WorldWideScience

Sample records for bench-scale test procedures

  1. 100 Area soil washing bench-scale test procedures

    International Nuclear Information System (INIS)

    Freeman, H.D.; Gerber, M.A.; Mattigod, S.V.; Serne, R.J.

    1993-03-01

    This document describes methodologies and procedures for conducting soil washing treatability tests in accordance with the 100 Area Soil Washing Treatability Test Plan (DOE-RL 1992, Draft A). The objective of this treatability study is to evaluate the use of physical separation systems and chemical extraction methods as a means of separating chemically and radioactively contaminated soil fractions from uncontaminated soil fractions. These data will be primarily used for determining feasibility of the individual unit operations and defining the requirements for a system, or systems, for pilot-scale testing

  2. 100 Area soil washing bench-scale test procedures

    Energy Technology Data Exchange (ETDEWEB)

    Freeman, H.D.; Gerber, M.A.; Mattigod, S.V.; Serne, R.J.

    1993-03-01

    This document describes methodologies and procedures for conducting soil washing treatability tests in accordance with the 100 Area Soil Washing Treatability Test Plan (DOE-RL 1992, Draft A). The objective of this treatability study is to evaluate the use of physical separation systems and chemical extraction methods as a means of separating chemically and radioactively contaminated soil fractions from uncontaminated soil fractions. These data will be primarily used for determining feasibility of the individual unit operations and defining the requirements for a system, or systems, for pilot-scale testing.

  3. 100 Area groundwater biodenitrification bench-scale treatability study procedures

    Energy Technology Data Exchange (ETDEWEB)

    Peyton, B.M.; Martin, K.R.

    1993-05-01

    This document describes the methodologies and procedures for conducting the bench-scale biodenitrification treatability tests at Pacific Northwest Laboratory{sup a} (PNL). Biodenitrification is the biological conversion of nitrate and nitrite to gaseous nitrogen. The tests will use statistically designed batch studies to determine if biodenitrification can reduce residual nitrate concentrations to 45 mg/L, the current maximum contaminant level (MCL). These tests will be carried out in anaerobic flasks with a carbon source added to demonstrate nitrate removal. At the pilot scale, an incremental amount of additional carbon will be required to remove the small amount of oxygen present in the incoming groundwater. These tests will be conducted under the guidance of Westinghouse Hanford Company (WHC) and the 100-HR-3 Groundwater Treatability Test Plan (DOE/RL-92-73) and the Treatability Study Program Plan (DOE/RL-92-48) using groundwater from 100-HR-3. In addition to the procedures, requirements for safety, quality assurance, reporting, and schedule are given. Appendices include analytical procedures, a Quality Assurance Project Plan, a Health and Safety Plan, and Applicable Material Data Safety Sheets. The procedures contained herein are designed specifically for the 100-HR-3 Groundwater Treatability Test Plan, and while the author believes that the methods described herein are scientifically valid, the procedures should not be construed or mistaken to be generally applicable to any other treatability study.

  4. Bench Scale Saltcake Dissolution Test Report

    International Nuclear Information System (INIS)

    BECHTOLD, D.B.; PACQUET, E.A.

    2000-01-01

    A potential scenario for retrieving saltcake from single shell tanks is the ''Rainbird(reg s ign) sprinkler'' method. Water is distributed evenly across the surface of the saltcake and allowed to percolate by gravity through the waste. The salt dissolves in the water, forming a saturated solution. The saturated liquid is removed by a saltwell pump situated near the bottom of the tank. By this method, there is never a large inventory of liquid in the tank that could pose a threat of leakage. There are many variables or factors that can influence the hydrodynamics of this retrieval process. They include saltcake porosity; saltwell pumping rate; salt dissolution chemistry; factors that could promote flow channeling (e.g. tank walls, dry wells, inclusions or discontinuities in the saltcake); method of water distribution; plug formation due to crystal formations or accumulation of insoluble solids. A brief literature search indicates that very little experimental data exist on these aspects of saltcake dissolution (Wiersma 1996, 1997). The tests reported here were planned (Herting, 2000) to provide preliminary data and information for planning future, scaled-up tests of the sprinkler method

  5. Goethite Bench-scale and Large-scale Preparation Tests

    Energy Technology Data Exchange (ETDEWEB)

    Josephson, Gary B.; Westsik, Joseph H.

    2011-10-23

    The Hanford Waste Treatment and Immobilization Plant (WTP) is the keystone for cleanup of high-level radioactive waste from our nation's nuclear defense program. The WTP will process high-level waste from the Hanford tanks and produce immobilized high-level waste glass for disposal at a national repository, low activity waste (LAW) glass, and liquid effluent from the vitrification off-gas scrubbers. The liquid effluent will be stabilized into a secondary waste form (e.g. grout-like material) and disposed on the Hanford site in the Integrated Disposal Facility (IDF) along with the low-activity waste glass. The major long-term environmental impact at Hanford results from technetium that volatilizes from the WTP melters and finally resides in the secondary waste. Laboratory studies have indicated that pertechnetate ({sup 99}TcO{sub 4}{sup -}) can be reduced and captured into a solid solution of {alpha}-FeOOH, goethite (Um 2010). Goethite is a stable mineral and can significantly retard the release of technetium to the environment from the IDF. The laboratory studies were conducted using reaction times of many days, which is typical of environmental subsurface reactions that were the genesis of this new process. This study was the first step in considering adaptation of the slow laboratory steps to a larger-scale and faster process that could be conducted either within the WTP or within the effluent treatment facility (ETF). Two levels of scale-up tests were conducted (25x and 400x). The largest scale-up produced slurries of Fe-rich precipitates that contained rhenium as a nonradioactive surrogate for {sup 99}Tc. The slurries were used in melter tests at Vitreous State Laboratory (VSL) to determine whether captured rhenium was less volatile in the vitrification process than rhenium in an unmodified feed. A critical step in the technetium immobilization process is to chemically reduce Tc(VII) in the pertechnetate (TcO{sub 4}{sup -}) to Tc(Iv)by reaction with the

  6. Bench-scale testing of a micronized magnetite, fine-coal cleaning process

    Energy Technology Data Exchange (ETDEWEB)

    Suardini, P.J. [Custom Coals, International, Pittsburgh, PA (United States)

    1995-11-01

    Custom Coals, International has installed and is presently testing a 500 lb/hr. micronized-magnetite, fine-coal cleaning circuit at PETC`s Process Research Facility (PRF). The cost-shared project was awarded as part of the Coal Preparation Program`s, High Efficiency Preparation Subprogram. The project includes design, construction, testing, and decommissioning of a fully-integrated, bench-scale circuit, complete with feed coal classification to remove the minus 30 micron slimes, dense medium cycloning of the 300 by 30 micron feed coal using a nominal minus 10 micron size magnetite medium, and medium recovery using drain and rinse screens and various stages and types of magnetic separators. This paper describes the project circuit and goals, including a description of the current project status and the sources of coal and magnetite which are being tested.

  7. Performance study of protective clothing against hot water splashes: from bench scale test to instrumented manikin test.

    Science.gov (United States)

    Lu, Yehu; Song, Guowen; Wang, Faming

    2015-03-01

    Hot liquid hazards existing in work environments are shown to be a considerable risk for industrial workers. In this study, the predicted protection from fabric was assessed by a modified hot liquid splash tester. In these tests, conditions with and without an air spacer were applied. The protective performance of a garment exposed to hot water spray was investigated by a spray manikin evaluation system. Three-dimensional body scanning technique was used to characterize the air gap size between the protective clothing and the manikin skin. The relationship between bench scale test and manikin test was discussed and the regression model was established to predict the overall percentage of skin burn while wearing protective clothing. The results demonstrated strong correlations between bench scale test and manikin test. Based on these studies, the overall performance of protective clothing against hot water spray can be estimated on the basis of the results of the bench scale hot water splashes test and the information of air gap size entrapped in clothing. The findings provide effective guides for the design and material selection while developing high performance protective clothing. Published by Oxford University Press on behalf of the British Occupational Hygiene Society 2014.

  8. 100 Area soil washing: Bench scale tests on 116-F-4 pluto crib soil

    Energy Technology Data Exchange (ETDEWEB)

    Field, J.G.

    1994-06-10

    The Pacific Northwest Laboratory conducted a bench-scale treatability study on a pluto crib soil sample from 100 Area of the Hanford Site. The objective of this study was to evaluate the use of physical separation (wet sieving), treatment processes (attrition scrubbing, and autogenous surface grinding), and chemical extraction methods as a means of separating radioactively-contaminated soil fractions from uncontaminated soil fractions. The soil washing treatability study was conducted on a soil sample from the 116-F-4 Pluto Crib that had been dug up as part of an excavation treatability study. Trace element analyses of this soil showed no elevated concentrations above typically uncontaminated soil background levels. Data on the distribution of radionuclide in various size fractions indicated that the soil-washing tests should be focused on the gravel and sand fractions of the 116-F-4 soil. The radionuclide data also showed that {sup 137}Cs was the only contaminant in this soil that exceeded the test performance goal (TPG). Therefore, the effectiveness of subsequent soil-washing tests for 116-F-4 soil was evaluated on the basis of activity attenuation of {sup 137}Cs in the gravel- and sand-size fractions.

  9. Continuous bench-scale slurry catalyst testing direct coal liquefaction rawhide sub-bituminous coal

    Energy Technology Data Exchange (ETDEWEB)

    Bauman, R.F.; Coless, L.A.; Davis, S.M. [and others

    1995-12-31

    In 1992, the Department of Energy (DOE) sponsored research to demonstrate a dispersed catalyst system using a combination of molybdenum and iron precursors for direct coal liquefaction. This dispersed catalyst system was successfully demonstrated using Black Thunder sub-bituminous coal at Wilsonville, Alabama by Southern Electric International, Inc. The DOE sponsored research continues at Exxon Research and Development Laboratories (ERDL). A six month continuous bench-scale program using ERDL`s Recycle Coal Liquefaction Unit (RCLU) is planned, three months in 1994 and three months in 1995. The initial conditions in RCLU reflect experience gained from the Wilsonville facility in their Test Run 263. Rawhide sub-bituminous coal which is similar to the Black Thunder coal tested at Wilsonville was used as the feed coal. A slate of five dispersed catalysts for direct coal liquefaction of Rawhide sub-bituminous coal has been tested. Throughout the experiments, the molybdenum addition rate was held constant at 100 wppm while the iron oxide addition rate was varied from 0.25 to 1.0 weight percent (dry coal basis). This report covers the 1994 operations and accomplishments.

  10. Domestic Wastewater Reuse in Concrete Using Bench-Scale Testing and Full-Scale Implementation

    Directory of Open Access Journals (Sweden)

    Ayoup M. Ghrair

    2016-08-01

    Full Text Available Demand for fresh water by the construction sector is expected to increase due to the high increase in the growth of construction activities in Jordan. This study aims to evaluate the potential of scale-up of the application of treated domestic wastewater in concrete from bench-scale to a full-scale. On the lab scale, concrete and mortar mixes using Primary and Secondary Treated Wastewater (PTW, STW and Distilled Water (DW were cast and tested after various curing ages (7, 28, 120, and 200 days. Based on wastewater quality, according to IS 456-2000, the STW is suitable for mortar and concrete production. Mortar made with STW at curing time up to 200 days has no significant negative effect on the mortar’s compressive strength. Conversely, the PTW exceeded the maximum permissible limits of total organic content and E coli. for concrete mixing-water. Using PTW results, a significant increase in the initial setting time of up to 16.7% and a decrease in the concrete workability are observed. In addition, using PTW as mixing water led to a significant reduction in the compressive strength up to 19.6%. The results that came out from scaling up to real production operation of ready-mix concrete were in harmony with the lab-scale results.

  11. Results of bench-scale plasma system testing in support of the Plasma Hearth Process

    International Nuclear Information System (INIS)

    Leatherman, G.L.; Cornelison, C.; Frank, S.

    1996-01-01

    The Plasma Hearth Process (PHP) is a high-temperature process that destroys hazardous organic components and stabilizes the radioactive components and hazardous metals in a leach-resistant vitreous slag waste form. The PHP technology development program is targeted at mixed waste that cannot be easily treated by conventional means. For example, heterogeneous debris, which may contain hazardous organics, toxic metals, and radionuclides, is difficult to characterize and cannot be treated with conventional thermal, chemical, or physical treatment methods. A major advantage of the PHP over other plasma processes is its ability to separate nonradioactive, non-hazardous metals from the non-metallic and radioactive components which are contained in the vitreous slag. The overall PHP program involves the design, fabrication, and operation of test hardware to demonstrate and certify that the PHP concept is viable for DOE waste treatment. The program involves bench-scale testing of PHP equipment in radioactive service, as well as pilot-scale demonstration of the PHP concept using nonradioactive, surrogate test materials. The fate of secondary waste streams is an important consideration for any technology considered for processing mixed waste. The main secondary waste stream generated by the PHP is flyash captured by the fabric- filter baghouse. The PHP concept is that flyash generated by the process can, to a large extent, be treated by processing this secondary waste stream in the PHP. Prior to the work presented in the paper, however, the PHP project has not quantitatively demonstrated the ability to treat PHP generated flyash. A major consideration is the quantity of radionuclides and RCRA-regulated metals in the flyash that can be retained the resultant waste form

  12. Bench scale testing of micronized magnetite beneficiation. Quarterly technical progress report 4, October--December, 1993

    Energy Technology Data Exchange (ETDEWEB)

    Anast, K.

    1994-01-25

    This project is aimed at development of a process that, by using ultra fine magnetite suspension, would expand the application of heavy media separation technology to processing fine, {minus}28 mesh coals. These coal fines, produced during coal mining and crushing, are separated in the conventional coal preparation plant and generally impounded in a tailings pond. Development of an economic process for processing these fines into marketable product will expand the utilization of coal for power production in an environmentally acceptable and economically viable way. This process has been successfully researched at PETC but has not been studied on a continuous bench-scale unit, which is a necessary step towards commercial development of this promising technology. The goal of the program is to investigate the technology in a continuous circuit at a reasonable scale to provide a design basis for larger plants and a commercial feasibility data.

  13. Crucible melts and bench-scale ISV [in situ vitrification] tests on simulated wastes in INEL [Idaho National Engineering Laboratory] soils

    International Nuclear Information System (INIS)

    Farnsworth, R.K.; Oma, K.H.; Reimus, M.A.H.

    1990-05-01

    This report summarizes the results of eight crucible melt tests and three bench-scale in situ vitrification (ISV) test that were performed on simulated metals/soils mixtures containing actual site soils from the Idaho National Engineering Laboratory (INEL). The crucible melt and bench-scale ISV tests are a part of efforts by the Pacific Northwest Laboratory (PNL) to assist the INEL in conducting a treatability study on ISV for application to the mixed waste buried at the INEL subsurface disposal area (SDA). The crucible melt tests were performed to evaluate the effect of various chemical additives and metal oxidation techniques on soil melting temperatures, melt viscosities, metals versus electrode oxidation potentials, and metals incorporation in the glass. The bench-scale ISV tests were performed to supplement the existing ISV data base with information on certain hazardous materials that have not been adequately evaluated in previous ISV tests. These materials included five EP toxicity metals, various volatile organic materials fixed in a cementitious matrix [including carbon tetrachloride (CCl 4 ), trichloroethylene (TCE), and tetrachloroethylene (PCE)], and asbestos. In addition, the bench-scale test were used to evaluated the effect of the proposed chemical additive on ISV processing performance and product quality. 8 refs., 24 figs., 19 tabs

  14. Bench Scale Development and Testing of Aerogel Sorbents for CO2 Capture Final Technical Report

    Energy Technology Data Exchange (ETDEWEB)

    Begag, Redouane [Aspen Aerogels, Northborough, MA (United States)

    2017-03-30

    The primary objective of this project was scaling up and evaluating a novel Amine Functionalized Aerogel (AFA) sorbent in a bench scale fluidized bed reactor. The project team (Aspen Aerogels, University of Akron, ADA-ES, and Longtail Consulting) has carried out numerous tests and optimization studies to demonstrate the CO2 capture performance of the AFA sorbent in all its forms: powder, pellet, and bead. The CO2 capture target performance of the AFA sorbent (all forms) were set at > 12 wt.% and > 6 wt.% for total and working CO2 capacity, respectively (@ 40 °C adsorption / 100 – 120 °C desorption). The optimized AFA powders outperformed the performance targets by more than 30%, for the total CO2 capacity (14 - 20 wt.%), and an average of 10 % more for working CO2 capacity (6.6 – 7.0 wt.%, and could be as high as 9.6 wt. % when desorbed at 120 °C). The University of Akron developed binder formulations, pellet production methods, and post treatment technology for increased resistance to attrition and flue gas contaminants. In pellet form the AFA total CO2 capacity was ~ 12 wt.% (over 85% capacity retention of that of the powder), and there was less than 13% degradation in CO2 capture capacity after 20 cycles in the presence of 40 ppm SO2. ADA-ES assessed the performance of the AFA powder, pellet, and bead by analyzing sorption isotherms, water uptake analysis, cycling stability, jet cup attrition and crush tests. At bench scale, the hydrodynamic and heat transfer properties of the AFA sorbent pellet in fluidized bed conditions were evaluated at Particulate Solid Research, Inc. (PSRI). After the process design requirements were completed, by Longtail Consulting LLC, a techno-economic analysis was achieved using guidance from The National Energy Technology Laboratory (NETL) report. This report provides the necessary framework to estimate costs for a temperature swing post

  15. Recommendations for Filler Material Composition and Delivery Method for Bench-Scale Testing

    Energy Technology Data Exchange (ETDEWEB)

    Hardin, Ernest [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Brady, Patrick Vane [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)

    2018-03-01

    This report supplements Joint Workplan on Filler Investigations for DPCs (SNL 2017) providing new and some corrected information for use in planning Phase 1 laboratory testing of slurry cements as possible DPC fillers. The scope description is to "Describe a complete laboratory testing program for filler composition, delivery, emplacement in surrogate canisters, and post-test examination. To the extent possible specify filler material and equipment sources." This report includes results from an independent expert review (Dr. Arun Wagh, retired from Argonne National Laboratory and contracted by Sandia) that helped to narrow the range of cement types for consideration, and to provide further guidance on mix variations to optimize injectability, durability, and other aspects of filler performance.

  16. Bench Scale Development and Testing of a Novel Adsorption Process for Post-Combustion CO₂ Capture

    Energy Technology Data Exchange (ETDEWEB)

    Jain, Ravi [Innosepra Limited Liability Company, Middlesex, NJ (United States)

    2015-09-01

    A physical sorption process to produce dry CO₂ at high purity (>98%) and high recovery (>90%) from the flue gas taken before or after the FGD was demonstrated both in the lab and in the field (one ton per day scale). A CO₂ recovery of over 94% and a CO₂ purity of over 99% were obtained in the field tests. The process has a moisture, SOX, and Hg removal stage followed by a CO₂ adsorption stage. Evaluations based on field testing, process simulation and detailed engineering studies indicate that the process has the potential for more than 40% reduction in the capital and more than 40% reduction in parasitic power for CO₂ capture compared to MEA. The process has the potential to provide CO₂ at a cost (<$40/tonne) and quality (<1 ppm H₂O, <1 ppm SOX, <10 ppm O₂) suitable for EOR applications which can make CO₂ capture profitable even in the absence of climate legislation. The process is applicable to power plants without SOX, Hg and NOX removal equipment.

  17. Permeable Reactive Biobarriers for In Situ Cr(VI) Reduction: Bench Scale Tests Using Cellulomonas sp. Strain ES6

    Energy Technology Data Exchange (ETDEWEB)

    Sridhar Viamajala; Brent M. Peyton; Robin Gerlach; Vaideeswaran; William A. Apel; James N. Petersen

    2008-12-01

    Chromate (Cr(VI)) reduction studies were performed in bench scale flow columns using the fermentative subsurface isolate Cellulomonas sp. strain ES6. In these tests, columns packed with either quartz sand or hydrous ferric oxide (HFO)-coated quartz sand, were inoculated with strain ES6 and fed nutrients to stimulate growth before nutrient-free Cr(VI) solutions were injected. Results show that in columns containing quartz sand, a continuous inflow of 2 mg/L Cr(VI) was reduced to below detection limits in the effluent for durations of up to 5.7 residence times after nutrient injection was discontinued proving the ability of strain ES6 to reduce chromate in the absence of an external electron donor. In the HFO-containing columns, Cr(VI) reduction was significantly prolonged and effluent Cr(VI) concentrations remained below detectable levels for periods of up to 66 residence times after nutrient injection was discontinued. Fe was detected in the effluent of the HFO-containing columns throughout the period of Cr(VI) removal indicating that the insoluble Fe(III) bearing solids were being continuously reduced to form soluble Fe(II) resulting in prolonged abiotic Cr(VI) reduction. Thus, growth of Cellulomonas within the soil columns resulted in formation of permeable reactive barriers that could reduce Cr(VI) and Fe(III) for extended periods even in the absence of external electron donors. Other bioremediation systems employing Fe(II)-mediated reactions require a continuous presence of external nutrients to regenerate Fe(II). After depletion of nutrients, contaminant removal within these systems occurs by reaction with surface-associated Fe(II) that can rapidly become inaccessible due to formation of crystalline Fe-minerals or other precipitates. The ability of fermentative organisms like Cellulomonas to reduce metals without continuous nutrient supply in the subsurface offers a viable and economical alternative technology for in situ remediation of Cr

  18. Permeable reactive biobarriers for in situ Cr(VI) reduction: bench scale tests using Cellulomonas sp. strain ES6.

    Science.gov (United States)

    Viamajala, Sridhar; Peyton, Brent M; Gerlach, Robin; Sivaswamy, Vaideeswaran; Apel, William A; Petersen, James N

    2008-12-15

    Chromate (Cr(VI)) reduction studies were performed in bench scale flow columns using the fermentative subsurface isolate Cellulomonas sp. strain ES6. In these tests, columns packed with either quartz sand or hydrous ferric oxide (HFO)-coated quartz sand, were inoculated with strain ES6 and fed nutrients to stimulate growth before nutrient-free Cr(VI) solutions were injected. Results show that in columns containing quartz sand, a continuous inflow of 2 mg/L Cr(VI) was reduced to below detection limits in the effluent for durations of up to 5.7 residence times after nutrient injection was discontinued proving the ability of strain ES6 to reduce chromate in the absence of an external electron donor. In the HFO-containing columns, Cr(VI) reduction was significantly prolonged and effluent Cr(VI) concentrations remained below detectable levels for periods of up to 66 residence times after nutrient injection was discontinued. Fe was detected in the effluent of the HFO-containing columns throughout the period of Cr(VI) removal indicating that the insoluble Fe(III) bearing solids were being continuously reduced to form soluble Fe(II) resulting in prolonged abiotic Cr(VI) reduction. Thus, growth of Cellulomonas within the soil columns resulted in formation of permeable reactive barriers that could reduce Cr(VI) and Fe(III) for extended periods even in the absence of external electron donors. Other bioremediation systems employing Fe(II)-mediated reactions require a continuous presence of external nutrients to regenerate Fe(II). After depletion of nutrients, contaminant removal within these systems occurs by reaction with surface-associated Fe(II) that can rapidly become inaccessible due to formation of crystalline Fe-minerals or other precipitates. The ability of fermentative organisms like Cellulomonas to reduce metals without continuous nutrient supply in the subsurface offers a viable and economical alternative technology for in situ remediation of Cr

  19. Bench-scale testing of on-line control of column flotation using a novel analyzer. Third quarterly technical progress report, April 1, 1993--June 30, 1993

    Energy Technology Data Exchange (ETDEWEB)

    1993-08-24

    This document contains the third quarterly technical progress report for PTI`s Bench-Scale Testing Project of a circuit integrating PTI`s KEN-FLOTETM Column Flotation Technology and PTI`s On-Line Quality Monitor and Control System. The twelve-month project involves installation and testing of a 200--300 lb/hr. bench-scale flotation circuit at PETC`s Coal Preparation Process Research Facility (CPPRF) for two bituminous coals (Upper Freeport and Pittsburgh No. 8 Seam Raw Coals). Figure 1 contains the project plan, as well as the approach to completing the major tasks within the twelve-month project schedule. The project is broken down into three phases, which include: Phase I -- Preparation: The preparation phase was performed principally at PTI`s Calumet offices from October through December, 1992. It involved building of the equipment and circuitry, as well as some preliminary design and equipment testing; Phase II -- ET Circuit Installation and Testing: This installation and testing phase of the project was performed at PETC`s CPPRF from January through June, 1993, and was the major focus of the project. It involved testing of the continuous 200--300 lb/hr. circuit; and Phase III -- Project Finalization: The project finalization phase is occurring from July through September, 1993, at PTI`s Calumet offices and involves finalizing analytical work and data evaluation, as well as final project reporting. This Third Quarterly Technical Progress Report principally summarizes the results from the benchscale testing with the second coal (Pittsburgh No. 8 Seam Coal), which occurred in April through June, 1993. It also contains preliminary economic evaluations that will go into the Final Report, as well as the plan for the final reporting task.

  20. BENCH SCALE SALTSTONE PROCESS DEVELOPMENT MIXING STUDY

    Energy Technology Data Exchange (ETDEWEB)

    Cozzi, A.; Hansen, E.

    2011-08-03

    The Savannah River National Laboratory (SRNL) was requested to develop a bench scale test facility, using a mixer, transfer pump, and transfer line to determine the impact of conveying the grout through the transfer lines to the vault on grout properties. Bench scale testing focused on the effect the transfer line has on the rheological property of the grout as it was processed through the transfer line. Rheological and other physical properties of grout samples were obtained prior to and after pumping through a transfer line. The Bench Scale Mixing Rig (BSMR) consisted of two mixing tanks, grout feed tank, transfer pump and transfer hose. The mixing tanks were used to batch the grout which was then transferred into the grout feed tank. The contents of the feed tank were then pumped through the transfer line (hose) using a progressive cavity pump. The grout flow rate and pump discharge pressure were monitored. Four sampling stations were located along the length of the transfer line at the 5, 105 and 205 feet past the transfer pump and at 305 feet, the discharge of the hose. Scaling between the full scale piping at Saltstone to bench scale testing at SRNL was performed by maintaining the same shear rate and total shear at the wall of the transfer line. The results of scaling down resulted in a shorter transfer line, a lower average velocity, the same transfer time and similar pressure drops. The condition of flow in the bench scale transfer line is laminar. The flow in the full scale pipe is in the transition region, but is more laminar than turbulent. The resulting plug in laminar flow in the bench scale results in a region of no-mixing. Hence mixing, or shearing, at the bench scale should be less than that observed in the full scale, where this plug is non existent due to the turbulent flow. The bench scale tests should be considered to be conservative due to the highly laminar condition of flow that exists. Two BSMR runs were performed. In both cases, wall

  1. TDT-3R Clean Multi Fuels. ECN contribution to WP3. Lab-/bench-scale pyrolysis test of biomass and analysis of byproducts

    International Nuclear Information System (INIS)

    Bos, A.; Oudhuis, A.B.J.; Zwart, R.W.R.; Boersma, A.R.

    2005-11-01

    Under the present conditions it is expected that coal will still be used for a long period as a energy source. Furthermore, biomass is emerging as a new renewable CO2-neutral energy source in the future. Both fuels need significantly lower emissions to meet new (future) European Union environmental norms for sustainable clean energy production. Several technologies and 'end-of pipe' solutions have been developed in the past to reach these stricter emission limits. Examples are integrated combined cycle gasification systems (IGCC) for large scale use (>250 MW capacity). Also, a large number of gas cleaning technologies have been developed. These technologies are up-to-now rather complicated and/or costly and therefore also new solutions have to be developed. The 3R Multifuel process is aimed to offer a solution to these problems, especially for low-rank coals like brown coal, lignite, high sulfur coal, derived fuels and biomass. The objectives for ECN in the Work Package 3 of this project are: (a) to summarise and update data for the potential of biomass and waste streams in Europe for power production; and (b) to select biomass/waste streams to be tested in the lab/bench-scale facility and to generate design data for clean solid fuel production from biomass to be used for a pilot facility in Hungary. TDT-3R stands for Thermal Desorption Technology-Recycle-Reduce-Reuse

  2. Bench-scale testing of the micronized magnetite process. Eighth quarterly technical progress report, April--June, 1996

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1996-08-13

    The major focus of the project is to install and test a 500 lbs./hr. fine-coal cleaning circuit at DOE`s Process Research Facility (PRF), located at the Pittsburgh Energy Technology Center (PETC). The circuit will utilize an extremely fine, micron-sized magnetite media and small diameter cyclones to make efficient density separations on minus-28-Mesh coal. The circuit consists of three subcircuits: Classification Circuit; Dense-Medium Cycloning Circuit; and Magnetite Recovery Circuit. The testing scope involves initial closed-loop testing of each subcircuit to optimize the performance of the equipment in each subcircuit (i.e., Component Testing), followed by open-circuit testing of the entire integrated circuit to optimize the process and quantify the process efficiency (i.e., Integrated Testing). This report contains a short discussion of the project description, objectives, budget, schedule, and teaming arrangement. It also includes a detailed discussion of the above mentioned project accomplishments and plans, organized by the various task series within the project work plan. The final section contains an outline of the specific project goals for the next quarterly reporting period.

  3. Production of Jet Fuels from Coal Derived Liquids. Volume 9. Results of Bench-Scale and Pilot Plant Testing

    Science.gov (United States)

    1989-06-01

    Great Plains Coal Gasification Plant in Beulah, North Dakota. Experiments show that the hydroprocessing conditions recommended in Task 1 are not severe...50 REFERENCES. ............................ 51 APPENDIX A: LCI Test Report on Expanded-Bed Al Hydroprocessing of 300*F+ Great Plains Tar ...recovered by gravity separation. The heaviest portion of the tar oil, which contains about 20 percent coal dust, is recycled to the gasifiers. The recycle

  4. Hydrogen production with short contact time. Catalytic partial oxidation of hydrocarbons and oxygenated compounds: Recent advances in pilot- and bench-scale testing and process design

    Energy Technology Data Exchange (ETDEWEB)

    Guarinoni, A.; Ponzo, R.; Basini, L. [ENI Refining and Marketing Div., San Donato Milanese (Italy)

    2010-12-30

    ENI R and D has been active for fifteen years in the development of Short Contact Time - Catalytic Partial Oxidation (SCT-CPO) technologies for producing Hydrogen/Synthesis Gas. From the beginning the experimental work addressed either at defining the fundamental principles or the technical and economical potential of the technology. Good experimental responses, technical solutions' simplicity and flexibility, favourable techno-economical evaluations promoted the progressive widening of the field of the investigations. From Natural Gas (NG) the range of ''processable'' Hydrocarbons extended to Liquefied Petroleum Gas (LPG) and Gasoils, including those characterised by high levels of unsaturated and sulphurated molecules and, lately, to other compounds with biological origin. The extensive work led to the definition of different technological solutions, grouped as follows: Technology 1: Air Blown SCT-CPO of Gaseous Hydrocarbons and/or Light Compounds with biological origin Technology 2: Enriched Air/Oxygen Blown SCT-CPO of Gaseous Hydrocarbons and/or Light Compounds with biological origin Technology 3: Enriched Air/Oxygen Blown SCT-CPO of Liquid Hydrocarbons and/or Compounds with biological origin Recently, the licence rights on a non-exclusive basis for the commercialisation of SCT-CPO based processes for H{sub 2}/Synthesis gas production from light hydrocarbons with production capacity lower than 5,000 Nm{sup 3}/h of H{sub 2} or 7,500 Nm3/h of syngas have been assigned to two external companies. In parallel, development of medium- and large-scale plant solutions is progressing within the ENI group framework. These last activities are addressed to the utilisation of SCT-CPO for matching the variable Hydrogen demand in several contexts of oil refining operation. This paper will report on the current status of SCT-CPO with a focus on experimental results obtained, either at pilot- and bench- scale level. (orig.)

  5. Bench scale demonstration and conceptual engineering for DETOXSM catalyzed wet oxidation

    International Nuclear Information System (INIS)

    Moslander, J.; Bell, R.; Robertson, D.; Dhooge, P.; Goldblatt, S.

    1994-01-01

    Laboratory and bench scale studies of the DETOX SM catalyzed wet oxidation process have been performed with the object of developing the process for treatment of hazardous and mixed wastes. Reaction orders, apparent rates, and activation energies have been determined for a range of organic waste surrogates. Reaction intermediates and products have been analyzed. Metals' fates have been determined. Bench scale units have been designed, fabricated, and tested with solid and liquid organic waste surrogates. Results from the laboratory and bench scale studies have been used to develop conceptual designs for application of the process to hazardous and mixed wastes

  6. Generalized Test Plan for the Vitrification of Simulated High-Level -Waste Calcine in the Idaho National Laboratory‘s Bench -Scale Cold Crucible Induction Melter

    Energy Technology Data Exchange (ETDEWEB)

    Vince Maio

    2011-08-01

    This Preliminary Idaho National Laboratory (INL) Test Plan outlines the chronological steps required to initially evaluate the validity of vitrifying INL surrogate (cold) High-Level-Waste (HLW) solid particulate calcine in INL's Cold Crucible Induction Melter (CCIM). Its documentation and publication satisfies interim milestone WP-413-INL-01 of the DOE-EM (via the Office of River Protection) sponsored work package, WP 4.1.3, entitled 'Improved Vitrification' The primary goal of the proposed CCIM testing is to initiate efforts to identify an efficient and effective back-up and risk adverse technology for treating the actual HLW calcine stored at the INL. The calcine's treatment must be completed by 2035 as dictated by a State of Idaho Consent Order. A final report on this surrogate/calcine test in the CCIM will be issued in May 2012-pending next fiscal year funding In particular the plan provides; (1) distinct test objectives, (2) a description of the purpose and scope of planned university contracted pre-screening tests required to optimize the CCIM glass/surrogate calcine formulation, (3) a listing of necessary CCIM equipment modifications and corresponding work control document changes necessary to feed a solid particulate to the CCIM, (4) a description of the class of calcine that will be represented by the surrogate, and (5) a tentative tabulation of the anticipated CCIM testing conditions, testing parameters, sampling requirements and analytical tests. Key FY -11 milestones associated with this CCIM testing effort are also provided. The CCIM test run is scheduled to be conducted in February of 2012 and will involve testing with a surrogate HLW calcine representative of only 13% of the 4,000 m3 of 'hot' calcine residing in 6 INL Bin Sets. The remaining classes of calcine will have to be eventually tested in the CCIM if an operational scale CCIM is to be a feasible option for the actual INL HLW calcine. This remaining calcine

  7. Bench-scale treatability studies for simulated incinerator scrubber blowdown containing radioactive cesium and strontium

    International Nuclear Information System (INIS)

    Coroneos, A.C.; Taylor, P.A.; Arnold, W.D. Jr.; Bostick, D.A.; Perona, J.J.

    1994-12-01

    The purpose of this report is to document the results of bench-scale testing completed to remove 137 Cs and 90 Sr from the Oak Ridge K-25 Site Toxic Substances Control Act (TSCA) Incinerator blowdown at the K-25 Site Central Neutralization Facility, a wastewater treatment facility designed to remove heavy metals and uranium from various wastewaters. The report presents results of bench-scale testing using chabazite and clinoptilolite zeolites to remove cesium and strontium; using potassium cobalt ferrocyanide (KCCF) to remove cesium; and using strontium chloride coprecipitation, sodium phosphate coprecipitation, and calcium sulfate coprecipitation to remove strontium. Low-range, average-range, and high-range concentration blowdown surrogates were used to complete the bench-scale testing

  8. Bench-Scale Demonstration of Hot-Gas Desulfurization Technology

    International Nuclear Information System (INIS)

    Portzer, Jeffrey W.; Gangwal, Santosh K.

    1997-01-01

    Prior to the current project, development of the DSRP was done in a laboratory setting, using synthetic gas mixtures to simulate the regeneration off-gas and coal gas feeds. The objective of the current work is to further the development of zinc titanate fluidized-bed desulfurization (ZTFBD) and the DSRP for hot-gas cleanup by testing with actual coal gas. The objectives of this project are to: (1) Develop and test an integrated, skid-mounted, bench-scale ZTFBD/DSRP reactor system with a slipstream of actual coal gas; (2) Test the bench-scale DSRP over an extended period with a slipstream of actual coal gas to quantify the degradation in performance, if any, caused by the trace contaminants present in coal gas (including heavy metals, chlorides, fluorides, and ammonia); (3) Expose the DSRP catalyst to actual coal gas for extended periods and then test its activity in a laboratory reactor to quantify the degradation in performance, if any, caused by static exposure to the trace contaminants in coal gas; (4) Design and fabricate a six-fold larger-scale DSRP reactor system for future slipstream testing; (5) Further develop the fluidized-bed DSRP to handle high concentrations (up to 14 percent) of SO 2 that are likely to be encountered when pure air is used for regeneration of desulfurization sorbents; and (6) Conduct extended field testing of the 6X DSRP reactor with actual coal gas and high concentrations of SO 2 . The accomplishment of the first three objectives--testing the DSRP with actual coal gas, integration with hot-gas desulfurization, and catalyst exposure testing--was described previously (Portzer and Gangwal, 1994, 1995; Portzer et al., 1996). This paper summarizes the results of previous work and describes the current activities and plans to accomplish the remaining objectives

  9. Bench-scale Kinetics Study of Mercury Reactions in FGD Liquors

    Energy Technology Data Exchange (ETDEWEB)

    Gary Blythe; John Currie; David DeBerry

    2008-03-31

    This document is the final report for Cooperative Agreement DE-FC26-04NT42314, 'Kinetics Study of Mercury Reactions in FGD Liquors'. The project was co-funded by the U.S. DOE National Energy Technology Laboratory and EPRI. The objective of the project has been to determine the mechanisms and kinetics of the aqueous reactions of mercury absorbed by wet flue gas desulfurization (FGD) systems, and develop a kinetics model to predict mercury reactions in wet FGD systems. The model may be used to determine optimum wet FGD design and operating conditions to maximize mercury capture in wet FGD systems. Initially, a series of bench-top, liquid-phase reactor tests were conducted and mercury species concentrations were measured by UV/visible light spectroscopy to determine reactant and byproduct concentrations over time. Other measurement methods, such as atomic absorption, were used to measure concentrations of vapor-phase elemental mercury, that cannot be measured by UV/visible light spectroscopy. Next, a series of bench-scale wet FGD simulation tests were conducted. Because of the significant effects of sulfite concentration on mercury re-emission rates, new methods were developed for operating and controlling the bench-scale FGD experiments. Approximately 140 bench-scale wet FGD tests were conducted and several unusual and pertinent effects of process chemistry on mercury re-emissions were identified and characterized. These data have been used to develop an empirically adjusted, theoretically based kinetics model to predict mercury species reactions in wet FGD systems. The model has been verified in tests conducted with the bench-scale wet FGD system, where both gas-phase and liquid-phase mercury concentrations were measured to determine if the model accurately predicts the tendency for mercury re-emissions. This report presents and discusses results from the initial laboratory kinetics measurements, the bench-scale wet FGD tests, and the kinetics modeling

  10. Test procedures and instructions for Hanford complexant concentrate supernatant cesium removal using CST

    Energy Technology Data Exchange (ETDEWEB)

    Hendrickson, D.W.

    1997-01-08

    This document provides specific test procedures and instructions to implement the test plan for the preparation and conduct of a cesium removal test, using Hanford Complexant Concentrate supernatant liquor from tank 241-AN-107, in a bench-scale column. The cesium sorbent to be tested is crystalline silicotitanate. The test plan for which this provides instructions is WHC-SD-RE-TP-023, Hanford Complexant Concentrate Supernatant Cesium Removal Test Plan.

  11. Test procedures and instructions for Hanford tank waste supernatant cesium removal

    Energy Technology Data Exchange (ETDEWEB)

    Hendrickson, D.W., Westinghouse Hanford

    1996-05-31

    This document provides specific test procedures and instructions to implement the test plan for the preparation and conduct of a cesium removal test using Hanford Double-Shell Slurry Feed supernatant liquor from tank 251-AW-101 in a bench-scale column.Cesium sorbents to be tested include resorcinol-formaldehyde resin and crystalline silicotitanate. The test plan for which this provides instructions is WHC-SD-RE-TP-022, Hanford Tank Waste Supernatant Cesium Removal Test Plan.

  12. A bench-scale biotreatability methodology to evaluate field bioremediation

    International Nuclear Information System (INIS)

    Saberiyan, A.G.; MacPherson, J.R. Jr.; Moore, R.; Pruess, A.J.; Andrilenas, J.S.

    1995-01-01

    A bench-scale biotreatability methodology was designed to assess field bioremediation of petroleum contaminated soil samples. This methodology was performed successfully on soil samples from more than 40 sites. The methodology is composed of two phases, characterization and experimentation. The first phase is physical, chemical, and biological characterization of the contaminated soil sample. This phase determines soil parameters, contaminant type, presence of indigenous contaminant-degrading bacteria, and bacterial population size. The second phase, experimentation, consists of a respirometry test to measure the growth of microbes indirectly (via generation of CO 2 ) and the consumption of their food source directly (via contaminant loss). Based on a Monod kinetic analysis, the half-life of a contaminant can be calculated. Abiotic losses are accounted for based on a control test. The contaminant molecular structure is used to generate a stoichiometric equation. The stoichiometric equation yields a theoretical ratio for mg of contaminant degraded per mg of CO 2 produced. Data collected from the respirometry test are compared to theoretical values to evaluate bioremediation feasibility

  13. Lab and Bench-Scale Pelletization of Torrefied Wood Chips

    DEFF Research Database (Denmark)

    Shang, Lei; Nielsen, Niels Peter K.; Stelte, Wolfgang

    2013-01-01

    content, additive addition, and the degree of torrefaction on the pelletizing properties and pellet quality, i.e., density, static friction, and pellet strength. Results were compared with pellet production using a bench-scale pelletizer. The results indicate that friction is the key factor when scaling...... up from single-pellet press to bench-scale pelletizer. Tuning moisture content or increasing the die temperature did not ease the pellet production of torrefied wood chips significantly. The addition of rapeseed oil as a lubricant reduced the static friction by half and stabilized pellet production...

  14. Polymeric Traypack Integrity: Bench-Scale Unit

    National Research Council Canada - National Science Library

    Canavan, Jeffrey

    2002-01-01

    .... Additional experimentation was conducted to determine the applicability of the unit for non-destructive residual gas testing since current destructive tests represent a substantial continuing expense...

  15. Bench scale flotation of spodume/quartz and lepidolite/quartz synthetic mixtures

    International Nuclear Information System (INIS)

    Valadao, G.E.S.; Gontijo, C.F.; Peres, A.E.C.

    1985-01-01

    Based on results of zeta potential determinations and microflotation tests, bench scale flotation experiments were carried out using spodume/quartz and lepodolite/quartz synthetic mixtures. Pure natural samples, further purified in laboratory, and commercial reagents were employed. The minerals were characterized by X-ray diffraction technique. Selectivity between spodume and quartz was achieved through modification with corn starch and between lepidolite and quartz through pH control in the acidic range. (Author) [pt

  16. Embedded Sensors and Controls to Improve Component Performance and Reliability -- Bench-scale Testbed Design Report

    Energy Technology Data Exchange (ETDEWEB)

    Melin, Alexander M. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Kisner, Roger A. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Drira, Anis [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Reed, Frederick K. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

    2015-09-01

    Embedded instrumentation and control systems that can operate in extreme environments are challenging due to restrictions on sensors and materials. As a part of the Department of Energy's Nuclear Energy Enabling Technology cross-cutting technology development programs Advanced Sensors and Instrumentation topic, this report details the design of a bench-scale embedded instrumentation and control testbed. The design goal of the bench-scale testbed is to build a re-configurable system that can rapidly deploy and test advanced control algorithms in a hardware in the loop setup. The bench-scale testbed will be designed as a fluid pump analog that uses active magnetic bearings to support the shaft. The testbed represents an application that would improve the efficiency and performance of high temperature (700 C) pumps for liquid salt reactors that operate in an extreme environment and provide many engineering challenges that can be overcome with embedded instrumentation and control. This report will give details of the mechanical design, electromagnetic design, geometry optimization, power electronics design, and initial control system design.

  17. Flue gas conditioning for improved particle collection in electrostatic precipitators. Second topical report, Results of bench-scale screening of additives

    Energy Technology Data Exchange (ETDEWEB)

    Durham, M.D.

    1993-08-13

    ADA Technologies, Inc. (ADA) has completed the bench-scale testing phase of a program to evaluate additives that will improve the collection of fine particles in electrostatic precipitators (ESPs). A bench-scale ESP was installed at the Consolidation Coal Company (CONSOL) combustion research and development facility in Library, PA in order to conduct the evaluation. During a two-week test, four candidate additives were injected into the flue gas ahead of a 100 acfm ESP to determine the effect on fly ash collectability. Two additives were found to reduce the emissions from the ESP. Additives ``C`` and ``D`` performed better than initially anticipated -- reducing emissions initially by 17%. Emissions were reduced by 27% after the ESP was modified by the installation of baffles to minimize sneakage. In addition to the measured improvements in performance, no detrimental effects (i.e., electrode fouling) were observed in the operation of the ESP during the testing. The measures of success identified for the bench-scale phase of the program have been surpassed. Since the additives will affect only non-rapping reentrainment particle losses, it is expected that an even greater improvement in particle collection will be observed in larger-scale ESPs. Therefore, positive results are anticipated during the pilot-scale phase of the program and during a future full-scale demonstration test. A preliminary economic analysis was performed to evaluate the cost of the additive process and to compare its costs against alternative means for reducing emissions from ESPs. The results show that conditioning with additive C at a rate of 0.05% (wt. additive to wt. fly ash) is much less expensive than adding new ESP capacity, and more cost competitive than existing chemical conditioning processes. Preliminary chemical analysis of conditioned fly ash shows that it passes the Toxicity Characteristic Leaching Procedure criteria.

  18. Electrodialytic remediation of air pollution control residues in bench scale

    DEFF Research Database (Denmark)

    Jensen, Pernille Erland; Ferreira, Celia; Hansen, Henrik K.

    2008-01-01

    Air pollution control (APC) residue from municipal solid waste incineration (MSWI) is considered a hazardous waste due to its alkalinity and high content of salts and mobile heavy metals. Various solutions for the handling of APC-residue exist in different regions; however, most commercial...... solutions are concerned with deposition. A demand for more environmentally friendly alternatives exists. Electrodialysis could be such an alternative, and the potential is being explored. This work presents a bench scale study of the feasibility of treating APC-residue from a dry system by electrodialysis....... A system resembling conventional electrodialysis was designed and adjusted to fit the high solids content feed solution (10% APC residue, 90% water). Experiments were made in bench scale with raw residue (natural pH > 12), water pre-residue (natural pH > 12), acid pre-washed residue (pH 10), and acid...

  19. Bench-scale arc melter for R&D in thermal treatment of mixed wastes

    Energy Technology Data Exchange (ETDEWEB)

    Kong, P.C.; Grandy, J.D.; Watkins, A.D.; Eddy, T.L.; Anderson, G.L.

    1993-05-01

    A small dc arc melter was designed and constructed to run bench-scale investigations on various aspects of development for high-temperature (1,500-1,800{degrees}C) processing of simulated transuranic-contaminated waste and soil located at the Radioactive Waste Management Complex (RWMC). Several recent system design and treatment studies have shown that high-temperature melting is the preferred treatment. The small arc melter is needed to establish techniques and procedures (with surrogates) prior to using a similar melter with the transuranic-contaminated wastes in appropriate facilities at the site. This report documents the design and construction, starting and heating procedures, and tests evaluating the melter`s ability to process several waste types stored at the RWMC. It is found that a thin graphite strip provides reliable starting with initial high current capability for partially melting the soil/waste mixture. The heating procedure includes (1) the initial high current-low voltage mode, (2) a low current-high voltage mode that commences after some slag has formed and arcing dominates over the receding graphite conduction path, and (3) a predominantly Joule heating mode during which the current can be increased within the limits to maintain relatively quiescent operation. Several experiments involving the melting of simulated wastes are discussed. Energy balance, slag temperature, and electrode wear measurements are presented. Recommendations for further refinements to enhance its processing capabilities are identified. Future studies anticipated with the arc melter include waste form processing development; dissolution, retention, volatilization, and collection for transuranic and low-level radionuclides, as well as high vapor pressure metals; electrode material development to minimize corrosion and erosion; refractory corrosion and/or skull formation effects; crucible or melter geometry; metal oxidation; and melt reduction/oxidation (redox) conditions.

  20. Bench-scale arc melter for R ampersand D in thermal treatment of mixed wastes

    International Nuclear Information System (INIS)

    Kong, P.C.; Grandy, J.D.; Watkins, A.D.; Eddy, T.L.; Anderson, G.L.

    1993-05-01

    A small dc arc melter was designed and constructed to run bench-scale investigations on various aspects of development for high-temperature (1,500-1,800 degrees C) processing of simulated transuranic-contaminated waste and soil located at the Radioactive Waste Management Complex (RWMC). Several recent system design and treatment studies have shown that high-temperature melting is the preferred treatment. The small arc melter is needed to establish techniques and procedures (with surrogates) prior to using a similar melter with the transuranic-contaminated wastes in appropriate facilities at the site. This report documents the design and construction, starting and heating procedures, and tests evaluating the melter's ability to process several waste types stored at the RWMC. It is found that a thin graphite strip provides reliable starting with initial high current capability for partially melting the soil/waste mixture. The heating procedure includes (1) the initial high current-low voltage mode, (2) a low current-high voltage mode that commences after some slag has formed and arcing dominates over the receding graphite conduction path, and (3) a predominantly Joule heating mode during which the current can be increased within the limits to maintain relatively quiescent operation. Several experiments involving the melting of simulated wastes are discussed. Energy balance, slag temperature, and electrode wear measurements are presented. Recommendations for further refinements to enhance its processing capabilities are identified. Future studies anticipated with the arc melter include waste form processing development; dissolution, retention, volatilization, and collection for transuranic and low-level radionuclides, as well as high vapor pressure metals; electrode material development to minimize corrosion and erosion; refractory corrosion and/or skull formation effects; crucible or melter geometry; metal oxidation; and melt reduction/oxidation (redox) conditions

  1. Test procedures and instructions for single shell tank saltcake cesium removal with crystalline silicotitanate

    Energy Technology Data Exchange (ETDEWEB)

    Duncan, J.B.

    1997-01-07

    This document provides specific test procedures and instructions to implement the test plan for the preparation and conduct of a cesium removal test, using Hanford Single Shell Tank Saltcake from tanks 24 t -BY- I 10, 24 1 -U- 108, 24 1 -U- 109, 24 1 -A- I 0 1, and 24 t - S-102, in a bench-scale column. The cesium sorbent to be tested is crystalline siticotitanate. The test plan for which this provides instructions is WHC-SD-RE-TP-024, Hanford Single Shell Tank Saltcake Cesium Removal Test Plan.

  2. In situ remediation of hexavalent chromium with pyrite fines : bench scale demonstration

    International Nuclear Information System (INIS)

    Cathum, S.; Wong, W.P.; Brown, C.E.

