WorldWideScience

Sample records for boron lined counters

  1. Boron-lined proportional counters with improved neutron sensitivity

    CERN Document Server

    Dighe, P M; Prasad, K R; Kataria, S K; Athavale, S N; Pappachan, A L; Grover, A K

    2003-01-01

    Boron-lined proportional counters with higher neutron sensitivity have been developed by introducing baffle structures within the sensitive volume. the results are compared to devices developed with multiple cathode assemblies in a single enclosure. in either case, the increase in the boron-coated surface area results in higher neutron sensitivity. one of these counters has 51 annular baffles coated with natural boron with 10 mm hole for the anode wire to pass through. filled with p-10 gas at 20 cm hg, it has an overall diameter of 30 and 300 mm length. multiple dip coating method was employed for better uniformity in boron thickness. the neutron sensitivity of this counter is 1.6 cps/nv, which is 2.5 times that of a counter with standard electrode geometry. another counter was developed with three cathode assemblies (30 mm IDx300 mm) coated with 92% sup 1 sup 0 B while the third has seven assemblies coated with natural boron (16 mm IDx750 mm length). the neutron sensitivity is 10 and 5.5 cps/nv, respectively...

  2. Boron-Lined Multitube Neutron Proportional Counter Test

    Energy Technology Data Exchange (ETDEWEB)

    Woodring, Mitchell L.; Ely, James H.; Kouzes, Richard T.; Stromswold, David C.

    2010-09-07

    Radiation portal monitors used for interdiction of illicit materials at borders include highly sensitive neutron detection systems. The main reason for having neutron detection capability is to detect fission neutrons from plutonium. The currently deployed radiation portal monitors (RPMs) from Ludlum and Science Applications International Corporation (SAIC) use neutron detectors based upon 3He-filled gas proportional counters, which are the most common large neutron detector. There is a declining supply of 3He in the world, and thus, methods to reduce the use of this gas in RPMs with minimal changes to the current system designs and sensitivity to cargo-borne neutrons are being investigated. Four technologies have been identified as being currently commercially available, potential alternative neutron detectors to replace the use of 3He in RPMs. These technologies are: 1) Boron trifluoride (BF3)-filled proportional counters, 2) Boron-lined proportional counters, 3) Lithium-loaded glass fibers, and 4) Coated non-scintillating plastic fibers. In addition, a few other companies have detector technologies that might be competitive in the near term as an alternative technology. Reported here are the results of tests of a boron-lined, “multitube” proportional counter manufactured by Centronic Ltd. (Surry, U.K. and Houston, TX). This testing measured the required performance for neutron detection efficiency and gamma-ray rejection capabilities of the detector.

  3. Study on the effect of moderator of the proportional Boron-lined counter on the neutron detection efficiency

    International Nuclear Information System (INIS)

    The proportional boron-lined counter as a common source-range detector is widely used in reactor monitoring, which has high detection efficiency for thermal neutron. The detection efficiency of the proportional boron-lined counter for fast reactor monitoring can be improved by using proper moderator. The relative detection efficiency and absolute detection efficiency of the proportional boron-lined counter in different thickness of the moderator for mono-energy neutrons of different energy were simulated by using MCNP, the tend-line of the relative detection efficiency and absolute detection efficiency were obtained. Also the detection efficiency of selected proportional boron-lined counter to the typical neutron spectrum of the fast reactor was simulated, and then the optimized moderator was designed. It would have some degree of guiding significance to design the nuclear measurement system of the fast reactor. (authors)

  4. Design and performance of A 3He-free coincidence counter based on parallel plate boron-lined proportional technology

    Science.gov (United States)

    Henzlova, D.; Menlove, H. O.; Marlow, J. B.

    2015-07-01

    Thermal neutron counters utilized and developed for deployment as non-destructive assay (NDA) instruments in the field of nuclear safeguards traditionally rely on 3He-based proportional counting systems. 3He-based proportional counters have provided core NDA detection capabilities for several decades and have proven to be extremely reliable with range of features highly desirable for nuclear facility deployment. Facing the current depletion of 3He gas supply and the continuing uncertainty of options for future resupply, a search for detection technologies that could provide feasible short-term alternative to 3He gas was initiated worldwide. As part of this effort, Los Alamos National Laboratory (LANL) designed and built a 3He-free full scale thermal neutron coincidence counter based on boron-lined proportional technology. The boron-lined technology was selected in a comprehensive inter-comparison exercise based on its favorable performance against safeguards specific parameters. This paper provides an overview of the design and initial performance evaluation of the prototype High Level Neutron counter-Boron (HLNB). The initial results suggest that current HLNB design is capable to provide ~80% performance of a selected reference 3He-based coincidence counter (High Level Neutron Coincidence Counter, HLNCC). Similar samples are expected to be measurable in both systems, however, slightly longer measurement times may be anticipated for large samples in HLNB. The initial evaluation helped to identify potential for further performance improvements via additional tailoring of boron-layer thickness.

  5. Design and performance of A 3He-free coincidence counter based on parallel plate boron-lined proportional technology

    International Nuclear Information System (INIS)

    Thermal neutron counters utilized and developed for deployment as non-destructive assay (NDA) instruments in the field of nuclear safeguards traditionally rely on 3He-based proportional counting systems. 3He-based proportional counters have provided core NDA detection capabilities for several decades and have proven to be extremely reliable with range of features highly desirable for nuclear facility deployment. Facing the current depletion of 3He gas supply and the continuing uncertainty of options for future resupply, a search for detection technologies that could provide feasible short-term alternative to 3He gas was initiated worldwide. As part of this effort, Los Alamos National Laboratory (LANL) designed and built a 3He-free full scale thermal neutron coincidence counter based on boron-lined proportional technology. The boron-lined technology was selected in a comprehensive inter-comparison exercise based on its favorable performance against safeguards specific parameters. This paper provides an overview of the design and initial performance evaluation of the prototype High Level Neutron counter—Boron (HLNB). The initial results suggest that current HLNB design is capable to provide ~80% performance of a selected reference 3He-based coincidence counter (High Level Neutron Coincidence Counter, HLNCC). Similar samples are expected to be measurable in both systems, however, slightly longer measurement times may be anticipated for large samples in HLNB. The initial evaluation helped to identify potential for further performance improvements via additional tailoring of boron-layer thickness

  6. Introduction to Neutron Coincidence Counter Design Based on Boron-10

    Energy Technology Data Exchange (ETDEWEB)

    Kouzes, Richard T.; Ely, James H.; Lintereur, Azaree T.; Siciliano, Edward R.

    2012-01-22

    The Department of Energy Office of Nonproliferation Policy (NA-241) is supporting the project 'Coincidence Counting With Boron-Based Alternative Neutron Detection Technology' at Pacific Northwest National Laboratory (PNNL) for development of an alternative neutron coincidence counter. The goal of this project is ultimately to design, build and demonstrate a boron-lined proportional tube based alternative system in the configuration of a coincidence counter. This report, providing background information for this project, is the deliverable under Task 1 of the project.

  7. Performance of Boron-10 based Neutron Coincidence Counters

    International Nuclear Information System (INIS)

    Helium-3 gas-filled detectors have been used in neutron coincidence counting for non-destructive assay for over 30 years. With the current shortage of 3He gas, GE's Reuter-Stokes business developed a 10B lined proportional counter and a 10B hybrid coincidence counter, in which a small amount of 3He is added to a 10B detector to enhance the neutron sensitivity. GE's Reuter-Stokes business modelled, designed, built and tested prototype coincidence counters using the 10B lined detectors and the 10B hybrid detectors. We will present these systems and their applications for non-destructive assay. (author)

  8. A passive rem counter based on CR39 SSNTD coupled with a boron converter

    CERN Document Server

    Agosteo, S; Ferrarini, c, M; Silari, M

    2009-01-01

    A passive neutron rem counter using a CR39 SSNTD coupled with a boron converter has been developed. The rem counter is a polythene sphere with cadmium and lead insets, designed to have a response function proportional to the fluence to ambient dose equivalent conversion coefficients, H*(10)/Φ, for energies ranging from thermal up to 1 GeV. At its centre is a thermal neutron detector made of a CR39 SSNTD coupled with an enriched boron neutron converter. The rem counter was first calibrated at CERN and at the Politecnico di Milano, and then tested in high-energy neutron fields at GSI, Darmstadt, Germany and at the CERF facility at CERN. Its most important features are a very high neutron sensitivity and conversely a complete insensitivity to gamma radiation.

  9. Development of position sensitive gas counter with delay line readout

    International Nuclear Information System (INIS)

    The position counter with delay line read out was developed using commercially available delay line chips. Their counting rate capability was evaluated with Monte Carlo simulation and compared with the case of charge division method. The delay line method is expected to gain advantage over the charge division method. The 25 cm prototype of the counter was tested in RCNP and the usefulness for the focal plane detector is shown. The 1.2 m one was developed and the performance is measured with X-ray source in proportional mode and SQS mode. The best position resolution obtained was 1 mm with 25 μm anode wire. The best position resolutions obtained with 50 μm anode wire in proportional and SQS mode were 1.4 mm and 1.7 mm, respectively. (J.P.N.)

  10. Ab initio study of boron nitride lines on graphene

    Science.gov (United States)

    Mata-Carrizal, Berenice; Sanginés-Mendoza, Raúl; Martinez, Edgar

    2013-03-01

    Graphene has unusual electronic properties which make it a promising material for electronic devices. Neverthless, the absence of a band gap sets limitations on its practical applications. Thus, it is crucial to find methods to create and tune the band gap of systems based on graphene. In this way, we explore the modulation of the electronic properties of graphene through doping with boron nitride lines. In particular, we studied the electronic structure of graphene sheets doped with boron nitride lines armchair and zigzag type. The calculations were performed using the pseudopotential LCAO method with a Generalized Gradient Approximation (GGA) for the exchange-correlation energy functional. We found that both doping lines type induce a bandgap and that the energy gap increases as the length of doping lines increases. Accordingly to our DFT calculations, we found that the energy gap on graphene doped with armchair and zigzag lines is due to a two different mechanisms to drain charge from pi- to sigma- orbitals. Thus, we found that doping graphene with boron nitride lines is a useful way to induce and modulate the bandgap on graphene. This research was supported by Consejo Nacional de Ciencia y Tecnología (Conacyt) under Grant No. 133022.

  11. Source Lines Counter (SLiC) Version 4.0

    Science.gov (United States)

    Monson, Erik W.; Smith, Kevin A.; Newport, Brian J.; Gostelow, Roli D.; Hihn, Jairus M.; Kandt, Ronald K.

    2011-01-01

    Source Lines Counter (SLiC) is a software utility designed to measure software source code size using logical source statements and other common measures for 22 of the programming languages commonly used at NASA and the aerospace industry. Such metrics can be used in a wide variety of applications, from parametric cost estimation to software defect analysis. SLiC has a variety of unique features such as automatic code search, automatic file detection, hierarchical directory totals, and spreadsheet-compatible output. SLiC was written for extensibility; new programming language support can be added with minimal effort in a short amount of time. SLiC runs on a variety of platforms including UNIX, Windows, and Mac OSX. Its straightforward command-line interface allows for customization and incorporation into the software build process for tracking development metrics. T

  12. Measuring the sensitivity of a boron-lined ion chamber

    International Nuclear Information System (INIS)

    Boron-lined ion chambers are used to monitor external neutron flux from fissionable materials assembled at the Los Alamos Critical Assembly Experiment Facility. The sensitivity of these chambers must be measured periodically in order to detect changes in filling gas and to evaluate other factors that may affect chamber performance. We delineate a procedure to measure ion chamber response using a particular neutron source (239PuBe) in a particular moderating geometry of polyethylene. We also discuss use of the amplifier, high-voltage power supply, recorders, and scram circuits that comprise the complete ion chamber monitoring system

  13. Annular shape silver lined proportional counter for on-line pulsed neutron yield measurement

    Energy Technology Data Exchange (ETDEWEB)

    Dighe, P.M., E-mail: pmdighe@barc.gov.in; Das, D.

    2015-04-01

    An annular shape silver lined proportional counter is developed to measure pulsed neutron radiation. The detector has 314 mm overall length and 235 mm overall diameter. The central cavity of 150 mm diameter and 200 mm length is used for placing the neutron source. Because of annular shape the detector covers >3π solid angle of the source. The detector has all welded construction. The detector is developed in two halves for easy mounting and demounting. Each half is an independent detector. Both the halves together give single neutron pulse calibration constant of 4.5×10{sup 4} neutrons/shot count. The detector operates in proportional mode which gives enhanced working conditions in terms of dead time and operating range compared to Geiger Muller based neutron detectors.

  14. Multiwire proportional counter (lecture by an electromagnetic delay line)

    International Nuclear Information System (INIS)

    For track localisation of ionizing particles with multiwire proportional chamber, an electronic chain including amplifying, shaping and memorizing circuits is required for each wire. In order to lower the cost of this type of detector, an electromagnetic delay line is proposed among various possibilities. In this paper, different coupling modes between chamber and delay line are studied with their respective advantages. The realization of one meter long delay line with a unit delay time of 15 ns per cm is also presented

  15. Solution In-Line Alpha Counter (SILAC) Instruction Manual-Version 4.00

    International Nuclear Information System (INIS)

    The Solution In-Line Alpha Counter (SILAC) provides near real-time alpha activity measurements of aqueous solutions in gloveboxes located in the Plutonium Facility (TA-55) at Los Alamos National Laboratory (LANL). The SILAC detector and its interface software were first developed by Joel Farnham at LANL [1]. This instruction manual describes the features of the SILAC interface software and contains the schematic and fabrication instructions for the detector

  16. Boron

    International Nuclear Information System (INIS)

    The trace element boron (B) is of interest in reclamation situations for several reasons. It plays an essential through largely unidentified role in the growth of higher plants. In argronomic situations B deficiencies are common, and deficiencies in reclamation situations have been suggested but not documented. Among micronutrients, B is unique because the range from deficient concentrations to toxic concentrations either in the soil solution or in plant tissue is narrower than for any other micronutrient. In reclamation situations excessive amounts of B can occur in the soil or in near-surface mining wastes and thus interfere with reclamation objectives, especially in arid and semiarid regions. Also, B is mobile and appears subject to both upward transport (and possible contamination of overlying material) and downward transport (and possible contamination of surface water and groundwater)

  17. The boron absorption line at 2089.6 AA in HD 140283 ?

    CERN Document Server

    Thoren, P H

    2000-01-01

    We have observed the B I line at 2089.6 AA in the metal poor star HD 140283 with HST/STIS. The observation was an attempt to confirm the B abundances derived from the 2497 AA B I line in earlier works in general, and for for this star in particular (Edvardsson et al. 1994 A&A 290, 176; Kiselman & Carlsson 1996, A&A 311, 680). The resulting spectrum gained from 8 orbits of observations is hardly consistent with the boron abundance derived in the earlier works. A pure 10^B line could produce the feature observed but no reasonable process can produce such a ratio between 10^B and 11^B. More likely the analysed feature is affected by a statistical fluctuation. A conservative upper limit estimate of the NLTE corrected boron abundance gives a value marginally consistent with that derived from the 2497 AA line. We are proposing further observations to derive a more definite abundance from the line.

  18. Development of gamma compensated boron lined ionization chamber with intermediate range monitor for reactor applications

    International Nuclear Information System (INIS)

    Gamma compensated boron lined ionization chamber with indigenously developed 40.5% enriched boron-10 and polyetheretherketone insulating spacers has been developed. The detector has an overall diameter of 85 mm and overall length of 315 mm. Tests on the chamber with intermediate range monitor have been conducted in both gamma and neutron fields. The detector has good saturation characteristics, adequate neutron sensitivity and required gamma compensation. The linearity of response of the detector at various reactor power levels was also found to be within the required limits. The Log P signal output variation due to change in amplifier temperature of IRM, was found to be within limits for temperature variations from 25℃ to 30.13℃ thus indicating stable output against changes in temperature of IRM amplifier at steady reactor power operation. (author)

  19. Boron-10 ABUNCL Models of Fuel Testing

    Energy Technology Data Exchange (ETDEWEB)

    Siciliano, Edward R.; Lintereur, Azaree T.; Kouzes, Richard T.; Ely, James H.

    2013-10-01

    The Department of Energy Office of Nuclear Safeguards and Security (NA-241) is supporting the project Coincidence Counting With Boron-Based Alternative Neutron Detection Technology at Pacific Northwest National Laboratory (PNNL) for the development of a 3He proportional counter alternative neutron coincidence counter. The goal of this project is to design, build and demonstrate a system based upon 10B-lined proportional tubes in a configuration typical for 3He-based coincidence counter applications. This report provides results from MCNP simulations of the General Electric Reuter-Stokes Alternative Boron-Based Uranium Neutron Coincidence Collar (ABUNCL) active configuration model with fuel pins previously measured at Los Alamos National Laboratory. A comparison of the GE-ABUNCL simulations and simulations of 3He based UNCL-II active counter (the system for which the GE-ABUNCL was targeted to replace) with the same fuel pin assemblies is also provided.

  20. Theoretical study on Position Sensitive Fission Counters designed with a transmission delay line structure

    International Nuclear Information System (INIS)

    Structures and electric characteristics of neutron counters were studied for the development of a Position Sensitive Fission Counter (PSFC). The PSFC was designed with a structure of transmission delay line and for measurement of fast neutrons. The PSFC has two output connectors at each end-side, and the signal pulse produced by one fission reaction is transmitted to both connectors with proper delay time. Neutron positions are detected by measurement of pulse intervals. Through the study, it was found that the PSFC could detect neutron positions with a high resolution and has an excellent transmission characteristic for signal pulses without causing pulse reflection. The reasons are that the PSFC can have an adequate transmission delay of signal pulses for detection of neutron positions and be designed to make impedance matching to a coaxial cable. The PSFC enables one to measure in-core power distributions in the reactor with high position resolution on real time. The development of PSFC for fast neutrons seems to bring about an advanced-type of in-core power distribution monitor. (author)

  1. Electronics and pulse counting error of position sensitive fission counters with a transmission delay line structure

    International Nuclear Information System (INIS)

    A new Position Sensitive Fission Counter (PSFC) had been proposed for measurement of neutron flux distribution in a reactor. It was designed with the electrode structure as a pulse delay line to give a high position sensitivity. The result of study has been reported. A composition of electronics was designed for a neutron measuring system with the PSFC. Each error of pulse counting due to the PSFC and the electronics was studied. It was found that a pulse delay device was useful to simplify the electronics in construction and for the neutron measurement at a high pulse counting rate on real time. The delay device has the same delay time as the PSFC. It was clear that the pulse counting error due to the PSFC was smaller than that of the electronics. The error due to the PSFC was less than 2% even if in a neutron measurement condition at pulse counting rate of 106 cps. (author)

  2. Development of a low-level, in-line alpha counter (LLILAC)

    International Nuclear Information System (INIS)

    This is the final report of a two-year, Laboratory-Directed Research and Development (LDRD) project at the Los Alamos National Laboratory (LANL). With the increasing awareness of water contamination issues and the rising consequences of any form of contamination, real-time continuous monitoring is rapidly becoming a necessity. In particular, monitoring for the presence of any radioactive material is paramount. The most difficult of such monitoring tasks is that of detecting alpha-emitting radionuclides in water. Our development of the Low Level In-Line Alpha Counter (LLILAC) addresses the need for on-line, near real-time monitoring of alpha-emitting radionuclides in aqueous streams in a wide variety of applications. Although primarily designed as an on-line instrument for real-time applications, the detector can also be used for long-term in situ/post-closure monitoring. This detection system operates by allowing the stream to be monitored to come in contact with a large number of small rods or tubes made of scintillation material. By maximizing the surface to volume ratio of the scintillator, the response to alpha particles is favored over other types of radiation. Several configurations of scintillator and light collection schemes have been investigated to optimize the detection efficiency. We have also written several Monte Carlo codes to help to predict and understand the detector performance

  3. Steam line break accident reanalysis for the reduction of 21000 ppm boron injection tank in Daya Bay NPPS

    International Nuclear Information System (INIS)

    Using WESTINGHOUSE codes and methodology, the impact of Boron Injection Tank (BIT) reduction (i.e., either removal of the BIT or reduction of the boron concentration) on Daya Bay Nuclear Power plant safety is analyzed. The design of the 21000 ppm BIT system is mainly to cover the steam line break accidents. The author covers only the core response part of steam line break accident analysis, excluding mass and energy release and dose calculations. The DNBR result are all within criterion limits for reduced boron concentration level to 7000, 2000 and 0 ppm with design or as built SG data. A reduction to 7000 ppm for the BIT system is recommended for necessary plant modification

  4. Development and testing of a Cerenkov counter for hyperon on line tagging (WA89 experiment at CERN)

    International Nuclear Information System (INIS)

    HYPOLIT (HYPerons On LIne Tagging) is a new Counter for tagging hyperons on line, in the 250 GeV/c beam (rms 7%) of the second phase of the WA89 experiment at CERN. It is a fast RICH counter with low angular acceptance but a great resolution power. The counter is equipped with a 6 m focal length spherical mirror and a chromatic corrector. The size of the Cerenkov rings is reduced by means of set of two conical mirrors to match the active area of an image intensifier. Its output window is devided into 160 pixels read with 160 photomultipliers via fibre optics. The counter has been tested at CERN in 2, 4 and 8 GeV/c electron beam and in 220 GeV/c pion beam containing also 5.3% kaons and 0.7% antiprotons. A spatial resolution of 0.125 mm was achieved on the radius, which represents 1/5 of the pion-Kaon separation. The ring radius is determined electronically in less than 2.5 microseconds. A Monte-Carlo simulation was performed at 360 GeV/c. It is shown that the tagging is also possible at this energy, despite the ten times greater emittance of this beam, after some modifications on the chromatic corrector and the detection system. (orig.)

  5. X-ray diffraction line profile analysis of deformation microstructure in boron modified Ti-6Al-4V alloy

    International Nuclear Information System (INIS)

    X-ray diffraction line profile analysis (XRDLPA) techniques have been applied to investigate the deformed microstructure of a recently developed boron modified two-phase titanium alloy Ti-6Al-4V. The alloy was hot compressed at 750 deg. C up to 50% height reduction at two different strain rates (10-3 S-1 and 1 S-1). Microstructural parameters like average domain size, average microstrain within the domain and dislocation density of the two phases were determined using X-ray diffraction line profile analysis. The results indicate an increase in the microstrain and dislocation density for the α-phase and decrease for the β-phase in the case of boron modified alloys as compared to the normal material. Microstructural modifications viz. the grain refinement and the presence of hard, brittle TiB particles in the case of boron modified alloy are held responsible for the observed difference in the dislocation density. - Research Highlights: → Microstructural examination of hot compressed Ti64 with and without boron addition by XRDLPA. → Smaller average domain size in alpha-phase compared to the corresponding alpha-phase in all cases. → Higher microstrain and dislocation density for α phase and lower for β phase in case of Ti64+B. → Decrease in domain size while increase in micro-strain and dislocation density with strain rate. → Strain accumulation around TiB particles responsible for high dislocation density in α phase.

  6. Beam Cherenkov counter conception for in line identification of 270 GeV/c Σ- Ξ- and Ω-

    International Nuclear Information System (INIS)

    The purpose of this thesis is to design a beam Cerenkov counter. This counter will provide an on line identification of the Σ-, Ξ- and Ω- hyperons (270 GeV/c) in the experiment WA89 at CERN. The acceptance of the detector should allow tagging these hyperons in a large momentum range (± 25%) and for a beam divergence up to 250 microrad. The first part of this report is devoted to the physical goals such as the study of charmed baryons, the search of multiquark states, and the determination of hadronic and electromagnetic hyperon radii. The experimental WA89 setup is also presented. The major part deals with the design of the Cerenkov counter. The dimension of the detector, the Cerenkov angle value, the focal length of the spherical mirror, etc... are derived from a Monte-Carlo simulation. Various methods of simple photon detection (gaz detector: TEA, TMAE; solid detectors: PM and Image Intensifier) are investigated. The most performing solution uses two conical mirrors in order to reduce the size of the Cerenkov circles and an image intensifier (which detects the single photon) followed by an optical fiber matrix transmitting the luminous signal to 160 photomultipliers. The on line procedure for calculating the radius of each circle (identification of the particle) is studied in detail. Finally, the optimization of the optical system to achromatize the Cerenkov light is discussed

  7. Safeguards Technology Factsheet 3He-free Neutron Coincidence Counter

    International Nuclear Information System (INIS)

    A full scale thermal neutron coincidence counter (High Level Neutron Counter - Boron: HLNB) based on 3He alternative detection technology was designed and built at LANL and field tested at Plutonium Conversion Development Facility (PCDF) of Japan Atomic Energy Agency (JAEA) during FY15. HLNB is based on boron-lined proportional plates that replace the traditional 3He proportional tubes and was designed as a direct alternative to 3He-based High Level Neutron Coincidence Counter (HLNC-II). During the JAEA field trial the HLNB demonstrated comparable performance to HLNC-II, which represents a key development in the area of 3He alternative technologies and provides a complete demonstration of the technology for nuclear safeguards applications including high mass MOX samples.

  8. Boron-10 ABUNCL Prototype Initial Testing

    Energy Technology Data Exchange (ETDEWEB)

    Kouzes, Richard T.; Ely, James H.; Lintereur, Azaree T.; Siciliano, Edward R.

    2012-12-01

    The Department of Energy Office of Nuclear Safeguards and Security (NA-241) is supporting the project Coincidence Counting With Boron-Based Alternative Neutron Detection Technology at Pacific Northwest National Laboratory (PNNL) for the development of a 3He proportional counter alternative neutron coincidence counter. The goal of this project is to design, build and demonstrate a system based upon 10B-lined proportional tubes in a configuration typical for 3He-based coincidence counter applications. This report provides results of initial testing of an Alternative Boron-Based Uranium Neutron Coincidence Collar (ABUNCL) design built by General Electric Reuter-Stokes. Several configurations of the ABUNCL models, which use 10B-lined proportional counters in place of 3He proportional counters for the neutron detection elements, were previously reported. The ABUNCL tested is of a different design than previously modeled. Initial experimental testing of the as-delivered passive ABUNCL was performed, and modeling will be conducted. Testing of the system reconfigured for active testing will be performed in the near future, followed by testing with nuclear fuel.

  9. Use of GEANT4 vs. MCNPX for the characterization of a boron-lined neutron detector

    Science.gov (United States)

    van der Ende, B. M.; Atanackovic, J.; Erlandson, A.; Bentoumi, G.

    2016-06-01

    This work compares GEANT4 with MCNPX in the characterization of a boron-lined neutron detector. The neutron energy ranges simulated in this work (0.025 eV to 20 MeV) are the traditional domain of MCNP simulations. This paper addresses the question, how well can GEANT4 and MCNPX be employed for detailed thermal neutron detector characterization? To answer this, GEANT4 and MCNPX have been employed to simulate detector response to a 252Cf energy spectrum point source, as well as to simulate mono-energetic parallel beam source geometries. The 252Cf energy spectrum simulation results demonstrate agreement in detector count rate within 3% between the two packages, with the MCNPX results being generally closer to experiment than are those from GEANT4. The mono-energetic source simulations demonstrate agreement in detector response within 5% between the two packages for all neutron energies, and within 1% for neutron energies between 100 eV and 5 MeV. Cross-checks between the two types of simulations using ISO-8529 252Cf energy bins demonstrates that MCNPX results are more self-consistent than are GEANT4 results, by 3-4%.

  10. Excitation wavelength dependence of water-window line emissions from boron-nitride laser-produced plasmas

    OpenAIRE

    Crank, M.; Harilal, S. S.; S.M. Hassan; Hassanein, A.

    2012-01-01

    We investigated the effects of laser excitation wavelength on water-window emission lines of laser-produced boron-nitride plasmas. Plasmas are produced by focusing 1064 nm and harmonically generated 532 and 266 nm radiation from a Nd:YAG laser on BN target in vacuum. Soft x-ray emission lines in the water-window region are recorded using a grazing-incidence spectrograph. Filtered photodiodes are used to obtain complementary data for water-window emission intensity and angular dependence. Spec...

  11. Boron-10 ABUNCL Prototype Models And Initial Active Testing

    Energy Technology Data Exchange (ETDEWEB)

    Kouzes, Richard T.; Ely, James H.; Lintereur, Azaree T.; Siciliano, Edward R.

    2013-04-23

    The Department of Energy Office of Nuclear Safeguards and Security (NA-241) is supporting the project Coincidence Counting With Boron-Based Alternative Neutron Detection Technology at Pacific Northwest National Laboratory (PNNL) for the development of a 3He proportional counter alternative neutron coincidence counter. The goal of this project is to design, build and demonstrate a system based upon 10B-lined proportional tubes in a configuration typical for 3He-based coincidence counter applications. This report provides results from MCNPX model simulations and initial testing of the active mode variation of the Alternative Boron-Based Uranium Neutron Coincidence Collar (ABUNCL) design built by General Electric Reuter-Stokes. Initial experimental testing of the as-delivered passive ABUNCL was previously reported.

  12. Boron neutron capture therapy (BNCT) using fast neutrons: Effects in two human tumor cell lines

    International Nuclear Information System (INIS)

    The results demonstrate that the effect of fast neutrons on cell survival in cell culture can be enhanced by boron neutron capture reaction. Even with lower enhancement ratios, the concept of NCT assisted fast neutron therapy may successfully be applied for tumor treatment with the Essen cyclotron. (orig.)

  13. A Neutron Rem Counter

    International Nuclear Information System (INIS)

    A neutron detector is described which measures the neutron dose rate in rem/h independently of the energy of the neutrons from thermal to 15 MeV. The detector consists of a BF3 proportional counter surrounded by a shield made of polyethylene and boron plastic that gives the appropriate amount of moderation and absorption to the impinging neutrons to obtain rem response. Two different versions have been developed. One model can utilize standard BF3 counters and is suitable for use in installed monitors around reactors and accelerators and the other model is specially designed for use in a portable survey instrument. The neutron rem counter for portable instruments has a sensitivity of 2.4 cps/mrem/h and is essentially nondirectional in response. With correct bias setting the counter is insensitive to gamma exposure up to 200 r/h from Co-60

  14. Safeguards Technology Factsheet 3He-free Neutron Coincidence Counter

    Energy Technology Data Exchange (ETDEWEB)

    Henzlova, Daniela [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Menlove, Howard Olsen [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2016-04-21

    A full scale thermal neutron coincidence counter (High Level Neutron CounterBoron: HLNB) based on 3He alternative detection technology was designed and built at LANL and field tested at Plutonium Conversion Development Facility (PCDF) of Japan Atomic Energy Agency (JAEA) during FY15. HLNB is based on boron-lined proportional plates that replace the traditional 3He proportional tubes and was designed as a direct alternative to 3He-based High Level Neutron Coincidence Counter (HLNC-II). During the JAEA field trial the HLNB demonstrated comparable performance to HLNC-II, which represents a key development in the area of 3He alternative technologies and provides a complete demonstration of the technology for nuclear safeguards applications including high mass MOX samples.

  15. Separation and purification of four compounds from Desmodium styracifolium using off-line two-dimensional high-speed counter-current chromatography.

    Science.gov (United States)

    Su, Wen; Liu, Qi; Yang, Qing; Yu, Jingang; Chen, Xiaoqing

    2013-10-01

    An off-line 2D high-speed counter-current chromatography technique in preparative scale has been successfully applied to separate and purify the main compounds from the ethyl acetate extract of Desmodium styracifolium. A two-phase solvent system composed of n-hexane/ethyl acetate/methanol/water at an optimized volume ratio of 1:2:1:2 v/v/v/v was used. Conventional high-speed counter-current chromatography was used as the first dimension, and the upper phase of the solvent system was used as the stationary phase in the head-to-tail elution mode at a flow rate of 2.0 mL/min and a rotation speed of 900 rpm. Recycling high-speed counter-current chromatography served as the second dimension to separate an impure fraction of the first dimension. A total of four well-separated substances including vanillic acid (1), β-sitosterol (2), formononetin (3), and aromadendrin (4) were obtained, and their purities and structures were identified by HPLC-MS and (1) H NMR spectroscopy. The results illustrated that off-line 2D high-speed counter-current chromatography is an effective way to isolate compounds in complex samples. PMID:23939907

  16. Emission Lines of Boron, Carbon, Oxygen and Iron in Tokamak Plasma

    Institute of Scientific and Technical Information of China (English)

    DI Long; WAN Bao-Nian; ZHAO Gang; ZHANG Jie; SHI Jian-Rong; WANG Shou-Jun; DONG Quan-Li; ZHAO Jing; LI Yu-Tong; FU Jia; WANG Fu-Di; SHI Yue-Jiang

    2011-01-01

    The emission lines of B,C,O and Fe in tokamak plasma are reported. The spectra are compared with those calculated by the CHIANTI code,which is based on the collisional-radiative models with a large amount of accurate atomic data.General agreement is obtained between the results of experiment and computation.Most of the lines in the spectra are identified,and the relative number density ratios orB,C,O and Fe are determined.It is found that the processes of line formation in our experiment are similar to those in the stellar coronae.The line-averaged electron density of the tokamak plasma is measured by the HCN laser,indicating a good agreement with the theoretical prediction by the density-dependent line ratio of Fe XXI.

  17. A gamma-ray telescope for on-line measurements of low boron concentrations in a head-phantom for BNCT

    International Nuclear Information System (INIS)

    In Boron Neutron Capture Therapy the 10B(n, α)7Li reaction is used to create a tumour destructing field by the emitted high-LET (Linear Energy Transfer) particles. This reaction is accompanied by the emission of a photon of energy 478 keV. This can serve as a probe for detection of the reaction rate and thereby provide a tool to assess the boron concentration during therapy. An experimental configuration has been designed for on-line measurements of the 10B prompt gamma rays in a background of hydrogen neutron capture prompt gamma rays, neutrons and gamma rays coming from the reactor. At a facility with epithermal neutrons of the Low Flux Reactor a head phantom has been irradiated with neutorns. This phantom is filled with water and a small volume of 7.8 cm3 containing 62 ppm 10B, simulating a tumour. The experimental configuration for prompt gamma measurements has been expanded to perform tomography. The reconstruction of the position and the size of the tumour and its boron cencentration appeared to be possible. The first experiments at the therapy room in the High Flux Reactor showed that this method can probably be expanded for on-line monitoring of the total boron amount in a patients head. Next to this, Monte Carlo calculations and foil activation measurements have been performed to obtain the neutron spectrum of the epithermal beam of the LFR. With the insight achieved with these calculations it has been possible to optimize the total neutron flux. By introduction of a graphite scatter in the beam tube close to the reactr core, the flux has been rainsed with about 65%. With the computer code DORT neutron distributions over the phantom have been calculated for 47 energy groups. These calculations are necessary for ultimate boron tomography. (orig.)

  18. A gamma-ray telescope for on-line measurements of low boron concentrations in a head-phantom for BNCT

    Energy Technology Data Exchange (ETDEWEB)

    Verbakel, W.F.A.R.

    1996-06-01

    In Boron Neutron Capture Therapy the {sup 10}B(n, {alpha}){sup 7}Li reaction is used to create a tumour destructing field by the emitted high-LET (Linear Energy Transfer) particles. This reaction is accompanied by the emission of a photon of energy 478 keV. This can serve as a probe for detection of the reaction rate and thereby provide a tool to assess the boron concentration during therapy. An experimental configuration has been designed for on-line measurements of the {sup 10}B prompt gamma rays in a background of hydrogen neutron capture prompt gamma rays, neutrons and gamma rays coming from the reactor. At a facility with epithermal neutrons of the Low Flux Reactor a head phantom has been irradiated with neutorns. This phantom is filled with water and a small volume of 7.8 cm{sup 3} containing 62 ppm {sup 10}B, simulating a tumour. The experimental configuration for prompt gamma measurements has been expanded to perform tomography. The reconstruction of the position and the size of the tumour and its boron cencentration appeared to be possible. The first experiments at the therapy room in the High Flux Reactor showed that this method can probably be expanded for on-line monitoring of the total boron amount in a patients head. Next to this, Monte Carlo calculations and foil activation measurements have been performed to obtain the neutron spectrum of the epithermal beam of the LFR. With the insight achieved with these calculations it has been possible to optimize the total neutron flux. By introduction of a graphite scatter in the beam tube close to the reactr core, the flux has been rainsed with about 65%. With the computer code DORT neutron distributions over the phantom have been calculated for 47 energy groups. These calculations are necessary for ultimate boron tomography. (orig.).

  19. Nutrition Counter

    Science.gov (United States)

    ... Counter: A Reference For The Kidney Patient AAKP Nutrition Counter: A Reference For The Kidney Patient Buy ... Harum RD, CSR, LD Certified Specialist in Renal Nutrition, Miami, Florida Reviewed by: 2005 – Maria Karalis, MBA, ...

  20. Needle counter

    International Nuclear Information System (INIS)

    Needle counter had been devised by Geiger about 60 years ago before the present GM counter appeared. It is suitable for the detection of weak radiation because it is limited in effective volume, if the background due to mainly cosmic ray is proportional to the effective volume of the counter. Recently the very low β detector having a needle counter as the main detector has been developed. It showed highly excellent performance in the measurements of small area samples, about ten times sensitive as compared with other detectors. The counter is installed in the very low radiation measuring well at Nokogiriyama, Chiba Prefecture, using a NaI scintillator as its guard counter. D. H. Wilkinson first treated a gas amplification counter theoretically and quantitatively. The authors have obtained good results in the comparison with the experiments of the counter using a generalized form of Wilkinson theory. The findings obtained through this study seem to be applicable to the electrode arrangement which is important for the counter design. It was found that the excellent rise time of induced pulses in a gas amplification counter was achieved in larger amplification factor and smaller convolution effect. In the detection of charged particles with small obstructing capability such as γ ray, faster rise time and higher pulses can be obtained with needle counters than wire counters. (Wakatsuki, Y.)

  1. On-line reconstruction of low boron concentrations by in vivo γ-ray spectroscopy for BNCT

    International Nuclear Information System (INIS)

    Boron neutron capture therapy (BNCT) is a radiation therapy in which the neutron capture reaction of 10B is used for the selective destruction of tumours. At the High Flux Reactor (HFR) in Petten, a therapy facility with an epithermal neutron beam has been built. In the first instance, patients with brain tumours will be treated. The doses delivered to the tumour and to the healthy tissue depend on the thermal neutron fluence and on the boron concentrations in these regions. An accurate determination of the patient dose during therapy requires knowledge of these time-dependent concentrations. For this reason, a γ-ray telescope system, together with a reconstruction formalism, have been developed. By using a γ-ray detector in a telescope configuration, boron neutron capture γ-rays of 478 keV emitted by a small specific region can be detected. The reconstruction formalism can calculate absolute boron concentrations using the measured boron γ-ray detection rates. Besides the boron γ-rays, a large component of 2.2 MeV γ-rays emitted at thermal neutron capture in hydrogen is measured. Since the hydrogen distribution is almost homogeneous within the head, this component can serve as a measure of the total number of thermal neutrons in the observed volume. By using the hydrogen γ-ray detection rate for normalization of the boron concentration, the reconstruction tool eliminates the greater part of the influence of the inhomogeneity of the thermal neutron distribution. MCNP calculations are used as a tool for the optimization of the detector configuration. Experiments on a head phantom with 5 ppm 10B in healthy tissue showed that boron detection with a standard deviation of 3% requires a minimum measuring time of 2 min live time. From two position-dependent measurements, boron concentrations in two compartments (healthy tissue and tumour) can be determined. The reconstruction of the boron concentration in healthy tissue can be done with a standard deviation of 6

  2. Separation of five flavonoids from tartary buckwheat (Fagopyrum tataricum (L.) Gaertn) grains via off-line two dimensional high-speed counter-current chromatography.

    Science.gov (United States)

    Jiang, Shujing; Liu, Qi; Xie, Yixi; Zeng, Hualiang; Zhang, Li; Jiang, Xinyu; Chen, Xiaoqing

    2015-11-01

    An off-line two dimensional (2D) high-speed counter-current chromatography (HSCCC) strategy was successfully used for preparative separation of five flavonoids from tartary buckwheat (Fagopyrum tataricum (L.) Gaertn) grains with different solvent systems for the first time in this paper. n-Hexane-ethyl acetate-methanol-water 3:5:3:5 (v/v) was selected as the first dimension solvent system to purify quercetin (4) and kaempferol (5). The second dimension solvent system, ethyl acetate-n-butanol-water 7:3:10 (v/v), was used to isolate quercetin 3-O-rutinoside-3'-O-β-glucopyranoside (1), rutin (2) and kaempferol 3-rutinoside (3). The purities of these compounds were all above 96.0% and their structures were identified through UV, MS and (1)H NMR. The results indicated that the off-line 2D HSCCC is an efficient technique to isolate flavonoids compounds from grains. PMID:25976805

  3. On-line coupling of counter-current chromatography and macroporous resin chromatography for continuous isolation of arctiin from the fruit of Arctium lappa L.

    Science.gov (United States)

    Guo, Mengzhe; Liang, Junling; Wu, Shihua

    2010-08-13

    In this work, we have developed a novel hybrid two-dimensional counter-current chromatography and liquid chromatography (2D CCC x LC) system for the continuous purification of arctiin from crude extract of Arctium lappa. The first dimensional CCC column has been designed to fractionalize crude complex extract into pure arctiin effluent using a one-component organic/salt-containing system, and the second dimensional LC column has been packed with macroporous resin for on-line adsorption, desalination and desorption of arctiin which was effluent purified from the first CCC dimension. Thus, the crude arctiin mixture has been purified efficiently and conveniently by on-line CCC x LC in spite of the use of a salt-containing solvent system in CCC separation. As a result, high purity (more than 97%) of arctiin has been isolated by repeated injections both using the ethyl acetate-8% sodium chloride aqueous solution and butanol-1% sodium chloride aqueous solution. By contrast with the traditional CCC processes using multi-component organic/aqueous solvent systems, the present on-line CCC x LC process only used a one-component organic solvent and thus the solvent is easier to recover and regenerate. All of used solvents such as ethyl acetate, n-butanol and NaCl aqueous solution are low toxicity and environment-friendly. Moreover, the lower phase of salt-containing aqueous solution used as mobile phase, only contained minor organic solvent, which will save much organic solvent in continuous separation. In summary, our results indicated that the on-line hybrid 2D CCC x LC system using one-component organic/salt-containing aqueous solution is very promising and powerful tool for high-throughput purification of arctiin from fruits of A. lappa. PMID:20619844

  4. Monte Carlo simulation of a new air-mixed gas-flow proportional counter for on-line airborne radon activity concentration measurements

    International Nuclear Information System (INIS)

    A Monte Carlo simulation code, named PROCSIM, has been written and used to optimize the design of a Multiple Cell Proportional Counter (MCPC) prototype intended for airborne radon activity concentration on-line measurements. PROCSIM code takes into account all the electrical and geometrical parameters and models the main physical processes that determine directly the detector performances such as the electric field distribution, the alpha stopping and primary electron-ion pairs production, the wall effect, the gas amplification process, the electron attachment effect and also the Gaussian broadening of the collected alpha pulse height spectra. The MCPC uses an argon-propane (1%) gas mixture to which is admixed up to 10 % of air, whose radon activity concentration has to be measured. Using PROCSIM code, the main design parameters of the MCPC prototype were optimized in order to achieve alpha detection efficiency greater than 95 %. The first run results show that the admixture of 10 % of air is sufficient to assess radon concentration activities as low as 1 Bq/m3 for a counting time period of 10 minutes, resulting thus in an expected radon activity concentration sensitivity of around 0.2 cpm/Bq.m-3, with an energy-equivalent discrimination threshold set to 0.5 MeV. Finally, the possibility to use the present MCPC prototype for on-line measurement of time varying airborne radon activity concentration is discussed. (author)

  5. Novel and efficient 10B lined tubelet detector as a replacement for 3He neutron proportional counters

    Science.gov (United States)

    Tsorbatzoglou, Kyriakos; McKeag, Robert D.

    2011-10-01

    This paper presents a novel and robust proportional detector which addresses the well publicized shortage of 3He gas by using a 10B lining applied to a tubelet configuration. The advantage of the tubelet structure is that it yields a detector maintaining the form factor of a conventional 3He tube whilst achieving a sensitivity of up to 75% of a 3 atm 3He device. The design and fabrication of the tubelet detector is presented and discussed with test data comparing the new detector to existing 3He and BF 3 tubes. The application of the tubelet design to security and industrial applications including retro-fitting to existing portals and suitability for high integrity oil and gas installations is addressed.

  6. Effects of Edge Passivations on the Electronic and Magnetic Properties of Zigzag Boron-Nitride Nanoribbons with Even and Odd-Line Stone-Wales (5-7 Pair) Defects

    OpenAIRE

    Yamijala, Sharma SRKC; Pati, Swapan K.

    2014-01-01

    First-principles spin-polarized calculations have been performed on passivated Boron-Nitride Nanoribbons (BNNRs) with pentagon-heptagon line-defects (PHLDs) (also called as Stone-Wales line-defects). Two kinds of PHLDs, namely, even-line and odd-line PHLDs, have been added either at one edge or at both edges of BNNRs. Single-edge (with all its different possibilities, for example, for a BNNR with 2-line PHLD at single-edge there are 8 possibilities) as well as both-edge passivations have been...

  7. Raman spectroscopy of boron carbides and related boron-containing materials

    International Nuclear Information System (INIS)

    Raman spectra of crystalline boron, boron carbide, boron arsenide (B12As2), and boron phosphide (B12P2) are reported. The spectra are compared with other boron-containing materials containing the boron icosahedron as a structural unit. The spectra exhibit similar features some of which correlate with the structure of the icosahedral units of the crystals. The highest Raman lines appear to be especially sensitive to the B-B distance in the polar triangle of the icosahedron. Such Raman structural markers are potentially useful in efforts to tailor electronic properties of these high temperature semiconductors and thermoelectrics

  8. Boron isotopic enrichment by displacement chromatography

    International Nuclear Information System (INIS)

    10B enriched boron is used in applications requiring high volumetric neutron absorption (absorption cross section- 3837 barn for thermal and 1 barn for 1 MeV fast neutron). It is used in fast breeder reactor (as control rod material), in neutron counter, in Boron Neutron Capture Therapy etc. Owing to very small separation factor, boron isotopic enrichment is a complex process requiring large number of separation stages. Heavy Water Board has ventured in industrial scale production of 10B enriched boron using Exchange Distillation Process as well as Ion Displacement Chromatography Process. Ion Displacement Chromatography process is used in Boron Enrichment Plant at HWP, Manuguru. It is based on isotopic exchange between borate ions (B(OH)4-) on anion exchange resin and boric acid passing through resin. The isotopic exchange takes place due to difference in zero point energy of 10B and 11B

  9. Body counter

    International Nuclear Information System (INIS)

    The paper gives a survey on some applications of the whole body counter in clinical practice and a critical study of its application as a routine testing method. Remarks on the necessary precautions are followed by a more detailed discussion of the determination of the natural potassium content, the iron metabolism, the vitamin B12 test, investigations of the metabolism of the bone using 47Ca and 85Sr, investigations with iodine and iodine-labelled substances, clearance investigations (in particular the 51Cr EDTA clearance test), as well as the possibilities of neutron activation in vivo. (ORU/AK)

  10. Electroextraction of boron from boron carbide scrap

    Energy Technology Data Exchange (ETDEWEB)

    Jain, Ashish [Chemistry Group, Indira Gandhi Centre for Atomic Research, Kalpakkam – 603102 (India); Anthonysamy, S., E-mail: sas@igcar.gov.in [Chemistry Group, Indira Gandhi Centre for Atomic Research, Kalpakkam – 603102 (India); Ghosh, C. [Physical Metallurgy Group, Indira Gandhi Centre for Atomic Research, Kalpakkam – 603102 (India); Ravindran, T.R. [Materials Science Group, Indira Gandhi Centre for Atomic Research, Kalpakkam – 603102 (India); Divakar, R.; Mohandas, E. [Physical Metallurgy Group, Indira Gandhi Centre for Atomic Research, Kalpakkam – 603102 (India)

    2013-10-15

    Studies were carried out to extract elemental boron from boron carbide scrap. The physicochemical nature of boron obtained through this process was examined by characterizing its chemical purity, specific surface area, size distribution of particles and X-ray crystallite size. The microstructural characteristics of the extracted boron powder were analyzed by using scanning electron microscopy and transmission electron microscopy. Raman spectroscopic examination of boron powder was also carried out to determine its crystalline form. Oxygen and carbon were found to be the major impurities in boron. Boron powder of purity ∼ 92 wt. % could be produced by the electroextraction process developed in this study. Optimized method could be used for the recovery of enriched boron ({sup 10}B > 20 at. %) from boron carbide scrap generated during the production of boron carbide. - Highlights: • Recovery of {sup 10}B from nuclear grade boron carbide scrap • Development of process flow sheet • Physicochemical characterization of electroextracted boron • Microscopic examination of electroextracted boron.

  11. Electroextraction of boron from boron carbide scrap

    International Nuclear Information System (INIS)

    Studies were carried out to extract elemental boron from boron carbide scrap. The physicochemical nature of boron obtained through this process was examined by characterizing its chemical purity, specific surface area, size distribution of particles and X-ray crystallite size. The microstructural characteristics of the extracted boron powder were analyzed by using scanning electron microscopy and transmission electron microscopy. Raman spectroscopic examination of boron powder was also carried out to determine its crystalline form. Oxygen and carbon were found to be the major impurities in boron. Boron powder of purity ∼ 92 wt. % could be produced by the electroextraction process developed in this study. Optimized method could be used for the recovery of enriched boron (10B > 20 at. %) from boron carbide scrap generated during the production of boron carbide. - Highlights: • Recovery of 10B from nuclear grade boron carbide scrap • Development of process flow sheet • Physicochemical characterization of electroextracted boron • Microscopic examination of electroextracted boron

  12. Separation of five compounds from leaves of Andrographis paniculata (Burm. f.) Nees by off-line two-dimensional high-speed counter-current chromatography combined with gradient and recycling elution.

    Science.gov (United States)

    Zhang, Li; Liu, Qi; Yu, Jingang; Zeng, Hualiang; Jiang, Shujing; Chen, Xiaoqing

    2015-05-01

    An off-line two-dimensional high-speed counter-current chromatography method combined with gradient and recycling elution mode was established to isolate terpenoids and flavones from the leaves of Andrographis paniculata (Burm. f.) Nees. By using the solvent systems composed of n-hexane/ethyl acetate/methanol/water with different volume ratios, five compounds including roseooside, 5,4'-dihydroxyflavonoid-7-O-β-d-pyranglucuronatebutylester, 7,8-dimethoxy-2'-hydroxy-5-O-β-d-glucopyranosyloxyflavon, 14-deoxyandrographiside, and andrographolide were successfully isolated. Purities of these isolated compounds were all over 95% as determined by high-performance liquid chromatography. Their structures were identified by UV, mass spectrometry, and (1) H NMR spectroscopy. It has been demonstrated that the combination of off-line two-dimensional high-speed counter-current chromatography with different elution modes is an efficient technique to isolate compounds from complex natural product extracts. PMID:25675944

  13. Off-line hyphenation of boronate affinity monolith-based extraction with matrix-assisted laser desorption/ionization time-of-flight mass spectrometry for efficient analysis of glycoproteins/glycopeptides.

