end architecture is the Charge Summing Mode (CSM). This mode consists of a charge reconstruction and hit allocation algorithm which eliminates event-by-event the low energy counts produced by charge-shared events between adjacent pixels. The present work focuses on the study of the CSM mode and compares it to the Single Pixel Mode (SPM) which is the conventional readout method for these kind of detectors and it is also implemented in Medipix3. Tests of a Medipix3 chip bump-bonded to a 300 mu m thick silicon photodiode sensor were performed at the Diamond Light Source synchrotron to evaluate the performan...

  1. The rise of Brazilian agriculture

    DEFF Research Database (Denmark)

    Jensen, Hans Grinsted; Vink, Nick; Sandrey, Ron

    2014-01-01

    The purpose of this article is to explore some of the possible lessons for South African agriculture from the Brazilian experience. To this end, the article discusses the performance of Brazilian agriculture in terms of land and labour use, production, and exports. This is followed by aspects...... of Brazilian agricultural policies, namely farmer support, the research and technology transfer system and land issues. The implications for South African agriculture can be summarized as the recognition that history, geography, the development path and agricultural policies all matter. The article...... then identifies five important lessons for agricultural development in South Africa....

  2. Brazilian Space Weather Program

    Science.gov (United States)

    Padilha, Antonio; Takahashi, Hisao; de Paula, Eurico; Sawant, Hanumant; de Campos Velho, Haroldo; Vitorello, Icaro; Costa, Joaquim; Souza, Jonas; Cecatto, José; Mendes, Odim; Gonzalez Alarcon, Walter Demétrio

    A space weather program is being initiated at the Brazilian National Institute for Space Research (INPE) to study events from their initiation on the sun to their impacts on the earth, including their effects on space-based and ground-based technological systems. The program is built on existing capabilities at INPE, which include scientists with a long tradition and excellence in the observation, analysis and modeling of solar and solar-terrestrial phenomena and an array of geophysical instruments that spans all over the Brazilian territory from the north to south of the magnetic dip equator. Available sensors include solar radio frequency receivers and telescopes, optical instruments and solar imagers, GNSS receivers, ionosondes, radars, allsky imagers, magnetometers and cosmic ray detectors. In the equatorial region, ionosphere and thermosphere constitute a coupled system with electrodynamical and plasma physical processes being responsible for a variety of peculiar phenomena. The most important of them are the equatorial electrojet current system and its instabilities, the equatorial ionization anomaly, and the plasma instabilities/irregularities of the night-time ionosphere (associated with the plasma bubble events). In addition, space weather events modify the equatorial ionosphere in a complex and up to now unpredictable manner. Consequently, a main focus of the program will be on monitoring the low, middle and upper atmosphere phenomena and developing a predictive model of the equatorial ionosphere through data assimilation, that could help to mitigate against the deleterious effects on radio communications and navigation systems. The technological, economic and social importance of such activities was recognized by the Brazilian government and a proposal for funding was approved for the period 2008-2011. New ground instruments will be installed during this period allowing us to extend our current capability to provide space weather observations, accurate

  3. brazilian subsidiaries of multinationals

    Directory of Open Access Journals (Sweden)

    Felipe Mendes Borini

    2012-01-01

    Full Text Available The theme of corporate social responsibility (CSR has not been widely examined in the context of multinationals. This dearth is even greater with respect to subsidiaries, particularly the subject of reverse transfer of practices, that is, the transfer of practices developed in subsidiaries back to the parent company. Because of this theoretical gap, the present article investigates the factors involved on reverse transfer of CSR practices. The research hypotheses test the importance of developing nonlocation-bound capabilities, of integration between subsidiaries and parent and of institutional distance. The data were obtained by a survey of the main foreign subsidiaries in Brazil. All told, we analyzed 150 Brazilian subsidiaries of multinationals, by applying multiple linear regression. The results indicate that the reverse transfer of CSR depends on the development of nonlocation-bound capabilities of the subsidiaries and integration between the parent company and its foreign subsidiaries.

  4. Brazilian Eratosthenes Project

    Science.gov (United States)

    Langhi, R.; Vilaça, J.

    2014-10-01

    The objective of Brazilian Eratosthenes Project is the development and application of teaching training actions according the ``docent autonomy" concept to basic Astronomy Education. Argentina coordinates the project in South America, but Brazil works in this project since 2010 with the theme ``Projeto Eratóstenes Brasil" in the homepage: http://sites.google.com/site/projetoerato. Two schools measure a sticks shadow and communicate their results. After, they calculate an average radius of Earth. The stick (gnomon) should stay in vertical position in the leveled ground. Since 2010, the project received hundreds of Brazilian schools with different experiments that were constructed with autonomy, because our site doesn't show some itinerary pre-ready to elaborate the experiments. To collect data for our research, we will use interviews via Skype with the teachers. These data are useful to researches about Science Education area and the Teaching Formation. Teaching professional practice could change and we see modifications in the teachers work, what depends of their realities and context. This project intents to respect the docent autonomy. This autonomy to responsible modifications during continued formation is called ``activist formative model" according Langhi & Nardi (Educação em Astronomia: repensando a formação de professores. São Paulo: Escrituras Editora, 2012). This project discusses about researches in Astronomy Education - still extreme rare in Brazil, when we compare with other areas in Science Education. We believe that actions like this could motivate the students to learn more Astronomy. Furthermore, this national action can be a rich source of data to investigations about teaching formation and scientific divulgation.

  5. INNOVATION IN BRAZILIAN SMALL COMPANIES

    Directory of Open Access Journals (Sweden)

    Tonny Kerley de Alencar Rodrigues

    2015-03-01

    Full Text Available This study aims to identify the interfaces and boundaries of innovation orientation of Brazilian MSEs because despite the importance of innovation for Brazilian MSEs, a thorough analysis of such initiatives in Brazil still has not actually happened. The search was developed from a quantitative approach, of applied nature and descriptive. For that a structured questionnaire was used where were interviewed 700 MSEs using a probabilistic sampling. The study offers two important conclusions. The challenges for innovation can be perceived along three dimensions: design innovation, the implementation of innovation and functional area of innovation. And the data confirms that small Brazilian companies generally have difficulties to sell their innovations. The study offers two important conclusions. The challenges for innovation can be perceived along three dimensions: design innovation, the implementation of innovation and functional area of innovation. And the data confirms that small Brazilian companies generally have difficulties to sell their innovations.

  6. Innovation in brazilian small companies

    OpenAIRE

    Tonny Kerley de Alencar Rodrigues; Átila de Melo Lira; Irenilza Alencar Naas

    2015-01-01

    This study aims to identify the interfaces and boundaries of innovation orientation of Brazilian MSEs because despite the importance of innovation for Brazilian MSEs, a thorough analysis of such initiatives in Brazil still has not actually happened. The search was developed from a quantitative approach, of applied nature and descriptive. For that a structured questionnaire was used where were interviewed 700 MSEs using a probabilistic sampling. The study offers two important conclusions. The ...

  7. Elliptical Undulators HU256 for Synchrotron SOLEIL

    Science.gov (United States)

    Batrakov, A.; Briquez, F.; Chubar, O.; Churkin, I.; Dael, A.; Ilyin, I.; Kolokolnikov, Yu.; Marcouile, O.; Marteau, F.; Roux, G.; Rouvinski, E.; Semenov, E.; Steshov, A.; Valleau, M.; Vobly, P.

    2007-01-01

    Three elliptical undulators HU256 of electromagnetic type were produced, tested and magnetically measured by the Budker Institute of Nuclear Physics (Russia) for Synchrotron Soleil (France). The undulators have a new design of a Bx & Bz closed structure for insertion vacuum chamber. In the elliptical undulator HU256 with period of the magnetic fields of 256 mm, the vertical magnetic field (Bzmax=0.44 T) formed by 27 Bz laminated dipole magnets is symmetric, and the horizontal magnetic field (Bxmax=0.33 T) formed by 28 Bx laminated dipole magnets is asymmetric. The undulator can work in standard mode as well as in a quasi-periodical mode. The vertical magnetic field may be modulated by switching on the modulation coils placed on the Bz dipoles. Two power supply systems allow us to modulate the horizontal magnetic field, and change the radiation spectrum. The magnetic calculations of the individual dipoles and dipoles in "undulator" environment were executed by means of Mermaid 3D Code. The magnetic measurements of the individual dipoles had confirmed the magnetic calculations. On basis of semiempirical dependences from the mechanical characteristics the estimates of the magnetic parameters for all dipoles were calculated. Sorting of dipoles in the undulators have been done, and it has improved the magnetic parameters of the assembled undulators in comparison with the statistical estimations. The magnetic measurements of the undulators HU256 were carried out at Budker INP by Hall probes and at Soleil by Hall probes and Stretched Wire. Now the 1st undulator HU256 is installed at Soleil Storage Ring.

  8. Nuclear dynamical diffraction using synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Brown, Dennis Eugene [Stanford Univ., CA (United States)

    1993-05-01

    The scattering of synchrotron radiation by nuclei is extensively explored in this thesis. From the multipole electric field expansion resulting from time-dependent nonrelativistic perturbation theory, a dynamical scattering theory is constructed. This theory is shown, in the many particle limit, to be equivalent to the semi-classical approach where a quantum mechanical scattering amplitude is used in the Maxwell inhomogeneous wave equation. The Moessbauer specimen whose low-lying energy levels were probed is a ferromagnetic lattice of 57Fe embedded in a yttrium iron garnet (YIG) crystal matrix. The hyperfine fields in YIG thin films were studied at low and room temperature using time-resolved quantum beat spectroscopy. Nuclear hyperfine structure quantum beats were measured using a fast plastic scintillator coincidence photodetector and associated electronics having a time resolution of 2.5 nsec. The variation of the quantum beat patterns near the Bragg [0 0 2] diffraction peak gave a Lamb-Moessbauer factor of 8.2±0.4. Exploring characteristic dynamical features in the higher order YIG [0 0 10] reflection revealed that one of the YIG crystals had bifurcated into two different layers. The dynamics of nuclear superradiance was explored. This phenomenon includes the radiative speedup exhibited by a collective state of particles, and, in striking concurrence, resonance frequency shifts. A speedup of a factor of 4 in the total decay rate and a beat frequency shift of 11/2 natural resonance linewidths were observed. Nuclear resonance scattering was also found to be a useful way of performing angular interferometry experiments, and it was used to observe the phase shift of a rotated quantum state. On the whole, nuclear dynamical diffraction theory has superbly explained many of the fascinating features of resonant magnetic dipole radiation scattered by a lattice of nuclei.

  9. 1994 activity report: Stanford Synchrotron Radiation Laboratory

    Energy Technology Data Exchange (ETDEWEB)

    Cantwell, K.; Dunn, L. [eds.

    1994-01-01

    The SSRL facility delivered 89% of the scheduled user beam to 25 experimental stations during 6.5 months of user running. Users from private industry were involved in 31% of these experiments. The SPEAR accelerator ran very well with no major component failures and an unscheduled down time of only 2.9%. In addition to this increased reliability, there was a significant improvement in the stability of the beam. The enhancements to the SPEAR orbit as part of a concerted three-year program were particularly noticeable to users. The standard deviation of beam movement (both planes) in the last part of the run was 80 microns, major progress toward the ultimate goal of 50-micron stability. This was a significant improvement from the previous year when the movement was 400 microns in the horizontal and 200 microns in the vertical. A new accelerator Personal Protection System (PPS), built with full redundancy and providing protection from both radiation exposure and electrical hazards, was installed in 1994. It is not possible to describe in this summary all of the scientific experimentation which was performed during the run. However, the flavor of current research projects and the many significant accomplishments can be realized by the following highlights: A multinational collaboration performed several experiments involving x-ray scattering from nuclear resonances; Studies related to nuclear waste remediation by groups from Los Alamos National Laboratory and Pacific Northwest Laboratories continued in 1994; Diffraction data sets for a number of important protein crystals were obtained; During the past two years a collaboration consisting of groups from Hewlett Packard, Intel, Fisons Instruments and SSRL has been exploring the utility of synchrotron radiation for total reflection x-ray fluorescence (TRXRF); and High-resolution angle-resolved photoemission experiments have continued to generate exciting new results from highly correlated and magnetic materials.

  10. Applications of synchrotron radiation to Chemical Engineering Science: Workshop report

    Energy Technology Data Exchange (ETDEWEB)

    1991-07-01

    This report contains extended abstracts that summarize presentations made at the Workshop on Applications of Synchrotron Radiation to Chemical Engineering Science held at Argonne National Laboratory (ANL), Argonne, IL, on April 22--23, 1991. The talks emphasized the application of techniques involving absorption fluorescence, diffraction, and reflection of synchrotron x-rays, with a focus on problems in applied chemistry and chemical engineering, as well as on the use of x-rays in topographic, tomographic, and lithographic procedures. The attendees at the workshop included experts in the field of synchrotron science, scientists and engineers from ANL, other national laboratories, industry, and universities; and graduate and undergraduate students who were enrolled in ANL educational programs at the time of the workshop. Talks in the Plenary and Overview Session described the status of and special capabilities to be offered by the Advanced Photon Source (APS), as well as strategies and opportunities for utilization of synchrotron radiation to solve science and engineering problems. Invited talks given in subsequent sessions covered the use of intense infrared, ultraviolet, and x-ray photon beams (as provided by synchrotrons) in traditional and nontraditional areas of chemical engineering research related to electrochemical and corrosion science, catalyst development and characterization, lithography and imaging techniques, and microanalysis.

  11. Vacuum chambers full of ideas for the Swedish synchrotron

    CERN Multimedia

    Corinne Pralavorio

    2016-01-01

    CERN’s Vacuum, Surfaces and Coatings group has contributed to the development of vacuum chambers for the MAX IV synchrotron, which has just been officially opened in Sweden.   A section of the new 3 GeV MAX IV synchrotron at the time of installation. In the centre of the magnets you can see the vacuum chamber developed in collaboration with CERN. (Photo: Marek Grabski, MAX IV Vacuum group) On 21 June, the King and the Prime Minister of Sweden officially opened MAX IV, a brand-new synchrotron in Lund, Sweden. The summer solstice, the longest day of the year, was deliberately chosen for the ceremony: MAX IV, a cutting-edge synchrotron, will deliver the brightest X-rays ever produced to more than 2000 users. Some 1500 kilometres away, a team at CERN followed the opening ceremony with a touch of pride. The Vacuum, Surfaces and Coatings group in the Technology department (TE-VSC) participated in the construction of this new synchrotron. Its contribution lies at the very hea...

  12. The Compact Light Source A Miniature Synchrotron Light Source

    CERN Document Server

    Ruth, Ronald D

    2005-01-01

    During the past 30 years, synchrotron light sources have become the x-ray probe of choice for physicists, chemists, biologists and research physicians. With their high-quality, intense x-ray beams, these national research facilities have spawned a broad array of applications. Past research at Stanford Linear Accelerator Center has led to a new x-ray source concept that can substantially reduce the size of the required synchrotron.* This research has spawned a new corporation, Lyncean Technologies, Inc. which is now developing the Compact Light Source (CLS). The CLS is a tunable, homelab x-ray source with up to three beamlines that can be used like the x-ray beamlines at the synchrotrons-but it is about 200 times smaller than a synchrotron light source. The compact size is achieved using a laser undulator and a miniature electron-beam storage ring. The photon flux on a sample will be comparable to the flux of highly productive synchrotron beamlines. At Lyncean Technologies, Inc. we have constructed a prototype...

  13. Optoelectronic Picosecond Detection of Synchrotron X-rays

    Energy Technology Data Exchange (ETDEWEB)

    Durbin, Stephen M. [Purdue Univ., West Lafayette, IN (United States)

    2017-08-04

    The goal of this research program was to develop a detector that would measure x-ray time profiles with picosecond resolution. This was specifically aimed for use at x-ray synchrotrons, where x-ray pulse profiles have Gaussian time spreads of 50-100 ps (FWHM), so the successful development of such a detector with picosecond resolution would permit x-ray synchrotron studies to break through the pulse width barrier. That is, synchrotron time-resolved studies are currently limited to pump-probe studies that cannot reveal dynamics faster than ~50 ps, whereas the proposed detector would push this into the physically important 1 ps domain. The results of this research effort, described in detail below, are twofold: 1) the original plan to rely on converting electronic signals from a semiconductor sensor into an optical signal proved to be insufficient for generating signals with the necessary time resolution and sensitivity to be widely applicable; and 2) an all-optical method was discovered whereby the x-rays are directly absorbed in an optoelectronic material, lithium tantalate, which can then be probed by laser pulses with the desired picosecond sensitivity for detection of synchrotron x-rays. This research program has also produced new fundamental understanding of the interaction of x-rays and optical lasers in materials that has now created a viable path for true picosecond detection of synchrotron x-rays.

  14. Spin dynamics in electron synchrotrons; Spindynamik in Elektronensynchrotronen

    Energy Technology Data Exchange (ETDEWEB)

    Schmidt, Jan Felix

    2017-07-14

    Providing spin polarized particle beams with circular accelerators requires the consideration of depolarizing resonances which may significantly reduce the desired degree of polarization at specific beam energies. The corresponding spin dynamical effects are typically analyzed with numerical methods. In case of electron beams the influence of the emission of synchrotron radiation has to be taken into account. On short timescales, as in synchrotrons with a fast energy ramp or in damping rings, spin dynamics are investigated with spin tracking algorithms. This thesis presents the spin tracking code Polematrix as a versatile tool to study the impact of synchrotron radiation on spin dynamics. Spin tracking simulations have been performed based on the well established particle tracking code Elegant. The numerical studies demonstrate effects which are responsible for beam depolarization: Synchrotron side bands of depolarizing resonances and decoherence of spin precession. Polematrix can be utilized for any electron accelerator with minimal effort as it imports lattice files from the tracking programs MAD-X or Elegant. Polematrix has been published as open source software. Currently, the Electron Stretcher Accelerator ELSA at Bonn University is the only electron synchrotron worldwide providing a polarized beam. Integer and intrinsic depolarizing resonances are compensated with dedicated countermeasures during the fast energy ramp. Polarization measurements from ELSA demonstrate the particular spin dynamics of electrons and confirm the results of the spin tracking code Polematrix.

  15. National Synchrotron Light Source 2008 Activity Report

    Energy Technology Data Exchange (ETDEWEB)

    Nasta,K.

    2009-05-01

    Funded by the U.S. Department of Energy's Office of Basic Energy Sciences, the National Synchrotron Light Source (NSLS) is a national user facility that operates two electron storage rings: X-Ray (2.8 GeV, 300 mA) and Vacuum Ultraviolet (VUV) (800 mev, 1.0A). These two rings provide intense light spanning the electromagnetic spectrum -- from very long infrared rays to ultraviolet light and super-short x-rays -- to analyze very small or highly dilute samples. The properties of this light, and the specially designed experimental stations, called beamlines, allow scientists in many diverse disciplines of research to perform experiments not possible at their own laboratories. Each year, about 2,200 scientists from more than 400 universities and companies use the NSLS for research in such diverse fields as biology, physics, chemistry, geology, medicine, and environmental and materials sciences. For example, researchers have used the NSLS to examine the minute details of computer chips, decipher the structures of viruses, probe the density of bone, determine the chemical composition of moon rocks, and reveal countless other mysteries of science. The facility has 65 operating beamlines, with 51 beamlines on the X-Ray Ring and 14 beamlines on the VUV-Infrared Ring. It runs seven days a week, 24 hours a day throughout the year, except during periods of maintenance and studies. Researchers are not charged for beam time, provided that the research results are published in open literature. Proprietary research is conducted on a full-cost-recovery basis. With close to 1,000 publications per year, the NSLS is one of the most prolific scientific facilities in the world. Among the many accolades given to its users and staff, the NSLS has won nine R&D 100 Awards for innovations ranging from a closed orbit feedback system to the first device able to focus a large spread of high-energy x-rays. In addition, a visiting NSLS researcher shared the 2003 Nobel Prize in Chemistry for

  16. DEVELOPMENTS IN SYNCHROTRON X-RAY COMPUTED MICROTOMOGRAPHY AT THE NATIONAL SYNCHROTRON LIGHT SOURCE.

    Energy Technology Data Exchange (ETDEWEB)

    DOWD,B.A.

    1999-07-23

    Last year, the X27A beamline at the National Synchrotron Light Source (NSLS) became dedicated solely to X-Ray Computed Microtomography (XCMT). This is a third-generation instrument capable of producing tomographic volumes of 1-2 micron resolution over a 2-3mm field of view. Recent enhancements will be discussed. These have focused on two issues: the desire for real-time data acquisition and processing and the need for highly monochromatic beam (.1 % energy bandpass). The latter will permit k-edge subtraction studies and will provide improved image contrast from below the Cr (6 keV) up to the Cs (36 keV) k-edge. A range of applications that benefit from these improvements will be discussed as well. These two goals are somewhat counterproductive, however; higher monochromaticity yields a lower flux forcing longer data acquisition times. To balance the two, a more efficient scintillator for X-ray conversion is being developed. Some testing of a prototype scintillator has been performed; preliminary results will be presented here. In the meantime, data reconstruction times have been reduced, and the entire tomographic acquisition, reconstruction and volume rendering process streamlined to make efficient use of synchrotron beam time. A Fast Filtered Back Transform (FFBT) reconstruction program recently developed helped to reduce the time to reconstruct a volume of 150 x 150 x 250 pixels{sup 3} (over 5 million voxels) from the raw camera data to 1.5 minutes on a dual R10,000 CPU. With these improvements, one can now obtain a ''quick look'' of a small tomographic volume ({approximately}10{sup 6}voxels) in just over 15 minutes from the start of data acquisition.

  17. Synchrotron radiation from a runaway electron distribution in tokamaks

    Energy Technology Data Exchange (ETDEWEB)

    Stahl, A.; Fülöp, T. [Department of Applied Physics, Nuclear Engineering, Chalmers University of Technology and Euratom-VR Association, SE-412 96 Göteborg (Sweden); Landreman, M. [Plasma Science and Fusion Center, MIT, Cambridge, Massachusetts 02139 (United States); Papp, G. [Department of Applied Physics, Nuclear Engineering, Chalmers University of Technology and Euratom-VR Association, SE-412 96 Göteborg (Sweden); Department of Nuclear Techniques, Budapest University of Technology and Economics, Association EURATOM, H-1111 Budapest (Hungary); Hollmann, E. [Center for Energy Research, University of California, San Diego, La Jolla, California 92093-0417 (United States)

    2013-09-15

    The synchrotron radiation emitted by runaway electrons in a fusion plasma provides information regarding the particle momenta and pitch-angles of the runaway electron population through the strong dependence of the synchrotron spectrum on these parameters. Information about the runaway density and its spatial distribution, as well as the time evolution of the above quantities, can also be deduced. In this paper, we present the synchrotron radiation spectra for typical avalanching runaway electron distributions. Spectra obtained for a distribution of electrons are compared with the emission of mono-energetic electrons with a prescribed pitch-angle. We also examine the effects of magnetic field curvature and analyse the sensitivity of the resulting spectrum to perturbations to the runaway distribution. The implications for the deduced runaway electron parameters are discussed. We compare our calculations to experimental data from DIII-D and estimate the maximum observed runaway energy.

  18. Transverse beam profile reconstruction using synchrotron radiation interferometry

    Directory of Open Access Journals (Sweden)

    L. Torino

    2016-12-01

    Full Text Available Transverse beam size measurements in new generation of synchrotron light sources is a challenging task due to their characteristic small beam emittances and low couplings. Since the late 1990s, synchrotron radiation interferometry (SRI has been used in many accelerators to measure the beam size through the analysis of the spatial coherence of the synchrotron light. However, the standard SRI using a double-aperture system provides the beam size projection in a given direction. For this reason, the beam shape is not fully characterized because information about possible transverse beam tilts is not determined. In this report, we describe a technique to fully reconstruct the transverse beam profile based on a rotating double-pinhole mask, together with experimental results obtained at ALBA under different beam couplings. We also discuss how this method allows us to infer ultrasmall beam sizes in case of limitations of the standard SRI.

  19. K-Edge Subtraction Angiography with Synchrotron X-Rays

    CERN Document Server

    Giacomini, J C

    1996-01-01

    The purpose of this project was to utilize dual energy, monochromatic X-rays produced from synchrotrons radiation in order to obtain noninvasive medical imaging. The application of synchrotrons radiation to medical imaging is based on the principle of iodine dichromography, first described by Bertil Jacobson of the Karolinska Institute in 1953. Medical imaging using synchrotrons radiation and K-edge dichromography was pioneered at Stanford University under the leadership of Dr. Ed Rubenstein, and the late Nobel Laureate in Physics, Dr. Robert Hofstadter. With progressive refinements in hardware, clinical-quality images were obtained of human coronary arteries utilizing peripheral injections of iodinated contrast agent. These images even now are far superior to those being presented by investigators using MRI as an imaging tool for coronary arteries. However, new supplies and instruments in the cardiac catheterization laboratory have served to transform coronary angiography into an outpatient procedure, with r...

  20. 6th International School “Synchrotron Radiation and Magnetism”

    CERN Document Server

    Bulou, Hervé; Joly, Loic; Scheurer, Fabrice; Magnetism and Synchrotron Radiation : Towards the Fourth Generation Light Sources

    2013-01-01

     Advances in the synthesis of new materials with often complex, nano-scaled structures require increasingly sophisticated experimental techniques that can probe the electronic states, the atomic magnetic moments and the magnetic microstructures responsible for the properties of these materials. At the same time, progress in synchrotron radiation techniques has ensured that these light sources remain a key tool of investigation, e.g. synchrotron radiation sources of the third generation are able to support magnetic imaging on a sub-micrometer scale. With the Sixth Mittelwihr School on Magnetism and Synchrotron Radiation the tradition of teaching the state-of-the-art on modern research developments continues and is expressed through the present set of extensive lectures provided in this volume. While primarily aimed at postgraduate students and newcomers to the field, this volume will also benefit researchers and lecturers actively working in the field.

  1. Synchrotron X-ray induced solution precipitation of nanoparticles

    CERN Document Server

    Lee, H J; Hwu, Y; Tsai, W L

    2003-01-01

    By irradiating a solution in electroless Ni deposition using synchrotron X-rays, Ni composite was found to nucleate homogeneously and eventually precipitate in the form of nanoparticles. The size of the nanoparticles precipitated is rather uniform (100-300 nm depending on the applied temperature). By the addition of an organic acid, well-dispersed nanoparticles could be effectively deposited on glass substrate. The hydrated electrons (e sub a sub q sup -), products of radiolysis of water molecules by synchrotron X-rays, may be responsible for the effective reduction of the metal ions, resulting in homogeneous nucleation and nanoparticle formation. Our results suggest that synchrotron X-ray can be used to induce solution precipitation of nanoparticles and therefore lead to a new method of producing nanostructured particles and coating.

  2. HSC5: synchrotron radiation and neutrons for cultural heritage studies

    Energy Technology Data Exchange (ETDEWEB)

    Michel, Anne [Institut Neel - CNRS, 38 - Grenoble (France); Artioli, G. [Padova Univ. (Italy); Bleuet, P.; Cotte, M.; Tafforeau, P.; Susini, J. [European Synchrotron Radiation Facility, 38 - Grenoble (France); Dumas, P.; Somogyl, A. [SOLEIL Synchrotron, 91 - Gif sur Yvette (France); Cotte, M. [Centre de Recherche et de Restauration des Musees de France, UMR171, 75 - Paris (France)]|[European Synchrotron Radiation Facility, 38 - Grenoble (France); Kockelmann, W. [Science and Technology Facilities Council, Rutherford Appleton Lab. (United Kingdom); Kolar, J. [Ljubljana Univ., Morana RTD, Slovenia, Faculty of Chemistry and Chemical Technology (Slovenia); Areon, I. [Nova Gorica Univ. (Slovenia); Meden, A.; Strlie, M. [Ljubljana Univ., Faculty of Chemistry and Chemical Technology (Slovenia); Pantos, M. [Daresbury Laboratory, Warrington (United Kingdom); Vendrell, M. [Barcelona Univ., dept. of Crystallography and Mineralogy (Spain); Wess, T. [Cardiff Univ., School of Optometry and Institute of Vision (Ireland); Gunneweg, J. [Hebrew Univ., Jerusalem (Israel)

    2007-07-01

    Synchrotron and neutron sources offer recent and additional insight into the records of our cultural past. Over the last years, there has been an increasing demand for access to synchrotron radiation- and neutron-based techniques, and their applications in the fields of archaeological science and cultural heritage. The purpose of this Hercules Specialized Course is to give the participants an introduction to the basic principles of synchrotron radiation and neutron techniques (imaging, microscopy, diffraction, absorption and fluorescence, IR spectroscopy). The school provides cross-disciplinary examples illustrating the abilities of these techniques in a representative range of scientific cases concerning painting, archaeological artefacts, inks, pigments, fossils and the Dead Sea scrolls. This document gathers only the resumes of the lectures.

  3. Transfiguration of extracting mirror in synchrotron radiation system at SSRF

    Science.gov (United States)

    Chen, Jie; Huang, GuoQing; Zhou, WeiMin; Ye, KaiRong; Leng, YongBin

    2011-12-01

    The first extracting mirror is very important for synchrotron radiation monitor (SRM). The SRM system of SSRF (Shanghai Synchrotron Radiation Facility) should extract the visible light with low optical distortion. The analysis of SR power spectrum and heat transfiguration based on Matlab is introduced in this paper, which will be used in calibration. One beryllium mirror with water-cooling is used to transmit X-ray and reflect visible light to satisfy the measurement request. The existing system suffers from a dynamic problem in some beam physics study. The system includes optics, image acquisition and interferometers. One of the instruments is a digital camera providing the image of the beam transverse profile. The hardware configuration will be summarized. The synchrotron radiation measurement system has been in operation in SSRF for more than one year.

  4. Rising dough and baking bread at the Australian synchrotron

    Science.gov (United States)

    Mayo, S. C.; McCann, T.; Day, L.; Favaro, J.; Tuhumury, H.; Thompson, D.; Maksimenko, A.

    2016-01-01

    Wheat protein quality and the amount of common salt added in dough formulation can have a significant effect on the microstructure and loaf volume of bread. High-speed synchrotron micro-CT provides an ideal tool for observing the three dimensional structure of bread dough in situ during proving (rising) and baking. In this work, the synchrotron micro-CT technique was used to observe the structure and time evolution of doughs made from high and low protein flour and three different salt additives. These experiments showed that, as expected, high protein flour produces a higher volume loaf compared to low protein flour regardless of salt additives. Furthermore the results show that KCl in particular has a very negative effect on dough properties resulting in much reduced porosity. The hundreds of datasets produced and analysed during this experiment also provided a valuable test case for handling large quantities of data using tools on the Australian Synchrotron's MASSIVE cluster.

  5. Transvenous coronary angiography in humans with synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Thomlinson, W.

    1994-10-01

    The transvenous coronary angiography project at the National Synchrotron Light Source (NSLS) is presently undergoing a significant upgrade to the hardware and software in the synchrotron medical facility. When completed, the project will have reached a level of maturity in the imaging technology which will allow the research team to begin to concentrate on medical research programs. This paper will review the status of the project and imaging technology and will discuss the current upgrades and future advanced technology initiatives. The advantages of using the radiation from a synchrotron, over that from a standard x-ray source, were the motivation for the project. A total of 23 human imaging sessions have been carried out with in the project. The primary goals have been to establish the imaging parameters and protocol necessary to obtain clinically useful images.

  6. High Intensity Beam Issues in the CERN Proton Synchrotron

    CERN Document Server

    Aumon, Sandra; Rivkin, Leonid

    This PhD work is about limitations of high intensity proton beams observed in the CERN Proton Synchrotron (PS) and, in particular, about issues at injection and transition energies. With its 53 years, the CERN PS would have to operate beyond the limit of its performance to match the future requirements. Beam instabilities driven by transverse impedance and aperture restrictions are important issues for the operation and for the High-Luminosity LHC upgrade which foresees an intensity increase delivered by the injectors. The main subject of the thesis concerns the study of a fast transverse instability occurring at transition energy. The proton beams crossing this energy range are particularly sensitive to wake forces because of the slow synchrotron motion. This instability can cause a strong vertical emittance blow-up and severe losses in less than a synchrotron period. Experimental observations show that the particles at the peak density of the beam longitudinal distribution oscillate in the vertical plane du...

  7. Chemical Dynamics, Molecular Energetics, and Kinetics at the Synchrotron

    Energy Technology Data Exchange (ETDEWEB)

    Leone, Stephen R.; Ahmed, Musahid; Wilson, Kevin R.

    2010-03-14

    Scientists at the Chemical Dynamics Beamline of the Advanced Light Source in Berkeley are continuously reinventing synchrotron investigations of physical chemistry and chemical physics with vacuum ultraviolet light. One of the unique aspects of a synchrotron for chemical physics research is the widely tunable vacuum ultraviolet light that permits threshold ionization of large molecules with minimal fragmentation. This provides novel opportunities to assess molecular energetics and reaction mechanisms, even beyond simple gas phase molecules. In this perspective, significant new directions utilizing the capabilities at the Chemical Dynamics Beamline are presented, along with an outlook for future synchrotron and free electron laser science in chemical dynamics. Among the established and emerging fields of investigations are cluster and biological molecule spectroscopy and structure, combustion flame chemistry mechanisms, radical kinetics and product isomer dynamics, aerosol heterogeneous chemistry, planetary and interstellar chemistry, and secondary neutral ion-beam desorption imaging of biological matter and materials chemistry.

  8. Amazon, priority for Brazilian National Defense Policy

    National Research Council Canada - National Science Library

    Pereira, Sergio

    2000-01-01

    .... The Brazilian national defense policy, issued in 1996, the first in the history of the country, established directives to orient the Brazilian military strategic planning as well as diplomatic...

  9. Singapore Synchrotron Light Source - Status, first results, program

    CERN Document Server

    Moser, H O; Kempson, V C; Kong, J R; Li, Z W; Nyunt, T; Qian, H J; Rossmanith, R; Tor, P H; Wilhelmi, O; Yang, P; Zheng, H W; Underhay, I J

    2003-01-01

    The Singapore Synchrotron Light Source is a general-purpose synchrotron radiation facility serving research organisations and industry. Beamlines active or coming up within 2002 include lithography for micro/nanofabrication, phase contrast imaging, surface science, and X-ray diffraction and absorption. An infrared spectro/microscopy beamline is expected to become operational in 2003. Further beamlines are under discussion with user groups. The Microtron Undulator Radiation Facility (MURF) is under development to provide brilliant VUV radiation and to prepare for subsequent development of an EUV and X-ray FEL.

  10. Synchrotron Polarization and Synchrotron Self-absorption Spectra for a Power-law Particle Distribution with Finite Energy Range

    Science.gov (United States)

    Fouka, M.; Ouichaoui, S.

    2011-12-01

    We have derived asymptotic forms for the degree of polarization of the optically thin synchrotron and for synchrotron self-absorption (SSA) spectra assuming a power-law particle distribution of the form N(γ) ~ γ-p with γ1 Lambert W function based on the analytical asymptotic form of the absorption coefficient, αν, for the high-frequency range ν Gt ν2 (with ν2 the synchrotron frequency corresponding to γ2). We have shown that the latter frequency may not have realistic applications in astrophysics, except in the case of an adequate set of parameters allowing one to neglect Comptonization effects. More detailed calculations and discussions are presented.

  11. National Synchrotron Light Source 2010 Activity Report

    Energy Technology Data Exchange (ETDEWEB)

    Rowe, M.; Snyder, K. J.

    2010-12-29

    This is a very exciting period for photon sciences at Brookhaven National Laboratory. It is also a time of unprecedented growth for the Photon Sciences Directorate, which operates the National Synchrotron Light Source (NSLS) and is constructing NSLS-II, both funded by the Department of Energy's Office of Science. Reflecting the quick pace of our activities, we chose the theme 'Discovery at Light Speed' for the directorate's 2010 annual report, a fiscal year bookended by October 2009 and September 2010. The year began with the news that NSLS users Venki Ramakrishnan of Cambridge University (also a former employee in Brookhaven's biology department) and Thomas A. Steitz of Yale University were sharing the 2009 Nobel Prize in Chemistry with Ada E. Yonath of the Weizmann Institute of Science. Every research project has the potential for accolades. In 2010, NSLS users and staff published close to 900 papers, with about 170 appearing in premiere journals. Those are impressive stats for a facility nearly three decades old, testament to the highly dedicated team keeping NSLS at peak performance and the high quality of its user community. Our NSLS users come from a worldwide community of scientists using photons, or light, to carry out research in energy and environmental sciences, physics, materials science, chemistry, biology and medicine. All are looking forward to the new capabilities enabled by NSLS-II, which will offer unprecedented resolution at the nanoscale. The new facility will produce x-rays more than 10,000 times brighter than the current NSLS and host a suite of sophisticated instruments for cutting-edge science. Some of the scientific discoveries we anticipate at NSLS-II will lead to major advances in alternative energy technologies, such as hydrogen and solar. These discoveries could pave the way to: (1) catalysts that split water with sunlight for hydrogen production; (2) materials that can reversibly store large quantities of

  12. Synchrotron-Radiation Induced X-Ray Emission (SRIXE)

    Energy Technology Data Exchange (ETDEWEB)

    Jones, Keith W.

    1999-09-01

    Elemental analysis using emission of characteristic x rays is a well-established scientific method. The success of this analytical method is highly dependent on the properties of the source used to produce the x rays. X-ray tubes have long existed as a principal excitation source, but electron and proton beams have also been employed extensively. The development of the synchrotron radiation x-ray source that has taken place during the past 40 years has had a major impact on the general field of x-ray analysis. Even tier 40 years, science of x-ray analysis with synchrotron x-ray beams is by no means mature. Improvements being made to existing synchrotron facilities and the design and construction of new facilities promise to accelerate the development of the general scientific use of synchrotron x-ray sources for at least the next ten years. The effective use of the synchrotron source technology depends heavily on the use of high-performance computers for analysis and theoretical interpretation of the experimental data. Fortunately, computer technology has advanced at least as rapidly as the x-ray technology during the past 40 years and should continue to do so during the next decade. The combination of these technologies should bring about dramatic advances in many fields where synchrotron x-ray science is applied. It is interesting also to compare the growth and rate of acceptance of this particular research endeavor to the rates for other technological endeavors. Griibler [1997] cataloged the time required for introduction, diffusion,and acceptance of technological, economic, and social change and found mean values of 40 to 50 years. The introduction of the synchrotron source depends on both technical and non-technical factors, and the time scale at which this seems to be occurring is quite compatible with what is seen for other major innovations such as the railroad or the telegraph. It will be interesting to see how long the present rate of technological change

  13. Brazilian medical publications: citation patterns for Brazilian-edited and non-Brazilian literature

    Directory of Open Access Journals (Sweden)

    J.R. Cunha-Melo

    2006-08-01

    Full Text Available Today, the quality of a scientific article depends on the periodical in which it is published and on the number of times the article is cited in the literature. In Brazil, the criteria for the evaluation of this scientific production are improving. However, there is still some resistance, with authors arguing that Brazilian publications must be preferentially addressed to the national readers and, therefore, they should ideally be written in Portuguese. In order to determine the kind of scientific journals cited in the reference lists of articles published in medical periodicals edited in Brazil, in the present study we determine the rate of Portuguese/English citations. Three issues of 43 periodicals (19 indexed in SciELO, 10 in PubMed, 10 in LILACS, and 4 in the ISI-Thompson base of different medical specialties were analyzed, and the number of both Portuguese and English citations in the reference list of each article was recorded. The results showed that in Brazilian-edited journals the mean number of citations/article was 20.9 ± 6.9 and the percentage of citations of international non-Brazilian periodicals was 86.0 ± 11.2%. Of the latter, 94.4 ± 7.0 are indexed by ISI-Thompson. Therefore, we conclude that Brazilian medical scientists cite the international non-Brazilian periodicals more than the national journals, and most of the cited papers are indexed by ISI-Thompson.

  14. White Beam, X-Ray, Energy-Dispersive Diffractometry using Synchrotron Radiation

    DEFF Research Database (Denmark)

    Gerward, Leif; Buras, B.; Olsen, J. Staun

    1978-01-01

    The special features of left double quote white right double quote beam X-ray energy-dispersive diffractometry using synchrotron radiation are discussed on the basis of experiments performed at the Deutsches Electronen-Synchrotron, DESY.......The special features of left double quote white right double quote beam X-ray energy-dispersive diffractometry using synchrotron radiation are discussed on the basis of experiments performed at the Deutsches Electronen-Synchrotron, DESY....

  15. Experimental Determination of the Hamiltonian for Synchrotron Motion with RF Phase Modulation

    Energy Technology Data Exchange (ETDEWEB)

    Minty, Michiko

    2003-07-11

    Synchrotron motion with rf phase modulation was studied experimentally. Poincare maps in the resonant processing frame were obtained from the experimental data and compared with the tori of the resonant Hamiltonian. The experimental data revealed island structure in longitudinal phase space. Experimental results for synchrotron motion excited by phase modulation at the third harmonic of the synchrotron frequency are also reported.

  16. The Scale Invariant Synchrotron Jet of Flat Spectrum Radio Quasars

    Indian Academy of Sciences (India)

    2016-01-27

    Jan 27, 2016 ... In this paper, the scale invariance of the synchrotron jet of Flat Spectrum Radio Quasars has been studied using a sample of combined sources from FKM04 and from SDSS DR3 catalogue. Since the research of scale invariance has been focused on sub-Eddington cases that can be fitted onto the ...

  17. The Scale Invariant Synchrotron Jet of Flat Spectrum Radio Quasars ...

    Indian Academy of Sciences (India)

    Abstract. In this paper, the scale invariance of the synchrotron jet of Flat. Spectrum Radio Quasars has been studied using a sample of combined sources from FKM04 and from SDSS DR3 catalogue. Since the research of scale invariance has been focused on sub-Eddington cases that can be fitted onto the fundamental ...

  18. Design and construction of the prototype synchrotron radiation detector

    Energy Technology Data Exchange (ETDEWEB)

    Anderhub, H.; Bates, J.R.; Baetzner, D.; Baumgartner, S.; Biland, A.; Camps, C.; Capell, M.; Commichau, V.; Djambazov, L.; Fanchiang, Y.-J.; Fluegge, G.; Fritschi, M.; Grimm, O.; Hangarter, K.; Hofer, H.; Horisberger, U.; Kan, R.; Kaestli, W.; Kenney, G.P.; Kim, G.N.; Kim, K.S.; Koutsenko, V.; Kraeber, M.; Kuipers, J.; Lebedev, A.; Lee, M.W.; Lee, S.-C.; Lewis, R.; Lustermann, W.; Pauss, F.; Rauber, T.; Ren, D.; Ren, Z.L.; Roeser, U.; Son, D.; Ting, S.C.C.; Tiwari, A.N.; Viertel, G.M. E-mail: viertel@particle.phys.ethz.ch; Gunten, H. von; Wicki, S. Waldmeier; Wang, T.-S.; Yang, J.; Zimmermann, B

    2002-09-21

    The Prototype Synchrotron Radiation Detector (PSRD) is a small-scale experiment designed to measure the rate of low-energy charged particles and photons in near the Earth's orbit. It is a precursor to the Synchrotron Radiation Detector (SRD), a proposed addition to the upgraded version of the Alpha Magnetic Spectrometer (AMS-02). The SRD will use the Earth's magnetic field to identify the charge sign of electrons and positrons with energies above 1 TeV by detecting the synchrotron radiation they emit in this field. The differential energy spectrum of these particles is astrophysically interesting and not well covered by the remaining components of AMS-02. Precise measurements of this spectrum offer the possibility to gain information on the acceleration mechanism and characteristics of all cosmic rays in our galactic neighbourhood. The SRD will discriminate against protons as they radiate only weakly. Both the number and energy of the synchrotron photons that the SRD needs to detect are small. The identification is complicated by the presence of a large particle and photon background. Existing measurements of these backgrounds are insufficient for the construction of the large-scale SRD, so a measurement in space was indispensable. The PSRD was designed to fly as a Space Shuttle secondary payload, within the Shuttle Small Payloads Project. The flight on board the Space Shuttle Endeavour took place from 5 to 17 December 2001. The scientific goal, hardware and the flight of the PSRD are described in this report.

  19. Magnetic X-Ray Scattering with Synchrotron Radiation

    DEFF Research Database (Denmark)

    Moncton, D. E.; Gibbs, D.; Bohr, Jakob

    1986-01-01

    With the availability of high-brilliance synchrotron radiation from multiple wigglers, magnetic X-ray scattering has become a powerful new probe of magnetic structure and phase transitions. Similar to the well-established magnetic neutron scattering technique, magnetic X-ray scattering methods have...

  20. CCD detectors for X-ray synchrotron radiation application

    CERN Document Server

    Fedotov, M G

    2000-01-01

    In this paper the possibility of the application of some types of CCDs for the study of fast processes (by recording an image formed by a short flash of synchrotron radiation) is considered. The first results of model experiments are also described.

  1. Design and construction of the prototype synchrotron radiation detector

    CERN Document Server

    Anderhub, H; Baetzner, D; Baumgartner, S; Biland, A; Camps, C; Capell, M; Commichau, V; Djambazov, L; Fanchiang, Y J; Flügge, G; Fritschi, M; Grimm, O; Hangarter, K; Hofer, H; Horisberger, Urs; Kan, R; Kaestli, W; Kenney, G P; Kim, G N; Kim, K S; Koutsenko, V F; Kraeber, M; Kuipers, J; Lebedev, A; Lee, M W; Lee, S C; Lewis, R; Lustermann, W; Pauss, Felicitas; Rauber, T; Ren, D; Ren, Z L; Röser, U; Son, D; Ting, Samuel C C; Tiwari, A N; Viertel, Gert M; Gunten, H V; Wicki, S W; Wang, T S; Yang, J; Zimmermann, B

    2002-01-01

    The Prototype Synchrotron Radiation Detector (PSRD) is a small-scale experiment designed to measure the rate of low-energy charged particles and photons in near the Earth's orbit. It is a precursor to the Synchrotron Radiation Detector (SRD), a proposed addition to the upgraded version of the Alpha Magnetic Spectrometer (AMS-02). The SRD will use the Earth's magnetic field to identify the charge sign of electrons and positrons with energies above 1 TeV by detecting the synchrotron radiation they emit in this field. The differential energy spectrum of these particles is astrophysically interesting and not well covered by the remaining components of AMS-02. Precise measurements of this spectrum offer the possibility to gain information on the acceleration mechanism and characteristics of all cosmic rays in our galactic neighbourhood. The SRD will discriminate against protons as they radiate only weakly. Both the number and energy of the synchrotron photons that the SRD needs to detect are small. The identificat...