    2002-01-01

    An in situ remediation technique for chromium contaminated soil with pyrite fines was presented. Past industrial activities and lack of disposal facilities have contributed to a serious problem dealing with chromium, which cannot be eliminated from the environment because it is an element. Both bench-scale and laboratory testing was conducted to confirm the efficiency of the proposed process which successfully converted Cr(VI) into Cr(III) in soil and water. Cr(III) is less toxic and immobile in the environment compared to Cr(VI) which moves freely in the soil matrix, posing a risk to the groundwater quality. pH in the range of 2.0 to 7.6 has no effect on the reactivity of pyrite towards Cr(VI). The optimization of the bench-scale treatment resulted in a large volume of chromium waste, mostly from the control experiments and column hydrology testing. These waste streams were treated according to municipal guidelines before disposal to the environment. Samples of chromium waste before and after treatment were analyzed. Cr (VI) was completely mineralized to below guideline levels. It was determined that several conditions, including contact time between pyrite and Cr(VI), are crucial for complete mineralization of Cr(VI). 13 refs., 8 tabs., 9 figs

  3. Bench-Scale Silicone Process for Low-Cost CO{sub 2} Capture

    Energy Technology Data Exchange (ETDEWEB)

    Wood, Benjamin; Genovese, Sarah; Perry, Robert; Spiry, Irina; Farnum, Rachael; Sing, Surinder; Wilson, Paul; Buckley, Paul; Acharya, Harish; Chen, Wei; McDermott, John; Vipperia, Ravikumar; Yee, Michael; Steele, Ray; Fresia, Megan; Vogt, Kirk

    2013-12-31

    A bench-scale system was designed and built to test an aminosilicone-based solvent. A model was built of the bench-scale system and this model was scaled up to model the performance of a carbon capture unit, using aminosilicones, for CO{sub 2} capture and sequestration (CCS) for a pulverized coal (PC) boiler at 550 MW. System and economic analysis for the carbon capture unit demonstrates that the aminosilicone solvent has significant advantages relative to a monoethanol amine (MEA)-based system. The CCS energy penalty for MEA is 35.9% and the energy penalty for aminosilicone solvent is 30.4% using a steam temperature of 395 °C (743 °F). If the steam temperature is lowered to 204 °C (400 °F), the energy penalty for the aminosilicone solvent is reduced to 29%. The increase in cost of electricity (COE) over the non-capture case for MEA is ~109% and increase in COE for aminosilicone solvent is ~98 to 103% depending on the solvent cost at a steam temperature of 395 °C (743 °F). If the steam temperature is lowered to 204 °C (400 °F), the increase in COE for the aminosilicone solvent is reduced to ~95-100%.

  4. Environmental data from laboratory- and bench-scale Pressurized Fluidized-Bed Hydroretorting of Eastern oil shale

    Energy Technology Data Exchange (ETDEWEB)

    Mensinger, M.C.; Rue, D.M.; Roberts, M.J.

    1991-01-01

    As part of a 3-year program to develop the Pressurized Fluidized-Bed Hydroretorting (PFH) Process for Eastern oil shales, IGT conducted tests in laboratory-scale batch and continuous units as well as a 45-kg/h bench-scale unit to generate a data base for 6 Eastern shales. Data were collected during PFH processing of raw Alabama and Indiana shales and a beneficiated Indiana shale for environmental mitigation analyses. The data generated include trace element analyses of the raw feeds and spent shales, product oils, and sour waters. The sulfur compounds present in the product gas and trace components in the sour water were also determined. In addition, the leaching characteristics of the feed and residue solids were determined. The data obtained were used to evaluate the environmental impact of a shale processing plant based on the PFH process. This paper presents the environmental data obtained from bench-scale tests conducted during the program.

  5. Environmental data from laboratory- and bench-scale Pressurized Fluidized-Bed Hydroretorting of Eastern oil shale

    Energy Technology Data Exchange (ETDEWEB)

    Mensinger, M.C.; Rue, D.M.; Roberts, M.J.

    1991-12-31

    As part of a 3-year program to develop the Pressurized Fluidized-Bed Hydroretorting (PFH) Process for Eastern oil shales, IGT conducted tests in laboratory-scale batch and continuous units as well as a 45-kg/h bench-scale unit to generate a data base for 6 Eastern shales. Data were collected during PFH processing of raw Alabama and Indiana shales and a beneficiated Indiana shale for environmental mitigation analyses. The data generated include trace element analyses of the raw feeds and spent shales, product oils, and sour waters. The sulfur compounds present in the product gas and trace components in the sour water were also determined. In addition, the leaching characteristics of the feed and residue solids were determined. The data obtained were used to evaluate the environmental impact of a shale processing plant based on the PFH process. This paper presents the environmental data obtained from bench-scale tests conducted during the program.

  6. Bench-Scale Development of a Non-Aqueous Solvent (NAS) CO2 Capture Process for Coal-Fired Power Plants

    Energy Technology Data Exchange (ETDEWEB)

    Lail, Marty

    2017-09-12

    The project aimed to advance RTI’s non-aqueous amine solvent technology by improving the solvent to reduce volatility, demonstrating long-term continuous operation at lab- (0.5 liters solvent) and bench-scale (~120 liters solvent), showing low reboiler heat duty measured during bench-scale testing, evaluating degradation products, building a rate-based process model, and evaluating the techno-economic performance of the process. The project team (RTI, SINTEF, Linde Engineering) and the technology performed well in each area of advancement. The modifications incorporated throughout the project enabled the attainment of target absorber and regenerator conditions for the process. Reboiler duties below 2,000 kJt/kg CO2 were observed in a bench-scale test unit operated at RTI.

  7. An integrated testing facility for bench scale catalyst research

    Energy Technology Data Exchange (ETDEWEB)

    Johnston, H.D.; Hogan, R.J.; McMurtrie, D.E.

    1983-08-01

    Discovering new catalysts and designing new catalytic processes has long been hindered by equipment that is either designed for hand operation with the data acquisition functions in some stage of automation or is patterned after refinery installations to smaller, pilot plant like facilities. The latter approach has required large vessels (and hence large amounts of experimental catalyst and feedstocks) to be used or the use of improperly fitted control equipment with constant attention to the operation of a small reactor system. Constant attention partially negates the intent of the automation effort. Results from some of these systems are often unsatisfactory because of poor material balances and control. The data from some schemes must then be manually transferred into other databases for use in reports, correlations, etc. An earlier paper from this laboratory (1) described an initial attempt to provide a reliable, reproducible method for more productive catalyst screening, but that system still lacked an automatic data management system and was not flexible with regards to wide range changes of pressure and flow. Also, several different types of experiments could not be run concurrently. Recently, several schemes have appeared (2-6) which deal with distributed systems as they apply to various laboratory and pilot plant operations. This paper describes an automated system that allows for up to 21 reactors to be in operation concurrently with a staff of five people. All units are independently run without normal operator intervention and the system is designed fail safe for unattended operation. It has been used extensively for screening exploratory catalysts, catalytic process optimization, kinetic modeling and increasingly in refinery process optimization.

  8. BENCH-SCALE STEAM REFORMING OF ACTUAL TANK 48H WASTE

    Energy Technology Data Exchange (ETDEWEB)

    Burket, P; Gene Daniel, G; Charles Nash, C; Carol Jantzen, C; Michael Williams, M

    2008-09-25

    Fluidized Bed Steam Reforming (FBSR) has been demonstrated to be a viable technology to remove >99% of the organics from Tank 48H simulant, to remove >99% of the nitrate/nitrite from Tank 48H simulant, and to form a solid product that is primarily carbonate based. The technology was demonstrated in October of 2006 in the Engineering Scale Test Demonstration Fluidized Bed Steam Reformer1 (ESTD FBSR) at the Hazen Research Inc. (HRI) facility in Golden, CO. The purpose of the Bench-scale Steam Reformer (BSR) testing was to demonstrate that the same reactions occur and the same product is formed when steam reforming actual radioactive Tank 48H waste. The approach used in the current study was to test the BSR with the same Tank 48H simulant and same Erwin coal as was used at the ESTD FBSR under the same operating conditions. This comparison would allow verification that the same chemical reactions occur in both the BSR and ESTD FBSR. Then, actual radioactive Tank 48H material would be steam reformed in the BSR to verify that the actual tank 48H sample reacts the same way chemically as the simulant Tank 48H material. The conclusions from the BSR study and comparison to the ESTD FBSR are the following: (1) A Bench-scale Steam Reforming (BSR) unit was successfully designed and built that: (a) Emulated the chemistry of the ESTD FBSR Denitration Mineralization Reformer (DMR) and Carbon Reduction Reformer (CRR) known collectively as the dual reformer flowsheet. (b) Measured and controlled the off-gas stream. (c) Processed real (radioactive) Tank 48H waste. (d) Met the standards and specifications for radiological testing in the Savannah River National Laboratory (SRNL) Shielded Cells Facility (SCF). (2) Three runs with radioactive Tank 48H material were performed. (3) The Tetraphenylborate (TPB) was destroyed to > 99% for all radioactive Bench-scale tests. (4) The feed nitrate/nitrite was destroyed to >99% for all radioactive BSR tests the same as the ESTD FBSR. (5) The

  9. Oxygen-controlled Biosurfactant Production in a Bench Scale Bioreactor

    Science.gov (United States)

    de Kronemberger, Frederico Araujo; Anna, Lidia Maria Melo Santa; Fernandes, Ana Carolina Loureiro Brito; de Menezes, Reginaldo Ramos; Borges, Cristiano Piacsek; Freire, Denise Maria Guimarães

    Rhamnolipids have been pointed out as promising biosurfactants. The most studied microorganisms for the aerobic production of these molecules are the bacteria of the genus Pseudomonas. The aim of this work was to produce a rhamnolipid-type biosurfactant in a bench-scale bioreactor by one strain of Pseudomonas aeruginosa isolated from oil environments. To study the microorganism growth and production dependency on oxygen, a nondispersive oxygenation device was developed, and a programmable logic controller (PLC) was used to set the dissolved oxygen (DO) concentration. Using the data stored in a computer and the predetermined characteristics of the oxygenation device, it was possible to evaluate the oxygen uptake rate (OUR) and the specific OUR (SOUR) of this microorganism. These rates, obtained for some different DO concentrations, were then compared to the bacterial growth, to the carbon source consumption, and to the rhamnolipid and other virulence factors production. The SOUR presented an initial value of about 60.0 mg02/gdw h. Then, when the exponential growth phase begins, there is a rise in this rate. After that, the SOUR reduces to about 20.0 mg02/gdw h. The carbon source consumption is linear during the whole process.

  10. Final PHP bench-scale report for the DOE-ID/SAIC sole source contract

    International Nuclear Information System (INIS)

    1997-04-01

    The Plasma Hearth Process (PHP) Technology Development Project was established to develop, test, and evaluate a new concept for treating mixed waste. The new concept uses direct current (dc) transferred-arc plasma torch technology to process mixed waste into a glass-like end-product. Under the cognizance of the US Department of Energy (DOE) Office of Technology Development (OTD) Mixed Waste Focus Area (MWFA), the technology is being explored for its potential to treat mixed waste. Because it is a mature technology, well-understood and commercially available, it is expected to develop rapidly in this new application. This report summarizes the radioactive bench-scale system activities funded under PHP Sole Source Contract DE-AC07-94ID13266 through the end of the contract

  11. Performance evaluation of the DCMD desalination process under bench scale and large scale module operating conditions

    KAUST Repository

    Francis, Lijo

    2014-04-01

    The flux performance of different hydrophobic microporous flat sheet commercial membranes made of poly tetrafluoroethylene (PTFE) and poly propylene (PP) was tested for Red Sea water desalination using the direct contact membrane distillation (DCMD) process, under bench scale (high δT) and large scale module (low δT) operating conditions. Membranes were characterized for their surface morphology, water contact angle, thickness, porosity, pore size and pore size distribution. The DCMD process performance was optimized using a locally designed and fabricated module aiming to maximize the flux at different levels of operating parameters, mainly feed water and coolant inlet temperatures at different temperature differences across the membrane (δT). Water vapor flux of 88.8kg/m2h was obtained using a PTFE membrane at high δT (60°C). In addition, the flux performance was compared to the first generation of a new locally synthesized and fabricated membrane made of a different class of polymer under the same conditions. A total salt rejection of 99.99% and boron rejection of 99.41% were achieved under extreme operating conditions. On the other hand, a detailed water characterization revealed that low molecular weight non-ionic molecules (ppb level) were transported with the water vapor molecules through the membrane structure. The membrane which provided the highest flux was then tested under large scale module operating conditions. The average flux of the latter study (low δT) was found to be eight times lower than that of the bench scale (high δT) operating conditions.

  12. Design of a Compact and Versatile Bench Scale Tubular Reactor

    Directory of Open Access Journals (Sweden)

    R. Prasad

    2009-06-01

    Full Text Available A compact and versatile laboratory tubular reactor has been designed and fabricated keeping in view of reducing capital cost and minimising energy consumption for gas/vapor-phase heterogeneous catalytic reactions. The reactor is consisted of two coaxial corning glass tubes with a helical coil of glass tube in between the coaxial tubes serving as vaporiser and pre-heater, the catalyst bed is in the inner tube. A schematic diagram of the reactor with detailed dimensions and working principles are described. The attractive feature of the reactor is that the vaporiser, pre-heater and fixed bed reactor are merged in a single compact unit. Thus, the unit minimises separate vaporiser and pre-heater, also avoids separate furnaces used for them and eliminate auxiliary instrumentation such as temperature controller etc. To demonstrate the system operation and illustrate the key features, catalyst screening data and the efficient collection of complete, and accurate intrinsic kinetic data are provided for oxidation of CO over copper chromite catalyst. CO oxidation is an important reaction for auto-exhaust pollution control. The suitability of the versatile nature of the reactor has been ascertained for catalytic reactions where either volatile or vaporizable feeds can be introduced to the reaction zone, e.g. oxidation of iso-octane, reduction of nitric oxide, dehydrogenation of methanol, ethanol and iso-propanol, hydrogenation of nitrobenzene to aniline, etc. Copyright (c 2009 by BCREC. All Rights reserved.[Received: 10 February 2009, Accepted: 9 May 2009][How to Cite: R. Prasad, G. Rattan. (2009. Design of a Compact and Versatile Bench Scale Tubular Reactor. Bulletin of Chemical Reaction Engineering and Catalysis, 4(1: 5-9.  doi:10.9767/bcrec.4.1.1250.5-9][How to Link/ DOI: http://dx.doi.org/10.9767/bcrec.4.1.1250.5-9

  13. Safety analysis of the CSTR-1 bench-scale coal liquefaction unit

    Energy Technology Data Exchange (ETDEWEB)

    Hulburt, D.A.

    1981-05-01

    The objective of the program reported herein was to provide a Safety Analysis of the CSTR-1 bench scale unit located in Building 167 at the Pittsburgh Energy Technology Center. It was apparent that considerable effort was expended in the design and construction of the unit, and in the development of operating procedures, with regard to safety. Exhaust ventilation, H/sub 2/ and H/sub 2/S monitoring, overpressure protection, overtemperature protection, and interlock systems have been provided. Present settings on the pressure and temperature safety systems are too high, however, to insure prevention of vessel deformation or damage in all cases. While the occurrence of catastrophic rupture of a system pressure vessel (e.g., reactor, high pressure separators) is unlikely, the potential consequences to personnel are severe. Feasibility of providing shielding for these components should be considered. A more probable mode of vessel failure in the event of overpressure or overtemperature and failure of the safety system is yielding of the closure bolts followed by high pressure flow across the mating surfaces. As a minimum, shielding should be designed to restrict travel of resultant spray. The requirements for personal protective equipment are presently stated in rather broad and general terms in the operating procedures. Safe practices and procedures would be more assured if specific requirements were stated and included for each operational step. Recommendations were developed for all hazards triggered by the guidelines.

  14. Treatment studies of plutonium-bearing INEEL waste surrogates in a bench-scale arc furnace

    International Nuclear Information System (INIS)

    Freeman, C.J.

    1997-05-01

    Since 1989, the Subsurface Disposal Area (SDA) at the Idaho National Environmental and Engineering Laboratory (INEEL) has been included on the National Priority List for remediation. Arc- and plasma-heated furnaces are being considered for converting the radioactive mixed waste buried in the SDA to a stabilized-vitreous form. Nonradioactive, surrogate SDA wastes have been melted during tests in these types of furnaces, but data are needed on the behavior of transuranic (TRU) constituents, primarily plutonium, during thermal treatment. To begin collecting this data, plutonium-spiked SDA surrogates were processed in a bench-scale arc furnace to quantify the fate of the plutonium and other hazardous and nonhazardous metals. Test conditions included elevating the organic, lead, chloride, and sodium contents of the surrogates. Blends having higher organic contents caused furnace power levels to fluctuate. An organic content corresponding to 50% INEEL soil in a soil-waste blend was the highest achievable before power fluctuations made operating conditions unacceptable. The glass, metal, and off-gas solids produced from each surrogate blend tested were analyzed for elemental (including plutonium) content and the partitioning of each element to the corresponding phase was calculated

  15. Bench-Scale Evaluation of Hydrothermal Processing Technology for Conversion of Wastewater Solids to Fuels

    Energy Technology Data Exchange (ETDEWEB)

    Marrone, Philip A.; Elliott, Douglas C.; Billing, Justin M.; Hallen, Richard T.; Hart, Todd R.; Kadota, Paul; Moeller, Jeff C.; Randel, Margaaret A.; Schmidt, Andrew J.

    2018-04-01

    Hydrothermal Liquefaction (HTL) and Catalytic Hydrothermal Gasification (CHG) proof-of-concept bench-scale tests were performed to assess the potential of hydrothermal treatment for handling municipal wastewater sludge. HTL tests were conducted at 300-350°C and 20 MPa on three different feeds: primary sludge, secondary sludge, and digested solids. Corresponding CHG tests were conducted at 350°C and 20 MPa on the HTL aqueous phase output using a ruthenium based catalyst. Biocrude yields ranged from 25-37%. Biocrude composition and quality were comparable to biocrudes generated from algae feeds. Subsequent hydrotreating of biocrude resulted in a product with comparable physical and chemical properties to crude oil. CHG product gas methane yields on a carbon basis ranged from 47-64%. Siloxane concentrations in the CHG product gas were below engine limits. The HTL-CHG process resulted in a chemical oxygen demand (COD) reduction of > 99.9% and a reduction in residual solids for disposal of 94-99%.

  16. Pyrolysis of automotive shredder residue in a bench scale rotary kiln.

    Science.gov (United States)

    Notarnicola, Michele; Cornacchia, Giacinto; De Gisi, Sabino; Di Canio, Francesco; Freda, Cesare; Garzone, Pietro; Martino, Maria; Valerio, Vito; Villone, Antonio

    2017-07-01

    Automotive shredder residue (ASR) can create difficulties when managing, with its production increasing. It is made of different type of plastics, foams, elastomers, wood, glasses and textiles. For this reason, it is complicated to dispose of in a cost effective way, while also respecting the stringent environmental restrictions. Among thermal treatments, pyrolysis seems to offer an environmentally attractive method for the treatment of ASR; it also allows for the recovery of valuable secondary materials/fuels such as pyrolysis oils, chars, and gas. While, there is a great deal of significant research on ASR pyrolysis, the literature on higher scale pyrolysis experiments is limited. To improve current literature, the aim of the study was to investigate the pyrolysis of ASR in a bench scale rotary kiln. The Italian ASR was separated by dry-sieving into two particle size fractions: d30mm. Both the streams were grounded, pelletized and then pyrolyzed in a continuous bench scale rotary kiln at 450, 550 and 650°C. The mass flow rate of the ASR pellets was 200-350g/h and each test ran for about 4-5h. The produced char, pyrolysis oil and syngas were quantified to determine product distribution. They were thoroughly analyzed with regard to their chemical and physical properties. The results show how higher temperatures increase the pyrolysis gas yield (44wt% at 650°C) as well as its heating value. The low heating value (LHV) of syngas ranges between 18 and 26MJ/Nm 3 dry. The highest pyrolysis oil yield (33wt.%) was observed at 550°C and its LHV ranges between 12.5 and 14.5MJ/kg. Furthermore, only two out of the six produced chars respect the LHV limit set by the Italian environmental regulations for landfilling. The obtained results in terms of product distribution and their chemical-physical analyses provide useful information for plant scale-up. Copyright © 2017 Elsevier Ltd. All rights reserved.

  17. Bench-scale demonstration of treatment technologies for contaminated sediments in Sydney Tar Ponds

    International Nuclear Information System (INIS)

    Volchek, K.; Velicogna, D.; Punt, M.; Wong, B.; Weimer, L.; Tsangaris, A.; Brown, C.E.

    2003-01-01

    A series of bench-scale tests were conducted to determine the capabilities of selected commercially available technologies for treating contaminated sediments from the South Pond of Sydney Tar Ponds. This study was conducted under the umbrella of a technology demonstration program aimed at evaluating technologies to be used in the remediation of such sediments. The following approach was proposed by SAIC Canada for the treatment of the sediments: (1) solvent extraction for the removal of organic contaminants, (2) acid/chelant leaching for the removal of inorganic contaminants such as heavy metals, and (3) plasma hearth process for the destruction of toxic streams resulting from the first two processes. Solvent extraction followed by plasma treatment proved effective for removing and destroying organic contaminants. The removal of metals did not achieve the expected results through leaching. An approach was proposed for treating those sediments based on the results of the study. The approach differed depending on the level of organic content. An assessment of associated process costs for both a pilot-scale field demonstration and a full-scale treatment was provided. 11 tabs., 4 figs

  18. Cometabolic biotreatment of TCE-contaminated groundwater: Laboratory and bench-scale development studies

    International Nuclear Information System (INIS)

    Donaldson, T.L.; Jennings, H.L.; Lucero, A.J.; Strandberg, G.W.; Morris, M.I.; Palumbo, A.V.; Boerman, P.A.; Tyndall, R.L.

    1992-01-01

    The Oak Ridge National Laboratory is conducting a demonstration of two cometabolic technologies for biotreatment of groundwater contaminated with trichloroethylene (TCE) and other organics. Technologies based on methanotrophic (methane-utilizing) and toluene-degrading microorganisms will be compared side-by-side on the same groundwater stream. Laboratory and bench-scale bioreactor studies have been conducted to guide selection of microbial cultures and operating conditions for the field demonstration. This report presents the results of the laboratory and bench-scale studies for the methanotrophic system

  19. Bench scale demonstration of the Supermethanol concept : The synthesis of methanol from glycerol derived syngas

    NARCIS (Netherlands)

    van Bennekom, J. G.; Venderbosch, R. H.; Assink, D.; Lemmens, K. P. J.; Heeres, H. J.

    2012-01-01

    An integrated process for the synthesis of methanol from aqueous glycerol involving reforming of the feed to syngas followed by methanol synthesis is successfully demonstrated in a continuous bench scale unit. Glycerol reforming was carried out at pressures of 24-27 MPa and temperatures of 948-998 K

  20. DEGRADATION OF POLYNUCLEAR AROMATIC HYDROCARBONS UNDER BENCH-SCALE COMPOST CONDITIONS

    Science.gov (United States)

    The relationship between biomass growth and degradation of polynuclear aromatic hydrocarbons (PAHs) in soil, and subsequent toxicity reduction, was evaluated in 10 in-vessel, bench-scale compost units. Field soil was aquired from the Reilly Tar and Chemical Company Superfund site...

  1. Bench-scale and full-scale studies of nitric oxides reduction by gaseous fuel reburning

    International Nuclear Information System (INIS)

    Su, S.; Xiang, J.; Sun, L.S.; Hu, S.; Zhu, J.M.

    2008-01-01

    Nitrogen oxides (NOx) emissions from coal-fired boilers are significant contributors to atmospheric pollution. China has specified more rigorous legal limits for NOx emissions from power plants. As a result of the need to reduce NOx emissions, cost-effective NOx reduction strategies must be explored. This paper presented detailed experimental studies on a gaseous fuel reburning process that was performed in a 36 kilowatt bench-scale down-fired furnace to define the optimal reburning operating conditions when different Chinese coals were fired in the furnace. In addition, the combustion system of a 350 megawatt full-scale boiler was retrofitted according to the experimental results. Finally, the gaseous fuel reburning was applied to the retrofitted full-scale boiler. The purpose of the study was to obtain a better understanding of the influence of the key parameters on nitric oxide (NO) reduction efficiency of the reburning process and demonstrate the gaseous fuel reburning on a 350 MWe coal-fired boiler in China. The paper described the experimental procedure with particular reference to the experimental facility and measurement; a schematic diagram of the experimental system; experimental fuels; and characteristics of coals for the reburning experiments. Results that were presented included influence of reburn zone residence time; influence of gaseous reburn fuel per cent; influence of excess air coefficient; and unburned carbon in fly ash. It was concluded that both an above 50 per cent NO reduction efficiency and low carbon loss can be obtained by the gaseous fuel reburning process under the optimal operating conditions. 20 refs., 5 tabs., 10 figs

  2. Extended Dry Storage Signature Bench Scale Detector Conceptual Design

    Energy Technology Data Exchange (ETDEWEB)

    Rauch, Eric Benton [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2016-09-02

    This report is the conceptual design of a detector based on research within the Extended Dry Storage Signature Development project under the DOE-­NE MPACT campaign. This is the second year of the project; from this year’s positive results, the next step is building a prototype and testing with real materials .

  3. Development of continuous bench scale unit for direct liquefaction

    Energy Technology Data Exchange (ETDEWEB)

    Yoon, Wang Lai [Korea Inst. of Energy and Resources, Daeduk (Korea, Republic of)

    1995-12-31

    Batch coal liquefaction experiments using tubing bombs and continuous experiments by cell liquefaction test facility were carried out. The main purpose was to maximize the coal liquefaction yields by improving the activity of coal dissolution catalysts which are oil soluble transition metal naphthenate and to supplement the incomplete research results. In the meantime, the study on the reaction characteristics of coal liquefaction and coal liquid upgrading catalyst upon sulfiding conditions and phosphorous addition have been conducted (author). 102 refs., 35 figs.

  4. Bench-Scale Silicone Process for Low-Cost CO{sub 2} Capture

    Energy Technology Data Exchange (ETDEWEB)

    Fresia, Megan; Vogt, Kirk

    2013-12-31

    GE Global Research is developing technology to remove carbon dioxide (CO{sub 2}) from the flue gas of coal-fired power plants. A mixture of 3-aminopropyl end-capped polydimethylsiloxane (GAP-1m) and triethylene glycol (TEG) is the preferred CO{sub 2} capture solvent. GE Global Research was contracted by the Department of Energy to test a bench-scale continuous CO{sub 2} absorption/desorption system using a GAP-1m/TEG mixture as the solvent. SiVance LLC was sub-contracted to provide the GAP-1m material and conduct an Environmental, Health, and Safety (EH&S) assessment for a 550 MW coal-fired power plant. Five components of the solvent, CAS#2469-55-8 (GAP-0), CAS#106214-84-0 (GAP-1-4), TEG, and methanol and xylene (minor contaminants from the aminosilicone) are included in this assessment. One by-product, GAP-1m/SOX salt, and dodecylbenzenesulfonic acid (DDBSA) were also identified for analysis. All of the solvent components and DDBSA are listed on the EPA’s TSCA Inventory allowing companies to manufacture and use the chemicals commercially. The toxicological effects of each component were defined, and control mechanisms necessary to comply with U.S. EH&S regulations are summarized. An engineering and control system, including environmental abatement, was described for minimizing exposure and release of the chemical components. Proper handling and storage recommendations are made for each chemical to minimize risk to workers and the surrounding community.

  5. Bench-Scale Evaluation of the Genifuel Hydrothermal Processing Technology for Wastewater Solids

    Energy Technology Data Exchange (ETDEWEB)

    Marrone, Philip A.; Elliott, Douglas C.; Billing, Justin M.; Hallen, Richard T.; Hart, Todd R.; Kadota, Paul; Moeller, Jeff C.; Randel, Margaaret A.; Schmidt, Andrew J.

    2017-10-03

    Hydrothermal Liquefaction (HTL) and Catalytic Hydrothermal Gasification (CHG) proof-of-concept bench-scale tests were performed to assess the potential of the Genifuel hydrothermal process technology for handling municipal wastewater sludge. HTL tests were conducted at 300-350°C and 20 MPa on three different feeds: primary sludge (11.9 wt% solids), secondary sludge (9.7 wt% solids), and post-digester sludge (also referred to as digested solids) (16.0 wt% solids). Corresponding CHG tests were conducted at 350°C and 20 MPa on the HTL aqueous phase output using a ruthenium based catalyst. A comprehensive analysis of all feed and effluent phases was also performed. Total mass and carbon balances closed to within ± 15% in all but one case. Biocrude yields from HTL tests were 37%, 25%, and 34% for primary sludge, secondary sludge, and digested solids feeds, respectively. The biocrude yields accounted for 59%, 39%, and 49% of the carbon in the feed for primary sludge, secondary sludge, and digested solids feeds, respectively. Biocrude composition and quality were comparable to that seen with biocrudes generated from algae feeds. Subsequent hydrotreating (i.e., upgrading) of the biocrude produced from primary sludge and digested solids resulted in a product with comparable physical and chemical properties to petroleum crude oil. CHG product gas consisted primarily of methane, with methane yields (relative to CHG input) on a carbon basis of 47%, 61%, and 64% for aqueous feeds that were the output of HTL tests with primary sludge, secondary sludge, and digested solids, respectively. Siloxane concentrations in the CHG product gas were below the detection limit and well below fuel input composition limits set by several engine manufacturers. Relative to that of the sludge feeds, the HTL-CHG process resulted in a reduction in chemical oxygen demand (COD) of greater than 99.9% and a reduction in residual solids for disposal of 94-99%. The test results, as a whole, support

  6. Bench Scale Process for Low Cost CO2 Capture Using a Phase-Changing Absorbent: Final Scientific/Technical Report

    Energy Technology Data Exchange (ETDEWEB)

    Westendorf, Tiffany [GE Global Research, Niskayuna, New York (United States); Buddle, Stanlee [GE Global Research, Niskayuna, New York (United States); Caraher, Joel [GE Global Research, Niskayuna, New York (United States); Chen, Wei [GE Global Research, Niskayuna, New York (United States); Doherty, Mark [GE Global Research, Niskayuna, New York (United States); Farnum, Rachel [GE Global Research, Niskayuna, New York (United States); Giammattei, Mark [GE Global Research, Niskayuna, New York (United States); Hancu, Dan [GE Global Research, Niskayuna, New York (United States); Miebach, Barbara [GE Global Research, Niskayuna, New York (United States); Perry, Robert [GE Global Research, Niskayuna, New York (United States); Rubinsztajn, Gosia; Spiry, Irina; Wilson, Paul; Wood, Benjamin

    2017-05-31

    The objective of this project is to design and build a bench-scale process for a novel phase-changing aminosilicone-based CO2-capture solvent. The project will establish scalability and technical and economic feasibility of using a phase-changing CO2-capture absorbent for post-combustion capture of CO2 from coal-fired power plants. The U.S. Department of Energy’s goal for Transformational Carbon Capture Technologies is the development of technologies available for demonstration by 2025 that can capture 90% of emitted CO2 with at least 95% CO2 purity for less than $40/tonne of CO2 captured. In the first budget period of the project, the bench-scale phase-changing CO2 capture process was designed using data and operating experience generated under a previous project (ARPA-e project DE-AR0000084). Sizing and specification of all major unit operations was completed, including detailed process and instrumentation diagrams. The system was designed to operate over a wide range of operating conditions to allow for exploration of the effect of process variables on CO2 capture performance. In the second budget period of the project, individual bench-scale unit operations were tested to determine the performance of each of each unit. Solids production was demonstrated in dry simulated flue gas across a wide range of absorber operating conditions, with single stage CO2 conversion rates up to 75mol%. Desorber operation was demonstrated in batch mode, resulting in desorption performance consistent with the equilibrium isotherms for GAP-0/CO2 reaction. Important risks associated with gas humidity impact on solids consistency and desorber temperature impact on thermal degradation were explored, and adjustments to the bench-scale process were made to address those effects. Corrosion experiments were conducted to support selection of suitable materials of construction for the major

  7. Design and fabrication of a glovebox for the Plasma Hearth Process radioactive bench-scale system

    International Nuclear Information System (INIS)

    Wahlquist, D.R.

    1996-01-01

    This paper presents some of the design considerations and fabrication techniques for building a glovebox for the Plasma Hearth Process (PHP) radioactive bench-scale system. The PHP radioactive bench-scale system uses a plasma torch to process a variety of radioactive materials into a final vitrified waste form. The processed waste will contain plutonium and trace amounts of other radioactive materials. The glovebox used in this system is located directly below the plasma chamber and is called the Hearth Handling Enclosure (HHE). The HHE is designed to maintain a confinement boundary between the processed waste and the operator. Operations that take place inside the HHE include raising and lowering the hearth using a hydraulic lift table, transporting the hearth within the HHE using an overhead monorail and hoist system, sampling and disassembly of the processed waste and hearth, weighing the hearth, rebuilding a hearth, and sampling HEPA filters. The PHP radioactive bench-scale system is located at the TREAT facility at Argonne National Laboratory-West in Idaho Falls, Idaho

  8. Bench-Scale Experiments to Evaluate ERT as a Monitoring Tool for Geologic CO2 Sequestration

    Science.gov (United States)

    Breen, S. J.; Detwiler, R. L.; Carrigan, C. R.

    2010-12-01

    Field-scale studies have shown Electrical Resistivity Tomography (ERT) to be an effective tool for imaging resistivity anomalies and monitoring changing saturations in the near subsurface. Despite the challenges of implementing ERT in the deep subsurface, it has potential as a surveying technology for visualizing sequestered CO2, in part because it can be localized within the target reservoir. Currently, the technology is being evaluated as part of a geologic sequestration project in Cranfield, MS, where supercritical CO2 is injected to ten thousand feet below the surface. In support of this field-scale activity, we have designed an analog bench-scale experimental system to further evaluate the ability of ERT to quantify both the volume and spatial distribution of gas injected into a saline aquifer. Our translucent sand chambers measure 58cm x 30cm x 1cm and are lined with twenty-one stainless steel electrodes on each long side, inserted into a nonconductive plastic gasket. We fill the chamber with quartz sand with different grain sizes with a filling procedure that generates small-scale layering within the injection zone, which is overlain by a fine-grained layer that serves as a capillary barrier. Prior to gas injection, the porous medium is saturated with a low resistivity salt solution. We then inject gas into the bottom of the injection zone. Buoyant forces drive gas migration into the chamber, resulting in a combination of small-scale trapping in horizontal layers, fingering between the horizontal layers, and large-scale trapping of the gas plume along the upper capillary barrier. During pauses in gas injection, a CCD camera captures high-resolution images, and an ERT data acquisition system scans the chamber. Quantitative visualization techniques are used to process the CCD images resulting in high-resolution measurements of the spatial distribution of the injected gas. These results are directly compared to resistivity fields that result from the inversion

  9. Bench-Scale Synthetic Optimization of 1,2-bis(2-aminophenylthio)ethane (APO-Link) Used in the Production of APO-BMI Resin

    Energy Technology Data Exchange (ETDEWEB)

    Hilary Wheeler; Crystal Densmore

    2007-07-31

    The diamine reagent 1,2-bis(2-aminophenylthio)ethane is no longer commercially available but still required for the synthesis of the bismaleimide resin, APO-BMI, used in syntactic foams. In this work, we examined the hydrolysis of benzothiazole followed the by reaction with dichloroethane or dibromoethane. We also studied the deprotonation of 2-aminothiophenol followed by the reaction with dibromoethane. We optimized the latter for scale-up by scrutinizing all aspects of the reaction conditions, work-up and recrystallization. On bench-scale, our optimized procedure consistently produced a 75-80% overall yield of finely divided, high purity product (>95%).

  10. Bench Scale Thin Film Composite Hollow Fiber Membranes for Post-Combustion Carbon Dioxide Capture

    Energy Technology Data Exchange (ETDEWEB)

    Glaser, Paul [General Electric Global Research, Niskayuna, NY (United States); Bhandari, Dhaval [General Electric Global Research, Niskayuna, NY (United States); Narang, Kristi [General Electric Global Research, Niskayuna, NY (United States); McCloskey, Pat [General Electric Global Research, Niskayuna, NY (United States); Singh, Surinder [General Electric Global Research, Niskayuna, NY (United States); Ananthasayanam, Balajee [General Electric Global Research, Niskayuna, NY (United States); Howson, Paul [General Electric Global Research, Niskayuna, NY (United States); Lee, Julia [General Electric Global Research, Niskayuna, NY (United States); Wroczynski, Ron [General Electric Global Research, Niskayuna, NY (United States); Stewart, Frederick [Idaho National Lab. (INL), Idaho Falls, ID (United States); Orme, Christopher [Idaho National Lab. (INL), Idaho Falls, ID (United States); Klaehn, John [Idaho National Lab. (INL), Idaho Falls, ID (United States); McNally, Joshua [Idaho National Lab. (INL), Idaho Falls, ID (United States); Rownaghi, Ali [Georgia Inst. of Technology, Atlanta, GA (United States); Lu, Liu [Georgia Inst. of Technology, Atlanta, GA (United States); Koros, William [Georgia Inst. of Technology, Atlanta, GA (United States); Goizueta, Roberto [Georgia Inst. of Technology, Atlanta, GA (United States); Sethi, Vijay [Western Research Inst., Laramie, WY (United States)

    2015-04-01

    GE Global Research, Idaho National Laboratory (INL), Georgia Institute of Technology (Georgia Tech), and Western Research Institute (WRI) proposed to develop high performance thin film polymer composite hollow fiber membranes and advanced processes for economical post-combustion carbon dioxide (CO2) capture from pulverized coal flue gas at temperatures typical of existing flue gas cleanup processes. The project sought to develop and then optimize new gas separations membrane systems at the bench scale, including tuning the properties of a novel polyphosphazene polymer in a coating solution and fabricating highly engineered porous hollow fiber supports. The project also sought to define the processes needed to coat the fiber support to manufacture composite hollow fiber membranes with high performance, ultra-thin separation layers. Physical, chemical, and mechanical stability of the materials (individual and composite) towards coal flue gas components was considered via exposure and performance tests. Preliminary design, technoeconomic, and economic feasibility analyses were conducted to evaluate the overall performance and impact of the process on the cost of electricity (COE) for a coal-fired plant including capture technologies. At the onset of the project, Membranes based on coupling a novel selective material polyphosphazene with an engineered hollow fiber support was found to have the potential to capture greater than 90% of the CO2 in flue gas with less than 35% increase in COE, which would achieve the DOE-targeted performance criteria. While lab-scale results for the polyphosphazene materials were very promising, and the material was incorporated into hollow-fiber modules, difficulties were encountered relating to the performance of these membrane systems over time. Performance, as measured by both flux of and selectivity for CO2 over other flue gas constituents was found to deteriorate over time, suggesting a system that was

  11. Accumulation of uranium, cesium, and radium by microbial cells: bench-scale studies

    International Nuclear Information System (INIS)

    Strandberg, G.W.; Shumate, S.E. II.

    1982-07-01

    This report describes bench-scale studies on the utilization of microbial cells for the concentration and removal of uranium, radium, and cesium from nuclear processing waste streams. Included are studies aimed at elucidating the basic mechanism of uranium uptake, process development efforts for the use of a combined denitrification-uranium removal process to treat a specific nuclear processing waste stream, and a preliminary investigation of the applicability of microorganisms for the removal of 137 Cs and 226 Ra from existing waste solutions

  12. From a single pellet press to a bench scale pellet mill - Pelletizing six different biomass feedstocks

    DEFF Research Database (Denmark)

    Puig Arnavat, Maria; Shang, Lei; Sárossy, Zsuzsa

    2016-01-01

    The increasing demand for biomass pellets requires the investigation of alternative raw materials for pelletizetion. In the present paper, the pelletization process of fescue, alfalfa, sorghum, triticale, miscanthus and willow is studied to determine if results obtained in a single pellet press...... (SPP) can be extrapolated to larger scale pellet mills. The single pellet press was used to find the optimum moisture content and die operating temperature for pellet production. Then, these results were compared with those obtained from a bench-scale pellet mill. A moisture content of around 10 wt...

  13. EFRT M12 Issue Resolution: Comparison of PEP and Bench-Scale Oxidative Leaching Results

    Energy Technology Data Exchange (ETDEWEB)

    Rapko, Brian M.; Brown, Christopher F.; Eslinger, Paul W.; Fountain, Matthew S.; Hausmann, Tom S.; Huckaby, James L.; Hanson, Brady D.; Kurath, Dean E.; Minette, Michael J.

    2009-08-14

    20 wt% solids using cross-flow ultrafiltration before the addition of caustic. For wastes that have significantly high chromium content, the caustic leaching and slurry dewatering is followed by adding sodium permanganate to UFP-VSL-T02A, and the slurry is subjected to oxidative leaching at nominally ambient temperature. The purpose of the oxidative leaching is to selectively oxidize the poorly alkaline-soluble Cr(III) believed to be the insoluble form in Hanford tank sludge to the much more alkaline-soluble Cr(VI), e.g., chromate. The work described in this report provides the test results that are related to the efficiency of the oxidative leaching process to support process modeling based on tests performed with a Hanford waste simulant. The tests were completed both at the lab-bench scale and in the PEP. The purpose of this report is to summarize the results from both scales that are related to oxidative leaching chemistry to support a scale factor for the submodels to be used in the G2 model, which predicts WTP operating performance. Owing to schedule constraints, the PEP test data to be included in this report are limited to those from Integrated Tests A (T01 A/B caustic leaching) and B (T02A caustic leaching).

  14. MITG test procedure and results

    International Nuclear Information System (INIS)

    Eck, M.E.; Mukunda, M.

    1983-01-01

    Elements and modules for Radioisotope Thermoelectric Generator have been performance tested since the inception of the RTG program. These test articles seldom resembled flight hardware and often lacked adequate diagnostic instrumentation. Because of this, performance problems were not identified in the early stage of program development. The lack of test data in an unexpected area often hampered the development of a problem solution. A procedure for conducting the MITG Test was developed in an effort to obtain data in a systematic, unambiguous manner. This procedure required the development of extensive data acquisition software and test automation. The development of a facility to implement the test procedure, the facility hardware and software requirements, and the results of the MITG testing are the subject of this paper

  15. In Developping a Bench-Scale Circulating Fluidized Bed Combustor to Burn High Ash Brazilian Coal-Dolomites Mixtures

    Science.gov (United States)

    Ramírez Behainne, Jhon Jairo; Hory, Rogério Ishikawa; Goldstein, Leonardo; Bernárdez Pécora, Araí Augusta

    This work considers some of the questions in burning high ash Brazilian coal-dolomite mixtures in a bench-scale circulating fluidized bed combustor (CFBC). Experimental tests were performed with the CE4500 coal from Santa Catarina State, in southern Brazil, with a Sauter mean diameter d p =43 μm. The coal particles were mixed with dolomite particles of d p = 111 μm and this fuel mixture was fed into the circulating fluidized reactor, previously loaded with quartz sand particles of d p =353 μm. This inert material was previously heated by the combustion of liquefied petroleum gas up to the ignition temperature of the fuel mixture. The CFBC unit has a 100mm internal diameter riser, 4.0m high, as well as a 62.8mm internal diameter downcomer. The loop has a cyclone, a sampling valve to collect particles and a 62.8mm internal diameter L-valve to recirculate the particles in the loop. A screw feeder with a rotation control system was used to feed the fuel mixture to the reactor. The operational conditions were monitored by pressure taps and thermocouples installed along the loop. A data acquisition system showed the main operational conditions to control. Experimental tests performed put in evidence the problems found during bed operation, with special attention to the solids feed device, to the L-valve operation, to particle size, solids inventory, fluidized gas velocity, fuel mixture and recirculated solids feeding positions.

  16. Inactivation of Escherichia coli by ozone under bench-scale plug flow and full-scale hydraulic conditions.

    Science.gov (United States)

    Smeets, P W M H; van der Helm, A W C; Dullemont, Y J; Rietveld, L C; van Dijk, J C; Medema, G J

    2006-10-01

    To determine the disinfection efficacy of ozonation, water companies can apply several disinfection calculation methods. The goal of this study was to evaluate the use of the T10 and continuous stirred tank reactor (CSTR) method to extrapolate inactivation rates of ozone sensitive microorganisms observed in laboratory tests to full-scale ozonation in drinking water treatment. The inactivation efficacy of the ozonation at the Amsterdam water treatment works was assessed by determining Escherichia coli concentrations in large volume samples before and after ozonation over a period of 1 year. The inactivation of dosed E. coli WR1 was tested in a bench-scale dissolved ozone plug flow reactor (DOPFR) on the same feed water as the full-scale ozonation in which a concentrated ozone solution in Milli-Q water was dosed. Applying the T10 method on the inactivation rates observed in the DOPFR strongly overestimated the inactivation capacity of the full-scale ozonation. The expected inactivation based on the CSTR method (LT2ESWTR) approached the observed inactivation at full-scale. Therefore, the CSTR method should be preferred to calculate inactivation of ozone sensitive organisms such as E. coli, viruses, Giardia and Campylobacter by full-scale ozonation.

  17. The hot bench scale plant Ester for the vitrification of high level wastes

    International Nuclear Information System (INIS)

    Nannicini, R.; Strazzer, A.; Cantale, C; Donato, A.; Grossi, G.

    1985-01-01

    In this paper the hot bench-scale plant ESTER for the vitrification of the high-level radioactive wastes is described, and the main results of the first radioactive campaign are reported. The ESTER plant, which is placed in the ADECO-ESSOR hot cells of the C.C.R.-EURATOM-ISPRA, has been built and is operated by the ENEA, Departement of Fuel Cycle. It began operating with real radioactive wastes about 1 year ago, solidifying a total of 12 Ci of fission products into 2,02 Kg of borosilicate glass, corresponding to 757 ml of glass. During the vitrification many samples of liquid and gaseous streams have been taken and analyzed. A radioactivity balance in the plant has been calculated, as well as a mass balance of nitrates and of the 137 Cs and 106 Ru volatized in the process

  18. TMACS Test Procedure TP011: Panalarm Interface

    International Nuclear Information System (INIS)

    Seghers, R.; Washburn, S.J.

    1994-01-01

    The TMACS Software Test Procedures translate the project's acceptance criteria into test steps. The TMACS Test Plan (WHC-SD-WM-TP-148) is fulfilled when all Test Cases are approved. This Test Procedure tests the TMACS Panalarm Interface functions

  19. Recycling of polyethene and polypropene in a novel bench-scale rotating cone reactor by high temperature pyrolysis.

    NARCIS (Netherlands)

    Westerhout, R.W.J.; Westerhout, R.W.J.; Waanders, J.; Kuipers, J.A.M.; van Swaaij, Willibrordus Petrus Maria

    1998-01-01

    The high-temperature pyrolysis of polyethene (PE), polypropene (PP), and mixtures of these polymers was studied in a novel bench-scale rotating cone reactor (RCR). Experiments showed that the effect of the sand or reactor temperature on the product spectrum obtained is large compared to the effect

  20. Performance of Dolomite Calcination in a Bench-Scale Rotary Kiln

    Directory of Open Access Journals (Sweden)

    Wulandari Winny

    2018-01-01

    Full Text Available Dolomite calcination is one of process steps to prepare calcined dolomite for raw materials in magnesium production. Calcination of dolomite involves heating the raw material at sufficient temperature in order to release the carbon dioxide from its carbonate minerals. This process is commonly conducted in a rotary kiln. There have been a number of calcination studies in a laboratory scale, but the study of dolomite calcination in a larger scale is very scarce. This research is aimed to study the performance of dolomite calcination in a bench-scale rotary kiln with 500 gram of feed. The effect of various parameters, including temperatures, feed rate, rotating frequency, and particle size were examined. The temperature of rotary kiln was varied between 700 and 1000 °C, while the particle size of dolomite was varied between 0.149 – 0.297 mm and up to 10 – 15 mm. The temperature distribution inside the rotary kiln was also measured. It is obtained that a conversion of 92% was attained at operation temperature of 1000 °C, which is at a higher temperature compared to the laboratory scale, where a conversion of 100% was obtained at 900 °C. This imply that the effect of heat transfer also plays important role in the calcination of dolomite especially at a larger scale.

  1. Destruction of chemical agent simulants in a supercritical water oxidation bench-scale reactor

    International Nuclear Information System (INIS)

    Veriansyah, Bambang; Kim, Jae-Duck; Lee, Jong-Chol

    2007-01-01

    A new design of supercritical water oxidation (SCWO) bench-scale reactor has been developed to handle high-risk wastes resulting from munitions demilitarization. The reactor consists of a concentric vertical double wall in which SCWO reaction takes place inside an inner tube (titanium grade 2, non-porous) whereas pressure resistance is ensured by a Hastelloy C-276 external vessel. The performances of this reactor were investigated with two different kinds of chemical warfare agent simulants: OPA (a mixture of isopropyl amine and isopropyl alcohol) as the binary precursor for nerve agent of sarin and thiodiglycol [TDG (HOC 2 H 4 ) 2 S] as the model organic sulfur heteroatom. High destruction rates based on total organic carbon (TOC) were achieved (>99.99%) without production of chars or undesired gases such as carbon monoxide and methane. The carbon-containing product was carbon dioxide whereas the nitrogen-containing products were nitrogen and nitrous oxide. Sulfur was totally recovered in the aqueous effluent as sulfuric acid. No corrosion was noticed in the reactor after a cumulative operation time of more than 250 h. The titanium tube shielded successfully the pressure vessel from corrosion

  2. A novel bench-scale column assay to investigate site-specific nitrification biokinetics in biological rapid sand filters

    DEFF Research Database (Denmark)

    Tatari, Karolina; Smets, Barth F.; Albrechtsen, Hans-Jørgen

    2013-01-01

    A bench-scale assay was developed to obtain site-specific nitrification biokinetic information from biological rapid sand filters employed in groundwater treatment. The experimental set-up uses granular material subsampled from a full-scale filter, packed in a column, and operated with controlled...... and continuous hydraulic and ammonium loading. Flowrates and flow recirculation around the column are chosen to mimic full-scale hydrodynamic conditions, and minimize axial gradients. A reference ammonium loading rate is calculated based on the average loading experienced in the active zone of the full......-scale filter. Effluent concentrations of ammonium are analyzed when the bench-scale column is subject to reference loading, from which removal rates are calculated. Subsequently, removal rates above the reference loading are measured by imposing short-term loading variations. A critical loading rate...

  3. TMACS Test Procedure TP009: Acromag Driver

    International Nuclear Information System (INIS)

    Washburn, S.J.

    1994-01-01

    The TMACS Software Project Test Procedures translate the project's acceptance criteria into test steps. Software releases are certified when the affected Test Procedures are successfully performed and the customers authorize installation of these changes. This Test Procedure tests the TMACS Acromag Software Driver (Bridge Code)

  4. TMACS Test Procedure TP007: System administration

    International Nuclear Information System (INIS)

    Scanlan, P.; Washburn, S.; Seghers, R.