    Science.gov (United States)

    Bie, Zijun; Chen, Yang; Li, Hengye; Wu, Ronghu; Liu, Zhen

    2014-06-27

    Boronate affinity materials have attracted increasing attentions as sample enrichment platforms for glycoproteomic analysis in recent years. However, most of the boronate affinity materials that have already employed for proteomic analysis are suffering from apparent disadvantages, such as alkaline pH for binding, weak affinity, and relatively poor selectivity. Benzoboroxoles are a unique class of boronic acids which have showed excellent binding properties for the recognition of cis-diol-containing compounds. Recently, a 3-carboxy-benzoboroxole-functionalized monolithic column had been reported and it had exhibited the best selectivity and affinity as well as the lowest binding pH among all reported boronate affinity monolithic columns. In this study, an off-line hyphenation of this boronate affinity monolithic column-based extraction with matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF MS) was developed and the powerfulness of this hyphenated approach in the analysis of glycoproteins and glycopeptides in complex samples was investigated. The approach was first applied to the analysis of glycopeptides in the tryptic digest of horseradish peroxidase (HRP). Totally 22 glycopeptides were identified. To the best of our knowledge, this is the best performance among all the boronic acid-functionalized materials. We further employed this approach to the analysis of intact proteins in human saliva. Totally 6 intact glycoproteins were successfully identified. As comparison, when the samples were analyzed without extraction, only a few glycopeptides were identified from the tryptic digest of HRP while no glycoproteins were found from the saliva samples. PMID:24928239

  14. Lattice dynamics of α boron and of boron carbide

    International Nuclear Information System (INIS)

    The atomic structure and the lattice dynamics of α boron and of B4C boron carbide have been studied by Density Functional Theory (D.F.T.) and Density Functional Perturbation Theory (D.F.P.T.). The bulk moduli of the unit-cell and of the icosahedron have been investigated, and the equation of state at zero temperature has been determined. In α boron, Raman diffusion and infrared absorption have been studied under pressure, and the theoretical and experimental Grueneisen coefficients have been compared. In boron carbide, inspection of the theoretical and experimental vibrational spectra has led to the determination of the atomic structure of B4C. Finally, the effects of isotopic disorder have been modeled by an exact method beyond the mean-field approximation, and the effects onto the Raman lines has been investigated. The method has been applied to isotopic alloys of diamond and germanium. (author)

  15. Cell diameter measurements obtained with a handheld cell counter could be used as a surrogate marker of G2/M arrest and apoptosis in colon cancer cell lines exposed to SN-38

    Energy Technology Data Exchange (ETDEWEB)

    Tahara, Makiko [Oncogene Research Unit/Cancer Prevention Unit, Tochigi Cancer Center Research Institute, Utsunomiya, Tochigi (Japan); Department of Gastrointestinal Surgery, Jichi Medical University, Shimotsuke, Tochigi (Japan); Inoue, Takeshi [Oncogene Research Unit/Cancer Prevention Unit, Tochigi Cancer Center Research Institute, Utsunomiya, Tochigi (Japan); Miyakura, Yasuyuki; Horie, Hisanaga; Yasuda, Yoshikazu [Department of Gastrointestinal Surgery, Jichi Medical University, Shimotsuke, Tochigi (Japan); Fujii, Hirofumi [Division of Clinical Oncology, Jichi Medical University, Shimotsuke, Tochigi (Japan); Kotake, Kenjiro [Department of Surgery, Tochigi Cancer Center, Utsunomiya, Tochigi (Japan); Sugano, Kokichi, E-mail: ksugano@tcc.pref.tochigi.lg.jp [Oncogene Research Unit/Cancer Prevention Unit, Tochigi Cancer Center Research Institute, Utsunomiya, Tochigi (Japan)

    2013-05-17

    Highlights: •Chemo-sensitivity to SN-38 was assayed by the automated cell counter. •Colon cancer cell line, HCT116 cells were more sensitive to SN-38 than HT29 cells. •Increase of cell size reflects G2/M arrest. •Appearance of small particles indicates cell apoptosis. -- Abstract: In vitro assessment of chemosensitivity are important for experiments evaluating cancer therapies. The Scepter 2.0 cell counter, an automated handheld device based on the Coulter principle of impedance-based particle detection, enables the accurate discrimination of cell populations according to cell size and volume. In this study, the effects of SN-38, the active metabolite of irinotecan, on the colon cancer cell lines HCT116 and HT29 were evaluated using this device. The cell count data obtained with the Scepter counter were compared with those obtained with the {sup 3}H-thymidine uptake assay, which has been used to measure cell proliferation in many previous studies. In addition, we examined whether the changes in the size distributions of these cells reflected alterations in the frequency of cell cycle arrest and/or apoptosis induced by SN-38 treatment. In our experiments using the Scepter 2.0 cell counter, the cell counts were demonstrated to be accurate and reproducible measure and alterations of cell diameter reflected G2/M cell cycle arrest and apoptosis. Our data show that easy-to-use cell counting tools can be utilized to evaluate the cell-killing effects of novel treatments on cancer cells in vitro.

  16. Cell diameter measurements obtained with a handheld cell counter could be used as a surrogate marker of G2/M arrest and apoptosis in colon cancer cell lines exposed to SN-38

    International Nuclear Information System (INIS)

    Highlights: •Chemo-sensitivity to SN-38 was assayed by the automated cell counter. •Colon cancer cell line, HCT116 cells were more sensitive to SN-38 than HT29 cells. •Increase of cell size reflects G2/M arrest. •Appearance of small particles indicates cell apoptosis. -- Abstract: In vitro assessment of chemosensitivity are important for experiments evaluating cancer therapies. The Scepter 2.0 cell counter, an automated handheld device based on the Coulter principle of impedance-based particle detection, enables the accurate discrimination of cell populations according to cell size and volume. In this study, the effects of SN-38, the active metabolite of irinotecan, on the colon cancer cell lines HCT116 and HT29 were evaluated using this device. The cell count data obtained with the Scepter counter were compared with those obtained with the 3H-thymidine uptake assay, which has been used to measure cell proliferation in many previous studies. In addition, we examined whether the changes in the size distributions of these cells reflected alterations in the frequency of cell cycle arrest and/or apoptosis induced by SN-38 treatment. In our experiments using the Scepter 2.0 cell counter, the cell counts were demonstrated to be accurate and reproducible measure and alterations of cell diameter reflected G2/M cell cycle arrest and apoptosis. Our data show that easy-to-use cell counting tools can be utilized to evaluate the cell-killing effects of novel treatments on cancer cells in vitro

  17. Determination of boron content in boron carbide, boron nitride and amorphous boron

    International Nuclear Information System (INIS)

    In the present article an analyzing method of determination of boron content in boron carbide, boron nitride and amorphous boron described. Examined samples were digested with potassium hydroxide and potassium nitrate in nickel crucible and the boron contents determined subsequently by an alcalimetric titration of boric acid in presence of mannite resp. sorbite. (author)

  18. Distributed performance counters

    Science.gov (United States)

    Davis, Kristan D; Evans, Kahn C; Gara, Alan; Satterfield, David L

    2013-11-26

    A plurality of first performance counter modules is coupled to a plurality of processing cores. The plurality of first performance counter modules is operable to collect performance data associated with the plurality of processing cores respectively. A plurality of second performance counter modules are coupled to a plurality of L2 cache units, and the plurality of second performance counter modules are operable to collect performance data associated with the plurality of L2 cache units respectively. A central performance counter module may be operable to coordinate counter data from the plurality of first performance counter modules and the plurality of second performance modules, the a central performance counter module, the plurality of first performance counter modules, and the plurality of second performance counter modules connected by a daisy chain connection.

  19. Inheritance of Boron Efficiency in Oilseed Rape

    Institute of Scientific and Technical Information of China (English)

    SHI Lei; WANG Yun-Hua; NIAN Fu-Zhao; LU Jian-Wei; MENG Jin-Ling; XU Fang-Sen

    2009-01-01

    Field experiments were conducted to study the inheritance of boron efficiency in oilseed rape (Brassica napus L.) by evaluating the boron (B) efficiency coefficient (BEC,the ratio of the seed yield at below the critical boron level to that at the boron-sufficient level) with 657 F2:3 fines of a population derived from a cross between a B-efficient cultivar,Qingyou 10,and a B-inefficient cultivar,Bakow.Qingyou i0 had high BEC as well as high seed yield at low available soil B.On the contrary,Bakow produced low seed yield at low B status.Boron deficiency decreased the seed yield of the F2:3 lines to different extents and the distribution of BEC of the population showed a bimodal pattern.When the 657 F2:3 lines were grouped into B-efficient lines and B-inefficient lines according to their BEC,the ratio of B-efficient lines to B-inefficient lines fitted the expected ratio (3:1),indicating that one major gene controlled the B-efficiency trait.127 F2:3 lines selected from the population at random,with distribution of BEC similar to that of the overall population,were used to identify the target region for fine mapping of the boron efficiency gene.

  20. Scintillation counter, segmented shield

    International Nuclear Information System (INIS)

    A scintillation counter, particularly for counting gamma ray photons, includes a massive lead radiation shield surrounding a sample-receiving zone. The shield is disassembleable into a plurality of segments to allow facile installation and removal of a photomultiplier tube assembly, the segments being so constructed as to prevent straight-line access of external radiation through the shield into radiation-responsive areas. Provisions are made for accurately aligning the photomultiplier tube with respect to one or more sample-transmitting bores extending through the shield to the sample receiving zone. A sample elevator, used in transporting samples into the zone, is designed to provide a maximum gamma-receiving aspect to maximize the gamma detecting efficiency. (U.S.)

  1. Calibration of the HB-line active well neutron coincidence counter for measure of LANL 3013 highly enriched uranium product splits

    International Nuclear Information System (INIS)

    In this paper, the setup, calibration, and testing of the F-Area Analytical Labs active well neutron coincidence counter (HV-221000-NDA-X-1-DKAWCC- 1) in SRNL are described for use in the Savannah River Site (SRS) transuranium metal production facility to enable assay of mixed uranium/plutonium metal product. The instrument was required within a three-month window for availability upon receipt of LANL uranium oxide samples into the SRS facility. Calibration of the instrument in the SRNL nuclear nondestructive assay facility in the range 10-400 g HEU is described. We also report qualification and installation of the instrument for assay of the initial suite of product samples. (author)

  2. Elementary boron and metal-boron compounds

    International Nuclear Information System (INIS)

    Elementary boron is of interest for its peculiar and difficult bonding behaviour in solids. Due to its high oxygen affinity we find no elementary boron in nature. For the same reason it is difficult to isolate pure, elementary boron, and much confusion about 'boron crystals' has been the result of more than 100 years of research. The polymorphic forms of elementary boron and its closely related higher carbides and higher metal borides as well as the simple metal borides, B3C and BN are reported. The quantum-mechanical background responsible for structure and stoichiometry of these crystals is given. (orig.)

  3. Clinical evaluation of neodymium-iron-boron (Ne2Fe14B) rare earth magnets in the treatment of mid line diastemas

    OpenAIRE

    Prasad, Mandava; Manoj-Kumar, Mitta; Gowri-Sankar, Singaraju; Chaitanya, Nellore; Vivek-Reddy, Ganugapanta; Venkatesh, Nettam

    2016-01-01

    Background: To evaluate the closure of midline diastema using the Neodymium-Iron-Boron magnets and to compare the treatment duration of midline diastemas with the use of magnets compared to regular orthodontic treatment. Materials and Methods: Thirty patients with age group 12 to 30 years with the midline diastema ranging from 0.5 to 3mm were selected. These patients were divided into two groups. Diastema closure in one group was accomplished by conventional method, in other group ...

  4. Clinical evaluation of neodymium-iron-boron (Ne2Fe14B) rare earth magnets in the treatment of mid line diastemas

    OpenAIRE

    Prasad, Mandava; Manoj-Kumar, Mitta; Gowri-Sankar, Singaraju; Chaitanya, Nellore; Vivek-Reddy, Ganugapanta; Venkatesh, Nettam

    2016-01-01

    Background To evaluate the closure of midline diastema using the Neodymium-Iron-Boron magnets and to compare the treatment duration of midline diastemas with the use of magnets compared to regular orthodontic treatment. Material and Methods Thirty patients with age group 12 to 30 years with the midline diastema ranging from 0.5 to 3mm were selected. These patients were divided into two groups. Diastema closure in one group was accomplished by conventional method, in other group was done with ...

  5. FLEXIBLE GEIGER COUNTER

    Science.gov (United States)

    Richter, H.G.; Gillespie, A.S. Jr.

    1963-11-12

    A flexible Geiger counter constructed from materials composed of vinyl chloride polymerized with plasticizers or co-polymers is presented. The counter can be made either by attaching short segments of corrugated plastic sleeving together, or by starting with a length of vacuum cleaner hose composed of the above materials. The anode is maintained substantially axial Within the sleeving or hose during tube flexing by means of polystyrene spacer disks or an easily assembled polyethylene flexible cage assembly. The cathode is a wire spiraled on the outside of the counter. The sleeving or hose is fitted with glass end-pieces or any other good insulator to maintain the anode wire taut and to admit a counting gas mixture into the counter. Having the cathode wire on the outside of the counter substantially eliminates the objectional sheath effect of prior counters and permits counting rates up to 300,000 counts per minute. (AEC)

  6. The first CEDAR counter

    CERN Multimedia

    1976-01-01

    The first differential Cerenkov counter with chromatic corrections (called CEDAR) successfully tested at the PS in July 75. These counters were used in the SPS hadronic beams for particle identification. Some of the eight photomultipliers can be seen: they receive the light reflected back through the annular diaphragm. René Maleyran stands on the left.

  7. Sputtering behavior of boron and boron carbide

    International Nuclear Information System (INIS)

    Sputtering yields of boron were measured with D+ and B+ ions for normal and oblique angles of incidence. Self-sputtering data of boron carbide were simulated in the experiment by using Ne+ ions. The energies of the impinging ions were between 20 eV and 10 keV. The measured data are compared with computer simulated values calculated with the TRIMSP program. The boron data for normal ion impact are higher than the calculated values, whereas those for oblique ion incidence are smaller than the calculation predicts. This discrepancy is explained by the surface roughness and supported by SEM micrographs. The comparison of the boron carbide data with TRIMSP calculations shows much better agreement than the boron data. In this case the target surface was much smoother. (orig.)

  8. Boron nitride converted carbon fiber

    Energy Technology Data Exchange (ETDEWEB)

    Rousseas, Michael; Mickelson, William; Zettl, Alexander K.

    2016-04-05

    This disclosure provides systems, methods, and apparatus related to boron nitride converted carbon fiber. In one aspect, a method may include the operations of providing boron oxide and carbon fiber, heating the boron oxide to melt the boron oxide and heating the carbon fiber, mixing a nitrogen-containing gas with boron oxide vapor from molten boron oxide, and converting at least a portion of the carbon fiber to boron nitride.

  9. Mass spectrometric determination of boron isotope in boron carbide

    International Nuclear Information System (INIS)

    Boron isotopes in boron carbide are measured by thermionic ionization mass spectrometry with no prior chemical separation. Boron is converted to sodium borate by fusion of the boron carbide with sodium hydroxide (or sodium carbonate) directly on the rhenium filament. The boron isotopic ratios are measured by using the Na2BO2+ ion

  10. A large Cerenkov counter

    CERN Multimedia

    1981-01-01

    The photo shows the vertex Cerenkov counter C0 back side (with 12 mirrors) of the NA9 experiment. On foreground are members of the team (CERN and Wuppertal Uni), Salvo .., Manfred Poetsch, ..., Jocelyn Thadome, Helmut Braun, Heiner Brueck.

  11. Design of Reversible Counter

    OpenAIRE

    Md. Selim Al Mamun; B. K. Karmaker

    2014-01-01

    This article presents a research work on the design and synthesis of sequential circuits and flip-flops that are available in digital arena; and describes a new synthesis design of reversible counter that is optimized in terms of quantum cost, delay and garbage outputs compared to the existing designs. We proposed a new model of reversible T flip-flop in designing reversible counter.

  12. Neutron dosimetry using proportional counters with tissue equivalent walls

    International Nuclear Information System (INIS)

    The author reminds the calculation method of the neutron absorbed dose in a material and deduce of it the conditions what this material have to fill to be equivalent to biological tissues. Various proportional counters are mode with walls in new tissue equivalent material and filled with various gases. The multiplication factor and neutron energy response of these counters are investigated and compared with those obtained with ethylene lined polyethylene counters. The conditions of working of such proportional counters for neutron dosimetry in energy range 10-2 to 15 MeV are specified. (author)

  13. Optical characteristic analysis of the boronization process by using carborane

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Wonwook; Park, Kyungdeuk; Choi, Youngsun; Oh, Chahwan [Hanyang University, Seoul (Korea, Republic of)

    2014-09-15

    Boronization with carborane (C{sub 2}B{sub 10}H{sub 12}) was achieved in a vacuum vessel coupled to a filament discharge system. Optical emission spectroscopy was employed to characterize the boronization process. The Balmer lines of hydrogen and deuterium were measured, and the boronization process was analyzed by using the intensity ratio of the H{sub α} to the D{sub α} line (I{sub H}/I{sub D}). The relation between the pressure and the intensity ratio was investigated, and the thickness of the deposited boron film was predicted. Also, the dilution ratio H/(H + D) of the boron film was analyzed and compared with the one predicted from an optical analysis of the emission spectrum.

  14. Analysis of counter-rotating wind turbines

    DEFF Research Database (Denmark)

    Shen, Wen Zhong; Zakkam, Vinod Arun Kumar; Sørensen, Jens Nørkær;

    2007-01-01

    This paper presents a study on the performance of a wind turbine with two counter-rotating (CRWT) rotors. The characteristics of the two counter-rotating rotors are on a 3-bladed Nordtank 500 kW rotor. The analysis has been carried out by using an Actuator Line technique implemented in the Navier......-Stokes code EllipSys3D. The analysis shows that the Annual Energy Production can be increased to about 43.5 %, as compared to a wind turbine with a single rotor. In order to determine the optimal settings of the CRWT turbine, parameters such as distance between two rotors and rotational speed have been...

  15. LINES

    Directory of Open Access Journals (Sweden)

    Minas Bakalchev

    2015-10-01

    Full Text Available The perception of elements in a system often creates their interdependence, interconditionality, and suppression. The lines from a basic geometrical element have become the model of a reductive world based on isolation according to certain criteria such as function, structure, and social organization. Their traces are experienced in the contemporary world as fragments or ruins of a system of domination of an assumed hierarchical unity. How can one release oneself from such dependence or determinism? How can the lines become less “systematic” and forms more autonomous, and less reductive? How is a form released from modernistic determinism on the new controversial ground? How can these elements or forms of representation become forms of action in the present complex world? In this paper, the meaning of lines through the ideas of Le Corbusier, Leonidov, Picasso, and Hitchcock is presented. Spatial research was made through a series of examples arising from the projects of the architectural studio “Residential Transformations”, which was a backbone for mapping the possibilities ranging from playfulness to exactness, as tactics of transformation in the different contexts of the contemporary world.

  16. Analysis of boron at Koeberg Power Station

    International Nuclear Information System (INIS)

    Soluble reactivity poisons, also called chemical shim, produce spatially uniform neutron absorption when dissolved in reactor coolant water. The boron-10 isotope having a high neutron absorption coefficient is used in commercial pressurised water reactors (PWR) to limit and control reactivity. This is achieved at Koeberg Nuclear Power Station (KNPS) and the majority of commercial PWR's worldwide by the addition of natural boric acid to the reactor coolant. The boric acid dissolved in the coolant decreases the thermal utilisation factor, causing a decrease in reactivity. By varying the concentration of boric acid (and hence also the B-10 concentration) in the coolant, a process referred to as boration and dilution, the reactivity of the core can be easily managed. An increase in boron concentration (boration) creates negative reactivity and if the boron concentration is reduced (dilution), positive reactivity is added. The changing of boron concentration in a PWR is used primarily to compensate for fuel burn-up or poison build-up. The variation in boron concentration allows control rod use to be minimised, which results in a flatter flux profile over the core than can be produced by control rod manipulation. Accurate laboratory and on-line chemical analysis of boron concentration is important because of its operational implications associated with reactivity control and also for nuclear safety. In a normal fuel cycle, as the nuclear fuel is being consumed, the reactor coolant boric acid (B-10) concentration must be reduced by dilution with purified water to maintain the reactor at constant power. Besides in the reactor coolant water, boric acid concentration is also important in the chemical and volume control system and reactor make-up system for operation. For nuclear safety, boric acid concentrations are technical specification parameters, maintained and monitored in the spent fuel system and safety injection systems. Boron concentration determination is

  17. Compressor surge counter

    Science.gov (United States)

    Castleberry, Kimberly N.

    1983-01-01

    A surge counter for a rotating compressor is provided which detects surging by monitoring the vibration signal from an accelerometer mounted on the shaft bearing of the compressor. The circuit detects a rapid increase in the amplitude envelope of the vibration signal, e.g., 4 dB or greater in less than one second, which is associated with a surge onset and increments a counter. The circuit is rendered non-responsive for a period of about 5 seconds following the detection which corresponds to the duration of the surge condition. This prevents multiple registration of counts during the surge period due to rapid swings in vibration amplitude during the period.

  18. An efficient anticoincidence counter

    CERN Multimedia

    1977-01-01

    This scintillation counter (about 25 cm diameter) was prepared at CERN for an experiment at the Saclay 600 MeV electron linac studying molecular processes originated in liquid hydrogen by muons. The counter is meant to surround the target and detect charged particles emerging from the hydrogen. The experiment was a CERN-Saclay collaboration which used the linac so as to take advantage of the time structure of the electron beam(see CERN Courier Sep 1977 and J. Bardin et al. Phys. Lett. B104 (1981) 320)

  19. Setting up and characterization of 4π -BF3 neutron counter

    International Nuclear Information System (INIS)

    In this paper, the refurbishment and characterization of a 4π-BF3 neutron counter are described. Almost flat efficiency of the outer set of detectors is observed. This counter was extensively used for the measurement of (p, n) cross-sections in the 80's. The counter is made operational with making of new beam line and new electronics

  20. Determination of boron and silicon in boron carbide

    International Nuclear Information System (INIS)

    A sodium carbonate fusion technique for the dissolution of boron carbide followed by the determination of boron by alkalimetric titration and silicon impurity by spectrophotometry is described. The elemental boron content in the commercially available boron carbide ranged from 77.2 to 77.60 % and the silicon in the range 1170 to 2500 ppm. (author)

  1. Microchip Coulter particle counter

    DEFF Research Database (Denmark)

    Larsen, Ulrik Darling; Blankenstein, Gert; Branebjerg, J.

    1997-01-01

    This paper presents a micro device employing the Coulter principle for counting and sizing of living cells and particles in liquid suspension. The microchip Coulter particle counter (μCPC) has been employed in a planar silicon structure covered with glass, which enables detailed observation during...

  2. Silica aerogel Cherenkov counter

    International Nuclear Information System (INIS)

    A practical method for making silica aerogel Cherenkov counters has been developed at KEK, and some tests were performed to evaluate the performance of the counters. The method for making silica aerogel with refractive index between 1.01 and 1.06 is explained in detail. Chemical reaction with methanol, pressure and temperature conditions, and the structure of the autoclave are described together with the whole process. About 20 l aerogel is now produced per week at KEK. The dimensions of the aerogel module is 200 x 100 x 300 mm3. The aerogel with refractive index larger than 1.06 is produced from the aerogel with refractive index 1.06 by heating it up to about 900 deg C. The refractive index can be controlled by the temperature and duration of heating. Refractive index in relation to these conditions is listed in a table. However, the dispersion of the index is about ten times as large as that for the aerogel with lower index (<1.06). The wave length dependence of the transmission length of light for the aerogel was measured and compared with other data obtained at various laboratories. The performance of the counter was evaluated through the experiment with π beam. Average number of photoelectrons gathered is plotted in relation to momentum. It is deduced from the experiment that the saturation thickness of the aerogel is about 10 cm. Two examples of the practical use of the aerogel counter at KEK are also shortly described. (Aoki, K.)

  3. The determination of boron in high-purity aluminium metal by spark-source mass spectrometry

    International Nuclear Information System (INIS)

    A method is described for the determination of boron in high-purity aluminium metal. Both isotopic boron lines (10B+1 and 11B+1) are used for the analysis. As there are no low-abundance isotopic lines for aluminium, measurements were made direct without reference to aluminium as an internal standard. The boron concentration values of eight aluminium samples analysed by this method compared favourably with results obtained from other techniques

  4. Scintillation counter: photomultiplier tube alignment

    International Nuclear Information System (INIS)

    A scintillation counter, particularly for counting gamma ray photons, includes a massive lead radiation shield surrounding a sample-receiving zone. The shield is disassembleable into a plurality of segments to allow facile installation and removal of a photomultiplier tube assembly, the segments being so constructed as to prevent straight-line access of external radiation through the shield into the sample receiving zone. Provisions are made for accurately aligning the photomultiplier tube with respect to one or more sample-transmitting bores extending through the shield to the sample receiving zone. A sample elevator, used in transporting samples into the zone, is designed to provide a maximum gamma-receiving aspect to maximize the gamma detecting efficiency. (auth)

  5. Scintillation counter, maximum gamma aspect

    International Nuclear Information System (INIS)

    A scintillation counter, particularly for counting gamma ray photons, includes a massive lead radiation shield surrounding a sample-receiving zone. The shield is disassembleable into a plurality of segments to allow facile installation and removal of a photomultiplier tube assembly, the segments being so constructed as to prevent straight-line access of external radiation through the shield into radiation-responsive areas. Provisions are made for accurately aligning the photomultiplier tube with respect to one or more sample-transmitting bores extending through the shield to the sample receiving zone. A sample elevator, used in transporting samples into the zone, is designed to provide a maximum gamma-receiving aspect to maximize the gamma detecting efficiency. (U.S.)

  6. Aerogel threshold Cherenkov counter

    International Nuclear Information System (INIS)

    The results of studying the SiO2 aerogel properties, used as radiator for the Cherenkov counters are presented. Brief data on the technology of preparing the aerogel samples and their optical characteristics are indicated. The formula binding the aerogel refractive index with its density with an account of light dispersion is analyzed. The results of the Cherenkov aerogel threshold counter testing on the charged particles beam within the pulse range of p = ∼ 0.4-2.5 eV/s are presented. The registration efficiency of pions with p ≥ 1 GeV/s constituted ∼ 97% and that of protons - ∼ 4% by the p ≤ 2.5 GeV/s

  7. First boronization in KSTAR

    Energy Technology Data Exchange (ETDEWEB)

    Hong, S.H., E-mail: sukhhong@nfri.re.kr [National Fusion Research Institute, 113 Gwahangno, Yusung-Gu, Daejeon 305-333 (Korea, Republic of); Center for Edge Plasma Science (cEps), Hanyang University, Seoul 133-791 (Korea, Republic of); Lee, K.S.; Kim, K.M.; Kim, H.T.; Kim, G.P. [National Fusion Research Institute, 113 Gwahangno, Yusung-Gu, Daejeon 305-333 (Korea, Republic of); Sun, J.H.; Woo, H.J. [Department of Electrical Engineering, Hanyang University, Seoul 133-791 (Korea, Republic of); Center for Edge Plasma Science (cEps), Hanyang University, Seoul 133-791 (Korea, Republic of); Park, J.M.; Kim, W.C.; Kim, H.K.; Park, K.R.; Yang, H.L.; Na, H.K. [National Fusion Research Institute, 113 Gwahangno, Yusung-Gu, Daejeon 305-333 (Korea, Republic of); Chung, K.S. [Department of Electrical Engineering, Hanyang University, Seoul 133-791 (Korea, Republic of); Center for Edge Plasma Science (cEps), Hanyang University, Seoul 133-791 (Korea, Republic of)

    2010-11-15

    First boronization in KSTAR is reported. KSTAR boronization system is based on a carborane (C{sub 2}B{sub 10}H{sub 12}) injection system. The design, construction, and test of the system are accomplished and it is tested by using a small vacuum vessel before it is mounted to a KSTAR port. After the boronization in KSTAR, impurity levels are significantly reduced by factor of 3 (oxygen) and by 10 (carbon). Characteristics of a-C/B:H thin films deposited by carborane vapor are investigated. Re-condensation of carborane vapor during the test phase has been reported.

  8. Band gap opening and semiconductor-metal phase transition in (n, n) single-walled carbon nanotubes with distinctive boron-nitrogen line defect.

    Science.gov (United States)

    Qiu, Ming; Xie, Yuanyuan; Gao, Xianfeng; Li, Jianyang; Deng, Yelin; Guan, Dongsheng; Ma, Lulu; Yuan, Chris

    2016-02-14

    Band gap opening and modulating are critical in dictating the functionalities of single walled carbon nanotubes (SWCNTs) in a broad array of nano-devices. Using first-principles density functional theory calculations, a class of semiconducting armchair SWCNTs with a distinctive BN line defect are studied, showing a super capacity to open the band gap of (4, 4) SWCNT to as large as 0.86 eV, while the opened band gap are found decreasing with the increasing diameters of SWCNTs. The opened band gap of SWCNTs can also be successfully modulated through both mechanical and electrical approaches by applying compressive uniaxial strain and electric field. This study provides novel insights into the large band gap opening and modulating of SWCNTs and could be useful in facilitating future applications of SWCNTs in electronic, optical and thermoelectric devices. PMID:26794602

  9. Holography without Counter Terms

    CERN Document Server

    Ahn, Byoungjoon; Kim, Kyung Kiu; Park, Sang-A; Yi, Sang-Heon

    2016-01-01

    By using the scaling symmetry in the reduced action formalism, we obtain novel Smarr-like relations for anti-de-Sitter planar black holes, which have useful information in the condensed matter systems through the AdS/CMT correspondence. By using our results, we propose another way to obtain the holographically renormalized on-shell action without counter terms. We find the complete consistency of our results with those in various models discussed in the recent literatures and obtain new implications.

  10. Physical properties of CVD boron-doped multiwalled carbon nanotubes

    Energy Technology Data Exchange (ETDEWEB)

    Mondal, Kartick C. [Molecular Sciences Institute and School of Chemistry, University of the Witwatersrand, P.O. Wits, 2050 Johannesburg (South Africa); DST/NRF Centre of Excellence in Strong Materials, P.O. Wits, 2050 Johannesburg (South Africa); Strydom, Andre M. [Department of Physics, University of Johannesburg, PO Box 524, Auckland Park 2006 (South Africa)], E-mail: amstrydom@uj.ac.za; Erasmus, Rudolph M.; Keartland, Jonathan M. [DST/NRF Centre of Excellence in Strong Materials, P.O. Wits, 2050 Johannesburg (South Africa); School of Physics, University of the Witwatersrand, P.O. Wits, 2050 Johannesburg (South Africa); Coville, Neil J. [Molecular Sciences Institute and School of Chemistry, University of the Witwatersrand, P.O. Wits, 2050 Johannesburg (South Africa); DST/NRF Centre of Excellence in Strong Materials, P.O. Wits, 2050 Johannesburg (South Africa)], E-mail: Neil.Coville@wits.ac.za

    2008-10-15

    The effects of boron doping and electron correlation on the transport properties of CVD boron-doped multiwalled carbon nanotubes are reported. The boron-doped multiwalled carbon nanotubes were characterized by TEM as well as Raman spectroscopy using different laser excitations (viz. 488, 514.5 and 647 nm). The intensity of the D-band laser excitation line increased after the boron incorporation into the carbon nanotubes. The G-band width increased on increasing the boron concentration, indicating the decrease of graphitization with increasing boron concentration. Electrical conductivity of the undoped and boron-doped carbon nanotubes reveal a 3-dimensional variable-range-hopping conductivity over a wide range of temperature, viz. from room temperature down to 2 K. The electrical conductivity is not found to be changed significantly by the present levels of B-doping. Electron Paramagnetic Resonance (EPR) results for the highest B-doped samples showed similarities with previously reported EPR literature measurements, but the low concentration sample gives a very broad ESR resonance line.

  11. Boron in sillimanite.

    Science.gov (United States)

    Grew, E S; Hinthorne, J R

    1983-08-01

    Sillimanite in six granulite-facies, kornerupine-bearing rocks contains 0.035 to 0.43 percent B(2)O(3) and 0.02 to 0.23 percent MgO (by weight). Substitution of boron for silicon and magnesium for aluminum is coupled such that the ratio of magnesium to boron is about 0.5. Sillimanite incorporates more than 0.1 percent B(2)O(3) only at high temperatures in a boron-rich environment at very low partial pressures of water. In the amphibolite facies, the sillimanite boron contents are too low to appreciably affect the stability relations of sillimanite with kyanite and andalusite. PMID:17830955

  12. Spectrographic determination of traces of boron in steels

    International Nuclear Information System (INIS)

    A spectrographic method has been developed to determine quantitatively boron in steels in the 0.5 to 250 ppm concentration range. The samples are dissolved in acids and transformed into oxides, avoiding boron losses by the addition of mannitol. For the fluoride evolution of boron in the dc arc the following compounds have been considered: CuF2, LiF, NaF, and SrF2. CuF2, at a concentration of 10%, provides the highest line-to-background intensity ratio. An arc current of 5 amperes eliminates the interference from iron spectrum on the most sensitive boron line - B 2497.7 A. Variations in chromium and nickel contents have no effect on the analytical results. (author)

  13. Boron nitride composites

    Energy Technology Data Exchange (ETDEWEB)

    Kuntz, Joshua D.; Ellsworth, German F.; Swenson, Fritz J.; Allen, Patrick G.

    2016-02-16

    According to one embodiment, a composite product includes hexagonal boron nitride (hBN), and a plurality of cubic boron nitride (cBN) particles, wherein the plurality of cBN particles are dispersed in a matrix of the hBN. According to another embodiment, a composite product includes a plurality of cBN particles, and one or more borate-containing binders.

  14. Fabrication of solar cells with counter doping prevention

    Science.gov (United States)

    Dennis, Timothy D; Li, Bo; Cousins, Peter John

    2013-02-19

    A solar cell fabrication process includes printing of dopant sources over a polysilicon layer over backside of a solar cell substrate. The dopant sources are cured to diffuse dopants from the dopant sources into the polysilicon layer to form diffusion regions, and to crosslink the dopant sources to make them resistant to a subsequently performed texturing process. To prevent counter doping, dopants from one of the dopant sources are prevented from outgassing and diffusing into the other dopant source. For example, phosphorus from an N-type dopant source is prevented from diffusing to a P-type dopant source comprising boron.

  15. Electromagnetic shower counter

    CERN Multimedia

    1974-01-01

    The octogonal block of lead glass is observed by eight photomultiplier tubes. Four or five such counters, arranged in succession, are used on each arm of the bispectrometer in order to detect heavy particles of the same family as those recently observed at Brookhaven and SLAC. They provide a means of identifying electrons. The arrangement of eight lateral photomultiplier tubes offers an efficient means of collecting the photons produced in the showers and determining, with a high resolution, the energy of the incident electrons. The total width at half-height is less than 6.9% for electrons having an energy of 1 GeV.

  16. Microdosimetry study of THOR BNCT beam using tissue equivalent proportional counter

    International Nuclear Information System (INIS)

    Boron neutron capture therapy (BNCT) is a cancer treatment modality using a nuclear reactor and a boron compound drug. In Taiwan, Tsing Hua open-pool reactor (THOR) has been modulated for the basic research of BNCT for years. A new BNCT beam port was built in 2004 and used to prepare the first clinical trial in the near future. This work reports the microdosimetry study of the THOR BNCT beam by means of the tissue equivalent proportional counter (TEPC). Two self-fabricated TEPCs (the boron-doped versus the boron-free counter wall) were introduced. These dual TEPCs were applied to measure the lineal energy distributions in air and water phantom irradiated by the THOR BNCT mixed radiation field. Dose contributions from component radiations of different linear energy transfers (LETs) were analyzed. Applying a lineal energy dependent biological weighting function, r(y), to the total and individual lineal energy distributions, the effective relative biological effectiveness (RBE), neutron RBE, photon RBE, and boron capture RBE (BNC RBE) were all determined at various depths of the water phantom. Minimum and maximum values of the effective RBE were 1.68 and 2.93, respectively. The maximum effective RBE occurred at 2 cm depth in the phantom. The average neutron RBE, photon RBE, and BNC RBE values were 3.160±0.020, 1.018±0.001, and 1.570±0.270, respectively, for the THOR BNCT beam.

  17. 13C NMR spectroscopy of amorphous hydrogenated carbon and amorphous hydrogenated boron carbide

    International Nuclear Information System (INIS)

    We report the 13C NMR spectrum of amorphous hydrogenated carbon and boron carbide. The amorphous hydrogenated carbon spectra consist primarily of an sp3 line at 40 ppm and an sp2 line at 140 ppm and are in reasonable agreement with the recent theoretical calculations of Mauri, Pfrommer, and Louie, but there are some notable discrepancies. The amorphous hydrogenated boron carbide spectra are very different from those of amorphous hydrogenated carbon, being dominated by one line at 15 ppm. We interpret this line as due to carbon bound in boron carbide icosahedra, because polycrystalline boron carbide with boron carbide icosahedra as the unit cell gives very similar NMR spectra. copyright 1999 The American Physical Society

  18. A track ion counter

    International Nuclear Information System (INIS)

    A method to measure the frequency of production of ions in a gas is described. The characteristics of a device, which is named a track ion counter, are presented. The counter consists of two cylindrical volumes separated by a diaphragm with 500μm dia. orifice. The device is connected to an oil diffusion pump with high pumping speed. The gas flow through the orifice determines the pressure in the upper and the lower volumes of the device. The positive ions produced in a cylindrical volume above an orifice by charged particles traversing that volume move in a constant electric field. Some of these ions passing through the orifice are accelerated and detected by an electron multiplier. The absolute efficiency of ions detection from the domain above the orifice have been determined. The measurements were carried out for single charged ions of N2, H2, CH4, CO2. The preliminary measurements of the frequency of ions created within cylindrical gas domain equivalent to 0.15nm dia. and 7.6nm height tissue cylinder are reported

  19. Position sensitive multiwire proportional counter for the crystal X-spectrometer of Tore Supra tokamak

    International Nuclear Information System (INIS)

    A position sensitive proportional counter, for use in the Tore Supra X-spectrometer, is developed. The physics of X-photons detection, in those counters, are reviewed. The detector's design and construction are presented. Its surface of detection is five times larger than that of the previous counter (40 cm2 times 8 cm2). The counter's spatial resolution is measured, in order to verify whether or not the spectrometer performance is modified. The dead time influence is studied and correction procedures are obtained. An optical transmission line, between the counter and the electronics of the data acquisition system, is considered for use in gamma radiation or fusion neutron environments

  20. Boronated liposome development and evaluation

    Energy Technology Data Exchange (ETDEWEB)

    Hawthorne, M.F. [Univ. of California, Los Angeles, CA (United States)

    1995-11-01

    The boronated liposome development and evaluation effort consists of two separate tasks. The first is the development of new boron compounds and the synthesis of known boron species with BNCT potential. These compounds are then encapsulated within liposomes for the second task, biodistribution testing in tumor-bearing mice, which examines the potential for the liposomes and their contents to concentrate boron in cancerous tissues.

  1. Magnetron sputter deposition of boron and boron carbide

    International Nuclear Information System (INIS)

    The fabrication of X-ray optical coatings with greater reflectivity required the development of sputter deposition processes for boron and boron carbide. The use of high density boron and boron carbide (B4C) and a vacuum-brazed target design was required to achieve the required sputter process stability and resistance to the thermal stress created by high rate sputtering. Our results include a description of the target fabrication procedures and sputter process parameters necessary to fabricate B4C and boron modulated thin film structures. (orig.)

  2. Space and power efficient hybrid counters array

    Science.gov (United States)

    Gara, Alan G.; Salapura, Valentina

    2010-03-30

    A hybrid counter array device for counting events. The hybrid counter array includes a first counter portion comprising N counter devices, each counter device for receiving signals representing occurrences of events from an event source and providing a first count value corresponding to a lower order bits of the hybrid counter array. The hybrid counter array includes a second counter portion comprising a memory array device having N addressable memory locations in correspondence with the N counter devices, each addressable memory location for storing a second count value representing higher order bits of the hybrid counter array. A control device monitors each of the N counter devices of the first counter portion and initiates updating a value of a corresponding second count value stored at the corresponding addressable memory location in the second counter portion. Thus, a combination of the first and second count values provide an instantaneous measure of number of events received.

  3. Space and power efficient hybrid counters array

    Science.gov (United States)

    Gara, Alan G.; Salapura, Valentina

    2009-05-12

    A hybrid counter array device for counting events. The hybrid counter array includes a first counter portion comprising N counter devices, each counter device for receiving signals representing occurrences of events from an event source and providing a first count value corresponding to a lower order bits of the hybrid counter array. The hybrid counter array includes a second counter portion comprising a memory array device having N addressable memory locations in correspondence with the N counter devices, each addressable memory location for storing a second count value representing higher order bits of the hybrid counter array. A control device monitors each of the N counter devices of the first counter portion and initiates updating a value of a corresponding second count value stored at the corresponding addressable memory location in the second counter portion. Thus, a combination of the first and second count values provide an instantaneous measure of number of events received.

  4. Counter-Learning under Oppression

    Science.gov (United States)

    Kucukaydin, Ilhan

    2010-01-01

    This qualitative study utilized the method of narrative analysis to explore the counter-learning process of an oppressed Kurdish woman from Turkey. Critical constructivism was utilized to analyze counter-learning; Frankfurt School-based Marcusian critical theory was used to analyze the sociopolitical context and its impact on the oppressed. Key…

  5. A plastic scintillation counter prototype

    International Nuclear Information System (INIS)

    A new prototype device for beta-ray measurement, a plastic scintillation counter, was assembled as an alternative device to liquid scintillation counters. This device uses plastic scintillation sheets (PS sheets) as a sample applicator without the use of a liquid scintillator. The performance was evaluated using tritium labeled compounds, and good linearity was observed between the activity and net count rate. The calculated detection limit of the device was 0.01 Bq mL−1 after 10 h measurement for 2 mL sample. - Highlights: • A new device of plastic scintillation counter was developed to measure beta emitters. • High sensitivity with low detection limit was performed for a tritium compound. • A detection limit of tritium was 0.01 Bq mL−1 for a 10 h measurement. • A plastic scintillation counter generated no radioactive organic waste fluid. • A plastic scintillation counter could analyze qualitatively and quantitatively

  6. Lattice dynamics of {alpha} boron and of boron carbide; Proprietes vibrationnelles du bore {alpha} et du carbure de bore

    Energy Technology Data Exchange (ETDEWEB)

    Vast, N

    1999-07-01

    The atomic structure and the lattice dynamics of {alpha} boron and of B{sub 4}C boron carbide have been studied by Density Functional Theory (D.F.T.) and Density Functional Perturbation Theory (D.F.P.T.). The bulk moduli of the unit-cell and of the icosahedron have been investigated, and the equation of state at zero temperature has been determined. In {alpha} boron, Raman diffusion and infrared absorption have been studied under pressure, and the theoretical and experimental Grueneisen coefficients have been compared. In boron carbide, inspection of the theoretical and experimental vibrational spectra has led to the determination of the atomic structure of B{sub 4}C. Finally, the effects of isotopic disorder have been modeled by an exact method beyond the mean-field approximation, and the effects onto the Raman lines has been investigated. The method has been applied to isotopic alloys of diamond and germanium. (author)

  7. Microdosimetry for Boron Neutron Capture Therapy

    International Nuclear Information System (INIS)

    The specific aims of the research proposal were as follows: (1) To design and construct small volume tissue equivalent proportional counters for the dosimetry and microdosimetry of high intensity thermal and epithermal neutron beams used in BNCT, and of modified fast neutron beams designed for boron neutron capture enhanced fast neutron therapy (BNCEFNT). (2) To develop analytical methods for estimating the biological effectiveness of the absorbed dose in BNCT and BNCEFNT based on the measured microdosimetric spectra. (3) To develop an analytical framework for comparing the biological effectiveness of different epithermal neutron beams used in BNCT and BNCEFNT, based on correlated sets of measured microdosimetric spectra and radiobiological data. Specific aims (1) and (2) were achieved in their entirety and are comprehensively documented in Jay Burmeister's Ph.D. dissertation entitled ''Specification of physical and biologically effective absorbed dose in radiation therapies utilizing the boron neutron capture reaction'' (Wayne State University, 1999). Specific aim (3) proved difficult to accomplish because of a lack of sufficient radiobiological data

  8. Boron cures cancer

    International Nuclear Information System (INIS)

    In this work the authors cite a few examples of the use of radiopharmaceuticals for diagnostic and therapeutic purposes in nuclear medicine. They point to the possibility of boron neutron capture therapy and the use for the neutron capture therapy of other light elements.

  9. Boron contamination in drinking - irrigation water and boron removal methods

    Directory of Open Access Journals (Sweden)

    Meltem Bilici Başkan

    2014-03-01

    Full Text Available Boron presents in IIIA group of periodic table and has high ionization capacity. Therefore it is classified as a metalloid. Average boron concentration in earth's crust is 10 mg/kg. It presents in the environment as a salts of Ca, Na, and Mg. Boron reserves having high concentration and economical extent are found mostly in Turkey and in arid, volcanic and high hydrothermal activity regions of U.S. as compounds of boron attached to oxygen. Boron is an essential micronutrient for plants, although it may be toxic at higher levels. The range in which it is converted from a nutrient to a contaminant is quite narrow. Boron presents in water environment as a boric acid and rarely borate salts. The main boron sources, whose presence is detected in surface waters, are urban wastes and industrial wastes, which can come from a wide range of different activities as well as several chemical products used in agriculture. In Turkey, the most pollutant toxic element in drinking and irrigation water is boron. Therefore boron removal is very important in terms of human health and agricultural products in high quality. Mainly boron removal methods from drinking water and irrigation water are ion exchange, ultrafiltration, reverse osmosis, and adsorption.

  10. BCM6: New Generation of Boron Meter

    International Nuclear Information System (INIS)

    Full text of publication follows: Rolls-Royce has developed a new generation of boron meter, based on more than 30 years of experience. The Rolls-Royce BCM6 boron meter provides Nuclear Power Plant (NPP) operators with the boron concentration of the primary circuit. The meter provides continuous and safe measurements with no manual sampling and no human contact. In this paper, technical features, advantages and customer benefits of the use of the new generation of Rolls-Royce BCM6 boron meter will be detailed. Values and associated alarms are provides over different media: 4-20 mA outputs, relays, displays in the main control room and in the chemical lab, and digital links. A special alarm avoids unexpected homogeneous dilution of the primary circuit, which is a critical operational parameter. The Rolls-Royce BCM6 boron meter is fully configurable over a set of parameters allowing adaptation to customer needs. It has a differential capability, thus eliminating neutronic noise and keeping measurements accurate, even in the case of fuel clad rupture. Measurements are accurate, reliable, and have a quick response time. Equipment meets state-of-the-art qualification requests. Designed in 2008, the BCM6 boron meter is the newest equipment of Rolls-Royce boron meters product line. It has been chosen to equip the French EPR NPP and complies with the state-of-the-art of the technology. Rolls-Royce has more than 30 years of experience in Instrumentation and Controls with more than 75 NPP units operating worldwide. All of this experience return has been put in this new generation of equipment to provide the customer with the best operation. About Rolls-Royce Rolls-Royce is a global business providing integrated power systems for use on land, at sea and in the air. The Group has a balanced business portfolio with leading market positions. Rolls-Royce has a broad range of civil nuclear expertise, including work related to licensing and safety reviews, engineering design

  11. Process for microwave sintering boron carbide

    International Nuclear Information System (INIS)

    A method of microwave sintering boron carbide comprises leaching boron carbide powder with an aqueous solution of nitric acid to form a leached boron carbide powder. The leached boron carbide powder is coated with a glassy carbon precursor to form a coated boron carbide powder. The coated boron carbide powder is consolidated in an enclosure of boron nitride particles coated with a layer of glassy carbon within a container for microwave heating to form an enclosed coated boron carbide powder. The enclosed coated boron carbide powder is sintered within the container for microwave heating with microwave energy

  12. Oscillatory counter-centrifugation

    Science.gov (United States)

    Xu, Shujing; Nadim, Ali

    2016-02-01

    In ordinary centrifugation, a suspended particle that is heavier than the displaced fluid migrates away from the rotation axis when the fluid-filled container rotates steadily about that axis. In contrast a particle that is lighter than the displaced fluid (e.g., a bubble) migrates toward the rotation axis in a centrifuge. In this paper, we show theoretically that if a fluid-filled container rotates in an oscillatory manner as a rigid body about an axis, at high enough oscillation frequencies, the sense of migration of suspended particles is reversed. That is, in that case particles denser than the fluid migrate inward, while those that are lighter than the fluid move outward. We term this unusual phenomenon "Oscillatory Counter-Centrifugation" or OCC, for short. Through application of the method of averaging to the equations of motion, we derive a simple criterion to predict the occurrence of OCC. The analysis also reveals that the time-average of the Coriolis force in the radial direction is the term that is responsible for this effect. In addition, we analyze the effects of the Basset history force and the Rubinow-Keller lift force on particle trajectories and find that OCC persists even when these forces are active. The phenomenon awaits experimental verification.

  13. Methods of producing continuous boron carbide fibers

    Energy Technology Data Exchange (ETDEWEB)

    Garnier, John E.; Griffith, George W.

    2015-12-01

    Methods of producing continuous boron carbide fibers. The method comprises reacting a continuous carbon fiber material and a boron oxide gas within a temperature range of from approximately 1400.degree. C. to approximately 2200.degree. C. Continuous boron carbide fibers, continuous fibers comprising boron carbide, and articles including at least a boron carbide coating are also disclosed.

  14. Over-the-Counter Medicines

    Science.gov (United States)

    Over-the-counter (OTC) medicines are drugs you can buy without a prescription. Some OTC medicines relieve aches, pains ... Others help manage recurring problems, like migraines. In the United States, the Food and Drug Administration decides ...

  15. Preliminary results of a new boron coated neutron detector

    Energy Technology Data Exchange (ETDEWEB)

    Gervino, G., E-mail: gervino@to.infn.it [Dipartimento di Fisica Università di Torino (Italy); INFN Torino (Italy); Balma, M.; Devona, D. [SELEX Galileo, San Maurizio Canavese, TO (Italy); Lavagno, A. [Dipartimento di Fisica Politecnico di Torino (Italy); INFN Torino (Italy); Palmisano, C. [Dipartimento di Fisica Università di Torino (Italy); Zamprotta, L. [Dipartimento di Fisica Università di Torino (Italy); INFN Torino (Italy); Scarfone, A. [ISC-CNR Torino (Italy); INFN Torino (Italy); Tintori, C. [C.A.E.N. S.p.A., Viareggio, LU (Italy)

    2013-08-01

    The proliferation of neutron detection applications based upon {sup 3}He counter has triggered a critical shortage of {sup 3}He gas. Nowadays there is an increasing demand for alternative neutron detectors that can cover large solid angles, have low sensitivity to gamma background and low cost. We present a low cost neutron detector based upon 3 cm diameter, 150 cm long cylindrical metal tube coated on the inside with a thin layer of {sup 10}B-enriched boron carbide ({sup 10}B{sub 4}C) fulfilled by 1 atm nitrogen.

  16. Sintered boron, production and properties

    International Nuclear Information System (INIS)

    Microhardness HV, tensile properties and Young modulus of sintered boron of different porosity were studied. It was shown that with density growth tensile properties improve. HV and brittle-ductile transition temperature Tsub(b) of sintered boron on the one hand and for silicon and titanium carbide on the other were compared and discussed. It was noted that the general level of HV and Tsub(b) for boron is rather high and at similar relative temperatures these characteristics are much higher. Temperature dependences of linear expansion coefficient, thermal capacity, thermal and temperature conductivity of sintered boron of 20% porosity were studied. Gruneisen parameter was evaluated

  17. Fivefold twinned boron carbide nanowires.

    Science.gov (United States)

    Fu, Xin; Jiang, Jun; Liu, Chao; Yuan, Jun

    2009-09-01

    Chemical composition and crystal structure of fivefold twinned boron carbide nanowires have been determined by electron energy-loss spectroscopy and electron diffraction. The fivefold cyclic twinning relationship is confirmed by systematic axial rotation electron diffraction. Detailed chemical analysis reveals a carbon-rich boron carbide phase. Such boron carbide nanowires are potentially interesting because of their intrinsic hardness and high temperature thermoelectric property. Together with other boron-rich compounds, they may form a set of multiply twinned nanowire systems where the misfit strain could be continuously tuned to influence their mechanical properties. PMID:19687534

  18. A 10B-based neutron detector with stacked Multiwire Proportional Counters and macrostructured cathodes

    CERN Document Server

    Stefanescu, I; Birch, J; Defendi, I; Hall-Wilton, R; Hoglund, C; Hultman, L; Zee, M; Zeitelhack, K

    2013-01-01

    We present the results of the measurements of the detection efficiency for a 4.7 \\r{A} neutron beam incident upon a detector incorporating a stack of up to five MultiWire Proportional Counters (MWPC) with Boron-coated cathodes. The cathodes were made of Aluminum and had a surface exhibiting millimeter-deep V-shaped grooves of 45{\\deg}, upon which the thin Boron film was deposited by DC magnetron sputtering. The incident neutrons interacting with the converter layer deposited on the sidewalls of the grooves have a higher capture probability, owing to the larger effective absorption film thickness. This leads to a higher overall detection efficiency for the grooved cathode when compared to a cathode with a flat surface. Both the experimental results and the predictions of the GEANT4 model suggests that a 5-counter detector stack with coated grooved cathodes has the same efficiency as a 7-counter stack with flat cathodes. The reduction in the number of counters in the stack without altering the detection efficie...

  19. Counter-ions at Charged Walls: Two Dimensional Systems

    OpenAIRE

    Samaj, L.; Trizac, E.

    2010-01-01

    We study equilibrium statistical mechanics of classical point counter-ions, formulated on 2D Euclidean space with logarithmic Coulomb interactions (infinite number of particles) or on the cylinder surface (finite particle numbers), in the vicinity of a single uniformly charged line (one single double-layer), or between two such lines (interacting double-layers). The weak-coupling Poisson-Boltzmann theory, which applies when the coupling constant Gamma is small, is briefly recapitulated (the c...

  20. Room-Temperature Near-Infrared Electroluminescence from Boron-Diffused Silicon Pn-Junction Diodes

    OpenAIRE

    Li, Si; Gao, Yuhan; Fan, Ruixin; Li, Dongsheng; Yang, Deren

    2015-01-01

    Silicon pn-junction diodes with different doping concentrations were prepared by boron diffusion into Czochralski n-type silicon substrate. Their room-temperature near-infrared electroluminescence (EL) was measured. In the EL spectra of the heavily boron doped diode, a luminescence peak at ~1.6 μm (0.78 eV) was observed besides the band-to-band line (~1.1 eV) under the condition of high current injection, while in that of the lightly boron doped diode only the band-to-band line was observed. ...