  2. Dedicated Beamline Facilities for Catalytic Research. Synchrotron Catalysis Consortium (SCC)

    Energy Technology Data Exchange (ETDEWEB)

    Chen, Jingguang [Columbia Univ., New York, NY; Frenkel, Anatoly [Yeshiva Univ., New York, NY (United States); Rodriguez, Jose [Brookhaven National Lab. (BNL), Upton, NY (United States); Adzic, Radoslav [Brookhaven National Lab. (BNL), Upton, NY (United States); Bare, Simon R. [UOP LLC, Des Plaines, IL (United States); Hulbert, Steve L. [Brookhaven National Lab. (BNL), Upton, NY (United States); Karim, Ayman [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Mullins, David R. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Overbury, Steve [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

    2015-03-04

    Synchrotron spectroscopies offer unique advantages over conventional techniques, including higher detection sensitivity and molecular specificity, faster detection rate, and more in-depth information regarding the structural, electronic and catalytic properties under in-situ reaction conditions. Despite these advantages, synchrotron techniques are often underutilized or unexplored by the catalysis community due to various perceived and real barriers, which will be addressed in the current proposal. Since its establishment in 2005, the Synchrotron Catalysis Consortium (SCC) has coordinated significant efforts to promote the utilization of cutting-edge catalytic research under in-situ conditions. The purpose of the current renewal proposal is aimed to provide assistance, and to develop new sciences/techniques, for the catalysis community through the following concerted efforts: Coordinating the implementation of a suite of beamlines for catalysis studies at the new NSLS-II synchrotron source; Providing assistance and coordination for catalysis users at an SSRL catalysis beamline during the initial period of NSLS to NSLS II transition; Designing in-situ reactors for a variety of catalytic and electrocatalytic studies; Assisting experimental set-up and data analysis by a dedicated research scientist; Offering training courses and help sessions by the PIs and co-PIs.

  3. Synchrotron Radiation Therapy from a Medical Physics point of view

    Science.gov (United States)

    Prezado, Y.; Adam, J. F.; Berkvens, P.; Martinez-Rovira, I.; Fois, G.; Thengumpallil, S.; Edouard, M.; Vautrin, M.; Deman, P.; Bräuer-Krisch, E.; Renier, M.; Elleaume, H.; Estève, F.; Bravin, A.

    2010-07-01

    Synchrotron radiation (SR) therapy is a promising alternative to treat brain tumors, whose management is limited due to the high morbidity of the surrounding healthy tissues. Several approaches are being explored by using SR at the European Synchrotron Radiation Facility (ESRF), where three techniques are under development Synchrotron Stereotactic Radiation Therapy (SSRT), Microbeam Radiation Therapy (MRT) and Minibeam Radiation Therapy (MBRT). The sucess of the preclinical studies on SSRT and MRT has paved the way to clinical trials currently in preparation at the ESRF. With this aim, different dosimetric aspects from both theoretical and experimental points of view have been assessed. In particular, the definition of safe irradiation protocols, the beam energy providing the best balance between tumor treatment and healthy tissue sparing in MRT and MBRT, the special dosimetric considerations for small field dosimetry, etc will be described. In addition, for the clinical trials, the definition of appropiate dosimetry protocols for patients according to the well established European Medical Physics recommendations will be discussed. Finally, the state of the art of the MBRT technical developments at the ESRF will be presented. In 2006 A. Dilmanian and collaborators proposed the use of thicker microbeams (0.36-0.68 mm). This new type of radiotherapy is the most recently implemented technique at the ESRF and it has been called MBRT. The main advantage of MBRT with respect to MRT is that it does not require high dose rates. Therefore it can be more easily applied and extended outside synchrotron sources in the future.

  4. Science minister puts French synchrotron back on the agenda

    CERN Multimedia

    2000-01-01

    The new French minister of Science has said that he would pursue plans to build a synchrotron in France, reversing the decision of his predecessor. He is still intending to participate in the British project Diamond though (1/2 page).

  5. Synchrotron light sources: The search for quantum chaos

    Energy Technology Data Exchange (ETDEWEB)

    Schlachter, Fred

    2001-02-01

    A storage ring is a specialized synchrotron in which a stored beam of relativistic electrons produces radiation in the vuv and x-ray regions of the spectrum. High-brightness radiation is used at the ALS to study doubly excited autoionizing states of the helium atom in the search for quantum chaos.

  6. Synchrotron Radiation in eRHIC Interaction Region

    CERN Document Server

    Beebe-Wang, Joanne; Montag, Christoph; Rondeau, Daniel J; Surrow, Bernd

    2005-01-01

    The eRHIC currently under study at BNL consists of an electron storage ring added to the existing RHIC complex. The interaction region of this facility has to provide the required low-beta focusing while accommodating the synchrotron radiation generated by beam separation close to the interaction point. In the current design, the synchrotron radiation caused by 10GeV electrons bent by low-beta triplet magnets will be guided through the interaction region and dumped 5m downstream. However, it is unavoidable to stop a fraction of the photons at the septum where the electron and ion vacuum system are separated. In order to protect the septum and minimize the backward scattering of the synchrotron radiation, an absorber and collimation system will be employed. In this paper, we first present the overview of the current design of the eRHIC interaction region with special emphasis on the synchrotron radiation. Then the initial design of the absorber and collimation system, including their geometrical and physical p...

  7. Dazzling new light source opens at Stanford synchrotron radiation laboratory

    CERN Multimedia

    2004-01-01

    SPEAR3, the Stanford Positron Electron Asymmetric Ring, was formally opened at a dedication ceremony at the Stanford Linear Accelerator Center on Jan. 29. It incorporates the latest technology to make it competitive with the best synchrotron sources in the world (1/2 page)

  8. Synchrotron-based X-ray fluorescence, imaging and elemental ...

    Indian Academy of Sciences (India)

    Analysis of the small areas will be better suited to establish the physiology of metals in specific structures like small animal shell and the distribution of other elements. Keywords. X-ray fluorescence; synchrotron-based excitation; imaging; elemental mapping; biological samples. PACS Nos 78.70.En; 29.20.dk; 87.59.

  9. Operation of the Australian Store.Synchrotron for macromolecular crystallography.

    Science.gov (United States)

    Meyer, Grischa R; Aragão, David; Mudie, Nathan J; Caradoc-Davies, Tom T; McGowan, Sheena; Bertling, Philip J; Groenewegen, David; Quenette, Stevan M; Bond, Charles S; Buckle, Ashley M; Androulakis, Steve

    2014-10-01

    The Store.Synchrotron service, a fully functional, cloud computing-based solution to raw X-ray data archiving and dissemination at the Australian Synchrotron, is described. The service automatically receives and archives raw diffraction data, related metadata and preliminary results of automated data-processing workflows. Data are able to be shared with collaborators and opened to the public. In the nine months since its deployment in August 2013, the service has handled over 22.4 TB of raw data (∼1.7 million diffraction images). Several real examples from the Australian crystallographic community are described that illustrate the advantages of the approach, which include real-time online data access and fully redundant, secure storage. Discoveries in biological sciences increasingly require multidisciplinary approaches. With this in mind, Store.Synchrotron has been developed as a component within a greater service that can combine data from other instruments at the Australian Synchrotron, as well as instruments at the Australian neutron source ANSTO. It is therefore envisaged that this will serve as a model implementation of raw data archiving and dissemination within the structural biology research community.

  10. Synchrotron radiation vacuum chamber installation and beam size

    Energy Technology Data Exchange (ETDEWEB)

    Shleifer, M.

    1985-01-01

    In this paper we address the question of storage ring vacuum chamber placement and its effect on the synchrotron radiation fan obtainable. We consider only horizonal errors and thus treat the problem two-dimensionally. Specifically, we describe the correlation between the parameters of the chamber and its position in the magnet and the size of the fan of radiation emerging from a port.

  11. Detection and spectral measurements of coherent synchrotron radiation at FLASH

    Energy Technology Data Exchange (ETDEWEB)

    Behrens, Christopher

    2010-02-15

    The operation of high-gain free-electron laser (FEL) underlies tremendous demands on high quality electron beams with high peak currents. At the Free-Electron-Laser in Hamburg (FLASH), two magnetic bunch compressors are used to compress the electron bunches longitudinally. In the bunch compressor magnets, these short electron bunches generate coherent synchrotron radiation (CSR). This CSR contains information on the longitudinal bunch profile, which is relevant for driving an FEL. In order to investigate coherent synchrotron radiation at the second bunch compressor BC3 at FLASH, a new setup behind the last dipole was installed. For the detection of coherent synchrotron radiation, which is emitted in the infrared regime, pyroelectric detectors were used. These pyroelectric detectors have been calibrated at the free-electron laser FELIX in the wavelength range from 5 {mu}m to 110 {mu}m. For characterisation of the emitted radiation, a transverse scanning device was used to measure the transverse intensity distribution. Various transmission filters were used to obtain additional information about the spectral content. In order to get spectral information with high resolution over a wide wavelength range, a rotating mirror spectrometer using reflective blazed gratings was installed. Using this spectrometer, the first spectral measurements of coherent synchrotron radiation at FLASH in a wavelength range from 10 {mu}m to 160 {mu}m were done. (orig.)

  12. Coherence Inherent in an Incoherent Synchrotron Radio Source ...

    Indian Academy of Sciences (India)

    Galaxies: active—quasars: general—radiation mechanisms: non-thermal—radio continuum: general. 1. Introduction. It is well known that synchrotron radiation mechanism does not allow MASER type coherent emission .... been sometimes called in the literature a 'cosmic conspiracy' (Cotton et al. 1980). Although one ...

  13. Observation of Coherent Synchrotron Radiation at NewSUBARU

    CERN Document Server

    Hashimoto, Satoshi; Shoji, Yoshihiko; Takahashi, Toshiharu

    2005-01-01

    Coherent Synchrotron Radiation from a short electron bunch in a storage ring was observed at NewSUBARU. The energy of electron was 1GeV. The ring was operated with quasi-isochronous mode. The linear momentum compaction factor was smaller than 2 X 10

  14. Sensitivity of transient synchrotron radiation to tokamak plasma parameters

    Energy Technology Data Exchange (ETDEWEB)

    Fisch, N.J.; Kritz, A.H.

    1988-12-01

    Synchrotron radiation from a hot plasma can inform on certain plasma parameters. The dependence on plasma parameters is particularly sensitive for the transient radiation response to a brief, deliberate, perturbation of hot plasma electrons. We investigate how such a radiation response can be used to diagnose a variety of plasma parameters in a tokamak. 18 refs., 13 figs.

  15. Initial scientific uses of coherent synchrotron radiation inelectron storage rings

    Energy Technology Data Exchange (ETDEWEB)

    Basov, D.N.; Feikes, J.; Fried, D.; Holldack, K.; Hubers, H.W.; Kuske, P.; Martin, M.C.; Pavlov, S.G.; Schade, U.; Singley, E.J.; Wustefeld, G.

    2004-11-23

    The production of stable, high power, coherent synchrotron radiation at sub-terahertz frequency at the electron storage ring BESSY opens a new region in the electromagnetic spectrum to explore physical properties of materials. Just as conventional synchrotron radiation has been a boon to x-ray science, coherent synchrotron radiation may lead to many new innovations and discoveries in THz physics. With this new accelerator-based radiation source we have been able to extend traditional infrared measurements down into the experimentally poorly accessible sub-THz frequency range. The feasibility of using the coherent synchrotron radiation in scientific applications was demonstrated in a series of experiments: We investigated shallow single acceptor transitions in stressed and unstressed Ge:Ga by means of photoconductance measurements below 1 THz. We have directly measured the Josephson plasma resonance in optimally doped Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8} for the first time and finally we succeeded to confine the sub-THz radiation for spectral near-field imaging on biological samples such as leaves and human teeth.

  16. Comparison of frailty among Japanese, Brazilian Japanese descendants and Brazilian community-dwelling older women.

    Science.gov (United States)

    Sampaio, Priscila Yukari Sewo; Sampaio, Ricardo Aurélio Carvalho; Yamada, Minoru; Ogita, Mihoko; Arai, Hidenori

    2015-06-01

    To investigate frailty in Japanese, Brazilian Japanese descendants and Brazilian older women. The collected data included sociodemographic and health-related characteristics, and the frailty index Kihon Checklist. We analyzed the differences between the mean scores of Kihon Checklist domains (using ancova) and the percentage of frail women (using χ(2)-test). We carried out a binary logistic regression with Kihon Checklist domains. A total of 211 participants (Japanese n = 84, Brazilian Japanese descendants n = 55, Brazilian n = 72) participated in this research. The Brazilian participants had the highest total Kihon Checklist scores (more frail), whereas the Brazilian Japanese descendants had the lowest scores (P Brazilian group had more participants with oral dysfunction (P Brazilian women were likely to be more frail than the participants in other groups. More than the environment itself, the lifestyle and sociodemographic conditions could affect the frailty of older Brazilian women. © 2014 Japan Geriatrics Society.

  17. Transverse beam stacking injection system for synchrotron light source booster synchrotrons

    Directory of Open Access Journals (Sweden)

    R. P. Fliller, III

    2011-02-01

    Full Text Available Beam intensity is a key performance parameter for particle accelerators. Modern high-performance storage rings demand injectors that can deliver large currents per injection cycle, which translates to an increase in machine size and consumed power. Therefore, it is justifiable to look for ways to increase the injector’s performance while minimizing the size increase. We have investigated a number of ways to accumulate charge in a booster synchrotron and applied one of them to the NSLS-II booster. We have designed a scheme to transversely stack two bunch trains from the injector linac in the booster. In this paper we discuss this stacking scheme. The relevant booster dynamics are studied. The charge transport efficiency of the stacking scheme is studied in detail at injection and through a full booster ramp. Pulsed magnet requirements for the injection system and methods to achieve them are discussed. We show that the charge transport efficiency of the stacking scheme is similar to a single bunch train in the booster. This has become a critical design feature of the NSLS-II booster.

  18. Synchrotron radiation applications in medical research at Brookhaven National Laboratory

    Energy Technology Data Exchange (ETDEWEB)

    Thomlinson, W.

    1997-08-01

    In the relatively short time that synchrotrons have been available to the scientific community, their characteristic beams of UV and X-ray radiation have been applied to virtually all areas of medical science which use ionizing radiation. The ability to tune intense monochromatic beams over wide energy ranges clearly differentiates these sources from standard clinical and research tools. The tunable spectrum, high intrinsic collimation of the beams, polarization and intensity of the beams make possible in-vitro and in-vivo research and therapeutic programs not otherwise possible. From the beginning of research operation at the National Synchrotron Light Source (NSLS), many programs have been carrying out basic biomedical research. At first, the research was limited to in-vitro programs such as the x-ray microscope, circular dichroism, XAFS, protein crystallography, micro-tomography and fluorescence analysis. Later, as the coronary angiography program made plans to move its experimental phase from SSRL to the NSLS, it became clear that other in-vivo projects could also be carried out at the synchrotron. The development of SMERF (Synchrotron Medical Research Facility) on beamline X17 became the home not only for angiography but also for the MECT (Multiple Energy Computed Tomography) project for cerebral and vascular imaging. The high energy spectrum on X17 is necessary for the MRT (Microplanar Radiation Therapy) experiments. Experience with these programs and the existence of the Medical Programs Group at the NSLS led to the development of a program in synchrotron based mammography. A recent adaptation of the angiography hardware has made it possible to image human lungs (bronchography). Fig. 1 schematically depicts the broad range of active programs at the NSLS.

  19. Hard X-ray Sources for the Mexican Synchrotron Project

    Science.gov (United States)

    Reyes-Herrera, Juan

    2016-10-01

    One of the principal tasks for the design of the Mexican synchrotron was to define the storage ring energy. The main criteria for choosing the energy come from studying the electromagnetic spectrum that can be obtained from the synchrotron, because the energy range of the spectrum that can be obtained will determine the applications available to the users of the future light source. Since there is a public demand of hard X-rays for the experiments in the synchrotron community users from Mexico, in this work we studied the emission spectra from some hard X-ray sources which could be the best options for the parameters of the present Mexican synchrotron design. The calculations of the flux and the brightness for one Bending Magnet and four Insertion Devices are presented; specifically, for a Superconducting Bending Magnet (SBM), a Superconducting Wiggler (SCW), an In Vacuum Short Period Undulator (IV-SPU), a Superconducting Undulator (SCU) and for a Cryogenic Permanent Magnet Undulator (CPMU). Two commonly available synchrotron radiation programs were used for the computation (XOP and SRW). From the results, it can be concluded that the particle beam energy from the current design is enough to have one or more sources of hard X-rays. Furthermore, a wide range of hard X-ray region can be covered by the analyzed sources, and the choice of each type should be based on the specific characteristics of the X-ray beam to perform the experiments at the involved beamline. This work was done within the project Fomix Conacyt-Morelos ”Plan Estrategico para la construccion y operación de un Sincrotron en Morelos” (224392).

  20. INNOVATION IN BRAZILIAN SMALL COMPANIES

    National Research Council Canada - National Science Library

    Rodrigues, Tonny Kerley de Alencar; Lira, Átila De Melo; Naas, Irenilza De Alencar

    2015-01-01

    .... And the data confirms that small Brazilian companies generally have difficulties to sell their innovations. Keywords: innovation, small enterprises, patents. 1. INTRODUCTION Companies worldwide are looking to technological innovation as feasible for your market expansion (BURNS; STALKER, 1961; NELSON, 1993) alternative. In Brazil, the change an...

  1. BRAZILIAN EXPORTS OF MANUFACTURED WOOD

    Directory of Open Access Journals (Sweden)

    Rafael de Azevedo Calderon

    2010-08-01

    Full Text Available The present work deals with the Brazilian exports of sawnwood of non-coniferous, veneer sheets and plywood, from 1961 to 2002. The data regarding the three studied products, sawnwood of non-coniferous, veneer sheets and plywood, were joined through the method of Fisher so that an econometric evaluation of the market of the three products could be carried out. Supply and demand models of the Brazilian exports were specified. The results were satisfactory and they match with the literature. The supply of exports presented a positive answer in relation to the exporter's remuneration, to the production, to the use of the installed capacity (cycles of domestic economical activity and to the tendency, and negative in relation to the internal demand. The demand for the Brazilian exports was influenced positively by the world income, participation index and tendency, and negatively for the relative price. The low elasticity-price of the found demand can have implications in the conservation of the Brazilian forest resources because the exporters can increase the prices, reduce the amounts and still increase the incomes.

  2. Deforestation in the Brazilian Amazon

    NARCIS (Netherlands)

    Boekhout van Solinge, T.|info:eu-repo/dai/nl/156696207

    2015-01-01

    This essay takes a (green) criminological and multidisciplinary perspective on deforestation in the Brazilian Amazon, by focusing on the crimes and damages that are associated with Amazonian deforestation. The analysis and results are partly based on longer ethnographic stays in North Brazil (Amazon

  3. Laboratory simulation of interplanetary ultraviolet radiation (broad spectrum) and its effects on Deinococcus radiodurans

    Science.gov (United States)

    Paulino-Lima, Ivan Gláucio; Pilling, Sérgio; Janot-Pacheco, Eduardo; de Brito, Arnaldo Naves; Barbosa, João Alexandre Ribeiro Gonçalves; Leitão, Alvaro Costa; Lage, Claudia de Alencar Santos

    2010-08-01

    The radiation-resistant bacterium Deinococcus radiodurans was exposed to a simulated interplanetary UV radiation at the Brazilian Synchrotron Light Laboratory (LNLS). Bacterial samples were irradiated on different substrates to investigate the influence of surface relief on cell survival. The effects of cell multi-layers were also investigated. The ratio of viable microorganisms remained virtually the same (average 2%) for integrated doses from 1.2 to 12 kJ m -2, corresponding to 16 h of irradiation at most. The asymptotic profiles of the curves, clearly connected to a shielding effect provided by multi-layering cells on a cavitary substrate (carbon tape), means that the inactivation rate may not change significantly along extended periods of exposure to radiation. Such high survival rates reinforce the possibility of an interplanetary transfer of viable microbes.

  4. Oxide Nanolayers in Stratified Samples Studied by X-Ray Resonant Raman Scattering at Grazing Incidence

    Directory of Open Access Journals (Sweden)

    Juan José Leani

    2015-01-01

    Full Text Available X-ray resonant Raman scattering is applied at grazing incidence conditions with the aim of discriminating and identifying chemical environment of iron in different layers of stratified materials using a low resolution energy dispersive system. The methodology allows for depth studies with nanometric resolution. Nanostratified samples of Fe oxides were studied at the Brazilian synchrotron facility (LNLS using monochromatic radiation and an EDS setup. The measurements were carried out in grazing incident regime with incident photon energy lower than and close to the Fe-K absorption edge. The result allowed for characterizing oxide nanolayers, not observable with conventional geometries, identifying the oxidation state present in a particular depth of a sample surface with nanometric, or even subnanometric, resolution using a low-resolution system.

  5. New sensor and non-contact geometrical survey for the vibrating wire technique

    Energy Technology Data Exchange (ETDEWEB)

    Geraldes, Renan [Brazilian Synchrotron Light Laboratory (LNLS), Campinas, SP (Brazil); Junqueira Leão, Rodrigo, E-mail: rodrigo.leao@lnls.br [Brazilian Synchrotron Light Laboratory (LNLS), Campinas, SP (Brazil); Cernicchiaro, Geraldo [Brazilian Center for Research in Physics (CBPF), Rio de Janeiro, RJ (Brazil); Terenzi Neuenschwander, Regis; Citadini, James Francisco; Droher Rodrigues, Antônio Ricardo [Brazilian Synchrotron Light Laboratory (LNLS), Campinas, SP (Brazil)

    2016-03-01

    The tolerances for the alignment of the magnets in the girders of the next machine of the Brazilian Synchrotron Light Laboratory (LNLS), Sirius, are as small as 40 µm for translations and 0.2 mrad for rotations. Therefore, a novel approach to the well-known vibrating wire technique has been developed and tested for the precise fiducialization of magnets. The alignment bench consists of four commercial linear stages, a stretched wire, a commercial lock-in amplifier working with phase-locked loop (PLL), a coordinate measuring machine (CMM) and a vibration sensor for the wire. This novel sensor has been designed for a larger linear region of operation. For the mechanical metrology step of the fiducialization of quadrupoles an innovative technique, using the vision system of the CMM, is presented. While the work with pitch and yaw orientations is still ongoing with promising partial results, the system already presents an uncertainty level below 10 µm for translational alignment.

  6. Catalyst analysis using synchrotron X-ray microscopy

    Science.gov (United States)

    Jones, K. W.; Spanne, P.; Webb, S. W.; Conner, W. C.; Beyerlein, R. A.; Reagan, W. J.; Dautzenberg, F. M.

    1991-05-01

    Synchrotron X-ray microscopy techniques have been used to characterize several different types of heterogeneous catalysts. Using a collimator to produce microbeams with a size of less than 10μm, maps of the elemental distributions based on detection of the fluorescent X-rays were made, and computed microtomography (CMT) techniques were applied to produce " phase/density contrast" maps. CMT techniques were also used to determine the distribution of a specific major element by making measurements above and below the K X-ray absorption edge. The measurements were made using bending magnet radiation and, in one case, radiation from a 4 T superconducting wiggler at the National Synchrotron Light Source. Examples of applications to the study of polyethylene polymerization particles, fluid catalytic cracking catalysts, and hydrotreating catalysts are given.

  7. Synchrotron-based FTIR spectromicroscopy Cytotoxicity and heating considerations

    CERN Document Server

    Holman, H Y N; McKinney, W R

    2002-01-01

    Synchrotron radiation-based Fourier transform infrared (SR-FTIR) spectromicroscopy is a newly emerging bioanalytical and imaging tool. This unique technique provides mid-infrared (IR) spectra, hence chemical information, with high signal-to-noise at spatial resolutions as fine as 3 to 10 microns. Thus it enables researchers to locate, identify, and track specific chemical events within an individual living mammalian cell. Mid-IR photons are too low in energy (0.05 - 0.5 eV) to either break bonds or to cause ionization. In this review, we show that the synchrotron IR beam has no detectable effects on the short- and long-term viability, reproductive integrity, cell-cycle progression, and mitochondrial metabolism in living human cells, and produces only minimal sample heating (< 0.5 degrees C). These studies have established an important foundation for SR-FTIR spectromicroscopy in biological and biomedical research.

  8. The Radio Synchrotron Background: Conference Summary and Report

    Science.gov (United States)

    Singal, J.; Haider, J.; Ajello, M.; Ballantyne, D. R.; Bunn, E.; Condon, J.; Dowell, J.; Fixsen, D.; Fornengo, N.; Harms, B.; Holder, G.; Jones, E.; Kellermann, K.; Kogut, A.; Linden, T.; Monsalve, R.; Mertsch, P.; Murphy, E.; Orlando, E.; Regis, M.; Scott, D.; Vernstrom, T.; Xu, L.

    2018-03-01

    We summarize the radio synchrotron background workshop that took place 2017 July 19–21 at the University of Richmond. This first scientific meeting dedicated to the topic was convened because current measurements of the diffuse radio monopole reveal a surface brightness that is several times higher than can be straightforwardly explained by known Galactic and extragalactic sources and processes, rendering it by far the least well understood photon background at present. It was the conclusion of a majority of the participants that the radio monopole level is at or near that reported by the ARCADE 2 experiment and inferred from several absolutely calibrated zero-level lower frequency radio measurements, and unanimously agreed that the production of this level of surface brightness, if confirmed, represents a major outstanding question in astrophysics. The workshop reached a consensus on the next priorities for investigations of the radio synchrotron background.

  9. Coherent synchrotron radiation by electrons moving on circular orbits

    Science.gov (United States)

    Cai, Yunhai

    2017-06-01

    We study coherent synchrotron radiation by electrons in the Frenet-Serret coordinate system with a constant curvature 1 /ρ . Based on the Hamiltonian in the Courant-Synder theory of particle accelerators, we find in general that the transverse force is essentially the Lorentz force but with a substitution of the transverse magnetic field Bx ,y→(1 +x /ρ )Bx ,y , where x and y are the transverse positions. The curvature term provides us a key to derive the point-charge wakefield explicitly in terms of the incomplete elliptic integrals of the first and second kind, resulting in a steady-state theory of the coherent synchrotron radiation in two-dimensional free space.

  10. Coherent synchrotron radiation by electrons moving on circular orbits

    Directory of Open Access Journals (Sweden)

    Yunhai Cai

    2017-06-01

    Full Text Available We study coherent synchrotron radiation by electrons in the Frenet-Serret coordinate system with a constant curvature 1/ρ. Based on the Hamiltonian in the Courant-Synder theory of particle accelerators, we find in general that the transverse force is essentially the Lorentz force but with a substitution of the transverse magnetic field B_{x,y}→(1+x/ρB_{x,y}, where x and y are the transverse positions. The curvature term provides us a key to derive the point-charge wakefield explicitly in terms of the incomplete elliptic integrals of the first and second kind, resulting in a steady-state theory of the coherent synchrotron radiation in two-dimensional free space.

  11. Study of spear as a dedicated source of synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Cerino, J.; Golde, A.; Hastings, J.; Lindau, I.; Salsburg, B.; Winick, H.; Lee, M.; Morton, P.; Garren, A.

    1977-11-01

    A study was made of the potential of SPEAR as a dedicated source of synchrotron radiation, based on the expectation that SPEAR will become increasingly available for this purpose as PEP, the 18-GeV colliding-beam storage ring now under construction by LBL and SLAC, becomes operational. A synchrotron radiation research program has been underway since May, 1974. Two beam ports capable of serving 9 simultaneous users are now operational. In single-beam multi-bunch operation high currents are possible (225 mA has been achieved and > approximately 300 mA is expected) and the electron beam emittance can be made smaller, resulting in higher source point brightness. Descriptions are given of SPEAR capabilities and of plans to expand the research capability by adding beam runs and by inserting wiggler magnets in SPEAR straight sections.

  12. Study of SPEAR as dedicated source of synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Cerino, J. (Stanford Univ., CA); Golde, A.; Hastings, J.; Lindau, I.; Salsburg, B.; Winick, H.; Lee, M.; Morton, P.; Garren, A.

    1977-06-01

    The potential of SPEAR as a dedicated source of synchrotron radiation was studied, based on the expectation that SPEAR will become increasingly available for this purpose as PEP, the 18-GeV colliding-beam storage ring now under construction by LBL and SLAC, becomes operational. A synchrotron radiation research program has been underway since May, 1974. Two beam ports capable of serving nine simultaneous users are now operational. In single-beam multi-bunch operation high currents are possible (225 mA has been achieved and greater than or approximately equal to 300 mA is expected) and the electron beam emittance can be made smaller, resulting in higher source point brightness. Descriptions are given of SPEAR capabilities and of plans to expand the research capability by adding beam runs and by inserting wiggler magnets in SPEAR straight sections.

  13. Theory and calculations of synchrotron instabilities and feedback-mechanism

    Energy Technology Data Exchange (ETDEWEB)

    Meijssen, T.E.M.

    1981-08-12

    The properties of the phenomenon synchrotron radiation are given with general theory on the basic processes and betatron and synchrotron oscillations. A more extended theoretical view at transverse instabilities and the influence of a damping feedback system are discussed. The longitudinal case is covered. For the calculations on the longitudinal case with M equally spaced pointbunches, with N electrons each, in the storage ring, the parasitic modes of the radio-frequency cavity were measured. A description of this is given. The values of damping rates of the longitudinal feedback system found, are as expected, but too low to damp the longitudinal instabilities calculated. This might be caused by the input data. The calculated growth rates are very sensitive to changes in frequency and width of the parasitic modes, which were measured under conditions differing slightly from the operating conditions.

  14. Surface modification of fluorocarbon polymers by synchrotron radiation

    CERN Document Server

    Kanda, K; Matsui, S; Ideta, T; Ishigaki, H

    2003-01-01

    The surface modification of a poly (tetrafluoroethylene) sheet was carried out by synchrotron radiation in the soft X-ray region. The poly (tetrafluoroethylene) substrate was exposed to synchrotron radiation while varying the substrate temperature from room temperature to 200degC. The contact angle of the modified surfaces with a water drop decreased from 96deg to 72deg by the irradiation at room temperature, while the contact angle increased to 143deg by the irradiation at the substrate temperature of 200degC. Scanning electron microscopy suggested that this repellence was ascribable to the microstructure of the poly (tetrafluoroethylene) surface. We succeeded in controlling the wettability of the poly (tetrafluoroethylene) surface from hydrophobic to hydrophilic by irradiation of the soft X-ray light. (author)

  15. Synchrotron-based FTIR spectromicroscopy: Cytotoxicity and heating considerations

    Energy Technology Data Exchange (ETDEWEB)

    Holman, Hoi-Ying N.; Martin, Michael C.; McKinney, Wayne R.

    2002-12-13

    Synchrotron radiation-based Fourier transform infrared (SR-FTIR) spectromicroscopy is a newly emerging bioanalytical and imaging tool. This unique technique provides mid-infrared (IR) spectra, hence chemical information, with high signal-to-noise at spatial resolutions as fine as 3 to 10 microns. Thus it enables researchers to locate, identify, and track specific chemical events within an individual living mammalian cell. Mid-IR photons are too low in energy (0.05 - 0.5 eV) to either break bonds or to cause ionization. In this review, we show that the synchrotron IR beam has no detectable effects on the short- and long-term viability, reproductive integrity, cell-cycle progression, and mitochondrial metabolism in living human cells, and produces only minimal sample heating (< 0.5 degrees C). These studies have established an important foundation for SR-FTIR spectromicroscopy in biological and biomedical research.

  16. Estimation of presampling modulation transfer function in synchrotron radiation microtomography

    CERN Document Server

    Mizutani, Ryuta; Takeuchi, Akihisa; Uesugi, Kentaro; Suzuki, Yoshio

    2016-01-01

    The spatial resolution achieved by recent synchrotron radiation microtomographs should be estimated from the modulation transfer function (MTF) on the micrometer scale. Step response functions of a synchrotron radiation microtomograph were determined by the slanted edge method by using high-precision surfaces of diamond crystal and ion-milled aluminum wire. Tilted reconstruction was introduced to enable any edge to be used as the slanted edge by defining the reconstruction pixel matrix in an arbitrary orientation. MTFs were estimated from the step response functions of the slanted edges. The obtained MTFs coincided with MTF values estimated from square-wave patterns milled on the aluminum surface. Although x-ray refraction influences should be taken into account to evaluate MTFs, any flat surfaces with nanometer roughness can be used to determine the spatial resolutions of microtomographs.

  17. New synchrotron powder diffraction facility for long-duration experiments.

    Science.gov (United States)

    Murray, Claire A; Potter, Jonathan; Day, Sarah J; Baker, Annabelle R; Thompson, Stephen P; Kelly, Jon; Morris, Christopher G; Yang, Sihai; Tang, Chiu C

    2017-02-01

    A new synchrotron X-ray powder diffraction instrument has been built and commissioned for long-duration experiments on beamline I11 at Diamond Light Source. The concept is unique, with design features to house multiple experiments running in parallel, in particular with specific stages for sample environments to study slow kinetic systems or processes. The instrument benefits from a high-brightness X-ray beam and a large area detector. Diffraction data from the commissioning work have shown that the objectives and criteria are met. Supported by two case studies, the results from months of measurements have demonstrated the viability of this large-scale instrument, which is the world's first dedicated facility for long-term studies (weeks to years) using synchrotron radiation.

  18. Rapid cycling medical synchrotron and beam delivery system

    Science.gov (United States)

    Peggs, Stephen G [Port Jefferson, NY; Brennan, J Michael [East Northport, NY; Tuozzolo, Joseph E [Sayville, NY; Zaltsman, Alexander [Commack, NY

    2008-10-07

    A medical synchrotron which cycles rapidly in order to accelerate particles for delivery in a beam therapy system. The synchrotron generally includes a radiofrequency (RF) cavity for accelerating the particles as a beam and a plurality of combined function magnets arranged in a ring. Each of the combined function magnets performs two functions. The first function of the combined function magnet is to bend the particle beam along an orbital path around the ring. The second function of the combined function magnet is to focus or defocus the particle beam as it travels around the path. The radiofrequency (RF) cavity is a ferrite loaded cavity adapted for high speed frequency swings for rapid cycling acceleration of the particles.

  19. Passages on Brazilian scientific cinema.

    Science.gov (United States)

    de Almeida, Jane; da Silva, Cicero Inacio; Suppia, Alfredo; Stalbaum, Brett

    2017-07-01

    The article examines the conditions of production and recognition of scientific cinema in Brazil by comparing three distinct moments and contexts: the first moment takes place in the nineteenth century, and it is related to the contribution of a Brazilian astronomer otherwise little known to Brazilian film scholars, the second addresses Benedito Junqueira Duarte's voluminous mid-twentieth-century filmography, and the third moment documents recent scientific film experiences within ultra high resolution movies transmitted over photonic networks. Future trajectories for aesthetic concerns and practical issues such as the archiving of ultra high definition cinema are usefully informed by these histories of scientific cinema, even as a current generation of multidisciplinary teams including scientists, filmmakers, computer scientists, and network engineers reinvent, rediscover, and necessarily expand the scientific cinema toward concerns of real time collaboration and teaching.

  20. Polymer research at synchrotron radiation sources: symposium proceedings

    Energy Technology Data Exchange (ETDEWEB)

    Russell, T.P.; Goland, A.N. (eds.)

    1985-01-01

    The twenty-two papers are arranged into eleven sessions entitled: general overviews; time-resolved x-ray scattering; studies using fluorescence, ion-containing polymers; time-resolved x-ray scattering; novel applications of synchrotron radiation; phase transitions in polymers; x-ray diffraction on polymers; recent detector advances; complementary light, x-ray and neutron studies; and neutron scattering studies. Seven of the papers are processed separately; three of the remainder have been previously processed. (DLC)

  1. NUMERICAL METHODS FOR THE SIMULATION OF HIGH INTENSITY HADRON SYNCHROTRONS.

    Energy Technology Data Exchange (ETDEWEB)

    LUCCIO, A.; D' IMPERIO, N.; MALITSKY, N.

    2005-09-12

    Numerical algorithms for PIC simulation of beam dynamics in a high intensity synchrotron on a parallel computer are presented. We introduce numerical solvers of the Laplace-Poisson equation in the presence of walls, and algorithms to compute tunes and twiss functions in the presence of space charge forces. The working code for the simulation here presented is SIMBAD, that can be run as stand alone or as part of the UAL (Unified Accelerator Libraries) package.

  2. X-ray imaging detectors for synchrotron and XFEL sources

    OpenAIRE

    Takaki Hatsui; Heinz Graafsma

    2015-01-01

    Current trends for X-ray imaging detectors based on hybrid and monolithic detector technologies are reviewed. Hybrid detectors with photon-counting pixels have proven to be very powerful tools at synchrotrons. Recent developments continue to improve their performance, especially for higher spatial resolution at higher count rates with higher frame rates. Recent developments for X-ray free-electron laser (XFEL) experiments provide high-frame-rate integrating detectors with both high sensitivit...

  3. Lifetime increase using passive harmonic cavities in synchrotron light sources

    Directory of Open Access Journals (Sweden)

    J. M. Byrd

    2001-03-01

    Full Text Available Harmonic cavities have been used in storage rings to increase beam lifetime and Landau damping by lengthening the bunch. The need for lifetime increase is particularly great in the present generation of low to medium energy synchrotron light sources where the small transverse beam sizes lead to relatively short lifetimes from large-angle intrabeam (Touschek scattering. We review the beam dynamics of harmonic radio-frequency systems and discuss optimization of the beam lifetime using passive harmonic cavities.

  4. Putting synchrotron radiation to work for technology: Analytic methods

    Energy Technology Data Exchange (ETDEWEB)

    1992-02-01

    This report contains viewgraphs on: Advanced Light Source; Ultra-ESCA: Advanced Capabilities of XPS with High-Brightness Synchrotron Radiation; High-Resolution (20 nm) XPS and XANES with the ALS; Photoelectron Spectroscopy in Industry: Current Capabilities, Needs, and Possible Roles for the ALS; Materials Analysis by Photoemission: Is This Practical at ALS?; Applications of Long-Wavelength X-Ray Fluorescence Spectrometry and X-Ray Powder Diffractometry.

  5. Putting synchrotron radiation to work for technology: Analytic methods

    Energy Technology Data Exchange (ETDEWEB)

    1992-02-01

    This report contains viewgraphs on: Advanced Light Source; Ultra-ESCA: Advanced Capabilities of XPS with High-Brightness Synchrotron Radiation; High-Resolution (20 nm) XPS and XANES with the ALS; Photoelectron Spectroscopy in Industry: Current Capabilities, Needs, and Possible Roles for the ALS; Materials Analysis by Photoemission: Is This Practical at ALS ; Applications of Long-Wavelength X-Ray Fluorescence Spectrometry and X-Ray Powder Diffractometry.

  6. Spectral Evolution of Synchrotron and Inverse Compton Emission in ...

    Indian Academy of Sciences (India)

    emission peaks in the optical band (e.g., Nieppola et al. 2006). In order to under- stand the evolution of synchrotron and IC spectra of BL Lac objects, the X-ray spectral analysis with XMM–Newton X-ray observations of PKS 2155–304 and. S5 0716+7145 (see Zhang 2008, 2010 for details) was performed. Here, the results.

  7. Generation of Coherent Synchrotron Radiation from JAERI-ERL

    CERN Document Server

    Hajima, R; Kikuzawa, N; Minehara, E J; Nagai, R; Nishitani, T; Sawamura, M

    2005-01-01

    An electron beam with high-average current and short bunch length can be accelerated by energy-recovery linac. Coherent synchrotron radiation (CSR) from such an electron beam will be a useful light source around millimeter wavelength. We report results from a preliminary measurement of CSR emitted from a bending magnet of JAERI-ERL. Possible enhancement of CSR power by FEL micro-bunching is also discussed.

  8. Investigating spintronics thin film systems with synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Schneider, C.M. [Institut f. Festkoerperforschung IFF-9, Forschungszentrum Juelich, D-52425 Juelich (Germany); JARA-Juelich-Aachen Research Alliance, Forschungszentrum Juelich, D-52425 Juelich (Germany)], E-mail: c.m.schneider@fz-juelich.de; Krug, I.; Mueller, M.; Matthes, F.; Kaiser, A.; Wiemann, C.; Cramm, S. [Institut f. Festkoerperforschung IFF-9, Forschungszentrum Juelich, D-52425 Juelich (Germany); JARA-Juelich-Aachen Research Alliance, Forschungszentrum Juelich, D-52425 Juelich (Germany); Elmers, H.-J.; Wegelin, F.; Krasyuk, A.; Nepijko, S.A.; Schoenhense, G. [Inst. f. Physik, Joh.-Gutenberg Universitaet Mainz, D-55099 Mainz (Germany)

    2009-10-15

    Spintronics is a research field involving a wide variety of different magnetic materials. Synchrotron radiation in the VUV and soft X-ray regime is ideally suited to investigate the relationships between magnetic properties and electronic structure of spintronics thin film stacks. Complex layered structures and nanomagnets are the main building blocks for current and future spintronics applications. In this contribution we describe the study of spintronics model systems with respect to the static and dynamic behavior with an emphasis on interfaces.

  9. Brands Repositioning: Brazilian case studies

    OpenAIRE

    Serralvo, Francisco Antonio; Furrier, Márcio Tadeu

    2008-01-01

    Based on the assumption of the increasing relevance of both brand positioning and equity in the context of marketing management in competitive environments, the objective of this work was to deepen the existing knowledge on the brand repositioning process. Four theoretical models of reference obtained after literature review supported the empiric verification represented by content analysis of six reports (cases) of Brazilian brands repositioning experiences awarded with the “Top of Marketing...

  10. Brazilian Participation in World War II

    Science.gov (United States)

    2006-12-15

    internal rebellions and secessionist movements such as the Canudos rebellion in 1897 and 1898 in Bahia province. As a 2 result, the Brazilian Army...Brazilian Army would play an important role in ending this dictatorship. Brazil had accepted large numbers of Italian and German immigrants for more than...including the Brazilian Armed Forces. They had a significant influence on decision makers. In the 1930s, German immigrants numbered more than 900,000 and

  11. First application of computed radiology to mammography with synchrotron radiation.

    Science.gov (United States)

    Quai, E; Longo, R; Zanconati, F; Jaconelli, G; Tonutti, M; Abrami, A; Arfelli, F; Dreossi, D; Tromba, G; Cova, M A

    2013-02-01

    The aim of this study was to evaluate the feasibility of phase-contrast mammography with synchrotron radiation using a high-resolution computed radiology (CR) system devoted to mammography. The study was performed at the Synchrotron Radiation for Medical Physics (SYRMEP) beamline of the Elettra synchrotron radiation (SR) facility in Trieste (Italy); X-ray beams were in the range 16-22 keV with a high degree of monochromaticity and spatial coherence. The CR system evaluated is the FCR Profect CS by Fujifilm Global. The first images were obtained from test objects and surgical breast specimens. Images obtained using SR and both screen-film and the CR system were compared with images of the same samples acquired with digital mammography equipment. In view of the good quality of the results obtained, the CR system was used in two mammographic examinations with SR. Images acquired using SR and both screen-film and CR were obtained with the same level of delivered dose. Image quality obtained with CR was similar or superior to that of screen-film images. Moreover, the digital images obtained with SR were always better than those acquired using the digital mammography system. Phase-contrast mammography with SR using the studied CR system is a feasible option.

  12. Simple modification of Compton polarimeter to redirect synchrotron radiation

    Directory of Open Access Journals (Sweden)

    J. Benesch

    2015-11-01

    Full Text Available Synchrotron radiation produced as an electron beam passes through a bending magnet is a significant source of background in many experiments. Using modeling, we show that simple modifications of the magnet geometry can reduce this background by orders of magnitude in some circumstances. Specifically, we examine possible modifications of the four dipole magnets used in Jefferson Lab’s Hall A Compton polarimeter chicane. This Compton polarimeter has been a crucial part of experiments with polarized beams and the next generation of experiments will utilize increased beam energies, up to 11 GeV, requiring a corresponding increase in Compton dipole field to 1.5 T. In consequence, the synchrotron radiation (SR from the dipole chicane will be greatly increased. Three possible modifications of the chicane dipoles are studied; each design moves about 2% of the integrated bending field to provide a gentle bend in critical regions along the beam trajectory which, in turn, greatly reduces the synchrotron radiation within the acceptance of the Compton polarimeter photon detector. Each of the modifications studied also softens the SR energy spectrum at the detector sufficiently to allow shielding with 5 mm of lead. Simulations show that these designs are each capable of reducing the background signal due to SR by three orders of magnitude. The three designs considered vary in their need for vacuum vessel changes and in their effectiveness.

  13. Methods for lipid nanostructure investigation at neutron and synchrotron sources

    Science.gov (United States)

    Kiselev, M. A.

    2011-03-01

    A lipid membrane is a main component of biological membranes. Contemporary bionanotechnologies use phospholipids and ceramides as basic components of drugs and cosmetic preparations. Phospholipids-based nanoparticles are used as drug carriers. Effective development of bionanotechnologies in Russia calls for creation of physical methods to diagnose the particle nanostructure which would be promising for application in pharmacology. Radiation with wavelengths of 1-10 Å is an adequate instrument for detecting the nanostructure of lipid bi- and monolayers. The review deals with methods that apply neutron scattering and synchrotron radiation for studying nanostructures of lipid membranes, phospholipid nanoparticles, and phospholipid monolayers on a water surface by techniques of diffraction, small-angle scattering, and reflectometry. The importance of the mutually complementary application of neutron and synchrotron radiation for solving urgent problems of membrane biophysics, microbiology, dermapharmacology, and bionanotechnologies is demonstrated by particular examples of studies of phospholipid membranes and ceramide-based membranes. The efficiency of development and application of new methods for solving urgent problems of biophysics is shown. The review is written on the basis of results obtained over the period of 1999-2010 at the Joint Institute for Nuclear Research (JINR) Laboratory of Neutron Physics in collaboration with the Pharmaceutical Departments of universities of France (Paris-Sud, Chatenay Malabry) and Germany (Martin Luther University, Halle). The experiments were performed at various European and Russian neutron and synchrotron sources.