    1994-01-01

    The TMACS Software Project Test Procedures translate the project's acceptance criteria into test steps. Software releases are certified when the affected Test Procedures are successfully performed and the customers authorize installation of these changes. This Test Procedure tests the TMACS System Administration functions

  5. TMACS Test Procedure TP002: Trending

    International Nuclear Information System (INIS)

    Scanlan, P.K.

    1994-01-01

    The TMACS Software Project Test Procedures translate the project's acceptance criteria into test steps. Software releases are certified when the affected Test Procedures are successfully performed and the customers authorize installation of these changes. This Test Procedure tests the TMACS Trending functions

  6. Bench-Scale Development of a Hot Carbonate Absorption Process with Crystallization-Enabled High-Pressure Stripping for Post-Combustion CO{sub 2} Capture

    Energy Technology Data Exchange (ETDEWEB)

    Lu, Yongqi; DeVries, Nicholas; Ruhter, David; Manoranjan, Sahu; Ye, Qing; Ye, Xinhuai; Zhang, Shihan; Chen, Scott; Li, Zhiwei; O' Brien, Kevin

    2014-03-31

    A novel Hot Carbonate Absorption Process with Crystallization-Enabled High-Pressure Stripping (Hot-CAP) has been developed by the University of Illinois at Urbana-Champaign and Carbon Capture Scientific, LLC in this three-year, bench-scale project. The Hot-CAP features a concentrated carbonate solution (e.g., K{sub 2}CO{sub 3}) for CO{sub 2} absorption and a bicarbonate slurry (e.g., KHCO{sub 3}) for high-pressure CO{sub 2} stripping to overcome the energy use and other disadvantages associated with the benchmark monoethanolamine (MEA) process. The project was aimed at performing laboratory- and bench-scale experiments to prove its technical feasibility and generate process engineering and scale-up data, and conducting a techno-economic analysis (TEA) to demonstrate its energy use and cost competitiveness over MEA. To meet project goals and objectives, a combination of experimental, modeling, process simulation, and economic analysis studies were applied. Carefully designed and intensive experiments were conducted to measure thermodynamic and reaction engineering data relevant to four major unit operations in the Hot-CAP (i.e., CO{sub 2} absorption, CO{sub 2} stripping, bicarbonate crystallization, and sulfate reclamation). The rate promoters that could accelerate the CO{sub 2} absorption rate into the potassium carbonate/bicarbonate (PCB) solution to a level greater than that into the 5 M MEA solution were identified, and the superior performance of CO{sub 2} absorption into PCB was demonstrated in a bench-scale packed-bed column. Kinetic data on bicarbonate crystallization were developed and applied for crystallizer design and sizing. Parametric testing of high-pressure CO{sub 2} stripping with concentrated bicarbonate-dominant slurries at high temperatures ({>=}140{degrees}C) in a bench-scale stripping column demonstrated lower heat use than with MEA. The feasibility of a modified process for combining SO{sub 2} removal with CO{sub 2} capture was preliminarily

  7. Heavy metal contaminant remediation study of western Xiamen Bay sediment, China: laboratory bench scale testing results.

    Science.gov (United States)

    Zhang, Luoping; Feng, Huan; Li, Xiaoxia; Ye, Xin; Jing, Youhai; Ouyang, Tong; Yu, Xingtian; Liang, Rongyuan; Chen, Weiqi

    2009-12-15

    A surface sediment sample (metal removal, whereas agitation, aeration and rotation of the samples in chemical complexation solutions yield much better metal removal efficiency (up to 90%). A low pH condition (e.g., pHliquid ratio (e.g., S:L=1:50) could increase metal removal efficiency. The experimental results suggest that 0.20 M (NH4)2C2O4+0.025 M EDTA combination with solid:liquid ratio=1:50 and 0.50 M ammonium acetate (NH4Ac)+0.025 M EDTA combination with solid:liquid ratio=1:50 are the most effective methods for metal removal from the contaminated sediments. This research provides additional useful information for sediment metal remediation technology development.

  8. Preschooler test or procedure preparation

    Science.gov (United States)

    ... your child during and after the procedure with books, songs, counting, deep breathing, or blowing bubbles. PLAY ... can be present during the procedure. Ask if anesthesia can be used to reduce your child's discomfort. ...

  9. Toddler test or procedure preparation

    Science.gov (United States)

    ... use after the procedure. Distract your child with books, songs, or a simple activity such as blowing ... can be present during the procedure. Ask if anesthesia can be used, if appropriate, to reduce your ...

  10. Size distribution of chromate paint aerosol generated in a bench-scale spray booth.

    Science.gov (United States)

    Sabty-Daily, Rania A; Hinds, William C; Froines, John R

    2005-01-01

    Spray painters are potentially exposed to aerosols containing hexavalent chromium [Cr(VI)] via inhalation of chromate-based paint sprays. Evaluating the particle size distribution of a paint spray aerosol, and the variables that may affect this distribution, is necessary to determine the site and degree of respiratory deposition and the damage that may result from inhaled Cr(VI)-containing paint particles. This study examined the effect of spray gun atomization pressure, aerosol generation source and aerosol aging on the size distribution of chromate-based paint overspray aerosols generated in a bench-scale paint spray booth. The study also determined the effect of particle bounce inside a Marple personal cascade impactor on measured size distributions of paint spray aerosols. Marple personal cascade impactors with a modified inlet were used for sample collection. The data indicated that paint particle bounce did not occur inside the cascade impactors sufficiently to affect size distribution when using uncoated stainless steel or PVC substrate sampling media. A decrease in paint aerosol mass median aerodynamic diameter (MMAD) from 8.2 to 7.0 mum was observed as gun atomization pressure increased from 6 to 10 psi. Overspray aerosols were sampled at two locations in the spray booth. A downstream sampling position simulated the exposure of a worker standing between the painted surface and exhaust, a situation encountered in booths with multiple workers. The measured mean MMAD was 7.2 mum. The distance between the painted surface and sampler was varied to sample oversprays of varying ages between 2.8 and 7.7 s. Age was not a significant factor for determining MMAD. Overspray was sampled at a 90 degrees position to simulate a worker standing in front of the surface being painted with air flowing to the worker's side, a common situation in field applications. The resulting overspray MMAD averaged 5.9 mum. Direct-spray aerosols were sampled at ages from 5.3 to 11.7 s

  11. Bench-scale evaluation of drinking water treatment parameters on iron particles and water quality.

    Science.gov (United States)

    Rahman, M Safiur; Gagnon, Graham A

    2014-01-01

    Discoloration of water resulting from suspended iron particles is one of the main customer complaints received by water suppliers. However, understanding of the mechanisms of discoloration as well as role of materials involved in the process is limited. In this study, an array of bench scale experiments were conducted to evaluate the impact of the most common variables (pH, PO4, Cl2 and DOM) on the properties of iron particles and suspensions derived from the oxygenation of Fe(II) ions in NaHCO3 buffered synthetic water systems. The most important factors as well as their rank influencing iron suspension color and turbidity formation were identified for a range of water quality parameters. This was accomplished using a 2(4) full factorial design approach at a 95% confidence level. The statistical analysis revealed that phosphate was found to be the most significant factor to alter color (contribution: 37.9%) and turbidity (contribution: 45.5%) in an iron-water system. A comprehensive study revealed that phosphate and chlorine produced iron suspension with reduced color and turbidity, made ζ-potential more negative, reduced the average particle size, and increased iron suspension stability. In the presence of DOM, color was observed to increase but a reverse trend was observed to decrease the turbidity and to alter particle size distribution. HPSEC results suggest that higher molecular weight fractions of DOM tend to adsorb onto the surfaces of iron particles at early stages, resulting in alteration of the surface charge of iron particles. This in turn limits particles aggregation and makes iron colloids highly stable. In the presence of a phosphate based corrosion inhibitor, this study demonstrated that color and turbidity resulting from suspended iron were lower at a pH value of 6.5 (compared to pH of 8.5). The same trend was observed in presence of DOM. This study also suggested that iron colloid suspension color and turbidity in chlorinated drinking water

  12. Soluble Microbial Product Characterization of Biofilm Formation in Bench-Scale

    KAUST Repository

    Mines, Paul

    2012-12-01

    The biological process known as activated sludge (AS) in conjunction with membrane separation technology for the treatment of wastewater has been employed for over four decades. While, membrane biological reactors (MBR) are now widely employed, the phenomenon of membrane fouling is still the most significant factor leading to performance decline of MBRs. Although much research has been done on the subject of MBR fouling over the past two decades, many questions remain unanswered, and consensus within the scientific community is rare. However, research has led to one system parameter generally being regarded as a contributor to membrane fouling, extracellular polymeric compounds (EPS). EPS, and more specifically, the soluble fraction of EPS known as soluble microbial products (SMP), must be further investigated in order to better understand membrane fouling. The biological activity and performance of the MBR is affected by myriad operational parameters, which in turn affects the SMP generated. A commonly varied operational parameter is, depending on the specific treatment needs of a MBR, the sludge retention time (SRT). This study aims to characterize the SMP in three bench-scale MBRs as the SRT is gradually lowered. By studying how the SMP change as the operation of the system is altered, greater understanding of how SMP are related to fouling can be achieved. At the onset of the study, a steady state was established in the system with a SRT of 20 days. Upon stabilization of a 20 day SRT, the system was gradually transitioned to a five and a half day SRT, in stepwise adjustments. Initially, both the trans-membrane pressure (TMP) and the SMP concentrations were at relatively low values, indicating the presence of minimal amounts of biofilm on the membrane surfaces. As the system was altered and more activated sludge was wasted from the reactors, the SRT inherently decreased. As the lower SRT was transitioned and established, the data from TMP measurements, as well

  13. Adolescent test or procedure preparation

    Science.gov (United States)

    ... someone else) during the procedure Playing hand-held video games Using guided imagery Trying other distractions, such as listening to music through headphones, if allowed When possible, let your ...

  14. Catalytic multi-stage liquefaction of coal at HTI: Bench-scale studies in coal/waste plastics coprocessing

    Energy Technology Data Exchange (ETDEWEB)

    Pradhan, V.R.; Lee, L.K.; Stalzer, R.H. [Hydrocarbon Technologies, Inc., Lawrenceville, NJ (United States)] [and others

    1995-12-31

    The development of Catalytic Multi-Stage Liquefaction (CMSL) at HTI has focused on both bituminous and sub-bituminous coals using laboratory, bench and PDU scale operations. The crude oil equivalent cost of liquid fuels from coal has been curtailed to about $30 per barrel, thus achieving over 30% reduction in the price that was evaluated for the liquefaction technologies demonstrated in the late seventies and early eighties. Contrary to the common belief, the new generation of catalytic multistage coal liquefaction process is environmentally very benign and can produce clean, premium distillates with a very low (<10ppm) heteroatoms content. The HTI Staff has been involved over the years in process development and has made significant improvements in the CMSL processing of coals. A 24 month program (extended to September 30, 1995) to study novel concepts, using a continuous bench scale Catalytic Multi-Stage unit (30kg coal/day), has been initiated since December, 1992. This program consists of ten bench-scale operations supported by Laboratory Studies, Modelling, Process Simulation and Economic Assessments. The Catalytic Multi-Stage Liquefaction is a continuation of the second generation yields using a low/high temperature approach. This paper covers work performed between October 1994- August 1995, especially results obtained from the microautoclave support activities and the bench-scale operations for runs CMSL-08 and CMSL-09, during which, coal and the plastic components for municipal solid wastes (MSW) such as high density polyethylene (HDPE)m, polypropylene (PP), polystyrene (PS), and polythylene terphthlate (PET) were coprocessed.

  15. 40 CFR 205.54 - Test procedures.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 24 2010-07-01 2010-07-01 false Test procedures. 205.54 Section 205.54 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) NOISE ABATEMENT PROGRAMS TRANSPORTATION EQUIPMENT NOISE EMISSION CONTROLS Medium and Heavy Trucks § 205.54 Test procedures. The procedures described...

  16. Treatment of waste gas containing low concentration of dimethyl sulphide (DMS) in a bench-scale biofilter.

    Science.gov (United States)

    Giri, B S; Mudliar, S N; Deshmukh, S C; Banerjee, S; Pandey, R A

    2010-04-01

    Biological treatment of dimethyl sulphide (DMS) was investigated in a bench-scale biofilter, packed with compost along with wood chips, and enriched with DMS degrading microorganism Bacillus sphaericus. The biofilter could remove 62-74% of the inlet DMS, at an optimum loading of 0.484 g/m(3)/h with optimum empty bed contact time (EBCT) of 384 s and an average moisture range of 65-70%. The biodegradative products of DMS were sulphide, thiosulphate and sulphate. Evaluation of microbiological status of the biofilter indicated the presence of other bacterial cultures viz. Paenibacillus polymyxa, and Bacillus megaterium, besides B. sphaericus. Copyright 2009 Elsevier Ltd. All rights reserved.

  17. Bench-Scale Process for Low-Cost Carbon Dioxide (CO2) Capture Using a Phase-Changing Absorbent

    Energy Technology Data Exchange (ETDEWEB)

    Westendorf, Tiffany; Caraher, Joel; Chen, Wei; Farnum, Rachael; Perry, Robert; Spiry, Irina; Wilson, Paul; Wood, Benjamin

    2015-03-31

    The objective of this project is to design and build a bench-scale process for a novel phase-changing aminosilicone-based CO2-capture solvent. The project will establish scalability and technical and economic feasibility of using a phase-changing CO2-capture absorbent for post-combustion capture of CO2 from coal-fired power plants with 90% capture efficiency and 95% CO2 purity at a cost of $40/tonne of CO2 captured by 2025 and a cost of <$10/tonne of CO2 captured by 2035. In the first budget period of this project, the bench-scale phase-changing CO2 capture process was designed using data and operating experience generated under a previous project (ARPA-e project DE-AR0000084). Sizing and specification of all major unit operations was completed, including detailed process and instrumentation diagrams. The system was designed to operate over a wide range of operating conditions to allow for exploration of the effect of process variables on CO2 capture performance.

  18. Treatment of Synthetic Wastewater Containing AB14 Pigment by Electrooxidation in both Pilot and Bench Scale Reactors

    Directory of Open Access Journals (Sweden)

    Jalal Basiri parsa

    2016-01-01

    Full Text Available The electrochemical oxidation process was used for the degradation of Acid Brown 14 in both bench and pilot scale reactors. The bench scale one with a working volume of 0.5 L was equipped with platinum plate used as the anode and stainless steel (SS-304 plates as the cathode. The pilot scale reactor had a volume of 9 L and was equipped with SS-304 plates used as both the anode and the cathode. Experiments were run using these reactors to investigate the two parameters of energy consumption and anode efficiency. The bench scale reactor was capable of removing 92% and 36% of the dye and COD, respectively, after 18 min of operation. The pilot scale reactor, however, was capable of removing 87% and 59% of the dye and the COD content, respectively, after 60 min of operation. The kinetic study of both the bench and pilot reactors for dye and COD removals showed that both processes followed a zero order kinetic.

  19. Bench Scale Process for Low Cost CO2 Capture Using a Phase-Changing Absorbent: Topical Report EH&S Risk Assessment

    Energy Technology Data Exchange (ETDEWEB)

    Westendorf, Tiffany; Farnum, Rachel; Perry, Robert; Herwig, Mark; Giolando, Salvatore; Green, Dianne; Morall, Donna

    2016-05-11

    GE Global Research was contracted by the Department of Energy to design and build a bench-scale process for a novel phase-changing aminosilicone-based CO2 capture solvent (award number DEFE0013687). As part of this program, a technology EH&S assessment (Subtask 5.1) has been completed for a CO2 capture system for a 550 MW coal-fired power plant. The assessment focuses on two chemicals used in the process, the aminosilicone solvent, GAP-0, and dodecylbenzenesulfonic acid (DDBSA), the GAP-0 carbamate formed upon reaction of the GAP-0 with CO2, and two potential byproducts formed in the process, GAP-0/SOx salts and amine-terminated, urea-containing silicone (also referred to as “ureas” in this report). The EH&S assessment identifies and estimates the magnitude of the potential air and water emissions and solid waste generated by the process and reviews the toxicological profiles of the chemicals associated with the process. Details regarding regulatory requirements, engineering controls, and storage and handling procedures are also provided in the following sections.

  20. 40 CFR 53.66 - Test procedure: Volatility test.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 5 2010-07-01 2010-07-01 false Test procedure: Volatility test. 53.66... Characteristics of Class II Equivalent Methods for PM2.5 § 53.66 Test procedure: Volatility test. (a) Overview. This test is designed to ensure that the candidate method's losses due to volatility when sampling semi...

  1. Handbook of mutagenicity test procedures

    International Nuclear Information System (INIS)

    Kilbey, B.J.; Legatov, M.

    1977-01-01

    27 articles are presented on particular techniques of mutagen testing. Background information is given in materials, experimental design, pitfalls and difficults, to enable the reader to perform these tests with minimal additional help. Also included is the use of data from population records, the handling and safety aspects of mutagens and carcinogens and some of the basic statistical concepts to be borne in mind when mutation experiments are designed. (C.F.)

  2. Treatability study for the bench-scale solidification of nonincinerable LDR low-level mixed waste

    International Nuclear Information System (INIS)

    Gering, K.L.

    1993-01-01

    The focus of this report is the solidification of nonincinerable, land disposal restricted (LDR) low-level mixed waste generated at the Idaho National Engineering Laboratory. Benchscale solidification was performed on samples of this mixed waste, which was done under a Resource Conservation and Recovery Act treatability study. Waste forms included liquids, sludges, and solids, and treatment techniques included the use of conventional Portland cement and sulphur polymer cement (SPC). A total of 113 monoliths were made under the experimental design matrix for this study; 8 of these were ''blank'' monoliths (contained no waste). Thus, 105 monoliths were used to solidify 21.6 kg of mixed waste; 92 were made with Portland cement systems, and 13 were made with SPC. Recipes for all monoliths are given, and suggested recipes (as based on the minimized leaching of toxic components) are summarized. In most cases, the results presented herein indicate that solidification was successful in immobilizing toxic metals, thereby transforming low-level mixed waste into low-level nonhazardous waste. The ultimate goal of this project is to use appropriate solidification techniques, as described in the literature, to transform low-level mixed waste to low-level nonhazardous waste by satisfying pertinent disposal requirements for this waste. Disposal requirements consider the toxicity characteristic leaching procedure tests, a free liquids test, and radiological analyses. This work is meaningful in that it will provide a basis for the disposal of waste that is currently categorized as LDR low-level mixed waste

  3. MITS Data Acquisition Subsystem Acceptance Test procedure

    International Nuclear Information System (INIS)

    Allison, R.

    1980-01-01

    This is an acceptance procedure for the Data Acquisition Subsystem of the Machine Interface Test System (MITS). Prerequisites, requirements, and detailed step-by-step instruction are presented for inspecting and performance testing the subsystem

  4. Caustic addition system operability test procedure

    International Nuclear Information System (INIS)

    Parazin, R.E.

    1994-11-01

    This test procedure provides instructions for performing operational testing of the major components of the 241-AN-107 Caustic Addition System by WHC and Kaiser personnel at the Rotating Equipment Shop run-in pit (Bldg. 272E)

  5. Acceptance test procedure for Project W-280

    International Nuclear Information System (INIS)

    Stites, C.G.

    1994-01-01

    This Document is the Acceptance Test Procedure for 200 Area C and SY Tank Farm Lighting Upgrade. This Acceptance Test Procedure has been prepared to demonstrate that the Tank Farm Lighting Systems function correctly as required by project criteria and as intended by design

  6. W-087 Acceptance test procedure. Revision 1

    International Nuclear Information System (INIS)

    Joshi, A.W.

    1997-01-01

    This Acceptance Test Procedure/Operational Test Procedure (ATP/OTP) has been prepared to demonstrate that the Electrical/Instrumentation and Mechanical systems function as required by project criteria and to verify proper operation of the integrated system including the interlocks

  7. Void fraction instrument acceptance test procedure

    International Nuclear Information System (INIS)

    Pearce, K.L.

    1994-01-01

    This acceptance test procedure (ATP) was written to test the void fraction instrument (VFI) and verify that the unit is ready for field service. The procedure verifies that the mechanical and electrical features (not specifically addressed in the software ATP) and software alarms are operating as designed

  8. 10 CFR 474.4 - Test procedures.

    Science.gov (United States)

    2010-01-01

    ... 10 Energy 3 2010-01-01 2010-01-01 false Test procedures. 474.4 Section 474.4 Energy DEPARTMENT OF ENERGY ENERGY CONSERVATION ELECTRIC AND HYBRID VEHICLE RESEARCH, DEVELOPMENT, AND DEMONSTRATION PROGRAM; PETROLEUM-EQUIVALENT FUEL ECONOMY CALCULATION § 474.4 Test procedures. (a) The electric vehicle energy...

  9. DACS upgrade acceptance test procedure

    Energy Technology Data Exchange (ETDEWEB)

    Zuehlke, A.C.

    1994-09-28

    The readiness of the Data Acquisition and Control System (DACS) to provide monitoring and control of the mixer pump, directional drive system, and the instrumentation associated with the SY-101 tank and support systems, and the proper functioning of the DACS with new Model 984-785 Programmable Logic Controllers (PLCs), new MODBUS PLUS version 2.01 software for the PLCs, and version 3.72 of the GENESIS software will be systematically evaluated by performance of this procedure. The DACS, which is housed in a trailer located just outside of the north fence at the SY tank farm, receives input signals from a variety of sensors located in and around the SY-101 tanks. These sensors provide information such as: tank vapor space and ventilation system H{sub 2} concentration; tank waste temperature; tank pressure; waste density; operating pump parameters such as speed, flow, rotational position, discharge pressure, and internal temperature; strain (for major equipment); and waste level. The output of these sensors is conditioned and transmitted to the DACS computers where these signals are displayed, recorded, and monitored for out-of-specification conditions. If abnormal conditions are detected, then, in certain situations, the DACS automatically generates alarms and causes the system to abort pump operations.

  10. DACS upgrade acceptance test procedure

    International Nuclear Information System (INIS)

    Zuehlke, A.C.

    1994-01-01

    The readiness of the Data Acquisition and Control System (DACS) to provide monitoring and control of the mixer pump, directional drive system, and the instrumentation associated with the SY-101 tank and support systems, and the proper functioning of the DACS with new Model 984-785 Programmable Logic Controllers (PLCs), new MODBUS PLUS version 2.01 software for the PLCs, and version 3.72 of the GENESIS software will be systematically evaluated by performance of this procedure. The DACS, which is housed in a trailer located just outside of the north fence at the SY tank farm, receives input signals from a variety of sensors located in and around the SY-101 tanks. These sensors provide information such as: tank vapor space and ventilation system H 2 concentration; tank waste temperature; tank pressure; waste density; operating pump parameters such as speed, flow, rotational position, discharge pressure, and internal temperature; strain (for major equipment); and waste level. The output of these sensors is conditioned and transmitted to the DACS computers where these signals are displayed, recorded, and monitored for out-of-specification conditions. If abnormal conditions are detected, then, in certain situations, the DACS automatically generates alarms and causes the system to abort pump operations

  11. Flexible Bench-Scale Recirculating Flow CPC Photoreactor for Solar Photocatalytic Degradation of Methylene Blue Using Removable TiO2 Immobilized on PET Sheets

    Directory of Open Access Journals (Sweden)

    Doaa M. EL-Mekkawi

    2016-01-01

    Full Text Available TiO2 immobilized on polyethylene (PET nonwoven sheet was used in the solar photocatalytic degradation of methylene blue (MB. TiO2 Evonik Aeroxide P25 was used in this study. The amount of loaded TiO2 on PET was approximately 24%. Immobilization of TiO2 on PET was conducted by dip coating process followed by exposing to mild heat and pressure. TiO2/PET sheets were wrapped on removable Teflon rods inside home-made bench-scale recirculating flow Compound Parabolic Concentrator (CPC photoreactor prototype (platform 0.7 × 0.2 × 0.4 m3. CPC photoreactor is made up of seven low iron borosilicate glass tubes connected in series. CPC reflectors are made of stainless steel 304. The prototype was mounted on a platform tilted at 30°N local latitude in Cairo. A centrifugal pump was used to circulate water containing methylene blue (MB dye inside the glass tubes. Efficient photocatalytic degradation of MB using TiO2/PET was achieved upon the exposure to direct sunlight. Chemical oxygen demand (COD analyses reveal the complete mineralization of MB. Durability of TiO2/PET composite was also tested under sunlight irradiation. Results indicate only 6% reduction in the amount of TiO2 after seven cycles. No significant change was observed for the physicochemical characteristics of TiO2/PET after the successive irradiation processes.

  12. Characterization of L-asparaginase from marine-derived Aspergillus niger AKV-MKBU, its antiproliferative activity and bench scale production using industrial waste.

    Science.gov (United States)

    Vala, Anjana K; Sachaniya, Bhumi; Dudhagara, Dushyant; Panseriya, Haresh Z; Gosai, Haren; Rawal, Rakesh; Dave, Bharti P

    2018-03-01

    L-asparaginase (LA), an enzyme with anticancer activities, produced by marine-derived Aspergillus niger was subjected to purification and characterization. The purified enzyme was observed to have molecular weight ∼90KDa. The enzyme retained activity over a wide range of pH, i.e. pH 4-10. The enzyme was quite stable in temperature range 20-40°C. Tween 80 and Triton X-100 were observed to enhance LA activity while inhibition of LA activity was observed in presence of heavy metals. The values for K m was found to be 0.8141 mM and V max was 6.228μM/mg/min. The enzyme exhibited noteworthy antiproliferative activity against various cancer cell lines tested. Successful bench scale production (in 5L bioreacator) of LA using groundnut oil cake as low cost substrate has also been carried out. Copyright © 2017 Elsevier B.V. All rights reserved.

  13. 40 CFR 53.64 - Test procedure: Static fractionator test.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 5 2010-07-01 2010-07-01 false Test procedure: Static fractionator test. 53.64 Section 53.64 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR... Performance Characteristics of Class II Equivalent Methods for PM2.5 § 53.64 Test procedure: Static...

  14. DOT-7A packaging test procedure

    International Nuclear Information System (INIS)

    Kelly, D.L.

    1995-01-01

    This test procedure documents the steps involved with performance testing of Department of Transportation Specification 7A (DOT-7A) Type A packages. It includes description of the performance tests, the personnel involved, appropriate safety considerations, and the procedures to be followed while performing the tests. Westinghouse Hanford Company (WHC) is conducting the evaluation and testing discussed herein for the Department of Energy-Headquarters, Division of Quality Verification and Transportation Safety (EH-321). Please note that this report is not in WHC format. This report is being submitted through the Engineering Documentation System so that it may be used for reference and information purposes

  15. 40 CFR 204.54 - Test procedures.

    Science.gov (United States)

    2010-07-01

    ... Auditing or Testing by the Administrator must be conducted and the measurement procedures that must be used... International Electrotechnical Commission (IEC) Publication No. 179, “Precision Sound Level Meters.” (2) A...

  16. Small Optics Laser Damage Test Procedure

    Energy Technology Data Exchange (ETDEWEB)

    Wolfe, Justin [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

    2017-10-19

    This specification defines the requirements and procedure for laser damage testing of coatings and bare surfaces designated for small optics in the National Ignition Facility (NIF) at Lawrence Livermore National Laboratory (LLNL).

  17. AZ-101 Mixer Pump Test Qualification Test Procedures (QTP)

    International Nuclear Information System (INIS)

    THOMAS, W.K.

    2000-01-01

    Describes the Qualification test procedure for the AZ-101 Mixer Pump Data Acquisition System (DAS). The purpose of this Qualification Test Procedure (QTP) is to confirm that the AZ-101 Mixer Pump System has been properly programmed and hardware configured correctly. This QTP will test the software setpoints for the alarms and also check the wiring configuration from the SIMcart to the HMI. An Acceptance Test Procedure (ATP), similar to this QTP will be performed to test field devices and connections from the field

  18. Parametric Sensitivity Tests- European PEM Fuel Cell Stack Test Procedures

    DEFF Research Database (Denmark)

    Araya, Samuel Simon; Andreasen, Søren Juhl; Kær, Søren Knudsen

    2014-01-01

    performed based on test procedures proposed by a European project, Stack-Test. The sensitivity of a Nafion-based low temperature PEMFC stack’s performance to parametric changes was the main objective of the tests. Four crucial parameters for fuel cell operation were chosen; relative humidity, temperature......, pressure, and stoichiometry at varying current density. Furthermore, procedures for polarization curve recording were also tested both in ascending and descending current directions....

  19. Experimental and modelling studies on continuous synthesis and refining of biodiesel in a dedicated bench scale unit using centrifugal contactor separator technology

    NARCIS (Netherlands)

    Abduh, Muhammad Yusuf; Martinez, Alberto Fernandez; Kloekhorst, Arjan; Manurung, Robert; Heeres, Hero J.

    Continuous synthesis and refining of biodiesel (FAME) using a laboratory scale bench scale unit was explored. The unit consists of three major parts: (i) a continuous centrifugal contactor separator (CCCS) to perform the reaction between sunflower oil and methanol; (ii) a washing unit for the crude

  20. In-plant testing of microbubble column flotation. Final report

    Energy Technology Data Exchange (ETDEWEB)

    Yoon, R.H.; Luttrell, G.H.; Adel, G.T.; Mankosa, M.J.

    1991-07-31

    Microbubble column flotation (MCF) was developed at the Virginia Center for Coal and Minerals Processing (VCCMP) for the selective recovery of fine particles. Bench-scale test work conducted at VCCMP, largely under the sponsorship of the U.S. Department of Energy (DOE), showed that the technology worked well for both coal and mineral applications. For the technology to be commercially successful, however, a full-scale demonstration of the MCF technology was deemed necessary. This report summarizes the results of work performed under the DOE project entitled ``In-plant Testing of Microbubble Column Flotation.`` The objectives of this research and development effort were to duplicate the bench-scale performance of the MCF process in a full-scale unit, to verify the scale-up procedure developed in an earlier project, and to demonstrate the applicability of the MCF technology to the coal industry.

  1. In-plant testing of microbubble column flotation

    Energy Technology Data Exchange (ETDEWEB)

    Yoon, R.H.; Luttrell, G.H.; Adel, G.T.; Mankosa, M.J.

    1991-07-31

    Microbubble column flotation (MCF) was developed at the Virginia Center for Coal and Minerals Processing (VCCMP) for the selective recovery of fine particles. Bench-scale test work conducted at VCCMP, largely under the sponsorship of the U.S. Department of Energy (DOE), showed that the technology worked well for both coal and mineral applications. For the technology to be commercially successful, however, a full-scale demonstration of the MCF technology was deemed necessary. This report summarizes the results of work performed under the DOE project entitled In-plant Testing of Microbubble Column Flotation.'' The objectives of this research and development effort were to duplicate the bench-scale performance of the MCF process in a full-scale unit, to verify the scale-up procedure developed in an earlier project, and to demonstrate the applicability of the MCF technology to the coal industry.

  2. WASTE SOLIDIFICATION BUILDING BENCH SCALE HIGH ACTIVITY WASTE SIMULANT VARIABILITY STUDY FY2008

    Energy Technology Data Exchange (ETDEWEB)

    Hansen, E; Timothy Jones, T; Tommy Edwards, T; Alex Cozzi, A

    2009-03-20

    The primary objective of this task was to perform a variability study of the high activity waste (HAW) acidic feed to determine the impact of feed variability on the quality of the final grout and on the mixability of the salt solution into the dry powders. The HAW acidic feeds were processed through the neutralization/pH process, targeting a final pH of 12. These fluids were then blended with the dry materials to make the final waste forms. A secondary objective was to determine if elemental substitution for cost prohibitive or toxic elements in the simulant affects the mixing response, thus providing a more economical simulant for use in full scale tests. Though not an objective, the HAW simulant used in the full scale tests was also tested and compared to the results from this task. A statistically designed test matrix was developed based on the maximum molarity inputs used to make the acidic solutions. The maximum molarity inputs were: 7.39 HNO{sub 3}, 0.11618 gallium, 0.5423 silver, and 1.1032 'other' metals based on their NO{sub 3}{sup -} contribution. Substitution of the elements aluminum for gallium and copper for silver was also considered in this test matrix, resulting in a total of 40 tests. During the NaOH addition, the neutralization/pH adjustment process was controlled to a maximum temperature of 60 C. The neutralized/pH adjusted simulants were blended with Portland cement and zircon flour at a water to cement mass ratio of 0.30. The mass ratio of zircon flour to Portland cement was 1/12. The grout was made using a Hobart N-50 mixer running at low speed for two minutes to incorporate and properly wet the dry solids with liquid and at medium speed for five minutes for mixing. The resulting fresh grout was measured for three consecutive yield stress measurements. The cured grout was measured for set, bleed, and density. Given the conditions of preparing the grout in this task, all of the grouts were visually well mixed prior to preparing the

  3. In-situ biogas upgrading during anaerobic digestion of food waste amended with walnut shell biochar at bench scale.

    Science.gov (United States)

    Linville, Jessica L; Shen, Yanwen; Ignacio-de Leon, Patricia A; Schoene, Robin P; Urgun-Demirtas, Meltem

    2017-06-01

    A modified version of an in-situ CO 2 removal process was applied during anaerobic digestion of food waste with two types of walnut shell biochar at bench scale under batch operating mode. Compared with the coarse walnut shell biochar, the fine walnut shell biochar has a higher ash content (43 vs. 36 wt%) and higher concentrations of calcium (31 vs. 19 wt% of ash), magnesium (8.4 vs. 5.6 wt% of ash) and sodium (23.4 vs. 0.3 wt% of ash), but a lower potassium concentration (0.2 vs. 40% wt% of ash). The 0.96-3.83 g biochar (g VS added ) -1 fine walnut shell biochar amended digesters produced biogas with 77.5%-98.1% CH 4 content by removing 40%-96% of the CO 2 compared with the control digesters at mesophilic and thermophilic temperature conditions. In a direct comparison at 1.83 g biochar (g VS added ) -1 , the fine walnut shell biochar amended digesters (85.7% CH 4 content and 61% CO 2 removal) outperformed the coarse walnut shell biochar amended digesters (78.9% CH 4 content and 51% CO 2 removal). Biochar addition also increased alkalinity as CaCO 3 from 2800 mg L -1 in the control digesters to 4800-6800 mg L -1 , providing process stability for food waste anaerobic digestion.

  4. PNNL Report on the Development of Bench-scale CFD Simulations for Gas Absorption across a Wetted Wall Column

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Chao; Xu, Zhijie; Lai, Canhai; Whyatt, Greg A.; Marcy, Peter; Gattiker, J. R.; Sun, Xin

    2016-05-01

    This report is prepared for the demonstration of hierarchical prediction of carbon capture efficiency of a solvent-based absorption column. A computational fluid dynamics (CFD) model is first developed to simulate the core phenomena of solvent-based carbon capture, i.e., the CO2 physical absorption and chemical reaction, on a simplified geometry of wetted wall column (WWC) at bench scale. Aqueous solutions of ethanolamine (MEA) are commonly selected as a CO2 stream scrubbing liquid. CO2 is captured by both physical and chemical absorption using highly CO2 soluble and reactive solvent, MEA, during the scrubbing process. In order to provide confidence bound on the computational predictions of this complex engineering system, a hierarchical calibration and validation framework is proposed. The overall goal of this effort is to provide a mechanism-based predictive framework with confidence bound for overall mass transfer coefficient of the wetted wall column (WWC) with statistical analyses of the corresponding WWC experiments with increasing physical complexity.

  5. Bench scale synthesis of p-hydroxybenzoic acid using whole-cell nitrilase of Gordonia terrae mutant E9.

    Science.gov (United States)

    Kumar, Vijay; Kumar, Virender; Thakur, Neerja; Bhalla, Tek Chand

    2015-07-01

    Mutants of Gordonia terrae were generated using chemical mutagens for better activity, stability and higher substrate/product tolerance of its nitrilase enzyme. Mutant E9 showed two-time increase in activity and tolerated p-hydroxybenzonitrile (p-HBN) up to 50 mM. Response surface methodology and inducer mediation approach further enhanced the production of enzyme to 2.5-fold. The bench scale production of p-hydroxybenzoic acid (p-HBA) was carried out in a fed-batch reaction (500-mL scale) using whole-cell nitrilase of mutant E9 in 0.1 M potassium phosphate buffer (pH 8.0) at 40 °C. Total six feedings each at an interval of 45 min resulted in accumulation of 360 mM (21.6 g) of p-HBA with a purity of 99%. The catalytic and volumetric productivity of bioprocess using mutant G. terrae was improved to 1.8 g h(-1) g DCW (-1) and 43.2 g L(-1), respectively, from 0.78 g h(-1) g DCW (-1) and 28.8 g L(-1) using resting cells of wild strain. K m and V max of purified nitrilase from mutant E9 were 55 U mg(-1) and 1.8 mM for p-HBN with a higher turnover number of 36 s(-1) × 10(-3).

  6. Modeling a bench-scale alternating aerobic/anoxic activated sludge system for nitrogen removal using a modified ASM1.

    Science.gov (United States)

    Kim, Hyunook; Noh, Soohong; Colosimo, Mark

    2009-07-01

    The Activated Sludge Model No. 1 (ASM1), developed by The International Association of Water Pollution Research and Control, was applied to model dynamics of NH4+, and NO3- in a bench scale alternating aerobic-anoxic (AAA) activated sludge system for nitrogen removal. The model was modified by eliminating inert soluble COD (S(I)) and inert particulate COD (X(I)) from the model's state variables as these two variables are not involved in any biological reaction and are not readily measurable with conventional routine COD analysis. It was assumed that the soluble COD and particulate COD of wastewater represent readily biodegradable COD (S(S)) and slowly biodegradable (X(S)) in the model, respectively. In addition, alkalinity was also removed from the model, since alkalinity of an AAA system remains stable due to the cyclic modes of the system. Even with the elimination of the three state variables and the assumption made, the model could reasonably predict the NH4+ and NO3- dynamics of the AAA system, and effluent NH4+ and NO3- concentrations with adjustment of only a few kinetic parameters. Compared to the original ASM1, it is expected that the modified ASM1 presented in this study can be more easily utilized by engineers in designing or operating an AAA system in practice, since it requires simple characterization of wastewater COD.

  7. 15N NMR investigation of the reduction and binding of TNT in an aerobic bench scale reactor simulating windrow composting

    Science.gov (United States)

    Thorn, K.A.; Pennington, J.C.; Hayes, C.A.

    2002-01-01

    T15NT was added to a soil of low organic carbon content and composted for 20 days in an aerobic bench scale reactor. The finished whole compost and fulvic acid, humic acid, humin, and lignocellulose fractions extracted from the compost were analyzed by solid-state CP/MAS and DP/MAS 15N NMR. 15N NMR spectra provided direct spectroscopic evidence for reduction of TNT followed by covalent binding of the reduced metabolites to organic matter of the composted soil, with the majority of metabolite found in the lignocellulose fraction, by mass also the major fraction of the compost. In general, the types of bonds formed between soil organic matter and reduced TNT amines in controlled laboratory reactions were observed in the spectra of the whole compost and fractions, confirming that during composting TNT is reduced to amines that form covalent bonds with organic matter through aminohydroquinone, aminoquinone, heterocyclic, and imine linkages, among others. Concentrations of imine nitrogens in the compost spectra suggestthat covalent binding bythe diamines 2,4DANT and 2,6DANT is a significant process in the transformation of TNT into bound residues. Liquid-phase 15N NMR spectra of the fulvic acid and humin fractions provided possible evidence for involvement of phenoloxidase enzymes in covalent bond formation.

  8. Production of uranium hexafluoride by the catalysed fluorox process: pilot plant and supporting bench-scale studies

    International Nuclear Information System (INIS)

    Janov, J.; Charlton, B.G.; LePage, A.H.; Vilkaitis, V.K.

    1982-04-01

    The feasibility of producing UF 6 by the catalysed reaction of UF 4 with oxygen (the Fluorox process) was investigated in a 150 mm diameter fluidised bed reactor and in supporting bench-scale experiments. The rate of the Fluorox reaction in batch experiments was increased by an order of magnitude with 1 to 5 per cent catalyst (containing 3 to 4 per cent platinum on alumina). The maximum UF 6 production rate at 650 deg. C was 0.9 kg h -1 . However, the platinum catalyst was completely poisoned after production of only 1 and 20 kg UF 6 per kg of catalyst when using respectively French and British UF 4 . Regeneration of the catalyst was demonstrated to be technically feasible by washing with water or ammonium oxalate solution or treating with hydrogen and hydrogen fluoride at 350-650 deg. C. However, since the very fast rate of poisoning would necessitate higher catalyst concentrations and/or frequent regeneration, the catalysed Fluorox process in unlikely to be economically competitive with the direct fluorination of UF 4

  9. Bench-scale study of active mine water treatment using cement kiln dust (CKD) as a neutralization agent.

    Science.gov (United States)

    Mackie, Allison L; Walsh, Margaret E

    2012-02-01

    The overall objective of this study was to investigate the potential impact on settled water quality of using cement kiln dust (CKD), a waste by-product, to replace quicklime in the active treatment of acidic mine water. Bench-scale experiments were conducted to evaluate the treatment performance of calcium hydroxide (Ca(OH)(2)) slurries generated using four different CKD samples compared to a control treatment with quicklime (CaO) in terms of reducing acidity and metals concentrations in acid mine drainage (AMD) samples taken from the effluent of a lead/zinc mine in Atlantic Canada. Results of the study showed that all of the CKD samples evaluated were capable of achieving greater than 97% removal of total zinc and iron. The amount of solid alkaline material required to achieve pH targets required for neutralization of the AMD was found to be higher for treatment with the CKD slurries compared to the quicklime slurry control experiments, and varied linearly with the free lime content of the CKD. The results of this study also showed that a potential benefit of treating mine water with CKD could be reduced settled sludge volumes generated in the active treatment process, and further research into the characteristics of the sludge generated from the use of CKD-generated calcium hydroxide slurries is recommended. Copyright © 2011 Elsevier Ltd. All rights reserved.

  10. Bench-scale study of the effect of phosphate on an aerobic iron oxidation plant for mine water treatment.

    Science.gov (United States)

    Tischler, Judith S; Wiacek, Claudia; Janneck, Eberhard; Schlömann, Michael

    2014-01-01

    At the opencast pit Nochten acidic iron- and sulfate-rich mine waters are treated biotechnologically in a mine-water treatment plant by microbial iron oxidation. Due to the low phosphate concentration in such waters the treatment plant was simulated in bench-scale to investigate the influence of addition of potassium dihydrogen phosphate on chemical and biological parameters of the mine-water treatment. As a result of the phosphate addition the number of cells increased, which resulted in an increase of the iron oxidation rate in the reactor with phosphate addition by a factor of 1.7 compared to a reference approach without phosphate addition. Terminal restriction fragment length polymorphism (T-RFLP) analysis during the cultivation revealed a shift of the microbial community depending on the phosphate addition. While almost exclusively iron-oxidizing bacteria related to "Ferrovum" sp. were detected with phosphate addition, the microbial community was more diverse without phosphate addition. In the latter case, iron-oxidizing bacteria ("Ferrovum" sp., Acidithiobacillus spp.) as well as non-iron-oxidizing bacteria (Acidiphilium sp.) were identified. Copyright © 2013 Elsevier Ltd. All rights reserved.

  11. Thermochemical water-splitting cycle, bench-scale investigations, and process engineering. Final report, February 1977-December 31, 1981

    Energy Technology Data Exchange (ETDEWEB)

    Norman, J.H.; Besenbruch, G.E.; Brown, L.C.; O' Keefe, D.R.; Allen, C.L.

    1982-05-01

    The sulfur-iodine water-splitting cycle is characterized by the following three reactions: 2H/sub 2/O + SO/sub 2/ + I/sub 2/ ..-->.. H/sub 2/SO/sub 4/ + 2HI; H/sub 2/SO/sub 4/ ..-->.. H/sub 2/O + SO/sub 2/ + 1/2 O/sub 2/; and 2HI ..-->.. H/sub 2/ + I/sub 2/. This cycle was developed at General Atomic after several critical features in the above reactions were discovered. These involved phase separations, catalytic reactions, etc. Estimates of the energy efficiency of this economically reasonable advanced state-of-the-art processing unit produced sufficiently high values (to approx.47%) to warrant cycle development effort. The DOE contract was largely directed toward the engineering development of this cycle, including a small demonstration unit (CLCD), a bench-scale unit, engineering design, and costing. The work has resulted in a design that is projected to produce H/sub 2/ at prices not yet generally competitive with fossil-fuel-produced H/sub 2/ but are projected to be favorably competitive with respect to H/sub 2/ from fossil fuels in the future.

  12. Dynamics of bacterial populations during bench-scale bioremediation of oily seawater and desert soil bioaugmented with coastal microbial mats.

    Science.gov (United States)

    Ali, Nidaa; Dashti, Narjes; Salamah, Samar; Sorkhoh, Naser; Al-Awadhi, Husain; Radwan, Samir

    2016-03-01

    This study describes a bench-scale attempt to bioremediate Kuwaiti, oily water and soil samples through bioaugmentation with coastal microbial mats rich in hydrocarbonoclastic bacterioflora. Seawater and desert soil samples were artificially polluted with 1% weathered oil, and bioaugmented with microbial mat suspensions. Oil removal and microbial community dynamics were monitored. In batch cultures, oil removal was more effective in soil than in seawater. Hydrocarbonoclastic bacteria associated with mat samples colonized soil more readily than seawater. The predominant oil degrading bacterium in seawater batches was the autochthonous seawater species Marinobacter hydrocarbonoclasticus. The main oil degraders in the inoculated soil samples, on the other hand, were a mixture of the autochthonous mat and desert soil bacteria; Xanthobacter tagetidis, Pseudomonas geniculata, Olivibacter ginsengisoli and others. More bacterial diversity prevailed in seawater during continuous than batch bioremediation. Out of seven hydrocarbonoclastic bacterial species isolated from those cultures, only one, Mycobacterium chlorophenolicum, was of mat origin. This result too confirms that most of the autochthonous mat bacteria failed to colonize seawater. Also culture-independent analysis of seawater from continuous cultures revealed high-bacterial diversity. Many of the bacteria belonged to the Alphaproteobacteria, Flavobacteria and Gammaproteobacteria, and were hydrocarbonoclastic. Optimal biostimulation practices for continuous culture bioremediation of seawater via mat bioaugmentation were adding the highest possible oil concentration as one lot in the beginning of bioremediation, addition of vitamins, and slowing down the seawater flow rate. © 2016 The Author. Microbial Biotechnology published by John Wiley & Sons Ltd and Society for Applied Microbiology.

  13. 40 CFR 1033.315 - Test procedures.

    Science.gov (United States)

    2010-07-01

    ... establish a Green Engine Factor for each regulated pollutant for each engine family, instead of (or in... obtain our approval prior to using a Green Engine Factor. For catalyst-equipped locomotives, you may... test procedures other than those in subpart F of this part during certification for the engine family...

  14. Copper recovery in a bench-scale carrier facilitated tubular supported liquid membrane system

    Directory of Open Access Journals (Sweden)

    Makaka S.

    2010-01-01

    Full Text Available The extraction of copper ions in a tubular supported liquid membrane using LIX 984NC as a mobile carrier was studied, evaluating the effect of the feed characteristics (flowrate, density, viscosity on the feedside laminar layer of the membrane. A vertical countercurrent, double pipe perspex benchscale reactor consisting of a single hydrophobic PVDF tubular membrane mounted inside was used in all test work. The membrane was impregnated with LIX 984NC and became the support for this organic transport medium. Dilute Copper solution passed through the centre pipe and sulphuric acid as strippant passed through the shell side. Copper was successfully transported from the feedside to the stripside and from the data obtained, a relationship between Schmidt, Reynolds and Sherwood number was achieved of.

  15. EFRT M-12 Issue Resolution: Comparison of PEP and Bench-Scale Oxidative Leaching Results

    Energy Technology Data Exchange (ETDEWEB)

    Rapko, Brian M.; Schonewill, Philip P.; Brown, Christopher F.; Eslinger, Paul W.; Fountain, Matthew S.; Hausmann, Tom S.; Huckaby, James L.; Hanson, Brady D.; Kurath, Dean E.; Minette, Michael J.

    2010-01-01

    Pacific Northwest National Laboratory (PNNL) has been tasked by Bechtel National Inc. (BNI) on the River Protection Project-Hanford Tank Waste Treatment and Immobilization Plant (RPP-WTP) project to perform research and development activities to resolve technical issues identified for the Pretreatment Facility (PTF). The Pretreatment Engineering Platform (PEP) was designed, constructed, and operated as part of a plan to respond to issue M12, “Undemonstrated Leaching Processes” of the External Flowsheet Review Team (EFRT) issue response plan.( ) The PEP is a 1/4.5-scale test platform designed to simulate the WTP pretreatment caustic leaching, oxidative leaching, ultrafiltration solids concentration, and slurry washing processes. The PEP replicates the WTP leaching processes using prototypic equipment and control strategies. The PEP also includes non-prototypic ancillary equipment to support the core processing.

  16. Bench-Scale and Pilot-Scale Treatment Technologies for the ...

    Science.gov (United States)

    Coal mine water (CMW) is typically treated to remove suspended solids, acidity, and soluble metals, but high concentrations of total dissolved solids (TDS) have been reported to impact the environment at several CMW discharge points. Consequently, various states have established TDS wastewater regulations and the US EPA has proposed a benchmark conductivity limit to reduce TDS impacts in streams near mining sites. Traditional CMW treatment effectively removes some TDS components, but is not effective in removing major salt ions due to their higher solubility. This paper describes the basic principles, effectiveness, advantages and disadvantages of various TDS removal technologies (adsorption, bioremediation, capacitive deionization, desalination, electro-chemical ion exchange, electrocoagulation, electrodialysis, ion exchange, membrane filtration, precipitation, and reverse osmosis) that have at least been tested in bench- and pilot-scale experiments. Recent discussions about new regulations to include total dissolved solids TDS) limits would propel interest in the TDS removal technologies focused on coal mine water. TDS removal is not a new concept and has been developed using different technologies for a number of applications, but coal mine water has unique characteristics (depending on the site, mining process, and solid-water-oxygen interactions), which make it unlikely to have a single technology predominating over others. What are some novel technolog

  17. Acceptance test procedure for core sample trucks

    International Nuclear Information System (INIS)

    Smalley, J.L.