  1. Room-temperature near-infrared electroluminescence from boron-diffused silicon pn junction diodes

    OpenAIRE

    Si eLi; Yuhan eGao; Ruixin eFan; Dongsheng eLi; Deren eYang

    2015-01-01

    Silicon pn junction diodes with different doping concentrations were prepared by boron diffusion into Czochralski (CZ) n-type silicon substrate. Their room-temperature near-infrared electroluminescence (EL) was measured. In the EL spectra of the heavily boron doped diode, a luminescence peak at ~1.6 m (0.78 eV ) was observed besides the band-to-band line (~1.1eV) under the condition of high current injection, while in that of the lightly boron doped diode only the band-to-band line was obser...

  2. Space-charge effects of the proportional counters in a multiple-ionization chamber

    International Nuclear Information System (INIS)

    At the ALADIN spectrometer of the GSI in october 1991 for the first time the new multiple ionization chamber was applied, in the two anode planes of which are additional multiwire-proportional counters. The proportional counters are required in order to make the detection of light fragments (Z4 gold projectiles per second by these positive space charges the homogeneous electric field of the MUSIC is disturbed. This effect is especially strong in the beam plane. As consequence of the space charge additionally electrons are focused on the proportional counter so that their amplitudes in dependence on the beam intensity increase up to the 2.5-fold. Furthermore the y coordinate is falsified, because the electrons are diverted to the medium plane. On the measurement of the x coordinate this diversion has with maximally 0.1% only a small influence. These space-charge effects can be qualitatively described by a schematic model, which assumes a stationary positive space charge. Additionally for the proportional counters, which are not in the beam plane, their resolution was determined. In these counters the space-charge effects are small, because essentially fewer particles are registrated than in the medium MWPC's. By this charges of fragments with Z<10 could be separated. The charge resolution amounted at lithium 0.8 charge units. The position resolution of the proportional counters in y direction was determined to less than 8 mm. The detection probability of the fragments amounts for lithium 90% and from boron all fragments are detected

  3. A proportional counter with reduced wall effect

    International Nuclear Information System (INIS)

    A proportional counter, using gaseous sources, in which the wall effects are considerably reduced, is described. The counter is fitted with a ring of internal shielding counters in anti-coincidence, separated from the main central counter only by a number of cathode wires. The counter can be readily assembled, giving flexibility in research investigations. Applications to a measurement of the L/K capture ratio in A37 and Fe55 are described. (author)

  4. Novel Components for Neutron Counters

    International Nuclear Information System (INIS)

    Neutron counters for safeguards proposes have been developed during the last thirty years at the Joint Research Centre. The paper describes some of the latest developments and implementations in modern neutron counter. The design of a neutron counter is nowadays largely done by MCNP calculations. We have studied the behaviour of some components for a specific counter with respect to optimising the performance of the counter. This includes the moderator materials, thermal neutron absorbers, and 3-He detectors. Also the electronics for neutron counter has evolved over the years. Modern neutron counters require a large number of detectors and signal amplifiers to provide optimised parameters for the data interpretation. For this purpose we have developed a new pre-amplifier/amplifier/discriminator circuit which is both compact and inexpensive. The new circuit will be used in existing and future neutron counters. Concerning the treatment of the digital signal pulse train we intend to makes use of the latest advances in computer technology. A novel electronic system has been developed with a maximum of 128 input channels, which can cope with the high count rate of more than 1 million counts per second with zero dead-time. The Multi Input-Pulse Train Analysis (MI-PTA) system can be used with standard instruments, like Shift Register Analysers. However, it has been designed to perform a variety of pulse train analysis techniques itself, or in combination with a Personal Computer to which the system is connected via a High Speed USB2.0 connection. Pulse data can exchanged between the MI-PTA and PC at the rate of 480 Mb/s, allowing real time analysis on a PC and providing the basis for a Virtual Instrument approach: by modifying the software new instruments can be configured. The system consists of a number of base units, each with 8 TTL compatible inputs. Only one unit, configured as a Master, is connected to a PC. Up-to 15 Slave units can be connected to the Master via a

  5. Explosion-proof scintillation counter

    International Nuclear Information System (INIS)

    It is noted that measuring devices used in the research works conducted with the help of radioactive isotopes on the chemical industry installations dangerous from the point of view of explosions, especially on the installations of the petrochemistry industry, must not limit the exploitation safety of these installations. The said especially concerns with the Geiger-Mueller type counters and scintillation detectors, located immediately in the places of measurements on the installations and supplied by high voltage power supply. It has been shown that electronic circuits for the detector's signals processing and obtaining working voltages can be located out of the explosive dangerous premices, for example, in the car trailer. Description is given of the device, with the help of which explosion safety is provided for the serially produced scintillation counter with forced ventilation (counter of the VA-S-50 type). Due to this device application, the exploitation parameters of the counter do not go down and there is no need for any changes in its design. Description is given of the device for external power supply and control of the counter which can swich off the power supply in the case of an accident, dangerous from the point of view of violation of the explosion safety conditions. The device is described for providing service to 10 measuring chanels, mounted on the car trailer

  6. TOP counter for particle identification at the Belle II experiment

    Science.gov (United States)

    Inami, Kenji

    2014-12-01

    Ring imaging Cherenkov counter, named TOP counter, utilizing precise photon detection timing has been developed as a particle identification detector for the Belle II experiment. The real size prototype has been produced and tested with 2 GeV positrons at Spring-8 LEPS beam line. The quartz radiator production and assembling with microchannel plate photomultipliers was successfully carried out. The beam test data shows good agreement with full Monte-Carlo simulation results in the ring image and the distribution of number of detected photons and timing information.

  7. Boron thermal regeneration system

    International Nuclear Information System (INIS)

    An ion exchanger which allows flow in both directions along a selected flow path is described. A separator plate divides the exchanger tank into two chambers each of which has a flow conduit so that flow may enter or leave from either chamber while prohibiting the resin particles from migrating from one side of the tank to the other. This ion exchanger permits a dual-directional flow process to be practised which results in immediate changes in the boron concentration within a nuclear reactor coolant system even if the ion exchanger resins have not been completely equilibrated during a previous operation. (author)

  8. BORONIZING OF STEEL

    Directory of Open Access Journals (Sweden)

    Arzum ULUKÖY

    2006-02-01

    Full Text Available Boride layer has many advantages in comparison with traditional hardening methods. The boride layer has high hardening value and keeps it's hardeness at high temperatures, and it also shows favorible properties, such as the resistance to wear, oxidation and corrosion. The process can be applied at variety of materials, for instance steel, cast iron, cast steel, nickel and cobalt alloys and cermets. In this rewiew, boronizing process properties, boride layer on steel surfaces and specifications and the factors that effect boride layer are examined

  9. Control stand of scintillation counters

    International Nuclear Information System (INIS)

    Paper describes a stand designed to test complex optical elements of the CMS endwindow hadron calorimeter. The optical element (the megatile) represents an assembly where 19 trapezoidal scintillators are sandwiched in light-absorbing and light-reflecting layers. The stand to test the quality of scintillation counters consists of a bench with a carriage double-coordinated actuation mechanism, a group of photodetectors, a high-voltage power unit, a laser control checking system, a PC and a scintillation counter to calibrate photodetectors. One studies in detail the procedure to test megatiles in the course of which minimum 100 trigger statistics is ensured for every megatile

  10. The assembly of the Belle II TOP counter

    International Nuclear Information System (INIS)

    A new type of ring-imaging Cherenkov counter, called TOP counter, has been developed for particle identification at the Belle II experiment to run at the SuperKEKB accelerator in KEK, Japan. The detector consists of 16 identical modules arranged azimuthally around the beam line. The assembly procedure for a TOP module is described. This procedure includes acceptance testing of the quartz mirror, prism, and quartz bar radiators. The acceptance tests include a chip search and measurements of bulk transmittance and total internal reflectance. The process for aligning and gluing the optical components together is described. - Highlights: • The fabrication process of the TOP counter has been established. • We did the acceptance tests for the first few optical components. • The qualities of the optical components satisfy our requirements. • The tests of the gluing procedure have been taking place

  11. PGNAA of human arthritic synovium for boron neutron capture synovectomy

    Energy Technology Data Exchange (ETDEWEB)

    Binello, E.; Yanch, J.C. [Massashucetts Institute of Technology, Cambridge, MA (United States); Shortkroff, S. [Brigham and Women`s Hospital, Boston, MA (United States)

    1997-12-01

    Boron neutron capture synovectomy (BNCS), is a proposed new therapy modality for the treatment of rheumatoid arthritis, an autoimmune disease afflicting the joints. The synovium, which is the membrane lining the joint, becomes inflamed and represents the target tissue for therapy. When a joint is unresponsive to drug treatment, physical removal of the synovium, termed synovectomy, becomes necessary. Existing options include surgery and radiation synovectomy. BNCS has advantages over these options in that it is noninvasive and does not require the administration of radioactive substances. Previous studies have shown that the uptake of {sup 10}B by human arthritic synovium ex vivo is high, ranging from 194 to 545 ppm with an unenriched boron compound. While tissue samples remain viable up to 1 week, ex vivo conditions do not accurately reflect those in vivo. This paper presents results from experiments assessing the washout of boron from the tissue and examines the implications for in vivo studies.

  12. Design and performance study of the TOP counter

    International Nuclear Information System (INIS)

    A novel RICH detector called TOP counter has been developed for particle identification in Belle II. It measures the time of propagation (TOP) of Cherenkov photons traveling in the quartz radiator with micro-channel-plate photomultiplier tubes (MCP-PMTs) with a precision of 50 ps. A prototype TOP counter was tested with the 1.2 GeV/c electron beam in the Laser Electron Photon beam line at SPring-8 (LEPS). The TOP distribution was obtained as expected after taking into account the dependence of the MCP-PMT quantum efficiency on light incidence angle and polarization. In this paper, the key features of the TOP counter design and the beam test results are presented. -- Highlights: •The TOP counter has been developed for particle identification in Belle II. •A time of propagation (TOP) of Cherenkov light in the quartz radiator is measured. •Cherenkov light is detected by the MCP-PMTs with a resolution of about 40 ps. •A prototype TOP counter was tested with the 1.2 GeV/c electron beam at LEPS. •The TOP distribution measured in the beam test agrees with the expectation

  13. The Micro Trench Gas Counter

    International Nuclear Information System (INIS)

    A novel design is presented for a gas avalanche chamber with micro-strip gas readout. While existing gaseous microstrip detectors (Micro-strip Gas Counters, Knife edge chambers) have a minimum anode pitch of the order of 100 μm, the pitch of the discussed Micro Trench Gas Counter goes down to 30-50 μm. This leads to a better position resolution and two track separation, and a higher radiation resistivity. Its efficiency and signal speed are expected to be the same as the Microstrip Gas Counter. The energy resolution of the device is expected to be equal to or better than 10 percent for the 55Fe peak. Since the anode strip dimensions are larger than those in a MSGC, the device may be not as sensitive to discharges and mechanical damage. In this report production of the device is briefly described, and predictions on its operation are made based on electric field calculations and experience with the Microstrip Gas Counter. The authors restrict themselves to the application in High Energy Physics. (author). 10 refs.; 9 figs

  14. Counter-Rotating Accretion Discs

    CERN Document Server

    Dyda, Sergei; Ustyugova, Galina V; Romanova, Marina M; Koldoba, Alexander V

    2014-01-01

    Counter-rotating discs can arise from the accretion of a counter-rotating gas cloud onto the surface of an existing co-rotating disc or from the counter-rotating gas moving radially inward to the outer edge of an existing disc. At the interface, the two components mix to produce gas or plasma with zero net angular momentum which tends to free-fall towards the disc center. We discuss high-resolution axisymmetric hydrodynamic simulations of a viscous counter-rotating disc for cases where the two components are vertically separated and radially separated. The viscosity is described by an isotropic $\\alpha-$viscosity including all terms in the viscous stress tensor. For the vertically separated components a shear layer forms between them. The middle of this layer free-falls to the disk center. The accretion rates are increased by factors $\\sim 10^2-10^4$ over that of a conventional disc rotating in one direction with the same viscosity. The vertical width of the shear layer and the accretion rate are strongly dep...

  15. Dietary boron, brain function, and cognitive performance.

    OpenAIRE

    Penland, J G

    1994-01-01

    Although the trace element boron has yet to be recognized as an essential nutrient for humans, recent data from animal and human studies suggest that boron may be important for mineral metabolism and membrane function. To investigate further the functional role of boron, brain electrophysiology and cognitive performance were assessed in response to dietary manipulation of boron (approximately 0.25 versus approximately 3.25 mg boron/2000 kcal/day) in three studies with healthy older men and wo...

  16. Cosmis Lithium-Beryllium-Boron Story

    Science.gov (United States)

    Vangioni-Flam, E.; Cassé, M.

    Light element nucleosynthesis is an important chapter of nuclear astrophysics. Specifically, the rare and fragile light nuclei Lithium, Beryllium and Boron (LiBeB) are not generated in the normal course of stellar nucleosynthesis (except Lithium-7) and are, in fact, destroyed in stellar interiors. This characteristic is reflected in the low abundance of these simple species. Up to recently, the most plausible interpretation was that galactic cosmic rays (GCR) interact with interstellar CNO to form LiBeB. Other origins have been also identified, primordial and stellar (Lithium-7) and supernova neutrino spallation (Lithium-7 and Boron-11). In contrast, Beryllium-9, Boron-10 and Lithium-6 are pure spallative products. This last isotope presents a special interest since the Lithium-7/Lithium-6 ratio has been measured in a few halo stars offering a new constraint on the early galactic evolution. However, in the nineties, new observations prompted astrophysicists to reassess the question. Optical measurements of the beryllium and boron abundances in halo stars have been achieved by the 10 meters KECK telescope and the Hubble Space Telescope. These observations indicate a quasi linear correlation between Be and B vs Fe, at least at low metallicity, unexpected on the basis of GCR scenario, predicting a quadratic relationship. As a consequence, the origin and the evolution of the LiBeB nuclei has been revisited. This linearity implies the acceleration of C and O nuclei freshly synthesized and their fragmentation on the the interstellar Hydrogen and Helium. Wolf-Rayet stars and supernovae via the shock waves induced, are the best candidates to the acceleration of their own material enriched into C and O; so LiBeB is produced independently of the Interstellar Medium chemical composition. Moreover, neutrinos emitted by the newly born neutron stars interacting with the C layer of the supernova could produce specifically Lithium-7 and Boron-11. This process is supported by the

  17. Banishing brittle bones with boron

    Energy Technology Data Exchange (ETDEWEB)

    A 6-month study indicates that boron, not even considered an essential nutrient for people and animals, may be a key to preventing osteoporosis, say nutritionist Forrest H. Nielsen and anatomist Curtiss D. Hunt at ARS' Grand Forks, North Dakota, Human Nutrition Research Center. They believe the results of the study - the first to look at the nutritional effects of boron in humans - will generate a lot of interest in the element. In the study, 12 postmenopausal women consumed a very low boron diet (0.25 milligrams per day) for 17 weeks then were given a daily 3-mg supplement - representing the boron intake from a well-balanced diet - for 7 more weeks. Within 8 days after the supplement was introduced, the lost 40 percent less calcium, one-third less magnesium, and slightly less phosphorus through the urine. In fact, their calcium and magnesium losses were lower than prestudy levels, when they were on their normal diets. Since boron isn't considered essential for people, there is not recommended intake and no boron supplement on the market. Nielsen says the supplement of sodium borate used in the study was specially prepared based on the amount of boron a person would get from a well-balanced diet containing fruits and vegetables. He says the average boron intake is about 1.5 mg - or half the experimental dose - but average means a lot of people get less and a lot get more. Hunt cautioned that large doses of boron can be toxic, even lethal. The lowest reported lethal dose of boric acid is about 45 grams (1.6 ounces) for an adult and only 2 grams (0.07 ounce) for an infant.

  18. Basic Research Needs for Countering Terrorism

    Energy Technology Data Exchange (ETDEWEB)

    Stevens, W.; Michalske, T.; Trewhella, J.; Makowski, L.; Swanson, B.; Colson, S.; Hazen, T.; Roberto, F.; Franz, D.; Resnick, G.; Jacobson, S.; Valdez, J.; Gourley, P.; Tadros, M.; Sigman, M.; Sailor, M.; Ramsey, M.; Smith, B.; Shea, K.; Hrbek, J.; Rodacy, P.; Tevault, D.; Edelstein, N.; Beitz, J.; Burns, C.; Choppin, G.; Clark, S.; Dietz, M.; Rogers, R.; Traina, S.; Baldwin, D.; Thurnauer, M.; Hall, G.; Newman, L.; Miller, D.; Kung, H.; Parkin, D.; Shuh, D.; Shaw, H.; Terminello, L.; Meisel, D.; Blake, D.; Buchanan, M.; Roberto, J.; Colson, S.; Carling, R.; Samara, G.; Sasaki, D.; Pianetta, P.; Faison, B.; Thomassen, D.; Fryberger, T.; Kiernan, G.; Kreisler, M.; Morgan, L.; Hicks, J.; Dehmer, J.; Kerr, L.; Smith, B.; Mays, J.; Clark, S.

    2002-03-01

    To identify connections between technology needs for countering terrorism and underlying science issues and to recommend investment strategies to increase the impact of basic research on efforts to counter terrorism.

  19. The Abundance of Boron in Diffuse Interstellar Clouds

    CERN Document Server

    Ritchey, A M; Sheffer, Y; Lambert, D L

    2010-01-01

    We present a comprehensive survey of boron abundances in diffuse interstellar clouds from observations made with the Space Telescope Imaging Spectrograph (STIS) of the Hubble Space Telescope. Our sample of 56 Galactic sight lines is the result of a complete search of archival STIS data for the B II 1362 resonance line, with each detection confirmed by the presence of absorption from O I 1355, Cu II 1358, and Ga II 1414 (when available) at the same velocity. Five previous measurements of interstellar B II from Goddard High Resolution Spectrograph observations are incorporated in our analysis, yielding a combined sample that more than quadruples the number of sight lines with significant boron detections. Our survey also constitutes the first extensive analysis of interstellar gallium from STIS spectra and expands on previously published results for oxygen and copper. The observations probe both high and low-density diffuse environments, allowing the density-dependent effects of interstellar depletion to be cle...

  20. Preparation of a radioactive boron compound (B-I-131-lipiodol) for neutron capture therapy of hepatoma

    International Nuclear Information System (INIS)

    In our research, a radioactive boron compound, B-I-131-lipiodol, that can be selectively retained in hepatoma cells was prepared. Combining the effect of α particles produced by boron neutron capture reaction with the β particles released by radionuclides in the radioactive boron compounds will produce a synergistic killing effect on cancer cells. Human hepatoma HepG2 cell cultures were used to examine the stability and the intracellular distribution of the radioactive boron drug. Microscopes were used to examine the interaction and retention of B-I-131-lipiodol globules in the individual hepatoma cell. Moreover, ICP-AES and NaI scintillation counter were performed to determine boron concentrations and I-131 radioactivity, respectively. Results showed that B-I-131-lipiodol with a boron concentration and a specific radioactivity ranged from 500-2000 ppm and 0.05-10 mCi/mL respectively was stably retained in serum. The radiochemical purity of B-I-131-lipiodol was 98%. After supplement with a medium containing B-I-131-lipiodol, the HepG2 cells had intracellular B-I-131-lipiodol globules in the cytoplasm as seen by inverted light microscope, the I-131 and boron can be stably retained in HepG2 cells. (author)

  1. A new and effective approach to boron removal by using novel boron-specific fungi isolated from boron mining wastewater.

    Science.gov (United States)

    Taştan, Burcu Ertit; Çakir, Dilara Nur; Dönmez, Gönül

    2016-01-01

    Boron-resistant fungi were isolated from the wastewater of a boron mine in Turkey. Boron removal efficiencies of Penicillium crustosum and Rhodotorula mucilaginosa were detected in different media compositions. Minimal Salt Medium (MSM) and two different waste media containing molasses (WM-1) or whey + molasses (WM-2) were tested to make this process cost effective when scaled up. Both isolates achieved high boron removal yields at the highest boron concentrations tested in MSM and WM-1. The maximum boron removal yield by P. crustosum was 45.68% at 33.95 mg l(-1) initial boron concentration in MSM, and was 38.97% at 42.76 mg l(-1) boron for R. mucilaginosa, which seemed to offer an economically feasible method of removing boron from the effluents. PMID:26877036

  2. GM Counters: Potential Measurement Uncertainty Sources

    International Nuclear Information System (INIS)

    This paper describes theoretically potential measurement uncertainty sources in radiation detection by GM counters. Procedure of obtaining expanded and combined uncertainties is shown experimentally for four technologically different types of GM counters. Based on experimental results obtained, it has been established that the uncertainties of an influenced random variables depend on the technological solution of the counter reading system and contribute in different ways to the expanded and combined uncertainty of the applied types of GM counters. (author)

  3. Large area flow gas proportional counters

    International Nuclear Information System (INIS)

    The ZJ-LD-800 and ZJ-LD-240 large area flow gas proportional counter tubes are described in detail, and the design of counter tube is expounded. The counter tube there have better than plateau length of 200 V and plateau slope of 2%/100 V and window uniformity of 90% for beta counting. So the counters are ideally suitable for use in Area and Contamination Monitors where both alpha and beta radiation are anticipated

  4. Training options for countering nuclear smuggling

    Energy Technology Data Exchange (ETDEWEB)

    Ball, D Y; Erickson, S A

    1999-07-01

    The burden of stopping a nuclear smuggling attempt at the border rests most heavily on the front-line customs inspector. He needs to know how to use the technological tools at his disposal, how to discern tell-tale anomalies in export documents and manifests, how to notice psychological signs of a smuggler's tension, and how to search anything that might hide nuclear material. This means that assistance in the counter-nuclear smuggling training of customs officers is one of the most critical areas of help that the United States can provide. This paper discusses the various modes of specialized training, both in the field and in courses, as well as the types of assistance that can be provided. Training for nuclear customs specialists, and supervisors and managers of nuclear smuggling detection systems is also important, and differs from front-line inspector training in several aspects. The limitations of training and technological tools such as expert centers that will overcome these limitations are also discussed. Training assistance planned by DOE/NN-43 to Russia within the Second Line of Defense program is discussed in the light of these options, and future possibilities for such training are projected.

  5. Training options for countering nuclear smuggling

    International Nuclear Information System (INIS)

    The burden of stopping a nuclear smuggling attempt at the border rests most heavily on the front-line customs inspector. He needs to know how to use the technological tools at his disposal, how to discern tell-tale anomalies in export documents and manifests, how to notice psychological signs of a smuggler's tension, and how to search anything that might hide nuclear material. This means that assistance in the counter-nuclear smuggling training of customs officers is one of the most critical areas of help that the United States can provide. This paper discusses the various modes of specialized training, both in the field and in courses, as well as the types of assistance that can be provided. Training for nuclear customs specialists, and supervisors and managers of nuclear smuggling detection systems is also important, and differs from front-line inspector training in several aspects. The limitations of training and technological tools such as expert centers that will overcome these limitations are also discussed. Training assistance planned by DOE/NN-43 to Russia within the Second Line of Defense program is discussed in the light of these options, and future possibilities for such training are projected

  6. Risk assessment for one-counter threads

    NARCIS (Netherlands)

    A. Ponse; M.B. van der Zwaag

    2008-01-01

    Threads as contained in a thread algebra are used for the modeling of sequential program behavior. A thread that may use a counter to control its execution is called a ‘one-counter thread’. In this paper the decidability of risk assessment (a certain form of action forecasting) for one-counter threa

  7. Tritium measurement with a proportional counter

    International Nuclear Information System (INIS)

    The purpose of this study is to investigate a feasibility of real-time measurement of tritium concentration with a proportional counter. For the purpose, we constructed a flow-through type of proportional counter. The characteristics of the counter for seven gases, PR, H2, D2, Ar, CH4, N2, and air, were investigated to research appropriate gases. (author)

  8. Science Experimenter: Experimenting with a Geiger Counter.

    Science.gov (United States)

    Mims, Forrest M., III

    1992-01-01

    Describes the use of geiger counters for scientific investigations and experiments. Presents information about background radiation, its sources and detection. Describes how geiger counters work and other methods of radiation detection. Provides purchasing information for geiger counters, related computer software and equipment. (MCO)

  9. Counter-Rotation in Disk Galaxies

    OpenAIRE

    Corsini, E. M.

    2014-01-01

    Counter-rotating galaxies host two components rotating in opposite directions with respect to each other. The kinematic and morphological properties of lenticulars and spirals hosting counter-rotating components are reviewed. Statistics of the counter-rotating galaxies and analysis of their stellar populations provide constraints on the formation scenarios which include both environmental and internal processes.

  10. Structural characterization of electrodeposited boron

    Indian Academy of Sciences (India)

    Ashish Jain; C Ghosh; T R Ravindran; S Anthonysamy; R Divakar; E Mohandas; G S Gupta

    2013-12-01

    Structural characterization of electrodeposited boron was carried out by using transmission electron microscopy and Raman spectroscopy. Electron diffraction and phase contrast imaging were carried out by using transmission electron microscopy. Phase identification was done based on the analysis of electron diffraction patterns and the power spectrum calculated from the lattice images from thin regions of the sample. Raman spectroscopic examination was carried out to study the nature of bonding and the allotropic form of boron obtained after electrodeposition. The results obtained from transmission electron microscopy showed the presence of nanocrystallites embedded in an amorphous mass of boron. Raman microscopic studies showed that amorphous boron could be converted to its crystalline form at high temperatures.

  11. Boron diffusion in silicon devices

    Science.gov (United States)

    Rohatgi, Ajeet; Kim, Dong Seop; Nakayashiki, Kenta; Rounsaville, Brian

    2010-09-07

    Disclosed are various embodiments that include a process, an arrangement, and an apparatus for boron diffusion in a wafer. In one representative embodiment, a process is provided in which a boric oxide solution is applied to a surface of the wafer. Thereafter, the wafer is subjected to a fast heat ramp-up associated with a first heating cycle that results in a release of an amount of boron for diffusion into the wafer.

  12. Discharge quenching circuit for counters

    International Nuclear Information System (INIS)

    A circuit for quenching discharges in gas-discharge detectors with working voltage of 3-5 kV based on transistors operating in the avalanche mode is described. The quenching circuit consists of a coordinating emitter follower, amplifier-shaper for avalanche key cascade control which changes potential on the counter electrodes and a shaper of discharge quenching duration. The emitter follower is assembled according to a widely used flowsheet with two transistors. The circuit permits to obtain a rectangular quenching pulse with front of 100 ns and an amplitude of up to 3.2 kV at duration of 500 μm-8 ms. Application of the quenching circuit described permits to obtain countering characteristics with the slope less than or equal to 0.02%/V and plateau extent greater than or equal to 300 V

  13. Proportional counter as neutron detector

    Science.gov (United States)

    Braby, L. A.; Badhwar, G. D.

    2001-01-01

    A technique to separate out the dose, and lineal energy spectra of neutrons and charged particles is described. It is based on using two proportional counters, one with a wall, and the other with similar characteristics but wall made from a non-hydrogen containing material. Results of a calibration in a neutron field are also shown. c2001 Elsevier Science Ltd. All rights reserved.

  14. Monte Carlo simulation on the application of boron-coated MRPC thermal neutron detector to the compensated neutron logging

    International Nuclear Information System (INIS)

    Background: The compensated neutron logging technology is widely used in oil exploration and development. The neutron detector commonly used in this technology is the helium-3 proportional counter. Due to the decreasing in supply of the helium-3 gas, the price of the helium-3 proportional counter rises quickly. Purpose: The aim is to develop a new type of neutron detector to replace the helium-3 tubes in the compensated neutron logging technology. Methods: A new thermal neutron detector coated with a layer of thermal neutron converter in the inner glass of the Multi-gap Resistive Plate Chamber (MRPC) was developed. Under the conventional and underbalanced conditions, Monte Carlo method was used to simulate the response of the boron-coated MRPC thermal neutron detector and helium-3 proportional counter employed in compensated neutron logging technology. Results: It is shown that the SS/LS increases with the rise of porosity using either the boron-coated MRPC thermal neutron detector or the helium-3 proportional counter, and the results of these two detectors are basically identical. Conclusion: It indicates that the boron-coated MRPC thermal neutron detector can be used for compensated neutron logging. (authors)

  15. Survey of boron detectors for thermal neutrons operating in the non proportional regime

    International Nuclear Information System (INIS)

    In gas counters, the alternative of directly detecting (i.e. without using the phenomenon of multiplication the charges ionized by the reaction 10B (n,α)7Li, offers many advantages as to the conception of such a detector. After examining the ionization phenomenon and deducing the characteristics of low-noise amplifiers, various prototypes are studied. - The D.I.N. 5/4, intended for fast neutrons detector, grants leave to have good isotropic proprieties thanks to its geometry and good sensitivity imputable to the BF3 filling pressure of 1 atm. - A flat counter (D.E.H. type), with plane and parallel electrodes, grants leave to work out a low height of influence, soil moisture measurer. The confrontation between various filling pressures (0.5, 1, 2, 3 atm.) points out the importance of attachment in BF3. - Thanks to neutronic diffraction counter (C.D.N. 2 type) filled under 2 atm and parallelepiped, one can considerably reduce the weight of the goniometer protection, and lightly increase its sensitivity. - The results given by the experimental boron coating device have allowed to build a boron coating counter to be used in current collection. (author)

  16. Boron Fullerenes: A First-Principles Study

    Directory of Open Access Journals (Sweden)

    Gonzalez Szwacki Nevill

    2007-01-01

    Full Text Available AbstractA family of unusually stable boron cages was identified and examined using first-principles local-density functional method. The structure of the fullerenes is similar to that of the B12icosahedron and consists of six crossing double-rings. The energetically most stable fullerene is made up of 180 boron atoms. A connection between the fullerene family and its precursors, boron sheets, is made. We show that the most stable boron sheets are not necessarily precursors of very stable boron cages. Our finding is a step forward in the understanding of the structure of the recently produced boron nanotubes.

  17. Stellar counter-rotation in lenticular galaxy NGC 448

    CERN Document Server

    Katkov, Ivan Yu; Chilingarian, Igor V; Uklein, Roman I; Egorov, Oleg V

    2016-01-01

    The counter-rotation phenomenon in disc galaxies directly indicates a complex galaxy assembly history which is crucial for our understanding of galaxy physics. Here we present the complex data analysis for a lenticular galaxy NGC 448, which has been recently suspected to host a counter-rotating stellar component. We collected deep long-slit spectroscopic observations using the Russian 6-m telescope and performed the photometric decomposition of Sloan Digital Sky Survey (SDSS) archival images. We exploited (i) a non-parametric approach in order to recover stellar line-of-sight velocity distributions and (ii) a parametric spectral decomposition technique in order to disentangle stellar population properties of both main and counter-rotating stellar discs. Our spectral decomposition stays in perfect agreement with the photometric analysis. The counter-rotating component contributes $\\approx$30 per cent to the total galaxy light. We estimated its stellar mass to be $9.0^{+2.7}_{-1.8}\\cdot10^{9}M_\\odot$. The radia...

  18. Wettability of boron carbide

    International Nuclear Information System (INIS)

    The wettability of boron carbide has been examined by means of the sessile drop method, using the following candidate alloys: (96wt%AG-4wt%Ti), (Ag-26.5wt%Cu-3wt%Ti), (Sn-10wt%Ag-4wt%Ti), Sn(99.95wt%) and Al(99.99wt%). The results show that B4C is completely wetted by the Ag-based alloys. Sn-10wt%Ag-4wt%Ti alloy and pure Al partly wet the B4C surface, while pure Sn does not wet B4C at all. For all the alloys used, except pure Sn, a reaction layer was observed at the interface between the ceramic part and the metal drop. Although the spreading kinetics of the Al-drop was much slower compared with the Ti-containing alloys, the reaction rate was considerably higher in the former case. This suggests that aluminium is an attractive candidate material for brazing of B4C. Formation of the low melting B2O3 at the B4C surface may cause oxidation of the filler metal during joining, which, in turn, leads to a low bond strength

  19. Thermal conductivity of boron carbide-boron nitride composites

    International Nuclear Information System (INIS)

    This paper reports that because of their preferred orientation, the addition of boron nitride dispersions to hot-pressed boron carbide was found to result in a considerable degree of anisotropy in thermal conductivity of the resulting composite, indicated by an increase in the thermal conductivity perpendicular to the hot-pressing direction by as much as a factor of 3 at the highest boron nitride volume fractions of this study, and a decrease in the thermal conductivity parallel to the hot-pressing direction by as much as a factor of 2. The composite data were found to be below the values expected from composite theory, which may represent indirect evidence for the existence of an interfacial thermal barrier

  20. The boron trifluoride nitromethane adduct

    Science.gov (United States)

    Ownby, P. Darrell

    2004-02-01

    The separation of the boron isotopes using boron trifluoride·organic-donor, Lewis acid·base adducts is an essential first step in preparing 10B enriched and depleted crystalline solids so vital to nuclear studies and reactor applications such as enriched MgB 2, boron carbide, ZrB 2, HfB 2, aluminum boron alloys, and depleted silicon circuits for radiation hardening and neutron diffraction crystal structure studies. The appearance of this new adduct with such superior properties demands attention in the continuing search for more effective and efficient means of separation. An evaluation of the boron trifluoride nitromethane adduct, its thermodynamic and physical properties related to large-scale isotopic separation is presented. Its remarkably high separation factor was confirmed to be higher than the expected theoretical value. However, the reportedly high acid/donor ratio was proven to be an order of magnitude lower. On-going research is determining the crystal structure of deuterated and 11B enriched 11BF 3·CD 3NO 2 by X-ray and neutron diffraction.

  1. Scintillation counter based radiation dosimeter

    International Nuclear Information System (INIS)

    The average human exposure per year is about 240mrem which is come from Radon and human body and terrestrial and cosmic radiation and man-made source. Specially radiation exposure through air from environmental radiation sources is 80mrem/yr(= 0.01mR/hr) which come from Terrestrial and cosmic radiation. Radiation dose is defined as energy deposit/mass. There are two major methods to detect radiation. First method is the energy integration using Air equivalent material like GM counter wall material. Second method is the spectrum to dose conversion method using NaI(Tl), HPGe. These two methods are using generally to detect radiation. But these methods are expensive. So we need new radiation detection method. The research purpose is the development of economical environmental radiation dosimeter. This system consists of Plastic/Inorganic scintillator and Si photo-diode based detector and counting based circuitry. So count rate(cps) can be convert to air exposure rate(R/hr). There are three major advantages in this system. First advantages is no high voltage power supply like GM counter. Second advantage is simple electronics. Simple electronics system can be achieved by Air-equivalent scintillation detector with Al filter for the same detection efficiency vs E curve. From former two advantages, we can know the most important advantages of the this system. Third advantage is economical system. The price of typical GM counter is about $1000. But the price of our system is below $100 because of plastic scintillator and simple electronics. The role of scintillation material is emitting scintillation which is the flash of light produced in certain materials when they absorb ionizing radiation. Plastic scintillator is organic scintillator which is kind of hydrocarbons. The special point are cheap price, large size production(∼ton), moderate light output, fast light emission(ns). And the role of Al filter is equalizing counting efficiency of air and scintillator for

  2. Condensation Particle Counter Instrument Handbook

    Energy Technology Data Exchange (ETDEWEB)

    Kuang, C. [Brookhaven National Lab. (BNL), Upton, NY (United States)

    2016-02-01

    The Model 3772 CPC is a compact, rugged, and full-featured instrument that detects airborne particles down to 10 nm in diameter, at an aerosol flow rate of 1.0 lpm, over a concentration range from 0 to 1x104 #/cc. This CPC is ideally suited for applications without high concentration measurements, such as basic aerosol research, filter and air-cleaner testing, particle counter calibrations, environmental monitoring, mobile aerosol studies, particle shedding and component testing, and atmospheric and climate studies.

  3. Root Responses to Boron Deficiency Mediated by Ethylene

    OpenAIRE

    González-Fontes, Agustín; Herrera-Rodríguez, M. B.; Martín-Rejano, Esperanza M.; Navarro-Gochicoa, M. T.; Rexach, Jesús; Camacho-Cristóbal, Juan J.

    2016-01-01

    Low boron (B) supply alters the architecture of the root system in Arabidopsis thaliana seedlings, leading to a reduction in the primary root growth and an increase in the length and number of root hairs. At short-term (hours), B deficiency causes a decrease in the cell elongation of the primary root, resulting in a lower growth. Experimental approaches using ethylene insensitive Arabidopsis mutants, inhibitors of ethylene response, and GUS reporter lines suggest that ethylene is involved in ...

  4. Boron carbide nanolumps on carbon nanotubes

    Science.gov (United States)

    Lao, J. Y.; Li, W. Z.; Wen, J. G.; Ren, Z. F.

    2002-01-01

    Boron carbide nanolumps are formed on the surface of multiwall carbon nanotubes by a solid-state reaction between boron and carbon nanotubes. The reaction is localized so that the integrity of the structure of carbon nanotubes is maintained. Inner layers of multiwall carbon nanotubes are also bonded to boron carbide nanolumps. These multiwall carbon nanotubes with boron carbide nanolumps are expected to be the ideal reinforcing fillers for high-performance composites because of the favorable morphology.

  5. NEW ADVANCES IN BORON SOIL CHEMISTRY

    Science.gov (United States)

    Boron is an essential micronutrient element required for plant growth. Boron deficiency is wide-spread in crop plants throughout the world especially in coarse-textured soils in humid areas. Boron toxicity can also occur, especially in arid regions under irrigation. Plants respond directly to the...

  6. Boron doping a semiconductor particle

    Science.gov (United States)

    Stevens, Gary Don; Reynolds, Jeffrey Scott; Brown, Louanne Kay

    1998-06-09

    A method (10,30) of boron doping a semiconductor particle using boric acid to obtain a p-type doped particle. Either silicon spheres or silicon powder is mixed with a diluted solution of boric acid having a predetermined concentration. The spheres are dried (16), with the boron film then being driven (18) into the sphere. A melt procedure mixes the driven boron uniformly throughout the sphere. In the case of silicon powder, the powder is metered out (38) into piles and melted/fused (40) with an optical furnace. Both processes obtain a p-type doped silicon sphere with desired resistivity. Boric acid is not a restricted chemical, is inexpensive, and does not pose any special shipping, handling, or disposal requirements.

  7. Programmable spark counter of tracks

    International Nuclear Information System (INIS)

    For the purpose, a new set-the programmable all-automatic spark counter AIST-4-has been developed and manufactured. Compared to our previous automated spark counter ISTRA, which was operated by the integrated fixed program, the new set is operated completely by a personal computer. The mechanism for pressing and pulling the aluminized foil is put into action by a step motor operated by a microcontroller. The step motor turns an axle. The axle has two eccentrics. One of them moves a pressing plate up and down. The second eccentric moves the aluminized foil by steps of ∼15mm after the end of each pulse counting. One turnover of the axle corresponds to one pulse count cycle. The step motor, the high-voltage block and the pulse count block are operated by the microcontroller PIC 16C84 (Microstar). The set can be operated either manually by keys on the front panel or by a PC using dialogue windows for radon or neutron measurements (for counting of alpha or fission fragment tracks). A number of algorithms are developed: the general procedures, the automatic stopping of the pulse counting, the calibration curve, determination of the count characteristics and elimination of the short circuit in a track

  8. Synchronous Counters Implemented in the PLD Devices

    Directory of Open Access Journals (Sweden)

    J. Kolouch

    1999-04-01

    Full Text Available The implementability of synchronous counters in the Programmable Logic Devices (PLD is discussed in this paper. The most commonly used counters are analysed from this point of view. The expressions for their individual bits are given and the number of product terms is derived to allow to estimate the size of the particular counter which can be implemented in the chosen PLD.

  9. Cherenkov counter for particle identification test beam

    International Nuclear Information System (INIS)

    The Cherenkov counter used for selecting electrons of the test beam has been studied in this article. The design, manufacture, assembly and testing of the Cherenkov counter are described. And the performance of this counter is measured. The CO2 gas is used as Cherenkov radiator, the XP2020Q photomultiplier is applied for recording signals of the Cherenkov light. The (99.0±0.5)% efficiency of the electron selection has been reached

  10. Fuzzy Logic Application in Boron and Cadmium Analysis in U3O8 use of Emission Spectrograph Method

    International Nuclear Information System (INIS)

    Boron and cadmium in U3O8 have been analyzed with emission spectrograph. Three inputs of emission spectrograph, current (A), exposure time (second) and gap between electrodes (mm) were varied. Two outputs, boron and cadmium lines intensities respectively were selected and measured. Thirteen experiments have been carried out and data found were calculated by fuzzy logic Mamdani-type. Three and five memberships functions of straight-line (Triangular, Trapezoidal), Generalized-bell and Gaussian curve were used to analyze the found data. The result found that five memberships functions had less error percentage range than three memberships functions of straight-line (Triangular, Trapezoidal), Generalized-bell and Gaussian curve. The error percentage range of cadmium analysis was wider than boron analysis with this method. Analysis of cadmium in U3O8 with this method needs much exposure time compare to analysis of boron. (author)

  11. Boron steel. I Part. Preparation

    International Nuclear Information System (INIS)

    With the advent of the first nuclear reactors arise the need for control rods and shielding duties for some types of radiations. One of the materials used for this purpose has been the high boron steel. This paper describes the melting and casting procedures employed for the production, at laboratory scale, of steels with Boron content ranging from 1 to 4 per cent, as well as the metallographic and X-Ray techniques used for the identification of the present phases. The electrolytic technique employed for the isolation of the Fe2B phase and its subsequent X-Ray identification has proved to be satisfactory. (Author) 11 refs

  12. Shear amorphization of boron suboxide

    International Nuclear Information System (INIS)

    We report for the first time the shear-induced local amorphization of boron suboxide subjected to nanoindentation. The amorphous bands have a width of ∼1–3 nm and a length of 200–300 nm along the (01¯11) crystal plane. We show direct experimental evidence that the amorphous shear bands of boron suboxide are driven from the coalescence of dislocation loops under high shear stresses. These observations provide insights into the microscopic deformation and failure of high-strength and lightweight ceramics

  13. Thermal conductivity of boron carbides

    Science.gov (United States)

    Wood, C.; Emin, D.; Gray, P. E.

    1985-01-01

    Knowledge of the thermal conductivity of boron carbide is necessary to evaluate its potential for high-temperature thermoelectric energy conversion applications. Measurements have been conducted of the thermal diffusivity of hot-pressed boron carbide BxC samples as a function of composition (x in the range from 4 to 9), temperature (300-1700 K), and temperature cycling. These data, in concert with density and specific-heat data, yield the thermal conductivities of these materials. The results are discussed in terms of a structural model that has been previously advanced to explain the electronic transport data. Some novel mechanisms for thermal conduction are briefly discussed.

  14. Mechanical properties of boron coatings

    International Nuclear Information System (INIS)

    Internal stress of coatings will cause reliability problems, such as adhesion failure and peeling. We measured the internal stress in boron coatings, which was prepared by the ion plating method, with an apparatus based on the optically levered laser technique. The boron coatings exhibited large compressive stress in the range from -0.5 GPa to -2.6 GPa. It was found that these compressive stresses were decreasing functions of the deposition rate and were increasing functions of the ion bombardment energy. ((orig.))

  15. Boron-enhanced diffusion of boron from ultralow-energy boron implantation

    International Nuclear Information System (INIS)

    The authors have investigated the diffusion enhancement mechanism of BED (boron enhanced diffusion), wherein the boron diffusivity is enhanced three to four times over the equilibrium diffusivity at 1,050 C in the proximity of a silicon layer containing a high boron concentration. It is shown that BED is associated with the formation of a fine-grain polycrystalline silicon boride phase within an initially amorphous Si layer having a high B concentration. For 0.5 keV B+, the threshold implantation dose which leads to BED lies between 3 x 1014 and of 1 x 1015/cm-2. Formation of the shallowest possible junctions by 0.5 keV B+ requires that the implant dose be kept lower than this threshold

  16. Compact fission counter for DANCE

    International Nuclear Information System (INIS)

    The Detector for Advanced Neutron Capture Experiments (DANCE) consists of 160 BF2 crystals with equal solid-angle coverage. DANCE is a 4π γ-ray calorimeter and designed to study the neutron-capture reactions on small quantities of radioactive and rare stable nuclei. These reactions are important for the radiochemistry applications and modeling the element production in stars. The recognition of capture event is made by the summed γ-ray energy which is equivalent of the reaction Q-value and unique for a given capture reaction. For a selective group of actinides, where the neutron-induced fission reaction competes favorably with the neutron capture reaction, additional signature is needed to distinguish between fission and capture γ rays for the DANCE measurement. This can be accomplished by introducing a detector system to tag fission fragments and thus establish a unique signature for the fission event. Once this system is implemented, one has the opportunity to study not only the capture but also fission reactions. A parallel-plate avalanche counter (PPAC) has many advantages for the detection of heavy charged particles such as fission fragments. These include fast timing, resistance to radiation damage, and tolerance of high counting rate. A PPAC also can be tuned to be insensitive to α particles, which is important for experiments with α-emitting actinides. Therefore, a PPAC is an ideal detector for experiments requiring a fast and clean trigger for fission. A PPAC with an ingenious design was fabricated in 2006 by integrating amplifiers into the target assembly. However, this counter was proved to be unsuitable for this application because of issues related to the stability of amplifiers and the ability to separate fission fragments from α's. Therefore, a new design is needed. A LLNL proposal to develop a new PPAC for DANCE was funded by NA22 in FY09. The design goal is to minimize the mass for the proposed counter and still be able to maintain a stable

  17. Compact fission counter for DANCE

    Energy Technology Data Exchange (ETDEWEB)

    Wu, C Y; Chyzh, A; Kwan, E; Henderson, R; Gostic, J; Carter, D; Bredeweg, T; Couture, A; Jandel, M; Ullmann, J

    2010-11-06

    The Detector for Advanced Neutron Capture Experiments (DANCE) consists of 160 BF{sub 2} crystals with equal solid-angle coverage. DANCE is a 4{pi} {gamma}-ray calorimeter and designed to study the neutron-capture reactions on small quantities of radioactive and rare stable nuclei. These reactions are important for the radiochemistry applications and modeling the element production in stars. The recognition of capture event is made by the summed {gamma}-ray energy which is equivalent of the reaction Q-value and unique for a given capture reaction. For a selective group of actinides, where the neutron-induced fission reaction competes favorably with the neutron capture reaction, additional signature is needed to distinguish between fission and capture {gamma} rays for the DANCE measurement. This can be accomplished by introducing a detector system to tag fission fragments and thus establish a unique signature for the fission event. Once this system is implemented, one has the opportunity to study not only the capture but also fission reactions. A parallel-plate avalanche counter (PPAC) has many advantages for the detection of heavy charged particles such as fission fragments. These include fast timing, resistance to radiation damage, and tolerance of high counting rate. A PPAC also can be tuned to be insensitive to {alpha} particles, which is important for experiments with {alpha}-emitting actinides. Therefore, a PPAC is an ideal detector for experiments requiring a fast and clean trigger for fission. A PPAC with an ingenious design was fabricated in 2006 by integrating amplifiers into the target assembly. However, this counter was proved to be unsuitable for this application because of issues related to the stability of amplifiers and the ability to separate fission fragments from {alpha}'s. Therefore, a new design is needed. A LLNL proposal to develop a new PPAC for DANCE was funded by NA22 in FY09. The design goal is to minimize the mass for the proposed

  18. Determination of boron in the waters of Troia by inductively coupled plasma-atomic emission spectrometry (ICP-AES

    Directory of Open Access Journals (Sweden)

    HASAN OZCAN

    2005-10-01

    Full Text Available The inductively coupled plasma-atomic emission spectrometry method (ICP-EAS is proposed for the determination of boron in Troia water sources. In this study, boron samples were taken from 25 different locations during November 2002 and May 2003. The 249.773 nm boron emmision line was not affected by the samplematrix. The boron content was determined without further pretreatment of samples proposed ICP-AES method. An analysis of a given sample was completed in about 15 min. The determined boron concentrations in surface and ground water sources were between 0.00444–1.11200mgl-1. Inorder to compare the results obtained by the proposed method, selected water samples were also analysed titrimetically. Pearson correlation coefficient analysis showed that there is a close relationship between the ICP-AES and the titrimetric method and the determination coefficient (R2 was calculated to be 91.34 %.

  19. Analytical boron diffusivity model in silicon for thermal diffusion from boron silicate glass film

    Science.gov (United States)

    Kurachi, Ikuo; Yoshioka, Kentaro

    2015-09-01

    An analytical boron diffusivity model in silicon for thermal diffusion from a boron silicate glass (BSG) film has been proposed in terms of enhanced diffusion due to boron-silicon interstitial pair formation. The silicon interstitial generation is considered to be a result of the silicon kick-out mechanism by the diffused boron at the surface. The additional silicon interstitial generation in the bulk silicon is considered to be the dissociation of the diffused pairs. The former one causes the surface boron concentration dependent diffusion. The latter one causes the local boron concentration dependent diffusion. The calculated boron profiles based on the diffusivity model are confirmed to agree with the actual diffusion profiles measured by secondary ion mass spectroscopy (SIMS) for a wide range of the BSG boron concentration. This analytical diffusivity model is a helpful tool for p+ boron diffusion process optimization of n-type solar cell manufacturing.

  20. Evaluation of Aluminum-Boron Carbide Neutron Absorbing Materials for Interim Storage of Used Nuclear Fuel

    International Nuclear Information System (INIS)

    The objective of this work was to understand the corrosion behavior of Boral® and Bortec® neutron absorbers over long-term deployment in a used nuclear fuel dry cask storage environment. Corrosion effects were accelerated by flowing humidified argon through an autoclave at temperatures up to 570°C. Test results show little corrosion of the aluminum matrix but that boron is leaching out of the samples. Initial tests performed at 400 and 570°C were hampered by reduced flow caused by the rapid build-up of solid deposits in the outlet lines. Analysis of the deposits by XRD shows that the deposits are comprised of boron trioxide and sassolite (H3BO3). The collection of boron- containing compounds in the outlet lines indicated that boron was being released from the samples. Observation of the exposed samples using SEM and optical microscopy show the growth of new phases in the samples. These phases were most prominent in Bortec® samples exposed at 570°C. Samples of Boral® exposed at 570°C showed minimal new phase formation but showed nearly the complete loss of boron carbide particles. Boron carbide loss was also significant in Boral samples at 400°C. However, at 400°C phases similar to those found in Bortec® were observed. The rapid loss of the boron carbide particles in the Boral® is suspected to inhibit the formation of the new secondary phases. However, Material samples in an actual dry cask environment would be exposed to temperatures closer to 300°C and less water than the lowest test. The results from this study conclude that at the temperature and humidity levels present in a dry cask environment, corrosion and boron leaching will have no effect on the performance of Boral® and Bortec® to maintain criticality control.

  1. Evaluation of Aluminum-Boron Carbide Neutron Absorbing Materials for Interim Storage of Used Nuclear Fuel

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Lumin [Univ. of Michigan, Ann Arbor, MI (United States). Department of Nuclear Engineering and Radiological Science; Wierschke, Jonathan Brett [Univ. of Michigan, Ann Arbor, MI (United States). Department of Nuclear Engineering and Radiological Science

    2015-04-08

    The objective of this work was to understand the corrosion behavior of Boral® and Bortec® neutron absorbers over long-term deployment in a used nuclear fuel dry cask storage environment. Corrosion effects were accelerated by flowing humidified argon through an autoclave at temperatures up to 570°C. Test results show little corrosion of the aluminum matrix but that boron is leaching out of the samples. Initial tests performed at 400 and 570°C were hampered by reduced flow caused by the rapid build-up of solid deposits in the outlet lines. Analysis of the deposits by XRD shows that the deposits are comprised of boron trioxide and sassolite (H3BO3). The collection of boron- containing compounds in the outlet lines indicated that boron was being released from the samples. Observation of the exposed samples using SEM and optical microscopy show the growth of new phases in the samples. These phases were most prominent in Bortec® samples exposed at 570°C. Samples of Boral® exposed at 570°C showed minimal new phase formation but showed nearly the complete loss of boron carbide particles. Boron carbide loss was also significant in Boral samples at 400°C. However, at 400°C phases similar to those found in Bortec® were observed. The rapid loss of the boron carbide particles in the Boral® is suspected to inhibit the formation of the new secondary phases. However, Material samples in an actual dry cask environment would be exposed to temperatures closer to 300°C and less water than the lowest test. The results from this study conclude that at the temperature and humidity levels present in a dry cask environment, corrosion and boron leaching will have no effect on the performance of Boral® and Bortec® to maintain criticality control.

  2. Countering 21st Century Threats

    DEFF Research Database (Denmark)

    Scharling Pedersen, Peter; Pillai, Chad M.; Hun, Lee Jae

    2015-01-01

    The United States and its Allies confront an increasingly volatile world where threats range from traditional state-on-state challenges to non-state transnational networks. To successfully combat these 21st Century problems, in an era of resource and geo-political power constraints, the U.S. and......), Counter-Terrorism (CT), and Security and Stability Operations (SSO). • Establishing a construct that allows a strategic Whole-of-Government capacity for operations coordinated by joint interagency task forces. • Continue to developing the Global SOF network. • Increased intelligence sharing in areas of...... shared interests pre-crisis. • Establish political agreements and/or intentions with partners to address potential threats. • Establishing mutual trust through Building Partnership Capacity with capable SOF and intelligence organizations....

