WorldWideScience

Sample records for beamline elements part

  1. Possible Scheme of the Analyzing Part of a Cyclotron Injection Beamline with Higher Energy

    CERN Document Server

    Kazarinov, Nikolay; Stetson, Jeffry W

    2005-01-01

    The ion beam produced with an ECR ion source (ECRIS) with an extraction voltage of 30 kV may be additionally accelerated using a negative voltage of -30 kV applied to the last electrode of the extraction system, connected to the beamline biased to the same -30 kV potential. In this way the kinetic energy of the beam is increased to 60 keV/q, decreasing to half the space charge effect on the beam emittance. Using a large gap analyzing magnet placed right after the ECRIS and no focusing element, the transmission is still close to 100%. The voltage on the beamline must be kept constant from the ECRIS till the image focal plane of the analyzing magnet where the full separation of the beam charge states is achieved. An insulator break separates the biased beamline from the downstream section, which is at zero potential. Passing through this section of the beamline, the ion beam is decelerated to 30 keV/q, the energy necessary for the injection in the cyclotron. In order to prevent the increase of the beam divergen...

  2. Double-crystal monochromator as the first optical element in BESSRC-CAT beamlines (abstract)

    Science.gov (United States)

    Beno, Mark A.; Ramanathan, Mohan

    1996-09-01

    The first optical element in the BESSRC-CAT beamlines at the Advanced Photon Source will be a monochromator, so that a standard design for this critical component is advantageous. The monochromator we have designed is a double-crystal, fixed-exit scheme with a constant offset designed for UHV operation, thereby allowing windowless operation of the beamlines. The crystals are mounted on a turntable with the first crystal at the center of rotation. A mechanical linkage is used to correctly position the second crystal and maintain a constant offset. The main drive for the rotary motion is provided by a vacuum-compatible Huber goniometer isolated from the main vacuum chamber. Rotary motion of the primary monochromator stage is accomplished by using two adjacent vacuum chambers connected only by the small annular opening around a hollow stainless steel shaft, which connects the Huber goniometer to the turntable on which the crystals are mounted. The design of the monochromator is such that it can accommodate both water and liquid nitrogen cooling for the crystal optics. The basic design for the monochromator linkage mechanism will be presented along with details of the monochromator chamber. The results of initial optical tests of the monochromator system using tilt sensors and a precision autocollimator will also be given.

  3. Confining continuous manipulations of accelerator beamline optics

    CERN Document Server

    Amstutz, Philipp; Bödewadt, Jörn; Lechner, Christoph; Plath, Tim; Vogt, Mathias

    2016-01-01

    Altering the optics in one section of a linear accelerator beamline will in general cause an alteration of the optics in all downstream sections. In circular accelerators, changing the optical properties of any beamline element will have an impact on the optical functions throughout the whole machine. In many cases, however, it is desirable to change the optics in a certain beamline section without disturbing any other parts of the machine. Such a local optics manipulation can be achieved by adjusting a number of additional corrector magnets that restore the initial optics after the manipulated section. In that case, the effect of the manipulation is confined in the region between the manipulated and the correcting beamline elements. Introducing a manipulation continuously, while the machine is operating, therefore requires continuous correction functions to be applied to the correcting quadrupole magnets. In this paper we present an analytic approach to calculate such continuous correction functions for six ...

  4. Simulation of temperature distribution by finite element analysis on different components of the EXAFS beamline at INDUS-II synchrotron source

    Indian Academy of Sciences (India)

    D Bhattacharyya; S N Jha; N C Das; Vishnu Verma; S G Markandeya; A K Ghosh

    2005-12-01

    An extended X-ray absorption fine structure (EXAFS) beamline is being developed for the INDUS-II synchrotron source. Several optical and mechanical components of the beamline are exposed to high intensity synchrotron radiation while in operation. The temperature rise on different components of the beamline on exposure to the synchrotron beam has been simulated by finite element analysis. Design of the cooling mechanism for each of these components has been carried out and estimation of the temperature rise has also been done incorporating the cooling mechanism.

  5. Beamlines of the biomedical imaging and therapy facility at the Canadian light source – part 3

    Energy Technology Data Exchange (ETDEWEB)

    Wysokinski, Tomasz W., E-mail: bmit@lightsource.ca [Canadian Light Source, Saskatoon, SK (Canada); Chapman, Dean [Anatomy and Cell Biology, University of Saskatchewan, Saskatoon, SK (Canada); Adams, Gregg [Western College of Veterinary Medicine, Saskatoon, SK (Canada); Renier, Michel [European Synchrotron Radiation Facility, Grenoble (France); Suortti, Pekka [Department of Physics, University of Helsinki (Finland); Thomlinson, William [Department of Physics, University of Saskatchewan, Saskatoon, SK (Canada)

    2015-03-01

    The BioMedical Imaging and Therapy (BMIT) facility provides synchrotron-specific imaging and radiation therapy capabilities [1–4]. We describe here the Insertion Device (ID) beamline 05ID-2 with the beam terminated in the SOE-1 (Secondary Optical Enclosure) experimental hutch. This endstation is designed for imaging and therapy research primarily in animals ranging in size from mice to humans to horses, as well as tissue specimens including plants. Core research programs include human and animal reproduction, cancer imaging and therapy, spinal cord injury and repair, cardiovascular and lung imaging and disease, bone and cartilage growth and deterioration, mammography, developmental biology, gene expression research as well as the introduction of new imaging methods. The source for the ID beamline is a multi-pole superconducting 4.3 T wiggler [5]. The high field gives a critical energy over 20 keV. The high critical energy presents shielding challenges and great care must be taken to assess shielding requirements [6–9]. The optics in the POE-1 and POE-3 hutches [4,10] prepare a monochromatic beam that is 22 cm wide in the last experimental hutch SOE-1. The double crystal bent-Laue or Bragg monochromator, or the single-crystal K-edge subtraction (KES) monochromator provide an energy range appropriate for imaging studies in animals (20–100+ keV). SOE-1 (excluding the basement structure 4 m below the experimental floor) is 6 m wide, 5 m tall and 10 m long with a removable back wall to accommodate installation and removal of the Large Animal Positioning System (LAPS) capable of positioning and manipulating animals as large as a horse [11]. This end-station also includes a unique detector positioner with a vertical travel range of 4.9 m which is required for the KES imaging angle range of +12.3° to –7.3°. The detector positioner also includes moveable shielding integrated with the safety shutters. An update on the status of the other two end-stations at BMIT