  14. DISCO: a low-energy multipurpose beamline at synchrotron SOLEIL.

    Science.gov (United States)

    Giuliani, Alexandre; Jamme, Frédéric; Rouam, Valérie; Wien, Frank; Giorgetta, Jean-Luc; Lagarde, Bruno; Chubar, Oleg; Bac, Stéphane; Yao, Isabelle; Rey, Solène; Herbeaux, Christian; Marlats, Jean-Louis; Zerbib, Daniel; Polack, François; Réfrégiers, Matthieu

    2009-11-01

    DISCO, a novel low-energy beamline covering the spectrum range from the VUV to the visible, has received its first photons at the French synchrotron SOLEIL. In this article the DISCO design and concept of three experimental stations serving research communities in biology and chemistry are described. Emphasis has been put on high flux generation and preservation of polarization at variable energy resolutions. The three experiments include a completely new approach for microscopy and atmospheric pressure experiments as well as a ;classical' synchrotron radiation circular dichroism station. Preliminary tests of the optical design and technical concept have been made. Theoretical predictions of the beam have been compared with the first images produced by the first photons originating from the large-aperture bending-magnet source. Results are also reported concerning the cold finger used to absorb hard X-ray radiation in the central part of the synchrotron beam and to avoid heavy thermal load on the following optics. Wavelength selection using monochromators with different gratings for each experimental set-up as well as beam propagation and conditioning throughout the optical system are detailed. First photons comply very well with the theoretical calculations.

  15. Coherent synchrotron radiation and bunch stability in a compactstorage ring

    Energy Technology Data Exchange (ETDEWEB)

    Venturini, Marco; Warnock, Robert; Ruth, Ronald; Ellison, James A.

    2004-04-09

    We examine the effect of the collective force due to coherent synchrotron radiation (CSR) in an electron storage ring with small bending radius. In a computation based on time-domain integration of the nonlinear Vlasov equation, we find the threshold current for a longitudinal microwave instability induced by CSR alone. The model accounts for suppression of radiation at long wave lengths due to shielding by the vacuum chamber. In a calculation just above threshold, small ripples in the charge distribution build up over a fraction of a synchrotron period, but then die out to yield a relatively smooth but altered distribution with eventual oscillations in bunch length. The instability evolves from small noise on an initial smooth bunch of r.m.s.length much greater than the shielding cutoff. The paper includes a derivation and extensive analysis of the complete impedance function Z for synchrotron radiation with parallel plate shielding. We find corrections to the lowest approximation to the coherent force which involve ''off-diagonal'' values of Z, that is, fields with phase velocity not equal to the particle velocity.

  16. Simulating synchrotron radiation in accelerators including diffuse and specular reflections

    Directory of Open Access Journals (Sweden)

    G. Dugan

    2017-02-01

    Full Text Available An accurate calculation of the synchrotron radiation flux within the vacuum chamber of an accelerator is needed for a number of applications. These include simulations of electron cloud effects and the design of radiation masking systems. To properly simulate the synchrotron radiation, it is important to include the scattering of the radiation at the vacuum chamber walls. To this end, a program called synrad3d has been developed which simulates the production and propagation of synchrotron radiation using a collection of photons. Photons generated by a charged particle beam are tracked from birth until they strike the vacuum chamber wall where the photon is either absorbed or scattered. Both specular and diffuse scattering is simulated. If a photon is scattered, it is further tracked through multiple encounters with the wall until it is finally absorbed. This paper describes the synrad3d program, with a focus on the details of its scattering model, and presents some examples of the program’s use.

  17. In situ electrochemical synchrotron radiation for Li-ion batteries.

    Science.gov (United States)

    Alemu, Tibebu; Wang, Fu Ming

    2018-01-01

    Observing the electronic structure, compositional change and morphological evolution of the surface and interface of a battery during operation provides essential information for developing new electrode materials for Li-ion batteries (LIBs); this is because such observations demonstrate the fundamental reactions occurring inside the electrode materials. Moreover, obtaining detailed data on chemical phase changes and distributions by analyzing an operating LIB is the most effective method for exploring the intercalation/de-intercalation process, kinetics and the relationship between phase change or phase distribution and battery performance, as well as for further optimizing the material synthesis routes for advanced battery materials. However, most conventional in situ electrochemical techniques (other than by using synchrotron radiation) cannot clearly or precisely demonstrate structural change, electron valence change and chemical mapping information. In situ electrochemical-synchrotron radiation techniques such as X-ray absorption spectroscopy, X-ray diffraction spectroscopy and transmission X-ray microscopy can deliver accurate information regarding LIBs. This paper reviews studies regarding various applications of in situ electrochemical-synchrotron radiation such as crystallographic transformation, oxidation-state changes, characterization of the solid electrolyte interphase and Li-dendrite growth mechanism during the intercalation/de-intercalation process. The paper also presents the findings of previous review articles and the future direction of these methods.

  18. Current advances in synchrotron radiation instrumentation for MX experiments

    Energy Technology Data Exchange (ETDEWEB)

    Owen, Robin L.; Juanhuix, Jordi; Fuchs, Martin

    2016-07-01

    Following pioneering work 40 years ago, synchrotron beamlines dedicated to macromolecular crystallography (MX) have improved in almost every aspect as instrumentation has evolved. Beam sizes and crystal dimensions are now on the single micron scale while data can be collected from proteins with molecular weights over 10 MDa and from crystals with unit cell dimensions over 1000 Å. Furthermore it is possible to collect a complete data set in seconds, and obtain the resulting structure in minutes. The impact of MX synchrotron beamlines and their evolution is reflected in their scientific output, and MX is now the method of choice for a variety of aims from ligand binding to structure determination of membrane proteins, viruses and ribosomes, resulting in a much deeper understanding of the machinery of life. A main driving force of beamline evolution have been advances in almost every aspect of the instrumentation comprising a synchrotron beamline. In this review we aim to provide an overview of the current status of instrumentation at modern MX experiments. The most critical optical components are discussed, as are aspects of endstation design, sample delivery, visualisation and positioning, the sample environment, beam shaping, detectors and data acquisition and processing.

  19. The VITROVAC Cavity for the TERA/PIMMS Medical Synchrotron

    CERN Document Server

    Crescenti, M; Primadei, G; Etzkorn, F J; Schnase, A; Fougeron, C

    2000-01-01

    A proton and light-ion medical synchrotron is characterised by a large frequency swing for the RF between the injection and the top energy. For this purpose, a VITROVAC®-loaded RF cavity has been developed for the Proton-Ion Medical Machine Study (PIMMS) at CERN, and for TERA, the Italian project of a proton and light-ion synchrotron for cancer therapy, based on the PIMMS study. The main features are a large frequency swing, particularly extended to the low frequency range, a very large relative permeability and a low Q factor. The total power needed is less than 100 kW, while a very small bias power is required for the frequency tuning. The main mechanical characteristics are compactness (less than 1.5 m), and simplicity of construction. As a result, the requirements of the medical synchrotron are comfortably satisfied, namely: 0.4 to 3 MHz swing, 3 kV peak voltage at a repetition rate of less than 1 s.

  20. A water-cooled mirror system for synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    DiGennaro, R.; Gee, B.; Guigli, J.; Hogrefe, H.; Howells, M.; Rarback, H.

    1987-06-01

    This paper describes the design and performance of a directly-cooled soft x-ray mirror system which has been developed at Lawrence Berkeley Laboratory for synchrotron radiation beam lines in which mirror thermal distortion must be minimized for acceptable optical performance. Two similar mirror systems are being built: the first mirror has been installed and operated at the National Synchrotron Light Source on the X-17T mini-undulator beam line and will be moved to the permanent X-1 beam line when a new, more powerful undulator is installed there. The second system is being built for installation at the Stanford Synchrotron Radiation Laboratory on Beam Line VI, where the total absorbed power on the mirror may be as high as 2400 W with peak absorbed power density of 520 W/cm/sup 2/. Direct cooling by convection is achieved using internal water channels in a brazed, dispersion-strengthened copper and OFHC copper substrate with a polished electroless-nickel surface. A simple kinematic linkage and flexural pivot mounting provide for mirror positioning about two rotational axes that coincide with the optical surface. Surface figure metrology, optical configurations, and tolerancing are also discussed. 11 refs., 8 figs.

  1. Brazilian Studies Then and Now

    Directory of Open Access Journals (Sweden)

    Anthony Pereira

    2012-09-01

    Full Text Available In 1912 the Brazilian diplomat and scholar Manuel de Oliveira Lima gave six lectures at Stanford University that encapsulated his views of what we now call Brazilian Studies. This article summarizes Oliveira Lima’s lectures. It then points out three aspects of Oliveira Lima’s worldview that are problematic from the perspective of the twenty-first century: his Eurocentrism; the unproblematic nature of the nation-state in his thinking; and his largely negative view of Brazil’s racial heritage. The third part of the essay analyzes three aspects of Oliveira Lima’s lectures that are still contemporary. These are the need to establish an adequate comparative context for the study of Brazil; the difficulty of justifying an academic discipline that revolves around the study of a single country; and the challenge of uniting disparate and specialized disciplines in order to appreciate Brazil’s complexity and trajectory in the modern world. In the conclusion, some guidelines for maintaining Brazilian Studies as a vibrant field are suggested.

  2. Monitoring environmental pollution of trace elements in tree-rings by synchrotron radiation total reflection X-ray fluorescence analysis (SR-TXRF)

    Energy Technology Data Exchange (ETDEWEB)

    Moreira, Silvana [Universidade Estadual de Campinas, SP (Brazil). Faculdade de Engenharia Civil, Arquitetura e Urbanismo]. E-mail: Silvana@fec.unicamp.br; Vives, Ana Elisa S. de [Universidade Metodista de Piracicaba (UNIMEP), Santa Barbara D' Oeste, SP (Brazil). Faculdade de Engenharia, Arquitetura e Urbanismo]. E-mail: aesvives@unimep.br; Brienza, Sandra Maria B. [Universidade Metodista de Piracicaba (UNIMEP), Santa Barbara D' Oeste, SP (Brazil) Faculdade de Ciencias Matematicas, da Natureza e de Tecnologia da Informacao]. E-mail: sbrienza@unimep.br; Medeiros, Jean Gabriel S.; Tomazello Filho, Mario [Sao Paulo Univ., Piracicaba, SP (Brazil). Escola Superior de Agricultura Luiz de Queiroz]. E-mail: jeangm@esalq.usp.br; mtomazel@esalq.usp.br; Zucchi, Orgheda L.A.D. [Sao Paulo Univ., Ribeirao Preto, SP (Brazil). Faculdade de Ciencias Farmaceuticas]. E-mail: olzucchi@fcfrp.usp.br; Nascimento Filho, Virgilio F. [Centro de Energia Nuclear na Agricultura (CENA), Piracicaba, SP (Brazil). Lab. de Instrumentacao Nuclear]. E-mail: virgilio@cena.usp.br

    2005-07-01

    This paper aims to study the environmental pollution in the tree development, as a manner to evaluate its use as bioindicator in urban and country sides. The sample collecting was carry out in Piracicaba city, Sao Paulo State, that presents high level of environmental contamination of the water, soil and air, due industrial activities, vehicles combustion, sugar-cane leaves burning in the harvesting, etc. It was selected the Caesalpinia peltophoroides ('Sibipiruna') specie because its very used in urban arborization. It was employed the analytical technique named total reflection X-ray fluorescence (TXRF) to identify and quantify the elements and metals of nutritional and toxicological importance in the wood samples. The analysis was done in the Brazilian Synchrotron Light Laboratory, using a white beam for excitation and a Si(Li) detector for characteristic X-ray detection. It was quantified the P, K, Ca, Ti, Fe, Sr, Ba e Pb elements. (author)

  3. Numerical calculation of beam coupling impedances in synchrotron accelerators

    Energy Technology Data Exchange (ETDEWEB)

    Haenichen, Lukas

    2016-07-01

    Beams of charged particles are of interest in various fields of research including particle and nuclear physics, material and medical science and many more. In synchrotron accelerators the accelerating section is passed periodically. A closed loop trajectory is enforced, by increasing the frequency of the accelerating electric field and the magnitude of the dipolar magnetic guide field synchronously. A synchrotron therefore consists of a circular assembly of various beamline elements which serve the purposes of accelerating and guiding the particle beam. For the flawless operation of such a machine it has to be assured that the particles perform a controlled motion along predefined trajectories. Amongst others, the fulfillment of the corresponding stability criteria is in close conjuction with the so-called beam coupling impedances which are an important figure of merit for collective effects in synchrotron accelerators. This work focuses on analytical and numerical methods for the calculation of beam coupling impedances. One of the primary objectives is to gain a better understanding of the electrodynamics related to charged particle beams, furthermore to recapitulate the mathematical description of charged particle beams in both time and frequency domain and finally establish the links between actual physics and numerical modeling. Analytical methods are usually restricted to symmetrical geometry and may solely serve for the approximate determination of the field distribution in real geometries or to validate certain numerical methods. More accurate prognosis is only possible with three-dimensional simulation models. Numerical simulation techniques have been established in the second half of the last century accompanying the evolution of many particle accelerators. Classical time domain codes were the prevailing simulation tools where the actual process of the particle motion sequence is reproduced. For the present case of a heavy ion synchrotron accelerator

  4. Medical physics aspects of the synchrotron radiation therapies: Microbeam radiation therapy (MRT) and synchrotron stereotactic radiotherapy (SSRT).

    Science.gov (United States)

    Bräuer-Krisch, Elke; Adam, Jean-Francois; Alagoz, Enver; Bartzsch, Stefan; Crosbie, Jeff; DeWagter, Carlos; Dipuglia, Andrew; Donzelli, Mattia; Doran, Simon; Fournier, Pauline; Kalef-Ezra, John; Kock, Angela; Lerch, Michael; McErlean, Ciara; Oelfke, Uwe; Olko, Pawel; Petasecca, Marco; Povoli, Marco; Rosenfeld, Anatoly; Siegbahn, Erik A; Sporea, Dan; Stugu, Bjarne

    2015-09-01

    Stereotactic Synchrotron Radiotherapy (SSRT) and Microbeam Radiation Therapy (MRT) are both novel approaches to treat brain tumor and potentially other tumors using synchrotron radiation. Although the techniques differ by their principles, SSRT and MRT share certain common aspects with the possibility of combining their advantages in the future. For MRT, the technique uses highly collimated, quasi-parallel arrays of X-ray microbeams between 50 and 600 keV. Important features of highly brilliant Synchrotron sources are a very small beam divergence and an extremely high dose rate. The minimal beam divergence allows the insertion of so called Multi Slit Collimators (MSC) to produce spatially fractionated beams of typically ∼25-75 micron-wide microplanar beams separated by wider (100-400 microns center-to-center(ctc)) spaces with a very sharp penumbra. Peak entrance doses of several hundreds of Gy are extremely well tolerated by normal tissues and at the same time provide a higher therapeutic index for various tumor models in rodents. The hypothesis of a selective radio-vulnerability of the tumor vasculature versus normal blood vessels by MRT was recently more solidified. SSRT (Synchrotron Stereotactic Radiotherapy) is based on a local drug uptake of high-Z elements in tumors followed by stereotactic irradiation with 80 keV photons to enhance the dose deposition only within the tumor. With SSRT already in its clinical trial stage at the ESRF, most medical physics problems are already solved and the implemented solutions are briefly described, while the medical physics aspects in MRT will be discussed in more detail in this paper. Copyright © 2015. Published by Elsevier Ltd.

  5. Brief historical aspects of the synchrotron radiation development in France; Bref historique du developpement du rayonnement synchrotron en France

    Energy Technology Data Exchange (ETDEWEB)

    Farge, Y. [Academie des Technologies, Grand Palais des Champs elysees, Porte C, Avenue Franklin D. Roosevelt, F-75008 Paris (France)

    2011-07-01

    France has played a major role in the development of synchrotron radiation. In 1971, a group of physicists and photo-chemists have created the LURE laboratory in Orsay (France) to exploit the radiation emitted by a small storage ring (ACO). In this ring, the radiation was emitted in curvature segments which gave to electrons a circular trajectory and a centripetal acceleration. Rapidly, the electrons have been submitted to others forms of acceleration. The source brilliancy has been improved to. In 1986 has been built the ESRF in Grenoble. For 2007, SOLEIL, a third generation synchrotron runs. It covers simultaneously the hard and soft X radiations and the early ultraviolet. The uses of the synchrotron radiation are extremely large and use all the photons interaction properties with matter: absorption, fluorescence, elastic scattering, inelastic scattering, photo-emissions...These techniques cover wide scientific domains as atomic physics, photochemistry, surfaces studies, high resolution imagery in the X-rays field or acute chemical analyses. (O.M.)

  6. Elemental concentration analysis in brain of young, adult and old wistar rats by X-ray total reflection fluorescence with synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Serpa, Renata F.B.; Jesus, Edgar F.O. de; Lopes, Ricardo T. [Universidade Federal, Rio de Janeiro, RJ (Brazil). Coordenacao dos Programas de Pos-graduacao de Engenharia. Lab. de Instrumentacao Nuclear]. E-mail: renata@lin.ufrj.br; Anjos, Marcelino J. dos [Universidade do Estado, Rio de Janeiro, RJ (Brazil). Inst. de Fisica]. E-mail: marcelin@lin.ufrj.br; Carmo, Maria da Graca T. do [Universidade Federal, Rio de Janeiro, RJ (Brazil). Inst. de Nutricao]. E-mail: tcarmo@editema.com.br; Rocha, Monica S. [Universidade Federal, Rio de Janeiro, RJ (Brazil). Dept. de Farmacologia]. E-mail: mrocha@farmaco.ufrj.br; Moreira, Silvana [Universidade Estadual de Campinas, SP (Brazil). Faculdade de Engenharia Civil]. E-mail: silvana@fec.unicamp.br; Martinez, Ana Maria B. [Universidade Federal, Rio de Janeiro, RJ (Brazil). Dept. de Histologia]. E-mail: martinez@histo.ufrj.br

    2005-07-01

    The mainly goal of this work is to compare the elemental concentrations with different postnatal ages (2, 8, 20, 48 and 72 weeks) at three different regions of the rat brain, namely temporal cortex, entorhinal cortex and hippocampus by X-Ray Total Reflection Fluorescence with Synchrotron Radiation (SR-TXRF). The advantages for this analytical multielemental technique are: low background, linear relation in the quantification analysis and low detection limit (ngg{sup -1}). The fluorescence measurements were carried out at XRF beamline at the Brazilian Light Synchrotron Laboratory (Campinas, Brazil). It was possible to determine the following elements: Ti, Mn, Fe, Cu, Zn, Br, Rb and Sr (at trace level) and P, S, Cl, K and Ca (at major levels) were determined in the brain. In general, Fe levels were more pronounced in entorhinal cortex. There was also observed that the hippocampus of the old female rat presented the highest concentrations for Al, P, S, K, and Zn. In contrast to this, the hippocampus and entorhinal cortex presented the less levels for Al and K in the young animals. On the other hand, Cl levels were more conspicuous in the entorhinal cortex of the oldest male animal studied. (author)

  7. Monitoring of the environmental pollution by trace element analysis in tree-rings using synchrotron radiation total reflection X-ray fluorescence

    Energy Technology Data Exchange (ETDEWEB)

    Sirito de Vives, Ana Elisa [School of Civil Engineering, Architecture and Urban Design Methodist University of Piracicaba, Rodovia Santa Barbara D' Oeste/Iracemapolis, km 01, 13450-000 Santa Barbara D' Oeste, SP (Brazil)]. E-mail: aesvives@unimep.br; Moreira, Silvana [State University of Campinas - UNICAMP/FEC (Brazil); Brienza, Sandra Maria Boscolo [School of Civil Engineering, Architecture and Urban Design Methodist University of Piracicaba, Rodovia Santa Barbara D' Oeste/Iracemapolis, km 01, 13450-000 Santa Barbara D' Oeste, SP (Brazil); Silva Medeiros, Jean Gabriel [University of Sao Paulo - USP/ ESALQ (Brazil); Tomazello Filho, Mario Tomazello [University of Sao Paulo - USP/ ESALQ (Brazil); Araujo Domingues Zucchi, Orgheda Luiza [University of Sao Paulo - USP/FCFRP (Brazil); Nascimento Filho, Virgilio Franco do [University of Sao Paulo - USP/CENA (Brazil)

    2006-11-15

    This paper aims to study the environmental pollution in the tree development, in order to evaluate its use as bioindicator in urban and country sides. The sample collection was carried out in Piracicaba city, Sao Paulo State, which presents high level of environmental contamination in water, soil and air, due to industrial activities, vehicles combustion, sugar-cane leaves burning in the harvesting, etc. The species Caesalpinia peltophoroides ('Sibipiruna') was selected because it is widely used in urban forestation. Synchrotron Radiation Total Reflection X-ray Fluorescence technique (SR-TXRF) was employed to identify and quantify the elements and metals of nutritional and toxicological importance in the wood samples. The analysis was performed in the Brazilian Synchrotron Light Source Laboratory, using a white beam for excitation and a Si(Li) detector for X-ray detection. In several samples, P, K, Ca, Ti, Fe, Sr, Ba and Pb were quantified. The K/Ca, K/P and Pb/Ca ratios were found to decrease towards the bark.

  8. Elemental changes in hemolymph and urine of Rhodnius prolixus induced by in-vivo exposure to mercury: A study using synchrotron radiation total reflection X-ray fluorescence

    Science.gov (United States)

    Mantuano, Andrea; Pickler, Arissa; Barroso, Regina C.; de Almeida, André P.; Braz, Delson; Cardoso, Simone C.; Gonzalez, Marcelo S.; Figueiredo, Marcela B.; Garcia, Eloi S.; Azambuja, Patricia

    2012-05-01

    In recent years, the effects of pollution on the health of humans and other vertebrates were extensively studied. However, the effects on some invertebrates are comparatively unknown. Recent studies have demonstrated that toxic metals interfere with the reproduction, development and immune defenses of some terrestrial and marine invertebrates. Some environmental conditions including pollution produce chronic and acute effects on different animal's organs and systems. In this work, we investigated changes in the concentrations of Cl, K, Ca, Fe and Zn in Rhodnius prolixus as insect model. The elements were quantified using urine and hemolymph samples collected on different days after feeding the insects with blood containing HgCl2. The synchrotron radiation total reflection X-ray fluorescence measurements were carried at the X-ray fluorescence beamline facility in Brazilian Synchrotron Light Laboratory. The observation reveals that the calcium level was higher in the hemolymph than in urine. On the other hand, the urine collected from insects treated with HgCl2 showed higher level of Cl than hemolymph samples. Ca, Fe and Zn concentrations decrease drastically in urine samples collected after 2 days of HgCl2 treatment. The regulation of triatomines excretion was discussed pointing out the importance of trace elements.

  9. 36th Brazilian Workshop on Nuclear Physics

    CERN Document Server

    Brandão de Oliveira, José Roberto; Barbosa Shorto, Julian Marco; Higa, Renato

    2014-01-01

    The Brazilian Workshop on Nuclear Physics (RTFNB, acronym in Portuguese) is organized annually by the Brazilian Physics Society since 1978, in order to: promote Nuclear Physics research in the country; stimulate and reinforce collaborations among nuclear physicists from around the country; disseminate advances in nuclear physics research and its applications; disseminate, disclose and evaluate the scientific production in this field.

  10. The new Brazilian national forest inventory

    Science.gov (United States)

    Joberto V. de Freitas; Yeda M. M. de Oliveira; Doadi A. Brena; Guilherme L.A. Gomide; Jose Arimatea Silva; < i> et al< /i>

    2009-01-01

    The new Brazilian national forest inventory (NFI) is being planned to be carried out through five components: (1) general coordination, led by the Brazilian Forest Service; (2) vegetation mapping, which will serve as the basis for sample plot location; (3) field data collection; (4) landscape data collection of 10 x 10-km sample plots, based on high-resolution...

  11. Brazilian Studies and Brazilianists: Conceptual remarks

    Directory of Open Access Journals (Sweden)

    Vinicius Mariano de Carvalho

    2017-01-01

    Full Text Available This article discusses the concept of Brazilian Studies. It does not intend to outline a defence for a new discipline, or to propose paradigms for that elusive field called ‘area studies’. It will, bring some reflections on epistemological and methodological issues realted to what it is been called Brazilian Studies.

  12. Types and myths in Brazilian thought

    Directory of Open Access Journals (Sweden)

    Octavio Ianni

    2005-01-01

    Full Text Available "Ideal types" elaborated by different authors and that have become emblematic, notorious or even definitive, sometimes representing myths are quite frequent in Brazilian thought. That is the case of the bandeirantes (colonial crusaders, the gaúcho, Jeca Tatu, Macunaíma, cordial man and others. It is worth contemplating this aspect of Brazilian culture and thought.

  13. Sociocultural Influences on Brazilian Children's Drawings.

    Science.gov (United States)

    Stokrocki, Mary

    2000-01-01

    Reports on insights about sociocultural influences on Brazilian children's drawings, using visual anthropology to examine children's drawings that depicted what they like to do. Discusses visual anthropology, provides information on Brazilian educational influences, and presents the context and findings of the study. (CMK)

  14. Elementary education in brazilian legislation

    OpenAIRE

    Veronese, Josiane Rose Petry; Vieira, Cleverton Elias

    2003-01-01

    The education was a present subject, directly or indirectly, in every Brazilian Constitutions. In the Federal Constitution of 1988, two aspects about education can be detached: the participation of the civil society in the elaboration of devices that regulate the national education and the treatment given to basic education, raised to the category of subjective public right. Child and Adolescent Statute practically repeats the devices of the&n...

  15. Quantitative X-ray microtomography with synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Donath, T. [GKSS-Forschungszentrum Geesthacht GmbH (Germany). Inst. fuer Materialforschung

    2007-07-01

    Synchrotron-radiation-based computed microtomography (SR{sub {mu}}CT) is an established method for the examination of volume structures. It allows to measure the x-ray attenuation coefficient of a specimen three-dimensionally with a spatial resolution of about one micrometer. In contrast to conventional x-ray sources (x-ray tubes), the unique properties of synchrotron radiation enable quantitative measurements that do not suffer from beam-hardening artifacts. During this work the capabilities for quantitative SR{sub {mu}}CT measurements have been further improved by enhancements that were made to the SR{sub {mu}}CT apparatus and to the reconstruction chain. For high-resolution SR{sub {mu}}CT an x-ray camera consisting of luminescent screen (x-ray phosphor), lens system, and CCD camera was used. A significant suppression of blur that is caused by reflections inside the luminescent screen could be achieved by application of an absorbing optical coating to the screen surface. It is shown that blur and ring artifacts in the tomographic reconstructions are thereby drastically reduced. Furthermore, a robust and objective method for the determination of the center of rotation in projection data (sinograms) is presented that achieves sub-pixel precision. By implementation of this method into the reconstruction chain, complete automation of the reconstruction process has been achieved. Examples of quantitative SR{sub {mu}}CT studies conducted at the Hamburger Synchrotronstrahlungslabor HASYLAB at the Deutsches Elektronen-Synchrotron DESY are presented and used for the demonstration of the achieved enhancements. (orig.)

  16. Finite element analysis of osteoporosis models based on synchrotron radiation

    Science.gov (United States)

    Xu, W.; Xu, J.; Zhao, J.; Sun, J.

    2016-04-01

    With growing pressure of social aging, China has to face the increasing population of osteoporosis patients as well as the whole world. Recently synchrotron radiation has become an essential tool for biomedical exploration with advantage of high resolution and high stability. In order to study characteristic changes in different stages of primary osteoporosis, this research focused on the different periods of osteoporosis of rats based on synchrotron radiation. Both bone histomorphometry analysis and finite element analysis were then carried on according to the reconstructed three dimensional models. Finally, the changes of bone tissue in different periods were compared quantitatively. Histomorphometry analysis showed that the structure of the trabecular in osteoporosis degraded as the bone volume decreased. For femurs, the bone volume fraction (Bone volume/ Total volume, BV/TV) decreased from 69% to 43%. That led to the increase of the thickness of trabecular separation (from 45.05μ m to 97.09μ m) and the reduction of the number of trabecular (from 7.99 mm-1 to 5.97mm-1). Simulation of various mechanical tests with finite element analysis (FEA) indicated that, with the exacerbation of osteoporosis, the bones' ability of resistance to compression, bending and torsion gradually became weaker. The compression stiffness of femurs decreased from 1770.96 Fμ m-1 to 697.41 Fμ m-1, the bending and torsion stiffness were from 1390.80 Fμ m-1 to 566.11 Fμ m-1 and from 2957.28N.m/o to 691.31 N.m/o respectively, indicated the decrease of bone strength, and it matched the histomorphometry analysis. This study suggested that FEA and synchrotron radiation were excellent methods for analysing bone strength conbined with histomorphometry analysis.

  17. High resolution 3D imaging of synchrotron generated microbeams

    Energy Technology Data Exchange (ETDEWEB)

    Gagliardi, Frank M., E-mail: frank.gagliardi@wbrc.org.au [Alfred Health Radiation Oncology, The Alfred, Melbourne, Victoria 3004, Australia and School of Medical Sciences, RMIT University, Bundoora, Victoria 3083 (Australia); Cornelius, Iwan [Imaging and Medical Beamline, Australian Synchrotron, Clayton, Victoria 3168, Australia and Centre for Medical Radiation Physics, University of Wollongong, Wollongong, New South Wales 2500 (Australia); Blencowe, Anton [Division of Health Sciences, School of Pharmacy and Medical Sciences, The University of South Australia, Adelaide, South Australia 5000, Australia and Division of Information Technology, Engineering and the Environment, Mawson Institute, University of South Australia, Mawson Lakes, South Australia 5095 (Australia); Franich, Rick D. [School of Applied Sciences and Health Innovations Research Institute, RMIT University, Melbourne, Victoria 3000 (Australia); Geso, Moshi [School of Medical Sciences, RMIT University, Bundoora, Victoria 3083 (Australia)

    2015-12-15

    Purpose: Microbeam radiation therapy (MRT) techniques are under investigation at synchrotrons worldwide. Favourable outcomes from animal and cell culture studies have proven the efficacy of MRT. The aim of MRT researchers currently is to progress to human clinical trials in the near future. The purpose of this study was to demonstrate the high resolution and 3D imaging of synchrotron generated microbeams in PRESAGE® dosimeters using laser fluorescence confocal microscopy. Methods: Water equivalent PRESAGE® dosimeters were fabricated and irradiated with microbeams on the Imaging and Medical Beamline at the Australian Synchrotron. Microbeam arrays comprised of microbeams 25–50 μm wide with 200 or 400 μm peak-to-peak spacing were delivered as single, cross-fire, multidirectional, and interspersed arrays. Imaging of the dosimeters was performed using a NIKON A1 laser fluorescence confocal microscope. Results: The spatial fractionation of the MRT beams was clearly visible in 2D and up to 9 mm in depth. Individual microbeams were easily resolved with the full width at half maximum of microbeams measured on images with resolutions of as low as 0.09 μm/pixel. Profiles obtained demonstrated the change of the peak-to-valley dose ratio for interspersed MRT microbeam arrays and subtle variations in the sample positioning by the sample stage goniometer were measured. Conclusions: Laser fluorescence confocal microscopy of MRT irradiated PRESAGE® dosimeters has been validated in this study as a high resolution imaging tool for the independent spatial and geometrical verification of MRT beam delivery.

  18. Room-temperature macromolecular serial crystallography using synchrotron radiation

    Directory of Open Access Journals (Sweden)

    Francesco Stellato

    2014-07-01

    Full Text Available A new approach for collecting data from many hundreds of thousands of microcrystals using X-ray pulses from a free-electron laser has recently been developed. Referred to as serial crystallography, diffraction patterns are recorded at a constant rate as a suspension of protein crystals flows across the path of an X-ray beam. Events that by chance contain single-crystal diffraction patterns are retained, then indexed and merged to form a three-dimensional set of reflection intensities for structure determination. This approach relies upon several innovations: an intense X-ray beam; a fast detector system; a means to rapidly flow a suspension of crystals across the X-ray beam; and the computational infrastructure to process the large volume of data. Originally conceived for radiation-damage-free measurements with ultrafast X-ray pulses, the same methods can be employed with synchrotron radiation. As in powder diffraction, the averaging of thousands of observations per Bragg peak may improve the ratio of signal to noise of low-dose exposures. Here, it is shown that this paradigm can be implemented for room-temperature data collection using synchrotron radiation and exposure times of less than 3 ms. Using lysozyme microcrystals as a model system, over 40 000 single-crystal diffraction patterns were obtained and merged to produce a structural model that could be refined to 2.1 Å resolution. The resulting electron density is in excellent agreement with that obtained using standard X-ray data collection techniques. With further improvements the method is well suited for even shorter exposures at future and upgraded synchrotron radiation facilities that may deliver beams with 1000 times higher brightness than they currently produce.

  19. Stanford Synchrotron Radiation Laboratory activity report for 1986

    Energy Technology Data Exchange (ETDEWEB)

    Cantwell, K. [ed.

    1987-12-31

    1986 was another year of major advances for SSRL as the ultimate capabilities of PEP as a synchrotron radiation source became more apparent and a second PEP beam line was initiated, while effective development and utilization of SPEAR proceeded. Given these various PEP developments, SSRL abandoned its plans for a separate diffraction limited ring, as they abandoned their plans for a 6--7 GeV ring of the APS type last year. It has become increasingly apparent that SSRL should concentrate on developing SPEAR and PEP as synchrotron radiation sources. Consequently, initial planning for a 3 GeV booster synchrotron injector for SPEAR was performed in 1986, with a proposal to the Department of Energy resulting. As described in Chapter 2, the New Rings Group and the Machine Physics Group were combined into one Accelerator Physics Group. This group is focusing mainly on the improvement of SPEAR`s operating conditions and on planning for the conversion of PEP into a fourth generation x-ray source. Considerable emphasis is also being given to the training of accelerator physics graduate students. At the same time, several improvements of SSRL`s existing facilities were made. These are described in Chapter 3. Chapter 4 describes new SSRL beam lines being commissioned. Chapter 5 discusses SSRL`s present construction projects. Chapter 6 discusses a number of projects presently underway in the engineering division. Chapter 7 describes SSRL`s advisory panels while Chapter 8 discusses SSRL`s overall organization. Chapter 9 describes the experimental progress reports.

  20. Hiroshima Synchrotron Radiation Center - An outline and scientific activities

    CERN Document Server

    Taniguchi, M

    2003-01-01

    High energy-resolution and low-temperature photoemission spectroscopies (DELTA E=4.5-20 meV and T=6-300 K) have been started on undulator beamlines at Hiroshima Synchrotron Radiation Center with a compact light source. Beamlines for high energy-resolution photoemission spectroscopy and their application to direct observation of pseudogap formation in Kondo systems (CeRhAs, CeRhSb, CePtSn and CeNiSn, LaNiSn) are presented.

  1. Calculation of the characteristics of infrared synchrotron radiation

    CERN Document Server

    Maslova, M V; Maltsev, M A

    2005-01-01

    Subroutines for calculating the spectral and angular characteristics of infrared synchrotron radiation are developed. Corresponding calculations are carried out for a number of proton and electron accelerators. The results obtained enable methods to be developed for beam diagnostics as well as highly sensitive detectors of infrared radiation for remote contactless nondestructive diagnostics and for investigating bunches and high-speed processes in ring-type (CERN /SEPS-LHC) and linear (GSI bunch target) accelerators, and also the thermal fields in nuclear power plants.

  2. Synchrotron radiation backgrounds for the FCC-hh experiments

    Science.gov (United States)

    Collamati, F.; Boscolo, M.; Burkhardt, H.; Kersevan, R.

    2017-07-01

    In this paper we present a detailed analysis of the Synchrotron Radiation emitted by the 50 TeV protons of the FCC-hh in the last bending and quadrupole magnets upstream of the interaction region. We discuss the characteristics of this radiation in terms of power, flux, photon spectrum and fans with and without crossing angle for comparison. We mainly focus our study on the fraction of photons that may hit the detector, with a full tracking in GEANT4 that simulates the interaction within the central beam pipe.

  3. Synchrotron-Radiation Photon Distributions for Highest Energy Circular Colliders

    CERN Document Server

    Maury Cuna, G H I; Dugan, G; Zimmermann, F

    2013-01-01

    At high energies, beam-induced synchrotron radiation is an important source of heating, beam-related vacuum pressure increase, and primary photoelectrons, which can give rise to an electron cloud. The photon distribution along the beam pipe wall is a key input to codes such as ECLOUD and PyECLOUD, which model the electron cloud build-up. For future high-energy colliders, like TLEP or SHE-LHC, photon stops and antechambers are considered in order to facilitate cooling and vacuum pressure control. We use the Synrad3D code developed at Cornell to simulate the photon distribution for the LHC.

  4. Synchrotron-Radiation Photon Distribution for Highest Energy Circular Colliders

    CERN Document Server

    Maury Cuna, GHI; Dugan, G; Zimmermann, F

    2013-01-01

    At high energies, beam-induced synchrotron radiation is an important source of heating, beam-related vacuum pressure increase, and primary photoelectrons, which can give rise to an electron cloud. The photon distribution along the beam pipe wall is a key input to codes such as ECLOUD and PyECLOUD, which model the electron cloud build-up. For future high-energy colliders, like TLEP or SHE-LHC, photon stops and antechambers are considered in order to facilitate cooling and vacuum pressure control. We use the Synrad3D code developed at Cornell to simulate the photon distribution for the LHC.

  5. Measurement of parameters in Indus-2 synchrotron radiation source.

    Science.gov (United States)

    Ghodke, A D; Husain, Riyasat; Kumar, Pradeep; Yadav, Surendra; Puntambekar, T A

    2012-10-01

    The paper presents the measurement of optics parameters in Indus-2 synchrotron radiation source, which include betatron tune, beta function, dispersion function, natural chromaticity, corrected chromaticity, central RF frequency, momentum compaction factor, and linear betatron coupling. Two methods were used for beta function measurement; a conventional quadrupole scan method and a method using the fitting of the orbit response matrix. A robust Levenberg-Marquardt algorithm was used for nonlinear least square fitting of the orbit response matrix. In this paper, detailed methods for the parameter measurements are described. The measured results are discussed and compared with the theoretical values obtained using accelerator simulation code Accelerator Toolbox in MATLAB.

  6. SYNCHROTRON X-RAY BASED CHARACTERIZATION OF CDZNTE CRYSTALS

    Energy Technology Data Exchange (ETDEWEB)

    Duff, M

    2006-09-28

    Synthetic CdZnTe or 'CZT' crystals can be used for the room temperature-based detection of {gamma}-radiation. Structural/morphological heterogeneities within CZT, such as twinning, inclusions, and polycrystallinity can affect detector performance. We used a synchrotron-based X-ray technique, specifically extended X-ray absorption fine-structure (EXAFS) spectroscopy, to determine whether there are differences on a local structural level between intact CZT of high and low radiation detector performance. These studies were complemented by data on radiation detector performance and transmission IR imaging. The EXAFS studies revealed no detectable local structural differences between the two types of CZT materials.

  7. A Tool for Longitudinal Beam Dynamics in Synchrotrons

    Energy Technology Data Exchange (ETDEWEB)

    Ostiguy, J.-F. [Fermilab; Lebedev, V. A. [Fermilab

    2017-05-01

    A number of codes are available to simulate longitudinal dynamics in synchrotrons. Some established ones include TIBETAN, LONG1D, ESME and ORBIT. While they embody a wealth of accumulated wisdom and experience, most of these codes were written decades ago and to some extent they reflect the constraints of their time. As a result, there is an interest for updated tools taking better advantage of modern software and hardware capabilities. At Fermilab, the PIP-II project has provided the impetus for development of such a tool. In this contribution, we discuss design decisions and code architecture. A selection of test cases based on an initial prototype are also presented.

  8. Current schemes for National Synchrotron Light Source UV beamlines

    Energy Technology Data Exchange (ETDEWEB)

    Williams, G.P.; Howells, M.R.; McKinney, W.R.

    1979-01-01

    We describe in some detail four beamlines proposed for the National Synchrotron Light Source uv ring at Brookhaven National Laboratory. Three grazing-incidence instruments, one of the plane grating Mijake type and two with toroidal gratings at grazing angles of 2-1/2/sup 0/ and 15/sup 0/ are described. Two normal incidence instruments, one using the source as entrance slit and accepting 75 milliradians horizontally are also discussed. In each case we have estimated the output fluxes expected from such beamlines.

  9. Oxides neutron and synchrotron X-ray diffraction studies

    CERN Document Server

    Sosnowska, I M

    1999-01-01

    We review some results from several areas of oxide science in which neutron scattering and X-ray synchrotron scattering exercise a complementary role to high-resolution transmission electron microscopy. The very high-resolution time-of-flight neutron diffraction technique and its role in studies of the magnetic structure of oxides is especially reviewed. The selected topics of structural studies for the chosen oxides are: crystal and magnetic structure of the so-called cellular random systems, magnetic structure and phase transitions in ferrites and the behaviour of water in non-stoichiometric protonic conductors and in the opal silica-water system. (40 refs).

  10. Beam Diagnostics for the J-PARC Main Ring Synchrotron

    CERN Document Server

    Toyama, Takeshi; Hashimoto, Yoshinori; Hayashi, Naoki; Kishiro, Junichi; Lee, Seishu; Miura, Takako; Muto, Suguru; Toyokawa, Ryoji

    2005-01-01

    Beam diagnostics: beam intensity monitors (DCCT, SCT, FCT, WCM), beam position monitors (ESM), beam loss monitors (proportional chamber, air ion chamber), beam profile monitors (secondary electron emission, gas-sheet) have been designed, tested, and will be installed for the Main Ring synchrotron of J-PARC (Japan Proton Accelerator Research Complex). This paper describes the basic design principle and specification of each monitor, with a stress on how to cope with high power beam (average circulation current of ~12 A) and low beam loss operation (less than 1 W/m except a collimator region). Some results of preliminary performance test using present beams and a radiation source will be reported.

  11. L-shell radiative transition rates by selective synchrotron ionization

    Energy Technology Data Exchange (ETDEWEB)

    Bonetto, R D [Centro de Investigacion y Desarrollo en Ciencias Aplicadas Dr. Jorge J. Ronco, CONICET-UNLP, Calle 47 No. 257-Cc 59 (1900) La Plata (Argentina); Carreras, A C [Facultad de Matematica, AstronomIa y FIsica, Universidad Nacional de Cordoba, Ciudad Universitaria (5000) Cordoba (Argentina); Trincavelli, J [Facultad de Matematica, AstronomIa y FIsica, Universidad Nacional de Cordoba, Ciudad Universitaria (5000) Cordoba (Argentina); Castellano, G [Facultad de Matematica, AstronomIa y FIsica, Universidad Nacional de Cordoba, Ciudad Universitaria (5000) Cordoba (Argentina)

    2004-04-14

    Relative L-shell radiative transition rates were obtained for a number of decays in Gd, Dy, Er, Yb, Hf, Ta and Re by means of a method for refining atomic and experimental parameters involved in the spectral analysis of x-ray irradiated samples. For this purpose, pure samples were bombarded with monochromatic synchrotron radiation tuning the incident x-ray energy in order to allow selective ionization of the different atomic shells. The results presented are compared to experimental and theoretical values published by other authors. A good general agreement was found and some particular discrepancies are discussed.

  12. Facilities for small-molecule crystallography at synchrotron sources.

    Science.gov (United States)

    Barnett, Sarah A; Nowell, Harriott; Warren, Mark R; Wilcox, Andrian; Allan, David R

    2016-01-01

    Although macromolecular crystallography is a widely supported technique at synchrotron radiation facilities throughout the world, there are, in comparison, only very few beamlines dedicated to small-molecule crystallography. This limited provision is despite the increasing demand for beamtime from the chemical crystallography community and the ever greater overlap between systems that can be classed as either small macromolecules or large small molecules. In this article, a very brief overview of beamlines that support small-molecule single-crystal diffraction techniques will be given along with a more detailed description of beamline I19, a dedicated facility for small-molecule crystallography at Diamond Light Source.

  13. Improvement of injection efficiency of carbon ions for medical synchrotron

    Science.gov (United States)

    Kim, J.; Yoon, M.

    2017-12-01

    This paper describes a systematic study for optimization of the multi-turn injection effciency of carbon-ions for medical synchrotron. This is accomplished by optimizing tunes, bump-magnet parameters, and the number of turns required for injection. For selecting optimal tunes, a frequency map is investigated which reveals various resonances limiting the injection efficiency. The injection bump and the number of turns are optimized by tracking numerous particles up to a few thousand turns after injection. Space-charge effects are considered and found to be non-negligible at the chosen injection energy, 7 MeV/u.