    1995-01-01

    The purpose of this Acceptance Test Procedure is to provide instruction and documentation for acceptance testing of the rotary mode core sample trucks, HO-68K-4600 and HO-68K-4647. The rotary mode core sample trucks were based upon the design of the second core sample truck (HO-68K-4345) which was constructed to implement rotary mode sampling of the waste tanks at Hanford. Acceptance testing of the rotary mode core sample trucks will verify that the design requirements have been met. All testing will be non-radioactive and stand-in materials shall be used to simulate waste tank conditions. Compressed air will be substituted for nitrogen during the majority of testing, with nitrogen being used only for flow characterization

  18. Uncertainty Quantification Analysis of Both Experimental and CFD Simulation Data of a Bench-scale Fluidized Bed Gasifier

    Energy Technology Data Exchange (ETDEWEB)

    Shahnam, Mehrdad [National Energy Technology Lab. (NETL), Morgantown, WV (United States). Research and Innovation Center, Energy Conversion Engineering Directorate; Gel, Aytekin [ALPEMI Consulting, LLC, Phoeniz, AZ (United States); Subramaniyan, Arun K. [GE Global Research Center, Niskayuna, NY (United States); Musser, Jordan [National Energy Technology Lab. (NETL), Morgantown, WV (United States). Research and Innovation Center, Energy Conversion Engineering Directorate; Dietiker, Jean-Francois [West Virginia Univ. Research Corporation, Morgantown, WV (United States)

    2017-10-02

    Adequate assessment of the uncertainties in modeling and simulation is becoming an integral part of the simulation based engineering design. The goal of this study is to demonstrate the application of non-intrusive Bayesian uncertainty quantification (UQ) methodology in multiphase (gas-solid) flows with experimental and simulation data, as part of our research efforts to determine the most suited approach for UQ of a bench scale fluidized bed gasifier. UQ analysis was first performed on the available experimental data. Global sensitivity analysis performed as part of the UQ analysis shows that among the three operating factors, steam to oxygen ratio has the most influence on syngas composition in the bench-scale gasifier experiments. An analysis for forward propagation of uncertainties was performed and results show that an increase in steam to oxygen ratio leads to an increase in H2 mole fraction and a decrease in CO mole fraction. These findings are in agreement with the ANOVA analysis performed in the reference experimental study. Another contribution in addition to the UQ analysis is the optimization-based approach to guide to identify next best set of additional experimental samples, should the possibility arise for additional experiments. Hence, the surrogate models constructed as part of the UQ analysis is employed to improve the information gain and make incremental recommendation, should the possibility to add more experiments arise. In the second step, series of simulations were carried out with the open-source computational fluid dynamics software MFiX to reproduce the experimental conditions, where three operating factors, i.e., coal flow rate, coal particle diameter, and steam-to-oxygen ratio, were systematically varied to understand their effect on the syngas composition. Bayesian UQ analysis was performed on the numerical results. As part of Bayesian UQ analysis, a global sensitivity analysis was performed based on the simulation results, which shows

  19. Effect of temperature downshifts on a bench-scale hybrid A/O system: Process performance and microbial community dynamics.

    Science.gov (United States)

    Zhou, Hexi; Li, Xiangkun; Chu, Zhaorui; Zhang, Jie

    2016-06-01

    Effect of temperature downshifts on process performance and bacterial community dynamics was investigated in a bench-scale hybrid A/O system treating real domestic wastewater. Results showed that the average COD removal in this system reached 90.5%, 89.1% and 90.3% for Run 1 (25 °C), Run 2 (15 °C) and Run 3 (10 °C), respectively, and variations in temperature barely affected the effluent COD concentration. The average removal efficiencies of NH4(+)-N were 98.4%, 97.8%, 95.7%, and that of TN were 77.1%, 61.8%, 72% at 25 °C, 15 °C and 10 °C, respectively. Although the hybrid system was subjected to low temperature, this process effectively removed NH4(+)-N and TN even at 10 °C with the average effluent concentrations of 2.4 mg/L and 14.3 mg/L, respectively. Results from high-throughput sequencing analysis revealed that when the operation temperature decreased from 25 °C to 10 °C, the richness and diversity indexes of the system decreased in the sludge samples, while underwent an increase in the biofilm samples. Furthermore, the major heterotrophic bacteria consisted of Lewinella, Lutimonas, Chitinophaga and Fluviicola at 10 °C, which could be central to effective COD removal at low temperature. Additionally, Azospira, one denitrifying-related genus increased from 0.4% to 4.45% in the biofilm samples, with a stable TN removal in response to temperature downshifts. Nitrosomonas and Nitrospira increased significantly in the biofilm samples, implying that the attached biofilm contributed to more nitrification at low temperature. Copyright © 2016 Elsevier Ltd. All rights reserved.

  20. Destruction of hazardous and mixed wastes using mediated electrochemical oxidation in a Ag(II)HNO3 bench scale system

    International Nuclear Information System (INIS)

    Balazs, B.; Chiba, Z.; Hsu, P.; Lewis, P.; Murguia, L.; Adamson, M.

    1997-01-01

    Mediated Electrochemical Oxidation (MEO) is a promising technology for the destruction of organic containing wastes and the remediation of mixed wastes containing transuranic components. The combination of a powerful oxidant and an acid solution allows the conversion of nearly all organics, whether present in hazardous or in mixed waste, to carbon dioxide. Insoluble transuranics are dissolved in this process and may be recovered by separation and precipitation.The MEO technique offers several advantages which are inherent in the system. First, the oxidation/dissolution processes are accomplished at near ambient pressures and temperatures (30-70 degrees C). Second, all waste stream components and oxidation products (with the exception of evolved gases) are contained in an aqueous environment. This electrolyte acts as an accumulator for inorganics which were present in the original waste stream, and the large volume of electrolyte provides a thermal buffer for the energy released during oxidation of the organics. Third, the generation of secondary waste is minimal, as the process needs no additional reagents. Finally, the entire process can be shut down by simply turning off the power, affording a level of control unavailable in some other techniques.Numerous groups, both in the United States and Europe, have made substantial progress in the last decade towards understanding the mechanistic pathways, kinetics, and engineering aspects of the process. At Lawrence Livermore National Laboratory, substantial contributions have been made to this knowledge base in these areas and others. Conceptual design and engineering development have been completed for a pilot plant-scale MEO system, and numerous data have been gathered on the efficacy of the process for a wide variety of anticipated waste components. This presentation will review the data collected at LLNL for a bench scale system based primarily on the use of a Ag(II) mediator in a nitric acid electrolyte; results

  1. Hydrogen generation from bioethanol reforming : bench-scale unit performance with Cu/Nb2O5 catalyst

    Energy Technology Data Exchange (ETDEWEB)

    Machado, N.R.C.F.; Rizzo, R.C.P.; Calsavara, V.; Takahashi, F.; Almeida, A.A.; Melo, F.R. de; Zschornack, M.A.; Bessani, A.N.; Rodrigues, R.M.O. [State University of Maringa, Maringa (Brazil). Dept. of Chemical Engineering Lab. of Catalysis; Schmal, M. [Cidade Universitaria, Rio de Janeiro (Brazil). Centro de Tecnologia, Graduate School and Research in Engineering Alberto Luiz Coimbra Institute; Cantao, M.P. [Institute of Technology for Development, Curitiba (Brazil). Dept. of Materials

    2003-07-01

    A series of experiments have been conducted to produce hydrogen from ethanol reforming. This paper presents the bench-scale study unit that uses a 5 per cent copper-niobium2oxygen5 (Cu/Nb2O5) catalyst previously selected in a micro reactor. X-ray diffraction analysis revealed that the catalyst contained copper oxide in an amorphous form and that the Nb2O5 was highly crystalline. The calcinated catalyst was analysed with X-ray photoelectron spectroscopy and showed that 35 per cent of total copper was on the surface as Cu{sup I} (55 per cent) and Cu{sup II} (45 per cent). The surface area was mainly comprised of meso and macro pores. There was a two-step reduction of Cu{sup II} to Cu at 245 and 306 degrees C, as shown by temperature programmed reduction, as well as a 6 per cent reduction of Nb2O5. An internal reactor with 16 grams (g) of catalyst pellets was contained in the reaction unit. To optimize hydrogen production, reaction temperature and feed rate were varied, and the major by-product was carbon dioxide. Reagents (water and ethanol) were fed into and vaporized in, an electric pre-heater in stoichiometric proportion. Mean conversion increased from 17 per cent to 35 per cent through an increase of reaction temperature from 300 to 400 degrees C. Minor by-products were detected in the form of ethene and ethyl ether. 9 refs., 3 tabs., 4 figs.

  2. Archaeal and bacterial community dynamics and bioprocess performance of a bench-scale two-stage anaerobic digester.

    Science.gov (United States)

    Gonzalez-Martinez, Alejandro; Garcia-Ruiz, Maria Jesus; Rodriguez-Sanchez, Alejandro; Osorio, Francisco; Gonzalez-Lopez, Jesus

    2016-07-01

    Two-stage technologies have been developed for anaerobic digestion of waste-activated sludge. In this study, the archaeal and bacterial community structure dynamics and bioprocess performance of a bench-scale two-stage anaerobic digester treating urban sewage sludge have been studied by the means of high-throughput sequencing techniques and physicochemical parameters such as pH, dried sludge, volatile dried sludge, acid concentration, alkalinity, and biogas generation. The coupled analyses of archaeal and bacterial communities and physicochemical parameters showed a direct relationship between archaeal and bacterial populations and bioprocess performance during start-up and working operation of a two-stage anaerobic digester. Moreover, results demonstrated that archaeal and bacterial community structure was affected by changes in the acid/alkalinity ratio in the bioprocess. Thus, a predominance of the acetoclastic methanogen Methanosaeta was observed in the methanogenic bioreactor at high-value acid/alkaline ratio, while a predominance of Methanomassilicoccaeceae archaea and Methanoculleus genus was observed in the methanogenic bioreactor at low-value acid/alkaline ratio. Biodiversity tag-iTag sequencing studies showed that methanogenic archaea can be also detected in the acidogenic bioreactor, although its biological activity was decreased after 4 months of operation as supported by physicochemical analyses. Also, studies of the VFA producers and VFA consumers microbial populations showed as these microbiota were directly affected by the physicochemical parameters generated in the bioreactors. We suggest that the results obtained in our study could be useful for future implementations of two-stage anaerobic digestion processes at both bench- and full-scale.

  3. Experimental investigation of pyrolysis of rice straw using bench-scale auger, batch and fluidized bed reactors

    International Nuclear Information System (INIS)

    Nam, Hyungseok; Capareda, Sergio C.; Ashwath, Nanjappa; Kongkasawan, Jinjuta

    2015-01-01

    Energy conversion efficiencies of three pyrolysis reactors (bench-scale auger, batch, and fluidized bed) were investigated using rice straw as the feedstock at a temperature of 500 °C. The highest bio-oil yield of 43% was obtained from the fluidized bed reactor, while the maximum bio-char yield of 48% was obtained from the batch reactor. Similar bio-oil yields were obtained from the auger and batch type reactors. The GCMS and FTIR were used to evaluate the liquid products from all reactors. The best quality bio-oil and bio-char from the batch reactor was determined to have a heating value of 31 MJ/kg and 19 MJ/kg, respectively. The highest alkali mineral was found in the bio-char produced from the auger reactor. The energy conversion efficiencies of the three reactors indicated that the majority of the energy (50–64%) was in the bio-char products from the auger and batch reactors, while the bio-oil from the fluidized bed reactor contained the highest energy (47%). A Sankey diagram has been produced to show the flows of product energy from each pyrolysis process. The result will help determine which conversion process would be optimal for producing specific products of bio-char, bio-oil, and gas depending on the needs. - Highlights: • Pyrolysis products from auger, batch, and fluidized bed reactor were examined. • O/C ratios of bio-oils stayed in specific ranges depending on the process reactors. • The largest quantity of bio-oil from fluidized, while the best quality from batch. • The highest alkali concentration of 37 g/kg included in the auger based bio-char. • Sankey diagram was used to understand the energy distribution from reactors.

  4. 118-B-1 excavation treatability test procedures

    International Nuclear Information System (INIS)

    Frain, J.M.

    1994-01-01

    This treatability study has two purposes: to support development of the approach to be used for burial ground remediation, and to provide specific engineering information for the design of burial grounds receiving waste generated from the 100 Area removal actions. Data generated from this test will also provide performance and cost information necessary for detailed analysis of alternatives for burial ground remediation. Further details on the test requirements, milestones and data quality objectives are described in detail in the 118-B-1 Excavation Treatability Test Plan (DOE/RL-94-43). These working procedures are intended for use by field personnel to implement the requirements of the milestone. A copy of the detailed Test Plan will be kept on file at the on-site field support trailer, and will be available for review by field personnel

  5. 118-B-1 excavation treatability test procedures

    Energy Technology Data Exchange (ETDEWEB)

    Frain, J.M.

    1994-08-01

    This treatability study has two purposes: to support development of the approach to be used for burial ground remediation, and to provide specific engineering information for the design of burial grounds receiving waste generated from the 100 Area removal actions. Data generated from this test will also provide performance and cost information necessary for detailed analysis of alternatives for burial ground remediation. Further details on the test requirements, milestones and data quality objectives are described in detail in the 118-B-1 Excavation Treatability Test Plan (DOE/RL-94-43). These working procedures are intended for use by field personnel to implement the requirements of the milestone. A copy of the detailed Test Plan will be kept on file at the on-site field support trailer, and will be available for review by field personnel.

  6. Dispersant testing : a study on analytical test procedures

    International Nuclear Information System (INIS)

    Fingas, M.F.; Fieldhouse, B.; Wang, Z.; Environment Canada, Ottawa, ON

    2004-01-01

    Crude oil is a complex mixture of hydrocarbons, ranging from small, volatile compounds to very large, non-volatile compounds. Analysis of the dispersed oil is crucial. This paper described Environment Canada's ongoing studies on various traits of dispersants. In particular, it describes small studies related to dispersant effectiveness and methods to improve analytical procedures. The study also re-evaluated the analytical procedure for the Swirling Flask Test, which is now part of the ASTM standard procedure. There are new and improved methods for analyzing oil-in-water using gas chromatography (GC). The methods could be further enhanced by integrating the entire chromatogram rather than just peaks. This would result in a decrease in maximum variation from 5 per cent to about 2 per cent. For oil-dispersant studies, the surfactant-dispersed oil hydrocarbons consist of two parts: GC-resolved hydrocarbons and GC-unresolved hydrocarbons. This study also tested a second feature of the Swirling Flask Test in which the side spout was tested and compared with a new vessel with a septum port instead of a side spout. This decreased the variability as well as the energy and mixing in the vessel. Rather than being a variation of the Swirling Flask Test, it was suggested that a spoutless vessel might be considered as a completely separate test. 7 refs., 2 tabs., 4 figs

  7. Some Remarks on Foundation Pile Testing Procedures

    Science.gov (United States)

    Rybak, Jarosław

    2017-10-01

    This work presents the review of pile capacity testing techniques. In an overview, the key points in pile designing are: determination of the appropriate computational schemes, reliable data on loads and the properties of structural materials (in particular, of the soil mass, which is marked by the greatest variability). The procedure of constructing a pile foundation should include: carrying out soil tests in the scope that ensures safe designing, selecting a piling technology that is relevant both to geotechnical conditions and expected loads, drafting a piling design together with the design of load tests, setting up a testing station for further load tests, static and/or dynamic tests of pile load capacity, preceded by supplementary soil tests when the conditions of test pile installation fail to comply with the design assumptions or when the pile length exceeds the depth of the previously investigated soil, making documentation of load capacity tests (with an additional correction of the piling design), the actual piling (ongoing analysis of pile driving logs and, if necessary, testing the piles’ integrity), drawing up the as-built documentation. Unfortunately, the design is corrected after the load test have been conducted only if the piles fail to show the designed bearing capacity. The designer is then obliged to revise the design assumptions on the basis of tests results. If the test results account for the a greater bearing capacity than necessary and it would be recommendable to limit the extent of the planned (i.e. set out in the contract) piling works, usually neither the contractor nor the designer, nor even the Construction Site Supervisor, acting for the benefit of the Investor, are willing to take on the responsibility for reducing the scope of the piling works. The necessity of conducting additional control tests before and during the implementation of the construction project is often treated by the investors as an attempt at extorting extra

  8. Report on COTECH test procedure and characterization techniques

    DEFF Research Database (Denmark)

    Islam, Mohammad Aminul

    .Characterization techniques and test procedure requirements for innovative self-ligating dental brackets (EO) Section 5.Characterization techniques and test procedure requirements for smart diagnostic chips comprising a microfluidic channel system (GBO) Section 6.Characterization techniques and test procedure...... requirements for multifunctional integrated lighting rear lamp for cars (CRP) Section 7.Characterization techniques and test procedure requirements for micro-fresnel lenses for cell phone flash lights (HEPTAGON) Section 8.Characterization techniques and test procedure requirements for 5 Pin Ric Connector...

  9. The effects of physical separtation treatment on the removal of uranium from contaminated soils at Fernald: A bench-scale study

    International Nuclear Information System (INIS)

    Sadler, K.G.; Krstich, M.A.

    1994-01-01

    A bench-scale treatability study incorporating the use of physical separation techniques and chemical dispersants/extractants was conducted on uranium contaminated soils at the Fernald Environmental Management Project (FEMP) site. The soils contained approximately 497 and 450 milligrams per kilogram (mg/kg) of total uranium, respectively. Geotechnical characterization indicated that 77.4 and 74.6 percent of the soil was in the less that 50 micrometer (μm) size fraction for the ID-A and ID-B soils, respectively. An initial characterization effort indicated that uranium was distributed among all particle size fractions. After each soil was dispersed in water, it was noted that the uranium concentrated in the sand and clay fractions for the ID-A soil (1028 and 1475 mg kg -1 , respectively) and the clay fraction for ID-B soil (2710 mg kg -1 ). Four 1 millimolar (mM) sodium reagent solutions (sodium hydroxide, sodium carbonate, sodium bicarbonate, and a sodium citrate-bicarbonate-dithionite mixture) and potable water were evaluated for effectiveness in dispersing each soil into single grain separates and extracting total uranium from each of the resulting particle size fractions. Dilute sodium solutions were more effective than water in dispersing the soil. The use of dispersants, as compared to water, on the less than 2 mm size fraction causes a shift in the distribution of uranium out of the sand fraction and into the silt and clay fractions for ID-A soil and into the clay fraction for the ID-B soil. Attrition scrubbing tests were conducted on the less than 2 mm size fraction for the ID-A and ID-B soils using water and three alkaline extraction solutions, sodium pyrophosphate, sodium carbonate/bicarbonate, and ammonium carbonate/bicarbonate. There was little difference among the chemical extractants on their effectiveness in removing uranium from the greater than 53 μm (sand) or less than 53 μm (silt and clay) soil fraction

  10. Removal of uranium from uranium-contaminated soils -- Phase 1: Bench-scale testing. Uranium in Soils Integrated Demonstration

    Energy Technology Data Exchange (ETDEWEB)

    Francis, C. W.

    1993-09-01

    To address the management of uranium-contaminated soils at Fernald and other DOE sites, the DOE Office of Technology Development formed the Uranium in Soils Integrated Demonstration (USID) program. The USID has five major tasks. These include the development and demonstration of technologies that are able to (1) characterize the uranium in soil, (2) decontaminate or remove uranium from the soil, (3) treat the soil and dispose of any waste, (4) establish performance assessments, and (5) meet necessary state and federal regulations. This report deals with soil decontamination or removal of uranium from contaminated soils. The report was compiled by the USID task group that addresses soil decontamination; includes data from projects under the management of four DOE facilities [Argonne National Laboratory (ANL), Los Alamos National Laboratory (LANL), Oak Ridge National Laboratory (ORNL), and the Savannah River Plant (SRP)]; and consists of four separate reports written by staff at these facilities. The fundamental goal of the soil decontamination task group has been the selective extraction/leaching or removal of uranium from soil faster, cheaper, and safer than current conventional technologies. The objective is to selectively remove uranium from soil without seriously degrading the soil`s physicochemical characteristics or generating waste forms that are difficult to manage and/or dispose of. Emphasis in research was placed more strongly on chemical extraction techniques than physical extraction techniques.

  11. Waste acid detoxification and reclamation: Summary of bench-scale tests for FY 1986 and FY 1987

    Energy Technology Data Exchange (ETDEWEB)

    Stewart, T.L.

    1987-09-01

    Processes to reduce the volume, quantity, and toxicity of metal-bearing waste acid are being demonstrated at Pacific Northwest Laboratory. Two precipitation processes and a distillation process are being developed to minimize waste from fuel fabrication operations, which comprise a series of metal-finishing operations. Waste process acids such as HF-HNO/sub 3/, etch solutions containing Zr as a major metal impurity, and HNO/sub 3/ strip solution containing Cu as a major metal impurity are detoxified and reclaimed by concurrently precipitating heavy metals and regenerating acid for recycle. Acid from a third waste acid stream generated from chemical milling operations will be reclaimed using distillation. This stream comprises HNO/sub 3/ and H/sub 2/SO/sub 4/ containing U as the major metal impurity. Distillation allows NO/sub 3//sup -/ to be displaced by SO/sub 4//sup -2/ in metal salts; free HNO/sub 3/ is then vaporized from the U-bearing sulfate stream. Uranium can be recovered from the sulfate stream in a downstream precipitation step. 10 refs., 15 figs., 13 tabs.

  12. Operator coil monitoring Acceptance Test Procedure

    International Nuclear Information System (INIS)

    Erhart, M.F.

    1995-01-01

    The readiness of the Data Acquisition and Control System (DACS) to provide monitoring and control of the Programmable Logic Controller (PLC) abort coils from the Master and RSS stations will be systematically tested during performance of this procedure. It should be noted that these are not physical abort coils but software coils controlled by the software's ladder logic. The readiness of the DACS to properly interface with the ENRAF wire level gauge installed in the SY-101 storage tank will also be tested. During this test, a verification of all abort coil indications will be conducted at the DACS Development Facility in the 306E Building by injecting an input signal for each DACS sensor that has an associated abort coil until the abort coil actuates, and then ensuring that the status of the abort coil indicated at the Master and RSS stations is correct. Each abort coil will also be tested to ensure that the ''ENABLE'' and ''DISABLE'' controls from the Master and RSS stations function correctly, and only with the use of proper passwords

  13. TMACS Test Procedure TP008: SACS Interface. Revision 5

    International Nuclear Information System (INIS)

    Washburn, S.J.

    1994-01-01

    The TMACS Software Project Test Procedures translate the project's acceptance criteria into test steps. Software releases are certified when the affected Test Procedures are successfully performed and the customers authorize installation of these changes. This Test Procedure tests the TMACS SACS Interface functions

  14. TMACS Test Procedure TP010: Integration summary. Revision 5

    International Nuclear Information System (INIS)

    Spurling, D.G.

    1994-01-01

    The TMACS Soft Project Test Procedures translate the project's acceptance criteria into test steps. Software releases are certified when the affected Test Procedures are successfully performed and the customers authorize installation of these changes

  15. Bench-scale Development of an Advanced Solid Sorbent-based CO2 Capture Process for Coal-fired Power Plants

    Energy Technology Data Exchange (ETDEWEB)

    Nelson, Thomas [Research Triangle Institute (RTI), Research Triangle Park, NC (United States); Kataria, Atish [Research Triangle Institute (RTI), Research Triangle Park, NC (United States); Soukri, Mustapha [Research Triangle Institute (RTI), Research Triangle Park, NC (United States); Farmer, Justin [Research Triangle Institute (RTI), Research Triangle Park, NC (United States); Mobley, Paul [Research Triangle Institute (RTI), Research Triangle Park, NC (United States); Tanthana, Jak [Research Triangle Institute (RTI), Research Triangle Park, NC (United States); Wang, Dongxiang [Research Triangle Institute (RTI), Research Triangle Park, NC (United States); Wang, Xiaoxing [Research Triangle Institute (RTI), Research Triangle Park, NC (United States); Song, Chunshan [Research Triangle Institute (RTI), Research Triangle Park, NC (United States)

    2015-12-31

    It is increasingly clear that CO2 capture and sequestration (CCS) must play a critical role in curbing worldwide CO2 emissions to the atmosphere. Development of these technologies to cost-effectively remove CO2 from coal-fired power plants is very important to mitigating the impact these power plants have within the world’s power generation portfolio. Currently, conventional CO2 capture technologies, such as aqueous-monoethanolamine based solvent systems, are prohibitively expensive and if implemented could result in a 75 to 100% increase in the cost of electricity for consumers worldwide. Solid sorbent CO2 capture processes – such as RTI’s Advanced Solid Sorbent CO2, Capture Process – are promising alternatives to conventional, liquid solvents. Supported amine sorbents – of the nature RTI has developed – are particularly attractive due to their high CO2 loadings, low heat capacities, reduced corrosivity/volatility and the potential to reduce the regeneration energy needed to carry out CO2 capture. Previous work in this area has failed to adequately address various technology challenges such as sorbent stability and regenerability, sorbent scale-up, improved physical strength and attrition-resistance, proper heat management and temperature control, proper solids handling and circulation control, as well as the proper coupling of process engineering advancements that are tailored for a promising sorbent technology. The remaining challenges for these sorbent processes have provided the framework for the project team’s research and development and target for advancing the technology beyond lab- and bench-scale testing. Under a cooperative agreement with the US Department of Energy, and part of NETL’s CO2 Capture Program, RTI has led an effort to address and mitigate the challenges associated with solid sorbent CO2 capture. The overall objective

  16. Laboratory procedures for waste form testing

    International Nuclear Information System (INIS)

    Mast, E.S.

    1994-01-01

    The 100 and 300 areas of the Hanford Site are included on the US Environmental Protection Agencies (EPA) National Priorities List under the Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA). Soil washing is a treatment process that is being considered for the remediation of the soil in these areas. Contaminated soil washing fines can be mixed or blended with cementations materials to produce stable waste forms that can be used for beneficial purposes in mixed or low-level waste landfills, burial trenches, environmental restoration sites, and other applications. This process has been termed co-disposal. The Co-Disposal Treatability Study Test Plan is designed to identify a range of cement-based formulations that could be used in disposal efforts in Hanford in co-disposal applications. The purpose of this document is to provide explicit procedural information for the testing of co-disposal formulations. This plan also provides a discussion of laboratory safety and quality assurance necessary to ensure safe, reproducible testing in the laboratory

  17. Laboratory procedures for waste form testing

    Energy Technology Data Exchange (ETDEWEB)

    Mast, E.S.

    1994-09-19

    The 100 and 300 areas of the Hanford Site are included on the US Environmental Protection Agencies (EPA) National Priorities List under the Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA). Soil washing is a treatment process that is being considered for the remediation of the soil in these areas. Contaminated soil washing fines can be mixed or blended with cementations materials to produce stable waste forms that can be used for beneficial purposes in mixed or low-level waste landfills, burial trenches, environmental restoration sites, and other applications. This process has been termed co-disposal. The Co-Disposal Treatability Study Test Plan is designed to identify a range of cement-based formulations that could be used in disposal efforts in Hanford in co-disposal applications. The purpose of this document is to provide explicit procedural information for the testing of co-disposal formulations. This plan also provides a discussion of laboratory safety and quality assurance necessary to ensure safe, reproducible testing in the laboratory.

  18. 40 CFR 89.404 - Test procedure overview.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Test procedure overview. 89.404... (CONTINUED) CONTROL OF EMISSIONS FROM NEW AND IN-USE NONROAD COMPRESSION-IGNITION ENGINES Exhaust Emission Test Procedures § 89.404 Test procedure overview. (a) The test consists of prescribed sequences of...

  19. Factory Acceptance Test Procedure Westinghouse 100 ton Hydraulic Trailer

    International Nuclear Information System (INIS)

    Aftanas, B.L.

    1994-01-01

    This Factory Acceptance Test Procedure (FAT) is for the Westinghouse 100 Ton Hydraulic Trailer. The trailer will be used for the removal of the 101-SY pump. This procedure includes: safety check and safety procedures; pre-operation check out; startup; leveling trailer; functional/proofload test; proofload testing; and rolling load test

  20. TMACS test procedure TP010: Integration summary. Revision 6

    International Nuclear Information System (INIS)

    Spurling, D.G.

    1994-01-01

    The TMACS Software Project Test Procedures translate the project's acceptance criteria into test steps. Software releases are certified when the affected Test Procedures are successfully performed and the customers authorize installation of these changes. This Test Procedure verifies that Test Procedures 1, 2, 3, 5 and 9 (WHC-SD-WM-TRP-105, 106, 107, 109 and 113) of TMACS Software Release 4.1 have been successfully completed

  1. 40 CFR 86.1111-87 - Test procedures for PCA testing.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 19 2010-07-01 2010-07-01 false Test procedures for PCA testing. 86... Light-Duty Trucks § 86.1111-87 Test procedures for PCA testing. (a)(1) For heavy-duty engines, the prescribed test procedure for PCA testing is the Federal Test Procedure as described in subparts N, I, and P...

  2. Antimicrobial Testing Methods & Procedures Developed by EPA's Microbiology Laboratory

    Science.gov (United States)

    We develop antimicrobial testing methods and standard operating procedures to measure the effectiveness of hard surface disinfectants against a variety of microorganisms. Find methods and procedures for antimicrobial testing.

  3. 40 CFR 60.547 - Test methods and procedures.

    Science.gov (United States)

    2010-07-01

    ... hour. Instrument calibration shall be performed by the procedure given in Method 25A using the single... 40 Protection of Environment 6 2010-07-01 2010-07-01 false Test methods and procedures. 60.547... Manufacturing Industry § 60.547 Test methods and procedures. (a) The test methods in appendix A to this part...

  4. 46 CFR 130.480 - Test procedure and operations manual.

    Science.gov (United States)

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Test procedure and operations manual. 130.480 Section....480 Test procedure and operations manual. (a) A procedure for tests to be conducted on automated... detailed operations manual that describes the operation and indicates the location of each system installed...

  5. 40 CFR 600.111-80 - Test procedures.

    Science.gov (United States)

    2010-07-01

    ... Model Year Automobiles-Test Procedures § 600.111-80 Test procedures. (a) The test procedures to be... analyzer. (3) Except in cases of component malfunction or failure, all emission control systems installed... under-vehicle cooling and for controlling high tire or brake temperatures during dynamometer operation...

  6. 40 CFR 600.111-93 - Test procedures.

    Science.gov (United States)

    2010-07-01

    ... Model Year Automobiles-Test Procedures § 600.111-93 Test procedures. (a) The test procedures to be... component malfunction or failure, all emission control systems installed on or incorporated in a new motor... controlling high tire or brake temperatures during dynamometer operation. (3) Preparation of the CVS must be...

  7. Bench-Scale Study of Hydrogen Separation Using Pre-Commercial Membranes; Estudio, a Escala de Planta Piloto, del Proceso de Separacion de Hidrogeno mediante Membranas Pre-Comerciales

    Energy Technology Data Exchange (ETDEWEB)

    Sanchez Hervas, J. M.; Marano, M.

    2011-11-10

    This report compiles the research undertaken by CIEMAT over 2009-2011 in the sub-project 8 Purification and Separation of Hydrogen of the PSE H2ENOV Project funded by the Spanish Ministry of Science and Innovation, MICINN. Permeability and hydrogen selectivity of a pre-commercial palladium membrane was studied at bench scale level. The effect of main operating parameters - pressure, temperature and feed-flow-rate- on permeate flow-rate was determined. The influence of other gas components on hydrogen permeation was evaluated. Mixtures of H{sub 2}-N{sub 2} and H{sub 2}-CO{sub 2} were studied. Although nitrogen and carbon dioxide did not permeate, both components decreased hydrogen permeation rate. Operating the membrane for around 1000 h under various conditions showed a small decrease in hydrogen permeation, but not in selectivity. A literature review was done in order to identify causes for permeation inhibition and reduction and for the definition of procedures for membrane regeneration. (Author) 29 refs.

  8. TMACS test procedure TP001: Alarm management. Revision 6

    International Nuclear Information System (INIS)

    Scanlan, P.K.

    1994-01-01

    The TMACS Software Project Test Procedures translate the project's acceptance criteria into test steps. Software releases are certified when the affected Test Procedures are successfully performed and the customers authorize installation of these changes. This Test Procedure addresses the Alarm Management requirements of the TMACS. The features to be tested are: real-time alarming on high and low level and discrete alarms, equipment alarms, dead-band filtering, alarm display color coding, alarm acknowledgement, and alarm logging

  9. TMACS test procedure TP003: Graphics. Revision 5

    International Nuclear Information System (INIS)

    Scanlan, P.K.

    1994-01-01

    The TMACS Software Project Test Procedures translate the project's acceptance criteria into test steps. Software releases are certified when the affected Test Procedures are successfully performed and the customers authorize installation of these changes. This Test Procedure addresses the graphics requirements of the TMACS. The features to be tested are the data display graphics and the graphic elements that provide for operator control and selection of displays

  10. TMACS test procedure TP003: Graphics. Revision 6

    International Nuclear Information System (INIS)

    Scanlan, P.K.; Washburn, S.

    1994-01-01

    The TMACS Software Project Test Procedures translate the project's acceptance criteria into test steps. Software releases are certified when the affected Test Procedures are successfully performed and the customers authorize installation of these changes. This Test Procedure addresses the graphics requirements of the TMACS. The features to be tested are the data display graphics and the graphic elements that provide for operator control and selection of displays

  11. 702AZ aging waste ventilation facility year 2000 test procedure

    International Nuclear Information System (INIS)

    Winkelman, W.D.

    1998-01-01

    This test procedure was developed to determine if the 702AZ Tank Ventilation Facility system is Year 2000 Compliant. The procedure provides detailed instructions for performing the operations necessary and documenting the results. This verification procedure will document that the 702AZ Facility Systems are year 2000 compliant and will correctly meet the criteria established in this procedure

  12. School age test or procedure preparation

    Science.gov (United States)

    ... reduce pain and anxiety. Distract your child with books, bubbles, games, hand-held video games, or other ... can be present during the procedure. Ask if anesthesia can be used, if appropriate, to reduce your ...

  13. 40 CFR 63.905 - Test methods and procedures.

    Science.gov (United States)

    2010-07-01

    ... secured in the closed position. (3) The detection instrument shall meet the performance criteria of Method... 40 Protection of Environment 10 2010-07-01 2010-07-01 false Test methods and procedures. 63.905...) National Emission Standards for Tanks-Level 1 § 63.905 Test methods and procedures. (a) Procedure for...

  14. 40 CFR 63.945 - Test methods and procedures.

    Science.gov (United States)

    2010-07-01

    ... criteria of Method 21 of 40 CFR part 60, appendix A, except the instrument response factor criteria in... 40 Protection of Environment 10 2010-07-01 2010-07-01 false Test methods and procedures. 63.945...) National Emission Standards for Surface Impoundments § 63.945 Test methods and procedures. (a) Procedure...

  15. 40 CFR 63.925 - Test methods and procedures.

    Science.gov (United States)

    2010-07-01

    ... secured in the closed position. (3) The detection instrument shall meet the performance criteria of Method... 40 Protection of Environment 10 2010-07-01 2010-07-01 false Test methods and procedures. 63.925...) National Emission Standards for Containers § 63.925 Test methods and procedures. (a) Procedures for...

  16. 40 CFR 89.406 - Pre-test procedures.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Pre-test procedures. 89.406 Section 89.406 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED... Procedures § 89.406 Pre-test procedures. (a) Allow a minimum of 30 minutes warmup in the standby or operating...

  17. Military Publications, Index of Test Operations Procedures

    Science.gov (United States)

    1981-10-01

    Rockwell, Brinell, Tukon, scleroscope, and Vickers), notched-bar impact tests ( Charpy and Izod), fracture toughness tests, and fatigue tests. 3-2-807 AD...wire and three-wire ballistic pendulums . Covers measurement of component displarement relative to time and distance and measurements of impulse and...firing tests, safety evaluation, environmental and rough handling t-ests, pendulum recoil tests, noise and blast measurements, toxic gases

  18. Cloud-based Electronic Test Procedures, Phase I

    Data.gov (United States)

    National Aeronautics and Space Administration — Test procedures are at the heart of any experimental process, especially those involving novel and complex hardware. Whether these procedures are for system...

  19. Joint Test and Evaluation Procedures Manual.

    Science.gov (United States)

    1980-09-01

    discipline needed to keep individual staff members from the natural tendency to procrastinate when the test is still a "long way off." Fourth, they...concept is not fully developed, it embodies useful notions. In adaptive testing, change is planned for in advance. Specifically, the test matrix is...design matrix can be modified, as appropriate, early during the test sequence to provide more useful data for the final analysis of the system undergoing

  20. 40 CFR 91.507 - Test procedures.

    Science.gov (United States)

    2010-07-01

    ... EMISSIONS FROM MARINE SPARK-IGNITION ENGINES Manufacturer Production Line Testing Program § 91.507 Test... emission results representative of production line engines. (d) The manufacturer may not perform any... production line testing, and an adjustment or repair is necessary because of shipment, the engine...

  1. 16 CFR 1201.4 - Test procedures.

    Science.gov (United States)

    2010-01-01

    ... percent of the average pull force for the control specimens. (2) Tensile strength test (organic-coated... test it for breaking strength in the tensile tester. (iv) Interpretation of results. The organic... test sample through which a 3 inch (76 millimeter) diameter solid steel sphere, weighing 4 pounds ±3 oz...

  2. 16 CFR 1631.4 - Test procedure.

    Science.gov (United States)

    2010-01-01

    ...) Apparatus—(1) Test chamber. The test chamber shall consist of an open top hollow cube made of noncombustible... gel desiccant. (7) Gloves. Nonhygroscopic gloves (such as rubber or polyethylene) for handling the... gloves, remove a test specimen from the desiccator and brush its traffic surface with a gloved hand in...

  3. Braking, Wheeled Vehicles. Test Operations Procedure (TOP)

    Science.gov (United States)

    2008-05-20

    are as follows: a. Micrometer calipers (inside, outside, and dial types). b. Surface finish gauges. c. Torque wrench. d. Brake shoe...HAZARDOUS CONDITION • The power assist unit fails to operate. 10. Front Drum Brakes Procedure: Equipment needed: Steel scale or Vernier ... Micrometer and dial indicator. Reject the vehicle if: • Rotors are broken or damaged, or cracks on the surface extend to the outer edges. • Two grooves

  4. 49 CFR 572.132 - Head assembly and test procedure.

    Science.gov (United States)

    2010-10-01

    ... shall not exceed 15 G (zero to peak). (c) Head test procedure. The test procedure for the head is as... °C (66 and 78 °F) and a relative humidity from 10 to 70 percent for at least four hours prior to a...). (5) Allow at least 2 hours between successive tests on the same head. ...

  5. 47 CFR 87.197 - ELT test procedures.

    Science.gov (United States)

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false ELT test procedures. 87.197 Section 87.197 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AVIATION SERVICES Aircraft Stations Emergency Locator Transmitters § 87.197 ELT test procedures. ELT testing must avoid...

  6. EVALUATION OF THE TREATABILITY OF MUNICIPAL WASTE LANDFILL LEACHATE IN A SBR AND BY COAGULATION-FLOCCULATION ON A BENCH SCALE

    Directory of Open Access Journals (Sweden)

    E. Fleck

    Full Text Available Abstract This article describes bench scale sequential, biological and coagulation-flocculation treatment of mature leachate for the removal of nitrogen and biodegradable and recalcitrant carbonaceous material. The biological stage was conducted on two SBRs, one of which inoculated with nitrifying sludge, another without an inoculum, for 152 and 133 days, respectively. The coagulation-flocculation stage used four coagulants at different doses and pH adjustments. The treatment conducted on the inoculated SBR when a pH control was used produced mean removals of BOD5, COD and TKN of 69.6%, 38.5% and 51.6%, respectively, and practically complete denitrification. Coagulation-flocculation applied to the effluent of the inoculated biological reactor showed a superior effectiveness of the ferric coagulants, when the pH was adjusted to close to 6.0, producing removals of turbidity, COD and true color close to 95%, 78% and 92%, respectively.

  7. Appling hydrolysis acidification-anoxic–oxic process in the treatment of petrochemical wastewater: From bench scale reactor to full scale wastewater treatment plant

    Energy Technology Data Exchange (ETDEWEB)

    Wu, Changyong [State Key Laboratory of Environmental Criteria and Risk Assessment, Chinese Research Academy of Environmental Sciences, Beijing 100012 (China); Research Center of Water Pollution Control Technology, Chinese Research Academy of Environment Sciences, Beijing 100012 (China); Zhou, Yuexi, E-mail: zhouyuexi@263.net [State Key Laboratory of Environmental Criteria and Risk Assessment, Chinese Research Academy of Environmental Sciences, Beijing 100012 (China); Research Center of Water Pollution Control Technology, Chinese Research Academy of Environment Sciences, Beijing 100012 (China); Sun, Qingliang [School of Chemical Engineering, Beijing University of Chemical Technology, Beijing 100029 (China); Fu, Liya [Research Center of Water Pollution Control Technology, Chinese Research Academy of Environment Sciences, Beijing 100012 (China); School of Environment, Tsinghua University, Beijing 100084 (China); Xi, Hongbo; Yu, Yin [State Key Laboratory of Environmental Criteria and Risk Assessment, Chinese Research Academy of Environmental Sciences, Beijing 100012 (China); Research Center of Water Pollution Control Technology, Chinese Research Academy of Environment Sciences, Beijing 100012 (China); Yu, Ruozhen [State Key Laboratory of Environmental Criteria and Risk Assessment, Chinese Research Academy of Environmental Sciences, Beijing 100012 (China)

    2016-05-15

    Highlights: • Hydrolysis acidification-anoxic–oxic process can be used to treat petrochemical wastewater. • The toxicity and treatability changed significantly after hydrolysis acidification. • The type and concentration of organics reduced greatly after treatment. • The effluent shows low acute toxicity by luminescent bacteria assay. • Advanced treatment is recommended for the effluent. - Abstract: A hydrolysis acidification (HA)-anoxic–oxic (A/O) process was adopted to treat a petrochemical wastewater. The operation optimization was carried out firstly by a bench scale experimental reactor. Then a full scale petrochemical wastewater treatment plant (PCWWTP, 6500 m{sup 3} h{sup −1}) was operated with the same parameters. The results showed that the BOD{sub 5}/COD of the wastewater increased from 0.30 to 0.43 by HA. The effluent COD was 54.4 mg L{sup −1} for bench scale reactor and 60.9 mg L{sup −1} for PCWWTP when the influent COD was about 480 mg L{sup −1} on optimized conditions. The organics measured by gas chromatography-mass spectrometry (GC–MS) reduced obviously and the total concentration of the 5 organics (1,3-dioxolane, 2-pentanone, ethylbenzene, 2-chloromethyl-1,3-dioxolane and indene) detected in the effluent was only 0.24 mg L{sup −1}. There was no obvious toxicity of the effluent. However, low acute toxicity of the effluent could be detected by the luminescent bacteria assay, indicating the advanced treatment is needed. The clone library profiling analysis showed that the dominant bacteria in the system were Acidobacteria, Proteobacteria and Bacteriodetes. HA-A/O process is suitable for the petrochemical wastewater treatment.

  8. Appling hydrolysis acidification-anoxic–oxic process in the treatment of petrochemical wastewater: From bench scale reactor to full scale wastewater treatment plant

    International Nuclear Information System (INIS)

    Wu, Changyong; Zhou, Yuexi; Sun, Qingliang; Fu, Liya; Xi, Hongbo; Yu, Yin; Yu, Ruozhen

    2016-01-01

    Highlights: • Hydrolysis acidification-anoxic–oxic process can be used to treat petrochemical wastewater. • The toxicity and treatability changed significantly after hydrolysis acidification. • The type and concentration of organics reduced greatly after treatment. • The effluent shows low acute toxicity by luminescent bacteria assay. • Advanced treatment is recommended for the effluent. - Abstract: A hydrolysis acidification (HA)-anoxic–oxic (A/O) process was adopted to treat a petrochemical wastewater. The operation optimization was carried out firstly by a bench scale experimental reactor. Then a full scale petrochemical wastewater treatment plant (PCWWTP, 6500 m 3 h −1 ) was operated with the same parameters. The results showed that the BOD 5 /COD of the wastewater increased from 0.30 to 0.43 by HA. The effluent COD was 54.4 mg L −1 for bench scale reactor and 60.9 mg L −1 for PCWWTP when the influent COD was about 480 mg L −1 on optimized conditions. The organics measured by gas chromatography-mass spectrometry (GC–MS) reduced obviously and the total concentration of the 5 organics (1,3-dioxolane, 2-pentanone, ethylbenzene, 2-chloromethyl-1,3-dioxolane and indene) detected in the effluent was only 0.24 mg L −1 . There was no obvious toxicity of the effluent. However, low acute toxicity of the effluent could be detected by the luminescent bacteria assay, indicating the advanced treatment is needed. The clone library profiling analysis showed that the dominant bacteria in the system were Acidobacteria, Proteobacteria and Bacteriodetes. HA-A/O process is suitable for the petrochemical wastewater treatment.

  9. Test procedure for boxed waste assay system

    International Nuclear Information System (INIS)

    Wachter, J.

    1994-01-01

    This document, prepared by Los Alamos National Laboratory's NMT-4 group, details the test methodology and requirements for Acceptance/Qualification testing of a Boxed Waste Assay System (BWAS) designed and constructed by Pajarito Scientific Corporation. Testing of the BWAS at the Plutonium Facility (TA55) at Los Alamos National Laboratory will be performed to ascertain system adherence to procurement specification requirements. The test program shall include demonstration of conveyor handling capabilities, gamma ray energy analysis, and imaging passive/active neutron accuracy and sensitivity. Integral to these functions is the system's embedded operating and data reduction software

  10. TMACS test procedure TP012: Panalarm software bridge

    International Nuclear Information System (INIS)

    Washburn, S.J.

    1994-01-01

    This Test Procedure addresses the testing of the functionality of the Tank Monitor and Control System (TMACS) Panalarm bridge software. The features to be tested are: Bridge Initialization Options; Bridge Communication; Bridge Performance; Testing Checksum Errors; and Testing Command Reject Errors. Only the first three could be tested; the last two have been deferred to a later date

  11. Some procedures for computerized ability testing

    NARCIS (Netherlands)

    van der Linden, Willem J.; Zwarts, Michel A.

    1989-01-01

    For computerized test systems to be operational, the use of item response theory is a prerequisite. As opposed to classical test theory, in item response models the abilities of the examinees and the properties of the items are parameterized separately. Hence, when measuring the abilities of

  12. 16 CFR 1630.4 - Test procedure.

    Science.gov (United States)

    2010-01-01

    ...) Test chamber. The test chamber shall consist of an open top hollow cube made of noncombustible material...) Gloves. Nonhygroscopic gloves (such as rubber polyethylene) for handling the sample after drying, and... in the draft-protected environment (hood with draft off) with its bottom in place. Wearing gloves...

  13. Summary of functional and performance test procedures

    DEFF Research Database (Denmark)

    Mitzel, Jens; Gülzow, Erich; Friedrich, K. Andreas

    Different Test Modules (TM) are defined for the functional and performance characterization of a PEMFC stack. The master document TM2.00 defines requirements and methodology for parameter variation, stability and data acquisition.......Different Test Modules (TM) are defined for the functional and performance characterization of a PEMFC stack. The master document TM2.00 defines requirements and methodology for parameter variation, stability and data acquisition....

  14. 47 CFR 11.61 - Tests of EAS procedures.

    Science.gov (United States)

    2010-10-01

    ... tests will conform with the procedures in the EAS Operating Handbook. (1) Required Monthly Tests of the..., activation must include transmission of the EAS header and EOM codes. Analog and digital television broadcast...

  15. Cloud-Based Electronic Test Procedures, Phase II

    Data.gov (United States)

    National Aeronautics and Space Administration — Procedures are critical to experimental tests as they describe the specific steps necessary to efficiently and safely carry out a test in a repeatable fashion. The...

  16. 40 CFR 610.64 - Track test procedures.

    Science.gov (United States)

    2010-07-01

    ... measured during track testing. (4) Fuel economy of a vehicle running on a track will be measured using... Federal test procedure. (2) The test vehicle will be preconditioned within the same time constraints given... methods. (d) Steady state tests. Steady state tests on the track will be run in the same manner as on the...

  17. 40 CFR 94.506 - Test procedures.

    Science.gov (United States)

    2010-07-01

    .... (c) Service Accumulation/Green Engine Factor. The manufacturer shall accumulate up to 300 hours of... establish a Green Engine Factor for each regulated pollutant for each engine family to be used in... using a Green Engine Factor. (d) The manufacturer may not perform any maintenance on test engines after...

  18. 40 CFR 92.506 - Test procedures.

    Science.gov (United States)

    2010-07-01

    ... to the performance of any test. (c) Service Accumulation/Green Engine factor. The manufacturer or... a Green Engine factor for each regulated pollutant for each engine family to be used in calculating... prior to using a Green Engine factor. (d) The manufacturer or remanufacturer may not perform any...

  19. 40 CFR 90.707 - Test procedures.

    Science.gov (United States)

    2010-07-01

    ... EMISSIONS FROM NONROAD SPARK-IGNITION ENGINES AT OR BELOW 19 KILOWATTS Manufacturer Production Line Testing... manufacturer on every production line engine or unless this adjustment, repair, preparation, modification and... good engineering judgment to obtain emission results representative of production line engines. (d...

  20. Test procedure for cation exchange chromatography

    International Nuclear Information System (INIS)

    Cooper, T.D.

    1994-01-01

    The purpose of this test plan is to demonstrate the synthesis of inorganic antimonate ion exchangers and compare their performance against the standard organic cation exchangers. Of particular interest is the degradation rate of both inorganic and organic cation exchangers. This degradation rate will be tracked by determining the ion exchange capacity and thermal stability as a function of time, radiation dose, and chemical reaction

  1. A new approach to household appliance energy test procedures

    Energy Technology Data Exchange (ETDEWEB)

    Ernebrant, S.; Wihlborg, M.

    1999-03-01

    Energy test procedures provides the industry with a method to measure its products energy consumption. The energy test procedures are the technical foundation to every energy standard and labelling system. Depending on which country the product is going to be sold in, the manufacturers must follow different standards. This report concentrates on appliance test procedures, with the main focus on refrigerators. Recently, a new technology -microcontrollers- is undermining the credibility of the test procedures. New features, saving energy in real-life, are not picked up by the test procedures. It is estimated that as much as 30% of energy could be saved with this technology. Microcontrollers have also led to the possibility to circumvent tests. A new model is presented in the report, which handles these energy savings and make it harder cheating on tests. The model divides the test procedure in two parts; hardware tests and software tests, and uses a Matlab/Simulink computer model to calculate the energy consumption. Examples of hardware- and software test methods for refrigerators are described. A refrigerator is used as an example to present the model. The possibility to harmonize the energy standards to one global standard, which could mean substantial savings and make international trade more efficient, is also discussed 24 refs, 30 figs. Examination paper

  2. Surface moisture measurement system hardware acceptance test procedure

    International Nuclear Information System (INIS)

    Ritter, G.A.