  6. Moly99 Production Facility: Report on Beamline Components, Requirements, Costs

    Energy Technology Data Exchange (ETDEWEB)

    Bishofberger, Kip A. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2015-12-23

    In FY14 we completed the design of the beam line for the linear accelerator production design concept. This design included a set of three bending magnets, quadrupole focusing magnets, and octopoles to flatten the beam on target. This design was generic and applicable to multiple different accelerators if necessary. In FY15 we built on that work to create specifications for the individual beam optic elements, including power supply requirements. This report captures the specification of beam line components with initial cost estimates for the NorthStar production facility.This report is organized as follows: The motivation of the beamline design is introduced briefly, along with renderings of the design. After that, a specific list is provided, which accounts for each beamline component, including part numbers and costs, to construct the beamline. After that, this report details the important sections of the beamline and individual components. A final summary and list of follow-on activities completes this report.

  7. Confining continuous manipulations of accelerator beamline optics

    Energy Technology Data Exchange (ETDEWEB)

    Amstutz, P.; Lechner, C.; Plath, T. [Hamburg Univ. (Germany). Dept. of Physics; Ackermann, S.; Boedewadt, J.; Vogt, M. [Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)

    2016-04-15

    Altering the optics in one section of a linear accelerator beamline will in general cause an alteration of the optics in all downstream sections. In circular accelerators, changing the optical properties of any beamline element will have an impact on the optical functions throughout the whole machine. In many cases, however, it is desirable to change the optics in a certain beamline section without disturbing any other parts of the machine. Such a local optics manipulation can be achieved by adjusting a number of additional corrector magnets that restore the initial optics after the manipulated section. In that case, the effect of the manipulation is confined in the region between the manipulated and the correcting beamline elements. Introducing a manipulation continuously, while the machine is operating, therefore requires continuous correction functions to be applied to the correcting quadrupole magnets. In this paper we present an analytic approach to calculate such continuous correction functions for six quadrupole magnets by means of a homotopy method. Besides a detailed derivation of the method, we present its application to an algebraic example, as well as its implementation at the seeding experiment sFLASH at the free-electron laser FLASH located at DESY in Hamburg.

  8. Radiation protection of a proton beamline at ELI-Beamlines

    Science.gov (United States)

    Bechet, S.; Versaci, R.; Rollet, S.; Olsovcova, V.; Fajstavr, A.; Zakova, M.; Margarone, D.

    2016-12-01

    ELI-Beamlines (ELI stands for Extreme Light Infrastructure) is a new EU funded laser facility located near Prague, in Czech Republic. It will use laser-driven plasma sources to accelerate particles and host a dedicated proton beamline called ELIMAIA (ELI Multidisciplinary Applications of laser- Ion Acceleration) designed to reach energies up to 250 MeV. This beamline could be exploited to study possible future medical application of laser-driven beams. The first part of this paper introduces the beamline, the corresponding source terms and the complete set-up. The second part of the paper details the evaluation of the ambient dose equivalent and the activation study inside the experimental halls based on Monte-Carlo simulation. These calculations show that the ELIMAIA operation is safe as long as nobody is present in the hall when the beam is on.

  9. Some aspects of SR beamline alignment

    Energy Technology Data Exchange (ETDEWEB)

    Gaponov, Yu.A., E-mail: Yury.Gaponov@maxlab.lu.se [MAX-lab, Lund University, P.O.B. 118, SE-221 00 Lund (Sweden); Cerenius, Y. [MAX-lab, Lund University, P.O.B. 118, SE-221 00 Lund (Sweden); Nygaard, J. [Faculty of Life Sciences, University of Copenhagen, DK-1871 Frederiksberg C (Denmark); Ursby, T.; Larsson, K. [MAX-lab, Lund University, P.O.B. 118, SE-221 00 Lund (Sweden)

    2011-09-01

    Based on the Synchrotron Radiation (SR) beamline optical element-by-element alignment with analysis of the alignment results an optimized beamline alignment algorithm has been designed and developed. The alignment procedures have been designed and developed for the MAX-lab I911-4 fixed energy beamline. It has been shown that the intermediate information received during the monochromator alignment stage can be used for the correction of both monochromator and mirror without the next stages of alignment of mirror, slits, sample holder, etc. Such an optimization of the beamline alignment procedures decreases the time necessary for the alignment and becomes useful and helpful in the case of any instability of the beamline optical elements, storage ring electron orbit or the wiggler insertion device, which could result in the instability of angular and positional parameters of the SR beam. A general purpose software package for manual, semi-automatic and automatic SR beamline alignment has been designed and developed using the developed algorithm. The TANGO control system is used as the middle-ware between the stand-alone beamline control applications BLTools, BPMonitor and the beamline equipment.