  14. Comparison of postmenopausal endogenous sex hormones among Japanese, Japanese Brazilians, and non-Japanese Brazilians

    Directory of Open Access Journals (Sweden)

    Maciel Maria

    2011-02-01

    Full Text Available Abstract Background Differences in sex hormone levels among populations might contribute to the variation in breast cancer incidence across countries. Previous studies have shown higher breast cancer incidence and mortality among Japanese Brazilians than among Japanese. To clarify the difference in hormone levels among populations, we compared postmenopausal endogenous sex hormone levels among Japanese living in Japan, Japanese Brazilians living in the state of São Paulo, and non-Japanese Brazilians living in the state of São Paulo. Methods A cross-sectional study was conducted using a control group of case-control studies in Nagano, Japan, and São Paulo, Brazil. Participants were postmenopausal women older than 55 years of age who provided blood samples. We measured estradiol, estrone, androstenedione, dehydroepiandrosterone sulfate (DHEAS, testosterone and free testosterone by radioimmunoassay; bioavailable estradiol by the ammonium sulfate precipitation method; and sex hormone-binding globulin (SHBG by immunoradiometric assay. A total of 363 women were included for the present analyses, comprising 185 Japanese, 44 Japanese Brazilians and 134 non-Japanese Brazilians. Results Japanese Brazilians had significantly higher levels of estradiol, bioavailable estradiol, estrone, testosterone and free testosterone levels, and lower SHBG levels, than Japanese. Japanese Brazilians also had significantly higher levels of bioavailable estradiol, estrone and DHEAS and lower levels of SHBG and androstenedione than non-Japanese Brazilians. Levels of estradiol, testosterone and free testosterone, however, did not differ between Japanese Brazilians and non-Japanese Brazilians. These differences were observed even after adjustment for known breast cancer risk factors. We also found an increase in estrogen and androgen levels with increasing body mass index, but no association for most of the other known risk factors. Conclusions We found higher levels of

  15. The phylogeography of African Brazilians.

    Science.gov (United States)

    Gonçalves, Vanessa F; Carvalho, Cláudia M B; Bortolini, Maria Cátira; Bydlowski, Sérgio P; Pena, Sérgio D J

    2008-01-01

    Approximately four million Africans were taken as slaves to Brazil, where they interbred extensively with Amerindians and Europeans. We have previously shown that while most White Brazilians carry Y chromosomes of European origin, they display high proportions of African and Amerindian mtDNA lineages, because of sex-biased genetic admixture. We studied the Y chromosome and mtDNA haplogroup structure of 120 Black males from Sao Paulo, Brazil. Only 48% of the Y chromosomes, but 85% of the mtDNA haplogroups were characteristic of sub-Saharan Africa, confirming our previous observation of sexually biased mating. We mined literature data for mtDNA and Y chromosome haplogroup frequencies for African native populations from regions involved in Atlantic Slave Trade. Principal Components Analysis and Bayesian analysis of population structure revealed no genetic differentiation of Y chromosome marker frequencies between the African regions. However, mtDNA examination unraveled considerable genetic structure, with three clusters at Central-West Africa, West Africa and Southeast Africa. A hypothesis is proposed to explain this structure. Using these mtDNA data we could obtain for the first time an estimate of the relative ancestral contribution of Central-West (0.445), West (0.431) and Southeast Africa (0.123) to African Brazilians from Sao Paulo. These estimates are consistent with historical information. Copyright 2008 S. Karger AG, Basel.

  16. Atmospheric pressure photoionization using tunable VUV synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Giuliani, A., E-mail: alexandre.giuliani@synchrotron-soleil.fr [Synchrotron SOLEIL, L' Orme des Merisiers, Saint Aubin, 91192 Gif-sur-Yvette (France); INRA, U1008 CEPIA, Rue de la Geraudiere, F-44316 Nantes (France); Giorgetta, J.-L.; Ricaud, J.-P. [Synchrotron SOLEIL, L' Orme des Merisiers, Saint Aubin, 91192 Gif-sur-Yvette (France); Jamme, F. [Synchrotron SOLEIL, L' Orme des Merisiers, Saint Aubin, 91192 Gif-sur-Yvette (France); INRA, U1008 CEPIA, Rue de la Geraudiere, F-44316 Nantes (France); Rouam, V.; Wien, F. [Synchrotron SOLEIL, L' Orme des Merisiers, Saint Aubin, 91192 Gif-sur-Yvette (France); Laprevote, O. [Laboratoire de Spectrometrie de Masse, ICSN-CNRS, 1 Avenue de la Terrasse, 91190 Gif-sur-Yvette (France); Laboratoire de Chimie-Toxicologie Analytique et cellulaire, IFR 71, Faculte des Sciences Pharmaceutiques et Biologiques, Universite Paris Descartes, 4 Avenue de l' Observatoire, 75006 Paris (France); Refregiers, M. [Synchrotron SOLEIL, L' Orme des Merisiers, Saint Aubin, 91192 Gif-sur-Yvette (France)

    2012-05-15

    Highlights: Black-Right-Pointing-Pointer Coupling of an atmospheric pressure photoionization source with a vacuum ultra-violet (VUV) beamline. Black-Right-Pointing-Pointer The set up allows photoionization up to 20 eV. Black-Right-Pointing-Pointer Compared to classical atmospheric pressure photoionization (APPI), our set up offers spectral purity and tunability. Black-Right-Pointing-Pointer Allows photoionization mass spectrometry on fragile and hard to vaporize molecules. - Abstract: We report here the first coupling of an atmospheric pressure photoionization (APPI) source with a synchrotron radiation beamline in the vacuum ultra-violet (VUV). A commercial APPI source of a QStar Pulsar i from AB Sciex was modified to receive photons from the DISCO beamline at the SOLEIL synchrotron radiation facility. Photons are delivered at atmospheric pressure in the 4-20 eV range. The advantages of this new set up, termed SR-APPI, over classical APPI are spectral purity and continuous tunability. The technique may also be used to perform tunable photoionization mass spectrometry on fragile compounds difficult to vaporize by classical methods.

  17. Electron cloud observations at the ISIS Proton Synchrotron

    CERN Document Server

    Pertica, A.

    2013-04-22

    The build up of electron clouds inside a particle accelerator vacuum chamber can produce strong transverse and longitudinal beam instabilities which in turn can lead to high levels of beam loss often requiring the accelerator to be run below its design specification. To study the behaviour of electron clouds at the ISIS Proton Synchrotron, a Micro-Channel Plate (MCP) based electron cloud detector has been developed. The detector is based on the Retarding Field Analyser (RFA) design and consists of a retarding grid, which allows energy analysis of the electron signal, and a MCP assembly placed in front of the collector plate. The MCP assembly provides a current gain over the range 300 to 25K, thereby increasing the signal to noise ratio and dynamic range of the measurements. This paper presents the first electron cloud observations at the ISIS Proton Synchrotron. These results are compared against signals from a beam position monitor and a fast beam loss monitor installed at the same location.

  18. Synchrotron radiation in transactinium research report of the workshop

    Energy Technology Data Exchange (ETDEWEB)

    1992-11-01

    This report contains viewgraphs on the following topics. The advanced light source U8 undulator beamline, 20--300 eV; gas-phase actinide studies with synchrotron radiation; atomic structure calculations for heavy atoms; flux growth of single crystal uranium intermetallics: Extension to transuranics; x-ray absorption near-edge structure studies of actinide compounds; surface as a new stage for studying actinides: Theoretical study of the surface electronic structure of uranium; magnetic x-ray scattering experiments at resonant energies; beamline instruments for radioactive materials; the search for x-ray absorption magnetic circular dichroism in actinide materials: preliminary experiments using UFe{sub 2} and U-S; the laser plasma laboratory light source: a source of preliminary transuranic data; electron spectroscopy of heavy fermion actinide materials; study of thin layers of actinides. Present status and future use of synchrotron radiation; electronic structure and correlated-electron theory for actinide materials; and heavy fermion and kondo phenomena in actinide materials.

  19. Synchrotron radiation in transactinium research report of the workshop

    Energy Technology Data Exchange (ETDEWEB)

    1992-11-01

    This report contains viewgraphs on the following topics. The advanced light source U8 undulator beamline, 20--300 eV; gas-phase actinide studies with synchrotron radiation; atomic structure calculations for heavy atoms; flux growth of single crystal uranium intermetallics: Extension to transuranics; x-ray absorption near-edge structure studies of actinide compounds; surface as a new stage for studying actinides: Theoretical study of the surface electronic structure of uranium; magnetic x-ray scattering experiments at resonant energies; beamline instruments for radioactive materials; the search for x-ray absorption magnetic circular dichroism in actinide materials: preliminary experiments using UFe[sub 2] and U-S; the laser plasma laboratory light source: a source of preliminary transuranic data; electron spectroscopy of heavy fermion actinide materials; study of thin layers of actinides. Present status and future use of synchrotron radiation; electronic structure and correlated-electron theory for actinide materials; and heavy fermion and kondo phenomena in actinide materials.

  20. Phase contrast imaging of breast tumours with synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Olivo, A. [Department of Medical Physics and Bioengineering, University College London, Malet Place, Gower Street, London WC1E 6BT (United Kingdom)], E-mail: aolivo@medphys.ucl.ac.uk; Rigon, L. [Istituto Nazionale di Fisica Nucleare, Sezione di Trieste, Area Science Park, Padriciano 99, 34012 Trieste (Italy)], E-mail: rigon@ts.infn.it; Vinnicombe, S.J. [Department of Radiology, St. Bartholomews Hospital, Barts and the London NHS Trust, West Smithfield, London EC1A 7BE (United Kingdom)], E-mail: s.j.vinnicombe@qmul.ac.uk; Cheung, K.C. [STFC Daresbury Laboratory, Keckwick Lane, Warrington, Cheshire WA4 4AD (United Kingdom)], E-mail: k.c.cheung@dl.ac.uk; Ibison, M. [Department of Physics, University of Liverpool, Oxford Street, Liverpool L69 7ZE (United Kingdom)], E-mail: m.ibison@dl.ac.uk; Speller, R.D. [Department of Medical Physics and Bioengineering, University College London, Malet Place, Gower Street, London WC1E 6BT (United Kingdom)], E-mail: rspeller@medphys.ucl.ac.uk

    2009-06-15

    Even though the potential of phase contrast (PC) imaging has been demonstrated in a number of biological tissue samples, the availability of free-space propagation phase contrast images of real breast tumours is still limited. The aim of this study was to obtain phase contrast images of two different pathological breast specimens containing tumours of differing morphological type at two synchrotron radiation (SR) facilities, and to assess any qualitative improvements in the evaluation and characterisation of the masses through the use of phase contrast imaging. A second aim was to assess the effects of parameters such as detector resolution, beam energy and sample-to-detector distance on image quality using the same breast specimens, as to date these effects have been modelled and discussed only for geometric phantoms. At each synchrotron radiation facility a range of images was acquired with different detectors and by varying the above parameters. Images of the same samples were also acquired with the absorption-based approach to allow a direct comparison and estimation of the advantages specifically ascribable to the PC technique.

  1. Measurement of Beam Loss at the Australian Synchrotron

    CERN Document Server

    Holzer, EB; Kastriotou, M; Boland, MJ; Jackson, PD; Rasool, RP; Schmidt, J; Welsch, CP

    2014-01-01

    The unprecedented requirements that new machines are setting on their diagnostic systems is leading to the development of new generation of devices with large dynamic range, sensitivity and time resolution. Beam loss detection is particularly challenging due to the large extension of new facilities that need to be covered with localized detector. Candidates to mitigate this problem consist of systems in which the sensitive part of the radiation detectors can be extended over long distance of beam lines. In this document we study the feasibility of a BLM system based on optical fiber as an active detector for an electron storage ring. The Australian Synchrotron (AS) comprises a 216m ring that stores electrons up to 3GeV. The Accelerator has recently claimed the world record ultra low transverse emittance (below pm rad) and its surroundings are rich in synchrotron radiation. Therefore, the AS provides beam conditions very similar to those expected in the CLIC/ILC damping rings. A qualitative benchmark of beam l...

  2. Optical synchrotron radiation beam imaging with a digital mask

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, Hao [Univ. of Maryland, College Park, MD (United States); Fiorito, Ralph [Univ. of Maryland, College Park, MD (United States); Corbett, Jeff [SLAC National Accelerator Lab., Menlo Park, CA (United States); Shkvarunets, Anatoly [Univ. of Maryland, College Park, MD (United States); Tian, Kai [SLAC National Accelerator Lab., Menlo Park, CA (United States); Fisher, Alan [SLAC National Accelerator Lab., Menlo Park, CA (United States); Douglas, D. [Thomas Jefferson National Accelerator Facility (TJNAF), Newport News, VA (United States); Wilson, F. [Thomas Jefferson National Accelerator Facility (TJNAF), Newport News, VA (United States); Zhang, S. [Thomas Jefferson National Accelerator Facility (TJNAF), Newport News, VA (United States); Mok, W. [SLAC National Accelerator Lab., Menlo Park, CA (United States); Mitsuhashi, T. [KEK, Tsukuba (Japan)

    2016-01-01

    The 3GeV SPEAR3 synchrotron light source operates in top-up injection mode with up to 500mA circulating in the storage ring (equivalently 392nC). Each injection pulse contains only 40-80 pC producing a contrast ratio between total stored charge and injected charge of about 6500:1. In order to study transient injected beam dynamics during User operations, it is desirable to optically image the injected pulse in the presence of the bright stored beam. In the present work this is done by re-imaging visible synchrotron radiation onto a digital micro-mirror-array device (DMD), which is then used as an optical mask to block out light from the bright central core of the stored beam. The physical masking, together with an asynchronously-gated, ICCD imaging camera makes it is possible to observe the weak injected beam component on a turn-by-turn basis. The DMD optical masking system works similar to a classical solar coronagraph but has some distinct practical advantages: i.e. rapid adaption to changes in the shape of the stored beam, high extinction ratio for unwanted light and minimum scattering from the primary beam into the secondary optics. In this paper we describe the DMD masking method, features of the high dynamic range point spread function for the SPEAR3 optical beam line and measurements of the injected beam in the presence of the stored beam.

  3. Dark Matter and Synchrotron Emission from Galactic Center Radio Filaments

    Energy Technology Data Exchange (ETDEWEB)

    Linden, Tim [Univ. of California, Santa Cruz, CA (United States); Hooper, Dan [Fermi National Accelerator Laboratory (FNAL), Batavia, IL (United States); Yusef-Zadeh, Farhad [Northwestern Univ., Evanston, IL (United States)

    2011-11-10

    The inner degrees of the Galactic center contain a large population of filamentary structures observed at radio frequencies. These so-called non-thermal radio filaments (NRFs) trace magnetic field lines and have attracted significant interest due to their hard (S_v ~ -0.1 +/- 0.4) synchrotron emission spectra. The origin of these filaments remains poorly understood. We show that the electrons and positrons created through the annihilations of a relatively light (~5-10 GeV) dark matter particle with the cross section predicted for a simple thermal relic can provide a compelling match to the intensity, spectral shape, and flux variation of the NRFs. Furthermore, the characteristics of the dark matter particle necessary to explain the synchrotron emission from the NRFs is consistent with those required to explain the excess gamma-ray emission observed from the Galactic center by the Fermi-LAT, as well as the direct detection signals observed by CoGeNT and DAMA/LIBRA.

  4. Synchrotron Radiation From Plasmas with Sub-Relativistic Temperatures

    Science.gov (United States)

    Necas, Ales; Putvinski, Sergei; Ryutov, Dmitri; Yushmanov, Peter; TAE Team

    2017-10-01

    A simple expression for power radiated by synchrotron radiation from plasmas with electron temperatures between 50 - 200 keV is developed. We shall start by re-deriving a general expression for power radiated in vacuum from an individual cyclotron harmonic. Adding up power radiated from individual harmonics shows an asymptotic approach to the power radiated from all harmonics. In a case of Te =50 keV, summing the first 10 harmonics well represents radiation from all harmonics. However, for Te =150 keV, we require to sum over 60 harmonics to adequately represent the total radiation. This is computationally demanding. What follows is a derivation of a simple expression for high harmonic power radiation in vacuum. It is of interested that this expression proofs to be reasonable even for low harmonic numbers. Next we shall present the derivation of the relativistic frequency spectra. A discussion of cut-off for the electromagnetic O-wave and X-wave follows as well as re-emission of synchrotron radiation. Wave propagation close to perpendicular to B field is assumed.

  5. Effect of scatter on image quality in synchrotron radiation mammography

    Science.gov (United States)

    Moeckli, Raphael; Verdun, Francis R.; Fiedler, Stefan; Pachoud, Marc; Schnyder, Pierre; Valley, Jean-Francois

    2001-06-01

    The display of low-contrast structures and fine microcalcifications is essential for the early diagnosis of breast cancer. In order to achieve a high image quality level with a minimum amount of radiation delivered to the patient, the use of different spectra (Mo or Rh anode and filters) was introduced. The European Synchrotron Radiation Facility is able to produce a monochromatic beam with a high photon flux. It is thus a powerful tool to study the effect of beam energy on image quality and dose in mammography. Our image quality assessment is based on the calculation of the size of the smallest microcalcification detectable on a radiograph, derived from the statistical decision theory. The mean glandular dose is simultaneously measured. Compared with conventional mammography units, the monochromaticity of synchrotron beams improves contrast and the use of a slit instead of an anti-scatter grid leads to a higher primary beam transmission. The relative contribution of these two effects on image quality and dose is discussed.

  6. Marginally fast cooling synchrotron models for prompt GRBs

    Science.gov (United States)

    Beniamini, Paz; Duran, Rodolfo Barniol; Giannios, Dimitrios

    2018-02-01

    Previous studies have considered synchrotron as the emission mechanism for prompt Gamma-Ray Bursts (GRBs). These works have shown that the electrons must cool on a timescale comparable to the dynamic time at the source in order to satisfy spectral constraints while maintaining high radiative efficiency. We focus on conditions where synchrotron cooling is balanced by a continuous source of heating, and in which these constraints are naturally satisfied. Assuming that a majority of the electrons in the emitting region are contributing to the observed peak, we find that the energy per electron has to be E ≳ 20 GeV and that the Lorentz factor of the emitting material has to be very large 103 ≲ Γem ≲ 104, well in excess of the bulk Lorentz factor of the jet inferred from GRB afterglows. A number of independent constraints then indicate that the emitters must be moving relativistically, with Γ΄ ≈ 10, relative to the bulk frame of the jet and that the jet must be highly magnetized upstream of the emission region, σup ≳ 30. The emission radius is also strongly constrained in this model to R ≳ 1016cm. These values are consistent with magnetic jet models where the dissipation is driven by magnetic reconnection that takes place far away from the base of the jet.

  7. Synchrotron X-ray imaging applied to solar photovoltaic silicon

    Science.gov (United States)

    Lafford, T. A.; Villanova, J.; Plassat, N.; Dubois, S.; Camel, D.

    2013-03-01

    Photovoltaic (PV) cell performance is dictated by the material of the cell, its quality and purity, the type, quantity, size and distribution of defects, as well as surface treatments, deposited layers and contacts. A synchrotron offers unique opportunities for a variety of complementary X-ray techniques, given the brilliance, spectrum, energy tunability and potential for (sub-) micron-sized beams. Material properties are revealed within in the bulk and at surfaces and interfaces. X-ray Diffraction Imaging (X-ray Topography), Rocking Curve Imaging and Section Topography reveal defects such as dislocations, inclusions, misorientations and strain in the bulk and at surfaces. Simultaneous measurement of micro-X-Ray Fluorescence (μ-XRF) and micro-X-ray Beam Induced Current (μ-XBIC) gives direct correlation between impurities and PV performance. Together with techniques such as microscopy and Light Beam Induced Current (LBIC) measurements, the correlation between structural properties and photovoltaic performance can be deduced, as well as the relative influence of parameters such as defect type, size, spatial distribution and density (e.g [1]). Measurements may be applied at different stages of solar cell processing in order to follow the evolution of the material and its properties through the manufacturing process. Various grades of silicon are under study, including electronic and metallurgical grades in mono-crystalline, multi-crystalline and mono-like forms. This paper aims to introduce synchrotron imaging to non-specialists, giving example results on selected solar photovoltaic silicon samples.

  8. Morphological breast imaging: tomography and digital mammography with synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Longo, Renata E-mail: renata.longo@ts.infn.it; Pani, Silvia; Arfelli, Fulvia; Dreossi, Diego; Olivo, Alessandro; Poropat, Paolo; Quaia, Emilio; Rigon, Luigi; Zanconati, Fabrizio; Palma, Ludovico Dalla; Castelli, Edoardo

    2003-01-21

    A synchrotron radiation-based X-ray source offers a powerful tool for mammography due to the energy spectrum properties and the peculiar laminar beam geometry. Significant improvements in image quality have been achieved by the SYRMEP (SYnchrotron Radiation for MEdical Physics) collaboration, which has designed and built a beamline devoted to medical physics at the SR facility Elettra in Trieste (Italy). The detection system developed for digital mammography consists of a silicon pixel detector with 200x300 {mu}m{sup 2} pixel size and high conversion efficiency. The detector is equipped with a low noise read-out electronics working in single photon counting mode. Mammographic phantoms and in vitro full breast samples have been investigated: the digital images show higher contrast resolution and lower absorbed dose than the images of the same samples obtained at the clinical mammographic unit.The SYRMEP collaboration is carrying out a breast tomography feasibility study to evaluate the image quality and the delivered dose. The SYRMEP beam is an ideal tool for tomography due to the laminar and monochromatic beam with negligible divergence. The experimental set-up and the acquisition protocol have been studied and the tomographic images of full breast samples acquired in the energy range 20-28 keV indicate that good quality images can be obtained with delivered doses comparable to conventional mammography.

  9. Stanford Synchrotron Radiation Laboratory activity report for 1987

    Energy Technology Data Exchange (ETDEWEB)

    Robinson, S.; Cantwell, K. [eds.

    1988-12-31

    During 1987, SSRL achieved many significant advances and reached several major milestones utilizing both SPEAR and PEP as synchrotron radiation sources as described in this report. Perhaps the following two are worthy of particular mention: (1) SPEAR reached an all time high of 4,190 delivered user-shifts during calendar year 1987, highlights of the many scientific results are given; (2) during a 12 day run in December of 1987, PEP was operated in a low emittance mode (calculated emittance 6.4 nanometer-radians) at 7.1 GeV with currents up to 33 mA. A second undulator beam line on PEP was commissioned during this run and used to record many spectra showing the extremely high brightness of the radiation. PEP is now by far the highest brightness synchrotron radiation source in the world. The report is divided into the following sections: (1) laboratory operations; (2) accelerator physics programs; (3) experimental facilities; (4) engineering division; (5) conferences and workshops; (6) SSRL organization; (7) experimental progress reports; (8) active proposals; (9) SSRL experiments and proposals by institution; and (10) SSRL publications.

  10. Brazilian scientific production on herbal medicines used in dentistry

    OpenAIRE

    R.D. Castro; J.A. Oliveira; Vasconcelos,L.C.; Maciel,P.P.; Brasil,V.L.M.

    2014-01-01

    The objective of this study was to critically analyze the scientific production published in specialized Brazilian journals concerning the use of medicinal plants in dentistry. A literature review was carried out using an indirect documentation technique by means of a bibliographical study. Four examiners performed independent searches in Brazilian journals of medicinal plants indexed in the database SciELO (Brazilian Journal of Pharmacognosy; Brazilian Journal of Medicinal Plants; Brazilian ...

  11. New developments in the application of synchrotron radiation to material science.

    Energy Technology Data Exchange (ETDEWEB)

    Sinha, S. K.

    1999-04-21

    Recent developments in the application of synchrotrons radiation to materials science are discussed, using techniques which exploit the high brilliance of the newer synchrotrons sources, such as microbeam techniques and correlation spectroscopy. These include studies of environmental systems, residual stress, slow dynamics of condensed matter systems and studies of liquid surfaces and thin magnetic films.

  12. Putting synchrotron radiation to work: New opportunities for industrial R D

    Energy Technology Data Exchange (ETDEWEB)

    1991-03-01

    This paper describes the basic categories of experimental techniques that have been successfully exploited at existing synchrotron facilities or, in some cases, that are expected to join the research armamentarium at the next-generation synchrotron sources now under construction, such as the ALS. In each case, a selection of typical industrial applications is noted.

  13. Using Jupiter's Synchrotron Radiation as a Probe into Jupiter's Inner Radiation Belts

    Science.gov (United States)

    Bolton, S. J.; Gulkis, S.; Klein, M. J.; Thorne, R. M.

    1995-01-01

    The Jovian decimetric emission is caused by the combined emission of synchrotron radiation originating from the relativistic electrons trapped in Jupiter's 'Van Allen radiation belts' and thermal emission from the planet's atmosphere. Synchrotron radiation characteristics and variations (which provides insight into the physical properties of Jupiter's inner radiation belts) will be amplified and discussed.

  14. Synchrotron vacuum ultraviolet radiation studies of the D 1Πu state of H2

    NARCIS (Netherlands)

    Dickenson, G. D.; Ivanov, T. I.; Roudjane, M.; de Oliveira, N.; Joyeux, D.; Nahon, L.; Tchang-Brillet, W. Ü L; Glass-Maujean, M.; Haas, I.; Ehresmann, A.; Ubachs, W.

    2010-01-01

    The 3pπD 1Πu state of the H2 molecule was reinvestigated with different techniques at two synchrotron installations. The Fourier transform spectrometer in the vacuum ultraviolet wavelength range of the DESIRS beamline at the SOLEIL synchrotron was used for recording absorption spectra of the D Π1u

  15. Summer-time blues French researchers, angry and upset over last week's synchrotron decision, deserve a full explanation

    CERN Multimedia

    1999-01-01

    Allegre needs to produce a detailed description of the calculations he used to make his decision to support the British synchrotron project. French researchers had been hoping to build their own synchrotron 'Soleil' on French territory (4 paragraphs)

  16. Report of the second workshop on synchrotron radiation sources for x-ray lithography

    Energy Technology Data Exchange (ETDEWEB)

    Barton, M.Q.; Craft, B.; Williams, G.P. (eds.)

    1986-01-01

    The reported workshop is part of an effort to implement a US-based x-ray lithography program. Presentations include designs for three storage rings (one superconducting and two conventional) and an overview of a complete lithography program. The background of the effort described, the need for synchrotron radiation, and the international competition in the area are discussed briefly. The technical feasibility of x-ray lithography is discussed, and synchrotron performance specifications and construction options are given, as well as a near-term plan. It is recommended that a prototype synchrotron source be built as soon as possible, and that a research and development plan on critical technologies which could improve cost effectiveness of the synchrotron source be established. It is further recommended that a small number of second generation prototype synchrotrons be distributed to IC manufacturing centers to expedite commercialization. (LEW)

  17. Neymar, defender of brazilian tradition

    Directory of Open Access Journals (Sweden)

    Francisca Islandia Cardoso da Silva

    2016-09-01

    Full Text Available The purpose of this article is to analyze how university students of Teresina-PI appropriate of the message of a report of the television show Esporte Espetacular. There was use of the technique of focus groups and analytical-descriptive method for collecting and analyzing data. The sample consisted of 24 university students, aged between 18 and 24 years. The report features Neymar as responsible to follow the "tradition" of Brazilians and to be crowned as the best player in the world. The subjects of research said that the speech conveyed by the report can reproduce and create a reality sometimes dreamlike, because objective to confer to Neymar great importance with regard to national identity.

  18. Best Practices in Brazilian Companies

    Directory of Open Access Journals (Sweden)

    Catia dos Reis Machado

    2013-04-01

    Full Text Available Competitive intelligence (CI is a systematic and ethical collection, analysis, dissemination and management of information about the external environment that may affect the plans, decisions and operations of the organization. Knowledge management (KM can be seen as a tool to promote organizational knowledge through the use of activities designed to identify, create, store, share and use knowledge. Companies face a challenge in the era of knowledge, it is the extraction and management of knowledge produced by people in the organization. CI and KM combined generates organizational intelligence. The exploratory study, based on literature and multicase study, we sought to identify best practices in processes of CI and KM in Brazilian companies. We identified practices related to the CI design process, the stages of the CI, the use of networks, and knowledge management. We also identified, points of attention on the internal/external organizational environment.

  19. Cerebrotendinous xanthomatosis: report of two Brazilian brothers.

    NARCIS (Netherlands)

    Lange, M.C.; Zetola, V.F.; Teive, H.; Scola, R.H.; Trentin, A.P.; Zavala, J.A.; Pereira, E.R.; Raskin, S.; Werneck, L.C.; Sistermans, E.A.

    2004-01-01

    Cerebrotendinous xanthomatosis is a treatable rare autossomal recessive disease characterized by lipid storage secondary to a sterol 27-hydroxylase deficiency in the formation of cholic and chenodeoxycholic acids. We describe two Brazilian brothers with cognitive impairement and chronic diarrhea.

  20. Synchrotron radiation studies of inorganic-organic semiconductor interfaces

    CERN Document Server

    Evans, D A; Vearey-Roberts, A R; Bushell, A; Cabailh, G; O'Brien, S; Wells, J W; McGovern, I T; Dhanak, V R; Kampen, T U; Zahn, D R T; Batchelor, D

    2003-01-01

    Organic semiconductors (polymers and small molecules) are widely used in electronic and optoelectronic technologies. Many devices are based on multilayer structures where interfaces play a central role in device performance and where inorganic semiconductor models are inadequate. Synchrotron radiation techniques such as photoelectron spectroscopy (PES), near-edge X-ray absorption fine structure (NEXAFS) and X-ray standing wave spectroscopy (XSW) provide a powerful means of probing the structural, electronic and chemical properties of these interfaces. The surface-specificity of these techniques allows key properties to be monitored as the heterostructure is fabricated. This methodology has been directed at the growth of hybrid organic-inorganic semiconductor interfaces involving copper phthalocyanine as the model organic material and InSb and GaAs as the model inorganic semiconductor substrates. Core level PES has revealed that these interfaces are abrupt and chemically inert due to the weak bonding between t...

  1. Error reduction techniques for measuring long synchrotron mirrors

    Energy Technology Data Exchange (ETDEWEB)

    Irick, S.

    1998-07-01

    Many instruments and techniques are used for measuring long mirror surfaces. A Fizeau interferometer may be used to measure mirrors much longer than the interferometer aperture size by using grazing incidence at the mirror surface and analyzing the light reflected from a flat end mirror. Advantages of this technique are data acquisition speed and use of a common instrument. Disadvantages are reduced sampling interval, uncertainty of tangential position, and sagittal/tangential aspect ratio other than unity. Also, deep aspheric surfaces cannot be measured on a Fizeau interferometer without a specially made fringe nulling holographic plate. Other scanning instruments have been developed for measuring height, slope, or curvature profiles of the surface, but lack accuracy for very long scans required for X-ray synchrotron mirrors. The Long Trace Profiler (LTP) was developed specifically for long x-ray mirror measurement, and still outperforms other instruments, especially for aspheres. Thus, this paper focuses on error reduction techniques for the LTP.

  2. Light fragment production at CERN Super Proton Synchrotron

    Science.gov (United States)

    Ivanov, Yu. B.; Soldatov, A. A.

    2017-11-01

    Recent data on the deutron and 3He production in central Pb+Pb collisions at the CERN Super Proton Synchrotron (SPS) energies measured by the NA49 Collaboration are analyzed within the model of the three-fluid dynamics (3FD) complemented by the coalescence model for the light-fragment production. The simulations are performed with different equations of state -with and without deconfinement transition. It is found that scenarios with the deconfinement transition are preferable for reproduction rapidity distributions of deuterons and 3 He, the corresponding results well agree with the experimental data. At the same time the calculated transverse-mass spectra at midrapidity do not agree that nicely with the experimental data. The latter apparently indicate that coalescence coefficients should be temperature and/or momentum dependent.

  3. Dynamics of synchrotron VUV-induced intracluster reactions

    Energy Technology Data Exchange (ETDEWEB)

    Grover, J.R. [Brookhaven National Laboratory, Upton, NY (United States)

    1993-12-01

    Photoionization mass spectrometry (PIMS) using the tunable vacuum ultraviolet radiation available at the National Synchrotron Light Source is being exploited to study photoionization-induced reactions in small van der Waals mixed complexes. The information gained includes the observation and classification of reaction paths, the measurement of onsets, and the determination of relative yields of competing reactions. Additional information is obtained by comparison of the properties of different reacting systems. Special attention is given to finding unexpected features, and most of the reactions investigated to date display such features. However, understanding these reactions demands dynamical information, in addition to what is provided by PIMS. Therefore the program has been expanded to include the measurement of kinetic energy release distributions.

  4. X-ray imaging detectors for synchrotron and XFEL sources

    Directory of Open Access Journals (Sweden)

    Takaki Hatsui

    2015-05-01

    Full Text Available Current trends for X-ray imaging detectors based on hybrid and monolithic detector technologies are reviewed. Hybrid detectors with photon-counting pixels have proven to be very powerful tools at synchrotrons. Recent developments continue to improve their performance, especially for higher spatial resolution at higher count rates with higher frame rates. Recent developments for X-ray free-electron laser (XFEL experiments provide high-frame-rate integrating detectors with both high sensitivity and high peak signal. Similar performance improvements are sought in monolithic detectors. The monolithic approach also offers a lower noise floor, which is required for the detection of soft X-ray photons. The link between technology development and detector performance is described briefly in the context of potential future capabilities for X-ray imaging detectors.

  5. Modelling and control of neutron and synchrotron beamline positioning systems

    Energy Technology Data Exchange (ETDEWEB)

    Nneji, S.O., E-mail: Stephen.nneji@open.ac.uk [The Open University, Materials Engineering, Walton Hall, Milton Keynes, Buckinghamshire MK7 6AA (United Kingdom); Science and Technology Facility Council , Rutherford Appleton Laboratory, Harwell Science and Innovation Campus, Didcot, OX110QX Oxfordshire (United Kingdom); Zhang, S.Y.; Kabra, S. [Science and Technology Facility Council , Rutherford Appleton Laboratory, Harwell Science and Innovation Campus, Didcot, OX110QX Oxfordshire (United Kingdom); Moat, R.J.; James, J.A. [The Open University, Materials Engineering, Walton Hall, Milton Keynes, Buckinghamshire MK7 6AA (United Kingdom)

    2016-03-21

    Measurement of residual stress using neutron or synchrotron diffraction relies on the accurate alignment of the sample in relation to the gauge volume of the instrument. Automatic sample alignment can be achieved using kinematic models of the positioning system provided the relevant kinematic parameters are known, or can be determined, to a suitable accuracy. In this paper, the use of techniques from robotic calibration theory to generate kinematic models of both off-the-shelf and custom-built positioning systems is demonstrated. The approach is illustrated using a positioning system in use on the ENGIN-X instrument at the UK's ISIS pulsed neutron source comprising a traditional XYZΩ table augmented with a triple axis manipulator. Accuracies better than 100 microns were achieved for this compound system. Discussed here in terms of sample positioning systems these methods are entirely applicable to other moving instrument components such as beam shaping jaws and detectors.

  6. Monochromator on a synchrotron undulator source for liquid surface studies

    DEFF Research Database (Denmark)

    Als-Nielsen, Jens Aage; Freund, A.K.

    1992-01-01

    % of the useful x rays, in full agreement with diffraction theory including secondary extinction. Heat load experiments reported elsewhere in this conference prove that Be crystals can withstand high beam power density and that the thermal deformation is small compared to the mosaic spread. The results...... a monochromator made of a beryllium mosaic crystal using the (002) reflection in Laue geometry placed in undulator beams of DORIS III at the Hamburger Synchrotronstrahlungslabor and of the European Synchrotron Radiation Facility. An analysis of the diffraction properties in terms of mosaic spread, heat load...... of the flux calculations are most encouraging: a gain of order 10(3) to 10(4) can be expected as compared to existing liquid surface spectrometers....

  7. A NEW THERMIONIC RF ELECTRON GUN FOR SYNCHROTRON LIGHT SOURCES

    Energy Technology Data Exchange (ETDEWEB)

    Kutsaev, Sergey; Agustsson, R.; Hartzell, J; Murokh, A.; Nassiri, A.; Savin, E.; Smirnov, A.V.; Smirnov, A. Yu; Sun, Y.; Verma, A; Waldschmidt, Geoff; Zholents, A.

    2017-06-02

    A thermionic RF gun is a compact and efficient source of electrons used in many practical applications. RadiaBeam Systems and the Advanced Photon Source at Argonne National Laboratory collaborate in developing of a reliable and robust thermionic RF gun for synchrotron light sources which would offer substantial improvements over existing thermionic RF guns and allow stable operation with up to 1A of beam peak current at a 100 Hz pulse repetition rate and a 1.5 μs RF pulse length. In this paper, we discuss the electromagnetic and engineering design of the cavity and report the progress towards high power tests of the cathode assembly of the new gun.

  8. Space-Charge Simulation of Integrable Rapid Cycling Synchrotron

    Energy Technology Data Exchange (ETDEWEB)

    Eldred, Jeffery [Fermilab; Valishev, Alexander [Fermilab

    2017-05-01

    Integrable optics is an innovation in particle accelerator design that enables strong nonlinear focusing without generating parametric resonances. We use a Synergia space-charge simulation to investigate the application of integrable optics to a high-intensity hadron ring that could replace the Fermilab Booster. We find that incorporating integrability into the design suppresses the beam halo generated by a mismatched KV beam. Our integrable rapid cycling synchrotron (iRCS) design includes other features of modern ring design such as low momentum compaction factor and harmonically canceling sextupoles. Experimental tests of high-intensity beams in integrable lattices will take place over the next several years at the Fermilab Integrable Optics Test Accelerator (IOTA) and the University of Maryland Electron Ring (UMER).

  9. Generic radiation safety design for SSRL synchrotron radiation beamlines

    Energy Technology Data Exchange (ETDEWEB)

    Liu, James C. [Radiation Protection Department, Stanford Linear Accelerator Center (SLAC), MS 48, P.O. Box 20450, Stanford, CA 94309 (United States)]. E-mail: james@slac.stanford.edu; Fasso, Alberto [Radiation Protection Department, Stanford Linear Accelerator Center (SLAC), MS 48, P.O. Box 20450, Stanford, CA 94309 (United States); Khater, Hesham [Radiation Protection Department, Stanford Linear Accelerator Center (SLAC), MS 48, P.O. Box 20450, Stanford, CA 94309 (United States); Prinz, Alyssa [Radiation Protection Department, Stanford Linear Accelerator Center (SLAC), MS 48, P.O. Box 20450, Stanford, CA 94309 (United States); Rokni, Sayed [Radiation Protection Department, Stanford Linear Accelerator Center (SLAC), MS 48, P.O. Box 20450, Stanford, CA 94309 (United States)

    2006-12-15

    To allow for a conservative, simple, uniform, consistent, efficient radiation safety design for all SSRL beamlines, a generic approach has been developed, considering both synchrotron radiation (SR) and gas bremsstrahlung (GB) hazards. To develop the methodology and rules needed for generic beamline design, analytic models, the STAC8 code, and the FLUKA Monte Carlo code were used to pre-calculate sets of curves and tables that can be looked up for each beamline safety design. Conservative beam parameters and standard targets and geometries were used in the calculations. This paper presents the SPEAR3 beamline parameters that were considered in the design, the safety design considerations, and the main pre-calculated results that are needed for generic shielding design. In the end, the rules and practices for generic SSRL beamline design are summarized.

  10. VUV photochemistry simulation of planetary upper atmosphere using synchrotron radiation.

    Science.gov (United States)

    Carrasco, Nathalie; Giuliani, Alexandre; Correia, Jean Jacques; Cernogora, Guy

    2013-07-01

    The coupling of a gas reactor, named APSIS, with a vacuum-ultraviolet (VUV) beamline at the SOLEIL synchrotron radiation facility, for a photochemistry study of gas mixtures, is reported. The reactor may be irradiated windowless with gas pressures up to hundreds of millibar, and thus allows the effect of energetic photons below 100 nm wavelength to be studied on possibly dense media. This set-up is perfectly suited to atmospheric photochemistry investigations, as illustrated by a preliminary report of a simulation of the upper atmospheric photochemistry of Titan, the largest satellite of Saturn. Titan's atmosphere is mainly composed of molecular nitrogen and methane. Solar VUV irradiation with wavelengths no longer than 100 nm on the top of the atmosphere enables the dissociation and ionization of nitrogen, involving a nitrogen chemistry specific to nitrogen-rich upper atmospheres.

  11. Electron cloud detection and characterization in the CERN Proton Synchrotron

    Directory of Open Access Journals (Sweden)

    Edgar Mahner

    2008-09-01

    Full Text Available We describe a dedicated electron cloud experiment which was installed in the CERN Proton Synchrotron in 2007. The setup comprises shielded button-type pickups, a fast vacuum logging, a dipole magnet, and a stripline electrode to experimentally verify the beneficial effect of electron cloud clearing. The electron cloud effect was observed within the last milliseconds before ejection of the nominal LHC proton beam consisting of 72 bunches with 25 ns spacing. Measurements of electron flux at the wall and vacuum pressure are presented for a set of magnetic fields and bias voltages on the clearing electrode, showing that efficient electron cloud suppression can be obtained for appropriate clearing voltages but revealing an unexpectedly complex dependence on magnetic field and voltage.

  12. Performance of multilayers in intense synchrotron x-ray beams

    Energy Technology Data Exchange (ETDEWEB)

    Ziegler, E.; Lepetre, Y.; Joksch, S.; Saile, V.; Mourikis, S.; Viccaro, P. J.; Rolland, G.; Laugier, F.

    1989-07-01

    The use of multilayer reflectors under intense synchroton x-ray beams requires to develop a new generation of multilayered materials that can withstand a high-power load in excess of 100 W/mm/sup 2/. Multilayers with the high-/ital Z/ layer consisting either of a pure element or of compounds such as carbides, nitrides, or silicides have been produced. Because the fabrication conditions are not yet optimized, thin films with satisfactory layer were not obtained leading to poor reflectivities. Such multilayers have been both thermally annealed in a furnace and exposed to a synchrotron beam with a power density of about 1 W/mm/sup 2/. The resulting damage ranges from the total destruction of the layering to a reduction of the reflectivity by typically 40%--60%. In some cases an only 1%--15% loss in reflectivity has been observed.

  13. Measurement and analysis of coherent synchrotron radiation effects at FLASH

    Energy Technology Data Exchange (ETDEWEB)

    Beutner, B.

    2007-12-15

    The vacuum-ultra-violet Free Electron Laser in Hamburg (FLASH) is a linac driven SASE-FEL. High peak currents are produced using magnetic bunch compression chicanes. In these magnetic chicanes, the energy distribution along an electron bunch is changed by eff ects of Coherent Synchrotron Radiation (CSR). Energy changes in dispersive bunch compressor chicanes lead to transverse displacements along the bunch. These CSR induced displacements are studied using a transverse deflecting RF-structure. Experiments and simulations concerning the charge dependence of such transverse displacements are presented and analysed. In these experiments an over-compression scheme is used which reduces the peak current downstream the bunch compressor chicanes. Therefore other self interactions like space charge forces which might complicate the measurements are suppressed. Numerical simulations are used to analyse the beam dynamics under the influence of CSR forces. The results of these numerical simulations are compared with the data obtained in the over-compression experiments at FLASH. (orig.)

  14. NanoESCA, a new nanospectroscopy tool with synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Patt, Marten; Wiemann, Carsten; Krug, Ingo; Schneider, Claus Michael [PGI-6, Forschungszentrum Juelich GmbH, Juelich (Germany); Escher, Matthias; Weber, Nils; Merkel, Michael [Focus GmbH, Huenstetten (Germany)

    2011-07-01

    Nanotechnology and nanoscience are developing more and more to smaller length scales. We face the need for the characterization of surface electronic and magnetic states in these reduced dimensions with a new energy-filtered photoelectron emission microscope (PEEM), which we have recently installed at the ELETTRA synchrotron facility (Italy). The instrument features a novel electrostatic lens system with 30 kV extraction voltage, enabling spatially resolved photoelectron imaging with a lateral resolution smaller than 100 nm and combines it with a double-hemispherical energy filter, a single-event counting detector unit and a liquid helium cooled sample manipulator with five degrees of freedom. A second operation mode provides the mapping of the angular distribution (k-space microscopy) of the photoelectrons. We discuss the capabilities and the performance of the instrument with respect to its lateral and energy resolution, sensitivity and signal-to-noise-ratio.

  15. The application of synchrotron radiation to non-invasive angiography

    Science.gov (United States)

    Hughes, E. B.; Zeman, H. D.; Campbell, L. E.; Hofstadter, R.; Meyer-Berkhout, U.; Otis, J. N.; Rolfe, J.; Stone, J. P.; Wilson, S.; Rubenstein, E.; Harrison, D. C.; Kernoff, R. S.; Thompson, A. C.; Brown, G. S.

    1983-04-01

    Synchrotron radiation provides a new source of X-rays highly-suited to iodine K-edge Digital Subtraction Angiography (DSA). The use of such beams provides maximum sensitivity to intra-arterial iodine and virtually eliminates image contrast due to non-vascular body structures. The intensity of the beams permits short exposure times and allows images to be recorded, in line-scan fashion, in sharp focus despite arterial motions. The sensitivity of this method offers the prospect of visualizing arteries, and in particular the coronary arteries, by peripheral venous injection. The principles of DSA have been demonstrated using phantoms and excised animal hearts, and in vivo studies in animals have begun. The instrumentation developed for this purpose and the results obtained to date are summarized.

  16. Spectrum Analyzer Application for the Proton Synchrotron Wall Current Monitors

    CERN Document Server

    Limpens, Rik

    The Proton Synchrotron (PS) is a key component in CERN's accelerator complex, where it usually accelerates either protons or heavy ions. The new acquisition system for the PS ring wall current monitors has been installed to be able to perform higher frequency measurements of a beam bunch. This is an important improvement, since the oscillating signals are related to losses of a beam bunch. The main goal of this project is to develop a LabVIEW application running on a Real-Time target to perform continuous and triggered spectral acquisition of a PS beam bunch and to provide a data visualization and analysis tool for the operators and users of the machine.

  17. In situ visualization of thermal distortions of synchrotron radiation optics

    Science.gov (United States)

    Revesz, P.; Kazimirov, A.; Bazarov, I.

    2007-06-01

    We have developed a new in situ method to measure heating-induced distortions of the surface of the first monochromator crystal exposed to high-power white synchrotron radiation beam. The method is based on recording the image of a stationary grid of dots captured by a CCD camera as reflected from the surface of a crystal with and without a heat load. The three-dimensional surface profile (heat bump) is then reconstructed from the distortions of the original pattern. In experiments performed at the CHESS A2 wiggler beam line we measured the heat bumps with the heights of up to 600 nm produced by a wiggler beam with total power in the range of 15-60 W incident on the (1 1 1) Si crystal at various angles between 3° and 15°.

  18. New Pulsed Orbit Bump Magnets for the Fermilab Booster Synchrotron

    CERN Document Server

    Lackey, James; John, Carson; Kashikhin, Vladimir; Makarov, Alexander; Prebys, Eric

    2005-01-01

    The beam from the Fermilab Linac is injected onto a bump in the closed orbit of the Booster Synchrotron where a carbon foil strips the electrons from the Linac’s negative ion hydrogen beam. Although the Booster itself runs at 15Hz, heat dissipation in the orbit bump magnets has been one limitation to the fraction of the cycles that can be used for beam. New, 0.28T pulsed window frame dipole magnets have been constructed that will fit into the same space as the old ones, run at the full repetition rate of the Booster, and provide a larger bump to allow a cleaner injection orbit. The new magnets use a high saturation flux density Ni-Zn ferrite in the yoke rather than laminated steel. The presented magnetic design includes two and three dimensional magnetic field calculations with eddy currents and ferrite nonlinear effects.