    1996-01-01

    The purpose of this acceptance test procedure is to verify that the mechanical and electrical features of the Surface Moisture Measurement System are operating as designed and that the unit is ready for field service. This procedure will be used in conjunction with a software acceptance test procedure, which addresses testing of software and electrical features not addressed in this document. Hardware testing will be performed at the 306E Facility in the 300 Area and the Fuels and Materials Examination Facility in the 400 Area. These systems were developed primarily in support of Tank Waste Remediation System (TWRS) Safety Programs for moisture measurement in organic and ferrocyanide watch list tanks

  3. Hierarchical calibration and validation for modeling bench-scale solvent-based carbon capture. Part 1: Non-reactive physical mass transfer across the wetted wall column: Original Research Article: Hierarchical calibration and validation for modeling bench-scale solvent-based carbon capture

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Chao [Physical and Computational Sciences Directorate, Pacific Northwest National Laboratory, Richland WA; Xu, Zhijie [Physical and Computational Sciences Directorate, Pacific Northwest National Laboratory, Richland WA; Lai, Canhai [Physical and Computational Sciences Directorate, Pacific Northwest National Laboratory, Richland WA; Whyatt, Greg [Pacific Northwest National Laboratory, Energy and Environment Directorate, Richland WA; Marcy, Peter [Statistical Sciences Group, Los Alamos National Laboratory, Los Alamos NM; Sun, Xin [Physical and Computational Sciences Directorate, Pacific Northwest National Laboratory, Richland WA

    2017-04-27

    A hierarchical model calibration and validation is proposed for quantifying the confidence level of mass transfer prediction using a computational fluid dynamics (CFD) model, where the solvent-based carbon dioxide (CO2) capture is simulated and simulation results are compared to the parallel bench-scale experimental data. Two unit problems with increasing level of complexity are proposed to breakdown the complex physical/chemical processes of solvent-based CO2 capture into relatively simpler problems to separate the effects of physical transport and chemical reaction. This paper focuses on the calibration and validation of the first unit problem, i.e. the CO2 mass transfer across a falling ethanolamine (MEA) film in absence of chemical reaction. This problem is investigated both experimentally and numerically using nitrous oxide (N2O) as a surrogate for CO2. To capture the motion of gas-liquid interface, a volume of fluid method is employed together with a one-fluid formulation to compute the mass transfer between the two phases. Bench-scale parallel experiments are designed and conducted to validate and calibrate the CFD models using a general Bayesian calibration. Two important transport parameters, e.g. Henry’s constant and gas diffusivity, are calibrated to produce the posterior distributions, which will be used as the input for the second unit problem to address the chemical adsorption of CO2 across the MEA falling film, where both mass transfer and chemical reaction are involved.

  4. Quality assurance of radiopharmaceuticals-specifications and test procedures

    International Nuclear Information System (INIS)

    Baldas, J.; Bonnyman, J.; Pojer, P.M.

    1981-08-01

    This report is a compilation of test methods used and specifications adopted for the Radiopharmaceutical Quality Assurance Test Programme conducted by the Australian Radiation Laboratory. In some cases test procedures described have been taken from various Pharmacopoeias or methods published in the literature. In other cases test methods have been developed at the ARL

  5. Biaxial testing for fabrics and foils optimizing devices and procedures

    CERN Document Server

    Beccarelli, Paolo

    2015-01-01

    This book offers a well-structured, critical review of current design practice for tensioned membrane structures, including a detailed analysis of the experimental data required and critical issues relating to the lack of a set of design codes and testing procedures. The technical requirements for biaxial testing equipment are analyzed in detail, and aspects that need to be considered when developing biaxial testing procedures are emphasized. The analysis is supported by the results of a round-robin exercise comparing biaxial testing machines that involved four of the main research laboratories in the field. The biaxial testing devices and procedures presently used in Europe are extensively discussed, and information is provided on the design and implementation of a biaxial testing rig for architectural fabrics at Politecnico di Milano, which represents a benchmark in the field. The significance of the most recent developments in biaxial testing is also explored.

  6. An Analytical Procedure for the Equipercentile Method of Equating Tests.

    Science.gov (United States)

    Lindsay, Carl A.; Prichard, Mark A.

    Prior use of the equipercentile method of test equating was based on a graphic procedure which is tedious, subject to smoothing errors, and non-analytical. Recognition of the equipercentile method as a curve-fitting procedure for two cumulative percentage distributions leads to a proposed analytical solution to the problem through use of linear…

  7. Vehicle accelerated corrosion test procedures for automotive in Malaysia

    Directory of Open Access Journals (Sweden)

    Anuar Liza

    2017-01-01

    Full Text Available An accelerated corrosion test, known as proving ground accelerated test, is commonly performed by automotive manufacturers to evaluate the corrosion performance of a vehicle. The test combines corrosion and durability inputs to detect potential failures that may occur during in-service conditions. Currently, the test is conducted at an external test center overseas. Such test is aimed to simulate the effects of one year accelerated corrosion in severe corrosive environment of the north-east and south east of America. However, the test results obtained do not correlate with the actual corrosion conditions observed in the Malaysian market, which is likely attributed to the different test environment of the tropical climate of vehicles in service. Therefore, a vehicle accelerated corrosion test procedure that suits the Malaysian market is proposed and benchmarked with other global car manufacturers that have their own dedicated corrosion test procedure. In the present work, a test track is used as the corrosion test ground and consists of various types of roads for structural durability exposures. Corrosion related facilities like salt trough, mud trough and gravel road are constructed as addition to the existing facilities. The establishment of accelerated corrosion test facilities has contributed to the development of initial accelerated corrosion test procedure for the national car manufacturer. The corrosion exposure is monitored by fitting test coupons at the underbody of test vehicle using mass loss technique so that the desired corrosion rate capable of simulating the real time corrosion effects for its target market.

  8. 49 CFR 572.123 - Neck assembly and test procedure.

    Science.gov (United States)

    2010-10-01

    ... procedure for the neck assembly is as follows: (1) Soak the neck assembly in a controlled environment at any... least four hours prior to a test. (2) Torque the jam nut (drawing 9000341) on the neck cable (drawing...

  9. Numerical comparison between different strength after impact test procedures

    Directory of Open Access Journals (Sweden)

    Klaus M.

    2010-06-01

    Full Text Available Different procedures are established to investigate the residual properties of sandwich panels after impact damage. Two used procedures for the testing of this properties are compression after impact (CAI and 4-point bending. In this paper a numerical procedure is presented for a first prediction of the behaviour of pre-damaged sandwich specimens under different boundary conditions (or testing procedures. A sequence of impact experiments using a drop tower is performed to assess the damage tolerance of sandwich panels with aramid paper foldcores and CFRP skins. The tested impact energy range allowed to investigate a variety of damage scenarios from barely visible damages (BVID to fibre fractures in all plies of the impacted face sheet. Additionally 4-point bending tests are performed with the panels previously damaged by impact loadings to assess the residual bending strength of these samples. The developed numerical procedure is used to reproduce these experiments (the impact as well as the 4-point bending tests. Also the same procedure is employed in an attempt to predict the behaviour of samples with the same build-up in simulated compression after impact tests.

  10. Characterization of mercury, arsenic, and selenium in the product streams of a bench-scale, inert-gas, oil shale retort

    Energy Technology Data Exchange (ETDEWEB)

    Olsen, K.B.; Evans, J.C.; Fruchter, J.S.; Girvin, D.C.; Nelson, C.L. (Pacific Northwest Lab., Richland, WA (USA))

    1990-02-01

    The purpose of this study was to determine the effects of heating rates and maximum temperatures on the redistribution of mercury, arsenic, and selenium into the shale oil, retort water, and offgas of a 6-kg bench-scale retort. A Green River shale (western) from Colorado and a New Albany shale (eastern) from Kentucky were heated at 1-2{degree}C/min to a maximum temperature of 500{degree}C. The eastern and western shales were also heated at 2{degree}C/min to 750{degree}C and at 10{degree}C/min to 750{degree}C. Real-time monitoring of the offgas stream for mercury was accomplished with Zeeman atomic absorption spectroscopy or a microwave-induced helium plasma spectroscopy. Microwave-induced helium plasma spectroscopy was also used to monitor for arsenic in the offgas during retorting; little or no arsenic was observed in the offgas. Mass balance calculations for arsenic and selenium accounted for essentially 100% of those elements in the spent shale, shale oil, and retort water. The mass balance calculations suggest little offgas component for arsenic and selenium. This agrees with the results of the MPD monitoring of the offgas. These results indicate the potential pathway for mercury to enter the environment is from the offgas. Arsenic and selenium preferential redistribution into the shale oil may present problems during the upgrading process.

  11. Influence of toluene and salinity on biosurfactant production by Bacillus sp.: scale up from flasks to a bench-scale bioreactor

    Directory of Open Access Journals (Sweden)

    Ellen Cristina Souza

    Full Text Available ABSTRACT To select the best biosurfactant producer, Pseudomonas putida, Bacillus megatherium, Bacillus licheniformis and Bacillus subtilis were cultured in flasks on media with different salinity [low salinity (LS, Bushnell-Haas (BH and artificial sea water (SW media] supplemented or not with toluene as a model pollutant. Toluene inhibited the growth of all microorganisms and stimulated the biosurfactant production. B. subtilis exhibited the best performance, being able to lower the surface tension (ST in the LS medium to 65.5 mN/min in the absence of toluene, and to 46.5 mN/min in the BH medium in the presence of toluene, corresponding to ST reductions of 13.0 and 27.5 mN/m, respectively. Scaling up the process to a bench-scale fermentor, the best results were obtained in the LS medium, where B. subtilis was able to reduce the toluene concentration from 26.0 to 4.3 g/L within 12 h and ST by 17.2 mN/m within 18 h. The results of this study point out that B. subtilis is an interesting biosurfactant producer, which could be used in the bioremediation of toluene-contaminated water.

  12. Integrating a 250 mL-spinner flask with other stirred bench-scale cell culture devices: a mass transfer perspective.

    Science.gov (United States)

    Vallejos, Jose R; Brorson, Kurt A; Moreira, Antonio R; Rao, Govind

    2011-01-01

    The bioprocess development cycle is a complex task that requires a complete understanding of the engineering of the process (e.g., mass transfer, mixing, CO(2) removal, process monitoring, and control) and its affect on cell biology and product quality. Despite their widespread use in bioprocess development, spinner flasks generally lack engineering characterization of critical physical parameters such as k(L)a, P/V, or mixing time. In this study, mass transfer characterization of a 250-mL spinner flask using optical patch-based sensors is presented. The results quantitatively show the effect of the impeller type, liquid filling volume, and agitation speed on the volumetric mass transfer coefficient (k(L)a) in a 250-mL spinner flask, and how they can be manipulated to match mass transfer capability at large culture devices. Thus, process understanding in spinner flasks can be improved, and these devices can be seamlessly integrated in a rational scale-up strategy from cell thawing to bench-scale bioreactors (and beyond) in biomanufacturing. Copyright © 2011 American Institute of Chemical Engineers (AIChE).

  13. Corrosion performance tests for reinforcing steel in concrete : test procedures.

    Science.gov (United States)

    2009-09-01

    The existing test method to assess the corrosion performance of reinforcing steel embedded in concrete, mainly : ASTM G109, is labor intensive, time consuming, slow to provide comparative results, and often expensive. : However, corrosion of reinforc...

  14. Chemical oil-spill dispersants: evaluation of three laboratory procedures for estimating performance

    International Nuclear Information System (INIS)

    Clayton, J.R.; Marsden, P.

    1992-09-01

    The report presents data from studies designed to evaluate characteristics of selected bench-scale test methods for estimating performance of chemical agents for dispersing oil from surface slicks into an underlying water column. In order to mitigate the effect of surface slicks with chemical dispersant agents, however, an on-scene coordinator must have information and an understanding of performance characteristics for available dispersant agents. Performance of candidate dispersant agents can be estimated on the basis of laboratory testing procedures that are designed to evaluate performance of different agents. Data presented in the report assist in the evaluation of candidate test methods for estimating performance of candidate dispersant agents. Three test methods were selected for evaluating performance: the currently accepted Revised Standard EPA test, Environmental Canada's Swirling Flask test, and the IFP-Dilution test

  15. Test Operations Procedure (TOP) 06-2-301 Wind Testing

    Science.gov (United States)

    2017-06-14

    Facilities. Item Requirement Wind Generation System The wind generation system, typically consisting of a fan , fan speed control, ducting, and...difficult it is to provide a uniform wind speed over the test cross sectional area. The tester should employ the wind generation equipment ( fans , wind...turbulence can be affected by protuberances both active and passive, fan speed variations, and atmospheric conditions. 3.5 Test Item Faces

  16. Effects of turbulence modelling on prediction of flow characteristics in a bench-scale anaerobic gas-lift digester

    OpenAIRE

    Coughtrie, AR; Borman, DJ; Sleigh, PA

    2013-01-01

    Flow in a gas-lift digester with a central draft-tube was investigated using computational fluid dynamics (CFD) and different turbulence closure models. The k-ω Shear-Stress-Transport (SST), Renormalization-Group (RNG) k-∊, Linear Reynolds-Stress-Model (RSM) and Transition-SST models were tested for a gas-lift loop reactor under Newtonian flow conditions validated against published experimental work. The results identify that flow predictions within the reactor (where flow is transitional) ar...

  17. Removal of strontium from drinking water by conventional treatment and lime softening in bench-scale studies.

    Science.gov (United States)

    O'Donnell, Alissa J; Lytle, Darren A; Harmon, Stephen; Vu, Kevin; Chait, Hannah; Dionysiou, Dionysios D

    2016-10-15

    The United States Environmental Protection Agency Contaminant Candidate List 3 lists strontium as a contaminant for potential regulatory consideration in drinking water. Very limited data is available on strontium removal from drinking water and as a result, there is an immediate need for treatment information. The objective of this work is to evaluate the effectiveness of coagulation/filtration and lime-soda ash softening treatment methods to remove strontium from surface and ground waters. Coagulation/filtration jar test results on natural waters showed that conventional treatment with aluminum and iron coagulants were able to achieve only 12% and 5.9% strontium removal, while lime softening removed as high as 78% from natural strontium-containing ground water. Controlled batch experiments on synthetic water showed that strontium removal during the lime-soda ash softening was affected by pH, calcium concentration and dissolved inorganic carbon concentration. In all softening jar tests, the final strontium concentration was directly related to the initial strontium concentration and the removal of strontium was directly associated with calcium removal. Precipitated solids showed well-formed crystals or agglomerates of mixed solids, two polymorphs of calcium carbonate (vaterite and calcite), and strontianite, depending on initial water quality conditions. X-ray diffraction analysis suggested that strontium was likely incorporated in the calcium carbonate crystal lattice and was likely responsible for removal during lime softening. Copyright © 2016. Published by Elsevier Ltd.

  18. Evaluation of adipic acid addition to a bench-scale Chiyoda Thoroughbred 121 FGD system. Final report

    Energy Technology Data Exchange (ETDEWEB)

    Behrens, G.P.

    1981-12-01

    An experimental laboratory study testing the effectiveness of adipic acid in the Chiyoda Thoroughbred 121 FGD system has been sponsored by the Electric Power Research Institute. Additionally, economic calculations for the cost effectiveness of usng adipic acid in a commercial scale CT-121 FGD system have been performed. The results of this study indicate that although adipic acid can increase the SO/sub 2/ removal capability of the CT-121 system, it is not an economically attractive process improvement. This result is due to the CT-121 process chemistry which minimizes limestone consumption and sludge volume without the need of adipic acid. These two areas realize major cost savings when adipic is used in a conventional limestone FGD system. The economic evaluation indicates even though a lower gas-side pressue drop is achieved when adipic acid is used, the savings in electrical costs are insufficient to offset the cost of adipic acid.

  19. Acceptance test procedure, 241-SY-101 Flexible Receiver System, Phase III testing

    International Nuclear Information System (INIS)

    Ritter, G.A.

    1994-01-01

    This Acceptance Test Procedure is for the 241-SY-101 Flexible Receiver System, Phase III Testing. This procedure will test the sealing integrity of the Flexible Receiver System to ensure that release of waste and aerosols will be minimized during the removal of the test mixer pump from tank SY-101

  20. Indoor Secondary Pollutants from Household Product Emissions inthe Presence of Ozone: A Bench-Scale Chamber Study

    Energy Technology Data Exchange (ETDEWEB)

    Destaillats, Hugo; Lunden, Melissa M.; Singer, Brett C.; Coleman,Beverly K.; Hodgson, Alfred T.; Weschler, Charles J.; Nazaroff, William W.

    2005-10-01

    Ozone-driven chemistry is a major source of indoor secondary pollutants of health concern. This study investigates secondary air pollutants formed from reactions between constituents of household products and ozone. Gas-phase product emissions were introduced along with ozone at constant rates into a 198-L Teflon-lined reaction chamber. Gas-phase concentrations of reactive terpenoids and oxidation products were measured. Formaldehyde was a predominant oxidation byproduct for the three studied products, with yields under most conditions of 20-30% with respect to ozone consumed. Acetaldehyde, acetone, glycolaldehyde, formic acid and acetic acid were each also detected for two or three of the products. Immediately upon mixing of reactants, a scanning mobility particle sizer detected particle nucleation events that were followed by a significant degree of ultrafine particle growth. The production of secondary gaseous pollutants and particles depended primarily on the ozone level and was influenced by other parameters such as the air-exchange rate. Hydroxyl radical concentrations in the range 0.04-200 x 10{sup 5} molecules cm{sup -3} were measured. OH concentrations were observed to vary strongly with residual ozone level in the chamber, which was in the range 1-25 ppb, as is consistent with expectations from a simplified kinetic model. In a separate test, we exposed the dry residue of two products to ozone in the chamber and observed the formation of gas-phase and particle-phase secondary oxidation products.

  1. Effects of turbulence modelling on prediction of flow characteristics in a bench-scale anaerobic gas-lift digester.

    Science.gov (United States)

    Coughtrie, A R; Borman, D J; Sleigh, P A

    2013-06-01

    Flow in a gas-lift digester with a central draft-tube was investigated using computational fluid dynamics (CFD) and different turbulence closure models. The k-ω Shear-Stress-Transport (SST), Renormalization-Group (RNG) k-∊, Linear Reynolds-Stress-Model (RSM) and Transition-SST models were tested for a gas-lift loop reactor under Newtonian flow conditions validated against published experimental work. The results identify that flow predictions within the reactor (where flow is transitional) are particularly sensitive to the turbulence model implemented; the Transition-SST model was found to be the most robust for capturing mixing behaviour and predicting separation reliably. Therefore, Transition-SST is recommended over k-∊ models for use in comparable mixing problems. A comparison of results obtained using multiphase Euler-Lagrange and singlephase approaches are presented. The results support the validity of the singlephase modelling assumptions in obtaining reliable predictions of the reactor flow. Solver independence of results was verified by comparing two independent finite-volume solvers (Fluent-13.0sp2 and OpenFOAM-2.0.1). Copyright © 2013 Elsevier Ltd. All rights reserved.

  2. Determination and modeling of the influence of the fluid-dynamics in hydro-treating bench scale plants

    Energy Technology Data Exchange (ETDEWEB)

    Burkhardt, T.

    1999-09-16

    At an industrial scale, the hydro-treating of oil fractions is carried out in multiphase fixed bed reactors. The oil and hydrogen cross the catalyst bed, usually in co-current downflow. Since the product specifications are steadily becoming more severe, the testing of new catalysts and of modified operating conditions in pilot plants becomes increasingly important. Although these pilot plants are frequently by a factor of 100 000 smaller than the industrial units, they still have to allow the up-scaling to industrial units. In the literature relatively low conversion degrees in pilot plants are frequently reported, especially in downflow. The significantly lower fluid velocities in pilot plants seem to be responsible for such differences, as the influence of fluid-dynamic non-idealities and of the extra-particle mass transfer phenomena increases with a decrease of the fluid velocities. In the present work, the influence of important fluid-dynamic non-idealities on the hydro-treating of gas oil fractions in pilot plants was examined. This was done on the one hand in experiments with different pilot plants and on the other hand by simulations with an especially developed multiphase model. The phenomena were considered as well in an isolated manner. In order to examine any interactions with the chemical reactions, they were also studied in a reactive system. This methodology was applied to the phenomena, 'axial dispersion'and 'gas-liquid mass transfer'. (author)

  3. Bench scale experiments for the remediation of Hanford Waste Treatment Plant low activity waste melter off-gas condensate

    Energy Technology Data Exchange (ETDEWEB)

    Taylor-Pashow, Kathryn M.L. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL); Poirier, Michael [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL); McCabe, Daniel J. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL)

    2017-08-11

    The Low Activity Waste (LAW) vitrification facility at the Hanford Waste Treatment and Immobilization Plant (WTP) will generate an aqueous condensate recycle stream (LAW Off-Gas Condensate) from the off-gas system. The plan for disposition of this stream during baseline operations is to send it to the WTP Pretreatment Facility, where it will be blended with LAW, concentrated by evaporation and recycled to the LAW vitrification facility again. The primary reason to recycle this stream is so that the semi-volatile 99Tc isotope eventually becomes incorporated into the glass. This stream also contains non-radioactive salt components that are problematic in the melter, so diversion of this stream to another process would eliminate recycling of these salts and would enable simplified operation of the LAW melter and the Pretreatment Facilities. This diversion from recycling this stream within WTP would have the effect of decreasing the LAW vitrification mission duration and quantity of glass waste. The concept being tested here involves removing the 99Tc so that the decontaminated aqueous stream, with the problematic salts, can be disposed elsewhere.

  4. Drawbar Pull (DP) Procedures for Off-Road Vehicle Testing

    Science.gov (United States)

    Creager, Colin; Asnani, Vivake; Oravec, Heather; Woodward, Adam

    2017-01-01

    As NASA strives to explore the surface of the Moon and Mars, there is a continued need for improved tire and vehicle development. When tires or vehicles are being designed for off-road conditions where significant thrust generation is required, such as climbing out of craters on the Moon, it is important to use a standard test method for evaluating their tractive performance. The drawbar pull (DP) test is a way of measuring the net thrust generated by tires or a vehicle with respect to performance metrics such as travel reduction, sinkage, or power efficiency. DP testing may be done using a single tire on a traction rig, or with a set of tires on a vehicle; this report focuses on vehicle DP tests. Though vehicle DP tests have been used for decades, there are no standard procedures that apply to exploration vehicles. This report summarizes previous methods employed, shows the sensitivity of certain test parameters, and provides a body of knowledge for developing standard testing procedures. The focus of this work is on lunar applications, but these test methods can be applied to terrestrial and planetary conditions as well. Section 1.0 of this report discusses the utility of DP testing for off-road vehicle evaluation and the metrics used. Section 2.0 focuses on test-terrain preparation, using the example case of lunar terrain. There is a review of lunar terrain analogs implemented in the past and a discussion on the lunar terrain conditions created at the NASA Glenn Research Center, including methods of evaluating the terrain strength variation and consistency from test to test. Section 3.0 provides details of the vehicle test procedures. These consist of a review of past methods, a comprehensive study on the sensitivity of test parameters, and a summary of the procedures used for DP testing at Glenn.

  5. The influence of different measurement structures on NRTA test procedures

    International Nuclear Information System (INIS)

    Beedgen, R.

    1986-01-01

    The development of sequential statistical test procedures in the area of near real time material accountancy (NRTA) mostly assumed a fixed measurement model of a given model facility. In this paper different measurement models (dispersion matrices) for a sequence of balance periods are studied. They are used to compare the detection probabilities of three different sequential test procedures for losses of material. It is shown how different plant models have an influence on the sensitivity of specified tests. Great importance for that analysis have the optimal loss patterns in each measurement situation

  6. Procedures for Selecting Items for Computerized Adaptive Tests.

    Science.gov (United States)

    Kingsbury, G. Gage; Zara, Anthony R.

    1989-01-01

    Several classical approaches and alternative approaches to item selection for computerized adaptive testing (CAT) are reviewed and compared. The study also describes procedures for constrained CAT that may be added to classical item selection approaches to allow them to be used for applied testing. (TJH)

  7. AP-102/104 Retrieval control system qualification test procedure

    International Nuclear Information System (INIS)

    RIECK, C.A.

    1999-01-01

    This Qualification Test Procedure documents the results of the qualification testing that was performed on the Project W-211, ''Initial Tank Retrieval Systems,'' retrieval control system (RCS) for tanks 241-AP-102 and 241-AP-104. The results confirm that the RCS has been programmed correctly and that the two related hardware enclosures have been assembled in accordance with the design documents

  8. 16 CFR 1209.7 - Test procedures for smoldering combustion.

    Science.gov (United States)

    2010-01-01

    ... 16 Commercial Practices 2 2010-01-01 2010-01-01 false Test procedures for smoldering combustion. 1209.7 Section 1209.7 Commercial Practices CONSUMER PRODUCT SAFETY COMMISSION CONSUMER PRODUCT SAFETY... for smoldering combustion. This section provides the test method for determining smoldering combustion...

  9. 49 CFR 572.133 - Neck assembly and test procedure.

    Science.gov (United States)

    2010-10-01

    ... pendulum's longitudinal centerline between 77 degrees and 91 degrees. During the time interval while the... interval while the rotation is within the specified corridor, the peak moment, measured by the neck... Hybrid III 5th Percentile Female Test Dummy, Alpha Version § 572.133 Neck assembly and test procedure. (a...

  10. European wind turbine procedure development blade test methods and techniques

    Energy Technology Data Exchange (ETDEWEB)

    Bulder, B.H.; Dam, J.J.D. van; Delft, D.R.V. van [and others

    1999-03-01

    In this paper the preliminary results obtained by performing the second task of the `European Wind Turbine Testing Procedure Development` project are presented. This project is performed within and with financial support of the Standards, Measurements and Testing programme of the European Commission. (au)

  11. Operational test procedure for SY tank farm replacement exhauster unit

    International Nuclear Information System (INIS)

    McClees, J.

    1995-01-01

    This operational test procedure will verify that the remaining functions not tested per WHC-SD-WM-ATP-080, or components disturbed during final installation, as well as interfaces with other tank farm equipment and remote monitoring stations are operating correctly

  12. 40 CFR 205.57-4 - Testing procedures.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 24 2010-07-01 2010-07-01 false Testing procedures. 205.57-4 Section 205.57-4 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) NOISE ABATEMENT PROGRAMS TRANSPORTATION EQUIPMENT NOISE EMISSION CONTROLS Medium and Heavy Trucks § 205.57-4 Testing...

  13. 49 CFR 572.142 - Head assembly and test procedure.

    Science.gov (United States)

    2010-10-01

    .... (2) Prior to the test, clean the impact surface of the head skin and the steel impact plate surface... the steel impact surface. The 3.3 mm (0.13 in) diameter holes, located on either side of the dummy's... 49 Transportation 7 2010-10-01 2010-10-01 false Head assembly and test procedure. 572.142 Section...

  14. Testing Procedure for the Single Fiber Fragmentation Test

    DEFF Research Database (Denmark)

    Feih, Stefanie; Wonsyld, Karen; Minzari, Daniel

    , specimens with one E-glass fiber placed inside an epoxy or polyester matrix were used. Elongating the specimens with a mini tensile tester, which was placed under a microscope, leads to fiber fragmentations. Different bonding strengths between fiber and matrix result in differences in the critical fracture......This report describes the details of the single fiber fragmentation test as conducted at the materials research department (AFM) at Risø. The equipment and specimen manufacture is described in detail. Furthermore, examples of results interpretation are given. For the experiments in this report...... length for the fiber and fracture characteristics....

  15. Quality Assurance Plan for the AL3 Test Procedure

    CERN Document Server

    Béjar-Alonso, Isabel

    1999-01-01

    This paper describes the new quality assurance plan for the Alarms-of-Level-3 (AL3) test. The aim of the plan is to introduce engineering techniques and to standardise and simplify the procedures for carrying out tests following Safety Instruction 37 (IS37). The procedures are to co-ordinate all the services involved (fire brigade, maintenance and computer support) and to create a consistent documentation. When the procedures are implemented, it will be possible to determine with confidence how field actions are carried out and to measure actual performance. The focus will be on personnel training and documentation. It is important however to keep documentation and procedures to a reasonable level that can be maintained at appropriate intervals. The plan is the result of an internal requirement from ST/MC and a formal request from Installations Nucléaires de Base (INB).

  16. A unified framework for weighted parametric multiple test procedures.

    Science.gov (United States)

    Xi, Dong; Glimm, Ekkehard; Maurer, Willi; Bretz, Frank

    2017-09-01

    We describe a general framework for weighted parametric multiple test procedures based on the closure principle. We utilize general weighting strategies that can reflect complex study objectives and include many procedures in the literature as special cases. The proposed weighted parametric tests bridge the gap between rejection rules using either adjusted significance levels or adjusted p-values. This connection is made by allowing intersection hypotheses of the underlying closed test procedure to be tested at level smaller than α. This may be also necessary to take certain study situations into account. For such cases we introduce a subclass of exact α-level parametric tests that satisfy the consonance property. When the correlation is known only for certain subsets of the test statistics, a new procedure is proposed to fully utilize this knowledge within each subset. We illustrate the proposed weighted parametric tests using a clinical trial example and conduct a simulation study to investigate its operating characteristics. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  17. European wind turbine testing procedure developments. Task 2: Power quality

    DEFF Research Database (Denmark)

    Sørensen, Poul Ejnar; Friis Pedersen, Troels; Gerdes, G.

    2001-01-01

    quality measuremnet procedure in the Measnet cooperation of European test stations for wind turbines. The first working item of the project has been toverify the state of the art of the measurement procedures by analyses and comparisons of the measurements and data processing software of the participating......The present report describes the work done in the power quality subtask of the European Wind Turbine Testing Procedure Developments project funded by the EU SMT program. The objective of the power quality subtask has been to make recommendations andprovide background for new standards...... for measurement and testing of wind turbine power quality. The focus in the work has been to support the ongoing standardisation work in IEC with a new standard IEC61400-21 for measurement and assessment of powerquality characteristics of grid connected wind turbines. The work has also been based on the power...

  18. Operability test procedure [Tank] 241-SY-101 equipment removal system

    International Nuclear Information System (INIS)

    Mast, J.C.

    1994-01-01

    The 241-SY-101 equipment removal system (ERS) consists of components, equipment, instrumentation and procedures that will provide the means to disconnect, retrieve, contain, load and transport the Mitigation Pump Assembly (MPA) from waste Tank 241-SY-101 to the Central Waste Complex (CWC). The Operability Test Procedure (OTP) will test the interfaces between ERS components and will rehearse the procedure for MPA removal and transportation to the extent they can be mocked-up at the CTF (Cold Test Facility). At the conclusion of the OTP, the ERS components and equipment will be removed from the CTF, entered into the Component Based Recall System (CBRS), and stored until needed for actual MPA removal and transportation

  19. Hydrogen generation from bioethanol reforming: bench-scale unit performance with Cu/Nb{sub 2}O{sub 5} catalyst

    Energy Technology Data Exchange (ETDEWEB)

    Fernandes Machado, N.R.C. [State Univ. of Maringa (UEM), Chemical Engineering Dept., Lab. of Catalysis, Maringa (Brazil); Schmal, M. [PEQ/COPPE/UFRJ Cidade Univ., Centro de Tecnologia, Graduate School and Research in Engineering Alberto Luiz Coimbra Institute, Rio De Janeiro (Brazil); Cantao, M.P. [LACTEC, Dept. of Materials, Inst. of Technology for Development, Curitiba (Brazil)] [and others

    2003-07-01

    As an alternative route for hydrogen production, ethanol reforming was studied in a bench-scale unit using a 5%Cu/Nb{sub 2}O{sub 5} catalyst previously selected in a micro reactor. X-Ray Diffraction analysis has shown that this catalyst contains copper oxide in an amorphous form, or in particles smaller than 20 nm, while the Nb{sub 2}O{sub 5} is highly crystalline. Analysis of the calcinated catalyst by X-Ray Photoelectron Spectroscopy revealed that 35% of total copper was on the surface as Cu{sup I} (55%) or Cu{sup II} (45%). The catalyst presented a low surface area (35 m{sup 2}/g), mainly from meso and macropores, as textural analysis revealed. Temperature Programmed Reduction showed a two-step reduction of Cu{sup II} to Cu, at 245{sup o}C and 306{sup o}C. It was also observed the reduction of 6% of Nb{sub 2}O{sub 5}. The reaction unit consisted of an integral reactor with 16 g of catalyst pellets, approximately 3 mm x 5 mm in size. Reaction temperature and feed rate were varied to optimize hydrogen production, with CO{sub 2} as the main byproduct. Reagents (water and ethanol) in stoichiometric proportion were fed into an electric pre-heater and vaporized. An increase on reaction temperature from 300{sup o}C to 400{sup o}C has led to an increase in mean conversion from 17% to 35%. Ethene and ethyl ether were also detected as minor byproducts. (author)

  20. Empirical testing of forecast update procedure forseasonal products

    DEFF Research Database (Denmark)

    Wong, Chee Yew; Johansen, John

    2008-01-01

    of a toy supply chain. The theoretical simulation involves historical weekly consumer demand data for 122 toy products. The empirical test is then carried out in real-time with 291 toy products. The results show that the proposed forecast updating procedure: 1) reduced forecast errors of the annual......Updating of forecasts is essential for successful collaborative forecasting, especially for seasonal products. This paper discusses the results of a theoretical simulation and an empirical test of a proposed time-series forecast updating procedure. It involves a two-stage longitudinal case study...

  1. Acceptance test procedure for High Pressure Water Jet System

    International Nuclear Information System (INIS)

    Crystal, J.B.

    1995-01-01

    The overall objective of the acceptance test is to demonstrate a combined system. This includes associated tools and equipment necessary to perform cleaning in the 105 K East Basin (KE) for achieving optimum reduction in the level of contamination/dose rate on canisters prior to removal from the KE Basin and subsequent packaging for disposal. Acceptance tests shall include necessary hardware to achieve acceptance of the cleaning phase of canisters. This acceptance test procedure will define the acceptance testing criteria of the high pressure water jet cleaning fixture. The focus of this procedure will be to provide guidelines and instructions to control, evaluate and document the acceptance testing for cleaning effectiveness and method(s) of removing the contaminated surface layer from the canister presently identified in KE Basin. Additionally, the desired result of the acceptance test will be to deliver to K Basins a thoroughly tested and proven system for underwater decontamination and dose reduction. This report discusses the acceptance test procedure for the High Pressure Water Jet

  2. 241-AZ-101 Mixer Pump Demonstration Test Gamma Cart Acceptance Test Procedure and Quality Test Plan (ATP and QTP)

    International Nuclear Information System (INIS)

    WHITE, D.A.

    2000-01-01

    Shop Test of the Gamma Cart System to be used in the AZ-101 Mixer Pump Demonstration Test. Tests hardware and software. This procedure involves testing the Instrumentation involved with the Gamma Cart System, local and remote, including: depth indicators, speed controls, interface to data acquisition software and the raising and lowering functions. This Procedure will be performed twice, once for each Gamma Cart System. This procedure does not test the accuracy of the data acquisition software

  3. 40 CFR 264.1063 - Test methods and procedures.

    Science.gov (United States)

    2010-07-01

    ... CFR part 60. (2) The detection instrument shall meet the performance criteria of Reference Method 21... determined as set forth in Reference Method 21. (3) The instrument probe shall be traversed around all... 40 Protection of Environment 25 2010-07-01 2010-07-01 false Test methods and procedures. 264.1063...

  4. The Effect of Sample Preparation and Testing Procedure

    African Journals Online (AJOL)

    handling and disturbance. Revisions to sample preparation and testing procedures are considered necessary and are proposed in utilizing these soils for civil engineering purposes. It is concluded that the plasticity chart should be regarded as a guidance tool only for evaluating the likely properties of laterite soils. It should.

  5. Operating experience and procedures at the tritium systems test assembly

    International Nuclear Information System (INIS)

    Carlson, R.V.; Binning, K.E.; Cole, S.P.; Jenkins, E.M.; Wilhelm, R.C.; Cole, S.P.

    1988-01-01

    Operating procedures are important for the safe and efficient operation of the Tritium Systems Test Assembly (TSTA). TSTA has been operating for four years with tritium in a safe and efficient manner. The inventory of tritium in the process loop is 100 grams and several milestone runs have been completed. This paper describes the methods used to operate TSTA. 3 refs., 1 fig

  6. Statistical approach for collaborative tests, reference material certification procedures

    International Nuclear Information System (INIS)

    Fangmeyer, H.; Haemers, L.; Larisse, J.

    1977-01-01

    The first part introduces the different aspects in organizing and executing intercomparison tests of chemical or physical quantities. It follows a description of a statistical procedure to handle the data collected in a circular analysis. Finally, an example demonstrates how the tool can be applied and which conclusion can be drawn of the results obtained

  7. 16 CFR 1700.20 - Testing procedure for special packaging.

    Science.gov (United States)

    2010-01-01

    .... 1700.20 Section 1700.20 Commercial Practices CONSUMER PRODUCT SAFETY COMMISSION POISON PREVENTION PACKAGING ACT OF 1970 REGULATIONS POISON PREVENTION PACKAGING § 1700.20 Testing procedure for special... and color(s) (e.g., white polypropylene). 8. Closure liner material. 9. TAC seal material. 10. Opening...

  8. 40 CFR 63.365 - Test methods and procedures.

    Science.gov (United States)

    2010-07-01

    ... for Volatile Alcohols in Water By Direct Aqueous-Injection Gas Chromatography, (incorporated by... 40 Protection of Environment 9 2010-07-01 2010-07-01 false Test methods and procedures. 63.365 Section 63.365 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS...

  9. 40 CFR 63.180 - Test methods and procedures.

    Science.gov (United States)

    2010-07-01

    ... pressure shall be measured using a pressure measurement device (gauge, manometer, or equivalent) which has... § 63.11(b)(8), as appropriate. (f) The following procedures shall be used to pressure test batch product-process equipment for pressure or vacuum loss to demonstrate compliance with the requirements of...

  10. The effect of sample preparation and testing procedure on the ...

    African Journals Online (AJOL)

    The effect of sample preparation and testing procedure on the geotechnical properties of tropically weathered residual laterite soils of Ethiopia. ... A combination of classification based on structure, mineralogical composition, and geo-morphological impact on soil formation together with conventional classification systems is ...

  11. 40 CFR 86.227-94 - Test procedures; overview.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 18 2010-07-01 2010-07-01 false Test procedures; overview. 86.227-94 Section 86.227-94 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS... 1994 and Later Model Year Gasoline-Fueled New Light-Duty Vehicles, New Light-Duty Trucks and New Medium...

  12. 32 CFR 634.35 - Chemical testing policies and procedures.

    Science.gov (United States)

    2010-07-01

    ... 32 National Defense 4 2010-07-01 2010-07-01 true Chemical testing policies and procedures. 634.35 Section 634.35 National Defense Department of Defense (Continued) DEPARTMENT OF THE ARMY (CONTINUED) LAW ENFORCEMENT AND CRIMINAL INVESTIGATIONS MOTOR VEHICLE TRAFFIC SUPERVISION Traffic Supervision § 634.35...

  13. 40 CFR 92.123 - Test procedure; general requirements.

    Science.gov (United States)

    2010-07-01

    ... the test. Auxiliary fan(s) may be used to maintain engine cooling during operation on the dynamometer... smoke. (1) In the raw exhaust sampling procedure, sample is collected directly from the exhaust stream... of another raw exhaust sample. The fuel flow rate for each throttle setting is measured. (2) For...

  14. PUREX (SAMCONS) uninterruptible power supply (UPS) acceptance test procedure

    International Nuclear Information System (INIS)

    Blackaby, W.B.

    1997-01-01

    This Acceptance Test Procedure for the PUREX Surveillance and Monitoring and Control System (SAMCONS) Uninterruptible Power Supply (UPS) provides for testing and verifying the proper operation of the control panel alarms and trouble functions, the 6roper functioning of the AC inverter, ability of the battery supply to maintain the SAMCONS load for a minimum of two hours , and proper interaction with the SAMCONS Video graphic displays for alarm displays

  15. Standard Operating Procedure for Accelerated Corrosion Testing at ARL

    Science.gov (United States)

    2017-11-01

    to scribe nonferrous materials so as to prevent contamination of the substrate during the process. The "X" scribe is made by scribing 2 intersecting...may include GMW14872 Cyclic Corrosion Testing (typically Exterior, Exposure C), ASTM B117 Neutral Salt Fog Testing, ASTM G50 Atmospheric Corrosion...using the same cleaning procedures, contamination of the substrate is minimized during the scribe process. All partners adhering to guidelines and

  16. Preoperative testing before low-risk surgical procedures

    Science.gov (United States)

    Kirkham, Kyle R.; Wijeysundera, Duminda N.; Pendrith, Ciara; Ng, Ryan; Tu, Jack V.; Laupacis, Andreas; Schull, Michael J.; Levinson, Wendy; Bhatia, R. Sacha

    2015-01-01

    Background: There is concern about increasing utilization of low-value health care services, including preoperative testing for low-risk surgical procedures. We investigated temporal trends, explanatory factors, and institutional and regional variation in the utilization of testing before low-risk procedures. Methods: For this retrospective cohort study, we accessed linked population-based administrative databases from Ontario, Canada. A cohort of 1 546 223 patients 18 years or older underwent a total of 2 224 070 low-risk procedures, including endoscopy and ophthalmologic surgery, from Apr. 1, 2008, to Mar. 31, 2013, at 137 institutions in 14 health regions. We used hierarchical logistic regression models to assess patient- and institution-level factors associated with electrocardiography (ECG), transthoracic echocardiography, cardiac stress test or chest radiography within 60 days before the procedure. Results: Endoscopy, ophthalmologic surgery and other low-risk procedures accounted for 40.1%, 34.2% and 25.7% of procedures, respectively. ECG and chest radiography were conducted before 31.0% (95% confidence interval [CI] 30.9%–31.1%) and 10.8% (95% CI 10.8%–10.8%) of procedures, respectively, whereas the rates of preoperative echocardiography and stress testing were 2.9% (95% CI 2.9%–2.9%) and 2.1% (95% CI 2.1%–2.1%), respectively. Significant variation was present across institutions, with the frequency of preoperative ECG ranging from 3.4% to 88.8%. Receipt of preoperative ECG and radiography were associated with older age (among patients 66–75 years of age, for ECG, adjusted odds ratio [OR] 18.3, 95% CI 17.6–19.0; for radiography, adjusted OR 2.9, 95% CI 2.8–3.0), preoperative anesthesia consultation (for ECG, adjusted OR 8.7, 95% CI 8.5–8.8; for radiography, adjusted OR 2.2, 95% CI 2.1–2.2) and preoperative medical consultation (for ECG, adjusted OR 6.8, 95% CI 6.7–6.9; for radiography, adjusted OR 3.6, 95% CI 3.5–3.6). The median ORs

  17. 75 FR 59105 - Procedures for Transportation Workplace Drug and Alcohol Testing Programs: Federal Drug Testing...

    Science.gov (United States)

    2010-09-27

    ... 2105-AE03 Procedures for Transportation Workplace Drug and Alcohol Testing Programs: Federal Drug..., Office of Drug and Alcohol Policy and Compliance, 1200 New Jersey Avenue, SE., Washington, DC 20590; 202... Part 40 Administrative practice and procedures, Alcohol abuse, Alcohol testing, Drug abuse, Drug...

  18. Test Procedure for Axially Loaded Piles in Sand

    DEFF Research Database (Denmark)

    Thomassen, Kristina

    The test procedure described in the following is used when examining the effects of static or cyclic loading on the skin friction of an axially loaded pile in dense sand. The pile specimen is only loaded in tension to avoid any contribution from the base resistance. The pile dimensions are chosen...... to resemble full scale dimension of piles used in offshore pile foundations today. In this report is given a detailed description of the soil preparation and pile installation procedures as well data acquisition methods....

  19. Project W-320, operational test procedure OTP-320-003 test report

    International Nuclear Information System (INIS)

    Bevins, R.R.

    1998-01-01

    This report documents and summarizes the results of OTP-320-003 Project W-320 Operational Testing of the WRSS Supernate Transfer System. Project W-320 Operational Test OTP-320-003 was performed to verify components of the Waste Retrieval Sluicing System (WRSS) supernate transfer system functioned as designed following construction completion and turnover to operations. All equipment operation was performed by Tank Farms Operations personnel following the operational test procedure and referenced operating procedures. Supernate Transfer line Flushing System Testing was completed over the course of approximately 4 weeks as tank farm conditions and configuration, equipment availability, and operations resources allowed. All testing was performed with the 702-AZ ventilation system and the 296-P-16 ventilation systems in operation. Test procedure OTP-320-003 required two revisions during testing to incorporate Procedure Changes Authorizations (PCAs) necessary to facilitate testing. Various sections of testing are documented on each procedure revision. The completed test procedure is included as Attachment A. Exception Reports generated during the course of testing are included as Attachment B

  20. Project W-320, operational test procedure OTP-320-003 test report

    Energy Technology Data Exchange (ETDEWEB)

    Bevins, R.R.

    1998-07-23

    This report documents and summarizes the results of OTP-320-003 Project W-320 Operational Testing of the WRSS Supernate Transfer System. Project W-320 Operational Test OTP-320-003 was performed to verify components of the Waste Retrieval Sluicing System (WRSS) supernate transfer system functioned as designed following construction completion and turnover to operations. All equipment operation was performed by Tank Farms Operations personnel following the operational test procedure and referenced operating procedures. Supernate Transfer line Flushing System Testing was completed over the course of approximately 4 weeks as tank farm conditions and configuration, equipment availability, and operations resources allowed. All testing was performed with the 702-AZ ventilation system and the 296-P-16 ventilation systems in operation. Test procedure OTP-320-003 required two revisions during testing to incorporate Procedure Changes Authorizations (PCAs) necessary to facilitate testing. Various sections of testing are documented on each procedure revision. The completed test procedure is included as Attachment A. Exception Reports generated during the course of testing are included as Attachment B.

  1. Bench Scale Process for Low Cost CO2 Capture Using a PhaseChanging Absorbent: Techno-Economic Analysis Topical Report

    Energy Technology Data Exchange (ETDEWEB)

    Miebach, Barbara [GE Global Research, Niskayuna, New York (United States); McDuffie, Dwayne [GE Global Research, Niskayuna, New York (United States); Spiry, Irina [GE Global Research, Niskayuna, New York (United States); Westendorf, Tiffany [GE Global Research, Niskayuna, New York (United States)

    2017-01-27

    The objective of this project is to design and build a bench-scale process for a novel phase-changing CO2 capture solvent. The project will establish scalability and technical and economic feasibility of using a phase-changing CO2 capture absorbent for post-combustion capture of CO2 from coal-fired power plants with 90% capture efficiency and 95% CO2 purity at a cost of $40/tonne of CO2 captured by 2025 and a cost of <$10/tonne of CO2 captured by 2035. This report presents system and economic analysis for a process that uses a phase changing aminosilicone solvent to remove CO2 from pulverized coal (PC) power plant flue gas. The aminosilicone solvent is a pure 1,3-bis(3-aminopropyl)-1,1,3,3-tetramethyldisiloxane (GAP-0). Performance of the phase-changing aminosilicone technology is compared to that of a conventional carbon capture system using aqueous monoethanolamine (MEA). This analysis demonstrates that the aminosilicone process has significant advantages relative to an MEA-based system. The first-year CO2 removal cost for the phase-changing CO2 capture process is $52.1/tonne, compared to $66.4/tonne for the aqueous amine process. The phase-changing CO2 capture process is less costly than MEA because of advantageous solvent properties that include higher working capacity, lower corrosivity, lower vapor pressure, and lower heat capacity. The phase-changing aminosilicone process has approximately 32% lower equipment capital cost compared to that of the aqueous amine process. However, this solvent is susceptible to thermal degradation at CSTR desorber operating temperatures, which could add as much as $88/tonne to the CO2 capture cost associated with solvent makeup. Future work is focused on mitigating this critical risk by developing an advanced low-temperature desorber that can deliver comparable desorption performance and significantly reduced

  2. In-situ subaqueous capping of mercury-contaminated sediments in a fresh-water aquatic system, Part I—Bench-scale microcosm study to assess methylmercury production

    Energy Technology Data Exchange (ETDEWEB)

    Randall, Paul M., E-mail: randall.paul@epa.gov [U.S. Environmental Protection Agency, Office of Research and Development, National Risk Management Research Laboratory, 26 W. Martin Luther King Drive, Cincinnati, OH 45268 (United States); Fimmen, Ryan [Geosyntec Consultants, 150 E. Wilson Bridge Road, Suite 232, Worthington, OH 43085 (United States); Lal, Vivek; Darlington, Ramona [Battelle, 505 King Ave., Columbus, OH 43201 (United States)

    2013-08-15

    Bench-scale microcosm experiments were designed to provide a better understanding of the potential for Hg methylation in sediments from an aquatic environment. Experiments were conducted to examine the function of sulfate concentration, lactate concentration, the presence/absence of an aqueous inorganic Hg spike, and the presence/absence of inoculums of Desulfovibrio desulfuricans, a strain of sulfate-reducing bacteria (SRB) commonly found in the natural sediments of aquatic environments. Incubations were analyzed for both the rate and extent of (methylmercury) MeHg production. Methylation rates were estimated by analyzing MeHg and Hg after 2, 7, 14, 28, and 42 days. The production of metabolic byproducts, including dissolved gases as a proxy for metabolic utilization of carbon substrate, was also monitored. In all treatments amended with lactate, sulfate, Hg, and SRB, MeHg was produced (37 ng/g-sediment dry weight) after only 48 h of incubation and reached a maximum sediment concentration of 127 ng/g-sediment dry weight after the 42 day incubation period. Aqueous phase production of MeHg was observed to be 10 ng/L after 2 day, reaching a maximum observed concentration of 32.8 ng/L after 14 days, and declining to 10.8 ng/L at the end of the incubation period (42 day). The results of this study further demonstrates that, in the presence of an organic carbon substrate, sulfate, and the appropriate consortia of microorganisms, sedimentary Hg will be transformed into MeHg through bacterial metabolism. Further, this study provided the basis for evaluation of an in-situ subaqueous capping strategy that may limit (or potentially enhance) MeHg production. -- Highlights: • Hg methylation by SRB is limited by the depletion of sulfate and carbon. • Hg methylation is sensitive to competition by methanogens for carbon substrate. • In high lactate environment, all lactate was utilized in the microcosms within seven days. • In the absence of adequate metabolic fuel, Me

  3. In-situ subaqueous capping of mercury-contaminated sediments in a fresh-water aquatic system, Part I—Bench-scale microcosm study to assess methylmercury production

    International Nuclear Information System (INIS)

    Randall, Paul M.; Fimmen, Ryan; Lal, Vivek; Darlington, Ramona

    2013-01-01

    Bench-scale microcosm experiments were designed to provide a better understanding of the potential for Hg methylation in sediments from an aquatic environment. Experiments were conducted to examine the function of sulfate concentration, lactate concentration, the presence/absence of an aqueous inorganic Hg spike, and the presence/absence of inoculums of Desulfovibrio desulfuricans, a strain of sulfate-reducing bacteria (SRB) commonly found in the natural sediments of aquatic environments. Incubations were analyzed for both the rate and extent of (methylmercury) MeHg production. Methylation rates were estimated by analyzing MeHg and Hg after 2, 7, 14, 28, and 42 days. The production of metabolic byproducts, including dissolved gases as a proxy for metabolic utilization of carbon substrate, was also monitored. In all treatments amended with lactate, sulfate, Hg, and SRB, MeHg was produced (37 ng/g-sediment dry weight) after only 48 h of incubation and reached a maximum sediment concentration of 127 ng/g-sediment dry weight after the 42 day incubation period. Aqueous phase production of MeHg was observed to be 10 ng/L after 2 day, reaching a maximum observed concentration of 32.8 ng/L after 14 days, and declining to 10.8 ng/L at the end of the incubation period (42 day). The results of this study further demonstrates that, in the presence of an organic carbon substrate, sulfate, and the appropriate consortia of microorganisms, sedimentary Hg will be transformed into MeHg through bacterial metabolism. Further, this study provided the basis for evaluation of an in-situ subaqueous capping strategy that may limit (or potentially enhance) MeHg production. -- Highlights: • Hg methylation by SRB is limited by the depletion of sulfate and carbon. • Hg methylation is sensitive to competition by methanogens for carbon substrate. • In high lactate environment, all lactate was utilized in the microcosms within seven days. • In the absence of adequate metabolic fuel, Me

  4. Test Report for Acceptance Test Procedure for Pumping Instrumentation and Control Skid L

    International Nuclear Information System (INIS)

    KOCH, M.R.