  3. Analysis of boronized wall in LHD

    International Nuclear Information System (INIS)

    Boronization has been carried out in some experimental fusion devices as one of wall conditioning Methods. The well-known merits of the boronization are as follows: 1) coated-boron on the first wall has strong gettering function for oxygen impurities and oxygen has been kept into boron films as a boron-oxide and 2) boron film covers first wall with apparently low Z materials facing the plasma. However, an operation scenario of boronization for next generation devices such as ITER is not optimized. In this paper, we discuss an optimized method of coated film uniformity in a wide area and a lifetime of boron film as an oxygen getter using experimental data in the large helical device (LHD). In LHD, boronization by glow discharges has been carried out a few times during each experimental campaign. Helium-diborane mixtured gas is used and plasma facing components (PFM) are stainless steel (SS) for the first wall and carbon for the divertor plates kept in the room temperature. Material probes made of SS316 and Si were installed in the vacuum vessel and exposed during the experimental campaign. Depth profiles of their impurities were analyzed using the X-ray Photoelectron Spectroscopy (XPS) and the Auger electron spectroscopy (AES). Two types of gettering process by boron film have been investigated. One is the process during boronization and the other is that after boronization. Concerning a lifetime of boron film, the distribution of oxygen near the top surface region (0 to 20 nm) indicates a process of oxygen gettering, it shows a contribution after boronization. In this paper, these kinds of process using material probes are shown. (authors)

  4. Boron Poisoning of Plutonium Solutions

    International Nuclear Information System (INIS)

    The results of a theoretical investigation into the possible relaxation of criticality concentration limits in wet chemical reprocessing plants, due to the introduction of boron poisoning, are reported. The following systems were considered: 1. 1 in. stainless steel tubes filled with boron carbide at various pitches in homogeneous mixtures of 239Pu (NO3)4, 5H2O and water. 2. 1 in. and 2 in borosilicate glass Raschig rings in homogeneous mixtures of 239Pu (NO3)4, 5H2O and water. 3. The concentration of natural boron required for k∞ = 1 in homogeneous mixtures of 239Pu-B-H2O. The method of calculation was Monte Carlo using the GEM code with Nuclear Data File cross-sections. The Raschig rings used are those commercially available. The core model consisted of a cubic arrangement of unit cubes of solution within each of which a Raschig ring was centrally placed. The arrangement was such that the rings were regularly stacked with axes parallel, but the side of the unit cube was fixed to preserve the random packing density. Comparison is made with other reported results on boron poisoning. (author)

  5. Boron sorption characteristics in resins

    International Nuclear Information System (INIS)

    The purpose of boron addition in a nuclear power plant is to control the reactivity. In PHWRs, it is injected into the moderator system in the form of boric anhydride solution, while in PHWRs, it is added to the primary heat transport system in the form of boric acid solution. The required boron levels in PHWRs are controlled by valving in strong base anion exchangers having exchangeable species in OD- form while in PHWRs, the same can be achieved by restoring to the use of Boron Thermal Regeneration System (BTRS). This system operates on the principle of existence of different amounts of various polyborate ions at different temperatures, solution pH's and the boric acid concentrations and on the reversible sorption of these polyions on strong base anion exchange resins. This report describes the salient features of boron sorption characteristics on four types of anion exchange resins, based on experimental data generated in the chemical laboratories of Reactor Engineering Division of the Bhabha Atomic Research Centre, Bombay. The report further makes an attempt to calculate the pH of the resin and solution phases and the percentages of different polyborates and undissociated boric acid, under the experimental conditions investigated. (author). 30 refs., 4 figs., 20 tables

  6. Advanced microstructure of boron carbide.

    Science.gov (United States)

    Werheit, Helmut; Shalamberidze, Sulkhan

    2012-09-26

    The rhombohedral elementary cell of the complex boron carbide structure is composed of B(12) or B(11)C icosahedra and CBC, CBB or B□B (□, vacancy) linear arrangements, whose shares vary depending on the actual chemical compound. The evaluation of the IR phonon spectra of isotopically pure boron carbide yields the quantitative concentrations of these components within the homogeneity range. The structure formula of B(4.3)C at the carbon-rich limit of the homogeneity range is (B(11)C) (CBC)(0.91) (B□B)(0.09) (□, vacancy); and the actual structure formula of B(13)C(2) is (B(12))(0.5)(B(11)C)(0.5)(CBC)(0.65)(CBB)(0.16) (B□B)(0.19), and deviates fundamentally from (B(12))CBC, predicted by theory to be the energetically most favourable structure of boron carbide. In reality, it is the most distorted structure in the homogeneity range. The spectra of (nat)B(x)C make it evident that boron isotopes are not randomly distributed in the structure. However, doping with 2% silicon brings about a random distribution. PMID:22945740

  7. Boron isotopes in geothermal systems

    International Nuclear Information System (INIS)

    Boron is a highly mobile element and during water-rock reactions, boron is leached out of rocks with no apparent fractionation. In geothermal systems where the water recharging the systems are meteoric in origin, the B isotope ratio of the geothermal fluid reflects the B isotope ratio of the rocks. Seawater has a distinctive B isotope ratio and where seawater recharges the geothermal system, the B isotope ratio of the geothermal system reflects the mixing of rock derived B and seawater derived B. Any deviations of the actual B isotope ratio of a mixture reflects subtle differences in the water-rock ratios in the cold downwelling limb of the hydrothermal system. This paper will present data from a variety of different geothermal systems, including New Zealand; Iceland; Yellowston, USA; Ibusuki, Japan to show the range in B isotope ratios in active geothermal systems. Some of these systems show well defined mixing trends between seawater and the host rocks, whilst others show the boron isotope ratios of the host rock only. In geothermal systems containing high amounts of CO2 boron isotope ratios from a volatile B source can also be inferred. (auth)

  8. On generating counter-rotating streamwise vortices

    KAUST Repository

    Winoto, S H

    2015-09-23

    Counter-rotating streamwise vortices are known to enhance the heat transfer rate from a surface and also to improve the aerodynamic performance of an aerofoil. In this paper, some methods to generate such counter-rotating vortices using different methods or physical conditions will be briefly considered and discussed.

  9. Friction anisotropy in boronated graphite

    Energy Technology Data Exchange (ETDEWEB)

    Kumar, N., E-mail: niranjan@igcar.gov.in [Materials Science Group, Indira Gandhi Centre for Atomic Research, Kalpakkam (India); Radhika, R. [Crystal Growth Centre, Anna University, Chennai (India); Kozakov, A.T. [Research Institute of Physics, Southern Federal University, Rostov-on-Don (Russian Federation); Pandian, R. [Materials Science Group, Indira Gandhi Centre for Atomic Research, Kalpakkam (India); Chakravarty, S. [UGC-DAE CSR, Kalpakkam (India); Ravindran, T.R.; Dash, S.; Tyagi, A.K. [Materials Science Group, Indira Gandhi Centre for Atomic Research, Kalpakkam (India)

    2015-01-01

    Graphical abstract: - Highlights: • Friction anisotropy in boronated graphite is observed in macroscopic sliding condition. • Low friction coefficient is observed in basal plane and becomes high in prismatic direction. • 3D phase of boronated graphite transformed into 2D structure after friction test. • Chemical activity is high in prismatic plane forming strong bonds between the sliding interfaces. - Abstract: Anisotropic friction behavior in macroscopic scale was observed in boronated graphite. Depending upon sliding speed and normal loads, this value was found to be in the range 0.1–0.35 in the direction of basal plane and becomes high 0.2–0.8 in prismatic face. Grazing-incidence X-ray diffraction analysis shows prominent reflection of (0 0 2) plane at basal and prismatic directions of boronated graphite. However, in both the wear tracks (1 1 0) plane become prominent and this transformation is induced by frictional energy. The structural transformation in wear tracks is supported by micro-Raman analysis which revealed that 3D phase of boronated graphite converted into a disordered 2D lattice structure. Thus, the structural aspect of disorder is similar in both the wear tracks and graphite transfer layers. Therefore, the crystallographic aspect is not adequate to explain anisotropic friction behavior. Results of X-ray photoelectron spectroscopy and Fourier transform infrared spectroscopy shows weak signature of oxygen complexes and functional groups in wear track of basal plane while these species dominate in prismatic direction. Abundance of these functional groups in prismatic plane indicates availability of chemically active sites tends to forming strong bonds between the sliding interfaces which eventually increases friction coefficient.

  10. Friction anisotropy in boronated graphite

    International Nuclear Information System (INIS)

    Graphical abstract: - Highlights: • Friction anisotropy in boronated graphite is observed in macroscopic sliding condition. • Low friction coefficient is observed in basal plane and becomes high in prismatic direction. • 3D phase of boronated graphite transformed into 2D structure after friction test. • Chemical activity is high in prismatic plane forming strong bonds between the sliding interfaces. - Abstract: Anisotropic friction behavior in macroscopic scale was observed in boronated graphite. Depending upon sliding speed and normal loads, this value was found to be in the range 0.1–0.35 in the direction of basal plane and becomes high 0.2–0.8 in prismatic face. Grazing-incidence X-ray diffraction analysis shows prominent reflection of (0 0 2) plane at basal and prismatic directions of boronated graphite. However, in both the wear tracks (1 1 0) plane become prominent and this transformation is induced by frictional energy. The structural transformation in wear tracks is supported by micro-Raman analysis which revealed that 3D phase of boronated graphite converted into a disordered 2D lattice structure. Thus, the structural aspect of disorder is similar in both the wear tracks and graphite transfer layers. Therefore, the crystallographic aspect is not adequate to explain anisotropic friction behavior. Results of X-ray photoelectron spectroscopy and Fourier transform infrared spectroscopy shows weak signature of oxygen complexes and functional groups in wear track of basal plane while these species dominate in prismatic direction. Abundance of these functional groups in prismatic plane indicates availability of chemically active sites tends to forming strong bonds between the sliding interfaces which eventually increases friction coefficient

  11. Novel oleanolic vinyl boronates: synthesis and antitumor activity.

    Science.gov (United States)

    Moreira, Vânia M; Salvador, Jorge A R; Simões, Sérgio; Destro, Federica; Gavioli, Riccardo

    2013-05-01

    A series of novel oleanane-type pentacyclic triterpenoids bearing a boronate ester moiety at C3 have been synthesized by palladium-catalyzed cross-coupling of bis(pinacolato)diboron with vinyl triflates, in the presence of base, and these compounds were fully characterized by 1D and 2D NMR techniques. Evaluation of their antiproliferative effects on a panel of hematological-based and solid tumor cell lines identified three active oleanolic vinyl boronates that inhibited the growth of leukemia (Jurkat, K562), Burkitt's lymphoma (Jijoye), cervix (Hela), colon (SW480), and ovary (SKOV-3) cancer cells without concomitant inhibition of non-tumoral human fibroblasts. Their mechanisms of action were investigated on the leukemia Jurkat cell line. The results show that the incorporation of boron in the oleanolic acid core combined with the presence of amide bonds afforded compounds with desirable biological effects such as apoptosis induction and inhibition of proteasomal activity on tumor cells, which makes them potential templates for further development in the anticancer drug setting. PMID:23455056

  12. An all-digital image synthesizer for countering high-resolution imaging radars

    OpenAIRE

    Ekestorm, Stig R.T.; Karow, Christopher

    2000-01-01

    The subject of this thesis is a digital image synthesizer (DIS), which is especially useful as a counter-targeting signal repeater, i.e., for synthesizing the characteristic echo signature of a pre-selected target. The DIS has a digital radio frequency memory (DRFM) and associated circuitry, including digital tapped delay lines and a modulator in each delay line to impose both amplitude and frequency modulation in each line. A unique property of the digital image synthesizer is its ability to...

  13. An all-digital image synthesizer for countering high-resolution imaging radars

    OpenAIRE

    Pace, Phillip E.; Ekestrom, S.; Karow, C.; Fouts, D.

    2000-01-01

    A digital image ssynthesizer (DIS), especially useful as a counter-targeting signal repeater, (i.e., for synthesizing the characteristic echo signature of a pre-selected target) is reported. The DIS has a digital radio frequency memory (DRFM) and associated circuitry, including digital tapped delay lines and a modulator in each delay line to impose both amplitude and frequency modulation in each line. A unique property of the digital image synthesizer is its ability to synthesize false targ...

  14. The Ω Counter, a Frequency Counter Based on the Linear Regression.

    Science.gov (United States)

    Rubiola, Enrico; Lenczner, Michel; Bourgeois, Pierre-Yves; Vernotte, Francois

    2016-07-01

    This paper introduces the Ω counter, a frequency counter-i.e., a frequency-to-digital converter-based on the linear regression (LR) algorithm on time stamps. We discuss the noise of the electronics. We derive the statistical properties of the Ω counter on rigorous mathematical basis, including the weighted measure and the frequency response. We describe an implementation based on a system on chip, under test in our laboratory, and we compare the Ω counter to the traditional Π and Λ counters. The LR exhibits the optimum rejection of white phase noise, superior to that of the Π and Λ counters. White noise is the major practical problem of wideband digital electronics, both in the instrument internal circuits and in the fast processes, which we may want to measure. With a measurement time τ , the variance is proportional to 1/τ(2) for the Π counter, and to 1/τ(3) for both the Λ and Ω counters. However, the Ω counter has the smallest possible variance, 1.25 dB smaller than that of the Λ counter. The Ω counter finds a natural application in the measurement of the parabolic variance, described in the companion article in this Journal [vol. 63 no. 4 pp. 611-623, April 2016 (Special Issue on the 50th Anniversary of the Allan Variance), DOI 10.1109/TUFFC.2015.2499325]. PMID:27244731

  15. The Omega Counter, a Frequency Counter Based on the Linear Regression

    CERN Document Server

    Rubiola, E; Bourgeois, P -Y; Vernotte, F

    2015-01-01

    This article introduces the {\\Omega} counter, a frequency counter -- or a frequency-to-digital converter, in a different jargon -- based on the Linear Regression (LR) algorithm on time stamps. We discuss the noise of the electronics. We derive the statistical properties of the {\\Omega} counter on rigorous mathematical basis, including the weighted measure and the frequency response. We describe an implementation based on a SoC, under test in our laboratory, and we compare the {\\Omega} counter to the traditional {\\Pi} and {\\Lambda} counters. The LR exhibits optimum rejection of white phase noise, superior to that of the {\\Pi} and {\\Lambda} counters. White noise is the major practical problem of wideband digital electronics, both in the instrument internal circuits and in the fast processes which we may want to measure. The {\\Omega} counter finds a natural application in the measurement of the Parabolic Variance, described in the companion article arXiv:1506.00687 [physics.data-an].

  16. Synthesis of boron nitride nanotubes by boron ink annealing.

    Science.gov (United States)

    Li, Lu Hua; Chen, Ying; Glushenkov, Alexey M

    2010-03-12

    Ball-milling and annealing is one effective method for the mass production of boron nitride nanotubes (BNNTs). We report that the method has been modified to a boron (B) ink annealing method. In this new process, the nanosize ball-milled B particles are mixed with metal nitrate in ethanol to form an ink-like solution, and then the ink is annealed in nitrogen-containing gas to form nanotubes. The new method greatly enhances the yield of BNNTs, giving a higher density of nanotubes. These improvements are caused by the addition of metal nitrate and ethanol, both of which can strongly boost the nitriding reaction, as revealed by thermogravimetric analysis. The size and structure of BNNTs can be controlled by varying the annealing conditions. This high-yield production of BNNTs in large quantities enables the large-scale application of BNNTs. PMID:20154372

  17. Synthesis of boron nitride nanotubes by boron ink annealing

    International Nuclear Information System (INIS)

    Ball-milling and annealing is one effective method for the mass production of boron nitride nanotubes (BNNTs). We report that the method has been modified to a boron (B) ink annealing method. In this new process, the nanosize ball-milled B particles are mixed with metal nitrate in ethanol to form an ink-like solution, and then the ink is annealed in nitrogen-containing gas to form nanotubes. The new method greatly enhances the yield of BNNTs, giving a higher density of nanotubes. These improvements are caused by the addition of metal nitrate and ethanol, both of which can strongly boost the nitriding reaction, as revealed by thermogravimetric analysis. The size and structure of BNNTs can be controlled by varying the annealing conditions. This high-yield production of BNNTs in large quantities enables the large-scale application of BNNTs.

  18. Over-the-Counter Medicines: What's Right for You?

    Science.gov (United States)

    ... counter medicine (OTCs) Over-the-Counter Medicines: What's Right for You? Share Tweet Linkedin Pin it More ... org Back to top More in Choosing the right over-the-counter medicine (OTCs) Resources for You ...

  19. The Principal and Staff Development: Countering the School Culture.

    Science.gov (United States)

    Martin, Mary; Rogus, Joseph F.

    1979-01-01

    After addressing the problems inherent in developing staff improvement programs, the author offers starter planning steps for countering the energy drainage of teachers, countering the weak technology of teaching, and countering the feeling of aloneness of the teacher. (KC)

  20. Synthesis of vinyl boronates from aldehydes by a practical boron-Wittig reaction.

    Science.gov (United States)

    Coombs, John R; Zhang, Liang; Morken, James P

    2015-04-01

    A highly stereoselective boron-Wittig reaction between stable and readily accessible 1,1-bis(pinacolboronates) and aldehydes furnishes a variety of synthetically useful di- and trisubstituted vinyl boronate esters. PMID:25799147

  1. Antibodies and antiestrogens combined with boron for use in the neutron capture therapy

    International Nuclear Information System (INIS)

    The ZR-75-1 cell line developed from a mammary carcinoma was chosen to characterise the binding of antiestrogen U23.469-M to the cell, which was subsequently compared to that of a derivative combined with boron. It was found that the original U23.469-M showed antiestrogenic activity, while this effect was largely abolished after the substance had been modified using b-decachloro-o-carborane. In this study, boron-conjugated antibodies were produced in order to find out whether those modified immunoglobulins would be suitable to bind sufficient quantities of boron to the tumour cells. It was calculated by experts on radiation biology that a minimum of 1000 boron atoms is required for a tumour-specific antibody to be therapeutically effective. When oxidated dextran of a molecular weight of 33 kD was used as a linking molecule, a reproducible method could be developed that permitted more than 1000 boron atoms to be bound per antibody. In one of the monoclonal antibodies tested here a combination with boron could, however, only be achieved at the expense of complete inactivation. A model was developed allowing to significantly increase the number modified antibodies attached to any one tumour cell. The cell binding experiments and radioimmunoassays then carried out were able to show that the number of antibodies bound to tumour cells can be increased to different degrees, depending on the monoclonal antibody used in each case. (orig./MG)

  2. Mechanical Effects of Hafnium and Boron Addition to Aluminum Alloy Films for Submicrometer LSI Interconnects

    Science.gov (United States)

    Onoda, Hiroshi; Takahashi, Eishi; Kawai, Yasuaki; Madokoro, Shoji; Fukuyo, Hideaki; Sawada, Susumu

    1993-11-01

    This is the first report on the mechanical properties of hafnium- and boron-added Al-Si-Cu alloy film for LSI interconnects. Two to three hundred ppm of hafnium and boron addition into Al-Si-Cu alloy film does not influence the Al alloy properties for metal lines as LSI interconnects, such as its low resistivity, low ohmic contact resistance with Si, and fine-line patterning feasibility. The mechanical properties of the Al alloy film, however, change greatly. Vertical hillock and lateral hillock formation is considerably suppressed during heat treatments used in LSI fabrication processes. Stress-induced void formation is also reduced during aging test at 125°C. These effects due to hafnium and boron addition are considered to be an impurity precipitation effect ihat was confirmed by X-ray diffraction analysis and electron probe microanalysis.

  3. Low energy recoil detection with a spherical proportional counter

    OpenAIRE

    I. Savvidis; Katsioulas, I.; Eleftheriadis, C.; Giomataris, I.; Papaevangellou, T.

    2016-01-01

    We present low energy recoil detection results in the keV energy region, from measurements performed with the Spherical Proportional Counter (SPC). An ${}^{241}Am-{}^{9}{Be}$ fast neutron source is used in order to obtain neutron-nucleus elastic scattering events inside the gaseous volume of the detector. The detector performance in the $keV$ energy region was resolved by observing the $5.9\\ keV$ line of a ${}^{55}Fe$ X-ray source, with energy resolution of $9\\%$ ($\\sigma$). The toolkit GEANT...

  4. Synthesis of Boron Nanowires, Nanotubes, and Nanosheets

    Directory of Open Access Journals (Sweden)

    Rajen B. Patel

    2015-01-01

    Full Text Available The synthesis of boron nanowires, nanotubes, and nanosheets using a thermal vapor deposition process is reported. This work confirms previous research and provides a new method capable of synthesizing boron nanomaterials. The materials were made by using various combinations of MgB2, Mg(BH42, MCM-41, NiB, and Fe wire. Unlike previously reported methods, a nanoparticle catalyst and a silicate substrate are not required for synthesis. Two types of boron nanowires, boron nanotubes, and boron nanosheets were made. Their morphology and chemical composition were determined through the use of scanning electron microscopy, transmission electron microscopy, and electron energy loss spectroscopy. These boron-based materials have potential for electronic and hydrogen storage applications.

  5. Analysis of magnetron sputtered boron oxide films

    Energy Technology Data Exchange (ETDEWEB)

    Buc, Dalibor [Slovak University of Technology in Bratislava (Slovakia); Bello, Igor [City University of Hong Kong, Kowloon, Hong Kong (China); Caplovicova, Maria [Comenius University in Bratislava (Slovakia); Mikula, Milan; Kovac, Jaroslav; Hotovy, Ivan [Slovak University of Technology in Bratislava (Slovakia); Chong, Yat Min [City University of Hong Kong, Kowloon, Hong Kong (China); Siu, Guei Gu [City University of Hong Kong, Kowloon, Hong Kong (China)], E-mail: apggsiu@cityu.edu.hk

    2007-10-15

    Boron oxide films were grown on silicon substrates by radio-frequency (rf) unbalanced magnetron sputtering of a boron target in argon-oxygen gas mixtures with different compositions. Microscopic analyses show that overall boron oxide films are amorphous. The film prepared at oxygen/argon flow rate ratio > 0.05 developed large crystallites of boric acid in localize areas of amorphous boron oxide matrices. These crystallites were unstable and at electron microscopic analysis they continuously transformed to a cubic HBO{sub 2} phase and then completely vanished leaving an underlying amorphous boron oxide film behind. The analyses indicate the coexistence of B{sub 6}O, HBO{sub 2} crystallites and amorphous boron oxide matrices. Fourier transform infrared (FTIR) spectra revealed spectral bands of BOH, BO, BOB and BH groups. Nanohardness and elastic modulus of a film prepared at low oxygen concentration approach 30 and 300 GPa, respectively. These parameters however vary with deposition conditions.

  6. Microwave sintering of boron carbide composites

    International Nuclear Information System (INIS)

    Boron carbide is an important ceramic material because of its high hardness and low specific gravity. it is used for applications involving impact and wear resistance. The disadvantages of boron carbide materials are difficulty in fabrication and sensitivity to brittle fracture. These problems are significantly reduced by production of cermets based on boron carbide and aluminum or aluminum alloys. Microwave heating of boron carbide materials results in ultrarapid heating and high temperatures. Therefore, a finer microstructure is obtained. The objective of this work was to define a technology that would allow the manufacture of boron carbide ceramics having mechanical properties similar to those exhibited by hot-pressed specimens. microwave heating would be used for the densification step. Mixtures of boron carbide and aluminum were considered for this research because aluminum simultaneously acts as a sintering aid and introduces phases that contribute to toughness enhancement

  7. Prediction of boron carbon nitrogen phase diagram

    Science.gov (United States)

    Yao, Sanxi; Zhang, Hantao; Widom, Michael

    We studied the phase diagram of boron, carbon and nitrogen, including the boron-carbon and boron-nitrogen binaries and the boron-carbon-nitrogen ternary. Based on the idea of electron counting and using a technique of mixing similar primitive cells, we constructed many ''electron precise'' structures. First principles calculation is performed on these structures, with either zero or high pressures. For the BN binary, our calculation confirms that a rhmobohedral phase can be stablized at high pressure, consistent with some experimental results. For the BCN ternary, a new ground state structure is discovered and an Ising-like phase transition is suggested. Moreover, we modeled BCN ternary phase diagram and show continuous solubility from boron carbide to the boron subnitride phase.

  8. GEIGER-MULLER TYPE COUNTER TUBE

    Science.gov (United States)

    Fowler, I.L.; Watt, L.A.K.

    1959-12-15

    A single counter tube capable of responding to a wide range of intensities is described. The counter tube comprises a tubular cathode and an anode extending centrally of the cathode. The spacing between the outer surface of the anode and the inner surface of the cathode is varied along the length of the tube to provide different counting volumes in adjacent portions of the tube. A large counting volume in one portion adjacent to a low-energy absorption window gives adequate sensitivity for measuring lowintensity radiation, while a smaller volume with close electrode spacing is provided in the counter to make possible measurement of intense garnma radiation fields.

  9. A new type of gas scintillation counter

    International Nuclear Information System (INIS)

    Design and construction of a new type of gas scintillation counter are discussed. It includes a scintillation gas proportional counter coupled to a photomultiplier. The electric field applied to the counter in the proportional region increases the number of photons resulting of the excitation of the inert gas, during the discharge produced by the passage of the primary ionizing particle. The number of initial photons is then increased and so is the impulse amplitude of the photomultiplier. The complexity of the electronic system necessary for the observation is thereby reduced. The influence of the electricfield on the resolution of the detector is especially emphasized. (I. C. R.)

  10. Note on the Typ. 2 counter problem

    International Nuclear Information System (INIS)

    The distribution function of the distance between two successive registered particles if the distribution function of the primary process, pulse distribution and the counter type and known is determined on the basis of the joint Laplace transform. The generating function of the number of particles arriving to the counting device during the dead time for the so-called Type 2 counter (counter with prolonging dead time) is determined toon some remarks on the registrations of m types of particles (m>= 1) are made

  11. CVD-produced boron filaments

    Science.gov (United States)

    Wawner, F. E.; Debolt, H. E.; Suplinskas, R. D.

    1980-01-01

    A technique for producing boron filaments with an average tensile strength of 6.89 GPa has been developed which involves longitudinal splitting of the filament and core (substrate) removal by etching. Splitting is accomplished by a pinch wheel device which continuously splits filaments in lengths of 3.0 m by applying a force to the side of the filament to create a crack which is then propagated along the axis by a gentle sliding action. To facilitate the splitting, a single 10 mil tungsten substrate is used instead of the usual 0.5 mil substrate. A solution of hot 30% hydrogen peroxide is used to remove the core without attacking the boron. An alternative technique is to alter the residual stress by heavily etching the filament. Average strengths in the 4.83-5.52 GPa range have been obtained by etching an 8 mil filament to 4 mil.

  12. Boron clusters in luminescent materials.

    Science.gov (United States)

    Mukherjee, Sanjoy; Thilagar, Pakkirisamy

    2016-01-21

    In recent times, luminescent materials with tunable emission properties have found applications in almost all aspects of modern material sciences. Any discussion on the recent developments in luminescent materials would be incomplete if one does not account for the versatile photophysical features of boron containing compounds. Apart from triarylboranes and tetra-coordinate borate dyes, luminescent materials consisting of boron clusters have also found immense interest in recent times. Recent studies have unveiled the opportunities hidden within boranes, carboranes and metalloboranes, etc. as active constituents of luminescent materials. From simple illustrations of luminescence, to advanced applications in LASERs, OLEDs and bioimaging, etc., the unique features of such compounds and their promising versatility have already been established. In this review, recent revelations about the excellent photophysical properties of such materials are discussed. PMID:26574714

  13. Microdosimetric spectra of the THOR neutron beam for boron neutron capture therapy

    International Nuclear Information System (INIS)

    A primary objective of the BNCT project in Taiwan, involving THOR (Tsing Hua Open Pool Reactor), was to examine the potential treatment of hepatoma. To characterise the epithermal neutron beam in THOR, the microdosimetry distributions in lineal energy were determined using paired tissue-equivalent proportional counters with and without boron microfoils. Microdosimetry results were obtained in free-air and at various depths in a PMMA phantom near the exit of the beam port. A biological weighting function, dependent on lineal energy, was used to estimate the relative biological effectiveness of the beam. An effective RBE of 2.7 was found at several depths in the phantom. (author)

  14. Conduction mechanism in boron carbide

    Science.gov (United States)

    Wood, C.; Emin, D.

    1984-01-01

    Electrical conductivity, Seebeck-coefficient, and Hall-effect measurements have been made on single-phase boron carbides, B(1-x)C(x), in the compositional range from 0.1 to 0.2 X, and between room temperature and 1273 K. The results indicate that the predominant conduction mechanism is small-polaron hopping between carbon atoms at geometrically inequivalent sites.

  15. Sintering behavior of boron carbide

    International Nuclear Information System (INIS)

    Pressureless sintering behavior of boron carbide (B4C) in argon was studied, with change in time and temperature, using carbon as sintering aid. Carbon was added via fenolic resin, acting also as a binder. After isostatic pressing the specimens were sintered in a graphite furnace at 19600C/1h, 21600C/15 minutes and 1h and 22000C/1h. The achieved density was 97% of the theoretical. Some mechanical properties and microstructural aspects have been evaluated. (author)

  16. Boron Enrichment in Martian Clay

    OpenAIRE

    James D Stephenson; Lydia J Hallis; Kazuhide Nagashima; Freeland, Stephen J.

    2013-01-01

    We have detected a concentration of boron in martian clay far in excess of that in any previously reported extra-terrestrial object. This enrichment indicates that the chemistry necessary for the formation of ribose, a key component of RNA, could have existed on Mars since the formation of early clay deposits, contemporary to the emergence of life on Earth. Given the greater similarity of Earth and Mars early in their geological history, and the extensive disruption of Earth's earliest minera...

  17. A Preliminary experimental study of the boron concentration in vapor and the isotopic A preliminary experimental study of the boron concentrationin vapor and the isotopic fractionation of boron betweenseawater and vapor during evaporation of seawater

    Institute of Scientific and Technical Information of China (English)

    XIAO; Yingkai

    2001-01-01

    [1]Gast, J. A., Thompson, T. G., Evaporation of boric acid from seawater, Tellus, 1959, 6: 344-347.[2]Nishimura, M., Tanaka, K., Seawater may not be a source of boron in the atmosphere, J. Geoph. Res., 1972, 77: 5239-5242.[3]Fogg, T. R., Duce, R. A., Fasching, J. L., Sampling and determination of boron in the atmosphere, Anal. Chem., 1983, 55:2179-2184.[4]Fogg, T. R., Duce, R. A., Boron in the troposphere: Distribution and fluxes, J. Geoph. Res., 1985, 90: 3781-3796.[5]Spivack, A. J., Berndt, M. E., Seyfreid, W. E., Boron isotope fractionation during supercritical phase separation, Geochim.Cosmochim. Acta, 1990, 54: 2337-2339.[6]Palmer, M. R., London, D., Morgan, G. B. et al., Experimental determination of fractionation of 11B/10B between tourma-line and aqueous vapor: A temperature and pressure-dependent isotopic system, Chem. Geol., 1992, 101:123-129.[7]Hervig, R. L., London, D., Morgan, G. B. et al., Large boron isotope fractionation between hydrous vapor and silicate meltat igneous temperatures, in the Seventh Annual V. M. Goldschmidt Conf., LPI Contribution No. 921, Houston: Lunar and Planetary Institute, 1997, 93-94.[8]Vengosh, A., Starinsky, A., Kolodny, Y. et al., Boron isotope variations during fractional evaporation of seawater: New constraints on the marine vs. nonmarine debate, Geology, 1992, 20: 799-802.[9]Zhang, X. P., Shi, Y. E, Yao, T. D., The variation characteristics of δo18O in precipitation in Northeastern Qing-Zhang Plateau, Science in China, Series B (in Chinese), 1995, 25(5): 540-547.[10]Yu, J. S., Yu, E J., Liu, D. P., The hydrogen and oxygen of isotopic compositions of meteoric water in the eastern part of China, Geochimica (in Chinese), 1987, (1): 22-26.[11]Xiao, Y. K., Xiao, Y., Swihart, G. H. et al., Separation of boron by ion exchange with boron specific resin, Acta Geosci.Sinica (in Chinese), 1997, 18: 286-289.[12]Kiss, E., Ion-exchange separation and spectrophotometric determination of

  18. Boron removal from geothermal waters by electrocoagulation

    International Nuclear Information System (INIS)

    Most of the geothermal waters in Turkey contain extremely high concentration of boron when they are used for irrigation. The use of geothermal waters for irrigation can results in excess amount deposition of boron in soil. On the other hand, a minimal boron concentration is required for irrigational waters. In this study, electrocoagulation (EC) was selected as a treatment process for the removal of boron from thermal waters obtained from Ilica-Erzurum in Turkey. Current density (CD), pH of solution and temperature of solution were selected as operational parameters. The results showed that boron removal efficiency increased from pH 4.0 to 8.0 and decreased at pH 10.0. Although boron removal efficiency was highest at pH 8.0, energy consumption was very high at this pH value compared to other pH intervals. Boron removal efficiency reached to 95% with increasing current density from 1.5 to 6.0 mA/cm2, but energy consumption was also increased in this interval. At higher temperatures of solution, such as 313 and 333 K, boron removal efficiency increased. At optimum conditions, boron removal efficiency in geothermal water reached up to 95%

  19. Boron removal from geothermal waters by electrocoagulation

    Energy Technology Data Exchange (ETDEWEB)

    Yilmaz, A. Erdem [Atatuerk University, Faculty of Engineering, Department of Environmental Engineering., 25240 Erzurum (Turkey)], E-mail: aerdemy@atauni.edu.tr; Boncukcuoglu, Recep [Atatuerk University, Faculty of Engineering, Department of Environmental Engineering., 25240 Erzurum (Turkey); Kocakerim, M. Muhtar [Atatuerk University, Faculty of Engineering, Department of Chemical Engineering, 25240 Erzurum (Turkey); Yilmaz, M. Tolga; Paluluoglu, Cihan [Atatuerk University, Faculty of Engineering, Department of Environmental Engineering., 25240 Erzurum (Turkey)

    2008-05-01

    Most of the geothermal waters in Turkey contain extremely high concentration of boron when they are used for irrigation. The use of geothermal waters for irrigation can results in excess amount deposition of boron in soil. On the other hand, a minimal boron concentration is required for irrigational waters. In this study, electrocoagulation (EC) was selected as a treatment process for the removal of boron from thermal waters obtained from Ilica-Erzurum in Turkey. Current density (CD), pH of solution and temperature of solution were selected as operational parameters. The results showed that boron removal efficiency increased from pH 4.0 to 8.0 and decreased at pH 10.0. Although boron removal efficiency was highest at pH 8.0, energy consumption was very high at this pH value compared to other pH intervals. Boron removal efficiency reached to 95% with increasing current density from 1.5 to 6.0 mA/cm{sup 2}, but energy consumption was also increased in this interval. At higher temperatures of solution, such as 313 and 333 K, boron removal efficiency increased. At optimum conditions, boron removal efficiency in geothermal water reached up to 95%.

  20. Boron deposition from fused salts. Final report

    International Nuclear Information System (INIS)

    A partial evaluation of the feasibility of a process to electrodeposit pure coherent coatings of elemental boron from molten fluorides has been performed. The deposit produced was powdery and acicular, unless the fluoride melt was purified to have very low oxygen concentration. When the oxygen activity was reduced in the melt by addition of crystalline elemental boron, dense, amorphous boron deposit was produced. The boron deposits produced had cracks but were otherwise pure and dense and ranged up to 0.35 mm thick. Information derived during this project suggests that similar deposits might be obtained crack-free up to 1.00 mm thick by process modifications and improvements

  1. Stable isotope ratio mass spectrometry of nanogram quantities of boron and sulfur

    Science.gov (United States)

    Wieser, Michael Eugene

    1998-09-01

    Instrumentation and analytical techniques were developed to measure isotope abundances from nanograms of sulfur and boron. Sulfur isotope compositions were determined employing continuous flow isotope ratio mass spectroscopy (CF-IRMS) procedures and AsS+ thermal ionization mass spectrometry techniques (AsS+-TIMS). Boron isotope abundances were determined by BO2/sp--TIMS. CF-IRMS measurements realized δ34S values from 10 μg sulfur with precisions of ±0.3/perthous. To extend sulfur isotope measurements to much smaller samples, a TIMS procedure was developed to measure 75As32S+ and 75As34S+ at masses 108 and 109 from 200 ng S on a Finnigan MAT 262 with an ion counter. This is possibly the smallest amount of sulfur which has been successfully analyzed isotopically. The internal precision of 32S/34S ratios measured by AsS+-TIMS was better than ±0.15 percent. δ34S-values calculated relative to the measured 32S/34S value of an IAEA AG2S standard (S-1) agreed with those determined by CF-IRMS to within ±3/perthous. The increasing sensitivity of S-isotope analyses permits hiterto impossible investigations e.g. sulfur in tree rings and ice cores. Boron isotope abundances were measured as BO2/sp- from 50 ng B using an older thermal ionization mass spectrometer which had been extensively upgraded including the addition of computer control electronics, sensitive ion current amplification and fiber optic data bus. The internal precisions of the measured 11B/10B ratios were ±0.15 percent and the precisions of δ11B values calculated relative to the accepted international standard (SRM-951) were ±3/perthous. Two applications of boron isotope abundance variations were initiated (1) ground waters of Northern Alberta and (2) coffee beans in different regions of the world. In the first it was demonstrated that boron isotopes could be used to trace boron released during steam injection of oil sands into the surrounding environment. Data from the second study suggest that boron

  2. Position sensitive counter development at the linac

    International Nuclear Information System (INIS)

    In a novel application of the multiwire proportional counter we have imaged a collimated neutron beam. Although preliminary, the results are of sufficient import to be described here because of the potential wide application of the multiwire proportional counter to Laboratory problems. The counter was operated with a counting gas pressure of 20 Torr; the counting gas was pure C4H10. The radiator was a 235U foil. Under these conditions, the counter is (1) relatively insensitive to charged particles (other than fission fragments), (2) insensitive to γ-radiation, and (3) has an efficiency for the detection of fission fragments independent of incident neutron energy over a wide range of neutron energies

  3. Development of a Mobile Ice Nucleus Counter

    Energy Technology Data Exchange (ETDEWEB)

    Kok, Gregory; Kulkarni, Gourihar

    2014-07-10

    An ice nucleus counter has been constructed. The instrument uses built-in refrigeration systems for wall cooling. A cascade refrigeration system will allow the cold wall to operate as low as -70 deg C, and a single stage system can operate the warm wall at -45 deg C. A unique optical particle counter has been constructed using polarization detection of the scattered light. This allows differentiation of the particles exiting the chamber to determine if they are ice or liquid.

  4. Counter public spheres and global modernity

    OpenAIRE

    Fenton, Natalie; Downey, John

    2015-01-01

    This article explores the concept of counter public spheres and their relationship to the dominant public sphere. We argue that counter public spheres are increasingly relevant due to particular social and political configurations that mark out a distinct stage of modernity. We suggest that this stage is characterised in particular by the intensification of globalisation, the rise of neo-liberalism and a decline of trust and social democracy resulting in instability in the dominant public sph...

  5. Counter public spheres and global modernity:

    OpenAIRE

    Downey, John; Fenton, Natalie

    2003-01-01

    This article explores the concept of counter public spheres and their relationship to the dominant public sphere. We argue that counter public spheres are increasingly relevant due to particular social and political configurations that mark out a distinct stage of modernity. We suggest that this stage is characterised in particular by the intensification of globalisation, the rise of neo-liberalism and a decline of trust and social democracy resulting in instability in the dominant public sph...

  6. Synchronization in counter-rotating oscillators

    OpenAIRE

    Bhowmick, S. K.; Ghosh, Dibakar; Dana, Syamal K.

    2011-01-01

    An oscillatory system can have clockwise and anticlockwise senses of rotation. We propose a general rule how to obtain counter-rotating oscillators from the definition of a dynamical system and then investigate synchronization. A type of mixed synchronization emerges in counter-rotating oscillators under diffusive scalar coupling when complete synchronization and antisynchronization coexist in different state variables. Stability conditions of mixed synchronization are obtained analytically i...

  7. Enantiomeric Separations using Chiral Counter-Ions

    OpenAIRE

    Haglöf, Jakob

    2010-01-01

    This thesis describes the use of chiral counter-ions for the enantiomeric separation of amines in non-aqueous capillary electrophoresis. The investigations have been concentrated on studies of the influence, of the chiral counter-ion, the solvent, the electrolyte and the analyte, on the enantioselective separation. Modified divalent dipeptides have been introduced in capillary electrophoresis for the separation of amino alcohols and chiral resolution of amines. Association constants for the i...

  8. Comparison of Heating Efficiency Between Co and Counter Neutral Beam injection in Large Helical Device

    Science.gov (United States)

    Ikeda, Katsunori; Kaneko, Osamu; Osakabe, Masaki; Takeiri, Yasuhiko; Tsumori, Katsuyoshi; Oka, Yoshihide; Murakami, Sadayoshi; Narihara, Kazumichi; Asano, Eiji E.; Kawamoto, Toshikazu; LHD Experiment Groups Team

    2001-10-01

    In the Large Helical Device, tangential neutral beam injection (NBI) is adopted in order to avoid that the fast ions are directly trapped in helical ripples. Then effective heating is realized by negative ion based high energy tangential NBI systems in Large Helical Device, two beam lines ware arranged counter -injection and the other one was arranged co-injection. However, it is predicted that the absorption efficiency of a NBI heating is also influenced by troidal drift motion of injected beam particle in weak magnetic field (Bt < 1T) operations such as high beta experiment. And also plasmas must be build up by using tangential NBI heating alone from the magnetic field strength Bt 0.5T to 1.5T, since heating by electron cyclotron heating can not be performed. So, the efficiency of co and counter NBI heating is an important issue for generating high beta plasma. According to experiment results, either of co and counter NBI was able to heat plasma efficiently in Bt=0.75T. Enhancement factors of energy confinement time without considering direct drift loss is almost the same in these plasmas. However, there is a difference in build up time of plasma by co and counter. There are no big difference in an electron temperature profile of co and counter heating as low as Bt=0.75 although the beam absorption profile may be different between co and counter injection.

  9. Method for determination of boron carbide in wurtzite-like boron nitride

    International Nuclear Information System (INIS)

    A technique for increase of sensitivity and analysis accuracy while boron carbide determination in wurtzite-like boron nitride is proposed. Boron nitride with an addition of boron carbide is bjected to treatment by the mixture of concentrated sulphuric acid and 0.1-0.5 N of porassium bichromate solution at ratio of (2-1):1 at the temperature of mixture boiling. Boron carboide content is calculated according to the quantity of restored Cr(3+), which is determined by titration of Cr(6+) excess with the Mohr's salt solution

  10. Boron coating on boron nitride coated nuclear fuels by chemical vapor deposition

    Energy Technology Data Exchange (ETDEWEB)

    Durmazucar, Hasan H.; Guenduez, Guengoer E-mail: ggunduz@metu.edu.tr

    2000-12-01

    Uranium dioxide-only and uranium dioxide-gadolinium oxide (5% and 10%) ceramic nuclear fuel pellets which were already coated with boron nitride were coated with thin boron layer by chemical vapor deposition to increase the burn-up efficiency of the fuel during reactor operation. Coating was accomplished from the reaction of boron trichloride with hydrogen at 1250 K in a tube furnace, and then sintering at 1400 and 1525 K. The deposited boron was identified by infrared spectrum. The morphology of the coating was studied by using scanning electron microscope. The plate, grainy and string (fiber)-like boron structures were observed.

  11. Boron coating on boron nitride coated nuclear fuels by chemical vapor deposition

    International Nuclear Information System (INIS)

    Uranium dioxide-only and uranium dioxide-gadolinium oxide (5% and 10%) ceramic nuclear fuel pellets which were already coated with boron nitride were coated with thin boron layer by chemical vapor deposition to increase the burn-up efficiency of the fuel during reactor operation. Coating was accomplished from the reaction of boron trichloride with hydrogen at 1250 K in a tube furnace, and then sintering at 1400 and 1525 K. The deposited boron was identified by infrared spectrum. The morphology of the coating was studied by using scanning electron microscope. The plate, grainy and string (fiber)-like boron structures were observed

  12. Nanodefects in ultrahard crystalline cubic boron nitride

    International Nuclear Information System (INIS)

    Cubic boron nitride (cBN), the second hardest known material after diamond, exhibits high thermal conductivity and an excellent ability to be n or p doped, which makes it a strong candidate for the next generation of high-temperature micro optical and micro electronic devices. According to recent studies, cBN exhibits a better resistance to radiation damage than diamond, which suggests potential applications in extreme radiation environments. Crystalline cBN powders of up to 0.5 mm linear size is obtained in a similar way as diamond, by catalytic conversion of hexagonal BN (hBN) to cBN at even higher pressures (> 5GPa) and temperatures (∼ 1900 K). Considering the essential role played by the nanodefects (point defects and impurities) in determining its physical properties, it is surprising how limited is the amount of published data concerning the properties of nanodefects in this material, especially by Electron Paramagnetic Resonance (EPR) spectroscopy, the most powerful method for identification and characterization of nanodefects in both insulators and semiconductors. This seems to be due mainly to the absence of natural cBN gems and the extreme difficulties in producing even mm3 sized synthetic crystals. We shall present our recent EPR studies on cBN crystalline powders, performed in a broad temperature range from room temperature (RT) down to 1.2 K on several sorts of large size cBN powder grits of yellow and amber color for industrial applications. Previous multifrequency (9.3 GHz and 95 GHz) EPR studies of brown to black cBN crystallites prepared with excess of boron, resulted in the discovery of two new types of paramagnetic point defects with different spectral properties, called the D1 and D2 centers. Our X(9.3 GHz)-band EPR investigations resulted in the observation in amber cBN crystalline powders of a spectrum with a strong temperature dependence of the lineshape. It was found that for high and low temperatures, respectively, the numerical

  13. Some physical properties of compacted specimens of highly dispersed boron carbide and boron suboxide

    International Nuclear Information System (INIS)

    Structure, shear modulus and internal friction (IF) of compacted specimens of boron carbide and boron suboxide have been investigated. Microtwins and stacking faults were observed along the {100} plane systems of polycrystalline specimens of boron carbide. Electrical conductivity of the specimens was that of p-type. Concentration of holes varied from 1017 to 1019 cm-3. The IF was measured in the temperature range 80-300 K. It was shown that the IF of boron carbide and that of boron suboxide were characterized with a set of similar relaxation processes. Mechanisms of the relaxation processes in boron carbide and boron suboxide are discussed in terms of the Hasiguti model of interaction between dislocations and point defects

  14. Boron carbide synthesis by carbothermic reduction of boron oxide

    International Nuclear Information System (INIS)

    Boron carbide (B4C) is a ceramic material of technological applications due to its extreme hardness and high chemical as well as thermal stability. Some parameters of the process for obtaining B4C by carbothermic reduction of B2O3 have been determined. The starting powders and the final products have been analysed by chemical, spectrographic and X-ray diffraction methods. The results show that the B4C obtained by the carbothermic reduction process is suitable for applications with a definite determination of the free carbon content. (author)

  15. Application of the boron neutron capture therapy to undifferentiated thyroid cancer using two boron compounds (BPA and BOPP)

    International Nuclear Information System (INIS)

    We have shown the selective uptake of boronophenylalanine (BPA) by undifferentiated thyroid cancer (UTC) human cell line ARO, both in vitro and in vivo. Moreover, a 50% histologic cure of mice bearing the tumor was observed when the complete boron neutron capture therapy was applied. More recently we have analyzed the biodistribution of BOPP (tetrakis-carborane carboxylate ester of 2,4-bis-(ba-dihydroxyethyl)-deutero-porphyrin IX) and showed that when BOPP was injected 5 days before BPA, and the animals were sacrificed 60 min after the ip injection of BPA, a significant increase in boron uptake by the tumor was found (38-45ppm with both compounds Vs. 20 ppm with BPA alone). Five days post the ip BOPP injection and 1 hr after BPA, the ratios were: tumor/blood 3,75; tumor /distal skin 2. Other important ratios were tumor/thyroid 6,65 and tumor/lung 3,8. The present studies were performed in mice transplanted with ARO cells and injected with BOPP and BPA. Only in mice treated with the neutron beam and injected with the boronated compounds we observed a 100% control of tumor growth. Two groups of mice received different total absorbed doses: 3.00 and 6.01 Gy, but no further improvement in the outcome was found compared to the previous results using BPA alone (4.3 Gy). (author)

  16. Study of boron detection limit using the in-air PIGE set-up at LAMFI-USP

    Science.gov (United States)

    Moro, M. V.; Silva, T. F.; Trindade, G. F.; Added, N.; Tabacniks, M. H.

    2014-11-01

    The quantification of small amounts of boron in materials is of extreme importance in different areas of materials science. Boron is an important contaminant and also a silicon dopant in the semiconductor industry. Boron is also extensively used in nuclear power plants, either for neutron shielding or for safety control and boron is an essential nutrient for life, either vegetable or animal. The production of silicon solar cells, by refining metallurgical-grade silicon (MG-Si) requires the control and reduction of several silicon contaminants to very low concentration levels. Boron is one of the contaminants of solar-grade silicon (SG-Si) that must be controlled and quantified at sub-ppm levels. In the metallurgical purification, boron quantification is usually made by Inductive Coupled Plasma Mass Spectrometry, (ICP-MS) but the results need to be verified by an independent analytical method. In this work we present the results of the analysis of silicon samples by Particle Induced Gamma-Ray Emission (PIGE) aiming the quantification of low concentrations of boron. PIGE analysis was carried out using the in-air external beam line of the Laboratory for Materials Analysis with Ion Beans (LAMFI-USP) by the 10B ( p ,αγ(7Be nuclear reaction, and measuring the 429 keV γ-ray. The in-air PIGE measurements at LAMFI have a quantification limit of the order of 1016 at/cm2.

  17. Possible toxicity of boron on sugar cane

    Energy Technology Data Exchange (ETDEWEB)

    Bravo C., M.

    Analyses of necrotic and green leaf tissues from sugar cane grown in the Tambo Valley (Arequipa, Peru) have shown that the boron concentration in necrotic tissue (average 657.7 ppm) is several times higher than that in the green tissue (average 55.7 ppm). This suggests that the necrosis may be due to boron toxicity.

  18. New techniques for producing thin boron films

    International Nuclear Information System (INIS)

    A review will be presented of methods for producing thin boron films using an electron gun. Previous papers have had the problem of spattering of the boron source during the evaporation. Methods for reducing this problem will also be presented. 12 refs., 4 figs

  19. Fabrication of boron-phosphide neutron detectors

    International Nuclear Information System (INIS)

    Boron phosphide is a potentially viable candidate for high neutron flux neutron detectors. The authors have explored chemical vapor deposition methods to produce such detectors and have not been able to produce good boron phosphide coatings on silicon carbide substrates. However, semi-conducting quality films have been produced. Further testing is required

  20. Computational Evidence for the Smallest Boron Nanotube

    Institute of Scientific and Technical Information of China (English)

    Xian Jie LIN; Dong Ju ZHANG; Cheng Bu LIU

    2006-01-01

    The structure of boron nanotubes (BNTs) was found not to be limited to hexagonal pyramidal structures. Based on density functional theory calculations we provided evidence for the smallest boron nanotube, a geometrical analog of the corresponding carbon nanotube. As shown by our calculations, the smallest BNT possesses highly structural, dynamical, and thermal stability, which should be interest for attempts at its synthesis.

  1. Boron carbide whiskers produced by vapor deposition

    Science.gov (United States)

    1965-01-01

    Boron carbide whiskers have an excellent combination of properties for use as a reinforcement material. They are produced by vaporizing boron carbide powder and condensing the vapors on a substrate. Certain catalysts promote the growth rate and size of the whiskers.

  2. Boron Carbides As Thermo-electric Materials

    Science.gov (United States)

    Wood, Charles

    1988-01-01

    Report reviews recent theoretical and experimental research on thermoelectric materials. Recent work with narrow-band semiconductors demonstrated possibility of relatively high thermoelectric energy-conversion efficiencies in materials withstanding high temperatures needed to attain such efficiencies. Among promising semiconductors are boron-rich borides, especially boron carbides.