  19. X-ray magnetic diffraction of ferromagnets with synchrotron radiation

    CERN Document Server

    Ito, M

    2002-01-01

    X-ray magnetic diffraction experiment of ferromagnets that utilizes elliptically polarized synchrotron radiation is presented. First we have reviewed shortly historical backgrounds and theoretical aspects of the experiment. We have presented how the magnetic form factors are measured and are separated into the spin-moment component and the orbital-moment component in this experiment. Peculiar features of the polarization factor of this experiment have been explained. We have introduced two examples of the experiment. One is the measurement of the spin-magnetic form factor of SmAl sub 2 with white X-rays from a bending magnet at the Photon Factory. The other is the measurement of the orbital-magnetic form factor of Holmium Iron Garnets with monochromatic X-rays from an undulator at the SPring-8. Finally we summarize the article and show some future prospects of this experiment. (author)

  20. Synchrotron Radiation Maps from Relativistic MHD Jet Simulations

    Directory of Open Access Journals (Sweden)

    Dimitrios Millas

    2017-11-01

    Full Text Available Relativistic jets from active galactic nuclei (AGN often display a non-uniform structure and are, under certain conditions, susceptible to a number of instabilities. An interesting example is the development of non-axisymmetric, Rayleigh-Taylor type instabilities in the case of differentially rotating two-component jets, with the toroidal component of the magnetic field playing a key role in the development or suppression of these instabilities. We have shown that higher magnetization leads to stability against these non-axisymmetric instabilities. Using ray-casting on data from relativistic MHD simulations of two-component jets, we now investigate the effect of these instabilities on the synchrotron emission pattern from the jets. We recover many well known trends from actual observations, e.g., regarding the polarization fraction and the distribution of the position angle of the electric field, in addition to a different emitting region, depending on the stability of the jet.

  1. Synchrotron X-Ray Radiation and Deformation Studies

    DEFF Research Database (Denmark)

    Fæster Nielsen, Søren

    machining. The conical slit has six 25µm thick conically shaped openings matching six of the Debye-Scherrer cones from a fcc powder. By combining the conical slit with a micro-focused incoming beam of hard X-rays an embedded gauge volume is defined. Using a 2D detector, fast and complete information can...... the embedded grains within thick samples in three dimensions. All essential features like the position, volume, orien-tation, stress-state of individual grains can be determined, including the morphology of the grain boundaries. The first results obtained by using the novel tracking technique are presented...... in combination with synchrotron X-ray tomography in order to gain new in-formation on the wetting kinetics of liquid gallium in aluminium grain boundaries. Finally, an electron microscopy investigation was carried out in order to describe the lattice rotations and texture evolution in uniaxially compressed...

  2. Calculations of synchrotron emission from the terrestrial radiation belts

    Science.gov (United States)

    Johnson, R.

    1972-01-01

    A theoretical model was developed to allow for the calculation of the synchrotron emission arising from high energy electrons trapped in the Van Allen belts of a planet with a dipole magnetic field. The model is general enough to allow for the calculation of the intensity of radiation received by an observer at any distance from and any latitude about the planet. The model is used to compute the emission from the earth's Van Allen belts that one should expect at various latitudes at a distance of 1.92 earth radii, the position of the Radio Astronomy Explorer satellite that was launched in 1968, for the frequencies 1.3 MHz and 2.2 MHz.

  3. CERN Proton Synchrotron Complex High-Level Controls Renovation

    CERN Document Server

    Deghaye, S; Garcia Quintas, D; Gourber-Pace, M; Kruk, G; Kulikova, O; Lezhebokov, V; Pasinelli, S; Peryt, M; Roderick, C; Roux, E; Sobczak, M; Steerenberg, R; Wozniak, J; Zaharieva, Z

    2009-01-01

    After a detailed study of the Proton Synchrotron (PS) complex requirements by experts of CERN controls & operation groups, a proposal to develop a new system, called Injector Controls Architecture (InCA), was presented to and accepted by the management late 2007. Aiming at the homogenisation of the control systems across CERN accelerators, InCA is based on components developed for the Large Hadron Collider (LHC) but also new components required to fulfil operation needs. In 2008, the project was in its elaboration phase and we successfully validated its architecture and critical use-cases during several machine development sessions. After description of the architecture put in place and the components used, this paper describes the planning approach taken combining iterative development phases with deployment in operation for validation sessions.

  4. On-line control of the nonlinear dynamics for synchrotrons

    Directory of Open Access Journals (Sweden)

    J. Bengtsson

    2015-07-01

    Full Text Available We propose a simple approach to the on-line control of the nonlinear dynamics in storage rings, based on compensation of the nonlinear resonance driving terms using beam losses as the main indicator of the strength of a resonance. The correction scheme is built on the analysis of the resonance driving terms in first perturbative order and on the possibility of using independent power supplies in the sextupole magnets, which is nowadays present in many synchrotron light sources. Such freedom allows the definition of “smart sextupole knobs” attacking each resonance separately. The compensation scheme has been tested at the Diamond light source and proved to be effective in opening up the betatron tune space, resonance free, available to the electron beam and to improve the beam lifetime.

  5. On-line control of the nonlinear dynamics for synchrotrons

    Science.gov (United States)

    Bengtsson, J.; Martin, I. P. S.; Rowland, J. H.; Bartolini, R.

    2015-07-01

    We propose a simple approach to the on-line control of the nonlinear dynamics in storage rings, based on compensation of the nonlinear resonance driving terms using beam losses as the main indicator of the strength of a resonance. The correction scheme is built on the analysis of the resonance driving terms in first perturbative order and on the possibility of using independent power supplies in the sextupole magnets, which is nowadays present in many synchrotron light sources. Such freedom allows the definition of "smart sextupole knobs" attacking each resonance separately. The compensation scheme has been tested at the Diamond light source and proved to be effective in opening up the betatron tune space, resonance free, available to the electron beam and to improve the beam lifetime.

  6. Lipidic cubic phase serial millisecond crystallography using synchrotron radiation

    Directory of Open Access Journals (Sweden)

    Przemyslaw Nogly

    2015-03-01

    Full Text Available Lipidic cubic phases (LCPs have emerged as successful matrixes for the crystallization of membrane proteins. Moreover, the viscous LCP also provides a highly effective delivery medium for serial femtosecond crystallography (SFX at X-ray free-electron lasers (XFELs. Here, the adaptation of this technology to perform serial millisecond crystallography (SMX at more widely available synchrotron microfocus beamlines is described. Compared with conventional microcrystallography, LCP-SMX eliminates the need for difficult handling of individual crystals and allows for data collection at room temperature. The technology is demonstrated by solving a structure of the light-driven proton-pump bacteriorhodopsin (bR at a resolution of 2.4 Å. The room-temperature structure of bR is very similar to previous cryogenic structures but shows small yet distinct differences in the retinal ligand and proton-transfer pathway.

  7. Space-Charge Experiments at the CERN Proton Synchrotron

    CERN Document Server

    Franchetti, Giuliano; Hofmann, I; Martini, M; Métral, E; Qiang, J; Ryne, D; Steerenberg, R; CFA Beam Dynamics Workshop “High Intensity and Brightness Hadron Beams”

    2005-01-01

    Benchmarking of the simulation codes used for the design of the next generation of high beam power accelerators is of paramount importance due to the very demanding requirements on the level of beam losses. This is usually accomplished by comparing simulation results against available theories, and more importantly, against experimental observations. To this aim, a number of well-defined test cases, obtained by accurate measurements made in existing machines, are of great interest. Such measurements have been made in the CERN Proton Synchrotron to probe three space-charge effects: (i) transverse emittance blow-up due to space-charge induced crossing of the integer or half-integer stop-band, (ii) space-charge and octupole driven resonance trapping, and (iii) intensity-dependent emittance transfer between the two transverse planes. The last mechanism is discussed in detail in this paper and compared to simulation predictions.

  8. The RF Cycle of the PIMMS Medical Synchrotron

    CERN Document Server

    Crescenti, M; Knaus, P

    2000-01-01

    This paper presents the design of the RF cycle of the medical synchrotron of the PIMMS (Proton-Ion Medical Machine Study) hosted at CERN. The cycle comprises adiabatic trapping, acceleration and RF gymnastics, for either protons or fully stripped carbon ions. The injection energy is 20 MeV for protons and 7 MeV/u for carbon. Maximum extraction energies are 250 MeV for protons and 400 MeV/u for carbon ions. The cycle duration is less than 1 s, with a maximum magnetic field ramp below 3 T/s. The simulations show that the beam stays inside the aperture of the machine, and that, theoretically, there are no longitudinal losses. At the end of the cycle, the beam is ready for extraction with a Dp/p = 0.4 %. The peak RF voltage is 3 kV and the frequency ranges from 0.4 to 3 MHz.

  9. Vavilov-Cherenkov and Synchrotron Radiation Foundations and Applications

    CERN Document Server

    Afanasiev, G. N

    2005-01-01

    The theory of the Vavilov-Cherenkov radiation observed by Cherenkov in 1934 was created by Tamm, Frank and Ginsburg who associated the observed blue light with the uniform charge motion of a charge at a velocity greater than the velocity of light in the medium. On the other hand, Vavilov, Cherenkov's teacher, attributed the observed blue light to the deceleration of electrons. This has given rise to the appearance of papers in which the radiation of a charge uniformly moving in a finite space interval was related to the Bremsstrahlung arising at the end points of the motion interval. This monograph is intended for students of the third year and higher, for postgraduates, for professional scientists (both experimentalists and theoreticians) dealing with Vavilov-Cherenkov and synchrotron radiation. An acquaintance with the three volumes of the Landau and Lifshitz course (Quantum Mechanics, Classical Field Theory and Macroscopic Electrodynamics) is sufficient for understanding the text.

  10. Futebol mulato: racial constructs in Brazilian football

    Directory of Open Access Journals (Sweden)

    Tiago Fernandes Maranhao

    2011-05-01

    Full Text Available The aim of this paper is to review Gilberto Freyre’s ideas about futebol mulato and the way these ideas have spread the notion of the Brazilian mulatto as a symbol of a ‘racial democracy’, unique in Brazil, around the world. The notion first appeared in 1938 in an article by Freyre for the Diários Associados, an important Brazilian newspaper. Football (soccer was employed by Freyre as the special arena where the multiracial Brazilian nation could shine and show the world a different way of being, opposed to the white and ‘rational’ way of European football. In Freyre’s work, the so-called ‘football-art’ was compared to poetry, while the European style was equated with prose. This essay argues that Freyre’s ideas were useful in constructing the Brazilian identity, a nation of harmony in all its aspects, including the area of race, and how the idea of the mulatto has been used to minimise social disparities within Brazilian society. Freyre’s ideas remain contemporary; many Brazilian intellectuals still refer to these concepts. As well, the press in this huge country, and especially in World Cup years, uses the concepts of mulatto and football-art to characterize Brazil and differentiate it from other countries.

  11. Phylodynamics of the Brazilian feline immunodeficiency virus.

    Science.gov (United States)

    Cano-Ortiz, Lucía; Junqueira, Dennis Maletich; Comerlato, Juliana; Costa, Cristina Santos; Zani, André; Duda, Naila Blatt; Tochetto, Caroline; Dos Santos, Raissa Nunes; da Costa, Fernanda Vieira Amorim; Roehe, Paulo Michel; Franco, Ana Cláudia

    2017-11-01

    Feline immunodeficiency virus (FIV), like other retroviruses, displays large genomic divergence when different isolates are compared. In this study, 31 FIV positive samples of domestic cats from Porto Alegre, RS, Brazil were used aiming at a detailed genomic characterization and a better understanding of the molecular epidemiology of the virus in Brazil. The proviral env genes were partially amplified, sequenced and compared with another 237 sequences from different continents. We identified several Brazilian highly supported clades (A, B1, B2, C and D) that suggest independent events of introduction of FIV in Brazil. Forty six reference-sequences from the GenBank were used with our 31 sequences to infer the virus subtypes. Our sequences belong to the subtype B and three of them result from a recombination with the previously described subtype F. The other 28 Brazilian samples belonging to subtype B and another 46 Brazilian sequences from the GenBank were used to estimate the time to the most recent common ancestor of each Brazilian clade, using a Bayesian approach and a relaxed molecular clock model. The analyses of Brazilian sequences suggest several different entries of the virus in the Brazilian cat population between 1981 and 1991. Copyright © 2017 Elsevier B.V. All rights reserved.

  12. 3rd BRAZILIAN CONSENSUS ON Helicobacter pylori

    Directory of Open Access Journals (Sweden)

    Luiz Gonzaga Coelho

    2013-04-01

    Full Text Available Significant progress has been obtained since the Second Brazilian Consensus Conference on Helicobacter pylori Infection held in 2004, in São Paulo, SP, Brazil, and justify a third meeting to establish updated guidelines on the current management of H. pylori infection. The Third Brazilian Consensus Conference on H pylori Infection was organized by the Brazilian Nucleus for the Study of Helicobacter, a Department of the Brazilian Federation of Gastroenterology and took place on April 12-15, 2011, in Bento Gonçalves, RS, Brazil. Thirty-one delegates coming from the five Brazilian regions and one international guest, including gastroenterologists, pathologists, epidemiologists, and pediatricians undertook the meeting. The participants were allocated in one of the five main topics of the meeting: H pylori, functional dyspepsia and diagnosis; H pylori and gastric cancer; H pylori and other associated disorders; H pylori treatment and retreatment; and, epidemiology of H pylori infection in Brazil. The results of each subgroup were submitted to a final consensus voting to all participants. Relevant data were presented, and the quality of evidence, strength of recommendation, and level of consensus were graded. Seventy per cent and more votes were considered as acceptance for the final statement. This article presents the main recommendations and conclusions to guide Brazilian doctors involved in the management of H pylori infection.

  13. National Synchrotron Light Source angiography personnel protection interlock

    Energy Technology Data Exchange (ETDEWEB)

    Gmuer, N.; Larson, R.; Thomlinson, W.

    1992-06-01

    This document has been written to describe the safety system operation at the NSLS X17B2 beamline Synchrotron Medical Research Facility (SMERF). The angiography exposure process involves scanning a patient up and down through dual fixed-position x-ray beams; exposure is controlled by opening and closing a fast-acting Safety Shutter mechanism at precise times in relation to the up and down motion of the scan chair. The fast-acting Safety Shutter mechanism is the primary radiation-stopping element protecting the patient while the chair is at rest and while it is reversing directions during the scan. Its fail-safe and fast operation is essential for the safety of the patient. Operation of X17B2 as a human subject angiography station necessitates the implementation of a personnel protection interlock system that, in conjunction with the Safety Shutters: permits safe access to the patient exposure area while the synchrotron radiation beam is illuminating the upstream dual energy monochromator; allows a patient to be imaged by the monochromatized beam under the supervision of a Responsible Physician, with scan chair motion and precision shutter actuation regulated by an angiography control computer, while providing a suitable number of safeguards against accidental radiation exposure; has different modes of operation to accommodate equipment set-up, test, and calibration; and patient exposure; and ensures the quick extinction of the beam if a potentially unsafe condition is detected. The interlock system which performs these safety functions is called the Angiography Personnel Protection Interlock (APPI). The APPI Document is organized such that the level of detail changes from a general overview to detailed engineering drawings of the hardware system.

  14. Stanford Synchrotron Radiation Laboratory. Activity report for 1989

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1996-01-01

    The April, 1990 SPEAR synchrotron radiation run was one of the two or three best in SSRL`s history. High currents were accumulated, ramping went easily, lifetimes were long, beam dumps were infrequent and the average current was 42.9 milliamps. In the one month of operation, 63 different experiments involving 208 scientists from 50 institutions received beam. The end-of-run summary forms completed by the experimenters indicated high levels of user satisfaction with the beam quality and with the outstanding support received from the SSRL technical and scientific staffs. These fine experimental conditions result largely from the SPEAR repairs and improvements performed during the past year and described in Section I. Also quite significant was Max Cornacchia`s leadership of the SLAG staff. SPEAR`s performance this past April stands in marked contrast to that of the January-March, 1989 run which is also described in Section I. It is, we hope, a harbinger of the operation which will be provided in FY `91, when the SPEAR injector project is completed and SPEAR is fully dedicated to synchrotron radiation research. Over the coming years, SSRL intends to give highest priority to increasing the effectiveness of SPEAR and its various beam lines. The beam line and facility improvements performed during 1989 are described in Section III. In order to concentrate effort on SSRL`s three highest priorities prior to the March-April run: (1) to have a successful run, (2) to complete and commission the injector, and (3) to prepare to operate, maintain and improve the SPEAR/injector system, SSRL was reorganized. In the new organization, all the technical staff is contained in three groups: Accelerator Research and Operations Division, Injector Project and Photon Research and Operations Division, as described in Section IV. In spite of the limited effectiveness of the January-March, 1989 run, SSRL`s users made significant scientific progress, as described in Section V of this report.

  15. Relativistic parsec-scale jets: II. Synchrotron emission

    Science.gov (United States)

    Pariev, V. I.; Istomin, Ya. N.; Beresnyak, A. R.

    2003-06-01

    We calculate the optically thin synchrotron emission of fast electrons and positrons in a spiral stationary magnetic field and a radial electric field of a rotating relativistic strongly magnetized force-free jet consisting of electron-positron pair plasma. The magnetic field has a helical structure with a uniform axial component and a toroidal component that is maximal inside the jet and decreasing to zero towards the boundary of the jet. Doppler boosting and swing of the polarization angle of synchrotron emission due to the relativistic motion of the emitting volume are calculated. The distribution of the plasma velocity in the jet is consistent with the electromagnetic field structure. Two spatial distributions of fast particles are considered: uniform, and concentrated in the vicinity of the Alfvén resonance surface. The latter distribution corresponds to the regular acceleration by an electromagnetic wave in the vicinity of its Alfvén resonance surface inside the jet. The polarization properties of the radiation have been obtained and compared with the existing VLBI polarization measurements of parsec-scale jets in BL Lac sources and quasars. Our results give a natural explanation of the observed bimodality in the alignment between the electric field vector of the polarized radiation and the projection of the jet axis on the plane of the sky. We interpret the motion of bright knots as a phase velocity of standing spiral eigenmodes of electromagnetic perturbations in a cylindrical jet. The degree of polarization and the velocity of the observed proper motion of bright knots depend upon the angular rotational velocity of the jet. The observed polarizations and velocities of knots indicate that the magnetic field lines are bent in the direction opposite to the direction of the jet rotation.

  16. Disruption of enamel crystal formation quantified by synchrotron microdiffraction.

    Science.gov (United States)

    Al-Jawad, Maisoon; Addison, Owen; Khan, Malik Arshman; James, Alison; Hendriksz, Christian J

    2012-12-01

    To understand the pathology of the ultrastructure of enamel affected by systemic disorders which disrupt enamel tissue formation in order to give insight into the precise mechanisms of matrix-mediated biomineralization in dental enamel in health and disease. Two-dimensional synchrotron X-ray diffraction has been utilized as a sophisticated and useful technique to spatially quantify preferred orientation in mineralized healthy deciduous dental enamel, and the disrupted crystallite organization in enamel affected by a systemic disease affecting bone and dental mineralization (mucopolysaccharidosis Type IVA and Type II are used as examples). The lattice spacing of the hydroxyapatite phase, the crystallite size and aspect ratio, and the quantified preferred orientation of crystallites across whole intact tooth sections, have been determined using synchrotron microdiffraction. Significant differences in mineral crystallite orientation distribution of affected enamel have been observed compared to healthy mineralized tissue. The gradation of enamel crystal orientation seen in healthy tissue is absent in the affected enamel, indicating a continual disruption in the crystallite alignment during mineral formation. This state of the art technique has the potential to provide a unique insight into the mechanisms leading to deranged enamel formation in a wide range of disease states. Characterising crystal orientation patterns and geometry in health and following disruption can be a powerful tool in advancing our overall understanding of mechanisms leading to the tissue phenotypes seen clinically. Findings can be used to inform the appropriate dental management of these tissues and/or to investigate the influence of therapeutic interventions or external stressors which may impact on amelogenesis. Copyright © 2012 Elsevier Ltd. All rights reserved.

  17. Time-resolved photoelectron spectroscopy using synchrotron radiation time structure.

    Science.gov (United States)

    Bergeard, N; Silly, M G; Krizmancic, D; Chauvet, C; Guzzo, M; Ricaud, J P; Izquierdo, M; Stebel, L; Pittana, P; Sergo, R; Cautero, G; Dufour, G; Rochet, F; Sirotti, F

    2011-03-01

    Synchrotron radiation time structure is becoming a common tool for studying dynamic properties of materials. The main limitation is often the wide time domain the user would like to access with pump-probe experiments. In order to perform photoelectron spectroscopy experiments over time scales from milliseconds to picoseconds it is mandatory to measure the time at which each measured photoelectron was created. For this reason the usual CCD camera-based two-dimensional detection of electron energy analyzers has been replaced by a new delay-line detector adapted to the time structure of the SOLEIL synchrotron radiation source. The new two-dimensional delay-line detector has a time resolution of 5 ns and was installed on a Scienta SES 2002 electron energy analyzer. The first application has been to characterize the time of flight of the photoemitted electrons as a function of their kinetic energy and the selected pass energy. By repeating the experiment as a function of the available pass energy and of the kinetic energy, a complete characterization of the analyzer behaviour in the time domain has been obtained. Even for kinetic energies as low as 10 eV at 2 eV pass energy, the time spread of the detected electrons is lower than 140 ns. These results and the time structure of the SOLEIL filling modes assure the possibility of performing pump-probe photoelectron spectroscopy experiments with the time resolution given by the SOLEIL pulse width, the best performance of the beamline and of the experimental station.

  18. Glass transition near the free surface studied by synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Sikorski, M.

    2008-06-15

    A comprehensive picture of the glass transition near the liquid/vapor interface of the model organic glass former dibutyl phthalate is presented in this work. Several surface-sensitive techniques using x-ray synchrotron radiation were applied to investigate the static and dynamic aspects of the formation of the glassy state from the supercooled liquid. The amorphous nature of dibutyl phthalate close to the free surface was confirmed by grazing incidence X-ray diffraction studies. Results from X-ray reflectivity measurements indicate a uniform electron density distribution close to the interface excluding the possibility of surface freezing down to 175 K. Dynamics on sub-{mu}m length-scales at the surface was studied with coherent synchrotron radiation via x-ray photon correlation spectroscopy. From the analysis of the dispersion relation of the surface modes, viscoelastic properties of the dibutyl phthalate are deduced. The Kelvin-Voigt model of viscoelastic media was found to describe well the properties of the liquid/vapor interface below room temperature. The data show that the viscosity at the interface matches the values reported for bulk dibutyl phthalate. The scaled relaxation rate at the surface agrees with the bulk data above 210 K. Upon approaching the glass transition temperature the free surface was observed to relax considerably faster close to the liquid/vapor interface than in bulk. The concept of higher relaxation rate at the free surface is also supported by the results of the quasielastic nuclear forward scattering experiment, during which dynamics on molecular length scales around the calorimetric glass transition temperature is studied. The data were analyzed using mode-coupling theory of the glass transition and the model of the liquid(glass)/vapor interface, predicting inhomogeneous dynamics near the surface. The quasielastic nuclear forward scattering data can be explained when the molecular mobility is assumed to decrease with the increasing

  19. Stanford Synchrotron Radiation Laboratory. Activity report for 1988

    Energy Technology Data Exchange (ETDEWEB)

    Cantwell, K. [ed.

    1996-01-01

    For SSRL operations, 1988 was a year of stark contrasts. The first extended PEP parasitic running since the construction of our two beam lines on that storage ring took place in November and December. Four experiments discussed below, were performed and detailed operational procedures which allowed synchrotron radiation an high energy users to coexist were established. SSRL anticipates that there will be significant amounts of beam time when PEP is run again for high energy physics. On the other hand, activity on SPEAR consisted of brief parasitic running on the VUV lines in December when the ring was operated at 1.85 GeV for colliding beam experiments. There was no dedicated SPEAR running throughout the entire calendar year. This is the first time since dedicated SPEAR operation was initiated in 1980 that there was no such running. The decision was motivated by both cost and performance factors, as discussed in Section 1 of this report. Fortunately, SLAC and SSRL have reached an agreement on SPEAR and PEP dedicated time charges which eliminates the cost volatility which was so important in the cancellation of the June-July dedicated SPEAR run. As discussed in Section 2, the 3 GeV SPEAR injector construction is proceeding on budget and on schedule. The injector will overcome the difficulties associated with the SLC-era constraint of only two injections per day. SSR and SLAC have also embarked on a program to upgrade SPEAR to achieve high reliability and performance. As a consequence, SSRL`s users may anticipate a highly effective SPEAR by 1991, at the latest. At that time, SPEAR is expected to be fully dedicated to synchrotron radiation research and operated by SSRL. Also contained in this report is a discussion of the improvements to SSRL`s experimental facilities and highlights of the experiments of the past year.

  20. Low-frequency radio constraints on the synchrotron cosmic web

    Science.gov (United States)

    Vernstrom, T.; Gaensler, B. M.; Brown, S.; Lenc, E.; Norris, R. P.

    2017-06-01

    We present a search for the synchrotron emission from the synchrotron cosmic web by cross-correlating 180-MHz radio images from the Murchison Widefield Array with tracers of large-scale structure (LSS). We use two versions of the radio image covering 21.76° × 21.76° with point sources brighter than 0.05 Jy subtracted, with and without filtering of Galactic emission. As tracers of the LSS, we use the Two Micron All-Sky Survey and the Wide-field InfraRed Explorer redshift catalogues to produce galaxy number density maps. The cross-correlation functions all show peak amplitudes at 0°, decreasing with varying slopes towards zero correlation over a range of 1°. The cross-correlation signals include components from point source, Galactic, and extragalactic diffuse emission. We use models of the diffuse emission from smoothing the density maps with Gaussians of sizes 1-4 Mpc to find limits on the cosmic web components. From these models, we find surface brightness 99.7 per cent upper limits in the range of 0.09-2.20 mJy beam-1 (average beam size of 2.6 arcmin), corresponding to 0.01-0.30 mJy arcmin-2. Assuming equipartition between energy densities of cosmic rays and the magnetic field, the flux density limits translate to magnetic field strength limits of 0.03-1.98 μG, depending heavily on the spectral index. We conclude that for a 3σ detection of 0.1 μG magnetic field strengths via cross-correlations, image depths of sub-mJy to sub-μJy are necessary. We include discussion on the treatment and effect of extragalactic point sources and Galactic emission, and next steps for building on this work.

  1. THE COURSE OF TRANSLATION AND INTERPRETATION PUBLICATIONS OF BRAZILIAN SIGN LANGUAGE IN SOME BRAZILIAN TRANSLATION JOURNALS

    Directory of Open Access Journals (Sweden)

    Silvana Aguiar dos Santos

    2016-07-01

    Full Text Available This essay describes and analyses the course of publications about Translation and Interpretation of Brazilian sign language in some Brazilian Translation journals. Results show a sum of 36 works published, distributed over Translation journals of different regions of Brazil. The established subjects and the ones that emerged from 1990 to 2014 were also examined in these publications.

  2. Influence of filling pattern structure on synchrotron radiation and beam spectrum at ANKA

    Energy Technology Data Exchange (ETDEWEB)

    Steinmann, Johannes; Brosi, Miriam; Bruendermann, Erik; Caselle, Michele; Blomley, Edmund; Hiller, Nicole; Kehrer, Benjamin; Mueller, Anke-Susanne; Schoenfeldt, Patrik; Schuh, Marcel; Schwarz, Markus; Siegel, Michael [Karlsruher Institut fuer Technologie, Karlsruhe (Germany)

    2016-07-01

    We present the effects of the filling pattern structure in multi-bunch mode on the beam spectrum. This effects can be seen by all detectors whose resolution is better than the RF frequency, ranging from stripline and Schottky measurements to high resolution synchrotron radiation measurements. Our heterodyne measurements of the emitted coherent synchrotron radiation at 270 GHz reveal the discrete frequency harmonics around the 100'000 revolution harmonic of ANKA, the synchrotron radiation facility in Karlsruhe, Germany. Significant effects of bunch spacing, gaps between bunch trains and variations in individual bunch currents on the emitted CSR spectrum are described by theory and supported by observations.

  3. Synchrotron light source data book: Version 4, Revision 05/96

    Energy Technology Data Exchange (ETDEWEB)

    Murphy, J.B.

    1996-05-01

    This book is as its name implies a collection of data on existing and planned synchrotron light sources. The intention was to provide a compendium of tools for the design of electron storage rings as synchrotron radiation sources. The slant is toward the accelerator physicist as other booklets such as the X-Ray Data Booklet address the use of synchrotron radiation. It is hoped that the booklet serves as a pocket sized reference to facilitate back of the envelope type calculations. It contains some useful formulae in practical units and a brief description of many of the existing and planned light source lattices.

  4. Metal quantification in water and sediment samples of billings reservoir by SR-TXRF

    Energy Technology Data Exchange (ETDEWEB)

    Sampaio, Sergio Arnaud; Moreira, Silvana [Universidade Estadual de Campinas (UNICAMP), Campinas, SP (Brazil). Faculdade de Engenharia Civil, Arquitetura e Urbanismo]. E-mails: silvana@fec.unicamp.br; sergioarnaud@hotmail.com; Vives, Ana Elisa Sirito de [Universidade Metodista de Piracicaba (UNIMEP), Santa Barbara D' Oeste, SP (Brazil). Faculdade de Engenharia Civil, Arquitetura e Urbanismo]. E-mail: aesvives@unimep.br

    2007-07-01

    Billings is the largest reservoir water of the metropolitan Sao Paulo area, with approximately 100km{sup 2} of water. Its basin hydrographic occupies more than 500km{sup 2} in six cities. It concentrates the largest industrial park of South America and only its margins are busy for almost a million inhabitants. The quality of its waters is, therefore, constant of concern of the whole society. In this work the Synchrotron Radiation Total Reflection X Ray Fluorescence (SR-TXRF) is applied for the identification and quantification of metals in waters and sediments of the Billings dam. A comparison of the levels of metals found with the maximum permissive limits established by the Brazilian legislation was made. The purpose of social context is to contribute for the preservation of the local springs and the rational use of its waters. For the field work they were chosen 19 collection points, included the margins and the central portion of the dam, in agreement with similar approaches the those adopted by the Company of Technology of Environmental Sanitation of Sao Paulo State (CETESB).The water and sediment samples, as well as the certified and standard samples, were analyzed at Brazilian Synchrotron Light Laboratory (LNLS), Campinas, SP, Brazil. Results indicate that the water and the sediments of the reservoir have concentrations above the legal limits. (author)

  5. Permeability measuremens of brazilian Eucalyptus

    Directory of Open Access Journals (Sweden)

    Marcio Rogério da Silva

    2010-09-01

    Full Text Available The permeability of Brazilian Eucalyptus grandis and Eucalyptus citriodora wood was measured in a custom build gas analysis chamber in order to determine which species could be successfully treated with preservatives. Liquid permeability was tested using an emulsion of Neen oil and a control of distillated water. Air was used to test the gas phase permeability. For both Eucalyptus grandis and Eucalyptus citriodora, the longitudinal permeability of gas was shown to be about twice as great as the liquid phase permeability. No radial permeability was observed for either wood. The permeability of air and water through the sapwood of Eucalyptus grandis was greater than that through the sapwood of Eucalyptus citriodora. The permeability of neen oil preservative through the sapwood of Eucalyptus grandis was also greater than through the sapwood of E. Citradora, but the difference was not statistically significant. Scanning Electron Microscopy images showed that the distribution and obstruction in the vessels could be correlated with observed permeability properties. Irrespective of the causes of differences in permeability between the species, the fluid phase flux through the sapwood of both species was significant, indicating that both Eucalyptus grandis and Eucalyptus citriodora could be successfully treated with wood preservative.

  6. Group dialogue empowers Brazilian women.

    Science.gov (United States)

    Badiani, R; Becker, J

    1995-11-01

    In response to an alarming rise in human immunodeficiency virus (HIV) infection among Brazilian women during the early 1990s, the Sociedade Civil Bem-Estar Familiar no Brazil (BEMFAM) developed a project that integrates HIV prevention with clinical services, community-based prevention activities, and sexually transmitted disease diagnosis and treatment. Preliminary interviews with clinic clients revealed that women's fears they would be considered unfaithful were impeding their ability to suggest condom use to their sexual partners. Condom use within a relationship was considered appropriate only for pregnancy prevention. To facilitate dialogue about sexual health, BEMFAM developed a women's group intervention project. All women who attend a BEMFAM clinic are invited to participate in a one-hour group discussion before receiving medical services. Novela-style booklets with stories and characters women can relate to their own lives are used to stimulate discussion. Participants learn to use condoms correctly by putting them on a penis model and anticipate situations in which they would be able to negotiate condom use. The group setting enables women to gain confidence and practice assertiveness in a non-threatening, supportive environment. Their identification with other women's stories empowers women to take control of their health and sexual lives. Between October 1994 and July 1995, 3464 women participated in group discussions organized by BEMFAM and 40,688 condoms were distributed; 18% of these women returned to the clinic for additional condoms.

  7. Brazilian Cerrado Soil Actinobacteria Ecology

    Directory of Open Access Journals (Sweden)

    Monique Suela Silva

    2013-01-01

    Full Text Available A total of 2152 Actinobacteria strains were isolated from native Cerrado (Brazilian Savannah soils located in Passos, Luminárias, and Arcos municipalities (Minas Gerais State, Brazil. The soils were characterised for chemical and microbiological analysis. The microbial analysis led to the identification of nine genera (Streptomyces, Arthrobacter, Rhodococcus, Amycolatopsis, Microbacterium, Frankia, Leifsonia, Nakamurella, and Kitasatospora and 92 distinct species in both seasons studied (rainy and dry. The rainy season produced a high microbial population of all the aforementioned genera. The pH values of the soil samples from the Passos, Luminárias, and Arcos regions varied from 4.1 to 5.5. There were no significant differences in the concentrations of phosphorus, magnesium, and organic matter in the soils among the studied areas. Samples from the Arcos area contained large amounts of aluminium in the rainy season and both hydrogen and aluminium in the rainy and dry seasons. The Actinobacteria population seemed to be unaffected by the high levels of aluminium in the soil. Studies are being conducted to produce bioactive compounds from Actinobacteria fermentations on different substrates. The present data suggest that the number and diversity of Actinobacteria spp. in tropical soils represent a vast unexplored resource for the biotechnology of bioactives production.

  8. Aflatoxins in Brazilian Peanut Confection.

    Science.gov (United States)

    2016-04-07

    The study's objectives were to evaluate a method for the determination of aflatoxins (AFs) in the Brazilian peanut confection "Paçoca" and to apply the method in investigating AF concentrations in Paçoca marketed in São Paulo State throughout 2013. Results of another survey conducted between 1994 and 2002 with another method were also reported. The current method consists of immunoaffinity column cleanup, LC with postcolumn derivatization for AF fluorescence enhancement, and fluorescence determination for the toxins. The mean recovery and mean RSD r values were 88.6 and 7.9%, respectively. The LODs for aflatoxin B 1 , aflatoxin B 2 , aflatoxin G 1 , and aflatoxin G 2 were 0.04, 0.01, 0.02, and 0.01 ng/g; and the LOQs were 0.15, 0.04, 0.07, and 0.04 ng/g, respectively. Results of the two survey studies indicate that the contamination of AFs in Paçoca remains a public health problem. In the 2013 survey, 71 of 100 samples (71%) had AFs contamination ranging from 0.3 to 41.8 ng/g, with 12 samples (12%) containing >20 ng/g of the toxins, whereas in the 1994-2002 survey, 73 of 150 samples (51%) had AFs contamination ranging from 9 to 1439 ng/g with 65 samples (45%) containing levels >20 ng/g.

  9. Case Study: Brazilian Virtual Herbarium

    Directory of Open Access Journals (Sweden)

    Cameron Neylon

    2017-10-01

    Full Text Available The Brazilian Virtual Herbarium (BVH is a project of the Brazillian Centro de Referência em Informação Ambiental (CRIA that has been running since 2009. The Virtual Herbarium provides an infrastructure that gathers digital records of plant specimens from primary source, mainly in Brazil, and makes them available through a central web portal. The source herbaria have complete control over what data is made through the portal and the data collected by BVH is made fully available. BVH in common with many data infrastructures, faces challenges in retaining funding. Most funding sources are project based and as has been noted elsewhere this creates problems for the sustaining of infrastructures. BVH therefore has an interest in demonstrating the use of the data resources it hosts. Through the OCSDNet project it has strengthened its capacity in this area to develop tools showing its wide usage. Overall the BVH hosts over eight million records (as of October 2017 and received 70 billion data requests in October 2017. Its users are mainly in Brazil but there is also substantial global usage. The primary uses are for research and education. There are a broad range of educational users, including universities but also schools. Through providing a central aggregation and access point BHV provides a data infrastructure that is greater – and more useful – than the sum of its parts.

  10. Educating Brazilian workers about AIDS.

    Science.gov (United States)

    1991-12-01

    This article contains a the script for a slide-tape presentation entitled Working Against AIDS, a presentation developed by the Brazil Family Planning Association (BEMFAM) which is designed to debunk common misconceptions about the disease. This audio-visual, which targets Brazilian workers, can be used during talks, seminars, and meetings. A discussion of the issues involved usually follows the presentation of Working Against AIDS. The presentation contains 30 illustrated slides (these are included in the article). The presentation begins by explaining that much of the information concerning AIDS is prejudicial and misleading. The next few slides point out some of the common misconceptions about AIDS, such as claims denying the existence of the disease, or suggestions that only homosexuals and prostitutes are at risk. The presentation then goes on to explain the ways in which the virus can and cannot be transmitted. Then it discusses how the virus destroys the body's natural defenses and explains the ensuing symptoms. Slides 14 and 15 point out that no cure yet exists for AIDS, making prevention essential. Slides 16-23 explain what actions are considered to be high risk and which ones do not entail risk. Noting that AIDS can be prevented, slide 24 says that the disease should not present an obstacle to spontaneous manifestations of human relations. The next slide explains that condoms should always be used when having sex with someone who could be infected with AIDS. Finally slides 26-30 demonstrate the proper way to use and dispose of a condom.

  11. Brazilian Cerrado soil Actinobacteria ecology.

    Science.gov (United States)

    Suela Silva, Monique; Naves Sales, Alenir; Teixeira Magalhães-Guedes, Karina; Ribeiro Dias, Disney; Schwan, Rosane Freitas

    2013-01-01

    A total of 2152 Actinobacteria strains were isolated from native Cerrado (Brazilian Savannah) soils located in Passos, Luminárias, and Arcos municipalities (Minas Gerais State, Brazil). The soils were characterised for chemical and microbiological analysis. The microbial analysis led to the identification of nine genera (Streptomyces, Arthrobacter, Rhodococcus, Amycolatopsis, Microbacterium, Frankia, Leifsonia, Nakamurella, and Kitasatospora) and 92 distinct species in both seasons studied (rainy and dry). The rainy season produced a high microbial population of all the aforementioned genera. The pH values of the soil samples from the Passos, Luminárias, and Arcos regions varied from 4.1 to 5.5. There were no significant differences in the concentrations of phosphorus, magnesium, and organic matter in the soils among the studied areas. Samples from the Arcos area contained large amounts of aluminium in the rainy season and both hydrogen and aluminium in the rainy and dry seasons. The Actinobacteria population seemed to be unaffected by the high levels of aluminium in the soil. Studies are being conducted to produce bioactive compounds from Actinobacteria fermentations on different substrates. The present data suggest that the number and diversity of Actinobacteria spp. in tropical soils represent a vast unexplored resource for the biotechnology of bioactives production.

  12. Dominance of foreign citations in Brazilian orthopedics journals.

    Science.gov (United States)

    Teixeira, Renan Kleber Costa; Yamaki, Vitor Nagai; Rosa, Rita de Cássia Rodrigues; de Barros, Rui Sergio Monteiro; Botelho, Nara Macedo

    2014-01-01

    To evaluate whether there is any preference for citing journals from other countries to the detriment of Brazilian journals, in three Brazilian orthopedics journals. All the references of articles published in 2011 by the journals Acta Ortopédica Brasileira, Coluna/Columna and Revista Brasileira de Ortopedia were evaluated to as certain how many of these came from Brazilian journals and how many from foreign journals. 3813 references distributed among 187 articles were analyzed. Out of this total, 306 (8.02%) were from Brazilian journals. There was no difference between the three journals analyzed. There were 76 articles (40.64%) without any citations of articles in Brazilian journals and only two articles (1%) cited more Brazilian articles than articles published elsewhere. There is a need for Brazilian researchers to cite articles from Brazilian journals more often.

  13. Brazilian Review of Finance 2013 Editorial Report

    Directory of Open Access Journals (Sweden)

    Ricardo Pereira Câmara Leal

    2014-06-01

    Full Text Available RBFin is the main Brazilian publication outlet of academic papers about finance. The contents of the Review are open and online with a printed version distributed to members of the Brazilian Finance Society. Using the Open Journals System to manage the editorial process, publication of RBFin adheres to a strict publication schedule. The Review is indexed by EconLit, RedALyC, Google Scholar, Gale, Proquest and Ebsco and is listed in the JEL, DOAJ, Latindex, OpenJGate, and Cabell's directories. RBFin is rated B1 in the business area of the Brazilian classification system and B2 in Economics. The editorial board undergoes partial turnover every year and comprises 19 individuals from four countries, the Brazilian members being affiliated with universities in five different Brazilian states. The acceptance rate was 27% for papers submitted in 2012, the most recent year in which all submissions have already received a final decision. The average number of days between receipt and acceptance for articles submitted in 2013 was 203. The worst case was 361 days. The average number of days between receipt and publication was 294. The worst case was 575 days. Fifty-three individuals served as reviewers in 2013.

  14. Global power and Brazilian nuclear decisions

    Energy Technology Data Exchange (ETDEWEB)

    Metri, Paulo, E-mail: pmetri@terra.com.br [Clube de Engenharia, Rio de Janeiro, RJ (Brazil)

    2017-07-01

    Brazilian society declares no intention to development a nuclear artifact. This is on its Constitution. The submarine of nuclear propulsion may be used as a weapon of defense and, therefore, has a peaceful objective. Nationalism must be applied only to benefit the society. Nationalist attention has always been devoted, at various occasions, to the Brazilian nuclear sector. However, since Brazilian society has many needs and the Brazilian government always had numerous energy options, this sector has not been developed as it could be. Other successful applications of nuclear technology, besides electric generation, are not considered here. At present, the country is experiencing a moment of harassment of liberal forces. It is difficult to know if the population understands what is going on, due to the traditional media control. This media belongs to the capital. The rise and the fall of the nationalist strand in a country follow a global tendency and also depend of actions of the international capital. In nationalist periods, more decisions with positive social impact are taken. Therefore, sovereignty is necessary to increase the benefits to society. Unfortunately, the Brazilians deceived by the companies of mass communication and corrupt political leaderships allow the country to be dominated. Even the armed forces had their projects paralyzed. The nuclear sector, as all other, suffers with the low budget and the future is difficult to predict. (author)

  15. Citizenship and decoloniality in Brazilian education

    Directory of Open Access Journals (Sweden)

    Viviane Conceição Antunes

    2014-08-01

    Full Text Available Reflecting on the importance of multiculturalism in teaching process and observing the otherness are primarily a challenge. This enables us to rethink what we have within ourselves, also to reconstitute memories involving discriminatory and unethical attitudes, which takes place in social fellowship. Based on the studies of Walsh (2007, 2009, Gomes (2007 and Tavares (2011, this work relies on decoloniality studies, mainly on the relevance of the history of Africa and Africanness in Brazilian education. Our corpus of analysis is found in the "Diretrizes Curriculares Nacionais para a Educação Básica" (DCN, 2013, the Brazilian Legislative Syllabus for Basic Education. Our focus is on the chapters concerning the Native-Brazilian and Quilomboa Education and ethnic-racial relations. Our most important aims are: to show the intercultural theoretical framework in which they are based on; to understand the immediate link established between the Native-Brazilian education and intercultural perspective; to clarify how the African diaspora was carried out in this particular case. Based on some Excel resources we were able to: 1 stablish the predominance of functional framework of interculturalism throughout these chapters, along with some critical features of interculturalism, as the issue of curricular decoloniality; 2 observe the established relationship between bilingualism and multiculturalism in the guidelines of Native-Brazilian education; and 3 identify a search for an effective inclusion of Africanness in curricula supported by the historical recognition and visibility of their sociocultural contribution.

  16. FT-IR microscopical analysis with synchrotron radiation: The microscope optics and system performance

    Energy Technology Data Exchange (ETDEWEB)

    Reffner, J.A.; Martoglio, P.A. [Spectra-Tech, Inc., Shelton, CT (United States); Williams, G.P. [Brookhaven National Lab., Upton, NY (United States)

    1995-01-01

    When a Fourier transform infrared (FT-IR) microspectrometer was first interfaced with the National Synchrotron Light Source (NSLS) in September 1993, there was an instant realization that the performance at the diffraction limit had increased 40-100 times. The synchrotron source transformed the IR microspectrometer into a true IR microprobe, providing high-quality IR spectra for probe diameters at the diffraction limit. The combination of IR microspectroscopy and synchrotron radiation provides a powerful new tool for molecular spectroscopy. The ability to perform IR microspectroscopy with synchrotron radiation is still under development at Brookhaven National Laboratory, but several initial studies have been completed that demonstrate the broad-ranging applications of this technology and its potential for materials characterization.

  17. Safety Analysis Report: X17B2 beamline Synchrotron Medical Research Facility

    Energy Technology Data Exchange (ETDEWEB)

    Gmuer, N.F.; Thomlinson, W.