  10. Internal elemental imaging by scanning X-ray fluorescence microtomography at the hard X-ray microprobe beamline of the SSRF: Preliminary experimental results

    Science.gov (United States)

    Qiu, Jingke; Deng, Biao; Yang, Qun; Yan, Fen; Li, Aiguo; Yu, Xiaohan

    2011-11-01

    Synchrotron-based X-ray micro-fluorescence (μ-SXRF) is a non-destructive analytical technique and has been widely used to detect and quantify the elemental composition of samples in their natural state. To determine the internal elemental distributions within samples, X-ray fluorescence microtomography has been developed based on the hard X-ray microprobe at beamline BL15U1 of the Shanghai Synchrotron Radiation Facility (SSRF) in Shanghai, China. This technique was applied to image the cross-sectional distributions of multiple elements within a single human hair, and its validity was evaluated by comparing the results with the elemental maps of a thin hair section obtained using the well-established μ-SXRF mapping method. Elemental images of S, Ca, Mn, Fe, Cu, and Zn within a virtual slice of the hair were reconstructed after the tomographic measurements. The tomographic images of heavy elements like Fe, Cu, and Zn were found to be in good agreement with the corresponding μ-SXRF maps. Light elements, such as S, however, represented different patterns due to non-negligible self-absorption in the sample, and sophisticated correction algorithms accounting for such effects are required for obtaining qualitatively and quantitatively more accurate images. Compared to μ-SXRF mapping, X-ray fluorescence microtomography reduces the sample preparation requirements and has been demonstrated in this work as being a more ideal and effective imaging modality to non-destructively mapping out the internal distribution of heavy elements within samples at the micrometer scale at the SSRF.

  11. The ELIMED transport and dosimetry beamline for laser-driven ion beams

    Energy Technology Data Exchange (ETDEWEB)

    Romano, F., E-mail: francesco.romano@lns.infn.it [Istituto Nazionale di Fisica Nucleare, Laboratori Nazionali del Sud, Via Santa Sofia 62, Catania (Italy); Schillaci, F.; Cirrone, G.A.P.; Cuttone, G. [Istituto Nazionale di Fisica Nucleare, Laboratori Nazionali del Sud, Via Santa Sofia 62, Catania (Italy); Scuderi, V. [Istituto Nazionale di Fisica Nucleare, Laboratori Nazionali del Sud, Via Santa Sofia 62, Catania (Italy); ELI-Beamlines Project, Institute of Physics ASCR, v.v.i. (FZU), 182 21 Prague (Czech Republic); Allegra, L.; Amato, A.; Amico, A.; Candiano, G.; De Luca, G.; Gallo, G. [Istituto Nazionale di Fisica Nucleare, Laboratori Nazionali del Sud, Via Santa Sofia 62, Catania (Italy); Giordanengo, S.; Guarachi, L. Fanola [Istituto Nazionale di Fisica Nucleare, Sezione di Torino, Via P. Giuria 1, Torino (Italy); Universita' di Torino, Dipartimento di Fisica, Via P. Giuria 1, Torino (Italy); Korn, G. [ELI-Beamlines Project, Institute of Physics ASCR, v.v.i. (FZU), 182 21 Prague (Czech Republic); Larosa, G. [Istituto Nazionale di Fisica Nucleare, Laboratori Nazionali del Sud, Via Santa Sofia 62, Catania (Italy); Leanza, R. [Istituto Nazionale di Fisica Nucleare, Laboratori Nazionali del Sud, Via Santa Sofia 62, Catania (Italy); Universita' di Catania, Dipartimento di Fisica e Astronomia, Via S. Sofia 64, Catania (Italy); Manna, R.; Marchese, V. [Istituto Nazionale di Fisica Nucleare, Laboratori Nazionali del Sud, Via Santa Sofia 62, Catania (Italy); Marchetto, F. [Istituto Nazionale di Fisica Nucleare, Sezione di Torino, Via P. Giuria 1, Torino (Italy); Margarone, D. [ELI-Beamlines Project, Institute of Physics ASCR, v.v.i. (FZU), 182 21 Prague (Czech Republic); and others

    2016-09-01

    A growing interest of the scientific community towards multidisciplinary applications of laser-driven beams has led to the development of several projects aiming to demonstrate the possible use of these beams for therapeutic purposes. Nevertheless, laser-accelerated particles differ from the conventional beams typically used for multiscipilinary and medical applications, due to the wide energy spread, the angular divergence and the extremely intense pulses. The peculiarities of optically accelerated beams led to develop new strategies and advanced techniques for transport, diagnostics and dosimetry of the accelerated particles. In this framework, the realization of the ELIMED (ELI-Beamlines MEDical and multidisciplinary applications) beamline, developed by INFN-LNS (Catania, Italy) and that will be installed in 2017 as a part of the ELIMAIA beamline at the ELI-Beamlines (Extreme Light Infrastructure Beamlines) facility in Prague, has the aim to investigate the feasibility of using laser-driven ion beams for multidisciplinary applications. In this contribution, an overview of the beamline along with a detailed description of the main transport elements as well as the detectors composing the final section of the beamline will be presented.

  12. Beamline for Schools 2016

    CERN Multimedia

    2016-01-01

    Two teams of high-school students from the UK and Poland had the opportunity to conduct their own experiments at a fully equipped CERN beamline. Two teams of high-school students from the UK and Poland had the opportunity to conduct their own experiments at a fully equipped CERN beamline, after winning the Beamline for Schools competition. The teams, ‘Pyramid Hunters’ from Poland and ‘Relatively Special’ from the United Kingdom, spent 10 days at CERN conducting the experiments they had dreamt up in their winning proposals. The Beamline for Schools competition gives high-school students the chance to run an experiment on a fully equipped CERN beamline, in the same way researchers do at the Large Hadron Collider and other CERN facilities every day. 

  13. Confining continuous manipulations of accelerator beam-line optics

    Science.gov (United States)

    Amstutz, Ph.; Plath, T.; Ackermann, S.; Bödewadt, J.; Lechner, C.; Vogt, M.