  3. Nuclear fuel management and boron carbide coating

    International Nuclear Information System (INIS)

    In recent years one way of introducing burnable absorber is to coat the fuel pellets by a thin layer of burnable absorber so called integral fuel burnable absorber (IFBA). In this method the fuel is coated with boron nitride or boron carbide. Boron has low absorption cross-section and when it exists on the surface of the fuel, it interacts with thermalized neutron. B4C is a boron compound, which can be used for coating the nuclear fuel. It has high thermal stability and withstands high pressure and temperatures. High technology product of boron carbide has different ratio of B: C. But in nuclear reactor when boron carbide is used, it must be rich with boron. In this research chemical vapor decomposition (CVD) has been using boron trichloride and carbon tetra chloride for reactant materials. The experiments were carried out at high temperatures (1050 degree Celsius, 1225 degree Celsius and 1325 degree Celsius). The coated samples were analyzed using X-Ray diffractometer (XRD), scanning electron microscopy (SEM) and will be presented in this paper. It was seen that decreasing the reaction temperature caused an increase on the quality and thickness of the coating

  4. Study of the response of a lithium yttrium borate scintillator based neutron rem counter by Monte Carlo radiation transport simulations

    Science.gov (United States)

    Sunil, C.; Tyagi, Mohit; Biju, K.; Shanbhag, A. A.; Bandyopadhyay, T.

    2015-12-01

    The scarcity and the high cost of 3He has spurred the use of various detectors for neutron monitoring. A new lithium yttrium borate scintillator developed in BARC has been studied for its use in a neutron rem counter. The scintillator is made of natural lithium and boron, and the yield of reaction products that will generate a signal in a real time detector has been studied by FLUKA Monte Carlo radiation transport code. A 2 cm lead introduced to enhance the gamma rejection shows no appreciable change in the shape of the fluence response or in the yield of reaction products. The fluence response when normalized at the average energy of an Am-Be neutron source shows promise of being used as rem counter.

  5. XPS analysis of boron doped heterofullerenes

    Energy Technology Data Exchange (ETDEWEB)

    Schnyder, B.; Koetz, R. [Paul Scherrer Inst. (PSI), Villigen (Switzerland); Muhr, H.J.; Nesper, R. [ETH Zurich, Zurich (Switzerland)

    1997-06-01

    Boron heterofullerenes were generated through arc-evaporation of doped graphite rods in a helium atmosphere. According to mass spectrometric analysis only mono-substituted fullerenes like C{sub 59}B, C{sub 69}B and higher homologues together with a large fraction of higher undoped fullerenes were extracted and enriched when pyridine was used as the solvent. XPS analysis of the extracts indicated the presence of two boron species with significantly different binding energies. One peak was assigned to borid acid. The second one corresponds to boron in the fullerene cage, which is mainly C{sub 59}B, according to the mass spectrum. This boron is in a somewhat higher oxidation state than that of ordinary boron-carbon compounds. The reported synthesis and extraction procedure opens a viable route for production of macroscopic amounts of these compounds. (author) 2 figs., 1 tab., 7 refs.

  6. Stabilization of boron carbide via silicon doping.

    Science.gov (United States)

    Proctor, J E; Bhakhri, V; Hao, R; Prior, T J; Scheler, T; Gregoryanz, E; Chhowalla, M; Giulani, F

    2015-01-14

    Boron carbide is one of the lightest and hardest ceramics, but its applications are limited by its poor stability against a partial phase separation into separate boron and carbon. Phase separation is observed under high non-hydrostatic stress (both static and dynamic), resulting in amorphization. The phase separation is thought to occur in just one of the many naturally occurring polytypes in the material, and this raises the possibility of doping the boron carbide to eliminate this polytype. In this work, we have synthesized boron carbide doped with silicon. We have conducted a series of characterizations (transmission electron microscopy, scanning electron microscopy, Raman spectroscopy and x-ray diffraction) on pure and silicon-doped boron carbide following static compression to 50 GPa non-hydrostatic pressure. We find that the level of amorphization under static non-hydrostatic pressure is drastically reduced by the silicon doping. PMID:25427850

  7. Stabilization of boron carbide via silicon doping

    Science.gov (United States)

    Proctor, J. E.; Bhakhri, V.; Hao, R.; Prior, T. J.; Scheler, T.; Gregoryanz, E.; Chhowalla, M.; Giulani, F.

    2015-01-01

    Boron carbide is one of the lightest and hardest ceramics, but its applications are limited by its poor stability against a partial phase separation into separate boron and carbon. Phase separation is observed under high non-hydrostatic stress (both static and dynamic), resulting in amorphization. The phase separation is thought to occur in just one of the many naturally occurring polytypes in the material, and this raises the possibility of doping the boron carbide to eliminate this polytype. In this work, we have synthesized boron carbide doped with silicon. We have conducted a series of characterizations (transmission electron microscopy, scanning electron microscopy, Raman spectroscopy and x-ray diffraction) on pure and silicon-doped boron carbide following static compression to 50 GPa non-hydrostatic pressure. We find that the level of amorphization under static non-hydrostatic pressure is drastically reduced by the silicon doping.

  8. Counter-ions between or at asymmetrically charged walls: 2D free-fermion point

    OpenAIRE

    Samaj, L.; Trizac, E.

    2014-01-01

    This work contributes to the problem of determining effective interaction between asymmetrically (likely or oppositely) charged objects whose total charge is neutralized by mobile pointlike counter-ions of the same charge, the whole system being in thermal equilibrium. The problem is formulated in two spatial dimensions with logarithmic Coulomb interactions. The charged objects correspond to two parallel lines at distance d, with fixed line charge densities. Two versions of the model are cons...

  9. Burnup performances of boron nitride and boron coated nuclear fuels

    International Nuclear Information System (INIS)

    The nuclear fuels of urania (UOV) and 5% and 10% gadolinia (Gd2O3) containing UO2 previously produced by sol-gel technique were coated with first boron nitride (BN) then boron (B) thin layer by chemical vapor deposition (CVD) and also by plasma enhanced chemical vapor deposition (PECVD) techniques to increase the fuel cycle length and to improve the physical properties. From the cross-sectional view of BN and B layers taken from scanning electron microscope (SEM), the excellent adherence of BN onto fuel and B onto BN layer was observed in both cases. The behavior of fuel burnup, depletion of BN and B, the effect of coating thickness and also Gd2O3 content on the burnup performances of the fuels were identified by using the code WIMS-D/4 for Pressurized Water Reactor (PWR) and Boiling Water Reactor (BWR) cores. The optimum thickness ratio of B to BN was found as 4 and their thicknesses were chosen as 40 mm and 10 mm respectively in both reactor types to get extended cycle length. The assemblies consisting of fuels with 5% Gd2O3 and also coated with 10 mm BN and 40 mm B layers were determined as candidates for getting higher burnup in both types of reactors

  10. Boron enrichment in martian clay.

    Directory of Open Access Journals (Sweden)

    James D Stephenson

    Full Text Available We have detected a concentration of boron in martian clay far in excess of that in any previously reported extra-terrestrial object. This enrichment indicates that the chemistry necessary for the formation of ribose, a key component of RNA, could have existed on Mars since the formation of early clay deposits, contemporary to the emergence of life on Earth. Given the greater similarity of Earth and Mars early in their geological history, and the extensive disruption of Earth's earliest mineralogy by plate tectonics, we suggest that the conditions for prebiotic ribose synthesis may be better understood by further Mars exploration.

  11. Boron enrichment in martian clay.

    Science.gov (United States)

    Stephenson, James D; Hallis, Lydia J; Nagashima, Kazuhide; Freeland, Stephen J

    2013-01-01

    We have detected a concentration of boron in martian clay far in excess of that in any previously reported extra-terrestrial object. This enrichment indicates that the chemistry necessary for the formation of ribose, a key component of RNA, could have existed on Mars since the formation of early clay deposits, contemporary to the emergence of life on Earth. Given the greater similarity of Earth and Mars early in their geological history, and the extensive disruption of Earth's earliest mineralogy by plate tectonics, we suggest that the conditions for prebiotic ribose synthesis may be better understood by further Mars exploration. PMID:23762242

  12. Acid dissolution of soils and rocks for the determination of boron by inductively coupled plasma atomic emission spectrometry

    International Nuclear Information System (INIS)

    The boron concentration in rocks, soils and standard reference materials was determined using hydrofluoric acid-aqua regia dissolution followed by inductively coupled plasma atomic emission spectrometry (ICP-AES) using the B 1 249.773 -nm line, corrected for spectral interference by iron. An excess of fluoride was complexed with aluminium to release boron from the stable fluoroborate ion and to protect the borosilicate and quartz components of the instrument. Boron was not lost by volatilisation during volume reduction. Soil and rock boron values determined using the recommended dissolution procedures were comparable to those obtained using the accepted sodium carbonate fusion procedure and by d.c. arc emission spectrophotometry, and those for standard reference materials showed good agreement and precision with the literature values. (author)

  13. The use of polycarbonate in proportional counters

    International Nuclear Information System (INIS)

    Proportional counters are relatively sensitive to contamination through outgassing and the range of electrical insulators suitable for use in their manufacture is quite limited. Although small amounts of plastics such as polychlorotrifluoroethylene have been used as feedthroughs, ceramics are most commonly used when sealed counters with long lives are required. Ceramics have poor and widely scattered mechanical properties and the use of a more robust material is often highly desirable. Of particular interest is the use of polymers and this work examines polycarbonate in particular. To investigate its suitability in terms of outgassing a simple cylindrical, single anode proportional counter containing a large sample of polycarbonate was baked at ∼100 degree C and filled with a CO2/Ar/Xe mixture (5:47.5:47.5 by pressure, respectively). Subsequent measurements of the counter indicated an increase in gain, which, after a second similar filling, was identified to be associated with a preferential loss of CO2 to the polycarbonate. The consequences of this result and the circumstances under which polycarbonate could be used on a large scale in the construction of proportional counters are discussed

  14. Fabrication and characterization of boron-doped nanocrystalline diamond-coated MEMS probes

    Science.gov (United States)

    Bogdanowicz, Robert; Sobaszek, Michał; Ficek, Mateusz; Kopiec, Daniel; Moczała, Magdalena; Orłowska, Karolina; Sawczak, Mirosław; Gotszalk, Teodor

    2016-04-01

    Fabrication processes of thin boron-doped nanocrystalline diamond (B-NCD) films on silicon-based micro- and nano-electromechanical structures have been investigated. B-NCD films were deposited using microwave plasma assisted chemical vapour deposition method. The variation in B-NCD morphology, structure and optical parameters was particularly investigated. The use of truncated cone-shaped substrate holder enabled to grow thin fully encapsulated nanocrystalline diamond film with a thickness of approx. 60 nm and RMS roughness of 17 nm. Raman spectra present the typical boron-doped nanocrystalline diamond line recorded at 1148 cm-1. Moreover, the change in mechanical parameters of silicon cantilevers over-coated with boron-doped diamond films was investigated with laser vibrometer. The increase of resonance to frequency of over-coated cantilever is attributed to the change in spring constant caused by B-NCD coating. Topography and electrical parameters of boron-doped diamond films were investigated by tapping mode AFM and electrical mode of AFM-Kelvin probe force microscopy (KPFM). The crystallite-grain size was recorded at 153 and 238 nm for boron-doped film and undoped, respectively. Based on the contact potential difference data from the KPFM measurements, the work function of diamond layers was estimated. For the undoped diamond films, average CPD of 650 mV and for boron-doped layer 155 mV were achieved. Based on CPD values, the values of work functions were calculated as 4.65 and 5.15 eV for doped and undoped diamond film, respectively. Boron doping increases the carrier density and the conductivity of the material and, consequently, the Fermi level.

  15. Experimental boron neutron capture therapy for melanoma: Systemic delivery of boron to melanotic and amelanotic melanoma

    International Nuclear Information System (INIS)

    The boron-containing melanin precursor analogue p-boronophenylalanine (BPA) has previously been shown to selectively deliver boron to pigmented murine melanomas when administered in a single intragastric dose. If boron neutron capture therapy is to become a clinically useful method of radiation therapy for human malignant melanoma, the boron carrier must be capable of delivering useful amounts of boron to remote tumor sites (metastases) and to poorly pigmented melanomas. The authors have now determined the ability of BPA to accumulate in several nonpigmented melanoma models including human melanoma xenografts in nude mice. The absolute amount of boron in the nonpigmented melanomas was about 50% of the observed in the pigmented counterparts but was still selectively concentrated in the tumor relative to normal tissues in amounts sufficient for effective neutron capture therapy. Single intragastric doses of BPA resulted in selective localization of boron in the amelanotic Greene melanoma carried in the anterior chamber of the rabbit eye and in a pigmented murine melanoma growing in the lungs. The ratio of the boron concentration in these tumors to the boron concentration in the immediately adjacent normal tissue was in the range of 3:1 to 4:1. These distribution studies support the proposal that boron neutron capture therapy may be useful as a regional therapy for malignant melanoma

  16. CORNELL: CLEO's counters

    International Nuclear Information System (INIS)

    Particle identification by measuring ionization is complicated by the fact that the energy lost to ionization in passing through matter has large fluctuations, first calculated by Landau. These large fluctuations imply that many measurements must be made in order to determine the most probable ionization value that is characteristic of the particle type. The JADE chamber at PETRA and the TPC chamber at PEP measure both the ionization and the momenta of tracks in the same device. In the CLEO experiment at Cornell's CESR ring, ionization is measured in dedicated energy loss counters contained in each of the eight octants surrounding the drift chamber and superconducting coil. The last of these were installed in the summer of 1981, replacing Cherenkov counters that were used while the energy loss counters were being developed and built

  17. Educational cosmic ray experiments with Geiger counters

    CERN Document Server

    Blanco, F; Rocca, P L; Librizzi, F; Parasole, O; Riggi, F

    2006-01-01

    Experiments concerning the physics of cosmic rays offer to high-school teachers and students a relatively easy approach to the field of research in high energy physics. The detection of cosmic rays does not necessarily require the use of sophisticated equipment, and various properties of the cosmic radiation can be observed and analysed even by the use of a single Geiger counter. Nevertheless, the variety of such kind of experiments and the results obtained are limited because of the inclusive nature of these measurements. A significant improvement may be obtained when two or more Geiger counters are operated in coincidence. In this paper we discuss the potential of performing educational cosmic ray experiments with Geiger counters. In order to show also the educational value of coincidence techniques, preliminary results of cosmic ray experiments carried out by the use of a simple coincidence circuit are briefly discussed.

  18. Neutron spectroscopy with the Spherical Proportional Counter

    CERN Document Server

    Bougamont, E; Derre, J; Galan, J; Gerbier, G; Giomataris, I; Gros, M; Katsioulas, I; Jourde, D; Magnier, P; Navick, X F; Papaevangelou, T; Savvidis, I; Tsiledakis, G

    2015-01-01

    A novel large volume spherical proportional counter, recently developed, is used for neutron measurements. Gas mixtures of $N_{2}$ with $C_{2}H_{6}$ and pure $N_{2}$ are studied for thermal and fast neutron detection, providing a new way for the neutron spectroscopy. The neutrons are detected via the ${}^{14}N(n, p)C^{14}$ and ${}^{14}N(n, \\alpha)B^{11}$ reactions. Here we provide studies of the optimum gas mixture, the gas pressure and the most appropriate high voltage supply on the sensor of the detector in order to achieve the maximum amplification and better resolution. The detector is tested for thermal and fast neutrons detection with a ${}^{252}Cf$ and a ${}^{241}Am-{}^{9}Be$ neutron source. The atmospheric neutrons are successfully measured from thermal up to several MeV, well separated from the cosmic ray background. A comparison of the spherical proportional counter with the current available neutron counters is also given.

  19. TOP counter prototype R&D

    Science.gov (United States)

    Inami, K.; Belle-II PID Group

    2011-05-01

    We have been developing a Cherenkov ring-imaging counter, named TOP counter, as a particle-identification device of the Belle-II detector for the super B-factory at KEK. In this presentation, we show the R&D status of the TOP counter prototype. We performed a beam test using 2 m long quartz radiator and MCP-PMTs, and evaluated the number of detected photons, time resolution and chromatic effects. We developed a square-shape MCP-PMT with Hamamatsu photonics, so as to obtain a sufficient lifetime under the Belle-II environment. We improved the lifetime of the quantum efficiency by changing the internal structure and production process, and then obtained a lifetime of >350 mC/cm2.

  20. Development of photocathodes for gas counters

    International Nuclear Information System (INIS)

    A lot of ways of physics needs the development of high sensibility imaging devices with large sensitive surface. The problems brought by the building of such devices may be solved by the use of gaz counters. But we must sensitize these counters to low energy photons (< 10 eV). We have particularly studied the response of solid state photocathodes working directly into the counter. We show first a method to increase the quantum efficiency of photocathodes. We experiment this method and take few conclusions. We also show a method to measure the photoelectric threshold of a metal under gas and we apply this method. Because of the limitations of our apparatus we have built a system which permit to manufacture and mesure photocathodes. This apparatus which have numerous possibilities and an automatic data taking system is described. We also describe results of its exploitation and the type of investigation that we are going to develop

  1. Colorimetric Sugar Sensing Using Boronic Acid-Substituted Azobenzenes

    OpenAIRE

    Yuya Egawa; Ryotaro Miki; Toshinobu Seki

    2014-01-01

    In association with increasing diabetes prevalence, it is desirable to develop new glucose sensing systems with low cost, ease of use, high stability and good portability. Boronic acid is one of the potential candidates for a future alternative to enzyme-based glucose sensors. Boronic acid derivatives have been widely used for the sugar recognition motif, because boronic acids bind adjacent diols to form cyclic boronate esters. In order to develop colorimetric sugar sensors, boronic acid-conj...

  2. Synthesis and characterization of ammonium phosphate fertilizers with boron

    OpenAIRE

    ANGELA MAGDA; RODICA PODE; CORNELIA MUNTEAN; MIHAI MEDELEANU; ALEXANDRU POPA

    2010-01-01

    The concentration of boron, an essential micronutrient for plants, presents a narrow range between deficiency and toxicity. In order to provide the boron requirement for plants, and to avoid toxicity problems, boron compounds are mixed with basic fertilizers. Sodium borate pentahydrate was used as a boron source. Ammonium orthophosphates fertilizers with boron were prepared by neutralizing phosphoric acid with ammonia and addition of variable amounts of sodium tetraborate pentahydrate to the ...

  3. Calibration of nuclear medicine gamma counters

    International Nuclear Information System (INIS)

    In this paper the practical problem of nuclear medicine gamma counters calibration has been solved by using dose calibrators CRC-15R with standard error ±5%. The samples from technetium generators have been measured both by dose calibrators CRC-15R and gamma counter ICN Gamma 3.33 taking into account decay correction. Only the linear part of the curve has practical meaning. The advantage of this procedure satisfies the requirements from international standards: the calibration of sources used for medical exposure be traceable to a standard dosimetry laboratory and radiopharmaceuticals for nuclear medicine procedures be calibrated in terms of activity of the radiopharmaceutical to be administered. (author)

  4. Whole Body Counters in Biomedical Research

    Directory of Open Access Journals (Sweden)

    S. C. Jain

    1994-01-01

    Full Text Available Whole body counter plays an important role in medical diagnosis and clinical research. It has been used for monitoring of radiation workers for the assessment of internal contamination or assessment of activity in persons exposed to radiation fallout. In a nuclear emergency like Chernobyl, neutron exposure to the radiation victims was assessed by measuring the induced activity of /sup 24/Na. Apart from its use in determining certain element composition in the body, it has got a number of clinical applications like absorption tests, and metabolic and kinetic studies. The work done at INMAS whole body counter facility is also discussed.

  5. An automatic light scattering CCN counter

    Science.gov (United States)

    Lala, G. G.

    1981-11-01

    The counter is a static thermal diffusion chamber which has been modified to include an optical system for the determination of droplet concentration by the measurement of scattered light. The determination of concentration is made by measurement of the peak scattered light signal from the cloud of growing droplets which is a function of both the droplet concentration and chamber supersaturation. Because the formation of the peak is related to the rate of growth of the droplets and sedimentation, both of which are determined by supersaturation, the system calibration can be uniquely determined by comparison with an absolute counter such as a static diffusion chamber with a photographic recording system.

  6. Whole body counters: types, performance and uses

    International Nuclear Information System (INIS)

    The present monograph deals with Whole Counters, since its definition, evolution, performance, clinical indications and results. Scintillation crystals detection systems were described as well as scintillant solutions, plastic scintillations, and gaseous detectors, including its interplay forms and basal characteristics. Geometric arrangements of standard chair, arc and hammock, arrangements with scintillant solutions and plastic scintillations, as well as special geometric arrangements were equally commented. Clinic and experimental studies were also dealt with Whole Body Counters, giving examples with potassium, iron vitamin B12 and albumin. (author)

  7. Extruded plastic counters with WLS fiber readout

    CERN Document Server

    Kudenko, Yu G; Mayatski, V A; Mineev, O V; Yershov, N V

    2001-01-01

    Extruded plastic scintillation counters with WLS fiber readout are described. For a 7 mm thick counter with 4.3 m long double-clad fibers spaced at 7 mm a light yield of 18.7 photoelectrons/MeV and a time resolution of 0.71 ns (sigma) were obtained. A prototype photon veto module consisting of 10 layers of 7 mm thick grooved plastic slabs interleaved with 1 mm lead sheets was also tested, which yielded 122 photoelectrons per minimum ionizing particle and time resolution of 360 ps.

  8. The determination of boron and carbon in reactor grade boron carbide

    International Nuclear Information System (INIS)

    The sealed tube method of dissolution at high temperature and pressure has been successfully applied in the analysis of reactor grade boron carbide for the determination of boron. A 50 mg sample of boron carbide is completely dissolved by heating with concentrated nitric acid in a sealed tube at 3000C. The boron content of the resultant sample solution is determined by the mannitol potentiometric titration method. The precision of the method for the determination of 2.5 mg of boron using the Harwell automatic potentiometric titrator is 0.2% (coefficient of variation). The carbon content of a boron carbide sample is determined by combustion of the sample at 10500C in a stream of oxygen using vanadium pentoxide to ensure the complete oxidation of the sample. The carbon dioxide produced from the sample is measured manometrically and the precision of the method for the determination of 4 mg of carbon is 0.4% (coefficient of variation). (author)

  9. Proceedings of workshop on 'Boron Chemistry and Boron Neutron Capture Therapy'

    International Nuclear Information System (INIS)

    This volume contains the proceedings of the 3rd Workshop on 'the Boron Chemistry and Boron Neutron Capture Therapy' held on February 12, in 1991. In this workshop, our attention was focused on the chemical nature of boron compounds and the boron neutron capture therapy (BNCT). First, clinical experiences of BNCT in KURRI in 1990 and 1991 were reported (Chap. 3). The feasibility of the gadolinium neutron capture therapy for brain tumors was discussed (Chap. 4). In the chemical field, a rapid spectrophotometric determination of trace amounts of borons in biological samples is described (Chap. 5). The chemical behaviours of p-boronophenylalanine and its analogs in aqueous solutions were investigated by a paper electrophoresis and infrared spectroscopy (Chap. 6). On the molecular design and synthesis of new boron carriers for BNCT, several new synthetic methods for B-10 containing nucleoside derivatives were shown (Chap. 7). (author)

  10. Quantitative boron detection by neutron transmission method

    International Nuclear Information System (INIS)

    //Quantitative boron detection is mainly performed by chemical methods like colorimetric titration. High neutron absorption cross section of natural boron makes attractive its detection by absorption measurements. This work is an extension of earlier investigations where neutron radiography technique was used for boron detection. In the present investigation, the neutron absorption rate of boron containing solutions is the way to measure quantitatively the boron content of the solutions. The investigation was carried out in Istanbul TRIGA Mark-II reactor. In the end of the experiments, it was observed that even |ppw| grade boron in aqueous solution can be easily detected. The use of this method is certainly very useful for boron utilizing industries like glass and steel industries.The major disadvantage of the method is the obligation to use always aqueous solutions to be able to detect homogeneously the boron content. Then, steel or glass samples have to be put first in an appropriate solution form. The irradiation of steel samples can give the distribution of boron by the help of a imaging and this suggested method will give its quantitative measurement. The superiority of this method are its quick response time and its accuracy. To test this accuracy, a supposed unknown , solution of boric acid is irradiated and then calculated by the help of the calibration curve. The measured value of boric acid was 0.89 mg and the calculated value was found to be 0.98 mg which gives an accuracy of 10 %. It was also seen that the method is more accurate for low concentration. (authors)

  11. X-ray diffraction study of boron produced by pyrolysis of boron tribromide

    Science.gov (United States)

    Rosenberg, David

    The goal of this research was to determine the composition of boron deposits produced by pyrolysis of boron tribromide, and to use the results to (a) determine the experimental conditions (reaction temperature, etc.) necessary to produce alpha-rhombohedral boron and (b) guide the development/refinement of the pyrolysis experiments such that large, high purity crystals of alpha-rhombohedral boron can be produced with consistency. Developing a method for producing large, high purity alpha-rhombohedral boron crystals is of interest because such crystals could potentially be used to achieve an alpha-rhombohedral boron based neutron detector design (a solid-state detector) that could serve as an alternative to existing neutron detector technologies. The supply of neutron detectors in the United States has been hampered for a number of years due to the current shortage of helium-3 (a gas used in many existing neutron detector technologies); the development of alternative neutron detector technology such as an alpha-rhombohedral boron based detector would help provide a more sustainable supply of neutron detectors in this country. In addition, the prospect/concept of an alpha-rhombohedral boron based neutron detector is attractive because it offers the possibility of achieving a design that is smaller, longer life, less power consuming, and potentially more sensitive than existing neutron detectors. The main difficulty associated with creating an alpha-rhombohedral boron based neutron detector is that producing large, high purity crystals of alpha-rhombohedral boron is extremely challenging. Past researchers have successfully made alpha-rhombohedral boron via a number of methods, but no one has developed a method for consistently producing large, high purity crystals. Alpha-rhombohedral boron is difficult to make because it is only stable at temperatures below around 1100-1200 °C, its formation is very sensitive to impurities, and the conditions necessary for its

  12. Sintering of boron carbide (B4C)

    International Nuclear Information System (INIS)

    Boron carbide (B4C) is used as a control element in different types of reactors due to the high fast and thermal neutron absorption cross-section of B-10. Requirements of the Advanced Reactor Division of the Bariloche Atomic Center triggered the study of the possibilities of fabricating B4C pellets by cold-pressing and sintering. The results of essays of sinterability of two different commercial boron carbide powders, sintered at temperatures between 1200 and 2200 deg C, are given. Characterizations of the samples were made to determine the evolution of density, porosity, microstructure and boron content as a function of sintering temperature. (Author)

  13. Developments in boron magnetic resonance imaging (MRI)

    Energy Technology Data Exchange (ETDEWEB)

    Schweizer, M.

    1995-11-01

    This report summarizes progress during the past year on maturing Boron-11 magnetic resonance imaging (MRI) methodology for noninvasive determination of BNCT agents (BSH) spatially in time. Three major areas are excerpted: (1) Boron-11 MRI of BSH distributions in a canine intracranial tumor model and the first human glioblastoma patient, (2) whole body Boron-11 MRI of BSH pharmacokinetics in a rat flank tumor model, and (3) penetration of gadolinium salts through the BBB as a function of tumor growth in the canine brain.

  14. First boronization in KSTAR: Experiences on carborane

    Energy Technology Data Exchange (ETDEWEB)

    Hong, Suk-Ho, E-mail: sukhhong@nfri.re.kr [National Fusion Research Institute, 113 Gwahangno, Yusung-Gu, Daejeon 305-333 (Korea, Republic of); Center for Edge Plasma Science (cEps), Hanyang University, Seoul 133-791 (Korea, Republic of); Lee, Kun-Su; Kim, Kwang-Pyo; Kim, Kyung-Min; Kim, Hong-Tack [National Fusion Research Institute, 113 Gwahangno, Yusung-Gu, Daejeon 305-333 (Korea, Republic of); Sun, Jong-Ho; Woo, Hyun-Jong [Center for Edge Plasma Science (cEps), Hanyang University, Seoul 133-791 (Korea, Republic of); Department of Electrical Engineering, Hanyang University, Seoul 133-791 (Korea, Republic of); Park, Jae-Min [National Fusion Research Institute, 113 Gwahangno, Yusung-Gu, Daejeon 305-333 (Korea, Republic of); Park, Eun-Kyong [Center for Edge Plasma Science (cEps), Hanyang University, Seoul 133-791 (Korea, Republic of); Department of Electrical Engineering, Hanyang University, Seoul 133-791 (Korea, Republic of); Kim, Woong-Chae; Kim, Hak-Kun; Park, Kap-Rai; Yang, Hyung-Lyeol; Oh, Yeong-Kook; Na, Hoon-Kyun [National Fusion Research Institute, 113 Gwahangno, Yusung-Gu, Daejeon 305-333 (Korea, Republic of); Lho, Taehyeop [National Fusion Research Institute, 113 Gwahangno, Yusung-Gu, Daejeon 305-333 (Korea, Republic of); Center for Edge Plasma Science (cEps), Hanyang University, Seoul 133-791 (Korea, Republic of); Chung, Kyu-Sun [Center for Edge Plasma Science (cEps), Hanyang University, Seoul 133-791 (Korea, Republic of); Department of Electrical Engineering, Hanyang University, Seoul 133-791 (Korea, Republic of)

    2011-08-01

    First boronization was performed in KSTAR tokamak during 2009 campaign in order to reduce oxygen impurities and to lower the power loss due to radiation. We report the results from the experiences on carborane during the first boronization in KSTAR. After the boronization, H{sub 2}O and O{sub 2} level in the vacuum vessel are reduced significantly. The characteristics of the deposited thin films were analyzed by variable angle spectroscopic ellipsometry, XPS, and AES. {approx}1.78 x 10{sup 16} cm{sup -2} s{sup -1} of carbon flux on the wall is estimated by using cavity technique.

  15. Boron site preference in ternary Ta and Nb boron silicides

    International Nuclear Information System (INIS)

    X-ray single crystal (XSC) and neutron powder diffraction data (NPD) were used to elucidate boron site preference for five ternary phases. Ta3Si1−xBx (x=0.112(4)) crystallizes with the Ti3P-type (space group P42/n) with B-atoms sharing the 8g site with Si atoms. Ta5Si3−x (x=0.03(1); Cr5B3- type) crystallizes with space group I4/mcm, exhibiting a small amount of vacancies on the 4a site. Both, Ta5(Si1−xBx)3, x=0.568(3), and Nb5(Si1−xBx)3, x=0.59(2), are part of solid solutions of M5Si3 with Cr5B3-type into the ternary M–Si–B systems (M=Nb or Ta) with B replacing Si on the 8h site. The D88-phase in the Nb–Si–B system crystallizes with the Ti5Ga4-type revealing the formula Nb5Si3B1−x (x=0.292(3)) with B partially filling the voids in the 2b site of the Mn5Si3 parent type. - Graphical abstract: The crystal structures of a series of compounds have been solved from X-ray single crystal diffractometry revealing details on the boron incorporation. Highlights: ► Structure of a series of compounds have been solved by X-ray single crystal diffractometry. ► Ta3(Si1−xBx) (x=0.112) crystallizes with the Ti3P-type, B and Si atoms randomly share the 8g site. ► Structure of Nb5Si3B1−x (x=0.292; Ti5Ga4-type) was solved from NPD.

  16. Synthesis of Boron Nanorods by Smelting Non-Toxic Boron Oxide in Liquid Lithium

    OpenAIRE

    Amartya Chakrabarti; Tao Xu; Laura K. Paulson; Krise, Kate J.; Maguire, John A; Hosmane, Narayan S.

    2010-01-01

    In contrast to the conventional bottom-up syntheses of boron nanostructures, a unique top-down and greener synthetic strategy is presented for boron nanorods involving nontoxic boron oxide powders ultrasonically smelted in liquid lithium under milder conditions. The product was thoroughly characterized by energy dispersive X-ray analysis, atomic emission spectroscopy, thermogravimetric analysis and, UV-Vis spectroscopy, including structural characterization by transmission electron microscop...

  17. Determination of boron isotope ratios in boron carbide by mass spectrometry

    International Nuclear Information System (INIS)

    This paper introduces the direct determination of boron isotope ratios in the boron carbide powder by thermal ionization mass spectrometry. The technique for sample loading, the procedure for heating and the eliminating of effects induced by oxygen are studied. The study indicates that the preparing process for the sample will be shorted, and the time for determination and the exposure dose of the laboratory assistant will be reduced for the reason of directly determination of boron carbide. (authors)

  18. Effect of boron concentration on physicochemical properties of boron-doped carbon nanotubes

    International Nuclear Information System (INIS)

    Boron-doped carbon nanotubes (B-CNTs) were synthesized using chemical vapour deposition (CVD) floating catalyst method. Toluene was used as the carbon source, triphenylborane as boron as well as the carbon source while ferrocene was used as the catalyst. The amount of triphenylborane used was varied in a solution of toluene and ferrocene. Ferrocene was kept constant at 2.5 wt.%. while a maximum temperature of 900 °C was used for the synthesis of the shaped carbon nanomaterial (SCNMs). SCNMs obtained were characterized by the use of transmission electron microscope (TEM), scanning electron microscope (SEM), high resolution-electron microscope, electron dispersive X-ay spectroscopy (EDX), Raman spectroscopy, inductively coupled plasma-optical emission spectroscopy (ICP-OES), vibrating sample magnetometer (VSM), nitrogen adsorption at 77 K, and inverse gas chromatography. TEM and SEM analysis confirmed SCNMs obtained were a mixture of B-CNTs and carbon nanofibres (B-CNF). EDX and ICP-OES results showed that boron was successively incorporated into the carbon hexagonal network of CNTs and its concentration was dependent on the amount of triphenylborane used. From the VSM results, the boron doping within the CNTs introduced ferromagnetic properties, and as the percentage of boron increased the magnetic coactivity and squareness changed. In addition, boron doping changed the conductivity and the surface energy among other physicochemical properties of B-CNTs. - Highlights: • Boron-doping of carbon nanotubes (CNTs) changes their physiochemical properties. • Amount of boron-doping was dependent on the wt.% of boron precursor used. • Boron-doping changed CNTs surfaces and the distribution of dispersive energy sites. • Boron-doping affected the conductivity and ferromagnetic properties. • Increased boron-doping results in a more favourable interaction with polar probes

  19. Personality Interactions and Scaffolding in On-Line Discussions

    Science.gov (United States)

    Nussbaum, E. Michael; Hartley, Kendall; Sinatra, Gale M.; Reynolds, Ralph E.; Bendixen, Lisa D.

    2004-01-01

    The potential of on-line discussions to prompt greater reflection of course material is often stymied by a tendency of students to agree with one another rather than to formulate counter-arguments. This article describes an experiment using note starters and elaborated cases to encourage counter-argumentation and examines interactions with…

  20. Investigation of boron extraction process with aid magnesium hydroxide from mother liquor of boron production

    International Nuclear Information System (INIS)

    Conditions of boron - magnesium concentrate preparation from mother liquor by coprecipitation of borate - ions by magnesium hydroxide are investigated. It is shown that boron - magnesium concentrate and products of its heat treatment at 100 - 500 deg C in water are dissolved partially, and in ammonium citrate - practically completely. Suppositions are made on the composition of the product prepared, on the the structure of its crystal lattice and the processes taking place in it during heat treatment. The conclusion is made on the perspectiveness of processing of mother liquor of boron industry for boron - magnesium concentrate

  1. High speed non-latching squid binary ripple counter

    International Nuclear Information System (INIS)

    High speed, single flux quantum (SFQ) binary scalers are important components in superconducting analog-to-digital converters (ADC). This paper reviews the concept for a SQUID ADC and the design of an SFQ binary ripple counter, and reports the simulation of key components, and fabrication and performance of non-latching SQUID scalers and SFQ binary ripple counters. The SQUIDs were fabricated with Nb/Nb2O5/PbIn junctions and interconnected by monolithic superconducting transmission lines and isolation resistors. Each SQUID functioned as a bistable flip-flop with the input connected to the center of the device and the output across one junction. All junctions were critically damped to optimize the pulse response. Operation was verified by observing the dc I-V curves of successive SQUIDs driven by a cw pulse train generated on the same chip. Each SQUID exhibited constant-voltage current steps at 1/2 the voltage of the preceding device as expected from the Josephson voltage-to-frequency relation. Steps were observed only for the same voltage polarity of successive devices and for proper phase bias of the SQUID. Binary frequency division was recorded up to 40GHz for devices designed to operate to 28GHz

  2. Boron

    International Nuclear Information System (INIS)

    This paper reports that borate minerals and refined borates are used extensively for the manufacture of vitreous materials such as insulation and textile fiberglasses, borosilicate glass, and porcelain enamels and frits. In North America, these applications are estimated to account for over 54% of the borate consumption. Other substantial uses are in soaps and detergents, metallurgy, fire retardants, industrial biocides, agriculture, and various miscellaneous applications. Reported domestic borate consumption in 1990 was estimated by the U.S. Bureau of Mines to be 320 000 metric tons B2O3 versus 354 000 metric tons B2O3 in 1989. Consumption is projected to remain essentially static in 1991. Imports were estimated by the Bureau to be 50 000 metric tons B2O3 in 1990. Exports of boric acid and refined borates were approximately 650 000 metric tons of product, a 15 000 metric ton increase from the 1989 level. This increase partially offsets the drop in the 1990 consumption level

  3. Micropipette as Coulter counter for submicron particles

    Science.gov (United States)

    Rudzevich, Yauheni; Ordonez, Tony; Evans, Grant; Chow, Lee

    2011-03-01

    Coulter counter based on micropipette has been around for several decades. Typical commercial Coulter counter has a pore size of 20 μ m, and is designed to detect micron-size blood cells. In recent years, there are a lot of interests in using nanometer pore size Coulter counter to detect single molecule and to sequence DNA. Here we describe a simple nanoparticle counter based on pulled micropipettes with a diameter of 50 -- 500 nm. Borosilicate micropipettes with an initial outer diameter of 1.00 mm and inner diameter of 0.5 mm are used. After pulling, the micropipettes are fire polished and ultrasound cleaned. Chlorinated Ag/AgCl electrodes and 0.1 M of KCl solution are used. The ionic currents are measured using an Axopatch 200B amplifier in the voltage-clamp mode. Several types and sizes of nanoparticles are measured, including plain silica and polystyrene nanospheres. The results will be discussed in terms of pH values of the solution and concentrations of the nanoparticles. Financial support from National Science Foundation (NSF-0901361) is acknowledged.

  4. Energy resolution of the proportional counter

    International Nuclear Information System (INIS)

    Resolution values 11.6% and 12.2% for 5.9 keV have been obtained experimentally for proportional counters with gas fillings Ne+0.5% Ar or Ar+0.5% C2H2. This is appreciably better than earlier measurements which exceed 14%. Theoretical computation indicates that even better resolutions can be obtained. (Auth.)

  5. Ultrafine Condensation Particle Counter Instrument Handbook

    Energy Technology Data Exchange (ETDEWEB)

    Kuang, C. [Brookhaven National Lab. (BNL), Upton, NY (United States)

    2016-02-01

    The Model 3776 Ultrafine Condensation Particle Counter (UCPC; pictured in Appendix A) is designed for researchers interested in airborne particles smaller than 20 nm. With sensitivity to particles down to 2.5 nm in diameter, this UCPC is ideally suited for atmospheric and climate research, particle formation and growth studies, combustion and engine exhaust research, and nanotechnology research.

  6. Sealed drift tube cosmic ray veto counters

    International Nuclear Information System (INIS)

    We describe a simple drift tube counter that has been used as a cosmic ray veto for the UCNA experiment, a first-ever measurement of the neutron beta-asymmetry using ultra-cold neutrons. These detectors provide an inexpensive alternative to more conventional scintillation detectors for large area cosmic ray anticoincidence detectors.

  7. A proportional-scintillation counter beta spectrometer

    International Nuclear Information System (INIS)

    Using a proportional counter for coincidence gating of events in a plastic scintillator provides selective registration of beta interactions in the scintillator. This technique has been used to construct a field instrument that can selectively collect beta spectra (coincidence gating) or gamma spectra (anticoincidence gating). Associated dose rates are calculated from the spectra

  8. Cerenkov counters at the Omega Facility

    CERN Multimedia

    1975-01-01

    P. Petroff on the left. Here one sees both the gas Cerenkov counters sitting in front of the magnet to select forward emitted particles. The smaller one, working at high pressure, sits nearest to the Omega magnet (see photo 7505073X), the other (see photo 7505071X) works at atmospheric pressure.

  9. Townsend coefficients of gases in avalanche counters

    International Nuclear Information System (INIS)

    Though much work has been done by many authors in the last few years in the development and application of avalanche counters for ion radiation, it is based upon values of the Townsend coefficients as the essential gas parameter, which were determined many years ago for much lower reduced field strengths F/p than prevail in such counters. Therefore absolute determinations of α in vapours of methyl alcohol, cyclohexane, acetone, and n-heptene were performed under original conditions of avalanche counters. The values obtained do not differ by more than 30%-50% from the former values indeed, extrapolated over F/p for the first three mentioned substances, but the amounts of A and B in the usual representation α/p=A exp(-B(F/p)) are much greater for the stronger reduced fields. This is of importance for such counter properties as the dependence of pulse heights on pressure, voltage, electrode distance etc., which are governed by other combinations of A and B than α/p itself. A comparison of results for different ionic radiations shows a marked influence of the primary ionization density along the particle tracks which is hard to explain. (Auth.)

  10. COUNTER-ROTATION IN RELATIVISTIC MAGNETOHYDRODYNAMIC JETS

    Energy Technology Data Exchange (ETDEWEB)

    Cayatte, V.; Sauty, C. [Laboratoire Univers et Théories, Observatoire de Paris, UMR 8102 du CNRS, Université Paris Diderot, F-92190 Meudon (France); Vlahakis, N.; Tsinganos, K. [Department of Astrophysics, Astronomy and Mechanics, Faculty of Physics, University of Athens, 15784 Zografos, Athens (Greece); Matsakos, T. [Department of Astronomy and Astrophysics, The University of Chicago, Chicago, IL 60637 (United States); Lima, J. J. G., E-mail: veronique.cayatte@obspm.fr [Centro de Astrofísica, Universidade do Porto, Rua das Estrelas, 4150-762 Porto (Portugal)

    2014-06-10

    Young stellar object observations suggest that some jets rotate in the opposite direction with respect to their disk. In a recent study, Sauty et al. showed that this does not contradict the magnetocentrifugal mechanism that is believed to launch such outflows. Motion signatures that are transverse to the jet axis, in two opposite directions, have recently been measured in M87. One possible interpretation of this motion is that of counter-rotating knots. Here, we extend our previous analytical derivation of counter-rotation to relativistic jets, demonstrating that counter-rotation can indeed take place under rather general conditions. We show that both the magnetic field and a non-negligible enthalpy are necessary at the origin of counter-rotating outflows, and that the effect is associated with a transfer of energy flux from the matter to the electromagnetic field. This can be realized in three cases: if a decreasing enthalpy causes an increase of the Poynting flux, if the flow decelerates, or if strong gradients of the magnetic field are present. An illustration of the involved mechanism is given by an example of a relativistic magnetohydrodynamic jet simulation.

  11. One-Counter Markov Decision Processes

    NARCIS (Netherlands)

    Brazdil, T.; Brozek, V.; Etessami, K.; Kucera, A.; Wojtczak, D.K.; Charikar, M.

    2010-01-01

    We study the computational complexity of central analysis problems for One-Counter Markov Decision Processes (OC-MDPs), a class of finitely-presented, countable-state MDPs. OC-MDPs are equivalent to a controlled extension of (discrete-time) Quasi-Birth-Death processes (QBDs), a stochastic model stud

  12. Effectiveness of a Television Counter Advertisement.

    Science.gov (United States)

    Lull, James T.; Mulac, Anthony

    This paper investigates the potential effectiveness of counter advertising in influencing the buying habits of a convinced audience. One month before the actual study, 109 subjects indicated a brand preference in a consumer questionnaire. The subjects were randomly assigned to groups that viewed one of the following: (1) a pro-Bayer aspirin…

  13. Performance of silica aerogel threshold Cerenkov counters

    International Nuclear Information System (INIS)

    Results from a series of test beam measurements are presented for a two-cell silica aerogel Cerenkov counter system. The main achievement is the detection of 13±1 photoelectrons in a full-sized n=1.008 silica aerogel cell which is read out with a fine mesh photomultiplier in different magnetic fields up to 1.35T. (orig.)

  14. A beta and gamma radiation counter device

    International Nuclear Information System (INIS)

    Between 1988 and 1990, 1800 small Geiger-Mueller counters have been distributed in French high schools (caesium 137 as the radioactive source) for pupils' information about radioactivity (vocabulary, protection, ...). The INSTN (Institute for nuclear science and technology) has set up seminars for teachers' formation

  15. Stark broadening of B IV spectral lines

    Science.gov (United States)

    Dimitrijević, Milan S.; Christova, Magdalena; Simić, Zoran; Kovačević, Andjelka; Sahal-Bréchot, Sylvie

    2016-08-01

    Stark broadening parameters for 157 multiplets of helium-like boron (B IV) have been calculated using the impact semiclassical perturbation formalism. Obtained results have been used to investigate the regularities within spectral series. An example of the influence of Stark broadening on B IV lines in DO white dwarfs is given.

  16. Stark broadening of B IV spectral lines

    CERN Document Server

    Dimitrijevic, Milan S; Simic, Zoran; Kovacevic, Andjelka; Sahal-Brechot, Sylvie

    2016-01-01

    Stark broadening parameters for 157 multiplets of helium like boron (B IV) have been calculated using the impact semiclassical perturbation formalism. Obtained results have been used to investigate the regularities within spectral series. An example of the influence of Stark broadening on B IV lines in DO white dwarfs is given.

  17. Boron-isotope fractionation in plants

    International Nuclear Information System (INIS)

    Naturally-occurring variations in the abundance of stable isotopes of carbon, nitrogen, oxygen, and other elements in plants have been reported and are now used to understand various physiological processes in plants. Boron (B) isotopic variation in several plant species have been documented, but no determination as to whether plants fractionate the stable isotopes of boron, 11B and 10B, has been made. Here, we report that plants with differing B requirements (wheat, corn and broccoli) fractionated boron. The whole plant was enriched in 11B relative to the nutrient solution, and the leaves were enriched in 10B and the stem in 11B relative to the xylem sap. Although at present, a mechanistic role for boron in plants is uncertain, potential fractionating mechanisms are discussed. (author)

  18. Synthesis of Boron-Containing Primary Amines

    Directory of Open Access Journals (Sweden)

    Sheng-Hsuan Chung

    2013-10-01

    Full Text Available In this study, boron-containing primary amines were synthesized for use as building blocks in the study of peptoids. In the first step, Gabriel synthesis conditions were modified to enable the construction of seven different aminomethylphenyl boronate esters in good to excellent yields. These compounds were further utilized to build peptoid analogs via an Ugi four-component reaction (Ugi-4CR under microwave irradiation. The prepared Ugi-4CR boronate esters were then successfully converted to the corresponding boronic acids. Finally, the peptoid structures were successfully modified by cross-coupling to aryl/heteroaryl chlorides via a palladium-mediated Suzuki coupling reaction to yield the corresponding derivatives in moderate to good yields.

  19. Boron toxicity in oil palm (Elaeis guineensis)

    Energy Technology Data Exchange (ETDEWEB)

    Rajaratnam, J.A.

    1973-01-01

    Potted oil palms were treated with fertilizer of borate-46 at several concentrations and the plants were observed for boron toxicity effects. Toxicity symptoms were apparent at high rates but not at rates equivalent to typical Malaysian soils.

  20. Boron adsorption on hematite and clinoptilolite

    International Nuclear Information System (INIS)

    This thesis describes experiments performed to determine the suitability of boron as a potential reactive tracer for use in saturated-zone C-well reactive tracer studies for the Yucca Mountain Project (YMP). Experiments were performed to identify the prevalent sorption mechanism of boron and to determine adsorption of boron on hematite and clinoptilolite as a function of pH. These minerals are present in the Yucca Mountain tuff in which the C-well studies will be conducted. Evaluation of this sorption mechanism was done by determining the equilibration time of boron-mineral suspensions, by measuring changes in equilibrium to titrations, and by measuring electrophoretic mobility. Experiments were performed with the minerals suspended in NaCl electrolytes of concentrations ranging from 0.1 N NaCl to 0.001 N NaCl. Experimentalconditions included pH values between 3 and 12 and temperature of about 38 degrees C

  1. Boron-Filled Hybrid Carbon Nanotubes.

    Science.gov (United States)

    Patel, Rajen B; Chou, Tsengming; Kanwal, Alokik; Apigo, David J; Lefebvre, Joseph; Owens, Frank; Iqbal, Zafar

    2016-01-01

    A unique nanoheterostructure, a boron-filled hybrid carbon nanotube (BHCNT), has been synthesized using a one-step chemical vapor deposition process. The BHCNTs can be considered to be a novel form of boron carbide consisting of boron doped, distorted multiwalled carbon nanotubes (MWCNTs) encapsulating boron nanowires. These MWCNTs were found to be insulating in spite of their graphitic layered outer structures. While conventional MWCNTs have great axial strength, they have weak radial compressive strength, and do not bond well to one another or to other materials. In contrast, BHCNTs are shown to be up to 31% stiffer and 233% stronger than conventional MWCNTs in radial compression and have excellent mechanical properties at elevated temperatures. The corrugated surface of BHCNTs enables them to bond easily to themselves and other materials, in contrast to carbon nanotubes (CNTs). BHCNTs can, therefore, be used to make nanocomposites, nanopaper sheets, and bundles that are stronger than those made with CNTs. PMID:27460526

  2. Boron neutron capture therapy. What is next?

    International Nuclear Information System (INIS)

    BNCT (Boron Neutron Capture Therapy) will have difficulties establishing itself without efficient and conclusive clinical trials of glioma, without the expansion to other tumors, and without efficient programs for compound development and testing. (author)

  3. Ni doping of semiconducting boron carbide

    International Nuclear Information System (INIS)

    The wide band gap, temperature stability, high resistivity, and robustness of semiconducting boron carbide make it an attractive material for device applications. Undoped boron carbide is p type; Ni acts as a n-type dopant. Here we present the results of controlled doping of boron carbide with Ni on thin film samples grown using plasma enhanced chemical vapor deposition. The change in the dopant concentration within the thin film as a function of the dopant flow rate in the precursor gas mixture was confirmed by x-ray photoelectron spectroscopy measurements; with increasing dopant concentration, current-voltage (I-V) curves clearly establish the trend from p-type to n-type boron carbide.

  4. High temperature thermoelectric properties of boron carbide

    International Nuclear Information System (INIS)

    Boron carbides are refractory solids with potential for application as very high temperature p-type thermoelectrics in power conversion applications. The thermoelectric properties of boron carbides are unconventional. In particular, the electrical conductivity is consistent with the thermally activated hopping of a high density (∼1021/cm3) of bipolarons; the Seebeck coefficient is anomalously large and increases with increasing temperature; and the thermal conductivity is surprisingly low. In this paper, these unusual properties and their relationship to the unusual structure and bonding present in boron carbides are reviewed. Finally, the potential for utilization of boron carbides at very high temperatures (up to 2200 degrees C) and for preparing n-type materials is discussed

  5. Interaction of iron with boron in metal-rich metallaboranes resulting in large deshielding and rapid relaxation processes of the boron-11 nucleus

    International Nuclear Information System (INIS)

    A first-order, parameterized model for calculating 11B chemical shifts in metal-rich ferraboranes and a correlation of chemical shift with boron Mulliken populations from Fenske-Hall calculations are presented. These correlations are qualitatively different from those reported earlier for boranes and suggest that direct iron-boron interactions lead to large deshielding due to substantial increases in multiple-bond contributions to the shielding tensor. Relaxation rates have been measured for [Fe4(CO)12BH/sub 3-n/]/sup n-/ (n = 0-2) and correlated with electric field gradients at the boron nucleus estimated from Fenske-Hall calculations. These results demonstrate that formation of the boride, [Fe4(CO)12B]3-, by deprotonation is accompanied by the development of large asymmetries in the electronic charge distribution around the boron nucleus. Finally, 7Li NMR is used to probe the nature of the anions [Fe4(CO)12BH/sub 3-n/]/sup n-/ (n = 1-3), and observed line shapes suggest close association of Li+ with the trianion. 28 references, 3 figures, 4 tables

  6. Room-temperature near-infrared electroluminescence from boron-diffused silicon pn junction diodes

    Science.gov (United States)

    Li, Si; Gao, Yuhan; Fan, Ruixin; Li, Dongsheng; Yang, Deren

    2015-02-01

    Silicon pn junction diodes with different doping concentrations were prepared by boron diffusion into Czochralski (CZ) n-type silicon substrate. Their room-temperature near-infrared electroluminescence (EL) was measured. In the EL spectra of the heavily boron doped diode, a luminescence peak at ~1.6 μm (0.78 eV ) was observed besides the band-to-band line (~1.1eV) under the condition of high current injection, while in that of the lightly boron doped diode only the band-to-band line was observed. The intensity of peak at 0.78 eV increases exponentially with current injection with no observable saturation at room temperature. Furthermore, no dislocations were found in the cross-sectional transmission electron microscopy image, and no dislocation-related luminescence was observed in the low-temperature photoluminescence spectra. We deduce the 0.78 eV emission originates from the irradiative recombination in the strain region of diodes caused by the diffusion of large number of boron atoms into silicon crystal lattice.