    1999-01-01

    This is a Test Report for Acceptance Test Procedure (ATP) RPP-5055. This test report provides the results of the inspection and testing of the new Pumping Instrumentation and Control (PIC) skid designed as ''L''. The ATP was successfully completed. A copy of the completed ATP is in the Appendix of this document

  5. Test Report for Acceptance Test Procedure for Pumping Instrumentation and Control Skid L

    Energy Technology Data Exchange (ETDEWEB)

    KOCH, M.R.

    1999-11-09

    This is a Test Report for Acceptance Test Procedure (ATP) RPP-5055. This test report provides the results of the inspection and testing of the new Pumping Instrumentation and Control (PIC) skid designed as ''L''. The ATP was successfully completed. A copy of the completed ATP is in the Appendix of this document.

  6. Test Report for Acceptance Test Procedure for Pumping and Instrumentation Control Skid ''K''

    CERN Document Server

    Johns, B R

    1999-01-01

    This is a Test Report for Acceptance Test Procedure (ATP) HNF-4276. This test report provides the results of the inspection and testing of the new Pumping and Instrumentation Control (PIC) skid designed as ''K''. The ATP was successfully completed. A copy of the completed ATP is in the Appendix of this document.

  7. Test Report for Acceptance Test Procedure for Pumping Instrumentation and Control Skid M

    International Nuclear Information System (INIS)

    KOCH, M.R.

    1999-01-01

    This is a Test Report for Acceptance Test Procedure (ATP) RPP-5073. This test report provides the results of the inspection and testing of the new Pumping Instrumentation and Control (PIC) skid designed as ''M''. The ATP was successfully completed. A copy of the completed ATP is in the Appendix of this document

  8. Loss on Ignition Furnace Acceptance and Operability Test Procedure

    International Nuclear Information System (INIS)

    JOHNSTON, D.C.

    2000-01-01

    The purpose of this Acceptance Test Procedure and Operability Test Procedure (ATP/OTP)is to verify the operability of newly installed Loss on Ignition (LOI) equipment, including a model 1608FL CMTM Furnace, a dessicator, and balance. The operability of the furnace will be verified. The arrangement of the equipment placed in Glovebox 157-3/4 to perform LOI testing on samples supplied from the Thermal Stabilization line will be verified. In addition to verifying proper operation of the furnace, this ATP/OTP will also verify the air flow through the filters, verify a damper setting to establish and maintain the required differential pressure between the glovebox and the room pressure, and test the integrity of the newly installed HEPA filter. In order to provide objective evidence of proper performance of the furnace, the furnace must heat 15 crucibles, mounted on a crucible rack, to 1000 C, according to a program entered into the furnace controller located outside the glovebox. The glovebox differential pressure will be set to provide the 0.5 to 2.0 inches of water (gauge) negative pressure inside the glovebox with an expected airflow of 100 to 125 cubic feet per minute (cfm) through the inlet filter. The glovebox inlet G1 filter will be flow tested to ensure the integrity of the filter connections and the efficiency of the filter medium. The newly installed windows and glovebox extension, as well as all disturbed joints, will be sonically tested via ultra probe to verify no leaks are present. The procedure for DOS testing of the filter is found in Appendix A

  9. Loss on Ignition Furnace Acceptance and Operability Test Procedure

    Energy Technology Data Exchange (ETDEWEB)

    JOHNSON, D.C.

    2000-06-01

    The purpose of this Acceptance Test Procedure and Operability Test Procedure (ATP/OTP)is to verify the operability of newly installed LOI equipment, including a model 1608FL CM{trademark} Furnace, a dessicator, and balance. The operability of the furnace will be verified. The arrangement of the equipment placed in Glovebox 157-3/4 to perform Loss on Ignition (LOI) testing on samples supplied from the Thermal Stabilization line will be verified. In addition to verifying proper operation of the furnace, this ATP/OTP will also verify the air flow through the filters, verify a damper setting to establish and maintain the required differential pressure between the glovebox and the room pressure, and test the integrity of the newly installed HEPA filter. In order to provide objective evidence of proper performance of the furnace, the furnace must heat 15 crucibles, mounted on a crucible rack, to 1000 C, according to a program entered into the furnace controller located outside the glovebox. The glovebox differential pressure will be set to provide the 0.5 to 2.0 inches of water (gauge) negative pressure inside the glovebox with an airflow of 100 to 125 cubic feet per minute (cfm) through the inlet filter. The glovebox inlet Glfilter will he flow tested to ensure the integrity of the filter connections and the efficiency of the filter medium. The newly installed windows and glovebox extension, as well as all disturbed joints, will be sonically tested via ultra probe to verify no leaks are present. The procedure for DOS testing of the filter is found in Appendix A.

  10. Project W-049H collection system Acceptance Test Procedure

    International Nuclear Information System (INIS)

    Carrigan, M.C.

    1994-01-01

    The purpose of this Acceptance Test Procedure (ATP) for the Project W-049H, Treated Effluent Disposal Facility, is to verify that the collection system equipment installed as Pump Station No. 1 (225-W) and Pump Station No. 2 (225-E) have been installed in accordance with the design documents and function as required by the project criteria. This will be a wet test with potable water being introduced into the pump pits to test for leakage. Potable water will also be employed in the testing of the pumps and related mechanical equipment. All Instrument and Control equipment related to the pump stations will be checked electronically with simulated inputs/outputs when actual input/output signals are unavailable. Water from Pump Station 1 will be moved through the TEDF piping system and discharged into the disposal ponds. This will check the proper function of the air/vac valves not tested during construction, and the automated samplers

  11. Advances in p-Value Based Multiple Test Procedures.

    Science.gov (United States)

    Tamhane, Ajit C; Gou, Jiangtao

    2018-01-01

    In this article we review recent advances in [Formula: see text]-value-based multiple test procedures (MTPs). We begin with a brief review of the basic tests of Bonferroni and Simes. Standard stepwise MTPs derived from them using the closure method of Marcus et al. (1976) are discussed next. They include the well-known MTPs of Holm (1979), Hochberg (1988) and Hommel (1988), and their extensions and improvements. This is followed by stepwise MTPs for a priori ordered hypotheses. Next we present gatekeeping MTPs (Dmitrienko and Tamhane, 2007) for hierarchically ordered families of hypotheses with logical relations among them. Finally, we give a brief review of the graphical approach (Bretz et al., 2009) to constructing and visualizing gatekeeping and other MTPs. Simple numerical examples are given to illustrate the various procedures.

  12. Acceptance Test Procedure: SY101 air pallet system

    International Nuclear Information System (INIS)

    Koons, B.M.

    1995-01-01

    The purpose of this test procedure is to verify that the system(s) procured to load the SY-101 Mitigation Test Pump package fulfills its functional requirements. It will also help determine the man dose expected due to handling of the package during the actual event. The scope of this procedure focuses on the ability of the air pallets and container saddles to carry the container package from the new 100 foot concrete pad into 2403-WD where it will be stored awaiting final disposition. This test attempts to simulate the actual event of depositing the SY-101 hydrogen mitigation test pump into the 2403-WD building. However, at the time of testing road modifications required to drive the 100 ton trailer into CWC were not performed. Therefore a flatbed trailer will be use to transport the container to CWC. The time required to off load the container from the 100 ton trailer will be recorded for man dose evaluation on location. The cranes used for this test will also be different than the actual event. This is not considered to be an issue due to minimal effects on man dose

  13. Hierarchical calibration and validation framework of bench-scale computational fluid dynamics simulations for solvent-based carbon capture. Part 2: Chemical absorption across a wetted wall column: Original Research Article: Hierarchical calibration and validation framework of bench-scale computational fluid dynamics simulations

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Chao [Pacific Northwest National Laboratory, Physical and Computational Sciences Directorate, Richland WA; Xu, Zhijie [Pacific Northwest National Laboratory, Physical and Computational Sciences Directorate, Richland WA; Lai, Kevin [Pacific Northwest National Laboratory, Physical and Computational Sciences Directorate, Richland WA; Whyatt, Greg [Energy and Environment Directorate, Pacific Northwest National Laboratory, Richland WA; Marcy, Peter W. [Los Alamos National Laboratory, Statistical Sciences Group, Los Alamos NM; Sun, Xin [Oak Ridge National Laboratory, Energy and Transportation Science Division, Oak Ridge TN

    2017-10-24

    The first part of this paper (Part 1) presents a numerical model for non-reactive physical mass transfer across a wetted wall column (WWC). In Part 2, we improved the existing computational fluid dynamics (CFD) model to simulate chemical absorption occurring in a WWC as a bench-scale study of solvent-based carbon dioxide (CO2) capture. To generate data for WWC model validation, CO2 mass transfer across a monoethanolamine (MEA) solvent was first measured on a WWC experimental apparatus. The numerical model developed in this work has the ability to account for both chemical absorption and desorption of CO2 in MEA. In addition, the overall mass transfer coefficient predicted using traditional/empirical correlations is conducted and compared with CFD prediction results for both steady and wavy falling films. A Bayesian statistical calibration algorithm is adopted to calibrate the reaction rate constants in chemical absorption/desorption of CO2 across a falling film of MEA. The posterior distributions of the two transport properties, i.e., Henry’s constant and gas diffusivity in the non-reacting nitrous oxide (N2O)/MEA system obtained from Part 1 of this study, serves as priors for the calibration of CO2 reaction rate constants after using the N2O/CO2 analogy method. The calibrated model can be used to predict the CO2 mass transfer in a WWC for a wider range of operating conditions.

  14. Project W-049H instrument and control Acceptance Test Procedure

    International Nuclear Information System (INIS)

    Carrigan, M.C.

    1994-01-01

    The purpose of this Acceptance Test Procedure (ATP) for the Project W-049H, Treated Effluent Disposal Facility, is to verify that the instrument and control systems have been installed in accordance with the design documents and function as required by the project criteria. The instrument and control system includes three operator control stations, modems, and general purpose LAN interface cabinets in the Effluent Treatment Facility control room; two pump stations; disposal station pumping building; and all local control units installed in the fold. Testing will be performed using actual signals when available and simulated signals when actual signals are unavailable

  15. Quality assurance of radiopharmaceuticals - specifications and test procedures

    International Nuclear Information System (INIS)

    Baldas, J.; Bonnyman, J.; Colmanet, S.F.; Ivanov, Z.; Lauder, R.A.

    1990-10-01

    The authors report on a Radiopharmaceutical Quality Assurance Test Programme carried out by the Australian Radiation Laboratory in which radiopharmaceuticals used in nuclear medicine in Australia are tested for compliance with specifications. Where the radiopharmaceutical is the subject of a monograph in the British Pharmacopoeia or the European Pharmacopoeia, then the specifications given in the Pharmacopoeia are adopted. In other cases the specifications given have been adopted by this Laboratory and have no legal status. In some cases test procedures described have been taken from various Pharmacopoeias or methods published in the literature. In other cases test methods described have been developed at this Laboratory. It should be noted that, unless stated otherwise, specifications listed apply at all times up until product expire

  16. Project W-314 performance mock-up test procedure

    International Nuclear Information System (INIS)

    CARRATT, R.T.

    1999-01-01

    The purpose of this Procedure is to assist construction in the pre-operational fabrication and testing of the pit leak detection system and the low point drain assembly by: (1) Control system testing of the pit leak detection system will be accomplished by actuating control switches and verifying that the control signal is initiated, liquid testing and overall operational requirements stated in HNF-SD-W314-PDS-003, ''Project Development Specification for Pit Leak Detection''. (2) Testing of the low point floor drain assembly by opening and closing the drain to and from the ''retracted'' and ''sealed'' positions. Successful operation of this drain will be to verify that the seal does not leak on the ''sealed'' position, the assembly holds liquid until the leak detector actuates and the assembly will operate from on top of the mock-up cover block

  17. Testing heated flint palaeodose protocols using dose recovery procedures

    International Nuclear Information System (INIS)

    Richter, D.; Temming, H.

    2006-01-01

    Thermoluminescence (TL) dating of materials from archaeological contexts has been shown to be an accurate method when comparisons are made with other chronometric dating methods; however, little has been published on the verification of the measurement protocols used to determine the equivalent dose (palaeodose). Instead of testing TL dating protocols for heated flint using archaeological material with unknown thermal and radiation history, dose recovery tests for three samples of different geological origin are presented. These samples exhibit TL emission in the UV, blue and orange-red wavelengths. In addition to the two multiple aliquot protocols (standard additive-regeneration and normalization) generally used to determine the palaeodose, the single-aliquot-regenerative-dose (SAR) TL and OSL procedure, a 'short' SAR-TL and isothermal luminescence (IT) decay procedures are applied using detection windows limited to these emissions. Accurate dose recovery is obtained for the standard and normalization protocols in the commonly employed detection window (UV-blue), the 'short' SAR in the orange-red window and some IT measurements. While the standard techniques give the most accurate and precise results, detection of the TL and IT orange-red emission in connection with a 'short' SAR protocol also gave accurate and precise results. Such procedures are especially suitable for samples too small for standard multiple aliquot techniques, which require large samples

  18. Lightning arrestor connector lead magnesium niobate qualification pellet test procedures.

    Energy Technology Data Exchange (ETDEWEB)

    Tuohig, W. (Honeywell FM& T, Kansas City, MO); Mahoney, Patrick A.; Tuttle, Bruce Andrew; Wheeler, Jill Susanne

    2009-02-01

    Enhanced knowledge preservation for DOE DP technical component activities has recently received much attention. As part of this recent knowledge preservation effort, improved documentation of the sample preparation and electrical testing procedures for lead magnesium niobate--lead titanate (PMN/PT) qualification pellets was completed. The qualification pellets are fabricated from the same parent powders used to produce PMN/PT lightning arrestor connector (LAC) granules at HWF&T. In our report, the procedures for fired pellet surface preparation, electrode deposition, electrical testing and data recording are described. The dielectric measurements described in our report are an information only test. Technical reasons for selecting the electrode material, electrode size and geometry are presented. The electrical testing is based on measuring the dielectric constant and dissipation factor of the pellet during cooling from 280 C to 220 C. The most important data are the temperature for which the peak dielectric constant occurs (Curie Point temperature) and the peak dielectric constant magnitude. We determined that the peak dielectric constant for our procedure would be that measured at 1 kHz at the Curie Point. Both the peak dielectric constant and the Curie point parameters provide semi-quantitative information concerning the chemical and microstructural homogeneity of the parent material used for the production of PMN/PT granules for LACs. Finally, we have proposed flag limits for the dielectric data for the pellets. Specifically, if the temperature of the peak dielectric constant falls outside the range of 250 C {+-} 30 C we propose that a flag limit be imposed that will initiate communication between production agency and design agency personnel. If the peak dielectric constant measured falls outside the range 25,000 {+-} 10,000 we also propose that a flag limit be imposed.

  19. Neurophysiological tests and neuroimaging procedures in non-acute headache

    DEFF Research Database (Denmark)

    Sandrini, G; Friberg, L; Jänig, W

    2004-01-01

    , a history of seizures and/or focal neurological signs or symptoms, magnetic resonance imaging (MRI) may be indicated. 6 If attacks can be fully accounted for by the standard headache classification [International Headache Society (IHS)], a positron emission tomography (PET) or single-photon emission......The use of instrumental examinations in headache patients varies widely. In order to evaluate their usefulness, the most common instrumental procedures were evaluated, on the basis of evidence from the literature, by an EFNS Task Force (TF) on neurophysiological tests and imaging procedures in non......-acute headache patients. The conclusions of the TF regarding each technique are expressed in the following guidelines for clinical use. 1 Interictal electroencephalography (EEG) is not routinely indicated in the diagnostic evaluation of headache patients. Interictal EEG is, however, indicated if the clinical...

  20. Applied field test procedures on petroleum release sites

    International Nuclear Information System (INIS)

    Gilbert, G.; Nichols, L.

    1995-01-01

    The effective remediation of petroleum contaminated soils and ground water is a significant issue for Williams Pipe Line Co. (Williams): costing $6.8 million in 1994. It is in the best interest, then, for Williams to adopt approaches and apply technologies that will be both cost-effective and comply with regulations. Williams has found the use of soil vapor extraction (SVE) and air sparging (AS) field test procedures at the onset of a petroleum release investigation/remediation accomplish these goals. This paper focuses on the application of AS/SVE as the preferred technology to a specific type of remediation: refined petroleum products. In situ field tests are used prior to designing a full-scale remedial system to first validate or disprove initial assumptions on applicability of the technology. During the field test, remedial system design parameters are also collected to tailor the design and operation of a full-scale system to site specific conditions: minimizing cost and optimizing effectiveness. In situ field tests should be designed and operated to simulate as close as possible the operation of a full-scale remedial system. The procedures of an in situ field test will be presented. The results of numerous field tests and the associated costs will also be evaluated and compared to full-scale remedial systems and total project costs to demonstrate overall effectiveness. There are many advantages of As/SVE technologies over conventional fluid extraction or SVE systems alone. However, the primary advantage is the ability to simultaneously reduce volatile and biodegradable compound concentrations in the phreatic, capillary fringe, and unsaturated zones

  1. TASK TECHNICAL AND QUALITY ASSURANCE PLAN FOR OUT-OF-TANK DESTRUCTION OF TETRAPHENYLBORATE VIA WET AIR OXIDATION TECHNOLOGY: PHASE I - BENCH SCALE TESTS

    Energy Technology Data Exchange (ETDEWEB)

    Adu-Wusu, K

    2006-03-31

    Tank 48H return to service is critical to the processing of high level waste (HLW) at Savannah River Site (SRS). Liquid Waste Disposition (LWD) management has the goal of returning Tank 48H to routine service by January 2010 or as soon as practical. Tank 48H currently holds legacy material containing organic tetraphenylborate (TPB) compounds from the operation of the In-Tank Precipitation process. This material is not compatible with the waste treatment facilities at SRS and must be removed or undergo treatment to destroy the organic compounds before the tank can be returned to Tank Farm service. Tank 48H currently contains {approx}240,000 gallons of alkaline slurry with about 2 wt % potassium and cesium tetraphenylborate (KTPB and CsTPB). The main radioactive component in Tank 48H is {sup 137}Cs. The waste also contains {approx}0.15 wt % Monosodium Titanate (MST) which has adsorbed {sup 90}Sr, U, and Pu isotopes. A System Engineering Evaluation of technologies/ideas for the treatment of TPB identified Wet Air Oxidation (WAO) as a leading alternative technology to the baseline aggregation approach. Over 75 technologies/ideas were evaluated overall. Forty-one technologies/ideas passed the initial screening evaluation. The 41 technologies/ideas were then combined to 16 complete solutions for the disposition of TPB and evaluated in detail. Wet Air Oxidation (WAO) is an aqueous phase process in which soluble or suspended waste components are oxidized using molecular oxygen contained in air. The process operates at elevated temperatures and pressures ranging from 150 to 320 C and 7 to 210 atmospheres, respectively. The products of the reaction are CO{sub 2}, H{sub 2}O, and low molecular weight oxygenated organics (e.g. acetate, oxalate). The basic flow scheme for a typical WAO system is as follows. The waste solution or slurry is pumped through a high-pressure feed pump. An air stream containing sufficient oxygen to meet the oxygen requirements of the waste stream is injected into the pressurized waste stream, and the air/liquid mixture is preheated to the required reactor inlet temperature. The reactor provides sufficient retention time to allow the oxidation to approach the desired level of organic decomposition. Typical reaction time is about 30-120 minutes. Heat exchangers are routinely employed to recover energy contained in the reactor effluent to preheat the waste feed/air entering the reactor. Auxiliary energy, usually steam, is necessary for startup and can provide trim heat if required. Since the oxidation reactions are exothermic, sufficient energy may be released in the reactor to allow the WAO system to operate without any additional heat input. After cooling, the oxidized reactor effluent passes through a pressure control valve where the pressure is reduced. A separator downstream of the pressure control valve allows the depressurized and cooled vapor to separate from the liquid. Typical industrial WAO applications have a feed flow rate of 1 to 220 gallons per minute (gpm) per train, with a chemical oxygen demand (COD) from 10,000 to 150,000 mg/L (higher CODs with dilution). Note that catalysts, such as homogeneous copper and iron, their heterogeneous counterparts, or precious metals can be used to enhance the effectiveness (i.e., to lower temperature, pressure, and residence time as well as increase oxidation efficiencies) of the WAO reaction if deemed necessary.

  2. Operational test procedure for Bldg 241-A-701 air compressor

    International Nuclear Information System (INIS)

    Desantis, G.N.

    1995-01-01

    This document is an Operability Test Procedure (OTP) which will verify and record that the 241-A-701 air compressor and associated equipment operates within their intended design parameters. The activities defined in this OTP will be performed to ensure the daily operation of the new compressed air system can be reliable and efficient. The Compressed Air System (CAS) for 241-A-701 supplies process and instrument air to the A, AX, AY, and AZ tank farms. The primary use of the CAS is for tank farms instrumentation, air operated valves, and air lift circulators

  3. Narrative elaboration: test of a new procedure for interviewing children.

    Science.gov (United States)

    Saywitz, K J; Snyder, L

    1996-12-01

    Because young children provide incomplete accounts of the past and tend to acquiesce to leading questions, procedures are needed to help them describe past events fully, without contaminating memory. This study tests the efficacy of "narrative elaboration," an innovative procedure designed to expand children's spontaneous reports of past events, reducing the need for leading questions. One hundred thirty-two children from 2 age groups (7-8 years and 10-11 years) were assigned randomly to 1 of 3 preparation conditions: (a) narrative elaboration intervention, (b) instruction-based intervention, and (c) control group. After participating in a staged activity and subsequent preparation sessions, children were interviewed about the activity. Children in the narrative elaboration condition demonstrated a 53% improvement in spontaneous recall over the control group, without compromising accuracy. Younger children using the narrative elaboration procedure performed at the level of older children in the control group. Discussion centers on implications for interviewing child witnesses and preparing them for courtroom examination.

  4. Scoring and Testing Procedures Devoted to Probabilistic Seismic Hazard Assessment

    Science.gov (United States)

    Albarello, Dario; D'Amico, Vera

    2015-03-01

    This review addresses long-term (tens of years) seismic ground-motion forecasting (seismic hazard assessment) in the presence of alternative computational models (the so-called epistemic uncertainty affecting hazard estimates). We review the different approaches that have been proposed to manage epistemic uncertainty in the context of probabilistic seismic hazard assessment (PSHA). Ex- ante procedures (based on the combination of expert judgments about inherent characteristics of the PSHA model) and ex- post approaches (based on empirical comparison of model outcomes and observations) should not be considered as mutually exclusive alternatives but can be combined in a coherent Bayesian view. Therefore, we propose a procedure that allows a better exploitation of available PSHA models to obtain comprehensive estimates, which account for both epistemic and aleatory uncertainty. We also discuss the respective roles of empirical ex-post scoring and testing of alternative models concurring in the development of comprehensive hazard maps. In order to show how the proposed procedure may work, we also present a tentative application to the Italian area. In particular, four PSHA models are evaluated ex-post against macroseismic effects actually observed in a large set of Italian municipalities during the time span 1957-2006. This analysis shows that, when the whole Italian area is considered, all the models provide estimates that do not agree with the observations. However, two of them provide results that are compatible with observations, when a subregion of Italy (Apulia Region) is considered. By focusing on this area, we computed a comprehensive hazard curve for a single locality in order to show the feasibility of the proposed procedure.

  5. Operability test procedure for PFP wastewater sampling facility

    International Nuclear Information System (INIS)

    Hirzel, D.R.

    1995-01-01

    Document provides instructions for performing the Operability Test of the 225-WC Wastewater Sampling Station which monitors the discharge to the Treated Effluent Disposal Facility from the Plutonium Finishing Plant. This Operability Test Procedure (OTP) has been prepared to verify correct configuration and performance of the PFP Wastewater sampling system installed in Building 225-WC located outside the perimeter fence southeast of the Plutonium Finishing Plant (PFP). The objective of this test is to ensure the equipment in the sampling facility operates in a safe and reliable manner. The sampler consists of two Manning Model S-5000 units which are rate controlled by the Milltronics Ultrasonic flowmeter at manhole No.C4 and from a pH measuring system with the sensor in the stream adjacent to the sample point. The intent of the dual sampling system is to utilize one unit to sample continuously at a rate proportional to the wastewater flow rate so that the aggregate tests are related to the overall flow and thereby eliminate isolated analyses. The second unit will only operate during a high or low pH excursion of the stream (hence the need for a pH control). The major items in this OTP include testing of the Manning Sampler System and associated equipment including the pH measuring and control system, the conductivity monitor, and the flow meter

  6. Safety panel and new procedures evaluation by simulator tests

    International Nuclear Information System (INIS)

    Meslin, T.

    1986-01-01

    With more than thirty weeks of simulator testing (for the last three years only) and approximately three hundred scenarios, EDF's experience in this field is extensive. This practice is well known within Fossil and Nuclear Generation and is well accepted by the operating teams which participate in it. Simulator testing appears to be an essential decision-making tool in the process of developing new operating aids in PWR plants. Accelerated development and the elimination of long and expensive modifications after commissioning is an economic advantage. The saving in time is obvious, since modifications are carried out continuously throughout the development phase. Finally, operators participate in the development of systems and receive fixed, well-defined applications. This practice has become systematic, and all new applications concerning the operation of PWR plants are simulator-tested, particularly 1300-MW unit computers and operating procedures, the new generation of 900-MW unit computers, and the new 1500-MW fully computerized control rooms. Finally, this simulator testing allows us to considerably increase our knowledge concerning the behavior of operators in accident situations, and special tests are performed for this purpose

  7. Acceptance test procedure for Project W-049H

    International Nuclear Information System (INIS)

    Buckles, D.I.

    1994-01-01

    The Acceptance Test Procedure (ATP) program for Project W-049H (200 Area Treated Effluent Disposal Facility [TEDF]) covers three activities as follows: (1) Disposal System; (2) Collection System; and (3) Instrumentation and Control System. Each activity has its own ATP. The purpose of the ATPs is to reverify that the systems have been constructed in accordance with the construction documents and to demonstrate that the systems function as required by the Project criteria. The Disposal System ATP covers the testing of the following: disposal line flowmeters, room air temperatures in the Disposal Station Sampling Building, effluent valves and position indicators, disposal pond level monitors, automated sampler, pressure relief valves, and overflow diversion sluice gates. The Collection System ATP covers the testing of the two pump stations and all equipment installed therein. The Instrumentation and Control (I and C) ATP covers the testing of the entire TEDF I and C system. This includes 3 OCS units, modem, and GPLI cabinets in the ETC control room; 2 pump stations; disposal station sampling building; and all LCUs installed in the field

  8. TMACS Test Procedure TP005: Sensor configuration, logging, and data conversion

    International Nuclear Information System (INIS)

    Washburn, S.J.

    1994-01-01

    The TMACS Software Project Test Procedures translate the projects acceptance criteria into test steps. Software releases are certified when the affected Test Procedures are successfully performed and the customers authorize installation of these changes

  9. Refractory Metal Heat Pipe Life Test - Test Plan and Standard Operating Procedures

    Science.gov (United States)

    Martin, J. J.; Reid, R. S.

    2010-01-01

    Refractory metal heat pipes developed during this project shall be subjected to various operating conditions to evaluate life-limiting corrosion factors. To accomplish this objective, various parameters shall be investigated, including the effect of temperature and mass fluence on long-term corrosion rate. The test series will begin with a performance test of one module to evaluate its performance and to establish the temperature and power settings for the remaining modules. The performance test will be followed by round-the-clock testing of 16 heat pipes. All heat pipes shall be nondestructively inspected at 6-month intervals. At longer intervals, specific modules will be destructively evaluated. Both the nondestructive and destructive evaluations shall be coordinated with Los Alamos National Laboratory. During the processing, setup, and testing of the heat pipes, standard operating procedures shall be developed. Initial procedures are listed here and, as hardware is developed, will be updated, incorporating findings and lessons learned.

  10. Methods for testing the logical structure of plant procedure documents

    International Nuclear Information System (INIS)

    Horne, C.P.; Colley, R.; Fahley, J.M.

    1990-01-01

    This paper describes an ongoing EPRI project to investigate computer based methods to improve the development, maintenance, and verification of plant operating procedures. This project began as an evaluation of the applicability of structured software analysis methods to operating procedures. It was found that these methods offer benefits, if procedures are transformed to a structured representation to make them amenable to computer analysis. The next task was to investigate methods to transform procedures into a structured representation. The use of natural language techniques to read and compile the procedure documents appears to be viable for this purpose and supports conformity to guidelines. The final task was to consider possibilities of automated verification methods for procedures. Methods to help verify procedures were defined and information requirements specified. These methods take the structured representation of procedures as input. The software system being constructed in this project is called PASS, standing for Procedures Analysis Software System

  11. 40 CFR 94.109 - Test procedures for Category 3 marine engines.

    Science.gov (United States)

    2010-07-01

    ... PROGRAMS (CONTINUED) CONTROL OF EMISSIONS FROM MARINE COMPRESSION-IGNITION ENGINES Test Procedures § 94.109 Test procedures for Category 3 marine engines. (a) Gaseous emissions shall be measured using the test... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Test procedures for Category 3 marine...

  12. Expose : procedure and results of the joint experiment verification tests

    Science.gov (United States)

    Panitz, C.; Rettberg, P.; Horneck, G.; Rabbow, E.; Baglioni, P.

    The International Space Station will carry the EXPOSE facility accommodated at the universal workplace URM-D located outside the Russian Service Module. The launch will be affected in 2005 and it is planned to stay in space for 1.5 years. The tray like structure will accomodate 2 chemical and 6 biological PI-experiments or experiment systems of the ROSE (Response of Organisms to Space Environment) consortium. EXPOSE will support long-term in situ studies of microbes in artificial meteorites, as well as of microbial communities from special ecological niches, such as endolithic and evaporitic ecosystems. The either vented or sealed experiment pockets will be covered by an optical filter system to control intensity and spectral range of solar UV irradiation. Control of sun exposure will be achieved by the use of individual shutters. To test the compatibility of the different biological systems and their adaptation to the opportunities and constraints of space conditions a profound ground support program has been developed. The procedure and first results of this joint Experiment Verification Tests (EVT) will be presented. The results will be essential for the success of the EXPOSE mission and have been done in parallel with the development and construction of the final hardware design of the facility. The results of the mission will contribute to the understanding of the organic chemistry processes in space, the biological adaptation strategies to extreme conditions, e.g. on early Earth and Mars, and the distribution of life beyond its planet of origin.

  13. Frequency modulation system test procedure shuttle task 501 approach and landing test configuration

    Science.gov (United States)

    Doland, G. D.

    1976-01-01

    Shuttle Task 501 is an in-line task to test the performance and compatibility of radiofrequency links between the SSO and ground, and relay via a satellite. Under Shuttle Task 501 approach and landing test (ALT) phase only a limited portion of the communication and tracking (C&T) equipment is to be tested. The principal item to be tested is a frequency modulated (FM) data link. To test this RF link, an ALT FM System was designed, constructed, and the console wiring verified. A step-by-step procedure to be used to perform the ALT FM system is presented. The ALT FM system test is to be performed prior to delivery of the equipment to the Electronic Systems Test Laboratory (ESTL).

  14. 77 FR 2829 - Energy Conservation Program: Test Procedure for Television Sets

    Science.gov (United States)

    2012-01-19

    ... Conservation Program: Test Procedure for Television Sets; Proposed Rule #0;#0;Federal Register / Vol. 77 , No... Television Sets AGENCY: Office of Energy Efficiency and Renewable Energy, Department of Energy. ACTION... test procedure for television sets (TVs). DOE repealed the prior Federal test procedure for TVs on...

  15. TMACS test procedure TP005: Sensor configuration, logging, and data conversion. Revision 4

    International Nuclear Information System (INIS)

    Washburn, S.J.

    1994-01-01

    The TMACS Software Project Test Procedures translate the project's acceptance criteria into test steps. Software releases are certified when the affected Test Procedures are successfully performed and the customers authorize installation of these changes. This Test Procedure addresses the sensor configuration, conversion and logging requirements of the TMACS. The features to be tested are as follows: sensor configuration data; conversion of continuous sensor data to engineering units; conversion of digital data to discrete states; discrete sensor data logging; and continuous sensor data logging

  16. AIChe equipment testing procedure centrifugal compressors : a guide to performance evaluation and site testing

    CERN Document Server

    AIChE

    2013-01-01

    With its engineer-tested procedures and thorough explanations, Centrifugal Compressors is an essential text for anyone engaged in implementing new technology in equipment design, identifying process problems, and optimizing equipment performance.  This condensed book presents a step by step approach to preparing for, planning, executing, and analyzing tests of centrifugal compressors, with an emphasis on methods that can be conducted on-site and with an acknowledgement of the strengths and limitations of these methods. The book opens with an extensive and detailed section offering definitions

  17. Weld Design, Testing, and Assessment Procedures for High Strength Pipelines

    Science.gov (United States)

    2011-12-20

    Long-distance high-strength pipelines are increasingly being constructed for the efficient transportation of energy products. While the high-strength linepipe steels and high productivity welding processes are being applied, the procedures employed f...

  18. Leach test of six 192-iridium pellets based on the IAEA 'special form' test procedures

    International Nuclear Information System (INIS)

    Gordon, G.; Gerdingh, R.

    1981-07-01

    The designation 'special form' may be applied to indispersible solid radioactive material if the material meets the requirements of the tests described in the International Atomic Energy Agency Regulations for the Safe Transport of Radioactive Type Materials. This report presents the procedures and results of a leach test performed as specified in the regulations on 6 'as received' active 192-iridium pellets. Mechanical tests were not carried out prior to or following the leach test. The activity of each of the first 6 water baths was found to be between 2.3 and 12.6 μCi, (8.5 x 10 4 and 4.7 x 10 5 Bq) and of the second 6, between 1.3 to 6.0 μCi, (4.8 x 10 4 to 2.2 x 10 5 Bq) thus exceeding the allowable limit

  19. 76 FR 27016 - Evaluating Test Procedures for Voting Systems

    Science.gov (United States)

    2011-05-10

    ... testing process beyond that which is necessary and sufficient for performing test method validation activities. Manufacturers should be aware that some of the testing could damage or destroy the equipment... NIST's main campus as required for the purpose of conducting usability tests. NIST will ensure that all...

  20. Sandia National Laboratories Electrochemical Storage System Abuse Test Procedure Manual

    Energy Technology Data Exchange (ETDEWEB)

    Unkelhaeuser, Terry; Smallwood David

    1999-07-01

    The series of tests described in this report are intended to simulate actual use and abuse conditions and internally initiated failures that may be experienced in electrochemical storage systems (ECSS). These tests were derived from Failure Mode and Effect Analysis, user input, and historical abuse testing. The tests are to provide a common framework for various ECSS technologies. The primary purpose of testing is to gather response information to external/internal inputs. Some tests and/or measurements may not be required for some ECSS technologies and designs if it is demonstrated that a test is not applicable, and the measurements yield no useful information.

  1. 40 CFR 60.106 - Test methods and procedures.

    Science.gov (United States)

    2010-07-01

    ... is to be used to determine particulate matter emissions and associated moisture content from affected... (Qr). (ii) The emission correction factor, integrated sampling and analysis procedure of Method 3B... shall be used to determine opacity. (c) If auxiliary liquid or solid fossil-fuels are burned in an...

  2. Operability test procedure for the TK-900 effluent monitoring station

    International Nuclear Information System (INIS)

    Weissenfels, R.D.

    1994-01-01

    This procedure will verify that the 221-B liquid effluent monitoring system, installed near the east end of the 6-in. chemical sewer header, functions as intended by design. TK-900B was installed near stairwell 3 in the 221-B electrical gallery by Project W-007H. The system is part of BAT/AKART for the BCE liquid effluent system

  3. 40 CFR 63.425 - Test methods and procedures.

    Science.gov (United States)

    2010-07-01

    ... CFR 60.503 of this chapter, except a reading of 500 ppm shall be used to determine the level of leaks... according to the procedures in this paragraph. (1) The leak definition shall be 21,000 ppm as propane. Use propane to calibrate the instrument, setting the span at the leak definition. The response time to 90...

  4. Operability test procedure for the Rotary Mode Core Sampling System Exhausters 3 and 4

    International Nuclear Information System (INIS)

    WSaldo, E.J.

    1995-01-01

    This document provides a procedure for performing operability testing of the Rotary Mode Core Sampling System Exhausters 3 ampersand 4. Upon completion of testing activities an operability testing report will be issued

  5. 40 CFR 86.127-12 - Test procedures; overview.

    Science.gov (United States)

    2010-07-01

    ... (CONTINUED) CONTROL OF EMISSIONS FROM NEW AND IN-USE HIGHWAY VEHICLES AND ENGINES Emission Regulations for... prescribed sequences of fueling, parking, and operating test conditions. Vehicles are tested for any or all... (variable dilution) sampler or critical flow venturi sampler. (c) The diesel-cycle exhaust emission test is...

  6. Tank Monitoring and Control System (TMACS) Acceptance Test Procedure

    International Nuclear Information System (INIS)

    HOLM, M.J.

    1999-01-01

    This document is intended to test the software portion of TMACS. The tests will be performed on the development system. The software to be tested is the TMACS knowledge bases (KB) and the I/O driver devices. The development system will not be talking to field equipment; instead, the field equipment is simulated using emulators or multiplexers in the lab

  7. 49 CFR 572.152 - Head assembly and test procedure.

    Science.gov (United States)

    2010-10-01

    ... period specified in this section. (2) Before the test, clean the impact surface of the head skin and the steel impact plate surface with isopropyl alcohol, trichlorethane, or an equivalent. Both impact surfaces shall be clean and dry for testing. (3)(i) For a frontal impact test, suspend the head assembly...

  8. 10 CFR 431.193 - Test procedures for measuring energy consumption of distribution transformers.

    Science.gov (United States)

    2010-01-01

    ... distribution transformers. 431.193 Section 431.193 Energy DEPARTMENT OF ENERGY ENERGY CONSERVATION ENERGY EFFICIENCY PROGRAM FOR CERTAIN COMMERCIAL AND INDUSTRIAL EQUIPMENT Distribution Transformers Test Procedures § 431.193 Test procedures for measuring energy consumption of distribution transformers. The test...

  9. 78 FR 4060 - Manufactured Home Construction and Safety Standards, Test Procedures for Roof Trusses

    Science.gov (United States)

    2013-01-18

    ..., such as metal connector plates or wood gussets or their equivalents, uplift testing in Wind Zone I is.... SUMMARY: This final rule amends the roof truss testing procedures in the Federal Manufactured Home... testing procedures in 2003. In response to public comments, HUD returned the proposal to MHCC for further...

  10. 49 CFR 40.253 - What are the procedures for conducting an alcohol confirmation test?

    Science.gov (United States)

    2010-10-01

    ... FOR TRANSPORTATION WORKPLACE DRUG AND ALCOHOL TESTING PROGRAMS Alcohol Confirmation Tests § 40.253 What are the procedures for conducting an alcohol confirmation test? As the BAT conducting an alcohol... 49 Transportation 1 2010-10-01 2010-10-01 false What are the procedures for conducting an alcohol...

  11. 40 CFR 1051.501 - What procedures must I use to test my vehicles or engines?

    Science.gov (United States)

    2010-07-01

    ... vehicles or engines? 1051.501 Section 1051.501 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR POLLUTION CONTROLS CONTROL OF EMISSIONS FROM RECREATIONAL ENGINES AND VEHICLES Test Procedures § 1051.501 What procedures must I use to test my vehicles or engines? This section describes test...

  12. Test procedures, AN/AIC-27 system and component units. [for space shuttle

    Science.gov (United States)

    Reiff, F. H.

    1975-01-01

    The AN/AIC-27 (v) intercommunication system is a 30-channel audio distribution which consists of: air crew station units, maintenance station units, and a central control unit. A test procedure for each of the above units and also a test procedure for the system are presented. The intent of the test is to provide data for use in shuttle audio subsystem design.

  13. A testing procedure for wind turbine generators based on the power grid statistical model

    DEFF Research Database (Denmark)

    Farajzadehbibalan, Saber; Ramezani, Mohammad Hossein; Nielsen, Peter

    2017-01-01

    In this study, a comprehensive test procedure is developed to test wind turbine generators with a hardware-in-loop setup. The procedure employs the statistical model of the power grid considering the restrictions of the test facility and system dynamics. Given the model in the latent space, the j...

  14. 77 FR 10291 - Energy Conservation Program: Test Procedure for Commercial Refrigeration Equipment

    Science.gov (United States)

    2012-02-21

    ... rule include updating references to industry test procedures to their current versions, incorporating... sensors and controls, and allowing testing of certain commercial refrigeration equipment at the lowest.... Updated References to Industry Test Procedures to Their Most Current Versions 2. Inclusion of a Method for...

  15. High-Frequency Axial Fatigue Test Procedures for Spectrum Loading

    Science.gov (United States)

    2016-07-20

    closed-loop digital test frame controller with a command feedback compensation scheme was used to minimize controller error during testing. 15...controller response during variable amplitude loading, and a closed-loop digital test frame controller with a command feedback compensation scheme was...failures beyond 10 7 cycles can be caused by several competing failure mechanisms and may result in a transition from surface dominated crack

  16. Tank Monitoring and Control System (TMACS) Acceptance Test Procedure

    Energy Technology Data Exchange (ETDEWEB)

    BARNES, D.A.

    2000-06-01

    The purpose of this document is to describe tests performed to validate Revision 12.0 of the TMACS Monitor and Control System (TMACS) and verify that the software functions as intended by design. This document is intended to test the software portion of TMACS. The tests will be performed on the development system. The software to be tested is the TMACS knowledge bases (KB) and the I/O driver/services. The development system will not be communicating to field equipment; instead, the field equipment is simulated using emulators or multiplexers in the lab.

  17. Tank Monitoring and Control System (TMACS) Acceptance Test Procedure

    International Nuclear Information System (INIS)

    BARNES, D.A.

    2000-01-01

    The purpose of this document is to describe tests performed to validate Revision 12.0 of the TMACS Monitor and Control System (TMACS) and verify that the software functions as intended by design. This document is intended to test the software portion of TMACS. The tests will be performed on the development system. The software to be tested is the TMACS knowledge bases (KB) and the I/O driver/services. The development system will not be communicating to field equipment; instead, the field equipment is simulated using emulators or multiplexers in the lab

  18. Evaluation procedures for single axis sinusoidal test to design spectrum requirements

    International Nuclear Information System (INIS)

    Sun, P.C.; Javid, A.

    1983-01-01

    Two simple procedures are provided in this paper for the purpose of evaluating the adequacy of a single frequency single axis test. For the purpose of evaluating the adequacy of single frequency test to meet broad-band response spectrum requirements, the proposed procedure is based on the equivalence of maximum response of a dynamic system when it is subjected to either type of design input. The required information used for the evaluation is usually recorded and available in the test report. This procedure is applicable to systems with or without closely-spaced modes. When evaluating against broad-band design spectra and multi-axes requirements, an empirical procedure is proposed and it has been found conservative. These two proposed procedures provide a quick assessment on the adequacy of a single frequency test performed earlier. The use of these procedures may eliminate the need of expensive and time consuming equipment re-testing. (orig./HP)

  19. 49 CFR 219.611 - Test result indicating prohibited alcohol concentration; procedures.

    Science.gov (United States)

    2010-10-01

    ... concentration; procedures. 219.611 Section 219.611 Transportation Other Regulations Relating to Transportation... concentration; procedures. Procedures for administrative handling by the railroad in the event an employee's confirmation test indicates an alcohol concentration of .04 or greater are set forth in § 219.104. ...

  20. 78 FR 22536 - Procedural Manual for the Election Assistance Commission's Voting System Test Laboratories...

    Science.gov (United States)

    2013-04-16

    ... ELECTION ASSISTANCE COMMISSION Procedural Manual for the Election Assistance Commission's Voting...) is publishing a procedural manual for its Voting System Testing and Certification Program. This... draft procedural manual on or before 5:00 p.m. EDT on June 17, 2013. ADDRESSES: Submit comments via...

  1. 75 FR 74025 - Procedural Manual for the Election Assistance Commission's Voting System Testing and...

    Science.gov (United States)

    2010-11-30

    ... ELECTION ASSISTANCE COMMISSION Procedural Manual for the Election Assistance Commission's Voting... (EAC) is publishing a procedural manual for its Voting System Testing and Certification Program. This... procedural manual on or before 5 p.m. EDT on January 31, 2011. ADDRESSES: Submit comments via e-mail to...

  2. Evaluation of Surface Infiltration Testing Procedures in Permeable Pavement Systems

    Science.gov (United States)

    The ASTM method (ASTM C1701) for measuring infiltration rate of in-place pervious concrete provides limited guidance on how to select testing locations, so research is needed to evaluate how testing sites should be selected and how results should be interpreted to assess surface ...

  3. 40 CFR 60.474 - Test methods and procedures.

    Science.gov (United States)

    2010-07-01

    ... product is shingle or mineral-surfaced roll roofing, the tests shall be conducted while 106.6-kg (235-lb) shingle is being produced. (2) If the final product is saturated felt or smooth-surfaced roll roofing, the... fiberglass shingle, the test shall be conducted while a nominal 100-kg (220-lb) shingle is being produced. (b...

  4. Test Item Development: Validity Evidence from Quality Assurance Procedures.

    Science.gov (United States)

    Downing, Steven M.; Haladyna, Thomas M.

    1997-01-01

    An ideal process is outlined for test item development and the study of item responses to ensure that tests are sound. Qualitative and quantitative methods are used to assess the item-level validity evidence for high-stakes examinations. A checklist for assessment is provided. (SLD)

  5. 40 CFR 86.127-00 - Test procedures; overview.

    Science.gov (United States)

    2010-07-01

    ... (CONTINUED) CONTROL OF EMISSIONS FROM NEW AND IN-USE HIGHWAY VEHICLES AND ENGINES Emission Regulations for... of fueling, parking, and operating test conditions. Vehicles are tested for any or all of the... diluted exhaust is collected continuously for subsequent analysis, using a constant volume (variable...

  6. A procedure for empirical initialization of adaptive testing algorithms

    NARCIS (Netherlands)

    van der Linden, Willem J.

    1997-01-01

    In constrained adaptive testing, the numbers of constraints needed to control the content of the tests can easily run into the hundreds. Proper initialization of the algorithm becomes a requirement because the presence of large numbers of constraints slows down the convergence of the ability

  7. 40 CFR 51.357 - Test procedures and standards.

    Science.gov (United States)

    2010-07-01

    ... following steps: (i) Test equipment shall be connected to the fuel tank canister hose at the canister end... minutes and monitor for a sudden pressure drop, indicating that the fuel tank was pressurized. (v) The... be performed without repair or adjustment at the inspection facility, prior to the test, except as...

  8. Investigation into the comparative severity of practical thermal test procedures

    International Nuclear Information System (INIS)

    Shultz, K.R.; White, M.C.; Gordon, G.

    In the advisory material for the application of the IAEA Transport Regulations three methods for determining whether a type B radioactive material packaging can withstand hypothetical fire conditions are presented. These comprise an open fire test and two tests involving exposure of the packaging in a furnace. The first furnace test (method I) uses a materials testing type of furnace and the second (method II) uses a heat-treatment furnace. Under method I the packaging is heated for 35 minutes from ambient temperature by firing the furnace so that its temperature increases in accordance with an ISO standard fire curve; under method II the heating is for 30 minutes at 800 0 C. Tests were carried out to detarmine if these tests were of comparable severity, and on which temperature the control of furnace firing in method I should be based. It was concluded that method II was the more severe test, and that furance wall temperatues are the dominant factor in determining heat exchange to specimens in the furnaces used. Furnace walls should meet or exceed the standard fire curve set out in the ISO standard. The characteristics of the furnances and specimens were not sufficiently understood to be able to predict the behaviour of the specimens

  9. Tank Monitoring and Control System (TMACS) Acceptance Test Procedure

    International Nuclear Information System (INIS)

    WANDLING, R.R.

    1999-01-01

    The purpose of this document is to describe tests performed to validate Revision 11.2 of the TMACS Monitor and Control System (TMCACS) and verify that the software functions as intended by design. The tests will be performed on the development system. The software to be tested is the TMACS knowledge bases (KB) and the I/O driver/services. The development system will not be talking to field equipment; instead, the field equipment is simulated using emulators or multiplexers in the lab

  10. Adhesion testing procedure for hot-poured crack sealants.

    Science.gov (United States)

    2008-11-01

    Crack sealing is a common pavement maintenance treatment because it extends pavement service life significantly. : However, crack sealant often fails prematurely due to a loss of adhesion. Because current test methods are mostly : empirical and only ...

  11. Acceptance test procedure MICON software exhaust fan control modifications; TOPICAL

    International Nuclear Information System (INIS)

    SILVAN, G.R.

    1999-01-01

    This acceptance test verifies the MICON program changes for the new automatic transfer switch ATS-2 alarms, the Closed Loop Cooling isolator status, the CB-3 position alarm, and the alarms for the new emergency fan damper backup air compressor

  12. MAC mini acceptance test procedure, software Version 3.0

    International Nuclear Information System (INIS)

    Russell, V.K.

    1994-01-01

    The K Basins Materials Accounting (MAC) programs had some major improvements made to it to organize the main-tables by Location, Canister, and Material. This ATP describes how the code was to be tested to verify its correctness

  13. Improvement in Shrimp Hatchery Procedures for Toxicity Tests

    International Nuclear Information System (INIS)

    Nor Azizah Marsiddi; Fazliana Mohd Saaya; Anee Suryani Sued

    2015-01-01

    Toxicity testing of brine shrimp Artemia salina Brine shrimp lethality assay is a screening test to determine half the dose mortality (LC50) for its shrimp given certain herbal extract at a concentration tested. The shrimp child mortality half a dose indicator to determine level of toxicity before further testing done on animal cell culture and animal experiments also on the mouse. The use of new hardware, namely Artemio 1 has increased its shrimp production at a rate that more and faster than the use of the black box hatching previously taken from the method by Solis, 1993. brine shrimp eggs from Artemio mix also easier to use because it contains egg and sea salt have been ready mixed for use in experiments. In conclusion, this method improvements help increase the number of offspring produced shrimp and produce experimental method easier than previous methods. (author)

  14. Single specimen fracture toughness determination procedure using instrumented impact test

    International Nuclear Information System (INIS)

    Rintamaa, R.