    2017-04-01

    Altering the optics in one section of a linear accelerator beam line will in general cause an alteration of the optics in all downstream sections. In circular accelerators, changing the optical properties of any beam-line element will have an impact on the optical functions throughout the whole machine. In many cases, however, it is desirable to change the optics in a certain beam-line section without disturbing any other parts of the machine. Such a local optics manipulation can be achieved by adjusting a number of additional corrector magnets that restore the initial optics after the manipulated section. In that case, the effect of the manipulation is confined in the region between the manipulated and the correcting beam-line elements. Introducing a manipulation continuously, while the machine is operating, therefore requires continuous correction functions to be applied to the correcting quadrupole magnets. In this paper, we present an approach to calculate such continuous correction functions for six quadrupole magnets by means of a homotopy method. Besides a detailed derivation of the method, we present its application to an algebraic example, as well as its demonstration at the seeding experiment sFLASH at the free-electron laser FLASH located at DESY in Hamburg.

  14. Design of the LBNE Beamline

    Energy Technology Data Exchange (ETDEWEB)

    Papadimitriou, Vaia [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Andrews, Richard [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Hylen, James [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Kobilarcik, Thomas [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Marchionni, Alberto [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Moore, Craig D. [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Schlabach, Phil [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Tariq, Salman [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States)

    2015-02-05

    The Long Baseline Neutrino Experiment (LBNE) will utilize a beamline facility located at Fermilab to carry out a compelling research program in neutrino physics. The facility will aim a wide band beam of neutrinos toward a detector placed at the Sanford Underground Research Facility in South Dakota, about 1,300 km away. The main elements of the facility are a primary proton beamline and a neutrino beamline. The primary proton beam (60-120 GeV) will be extracted from the MI-10 section of Fermilab’s Main Injector. Neutrinos are produced after the protons hit a solid target and produce mesons which are sign selected and subsequently focused by a set of magnetic horns into a 204 m long decay pipe where they decay mostly into muons and neutrinos. The parameters of the facility were determined taking into account the physics goals, spacial and radiological constraints, and the experience gained by operating the NuMI facility at Fermilab. The initial beam power is expected to be ~1.2 MW; however, the facility is designed to be upgradeable for 2.3 MW operation. We discuss here the status of the design and the associated challenges.

  15. Design of the LBNE Beamline

    CERN Document Server

    Papadimitriou, V; Hylen, J; Kobilarcik, T; Marchionni, A; Moore, C D; Schlabach, P; Tariq, S

    2015-01-01

    The Long Baseline Neutrino Experiment (LBNE) will utilize a beamline facility located at Fermilab to carry out a compelling research program in neutrino physics. The facility will aim a wide band beam of neutrinos toward a detector placed at the Sanford Underground Research Facility in South Dakota, about 1,300 km away. The main elements of the facility are a primary proton beamline and a neutrino beamline. The primary proton beam (60 -120 GeV) will be extracted from the MI-10 section of Fermilab's Main Injector. Neutrinos are produced after the protons hit a solid target and produce mesons which are sign selected and subsequently focused by a set of magnetic horns into a 204 m long decay pipe where they decay mostly into muons and neutrinos. The parameters of the facility were determined taking into account the physics goals, spacial and radiological constraints and the experience gained by operating the NuMI facility at Fermilab. The initial beam power is expected to be ~1.2 MW, however the facility is desi...

  16. Design of the LBNF Beamline

    Energy Technology Data Exchange (ETDEWEB)

    Papadimitriou, V.; Andrews, R.; Hylen, J.; Kobilarcik, T.; Krafczyk, G.; Marchinonni, A.; Moore, C. D.; Schlabach, P.; Tariq, S.

    2015-08-30

    The Long Baseline Neutrino Facility (LBNF) will utilize a beamline located at Fermilab to carry out a compelling research program in neutrino physics. The facility will aim a wide band neutrino beam toward underground detectors placed at the SURF Facility in South Dakota, about 1,300 km away. The main elements of the facility are a primary proton beamline and a neutrino beamline. The primary proton beam (60-120 GeV) will be extracted from the MI-10 section of Fermilab’s Main Injector. Neutrinos are produced after the protons hit a solid target and produce mesons which are subsequently focused by magnetic horns into a 204 m long decay pipe where they decay into muons and neutrinos. The parameters of the facility were determined taking into account the physics goals, spacial and radiological constraints and the experience gained by operating the NuMI facility at Fermilab. The initial proton beam power is expected to be 1.2 MW; however, the facility is designed to be upgradeable to 2.4 MW. We discuss here the design status and the associated challenges as well as plans for improvements before baselining the facility.

  17. The new confocal heavy ion microprobe beamline at ANSTO: The first microprobe resolution tests and applications for elemental imaging and analysis

    Science.gov (United States)

    Pastuovic, Z.; Siegele, R.; Cohen, D. D.; Mann, M.; Ionescu, M.; Button, D.; Long, S.

    2017-08-01

    The Centre for Accelerator Science facility at ANSTO has been expanded with the new NEC 6 MV ;SIRIUS; accelerator system in 2015. In this paper we present a detailed description of the new nuclear microprobe-Confocal Heavy Ion Micro-Probe (CHIMP) together with results of the microprobe resolution testing and the elemental analysis performed on typical samples of mineral ore deposits and hyper-accumulating plants regularly measured at ANSTO. The CHIMP focusing and scanning systems are based on the OM-150 Oxford quadrupole triplet and the OM-26 separated scan-coil doublet configurations. A maximum ion rigidity of 38.9 amu-MeV was determined for the following nuclear microprobe configuration: the distance from object aperture to collimating slits of 5890 mm, the working distance of 165 mm and the lens bore diameter of 11 mm. The overall distance from the object to the image plane is 7138 mm. The CHIMP beamline has been tested with the 3 MeV H+ and 6 MeV He2+ ion beams. The settings of the object and collimating apertures have been optimized using the WinTRAX simulation code for calculation of the optimum acceptance settings in order to obtain the highest possible ion current for beam spot sizes of 1 μm and 5 μm. For optimized aperture settings of the CHIMP the beam brightness was measured to be ∼0.9 pA μm-2 mrad-2 for 3 MeV H+ ions, while the brightness of ∼0.4 pA μm-2 mrad-2 was measured for 6 MeV He2+ ions. The smallest beam sizes were achieved using a microbeam with reduced particle rate of 1000 Hz passing through the object slit apertures several micrometers wide. Under these conditions a spatial resolution of ∼0.6 μm × 1.5 μm for 3 MeV H+ and ∼1.8 μm × 1.8 μm for 6 MeV He2+ microbeams in horizontal (and vertical) dimension has been achieved. The beam sizes were verified using STIM imaging on 2000 and 1000 mesh Cu electron microscope grids.