  7. Room-temperature near-infrared electroluminescence from boron-diffused silicon pn junction diodes

    Directory of Open Access Journals (Sweden)

    Si eLi

    2015-02-01

    Full Text Available Silicon pn junction diodes with different doping concentrations were prepared by boron diffusion into Czochralski (CZ n-type silicon substrate. Their room-temperature near-infrared electroluminescence (EL was measured. In the EL spectra of the heavily boron doped diode, a luminescence peak at ~1.6 m (0.78 eV was observed besides the band-to-band line (~1.1eV under the condition of high current injection, while in that of the lightly boron doped diode only the band-to-band line was observed. The intensity of peak at 0.78 eV increases exponentially with current injection with no observable saturation at room temperature. Furthermore, no dislocations were found in the cross-sectional transmission electron microscopy image, and no dislocation-related luminescence was observed in the low-temperature photoluminescence spectra. We deduce the 0.78 eV emission originates from the irradiative recombination in the strain region of diodes caused by the diffusion of large number of boron atoms into silicon crystal lattice.

  8. Lithium-Beryllium-Boron : Origin and Evolution

    OpenAIRE

    Vangioni-Flam, Elisabeth; Casse, Michel; Audouze, Jean

    1999-01-01

    The origin and evolution of Lithium-Beryllium-Boron is a crossing point between different astrophysical fields : optical and gamma spectroscopy, non thermal nucleosynthesis, Big Bang and stellar nucleosynthesis and finally galactic evolution. We describe the production and the evolution of Lithium-Beryllium-Boron from Big Bang up to now through the interaction of the Standard Galactic Cosmic Rays with the interstellar medium, supernova neutrino spallation and a low energy component related to...

  9. Innovative boron nitride-doped propellants

    OpenAIRE

    Thelma Manning; Richard Field; Kenneth Klingaman; Michael Fair; John Bolognini; Robin Crownover; Carlton P. Adam; Viral Panchal; Eugene Rozumov; Henry Grau; Paul Matter; Michael Beachy; Christopher Holt; Samuel Sopok

    2016-01-01

    The U.S. military has a need for more powerful propellants with balanced/stoichiometric amounts of fuel and oxidants. However, balanced and more powerful propellants lead to accelerated gun barrel erosion and markedly shortened useful barrel life. Boron nitride (BN) is an interesting potential additive for propellants that could reduce gun wear effects in advanced propellants (US patent pending 2015-026P). Hexagonal boron nitride is a good lubricant that can provide wear resistance and lower ...

  10. A neutron diffraction study of amorphous boron

    Science.gov (United States)

    Delaplane, R. G.; Lundström, T.; Dahlborg, U.; Howells, W. S.

    1991-07-01

    The structure of amorphous boron has been studied with pulsed neutron diffraction techniques using the ISIS facilities at the Rutherford Appleton Laboratory. The experimental static structure factor S(Q) and radial distribution function support a structural model based on units of B12 icosahedra resembling those found in crystalline β-rhombohedral boron, but with a certain degree of disorder occurring in the linking between these subunits.

  11. Design and Performance of INMAS Whole Body Counter

    Directory of Open Access Journals (Sweden)

    K. K. Kapoor

    1974-07-01

    Full Text Available A whole-body counter has been commissioned at INMAS for radiation protection and clinical applications including body potassium estimations. It has 4-crystal bed geometry inside a shielded enclosure. The background index of the system (counts per minute per cc detector volume in the energy band 0.1-2 me V is about 0.6 comparing favorably with other whole-body monitors in the world. The sensitivity is 0.5 cpm per gram of K. Body potassium can be estimated can be estimated correct to 10 g for one hour counting. The variation in detector response to a point source on the mid-line of the bed is + - 10% of the mean over a length of 170 cm. The usefulness of the large dimensions of the enclosure chosen is discussed.

  12. Simultaneous Observation of Cells and Nuclear Tracks from the Boron Neutron Capture Reaction by UV-C Sensitization of Polycarbonate.

    Science.gov (United States)

    Portu, Agustina; Rossini, Andrés Eugenio; Thorp, Silvia Inés; Curotto, Paula; Pozzi, Emiliano César Cayetano; Granell, Pablo; Golmar, Federico; Cabrini, Rómulo Luis; Martin, Gisela Saint

    2015-08-01

    The distribution of boron in tissue samples coming from boron neutron capture therapy protocols can be determined through the analysis of its autoradiography image on a nuclear track detector. A more precise knowledge of boron atom location on the microscopic scale can be attained by the observation of nuclear tracks superimposed on the sample image on the detector. A method to produce an "imprint" of cells cultivated on a polycarbonate detector was developed, based on the photodegradation properties of UV-C radiation on this material. Optimal conditions to generate an appropriate monolayer of Mel-J cells incubated with boronophenylalanine were found. The best images of both cells and nuclear tracks were obtained for a neutron fluence of 1013 cm-2, 6 h UV-C (254 nm) exposure, and 4 min etching time with a KOH solution. The imprint morphology was analyzed by both light and scanning electron microscopy. Similar samples, exposed to UV-A (360 nm) revealed no cellular imprinting. Etch pits were present only inside the cell imprints, indicating a preferential boron uptake (about threefold the incubation concentration). Comparative studies of boron absorption in different cell lines and in vitro evaluation of the effect of diverse boron compounds are feasible with this methodology. PMID:26155721

  13. Upaya Perumusan Prinsip Counter Accounting Melalui Filosofi Punk sebagai Counter Culture

    OpenAIRE

    Dayno Utama

    2015-01-01

    The aim of this research is to demonstrate that resistance to mainstream research contained in top/elite accounting journals for sparking creativity and innovation unconsciously has utilized the philosophy of punk. The research method of this research is argumentation technique. The result of this research shows that the philosophy of punk as counter culture can be utilized for accounting research through formulation the accounting principles namely counter accounting. Creative and innovative...

  14. Discharge cleaning on TFTR after boronization

    International Nuclear Information System (INIS)

    At the beginning of the 1990 TFTR experimental run, after replacement of POCO-AXF-5Q graphite tiles on the midplane of the bumper limiter by carbon fiber composite (CFC) tiles and prior to any Pulse Discharge Cleaning (PDC), boronization was performed. Boronization is the deposition of a layer of boron and carbon on the vacuum vessel inner surface by a glow discharge in a diborane, methane and helium mixture. The amount of discharge cleaning required after boronization was substantially reduced compared to that which was needed after previous openings when boronization was not done. Previously, after a major shutdown, about 105 low current (∼20 kA) Taylor Discharge Cleaning (TDC) pulses were required before high current (∼400 kA) aggressive Pulse Discharge Cleaning (PDC) pulses could be performed successfully. Aggressive PDC is used to heat the limiters from the vessel bakeout temperature of 150 degrees C to 250 degrees C for a period of several hours. Heating the limiters is important to increase the rate at which water is removed from the carbon limiter tiles. After boronization, the number of required TDC pulses was reduced to <5000. The number of aggressive PDC pulses required was approximately unchanged. 14 refs., 1 tab

  15. Amorphous boron nitride at high pressure

    Science.gov (United States)

    Durandurdu, Murat

    2016-06-01

    The pressure-induced phase transformation in hexagonal boron nitrite and amorphous boron nitrite is studied using ab initio molecular dynamics simulations. The hexagonal-to-wurtzite phase transformation is successfully reproduced in the simulation with a transformation mechanism similar to one suggested in experiment. Amorphous boron nitrite, on the other hand, gradually transforms to a high-density amorphous phase with the application of pressure. This phase transformation is irreversible because a densified amorphous state having both sp3 and sp2 bonds is recovered upon pressure release. The high-density amorphous state mainly consists of sp3 bonds and its local structure is quite similar to recently proposed intermediate boron nitrite phases, in particular tetragonal structure (P42/mnm), rather than the known the wurtzite or cubic boron nitrite due to the existence of four membered rings and edge sharing connectivity. On the basis of this finding we propose that amorphous boron nitrite might be best candidate as a starting structure to synthesize the intermediate phase(s) at high pressure and temperature (probably below 800 °C) conditions.

  16. Innovative boron nitride-doped propellants

    Directory of Open Access Journals (Sweden)

    Thelma Manning

    2016-04-01

    Full Text Available The U.S. military has a need for more powerful propellants with balanced/stoichiometric amounts of fuel and oxidants. However, balanced and more powerful propellants lead to accelerated gun barrel erosion and markedly shortened useful barrel life. Boron nitride (BN is an interesting potential additive for propellants that could reduce gun wear effects in advanced propellants (US patent pending 2015-026P. Hexagonal boron nitride is a good lubricant that can provide wear resistance and lower flame temperatures for gun barrels. Further, boron can dope steel, which drastically improves its strength and wear resistance, and can block the formation of softer carbides. A scalable synthesis method for producing boron nitride nano-particles that can be readily dispersed into propellants has been developed. Even dispersion of the nano-particles in a double-base propellant has been demonstrated using a solvent-based processing approach. Stability of a composite propellant with the BN additive was verified. In this paper, results from propellant testing of boron nitride nano-composite propellants are presented, including closed bomb and wear and erosion testing. Detailed characterization of the erosion tester substrates before and after firing was obtained by electron microscopy, inductively coupled plasma and x-ray photoelectron spectroscopy. This promising boron nitride additive shows the ability to improve gun wear and erosion resistance without any destabilizing effects to the propellant. Potential applications could include less erosive propellants in propellant ammunition for large, medium and small diameter fire arms.

  17. Innovative boron nitride-doped propellants

    Institute of Scientific and Technical Information of China (English)

    Thelma MANNING; Henry GRAU; Paul MATTER; Michael BEACHY; Christopher HOLT; Samuel SOPOK; Richard FIELD; Kenneth KLINGAMAN; Michael FAIR; John BOLOGNINI; Robin CROWNOVER; Carlton P. ADAM; Viral PANCHAL; Eugene ROZUMOV

    2016-01-01

    The U.S. military has a need for more powerful propellants with balanced/stoichiometric amounts of fuel and oxidants. However, balanced and more powerful propellants lead to accelerated gun barrel erosion and markedly shortened useful barrel life. Boron nitride (BN) is an interesting potential additive for propellants that could reduce gun wear effects in advanced propellants (US patent pending 2015-026P). Hexagonal boron nitride is a good lubricant that can provide wear resistance and lower flame temperatures for gun barrels. Further, boron can dope steel, which drastically improves its strength and wear resistance, and can block the formation of softer carbides. A scalable synthesis method for producing boron nitride nano-particles that can be readily dispersed into propellants has been developed. Even dispersion of the nano-particles in a double-base propellant has been demonstrated using a solvent-based processing approach. Stability of a composite propellant with the BN additive was verified. In this paper, results from propellant testing of boron nitride nano-composite propellants are presented, including closed bomb and wear and erosion testing. Detailed characterization of the erosion tester substrates before and after firing was obtained by electron microscopy, inductively coupled plasma and x-ray photoelectron spectroscopy. This promising boron nitride additive shows the ability to improve gun wear and erosion resistance without any destabilizing effects to the propellant. Potential applications could include less erosive propellants in propellant ammunition for large, medium and small diameter fire arms.

  18. Boronization of Russian tokamaks from carborane precursors

    International Nuclear Information System (INIS)

    A new and cheap boronization technique using the nontoxic and nonexplosive solid substance carborane has been developed and successfully applied to the Russian tokamaks T-11M, T-3M, T-10 and TUMAN-3. The glow discharge in a mixture of He and carborane vapor produced the amorphous B/C coating with the B/C ratio varied from 2.0-3.7. The deposition rate was about 150 nm/h. The primary effect of boronization was a significant reduction of the impurity influx and the plasma impurity contamination, a sharp decrease of the plasma radiated power, and a decrease of the effective charge. Boronization strongly suppressed the impurity influx caused by additional plasma heating. ECR- and ICR-heating as well as ECR current drive were more effective in boronized vessels. Boronization resulted in a significant extension of the Ne- and q-region of stable tokamak operation. The density limit rose strongly. In Ohmic H-mode energy confinement time increased significantly (by a factor of 2) after boronization. It rose linearly with plasma current Ip and was 10 times higher than Neo-Alcator time at maximum current. ((orig.))

  19. Fano interference of the Raman phonon in heavily boron-doped diamond films grown by chemical vapor deposition

    International Nuclear Information System (INIS)

    A series of boron-doped polycrystalline diamond films grown by direct current and microwave plasma deposition was studied with Raman and infrared (IR) absorption spectroscopy. A Fano line shape is observed in the Raman spectra for films with a boron concentration in a narrow range near 1021 cm-3. The appearance of the Fano line shape is correlated with the disappearance of discrete electronic transitions of the boron acceptor observed in the IR spectrum and the shift of the broadened peak to lower energy. The Fano interaction is attributed to a quantum mechanical interference between the Raman phonon (0.165 eV) and transitions from the broadened impurity band to continuum states composed of excited acceptor and valence band states

  20. Counter-diffusion and counter-permeation of deuterium and hydrogen through palladium

    International Nuclear Information System (INIS)

    Experiments for counter-diffusion and counter-permeation of deuterium and hydrogen through a palladium membrane (25 μm thick) were performed. Deuterium permeation rates as a function of upstream D2 pressure were measured under condition where hydrogen permeated in the opposite direction by supplying H2 gas at the 'other' side (downstream, corresponding to D permeation) of the membrane. It was found that significant deuterium permeation occurred even when the deuterium upstream pressure was much smaller than the hydrogen downstream pressure. The deuterium permeation rate was gradually reduced by increasing the downstream H2 pressure and the corresponding counter H permeation. The deuterium permeation rate under counter H permeation can be represented reasonably well by a simple model in which the ratio of the deuterium permeation rates with and without counter H permeation are assumed to be proportional to the fractional concentration of deuterium in the bulk. However, as the hydrogen counter flow increases, the deuterium permeation rate deviates from the model. This implies that adsorption (absorption) of D2 from the gas phase may be inhibited, and also surface recombination of deuterium may be blocked by hydrogen. (orig.)

  1. Synthesis and properties of low-carbon boron carbides

    International Nuclear Information System (INIS)

    This paper reports on the production of boron carbides of low carbon content (3 and CCl4 at 1273-1673 K in a chemical vapor deposition (CVD) reactor. Transmission electron microscopy (TEM) revealed that phase separation had occurred, and tetragonal boron carbide was formed along with β-boron or α-boron carbide under carbon-depleted gas-phase conditions. At temperatures greater than 1390 degrees C, graphite substrates served as a carbon source, affecting the phases present. A microstructure typical of CVD-produced α-boron carbide was observed. Plan view TEM of tetragonal boron carbide revealed a blocklike structure

  2. Development of magnetic resonance technology for noninvasive boron quantification

    International Nuclear Information System (INIS)

    Boron magnetic resonance imaging (MRI) and spectroscopy (MRS) were developed in support of the noninvasive boron quantification task of the Idaho National Engineering Laboratory (INEL) Power Burst Facility/Boron Neutron Capture Therapy (PBF/BNCT) program. The hardware and software described in this report are modifications specific to a GE Signa trademark MRI system, release 3.X and are necessary for boron magnetic resonance operation. The technology developed in this task has been applied to obtaining animal pharmacokinetic data of boron compounds (drug time response) and the in-vivo localization of boron in animal tissue noninvasively. 9 refs., 21 figs

  3. Neutron proportional counter with low self-background level

    International Nuclear Information System (INIS)

    It is suggested to cover the inner surface of neutron counter with α-absorption substance layer to reduce level of self-background of neutron counter filled with 3He+30Ar mixture. Application of 50-60 mm thickness fluoroplastic cover turned to be the most perspective. Analysis of energy spectra within 1-10 MeV energy range has shown, that neutron counters with fluoroplastic cover have the background level by one order less, than counters without cover

  4. Expanded uncertainty in measurements of Geiger-Mueller's counter

    International Nuclear Information System (INIS)

    This paper explains the procedure of obtaining expanded uncertainty in measurement for four types of GM counters with the same counter's tube in cases when the contributors of uncertainties in measurement are cosmic background radiation and induced overvoltage phenomenon. According to experiment and obtained experimental results it is established that uncertainties of influenced random variables depend on technological solution of counter and for that purpose they give different contribution to expanded uncertainty in measurement of applied GM counters

  5. A novel method of boron delivery using sodium iodide symporter for boron neutron capture therapy

    International Nuclear Information System (INIS)

    Boron Neutron Capture Therapy (BNCT) effectiveness depends on the preferential sequestration of boron in cancer cells relative to normal tissue cells. We present a novel strategy for sequestering boron using an adenovirus expressing the sodium iodide symporter (NIS). Human glioma grown subcutaneously in athymic mice and orthotopic rat brain tumors were transfected with NIS using a direct tumor injection of adenovirus. Boron bound as sodium tetrafluoroborate (NaBF4) was administered systemically several days after transfection. Tumors were excised hours later and assessed for boron concentration using inductively coupled plasma atomic emission spectroscopy. In the human glioma transfected with NIS, boron concentration was more than 10 fold higher with 100 mg/kg of NaBF4, compared to tumor not transfected. In the orthotopic tumor model, the presence of NIS conferred almost 4 times the boron concentration in rat tumors transfected with human virus compared with contralateral normal brain not transfected. We conclude that adenovirus expressing NIS has the potential to be used as a novel boron delivery agent and should be explored for future clinical applications. (author)

  6. Spectromicroscopy of boron for the optimization of boron neutron capture therapy (BNCT) for cancer

    International Nuclear Information System (INIS)

    We used synchrotron spectromicroscopy to study the microscopic distribution of boron in rat brain tumour and healthy tissue in the field of boron neutron capture therapy (BNCT). The success of this experimental cancer therapy depends on the preferential uptake of 10B in tumour cells after injection of a boron compound (in our case B12H11SH, or BSH). With the Mephisto (microscope a emission de photoelectrons par illumination synchrotronique de type onduleur) spectromicroscope, high-magnification imaging and chemical analysis was performed on brain tissue sections from a rat carrying an implanted brain tumour and the results were compared with inductively coupled plasma-atomic emission spectroscopy (ICP-AES) detection of boron in bulk tissue. Boron was found to have been taken up more favourably by regions of tumour rather than healthy tissue, but the resulting boron distribution in the tumour was inhomogeneous. The results demonstrate that Mephisto can perform microchemical analysis of tissue sections, detect and localize the presence of boron with submicron spatial resolution. The application of this technique to boron in brain tissue can therefore be used to evaluate the current efforts to optimize BNC therapy. (author)

  7. Proceedings of workshop on 'boron science and boron neutron capture therapy'

    Energy Technology Data Exchange (ETDEWEB)

    Kitaoka, Y. [ed.

    1998-12-01

    This volume contains the abstracts and programs of the 8th (1996), 9th (1997) and 10th (1998) of the workshop on 'the Boron Science and Boron Neutron Capture Therapy' and the recent progress reports especially subscribed. The 11 of the presented papers are indexed individually. (J.P.N.)

  8. Efficiency calibration of solid track spark auto counter

    International Nuclear Information System (INIS)

    The factors influencing detection efficiency of solid track spark auto counter were analyzed, and the best etch condition and parameters of charge were also reconfirmed. With small plate fission ionization chamber, the efficiency of solid track spark auto counter at various experiment assemblies was re-calibrated. The efficiency of solid track spark auto counter at various experimental conditions was obtained. (authors)

  9. 21 CFR 870.5225 - External counter-pulsating device.

    Science.gov (United States)

    2010-04-01

    ... 21 Food and Drugs 8 2010-04-01 2010-04-01 false External counter-pulsating device. 870.5225... counter-pulsating device. (a) Identification. An external counter-pulsating device is a noninvasive device used to assist the heart by applying positive or negative pressure to one or more of the body's...

  10. 21 CFR 864.5200 - Automated cell counter.

    Science.gov (United States)

    2010-04-01

    ... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Automated cell counter. 864.5200 Section 864.5200....5200 Automated cell counter. (a) Identification. An automated cell counter is a fully-automated or semi... corpuscular hemoglobin concentration). These devices may use either an electronic particle counting method...

  11. A quantitative comparison between electrocoagulation and chemical coagulation for boron removal from boron-containing solution

    Energy Technology Data Exchange (ETDEWEB)

    Yilmaz, A. Erdem [Atatuerk University, Faculty of Engineering, Department of Environmental Engineering, 25240 Erzurum (Turkey)], E-mail: aerdemy@atauni.edu.tr; Boncukcuoglu, Recep [Atatuerk University, Faculty of Engineering, Department of Environmental Engineering, 25240 Erzurum (Turkey); Kocakerim, M. Muhtar [Atatuerk University, Faculty of Engineering, Department of Chemical Engineering, 25240 Erzurum (Turkey)

    2007-10-22

    This paper provides a quantitative comparison of electrocoagulation and chemical coagulation approaches based on boron removal. Electrocoagulation process delivers the coagulant in situ as the sacrificial anode corrodes, due to a fixed current density, while the simultaneous evolution of hydrogen at the cathode allows for pollutant removal by flotation. By comparison, conventional chemical coagulation typically adds a salt of the coagulant, with settling providing the primary pollutant removal path. Chemical coagulation was carried out via jar tests using aluminum chloride. Comparison was done with the same amount of coagulant between electrocoagulation and chemical coagulation processes. Boron removal obtained was higher with electrocoagulation process. In addition, it was seen that chemical coagulation has any effect for boron removal from boron-containing solution. At optimum conditions (e.g. pH 8.0 and aluminum dose of 7.45 g/L), boron removal efficiencies for electrocoagulation and chemical coagulation were 94.0% and 24.0%, respectively.

  12. A quantitative comparison between electrocoagulation and chemical coagulation for boron removal from boron-containing solution

    International Nuclear Information System (INIS)

    This paper provides a quantitative comparison of electrocoagulation and chemical coagulation approaches based on boron removal. Electrocoagulation process delivers the coagulant in situ as the sacrificial anode corrodes, due to a fixed current density, while the simultaneous evolution of hydrogen at the cathode allows for pollutant removal by flotation. By comparison, conventional chemical coagulation typically adds a salt of the coagulant, with settling providing the primary pollutant removal path. Chemical coagulation was carried out via jar tests using aluminum chloride. Comparison was done with the same amount of coagulant between electrocoagulation and chemical coagulation processes. Boron removal obtained was higher with electrocoagulation process. In addition, it was seen that chemical coagulation has any effect for boron removal from boron-containing solution. At optimum conditions (e.g. pH 8.0 and aluminum dose of 7.45 g/L), boron removal efficiencies for electrocoagulation and chemical coagulation were 94.0% and 24.0%, respectively

  13. Ceramic silicon-boron-carbon fibers from organic silicon-boron-polymers

    Science.gov (United States)

    Riccitiello, Salvatore R. (Inventor); Hsu, Ming-Ta S. (Inventor); Chen, Timothy S. (Inventor)

    1993-01-01

    Novel high strength ceramic fibers derived from boron, silicon, and carbon organic precursor polymers are discussed. The ceramic fibers are thermally stable up to and beyond 1200 C in air. The method of preparation of the boron-silicon-carbon fibers from a low oxygen content organosilicon boron precursor polymer of the general formula Si(R2)BR(sup 1) includes melt-spinning, crosslinking, and pyrolysis. Specifically, the crosslinked (or cured) precursor organic polymer fibers do not melt or deform during pyrolysis to form the silicon-boron-carbon ceramic fiber. These novel silicon-boron-carbon ceramic fibers are useful in high temperature applications because they retain tensile and other properties up to 1200 C, from 1200 to 1300 C, and in some cases higher than 1300 C.

  14. Boron-11 NMR spectroscopy of excised mouse tissues after infusion of boron compound used in neutron capture therapy

    International Nuclear Information System (INIS)

    Boron neutron capture therapy (BNCT) is based on selective boron uptake by the tumor and in situ activation by neutron beam. The authors propose the use of B-11 MR spectroscopy to noninvasively study boron uptake in animal tumor models. Sodium mercaptoundeca-hydrododecaborate was infused into female BALB/cJ mice and liver, brain, spleen, kidney, and tumor tissues were excised for MR (27.4MHz) and total boron content measurements. Boron-11 was easily detectable in tumor, liver, spleen, and skin. The results gave a very good correlation (correlation coefficient of .997) between B-11 MR measurements and total boron content of excised mouse tissues

  15. Effect of Results on the Calibration of the On-line Liquid Automatic Particle Counter for the Multi-pass Method of the Filter Paper%在线液体颗粒计数器的校准对滤纸多次通过试验结果的影响

    Institute of Scientific and Technical Information of China (English)

    刘尧军; 梁云; 曾靖山; 沈栋

    2011-01-01

    Before and after of the calibration of the automatic particle counter, the change of five dimensions of the particle is analyzed. The effect of this change for the multi-pass test was validated by the experiment. And the average filtration ration before of the calibration was lower than that of after the calibration. At the same time, it was analyzed and pointed out that the negative effect of the test result when the coefficient of the compensation was used instead of the calibration of the automatic particle counter. It is made sure that the experiment system needed to be calibrated in the stated time.%分析了颗粒计数器校准前、后5种尺寸的颗粒数变化情况,并用实验验证了颗粒计数器的校准对滤纸多通试验结果的影响,校准前平均过滤比值均低于校准后的值.此外,分析说明了用颗粒数补偿法来替代颗粒计数器校准会降低试验结果的准确性,明确了定期对颗粒计数器进行校准的重要性.

  16. Simultaneous determination of boron-10 and boron-11 under proton bombardment

    International Nuclear Information System (INIS)

    The isotopic analysis of boron gained importance with increased use of boron-10 in nuclear technology. Former techniques for determining the stable boron isotope either were limited to the determination of a single isotope or required tedious experimental prodecure. The use of proton induced reactions was therefore investigated as an alternative method for the simultaneous analysis of both stable isotopes of boron through a relatively simple experimental procedure. Aqueous solutions of natural boric acid (19,78 at. % 10B) and enriched boric acid (92,41 at. % 10B) were mixed and evaporated to dryness in order to obtain samples in which the isotopic concentration of boron was known. Thin targets were produced by evaporating boron oxide, converted by heat from the boric acid mixture, onto tantalum backing material. Standard samples with known contents of boron oxide were prepared by dry mixing standard reference boron-containing glass powers in a ball mill. Thick targets containing boron of different isotopic compositions were prepared in matrices of potassium bromide and of ion-exchange resins by mixing the matrix with aqueous solutions of boric acid and of sodium carbonate by fusion with boric oxide. The most intense prompt gamma-rays emitted from boron isotopes under irradiation with protons up to 4,5 MeV were the 428-KeV 10B α(1,0), 718-KeV 10B p(1,0) and the 2124-KeV 11B p(1,0) gamma-rays. Excitation functions for the production of each of these were measured using both thick and thin targets

  17. Scintillation Counters for Neutron Scattering Experiments

    International Nuclear Information System (INIS)

    Scintillation counters discussed in this paper are of two types : (i) UP or B2O3 fixed with zinc sulphide in varving composition, (ii) Li containing glasses of varying composition. The ideal composition of each rype for neutron scattering experiments and their relative sensitivity tae neutrons and γ-rays are considered. The ZnS type can be used with a γ-ray pulse shape discriminator and practical experience of its use in a multi-counter time-of-flight experiment is described. The Li glass has higher γ-background but also higher neutron efficiency. Performance figures of a scintillator containing 25% by wt. Li2O and 1 mm thick will be given. (author)

  18. Study on characteristics of Ladu counter

    International Nuclear Information System (INIS)

    The angular response, the radial differential response, the energy response and the distribution of neutron counting rate inside sphere cavity of the Ladu counter are measured, and the effective centre is estimated. The angular responses remain within 5%. The radial differential responses are consistent with those of solid spherical detector. Under the conditions that source distances are five times more than the radius of the counter, the error is less than 0.7% while the difference between effective centre and geometrical centre is ignored. Inside the sphere cavity, the ratio of ultra thermal neutron counting rate to thermal one is less than 10%, but the counting rates slightly depend on the position of thermal neutron detector. In the energy range from 200 eV to 5 MeV, the energy response values extend horizontally within +- 18%

  19. Recalibration of the Cameco mobile lung counter.

    Science.gov (United States)

    Kramer, Gary H; Hauck, Barry; Allen, Steve A

    2009-06-01

    The Cameco lung counter has been recalibrated using the Lawrence Livermore National Laboratory torso phantom using an extended lung set (i.e., longer than the original set). The previous calibration had used the Japanese Atomic Energy Research Institute torso phantom. The new calibration had lower counting efficiencies and, as a result, higher minimum detectable activities. The recalibrated Cameco lung counter was used to measure an extended lung set that had the volume reduced by using modified planar inserts for the sliced lungs as the extended lung set has a lung volume that is larger than Reference Man. This work has shown that sliced lungs can be used to alter the characteristics of the phantom's lung inserts substantially and provide flexibility in measurements previously not recognized. PMID:19430220

  20. Securitization and Counter-Securitization in Afghanistan

    OpenAIRE

    Stritzel, Holger; Chang, Sean C

    2015-01-01

    This article confronts securitization theory with the war in Afghanistan and thus explores questions and dynamics of securitization in a specific communicative situation of military combat. The confrontation highlights not only less well researched questions of implementation, resistance, legitimacy and difficulties of establishing authority in securitizations, but it also inspires a conceptualization of counter-securitization within the theory. In Afghanistan sovereign power to control and r...

  1. Reflexivity, social transformation, and counter culture

    OpenAIRE

    Cox, Laurence

    1997-01-01

    This paper attempts to identify how reflexivity works within the local rationalities of social movement milieux that, it is argued, represent an important source of the development of reflexivity in contemporary lifeworlds. In interviews in the Dublin counter culture, reflexivity appears above all as the institutionalisation of autonomy, the creation of new social forms for self-determined purposes. A starting point is strategies of distancing from the taken-for-granted assumptions of in...

  2. Reforms and counter-reforms in Bolivia

    OpenAIRE

    Jemio, Luis Carlos; Candia, Fernando; Evia, Jose Luis

    2009-01-01

    This paper analyzes reforms and counter-reforms in Bolivia in recent decades and their effects on the policymaking process (PMP) and productivity. Bolivia’s PMP has shifted from a formal representative democracy to a “participative and direct type of democracy” where street protest and other non-conventional forms of political participation have become dominant. While reforms have increased productivity, they have failed to secure the political support necessary to assure long-term sustainabi...

  3. Gunnislake Fish Counter Annual Report 2002

    OpenAIRE

    2003-01-01

    This is the Gunnislake Fish Counter Annual Report 2002 from the Environment Agency South West Region, which was held on March 2002. It presents the daily upstream counts of migratory salmonids recorded on the River Tamar at Gunnislake Weir fish counting station in 2002. The data within this report covers the period of the commercial migratory salmonid net buy-back scheme and the National Spring Salmon Bylaws. The report contains section on Net Buy-Back; Species Apportionment; Validation of co...

  4. Clearing over-the-counter derivatives

    OpenAIRE

    Ed Nosal

    2011-01-01

    Prior to the financial crisis of 2008, the over-the-counter derivatives market was not required to “clear” transactions. This changed with the signing of the new financial reform legislation, the Dodd–Frank Act on July 21, 2010. Going forward, most OTC derivatives will be cleared through a particular set of institutional arrangements: a regulated clearinghouse. This article provides an overview of how clearing works, the potential benefits of central clearing for OTC derivatives, and the opti...

  5. An ellipsoidal grid gas proportional scintillation counter

    OpenAIRE

    Silva, Rui M. C.; Santos, J. M. F. dos; Conde, C. A. N.

    1999-01-01

    Gas Proportional Scintillation Counters using curved grids for solid angle and reflection compensation have been described in the recent literature. They allow large radiation windows with diameters of 25 mm keeping at the same time the good energy resolutions characteristic of those X-ray detectors. However, the grids used have a spherical curvature, which does not correspond to the optimal curvature. In the present work we have calculated by computer simulation an improved shape for the cur...

  6. Use of silica aerogel in Cherenkov counters

    International Nuclear Information System (INIS)

    Silica aerogel has been widely used as a radiator for Cherenkov detectors. The review is devoted to the consideration of various aspects concerning aerogel: its production methods, optical and physical properties, including transparency, absorption, and scattering lengths, the number of photoelectrons and also factors affecting the accuracy of particle identification. The use of silica aerogel in various threshold Cherenkov counters as BELLE (KEK), TASSO (DESY), KEDR (VEPP-4M) is described

  7. Tests of a silica aerogel Cherenkov counter

    International Nuclear Information System (INIS)

    A Cherenkov counter with silica aerogel of refractive index 1.06 as radiator has been constructed and tested. The Cherenkov light produced in 9 cm thick silica aerogel was detected with four 5''-photomultipliers through a 162 cm long air light guide. The photoelectron yield for a 1 GeV/c pion beam was found to be 6 and uniform over a sensitive area of 40 x 30 cm2. (orig.)

  8. Protection of Human Rights in Countering Terrorism

    OpenAIRE

    Yu Nie

    2009-01-01

    Although the violent action occurred increasingly in the world, the definition of terrorism has not come into consensus yet. In countering terrorism, human right protection for the terrorist suspects should also be guaranteed, for the “fair” trial and the minimum procedural guarantees are the basic element of the rule of law. Moreover, the terrorist suspects should be protected by the minimum standard of the fair trial even if before the military commission. Because the minimum due process gu...

  9. Nonlinear Doppler - Free comb-spectroscopy in counter-propagating fields

    CERN Document Server

    Pulkin, S A; Arnautov, V; Uvarova, S V; Savel'eva, S

    2014-01-01

    The method of Doppler - free comb - spectroscopy for dipole transitions was proposed. The calculations for susceptibility spectrum for moving two-level atoms driving by strong counter propagating combs have been done. The used theoretical method based on the Fourier expansion of the components of density matrix on two rows on kv (v-velocity of group of atoms, k-projection of wave vector) and {\\Omega} (frequency between comb components). For testing of validity of this method the direct numerical integration was done. The narrow peaks with homogeneous width arise on the background of Doppler counter. The contrast of these peaks is large for largest amplitudes of comb-components. Power broadening is increasing with increase of field amplitudes. The spectral range of absorption spectrum is determined by the spectral range of comb generator and all homogeneous lines arise simultaneously. The spectral resolution is determined by the width of homogeneously-broadening lines. The physical nature of narrow peaks is in...

  10. The GlueX Start Counter

    Science.gov (United States)

    Pooser, Eric; GlueX Collaboration

    2015-04-01

    The GlueX experiment will study meson photoproduction with unprecedented precision. This experiment will use the coherent bremsstrahlung technique to produce a 9 GeV linearly polarized photon beam incident on a liquid H2 target. A Start Counter detector has been fabricated to identify the accelerator electron beam buckets, approximately 2 ns apart, and to provide accurate timing information which is used in the level-1 trigger of the experiment. This detector is designed to operate at photon intensities of up to 108 γ / s in the coherent peak and provide a timing resolution electron beam buckets to within 99 % accuracy. Furthermore, the Start Counter detector will provide excellent solid angle coverage, ~ 90 % of 4 π hermeticity , and a high degree of segmentation for background rejection. It consists of a cylindrical array of 30 scintillators with pointed ends that bend towards the beam at the downstream end. Silicon PhotoMultiplier (SiPM) detectors have been selected as the readout system. The physical properties of the Start Counter have been studied extensively. The results of theses studies are discussed. This material is based upon work supported by the U.S. Department of Energy, Office of Science, Office of Nuclear Physics under Contracts DE-AC05-06OR23177 & DE-FG02-99ER41065.

  11. Which future for nuclear counter-proliferation?

    International Nuclear Information System (INIS)

    Dealing with the case of nuclear weapons possessed by nuclear states (but not eventually by terrorists), the author first identifies the constants of counter-proliferation: it is linked to interest conflicts between those who try to preserve their monopoly and those who try to acquire a new weapon either because of a threat or for reasons of regional prestige, the evolution from use to deterrence, the appearance of new actors after the USA and Russia, the role of nuclear tactical weapons, and the future of Russian weapons and know-how. He presents the international counter-proliferation context: the Non Proliferation Treaty (NPT), the IAEA and its controls, the Nuclear Supplier Group (NSG), the nuclear-free zones, the Comprehensive Test Ban Treaty (CTBT), the Missile Technology Control Regime (MTCR). He describes how and why proliferation occurs: uranium enrichment and plutonium technology, political reasons in different parts of the world. Then, he gives an overview of the proliferation status by commenting the cases of Israel, Iraq, India, Pakistan, North Korea, and Iran. He discusses the future of proliferation (involved countries, existence of a nuclear black market) and of counter-proliferation as far as Middle-East and North Korea are concerned. He tries finally to anticipate the consequences for nuclear deterrence strategy, and more particularly for Europe and France

  12. Development of aerogel Cherenkov counters at Novosibirsk

    International Nuclear Information System (INIS)

    The work on aerogel Cherenkov counters was started in Novosibirsk in 1986. Production of aerogels with refractive indices of 1.006-1.13 and thicknesses of blocks up to 50mm was developed. The light absorption length at 400nm is 5-7m, the scattering length is 4-5cm. By these parameters, the Novosibirsk aerogel is one of the best in the world. The ASHIPH Cherenkov counters with light collection on wavelength shifters have been developed. The ASHIPH system of the KEDR detector contains 1000l of aerogel. The π/K separation is 4.5σ. A project of ASHIPH counters for the SND detector has been developed. Aerogel RICH for LHCb gives a possibility to identify hadrons in the momentum range of 2-10GeV/c. The Novosibirsk group is developing an aerogel RICH for the endcap for the SuperBaBar project. Calculations performed by a group of physicists from Novosibirsk and DESY-Zeuthen have shown that aerogel radiators enable to achieve time resolution up to 20fs

  13. Boron Depletion in F and G Dwarf Stars and the Beryllium-Boron Correlation

    CERN Document Server

    Boesgaard, A M; Steinhauer, A; Boesgaard, Ann Merchant; Deliyannis, Constantine P.; Steinhauer, Aaron

    2004-01-01

    Boron provides a special probe below the stellar surface as it survives to greater depths than do Li and Be. To search for B depletions we have observed B in 13 F and G dwarfs with large Be depletions; for comparison we also obtained spectra of five stars which are undepleted in Li and Be. We have used HST with STIS to obtain spectra of the B I resonance line at 2497 \\AA. The spectral resolution is 30,000 or 114,000 and the median signal-to-noise ratio is 70 per pixel. New Be and Li spectra have been obtained at Keck I with HIRES of four of the five standard stars at $\\sim$48,000 resolution. Abundances have been determined by the spectrum synthesis method with MOOG. A comparison between the standard stars and those with severe Be depletions shows a distinct difference in the B abundances between the two groups of 0.22 dex. We have discovered a correlation between the Be and B abundances. The slope between A(Be) and A(B)$_{NLTE}$ is 0.22 $\\pm$0.05 (where A(element) = log N(element)/N(H) + 12.00) which, as expe...

  14. Boron: out of the sky and onto the ground

    International Nuclear Information System (INIS)

    Now an accepted, engineered material for aerospace applications, boron is taking its place on the ground. Both current production applications, prototype (development) applications, and speculative applications abound. In the leisure product market, boron epoxy or boron aluminum has been used or tried in golf clubs (in combination with graphite epoxy or to reinforce aluminum or steel), in tennis racquets, in bicycles, racing shells, skis and skipoles, bows and arrows, and others. In the industrial area, boron has been used to reduce fatigue, increase stiffness, or for its abrasive properties. Textile machinery, honing tools, and cut off wheels or saws are among the applications. In the medical field, prosthetics and orthotic braces, wheel chairs, canes, and crutches are all good applications for boron. Applications for boron in transportation, construction, and heavy industry are also possible. The volume of boron used in these applications could have a major impact on prices, making boron composite parts cost competitive with conventional materials. (U.S.)

  15. 15th International Conference on Boron Chemistry (IMEBORON XV)

    Czech Academy of Sciences Publication Activity Database

    Grüner, Bohumír; Štíbr, Bohumil

    2015-01-01

    Roč. 87, č. 2 (2015), s. 121. ISSN 0033-4545 Institutional support: RVO:61388980 Keywords : boranes * boron * boron materials * carboranes * IMEBORON XV * medicinal chemistry Subject RIV: CA - Inorganic Chemistry

  16. Boron Removal in Seawater Reverse Osmosis System

    KAUST Repository

    Rahmawati, Karina

    2011-07-01

    Reverse osmosis successfully proves to remove more than 99% of solute in seawater, providing fresh water supply with satisfied quality. Due to some operational constraints, however, some trace contaminants removal, such as boron, cannot be achieved in one pass system. The stringent criterion for boron from World Health Organization (WHO) and Saudi Arabia local standard (0.5 mg/l) is hardly fulfilled by single pass sea water reverse osmosis (SWRO) plants. Some design processes have been proposed to deal with boron removal, but they are not economically efficient due to high energy and chemical consumption. The objective of this study was to study boron removal by different reverse osmosis membranes in two pH conditions, with and without antiscalant addition. Thus, it was expected to observe the possibility of operating single pass system and necessity to operate two pass system using low energy membrane. Five membrane samples were obtained from two different manufacturers. Three types of feed water pH were used, pH 8, pH 10, and pH 10 with antiscalant addition. Experiment was conducted in parallel to compare membrane performance from two manufacturers. Filtration was run with fully recycle mode for three days. Sample of permeate and feed were taken every 12 hours, and analyzed for their boron and TDS concentration. Membrane samples were also tested for their surface charge. The results showed that boron rejection increases as the feed pH increases. This was caused by dissociation of boric acid to negatively charged borate ion and more negatively charged membrane surface at elevated pH which enhance boron rejection. This study found that single pass reverse osmosis system, with and without elevating the pH, may not be possible to be applied because of two reasons. First, permeate quality in term of boron, does not fulfill WHO and local Saudi Arabia regulations. Second, severe scaling occurs due to operation in alkaline condition, since Ca and Mg concentration are

  17. ICRF Impurity Behavior with Boron Coated Molybdenum Tiles in Alcator C-Mod

    International Nuclear Information System (INIS)

    Full text: Although ion cyclotron range of frequency (ICRF) heating is considered an excellent candidate for bulk heating, minimizing impurity production associated with ICRF operation, particularly with metallic plasma facing components (PFC), remains one of the primary challenges for ICRF utilization. In C-Mod and present experiments, boronization, an in-situ applied boron film, is utilized to control impurities and its effectiveness has a limited lifetime. In C-Mod, the lifetime has been observed to be proportional to integrated injected RF Joules and the degradation is faster than in equivalent ohmic heated discharges the ICRF is enhancing the erosion rate of the boron film. In an effort to identify important erosion and impurity source locations, we have vacuum plasma sprayed ∼ 100 microns of boron on molybdenum tiles from the outer divertor shelf, main plasma limiters, and the RF antennas. We have also modified the shape of the main plasma limiter and increased our spectroscopic monitoring diagnostics of the main plasma limiter. Finally, we have installed a set of probes to monitor the plasma potential and RF fields on field lines connected an antenna. For ICRF heated H-modes, the core molybdenum levels was significantly reduced and remained at low levels for increased integrated injected RF Joules. The core molybdenum levels also no longer scales with RF power in L-mode in contrast with previous results with boronization and molybdenum plasma facing components. Initial Post campaign analysis of the boron coating will also be presented. Boronization and impurity, typically nitrogen or neon, seeded discharges enabled high plasma and ICRF antenna performance. The boronization suggests that other impurity sources are important but are yet to be identified. Impurity seeding had two important effects: reduced core molybdenum levels and suppressed antenna faults due to arcs and injections from antenna structure. The lower core molybdenum level is surprising since

  18. Relativistic Static Thin Disks The Counter-Rotating Model

    CERN Document Server

    Espitia, O A; Espitia, Omar A.; Gonzalez, Guillermo A.

    2001-01-01

    A detailed study of the Counter-Rotating Model (CRM) for generic finite static axially symmetric thin disks with nonzero radial pressure is presented. We find a general constraint over the counter-rotating tangential velocities needed to cast the surface energy-momentum tensor of the disk as the superposition of two counter-rotating perfect fluids. We also found expressions for the energy density and pressure of the counter-rotating fluids. Then we shown that, in general, there is not possible to take the two counter-rotating fluids as circulating along geodesics neither take the two counter-rotating tangential velocities as equal and opposite. An specific example is studied where we obtain some CRM with well defined counter-rotating tangential velocities and stable against radial perturbations. The CRM obtained are in agree with the strong energy condition, but there are regions of the disks with negative energy density, in violation of the weak energy condition.

  19. Hardware support for software controlled fast multiplexing of performance counters

    Science.gov (United States)

    Salapura, Valentina; Wisniewski, Robert W.

    2013-01-01

    Performance counters may be operable to collect one or more counts of one or more selected activities, and registers may be operable to store a set of performance counter configurations. A state machine may be operable to automatically select a register from the registers for reconfiguring the one or more performance counters in response to receiving a first signal. The state machine may be further operable to reconfigure the one or more performance counters based on a configuration specified in the selected register. The state machine yet further may be operable to copy data in selected one or more of the performance counters to a memory location, or to copy data from the memory location to the counters, in response to receiving a second signal. The state machine may be operable to store or restore the counter values and state machine configuration in response to a context switch event.

  20. First gaseous boronization during pulsed discharge cleaning

    Energy Technology Data Exchange (ETDEWEB)

    Ko, J., E-mail: jinseok@nfri.re.kr [Department of Physics, University of Wisconsin, Madison, WI (United States); Den Hartog, D.J.; Goetz, J.A.; Weix, P.J.; Limbach, S.T. [Department of Physics, University of Wisconsin, Madison, WI (United States)

    2013-01-15

    The first successful gaseous boronization during a pulsed discharge is reported. Sublimation of o-carborane (C{sub 2}B{sub 10}H{sub 12}) combined with pulsed discharge plasmas with a repetition rate of 1 Hz is used to produce a hard boron-containing coating for reversed field pinch (RFP) plasmas in the Madison Symmetric Torus. X-ray photoelectron spectroscopy with Ar ion beam etching for silicon coupons installed at the plasma boundary shows about 60% boron concentration in the deposited layer. Both profilometer and scanning electron microscope analyses of the silicon coupons imply a strong toroidally non-uniform deposition depending on the location of the o-carborane injection. The layer thickness ranges from 50 to 300 nm. Ellipsometry calibrated with the profilometer results yields a refractive index of 2.2-2.3 for the films. The high refractive index implies that the coating is hard and has a well-ordered morphology. A reduction in wall recycling has consistently been observed after all boronization sessions. Comparison of the X-ray spectra in standard RFP plasmas before and after boronization indicates a slight decrease in the effective ionic charge.

  1. Boron isotope fractionation during brucite deposition from artificial seawater

    OpenAIRE

    J. Xiao; Xiao, Y. K.; Liu, C. Q.; Z. D. Jin

    2011-01-01

    Experiments involving boron incorporation into brucite (Mg(OH)2) from magnesium-free artificial seawater with pH values ranging from 9.5 to 13.0 were carried out to better understand the incorporation behavior of boron into brucite. The results show that both concentration of boron in deposited brucite ([B]d) and its boron partition coefficient (Kd) between deposited brucite and final seawater are controll...

  2. Characterization of boron carbide with an electron microprobe

    Science.gov (United States)

    Matteudi, G.; Ruste, J.

    1983-01-01

    Within the framework of a study of heterogeneous materials (Matteudi et al., 1971: Matteudi and Verchery, 1972) thin deposits of boron carbide were characterized. Experiments using an electronic probe microanalyzer to analyze solid boron carbide or boron carbide in the form of thick deposits are described. Quantitative results on boron and carbon are very close to those obtained when applying the Monte Carlo-type correction calculations.

  3. Technology of boron-containing polyphosphate fertilizer 'Phosphobor'

    International Nuclear Information System (INIS)

    A technology is developed for producing 'Phosphobor' fertilizer based on the rock phosphate weal (17-18% P2O5) with additions of boron-magnesium compound. Boron is part of polyphosphate fertilizer in the form of polymeric compounds of phosphorus and boron. Phosphorus and boron copolymers -boratophosphates - are easily formed in the process of polyphosphate fertilizers production, since borates undergo a mutual polycondensation reaction with phosphates. 8 refs., 1 fig

  4. Glass manufacturing process having boron and fluorine pollution abating features

    Energy Technology Data Exchange (ETDEWEB)

    Froberg, M.L.; Schroeder, C.F.

    1981-11-03

    Boron and/or fluorine values are reclaimed from a boron and/or fluorine laden gas stream emanating from a glass melter by means of a preheating bed of glass-forming batch agglomerates. The boron and/or fluorine values in such gases are first reacted with a boron and/or fluorine reactive material and the gases then conveyed into such a preheating bed to separate at least a portion of the reaction products.

  5. Glass manufacturing process having boron and fluorine pollution abating features

    International Nuclear Information System (INIS)

    Boron and/or fluorine values are reclaimed from a boron and/or fluorine laden gas stream emanating from a glass melter by means of a preheating bed of glass-forming batch agglomerates. The boron and/or fluorine values in such gases are first reacted with a boron and/or fluorine reactive material and the gases then conveyed into such a preheating bed to separate at least a portion of the reaction products

  6. Unveiling the counter-rotating nature of the kinematically distinct core in NGC5813 with MUSE

    CERN Document Server

    Krajnovic, Davor; Urrutia, Tanya; Emsellem, Eric; Carollo, C Marcella; Shirazi, Maryam; Bacon, Roland; Contini, Thierry; Epinat, Benoit; Kamann, Sebastian; Martinsson, Thomas; Steinmetz, Matthias

    2015-01-01

    MUSE observations of NGC5813 reveal a complex structure in the velocity dispersion map, previously hinted by SAURON observations. The structure is reminiscent of velocity dispersion maps of galaxies comprising two counter-rotating discs, and may explain the existence of the kinematically distinct core (KDC). Further evidence for two counter-rotating components comes from the analysis of the higher moments of the stellar line-of-sight velocity distributions and fitting MUSE spectra with two separate Gaussian line-of-sight velocity distributions. The emission-line kinematics show evidence of being linked to the present cooling flows and the buoyant cavities seen in X-rays. We detect ionised gas in a nuclear disc-like structure, oriented like the KDC, which is, however, not directly related to the KDC. We build an axisymmetric Schwarzschild dynamical model, which shows that the MUSE kinematics can be reproduced well with two counter-rotating orbit families, characterised by relatively low angular momentum compon...

  7. The difference in age of the two counter-rotating stellar disks of the spiral galaxy NGC 4138

    CERN Document Server

    Pizzella, Alessandro; Corsini, Enrico Maria; Bontá, Elena Dalla; Coccato, Lodovico; Sanjana, Georgina

    2014-01-01

    The Sa spiral NGC 4138 is known to host two counter-rotating stellar disks, with the ionized gas co-rotating with one of them. We measured the kinematics and properties of the two counter-rotating stellar populations to constrain their formation scenario. A spectroscopic decomposition of the observed major-axis spectrum was performed to disentangle the relative contribution of the two counter-rotating stellar and one ionized-gas components. The line-strength indices of the two counter-rotating stellar components were measured and modeled with single stellar population models that account for the alpha/Fe overabundance. The counter-rotating stellar population is younger, marginally more metal poor, and more alpha-enhanced than the main stellar component. The younger stellar component is also associated with a star-forming ring. The different properties of the counter-rotating stellar components of NGC~4138 rule out the idea that they formed due to bar dissolution. Our findings support the results of numerical ...