    1993-04-01

    In the study a new single specimen test method and testing facility for evaluating dynamic fracture toughness has been developed. The method is based on the application of a new pendulum type instrumented impact tester equipped with and optical crack mouth opening displacement (COD) extensometer. The fracture toughness measurement technique uses the Double Displacement Ratio (DDR) method, which is based on the assumption that the specimen is deformed as two rigid arms that rotate around an apparent centre of rotation. This apparent moves as the crack grows, and the ratio of COD versus specimen displacement changes. As a consequence the onset ductile crack initiation can be detected on the load-displacement curve. Thus, an energy-based fracture toughness can be calculated. In addition the testing apparatus can use specimens with the Double ligament size as compared with the standard Charpy specimen which makes the impact testing more appropriate from the fracture mechanics point of view. The novel features of the testing facility and the feasibility of the new DDR method has been verified by performing an extensive experimental and analytical study. (99 refs., 91 figs., 27 tabs.)

  15. A simplified test procedure for determining the effectiveness of adsorbents for the removal of methyl iodide

    International Nuclear Information System (INIS)

    Underhill, D.W.

    1993-01-01

    ASTM Test Procedure D3803 measures the ability of nuclear-grade carbon to remove methyl iodide from a stream of humidified air. This test, unlike all the other procedures developed by ASTM Committee D28, has evolved to become extremely complex. The intricacy of this test as well as the great difficulty in obtaining inter-laboratory agreement, creates doubt as tot the actual meaning of the results. Here a far simpler test system is described in which thermodynamic principles are used to maintain a constant, reproducible test procedure. This paper describes a system implementing these elements, its cost to build, and the factors affecting its accuracy. 11 refs., 1 fig

  16. Acceptance Test Procedure for New Pumping Instrumentation and Control Skid ''V''

    International Nuclear Information System (INIS)

    KOCH, M.R.

    2000-01-01

    This Acceptance Test Procedure (ATP) provides for the inspection and testing of the new Pumping Instrumentation and Control (PIC) skid designated as ''V''. The ATP will be performed after the construction of the PIC skid in the fabrication shop

  17. Acceptance Test Procedure for New Pumping Instrumentation and Control Skid R

    International Nuclear Information System (INIS)

    KOCH, M.R.

    2000-01-01

    This Acceptance Test Procedure (ATP) provides for the inspection and testing of the new Pumping Instrumentation and Control (PIC) skid designed as ''R''. The ATP will be performed after the construction of the PIC skid in the fabrication shop

  18. Acceptance Test Procedure for New Pumping Instrumentation and Control Skid ''P''

    International Nuclear Information System (INIS)

    KOCH, M.R.

    2000-01-01

    This Acceptance Test Procedure (ATP) provides for the inspection and testing of the new Pumping Instrumentation and Control (PIC) skid designed as ''P''. The ATP will be performed after the construction of the PIC skid in the fabrication shop

  19. Acceptance Test Procedure for New Pumping Instrumentation and Control Skid ''U''

    International Nuclear Information System (INIS)

    KOCH, M.R.

    2000-01-01

    This Acceptance Test Procedure (ATP) provides for the inspection and testing of the new Pumping Instrumentation and Control (PIC) skid designed as ''U''. The ATP will be performed after the construction of the PIC skid in the fabrication shop

  20. Acceptance Test Procedure for New Pumping Instrumentation and Control Skid ''T''

    International Nuclear Information System (INIS)

    KOCH, M.R.

    2000-01-01

    This Acceptance Test Procedure (ATP) provides for the inspection and testing of the new Pumping Instrumentation and Control (PIC) skid designated as ''T''. The ATP will be performed after the construction of the PIC skid in the fabrication shop

  1. Acceptance Test Procedure for New Pumping and Instrumentation Control Skid N

    International Nuclear Information System (INIS)

    KOCH, M.R.

    1999-01-01

    This Acceptance Test Procedure (ATP) provides for the inspection and testing of the new Pumping and Instrumentation Control (PIC) skid designed as ''N''. The ATP will be performed after the construction of the PIC skid in the shop

  2. Acceptance Test Procedure for New Pumping Instrumentation and Control Skid T

    International Nuclear Information System (INIS)

    KOCH, M.R.

    2000-01-01

    This Acceptance Test Procedure (ATP) provides for the inspection and testing Of the new Pumping Instrumentation and Control (PIC) skid designed as ''T''. The ATP will be performed after the construction of the PIC skid in the fabrication shop

  3. Acceptance Test Procedure for New Pumping and Instrumentation Control Skid L

    International Nuclear Information System (INIS)

    KOCH, M.R.

    1999-01-01

    This Acceptance Test Procedure (ATP) provides for the inspection and testing of the new Pumping and Instrumentation Control (PIC) skid designed as ''L''. The ATP will be performed after the construction of the PIC skid in the shop

  4. 78 FR 45010 - Modifications to the Disability Determination Procedures; Extension of Testing of Some Disability...

    Science.gov (United States)

    2013-07-25

    ... SOCIAL SECURITY ADMINISTRATION [Docket No. SSA-2013-0030] Modifications to the Disability Determination Procedures; Extension of Testing of Some Disability Redesign Features AGENCY: Social Security Administration. ACTION: Notice of the extension of tests involving modifications to the disability determination...

  5. 77 FR 35464 - Modifications to the Disability Determination Procedures; Extension of Testing of Some Disability...

    Science.gov (United States)

    2012-06-13

    ... SOCIAL SECURITY ADMINISTRATION [Docket No. SSA-2012-0029] Modifications to the Disability Determination Procedures; Extension of Testing of Some Disability Redesign Features AGENCY: Social Security Administration. ACTION: Notice of the Extension of Tests Involving Modifications to the Disability Determination...

  6. Acceptance Test Procedure for New Pumping Instrumentation and Control Skid V

    International Nuclear Information System (INIS)

    KOCH, M.R.

    2000-01-01

    This Acceptance Test Procedure (ATP) provides for the inspection and testing of the new Pumping Instrumentation and Control. (PIC) skid designed as ''V''. The ATP will be performed after the construction of the PIC skid in the fabrication shop

  7. Acceptance Test Procedure for New Pumping Instrumentation and Control Skid W

    International Nuclear Information System (INIS)

    KOCH, M.R.

    2000-01-01

    This Acceptance Test Procedure (ATP) provides for the inspection and testing of the new Pumping Instrumentation and Control (PIC) skid designed as ''W''. The ATP will be performed after the construction of the PIC skid in the fabrication shop

  8. 75 FR 71570 - Energy Conservation Program: Test Procedures for Fluorescent Lamp Ballasts

    Science.gov (United States)

    2010-11-24

    ... validity. In contrast, NEMA noted that for the ballast efficiency (BE) measurement proposed in the NOPR... measurement variation and testing burden compared to the existing test procedure. In contrast to BEF and RSE...

  9. RADIOACTIVE DEMONSTRATION OF FINAL MINERALIZED WASTE FORMS FOR HANFORD WASTE TREATMENT PLANT SECONDARY WASTE BY FLUIDIZED BED STEAM REFORMING USING THE BENCH SCALE REFORMER PLATFORM

    Energy Technology Data Exchange (ETDEWEB)

    Crawford, C.; Burket, P.; Cozzi, A.; Daniel, W.; Jantzen, C.; Missimer, D.

    2012-02-02

    ceramic (mineral) waste form. The mineral waste form that is produced by co-processing waste with kaolin clay in an FBSR process has been shown to be as durable as LAW glass. Monolithing of the granular FBSR product is being investigated to prevent dispersion during transport or burial/storage, but is not necessary for performance. A Benchscale Steam Reformer (BSR) was designed and constructed at the SRNL to treat actual radioactive wastes to confirm the findings of the non-radioactive FBSR pilot scale tests and to qualify the waste form for applications at Hanford. BSR testing with WTP SW waste surrogates and associated analytical analyses and tests of granular products (GP) and monoliths began in the Fall of 2009, and then was continued from the Fall of 2010 through the Spring of 2011. Radioactive testing commenced in 2010 with a demonstration of Hanford's WTP-SW where Savannah River Site (SRS) High Level Waste (HLW) secondary waste from the Defense Waste Processing Facility (DWPF) was shimmed with a mixture of {sup 125/129}I and {sup 99}Tc to chemically resemble WTP-SW. Prior to these radioactive feed tests, non-radioactive simulants were also processed. Ninety six grams of radioactive granular product were made for testing and comparison to the non-radioactive pilot scale tests. The same mineral phases were found in the radioactive and non-radioactive testing.

  10. Operability test procedure for 244-U DCRT. Revision 1

    International Nuclear Information System (INIS)

    Erhart, M.F.

    1995-01-01

    This OPT will insure the operability of various systems and their general equipment, used in the operation of the 244-U DCRT. Systems that will be tested include the following: Leak Detection Systems; Heat Trace System; Vessel Temperature Measurement System; Dip Tube Water System; Weight Factor and Specific Gravity System; Instrument Air System; Vessel Liquid Level System; Vessel Liquid Transfer System; and Exhauster Differential Pressure Indicating Controller System. The tests will cover checks on equipment operation and electrical interlocks, but will not cover checks on associated annunciator alarms which are covered in a separate OTP

  11. 77 FR 26471 - Procedures for Transportation Workplace Drug and Alcohol Testing Programs: 6-acetylmorphine (6-AM...

    Science.gov (United States)

    2012-05-04

    ...). Consumption of food products (e.g., poppy seeds) must not be considered a legitimate medical explanation for... 2105-AE14 Procedures for Transportation Workplace Drug and Alcohol Testing Programs: 6-acetylmorphine... Department is amending certain provisions of its drug testing procedures for 6-acetylmorphine (6-AM), a...

  12. 78 FR 63410 - Energy Conservation Program for Consumer Products: Test Procedures for Direct Heating Equipment...

    Science.gov (United States)

    2013-10-24

    ... Conservation Program for Consumer Products: Test Procedures for Direct Heating Equipment and Pool Heaters... test procedures for direct heating equipment and pool heaters established under the Energy Policy and... covered products at least once every seven years. For direct heating equipment, the proposed amendments...

  13. 76 FR 63211 - Energy Efficiency Program: Test Procedures for Residential Water Heaters, Direct Heating...

    Science.gov (United States)

    2011-10-12

    ... Efficiency Program: Test Procedures for Residential Water Heaters, Direct Heating Equipment, and Pool Heaters... residential water heaters, direct heating equipment, and pool heaters. This rulemaking is intended to fulfill... water heaters, possible clarifications and improvement of the direct heating equipment test procedures...

  14. 76 FR 34801 - Petition for Modification of Single Car Air Brake Test Procedures

    Science.gov (United States)

    2011-06-14

    ... reference in 49 CFR 232.305) is intended for freight cars with automatic brake systems that are...] Petition for Modification of Single Car Air Brake Test Procedures In accordance with Part 232 of Title 49... Railroad Administration (FRA) grant a modification of the single car air brake test procedures as...

  15. 30 CFR 56.19120 - Procedures for inspection, testing, and maintenance.

    Science.gov (United States)

    2010-07-01

    ... 30 Mineral Resources 1 2010-07-01 2010-07-01 false Procedures for inspection, testing, and... LABOR METAL AND NONMETAL MINE SAFETY AND HEALTH SAFETY AND HEALTH STANDARDS-SURFACE METAL AND NONMETAL MINES Personnel Hoisting Inspection and Maintenance § 56.19120 Procedures for inspection, testing, and...

  16. 30 CFR 57.19120 - Procedures for inspection, testing, and maintenance.

    Science.gov (United States)

    2010-07-01

    ... 30 Mineral Resources 1 2010-07-01 2010-07-01 false Procedures for inspection, testing, and... LABOR METAL AND NONMETAL MINE SAFETY AND HEALTH SAFETY AND HEALTH STANDARDS-UNDERGROUND METAL AND NONMETAL MINES Personnel Hoisting Inspection and Maintenance § 57.19120 Procedures for inspection, testing...

  17. 75 FR 42611 - Energy Conservation Program for Consumer Products: Test Procedure for Microwave Ovens

    Science.gov (United States)

    2010-07-22

    ... for Microwave Ovens AGENCY: Office of Energy Efficiency and Renewable Energy, Department of Energy... current active mode provisions in its test procedure for microwave ovens do not produce accurate and... concerns with the DOE microwave oven cooking efficiency test procedure. Elsewhere in today's Federal...

  18. 10 CFR 431.16 - Test procedures for the measurement of energy efficiency.

    Science.gov (United States)

    2010-01-01

    ... 10 Energy 3 2010-01-01 2010-01-01 false Test procedures for the measurement of energy efficiency. 431.16 Section 431.16 Energy DEPARTMENT OF ENERGY ENERGY CONSERVATION ENERGY EFFICIENCY PROGRAM FOR... Methods of Determining Efficiency § 431.16 Test procedures for the measurement of energy efficiency. For...

  19. 77 FR 28673 - Energy Conservation Program for Consumer Products: Test Procedures for Residential Furnace Fans

    Science.gov (United States)

    2012-05-15

    ... multipliers based on climate, consumer behavior assumptions, and product characteristics (e.g., multi-stage or... Conservation Program for Consumer Products: Test Procedures for Residential Furnace Fans; Proposed Rule #0;#0... Conservation Program for Consumer Products: Test Procedures for Residential Furnace Fans AGENCY: Office of...

  20. 75 FR 8528 - Procedures for Transportation Workplace Drug and Alcohol Testing Programs

    Science.gov (United States)

    2010-02-25

    ... OST 2105-AD84 Procedures for Transportation Workplace Drug and Alcohol Testing Programs AGENCY: Office... technical amendments to its drug and alcohol testing procedures to authorize employers to begin using the... INFORMATION CONTACT: For program issues, Bohdan Baczara, Office of Drug and Alcohol Policy and Compliance...

  1. 75 FR 8526 - Procedures for Transportation Workplace Drug and Alcohol Testing Programs

    Science.gov (United States)

    2010-02-25

    ... 2105-AD64 Procedures for Transportation Workplace Drug and Alcohol Testing Programs AGENCY: Office of..., U.S. Department of Transportation, Office of Drug and Alcohol Policy and Compliance, 1200 New Jersey.... PART 40--PROCEDURES FOR TRANSPORTATION WORKPLACE DRUG AND ALCOHOL TESTING PROGRAMS 0 Accordingly, the...

  2. Building Energy Simulation Test for Existing Homes (BESTEST-EX); Phase 1 Test Procedure: Building Thermal Fabric Cases

    Energy Technology Data Exchange (ETDEWEB)

    Judkoff, R.; Polly, B.; Bianchi, M.; Neymark, J.

    2010-08-01

    The U.S. Department of Energy tasked NREL to develop a process for testing the reliability of models that predict retrofit energy savings, including their associated calibration methods. DOE asked NREL to conduct the work in phases so that a test procedure would be ready should DOE need it to meet legislative requirements related to residential retrofits in FY 2010. This report documents the initial 'Phase 1' test procedure.

  3. CENRTC Project number-sign 2F3EOA, OCB A-376, acceptance test procedure

    International Nuclear Information System (INIS)

    Akerson, A.W.

    1995-01-01

    This test procedure provides the steps necessary to verify correct functional operation of controls, annunciators, alarms, protective relays and related systems impacted by CENRTC number-sign 2F3E0A, Microwave Transfer Trip Project, modification work performed under work package 6B-93-00041/M. This procedure separates three tests into separate sections: energization of A-376 duplex panel and circuits; SCADA tests; and A-376 local trip tests

  4. Parametric Sensitivity Tests—European Polymer Electrolyte Membrane Fuel Cell Stack Test Procedures

    DEFF Research Database (Denmark)

    Araya, Samuel Simon; Andreasen, Søren Juhl; Kær, Søren Knudsen

    2014-01-01

    performed based on test procedures proposed by a European project, Stack-Test. The sensitivity of a Nafion-based low temperature PEMFC stack’s performance to parametric changes was the main objective of the tests. Four crucial parameters for fuel cell operation were chosen; relative humidity, temperature......, pressure, and stoichiometry at varying current density. Furthermore, procedures for polarization curve recording were also tested both in ascending and descending current directions....

  5. Test plan: Potash Core Test. WIPP experimental program borehole plugging

    International Nuclear Information System (INIS)

    Christensen, C.L.

    1979-09-01

    The Potash Core Test will utilize a WIPP emplaced plug to obtain samples of an in-situ cured plug of known mix constituents for bench scale testing. An earlier effort involved recovery at the salt horizon of Plug 217, a 17 year old plug in a potash exploration hole for bond testing, but the lack of particulars in the emplacement precluded significant determination of plug performance

  6. 40 CFR 90.408 - Pre-test procedures.

    Science.gov (United States)

    2010-07-01

    ....408 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED... during service accumulation is allowed only in accordance with § 90.118. (b) Engine pre-test preparation... by § 90.324(a). If necessary, allow the heated sample line, filters, and pumps to reach operating...

  7. 40 CFR 91.408 - Pre-test procedures.

    Science.gov (United States)

    2010-07-01

    ....408 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED... accordance with § 91.117. (b) Engine pre-test preparation. (1) Drain and charge the fuel tank(s) with the..., including the sample probe, using mode 1 from Table 2 in appendix A of this subpart. The emission sampling...

  8. Testing Policy as Part of Kindergarten Entrance Procedures.

    Science.gov (United States)

    Tanner, C. Kenneth; And Others

    1993-01-01

    Examines the appropriateness of using the ABC Inventory and the Developing Skills Checklists to identify or label kindergartners for special education assistance. Data were collected on 92 subjects, including participants in a special instructional assistance program and a comparison group. Findings indicate that using either test for identifying…

  9. 40 CFR 90.404 - Test procedure overview.

    Science.gov (United States)

    2010-07-01

    ... brake-specific emissions of hydrocarbons, carbon monoxide, carbon dioxide, and oxides of nitrogen and... also designed to determine the brake-specific emissions of non-methane hydrocarbons. The test consists... is for Class I-A, III, IV, and V engines (see § 90.103(a) and § 90.116(b) for the definitions of...

  10. 40 CFR 86.527-90 - Test procedures, overview.

    Science.gov (United States)

    2010-07-01

    ... (CONTINUED) CONTROL OF EMISSIONS FROM NEW AND IN-USE HIGHWAY VEHICLES AND ENGINES Emission Regulations for... sequences of fueling, parking, and operating conditions. (c) The exhaust emission test is designed to... constant volume (variable dilution) sampler. (d) Except in cases of component malfunction or failure, all...

  11. 40 CFR 86.127-96 - Test procedures; overview.

    Science.gov (United States)

    2010-07-01

    ... (CONTINUED) CONTROL OF EMISSIONS FROM NEW AND IN-USE HIGHWAY VEHICLES AND ENGINES Emission Regulations for... consists of prescribed sequences of fueling, parking, and operating conditions. Vehicles are tested for any... volume (variable dilution) sampler or critical flow venturi sampler. (c) The diesel-cycle exhaust...

  12. 40 CFR 86.154-98 - Measurement procedure; refueling test.

    Science.gov (United States)

    2010-07-01

    ... concentration of methanol as described in § 86.133-96(i)(6). (6) Within one minute of obtaining the initial FID... immediately prior to the test. Warning: If at any time the concentration of hydrocarbons, of methanol, or of methanol and hydrocarbons exceeds 15,000 ppm C, the enclosure should be immediately purged. This...

  13. 40 CFR 60.46 - Test methods and procedures.

    Science.gov (United States)

    2010-07-01

    ... material balance over the steam generating system shall be used to confirm the rate. (d) The owner or...-Fired Steam Generators for Which Construction Is Commenced After August 17, 1971 § 60.46 Test methods... D2015, or D5865 (solid fuels), D240 (liquid fuels), or D1826 (gaseous fuels) (all of these methods are...

  14. Start-Stop Test Procedures on the PEMFC Stack Level

    DEFF Research Database (Denmark)

    Mitzel, Jens; Nygaard, Frederik; Veltzé, Sune

    The test is addressed to investigate the influence on stack durability of a long stop followed by a restart of a stack. Long stop should be defined as a stop in which the anodic compartment is fully filled by air due to stack leakages. In systems, leakage level of the stack is low and time to fil...

  15. 40 CFR 85.1414 - Alternative test procedures.

    Science.gov (United States)

    2010-07-01

    ... (CONTINUED) CONTROL OF AIR POLLUTION FROM MOBILE SOURCES Urban Bus Rebuild Requirements § 85.1414 Alternative... shall be representative of in-use urban bus operation. The requestor shall supply relevant technical... test is representative of in-use urban bus operation, the Agency shall determine whether to set such...

  16. 40 CFR 91.118 - Certification procedure-testing.

    Science.gov (United States)

    2010-07-01

    ... 2000 based on the function 151+557/P 0.9 where P=average power of an engine family in kW (sales... compliance with the Family Emission Limit (FEL). (ii) Prior to the performance of such a test, the... adjustable range of that parameter, to determine whether the engine conforms to the applicable Family...

  17. 40 CFR 61.304 - Test methods and procedures.

    Science.gov (United States)

    2010-07-01

    ...) Calibrate and install a pressure measurement device (liquid manometer, magnehelic gauge, or equivalent... pressured to during the most recent vapor-tightness test. (2) Connect the pressure measurement device to a pressure tap in the affected facility's vapor collection system, located as close as possible to the...

  18. 14 CFR Appendix F to Part 23 - Test Procedure

    Science.gov (United States)

    2010-01-01

    ... specimen must be supported vertically. The specimen must be exposed to a Bunsen or Tirrill burner with a.... The specimen must be exposed to a Bunsen burner or Tirrill burner with a nominal 3/8-inch I.D. tube... test. The specimens must be exposed to a Bunsen or Tirrill burner with a nominal 3/8 inch I.D. tube...

  19. Hydrothermal and alkaline hydrothermal pretreatments plus anaerobic digestion of sewage sludge for dewatering and biogas production: Bench-scale research and pilot-scale verification.

    Science.gov (United States)

    Li, Chunxing; Wang, Xingdong; Zhang, Guangyi; Yu, Guangwei; Lin, Jingjiang; Wang, Yin

    2017-06-15

    To test the feasibility and practicability of the process combing hydrothermal pretreatment for dewatering with biogas production for full utilization of sewage sludge, hydrothermal/alkaline hydrothermal pretreatments and in turn anaerobic digestion of the filtrates obtained after dewatering the pretreated sludge were performed at bench- and pilot-scales. The hydrothermal temperature fell within the range of 140 °C-220 °C and the pretreatment time varied from 30 min to 120 min. For the alkaline hydrothermal pretreatment the pH value of the sludge was adjusted to 9.0-11.0 by adding Ca(OH) 2 . The results showed that the dewaterability of the sewage sludge was improved with increasing pretreatment temperature but the impact of the pretreatment time was not significant. The addition of Ca(OH) 2 gave better performance on the subsequent mechanical dewatering of the pretreated sludge compared to pure hydrothermal pretreatment, and the higher the pH value was, the better the dewaterability of the pretreated sludge was. The conditions of 180 °C/30 min and 160 °C/60 min/pH = 10.0 (for hydrothermal and alkaline hydrothermal pretreatments, respectively) resulted in relatively good results in the theoretical energy balance, which were verified in the pilot-scale tests. Based on the data from the pilot tests, the alkaline hydrothermal process realized self-sufficiency in energy at the cost of a proper amount of CaO. Copyright © 2017 Elsevier Ltd. All rights reserved.

  20. Soil washing physical separations test procedure - 300-FF-1 operable unit

    International Nuclear Information System (INIS)

    Belden, R.D.

    1993-01-01

    This procedure provides the operations approach, a field sampling plan, and laboratory procedures for a soil washing test to be conducted by Alternative Remedial Technologies, Inc. (ART) in the 300-FF-1 area at the Hanford site. The open-quotes Quality Assurance Project Plan for the Soil Washing Physical Separations Test, 300-FF-1 Operable Unit,close quotes Hanford, Washington, Alternative Remedial Technologies, Inc., February 1994 (QAPP) is provided in a separate document that presents the procedural and organizational guidelines for this test. This document describes specifications, responsibilities, and general procedures to be followed to conduct physical separation soil treatability tests in the North Process Pond of the 300-FF-1 Operable Unit (OU) at the Hanford Site. These procedures are based on the open-quotes 300-FF-1 Physical Separations CERCLA Treatability Test Plan, DOE/RL 92-2l,close quotes (DOE-RL 1993)

  1. Comparison of likelihood testing procedures for parallel systems with covariances

    International Nuclear Information System (INIS)

    Ayman Baklizi; Isa Daud; Noor Akma Ibrahim

    1998-01-01

    In this paper we considered investigating and comparing the behavior of the likelihood ratio, the Rao's and the Wald's statistics for testing hypotheses on the parameters of the simple linear regression model based on parallel systems with covariances. These statistics are asymptotically equivalent (Barndorff-Nielsen and Cox, 1994). However, their relative performances in finite samples are generally known. A Monte Carlo experiment is conducted to stimulate the sizes and the powers of these statistics for complete samples and in the presence of time censoring. Comparisons of the statistics are made according to the attainment of assumed size of the test and their powers at various points in the parameter space. The results show that the likelihood ratio statistics appears to have the best performance in terms of the attainment of the assumed size of the test. Power comparisons show that the Rao statistic has some advantage over the Wald statistic in almost all of the space of alternatives while likelihood ratio statistic occupies either the first or the last position in term of power. Overall, the likelihood ratio statistic appears to be more appropriate to the model under study, especially for small sample sizes

  2. Building Energy Simulation Test for Existing Homes (BESTEST-EX): Instructions for Implementing the Test Procedure, Calibration Test Reference Results, and Example Acceptance-Range Criteria

    Energy Technology Data Exchange (ETDEWEB)

    Judkoff, R.; Polly, B.; Bianchi, M.; Neymark, J.; Kennedy, M.

    2011-08-01

    This publication summarizes building energy simulation test for existing homes (BESTEST-EX): instructions for implementing the test procedure, calibration tests reference results, and example acceptance-range criteria.

  3. 105-KE Isolation Barrier leak rate acceptance test procedure WHC-SD-SNF-ATP-005

    International Nuclear Information System (INIS)

    Whitehurst, R.; McCracken, K.; Papenfuss, J.N.

    1994-01-01

    This document establishes the procedure for performing the acceptance test on the two isolation barriers being installed in K East basin. This acceptance test procedure shall be used to : First establish a basin water loss rate prior to installation of the two isolation barriers between the main basin and the discharge chute in K-Basin East. Second, perform an acceptance test to verify an acceptable leakage rate through the barrier seals. This Acceptance Test Procedure (ATP) has been prepared in accordance with CM-6-1 EP 4.2, Standard Engineering Practices

  4. MBA acceptance test procedures, software Version 1.4

    International Nuclear Information System (INIS)

    Mullaney, J.E.; Russell, V.K.

    1994-01-01

    The Mass Balance Program (MBA) is an adjunct to the Materials Accounting database system, Version 3.4. MBA was written to equip the personnel performing K-Basin encapsulation tasks with a conservative estimate of accumulated sludge during the processing of canisters into and out of the chute. The K Basins Materials Balance programs had some minor improvements made to it to feedback the chute processing status to the operator better. This ATP describes how the code was to be tested to verify its correctness

  5. Increasing Desalination by Mitigating Anolyte pH Imbalance Using Catholyte Effluent Addition in a Multi-Anode Bench Scale Microbial Desalination Cell

    KAUST Repository

    Davis, Robert J.

    2013-09-03

    A microbial desalination cell (MDC) uses exoelectrogenic bacteria to oxidize organic matter while desalinating water. Protons produced from the oxidation of organics at the anode result in anolyte acidification and reduce performance. A new method was used here to mitigate anolyte acidification based on adding non-buffered saline catholyte effluent from a previous cycle to the anolyte at the beginning of the next cycle. This method was tested using a larger-scale MDC (267 mL) containing four anode brushes and a three cell pair membrane stack. With an anolyte salt concentration increased by an equivalent of 75 mM NaCl using the catholyte effluent, salinity was reduced by 26.0 ± 0.5% (35 g/L NaCl initial solution) in a 10 h cycle, compared to 18.1 ± 2.0% without catholyte addition. This improvement was primarily due to the increase in buffering capacity of the anolyte, although increased conductivity slightly improved performance as well. There was some substrate loss from the anolyte by diffusion into the membrane stack, but this was decreased from 11% to 2.6% by increasing the anolyte conductivity (7.6 to 14 mS/cm). These results demonstrated that catholyte effluent can be utilized as a useful product for mitigating anolyte acidification and improving MDC performance. © 2013 American Chemical Society.

  6. Apparatus and Experimental Procedures to Test Crystal Collimation

    CERN Document Server

    Montesano, S

    2012-01-01

    UA9 is an experimental setup operated in the CERN-SPS in view of investigating the feasibility of halo collimation assisted by bent crystals. The test collimation system is composed of one crystal acting as primary halo deflector in the horizontal plane and an absorber. Different crystals are tested in turn using two-arm goniometers with an angular reproducibility of better than 10 microrad. The performance of the system is assessed through the study of the secondary and tertiary halo in critical areas, by using standard machine instrumentation and few customized equipments. The alignment of the crystal is verified by measuring the loss rate close to the crystal position. The collimation efficiency is computed by intercepting the deflected halo with a massive collimator or with an imaging device installed into a Roman Pot. The leakage of the system is evaluated in the dispersion suppressor by means of movable aperture restrictions. In this contribution the setup and the experimental methods in use are revisit...

  7. Operability test procedure for TRUSAF assayer software upgrade

    International Nuclear Information System (INIS)

    Cejka, C.C.

    1995-01-01

    This OTP is to be used to ensure the operability of the Transuranic Waste Assay System (TRUWAS). The system was upgraded and requires a retest to assure satisfactory operation. The upgrade consists of an AST 486 computer to replace the IBM-PC/XT, and a software upgrade (CNEUT). The software calculations are performed in the same manner as in the previous system (NEUT), however, the new software is written in C Assembly Language. CNEUT is easier to use and far more powerful than the previous program. The TRUWAS is used to verify the TRU content of waste packages sent for storage in the Transuranic Storage and Assay Facility (TRUSAF). The TRUSAF is part of Westinghouse Hanford's certification program for waste to be shipped to the Waste Isolation Pilot Plant (WIPP) in New Mexico. The Transuranic Waste Assayer uses a combination passive-active neutron interrogation system to determine the TRU content of 55-gallon waste drums. The system consists of a shielded assay chamber; Deuterium-Tritium neutron generator; Helium-3 proportional counters; drum handling system; electronics including preamplifier, amplifier, and discriminator for each of the counter packages; and an AST 486 computer/printer system for data acquisition and analysis. The system can detect down to TRU levels of 10 nCi/g in the waste matrix. The equipment to be tested is: Assay Chamber Door Drum Turntable and Automatic Loading Platform Interlocks Assayer Software; and IBM computer/printer software. The objective of the test is to verify that the system is operational with the AST 486 computer, the software used in the new computer system correctly calculates TRU levels, and the new computer system is capable of storing and retrieving data

  8. Comparison of Test Administration Procedures for Placement Decisions in a Mathematics Course.

    Science.gov (United States)

    Straetmans, Gerard J. J. M.; Eggen, Theo J. H. M.

    1998-01-01

    Three test administration procedures for making placement decisions in adult education were compared (paper-based, computer-based, and computerized-adaptive tests) with 90 adult-education students. Test performance was not differentially affected by the mode of administration, but the computerized adaptive test always yielded more precise ability…

  9. 76 FR 50145 - Energy Conservation Program: Test Procedures for Residential Clothes Dryers

    Science.gov (United States)

    2011-08-12

    ... electronic comments in WordPerfect, Microsoft Word, PDF, or ASCII file format and avoid the use of special... dryer and room air conditioner test procedures concerning the active mode for these products. 76 FR 972... testing revealed that all of the clothes dryers tested significantly over-dried the DOE test load to near...

  10. Acceptance test procedure for the 105-KW isolation barrier leak rate

    Energy Technology Data Exchange (ETDEWEB)

    McCracken, K.J.

    1995-05-19

    This acceptance test procedure shall be used to: First establish a basin water loss rate prior to installation of the two isolation barriers between the main basin and the discharge chute in K-Basin West. Second, perform an acceptance test to verify an acceptable leakage rate through the barrier seals. This Acceptance Test Procedure (ATP) has been prepared in accordance with CM-6-1 EP 4.2, Standard Engineering Practices.

  11. [Voluntary testing procedures of farm animal housing equipment according to the Animal Welfare Act of 1998].

    Science.gov (United States)

    Hesse, D; Knierim, U; von Borell, E; Herrmann, H; Koch, L; Müller, C; Rauch, H W; Sachser, N; Schwabenbauer, K; Zerbe, F

    1999-04-01

    Before its broad application in practice, housing equipment should be tested, in particular with regard to animal welfare. The differing positions of the German Federal Council (Bundesrat) and the German Federal Parliament (Bundestag), whether such testing should be mandatory or voluntary, have been conciliated in the amended animal welfare act by empowering the Federal Ministry of Food, Agriculture and Fisheries (BML) to fix official standards for voluntary testing procedures by regulation. On request of the BML, a report as scientific basis for a draft regulation is currently prepared by the scientific animal welfare committee of the German Agricultural Society (DLG). The scientific animal welfare committee has been appointed by the DLG in order to provide support in the effort to strengthen animal welfare aspects in the DLG-utility testing procedure of housing equipment, which is in place since 1953. The committee elaborates standards concerning testing methods, assessment criteria and the necessary size of investigations. As required, the scientific animal welfare committee may support the DLG-testing bodies in the implementation of the animal welfare part of the testing procedure. It will, moreover, be involved in the welfare assessment based on the testing results. The amendments of the already established testing procedure will help to fulfill the general requirements on an acceptable animal welfare testing procedure. While keeping in mind that there are certain limits in what can be achieved by a voluntary testing procedure, the enhanced consideration of animal welfare aspects within the DLG-utility testing procedure has the advantage to be relatively unbureaucratic and in line with EU legislation, and is, therefore, an appropriate tool for a contibrution to improved animal welfare in livestock housing.

  12. THOR Bench-Scale Steam Reforming Demonstration

    Energy Technology Data Exchange (ETDEWEB)

    D. W. Marshall; N. R. Soelberg; K. M. Shaber

    2003-05-01

    The Idaho Nuclear Technology and Engineering Center (INTEC) was home to nuclear fuel reprocessing activities for decades at the Idaho National Engineering and Environmental Laboratory. As a result of the reprocessing activities, INTEC has accumulated approximately one million gallons of acidic, radioactive, sodium-bearing waste (SBW). The purpose of this demonstration was to investigate a reforming technology, offered by THORsm Treatment Technologies, LLC, for treatment of SBW into a "road ready" waste form that would meet the waste acceptance criteria for the Waste Isolation Pilot Plant (WIPP). A non-radioactive simulated SBW was used based on the known composition of waste tank WM-180 at INTEC. Rhenium was included as a non-radioactive surrogate for technetium. Data was collected to determine the nature and characteristics of the product, the operability of the technology, the composition of the off-gases, and the fate of key radionuclides (cesium and technetium) and volatile mercury compounds. The product contained a low fraction of elemental carbon residues in the cyclone and filter vessel catches. Mercury was quantitatively stripped from the product but cesium, rhenium (Tc surrogate), and the heavy metals were retained. Nitrates were not detected in the product and NOx destruction exceeded 98%. The demonstration was successful.

  13. TWR Bench-Scale Steam Reforming Demonstration

    Energy Technology Data Exchange (ETDEWEB)

    Marshall, D.W.; Soelberg, N.R.

    2003-05-21

    The Idaho Nuclear Technology and Engineering Center (INTEC) was home to nuclear fuel reprocessing activities for decades at the Idaho National Engineering and Environmental Laboratory. As a result of the reprocessing activities, INTEC has accumulated approximately one million gallons of acidic, radioactive, sodium-bearing waste (SBW). The purpose of this demonstration was to investigate a reforming technology, offered by ThermoChem Waste Remediation, LLC, (TWR) for treatment of SBW into a ''road ready'' waste form that would meet the waste acceptance criteria for the Waste Isolation Pilot Plant (WIPP). TWR is the licensee of Manufacturing Technology Conservation International (MTCI) steam-reforming technology in the field of radioactive waste treatment. A non-radioactive simulated SBW was used based on the known composition of waste tank WM-180 at INTEC. Rhenium was included as a non-radioactive surrogate for technetium. Data was collected to determine the nature and characteristics of the product, the operability of the technology, the composition of the off-gases, and the fate of key radionuclides (cesium and technetium) and volatile mercury compounds. The product contained a low fraction of elemental carbon residues in the cyclone and filter vessel catches. Mercury was quantitatively stripped from the product but cesium, rhenium (Tc surrogate), and the heavy metals were retained. Nitrate residues were about 400 ppm in the product and NOx destruction exceeded 86%. The demonstration was successful.

  14. TWR Bench-Scale Steam Reforming Demonstration

    Energy Technology Data Exchange (ETDEWEB)

    D. W. Marshall; N. R. Soelberg

    2003-05-01

    The Idaho Nuclear Technology and Engineering Center (INTEC) was home to nuclear fuel reprocessing activities for decades at the Idaho National Engineering and Environmental Laboratory. As a result of the reprocessing activities, INTEC has accumulated approximately one million gallons of acidic, radioactive, sodium-bearing waste (SBW). The purpose of this demonstration was to investigate a reforming technology, offered by ThermoChem Waste Remediation, LLC, (TWR) for treatment of SBW into a "road ready" waste form that would meet the waste acceptance criteria for the Waste Isolation Pilot Plant (WIPP). TWR is the licensee of Manufacturing Technology Conservation International (MTCI) steam-reforming technology in the field of radioactive waste treatment. A non-radioactive simulated SBW was used based on the known composition of waste tank WM-180 at INTEC. Rhenium was included as a non-radioactive surrogate for technetium. Data was collected to determine the nature and characteristics of the product, the operability of the technology, the composition of the off-gases, and the fate of key radionuclides (cesium and technetium) and volatile mercury compounds. The product contained a low fraction of elemental carbon residues in the cyclone and filter vessel catches. Mercury was quantitatively stripped from the product but cesium, rhenium (Tc surrogate), and the heavy metals were retained. Nitrate residues were about 400 ppm in the product and NOx destruction exceeded 86%. The demonstration was successful.

  15. THOR Bench-Scale Steam Reforming Demonstration

    Energy Technology Data Exchange (ETDEWEB)

    Marshall, D.W.; Soelberg, N.R.; Shaber, K.M.

    2003-05-21

    The Idaho Nuclear Technology and Engineering Center (INTEC) was home to nuclear fuel reprocessing activities for decades at the Idaho National Engineering and Environmental Laboratory. As a result of the reprocessing activities, INTEC has accumulated approximately one million gallons of acidic, radioactive, sodium-bearing waste (SBW). The purpose of this demonstration was to investigate a reforming technology, offered by THORsm Treatment Technologies, LLC, for treatment of SBW into a ''road ready'' waste form that would meet the waste acceptance criteria for the Waste Isolation Pilot Plant (WIPP). A non-radioactive simulated SBW was used based on the known composition of waste tank WM-180 at INTEC. Rhenium was included as a non-radioactive surrogate for technetium. Data was collected to determine the nature and characteristics of the product, the operability of the technology, the composition of the off-gases, and the fate of key radionuclides (cesium and technetium) and volatile mercury compounds. The product contained a low fraction of elemental carbon residues in the cyclone and filter vessel catches. Mercury was quantitatively stripped from the product but cesium, rhenium (Tc surrogate), and the heavy metals were retained. Nitrates were not detected in the product and NOx destruction exceeded 98%. The demonstration was successful.

  16. THOR Bench-Scale Steam Reforming Demonstration

    International Nuclear Information System (INIS)

    Marshall, D.W.; Soelberg, N.R.; Shaber, K.M.

    2003-01-01

    The Idaho Nuclear Technology and Engineering Center (INTEC) was home to nuclear fuel reprocessing activities for decades at the Idaho National Engineering and Environmental Laboratory. As a result of the reprocessing activities, INTEC has accumulated approximately one million gallons of acidic, radioactive, sodium-bearing waste (SBW). The purpose of this demonstration was to investigate a reforming technology, offered by THORsm Treatment Technologies, LLC, for treatment of SBW into a ''road ready'' waste form that would meet the waste acceptance criteria for the Waste Isolation Pilot Plant (WIPP). A non-radioactive simulated SBW was used based on the known composition of waste tank WM-180 at INTEC. Rhenium was included as a non-radioactive surrogate for technetium. Data was collected to determine the nature and characteristics of the product, the operability of the technology, the composition of the off-gases, and the fate of key radionuclides (cesium and technetium) and volatile mercury compounds. The product contained a low fraction of elemental carbon residues in the cyclone and filter vessel catches. Mercury was quantitatively stripped from the product but cesium, rhenium (Tc surrogate), and the heavy metals were retained. Nitrates were not detected in the product and NOx destruction exceeded 98%. The demonstration was successful

  17. Surfactant studies for bench-scale operation

    Science.gov (United States)

    Hickey, Gregory S.; Sharma, Pramod K.

    1993-01-01

    A phase 2 study has been initiated to investigate surfactant-assisted coal liquefaction, with the objective of quantifying the enhancement in liquid yields and product quality. This report covers the second quarter of work. The major accomplishments were: completion of coal liquefaction autoclave reactor runs with Illinois number 6 coal at processing temperatures of 300, 325, and 350 C, and pressures of 1800 psig; analysis of the filter cake and the filtrate obtained from the treated slurry in each run; and correlation of the coal conversions and the liquid yield quality to the surfactant concentration. An increase in coal conversions and upgrading of the liquid product quality due to surfactant addition was observed for all runs.

  18. 77 FR 74559 - Energy Conservation Program for Consumer Products: Test Procedures for Residential Water Heaters...

    Science.gov (United States)

    2012-12-17

    ... Energy (DOE) is amending its test procedures for residential water heaters, direct heating equipment (DHE... procedures for residential water heaters include a full- year accounting of energy use, both electricity and... water heaters already account for standby mode and off mode energy consumption. III. Discussion In the...

  19. 76 FR 56347 - Energy Conservation Program for Consumer Products: Test Procedures for Residential Water Heaters...

    Science.gov (United States)

    2011-09-13

    ... procedure for residential water heaters fully addresses standby mode and off mode energy consumption, this... DEPARTMENT OF ENERGY 10 CFR Part 430 [Docket No. EERE-2009-BT-TP-0013] RIN 1904-AB95 Energy Conservation Program for Consumer Products: Test Procedures for Residential Water Heaters, Direct Heating...

  20. Robustness of Two-Level Testing Procedures under Distortions of First Level Statistics

    OpenAIRE

    Kostevich, A. L.; Nikitina, I. S.

    2007-01-01

    We investigate robustness of some two-level testing procedures under distortions induced by using an asymptotic distribution of first level statistics instead of an exact one. We demonstrate that ignoring the distortions results in unreliable conclusions and we propose robustness conditions for the two-level procedures.

  1. 78 FR 19606 - Energy Conservation Program for Consumer Products: Test Procedures for Residential Furnace Fans

    Science.gov (United States)

    2013-04-02

    ... Procedures for Residential Furnace Fans AGENCY: Office of Energy Efficiency and Renewable Energy, Department... referred to as ``furnace fans.'' DOE proposes a test procedure that would be applicable to furnace fans..., even though DOE interprets its authority as encompassing more than just circulation fans used in...

  2. 40 CFR 63.8687 - What performance tests, design evaluations, and other procedures must I use?

    Science.gov (United States)

    2010-07-01

    ... evaluations, and other procedures must I use? 63.8687 Section 63.8687 Protection of Environment ENVIRONMENTAL... What performance tests, design evaluations, and other procedures must I use? (a) You must conduct each... run must last at least 1 hour. (e) You must use the following equations to determine compliance with...

  3. 40 CFR 63.7112 - What performance tests, design evaluations, and other procedures must I use?

    Science.gov (United States)

    2010-07-01

    ... evaluations, and other procedures must I use? 63.7112 Section 63.7112 Protection of Environment ENVIRONMENTAL..., design evaluations, and other procedures must I use? (a) You must conduct each performance test in Table... use wet dust suppression to control PM from PSH operations, a visible mist is sometimes generated by...

  4. 16 CFR 1611.33 - Test procedures for textile fabrics and film.

    Science.gov (United States)

    2010-01-01

    ... 16 Commercial Practices 2 2010-01-01 2010-01-01 false Test procedures for textile fabrics and film. 1611.33 Section 1611.33 Commercial Practices CONSUMER PRODUCT SAFETY COMMISSION FLAMMABLE FABRICS ACT... procedures for textile fabrics and film. (a)(1) All textile fabrics (except those with a nitro-cellulose...

  5. 10 CFR 431.444 - Test procedures for the measurement of energy efficiency.

    Science.gov (United States)

    2010-01-01

    ... 10 Energy 3 2010-01-01 2010-01-01 false Test procedures for the measurement of energy efficiency. 431.444 Section 431.444 Energy DEPARTMENT OF ENERGY ENERGY CONSERVATION ENERGY EFFICIENCY PROGRAM FOR... procedures for the measurement of energy efficiency. (a) Scope. Pursuant to section 346(b)(1) of EPCA, this...

  6. Eficiencia del proceso de lavado en la obtención del citrato de calcio y magnesio a escala de banco Effectiveness of washout process to obtain calcium and magnesium citrate at bench scale

    Directory of Open Access Journals (Sweden)

    Jorge E Rodríguez Chanfrau

    2010-03-01

    Full Text Available Como parte de la optimización del proceso tecnológico para obtener citrato de calcio y magnesio a partir de dolomitas, se estudió a escala de banco la etapa de lavado para disminuir el contenido de ácido cítrico libre. Las variantes de lavado estudiadas permitieron disminuir el contenido de ácido cítrico libre por debajo del 3 %, mientras que los valores de calcio y magnesio son similares a los del lote antes de realizar el proceso de lavado. Por otro lado, el estudio toxicológico en ratas, comprobó que los lotes a los cuales se les aplicó las diferentes variantes de lavado no provocaron irritabilidad gástrica a las dosis de 2 000 mg/kg de peso corporal, por lo que se puede afirmar que el proceso de lavado establecido es adecuado para garantizar la calidad de la materia prima.As part of the technological process optomization to obtain calcium citrate and magnesium from dolomites, we studied at bench scale, the washout stage to decrease the free citric acid content. Washout variants allowed to decrease the free citric acid content under 3 %, whereas the calcium and magnesium values are similar to those of batch before to carry out the wahout process. On the other hand, toxicity study in rats, proved that the batches where different washout variables were applied not provoke gastric irritability at doses of 2 000 mg/kg of body weight confirming that above mentioned established process is approproate to guarantee the raw material quality.

  7. CENRTC Project number-sign 2F3EOA, OCB A-386, acceptance test procedure

    International Nuclear Information System (INIS)

    Akerson, A.W.

    1995-01-01

    This test procedure provides the steps necessary to verify correct functional operation of controls, annunciators, alarms, protective relays and related systems impacted by CENRTC number-sign 2F3EOA, Microwave Transfer Trip Project, modification work performed under work package 6B-93-00043/M (CENRTC 2F3EOA MWTT OCB A-386 PACKAGE). This procedure separates four tests into separate sections: Energization of A-386 Duplex Panel and Circuits; Local RFL 6750 function tests and start-up; SCADA tests; and A-386 local trip tests

  8. Characterization Test Procedures for Intersection Collision Avoidance Systems Based on Vehicle-to-Vehicle Communications

    Science.gov (United States)

    2015-12-01

    Characterization test procedures have been developed to quantify the performance of intersection collision avoidance (ICA) systems based on vehicle-to-vehicle communications. These systems warn the driver of an imminent crossing-path collision at a r...

  9. 76 FR 56339 - Energy Conservation Program for Consumer Products: Test Procedures for Residential Furnaces and...

    Science.gov (United States)

    2011-09-13

    ...-Conditioning and Warm Air Heating Equipment and Commercial and Industrial Refrigeration Equipment Manufacturing... Refrigeration Institute (AHRI) recommended that to avoid unnecessary burden, the existing test procedure..., and Refrigeration Institute's Directory of Certified Product Performance for Residential Furnaces and...

  10. A Comparison of Procedures for Content-Sensitive Item Selection in Computerized Adaptive Tests.

    Science.gov (United States)

    Kingsbury, G. Gage; Zara, Anthony R.

    1991-01-01

    This simulation investigated two procedures that reduce differences between paper-and-pencil testing and computerized adaptive testing (CAT) by making CAT content sensitive. Results indicate that the price in terms of additional test items of using constrained CAT for content balancing is much smaller than that of using testlets. (SLD)

  11. Soil-contact decay tests using small blocks : a procedural analysis

    Science.gov (United States)

    Rodney C. De Groot; James W. Evans; Paul G. Forsyth; Camille M. Freitag; Jeffrey J. Morrell

    Much discussion has been held regarding the merits of laboratory decay tests compared with field tests to evaluate wood preservatives. In this study, procedural aspects of soil jar decay tests with 1 cm 3 blocks were critically examined. Differences among individual bottles were a major source of variation in this method. The reproducibility and sensitivity of the soil...

  12. 49 CFR Appendix C to Part 173 - Procedure for Base-level Vibration Testing

    Science.gov (United States)

    2010-10-01

    ... 49 Transportation 2 2010-10-01 2010-10-01 false Procedure for Base-level Vibration Testing C... Base-level Vibration Testing Base-level vibration testing shall be conducted as follows: 1. Three... platform. 4. Immediately following the period of vibration, each package shall be removed from the platform...

  13. 49 CFR 232.307 - Modification of the single car air brake test procedures.

    Science.gov (United States)

    2010-10-01

    ... Requirements § 232.307 Modification of the single car air brake test procedures. (a) Request. The AAR or other authorized representative of the railroad industry may seek modification of the single car air brake test... 49 Transportation 4 2010-10-01 2010-10-01 false Modification of the single car air brake test...

  14. 78 FR 7681 - Energy Conservation Program for Consumer Products: Test Procedures for Residential Furnaces and...

    Science.gov (United States)

    2013-02-04

    ...-up tests specified in 9.5 and 9.6 may be omitted on such units. In lieu of conducting the cool-down... the tester to skip the heat-up and cool-down tests. This error carries through to the software... units have no measurable off-cycle airflow in a separate, ongoing test procedure rulemaking for furnaces...