  18. RESEARCH ON VIRTUAL-PART-BASED CONNECTING ELEMENT MODELING

    Institute of Scientific and Technical Information of China (English)

    2003-01-01

    Based on the inner character analysis of interpart, detail modification and assembly relation of mechanical connecting element, the idea, which extends the feature modeling of part to the interpart feature modeling for assembly purpose, is presented, and virtual-part-based connecting element modeling is proposed. During the assembly modeling, base parts are modified by the Boolean subtraction between the virtual part and the part to be connected. Dynamic matching algorithm, which is based on list database, is designed for dynamic extension and off-line editing of connecting part and virtual part, and design rules of connecting element is encapsulated by the virtual part. A prototyped software module for rapid design of connecting elements is implemented under self-developed CAD/CAM platform-SuperMan.

  19. Upgraded ESRF BM29 beamline for SAXS on macromolecules in solution

    Energy Technology Data Exchange (ETDEWEB)

    Pernot, Petra, E-mail: rejma@esrf.fr [ESRF, 6 Jules Horowitz, F-38043 Grenoble (France); Round, Adam [EMBL, 6 Jules Horowitz, F-38042 Grenoble (France); Barrett, Ray; De Maria Antolinos, Alejandro [ESRF, 6 Jules Horowitz, F-38043 Grenoble (France); Gobbo, Alexandre [EMBL, 6 Jules Horowitz, F-38042 Grenoble (France); Gordon, Elspeth [ESRF, 6 Jules Horowitz, F-38043 Grenoble (France); Huet, Julien [EMBL, 6 Jules Horowitz, F-38042 Grenoble (France); Kieffer, Jerôme; Lentini, Mario; Mattenet, Muriel; Morawe, Christian; Mueller-Dieckmann, Christoph; Ohlsson, Staffan; Schmid, Werner; Surr, John; Theveneau, Pascal; Zerrad, Louiza; McSweeney, Sean [ESRF, 6 Jules Horowitz, F-38043 Grenoble (France)

    2013-07-01

    A description of the new ESRF BioSAXS beamline is given. The beamline presented is dedicated to small-angle X-ray scattering of macromolecules in solution operating with a high-throughput sample-changer robot and automated data analysis for quality control and feedback. Small-angle X-ray scattering (SAXS) measurements of proteins in solution are becoming increasingly popular with biochemists and structural biologists owing to the presence of dedicated high-throughput beamlines at synchrotron sources. As part of the ESRF Upgrade program a dedicated instrument for performing SAXS from biological macromolecules in solution (BioSAXS) has been installed at the renovated BM29 location. The optics hutch has been equipped with new optical components of which the two principal elements are a fixed-exit double multilayer monochromator and a 1.1 m-long toroidal mirror. These new dedicated optics give improved beam characteristics (compared with the previous set-up on ID14-3) regarding the energy tunability, flux and focusing at the detector plane leading to reduced parasitic scattering and an extended s-range. User experiments on the beamline have been successfully carried out since June 2012. A description of the new BioSAXS beamline and the set-up characteristics are presented together with examples of obtained data.

  20. Status of the ELIMED multidisciplinary and medical beam-line at ELI-Beamlines

    Science.gov (United States)

    Romano, F.; Cirrone, G. A. P.; Cuttone, G.; Schillaci, F.; Scuderi, V.; Amico, A.; Candiano, G.; Giordanengo, S.; Guarachi, L. F.; Korn, G.; Larosa, G.; Leanza, R.; Manna, R.; Marchese, V.; Marchetto, F.; Margarone, D.; Milluzzo, G.; Petringa, G.; Pipek, J.; Sacchi, R.; Vignati, A.

    2017-01-01

    Nowadays, one of the biggest challenges consists in using high intensity laser-target interaction to generate high-energy ions for medical purposes, eventually replacing the old paradigm of acceleration characterized by huge and complex machines. In order to investigate the feasibility of using laser-driven ion beams for multidisciplinary application, a dedicated beam transport line will be installed at the ELI-Beamlines facility in Prague (CZ), as a part of the User-oriented ELIMAIA beam-line dedicated to ion acceleration and their potential applications. The beam-line section dedicated to transport and dosimetric endpoints is called ELIMED (ELI-Beamlines MEDical and multidisciplinary applications) and will be developed by the INFN-LNS.

  1. Beamlines at Siam photon laboratory

    CERN Document Server

    Songsiriritthigul, P; Ishii, T; Kakizaki, A

    2003-01-01

    This report provides the up-to-date information on the present and future beamlines at the Siam Photon Laboratory. The first two beamlines, BL-4 and BL-6, have already been installed, and are now in commissioning. BL-4 is a VUV beamline to be used for investigating the electronic structures of solids and solid surfaces using the angle-resolved photoemission experimental technique. BL-6 is a beamline for electron beam monitoring. Future beamlines utilizing synchrotron light generated by a planar undulator and a superconducting magnet wiggler are discussed.