    1990-02-01

    This report contains a safety analysis for the X17B2 beamline synchrotron medical research facility. Health hazards, risk assessment and building systems are discussed. Reference is made to transvenous coronary angiography. (LSP)

  18. Preliminary results from the prototype synchrotron radiation detector on space shuttle mission STS-108

    Energy Technology Data Exchange (ETDEWEB)

    Anderhub, H.; Bates, J.R.; Baetzner, D.; Baumgartner, S.; Biland, A. E-mail: biland@particle.phys.ethz.ch; Camps, C.; Capell, M.; Commichau, V.; Djambazov, L.; Fanchiang, Y.-J.; Fluegge, G.; Fritschi, M.; Grimm, O.; Hangarter, K.; Hofer, H.; Horisberger, U.; Kan, R.; Kaestli, W.; Kenney, G.P.; Kim, G.N.; Kim, K.S.; Koutsenko, V.; Kraeber, M.; Kuipers, J.; Lebedev, A.; Lee, M.W.; Lee, S.-C.; Lewis, R.; Lustermann, W.; Pauss, F.; Rauber, T.; Ren, D.; Ren, Z.L.; Roeser, U.; Son, D.; Ting, Samuel C.C.; Tiwari, A.N.; Viertel, G.M.; Gunten, H. von; Wicki, S. Waldmeier; Wang, T.-S.; Yang, J.; Zimmermann, B

    2002-12-01

    A Synchrotron Radiation Detector measures synchrotron radiation emitted by high energetic particles in the earth magnetic field. This allows to identify cosmic ray electrons and positrons with energies in the TeV region. One possibility for such a detector outside the atmosphere uses YAP crystals to measure synchrotron photons with energies in the keV range. As such a detector can not distinguish between photons and electrons, the main problems are the diffuse cosmic ray gamma background and low energetic electrons in the vicinity of the earth. While the intensity of the diffuse gamma rays is known quite well, there exists limited knowledge about keV-electrons in low earth orbits. To measure these electrons a Prototype Synchrotron Radiation Detector (PSRD) was flown with Space Shuttle mission STS-108 (Dec.2001) and preliminary analysis of the data show very favorable results.

  19. Experimental investigations of synchrotron radiation at the onset of the quantum regime

    DEFF Research Database (Denmark)

    Andersen, Kristoffer; Uggerhøj, Ulrik Ingerslev

    the magnetic field is comparable to the critical field, quantum corrections are essential for the description of synchrotron radiation to conserve energy. With electrons of energies 10-150 GeV penetrating a germanium single crystal along the axis, we have experimentally investigated the transition from......The classical description of synchrotron radiation fails at large Lorentz factors for relativistic electrons crossing strong transverse magnetic fields. In the rest frame of the electron this field is comparable to the so-called critical field of 4.414*109 T. When the Lorentz factor times...... the regime where classical synchrotron radiation is an adequate description, to the regime where the emission drastically changes character; not only in magnitude, but also in spectral shape. The spectrum can only be described by quantum synchrotron radiation formulas. Apart from being a test of strong...

  20. Experimental investigations of synchrotron radiation at the onset of the quantum regime

    DEFF Research Database (Denmark)

    Andersen, Kristoffer; Knudsen, Helge; Uggerhøj, Ulrik Ingerslev

    2012-01-01

    = \\gamma B/B_0 \\simeq 1$ quantum corrections are essential for the description of synchrotron radiation to conserve energy. With electrons of energies 10-150 GeV penetrating a germanium single crystal along the $\\langle110\\rangle$ axis, we have experimentally investigated the transition from the regime......The classical description of synchrotron radiation fails at large Lorentz factors, $\\gamma$, for relativistic electrons crossing strong transverse magnetic fields $B$. In the rest frame of the electron this field is comparable to the so-called critical field $B_0 = 4.414\\cdot10^9$ T. For $\\chi...... where classical synchrotron radiation is an adequate description, to the regime where the emission drastically changes character; not only in magnitude, but also in spectral shape. The spectrum can only be described by quantum synchrotron radiation formulas. Apart from being a test of strong...

  1. Development of compact synchrotron light source LUNA for x-ray lithography

    Science.gov (United States)

    Takahashi, M.; Mandai, S.; Hoshi, Y.; Kohno, Y.

    1992-01-01

    A compact synchrotron light source LUNA has been developed by Ishikawajima-Harima Heavy Industries Co., Ltd. (IHI), especially for x-ray lithography. It consists of a 45-MeV linac as an electron injector and an 800-MeV synchrotron. The peak wavelength of synchrotron radiation is around 10 Å. The installation of LUNA was completed in April 1989 at the Tsuchiura Facility of IHI. The synchrotron radiation was first observed in December 1989. A stored beam current of 50 mA at 800 MeV and a lifetime over 1 h have been achieved. At present, experiments are still continuing to increase the stored current and the lifetime. X-ray lithography testing is scheduled to begin in a clean room in this facility. This paper describes the outline of LUNA and the present status.

  2. National synchrotron light source. [Annual report], October 1, 1992--September 30, 1993

    Energy Technology Data Exchange (ETDEWEB)

    Rothman, E.Z.; Hulbert, S.L.; Lazarz, N.M. [eds.

    1994-04-01

    This report contains brief discussions on the research being conducted at the National Synchrotron Light source. Some of the topics covered are: X-ray spectroscopy; nuclear physics; atomic and molecular science; meetings and workshops; operations; and facility improvements.

  3. Design and Optimisation Strategies of Nonlinear Dynamics for Diffraction Limited Synchrotron Light Source

    CERN Document Server

    Bartolini, R.

    2016-01-01

    This paper introduces the most recent achievements in the control of nonlinear dynamics in electron synchrotron light sources, with special attention to diffraction limited storage rings. Guidelines for the design and optimization of the magnetic lattice are reviewed and discussed.

  4. Elemental changes in hemolymph and urine of Rhodnius prolixus induced by in-vivo exposure to mercury: A study using synchrotron radiation total reflection X-ray fluorescence

    Energy Technology Data Exchange (ETDEWEB)

    Mantuano, Andrea, E-mail: mantuanoandrea@gmail.com [Physics Institute, State University of Rio de Janeiro (Brazil); Pickler, Arissa; Barroso, Regina C. [Physics Institute, State University of Rio de Janeiro (Brazil); Almeida, Andre P. de; Braz, Delson [Nuclear Engineering Program, Federal University of Rio de Janeiro (Brazil); Cardoso, Simone C. [Physics Institute, Federal University of Rio de Janeiro (Brazil); Gonzalez, Marcelo S. [Department of General Biology, Fluminense Federal University (Brazil); Figueiredo, Marcela B.; Garcia, Eloi S.; Azambuja, Patricia [Laboratory of Biochemistry and Physiology of Insects, Oswaldo Cruz Foundation (Brazil)

    2012-05-15

    In recent years, the effects of pollution on the health of humans and other vertebrates were extensively studied. However, the effects on some invertebrates are comparatively unknown. Recent studies have demonstrated that toxic metals interfere with the reproduction, development and immune defenses of some terrestrial and marine invertebrates. Some environmental conditions including pollution produce chronic and acute effects on different animal's organs and systems. In this work, we investigated changes in the concentrations of Cl, K, Ca, Fe and Zn in Rhodnius prolixus as insect model. The elements were quantified using urine and hemolymph samples collected on different days after feeding the insects with blood containing HgCl{sub 2}. The synchrotron radiation total reflection X-ray fluorescence measurements were carried at the X-ray fluorescence beamline facility in Brazilian Synchrotron Light Laboratory. The observation reveals that the calcium level was higher in the hemolymph than in urine. On the other hand, the urine collected from insects treated with HgCl{sub 2} showed higher level of Cl than hemolymph samples. Ca, Fe and Zn concentrations decrease drastically in urine samples collected after 2 days of HgCl{sub 2} treatment. The regulation of triatomines excretion was discussed pointing out the importance of trace elements. - Highlights: Black-Right-Pointing-Pointer Changes in Cl, K, Ca, Fe and Zn contents in Rhodnius prolixus were evaluated. Black-Right-Pointing-Pointer In triatomines these elements have not been previously described. Black-Right-Pointing-Pointer Cl, Ca, Zn levels were lower than control in hemolymph after 5 days of HgCl{sub 2} fed. Black-Right-Pointing-Pointer Cl, Ca, Zn levels were higher than control in urine after 2 days of HgCl{sub 2} fed.

  5. Evaluation of growth tree rings of Tipuana Tipu as biomonitoring of environmental pollution by synchrotron radiation total reflection X-ray fluorescence

    Energy Technology Data Exchange (ETDEWEB)

    Moreira, Silvana; Geraldo, Simoni Michetti; Canteras, Felippe Benavente, E-mail: silvana@fec.unicamp.br, E-mail: felippe.canteras@gmail.com [Universidade Estadual de Campinas (FEC/UNICAMP), Campinas, SP (Brazil). Dept. de Saneamento e Ambiente

    2013-07-01

    The bioindicators, plants or animals capable to present qualitative and/or quantitative answers, when exposed to pollutant substances. Trees record and incorporate in their log, developed year after year, the impressions of the environment, becoming possible the study of the different environmental changes, including contamination, that have occurred over the life of these trees. The selected species, Tipuana Tipu, of the Leguminosae family, is native of Argentina and Bolivia and was introduced in Brazil as an ornamental plant. It is one of the most common trees in the urban landscaping in Sao Paulo city. The present project has as main objective the determination of the content of potentially toxic elements in samples of growth the tree rings of Tipuana Tipu, previously dated, collected in strategically locations of Sao Paulo, using Synchrotron Radiation Total Reflection X-Ray Fluorescence. Samples were also collected in the Piracicaba (SP), local of little access and small flow traffic. The SR-TXRF analysis was carried out in the X-ray Fluorescence Beamline at the Brazilian Synchrotron Light Source Laboratory, located in Campinas city, Sao Paulo State, Brazil. Some trace elements present concentrations higher than considered as normal in some periods. In this paper the highest value for Pb was 123.54 μg.g{sup -1} considered as threshold value was observed for the period 1998 to 2000 for University of Sao Paulo, Butanta site. For the same period excessive level was also observed for samples collected in Piracicaba city. In Sao Paulo city, sample collected in the campus of University of Sao Paulo (Butanta), showed the highest toxicity, with concentration above the tolerable limit for Ti, Cr and Cu. For the samples collected in Piracicaba city the concentrations of Cr, Ni, Cu, and Pb exceeding the toxicity limits. (author)

  6. The Brazilian national system of forest permanent plots

    Science.gov (United States)

    Yeda Maria Malheiros de Oliveira; Maria Augusta Doetzer Rosot; Patricia Povoa de Mottos; Joberto Veloso de Freitas; Guilherme Luis Augusto Gomide; < i> et al< /i>

    2009-01-01

    The Brazilian National System of Forest Permanent Plots (SisPP) is a governmental initiative designed and being implemented in partnership by the Ministry of Environment (MMA), represented by the National Forest Programme (PNF) and the Brazilian Forest Service (SFB) and the Embrapa Forestry (a research center of the Brazilian Agricultural Research Corporation - Embrapa...

  7. Variable Magnification With Kirkpatrick-Baez Optics for Synchrotron X-Ray Microscopy

    OpenAIRE

    Jach, Terrence; Bakulin, Alex S.; Durbin, Stephen M.; Pedulla, Joseph; Macrander, Albert

    2006-01-01

    We describe the distinction between the operation of a short focal length x-ray microscope forming a real image with a laboratory source (convergent illumination) and with a highly collimated intense beam from a synchrotron light source (K?hler illumination). We demonstrate the distinction with a Kirkpatrick-Baez microscope consisting of short focal length multilayer mirrors operating at an energy of 8 keV. In addition to realizing improvements in the resolution of the optics, the synchrotron...

  8. Coherent and incoherent components of a synchrotron radiation spot produced by separate capillaries

    Energy Technology Data Exchange (ETDEWEB)

    Dabagov, S.B.; Murashova, V.A.; Fedorchuk, R.V.; Yakimenko, M.N. [P.N., Lebedev Physical Institute, Ras, Moscow (Russian Federation); Istituto Nazionale di Fisica Nucleare, Frascati, (Italy). Laboratori Nazionali di Frascati; Marcelli, A; Svyatoslavsky, N.L. [Center for Photochemistry, Ras, Moscow (Russian Federation)

    1999-07-01

    In this work the focusing properties of soft X-ray synchrotron radiation by separate capillaries are discussed. It is shown that a not negligible fraction of the synchrotron radiation beam transmitted by the capillary has a mode representation. Experimental and theoretical data are discussed to explain the superposition pattern of the X-rays in the focal plane due to the interference phenomena of electromagnetic radiation propagating through separate capillaries.

  9. My Precious! the location and diffusion of scientific research: evidence from the synchrotron diamond light source

    OpenAIRE

    Christian Helmers; Henry G. Overman

    2013-01-01

    We analyze the impact of the establishment of a GBP 380 million basic scientific research facility in the UK on the geographical distribution of related research. We investigate whether the siting of the Diamond Light Source, a 3rd generation synchrotron light source, in Oxfordshire induced a clustering of related research in its geographic proximity. To account for the potentially endogenous location choice of the synchrotron, we exploit the availability of a `runner-up' site near Manchester...

  10. Novel portable press for synchrotron time-resolved 3-D micro-imagining under extreme conditions

    Energy Technology Data Exchange (ETDEWEB)

    Philippe, J.; Le Godec, Y., E-mail: yann.legodec@impmc.upmc.fr; Bergame, F.; Morand, M. [IMPMC, Université Pierre et Marie Curie, Paris (France); Mezouar, M.; Bauchau, S.; Alvarez-Murga, M. [European Synchrotron Radiation Facility, Grenoble (France); Perrillat, J. P. [Laboratoire de Géologie de Lyon, Université Claude Bernard Lyon1, Lyon (France); Bromiley, G.; Berg, M. [School of GeoSciences, University of Edinburgh, Edinburgh (United Kingdom); King, A.; Guignot, N.; Itié, J. P. [Synchrotron SOLEIL, St Aubin France (France); Atwood, Robert [Diamond Light Source Ltd., Harwell Science and Innovation Campus, Didcot (United Kingdom)

    2016-07-27

    Here we present the instrumental development to extend the synchrotron X-ray microtomography techniques to in situ studies under static compression (HP) or shear stress or the both conditions at high temperatures (HT). To achieve this, a new rotating tomography Paris-Edinburgh cell (rotoPEc) has been developed. This ultra-compact portable device, easily and successfully adapted to various multi-modal synchrotron experimental set-up at ESRF, SOLEIL and DIAMOND is explained in detail.

  11. [Brazilian Consensus on Chagas Disease, 2015].

    Science.gov (United States)

    Dias, João Carlos Pinto; Ramos, Alberto Novaes; Gontijo, Eliane Dias; Luquetti, Alejandro; Shikanai-Yasuda, Maria Aparecida; Coura, José Rodrigues; Torres, Rosália Morais; Melo, José Renan da Cunha; Almeida, Eros Antonio de; Oliveira, Wilson de; Silveira, Antônio Carlos; Rezende, Joffre Marcondes de; Pinto, Fabiane Scalabrini; Ferreira, Antonio Walter; Rassi, Anis; Fragata, Abílio Augusto; Sousa, Andréa Silvestre de; Correia, Dalmo; Jansen, Ana Maria; Andrade, Glaucia Manzan Queiroz; Britto, Constança Felícia De Paoli de Carvalho; Pinto, Ana Yecê das Neves; Rassi, Anis; Campos, Dayse Elisabeth; Abad-Franch, Fernando; Santos, Silvana Eloi; Chiari, Egler; Hasslocher-Moreno, Alejandro Marcel; Moreira, Eliane Furtado; Marques, Divina Seila de Oliveira; Silva, Eliane Lages; Marin-Neto, José Antonio; Galvão, Lúcia Maria da Cunha; Xavier, Sergio Salles; Valente, Sebastião Aldo da Silva; Carvalho, Noêmia Barbosa; Cardoso, Alessandra Viana; Silva, Rafaella Albuquerque E; Costa, Veruska Maia da; Vivaldini, Simone Monzani; Oliveira, Suelene Mamede; Valente, Vera da Costa; Lima, Mayara Maia; Alves, Renato Vieira

    2016-06-01

    Chagas disease is a neglected chronic condition that presents high morbidity and mortality burden, with considerable psychological, social, and economic impact. The disease represents a significant public health issue in Brazil, with different regional patterns. This document presents the evidence that resulted in the Brazilian Consensus on Chagas Disease. The objective was to review and standardize strategies for diagnosis, treatment, prevention, and control of Chagas disease in the country, based on the available scientific evidence. The consensus is based on collaboration and contribution of renowned Brazilian experts with vast knowledge and experience on various aspects of the disease. It is the result of close collaboration between the Brazilian Society of Tropical Medicine and the Ministry of Health. This document shall strengthen the development of integrated control measures against Chagas disease in the country, focusing on epidemiology, management, comprehensive care (including families and communities), communication, information, education, and research.

  12. Efficient computation of coherent synchrotron radiation in a rectangular chamber

    Directory of Open Access Journals (Sweden)

    Robert L. Warnock

    2016-09-01

    Full Text Available We study coherent synchrotron radiation (CSR in a perfectly conducting vacuum chamber of rectangular cross section, in a formalism allowing an arbitrary sequence of bends and straight sections. We apply the paraxial method in the frequency domain, with a Fourier development in the vertical coordinate but with no other mode expansions. A line charge source is handled numerically by a new method that rids the equations of singularities through a change of dependent variable. The resulting algorithm is fast compared to earlier methods, works for short bunches with complicated structure, and yields all six field components at any space-time point. As an example we compute the tangential magnetic field at the walls. From that one can make a perturbative treatment of the Poynting flux to estimate the energy deposited in resistive walls. The calculation was motivated by a design issue for LCLS-II, the question of how much wall heating from CSR occurs in the last bend of a bunch compressor and the following straight section. Working with a realistic longitudinal bunch form of r.m.s. length 10.4  μm and a charge of 100 pC we conclude that the radiated power is quite small (28 W at a 1 MHz repetition rate, and all radiated energy is absorbed in the walls within 7 m along the straight section.

  13. Study of structural model of biological membranes by synchrotron radiation

    CERN Document Server

    Cavalcanti, L P

    2001-01-01

    The objective of this work has been to study, from the structural point of view, the process of incorporation of various types of hydrophobic compounds into the lamellar phase of liposomes and multilayers of the zwitterionic phospholipid DPPC. X-ray diffraction and scattering techniques using synchrotron radiation, have been used to monitor changes of several bilayer systems. Thermotropic phase transitions as well as the order of the lamellar packing were studied in situ experiments. The behavior of the L beta' and L alpha phases was followed as a function of the water content in dispersions of DPPC multi lamellar vesicles with the addition of the alkaloid Ellipticine in several concentrations. The results showed a decrease in the temperature of the pre-transition as well as that of the main transition (P beta' ->L alpha). The decrease of the lamellar spacing as a function of temperature in the liquid crystalline phase leads to the description of the thermal compression coefficient in the L alpha phase. It wa...

  14. Nonlinear Resonance Islands and Modulational Effects in a Proton Synchrotron

    Energy Technology Data Exchange (ETDEWEB)

    Satogata, Todd Jeffrey [Northwestern Univ., Evanston, IL (United States)

    1993-01-01

    We examine both one-dimensional and two-dimensional nonlinear resonance islands created in the transverse phase space of a proton synchrotron by nonlinear magnets. We also examine application of the theoretical framework constructed to the phenomenon of modulational diffusion in a collider model of the Fermilab Tevatron. For the one-dimensional resonance island system, we examine the effects of two types of modulational perturbations on the stability of these resonance islands: tune modulation and beta function modulation. Hamiltonian models are presented which predict stability boundaries that depend on only three paramders: the strength and frequency of the modulation and the frequency of small oscillations inside the resonance island. These. models are compared to particle tracking with excellent agreement. The tune modulation model is also successfully tested in experiment, where frequency domain analysis coupled with tune modulation is demonstrated to be useful in measuring the strength of a nonlinear resonance. Nonlinear resonance islands are also examined in two transverse dimensions in the presence of coupling and linearly independent crossing resonances. We present a first-order Hamiltonian model which predicts fixed point locations, but does not reproduce small oscillation frequencies seen in tracking; therefore in this circumstance such a model is inadequate. Particle tracking is presented which shows evidence of two-dimensional persistent signals, and we make suggestions on methods for observing such signals in future experiment.

  15. The Proton Synchrotron, going strong at fifty years

    CERN Multimedia

    Django Manglunki

    It was on the evening of 24 November 1959 that an incredulous Hildred Blewett, on detachment to CERN from the Brookhaven laboratory, exclaimed “Yes! We’re through transition!” The first beam of ten billion protons had not only broken through the 5.2 GeV barrier but gone on all the way to 24 GeV, the machine’s top energy at that time.   An operational screenshot from the PS, taken on its 50th anniversary. The three white peaks depict different phases (cycles) of the PS’s operation. In the first and third cycle, the PS is producing a very low-intensity beam for LHC commissioning. In the second cycle, protons are being spilled out for use in the East Area. Fifty years ago the PS, the first strong-focusing proton synchrotron using alternating gradient technology, first began to circulate beams at an unprecedented level of energy. Over the years, a complex of linear and circular accelerators and storage rings grew up around the PS. In the mid-1990s ...

  16. Genome-wide transcription responses to synchrotron microbeam radiotherapy.

    Science.gov (United States)

    Sprung, Carl N; Yang, Yuqing; Forrester, Helen B; Li, Jason; Zaitseva, Marina; Cann, Leonie; Restall, Tina; Anderson, Robin L; Crosbie, Jeffrey C; Rogers, Peter A W

    2012-10-01

    The majority of cancer patients achieve benefit from radiotherapy. A significant limitation of radiotherapy is its relatively low therapeutic index, defined as the maximum radiation dose that causes acceptable normal tissue damage to the minimum dose required to achieve tumor control. Recently, a new radiotherapy modality using synchrotron-generated X-ray microbeam radiotherapy has been demonstrated in animal models to ablate tumors with concurrent sparing of normal tissue. Very little work has been undertaken into the cellular and molecular mechanisms that differentiate microbeam radiotherapy from broad beam. The purpose of this study was to investigate and compare the whole genome transcriptional response of in vivo microbeam radiotherapy versus broad beam irradiated tumors. We hypothesized that gene expression changes after microbeam radiotherapy are different from those seen after broad beam. We found that in EMT6.5 tumors at 4-48 h postirradiation, microbeam radiotherapy differentially regulates a number of genes, including major histocompatibility complex (MHC) class II antigen gene family members, and other immunity-related genes including Ciita, Ifng, Cxcl1, Cxcl9, Indo and Ubd when compared to broad beam. Our findings demonstrate molecular differences in the tumor response to microbeam versus broad beam irradiation and these differences provide insight into the underlying mechanisms of microbeam radiotherapy and broad beam.

  17. Simple method for particle tracking with coherent synchrotron radiation

    Directory of Open Access Journals (Sweden)

    M. Borland

    2001-07-01

    Full Text Available Coherent synchrotron radiation (CSR is of great interest to those designing accelerators as drivers for free-electron lasers (FELs. Although experimental evidence is incomplete, CSR is predicted to have potentially severe effects on the emittance of high-brightness electron beams. The performance of an FEL depends critically on the emittance, current, and energy spread of the beam. Attempts to increase the current through magnetic bunch compression can lead to increased emittance and energy spread due to CSR in the dipoles of such a compressor. The code elegant was used for design and simulation of the bunch compressor [M. Borland et al., in Proceedings of the 2000 Linear Accelerator Conference, Monterey, CA (SLAC, Menlo Park, CA, 2001, p. 863] for the low-energy undulator test line (LEUTL FEL [S. V. Milton et al., Phys. Rev. Let. 85, 988 (1999] at the Advanced Photon Source (APS. In order to facilitate this design, a fast algorithm was developed based on the 1D formalism of Saldin and co-workers [E. L. Saldin, E. A. Schneidmiller, and M. V. Yurkov, Nucl. Instrum. Methods Phys. Res., Sect. A 398, 373 (1997]. In addition, a method of including CSR effects in drift spaces following the chicane magnets was developed and implemented. The algorithm is fast enough to permit running hundreds of tolerance simulations including CSR for 50 000 particles. This article describes the details of the implementation and shows results for the APS bunch compressor.

  18. Synchrotron radiation macromolecular crystallography: science and spin-offs

    Directory of Open Access Journals (Sweden)

    John R. Helliwell

    2015-03-01

    Full Text Available A current overview of synchrotron radiation (SR in macromolecular crystallography (MX instrumentation, methods and applications is presented. Automation has been and remains a central development in the last decade, as have the rise of remote access and of industrial service provision. Results include a high number of Protein Data Bank depositions, with an increasing emphasis on the successful use of microcrystals. One future emphasis involves pushing the frontiers of using higher and lower photon energies. With the advent of X-ray free-electron lasers, closely linked to SR developments, the use of ever smaller samples such as nanocrystals, nanoclusters and single molecules is anticipated, as well as the opening up of femtosecond time-resolved diffraction structural studies. At SR sources, a very high-throughput assessment for the best crystal samples and the ability to tackle just a few micron and sub-micron crystals will become widespread. With higher speeds and larger detectors, diffraction data volumes are becoming long-term storage and archiving issues; the implications for today and the future are discussed. Together with the rise of the storage ring to its current pre-eminence in MX data provision, the growing tendency of central facility sites to offer other centralized facilities complementary to crystallography, such as cryo-electron microscopy and NMR, is a welcome development.

  19. Synchrotron radiation macromolecular crystallography: science and spin-offs.

    Science.gov (United States)

    Helliwell, John R; Mitchell, Edward P

    2015-03-01

    A current overview of synchrotron radiation (SR) in macromolecular crystallography (MX) instrumentation, methods and applications is presented. Automation has been and remains a central development in the last decade, as have the rise of remote access and of industrial service provision. Results include a high number of Protein Data Bank depositions, with an increasing emphasis on the successful use of microcrystals. One future emphasis involves pushing the frontiers of using higher and lower photon energies. With the advent of X-ray free-electron lasers, closely linked to SR developments, the use of ever smaller samples such as nanocrystals, nanoclusters and single molecules is anticipated, as well as the opening up of femtosecond time-resolved diffraction structural studies. At SR sources, a very high-throughput assessment for the best crystal samples and the ability to tackle just a few micron and sub-micron crystals will become widespread. With higher speeds and larger detectors, diffraction data volumes are becoming long-term storage and archiving issues; the implications for today and the future are discussed. Together with the rise of the storage ring to its current pre-eminence in MX data provision, the growing tendency of central facility sites to offer other centralized facilities complementary to crystallography, such as cryo-electron microscopy and NMR, is a welcome development.

  20. [Clinical applications of synchrotron radiation X-ray].

    Science.gov (United States)

    Uyama, C

    1994-09-01

    Synchrotron Radiation X-ray (SR X-ray) is an extremely strong X-ray source with a photon number more than 10(4) compared with that of the current X-ray tube. X-rays obtained by monochromatizing SR X-ray have been applied to new techniques for medical diagnosis. Several studies are now being conducted at the beam site for medical use at the Accumulation Ring of the High Energy Physics Research Institute, Tsukuba. Applications being studied include (1) energy subtraction coronary angiography. (2) microdetection of metas in samples excised from subjects. (3) monochromatic X-ray computed tomography and so on. Energy subtraction coronary angiography might have a safety advantage over the current selective coronary angiography. Microdetection of mandatory metals and poisonous heavy metals in in vivo samples contributes to the development of pathologic knowledge and clinical treatment of cancer and heavy metal toxications. Monochromatic X-ray CT is expected to detect diseases in the early stage due to increased accuracy in CT values.

  1. Synchrotron Radiation Pair Distribution Function Analysis of Gels in Cements

    Directory of Open Access Journals (Sweden)

    Ana Cuesta

    2017-10-01

    Full Text Available The analysis of atomic ordering in a nanocrystalline phase with small particle sizes, below 5 nm, is intrinsically complicated because of the lack of long-range order. Furthermore, the presence of additional crystalline phase(s may exacerbate the problem, as is the case in cement pastes. Here, we use the synchrotron pair distribution function (PDF chiefly to characterize the local atomic order of the nanocrystalline phases, gels, in cement pastes. We have used a multi r-range analysis approach, where the ~4–7 nm r-range allows determining the crystalline phase contents; the ~1–2.5 nm r-range is used to characterize the atomic ordering in the nanocrystalline component; and the ~0.2–1.0 nm r-range gives insights about additional amorphous components. Specifically, we have prepared four alite pastes with variable water contents, and the analyses showed that a defective tobermorite, Ca11Si9O28(OH2.8.5H2O, gave the best fit. Furthermore, the PDF analyses suggest that the calcium silicate hydrate gel is composed of this tobermorite and amorphous calcium hydroxide. Finally, this approach has been used to study alternative cements. The hydration of monocalcium aluminate and ye’elimite pastes yield aluminum hydroxide gels. PDF analyses show that these gels are constituted of nanocrystalline gibbsite, and the particle size can be as small as 2.5 nm.

  2. Soft X-ray diffractometer for synchrotron radiation

    CERN Document Server

    Gau, T S; Liu, K Y; Chung, C H; Chen, C K; Lai, S C; Shu, C H; Huang, Y S; Chao, C H; Lee, Y R; Chen, C T; Chang, S L

    2001-01-01

    An ultra-high vacuum soft X-ray diffractometer has been constructed and commissioned at the Synchrotron Radiation Research Center (SRRC) to investigate materials structures in mesoscale. The diffractometer, housed in a UHV tank, consists of a 6-circle goniometer, together with the systems for beam-collimation, signal detection, vacuum, and control panels. The kappa-phi (cursive,open) Greek-psi goniostat is adopted for the sample orientation. Crystal samples can be rotated along a given reciprocal lattice vector by using psi scan. Two orthogonal axes, gamma (or 2 theta) and delta, are used to move the detector. The detector is a semiconductor pin diode, which can be used in UHV ambient. This 6-circle goniometer allows for sample scanning of a wide range in the momentum space. The motors used for goniometer rotation and slit selection are UHV compatible. The UHV tank is placed on an XYZ table capable of positioning the center of the goniometer onto the incident beam. Test experiments have been carried on the 1-...

  3. Capacitive energy storage and recovery for synchrotron magnets

    Science.gov (United States)

    Koseki, K.

    2014-06-01

    Feasibility studies on capacitive energy storage and recovery in the main-ring synchrotron of the Japan Proton Accelerator Research Complex were conducted by circuit simulation. The estimated load fluctuation was 96 MVA in total for dipole magnets, which is likely to induce a serious disturbance in the main grid. It was found that the energy stored in the magnets after the excitation period can be recovered to the storage capacitor by controlling the voltage across the energy-storage capacitor using a pulse-width-modulation converter and reused in the next operational cycle. It was also found that the power fluctuation in the main grid can be reduced to 12 MVA. An experimental evaluation of an aluminum metalized film capacitor revealed that capacitance loss was induced by a fluctuating voltage applied to the storage capacitor when applying the proposed method. The capacitance loss was induced by corona discharge around the edges of segmented electrodes of a self-healing capacitor. The use of aluminum-zinc alloy was evaluated as a countermeasure to mitigate the effect induced by the corona discharge. For a zinc content of 8%, which was optimized experimentally, a capacitor with a sufficient life time expectancy of 20 years and a working potential gradient of 250 V/μm was developed.

  4. In situ Synchrotron X-ray Thermodiffraction of Boranes

    Directory of Open Access Journals (Sweden)

    Pascal G. Yot

    2016-01-01

    Full Text Available Boranes of low molecular weight are crystalline materials that have been much investigated over the past decade in the field of chemical hydrogen storage. In the present work, six of them have been selected to be studied by in situ synchrotron X-ray thermodiffraction. The selected boranes are ammonia borane NH3BH3 (AB, hydrazine borane N2H4BH3 (HB, hydrazine bisborane N2H4(BH32 (HBB, lithium LiN2H3BH3 (LiHB and sodium NaN2H3BH3 (NaHB hydrazinidoboranes, and sodium triborane NaB3H8 (STB. They are first investigated separately over a wide range of temperature (80–300 K, and subsequently compared. Differences in crystal structures, the existence of phase transition, evolutions of unit cell parameters and volumes, and variation of coefficients of thermal expansion can be observed. With respect to AB, HB and HBB, the differences are mainly explained in terms of molecule size, conformation and motion (degree of freedom of the chemical groups (NH3, N2H4, BH3. With respect to LiHB, NaHB and STB, the differences are explained by a stabilization effect favored by the alkali cations via M···H interactions with four to five borane anions. The main results are presented and discussed herein.

  5. Polarization experiments with the SPIN setup at the ITEP synchrotron

    CERN Document Server

    Alekseev, I G; Kanavets, V P; Koroleva, L I; Morozov, B V; Nesterov, V M; Ryltzov, V V; Svirida, D N; Sulimov, A D; Zhurkin, V V; Beloglasov, Yu A; Kovalev, A I; Kruglov, S P; Novinsky, D V; Shchedrov, V A; Sumachev, Yu V; Trautman, V Yu; Bazhanov, N A; Bunyatova, E I

    2002-01-01

    New experimental data on the spin-rotation parameters A and R measured for elastic pi /sup +or-/p scattering in the resonance region and on the asymmetry in pC scattering at primary momenta in the range 1.35-2.02 GeV/c, as well as in quasielastic proton scattering on nuclei in the same momentum range, are summarized., All these data were recently obtained by using the proton synchrotron installed at the Institute of Theoretical and Experimental Physics (ITEP, Moscow). The spectrum and features of seven isospin-3/2 baryon resonances that form a peak in the total cross section at a c.m. energy of 1.9 GeV are analyzed on the basis of new data on the parameters A and R, and the results of this analysis are presented. The experiments surveyed in this article were performed by a collaboration of researchers from ITEP and the Petersburg Nuclear Physics Institute (PNPI, Gatchina), the ITEP-PNPI collaboration. (29 refs).

  6. DELSY project: status and development Dubna Electron Synchrotron

    CERN Document Server

    Balalykin, N; Bykovsky, V

    2003-01-01

    The DELSY (Dubna Electron Synchrotron) project is under development at the Joint Institute for Nuclear Research. It is based on an acceleration facility donated to the Joint Institute for Nuclear Research by the Institute for Nuclear and High Energy Physics (NIKHEF, Amsterdam). The NIKHEF accelerator facility consists of the linear electron accelerator MEA, which has an electron energy of 700 MeV, and the electron storage ring AmPS, with a maximum energy of 900 MeV and a beam current of 200 mA. There are three phases to the construction of the DELSY facility. Phase I will be accomplished with the construction of a complex of free-electron lasers covering continuously the spectrum from the far infrared down to the ultraviolet (approx 150 nm). Phase II will be accomplished with the commissioning of the storage ring DELSY. Complete commissioning of the DELSY project will take place after finishing Phase III, the construction of an X-ray free-electron laser. This phase is considered as the ultimate goal of the pr...

  7. Serial crystallography on in vivo grown microcrystals using synchrotron radiation

    Directory of Open Access Journals (Sweden)

    Cornelius Gati

    2014-03-01

    Full Text Available Crystal structure determinations of biological macromolecules are limited by the availability of sufficiently sized crystals and by the fact that crystal quality deteriorates during data collection owing to radiation damage. Exploiting a micrometre-sized X-ray beam, high-precision diffractometry and shutterless data acquisition with a pixel-array detector, a strategy for collecting data from many micrometre-sized crystals presented to an X-ray beam in a vitrified suspension is demonstrated. By combining diffraction data from 80 Trypanosoma brucei procathepsin B crystals with an average volume of 9 µm3, a complete data set to 3.0 Å resolution has been assembled. The data allowed the refinement of a structural model that is consistent with that previously obtained using free-electron laser radiation, providing mutual validation. Further improvements of the serial synchrotron crystallography technique and its combination with serial femtosecond crystallography are discussed that may allow the determination of high-resolution structures of micrometre-sized crystals.

  8. Use of synchrotron tomography to image naturalistic anatomy in insects

    Science.gov (United States)

    Socha, John J.; De Carlo, Francesco

    2008-08-01

    Understanding the morphology of anatomical structures is a cornerstone of biology. For small animals, classical methods such as histology have provided a wealth of data, but such techniques can be problematic due to destruction of the sample. More importantly, fixation and physical slicing can cause deformation of anatomy, a critical limitation when precise three-dimensional data are required. Modern techniques such as confocal microscopy, MRI, and tabletop x-ray microCT provide effective non-invasive methods, but each of these tools each has limitations including sample size constraints, resolution limits, and difficulty visualizing soft tissue. Our research group at the Advanced Photon Source (Argonne National Laboratory) studies physiological processes in insects, focusing on the dynamics of breathing and feeding. To determine the size, shape, and relative location of internal anatomy in insects, we use synchrotron microtomography at the beamline 2-BM to image structures including tracheal tubes, muscles, and gut. Because obtaining naturalistic, undeformed anatomical information is a key component of our studies, we have developed methods to image fresh and non-fixed whole animals and tissues. Although motion artifacts remain a problem, we have successfully imaged multiple species including beetles, ants, fruit flies, and butterflies. Here we discuss advances in biological imaging and highlight key findings in insect morphology.

  9. Synchrotron FTIR imaging of OH in quartz mylonites

    Science.gov (United States)

    Kronenberg, Andreas K.; Hasnan, Hasnor F. B.; Holyoke, Caleb W., III; Law, Richard D.; Liu, Zhenxian; Thomas, Jay B.

    2017-10-01

    Previous measurements of water in deformed quartzites using conventional Fourier transform infrared spectroscopy (FTIR) instruments have shown that water contents of larger grains vary from one grain to another. However, the non-equilibrium variations in water content between neighboring grains and within quartz grains cannot be interrogated further without greater measurement resolution, nor can water contents be measured in finely recrystallized grains without including absorption bands due to fluid inclusions, films, and secondary minerals at grain boundaries.Synchrotron infrared (IR) radiation coupled to a FTIR spectrometer has allowed us to distinguish and measure OH bands due to fluid inclusions, hydrogen point defects, and secondary hydrous mineral inclusions through an aperture of 10 µm for specimens > 40 µm thick. Doubly polished infrared (IR) plates can be prepared with thicknesses down to 4-8 µm, but measurement of small OH bands is currently limited by strong interference fringes for samples detectable water in highly sheared MCT mylonites challenge our understanding of quartz rheology. However, where water absorption bands can be detected and compared with deformation microstructures, OH concentration maps provide information on the histories of deformation and recovery, evidence for the introduction and loss of fluid inclusions, and water weakening processes.

  10. Cadmium-zinc telluride detector arrays for synchrotron radiation applications

    Science.gov (United States)

    Kakuno, Edson M.; Camarda, Giuseppe S.; Siddons, D. P.

    2004-01-01

    We have begun a program to develop CZT-based detectors optimized for Synchrotron Radiation (SR) applications. SR provides high brightness beams of hard x-rays, typically in the range 5-100keV. Below 10keV, Peltier-cooled silicon detector arrays can provide high throughput with good spectroscopic resolution. At higher energies, only cryo-cooled germanium detectors or scintillation counters are available. Neither are easily available in large arrays, and scintillation counters lack energy resolution. CZT offers a solution to both these problems. Our development has focused on surface preparation and contact definition technologies which minimize device leakage currents while allowing high-definition contact patterns suitable for SR applications. We have used SR also for diagnostic purposes in these developments, both for detector testing and material characterization. X-ray diffraction, Infrared microscopy and photoemission are all relevant SR-based tools which we are using in our work. As an example, we have observed that bromine remains attached to the CZT surface after chemical etching, and is remarkably persistent in the face of surface cleaning and argon ion sputtering, as revealed by photoemission spectroscopy and x-ray absorption spectroscopy.

  11. Synchrotron quantification of fracturing during maturation of shales

    Science.gov (United States)

    Figueroa Pilz, Fernando; Fauchille, Anne-Laure; Dowey, Patrick; Courtois, Loic; Bay, Brian; Ma, Lin; Taylor, Kevin; Mecklenburgh, Julian; Lee, Peter

    2017-04-01

    To understand both the hydrocarbon migration within and from shale rocks, and during hydraulic fracturing, is needed to evaluate and predict its environmental footprint. As a consequence, the time characterization of fracture networks in shale is particularly important. Time resolved synchrotron X-ray tomography was used to quantify the initiation and propagation of fractures during the simulated maturation of an organic-rich Kimmeridge Clay shale from the µm to mm scales. Scanning electron microscopy (SEM) observations were performed before and after maturation in order to compare the microstructure evolution and better understand the fracture location. Fracture and strain development during heating was quantified in 3D by Digital Volume Correlation (DVC) (Bay et al., 1999). The combination of DVC, X-Ray tomography and SEM obtained direct 4D strain measurements of the anisotropic mechanical behaviour of Kimmeridge shale with the temperature during an accelerated thermal maturation (Figueroa Pilz et al.). Such a combination has rarely been investigated in 4D at these scales in the past. In the study conditions, the results demonstrated the anisotropy in thermal expansion and the aperture fracture pathways through organic matter and clay matrix.

  12. Modeling Longitudinal Dynamics in the Fermilab Booster Synchrotron

    Energy Technology Data Exchange (ETDEWEB)

    Ostiguy, Jean-Francois [Fermilab; Bhat, Chandra [Fermilab; Lebedev, Valeri [Fermilab

    2016-06-01

    The PIP-II project will replace the existing 400 MeV linac with a new, CW-capable, 800 MeV superconducting one. With respect to current operations, a 50% increase in beam intensity in the rapid cycling Booster synchrotron is expected. Booster batches are combined in the Recycler ring; this process limits the allowed longitudinal emittance of the extracted Booster beam. To suppress eddy currents, the Booster has no beam pipe; magnets are evacuated, exposing the beam to core laminations and this has a substantial impact on the longitudinal impedance. Noticeable longitudinal emittance growth is already observed at transition crossing. Operation at higher intensity will likely necessitate mitigation measures. We describe systematic efforts to construct a predictive model for current operating conditions. A longitudinal only code including a laminated wall impedance model, space charge effects, and feedback loops is developed. Parameter validation is performed using detailed measurements of relevant beam, rf and control parameters. An attempt is made to benchmark the code at operationally favorable machine settings.

  13. Nanofocusing optics for synchrotron radiation made from polycrystalline diamond.

    Science.gov (United States)

    Fox, O J L; Alianelli, L; Malik, A M; Pape, I; May, P W; Sawhney, K J S

    2014-04-07

    Diamond possesses many extreme properties that make it an ideal material for fabricating nanofocusing x-ray optics. Refractive lenses made from diamond are able to focus x-ray radiation with high efficiency but without compromising the brilliance of the beam. Electron-beam lithography and deep reactive-ion etching of silicon substrates have been used in a transfer-molding technique to fabricate diamond optics with vertical and smooth sidewalls. Latest generation compound refractive lenses have seen an improvement in the quality and uniformity of the optical structures, resulting in an increase in their focusing ability. Synchrotron beamline tests of two recent lens arrays, corresponding to two different diamond morphologies, are described. Focal line-widths down to 210 nm, using a nanocrystalline diamond lens array and a beam energy of E = 11 keV, and 230 nm, using a microcrystalline diamond lens at E = 15 keV, have been measured using the Diamond Light Source Ltd. B16 beamline. This focusing prowess is combined with relatively high transmission through the lenses compared with silicon refractive designs and other diffractive optics.

  14. Construction and Performance of Superconducting Magnets for Synchrotron Radiation

    CERN Document Server

    Hwang, Ching-Shiang; Chang, Cheng-Kuo; Chang, Ho-Ping; Chen Chien Te; Chen Hui Huang; Chen, Jenny; Chen June Rong; Chien, Yuan-Chen; Fan, Tai-Ching; Hsiung, Gao-Yu; Hsu, Kuo-Tung; Hsu, Shen-Nung; Huang, Ming-Hsiung; Kuo, Chin-Cheng; Lin, Fu-Yuan

    2005-01-01

    Two superconducting magnets, one wavelength shifter (SWLS) with a field of 5 T and one wiggler (SW6) with a field of 3.2 T, were constructed and routinely operated at NSRRC for generating synchrotron x-rays. In addition, three multipole wigglers (IASW) with fields of 3.1 T will be constructed and installed each in the three achromatic short straight sections. A warm beam duct of 20 mm inner gap and a 1.5 W GM type cryo-cooler were chosen for the SWLS to achieve cryogen-free operation. For the SW6, a cold beam duct of 11 mm inner gap was kept at 100 K temperature and no trim coil compensation is necessary for its operation. Meanwhile, no beam loss was observed when the SW6 was quenched. A cryogenic plant with cooling power of 450 W was constructed to supply the liquid helium for the four superconducting wigglers. The design concept, magnetic field quality, the commissioning results, and the operation performance of these magnets will be presented.

  15. Synchrotron x-ray study of multilayers in Laue geometry

    Energy Technology Data Exchange (ETDEWEB)

    Kang, H C; Stephenson, G B; Liu, C; Conley, R; Macrander, A T; Maser, J; Bajt, S; Chapman, H N

    2004-07-21

    Zone plates with depth to zone-width ratios as large as 100 are needed for focusing of hard x-rays. Such high aspect ratios are challenging to produce by lithography. We are investigating the fabrication of high-aspect-ratio linear zone plates by multilayer deposition followed by sectioning. As an initial step in this work, we present a synchrotron x-ray study of constant-period multilayers diffracting in Laue (transmission) geometry. Data are presented from two samples: a 200 period W/Si multilayer with d-spacing of 29 nm, and a 2020 period Mo/Si multilayer with d-spacing of 7 nm. By cutting and polishing we have successfully produced thin cross sections with section depths ranging from 2 to 12 {micro}m. Transverse scattering profiles (rocking curves) across the Bragg reflection exhibit well-defined interference fringes originating from the depth of the sample, in agreement with dynamical diffraction theory for a multilayer in Laue geometry.

  16. National Synchrotron Light Source guidelines for the conduct of operations

    Energy Technology Data Exchange (ETDEWEB)

    Buckley, M. [Brookhaven National Lab., Upton, NY (United States). National Synchrotron Light Source

    1998-01-01

    To improve the quality and uniformity of operations at the Department of Energy`s facilities, the DOE issued Order 5480.19 ``Conduct of Operations Requirements at DOE facilities.`` This order recognizes that the success of a facilities mission critically depends upon a high level of performance by its personnel and equipment. This performance can be severely impaired if the facility`s Conduct of Operations pays inadequate attention to issues of organization, safety, health, and the environment. These guidelines are Brookhaven National Laboratory`s and the National Synchrotron Light Source`s acknowledgement of the principles of Conduct of Operations and the response to DOE Order 5480.19. These guidelines cover the following areas: (1) operations organization and administration; (2) shift routines and operating practices; (3) control area activities; (4) communications; (5) control of on-shift training; (6) investigation of abnormal events; (7) notifications; (8) control of equipment and system studies; (9) lockouts and tagouts; (10) independent verification; (11) log-keeping; (12) operations turnover; (13) operations aspects of facility process control (14) required reading; (15) timely orders to operators; (16) operations procedures; (17) operator aid posting; and (18) equipment sizing and labeling.