  15. Test Operations Procedure (TOP) 02-2-603A Vehicle Fuel Consumption

    Science.gov (United States)

    2012-05-10

    Final 3. DATES COVERED (From - To) 4. TITLE AND SUBTITLE Test Operations Procedure (TOP) 02-2-603A Vehicle Fuel Consumption 5a. CONTRACT...test methods used to measure and present the fuel consumption characteristics for wheeled and tracked vehicles. Specific facilities, instrumentation...test controls, and analysis techniques are presented. 15. SUBJECT TERMS fuel consumption traction battery hybrid

  16. 75 FR 38422 - Procedures for Transportation Workplace Drug and Alcohol Testing Programs

    Science.gov (United States)

    2010-07-02

    ... 2105-AD84 Procedures for Transportation Workplace Drug and Alcohol Testing Programs AGENCY: Office of..., Bohdan Baczara, Office of Drug and Alcohol Policy and Compliance, 1200 New Jersey Avenue, SE., Washington..., Alcohol abuse, Alcohol testing, Drug abuse, Drug testing, Laboratories, Reporting and recordkeeping...

  17. 75 FR 5722 - Procedures for Transportation Workplace Drug and Alcohol Testing Programs

    Science.gov (United States)

    2010-02-04

    ... 2105-AD95 Procedures for Transportation Workplace Drug and Alcohol Testing Programs AGENCY: Office of..., Senior Policy Advisor (S- 1), Office of Drug and Alcohol Policy and Compliance, 1200 New Jersey Ave., SE..., Alcohol testing, Drug abuse, Drug testing, Laboratories, Reporting and recordkeeping requirements, Safety...

  18. 75 FR 26183 - Procedures for Transportation Workplace Drug and Alcohol Testing Programs

    Science.gov (United States)

    2010-05-11

    ... 2105-AE01 Procedures for Transportation Workplace Drug and Alcohol Testing Programs AGENCY: Office of...: For program issues, Bohdan Baczara, Office of Drug and Alcohol Policy and Compliance, 1200 New Jersey..., Alcohol abuse, Alcohol testing, Drug abuse, Drug testing, Laboratories, Reporting and recordkeeping...

  19. Investigation of Bending Test Procedures for Engineered Polymer Composite Railroad Ties

    Science.gov (United States)

    2016-12-01

    ER D C/ CE RL C R- 16 -6 Investigation of Bending Test Procedures for Engineered Polymer Composite Railroad Ties Co ns tr uc tio n En...Test Procedures for Engineered Polymer Composite Railroad Ties Claire G. Ball CTL Group 5400 Old Orchard Road Skokie, IL 60077 Final report...conducting in- vestigations to help develop and evaluate engineered polymer composite railroad ties since 1993. Recent efforts, through funding and

  20. Preanalytical errors in primary healthcare: a questionnaire study of information search procedures, test request management and test tube labelling.

    Science.gov (United States)

    Söderberg, Johan; Brulin, Christine; Grankvist, Kjell; Wallin, Olof

    2009-01-01

    Most errors in laboratory medicine occur in the preanalytical phase and are the result of human mistakes. This study investigated information search procedures, test request management and test tube labelling in primary healthcare compared to the same procedures amongst clinical laboratory staff. A questionnaire was completed by 317 venous blood sampling staff in 70 primary healthcare centres and in two clinical laboratories (response rate = 94%). Correct procedures were not always followed. Only 60% of the primary healthcare staff reported that they always sought information in the updated, online laboratory manual. Only 12% reported that they always labelled the test tubes prior to drawing blood samples. No major differences between primary healthcare centres and clinical laboratories were found, except for test tube labelling, whereby the laboratory staff reported better practices. Re-education and access to documented routines were not clearly associated with better practices. The preanalytical procedure in the surveyed primary healthcare centres was associated with a risk of errors which could affect patient safety. To improve patient safety in laboratory testing, all healthcare providers should survey their preanalytical procedures and improve the total testing process with a systems perspective.

  1. Test and evaluation procedures for Sandia's Teraflops Operating System (TOS) on Janus.

    Energy Technology Data Exchange (ETDEWEB)

    Barnette, Daniel Wayne

    2005-10-01

    This report describes the test and evaluation methods by which the Teraflops Operating System, or TOS, that resides on Sandia's massively-parallel computer Janus is verified for production release. Also discussed are methods used to build TOS before testing and evaluating, miscellaneous utility scripts, a sample test plan, and a proposed post-test method for quickly examining the large number of test results. The purpose of the report is threefold: (1) to provide a guide to T&E procedures, (2) to aid and guide others who will run T&E procedures on the new ASCI Red Storm machine, and (3) to document some of the history of evaluation and testing of TOS. This report is not intended to serve as an exhaustive manual for testers to conduct T&E procedures.

  2. Design of test and emergency procedures to improve operator behaviour in French nuclear power plants

    International Nuclear Information System (INIS)

    Griffon-Fouco, M.; Gomolinski, M.

    1982-09-01

    The incident analyses performed in French nuclear power plants high-lighted that deficiencies in the design of procedures are frequent causes of human errors. The process for developing new guidelines for the writing of test and emergency procedures is presented: this process is based on operators interviews and observations at the plants or at simulators. The main principles for the writing of procedures are developed. For example: - the elaboration of a procedure for action and of a separate educational procedure, - the coordination of crew responses, - the choice of vocabulary, graphs, flow charts and so on as regards the format. Other complementary actions, such as the training of operators in the use of procedures, are described

  3. Development and pilot testing of full-scale membrane distillation modules for deployment of waste heat

    NARCIS (Netherlands)

    Jansen, A.E.; Assink, J.W.; Hanemaaijer, J.H.; Medevoort, J. van; Sonsbeek, E. van

    2013-01-01

    Membrane distillation is an attractive technology for extracting fresh water from seawater. Newly developed modules have been used in pilot tests and bench scale tests to demonstrate the potential of producing excellent product water quality in a single step, little need for water pretreatment and a

  4. The Effects of Dynamic Assessment Procedures on Raven Matrices Performance, Visual Search Behavior, Test Anxiety and Test Orientation.

    Science.gov (United States)

    Bethge, Hans-Jorg; And Others

    1982-01-01

    Dynamic assessment procedures involving either verbalization or elaborated feedback lead to higher levels of Ravens Matrices performance, modified visual search behaviors, reduced test anxiety, and reduced negative orientations to the testing situation in third graders. Results are interpreted on offering construct validation to the assessment…

  5. A testing procedure for triaxial tests and a numerical method for the calculation of powder flow properties

    NARCIS (Netherlands)

    Eelkman Rooda, J.; Haaker, G.

    1977-01-01

    A testing procedure for measuring flow properties of powders is developed which makes it possible to use results from triaxial tests in the Jenike bin theory. For the elaboration of the results a numerical method is used, based upon the Warren Spring equation (τ/C)N = (σ + T)/T. In this equation σ

  6. Candidate reagents and procedures for the dissolution of Hanford Site single-shell tank sludges

    International Nuclear Information System (INIS)

    Schulz, W.W.; Kupfer, M.J.

    1991-10-01

    At least some of the waste in the 149 single-shell tanks (SST) at the US Department of Energy (DOE) Hanford Site will be retrieved, treated, and disposed of. Although the importance of devising efficient and cost-effective sludge dissolution procedures has long been recognized, a concerted bench-scale effort to devise and test such procedures with actual solids representative of those in Hanford Site SSTs has not been performed. Reagents that might be used, either individually or serially, to dissolve sludges include HNO 3 , HNO 3 -oxalic acid, and HNO 3 -HF. This report consolidates and updates perspectives and recommendations concerning reagents and procedures for dissolving Hanford Site SST and selected double-shell tank (DST) sludges. The principal objectives of this report are as follows: (1) Compile and review existing experimental data on dissolution of actual Hanford Site SST and DST sludges. (2) Further inform Hanford Site engineers and scientists concerning the utility of combinations of thermally unstable complexants (TUCS) reagents and various reducing agents for dissolving SST and DST sludges. (This latter technology has recently been explored at the Argonne National Laboratory.) (3) Provide guidance in laying out a comprehensive experimental program to develop technology for dissolving all types of Hanford Site SST and DST sludges. 6 refs., 1 fig., 4 tabs

  7. EFAM GTP 02 - the GKSS test procedure for determining the fracture behaviour of materials

    International Nuclear Information System (INIS)

    Schwalbe, K.H.; Heerens, J.; Zerbst, U.; Kocak, M.

    2002-01-01

    This document describes a unified fracture mechanics test method in procedural form for quasi-static testing of materials. It is based on the ESIS Procedures P1 and P2 and introduces additional features, such as middle cracked tension specimens, shallow cracks, the δ 5 crack tip opening displacement, the crack tip opening angle, the rate of dissipated energy, testing of weldments, and guidance for statistical treatment of scatter. Special validity criteria are given for tests on specimens with low constraint. This document represents an updated version of EFAM GTP 94. (orig.) [de

  8. Test Operations Procedure (TOP) 01-2-603 Rotorcraft Laboratory Vibration Test Schedules

    Science.gov (United States)

    2017-06-12

    NIST). The validity of equipment calibration was verified prior to test . C.3 TEST OBJECTIVE. The objective of the test was to develop new LVTS...Endurance test duration. C.5.6 Reliability Test Considerations. a. The LVTSs as published in this TOP have been compressed to provide the equivalent of...2500 hours of flight in four hours of runtime per axis. For reliability testing it is sometimes desired to operate a test item for hundreds of hours in

  9. Review of Test Procedure for Determining HSPFs of Residential Variable-Speed Heat Pumps

    Energy Technology Data Exchange (ETDEWEB)

    Rice, C. Keith [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Munk, Jeffrey D. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Shrestha, Som S. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

    2015-08-01

    This report reviews the suitability of the existing Heating Seasonal Performance Factor (HSPF) ratings and testing requirements for the current generation of variable-speed (VS) air-source heat pumps. Recent field test results indicate larger discrepancies between rated HSPF and field-observed HSPF for VS models than for single-speed models in the same houses. These findings suggest that the heating season test and ratings procedure should be revisited for VS heat pumps. The ratings and testing procedures are described in ANSI/AHRI 210/240 (2008) for single-speed, two-capacity, and variable-speed units. Analysis of manufacturer and independent test performance data on VS units reveals why the current VS testing/ratings procedure results in overly optimistic HSPF ratings for some VS units relative to other types of heat pumps. This is due to a combination of extrapolation of low speed test data beyond the originally anticipated ambient temperature operating range and the constraints of unit controls, which prevent low speed operation over the range of ambient temperatures assumed in the procedure for low speed. As a result, the HSPFs of such units are being overpredicted relative to those for single- and two-capacity designs. This overprediction has been found to be significantly reduced by use in the HSPF ratings procedure of an alternative higher-load heating load line, described in a companion report (Rice et al., 2015).

  10. Interim test methods and procedures for determining the performance of small photovoltaic systems

    Energy Technology Data Exchange (ETDEWEB)

    McNutt, P.; Kroposki, B.; Hansen, R.; DeBlasio, R.

    1998-07-01

    This document provides test methods and procedures for determining the performance of small stand-alone and utility-grid connected PV systems. The procedures in this document provide a common approach for evaluating whether a given PV system is suitable to perform the function it was designed and manufactured to accomplish and meet the application load. This test document fills a testing void and provides the catalyst and focus for establishing the technical foundation and bridging the institutional barriers needed to reduce uncertainty that a system`s performance will be what its designers and builders claim. The need for this document was recently made more apparent with the initiation of a PV Global Approval Program (PVGAP) at the international level and is in response to concerns that PV systems being fielded must meet performance standards and that these standards include system-level performance type tests. The title of these test procedures is prefaced with the word interim because experience in using the procedures is needed before a consensus standard is developed and accepted by the PV community through its activities with the IEEE Standards Coordinating Committee 21 (SCC21) and International Electrotechnical Commission Technical Committee 82 (IEC TC82) national and international standards-making bodies. Both entities have initiated projects to develop test standards and will need the technical basis and validation of test procedures such as those presented in this document before a consensus is achieved by the PV community.

  11. Testing procedures based on the empirical characteristic functions II: k-sample problem, change point problem

    Czech Academy of Sciences Publication Activity Database

    Hušková, Marie; Meintanis, S. G.

    2008-01-01

    Roč. 39, - (2008), s. 235-243 ISSN 1210-3195 Grant - others:GA AV(CZ) GA201/06/0186 Institutional research plan: CEZ:AV0Z10750506 Keywords : goodness-of-fit test * symmetry test * test for independence Subject RIV: BB - Applied Statistics, Operational Research http://library.utia.cas.cz/separaty/2008/SI/huskova- test ing procedures based on the empirical characteristic functions ii k-sample problem change point problem.pdf

  12. An Iterative Procedure for Efficient Testing of B2B: A Case in Messaging Service Tests

    Energy Technology Data Exchange (ETDEWEB)

    Kulvatunyou, Boonserm [ORNL

    2007-03-01

    Testing is a necessary step in systems integration. Testing in the context of inter-enterprise, business-to-business (B2B) integration is more difficult and expensive than intra-enterprise integration. Traditionally, the difficulty is alleviated by conducting the testing in two stages: conformance testing and then interoperability testing. In conformance testing, systems are tested independently against a reference system. In interoperability testing, they are tested simultaneously against one another. In the traditional approach for testing, these two stages are performed sequentially with little feedback between them. In addition, test results and test traces are left only to human analysis or even discarded if the solution passes the test. This paper proposes an approach where test results and traces from both the conformance and interoperability tests are analyzed for potential interoperability issues; conformance test cases are then derived from the analysis. The result is that more interoperability issues can be resolved in the lower-cost conformance testing mode; consequently, time and cost required for achieving interoparble solutions are reduced.

  13. Test Plan for Cask Identification Detector

    Energy Technology Data Exchange (ETDEWEB)

    Rauch, Eric Benton [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2016-09-29

    This document serves to outline the testing of a Used Fuel Cask Identification Detector (CID) currently being designed under the DOE-NE MPACT Campaign. A bench-scale prototype detector will be constructed and tested using surrogate neutron sources. The testing will serve to inform the design of the full detector that is to be used as a way of fingerprinting used fuel storage casks based on the neutron signature produced by the used fuel inside the cask.

  14. ENRAF Series 854 Advanced Technology Gauge (ATG) with SPU ll Card for Leak Detector Use Acceptance Test Procedure

    International Nuclear Information System (INIS)

    SMITH, S.G.

    1999-01-01

    The following Acceptance Test Procedure was written to test the Enraf Series 854 ATG with SPU-II card prior to installation in the Tank Farms. The procedure sets various parameters and verifies the gauge and the alarms functionality

  15. Initial land reclamation procedures related to possible Pu-cleanup activities at the Tonopah Test Range

    International Nuclear Information System (INIS)

    Wallace, A.; Romney, E.M.

    1976-02-01

    If areas of the Tonopah Test Range (TTR) are to be used for experimental tests of procedures for clean-up of 239 Pu contamination, there are experiences in the Great Basin Desert portions of the Nevada Test Site (NTS) which can serve as guides to reclamation and revegetation of such arid lands. Procedures which will encourage development of the grasses Hilaria jamesii and Oryzopsis hymenoides, as well as the perennial shrubs Eurotia lanata and Atriplex canescens would greatly improve the area as range land

  16. Acceptance Test Procedure for New Pumping Instrumentation and Control Skid ''V''

    International Nuclear Information System (INIS)

    KOCH, M.R.

    2000-01-01

    This Acceptance Test Procedure (ATP) verifies proper construction per the design drawings and tests for proper functioning of the Pumping Instrumentation and Control (PIC) skid ''V''. The scope section lists the systems and functions to be checked. This ATP will be performed at the Site Fabrication Services (SFS) shop upon completion of the construction of the PIC skid

  17. 76 FR 25211 - Energy Conservation Program: Test Procedures for Fluorescent Lamp Ballasts

    Science.gov (United States)

    2011-05-04

    ... resistor loads. If DOE determines that amendments to the fluorescent lamp ballast energy conservation... the ballast test load is a resistor. DOE also believed that the use of electrical measurements and the... DOE's observations and arguments regarding the drawbacks of the resistor-based test procedure and the...

  18. 75 FR 14287 - Energy Conservation Program: Test Procedures for Fluorescent Lamp Ballasts

    Science.gov (United States)

    2010-03-24

    ... Procedure Improvement Options 1. Resistor-Based Ballast Efficiency Correlated to Ballast Efficacy Factor 2..., and Results 7. Resistor Value Determination 8. Non-Operational Ballasts When Connected to a Resistor 9... Ballasts 4. Resistor-based Ballast Efficiency Test Method 5. Alternative Approaches to Amending the Test...

  19. 76 FR 971 - Energy Conservation Program for Consumer Products: Test Procedures for Clothes Dryers and Room...

    Science.gov (United States)

    2011-01-06

    ... Conditioner Standby Mode and Off Mode Testing a. Clothes Dryers b. Room Air Conditioners 4. Calculation of... Conditioner Active Mode Test Procedures 1. Correction of Text Describing Energy Factor Calculation for Clothes... the Per-Cycle Gas Dryer Continuously Burning Pilot Light Gas Energy Consumption 9. Clarification of...

  20. 75 FR 37593 - Energy Conservation Program for Consumer Products: Test Procedures for Clothes Dryers and Room...

    Science.gov (United States)

    2010-06-29

    ... Testing a. Clothes Dryers b. Room Air Conditioners 4. Calculation of Energy Use Associated With Standby... Mode Test Procedures 1. Correction of Text Describing Energy Factor Calculation for Clothes Dryers 2... Gas Dryer Continuously Burning Pilot Light Gas Energy Consumption 9. Clarification of the Gas Supply...

  1. Resampling-based multiple comparison procedure with application to point-wise testing with functional data.

    Science.gov (United States)

    Vsevolozhskaya, Olga A; Greenwood, Mark C; Powell, Scott L; Zaykin, Dmitri V

    2015-03-01

    In this paper we describe a coherent multiple testing procedure for correlated test statistics such as are encountered in functional linear models. The procedure makes use of two different p -value combination methods: the Fisher combination method and the Šidák correction-based method. P -values for Fisher's and Šidák's test statistics are estimated through resampling to cope with the correlated tests. Building upon these two existing combination methods, we propose the smallest p -value as a new test statistic for each hypothesis. The closure principle is incorporated along with the new test statistic to obtain the overall p -value and appropriately adjust the individual p -values. Furthermore, a shortcut version for the proposed procedure is detailed, so that individual adjustments can be obtained even for a large number of tests. The motivation for developing the procedure comes from a problem of point-wise inference with smooth functional data where tests at neighboring points are related. A simulation study verifies that the methodology performs well in this setting. We illustrate the proposed method with data from a study on the aerial detection of the spectral effect of below ground carbon dioxide leakage on vegetation stress via spectral responses.

  2. 49 CFR 572.75 - Lumbar spine, abdomen, and pelvis assembly and test procedure.

    Science.gov (United States)

    2010-10-01

    ... 49 Transportation 7 2010-10-01 2010-10-01 false Lumbar spine, abdomen, and pelvis assembly and...) ANTHROPOMORPHIC TEST DEVICES 6-Year-Old Child § 572.75 Lumbar spine, abdomen, and pelvis assembly and test procedure. (a) Lumbar spine, abdomen, and pelvis assembly. The lumbar spine, abdomen, and pelvis consist of...

  3. 77 FR 28519 - Test Procedure Guidance for Room Air Conditioners, Residential Dishwashers, and Residential...

    Science.gov (United States)

    2012-05-15

    ..., along with simple instructions on how to access all documents, including public comments, in the docket... information regarding the current practices of manufacturer-run and private testing facilities. The Department seeks to understand how interested parties have interpreted test procedures provisions that they believe...

  4. 77 FR 8178 - Test Procedures for Central Air Conditioners and Heat Pumps: Public Meeting

    Science.gov (United States)

    2012-02-14

    ..., manufacturers inquired how to test and rate condensing units and outdoor units using R-22 refrigerant. DOE has.... EERE-2010-BT-TP-0038] Test Procedures for Central Air Conditioners and Heat Pumps: Public Meeting... . Participants are responsible for ensuring that their systems are compatible with the webinar software...

  5. Standard testing procedures for optical fiber and unshielded twisted pair at Sandia National Laboratories

    Energy Technology Data Exchange (ETDEWEB)

    Adams, R.L.

    1993-11-01

    This document will establish a working standard for testing optical fiber and unshielded twisted pair cables included in the Lab-wide telecommunications cabling system. The purpose of these standard testing procedures is to deliver to all Sandians a reliable, low-maintenance, state-of-the-art, ubiquitous telecommunications cabling infrastructure capable of satisfying all current and future telecommunication needs.

  6. MOT Test Procedures. Youth Training Scheme. Core Exemplar Work Based Project.

    Science.gov (United States)

    Further Education Staff Coll., Blagdon (England).

    This trainer's guide is intended to assist supervisors of work-based career training projects in teaching students the procedures of conducting the MOT (Ministry of Transportation) Test (Great Britain's motor vehicle inspection test) and dealing with the customers on whose cars the inspection is performed. The guide is one in a series of core…

  7. 75 FR 31223 - Energy Conservation Program for Consumer Products: Test Procedure for Residential Central Air...

    Science.gov (United States)

    2010-06-02

    ... incorporating thermal storage, such expansion of the test procedure is beyond the scope of this rulemaking. This... conditioners and heat pumps having rated cooling capacities less than 65,000 British thermal units/hour (Btu/h... endorse the recommendation to add testing at 115 [deg]F outdoor temperature. A linear fit of data...

  8. Communication with patients during the prenatal testing procedure: an explorative qualitative study

    NARCIS (Netherlands)

    van Zwieten, Myra; Willems, Dick; Knegt, Lia; Leschot, Nico

    2006-01-01

    OBJECTIVE: While generally two phases of prenatal genetic counseling are distinguished, i.e. pre- and post-test counseling, we revealed a third form of communication during the testing procedure. The content of this intermediate communication was explored. METHODS: A secondary analysis was performed

  9. 76 FR 69869 - Energy Conservation Program: Test Procedures for Residential Clothes Washers

    Science.gov (United States)

    2011-11-09

    ... ensure that the test procedure is representative of consumer behavior and repeatable among different test... would not be factored into its energy efficiency rating. This would imply that consumer behavior would... previous section, DOE does not have data to verify how consumers may adjust their behavior based on the...

  10. 75 FR 8524 - Procedures for Transportation Workplace Drug and Alcohol Testing Programs

    Science.gov (United States)

    2010-02-25

    ... 2105-AD67 Procedures for Transportation Workplace Drug and Alcohol Testing Programs AGENCY: Office of... employers in the Department's drug and alcohol testing program to disclose to State commercial driver licensing (CDL) authorities the drug and alcohol violations of employees who hold CDLs and operate...

  11. 75 FR 49850 - Procedures for Transportation Workplace Drug and Alcohol Testing Programs

    Science.gov (United States)

    2010-08-16

    ... 2105-AD95 Procedures for Transportation Workplace Drug and Alcohol Testing Programs AGENCY: Office of... Drug and Alcohol Policy and Compliance, 1200 New Jersey Avenue, SE., Washington, DC 20590; telephone... methodology upon which DOT can rely in making its drug and alcohol testing regulations; we follow the HHS...

  12. 78 FR 7939 - Energy Conservation Program: Test Procedures for Microwave Ovens (Active Mode)

    Science.gov (United States)

    2013-02-04

    ... provisions designed to improve energy efficiency. (All references to EPCA refer to the statute as amended... section shall be reasonably designed to produce test results that measure energy efficiency, energy use or.... Products Covered by This Test Procedure Rulemaking DOE defines ``microwave oven'' as a class of kitchen...

  13. Test-Induced Priming Impairs Source Monitoring Accuracy in the DRM Procedure

    Science.gov (United States)

    Dewhurst, Stephen A.; Knott, Lauren M.; Howe, Mark L.

    2011-01-01

    Three experiments investigated the effects of test-induced priming (TIP) on false recognition in the Deese/Roediger-McDermott procedure (Deese, 1959; Roediger & McDermott, 1995). In Experiment 1, TIP significantly increased false recognition for participants who made old/new decisions at test but not for participants who made remember/know…

  14. Recommended procedures for performance testing of radiobioassay laboratories: Volume 2, In vitro samples

    International Nuclear Information System (INIS)

    Fenrick, H.W.; MacLellan, J.A.

    1988-11-01

    Draft American National Standards Institute (ANSI) Standard N13.30 (Performance Criteria for Radiobioassay) was developed for the US Department of Energy and the US Nuclear Regulatory Commission to help ensure that bioassay laboratories provide accurate and consistent results. The draft standard specifies the criteria for defining the procedures necessary to establish a bioassay performance-testing laboratory and program. The bioassay testing laboratory will conduct tests to evaluate the performance of service laboratories. Pacific Northwest Laboratory helped develop testing procedures as part of an effort to evaluate the performance criteria by testing the existing measurement capabilities of various bioassay laboratories. This report recommends guidelines for the preparation, handling, storage, distribution, shipping, and documentation of in vitro test samples (artificial urine and fecal matter) for indirect bioassay. The data base and recommended records system for documenting radiobioassay performance at the service laboratories are also presented. 8 refs., 3 tabs

  15. Test Report for Acceptance Test Procedure for Pumping Instrumentation and Control Skid ''P''

    International Nuclear Information System (INIS)

    KOCH, M.R.

    2000-01-01

    This Acceptance Test Report (ATR) provides the test results for the inspection and testing of the new Pumping Instrumentation and Control (PIC) skid designed as ''P''. The ATR summaries the results and provides a copy of the ATP and inspections in the Appendix

  16. Test Report for Acceptance Test Procedure for Pumping Instrumentation and Control Skid Q

    International Nuclear Information System (INIS)

    KOCH, M.R.

    2000-01-01

    This Acceptance Test Report (ATR) provides the test results for the inspection and testing of the new Pumping Instrumentation and Control (PIC) skid designed as ''Q''. The ATR summaries the results and provides a copy of the ATP and inspections in the Appendix

  17. Simulating wall and corner fire tests on wood products with the OSU room fire model

    Science.gov (United States)

    H. C. Tran

    1994-01-01

    This work demonstrates the complexity of modeling wall and corner fires in a compartment. The model chosen for this purpose is the Ohio State University (OSU) room fire model. This model was designed to simulate fire growth on walls in a compartment and therefore lends itself to direct comparison with standard room test results. The model input were bench-scale data...

  18. Acceptance test procedure for a portable, self-contained nitrogen supply

    International Nuclear Information System (INIS)

    Kostelnik, A.J.

    1994-01-01

    This Acceptance Test Procedure (ATP) will document compliance with the requirements of WHC-S-0249 Rev. 1 and ECN 606112. The equipment being tested is a Portable, Self-Contained Nitrogen Supply. The unit was purchased as a Design and Fabrication procurement activity. The Functional Test was written by the Seller and is contained in Appendix A. The Functional test will be performed by the Seller with representatives of the Westinghouse Hanford Company performing inspection and witnessing the functional test at the Seller's location

  19. Acceptance test procedure for a portable, self-contained nitrogen supply

    Energy Technology Data Exchange (ETDEWEB)

    Kostelnik, A.J.

    1994-10-04

    This Acceptance Test Procedure (ATP) will document compliance with the requirements of WHC-S-0249 Rev. 1 and ECN 606112. The equipment being tested is a Portable, Self-Contained Nitrogen Supply. The unit was purchased as a Design and Fabrication procurement activity. The Functional Test was written by the Seller and is contained in Appendix A. The Functional test will be performed by the Seller with representatives of the Westinghouse Hanford Company performing inspection and witnessing the functional test at the Seller`s location.

  20. Hanford spent nuclear fuel cold vacuum drying proof of performance test procedure

    International Nuclear Information System (INIS)

    McCracken, K.J.

    1998-01-01

    This document provides the test procedure for cold testing of the first article skids for the Cold Vacuum Drying (CVD) process at the Facility. The primary objective of this testing is to confirm design choices and provide data for the initial start-up parameters for the process. The current scope of testing in this document includes design verification, drying cycle determination equipment performance testing of the CVD process and MCC components, heat up and cool-down cycle determination, and thermal model validation

  1. RELIABILITY AND VALIDITY OF A TEST AND ITS PROCEDURE CONDUCTED AT A JAPANESE HIGH SCHOOL

    OpenAIRE

    Nadasdy,Paul Bela

    2011-01-01

    This paper analyses the validity and reliability of an English listening test being used at a private Japanese high school. Through an analysis of the test results,an attempt was made to make salient the qualities and deficiencies of the test and its procedure.The test's reliability was analysed using a split-half method measuring the coefficient of internal consistency. The split-test's coefficient results suggested that there was a certain amount of unreliability between the two halves of t...

  2. European wind turbine testing procedure developments. Task 1: Measurement method to verify wind turbine performance characteristics

    DEFF Research Database (Denmark)

    Hunter, R.; Friis Pedersen, Troels; Dunbabin, P.

    2001-01-01

    There is currently significant standardisation work ongoing in the context of wind farm energy yield warranty assessment and wind turbine power performance testing. A standards maintenance team is revising the current IEC (EN) 61400-12 Ed 1 standard forwind turbine power performance testing...... standard. The work was wide ranging and addressed 'grey' areas of knowledge, regarding existing methodologies or to carry out basic research in support offundamentally new procedures. The work has given rise to recommendations in all areas of the work, including site calibration procedures, nacelle...

  3. Clean fog rapid procedure test of artificially and naturally polluted HVDC porcelain barrel insulators

    Energy Technology Data Exchange (ETDEWEB)

    Vlastos, A.E. (Univ. of Technology, Gothenberg (SE))

    1992-07-01

    The first question asked in this paper refers to the variation of the peak leakage current prior to the flashover and the variation of the time prior to flashover in the test of artificially polluted insulators when using the up-and-down method. To answer this question sums up the test procedure used in the up-and-down method. For each trial represented the insulator was again polluted artificially and then dried following the procedure described in the paper. Then the insulator was transported into the fog chamber and the voltage and fog was switched on simultaneously. In these experiments a low fog injection rate was used.

  4. Test procedure for anion exchange testing with Argonne 10-L solutions

    International Nuclear Information System (INIS)

    Compton, J.A.

    1995-01-01

    Four anion exchange resins will be tested to confirm that they will sorb and release plutonium from/to the appropriate solutions in the presence of other cations. Certain cations need to be removed from the test solutions to minimize adverse behavior in other processing equipment. The ion exchange resins will be tested using old laboratory solutions from Argonne National Laboratory; results will be compared to results from other similar processes for application to all plutonium solutions stored in the Plutonium Finishing Plant

  5. A test procedure for energetic and performance analysis of cold appliances for the food industry

    Science.gov (United States)

    Armani, F.; Boscolo, A.

    2013-09-01

    In this article we present a novel approach for the characterization of cold appliances and in particular of refrigerators based on the standard vapour compression cycle with a reciprocating on/off compressor. The test procedure is based on a virtual instrument that perform both the stimulus and the data acquisition on the device under test. Acquired data is elaborated to fit a semi-empirical model based on the energetic balances between thermal and electrical sub systems and the heat exchanged with the environment. This approach results in a simple method to calculate useful parameters of the refrigerator, such as energetic performance, cooling effect and limit values of thermal loads. The test procedure requires only a few temperatures and the electric power consumption to be monitored, resulting in a low impact on the refrigerator. Preliminary tests showed a good estimation of parameters and prediction of energy consumption and heat extraction capacity of the refrigerator under test.

  6. Efficient Noninferiority Testing Procedures for Simultaneously Assessing Sensitivity and Specificity of Two Diagnostic Tests

    Directory of Open Access Journals (Sweden)

    Guogen Shan

    2015-01-01

    Full Text Available Sensitivity and specificity are often used to assess the performance of a diagnostic test with binary outcomes. Wald-type test statistics have been proposed for testing sensitivity and specificity individually. In the presence of a gold standard, simultaneous comparison between two diagnostic tests for noninferiority of sensitivity and specificity based on an asymptotic approach has been studied by Chen et al. (2003. However, the asymptotic approach may suffer from unsatisfactory type I error control as observed from many studies, especially in small to medium sample settings. In this paper, we compare three unconditional approaches for simultaneously testing sensitivity and specificity. They are approaches based on estimation, maximization, and a combination of estimation and maximization. Although the estimation approach does not guarantee type I error, it has satisfactory performance with regard to type I error control. The other two unconditional approaches are exact. The approach based on estimation and maximization is generally more powerful than the approach based on maximization.

  7. Procedure to select test organisms for environmental risk assessment of genetically modified crops in aquatic systems.

    Science.gov (United States)

    Hilbeck, Angelika; Bundschuh, Rebecca; Bundschuh, Mirco; Hofmann, Frieder; Oehen, Bernadette; Otto, Mathias; Schulz, Ralf; Trtikova, Miluse

    2017-11-01

    For a long time, the environmental risk assessment (ERA) of genetically modified (GM) crops focused mainly on terrestrial ecosystems. This changed when it was scientifically established that aquatic ecosystems are exposed to GM crop residues that may negatively affect aquatic species. To assist the risk assessment process, we present a tool to identify ecologically relevant species usable in tiered testing prior to authorization or for biological monitoring in the field. The tool is derived from a selection procedure for terrestrial ecosystems with substantial but necessary changes to adequately consider the differences in the type of ecosystems. By using available information from the Water Framework Directive (2000/60/EC), the procedure can draw upon existing biological data on aquatic systems. The proposed procedure for aquatic ecosystems was tested for the first time during an expert workshop in 2013, using the cultivation of Bacillus thuringiensis (Bt) maize as the GM crop and 1 stream type as the receiving environment in the model system. During this workshop, species executing important ecological functions in aquatic environments were identified in a stepwise procedure according to predefined ecological criteria. By doing so, we demonstrated that the procedure is practicable with regard to its goal: From the initial long list of 141 potentially exposed aquatic species, 7 species and 1 genus were identified as the most suitable candidates for nontarget testing programs. Integr Environ Assess Manag 2017;13:974-979. © 2017 SETAC. © 2017 SETAC.

  8. Procedure for vibration test of the fuel rod supported by spacer grids

    International Nuclear Information System (INIS)

    Choi, Myoung Hwan; Kang, Heung Seok; Yoon, Kyung Ho; Kim, Hyung Kyu; Song, Kee Nam

    2002-07-01

    One of the methods that are used to compare and verify the supporting performance of the spacer grids developed is the vibration characteristic test. In this report there are two aims. One is of the understand of the experimental method and procedure performing the modal testing using I-DEAS TDAS module. The other is the investigation of the vibration behaviors of a dummy fuel rod supported by 8 optimized H type spacer grids. This report describes the method and procedure of modal testing to obtain the vibration characteristics such as amplitudes, natural frequencies and mode shapes of the fuel rod using a shaker, a non-contact gap sensor and an accelerometer. This report provides a test procedure in detail so that anyone can be easily understood and use the I-DEAS TDAS program. The I-DEAS TDAS program related to the modal testing has several tasks including the Modal analysis, Signal Processing et al.. This report includes model preparation to prepare the geometrical model, Signal Processing (Sine/Standard measurement) to acquire the signal, Modal analysis to obtain the frequencies and mode shapes, Correlation to analyze the relation between the test and FE analysis and Post Processing tasks. In addition, this report contains the actual test and analysis data of a dummy fuel rod in length 3847mm supported by 8 optimized H type spacer grids

  9. First steps towards fuel cells testing harmonisation: Procedures and parameters for single cell performance evaluation

    Energy Technology Data Exchange (ETDEWEB)

    Lunghi, P. [Department of Industrial Engineering, University of Perugia, Via Duranti 93, Perugia (Italy); Ubertini, S. [Department of Mechanical Engineering, University of Rome ' ' Tor Vergata' ' , Via di Torvergata, 110, Rome (Italy)

    2004-01-01

    The great interest in Fuel Cell Systems, combined with the innovation of the device itself, has led to a huge developmental effort to make the steps necessary for future FC plant commissioning. The clearest and most effective way to evaluate the performance of a fuel cell is to measure it directly and, since few fuel cell test rigs are available at the moment, standard experimental procedures have not been realized so far. Our research group is currently performing single cell testing at the University of Perugia fuel cell laboratory and particular emphasis has been put on the definition of procedures and the testing of parameterisation. The work team strongly believes that this is the key to effective system testing and reliable performance evaluation. In this work, the test parameterisation developed by the team, and the resulting advanced control procedure used for a single MCFC experimental characterization are presented. Efforts have been dedicated to obtain some relevant non-dimensional parameters to allow an easy understanding of the results and quick comparisons with other tests under different operating conditions, or with results obtained on different cells eventually tested in different laboratories. The authors strongly emphasise this topic to avoid the data that developers and research institutions collect being of no practical use due to a lack of shared rules. (Abstract Copyright [2003], Wiley Periodicals, Inc.)

  10. Acceptance test procedure for K basins dose reduction project clean and coat equipment

    International Nuclear Information System (INIS)

    Creed, R.F.

    1996-01-01

    This document is the Acceptance Test Procedure (ATP) for the clean and coat equipment designed by Oceaneering Hanford, Inc. under purchase order MDK-XVC-406988 for use in the 105 K East Basin. The ATP provides the guidelines and criteria to test the equipment's ability to clean and coat the concrete perimeter, divider walls, and dummy elevator pit above the existing water level. This equipment was designed and built in support of the Spent Nuclear Fuel, Dose Reduction Project. The ATP will be performed at the 305 test facility in the 300 Area at Hanford. The test results will be documented in WHC-SD-SNF-ATR-020

  11. CENRTC Project No. 2F3EOA, OCB A-372, acceptance test procedure

    International Nuclear Information System (INIS)

    Akerson, A.W.

    1995-01-01

    This test procedure provides the steps necessary to verify correct functional operation of controls, annunciators, alarms, protective relays and related systems impacted by CENRTC No. 2F3EOA, Microwave Transfer Trip Project, modification work performed under work package 6B-93-00038/M (CENRTC 2F3EOA MWTT OCB A-372 PACKAGE)

  12. 78 FR 64295 - Energy Conservation Program: Test Procedure for Commercial Refrigeration Equipment

    Science.gov (United States)

    2013-10-28

    ... Reduction Act D. Review Under the National Environmental Policy Act E. Review Under Executive Order 13132 F... procedure to make such representations. However, DOE has not considered the energy usage of these types of..., as well as translucent fiberglass and multicell plastic panels, which cannot be tested with a...

  13. Comparing Treatment and Control Groups on Multiple Outcomes: Robust Procedures for Testing a Directional Alternative Hypothesis

    Science.gov (United States)

    Lix, Lisa M.; Deering, Kathleen N.; Fouladi, Rachel T.; Manivong, Phongsack

    2009-01-01

    This study considers the problem of testing the difference between treatment and control groups on m [greater than or equal to] 2 measures when it is assumed a priori that the treatment group will perform better than the control group on all measures. Two procedures are investigated that do not rest on the assumptions of covariance homogeneity or…

  14. 75 FR 72739 - Compliance Testing Procedures: Correction Factor for Room Air Conditioners

    Science.gov (United States)

    2010-11-26

    ... products and innovation, is essential to U.S. consumer lifestyle, health, safety and convenience. Through... economic security. Home appliances also are a success story in terms of energy efficiency and environmental... discussed below, the issue relates to the current DOE recommended test procedure's failure to correct for...

  15. 77 FR 49063 - Energy Conservation Program: Test Procedures for Residential Dishwashers and Cooking Products

    Science.gov (United States)

    2012-08-15

    ..., commenters noted that two preconditioning cycles would help to clean out residual dirt from the machine prior... comments in this test procedure rulemaking process that the items are obsolete. The replacement items are..., N = the representative average dishwasher use of 215 cycles per year, M = the machine energy...

  16. 75 FR 2122 - Additional Guidance Regarding Application of Current Procedures for Testing Energy Consumption of...

    Science.gov (United States)

    2010-01-14

    ... Energy Consumption of Refrigerator-Freezers With Automatic Ice Makers AGENCY: Office of the General...) to prescribe standardized test procedures to measure the energy consumption of certain consumer... Energy Consumption of Electric Refrigerators and Electric Refrigerator- Freezers (Appendix A1). DOE...

  17. 40 CFR 61.355 - Test methods, procedures, and compliance provisions.

    Science.gov (United States)

    2010-07-01

    ... sample and each 1-hour period shall correspond to the periods when the waste feed is sampled. (ii) A run... Emission Standard for Benzene Waste Operations § 61.355 Test methods, procedures, and compliance provisions. (a) An owner or operator shall determine the total annual benzene quantity from facility waste by the...

  18. Comparison of IRT Likelihood Ratio Test and Logistic Regression DIF Detection Procedures

    Science.gov (United States)

    Atar, Burcu; Kamata, Akihito

    2011-01-01

    The Type I error rates and the power of IRT likelihood ratio test and cumulative logit ordinal logistic regression procedures in detecting differential item functioning (DIF) for polytomously scored items were investigated in this Monte Carlo simulation study. For this purpose, 54 simulation conditions (combinations of 3 sample sizes, 2 sample…

  19. 16 CFR 1610.35 - Procedures for testing special types of textile fabrics under the standard.

    Science.gov (United States)

    2010-01-01

    ... textile fabrics under the standard. 1610.35 Section 1610.35 Commercial Practices CONSUMER PRODUCT SAFETY COMMISSION FLAMMABLE FABRICS ACT REGULATIONS STANDARD FOR THE FLAMMABILITY OF CLOTHING TEXTILES Rules and Regulations § 1610.35 Procedures for testing special types of textile fabrics under the standard. (a) Fabric...

  20. 16 CFR 1610.33 - Test procedures for textile fabrics and film.

    Science.gov (United States)

    2010-01-01

    ... 16 Commercial Practices 2 2010-01-01 2010-01-01 false Test procedures for textile fabrics and film. 1610.33 Section 1610.33 Commercial Practices CONSUMER PRODUCT SAFETY COMMISSION FLAMMABLE FABRICS ACT... for textile fabrics and film. (a)(1) All textile fabrics (except those with a nitro-cellulose fiber...

  1. 40 CFR Appendix A to Subpart T of... - Test of Solvent Cleaning Procedures

    Science.gov (United States)

    2010-07-01

    ... CATEGORIES National Emission Standards for Halogenated Solvent Cleaning Pt. 63, Subpt. T, App. A Appendix A to Subpart T of Part 63—Test of Solvent Cleaning Procedures General Questions ___ 1. What is the... disturbances. A. Fans B. Open doors C. Open windows D. Ventilation vents E. All of the above ___ 4. What are...

  2. 76 FR 65631 - Energy Conservation Program: Test Procedures for Microwave Ovens

    Science.gov (United States)

    2011-10-24

    ... Conservation Program: Test Procedures for Microwave Ovens AGENCY: Office of Energy Efficiency and Renewable... residential microwave ovens. DOE specifically is seeking information, data, and comments regarding representative and repeatable methods for measuring the energy use of microwave-only ovens and combination...

  3. 77 FR 13887 - Energy Conservation Program: Test Procedures for Residential Clothes Washers

    Science.gov (United States)

    2012-03-07

    ... dryer usage factor; and (5) replaces the current representative load size calculation in the drying... specifications for the dryer to be used for bone-drying the test cloth; (10) clarifies the procedures for.... 12 at p. 4-5) NEEA expressed concern that the definition of the active washing mode leaves out...

  4. 75 FR 57556 - Energy Conservation Program for Consumer Products: Test Procedure for Residential Clothes Washers

    Science.gov (United States)

    2010-09-21

    ... technologies not covered by the current procedure; (2) more accurately reflect current consumer behavior and... Part II Department of Energy 10 CFR Part 430 Energy Conservation Program for Consumer Products... [Docket No. EERE-2010-BT-TP-0021] RIN 1904-AC08 Energy Conservation Program for Consumer Products: Test...

  5. 75 FR 57555 - Energy Conservation Program for Consumer Products: Test Procedure for Residential Clothes Washers

    Science.gov (United States)

    2010-09-21

    ... technologies not covered by the current procedure; (2) more accurately reflect current consumer behavior and... Part II Department of Energy 10 CFR Part 430 Energy Conservation Program for Consumer Products... [Docket No. EERE-2010-BT-TP-0021] RIN 1904-AC08 Energy Conservation Program for Consumer Products: Test...

  6. 75 FR 13009 - Procedures for Transportation Workplace Drug and Alcohol Testing Programs

    Science.gov (United States)

    2010-03-18

    ... DEPARTMENT OF TRANSPORTATION Office of the Secretary 49 CFR Part 40 [Docket DOT-OST-2008-0088] RIN OST 2105-AD84 Procedures for Transportation Workplace Drug and Alcohol Testing Programs Correction In rule document 2010-3731 beginning on page 8528 in the issue of Thursday, February 25, 2010, make the...

  7. 75 FR 42579 - Energy Conservation Program for Consumer Products: Test Procedure for Microwave Ovens; Repeal of...

    Science.gov (United States)

    2010-07-22

    ... forth a variety of provisions designed to improve energy efficiency. Part A of Title III (42 U.S.C. 6291... procedures be reasonably designed to produce test results which measure energy efficiency, energy use, or...-12), which amended EPCA, established prescriptive standards for kitchen ranges and ovens, but no...

  8. 78 FR 4015 - Energy Conservation Program: Test Procedures for Microwave Ovens

    Science.gov (United States)

    2013-01-18

    ... kitchen ranges and ovens which is a household cooking appliance consisting of a compartment designed to...'' or, ``the Act'') sets forth a variety of provisions designed to improve energy efficiency. (All... procedures prescribed or amended under this section shall be reasonably designed to produce test results...

  9. 75 FR 42612 - Energy Conservation Program for Consumer Products: Test Procedure for Microwave Ovens

    Science.gov (United States)

    2010-07-22

    ... forth a variety of provisions designed to improve energy efficiency. Part A of Title III (42 U.S.C. 6291... procedures be reasonably designed to produce test results which measure energy efficiency, energy use, or... amended EPCA, established prescriptive standards for kitchen ranges and ovens, but no standards were...

  10. 49 CFR 572.143 - Neck-headform assembly and test procedure.

    Science.gov (United States)

    2010-10-01

    ...), neck mounting plate (drawing TE-250-021), two jam nuts (drawing 9001336), load-moment transducer... procedure. (1) Soak the neck assembly in a controlled environment at any temperature between 20.6 and 22.2... test. (2) Torque the jam nut (drawing 9001336) on the neck cable (drawing 210-2040) between 0.2 N-m and...

  11. Operational Control Procedures for the Activated Sludge Process, Part I - Observations, Part II - Control Tests.

    Science.gov (United States)

    West, Alfred W.

    This is the first in a series of documents developed by the National Training and Operational Technology Center describing operational control procedures for the activated sludge process used in wastewater treatment. Part I of this document deals with physical observations which should be performed during each routine control test. Part II…

  12. 46 CFR 197.206 - Substitutes for required equipment, materials, apparatus, arrangements, procedures, or tests.

    Science.gov (United States)

    2010-10-01

    ... 46 Shipping 7 2010-10-01 2010-10-01 false Substitutes for required equipment, materials, apparatus, arrangements, procedures, or tests. 197.206 Section 197.206 Shipping COAST GUARD, DEPARTMENT OF HOMELAND... Operations General § 197.206 Substitutes for required equipment, materials, apparatus, arrangements...

  13. Performance and Health Test Procedure for Grid Energy Storage Systems: Preprint

    Energy Technology Data Exchange (ETDEWEB)

    Baggu, Murali M [National Renewable Energy Laboratory (NREL), Golden, CO (United States); Smith, Kandler A [National Renewable Energy Laboratory (NREL), Golden, CO (United States); Friedl, Andrew [San Diego Gas and Electric; Bialek, Thomas [San Diego Gas and Electric; Schimpe, Michael Robert [Technical University of Munich

    2017-07-27

    A test procedure to evaluate the performance and health of field installations of grid-connected battery energy storage systems (BESS) is described. Performance and health metrics captured in the procedures are: Round-trip efficiency, Standby losses, Response time/accuracy, and Useable Energy/ State of Charge at different discharge/charge rates over the system's lifetime. The procedures are divided into Reference Performance Tests, which require the system to be put in a test mode and are to be conducted in intervals, and Real-time Monitoring tests, which collect data during normal operation without interruption. The procedures can be applied on a wide array of BESS with little modifications and can thus support BESS operators in the management of BESS field installations with minimal interruption and expenditures.can be applied on a wide array of BESS with little modifications and can thus support BESS operators in the management of BESS field installations with minimal interruption and expenditures.

  14. 7 CFR 28.603 - Procedures for air flow tests of micronaire reading.

    Science.gov (United States)

    2010-01-01

    ... 7 Agriculture 2 2010-01-01 2010-01-01 false Procedures for air flow tests of micronaire reading... micronaire reading. In determining in terms of micronaire readings, the fiber fineness and maturity, in... cotton in terms of micronaire reading on the curvilinear scale adopted in September 1950 by the...

  15. 75 FR 29823 - Energy Conservation Program for Consumer Products: Test Procedures for Refrigerators...

    Science.gov (United States)

    2010-05-27

    ... can be conducted in a fashion that would measure the representative energy use of the product. HRF-1... Part II Department of Energy 10 CFR Part 430 Energy Conservation Program for Consumer Products... Consumer Products: Test Procedures for Refrigerators, Refrigerator-Freezers, and Freezers AGENCY: Office of...

  16. 76 FR 77914 - Energy Conservation Program for Certain Commercial and Industrial Equipment: Test Procedures for...

    Science.gov (United States)

    2011-12-15

    ... Energy Conservation Program for Certain Commercial and Industrial Equipment: Test Procedures for High... Illuminating Engineering Society of North America (IES), and the International Commission on Illumination... docket web page can be found at: http://www1.eere.energy.gov/buildings/appliance_standards/commercial...

  17. 40 CFR 205.54-1 - Low speed sound emission test procedures.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 24 2010-07-01 2010-07-01 false Low speed sound emission test procedures. 205.54-1 Section 205.54-1 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) NOISE ABATEMENT PROGRAMS TRANSPORTATION EQUIPMENT NOISE EMISSION CONTROLS Medium and Heavy Trucks § 205...

  18. 40 CFR 53.62 - Test procedure: Full wind tunnel test.

    Science.gov (United States)

    2010-07-01

    ... test particles with a size resolution of 0.1 µm or less. The accuracy of the particle size verification... aerosol generator. (ii) Check for the presence of satellites and adjust the generator as necessary. (iii... isokinetic sampler as: Equation 7 ER18jy97.100 where: i = replicate number; j = isokinetic sampler number...

  19. MINIPILOT SOLAR SYSTEM: DESIGN/OPERATION OF SYSTEM AND RESULTS OF NON-SOLAR TESTING AT MRI

    Science.gov (United States)

    Prior to this project, MRI had carried out work for the Environmental Protection Agency (EPA) on the conceptual design of a solar system for solid waste disposal and a follow-on project to study the feasibility of bench-scale testing of desorption of organics from soil with destr...

  20. Acceptance test procedure, 241-SY-101/241-C-106 shot loading system

    International Nuclear Information System (INIS)

    Ostrom, M.J.

    1994-01-01

    This Acceptance Test Procedure is for the 241-SY-101/241-C-106 Shot Loading System. The procedure will test the components of the Shot Loading System and its capability of adequately loading shot into the annular space of the Container. The loaded shot will provide shielding as required for transporting and storage of a contaminated pump after removal from the tank. This test serves as verification that the SLS is acceptable for use in the pump removal operations for Tanks 241-SY-101, 241-C-106 and 241-AY-102. The pump removal operation for these three tanks will be performed by two different organizations with different equipment, but the Shot Loading System will be compatible between the two operations