  2. The ID23-2 structural biology microfocus beamline at the ESRF

    Energy Technology Data Exchange (ETDEWEB)

    Flot, David, E-mail: flot@esrf.fr [European Molecular Biology Laboratory, 6 rue Jules Horowitz, BP 181, 38042 Grenoble (France); Mairs, Trevor; Giraud, Thierry; Guijarro, Matias; Lesourd, Marc; Rey, Vicente; Brussel, Denis van; Morawe, Christian; Borel, Christine; Hignette, Olivier; Chavanne, Joel; Nurizzo, Didier; McSweeney, Sean; Mitchell, Edward [European Synchrotron Radiation Facility, 6 rue Jules Horowitz, BP 181, 38043 Grenoble (France)

    2010-01-01

    Beamline ID23-2, the first dedicated and highly automated high-throughput monochromatic macromolecular crystallography microfocus beamline, is described. The first phase of the ESRF beamline ID23 to be constructed was ID23-1, a tunable MAD-capable beamline which opened to users in early 2004. The second phase of the beamline to be constructed is ID23-2, a monochromatic microfocus beamline dedicated to macromolecular crystallography experiments. Beamline ID23-2 makes use of well characterized optical elements: a single-bounce silicon (111) monochromator and two mirrors in Kirkpatrick–Baez geometry to focus the X-ray beam. A major design goal of the ID23-2 beamline is to provide a reliable, easy-to-use and routine microfocus beam. ID23-2 started operation in November 2005, as the first beamline dedicated to microfocus macromolecular crystallography. The beamline has taken the standard automated ESRF macromolecular crystallography environment (both hardware and software), allowing users of ID23-2 to be rapidly familiar with the microfocus environment. This paper describes the beamline design, the special considerations taken into account given the microfocus beam, and summarizes the results of the first years of the beamline operation.

  3. ERLP Gun Commissioning Beamline Design

    CERN Document Server

    Holder, D J; Hannon, F E

    2004-01-01

    The 4GLS project is a novel next-generation solution for a UK national light source. It is based on an energy recovery linac (ERL) operating at high average beam currents up to 100 mA and with compression schemes producing pulses in the 10 - 100 fs range. This challenging accelerator technology, new to Europe, necessitates a significant R&D programme and a major part of this is a low-energy prototype, the ERLP, which is currently under construction at Daresbury Laboratory, in the north-west of England. The first components of ERLP to be built will be the DC photocathode gun and low-energy beam transport and diagnostics. The gun will initially be operated with a diagnostic beamline in order to measure the properties of the high-brightness beams generated as fully as possible. This will allow comparison of its performance with the results of multi-particle tracking codes, prior to its integration into the ERLP machine. The diagnostic beamline will include diagnostics for measuring the transverse and longitu...

  4. Beamline for schools

    CERN Multimedia

    2015-01-01

    This video is about BL4S Snapshot 22 Sep 2015 12:02:47From 10–20 September, winners of the Beamline for Schools competition visited CERN to perform their experiments. Two teams of high-school students – “Accelerating Africa” from South Africa and “Leo4G” from Italy – were chosen from a total of 119 teams, adding up to 1050 high-school students. “When we were told we’d won we never believed it. People’s parents thought we were lying,” says Michael Copeland from Accelerating Africa. The two teams shared a fully equipped accelerator beamline and conducted their experiment just like other researchers at CERN.

  5. Optical pseudomotors for soft x-ray beamlines.

    Science.gov (United States)

    Pedreira, P; Sics, I; Sorrentino, A; Pereiro, E; Aballe, L; Foerster, M; Pérez-Dieste, V; Escudero, C; Nicolas, J

    2016-05-01

    Optical elements of soft x-ray beamlines usually have motorized translations and rotations that allow for the fine alignment of the beamline. This is to steer the photon beam at some positions and to correct the focus on slits or on sample. Generally, each degree of freedom of a mirror induces a change of several parameters of the beam. Inversely, several motions are required to actuate on a single optical parameter, keeping the others unchanged. We define optical pseudomotors as combinations of physical motions of the optical elements of a beamline, which allow modifying one optical parameter without affecting the others. We describe a method to obtain analytic relationships between physical motions of mirrors and the corresponding variations of the beam parameters. This method has been implemented and tested at two beamlines at ALBA, where it is used to control the focus of the photon beam and its position independently.

  6. An Updated AP2 Beamline TURTLE Model

    Energy Technology Data Exchange (ETDEWEB)

    Gormley, M.; O' Day, S.

    1991-08-23

    This note describes a TURTLE model of the AP2 beamline. This model was created by D. Johnson and improved by J. Hangst. The authors of this note have made additional improvements which reflect recent element and magnet setting changes. The magnet characteristics measurements and survey data compiled to update the model will be presented. A printout of the actual TURTLE deck may be found in appendix A.

  7. Novel approaches in the SR beamline design

    Energy Technology Data Exchange (ETDEWEB)

    Kaznatcheev, K., E-mail: kaznatch@bnl.gov [Photon Science Directorates, Brookhaven National Laboratory, Upton, NY 11973-5000 (United States); Idir, M.; Chubar, O. [Photon Science Directorates, Brookhaven National Laboratory, Upton, NY 11973-5000 (United States)

    2013-05-11

    High brightness third generation x-ray sources bring new experimental possibilities and impose new challenges. Coherent scattering and diffraction-limited microscopy require wave-preserving optics, high-resolution inelastic scattering novel optical elements, where x-ray interferometry or the requirements of precise polarization measurements change the optical layout. With NSLS-II development as an illustration we discuss recent trends in beamline design.

  8. 45 CFR Appendix A to Part 1356 - NYTD Data Elements

    Science.gov (United States)

    2010-10-01

    ... Employment programs or vocational training Yes No 25 Budget and financial management Yes No 26 Housing... 45 Public Welfare 4 2010-10-01 2010-10-01 false NYTD Data Elements A Appendix A to Part 1356 Public Welfare Regulations Relating to Public Welfare (Continued) OFFICE OF HUMAN DEVELOPMENT SERVICES...