  17. An assessment of research opportunities and the need for synchrotron radiation facilities

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1995-12-31

    The workshop focused on six topics, all of which are areas of active research: (1) speciation, reactivity and mobility of contaminants in aqueous systems, (2) the role of surfaces and interfaces in molecular environmental science, (3) the role of solid phases in molecular environmental science, (4) molecular biological processes affecting speciation, reactivity, and mobility of contaminants in the environment, (5) molecular constraints on macroscopic- and field-scale processes, and (6) synchrotron radiation facilities and molecular environmental sciences. These topics span a range of important issues in molecular environmental science. They focus on the basic knowledge required for understanding contaminant transport and fate and for the development of science-based remediation and waste management technologies. Each topic was assigned to a working group charged with discussing recent research accomplishments, significant research opportunities, methods required for obtaining molecular-scale information on environmental contaminants and processes, and the value of synchrotron x-ray methods relative to other methods in providing this information. A special working group on synchrotron radiation facilities was convened to provide technical information about experimental facilities at the four DOE-supported synchrotron radiation sources in the US (NSLS, SSRL, AS and UPS) and synchrotron- based methods available for molecular environmental science research. Similar information on the NSF-funded Cornell High Energy synchrotron Source (CHESS) was obtained after the workshop was held.

  18. Development of compact synchrotron light source for x-ray lithography (abstract)

    Science.gov (United States)

    Mandai, S.; Hoshi, Y.; Kohno, Y.

    1989-07-01

    Ishikawajima-Harima Heavy Industries Co., Ltd., (IHI) has developed a prototype compact synchrotron light source for x-ray lithography of semiconductors. It consists of 45-MeV linear accelerator as an electron injector and an 800-MeV synchrotron. Peak wavelength of synchrotron radiation is around 10 Å. The basic parameter of the synchrotron is as follows: (1) Beam current: more than 50 mA; (2) Beam life: more than 1 hr; (3) Circumference: 23.5 m; (4) Bending magnet: 1.33 T, 90° sector laminated core; (5) rf system: 178.5 MHz tetrode power supply. Our synchrotron is a so-called low-energy injection accelerator and various difficult problems such as ion trapping, vacuum, Touscheck effect will occur. So, we provide ion cleaning electrodes inside the vacuum chamber to avoid ion trapping. Also, we have adopted a trapezoidal magnet excitation method as an injection scheme to stimulate gas desorption of the vacuum chamber. The beamline extracted from the bending magnet will be used for various research subjects which include x-ray lithography, photoelectron spectroscopy, EXAFS, fluorescence analysis, and so on. This machine will be completed by the end of 1988 and is scheduled to use synchrotron radiation in the spring of 1989.

  19. Climate change in the Brazilian northeast

    Science.gov (United States)

    Rodrigues, Regina R.; Haarsma, Reindert J.; Hoelzemann, Judith J.

    2012-10-01

    Climate Change, Impacts and Vulnerabilities in Brazil: Preparing the Brazilian Northeast for the Future; Natal, Brazil, 27 May to 01 June 2012 The variability of the semiarid climate of the Brazilian northeast has enormous environmental and social implications. Because most of the population in this area depends on subsistence agriculture, periods of severe drought in the past have caused extreme poverty and subsequent migration to urban centers. From the ecological point of view, frequent and prolonged droughts can lead to the desertification of large areas. Understanding the causes of rainfall variability, in particular periods of severe drought, is crucial for accurate forecasting, mitigation, and adaptation in this important region of Brazil.

  20. Huntington disease: DNA analysis in brazilian population

    OpenAIRE

    RASKIN, SALMO; ALLAN, NASSER; TEIVE, HÉLIO A.G.; CARDOSO, FRANCISCO; HADDAD, MÔNICA SANTORO; LEVI, GILBERTO; BOY, RAQUEL; LERENA JR, JUAN; SOTOMAIOR, VANESSA SANTOS; JANZEN-DÜCK, MÔNICA; JARDIM, LAURA BANNACH; FELLANDER, FLÁVIO R.; ANDRADE, LUIZ AUGUSTO FRANCO

    2000-01-01

    Huntington disease (HD) is associated with expansions of a CAG trinucleotide repeat in the HD gene. Accurate measurement of a specific CAG repeat sequence in the HD gene in 92 Brazilian controls without HD, 44 Brazilian subjects with clinical findings suggestive of HD and 40 individuals from 6 putative HD families, showed a range from 7 to 33 repeats in normal subjects and 39 to 88 repeats in affected subjects. A trend between early age at onset of first symptoms and increasing number of repe...

  1. The influence of the solid waste disposal areas in Campinas city, Sao Paulo state (Brazil) on water quality: determination of metals using synchrotron radiation total reflection X-ray fluorescence

    Energy Technology Data Exchange (ETDEWEB)

    Oliveira, Bruna F.F., E-mail: bffaria@yahoo.com.br [Universidade Federal de Uberlandia (UFU), Uberlandia, MG (Brazil). Inst. de Ciencias Agrarias. Dept. de Engenharia Ambiental; Moreira, Silvana; Canteras, Felippe Benavente, E-mail: silvana@fec.unicamp.br, E-mail: felippe.canteras@gmail.com [Universidade Estadual de Campinas (UNICAMP), Campinas, SP (Brazil). Dept. de Saneamento e Ambiente

    2013-07-01

    Among the many forms of waste disposal, landfills today are best suited to Brazilian conditions, this because their construction allows minimizing the negative effects of landfill gas and slurry produced. However, the confinement of pollutants from landfills is linked to its construction and operation and when the construction and/or is wrong they can endanger air, groundwater and surface waters qualities. Thus, the main objective of this study was to analyze the concentration of heavy metals in samples of groundwater, surface water and slurry coming from solid waste disposal locations in the city of Campinas, SP - Delta, Santa Barbara and Pirelli Landfills. The samples were analyzed at the Brazilian Synchrotron Light Laboratory using Synchrotron Radiation Total Reflection X-Ray Fluorescence technique (SR-TXRF). In Pirelli Landfill, the highest concentrations were observed in one of the wells located to downstream of the Landfill (in relation to the groundwater flux) - the monitoring well PM04, exceeding the intervention value defined by CETESB. For Santa Barbara landfill in one upstream monitoring well the concentrations of Ni, Mn, Pb and Cr, surpassed the maximum permissive values. The manganese in Landfill Delta showed to be higher in wells located downstream and 50% of the wells analyzed exceeded the maximum permissive value for groundwater samples. In the case of surface waters located in the vicinity of landfill sites, the metals that surpassed the maximum permissive values according the legislation in most of the points analyzed were Mn, Cu and Pb. For slurry samples collected in Delta Landfill, the average concentrations for Mn, Ni, Cu and Pb not exceeded the maximum permissive values during the period studied. Moreover for Santa Barbara the average concentration of Mn, Cu and Zn surpassed the permissive limits, as was observed for Mn in the Pirelli Landfill. (author)

  2. NSLS-II: Nonlinear Model Calibration for Synchrotrons

    Energy Technology Data Exchange (ETDEWEB)

    Bengtsson, J.

    2010-10-08

    This tech note is essentially a summary of a lecture we delivered to the Acc. Phys. Journal Club Apr, 2010. However, since the estimated accuracy of these methods has been naive and misleading in the field of particle accelerators, i.e., ignores the impact of noise, we will elaborate on this in some detail. A prerequisite for a calibration of the nonlinear Hamiltonian is that the quadratic part has been understood, i.e., that the linear optics for the real accelerator has been calibrated. For synchrotron light source operations, this problem has been solved by the interactive LOCO technique/tool (Linear Optics from Closed Orbits). Before that, in the context of hadron accelerators, it has been done by signal processing of turn-by-turn BPM data. We have outlined how to make a basic calibration of the nonlinear model for synchrotrons. In particular, we have shown how this was done for LEAR, CERN (antiprotons) in the mid-80s. Specifically, our accuracy for frequency estimation was {approx} 1 x 10{sup -5} for 1024 turns (to calibrate the linear optics) and {approx} 1 x 10{sup -4} for 256 turns for tune footprint and betatron spectrum. For a comparison, the estimated tune footprint for stable beam for NSLS-II is {approx}0.1. Since the transverse damping time is {approx}20 msec, i.e., {approx}4,000 turns. There is no fundamental difference for: antiprotons, protons, and electrons in this case. Because the estimated accuracy for these methods in the field of particle accelerators has been naive, i.e., ignoring the impact of noise, we have also derived explicit formula, from first principles, for a quantitative statement. For e.g. N = 256 and 5% noise we obtain {delta}{nu} {approx} 1 x 10{sup -5}. A comparison with the state-of-the-arts in e.g. telecomm and electrical engineering since the 60s is quite revealing. For example, Kalman filter (1960), crucial for the: Ranger, Mariner, and Apollo (including the Lunar Module) missions during the 60s. Or Claude Shannon et al

  3. Flux and brightness calculations for various synchrotron radiation sources

    Energy Technology Data Exchange (ETDEWEB)

    Weber, J.M.; Hulbert, S.L.

    1991-11-01

    Synchrotron radiation (SR) storage rings are powerful scientific and technological tools. The first generation of storage rings in the US., e.g., SURF (Washington, D.C.), Tantalus (Wisconsin), SSRL (Stanford), and CHESS (Cornell), revolutionized VUV, soft X-ray, and hard X-ray science. The second (present) generation of storage rings, e.g. the NSLS VUV and XRAY rings and Aladdin (Wisconsin), have sustained the revolution by providing higher stored currents and up to a factor of ten smaller electron beam sizes than the first generation sources. This has made possible a large number of experiments that could not performed using first generation sources. In addition, the NSLS XRAY ring design optimizes the performance of wigglers (high field periodic magnetic insertion devices). The third generation storage rings, e.g. ALS (Berkeley) and APS (Argonne), are being designed to optimize the performance of undulators (low field periodic magnetic insertion devices). These extremely high brightness sources will further revolutionize x-ray science by providing diffraction-limited x-ray beams. The output of undulators and wigglers is distinct from that of bending magnets in magnitude, spectral shape, and in spatial and angular size. Using published equations, we have developed computer programs to calculate the flux, central intensity, and brightness output bending magnets and selected wigglers and undulators of the NSLS VUV and XRAY rings, the Advanced Light Source (ALS), and the Advanced Photon Source (APS). Following is a summary of the equations used, the graphs and data produced, and the computer codes written. These codes, written in the C programming language, can be used to calculate the flux, central intensity, and brightness curves for bending magnets and insertion devices on any storage ring.

  4. 3D synchrotron x-ray microtomography of paint samples

    Science.gov (United States)

    Ferreira, Ester S. B.; Boon, Jaap J.; van der Horst, Jerre; Scherrer, Nadim C.; Marone, Federica; Stampanoni, Marco

    2009-07-01

    Synchrotron based X-ray microtomography is a novel way to examine paint samples. The three dimensional distribution of pigment particles, binding media and their deterioration products as well as other features such as voids, are made visible in their original context through a computing environment without the need of physical sectioning. This avoids manipulation related artefacts. Experiments on paint chips (approximately 500 micron wide) were done on the TOMCAT beam line (TOmographic Microscopy and Coherent rAdiology experimenTs) at the Paul Scherrer Institute in Villigen, CH, using an x-ray energy of up to 40 keV. The x-ray absorption images are obtained at a resolution of 350 nm. The 3D dataset was analysed using the commercial 3D imaging software Avizo 5.1. Through this process, virtual sections of the paint sample can be obtained in any orientation. One of the topics currently under research are the ground layers of paintings by Cuno Amiet (1868- 1961), one of the most important Swiss painters of classical modernism, whose early work is currently the focus of research at the Swiss Institute for Art Research (SIK-ISEA). This technique gives access to information such as sample surface morphology, porosity, particle size distribution and even particle identification. In the case of calcium carbonate grounds for example, features like microfossils present in natural chalks, can be reconstructed and their species identified, thus potentially providing information towards the mineral origin. One further elegant feature of this technique is that a target section can be selected within the 3D data set, before exposing it to obtain chemical data. Virtual sections can then be compared with cross sections of the same samples made in the traditional way.

  5. Electronic Structure of Germanium Nanocrystal Films Probed with Synchrotron Radiation

    Energy Technology Data Exchange (ETDEWEB)

    Bostedt, C

    2002-05-01

    The fundamental structure--property relationship of semiconductor quantum dots has been investigated. For deposited germanium nanocrystals strong quantum confinement effects have been determined with synchrotron radiation based x-ray absorption and photoemission techniques. The nanocrystals are condensed out of the gas phase with a narrow size distribution and subsequently deposited in situ onto various substrates. The particles are crystalline in the cubic phase with a structurally disordered surface shell and the resulting film morphology depends strongly on the substrate material and condition. The disordered surface region has an impact on the overall electronic structure of the particles. In a size-dependent study, the conduction and valence band edge of germanium nanocrystals have been measured for the first time and compared to the bulk crystal. The band edges move to higher energies as the particle size is decreased, consistent with quantum confinement theory. To obtain a more accurate analysis of confinement effects in the empty states, a novel analysis method utilizing an effective particle size for the x-ray absorption experiment, which allows a deconvolution of absorption edge broadening effects, has been introduced. Comparison of the present study to earlier studies on silicon reveals that germanium exhibits stronger quantum confinement effects than silicon. Below a critical particle size of 2.3 {+-} 0.7 nm, the band gap of germanium becomes larger than that of silicon--even if it is the opposite for bulk materials. This result agrees phenomenologically with effective mass and tight binding theories but contradicts the findings of recent pseudopotential calculations. The discrepancy between theory and experiments is attributed to the differences in the theoretical models and experimental systems. The experimentally observed structural disorder of the particle surface has to be included in the theoretical models.

  6. Variations of Synchrotron Radio Emissions from Jupiter's Inner Radiation Belt

    Science.gov (United States)

    Lou, Y.-Q.

    2017-09-01

    Variations of Synchrotron Radio Emissions from Jupiter's Inner Radiation Belt Yu-Qing Lou* Physics Department, Tsinghua Centre for Astrophysics (THCA), Tsinghua-National Astronomical Observatories of China (NAOC) joint Research Centre for Astrophysics, Tsinghua University, Beijing 100084, China We describe the basic phenommenology of quasi-periodic 40 minute (QP-40) polar burst activities of Jupiter and their close correlation with the solar wind speed variations at the Jovian magnetosphere. Physically, relativistic electrons of QP-40 bursts most likely come from the circumpolar regions of the inner radiation belt (IRB) which gives off intense synchroton radio emissions in a wide wavelength range. Such relativistic electron bursts also give rise to beamed low-frequency radio bursts along polar magnetic field lines with distinct polarizations from Jupiter's two polar regions. Jovian aurora activities are expected to be also affected by such QP-40 burst activities. We present evidence of short-term (typical timescales shorter than an hour) variabilities of the IRB at 6cm wavelength and describe recent joint radio telescope observation campaign to monitor Jupiter in coordination with JUNO spacecraft. Except for low-frequency polarization features, we anticipate JUNO to detect QP-40 activities from both polar regions during the arrival of high-speed solar wind with intermittency. References 1. Y.-Q. Lou, The Astrophysical Journal, 548, 460 (2001). 2. Y.-Q. Lou, and C. Zheng, Mon. Not. Roy. Astron. Soc. Letters, 344, L1 (2003). 3. Y.-Q. Lou, H. G. Song, Y.Y. Liu, and M. Yang, Mon. Not. Roy. Astron. Soc. Letters, 421, L62 (2012). 4. Y.-Q. Lou, Geophysical Research Letters, 23, 609 (1996). 5. Y.-Q. Lou, Journal of Geophysical Research, 99, 14747 (1994). 6. G. R. Gladstone, et al., Nature, 415, 1000 (2002).

  7. New Developments and Geoscience Applications of Synchrotron Computed Microtomography (Invited)

    Science.gov (United States)

    Rivers, M. L.; Wang, Y.; Newville, M.; Sutton, S. R.; Yu, T.; Lanzirotti, A.

    2013-12-01

    Computed microtomography is the extension to micron spatial resolution of the CAT scanning technique developed for medical imaging. Synchrotron sources are ideal for the method, since they provide a monochromatic, parallel beam with high intensity. High energy storage rings such as the Advanced Photon Source at Argonne National Laboratory produce x-rays with high energy, high brilliance, and high coherence. All of these factors combine to produce an extremely powerful imaging tool for earth science research. Techniques that have been developed include: - Absorption and phase contrast computed tomography with spatial resolution below one micron. - Differential contrast computed tomography, imaging above and below the absorption edge of a particular element. - High-pressure tomography, imaging inside a pressure cell at pressures above 10GPa. - High speed radiography and tomography, with 100 microsecond temporal resolution. - Fluorescence tomography, imaging the 3-D distribution of elements present at ppm concentrations. - Radiographic strain measurements during deformation at high confining pressure, combined with precise x-ray diffraction measurements to determine stress. These techniques have been applied to important problems in earth and environmental sciences, including: - The 3-D distribution of aqueous and organic liquids in porous media, with applications in contaminated groundwater and petroleum recovery. - The kinetics of bubble formation in magma chambers, which control explosive volcanism. - Studies of the evolution of the early solar system from 3-D textures in meteorites - Accurate crystal size distributions in volcanic systems, important for understanding the evolution of magma chambers. - The equation-of-state of amorphous materials at high pressure using both direct measurements of volume as a function of pressure and also by measuring the change x-ray absorption coefficient as a function of pressure. - The location and chemical speciation of toxic

  8. Security of the Brazilian Amazon Area

    Science.gov (United States)

    1992-04-01

    Thk document may not be Mased fog openi puiks&adM tr it ha beat domed by the appropriate militarvice or TIC M AY5, 1921 SECURITY OF THE BRAZILIAN AMAZON...34Seguridad y Ecologia. Reforinulacion de tin concepto". Nueva Sociedad . (may/June 1990 - no 107): 21- 26. McIntyre, Loren. "Last Days of Eden

  9. Anthropometry of Brazilian Air Force pilots.

    Science.gov (United States)

    da Silva, Gilvan V; Halpern, Manny; Gordon, Claire C

    2017-10-01

    Anthropometric data are essential for the design of military equipment including sizing of aircraft cockpits and personal gear. Currently, there are no anthropometric databases specific to Brazilian military personnel. The aim of this study was to create a Brazilian anthropometric database of Air Force pilots. The methods, protocols, descriptions, definitions, landmarks, tools and measurements procedures followed the instructions outlined in Measurer's Handbook: US Army and Marine Corps Anthropometric Surveys, 2010-2011 - NATICK/TR-11/017. The participants were measured countrywide, in all five Brazilian Geographical Regions. Thirty-nine anthropometric measurements related to cockpit design were selected. The results of 2133 males and 206 females aged 16-52 years constitute a set of basic data for cockpit design, space arrangement issues and adjustments, protective gear and equipment design, as well as for digital human modelling. Another important implication is that this study can be considered a starting point for reducing gender bias in women's career as pilots. Practitioner Summary: This paper describes the first large-scale anthropometric survey of the Brazilian Air Force pilots and the development of the related database. This study provides critical data for improving aircraft cockpit design for ergonomics and comprehensive pilot accommodation, protective gear and uniform design, as well as digital human modelling.

  10. Spirometry reference values in the Brazilian population.

    Science.gov (United States)

    Rufino, R; Costa, C H; Lopes, A J; Maiworm, A I; Maynard, K; Silva, L M R A; Dias, R M

    2017-03-02

    The aim of the present study was to provide new spirometry reference equations in a sample of the Brazilian population for the following parameters: forced vital capacity (FVC), forced expiratory volume in 1 second (FEV1), FEV1/FVC ratio, peak of expiratory flow (PEF), forced expiratory flow at 50% (FEF50%), 75% average vital capacity (FEF25-75%), and average forced expiratory flow time (FEFT). This was a prospective study using results from chest radiographs, electrocardiograms, and questionnaires to investigate the participants' respiratory symptoms, sedentarism, and comorbidities (Charlson comorbidity index). From December 2010 to July 2014, individuals were randomly selected from various locations in the state of Rio de Janeiro. All individuals were examined by a single technician in the morning at the laboratory, and performed the spirometry with the same spirometer. Spirometry values were tabulated for the creation of three equation models: linear regression, logarithmic regression, and logarithms through a method that incorporates the lambda, median, and coefficient of variation (LMS method). Initially, 7003 individuals from both genders were contacted, and 454 were recruited. The data from the new equations were compared with one Brazilian and eight international equations, resulting in a high correlation (r>0.9). The values derived from the LMS method and linear regression were very similar (P>0.5), and both could be used to acquire the reference values for Brazilian spirometry. Data derived from the equations of this study were different from the current Brazilian equation, which could be justified by the different method used.

  11. A Grammar of Spoken Brazilian Portuguese.

    Science.gov (United States)

    Thomas, Earl W.

    This is a first-year text of Portuguese grammar based on the Portuguese of moderately educated Brazilians from the area around Rio de Janeiro. Spoken idiomatic usage is emphasized. An important innovation is found in the presentation of verb tenses; they are presented in the order in which the native speaker learns them. The text is intended to…

  12. Transcultural Diabetes Nutrition Algorithm: Brazilian Application

    Directory of Open Access Journals (Sweden)

    Fabio Moura

    2015-09-01

    Full Text Available The prevalence of obesity, pre-diabetes, and type 2 diabetes (T2D is increasing worldwide, especially in the developing nations of South America. Brazil has experienced an exponential increase in the prevalence of these chronic non-communicable diseases. The rising prevalence is probably due to changing eating patterns, sedentary living, and a progressive aging of the population. These trends and their underlying causes carry untoward consequences for all Brazilians and the future of Brazilian public health and the healthcare system. Lifestyle changes that include healthy eating (nutrition therapy and regular physical activity (structured exercise represent efficient inexpensive measures to prevent and/or treat the aforementioned disorders and are recommended for all afflicted patients. Regrettably, the implementation of lifestyle changes is fraught with clinical and personal challenges in real life. The transcultural Diabetes Nutrition Algorithm (tDNA is a therapeutic tool intended to foster implementation of lifestyle recommendations and to improve disease-related outcomes in common clinical settings. It is evidence-based and amenable to cultural adaptation. The Brazilian Diabetes Association, Society of Cardiology and Ministry of Health guidelines for nutrition therapy and physical exercise were considered for the Brazilian adaptation. The resultant tDNA-Brazil and its underlying recommendations are presented and explained.

  13. Brazilian Review of Finance 2012 Editorial Report

    Directory of Open Access Journals (Sweden)

    Ricardo Pereira Câmara Leal

    2013-03-01

    Full Text Available RBFin is the main Brazilian publication outlet of academic papers about finance. The contents of the Review are open and online; a printed version is maintained, in part, thanks to a grant from CNPq/CAPES. Using the Open Journals System to manage the editorial process, publication of RBFin adheres to a strict publication schedule. The journal is indexed by EconLit, Google Scholar, DOAJ, Gale and Ebsco and is listed in the JEL, Latindex, OpenJGate, and Cabell's directories. RBFin is rated B1 in the business area of the Brazilian classification system. The editorial board undergoes partial turnover every year and comprises 18 individuals from four countries, the Brazilian members being affiliated with universities in five different Brazilian states. The acceptance rate was 30% for papers submitted in 2010, the most recent year in which all submissions have already received a final decision. The average number of days between receipt and acceptance for all articles published in 2011 was 266. The worst case was 462 days. The average number of days between receipt and publication was 432. The worst case was 599 days. The average number of hits per article as of January 2012 was 1,249. Sixty-four individuals served as reviewers in 2011.

  14. Hemoglobin Variant Profiles among Brazilian Quilombola Communities.

    Science.gov (United States)

    Santiago, Rayra P; Oliveira, Rodrigo M; Soares, Leonardo F; Figueiredo, Camylla V B; Silva, Denise Oliveira; Hurtado-Guerrero, Ana F; Fiuza, Luciana M; Guarda, Caroline C; Adorno, Elisângela V; Barbosa, Cynara G; Gonçalves, Marilda S

    2017-03-01

    Brazilian Quilombolas are communities composed of African-derived populations that have their territories guaranteed by the Brazilian Constitution. The present study investigated the hemoglobin (Hb) variants among these population groups. This study was conducted in a total of 2843 individuals of Brazilian Quilombola communities of the Bahia, Pará, and Piauí states. All the participants had their Hb profiles evaluated. The Hb S (HBB: c.20A>T) variant was described in all the studied localities. However, the individuals in Bahia State had the highest frequency of the Hb C (HBB: c.19G>A) variant; individuals from Piauí State had a higher frequency of the Hb D-Punjab (HBB: c.364G>C) variant compared to the other states, and individuals from Pará State only carried the Hb S variant. The present study revealed a specific distribution of Hb variants that could represent different waves of African influence in these Brazilian populations.

  15. Selective logging in the Brazilian Amazon.

    Science.gov (United States)

    G. P. Asner; D. E. Knapp; E. N. Broadbent; P. J. C. Oliveira; M Keller; J. N. Silva

    2005-01-01

    Amazon deforestation has been measured by remote sensing for three decades. In comparison, selective logging has been mostly invisible to satellites. We developed a large-scale, high-resolution, automated remote-sensing analysis of selective logging in the top five timber-producing states of the Brazilian Amazon. Logged areas ranged from 12,075 to 19,823 square...

  16. The Brazilian investment in science and technology

    Directory of Open Access Journals (Sweden)

    Pinheiro-Machado R.

    2001-01-01

    Full Text Available An analysis of Brazilian federal expenditures in science and technology is presented is this study. The 1990-1999 data were compiled from records provided by two federal agencies (MCT and CNPq responsible for managing most of the national budget related to these activities. The results indicate that the federal investments in Brazilian science and technology stagnated during the last decade (US$ 2.32 billion in 1990, US$ 2.39 billion in 1996, and US$ 2.36 billion in 1999. In contrast, a great increase in private investments in research was acknowledged both by industry and by the government during the same period, from US$ 2.12 to US$ 4.64 billion. However, this investment did not result in an increase in invention patents granted to residents (492 in 1990 and only 232 in 1997 or in a reduction of patent costs. Despite this unfavorable scenario, the number of graduate programs in the country has increased two-fold in the last decade and the contribution of Brazilians to the database of the Institute for Scientific Information has increased 4.7-fold from 1990 (2,725 scientific publications to 2000 (12,686 scientific publications. Unstable federal resources for science, together with the poor returns of private resources in terms of developing new technologies, may jeopardize the future of Brazilian technological development.

  17. Lizards of Brazilian Amazonia (Reptilia: Squamata)

    NARCIS (Netherlands)

    Avila-Pires, T.C.S.

    1995-01-01

    Eighty-nine species of lizards, six of which polytypic (forming a total of 97 taxa), are presently known from Brazilian Amazonia. This number includes six species and one subspecies described as new to science in this paper: Stenocercus fimbriatus, Lepidoblepharis hoogmoedi, Leposoma osvaldoi, L.

  18. Bullying in Brazilian Schools and Restorative Practices

    Science.gov (United States)

    Grossi, Patricia Krieger; dos Santos, Andreia Mendes

    2012-01-01

    Bullying is a widespread phenomenon that affects many children and adolescents in Brazilian schools. A pilot research study was carried out in four schools (one private and three public) located in Porto Alegre, RS, Brazil. A combination of self-administered questionnaires and focus groups with students as well as interviews with teachers were…

  19. Translating Ovide Decroly's Ideas to Brazilian Teachers

    Science.gov (United States)

    Hai, Alessandra Arce; Simon, Frank; Depaepe, Marc

    2015-01-01

    This article seeks to analyse, comprehend and apprehend the appropriation processes of Ovide Decroly's ideas in Brazil through the translation of his books and that of Amélie Hamaïde into Portuguese. The article discusses the following questions. Why did Brazilian intellectuals and teachers need to import Decroly's ideas to be applied in Brazilian…

  20. Earning management in Brazilian financial institutions

    Directory of Open Access Journals (Sweden)

    Adriana Bruscato Bortoluzzo

    2016-06-01

    Full Text Available ABSTRACT The present study aims to study earnings management in a significant sample of 123 banks in the Brazilian market between 2001 and 2012. Given the important role that banks play in a country's economy, it is important to understand that there are discretionary factors involved in the reporting of a financial institution's profitability. Credit provisioning guidelines for Brazilian financial institutions are described in Resolution 2682/99 of the National Monetary Council (Conselho Monetário Nacional. Because of the discretion allowed in this resolution, loan loss provision is used as instrument of earnings management, which is not an illegal practice, but this behavior does affect the risk perception of agents and analysts, and they should be aware of it and understand it. We found that credit provisioning is used as an earnings management mechanism to smooth the net income of Brazilian financial institutions. Brazilian banks tend to avoid not only negative net income pre-loan loss provisions and taxes, but also negative net income pre-loan loss provisions and taxes in relation to the previous period. Contrary to the previous studies, it is not clear if banks avoid lower net income pre-loan loss provisions and taxes than a given peer group.

  1. Recent trends in Brazilian Historical Linguistics

    OpenAIRE

    SILVA, Rosa Virgínia Mattos e

    1999-01-01

    The paper concentrates on the new directions taken by Historical Linguistics in Brazil, which gives special attention to Brazilian Portuguese, studying dialectal and sociolinguistic aspects. A special reference is made to projects that bring together researchers from several universities in the country.

  2. Experiment on space charge driven nonlinear resonance crossing in an ion synchrotron

    Directory of Open Access Journals (Sweden)

    G. Franchetti

    2010-11-01

    Full Text Available Trapping of particles in nonlinear resonances in the presence of space charge and synchrotron motion may be a source of beam halo generation and beam loss in high intensity synchrotrons, in particular for extended storage times at the injection plateau as planned for the SIS100 synchrotron of the FAIR project. Although extensive simulation studies have theoretically demonstrated this mechanism, experimental evidence was so far limited to demonstration experiments at the CERN Proton Synchrotron (PS in 2002–2003 using an octupolar resonance. Here we describe new experiments at the SIS18 synchrotron at GSI, where the resonance is driven by a sextupolar field error and horizontal static tune scans are taken across the resonance stop band. The new data significantly extend the previous observations by a complete set of measurements comparing beams with and without rf, both at low and high intensity. The correlation between transverse beam loss and simultaneous bunch length shortening provides strong evidence that the measured emittance and the loss in intensity are indeed caused by periodic resonance crossing, leading to the main effect of scattering but also to a lesser extent to the trapping of particles due to the combined effect of the nonlinear resonance and the space charge.

  3. Evaluating scintillator performance in time-resolved hard X-ray studies at synchrotron light sources

    Energy Technology Data Exchange (ETDEWEB)

    Rutherford, Michael E.; Chapman, David J.; White, Thomas G. [Imperial College London, London (United Kingdom); Drakopoulos, Michael [Diamond Light Source, I12 Joint Engineering, Environmental, Processing (JEEP) Beamline, Didcot, Oxfordshire (United Kingdom); Rack, Alexander [European Synchrotron Radiation Facility, Grenoble (France); Eakins, Daniel E., E-mail: d.eakins@imperial.ac.uk [Imperial College London, London (United Kingdom)

    2016-03-24

    Scintillator performance in time-resolved, hard, indirect detection X-ray studies on the sub-microsecond timescale at synchrotron light sources is reviewed, modelled and examined experimentally. LYSO:Ce is found to be the only commercially available crystal suitable for these experiments. The short pulse duration, small effective source size and high flux of synchrotron radiation is ideally suited for probing a wide range of transient deformation processes in materials under extreme conditions. In this paper, the challenges of high-resolution time-resolved indirect X-ray detection are reviewed in the context of dynamic synchrotron experiments. In particular, the discussion is targeted at two-dimensional integrating detector methods, such as those focused on dynamic radiography and diffraction experiments. The response of a scintillator to periodic synchrotron X-ray excitation is modelled and validated against experimental data collected at the Diamond Light Source (DLS) and European Synchrotron Radiation Facility (ESRF). An upper bound on the dynamic range accessible in a time-resolved experiment for a given bunch separation is calculated for a range of scintillators. New bunch structures are suggested for DLS and ESRF using the highest-performing commercially available crystal LYSO:Ce, allowing time-resolved experiments with an interframe time of 189 ns and a maximum dynamic range of 98 (6.6 bits)

  4. Elemental concentration analysis in brain structures from young, adult and old Wistar rats by total reflection X-ray fluorescence with synchrotron radiation

    Science.gov (United States)

    Serpa, R. F. B.; de Jesus, E. F. O.; Anjos, M. J.; do Carmo, M. G. T.; Moreira, S.; Rocha, M. S.; Martinez, A. M. B.; Lopes, R. T.

    2006-11-01

    The knowledge of the spatial distribution and the local concentration of trace elements in tissues are of great importance since trace elements are involved in a number of metabolic and physiological processes in the human body, and their deficiency and excess may lead to different metabolic disorders. In this way, the main goal of this work is to compare the elemental concentration in different brain structures, namely temporal cortex, entorhinal cortex, visual cortex and hippocampus, from Wistar female rats ( n = 15) with different ages: 2, 8 and 48 weeks. The measurements were performed at the Synchrotron Light Brazilian Laboratory, Campinas, São Paulo, Brazil. In the entorhinal cortex, the following elements decreased with age: Zn, S, Cl, K, Ca and Br. In the temporal cortex, Ca, Fe and Br levels increased with aging and on the other hand, P, S, Cl, K and Rb levels decreased with aging. In the visual cortex almost all the elements decreased with aging: Cl, Ca, Fe, Ni and Zn. In the hippocampus, in turn, most of the elements identified, increased with aging: Al, P, S, K, Fe, Cu, Zn and Rb. The increase of Fe with aging in the hippocampus is an important fact that will be studied, since it is involved in oxidative stress. It is believed that oxidative stress is the one of the main causes responsible for neuronal death in Parkinson's disease.

  5. Synchrotron FTIR imaging of OH in quartz mylonites

    Directory of Open Access Journals (Sweden)

    A. K. Kronenberg

    2017-10-01

    Full Text Available Previous measurements of water in deformed quartzites using conventional Fourier transform infrared spectroscopy (FTIR instruments have shown that water contents of larger grains vary from one grain to another. However, the non-equilibrium variations in water content between neighboring grains and within quartz grains cannot be interrogated further without greater measurement resolution, nor can water contents be measured in finely recrystallized grains without including absorption bands due to fluid inclusions, films, and secondary minerals at grain boundaries.Synchrotron infrared (IR radiation coupled to a FTIR spectrometer has allowed us to distinguish and measure OH bands due to fluid inclusions, hydrogen point defects, and secondary hydrous mineral inclusions through an aperture of 10 µm for specimens > 40 µm thick. Doubly polished infrared (IR plates can be prepared with thicknesses down to 4–8 µm, but measurement of small OH bands is currently limited by strong interference fringes for samples < 25 µm thick, precluding measurements of water within individual, finely recrystallized grains. By translating specimens under the 10 µm IR beam by steps of 10 to 50 µm, using a software-controlled x − y stage, spectra have been collected over specimen areas of nearly 4.5 mm2. This technique allowed us to separate and quantify broad OH bands due to fluid inclusions in quartz and OH bands due to micas and map their distributions in quartzites from the Moine Thrust (Scotland and Main Central Thrust (Himalayas.Mylonitic quartzites deformed under greenschist facies conditions in the footwall to the Moine Thrust (MT exhibit a large and variable 3400 cm−1 OH absorption band due to molecular water, and maps of water content corresponding to fluid inclusions show that inclusion densities correlate with deformation and recrystallization microstructures. Quartz grains of mylonitic orthogneisses and paragneisses deformed

  6. Unexpected methyl migrations of ethanol dimer under synchrotron VUV radiation

    Energy Technology Data Exchange (ETDEWEB)

    Xiao, Weizhan; Hu, Yongjun, E-mail: yjhu@scnu.edu.cn, E-mail: lssheng@ustc.edu.cn; Li, Weixing; Guan, Jiwen [MOE Key Laboratory of Laser Life Science and Institute of Laser Life Science, College of Biophotonics, South China Normal University, Guangzhou 510631 (China); Liu, Fuyi; Shan, Xiaobin; Sheng, Liusi, E-mail: yjhu@scnu.edu.cn, E-mail: lssheng@ustc.edu.cn [National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029 (China)

    2015-01-14

    While methyl transfer is well known to occur in the enzyme- and metal-catalyzed reactions, the methyl transfer in the metal-free organic molecules induced by the photon ionization has been less concerned. Herein, vacuum ultraviolet single photon ionization and dissociation of ethanol dimer are investigated with synchrotron radiation photoionization mass spectroscopy and theoretical methods. Besides the protonated clusters cation (C{sub 2}H{sub 5}OH) ⋅ H{sup +} (m/z = 47) and the β-carbon-carbon bond cleavage fragment CH{sub 2}O ⋅ (C{sub 2}H{sub 5}OH)H{sup +} (m/z = 77), the measured mass spectra revealed that a new fragment (C{sub 2}H{sub 5}OH) ⋅ (CH{sub 3}){sup +} (m/z = 61) appeared at the photon energy of 12.1 and 15.0 eV, where the neutral dimer could be vertically ionized to higher ionic state. Thereafter, the generated carbonium ions are followed by a Wagner-Meerwein rearrangement and then dissociate to produce this new fragment, which is considered to generate after surmounting a few barriers including intra- and inter-molecular methyl migrations by the aid of theoretical calculations. The appearance energy of this new fragment is measured as 11.55 ± 0.05 eV by scanning photoionization efficiency curve. While the signal intensity of fragment m/z = 61 starts to increase, the fragments m/z = 47 and 77 tend to slowly incline around 11.55 eV photon energy. This suggests that the additional fragment channels other than (C{sub 2}H{sub 5}OH) ⋅ H{sup +} and CH{sub 2}O ⋅ (C{sub 2}H{sub 5}OH)H{sup +} have also been opened, which consume some dimer cations. The present report provides a clear description of the photoionization and dissociation processes of the ethanol dimer in the range of the photon energy 12-15 eV.

  7. Geoscience Applications of Synchrotron X-ray Computed Microtomography

    Science.gov (United States)

    Rivers, M. L.

    2009-05-01

    Computed microtomography is the extension to micron spatial resolution of the CAT scanning technique developed for medical imaging. Synchrotron sources are ideal for the method, since they provide a monochromatic, parallel beam with high intensity. High energy storage rings such as the Advanced Photon Source at Argonne National Laboratory produce x-rays with high energy, high brilliance, and high coherence. All of these factors combine to produce an extremely powerful imaging tool for earth science research. Techniques that have been developed include: - Absorption and phase contrast computed tomography with spatial resolution approaching one micron - Differential contrast computed tomography, imaging above and below the absorption edge of a particular element - High-pressure tomography, imaging inside a pressure cell at pressures above 10GPa - High speed radiography, with 100 microsecond temporal resolution - Fluorescence tomography, imaging the 3-D distribution of elements present at ppm concentrations. - Radiographic strain measurements during deformation at high confining pressure, combined with precise x- ray diffraction measurements to determine stress. These techniques have been applied to important problems in earth and environmental sciences, including: - The 3-D distribution of aqueous and organic liquids in porous media, with applications in contaminated groundwater and petroleum recovery. - The kinetics of bubble formation in magma chambers, which control explosive volcanism. - Accurate crystal size distributions in volcanic systems, important for understanding the evolution of magma chambers. - The equation-of-state of amorphous materials at high pressure using both direct measurements of volume as a function of pressure and also by measuring the change x-ray absorption coefficient as a function of pressure. - The formation of frost flowers on Arctic sea-ice, which is important in controlling the atmospheric chemistry of mercury. - The distribution of

  8. Synchrotron FTIR imaging of OH in quartz mylonites

    Energy Technology Data Exchange (ETDEWEB)

    Kronenberg, Andreas K.; Hasnan, Hasnor F. B.; Holyoke III, Caleb W.; Law, Richard D.; Liu, Zhenxian; Thomas, Jay B.

    2017-01-01

    Previous measurements of water in deformed quartzites using conventional Fourier transform infrared spectroscopy (FTIR) instruments have shown that water contents of larger grains vary from one grain to another. However, the non-equilibrium variations in water content between neighboring grains and within quartz grains cannot be interrogated further without greater measurement resolution, nor can water contents be measured in finely recrystallized grains without including absorption bands due to fluid inclusions, films, and secondary minerals at grain boundaries.

    Synchrotron infrared (IR) radiation coupled to a FTIR spectrometer has allowed us to distinguish and measure OH bands due to fluid inclusions, hydrogen point defects, and secondary hydrous mineral inclusions through an aperture of 10 µm for specimens > 40 µm thick. Doubly polished infrared (IR) plates can be prepared with thicknesses down to 4–8 µm, but measurement of small OH bands is currently limited by strong interference fringes for samples < 25 µm thick, precluding measurements of water within individual, finely recrystallized grains. By translating specimens under the 10 µm IR beam by steps of 10 to 50 µm, using a software-controlled x-y stage, spectra have been collected over specimen areas of nearly 4.5 mm2. This technique allowed us to separate and quantify broad OH bands due to fluid inclusions in quartz and OH bands due to micas and map their distributions in quartzites from the Moine Thrust (Scotland) and Main Central Thrust (Himalayas).

    Mylonitic quartzites deformed under greenschist facies conditions in the footwall to the Moine Thrust (MT) exhibit a large and variable 3400 cm-1 OH absorption band due to molecular water, and maps of water content corresponding to fluid inclusions show that inclusion densities correlate with deformation and recrystallization microstructures. Quartz grains of mylonitic orthogneisses and

  9. [Brazilian colonization in the Paraguayan agricultural frontier].

    Science.gov (United States)

    Neupert, R F

    1991-04-01

    This work briefly describes Brazilian colonization of the Paraguayan agricultural frontier, analyzes factors responsible for expelling population from Brazil and for attracting Brazilians to Paraguay, and assesses the economic and social consequences of immigration to the area. Paraguay's vast and sparsely populated agricultural frontier in areas outside the Central subregion underwent a process of intense colonization from the early 1960s to the mid-1980s. The Paraguayan government initiated an ambitious colonization program in 1963 to increase production, relieve population pressure and subdivision of small parcels in the Central subregion, encourage agricultural modernization, and produce a more diversified agriculture. Paraguayan agriculture in the early 1960s suffered from excessive concentration of land in a few hands and resulting exclusion of around 3/4 of workers from ownership and from any possibility of obtaining credit to fund technological improvements. Results of studies 2 decades after implementation of the colonization plan suggest that it has failed in significant areas. Although a considerable population redistribution alleviated pressure in the Central subregion, it apparently resulted more from spontaneous movement of peasants outside the colonization areas than from the official program. Concentration of lands is now occurring in the colonization area. Assistance for agricultural modernization and diversification of production in the peasant sector has been minimal. On the other hand, production of soy, wheat, and cotton for export increased substantially, because of an entrepreneurial agriculture capitalized by foreign as well as national interests The unmet goals of the colonization program would have required structural reforms rather than simple spatial redistribution of the population. Many of the colonists in the 1970s were Brazilian families displaced by mechanized agriculture in the southern states of Parana, Santa Catarina, and Rio

  10. A single-photon counting “edge-on” silicon detector for synchrotron radiation mammography

    Science.gov (United States)

    Rigon, L.; Arfelli, F.; Astolfo, A.; Bergamaschi, A.; Dreossi, D.; Longo, R.; Menk, R.-H.; Schmitt, B.; Vallazza, E.; Castelli, E.

    2009-09-01

    The Phase Imaging for Clinical Application with Silicon detector and Synchrotron radiatiOn (PICASSO) project is developing an "edge-on" silicon microstrip detector for mammography with synchrotron radiation. The sensor is equipped with a fast single-photon counting electronics based on the Mythen-II application-specific integrated circuit. A first prototype has been assembled and tested at the SYnchrotron Radiation for MEdical Physics (SYRMEP) beamline at Elettra in Trieste, Italy. The first results are presented in this study including evidence of high-rate single-photon counting with negligible losses up to 1.2×10 6 incident photons per pixel per second; spatial resolution consistent with the pixel aperture (0.3 mm×0.05 mm); high-quality imaging of test-objects, obtained with a dose comparable to the one delivered in modern full-field digital mammographic systems.

  11. Synchrotron Radiation Effects in the IR Solenoid Flux Excluder(LCC-0007)

    Energy Technology Data Exchange (ETDEWEB)

    Tenenbaum, P

    2004-04-22

    We examine the emittance dilution due to synchrotron radiation in the fringing fields at the end of the ''flux excluder'' solenoid which protects the final doublet quadrupoles from the main detector solenoid field, and also the effect of SR in the main solenoid field itself.Because the deflection due to the excluder fringe field is opposite in polarity from that of the main solenoid, the resulting dispersive rays cancel at the IP; as a result the synchrotron radiation from the two magnetic fields produces only a small dilution of the vertical spot size. The contribution to the spot size from the finite opening angle of the synchrotron flux is found to be comparable to the contribution from solenoidal dispersion, and both are acceptable. We conclude that SR considerations do not rule out use of a flux excluder, and that the range of crossing angles and solenoidal fields available is large.

  12. Monte Carlo simulations of ultra high vacuum and synchrotron radiation for particle accelerators

    CERN Document Server

    AUTHOR|(CDS)2082330; Leonid, Rivkin

    With preparation of Hi-Lumi LHC fully underway, and the FCC machines under study, accelerators will reach unprecedented energies and along with it very large amount of synchrotron radiation (SR). This will desorb photoelectrons and molecules from accelerator walls, which contribute to electron cloud buildup and increase the residual pressure - both effects reducing the beam lifetime. In current accelerators these two effects are among the principal limiting factors, therefore precise calculation of synchrotron radiation and pressure properties are very important, desirably in the early design phase. This PhD project shows the modernization and a major upgrade of two codes, Molflow and Synrad, originally written by R. Kersevan in the 1990s, which are based on the test-particle Monte Carlo method and allow ultra-high vacuum and synchrotron radiation calculations. The new versions contain new physics, and are built as an all-in-one package - available to the public. Existing vacuum calculation methods are overvi...

  13. Stanford Synchrotron Radiation Laboratory 1991 activity report. Facility developments January 1991--March 1992

    Energy Technology Data Exchange (ETDEWEB)

    Cantwell, K.; St. Pierre, M. [eds.