  8. Establishment and problem of the observing system for boron in steels by alpha-particle track etching method using pneumatic tube of JRR-3 and JRR-4

    International Nuclear Information System (INIS)

    The addition of small amount of boron to steel is often employed to improve various properties of steel, but there are still many uncertainties in the behavior of boron in steel. It is necessary to clarify the precipitation segregation behaviors of boron to develop advanced steels. Alpha-particle track etching (ATE) method is effective to observe the behaviors of boron, but as the irradiation equipment of Japan Atomic Energy Agency (JAEA) has been more intensively used for medical research and treatment purposes recently, time available for the ATE method has been limited. In this study, ATE method using the pneumatic tube is investigated to make the analysis of boron in steel easier under such condition. Results indicate that JRR-3 'PN-3' equipment of JAEA is the most applicable to the ATE method using the pneumatic tube. Since the ratio of cadmium of PN-3 is 290, the thermal neutron flux is sufficiently high with low level of background. Boron containing precipitates can be detected as dark spots and the grain boundary segregation of boron as dark lines. It is found, however, that the size of the spots in ATE images is not exactly the same as that of actual precipitates. When the ATE images are compared with TEM images using carbon extraction replica, borides are exaggerated as about hundred-times larger precipitates in the ATE images. (author)

  9. Proceedings of workshop on 'boron chemistry and boron neutron capture therapy'

    International Nuclear Information System (INIS)

    This volume contains the proceedings of the 4th Workshop on 'the Boron Chemistry and Boron Neutron Capture Therapy' held on February 24 in 1992. First, clinical experiences of BNCT in the Kyoto University Research Reactor in 1992 were briefly reported. Then, the killing effects of boron cluster-containing nucleic acid precursors on tumor cells were shown (Chap. 2). The various trials of the optical resolution of B-p-boronophenylalanine for neutron capture therapy were made (Chap. 3). The borate-dextran gel complexes were investigated by the nuclear magnetic resonance spectroscopy. The stability constants of borate complexes were listed, and are useful in the solution chemistry of boron compounds (Chap. 4). The interactions between boron compounds and biological materials were studied by the paper electrophoresis which had been developed by us (Chap. 5). Molecular design of boron-10 carriers and their organic synthesis were reported (Chap. 6). Carborane-containing aziridine boron carriers which were directed to the DNA alkylation were synthesized and their cancer cell killing efficacies were tested (Chap. 7). The solution chemistry of deuterium oxide which is a good neutron moderator was reported, relating to the BNCT (Chap. 8). (author)

  10. Synthesis of multiwall boron nitride nanotubes dependent on crystallographic structure of boron

    International Nuclear Information System (INIS)

    Synthesis and growth of multiwall boron nitride nanotubes (BNNTs) under the B and ZrO2 seed system in the milling–annealing process were investigated. BNNTs were synthesized by annealing a mechanically activated boron powder under nitrogen environment. We explored the aspects of the mechanical activation energy transferred to milled crystalline boron powder producing structural disorder and borothermal reaction of the ZrO2 seed particles on the synthesis of BNNTs during annealing. Under these circumstances, the chemical reaction of amorphous boron coated on the seed nanoparticles with nitrogen synthesizing amorphous BN could be enhanced. It was found that amorphous BN was crystallized to the layer structure and then grown to multiwall BNNTs during annealing. Especially, bamboo-type multiwall BNNTs were mostly produced and grown to the tail-side of the nanotube not to the round head-side. Open gaps with ∼0.3 nm of the bamboo side walls of BNNTs were also observed. Based on these understandings, it might be possible to produce bamboo-type multiwall BNNTs by optimization of the structure and shape of boron coat on the seed nanoparticles. -- Highlights: ► Structure of B is a key factor for BNNT synthesis for milling–annealing method. ► Amorphous boron is coated on the seed during milling of crystalline boron. ► Amorphous BN nanoclusters are crystallized during annealing. ► Growing of bamboo BNNTs is not to the round head-side but to the tail-side.

  11. INFLUENCE OF FINE-DISPERSED BORON CARBIDE ON THE STRUCTURE AND CHARACTERISTICS OF IRON-BORON ALLOY

    Directory of Open Access Journals (Sweden)

    N. F. Nevar

    2016-02-01

    Full Text Available The influence of boron carbide as fine-dispersed material input into the melt on structure morphology, founding, technological and exploitation characterisstics of cast iron-boron material is shown.

  12. Colorimetric Sugar Sensing Using Boronic Acid-Substituted Azobenzenes

    Directory of Open Access Journals (Sweden)

    Yuya Egawa

    2014-02-01

    Full Text Available In association with increasing diabetes prevalence, it is desirable to develop new glucose sensing systems with low cost, ease of use, high stability and good portability. Boronic acid is one of the potential candidates for a future alternative to enzyme-based glucose sensors. Boronic acid derivatives have been widely used for the sugar recognition motif, because boronic acids bind adjacent diols to form cyclic boronate esters. In order to develop colorimetric sugar sensors, boronic acid-conjugated azobenzenes have been synthesized. There are several types of boronic acid azobenzenes, and their characteristics tend to rely on the substitute position of the boronic acid moiety. For example, o-substitution of boronic acid to the azo group gives the advantage of a significant color change upon sugar addition. Nitrogen-15 Nuclear Magnetic Resonance (NMR studies clearly show a signaling mechanism based on the formation and cleavage of the B–N dative bond between boronic acid and azo moieties in the dye. Some boronic acid-substituted azobenzenes were attached to a polymer or utilized for supramolecular chemistry to produce glucose-selective binding, in which two boronic acid moieties cooperatively bind one glucose molecule. In addition, boronic acid-substituted azobenzenes have been applied not only for glucose monitoring, but also for the sensing of glycated hemoglobin and dopamine.

  13. Boron-containing amino carboxylic acid compounds and uses thereof

    International Nuclear Information System (INIS)

    Novel compounds which are useful for boron neutron capture therapy (BNCT) are disclosed. The compounds comprise a stable boron-containing group and an aminocycloalkane carboxylic acid group or a boronated acyclic hydrocarbon-linked amino carboxylic acid. Methods for synthesis of the compounds and for use of the compounds in BNCT are disclosed

  14. Consumer Preferences for High Welfare Meat in Germany: Self-service Counter or Service Counter?

    Directory of Open Access Journals (Sweden)

    Ramona Weinrich

    2015-01-01

    Full Text Available Many people view animal welfare standards in the agricultural industry as critical and some consumers would prefer to buy high welfare meat. In order to successfully introduce high welfare meat products onto the market, some important marketing decisions must be made. Due to limited shelf space in retail outlets, niche products like high welfare meat cannot be placed both at the self-service counter and at the service counter. In order to analyze where to place it best an online survey of 642 German consumers was conducted. By means of factor and cluster analyses, consumers’ animal welfare attitudes and their preference for a point of purchase were combined. The different target groups were joint using cross tabulation analysis. The results reveal that consumers in the target group show a more positive attitude to the service counter.

  15. Enhanced Plasma Performance by ICRF Boronization

    Institute of Scientific and Technical Information of China (English)

    万宝年; 赵燕平; 李建刚; 宋梅; 吴振伟; 罗家融; 李成富; 王小明

    2002-01-01

    Boronization with carborane (C2B10H12) by ICRF has been applied routinely to the walls of HT-7 super-conducting tokamak for the reduction of impurity influx, especially carbon and oxygen. Significant suppression of metallic impurities and radiating power fraction are achieved. The improved confinement for both particle and energy is observed in full range of operation parameters. Energy balance analysis shows that electron heat diffusion coefficient is strongly reduced. Measurements by Langmuir probes at the edge plasma show that the poloidal velocity shear after boronization is changed to a profile favoring to good confinement. The main emphasis of this paper is to describe effects of boronization on aspects of the enhanced plasma performance.

  16. Anomalous electronic transport in boron carbides

    Science.gov (United States)

    Emin, D.; Samara, G. A.; Wood, C.

    The boron carbides are composed of icosahedral units, B12 and B11C1, linked together by strong intericosahedral bonds. With such distributions of icosahedral and intericosahedral compositions, boron carbides, B/sub 1-x/C/sub x/, are single phase over 0.1 less than or equal to x less than or equal to 0.2. The electronic transport properties of the boron carbides were examined within this single-phase region. Results are inconsistent with conventional analyses of both itinerant and hopping transport. Most striking are Seebeck coefficients which are both large and rapidly increasing functions of temperature despite thermally activated dc conductivities. These results manifest the hopping of small bipolaronic holes between carbon-containing icosahedral that are inequivalent in energy and electron-lattice coupling strength. Under hydrostatic pressures up to approx. 25 kbar, the dc conductivities increase with pressure. This anomalous behavior for hopping conduction reflects the distinctive structure and bonding of these materials.

  17. Single step synthesis of nanostructured boron nitride for boron neutron capture therapy

    International Nuclear Information System (INIS)

    Nanostructured Boron Nitride (BN) has been successfully synthesized by carbo-thermic reduction of Boric Acid (H3BO3). This method is a relatively low temperature synthesis route and it can be used for large scale production of nanostructured BN. The synthesized nanoparticles have been characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and differential thermal analyzer (DTA). XRD analysis confirmed the formation of single phase nanostructured Boron Nitride. SEM analysis showed that the particles are spherical in shape. DTA analysis showed that the phase is stable upto 900 °C and the material can be used for high temperature applications as well boron neutron capture therapy (BNCT)

  18. Single step synthesis of nanostructured boron nitride for boron neutron capture therapy

    Science.gov (United States)

    Singh, Bikramjeet; Singh, Paviter; Kumar, Manjeet; Thakur, Anup; Kumar, Akshay

    2015-05-01

    Nanostructured Boron Nitride (BN) has been successfully synthesized by carbo-thermic reduction of Boric Acid (H3BO3). This method is a relatively low temperature synthesis route and it can be used for large scale production of nanostructured BN. The synthesized nanoparticles have been characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and differential thermal analyzer (DTA). XRD analysis confirmed the formation of single phase nanostructured Boron Nitride. SEM analysis showed that the particles are spherical in shape. DTA analysis showed that the phase is stable upto 900 °C and the material can be used for high temperature applications as well boron neutron capture therapy (BNCT).

  19. boron and boron nitride coated nuclear fuel production in plasma atmosphere

    International Nuclear Information System (INIS)

    In these study uranium dioxide (UO2) and 5, 10 % gadolinium oxide (Gd2O3) containing UO2 nuclear fuel pellets were coated with first boron nitride (BN) then boron (B) layers as the results of the reactions between boron trichloride (BCl3) with ammonia (NH3) and BCl3 with hydrogen (H2) in the medium of argon (Ar) plasma created at 650 W and 500 W and 27.12 MHz to increase the fuel burnup efficiency and reactor core life by the method of plasma enhanced chemical vapor deposition (PECVD). Grainy BN and B structures were observed on the photographs taken from scanning electron microscope (SEM)

  20. A system to deposit boron films (boronization) in the DIII-D tokamak

    International Nuclear Information System (INIS)

    A system has been added to the D3-D tokamak to coat its plasma facing surfaces with a film of boron using diborane gas. The system includes special health and safety equipment for handling the diborane gas which is toxic and inflammable. The purpose of the boron film is to reduce the levels of impurity atoms in the D3-D plasmas. Experiments following the application of the boron film in D3-D have led to significant reductions in plasma impurity levels and the observation of a new, very high confinement regime. 9 refs., 1 fig

  1. Counter-Narratives and the Unrehearsed Stories Counter-Terrorists Unwittingly Produce

    Directory of Open Access Journals (Sweden)

    Beatrice de Graaf

    2010-11-01

    Full Text Available Governments produce both deliberate and involuntary (and less conscious narratives when countering terrorism. The thesis of this article is that such unintended messages can be much more powerful and consequential than is realized; in fact, they can completely contradict the intended official 'counter-narrative'. To substantiate this hypothesis, the author looks at the experience of the German Federal Republic in the 1970s and beyond when state and society were confronted with the Red Army Faction (RAF and similar left-wing "revolutionaries" like those of the 2nd of June Movement or the Red Zora.

  2. Boron Nitride Nanotubes for Spintronics

    Directory of Open Access Journals (Sweden)

    Kamal B. Dhungana

    2014-09-01

    Full Text Available With the end of Moore’s law in sight, researchers are in search of an alternative approach to manipulate information. Spintronics or spin-based electronics, which uses the spin state of electrons to store, process and communicate information, offers exciting opportunities to sustain the current growth in the information industry. For example, the discovery of the giant magneto resistance (GMR effect, which provides the foundation behind modern high density data storage devices, is an important success story of spintronics; GMR-based sensors have wide applications, ranging from automotive industry to biology. In recent years, with the tremendous progress in nanotechnology, spintronics has crossed the boundary of conventional, all metallic, solid state multi-layered structures to reach a new frontier, where nanostructures provide a pathway for the spin-carriers. Different materials such as organic and inorganic nanostructures are explored for possible applications in spintronics. In this short review, we focus on the boron nitride nanotube (BNNT, which has recently been explored for possible applications in spintronics. Unlike many organic materials, BNNTs offer higher thermal stability and higher resistance to oxidation. It has been reported that the metal-free fluorinated BNNT exhibits long range ferromagnetic spin ordering, which is stable at a temperature much higher than room temperature. Due to their large band gap, BNNTs are also explored as a tunnel magneto resistance device. In addition, the F-BNNT has recently been predicted as an ideal spin-filter. The purpose of this review is to highlight these recent progresses so that a concerted effort by both experimentalists and theorists can be carried out in the future to realize the true potential of BNNT-based spintronics.

  3. Reactive sputter deposition of boron nitride

    International Nuclear Information System (INIS)

    The preparation of fully dense, boron targets for use in planar magnetron sources has lead to the synthesis of Boron Nitride (BN) films by reactive rf sputtering. The deposition parameters of gas pressure, flow and composition are varied along with substrate temperature and applied bias. The films are characterized for composition using Auger electron spectroscopy, for chemical bonding using Raman spectroscopy and for crystalline structure using transmission electron microscopy. The deposition conditions are established which lead to the growth of crystalline BN phases. In particular, the growth of an adherent cubic BN coating requires 400--500 C substrate heating and an applied -300 V dc bias

  4. Can Two-Dimensional Boron Superconduct?

    Science.gov (United States)

    Penev, Evgeni S; Kutana, Alex; Yakobson, Boris I

    2016-04-13

    Two-dimensional boron is expected to exhibit various structural polymorphs, all being metallic. Additionally, its small atomic mass suggests strong electron-phonon coupling, which in turn can enable superconducting behavior. Here we perform first-principles analysis of electronic structure, phonon spectra, and electron-phonon coupling of selected 2D boron polymorphs and show that the most stable structures predicted to feasibly form on a metal substrate should also exhibit intrinsic phonon-mediated superconductivity, with estimated critical temperature in the range of Tc ≈ 10-20 K. PMID:27003635

  5. Thermal conductivity behavior of boron carbides

    Science.gov (United States)

    Wood, C.; Zoltan, A.; Emin, D.; Gray, P. E.

    1983-01-01

    Knowledge of the thermal conductivity of boron carbides is necessary to evaluate its potential for high temperature thermoelectric energy conversion applications. The thermal diffusivity of hot pressed boron carbide B/sub 1-x/C/sub x/ samples as a function of composition, temperature and temperature cycling was measured. These data in concert with density and specific heat data yield the thermal conductivities of these materials. The results in terms of a structural model to explain the electrical transport data and novel mechanisms for thermal conduction are discussed.

  6. Geiger-Muller (GM) counters. Associated circuits and counting techniques

    International Nuclear Information System (INIS)

    This article presents the Geiger-Muller counters which present the great benefit of being simple and steady in comparison with other known sensors. The authors propose an overview of problems related to the use of Geiger-Muller counters (GM counters). They first describe their operation (discharge initiation, discharge propagation, collection of positive ions and current in the counter). They discuss their limitations which are related to the migration delay of primary electrons and positive ions. They describe the operation circuit for counters with organic vapour, and for counters associated with counters using halogens. They address the main properties of GM counters, and the different factors to be taken into account when using them to count radioactive sources. The main types of GM counters are then described (they are used to measure different types of radiation). Measurement techniques are discussed for beta radiation (relationship between the number of disintegrations and the noticed counting rate, case of backscattering, absorption and diffusion in the counter window and in the air, influence of absorption and backscattering in the source), for alpha radiation, and for gamma radiation

  7. Evidence for Defect-Mediated Tunneling in Hexagonal Boron Nitride-Based Junctions.

    Science.gov (United States)

    Chandni, U; Watanabe, K; Taniguchi, T; Eisenstein, J P

    2015-11-11

    We investigate electron tunneling through atomically thin layers of hexagonal boron nitride (hBN). Metal (Cr/Au) and semimetal (graphite) counter-electrodes are employed. While the direct tunneling resistance increases nearly exponentially with barrier thickness as expected, the thicker junctions also exhibit clear signatures of Coulomb blockade, including strong suppression of the tunnel current around zero bias and step-like features in the current at larger biases. The voltage separation of these steps suggests that single-electron charging of nanometer-scale defects in the hBN barrier layer are responsible for these signatures. We find that annealing the metal-hBN-metal junctions removes these defects and the Coulomb blockade signatures in the tunneling current. PMID:26509431

  8. Cerenkov counter for the experiment NA3

    CERN Multimedia

    1978-01-01

    The program of the NA3 experiment included the study of hadronic interactions with a large transverse momentum pT, thus the inclusion in the set-up of three gas threshold Cerenkov counters of large acceptance. The photo shows the downstream part of the second Cerenkov (located at the output of the magnet). The yellow membrane is a temporary protection for the optics (shown in photo 7810540X) to be taken away when fixing this part to the gas tank (entering the magnet and not shown). The photomultipliers all around are heavily shielded.

  9. PRELIMINARY PROGRAMMED WHOLE—BODY COUNTER

    Institute of Scientific and Technical Information of China (English)

    张少东; 郑文忠; 等

    1995-01-01

    It is capable of giving the initial intakes of radionuclides and the assessment quantitites used in radiation protection according to its measured results of radionuclides in vivo.It is accomplished by providing the software of controlling,interface and internal dose estimation programs to the original iron cabin shielding whole-body counter.The preliminary application shows that its data processing is rapid and correct,and can meet the requirement of rapid internal radioactive contamination monitoring and diagnosing in case of lots of internal contamination subjects happened in nuclear accident.

  10. Taxing junk food to counter obesity.

    Science.gov (United States)

    Franck, Caroline; Grandi, Sonia M; Eisenberg, Mark J

    2013-11-01

    We examined the advantages and disadvantages of implementing a junk food tax as an intervention to counter increasing obesity in North America. Small excise taxes are likely to yield substantial revenue but are unlikely to affect obesity rates. High excise taxes are likely to have a direct impact on weight in at-risk populations but are less likely to be politically palatable or sustainable. Ultimately, the effectiveness of earmarked health programs and subsidies is likely to be a key determinant of tax success in the fight against obesity. PMID:24028245

  11. Test of lead glass shower counters

    International Nuclear Information System (INIS)

    Lead glass counters made of wedge shaped blocks of SF6 were tested with positrons at SLAC. The beam energy ranged from 2 to 17.5 GeV. Energy dependence and beam position dependence of pulse height and energy resolution were studied with lead glass blocks of various lengths. The effect of a BK-7 light guide on pulse height was clearly observed. Degradation of the energy resolution due to aluminum absorbers of various lengths was investigated. A mesh type photomultiplier was also tested

  12. Neutron spectroscopy with the Spherical Proportional Counter

    OpenAIRE

    Bougamont, E .; Dastgheibi, A.; Derre, J.; Galan, J.; Gerbier, G.; Giomataris, I.; Gros, M.; Katsioulas, I.; Jourde, D.; Magnier, P.; Navick, X. F.; Papaevangelou, T.; Savvidis, I.; Tsiledakis, G.

    2015-01-01

    A novel large volume spherical proportional counter, recently developed, is used for neutron measurements. Gas mixtures of $N_{2}$ with $C_{2}H_{6}$ and pure $N_{2}$ are studied for thermal and fast neutron detection, providing a new way for the neutron spectroscopy. The neutrons are detected via the ${}^{14}N(n, p)C^{14}$ and ${}^{14}N(n, \\alpha)B^{11}$ reactions. Here we provide studies of the optimum gas mixture, the gas pressure and the most appropriate high voltage supply on the sensor o...

  13. Use of parallel counters for triggering

    Science.gov (United States)

    Nikityuk, N. M.

    1992-10-01

    The results of an investigation into using parallel counters, majority coincidence schemes and parallel compressors for triggering in multichannel high energy spectrometers are described. Concrete examples of methods of constructing fast and economical new devices used to determine multiplicity hits t > 900 registered in a hodoscopic plane and a pixel detector are given. For this purpose the author uses the syndrome coding method and cellular arrays. In addition, the author has created an effective coding matrix which can be used for light signal coding. For example, such signals are supplied from scintillators to photomultipliers. The investigation has been performed at the Laboratory of High Energies, JINR.

  14. Industrial espionage and technical surveillance counter measurers

    CERN Document Server

    Androulidakis, Iosif

    2016-01-01

    This book examines technical aspects of industrial espionage and its impact in modern companies, organizations, and individuals while emphasizing the importance of intellectual property in the information era. The authors discuss the problem itself and then provide statistics and real world cases. The main contribution provides a detailed discussion of the actual equipment, tools and techniques concerning technical surveillance in the framework of espionage. Moreover, they present the best practices and methods of detection (technical surveillance counter measures) as well as means of intellectual property protection.

  15. Cooperation in counter-pollution response

    International Nuclear Information System (INIS)

    This paper reports that counter-pollution arrangements in Europe are the object of an effective, dynamic, and highly organized international cooperation. The North sea area, in particular, is characterized by an impressive concentration of oil-combating equipment and by a high level of know-how. Though national policies with respect to spill management may still differ on many counts, governments are striving towards a harmonized approach of spill combating. Technically, the ability to prevent environmental damage in case of a large oil spill remains limited, but the European approach could be regarded as a valid attempt to mitigate damage, prevent chaos and limit the waste of valuable resources

  16. Unveiling the counter-rotating nature of the kinematically distinct core in NGC 5813 with MUSE

    Science.gov (United States)

    Krajnović, Davor; Weilbacher, Peter M.; Urrutia, Tanya; Emsellem, Eric; Carollo, C. Marcella; Shirazi, Maryam; Bacon, Roland; Contini, Thierry; Epinat, Benoît; Kamann, Sebastian; Martinsson, Thomas; Steinmetz, Matthias

    2015-09-01

    Multi-Unit Spectroscopic Explorer (MUSE) observations of NGC 5813 reveal a complex structure in the velocity dispersion map, previously hinted at by SAURON observations. The structure is reminiscent of velocity dispersion maps of galaxies comprising two counter-rotating discs, and might explain the existence of the kinematically distinct core (KDC). Further evidence for two counter-rotating components comes from the analysis of the higher moments of the stellar line-of-sight velocity distributions and fitting MUSE spectra with two separate Gaussian line-of-sight velocity distributions. The emission-line kinematics show evidence of being linked to the present cooling flows and the buoyant cavities seen in X-rays. We detect ionized gas in a nuclear disc-like structure, oriented like the KDC, which is, however, not directly related to the KDC. We build an axisymmetric Schwarzschild dynamical model, which shows that the MUSE kinematics can be reproduced well with two counter-rotating orbit families, characterized by relatively low angular momentum components, but clearly separated in integral phase space and with radially varying contributions. The model indicates that the counter-rotating components in NGC 5813 are not thin discs, but dynamically hot structures. Our findings give further evidence that KDCs in massive galaxies should not necessarily be considered as structurally or dynamically decoupled regions, but as the outcomes of the mixing of different orbital families, where the balance in the distribution of mass of the orbital families is crucial. We discuss the formation of the KDC in NGC 5813 within the framework of gas accretion, binary mergers and formation of turbulent thick discs from cold streams at high redshift.

  17. Boron carbide-based ceramics via polymer route synthesis

    International Nuclear Information System (INIS)

    Boron carbide is a ceramic material with excellent high temperature physical properties. As compared to conventional techniques, the preparation of boron carbide from polymeric precursors is attractive as this technique offers a number of unique advantages. In this paper, the screening of polymeric precursors to boron carbide will be discussed. Two promising boron carbide, carborane containing polymeric precursors have resulted in 60-70 wt.% ceramic yields. The chemistry of polymer synthesis and the transformations from the polymer to amorphous and crystalline boron carbide were investigated with infrared spectroscopy, NMR spectroscopy, thermal analysis, and x-ray diffraction

  18. Determination of carbon and sulphur in boron carbide

    International Nuclear Information System (INIS)

    Boron carbide is used in control rods of nuclear power reactors. The chemical specification for carbon in boron carbide ranges between 15 - 24 wt.% depending upon the grade of boron carbide. Hence carbon in boron carbide is to be determined accurately to find out the stoichiometry. Sulphur, which is present in trace quantities, is also to be determined to find out the purity of boron carbide. Carbon is determined by combustion followed by (i) thermal conductivity detection and (ii) infrared detection. Sulphur is determined by (i) combustion followed by infrared detection and (ii) vacuum combustion extraction - quadrupole mass spectrometry. The results are compared. (author)

  19. Direct evidence of metallic bands in a monolayer boron sheet

    Science.gov (United States)

    Feng, Baojie; Zhang, Jin; Liu, Ro-Ya; Iimori, Takushi; Lian, Chao; Li, Hui; Chen, Lan; Wu, Kehui; Meng, Sheng; Komori, Fumio; Matsuda, Iwao

    2016-07-01

    The search for metallic boron allotropes has attracted great attention in the past decades and recent theoretical works predict the existence of metallicity in monolayer boron. Here, we synthesize the β12-sheet monolayer boron on a Ag(111) surface and confirm the presence of metallic boron-derived bands using angle-resolved photoemission spectroscopy. The Fermi surface is composed of one electron pocket at the S ¯ point and a pair of hole pockets near the X ¯ point, which is supported by the first-principles calculations. The metallic boron allotrope in β12 sheet opens the way to novel physics and chemistry in material science.

  20. Medical chemistry of boron neutron capture agents having pharmacological activity

    International Nuclear Information System (INIS)

    Boron neutron capture therapy (BNCT) is a cancer treatment that selectively destroys cancer cells following administering a cancer-selective drug containing stable isotope boron-10 and neutron irradiation. In clinical trial of BNCT, disodium mercaptoundecahydro-closo-dodecaborate (BSH) and p-boronophenylalanine (BPA) have been used, however, development of a new drugs with high cancer selectivity and therapeutic efficiency is expected. Therefore, we review boron-containing drugs as a boron neutron capture agents having pharmacological activity, BNCT research on boron-modified porphyrin derivatives which have photosensitivity and neutron capture activity and our proposed neutron sensitizing agent. (author)

  1. Neutronic calculations for Angra-1 steam line break accident

    International Nuclear Information System (INIS)

    The reduction of boron concentration in the Boron Injection Tank (BIT), to the room temperature solubility level, makes necessary a reanalysis of the steam line break accident of Angra 1 NPP. This paper describes the neutronic calculation related to this reanalysis. The main steps of the work were: review of reactivity parameters used in the accident simulation; search of xenon profiles that cause the most severe core power distribution; calculation of hot channel factors and other neutronic parameters necessary for DNBR determination. The final conclusion, related to the steam line break accident, states the BIT concentration may be reduced to 2000 ppm. (author)

  2. Inefficiency of high boron concentrations for cell killing in boron neutron capture therapy

    International Nuclear Information System (INIS)

    This study is to investigate the relationship between the cell-killing effect of the 10B(n, α)7Li capture reaction, intracellular boron concentration, and thermal neutron fluence in boron neutron capture therapy using in vitro cell survival based on a clonogenic assay, and biophysical analysis. Our results showed that the cell-killing yield of the 10B(n, α)7Li capture reaction per unit thermal neutron fluence declined with an increase in the intracellular boron concentration above 45 μg/ml 10B. The cell-killing effect was well described using an empirical power function of the intracellular boron concentration, with exponent 0.443. Knowledge of this effect will help in the optimization of BNCT. (author)

  3. Effect of metal hydrides on the burning characteristics of boron

    International Nuclear Information System (INIS)

    Highlights: • The effect of some metal hydrides on the burning characteristics of boron is studied for the first time. • We are the first to conduct a TG experiment on boron samples at high temperatures (a maximum of 1750 °C). • The thermal reaction process of boron is firstly divided into five stages according to the weight gain rate of the sample. • Specific values of metal hydrides on ignition delay time and combustion intensity of boron are obtained. - Abstract: In this study, the effect of four metal hydrides on the burning characteristics of boron was investigated. Thermogravimetric experiment results show that the thermal reaction process of boron samples can be divided into five stages. The thermal reactions of boron can be significantly promoted with LiH, which can reduce the initial temperature of the first violent reaction stage by ∼140 °C. The starting temperature of the post-reaction stage also decreases by ∼260 °C. The results of the laser ignition experiment suggest that all four metal hydrides can promote boron burning. Nonetheless, different metal hydrides display varied promotional effects. Among the studied hydrides, LiH is the most effective additive and shortens the ignition delay time of boron by ∼34.1%. Moreover, it enhances the combustion intensity of boron by ∼117.6%. The other three metal hydrides (CaH2, TiH2, and ZrH2) can also contribute to boron burning

  4. Removal properties of dissolved boron by glucomannan gel.

    Science.gov (United States)

    Oishi, Kyoko; Maehata, Yugo

    2013-04-01

    Boron ions have long been known to form complexes with the cis-diol group of a polysaccharide. Konjac glucomannan (KGM) which is one of polysaccharides was used to remove dissolved boron in this study. KGM forms a complex with boron, but does not remove boron from contaminated waters as well as other polysaccharides because of its high water solubility. Therefore, the removal efficiencies of dissolved boron were examined using both an insoluble KGM gel and KGM semi-gel. The former did not remove dissolved boron, but the latter did. The difference in the ability of boron removal was due to the presence of diol group inside. KGM loses free diol group during the process of gelation. On the other hand, the semi-gel gelated only surface layer in water has diol group inside. The boron removal capacity of the semi-gel was highest at pHs⩾11, when the boron species is present as B(OH)4(-). The capacity was slightly increased by the addition of Al, Ca and Mg under high pH conditions. This was due to co-precipitation of boron with Ca dissolved from the semi-gel. The boron adsorbed to the semi-gel easily was desorbed under low pH conditions and the hysteresis was not found. PMID:23260255

  5. Relationship Between Soil Boron Adsorption Kinetics and Rape Plant Boron Response

    Institute of Scientific and Technical Information of China (English)

    ZHUDUANWEI; PIMEIMEI; 等

    1997-01-01

    The boron adsorption kinetic experiment in soil by means a flow displacement technique showed that the kinetic data could be described with some mathematic equations.The average values of the coorealtion coefficeint for zero-order,first-order,parabolic diffusion ,Elovich,power function and eponential equations were 0.957,0.982,0.981,0.984,0.981 and 0.902 ,respectively,The correlation between adsorbed boron or its other expression form and time were the highest for first-order ,parabloic diffusion Elovich,and pwer function equations,the second for the zeroorder equation,and the tlowest for the exponential equation.The parabloic diffusion equation fitted well the expermiental results,with the least standard error among the six kinetic equation,showing that the monvemetn of boron from soil solution to soil colloid surface may be controlled by boron diffusion speed.The boron content of rape seedling obtained from soil cultvation was correlated with the rate constants of the kinetic equations.The constants of first-order ,parabloic diffusion,and exponential equaitions were significanlty correlated with the boron content of the crop of NPK treatment at a 95% probaility level ,with correation coeffecients being 0.686,0.691 and 0.64 and 0.641,respectively.In the case of zero-order equation,it Was significant at 99% probability level(r=0.736),These results showed that the adsorption kinetic constants of soil boron were closely related with the rape plant response to boron.

  6. The structure and local chemical properties of boron-terminated tetravacancies in hexagonal boron-nitride

    OpenAIRE

    Cretu, Ovidiu; Lin, Yung-Chang; Koshino, Masanori; Tizei, Luiz H. G.; Liu, Zheng; Suenaga, Kazutomo

    2014-01-01

    Imaging and spectroscopy performed in a low-voltage scanning transmission electron microscope (LV-STEM) are used to characterize the structure and chemical properties of boron-terminated tetravacancies in hexagonal boron nitride (h-BN). We confirm earlier theoretical predictions about the structure of these defects and identify new features in the electron energy-loss spectra (EELS) of B atoms using high resolution chemical maps, highlighting differences between these areas and pristine sampl...

  7. A colorimetric determination of boron in biological sample for boron neutron capture therapy (BNCT)

    International Nuclear Information System (INIS)

    The boron neutron capture therapy (BNCT) has shown better prognosis in the treatment of glyemas and gluoblastomas grade III and IV than other therapies. During the treatment the levels of Na210B12H11SH must be known in several compartiments of the organism and with this purpose the method of colorimetric determination of boron using curcumine was established. This method is simple, reprodutible and adequate sensitivity for this control. (author)

  8. Study of boron dilution phenomenon in the core and fuel assemblies of Bushehr VVERr-1000 reactor in normal operating conditions

    International Nuclear Information System (INIS)

    The spatial temperature distributions in fuel and coolant, results in appearing local changes in those elements densities in the reactor core, and also due to the complete solubility of boric acid in the coolant, there will be a direct correlation between the changes in the boron concentration and the coolant density. Because of the gradual reduction of boron concentration, first a local positive reactivity will be inserted into the core which will cause slight thermo-neutronic fluctuations in the reactor core. Of course, the trend of this process in the case of excessive reduction of the density of the coolant and evaporation of water (accident scenarios) will be reversed and subsequently the negative reactivity will be given to the system. With regard to the importance of this phenomenon, the spatial changes of boron concentration in the core and fuel assemblies of Bushehr VVER-1000 reactor have been examined. In line with this, by designing a complete thermo-neutronic cycle and by using CITATION, WIMS D-5 and COBRAN-EN codes, coolant temperature distribution and boron concentration will be calculated through this procedure, which first by using the output results of WIMS and CITATION codes, the thermal power of each fuel assembly will be calculated and finally, by linking these data to COBRA-EN code and using core and sub-channel analysis methods, the three-dimensional (3D) calculations of boron dilution will be obtained in the core as well as the fuel assemblies of the reactor. (authors)

  9. Improved proportional counters for practical applications

    International Nuclear Information System (INIS)

    Gas filled proportional counters are useful room-temperature X-ray detectors in various gauges and spectrometers. New gas mixtures have made it possible to improve the properties of these detectors. Penning mixtures offer some special advantages. These mixtures are formed when parent gas is diluted with a small amount of impurity whose ionization energy is lower than the lowest excited state of the parent atoms. The excitations of these atoms can subsequently be turned into ionizations. The result of this additional ionization is that the average ionization energy of the mixture falls below that of the pure gases. This also improves the energy resolution of the detector. Another feature of Penning mixtures is the fact that the first Townsend ionization coefficient is high. This in turn is reflected by an unusually low anode voltage required by the detector. This makes it possible to use high filling pressures and to realize the advantages such pressures offer: the achievement of good energy resolution with a commercial low noise preamplifier; a decrease in the background caused by the wall effect because of the subsequently shorter photoelectron traces; and an increase in the efficiency of the detector. The type of detector used in this paper is a sealed side window counter. Some of its properties, when filled with the mixtures Ar-C4H10, Ar-Xe, and Ne-Ar, are presented

  10. Instability patterns between counter-rotating disks

    Directory of Open Access Journals (Sweden)

    F. Moisy

    2003-01-01

    Full Text Available The instability patterns in the flow between counter-rotating disks (radius to height ratio R/h from 3.8 to 20.9 are investigated experimentally by means of visualization and Particle Image Velocimetry. We restrict ourselves to the situation where the boundary layers remain stable, focusing on the shear layer instability that occurs only in the counter-rotating regime. The associated pattern is a combination of a circular chain of vortices, as observed by Lopez et al. (2002 at low aspect ratio, surrounded by a set of spiral arms, first described by Gauthier et al. (2002 in the case of high aspect ratio. Stability curve and critical modes are measured for the whole range of aspect ratios. From the measurement of a local Reynolds number based on the shear layer thickness, evidence is given that a free shear layer instability, with only weak curvature effect, is responsible for the observed patterns. Accordingly, the number of vortices is shown to scale as the shear layer radius, which results from the competition between the centrifugal effects of each disk.

  11. Finding Feasible Abstract Counter-Examples

    Science.gov (United States)

    Pasareanu, Corina S.; Dwyer, Matthew B.; Visser, Willem; Clancy, Daniel (Technical Monitor)

    2002-01-01

    A strength of model checking is its ability to automate the detection of subtle system errors and produce traces that exhibit those errors. Given the high computational cost of model checking most researchers advocate the use of aggressive property-preserving abstractions. Unfortunately, the more aggressively a system is abstracted the more infeasible behavior it will have. Thus, while abstraction enables efficient model checking it also threatens the usefulness of model checking as a defect detection tool, since it may be difficult to determine whether a counter-example is feasible and hence worth developer time to analyze. We have explored several strategies for addressing this problem by extending an explicit-state model checker, Java PathFinder (JPF), to search for and analyze counter-examples in the presence of abstractions. We demonstrate that these techniques effectively preserve the defect detection ability of model checking in the presence of aggressive abstraction by applying them to check properties of several abstracted multi-threaded Java programs. These new capabilities are not specific to JPF and can be easily adapted to other model checking frameworks; we describe how this was done for the Bandera toolset.

  12. Neutron pileup algorithms for multiplicity counters

    Science.gov (United States)

    Robinson, Sean M.; Stave, Sean; Lintereur, Azaree; Siciliano, Edward; Kouzes, Richard; Bliss, Mary

    2015-06-01

    The shortage of helium-3 (3He) has created a need to identify alternative neutron detection options for a variety of nuclear nonproliferation applications. One application that may be affected by 3He replacement technology is that of mass accountancy for safeguards, which utilizes coincidence and multiplicity counters to verify special nuclear material declarations. The use of neutron scintillation materials, such as LiF-ZnS sheets, as an alternative to 3He proportional tubes in multiplicity counters requires novel techniques for Pulse Shape Discrimination to distinguish between neutrons and gamma rays. These techniques must work under high count rates, as the maximum momentary rate for incoming neutrons from multiplicity events can be quite large. We have created a fast and accurate neutron discrimination algorithm based on time window filtering and signature comparison that can operate quickly on data with high degrees of gamma ray and neutron pileup. This algorithm is evaluated for its capability to separate signals as the pileup rate increases, and the possibility for implementation on fast hardware (e.g., FPGA hardware) for real-time operation is explored.

  13. Effects of boron number per unit volume on the shielding properties of composites made with boron ores form China

    International Nuclear Information System (INIS)

    The total macroscopic removal cross sections, deposited energies and the absorbed doses of three new shielding composites loaded with specific boron-rich slag, boron concentrate ore and boron mud of China for 252Cf neutron source were investigated by experimental and Monte Carlo calculation. The results were evaluated by boron mole numbers per unit volume in composites. The half value layers of the composites were calculated and compared with that of Portland concrete, indicating that ascending boron mole numbers per unit volume in the composites can enhance the shielding properties of the composites for 252Cf neutron source. (authors)

  14. Synthesis and evaluation of boron folates for Boron-Neutron-Capture-Therapy (BNCT)

    Energy Technology Data Exchange (ETDEWEB)

    Kettenbach, Kathrin; Schieferstein, Hanno; Grunewald, Catrin; Hampel, Gabriele; Schuetz, Christian L. [Mainz Univ. (Germany). Inst. of Nuclear Chemistry; Iffland, Dorothee; Bings, Nicolas H. [Mainz Univ. (Germany). Inst. of Inorganic Chemistry and Analytical Chemistry; Reffert, Laura M. [Hannover Medical School (Germany). Radiopharmaceutical Chemistry; Ross, Tobias L. [Mainz Univ. (Germany). Inst. of Nuclear Chemistry; Hannover Medical School (Germany). Radiopharmaceutical Chemistry

    2015-07-01

    Boron neutron capture therapy (BNCT) employs {sup 10}B-pharmaceuticals administered for the treatment of malignancies, and subsequently irradiated with thermal neutrons. So far, clinical established pharmaceuticals like boron phenylalanine (BPA) or sodium boron mercaptate (BSH) use imperfect (BPA) or passive (BSH) targeting for accumulation at target sites. Due to the need of a selective transportation of boron drugs into cancer cells and sparing healthy tissues, we combined the BNCT approach with the specific and effective folate receptor (FR) targeting concept. The FR is overexpressed on many human carcinomas and provides a selective and specific target for molecular imaging as well as for tumor therapy. We synthesized and characterized a carborane-folate as well as a BSH-folate to study their in vitro characteristics and their potential as new boron-carriers for BNCT. Uptake studies were carried out using human KB cells showing a significant increase of the boron content in cells and demonstrating the successful combination of active FR-targeting and BNCT.

  15. Rapid mass-spectrometric determination of boron isotopic distribution in boron carbide.

    Science.gov (United States)

    Rein, J E; Abernathey, R M

    1972-07-01

    Boron isotopic ratios are measured in boron carbide by thermionic ionization mass spectrometry with no prior chemical separation. A powder blend of boron carbide and sodium hydroxide is prepared, a small portion is transferred to a tantalum filament, the filament is heated to produce sodium borate, and the filament is transferred to the mass spectrometer where the(11)B/(10)B ratio is measured, using the Na(2)BO(2)(+) ion. Variables investigated for their effect on preferential volatilization of (10)B include the sodium hydroxide-boron carbide ratio and the temperature and duration of filament heating. A series of boron carbide pellets containing natural boron, of the type proposed for the control rods of the Fast Flux Test Facility reactor, were analysed with an apparently unbiased result of 4.0560 for the (11)B/(10)B ratio (standard deviation 0.0087). The pellets contained over 3% metal impurities typically found in this material. Time of analysis is 45 min per sample, with one analyst. PMID:18961131

  16. Coadsorption of lanthanum with boron and gadolinium with boron on Mo(1 1 0)

    Science.gov (United States)

    Magkoev, Tamerlan T.; Vladimirov, Georgij G.; Rump, Gennadij A.

    2008-05-01

    Submonolayer to multilayer coadsorption of lanthanum (La) with boron (B) and gadolinium (Gd) with boron on the surface of Mo(1 1 0) has been studied by means of Auger electron spectroscopy (AES), electron energy loss spectroscopy (EELS) and work function ( ϕ) measurements. The equilibrium state of double adsorbate systems achieved either by adsorption of rare-earth metal (REM) on boron precovered Mo(1 1 0) surface held at room temperature or after moderate annealing of the system with opposite order of adsorption (B on REM films) is the layer which is the inhomogeneous mixture of boron and REM atoms with preferential concentration of boron in the surface area of the mixed film. The work function of such films even at REM to boron concentration ratio much higher than 1/6 are very close to the values of corresponding bulk LaB 6 and GdB 6, favoring assumption of surface rearrangement as the dominant reason of high electron emission efficiency of hexaborides. Almost total similarity of the results for La-B and Gd-B systems can be viewed as the consequence of weak participation of Gd f-electrons in determining the thermionic properties of corresponding double layers.

  17. Multi-dimensional boron transport modeling in subchannel approach: Part II. Validation of CTF boron tracking model and adding boron precipitation model

    International Nuclear Information System (INIS)

    Highlights: • Validation of implemented multi-dimensional subchannel boron transport model. • Extension of boron transport model to entrained droplets. • Implementation of boron precipitation model. • Testing of the boron precipitation model under transient condition. - Abstract: The risk of small-break loss of coolant accident (SB-LOCA) and other reactivity initiated transients caused by boron dilution in the light water reactors (LWRs), and the complications of tracking the soluble boron concentration experimentally inside the primary coolant have stimulated the interest in computational studies for accurate boron tracking simulations in nuclear reactors. In Part I of this study, the development and implementation of a multi-dimensional boron transport model with modified Godunov scheme based on a subchannel approach within the COBRA-TF (CTF) thermal-hydraulic code was presented. The modified Godunov scheme approach with a physical diffusion term was determined to provide the most accurate and precise solution. Current paper extends these conclusions and presents the model validation studies against experimental data from the Rossendorf coolant mixing model (ROCOM) test facility. In addition, the importance of the two-phase flow characteristics in modeling boron transient are emphasized, especially during long-term cooling period after the loss of coolant accident (LOCA) condition in pressurized water reactors (PWRs). The CTF capabilities of boron transport modeling are further improved based on the three-field representation of the two-phase flow utilized in the code. The boron transport within entrained droplets is modeled, and a model for predicting the boron precipitation under transient conditions is developed and tested. It is aimed to extend the applicability of CTF to reactor transient simulations, and particularly to a large-break loss of coolant accident (LB-LOCA) analysis

  18. Over-the-counter Acne Treatments: A Review

    OpenAIRE

    Decker, Ashley; Graber, Emmy M.

    2012-01-01

    Acne is a common dermatological disorder that most frequently affects adolescents; however, individuals may be affected at all ages. Many people who suffer from acne seek treatment from both prescription and over-the-counter acne medications. Due to convenience, lower cost, and difficulty getting an appointment with a dermatologist, the use of over-the-counter acne treatments is on the rise. As the plethora of over-the-counter acne treatment options can be overwhelming, it is important that d...

  19. Wind tunnel tests of stratospheric airship counter rotating propellers

    OpenAIRE

    Yaxi Chen; Peiqing Liu; Zhihao Tang; Hao Guo

    2015-01-01

    Aerodynamic performance of the high-altitude propeller, especially the counter rotation effects, is experimentally studied. Influences of different configurations on a stratospheric airship, included 2-blade counter-rotating propeller (CRP), dual 2-blade single rotation propellers (SRPs) and 4-blade SRP, are also indicated. This research indicates that the effect of counter rotation can greatly improve the efficiency. It shows that the CRP configuration results in a higher efficiency than the...

  20. Particle Counter Determination of Bacterial Biomass in Seawater

    OpenAIRE

    Kogure, Kazuhiro; Koike, Isao

    1987-01-01

    The applicability of the Elzone particle counter to the determination of marine bacterial biomass was investigated. The biomass of bacterial pure cultures and a mixed natural population were followed by using the particle counter, a CHN analyzer, and an ATP analyzer. The particle counter showed the precise size distribution of number and volume of submicron-size particles in seawater. For the pure cultured bacterial strains, the conversion factor from volume to carbon is 0.209 mg of C per mm3...

  1. Investigation of new gas mixtures for the Pestov Counter

    CERN Document Server

    Sann, H; CERN. Geneva; Eschke, J; Lühning, J; Lynen, U; Neyer, C; Pestov, Yu N; Schmidt, H R; Schreiber, B M; Schulze, R; Stelzer, H; Woerner, A; Frankenfeld, U

    2000-01-01

    The physical principle of discharge localization in Pestor spark counters is described. It was experimentally shown that Isoprene is one of the promising candidates to replace 1,3-Butadiene in the standard gas mixture. In the spark counter with the DME-Argon gas mixture and an aluminium nitrite cathode a discharge localization was obtained for the first time. This result is considered as the beginning of a new spark counter technology without conditioning.

  2. Threshold aerogel Cherenkov counters of the KEDR detector

    International Nuclear Information System (INIS)

    Particle identification system based on aerogel threshold Cherenkov counters ASHIPH (Aerogel SHifter PHotomultiplier) was installed in the KEDR detector in 2013. The system consists of 160 counters arranged in two layers and contains 1000 liters of aerogel with refractive index of 1.05 and 160 MCP PMTs with multialkali photocathode. The efficiency of relativistic particles detection was measured. Long-term stability of ASHIPH counters was studied. The main reasons of efficiency degradation are presented

  3. PWR core response to boron dilution transient

    International Nuclear Information System (INIS)

    This paper illustrates the steps followed in order to set up a tool (composed of a plant model and of a procedure) that allows accounting for boron reactivity feedbacks during plant transients. The procedure that has been developed allows to find out the values of the boron feedback coefficients, given the differential boron worth, and to properly initialize the Thermal Hydraulic and the Neutronic (TH/NEU) system. Once the tool has been developed, it has been used to analyze different scenarios, resulting from deborated water injection from the reactor make-up system. The most important parameter, during this Reactivity Insertion Accidents (RIAs), is the Energy Released to the Fuel (ERF) and it has been monitored, in order to identify the situations when the fuel might be damaged (ERF > 250 kJ/kg, for high burnup fuel). The analyses have been performed using the RELAP5-3D computer code. The conclusion of the study is that the limited capability of modeling mixing phenomena provided by most common plant codes (such as RELAP5-3D) is not suitable to perform BE analyses of RIAs, since those accidents are so sensitive to boron concentration changes that the effect of uncertainties cannot be neglected. The use of Computational Fluid Dynamics (CFD) codes could reduce uncertainties enough to perform BE analyses and thus it should be recommended. (author)

  4. Pechmann Reaction Promoted by Boron Trifluoride Dihydrate

    Directory of Open Access Journals (Sweden)

    J. Mezger

    2005-08-01

    Full Text Available The Pechmann reaction of substituted phenols 1a-e with methyl acetoacetate (2 can be activated by boron trifluoride dihydrate (3 to give the corresponding 4-methyl- coumarin derivatives 4a-e in excellent yield (98-99 %.

  5. New insight into pecan boron nutrition

    Science.gov (United States)

    Alternate bearing by individual pecan [Carya illinoinensis (Wangenh.) K. Koch] trees is problematic for nut producers and processors. There are many unknowns regarding alternate bearing physiology, such as the relationship between boron and fruit set, nutmeat quality, and kernel maladies. Evidence...

  6. Channeling of boron ions into silicon

    International Nuclear Information System (INIS)

    Channeled and random distributions of boron ions implanted over the energy range 50 keV--1.8 MeV into silicon have been measured using the differential capacitance technique. When implantations are performed along the or axis, profiles exhibit a strong orientation dependance. The best channeled profiles shows that more than 70% of the implanted dose is in the channeled peak

  7. Influence of pollution of boron chlorinity ratio

    Digital Repository Service at National Institute of Oceanography (India)

    Narvekar, P.V.; Zingde, M.D.

    Presence of boron in domestic wastewater has resulted in high B/CI ratio at some locations in the coastal water around Bombay. A widest range (0.215-0.281) of B/CI was observed at a location with high influence of wastewater release. The mean B...

  8. Boron carbide morphology changing under purification

    Science.gov (United States)

    Rahmatullin, I. A.; Sivkov, A. A.

    2015-10-01

    Boron carbide synthesized by using coaxial magnetoplasma accelerator with graphite electrodes was purified by two different ways. XRD-investigations showed content changing and respectively powder purification. Moreover TEM-investigations demonstrated morphology changing of product under purification that was discussed in the work.

  9. Boron carbide synthesis at plasma spray process

    Czech Academy of Sciences Publication Activity Database

    Ctibor, Pavel; Brožek, Vlastimil; Hofman, R.

    Bari : Department of Chemistry, University of Bari, 2003 - (d'Agostino, R.; Favia, P.; Fracassi, F.; Palumbo, F.). s. 631 [International Symposium on Plasma Chemistry/16th./. 22.06.2003-27.06.2003, Taormina] Institutional research plan: CEZ:AV0Z2043910 Keywords : boron carbide , plasma spray process Subject RIV: BL - Plasma and Gas Discharge Physics

  10. Joining of boron carbide using nickel interlayer

    International Nuclear Information System (INIS)

    Carbide ceramics such as boron carbide due to their unique properties such as low density, high refractoriness, and high strength to weight ratio have many applications in different industries. This study focuses on direct bonding of boron carbide for high temperature applications using nickel interlayer. The process variables such as bonding time, temperature, and pressure have been investigated. The microstructure of the joint area was studied using electron scanning microscope technique. At all the bonding temperatures ranging from 1150 to 1300degC a reaction layer formed across the ceramic/metal interface. The thickness of the reaction layer increased by increasing temperature. The strength of the bonded samples was measured using shear testing method. The highest strength value obtained was about 100 MPa and belonged to the samples bonded at 1250 for 75 min bonding time. The strength of the joints decreased by increasing the bonding temperature above 1250degC. The results of this study showed that direct bonding technique along with nickel interlayer can be successfully utilized for bonding boron carbide ceramic to itself. This method may be used for bonding boron carbide to metals as well.

  11. Boron nitride nanosheets reinforced glass matrix composites

    Czech Academy of Sciences Publication Activity Database

    Saggar, Richa; Porwal, H.; Tatarko, P.; Dlouhý, Ivo; Reece, M. J.

    2015-01-01

    Roč. 114, SEP (2015), S26-S32. ISSN 1743-6753 R&D Projects: GA MŠk(CZ) 7AMB14SK155 EU Projects: European Commission(XE) 264526 Institutional support: RVO:68081723 Keywords : Boron nitride nanosheets * Borosilicate glass * Mechanical properties Subject RIV: JL - Materials Fatigue, Friction Mechanics Impact factor: 1.163, year: 2014

  12. The manufacturing method of boron carbide

    International Nuclear Information System (INIS)

    The new method for manufacturing of boron carbide as powder with controlled purity and surface development has been described. The suspension of boric acid aqueous solution and carbon black in alcohol has been homogenized mechanically. Water and alcohol are then evaporated during mixing. After drying homogenous mixture is heated in temperature range of 1270-1870 C during one hour

  13. Novel Boron Based Multilayer Thermal Neutron Detector

    CERN Document Server

    SCHIEBER, M

    2010-01-01

    The detector contains four or more layers of natural Boron absorbing thermal neutrons. Thickness of a layer is 0.4 - 1.2 mg/cm2. The layers are deposited on one or on both sides of a metal surface used as contacts. Between the absorbing layers there are gas-filled gaps 3 - 6 mm thick. Electric field of 100 - 200 V/cm is applied to the gas-filled gaps. Natural Boron contains almost 20% of 10B isotope. When atoms of 10B capture a thermal neutron, nuclear reaction occurs, as a result of which two heavy particles - alpha particle and ion 7Li - from the thin absorber layer are emitted in opposing sides. One of the two particles penetrates into gas-filled gap between Boron layers and ionizes the gas. An impulse of electric current is created in the gas-filled gap actuated by the applied electric field. The impulse is registered by an electronic circuit. We have made and tested detectors containing from two to sixteen layers of natural Boron with an efficiency of thermal neutron registration from 2.9% to 12.5% accor...