  9. LNLS: light source, beamlines, end stations and scientific instrumentation

    Energy Technology Data Exchange (ETDEWEB)

    Vicentin, Flavio Cesar [Laboratorio Nacional de Luz Sincrotron (LNLS), Campinas, SP (Brazil)

    2012-07-01

    Full text: The LNLS is operational since 1997 and has a second-generation light source with a 1,37GeV electron storage ring and 2,08 keV critical energy. Besides the storage ring there are various beamlines installed mainly in magnetic dipoles, however were opened three beamlines based in insertion devices, wiggler and undulator. The LNLS is now operating with 16 beamlines which are open to the external user community: 9 of them are dedicated to structural studies and the other 7 to spectroscopic techniques. The beamlines devoted to structural studies involve X-ray diffraction (XRD1, XRD2, XPD and XDS), small-angle X-ray scattering (SAXS1 and SAXS2), protein crystallography (MX1 and MX2) and X-ray fluorescence (XRF). The beamlines dedicated to spectroscopic studies are X-ray absorption fine structure (XAFS1, XAFS2 and DXAS), soft X-ray spectroscopy (SXS), spherical grating monochromator (SGM), plane grating monochromator (PGM) and toroidal grating monochromator (TGM). Two more beamlines are expected to begin their operation in 2012: X-ray tomography and infrared spectroscopy. Each beamline has its own characteristics in terms of photon energy range, flux, resolution and beam size, but many of the optical elements and instrumentation are common to various beamlines and the main are mirrors, monochromators (crystal and diffraction grating), slits and filters. For X-ray and VUV spectroscopy, several experimental techniques can be explored including XAS, XMCD, XMLD, XPS, AES, UPS, XEOL, reflectivity and PePiCo. For that, these beamlines share different end stations and instrumentation that can be easily installed and commissioned for attend a specific experiment. (author)

  10. Energy-dispersive X-ray diffraction beamline at Indus-2 synchrotron source

    Indian Academy of Sciences (India)

    K K Pandey; H K Poswal; A K Mishra; Abhilash Dwivedi; R Vasanthi; Nandini Garg; Surinder M Sharma

    2013-04-01

    An energy-dispersive X-ray diffraction beamline has been designed, developed and commissioned at BL-11 bending magnet port of the Indian synchrotron source, Indus-2. The performance of this beamline has been benchmarked by measuring diffraction patterns from various elemental metals and standard inorganic powdered samples. A few recent high-pressure investigations are presented to demonstrate the capabilities of the beamline.

  11. The macromolecular crystallography beamline I911-3 at the MAX IV laboratory

    Energy Technology Data Exchange (ETDEWEB)

    Ursby, Thomas, E-mail: thomas.ursby@maxlab.lu.se; Unge, Johan; Appio, Roberto [Lund University, POB 118, Lund SE-221 00 (Sweden); Logan, Derek T. [Lund University, POB 124, Lund SE-221 00 (Sweden); Fredslund, Folmer; Svensson, Christer; Larsson, Krister; Labrador, Ana [Lund University, POB 118, Lund SE-221 00 (Sweden); Thunnissen, Marjolein M. G. M. [Lund University, POB 124, Lund SE-221 00 (Sweden)

    2013-07-01

    The updated macromolecular crystallography beamline I911-3 at the MAX II storage ring is described. The macromolecular crystallography beamline I911-3, part of the Cassiopeia/I911 suite of beamlines, is based on a superconducting wiggler at the MAX II ring of the MAX IV Laboratory in Lund, Sweden. The beamline is energy-tunable within a range between 6 and 18 keV. I911-3 opened for users in 2005. In 2010–2011 the experimental station was completely rebuilt and refurbished such that it has become a state-of-the-art experimental station with better possibilities for rapid throughput, crystal screening and work with smaller samples. This paper describes the complete I911-3 beamline and how it is embedded in the Cassiopeia suite of beamlines.

  12. Upgraded ESRF BM29 beamline for SAXS on macromolecules in solution.

    Science.gov (United States)

    Pernot, Petra; Round, Adam; Barrett, Ray; De Maria Antolinos, Alejandro; Gobbo, Alexandre; Gordon, Elspeth; Huet, Julien; Kieffer, Jerôme; Lentini, Mario; Mattenet, Muriel; Morawe, Christian; Mueller-Dieckmann, Christoph; Ohlsson, Staffan; Schmid, Werner; Surr, John; Theveneau, Pascal; Zerrad, Louiza; McSweeney, Sean

    2013-07-01

    Small-angle X-ray scattering (SAXS) measurements of proteins in solution are becoming increasingly popular with biochemists and structural biologists owing to the presence of dedicated high-throughput beamlines at synchrotron sources. As part of the ESRF Upgrade program a dedicated instrument for performing SAXS from biological macromolecules in solution (BioSAXS) has been installed at the renovated BM29 location. The optics hutch has been equipped with new optical components of which the two principal elements are a fixed-exit double multilayer monochromator and a 1.1 m-long toroidal mirror. These new dedicated optics give improved beam characteristics (compared with the previous set-up on ID14-3) regarding the energy tunability, flux and focusing at the detector plane leading to reduced parasitic scattering and an extended s-range. User experiments on the beamline have been successfully carried out since June 2012. A description of the new BioSAXS beamline and the set-up characteristics are presented together with examples of obtained data.

  13. A microtomography beamline at the Louisiana State University Center for Advanced Microstructures and Devices synchrotron

    Science.gov (United States)

    Ham, Kyungmin; Jin, Hua; Butler, Leslie G.; Kurtz, Richard L.

    2002-03-01

    A microtomography beamline has been recently assembled and is currently operating at the Louisiana State University's Center for Advanced Microstructures and Devices synchrotron (CAMD). It has been installed on a bending magnet white-light beamline at port 7A. With the storage ring operating at 1.5 GeV, this beamline has a maximum usable x-ray energy of ˜15 keV. The instrumentation consists of computer-controlled positioning stages for alignment and rotation, a CsI(Tl) phosphor screen, a reflecting mirror, a microscope objective (1:1, 1:4), and Linux/LabVIEW-controlled charge coupled device. With the 1:4 objective, the maximum spatial resolution is 2.25 μm. The positioning and image acquisition computers communicate via transfer control protocol/internet protocol (TCP/IP). A small G4/Linux cluster has been installed for the purpose of on-site reconstruction. Instrument, alignment and reconstruction programs are written in MATLAB, IDL, and C. The applications to date are many and we present several examples. Several biological samples have been studied as part of an effort on biological visualization and computation. Future improvements to this microtomography station include the addition of a double-multilayer monochromator, allowing one to evaluate the three-dimensional elemental composition of materials. Plans also include eventual installation at the CAMD 7 T wiggler beamline, providing x rays in excess of 50 keV to provide better penetration of higher mass-density materials.