    1992-12-31

    SSRL is a national facility supported primarily by the Department of Energy for the utilization of synchrotron radiation for basic and applied research in the natural sciences and engineering. It is a user-oriented facility which welcomes proposals for experiments from all researchers. The synchrotron radiation is produced by the 3.5 GeV storage ring, SPEAR, located at the Stanford Linear Accelerator Center (SLAC). SPEAR is a fully dedicated synchrotron radiation facility which operates for user experiments 7 to 9 months per year. SSRL currently has 24 experimental stations on the SPEAR storage ring. There are 145 active proposals for experimental work from 81 institutions involving approximately 500 scientists. There is normally no charge for use of beam time by experimenters. This report summarizes the activity at SSRL for the period January 1, 1991 to December 31, 1991 for research. Facility development through March 1992 is included.

  14. Finite element analysis of the distortion of a crystal monochromator from synchrotron radiation thermal loading

    Energy Technology Data Exchange (ETDEWEB)

    Edwards, W.R.; Hoyer, E.H.; Thompson, A.C.

    1985-10-01

    The first crystal of the Brown-Hower x-ray monochromator of the LBL-EXXON 54 pole wiggler beamline at Stanford Synchrotron Radiation Laboratory (SSRL) is subjected to intense synchrotron radiation. To provide an accurate thermal/structural analysis of the existing monochromator design, a finite element analysis (FEA) was performed. A very high and extremely localized heat flux is incident on the Si (220) crystal. The crystal, which possesses pronouncedly temperature-dependent orthotropic properties, in combination with the localized heat load, make the analysis ideally suited for finite element techniques. Characterization of the incident synchrotron radiation is discussed, followed by a review of the techniques employed in modeling the monochromator and its thermal/structural boundary conditions. The results of the finite element analysis, three-dimensional temperature distributions, surface displacements and slopes, and stresses, in the area of interest, are presented. Lastly, the effects these results have on monochromator output flux and resolution are examined.

  15. Ultraintense laser absorption and γ-ray synchrotron radiation in near critical density plasmas

    Science.gov (United States)

    Chang, H. X.; Qiao, B.; Zhang, Y. X.; Xu, Z.; Yao, W. P.; Zhou, C. T.; He, X. T.

    2017-04-01

    Ultraintense laser absorption and γ-ray synchrotron radiation in near-critical-density (NCD) plasmas are investigated. Besides the known skin-depth emission and reinjected electron synchrotron emission in NCD plasmas, we find a new γ-ray emission mechanism, where γ-rays are dominantly produced by the Transversely Oscillating Electron synchrotron Emission (TOEE). In this new TOEE mechanism, electrons mainly oscillate in the transverse direction under the balance between the longitudinal laser ponderomotive force and the restoring electrostatic force. A great amount of γ photons are emitted in the transverse direction, where the peak radiation power is enhanced by twice and the photon divergence angle is relatively decreased. The features of γ-rays produced from this new TOEE mechanism have been identified and compared with the other two mechanisms by two-dimensional particle-in-cell simulations.

  16. Applications of Synchrotron Radiation Micro Beams in Cell Micro Biology and Medicine

    CERN Document Server

    Ide-Ektessabi, Ari

    2007-01-01

    This book demonstrates the applications of synchrotron radiation in certain aspects of cell microbiology, specifically non-destructive elemental analyses, chemical-state analyses and imaging (distribution) of the elements within a cell. The basics for understanding and applications of synchrotron radiation are also described to make the contents easier to be understood for a wide group of researchers in medical and biological sciences who might not be familiar with the physics of synchrotron radiation. The two main techniques that are discussed in this book are the x-ray fluorescence spectroscopy (XRF) and the x-ray fine structure analysis (XAFS). Application of these techniques in investigations of several important scientific fields, such as neurodegeneration and other diseases related to cell malfunctioning, are demonstrated in this book.

  17. Analysis of cortical bone porosity using synchrotron radiation microtomography to evaluate the effects of chemotherapy

    Science.gov (United States)

    Alessio, R.; Nogueira, L. P.; Salata, C.; Mantuano, A.; Almeida, A. P.; Braz, D.; de Almeida, C. E.; Tromba, G.; Barroso, R. C.

    2015-11-01

    Microporosities play important biologic and mechanical roles on health. One of the side effects caused by some chemotherapy drugs is the induction of amenorrhea, temporary or not, in premenopausal women, with a consequent decrease in estrogen production, which can lead to cortical bone changes. In the present work, the femur diaphysis of rats treated with chemotherapy drugs were evaluated by 3D morphometric parameters using synchrotron radiation microtomography. Control animals were also evaluated for comparison. The 3D tomographic images were obtained at the SYRMEP (SYnchrotron Radiation for MEdical Physics) beamline at the ELETTRA Synchrotron Laboratory in Trieste, Italy. Results showed significant differences in morphometric parameters measured from the 3D images of femur diaphysis of rats.

  18. Synchrotron radiation X-ray powder diffraction techniques applied in hydrogen storage materials - A review

    Directory of Open Access Journals (Sweden)

    Honghui Cheng

    2017-02-01

    Full Text Available Synchrotron radiation is an advanced collimated light source with high intensity. It has particular advantages in structural characterization of materials on the atomic or molecular scale. Synchrotron radiation X-ray powder diffraction (SR-XRPD has been successfully exploited to various areas of hydrogen storage materials. In the paper, we will give a brief introduction on hydrogen storage materials, X-ray powder diffraction (XRPD, and synchrotron radiation light source. The applications of ex situ and in situ time-resolved SR-XRPD in hydrogen storage materials, are reviewed in detail. Future trends and proposals in the applications of the advanced XRPD techniques in hydrogen storage materials are also discussed.

  19. PROTON SYNCHROTRON RADIATION FROM EXTENDED JETS OF PKS 0637–752 AND 3C 273

    Energy Technology Data Exchange (ETDEWEB)

    Bhattacharyya, Wrijupan; Gupta, Nayantara, E-mail: wriju.phys@gmail.com [Raman Research Institute, C. V. Raman Avenue, Sadashivanagar, Bangalore 560080 (India)

    2016-02-01

    Many powerful radio quasars are associated with large-scale jets, exhibiting bright knots as shown by high-resolution images from the Hubble Space Telescope (HST) and the Chandra X-ray Observatory. The radio-optical flux component from these jets can be attributed to synchrotron radiation by accelerated relativistic electrons while the IC/CMB model, by far, has been the most popular explanation for the observed X-ray emission from these jets. Recently, the IC/CMB X-ray mechanism has been strongly disfavored for 3C 273 and PKS 0637–752 since the anomalously hard and steady gamma-ray emission predicted by such models violates the observational results from Fermi-LAT. Here we propose the proton synchrotron origin of the X-ray–gamma-ray flux from the knots of PKS 0637–752 with a reasonable budget in luminosity, by considering synchrotron radiation from an accelerated proton population. Moreover, for the source 3C 273, the optical data points near 10{sup 15} Hz could not be fitted using electron synchrotron. We propose an updated proton synchrotron model, including the optical data from HST, to explain the common origin of optical-X-ray–gamma-ray emission from the knots of quasar 3C 273 as an extension of the work done by Kundu and Gupta. We also show that TeV emission from large-scale quasar jets, in principle, can arise from proton synchrotron, which we discuss in the context of knot wk8.9 of PKS 0637–752.

  20. Probes of turbulent driving mechanisms in molecular clouds from fluctuations in synchrotron intensity

    Science.gov (United States)

    Herron, C. A.; Federrath, C.; Gaensler, B. M.; Lewis, G. F.; McClure-Griffiths, N. M.; Burkhart, Blakesley

    2017-04-01

    Previous studies have shown that star formation depends on the driving of molecular cloud turbulence, and differences in the driving can produce an order of magnitude difference in the star formation rate. The turbulent driving is characterized by the parameter ζ, with ζ = 0 for compressive, curl-free driving (e.g. accretion or supernova explosions), and ζ = 1 for solenoidal, divergence-free driving (e.g. Galactic shear). Here we develop a new method to measure ζ from observations of synchrotron emission from molecular clouds. We calculate statistics of mock synchrotron intensity images produced from magnetohydrodynamic simulations of molecular clouds, in which the driving was controlled to produce different values of ζ. We find that the mean and standard deviation of the log-normalized synchrotron intensity are sensitive to ζ, for values of ζ between 0 (curl-free driving) and 0.5 (naturally mixed driving). We quantify the dependence of zeta on the direction of the magnetic field relative to the line of sight. We provide best-fitting formulae for ζ in terms of the log-normalized mean and standard deviation of synchrotron intensity, with which ζ can be determined for molecular clouds that have similar Alfvénic Mach number to our simulations. These formulae are independent of the sonic Mach number. Signal-to-noise ratios larger than 5, and angular resolutions smaller than 5 per cent of the cloud diameter, are required to apply these formulae. Although there are no firm detections of synchrotron emission from molecular clouds, by combining Green Bank Telescope and Very Large Array observations it should be possible to detect synchrotron emission from molecular clouds, thereby constraining the value of ζ.

  1. Analysis of the Brazilian Entrepreneurial Ecosystem

    Directory of Open Access Journals (Sweden)

    Edmundo Inácio Júnior

    2016-01-01

    Full Text Available The objective of this study was to analyze the Brazilian entrepreneurial ecosystem in the light of the National System of Entrepreneurship – NSE theory, through the implementation of the Global Entrepreneurship Index methodology – GEI. The study indicates that Brazil has low quality average institutional interaction. However, social context is the main bottleneck in the national entrepreneurial ecosystem. Differences between the performance quality of the institutional framework and social factors promote entrepreneurship low socioeconomic impact. The results of the article show that the Brazilian entrepreneurial ecosystem presents low internationalization of companies, innovation in pro- ducts and processes, formation of human capital and high-growth enterprises. The results of the article provide insights for decision makers on the factors that determine the opening of new businesses.

  2. Evaluating efficiency in the Brazilian trucking industry

    Directory of Open Access Journals (Sweden)

    Peter Fernandes Wanke

    2013-09-01

    Full Text Available The purpose of this study is to investigate the issue of efficiency in the Brazilian motor carrier industry using both DEA (Data Envelopment Analysis and SFA (Stochastic Frontier Analysis in a complimentary fashion. The study is based on secondary data collected from Transporte Moderno/Maiores e Melhores, a specialized magazine that annually reports statistics on the largest Brazilian trucking companies. Results corroborate not only that increasing returns to scale prevail within this industry, but also provide support for a moderate impact of economies of scope on efficiency levels. Implications in terms of mergers and acquisitions and the impact of cargo diversity and the geographical scope of the operation on virtual efficiency levels are also addressed.

  3. Evaluating efficiency in the Brazilian trucking industry

    Directory of Open Access Journals (Sweden)

    Peter Fernandes Wanke

    2012-01-01

    Full Text Available The purpose of this study is to investigate the issue of efficiency in the Brazilian motor carrier industry using both DEA (Data Envelopment Analysis and SFA (Stochastic Frontier Analysis in a complimentary fashion. The study is based on secondary data collected from Transporte Moderno/Maiores e Melhores, a specialized magazine that annually reports statistics on the largest Brazilian trucking companies. Results corroborate not only that increasing returns to scale prevail within this industry, but also provide support for a moderate impact of economies of scope on efficiency levels. Implications in terms of mergers and acquisitions and the impact of cargo diversity and the geographical scope of the operation on virtual efficiency levels are also addressed.

  4. Aspectual Verbs in European and Brazilian Portuguese

    Directory of Open Access Journals (Sweden)

    Fátima Oliveira

    2004-06-01

    Full Text Available This paper is about the semantics and the syntax of aspectual verbs in European and Brazilian Portuguese. Some of these verbs select a+Infinitive in the European variety whereas the same verbs select that structure and Gerund in the Brazilian variety. We show that this discrepancy can be explained in semantic and syntactic grounds due to the different nature of the semantic ‘input’ (stative or eventive, the availability of tense constructions and the functional structure of the embedded domain. Another group of aspectual verbs do not differ in their syntactic structure in the two varieties as their structure (de+Infinitive is the same, although syntactically different from a+ Infinitive, but they do differ in their semantics and also in the selection of different verbs.

  5. TRADING FORWARD IN THE BRAZILIAN ELECTRICITY MARKET

    Directory of Open Access Journals (Sweden)

    Paulo Cesar Coutinho

    2013-01-01

    Full Text Available We study the interaction between forward and spot electricity markets in a scenario where buyers and sellers are price takers in the forward market and trade through marketers, who play a Cournot game. Our model’s main features come from the Brazilian electricity market, where a free contract market coexists with a regulated contract market, and the spot price is the output of a stochastic dynamic algorithm. We are able to show that the price of energy bought (sold forward decreases (increases with the number of marketers, and that, as a result, full hedging is achieved in the limit. We also investigate the effects on prices of changes in the number of market participants and in aggregate consumption and supply, an exercise that yields important policy recommendations for the Brazilian regulator.

  6. Genetic base of Brazilian irrigated rice cultivars

    Directory of Open Access Journals (Sweden)

    Hudson de Oliveira Rabelo

    2015-08-01

    Full Text Available The aim of this study was to estimate the genetic base of Brazilian irrigated rice cultivars released in the period from 1965 to 2012. The genealogies of the cultivars were obtained based on information from marketing folders, websites, crossings records, and scientific articles. The following factors were calculated: relative genetic contribution (RGC, accumulated genetic contribution (AGC, frequency (in percentage of each ancestor in the genealogy (FAG, number of ancestors that constitute each cultivar (NAC,number of ancestors responsible for 60%, 70%, 80% and 90% of the genetic base (NAGB, and average number of ancestor per cultivar (ANAC. The cultivars were also grouped based on the period of release (1965-1980, 1981-1990, 1991-2000 and 2001-2012. For each grouping, the previously described factors were also estimated. A total of 110 cultivars were studied and it was concluded that the genetic base of Brazilian irrigated rice cultivars is narrow.

  7. Antimicrobial resistance among Brazilian Corynebacterium diphtheriae strains.

    Science.gov (United States)

    Pereira, Gabriela Andrade; Pimenta, Fabrícia Pires; Santos, Fátima Rejane Wink dos; Damasco, Paulo Vieira; Hirata Júnior, Raphael; Mattos-Guaraldi, Ana Luíza

    2008-08-01

    The increasing problems with multidrug resistance in relation to Corynebacterium, including C. diphtheriae, are examples of challenges confronting many countries. For this reason, Brazilian C. diphtheriae strains were evaluated by the E-Test for their susceptibility to nine antibacterial drugs used in therapy. Resistance (MIC tested. Although erythromycin (MIC90 0.75 microg/ml) and azithromycin (MIC90 0.064 microg/ml) were active against C. diphtheriae in this study, 4.2% of the strains showed decreased susceptibility (MIC 1.0 microg/ml) to erythromycin. Multiple resistance profiles were determined by the disk diffusion method using 31 antibiotics. Most C. diphtheriae strains (95.74%) showed resistance to mupirocin, aztreonam, ceftazidime, and/or oxacillin, ampicillin, penicillin, tetracycline, clindamycin, lincomycin, and erythromycin. This study presents the antimicrobial susceptibility profiles of Brazilian C. diphtheriae isolates. The data are of value to practitioners, and suggest that some concern exists regarding the use of penicillin.

  8. Brazilian agroforestry systems for cattle and sheep

    Directory of Open Access Journals (Sweden)

    Roberto G. de Almeida

    2013-12-01

    Full Text Available Agroforestry systems for animal husbandry in Brazil, including integrated crop-livestock-forest systems (ICLF, are very diverse, and present several technical, environmental and socio-economic benefits. For each of the country’s 5 regions (Southeast, Central-West, North, Northeast and South the prevailing agroforestry systems holding animals are presented, their potential and constraints discussed and research needs identified. In general, such systems are not broadly adopted, mainly because of their level of complexity compared with traditional systems, as well as some lack of understanding by farmers regarding their benefits. To change this situation, in the last 5 years, the Brazilian Government has allocated financial resources in terms of credit for development as well as for research and technology transfer addressing ICLF systems, including good agricultural practices and mitigation of greenhouse gas emissions. The goal is to improve competitiveness of the Brazilian agribusiness sector.

  9. Characterization of Polycrystalline Materials Using Synchrotron X-ray Imaging and Diffraction Techniques

    DEFF Research Database (Denmark)

    Ludwig, Wolfgang; King, A.; Herbig, M.

    2010-01-01

    The combination of synchrotron radiation x-ray imaging and diffraction techniques offers new possibilities for in-situ observation of deformation and damage mechanisms in the bulk of polycrystalline materials. Minute changes in electron density (i.e., cracks, porosities) can be detected using...... propagation based phase contrast imaging, a 3-D imaging mode exploiting the coherence properties of third generation synchrotron beams. Furthermore, for some classes of polycrystalline materials, one may use a 3-D variant of x-ray diffraction imaging, termed x-ray diffraction contrast tomography. X-ray...

  10. Heavy Ion Injection Into Synchrotrons, Based On Electron String Ion Sources

    CERN Document Server

    Donets, E E; Syresin, E M

    2004-01-01

    A possibility of heavy ions injection into synchrotrons is discussed on the base of two novel ion sources, which are under development JINR during last decade: 1) the electron string ion source (ESIS), which is a modified version of a conventional electron beam ion source (EBIS), working in a reflex mode of operation, and 2) the tubular electron string ion source (TESIS). The Electron String Ion Source "Krion-2" (VBLHE, JINR, Dubna) with an applied confining magnetic field of 3 T was used for injection into the superconducting JINR synchrotron - Nuclotron and during this runs the source provided a high pulse intensity of the highly charged ion beams: Ar16+

  11. Radio galaxies radiation transfer, dynamics, stability and evolution of a synchrotron plasmon

    CERN Document Server

    Pacholczyk, A G

    1977-01-01

    Radio Galaxies: Radiation Transfer, Dynamics, Stability and Evolution of a Synchrotron Plasmon deals with the physics of a region in space containing magnetic field and thermal and relativistic particles (a plasmon). The synchrotron emission and absorption of this region are discussed, along with the properties of its spectrum; its linear and circular polarization; transfer of radiation through such a region; its dynamics and expansion; and interaction with external medium.Comprised of eight chapters, this volume explores the stability, turbulence, and acceleration of particles in a synchrotro

  12. Study of a Rapid Cycling Synchrotron to replace the CERN PS Booster

    CERN Document Server

    Hanke, K; Angoletta, M E; Balhan, B; Bartmann, W; Benedikt, M; Borburgh, J; Bozzini, D; Carli, C; Dahlen, P; Dobers, T; Fitterer, M; Garoby, R; Gilardoni, S; Goddard, B; Hansen, J; Hermanns, T; Lopez-Hernandez, L A; Hourican, M; Jensen, S; Kosmicki, A; Meddahi, M; Mikulec, B; Newborough, A; Nonis, M; Olek, S; Paoluzzi, M; Pittet, S; Puccio, B; Raginel, V; Ruehl, I; Schönauer, H; Sermeus, L; Steerenberg, R; Tan, J; Tückmantel, J; Vretenar, M; Widorski, M

    2011-01-01

    CERN’s proton injector chain is undergoing a massive consolidation and upgrade program in order to deliver beams meeting the needs of the LHC Luminosity Upgrade. As an alternative to the upgrade of the existing Proton Synchrotron Booster (PSB), the construction of a Rapid Cycling Synchrotron (RCS) has been studied. This machine would replace the PSB and deliver beams to the LHC as well as to CERN’s rich fixed-target physics program. This paper summarizes the outcome of the feasibility study along with a tentative RCS design.

  13. First Observation of the LHC Beam Halo Using a Synchrotron Radiation Coronagraph

    OpenAIRE

    Mitsuhashi, Toshiyuki; Bravin, Enrico; Roncarolo, Federico; Trad, Georges

    2017-01-01

    A test coronagraph for the observation of beam halo has been installed in the Synchrotron radiation monitor line LHCB2 in 2015. This coronagraph is commissioned with LHC operation at 450GeV (injection energy). After some optical testing of the coronagraph with visible Synchrotron radiation in B2, we try to observe artificially-made beam halo. The beam halo of 10⁻³ order of magnitude against the beam core is excited by the kicker of the transverse damper. We have succeeded to observe a diffrac...

  14. Synchrotron X-ray CT characterization of titanium parts fabricated by additive manufacturing. Part I. Morphology.

    Science.gov (United States)

    Scarlett, Nicola Vivienne Yorke; Tyson, Peter; Fraser, Darren; Mayo, Sheridan; Maksimenko, Anton

    2016-07-01

    Synchrotron X-ray tomography has been applied to the study of titanium parts fabricated by additive manufacturing (AM). The AM method employed here was the Arcam EBM(®) (electron beam melting) process which uses powdered titanium alloy, Ti64 (Ti alloy with approximately 6%Al and 4%V), as the feed and an electron beam for the sintering/welding. The experiment was conducted on the Imaging and Medical Beamline of the Australian Synchrotron. Samples were chosen to examine the effect of build direction and complexity of design on the surface morphology and final dimensions of the piece.

  15. Experimental studies on coherent synchrotron radiation at an emittance exchange beam line

    Directory of Open Access Journals (Sweden)

    J. C. T. Thangaraj

    2012-11-01

    Full Text Available One of the goals of the Fermilab A0 photoinjector is to investigate experimentally the transverse to longitudinal emittance exchange (EEX principle. Coherent synchrotron radiation in the emittance exchange line could limit the performance of the emittance exchanger at short bunch lengths. In this paper, we present experimental and simulation studies of the coherent synchrotron radiation (CSR in the emittance exchange line at the A0 photoinjector. We report on time-resolved CSR studies using a skew-quadrupole technique. We also demonstrate the advantages of running the EEX with an energy-chirped beam.

  16. Extended one-dimensional method for coherent synchrotron radiation including shielding

    Directory of Open Access Journals (Sweden)

    David Sagan

    2009-04-01

    Full Text Available Coherent synchrotron radiation can severely limit the performance of accelerators designed for high brightness and short bunch length. Examples include light sources based on energy recovery LINAC or free-electron lasers, and bunch compressors for linear colliders. In order to better simulate coherent synchrotron radiation, a one-dimensional formalism due to Saldin, Schneidmiller, and Yurkov has been implemented in the general beam dynamics code Bmad. Wide vacuum chambers are simulated by means of vertical image charges. Results from Bmad are here compared to analytical approximations, to numerical solutions of the Maxwell equations, and to the simulation code elegant and the code of Agoh and Yokoya.

  17. The sequences of a Brazilian political sociology

    Directory of Open Access Journals (Sweden)

    André Botelho

    2008-01-01

    Full Text Available By analytically reconstituting how the ideas of Oliveira Vianna were received in research by Victor Nunes Leal, Maria Isaura Pereira de Queiroz, and Maria Sylvia de Carvalho Franco, the article discusses the formation, from the 1920s to the 1970s, of a watershed in Brazilian political sociology oriented towards the investigation of conflict between the private and public orders in the specific configuration of political domination in Brazil.

  18. Spirometry reference values in the Brazilian population

    Directory of Open Access Journals (Sweden)

    R. Rufino

    Full Text Available The aim of the present study was to provide new spirometry reference equations in a sample of the Brazilian population for the following parameters: forced vital capacity (FVC, forced expiratory volume in 1 second (FEV1, FEV1/FVC ratio, peak of expiratory flow (PEF, forced expiratory flow at 50% (FEF50%, 75% average vital capacity (FEF25-75%, and average forced expiratory flow time (FEFT. This was a prospective study using results from chest radiographs, electrocardiograms, and questionnaires to investigate the participants' respiratory symptoms, sedentarism, and comorbidities (Charlson comorbidity index. From December 2010 to July 2014, individuals were randomly selected from various locations in the state of Rio de Janeiro. All individuals were examined by a single technician in the morning at the laboratory, and performed the spirometry with the same spirometer. Spirometry values were tabulated for the creation of three equation models: linear regression, logarithmic regression, and logarithms through a method that incorporates the lambda, median, and coefficient of variation (LMS method. Initially, 7003 individuals from both genders were contacted, and 454 were recruited. The data from the new equations were compared with one Brazilian and eight international equations, resulting in a high correlation (r>0.9. The values derived from the LMS method and linear regression were very similar (P>0.5, and both could be used to acquire the reference values for Brazilian spirometry. Data derived from the equations of this study were different from the current Brazilian equation, which could be justified by the different method used.

  19. Brazilian public controllership institutions theory versus practice

    OpenAIRE

    Suzart, Janilson Antonio da Silva; Marcelino, Carolina Venturini; Rocha, Joseilton Silveira da

    2012-01-01

    The creation of a General Controllership (CGU) in the executive branch of the Brazilian federal government in 2003 brought in its wake the creation or transformation of a variety of institutions in public controllership at the state level. We have assumed that this development resulted from the needs of public managers for institutions that can not only monitor the actions taken by the public administration but also provide information useful to government managers, but this a...

  20. Segmentation in the brazilian labor market

    OpenAIRE

    Botelho, Fernando; Ponczek, Vladimir Pinheiro

    2007-01-01

    This paper measures the degree of segmentation in the brazilian labor market. Controlling for observable and unobservable characteristics, workers earn more in the formal sector, which supports the segmentation hypothesis. We break down the degree of segmentation by socio-economic attributes to identify the groups where this phenomenon is more prevalent. We investigate the robustness of our findings to the inclusion of self-employed individuals, and apply a two-stage panel probit model using ...

  1. Bioactive Constituents of Brazilian Red Propolis

    Directory of Open Access Journals (Sweden)

    Boryana Trusheva

    2006-01-01

    Full Text Available In a new propolis type, red Brazilian propolis, 14 compounds were identified (six of them new for propolis, among them simple phenolics, triterepenoids, isoflavonoids, prenylated benzophenones and a naphthoquinone epoxide (isolated for the first time from a natural source. Three of the major components demonstrated significant antimicrobial activity, and two (obtained as inseparable mixture possessed radical scavenging activity against 1,1-diphenyl-2-picrylhydrazyl (DPPH.

  2. Modal survey of the Brazilian launch vehicle

    Science.gov (United States)

    Carneiro, S. H. S.; Teixeira, H. S., Jr.; Pirk, R.; Arruda, J. R. F.

    This paper describes the Brazilian satellite launch vehicle modal analysis program being currently performed. A full scale mock-up of the solid propellant four-stage launcher will be tested in five different configurations. To simulate free-free boundary conditions, a pneumatic suspension system was developed, and its influence in the mock-up dynamic behavior was investigated. The theoretical FEM models and preliminary results of the modal test are shown, along with theoretical/experimental correlation discussions.

  3. Sociocultural factors in Brazilian neuropsycholinguistic studies

    OpenAIRE

    Parente, Maria Alice de Mattos Pimenta; Carthery-Goulart, Maria Teresa; Zimmermann, Nicolle; Fonseca, Rochele Paz

    2012-01-01

    The history of Brazilian neuropsychology is traced at different neuropsycholinguistic stages with a focus on the importance of sociocultural factors. We first focus on language disorders, the sequelae of injuries in the left hemisphere, and neuropsychology restricted to the medical field in Europe, the United States, and Brazil. In the middle of the last century, attention to the interdisciplinary importance of studies on the right hemisphere began. Studies consequently emerged on the individ...

  4. Aromatic compounds from three Brazilian Lauraceae species

    Energy Technology Data Exchange (ETDEWEB)

    Batista, Andrea Nastri de Luca; Batista Junior, Joao Marcos; Lopez, Silvia Noeli; Furlan, Maysa; Cavalheiro, Alberto Jose; Silva, Dulce Helena Siqueira; Bolzani, Vanderlan da Silva [UNESP, Araraquara, SP (Brazil). Inst. de Quimica. Dept. de Quimica Organica; Nunomura, Sergio Massayoshi [Instituto Nacional de Pesquisa da Amazonia (INPA), Manaus, AM (Brazil). Dept. de Produtos Naturais; Yoshida, Massayoshi [Centro de Biotecnologia da Amazonia, Manaus, AM (Brazil)

    2010-07-01

    Phytochemical investigations on three Brazilian Lauraceae species from the Cerrado region of Sao Paulo State, Ocotea corymbosa (Meins) Mez., O. elegans Mez. and Persea pyrifolia Nees and Mart. ex Nees resulted in the isolation of flavonoids, an ester of the 4-O-E-caffeoylquinic acid, an aromatic sesquiterpene besides furofuran lignans. This is the first chemical study on the leaves of Ocotea elegans and O. corymbosa as well as the first report of non-volatile compounds from Persea pyrifolia. (author)

  5. HUMAN RESOURCE MANAGEMENT PRACTICES IN BRAZILIAN COMPANIES

    OpenAIRE

    Li, Y.

    2017-01-01

    The article considers the analysis of human resource management practices for Brazilian companies. The country-specific context and organizational behavior peculiarities of Brazil define the companies’ approach for HRM practices. The example of “CCR Group” is considered as a case study example. Analysis from company structure, culture specific context, current situation of human resource management not only in this company, but also in Brazil, in order to give the recommendation about how to ...

  6. Resistance Stories of African-Brazilian Women

    Directory of Open Access Journals (Sweden)

    Stela Nazareth Meneghel

    2005-01-01

    Full Text Available This study consists of an intervention using narrative workshops as a device to stimulate the empowerment of women. Ten women, victims of gender violence, took part in a workshop developed by non-governmental organization for African-Brazilian women Maria Mulher, which gives assistance to women living in Vila Cruzeiro do Sul, in the city of Porto Alegre. The main objective of the research was to debate questions related to gender and violence, making use of stories and histories related to the feminine, specifically African-Brazilian stories. Five meetings were held, where the women told and were told stories, took part in group discussions, experiences and rituals. The workshops gave those women a space where they could tell and hear stories, take part in the rituals of the orixás [African-Brazilian deities] of the black culture and tell their personal histories using those experiences. This intervention was an attempt at invoking different subjective experiences, and made it possible to empower the women who took part in the research, contributing for the rescue of the individual and collective memory of this group.

  7. [Profile of clinical trials enrolling Brazilian children].

    Science.gov (United States)

    Vieira, Jean Mendes de Lucena; Lima, Elisangela da Costa; Land, Marcelo Gerardin Poirot; Ventura, Miriam; Coelho, Helena Lutescia Luna

    2017-06-12

    This study aimed to characterize the clinical trials with medicines enrolling Brazilian children and adolescents, registered in the databases of Clinical Trials and the Brazilian Clinical Trials Network (ReBEC) from 1994 to 2014. Only 462 clinical trials enrolled Brazilian children and adolescents. There was an increase in registrations beginning in 2003, with an important drop in 2011. Among these trials, 35.5% were hosted in Brazil. The international clinical trials were mostly conducted by North American companies. In both cases, multinational industry was the principal source of funding. The clinical trials were predominantly phase III with injectable and solid oral pharmaceutical forms of antiviral drugs. Domestic clinical trials showed wider variation in the pharmaceutical forms and higher percentage of liquid formulations, when compared to the international trials. In addition to heavy external dependence for conducting clinical trials, the study emphasized the challenge for pediatric care in Brazil, which presents epidemiological peculiarities in an environment prone to the use of unlicensed medicines for children.

  8. Indoor Air Quality in Brazilian Universities

    Directory of Open Access Journals (Sweden)

    Sonia R. Jurado

    2014-07-01

    Full Text Available This study evaluated the indoor air quality in Brazilian universities by comparing thirty air-conditioned (AC (n = 15 and naturally ventilated (NV (n = 15 classrooms. The parameters of interest were indoor carbon dioxide (CO2, temperature, relative humidity (RH, wind speed, viable mold, and airborne dust levels. The NV rooms had larger concentration of mold than the AC rooms (1001.30 ± 125.16 and 367.00 ± 88.13 cfu/m3, respectively. The average indoor airborne dust concentration exceeded the Brazilian standards (<80 µg/m3 in both NV and AC classrooms. The levels of CO2 in the AC rooms were significantly different from the NV rooms (1433.62 ± 252.80 and 520.12 ± 37.25 ppm, respectively. The indoor air quality in Brazilian university classrooms affects the health of students. Therefore, indoor air pollution needs to be considered as an important public health problem.

  9. Preliminary studies of the quickly pulsed synchrotron involved in the Beta-Beam project; Etudes preliminaires du synchrotron rapidement pulse du projet Beta-Beam

    Energy Technology Data Exchange (ETDEWEB)

    Lachaize, A

    2007-07-01

    This study presents a quickly-pulsed synchrotron able to accelerate He{sup 6} and Ne{sup 18} beams from 100 MeV/u till 3.5 GeV (proton equivalent) The accelerator is made up of 48 bending dipoles and 42 focusing quadrupoles. The design of the HF accelerating system, the bunch injection and the correction of errors in beam dynamics are dealt with.

  10. Experiências simultâneas de espalhamento de raios X e calorimetria diferencial de varredura (SAXS/WAXD/DSC com resolução temporal utilizando radiação síncrotron Simultaneous and time resolved X-ray scattering and differential Scanning calorimetry experiments (SAXS/WAXD/DSC using synchrotron radiation

    Directory of Open Access Journals (Sweden)

    Tomás S. Plivelic

    2005-07-01

    Full Text Available Neste trabalho apresentamos uma nova instrumentação instalada na linha de SAXS do LNLS. Este equipamento permite a realização de experimentos simultâneos e resolvidos no tempo de espalhamento de raios X a baixos e altos ângulos (SAXS/WAXD e calorimetria diferencial de varredura (DSC. O dispositivo de DSC mostrou-se comparável a equipamentos convencionais, com taxas de variação de temperatura de até 60 °C/min e uma precisão de 0.1 °C. O uso de uma fonte de radiação síncrotron e de detetores de raios X sensíveis à posição permitiu a obtenção de dados com uma resolução temporal de 30 s. A aplicação deste arranjo experimental no estudo da cristalização isotérmica e da fusão em materiais poliméricos é mostrada para o caso da policaprolactona (PCL e suas blendas com polietileno clorado (PCL/PECl. As experiências mostraram a formação simultânea da estrutura cristalina e da morfologia lamelar nos diferentes estágios da cristalização assim como mudanças na cinética do processo com o tratamento isotérmico e a composição da blenda. Finalmente cabe destacar que experimentos simultâneos de SAXS/WAXD/DSC permitem o estudo de distintos processos abrangendo não apenas os de cristalização, mas também a formação de colóides e géis ou as transições de fase estruturais em diversos materiais.New instrumentation designed to perform simultaneous time-resolved X-ray scattering experiments at small and wide angles (SAXS/WAXD as well as differential scanning calorimetry (DSC has recently been installed at the SAXS beamline of the Laboratório Nacional de Luz Síncrotron. The DSC device proved to be comparable with conventional equipment, allowing temperature variation with rates of up to 60 °C/min with precision of 0.1 °C. The use of a synchrotron radiation source and position sensitive X-ray detectors allows data collection in real time with 30 s resolution. The application of this experimental set-up in the

  11. Mobile setup for synchrotron based in situ characterization during thermal and plasma-enhanced atomic layer deposition

    NARCIS (Netherlands)

    Dendooven, Jolien; Solano, Eduardo; Minjauw, Matthias M; Van de Kerckhove, Kevin; Coati, Alessandro; Fonda, Emiliano; Portale, Giuseppe; Garreau, Yves; Detavernier, Christophe

    2016-01-01

    We report the design of a mobile setup for synchrotron based in situ studies during atomic layer processing. The system was designed to facilitate in situ grazing incidence small angle x-ray scattering (GISAXS), x-ray fluorescence (XRF), and x-ray absorption spectroscopy measurements at synchrotron

  12. Match analysis on no-gi Brazilian jiu-jitsu

    OpenAIRE

    Simola, Tuomas

    2017-01-01

    Gi and no-gi Brazilian jiu-jitsu are fast growing sports. The aim of this thesis is to conclude a match analysis on no-gi Brazilian jiu-jitsu. Match analysis is used to identify the most used techniques in no-gi Brazilian jiu-jitsu. There is no sport analysis done for either gi or no-gi Brazilian jiu-jitsu, therefore the match analysis and its results can be utilized later as a base for sport analysis. The goal of this study is to find out the match duration, the type of match ending, the...

  13. Future Synchrotron Light Sources Based on Ultimate Storage Rings

    Energy Technology Data Exchange (ETDEWEB)

    Cai, Yunhai; /SLAC

    2012-04-09

    The main purpose of this talk is to describe how far one might push the state of the art in storage ring design. The talk will start with an overview of the latest developments and advances in the design of synchrotron light sources based on the concept of an 'ultimate' storage ring. The review will establish how bright a ring based light source might be, where the frontier of technological challenges are, and what the limits of accelerator physics are. Emphasis will be given to possible improvements in accelerator design and developments in technology toward the goal of achieving an ultimate storage ring. An ultimate storage ring (USR), defined as an electron ring-based light source having an emittance in both transverse planes at the diffraction limit for the range of X-ray wavelengths of interest for a scientific community, would provide very high brightness photons having high transverse coherence that would extend the capabilities of X-ray imaging and probe techniques beyond today's performance. It would be a cost-effective, high-coherence 4th generation light source, competitive with one based on energy recovery linac (ERL) technology, serving a large number of users studying material, chemical, and biological sciences. Furthermore, because of the experience accumulated over many decades of ring operation, it would have the great advantage of stability and reliability. In this paper we consider the design of an USR having 10-pm-rad emittance. It is a tremendous challenge to design a storage ring having such an extremely low emittance, a factor of 100 smaller than those in existing light sources, especially such that it has adequate dynamic aperture and beam lifetime. In many ultra-low emittance designs, the injection acceptances are not large enough for accumulation of the electron beam, necessitating on-axis injection where stored electron bunches are completely replaced with newly injected ones. Recently, starting with the MAX-IV 7-bend

  14. Synchrotron X-ray adaptative monochromator: study and realization of a prototype; Monochromateur adaptatif pour rayonnement X synchrotron: etude et realisation d`un prototype

    Energy Technology Data Exchange (ETDEWEB)

    Dezoret, D.

    1995-12-12

    This work presents a study of a prototype of a synchrotron X-ray monochromator. The spectral qualities of this optic are sensitive to the heat loads which are particularly important on third synchrotron generation like ESRF. Indeed, powers generated by synchrotron beams can reach few kilowatts and power densities about a few tens watts per square millimeters. The mechanical deformations of the optical elements of the beamlines issue issue of the heat load can damage their spectral efficiencies. In order to compensate the deformations, wa have been studying the transposition of the adaptive astronomical optics technology to the x-ray field. First, we have considered the modifications of the spectral characteristics of a crystal induced by x-rays. We have established the specifications required to a technological realisation. Then, thermomechanical and technological studies have been required to transpose the astronomical technology to an x-ray technology. After these studies, we have begun the realisation of a prototype. This monochromator is composed by a crystal of silicon (111) bonded on a piezo-electric structure. The mechanical control is a loop system composed by a infrared light, a Shack-Hartmann CDD and wave front analyser. This system has to compensate the deformations of the crystal in the 5 kcV to 60 kcV energy range with a power density of 1 watt per square millimeters. (authors).

  15. X-Ray microfluorescence analysis of pigments in decorative paintings from sarcophagus cartonage of an Egyptian mummy

    Energy Technology Data Exchange (ETDEWEB)

    Calza, Cristiane; Lopes, Ricardo Tadeu [Universidade Federal, Rio de Janeiro, RJ (Brazil). Coordenacao dos Programas de Pos-graduacao de Engenharia. Lab. de Instrumentacao Nuclear]. E-mail: ccalza@lin.ufrj.br; ricardo@lin.ufrj.br; Anjos, Marcelino J. [Universidade do Estado, Rio de Janeiro, RJ (Brazil). Inst. de Fisica]. E-mail: marcelin@lin.ufrj.br; Souza, Sheila M.F. Mendonca de [Fundacao Inst. Oswaldo Cruz (FIOCRUZ), Rio de Janeiro, RJ (Brazil)]. E-mail: sferraz@ensp.fiocruz.br; Brancaglion Junior, Antonio [Museu Nacional, Rio de Janeiro, RJ (Brazil)]. E-mail: anubis@ufrj.br

    2005-07-01

    This work evaluated the pigments used in decorative paintings from sarcophagus cartonage fragments of an Egyptian mummy using X-Ray Microfluorescence with Synchrotron Radiation technique. This female mummy (n.158) is considered one of the most important pieces of the National Museum (Rio de Janeiro, Brazil) because of its unconventional embalming with legs and arms swathed separately. This embalming procedure probably was used by a Theban family from the Roman period (first century BC), whose tomb was recently discovered. Only seven mummies like this were discovered and they are exposed in European museums. The results obtained for the cartonage samples were compared to those obtained for a linen wrapping fragment of which provenance was known. The objective of this work was to characterize the elemental composition of the cartonage pigments and to verify if they were according to those used by Egyptian craftsmen in the Roman period. The measurements were performed at the XRF beamline of the Brazilian Synchrotron Light Laboratory (LNLS), using white beam and a Si(Li) detector with resolution of 165 eV. The elements found in the samples were: Si, S, Cl, K, Ca, Ti, Cr, Mn, Fe, Ni, Cu, Zn, As, Sr, Hg and Pb. (author)

  16. Brazing vacuum ceramic tubes for magnets applications

    Energy Technology Data Exchange (ETDEWEB)

    Bagnato, O.R.; Francisco, R.F. [Laboratorio Nacional de Luz Sincrotron (LNLS), SP (Brazil); Gobbi, A.L. [Laboratorio Nacional de Nanotecbologia (LNNano), SP (Brazil); Falvo, T. [Engecer Ltda, Sao Carlos, SP (Brazil)

    2014-07-01

    Full text: The Sirius Project is an initiative of the Brazilian Synchrotron Light Laboratory - LNLS (CNPEM - MCTI ), for the design, construction and operation of a new synchrotron radiation source 3rd generation, with high brightness and energy of the electrons of 3. 0 GeV. Among many other components, will be built 80 ceramic cameras embedded in specials magnets, whose function is to act to correct the orbit of the electron beam in the storage ring. The ceramic chamber is crucial for this application because this material is transparent to the magnetic field generated in the electro magnet and thus acts directly on the electron beam. The difficulty of these constructive components lies in the fact that, the ceramic components must be attached to metal components will join vacuum chambers that make up the ring, and then must present excellent mechanical and vacuum tight. The process of chemical bonding between the ceramic and metal components is performed by brazing in high vacuum. After brazing, is deposited a film of copper with 7 micrometers thickness. The objective of this paper is to describe the process of film deposition and brazing of copper and the excellent results obtained in the production, mechanical characterization, microstructural and tightness. The results obtained with the process indicate an homogeneous film with high adhesion and electrical resistance near the estimated values??. Tests are being carried out by XPS and SEM techniques for chemical and structural characterization. (author)

  17. Espectroscopia de fotoelétrons de limiares de átomos e moléculas Atomic and molecular threshold photoelectron spectroscopy

    Directory of Open Access Journals (Sweden)

    Maria Cristina Andreolli Lopes

    2006-02-01

    Full Text Available A threshold photoelectron spectrometer applied to the study of atomic and molecular threshold photoionization processes is described. The spectrometer has been used in conjunction with a toroidal grating monochromator at the National Synchrotron Radiation Laboratory (LNLS, Brazil. It can be tuned to accept threshold electrons (< 20 meV and work with a power resolution of 716 (~18 meV at 12 eV with a high signal/noise ratio. The performance of this apparatus and some characteristics of the TGM (Toroidal Grating Monochromator beam line of LNLS are described and discussed by means of argon, O2 and N2 threshold photoelectron spectra.

  18. Experimental investigations of synchrotron radiation at the onset of the quantum regime

    CERN Document Server

    Andersen, Kristoffer K; Knudsen, H; Thomsen, H D; Uggerhøj, U I; Sona, P; Mangiarotti, A; Ketel, T J; Dizdar, A; Ballestrero, S

    2012-01-01

    The classical description of synchrotron radiation fails at large Lorentz factors, $\\gamma$, for relativistic electrons crossing strong transverse magnetic fields $B$. In the rest frame of the electron this field is comparable to the so-called critical field $B_0 = 4.414\\cdot10^9$ T. For $\\chi = \\gamma B/B_0 \\simeq 1$ quantum corrections are essential for the description of synchrotron radiation to conserve energy. With electrons of energies 10-150 GeV penetrating a germanium single crystal along the $$ axis, we have experimentally investigated the transition from the regime where classical synchrotron radiation is an adequate description, to the regime where the emission drastically changes character; not only in magnitude, but also in spectral shape. The spectrum can only be described by quantum synchrotron radiation formulas. Apart from being a test of strong-field quantum electrodynamics, the experimental results are also relevant for the design of future linear colliders where beamstrahlung - a closely r...

  19. Support for the Advanced Polymers Beamline at the National Synchrotron Light Source

    Energy Technology Data Exchange (ETDEWEB)

    Hsiao, Benjamin S. [State Univ. of New York (SUNY), Stonybrook, NY (United States)

    2008-10-01

    The primary focus of the X27C beamline is to investigate frontier polymer science and engineering problems with emphasis on real-time studies of structures, morphologies and dynamics from atomic, nanoscopic, microscopic to mesoscopic scales using simultaneous small-angle X-ray scattering (SAXS) and wide-angle X-ray diffraction (WAXD) techniques. The scientific merit of this project is as follows. Currently, many unique sample chambers for in-situ synchrotron studies, developed by the PI (B. Hsiao) and Co-PI (B. Chu), are available for general users of X27C at NSLS. These instruments include a gel/melt spinning apparatus, a continuous fiber drawing apparatus, a tensile stretching apparatus, a high pressure X-ray cell using supercritical carbon dioxide, a parallel plate strain-controlled shear stage and a dynamic rheometer for small-strain oscillatory deformation study. Based on the use of these instruments in combination with synchrotron X-rays, many new insights into the relationships between processing and structure have been obtained in recent years. The broader impact of this project is as follows. The X27C beamline is the first synchrotron facility in the United States dedicated to chemistry/materials research (with emphasis on polymers). The major benefit of this facility to the materials community is that no extensive synchrotron experience and equipment preparation are required from general users to carry out cutting-edge experiments.

  20. Bringing Physics, Synchrotron Light and Probing Neutrons to the Public: A Collaborative Outreach

    Science.gov (United States)

    Micklavzina, Stanley; Almqvist, Monica; Sörensen, Stacey L.

    2014-01-01

    Stanley Micklavzina, a US physics educator on sabbatical, teams up with a Swedish national research laboratory, a synchrotron radiation experimental group and a university science centre to develop and create educational and public outreach projects. Descriptions of the physics, science centre displays and public demonstrations covering the…