  14. Position-sensitive proportional counter with low-resistance metal-wire anode

    International Nuclear Information System (INIS)

    A position-sensitive proportional counter circuit is provided which uses a conventional (low-resistance, metal-wire anode) proportional counter for spatial resolution of an ionizing event along the anode of the counther. A pair of specially designed activecapacitance preamplifiers terminate the anode ends wherein the anode is treated as an RC line. The preamplifiers act as stabilized active capacitance loads and each is composed of a series-feedback, lownoise amplifier, a unity-gain, shunt-feedback amplifier whose output is connected through a feedback capacitor to the series-feedback amplifier input. The stabilized capacitance loading of the anode allows distributed RC-line position encoding and subsequent time difference decoding by sensing the difference in rise times of pulses at te anode ends where the difference is primarily in response to the distributed capacitance along the anode. This allows the use of lower resistance wire anodes for spatial radiation detection which simplifies the counter construction and handling of the anodes, and stabilizes the anode resistivity at high count rates

  15. Isotope effect on the spin resonance of boron in silicon

    International Nuclear Information System (INIS)

    The fourfold degeneracy of the boron acceptor ground state in silicon, which is easily lifted by any symmetry breaking perturbation, allows for a strong inhomogeneous broadening of the B-related electron paramagnetic resonance (EPR) lines, e.g. by randomly distributed, defect-induced local strain. In previous studies a number of fundamental questions concerning the line shape, the magnitude of the residual broadening, and the substructure of the B resonances have remained unsolved. We show that local fluctuations of the valence band edge due to the presence of different Si isotopes in the vicinity of the B acceptors can quantitatively account for all inhomogeneous broadening effects in high purity Si with a natural isotope composition. A comparison of our calculations with previous work investigating the B acceptor ground state in the absence of an external magnetic field, provides an independent verification of the energy offsets between the valence bands of 28Si, 29Si, and 30Si. Moreover, our calculations show that the isotopic perturbation also leads to a shift in the g-value of different B-related resonance lines, which could be verified in our experiments.

  16. Boron carbide nanowires: Synthesis and characterization

    Science.gov (United States)

    Guan, Zhe

    Bulk boron carbide has been widely used in ballistic armored vest and the property characterization has been heavily focused on mechanical properties. Even though boron carbides have also been projected as a promising class of high temperature thermoelectric materials for energy harvesting, the research has been limited in this field. Since the thermal conductivity of bulk boron carbide is still relatively high, there is a great opportunity to take advantage of the nano effect to further reduce it for better thermoelectric performance. This dissertation work aims to explore whether improved thermoelectric performance can be found in boron carbide nanowires compared with their bulk counterparts. This dissertation work consists of four main parts. (1) Synthesis of boron carbide nanowires. Boron carbide nanowires were synthesized by co-pyrolysis of diborane and methane at low temperatures (with 879 °C as the lowest) in a home-built low pressure chemical vapor deposition (LPCVD) system. The CVD-based method is energy efficient and cost effective. The as-synthesized nanowires were characterized by electron microscopy extensively. The transmission electron microscopy (TEM) results show the nanowires are single crystalline with planar defects. Depending on the geometrical relationship between the preferred growth direction of the nanowire and the orientation of the defects, the as-synthesized nanowires could be further divided into two categories: transverse fault (TF) nanowires grow normal to the defect plane, while axial fault (AF) ones grow within the defect plane. (2) Understanding the growth mechanism of as-synthesized boron carbide nanowires. The growth mechanism can be generally considered as the famous vapor-liquid-solid (VLS) mechanism. TF and AF nanowires were found to be guided by Ni-B catalysts of two phases. A TF nanowire is lead by a hexagonal phase catalyst, which was proved to be in a liquid state during reaction. While an AF nanowires is catalyzed by a

  17. Development of tecniques for constructing Geiger-Mueller counters

    International Nuclear Information System (INIS)

    A systematic study of several construction techniques of Geiger-Mueller counters was carried out in order to establish the most suitable technology for such purpose. The results obtained with counters for alpha, beta and gamma rays, which were designed and built in the laboratory of Sao Paulo University (USP) are described. Most of the counters were built inside Pyrex-glass envelope and their cathodes were made of electrolytic copper or brass foils of still a silver layer deposited by chemical process. Some counters were made with cilyndrical brass tube. Anode wires of different materials and diameters and severals quenching vapors were used and the results obtained are described. All the procedures used in preparation of surfaces, cleaning of materials, purification of filling mixtures, the procedures for operating evacuation and filling of counters are described. The results obtained with self quenching counters using soda glass and an external colloidas graphite cathode are presented and the influence of filling mixtures is analysed. A technology to produce reliable counters from materials and gases easily available in the country was established. It is shown that counters with an external cathode can be used when recovery time on order of 2 μs are required. The plateus obtained for such counters were on order of 1000V with slope of about 0.5%. (Author)

  18. Discharge quenching circuit for Geiger-Mueller counters

    International Nuclear Information System (INIS)

    Electron discharge quenching circuit in halogen Geiger-Mueller counters with the total time of counter supply switch on after the signal appearence at the input of approximately 70 ns at input sensitivity of approximately 50 mV is described. The circuit provides the parallel control of five STS-5 counters at the quenching pulse duration of 4.5 μs. For two STS-5 counters the counting characteristics with the inclination up to 0.131%/V and flat-top of 100 V at the load of 60 thousand pulse/s. Maximum loading is 120 thousand pulse/s

  19. Relativistic Static Thin Disks: The Counter-Rotating Model

    OpenAIRE

    Espitia, Omar A.; Gonzalez, Guillermo A.

    2001-01-01

    A detailed study of the Counter-Rotating Model (CRM) for generic finite static axially symmetric thin disks with nonzero radial pressure is presented. We find a general constraint over the counter-rotating tangential velocities needed to cast the surface energy-momentum tensor of the disk as the superposition of two counter-rotating perfect fluids. We also found expressions for the energy density and pressure of the counter-rotating fluids. Then we shown that, in general, there is not possibl...

  20. Hardware support for software controlled fast reconfiguration of performance counters

    Science.gov (United States)

    Salapura, Valentina; Wisniewski, Robert W.

    2013-06-18

    Hardware support for software controlled reconfiguration of performance counters may include a plurality of performance counters collecting one or more counts of one or more selected activities. A storage element stores data value representing a time interval, and a timer element reads the data value and detects expiration of the time interval based on the data value and generates a signal. A plurality of configuration registers stores a set of performance counter configurations. A state machine receives the signal and selects a configuration register from the plurality of configuration registers for reconfiguring the one or more performance counters.

  1. Influence of guard wires in the response of spark counters

    International Nuclear Information System (INIS)

    A systematic study of the operation characteristics of Spark Counters with air filling at atmospheric pressure, was carried out for alpha particles (241 Am). Anode wires of different chemical compositions and diameters were used. The influence of guard wires in the efficiency of the counter has improved its efficiency by 25%. The properties of these counters such as very low background, high efficiency of detection foir heavily ionizing particles, their directional propertiesd and their negligible efficiency for beta and gamma radiation show that they can be used with great advantage over conventional counters in several Nuclear Physics problems. (author). 14 refs, 10 figs

  2. EPR observation of first point defects in cubic boron nitride crystalline powders

    Science.gov (United States)

    Nistor, S. V.; Stefan, M.; Schoemaker, D.; Dinca, G.

    2000-05-01

    An X-band electron paramagnetic resonance (EPR) study of nominally pure, diamond-like cubic boron nitride (c-BN) crystalline powders, has led to the first identification of a spectrum attributed to two related paramagnetic species. The composite EPR spectrum can be observed only in dark brown colored powders known to contain excess of boron. It consists of two superimposed lorentzian components, called D1 and D2, centered at g1=2.0063 and g2=2.0084, with peak-to-peak linewidths of 3.3 and 17.9 mT, respectively. The temperature dependence of the integrated intensities, their linewidths and intensity ratio D2/D1 allows one to conclude that the narrow line D1 originates from EPR transitions inside a S=1/2 ground doublet and the broad line D2 from transitions inside the excited levels of another center. Evidence suggests that both centers are boron related paramagnetic species.

  3. Proportional counters as monitoring detectors of BAC chambers at the ZEUS experiment

    International Nuclear Information System (INIS)

    The aim of the investigations presented is the elaboration of the system monitoring working conditions of BAC chambers. The backing calorimeter (BAC) at the ZEUS detector of the HERA accelerator consisting of 5000 proportional chambers of a total volume of 60 m3 is supplied with a gas mixture of Ar+10% CO2 by an open gas system. Flow proportional counters with a 55Fe source are used as gas system monitoring detectors. These counters and sources were designed and made exclusively for that application. The ageing effect of the Ar+CO2 mixture has also been studied. Monitoring measurements of the pulse height distribution enable us to follow the changes of gas pressure and composition in BAC proportional chambers. The results of these measurements will be used for off-line corrections of BAC data. (orig.)

  4. Antitumor potential induction and free radicals production in melanoma cells by Boron Neutron Capture Therapy

    International Nuclear Information System (INIS)

    Antiproliferative and oxidative damage effects occurring in Boron Neutron Capture Therapy (BNCT) in normal fibroblasts and melanoma cell lines were analyzed. Melanoma cells and normal fibroblasts were treated with different concentrations of Boronophenylalanine and irradiated with thermal neutron flux. The cellular viability and the oxidative stress were determined. BNCT induced free radicals production and proliferative potential inhibition in melanoma cells. Therefore, this therapeutic technique could be considered efficient to inhibit growth of melanoma with minimal effects on normal tissues. - Highlights: ► Boron Neutron Capture Therapy (BNCT) induces melanoma cell death. ► BNCT stimulates free radicals production and proliferative inhibition in melanoma cells. ► It produces tumor membrane degeneration and destruction with apoptotic bodies formation. ► This therapy damages tumor cells selectively, with minimum effects on normal adjacent tissue.

  5. Absorption spectrum of the excitons bound on neutral boron atoms in cubic silicon carbide

    International Nuclear Information System (INIS)

    Absorption spectrum of the excitons strongly bound on neutral deep acceptors (boron) is observed for the first time in silicon carbide 3C-SiC:B cubic crystals. The exciton binding energy with EBex acceptor equals 227 meV. The spectrum consists of three absorption lines at photon energies 2.1508; 2.1585 and 2.189 eV and a series of high energy maxima. The spectrum structure is explained by splitting of coupled exciton states by hole-hole exchange interaction in the local acceptor field. It is shown that because of extremely high probability of Auger-processes the decay of excitons bound on neutral boron in 3C-SiC is a radiationless one

  6. Mapping boron in silicon solar cells using electron energy-loss spectroscopy

    DEFF Research Database (Denmark)

    Amorphous silicon solar cells typically consist of stacked layers deposited on plastic or metallic substrates making sample preparation for transmission electron microscopy (TEM) difficult. The amorphous silicon layer - the active part of the solar cell - is sandwiched between 10-nm-thick n- and p...... focused ion beam milling in order to map the boron distribution across a 200-nm-thick n-p amorphous silicon junction using energy-filtered TEM and EELS spectrum acquisition. EELS line scans are used to detect boron concentrations as low as 10^20cm-3. We also use monochromated EELS to measure changes in...... resolution using TEM is highly challenging [3]. Recently, scanning TEM (STEM) combined with electron energy-loss spectroscopy (EELS) and spherical aberration-correction has allowed the direct detection of dopant concentration of 10^20cm-3 in 65-nm-wide silicon devices [4]. Here, we prepare TEM samples by...

  7. Antitumor potential induction and free radicals production in melanoma cells by Boron Neutron Capture Therapy

    Energy Technology Data Exchange (ETDEWEB)

    Faiao-Flores, F. [Biochemical and Biophysical Laboratory, Butantan Institute, 1500 Vital Brasil Avenue, Sao Paulo (Brazil)] [Faculty of Medicine, University of Sao Paulo, 455 Doutor Arnaldo Avenue, Sao Paulo (Brazil); Coelho, P.R.P.; Muniz, R.O.R.; Souza, G.S. [Institute for Nuclear and Energy Research, 2242 Lineu Prestes Avenue, Sao Paulo (Brazil); Arruda-Neto, J. [Physics Institute, University of Sao Paulo, 187 Matao Street, Sao Paulo (Brazil)] [FESP, Sao Paulo Engineering School, 5520 Nove de Julho Avenue, Sao Paulo (Brazil); Maria, Durvanei A., E-mail: durvaneiaugusto@yahoo.com.br [Biochemical and Biophysical Laboratory, Butantan Institute, 1500 Vital Brasil Avenue, Sao Paulo (Brazil)

    2011-12-15

    Antiproliferative and oxidative damage effects occurring in Boron Neutron Capture Therapy (BNCT) in normal fibroblasts and melanoma cell lines were analyzed. Melanoma cells and normal fibroblasts were treated with different concentrations of Boronophenylalanine and irradiated with thermal neutron flux. The cellular viability and the oxidative stress were determined. BNCT induced free radicals production and proliferative potential inhibition in melanoma cells. Therefore, this therapeutic technique could be considered efficient to inhibit growth of melanoma with minimal effects on normal tissues. - Highlights: Black-Right-Pointing-Pointer Boron Neutron Capture Therapy (BNCT) induces melanoma cell death. Black-Right-Pointing-Pointer BNCT stimulates free radicals production and proliferative inhibition in melanoma cells. Black-Right-Pointing-Pointer It produces tumor membrane degeneration and destruction with apoptotic bodies formation. Black-Right-Pointing-Pointer This therapy damages tumor cells selectively, with minimum effects on normal adjacent tissue.

  8. Effects of auxin and boron on the rooting of Laurus nobilis L. stem cuttings

    Directory of Open Access Journals (Sweden)

    Fernando Perez Leal

    2004-05-01

    Full Text Available The purpose of this study was to evaluate the effect of indolebutyric acid (IBA, applied with or without boric acid, on rooting laurel (Laurus nobilis L. stem cuttings. The cuttings (15cm that presented two apical leaves were collected from the apexes. They were treated with IBA 0, 50, 150 and 300 mg L-1, with or without boron 150 mg mL-1, for 24 hours. After the treatments, the cuttings were cultivated in polystyrene trays with carbonized rice linings and maintained under intermittent nebulization for 70 days when the percentages for rooting, stem cuttings with callus, and live and dead cuttings, root numbers and root lengths were evaluated. The results showed that IBA 50 mg L-1, IBA 150 and 300mg L-1 with boron enhanced the rooting percentage. The treatment with IBA 150 mg L-1 showed the highest root number in stem cuttings.

  9. Higher boron rejection with a new TFC forward osmosis membrane

    KAUST Repository

    Valladares Linares, Rodrigo

    2014-07-17

    Due to the stringent limits for boron in drinking and irrigation water, water treatment facilities have to incur additional treatment to remove boron down to a safe concentration. Forward osmosis (FO) is a membrane technology that may reduce the energy required to remove boron present in seawater. In direct FO desalination hybrid systems, fresh water is recovered from seawater using a recoverable draw solution, FO membranes are expected to show high boron rejection. This study focuses on determining the boron rejection capabilities of a new generation thin-film composite (TFC) FO membrane compared to a first generation cellulose triacetate (CTA) FO membrane. The effects of water permeate flux, membrane structure, draw solute charge, and reverse solute flux on boron rejection were determined. For TFC and CTA FO membranes, experiments showed that when similar operating conditions are applied (e.g. membrane type and draw solute type) boron rejection decreases with increase in permeate flux. Reverse draw solute flux and membrane fouling have no significant impact on boron rejection. Compared to the first generation CTA FO membrane operated at the same conditions, the TFC FO membrane showed a 40% higher boron rejection capability and a 20% higher water flux. This demonstrates the potential for boron removal for new generation TFC FO membranes. © 2014 © 2014 Balaban Desalination Publications. All rights reserved.

  10. Boron removal from aqueous solution by direct contact membrane distillation

    International Nuclear Information System (INIS)

    The removal of boron from aqueous solution by direct contact membrane distillation (DCMD) was studied with self-prepared polyvinylidene fluoride (PVDF) hollow fiber membranes in the present work. The effect of pH, boron concentration, temperature and salt concentration of the feed solution on the boron rejection was investigated. The experimental results indicated that boron rejection was less dependent on the feed pH and salt concentration. DCMD process had high boron removal efficiency (>99.8%) and the permeate boron was below the maximum permissible level even at feed concentration as high as 750 mg/L. Although the permeate flux was enhanced exponentially with the feed temperature increasing, the influence of feed temperature on the boron rejection could be neglected. Finally, the natural groundwater sample containing 12.7 mg/L of boron was treated by DCMD process. The permeate boron kept below 20 μg/L whether the feed was acidified or not, but pre-acidification was helpful to maintain the permeate flux stability. All the experimental results indicated that DCMD could be efficiently used for boron removal from aqueous solution.

  11. ISOBORDAT: An Online Data Base on Boron Isotopes

    International Nuclear Information System (INIS)

    From 1986, boron isotope data in natural substances increased sharply in scientific publications. Analytical difficulties derived from complex geochemical matrices have been faced and interlaboratory calibrations reported in the boron literature. Boron isotopes are nowdays applied to investigate boron origin and migration in natural waters, sources of boron contamination, water-rock interactions and also contribute to water resource management. This is especially important in those areas where boron content exceeds the local regulations for drinking water supply and boron sources need to be identified. ISOBORDAT, an interactive database on boron isotope composition and content in natural waters is presented to the wider community of boron isotope users. The database's structure, scope and applications are reported, along with a discussion on δ11B values obtained in Italian waters. In the database boron data are structured in the following categories: rainwater, rivers, lakes, groundwater and potential contaminants. New categories (medium and high enthalpy fluids from volcanic and geothermal areas) are anticipated. ISOBORDAT aims to be as interactive as possible and will be developed taking into account information and suggestions received. The database is continually undergoing revision to keep pace with continuous data publication. Indications of data that are missing at present are greatly appreciated. (author)

  12. Synthesis and characterization of ammonium phosphate fertilizers with boron

    Directory of Open Access Journals (Sweden)

    ANGELA MAGDA

    2010-07-01

    Full Text Available The concentration of boron, an essential micronutrient for plants, presents a narrow range between deficiency and toxicity. In order to provide the boron requirement for plants, and to avoid toxicity problems, boron compounds are mixed with basic fertilizers. Sodium borate pentahydrate was used as a boron source. Ammonium orthophosphates fertilizers with boron were prepared by neutralizing phosphoric acid with ammonia and addition of variable amounts of sodium tetraborate pentahydrate to the reaction mixture at a NH3:H3PO4 molar ratio of 1.5. The fertilizers obtained with boron contents ranging from 0.05 to 1 % (w/w were fully characterized by chemical analysis, thermal analysis, X-ray diffraction and infrared spectrophotometry. The studies showed that up to 500 °C, regardless of the boron content, no significant changes concerning thermal stability and nutritional properties occurred. Above 500 °C, an increase of thermal stability with an increase of the boron content was observed. X-Ray diffraction of a heat-treated sample containing 5 % (w/w boron indicated the appearance of boron orthophosphate, BPO4, as a new crystalline phase, and the disappearance of the previous structures above 500 °C, which explains the increase in thermal stability.

  13. Structure and single-phase regime of boron carbides

    Science.gov (United States)

    Emin, David

    1988-09-01

    The boron carbides are composed of twelve-atom icosahedral clusters which are linked by direct covalent bonds and through three-atom intericosahedral chains. The boron carbides are known to exist as a single phase with carbon concentrations from about 8 to about 20 at. %. This range of carbon concentrations is made possible by the substitution of boron and carbon atoms for one another within both the icosahedra and intericosahedral chains. The most widely accepted structural model for B4C (the boron carbide with nominally 20% carbon) has B11C icosahedra with C-B-C intericosahedral chains. Here, the free energy of the boron carbides is studied as a function of carbon concentration by considering the effects of replacing carbon atoms within B4C with boron atoms. It is concluded that entropic and energetic considerations both favor the replacement of carbon atoms with boron atoms within the intericosahedral chains, C-B-C-->C-B-B. Once the carbon concentration is so low that the vast majority of the chains are C-B-B chains, near B13C2, subsequent substitutions of carbon atoms with boron atoms occur within the icosahedra, B11C-->B12. Maxima of the free energy occur at the most ordered compositions: B4C,B13C2,B14C. This structural model, determined by studying the free energy, agrees with that previously suggested by analysis of electronic and thermal transport data. These considerations also provide an explanation for the wide single-phase regime found for boron carbides. The significant entropies associated with compositional disorder within the boron carbides, the high temperatures at which boron carbides are formed (>2000 K), and the relatively modest energies associated with replacing carbon atoms with boron atoms enable the material's entropy to be usually important in determining its composition. As a result, boron carbides are able to exist in a wide range of compositions.

  14. Absolute calibration of TFTR helium proportional counters

    International Nuclear Information System (INIS)

    The TFTR helium proportional counters are located in the central five (5) channels of the TFTR multichannel neutron collimator. These detectors were absolutely calibrated using a 14 MeV neutron generator positioned at the horizontal midplane of the TFTR vacuum vessel. The neutron generator position was scanned in centimeter steps to determine the collimator aperture width to 14 MeV neutrons and the absolute sensitivity of each channel. Neutron profiles were measured for TFTR plasmas with time resolution between 5 msec and 50 msec depending upon count rates. The He detectors were used to measure the burnup of 1 MeV tritons in deuterium plasmas, the transport of tritium in trace tritium experiments, and the residual tritium levels in plasmas following 50:50 DT experiments

  15. Fast-neutron coincidence-counter manual

    International Nuclear Information System (INIS)

    The fast neutron counter (FNC) described in this report is a computer-based assay system employing fast-pulse counting instrumentation. It is installed below a glove box in the metal electrorefining area of the Los Alamos National Laboratory Plutonium Processing Facility. The instrument was designed to assay plutonium salts and residues from this process and to verify the mass of electrorefined metal. Los Alamos National Laboratory Groups Q-1, Q-3, and CMB-11 carried out a joint test and evaluation plan of this instrument between May 1978 and May 1979. The results of that evaluation, a description of the FNC, and operating instructions for further use are given in this report

  16. Test of a ring imaging Cherenkov counter

    International Nuclear Information System (INIS)

    We have tested a ring imaging Cherenkov counter with readout of the projection chamber type. A specific detector response of N0=80 cm-1 was measured which corresponds to 8 photoelectrons per event in a 1.60 m long nitrogen radiator. The resolution of the ring radius was measured to be Δr/r=3.6%. The crosstalk between neighboring wires due to photons generated in the avalanche process was estimated to contribute up to 50% per hit. It was reduced considerably by inserting shielding walls between the wires and by adding C2H6 or iC4H10 to the CH4-TMAE gas mixture. (orig.)

  17. EFFECT OF COUNTERS IN PERFORMANCE OF HADOOP

    Directory of Open Access Journals (Sweden)

    Preeti Jain

    2015-10-01

    Full Text Available Recent technological advancements have led to an overflow of data from distinctive domains (e.g., health care and scientific sensors, user-generated data, Internet and financial companies, and supply chain systems over the past two decades [1]. Big data is commonly unstructured, huge in volume and require more real-time analysis. This paper discusses a Big Data problem from NCDC for huge volume of weather data collected from various parts of world. We had generated map ( and reduce ( function for solving this problem and experimental results of these applications on a Hadoop cluster are being discussed. In this paper, performance of above application has been shown with respect to some counters available.

  18. A single-electron counter for nanodosimetry

    Energy Technology Data Exchange (ETDEWEB)

    Breskin, A.; Chechik, R.; Pansky, A.; Shchemelinin, S. [Weizmann Inst. of Science, Rehovot (Israel). Dept. of Particle Physics; Colautti, P.; Conte, V.; De Nardo, L.; Talpo, G. [Istituto Nazionale di Fisica Nucleare, Legnaro (Italy); Tornielli, G. [Istituto Nazionale di Fisica Nucleare, Padua (Italy)

    1995-12-31

    A detector has been devised able to measure with high resolution the primary ionisation yield in tissue-equivalent gas volumes of a few nanometers equivalent length. The sensitive ionisation volume is a wall-less millimetric region defined by a properly shaped electric field. Free electrons created by the radiation inside the sensitive volume are collected into an electron multiplier, capable of efficiently counting single electrons at low gas pressure. The single-electron detection system consists of a long drift column attached to a multistep proportional counter. The electron cloud created by the radiation inside the sensitive volume, diffuses along the drift column. Single electrons, successively arriving at the multiplier are amplified, giving rise to a pulse trail from which the original number of ionisation electrons is counted. The experimental set-up, the electron counting principle, and first data are presented and discussed. (author).

  19. A single-electron counter for nanodosimetry

    International Nuclear Information System (INIS)

    A detector has been devised able to measure with high resolution the primary ionisation yield in tissue-equivalent gas volumes of a few nanometers equivalent length. The sensitive ionisation volume is a wall-less millimetric region defined by a properly shaped electric field. Free electrons created by the radiation inside the sensitive volume are collected into an electron multiplier, capable of efficiently counting single electrons at low gas pressure. The single-electron detection system consists of a long drift column attached to a multistep proportional counter. The electron cloud created by the radiation inside the sensitive volume, diffuses along the drift column. Single electrons, successively arriving at the multiplier are amplified, giving rise to a pulse trail from which the original number of ionisation electrons is counted. The experimental set-up, the electron counting principle, and first data are presented and discussed. (author)

  20. Fluctuation phenomena in the proportional counter

    International Nuclear Information System (INIS)

    Fluctuations in the number of electron-ion pairs produced in the primary ionization and in the size of the subsequent electron avalanche, can be reduced by improving the efficiency of the ionization mechanisms by the Penning effect. Energy spent exciting metastable states is used to increase the ionization yield by introducing a second gas whose first ionization potential is slightly lower than the first metastable level of the main gas. A proportional counter filled with a range of Penning mixtures has been investigated experimentally. The Penning mixture argon-xenon gives an increased resolution over argon-methane. For fundamental studies of avalanche fluctuations in Penning mixtures, a uniform field chamber has been constructed. Experimental studies of f (the relative variance of the avalanche size) are compared with values predicted by various avalanche models. The results are reasonably close to predictions based on experimental measurements of ionization probability. (U.K.)

  1. An over-the-counter omission.

    Science.gov (United States)

    Scheurer, Danielle Bowen

    2006-09-01

    Despite the widespread use of over-the-counter (OTC) medications, their utilization is rarely ascertained at hospital admission. Presented here is an interesting case of acute renal failure and hemolytic anemia attributable to a commonly utilized OTC medication. The chronic use of phenazopyridine accounted for all of these findings. Upon discontinuation, everything normalized within one month. Although the differential diagnosis for renal failure and hemolytic anemia is extensive, scleral icterus, normal bilirubin, and orange-colored urine raised the suspicion of phenazopyridine use. This case report highlights overuse of common OTC medications, as well as a lack of knowledge of potential adverse reactions. With history-taking vigilance and patient education, adverse events from OTC medications can be minimized. PMID:17004539

  2. Modelling of an IR scintillation counter

    CERN Document Server

    Fraga, M M F; Policarpo, Armando

    2000-01-01

    A systematic study of the excitation and de-excitation mechanisms in ternary gas mixtures Ar+CO sub 2 +N sub 2 is presented regarding the possibility of developing a proportional scintillation counter based on the detection of the infrared molecular emissions associated with the lowest vibrational states of molecules. The use of visible or near-infrared photons (lambda<1 mu m) for applications like imaging and quality control of microstructure detectors has been reported. In view of these applications we analyse the processes leading to near-infrared emissions in pure argon and give an estimation of the number of photons emitted per electron, at several pressures, as a function of the charge gain.

  3. Bragg Curve Counter for primary beam monitor

    International Nuclear Information System (INIS)

    The prototype Bragg Curve Counter (BCC) has been tested by α-source (241Am) with a continuous gas flow system (P-10: 90% Ar+10% CH4, at 300Torr). Two types of the Frisch grid were prepared for the BCC. One was made of expanded metal meshes, which consist of 175 meshes/inch2 with a 100μmt nickel sheet. The other was made of a 1mm pitch wire with φ 50 μm of the tungsten. The shape of Bragg peak signal was compared each other. It was found that the energy spectrum obtained by the wire grid is a little sharper than that obtained by the meshes grid. However the meshes grid is superior than the wire grid so far as handling and durability are concerned. (author)

  4. Air-ion counter and mobility spectrometer

    International Nuclear Information System (INIS)

    Mono-electrode self “zeroing” air-ion counter and mobility (size) scanning spectrometer (CDI-011) based on the Gerdien aspirated condenser principle has been developed. Instrument is intended for short- and long-term indoor and outdoor air-ion concentration measurements and scanning of air-ions by mobility. Measuring small currents (typically 10−14 A) generated by the air-ions in outdoor conditions is demanding and causes many problems related to change of temperature, relative humidity, wind and electromagnetic noise. Also, measuring of both ion polarities with mono electrode detector require alternate changes of the polarizing voltage sign which produces capacitive current spikes. Various techniques, including “zeroing” method, have been applied to successfully overcome most of these measuring interferences.

  5. Air-ion counter and mobility spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Kolarz, Predrag, E-mail: kolarz@ipb.ac.rs [Institute of Physics, University of Belgrade, Pregrevica 118, 11080 Belgrade (Serbia); Miljkovic, Budimir [Merni Instrumenti D.O.O., Ljube Stojanovica 38, 11000 Belgrade (Serbia); Curguz, Zoran [Faculty of Transport and Traffic Engineering, University of East Sarajevo, Vojvode Misica 52, 74000 Doboj (Bosnia and Herzegowina)

    2012-05-15

    Mono-electrode self 'zeroing' air-ion counter and mobility (size) scanning spectrometer (CDI-011) based on the Gerdien aspirated condenser principle has been developed. Instrument is intended for short- and long-term indoor and outdoor air-ion concentration measurements and scanning of air-ions by mobility. Measuring small currents (typically 10{sup -14} A) generated by the air-ions in outdoor conditions is demanding and causes many problems related to change of temperature, relative humidity, wind and electromagnetic noise. Also, measuring of both ion polarities with mono electrode detector require alternate changes of the polarizing voltage sign which produces capacitive current spikes. Various techniques, including 'zeroing' method, have been applied to successfully overcome most of these measuring interferences.

  6. The Role of Hackers in Countering Surveillance and Promoting Democracy

    Directory of Open Access Journals (Sweden)

    Sebastian Kubitschko

    2015-09-01

    Full Text Available Practices related to media technologies and infrastructures (MTI are an increasingly important part of democratic constellations in general and of surveillance tactics in particular. This article does not seek to discuss surveillance per se, but instead to open a new line of inquiry by presenting qualitative research on the Chaos Computer Club (CCC—one of the world’s largest and Europe’s oldest hacker organizations. Despite the longstanding conception of hacking as infused with political significance, the scope and style of hackers’ engagement with emerging issues related to surveillance remains poorly understood. The rationale of this paper is to examine the CCC as a civil society organization that counter-acts contemporary assemblages of surveillance in two ways: first, by de-constructing existing technology and by supporting, building, maintaining and using alternative media technologies and infrastructures that enable more secure and anonymous communication; and second, by articulating their expertise related to contemporary MTI to a wide range of audiences, publics and actors. Highlighting the significance of “privacy” for the health of democracy, I argue that the hacker organization is co-determining “interstitial spaces within information processing practices” (Cohen, 2012, p. 1931, and by doing so is acting on indispensable structural features of contemporary democratic constellations.

  7. Low energy recoil detection with a spherical proportional counter

    CERN Document Server

    Savvidis, I; Eleftheriadis, C; Giomataris, I; Papaevangellou, T

    2016-01-01

    We present low energy recoil detection results in the keV energy region, from measurements performed with the Spherical Proportional Counter (SPC). An ${}^{241}Am-{}^{9}{Be}$ fast neutron source is used in order to obtain neutron-nucleus elastic scattering events inside the gaseous volume of the detector. The detector performance in the $keV$ energy region was resolved by observing the $5.9\\ keV$ line of a ${}^{55}Fe$ X-ray source, with energy resolution of $9\\%$ ($\\sigma$). The toolkit GEANT4 was used to simulate the irradiation of the detector by an ${}^{241}Am-{}^{9}{Be}$ source, while SRIM was used to calculate the Ionization Quenching Factor (IQF). The GEANT4 simulated energy deposition spectrum in addition with the SRIM calculated quenching factor provide valuable insight to the experimental results. The performance of the SPC in low energy recoil detection makes the detector a good candidate for a wide range of applications, including Supernova or reactor neutrino detection and Dark Matter (WIMP) searc...

  8. Efficiency measurement for solid track spark auto counters

    International Nuclear Information System (INIS)

    The theory of solid track spark auto counters was introduced. The best etch condition was explored. Efficiency for spark auto counters was measured. The ameliorating-factor for the hull's thickness and etch-thickness was measured. The measurement for ameliorating factors and efficiency makes solid track detect system, can be used for absolute fission rate measurement. (authors)

  9. 21 CFR 892.1130 - Nuclear whole body counter.

    Science.gov (United States)

    2010-04-01

    ... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Nuclear whole body counter. 892.1130 Section 892.1130 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES RADIOLOGY DEVICES Diagnostic Devices § 892.1130 Nuclear whole body counter....

  10. Majorizational Choosing of SeveralDifferent Fuzzy Counter Operator

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    Different fuzzy reasoning methods were made by choosing different fuzzy operater. This article generally introduced the basic structure of fuzzy controller ,and gave several different fuzzy controllers ,and compared and analyzed different fuzzy counters in theory and computer simulating control and realized majorizational choosing of several fuzzy counters.

  11. Automatic calibration system for VENUS lead glass counters

    International Nuclear Information System (INIS)

    Automatic calibration system for VENUS lead glass counters has been constructed. It consists of a moving table, position sensors, control electronics and a master minicomputer, (micro-11 of DEC). The system has been well operated for six months and one third of VENUS lead glass counters have been calibrated. (author)

  12. The Counter Terrorist Classroom: Religion, Education, and Security

    Science.gov (United States)

    Gearon, Liam

    2013-01-01

    The article identifies international cases--from the United States, Europe, and the United Nations--of an emergent interface of religion, education, and security. This is manifest in the uses of religion in education to counter religious extremism, the notional "counter terrorist classroom." To avoid an over-association of extremism with religion,…

  13. Test of TOF Scintillator Counters for ALICE Detector

    CERN Document Server

    Semenov, P; Malakhov, A; Melkumov, G L

    1996-01-01

    The manufactured counters of the fast response scintillators with the photomultipliers valid for operation in the magnetic field environment is being considered among the options for the time-of-flight (TOF) measurements as a particle identification tool for the ALICE experiment. Here we discuss how the tests of such counters have been implemented on the particle beam in respect to the time resolution.

  14. Investigation of sampling tubes of end-cap shower counter

    International Nuclear Information System (INIS)

    The measurement and investigation were conducted for the performances of sampling tubes of end-cap shower counter in BES. It is shown that the self-quenching streamer tube with 12.8 x 12.8 (1 + 2 + 1) is suitable for end-cap shower counter

  15. Recent results on aerogel development for use in Cherenkov counters

    CERN Document Server

    Danilyuk, A F; Savelieva, M D; Bobrovnikov, V S; Buzykaev, A R; Kravchenko, E A; Lavrov, A V; Onuchin, A P

    2002-01-01

    Synthesis of silica aerogel for Cherenkov counters is being studied for more than 10 years at the Boreskov Institute of Catalysis in collaboration with the Budker Institute of Nuclear Physics. Index of refraction, light scattering length and light absorption length are optical characteristics which determine the quality of aerogel Cherenkov counter. These parameters were measured for the aerogel produced. The results are presented.

  16. High pressure proportional counters operating in pure hydrogen

    International Nuclear Information System (INIS)

    Construction and operation of high pressure proportional counters designed for pressures up to 92 atm which work in pure hydrogen are described. This type of counter offering track reconstruction as well as energy loss determination will be employed as live-target for low-energy recoil measurements in elastic np scattering. (Auth.)

  17. Electrovacuum Static Counter-Rotating Relativistic Dust Disks

    CERN Document Server

    González, G A

    2002-01-01

    A detailed study of the Counter-Rotating Model (CRM) for generic electrostatic (magnetostatic) axially symmetric thin disks without radial pressure is presented. We find a general constraint over the counter-rotating tangential velocities needed to cast the surface energy-momentum tensor of the disk as the superposition of two counter-rotating charged dust fluids. We then show that this constraint is satisfied if we take the two counter-rotating streams as circulating along electrogeodesics with equal and opposite tangential velocities. We also find explicit expressions for the energy densities, electrostatic (magnetostatic) charge densities and velocities of the counter-rotating fluids. Three specific examples are considered where we obtain some CRM well behaved based in simple solutions to the Einstein-Maxwell equations. The considered solutions are Reissner-Nordstrom in the electrostatic case, its magnetostatic counterpart and two solutions obtained from Taub-NUT and Kerr solutions.

  18. DESIGN OF TERNARY COUNTER BASED ON ADIABATIC DOMINO CIRCUIT

    Institute of Scientific and Technical Information of China (English)

    Yang Qiankun; Wang Pengjun; Zheng Xuesong

    2013-01-01

    By researching the ternary counter and low power circuit design method,a novel design of low power ternary Domino counter on switch-level is proposed.Firstly,the switch-level structure expression of ternary loop operation circuit with enable pin is derived according to the switch-signal theory,and the one bit ternary counter is obtained combining the ternary adiabatic Domino literal operation circuit and buffer.Then the switch-level structure expression of enable signal circuit is derived,and the four bits ternary counter is obtained by cascade connection.Finally,the circuit is simulated by Spice tool and the output waveforms transform in proper order indicating that the logic function is correct.The energy consumption of the four bits ternary adiabatic Domino counter is 63% less than the conventional Domino counterpart.

  19. Potential of using boric acid as a boron drug for boron neutron capture therapy for osteosarcoma

    International Nuclear Information System (INIS)

    Osteosarcoma is a malignant tumor commonly found in human and animals. The ability of boric acid (BA) to accumulate in osteosarcoma due to the mechanism of the bone formation of cancer cells would make boron neutron capture therapy (BNCT) an alternative therapy for osteosarcoma. This study evaluated the feasibility of using BA as the boron drug for BNCT of bone cancer. The cytotoxicity of BA to L929 cells exceeded that of UMR-106 cells. With 25 μg 10B/mL medium of BA treatment, the boron concentration in UMR-106 cells was higher than that in L929 cells. The biodistribution and pharmacokinetics of BA in Sprague–Dawley (SD) rats were studied by administrating 25 mg 10B/kg body weight to SD rats. Blood boron level decreased rapidly within one hour after BA injection. Boron concentration in the long bone was 4–6 time higher than that of blood. Results of this study suggest that BA may be a potential drug for BNCT for osteosarcoma.

  20. Diffusion Boronizing of H11 Hot Work Tool Steel

    Science.gov (United States)

    Jurči, Peter; Hudáková, Mária

    2011-10-01

    The H11 hot work tool steel was boronized at various processing parameters, austenitized, quenched, and tempered to a core hardness of 47-48 HRC. Microstructure, phase constitution, and microhardness of boronized layers were investigated. Effect of boronized region on the bulk properties was determined by the Charpy impact test. Structure of boronized regions is formed by the compound layers and diffusion inter-layer. The compound layers consisted of only (Fe,Cr)2B phase, but in the case of longer processing time, they contained also of the (Fe,Cr)B-phase. The inter-layer contained enhanced portion of carbides, formed due to carbon diffusion from the boride compounds toward the substrate. Microhardness of boronized layers exceeded considerably 2000 HV 0.1. However, boronizing led to a substantial lowering of the Charpy impact toughness of the material.

  1. Boron Rich Solids Sensors, Ultra High Temperature Ceramics, Thermoelectrics, Armor

    CERN Document Server

    Orlovskaya, Nina

    2011-01-01

    The objective of this book is to discuss the current status of research and development of boron-rich solids as sensors, ultra-high temperature ceramics, thermoelectrics, and armor. Novel biological and chemical sensors made of stiff and light-weight boron-rich solids are very exciting and efficient for applications in medical diagnoses, environmental surveillance and the detection of pathogen and biological/chemical terrorism agents. Ultra-high temperature ceramic composites exhibit excellent oxidation and corrosion resistance for hypersonic vehicle applications. Boron-rich solids are also promising candidates for high-temperature thermoelectric conversion. Armor is another very important application of boron-rich solids, since most of them exhibit very high hardness, which makes them perfect candidates with high resistance to ballistic impact. The following topical areas are presented: •boron-rich solids: science and technology; •synthesis and sintering strategies of boron rich solids; •microcantileve...

  2. Boron carbide whisker and platelet reinforced ceramic matrix composites

    International Nuclear Information System (INIS)

    Boron carbide whisker and platelet-reinforced alumina and boron-carbide-whisker-reinforced silicon carbide composites were prepared by hot-pressing. The mechanical properties of hot-pressed boron carbide platelet and whisker-reinforced composites are better than the inherent ceramic matrix. A maximum fracture toughness, K(lc), of 9.5 MPa sq rt m is achieved for alumina/boron carbide whisker composites, 8.6 MPa sq rt m is achieved for alumina/boron carbide platelet composites, and 3.8 MPa sq rt m is achieved for silicon carbide/boron carbide whisker composites. The fracture toughness is dependent on the volume fraction of the platelets and whiskers. 12 refs

  3. Van Hove singularities of some icosahedral boron-rich solids by differential reflectivity spectra

    Science.gov (United States)

    Werheit, Helmut

    2015-09-01

    Differential reflectivity spectra of some icosahedral boron rich solids, β-rhombohedral boron, boron carbide and YB66-type crystals, were measured. The derivatives yield the van Hove singularities, which are compared with results obtained by other experimental methods.

  4. Three-dimensional atomic-scale imaging of impurity segregation to line defects

    Science.gov (United States)

    Blavette; Cadel; Fraczkiewicz; Menand

    1999-12-17

    Clouds of impurity atoms near line defects are believed to affect the plastic deformation of alloys. Three-dimensional atom probe techniques were used to image these so-called Cottrell atmospheres directly. Ordered iron-aluminum alloys (40 atomic percent aluminum) doped with boron (400 atomic parts per million) were investigated on an atomic scale along the direction. A boron enrichment was observed in the vicinity of an edge dislocation. The enriched region appeared as a three-dimensional pipe 5 nanometers in diameter, tangent to the dislocation line. The dislocation was found to be boron-enriched by a factor of 50 (2 atomic percent) relative to the bulk. The local boron enrichment is accompanied by a strong aluminum depletion of 20 atomic percent. PMID:10600736

  5. Multidimensional boron transport modeling in subchannel approach

    International Nuclear Information System (INIS)

    The main objective of this study is to implement a solute tracking model into the subchannel code CTF for simulations of boric acid transients. Previously, three different boron tracking models have been implemented into CTF and based on the applied analytical and nodal sensitivity studies the Modified Godunov Scheme approach with a physical diffusion term has been selected as the most accurate and best estimate solution. This paper will present the implementation of a multidimensional boron transport modeling with Modified Godunov Scheme within a thermal-hydraulic code based on a subchannel approach. Based on the cross flow mechanism in a multiple-subchannel rod bundle geometry, heat transfer and lateral pressure drop effects will be discussed in deboration and boration case studies. (author)

  6. Synthesis and characterization of boron nitrides nanotubes

    International Nuclear Information System (INIS)

    This paper presents a new synthesis for the production of boron nitride nanotubes (BNNT) from boron powder, ammonium nitrate and hematite tube furnace CVD method. The samples were subjected to some characterization techniques as infrared spectroscopy, thermal analysis, X-ray diffraction and scanning electron microscopy and transmission. By analyzing the results can explain the chemical reactions involved in the process and confirm the formation of BNNT with several layers and about 30 nanometers in diameter. Due to excellent mechanical properties and its chemical and thermal stability this material is promising for various applications. However, BNNT has received much less attention than carbon nanotubes, it is because of great difficulty to synthesize appreciable quantities from the techniques currently known, and this is one of the main reasons this work.(author)

  7. Microadditions of boron and vanadium in ADI

    Directory of Open Access Journals (Sweden)

    Rzychoń T.

    2007-01-01

    Full Text Available In the second part of the study, describing the role of vanadium and boron microadditions in the process of structure formation in heavy-walled castings made from ADI, the results of own investigations were presented. Within this study two series of melts of the ductile iron were made, introducing microadditions of the above mentioned elements to both unalloyed ductile iron and the ductile iron containing high levels of nickel and copper (the composition typical of ADI. Melts were conducted with iron-nickel-magnesium master alloy. Thermal analysis of the solidification process of the cast keel blocks was conducted, the heat treatment of the alloys was carried out, and then the effect of the introduced additions of boron and vanadium on the hardenability of the investigated cast iron was examined and evaluated.

  8. The spectrophotometric determination of boron in tourmalines

    Directory of Open Access Journals (Sweden)

    LJILJANA JAKSIC

    2005-02-01

    Full Text Available A procedure for the spectrophotometric determination of macro amounts of boron in tourmaline with azomethine H is described. The used tourmaline concentrate was obtained by magnetic separation and heavy-liquids purification of the schorl zone of pegmatite or granite aplite. The samples of tourmaline were decomposed by fusion with anhydrous sodium carbonate and taken up in dilute hydrochloric acid. The interfering effects of iron and aluminium were eliminated by masking with an EDTA – NTA solution. After pH adjustment, the boron was reacted with azomethine H and the absorbance of the obtained coloured complex was measured at 415 nm. The results are compared with those obtained by other procedures. The relative error of the determination was less than 3 %.

  9. Facile Synthesis of Ternary Boron Carbonitride Nanotubes

    Directory of Open Access Journals (Sweden)

    Luo Lijie

    2009-01-01

    Full Text Available Abstract In this study, a novel and facile approach for the synthesis of ternary boron carbonitride (B–C–N nanotubes was reported. Growth occurred by heating simple starting materials of boron powder, zinc oxide powder, and ethanol absolute at 1150 °C under a mixture gas flow of nitrogen and hydrogen. As substrate, commercial stainless steel foil with a typical thickness of 0.05 mm played an additional role of catalyst during the growth of nanotubes. The nanotubes were characterized by SEM, TEM, EDX, and EELS. The results indicate that the synthesized B–C–N nanotubes exhibit a bamboo-like morphology and B, C, and N elements are homogeneously distributed in the nanotubes. A catalyzed vapor–liquid–solid (VLS mechanism was proposed for the growth of the nanotubes.

  10. Behavior of Disordered Boron Carbide under Stress

    Science.gov (United States)

    Fanchini, Giovanni; McCauley, James W.; Chhowalla, Manish

    2006-07-01

    Gibbs free-energy calculations based on density functional theory have been used to determine the possible source of failure of boron carbide just above the Hugoniot elastic limit (HEL). A range of B4C polytypes is found to be stable at room pressure. The energetic barrier for shock amorphization of boron carbide is by far the lowest for the B12(CCC) polytype, requiring only 6GPa≈P(HEL) for collapse under hydrostatic conditions. The results clearly demonstrate that the collapse of the B12(CCC) phase leads to segregation of B12 and amorphous carbon in the form of 2 3 nm bands along the (113) lattice direction, in excellent agreement with recent transmission electron microscopy results.

  11. Investigation of boron segregation in low carbon steel

    OpenAIRE

    J. Lis; Lis, A; Kolan, C.

    2011-01-01

    Traces of born in the range 0,002-0,009 % are usually added to many grades of steel. The effect of boron on phase transformations and hardenability of low carbon low alloy steels depends on the form of its behavior in solid solution either in segregations or in precipitations. Temperature and cooling rate determine the existence of boron segregations on grain boundaries. In present paper simulations of boron concentrations were calculated with computer programme DICTRA for low carbon 0,08 %C ...

  12. Boron/aluminum shelf for shuttle orbiter

    International Nuclear Information System (INIS)

    Boron/aluminum skins and channels were used in the fabrication of a prototype honeycomb sandwich avionics shelf. The avionic shelves are stiffness-critical and must be vibration tolerant. In conjunction with the shelf mounting system, they must isolate the avionics equipment from the severe vibration of the primary and secondary structure nearby. Design rationale, fabrication procedures, vibration test criteria and test results are presented. (9 fig) (U.S.)

  13. Boron Nitride Nanosheets for Metal Protection

    OpenAIRE

    Li, Lu Hua; Xing, Tan; Chen, Ying; Jones, Rob

    2015-01-01

    Although the high impermeability of graphene makes it an excellent barrier to inhibit metal oxidation and corrosion, graphene can form a galvanic cell with the underlying metal that promotes corrosion of the metal in the long term. Boron nitride (BN) nanosheets which have a similar impermeability could be a better choice as protective barrier, because they are more thermally and chemically stable than graphene and, more importantly, do not cause galvanic corrosion due to their electrical insu...

  14. Anomalous thermal conductivity of monolayer boron nitride

    Science.gov (United States)

    Tabarraei, Alireza; Wang, Xiaonan

    2016-05-01

    In this paper, we use nonequilibrium molecular dynamics modeling to investigate the thermal properties of monolayer hexagonal boron nitride nanoribbons under uniaxial strain along their longitudinal axis. Our simulations predict that hexagonal boron nitride shows an anomalous thermal response to the applied uniaxial strain. Contrary to three dimensional materials, under uniaxial stretching, the thermal conductivity of boron nitride nanoribbons first increases rather than decreasing until it reaches its peak value and then starts decreasing. Under compressive strain, the thermal conductivity of monolayer boron nitride ribbons monolithically reduces rather than increasing. We use phonon spectrum and dispersion curves to investigate the mechanism responsible for the unexpected behavior. Our molecular dynamics modeling and density functional theory results show that application of longitudinal tensile strain leads to the reduction of the group velocities of longitudinal and transverse acoustic modes. Such a phonon softening mechanism acts to reduce the thermal conductivity of the nanoribbons. On the other hand, a significant increase in the group velocity (stiffening) of the flexural acoustic modes is observed, which counteracts the phonon softening effects of the longitudinal and transverse modes. The total thermal conductivity of the ribbons is a result of competition between these two mechanisms. At low tensile strain, the stiffening mechanism overcomes the softening mechanism which leads to an increase in the thermal conductivity. At higher tensile strain, the softening mechanism supersedes the stiffening and the thermal conductivity slightly reduces. Our simulations show that the decrease in the thermal conductivity under compressive strain is attributed to the formation of buckling defects which reduces the phonon mean free path.

  15. Formation and Structure of Boron Nitride Nanotubes

    Institute of Scientific and Technical Information of China (English)

    Jiang ZHANG; Zongquan LI; Jin XU

    2005-01-01

    Boron nitride (BN) nanotubes were simply synthesized by heating well-mixed boric acid, urea and iron nitrate powders at 1000℃. A small amount of BN nanowires was also obtained in the resultants. The morphological and structural characters of the BN nanostructures were studied using transmission electron microscopy. Other novel BN nanostructures, such as Y-junction nanotubes and bamboo-like nanotubes, were simultaneously observed. The growth mechanism of the BN nanotubes was discussed briefly.

  16. Thermal conductivity of nanostructured boron nitride materials.

    Science.gov (United States)

    Tang, Chengchun; Bando, Yoshio; Liu, Changhong; Fan, Shoushan; Zhang, Jun; Ding, Xiaoxia; Golberg, Dmitri

    2006-06-01

    We have measured the thermal conductivity of bulky pellets made of various boron nitride (BN)-based nanomaterials, including spherical nanoparticles, perfectly structured, bamboo-like nanotubes, and collapsed nanotubes. The thermal conductivity strongly depends on the morphology of the BN nanomaterials, especially on the surface structure. Spherical BN particles have the lowest thermal conductivity while the collapsed BN nanotubes possess the best thermoconductive properties. A model was proposed to explain the experimental observations based on the heat percolation passage considerations. PMID:16722739

  17. Channeling of boron ions into silicon

    Energy Technology Data Exchange (ETDEWEB)

    Lecrosnier, D.; Paugam, J.; Gallou, J.

    1977-04-01

    Channeled and random distributions of boron ions implanted over the energy range 50 keV--1.8 MeV into silicon have been measured using the differential capacitance technique. When implantations are performed along the <110> or <111> axis, profiles exhibit a strong orientation dependance. The best channeled profiles shows that more than 70% of the implanted dose is in the channeled peak.

  18. Boron content of the Freetown drinking water

    International Nuclear Information System (INIS)

    A method is described for the analyses of water samples in the Freetown area of Sierra Leone for their boron concentrations. The method involves alpha counting during thermal neutron irradiation of the samples utilising the 10Ba(n,α)7Li reaction. The alpha counting is via a liquid scintillator which also incorporates the water samples. A detailed outline of the experimental setup is given and the results obtained from measurement on water samples presented. (author)

  19. Boron carbide synthesis by plasma spray process

    Czech Academy of Sciences Publication Activity Database

    Ctibor, Pavel; Brožek, Vlastimil; Hofman, R.

    Bari : Department of Chemistry, University of Bari, 2003 - (d'Agostino, R.; Favia, P.; Fracassi, F.; Palumbo, F.), s. - [International Symposium on Plasma Chemistry/16th./. Taormina (IT), 22.06.2003-27.06.2003] R&D Projects: GA ČR GA104/01/0149 Institutional research plan: CEZ:AV0Z2043910 Keywords : boron carbide , plasma spray, synthesis Subject RIV: BL - Plasma and Gas Discharge Physics

  20. Plasma Spray Deposition of Boron Carbide

    Czech Academy of Sciences Publication Activity Database

    Brožek, Vlastimil; Hofman, R.; Ctibor, Pavel; Hrabovský, Milan

    Praha : MAXDORF, s.r.o., 2002 - (Nitsch, K.; Rodová, M.). s. 11-12 [Development of Materials Science in Research and Education.. 10.09.2002-12.09.2002, Ostravice] R&D Projects: GA ČR GA104/01/0149; GA ČR GA202/01/1563 Institutional research plan: CEZ:AV0Z2043910 Keywords : plasma spray, boron carbide Subject RIV: BL - Plasma and Gas Discharge Physics