  14. The Low Density Matter (LDM) beamline at FERMI: optical layout and first commissioning.

    Science.gov (United States)

    Svetina, Cristian; Grazioli, Cesare; Mahne, Nicola; Raimondi, Lorenzo; Fava, Claudio; Zangrando, Marco; Gerusina, Simone; Alagia, Michele; Avaldi, Lorenzo; Cautero, Giuseppe; de Simone, Monica; Devetta, Michele; Di Fraia, Michele; Drabbels, Marcel; Feyer, Vitaliy; Finetti, Paola; Katzy, Raphael; Kivimäki, Antti; Lyamayev, Viktor; Mazza, Tommaso; Moise, Angelica; Möller, Thomas; O'Keeffe, Patrick; Ovcharenko, Yevheniy; Piseri, Paolo; Plekan, Oksana; Prince, Kevin C; Sergo, Rudi; Stienkemeier, Frank; Stranges, Stefano; Coreno, Marcello; Callegari, Carlo

    2015-05-01

    The Low Density Matter (LDM) beamline has been built as part of the FERMI free-electron laser (FEL) facility to serve the atomic, molecular and cluster physics community. After the commissioning phase, it received the first external users at the end of 2012. The design and characterization of the LDM photon transport system is described, detailing the optical components of the beamline.

  15. Emittance Measurement for Beamline Extension at the PET Cyclotron

    Directory of Open Access Journals (Sweden)

    Sae-Hoon Park

    2016-01-01

    Full Text Available Particle-induced X-ray emission is used for determining the elemental composition of materials. This method uses low-energy protons (of several MeV, which can be obtained from high-energy (of tens MeV accelerators. Instead of manufacturing an accelerator for generating the MeV protons, the use of a PET cyclotron has been suggested for designing the beamline for multipurpose applications, especially for the PIXE experiment, which has a dedicated high-energy (of tens MeV accelerator. The beam properties of the cyclotron were determined at this experimental facility by using an external beamline before transferring the ion beam to the experimental chamber. We measured the beam profile and calculated the emittance using the pepper-pot method. The beam profile was measured as the beam current using a wire scanner, and the emittance was measured as the beam distribution at the beam dump using a radiochromic film. We analyzed the measurement results and are planning to use the results obtained in the simulations of external beamline and aligned beamline components. We will consider energy degradation after computing the beamline simulation. The experimental study focused on measuring the emittance from the cyclotron, and the results of this study are presented in this paper.

  16. Simulating the Beam-line at CERN's ISOLDE Experiment

    CERN Document Server

    McGrath, Casey

    2013-01-01

    Maximizing the optical matching along portions of the ISOLDE beam-line and automating this procedure will make it easier for scientists to determine what the strengths of the electrical elds of each beam-line element should be in order to reduce particle loss. Simulations are run using a program called MAD-X, however, certain issues were discovered that hindered an immediate success of the simulations. Specifically, the transfer matrices for electrostatic components like the switchyards, kickers, and electric quadrupoles were missing from the original coding. The primary aim of this project was to design these components using AutoCAD and then extract the transfer matrices using SIMION. Future work will then implement these transfer matrices into the MAD-X code to make the simulations of the beam-line more accurate.

  17. A consistent partly cracked XFEM element for cohesive crack growth

    DEFF Research Database (Denmark)

    Asferg, Jesper L.; Poulsen, Peter Noe; Nielsen, Leif Otto

    2007-01-01

    capable of modelling variations in the discontinuous displacement field on both sides of the crack and hence also capable of modelling the case where equal stresses are present on each side of the crack. The enrichment was implemented for the 3-node constant strain triangle (CST) and a standard algorithm...... was used to solve the non-linear equations. The performance of the element is illustrated by modelling fracture mechanical benchmark tests. Investigations were carried out on the performance of the element for different crack lengths within one element. The results are compared with previously obtained...

  18. ALS beamline design requirements: A guide for beamline designers

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1996-06-01

    This manual is written as a guide for researchers in designing beamlines and endstations acceptable for use at the ALS. It contains guidelines and policies related to personnel safety and equipment and vacuum protection. All equipment and procedures must ultimately satisfy the safety requirements set aside in the Lawrence Berkeley National Laboratory (LBNL) Health and Safety Manual (PUB-3000) which is available from the ALS User Office or on the World WideWeb from the LBNL Homepage (http:// www.lbl.gov).

  19. Essential elements in depression and anxiety. Part I.

    Science.gov (United States)

    Młyniec, Katarzyna; Davies, Claire Linzi; de Agüero Sánchez, Irene Gómez; Pytka, Karolina; Budziszewska, Bogusława; Nowak, Gabriel

    2014-08-01

    Essential elements are very important for the proper functioning of the human body. They are required for fundamental life processes such as cell division and differentiation and protein synthesis. Thus a deficiency of these essential elements is associated with an enormous health risk that can ultimately lead to death. In recent years, studies have provided valuable information on the involvement of essential elements in psychiatric disorders, in particular depression and anxiety. There is strong evidence indicating that deficiency of essential elements can lead to the development of depressive and/or anxiogenic behaviour and supplementation can enhance therapeutic effect of antidepressants and anxiolytics. This review presents the most important results from preclinical and clinical studies showing involvement of essential elements such as zinc, magnesium, lithium, iron, calcium and chromium in depression and anxiety. From these studies it is evident that different types of depression and anxiety respond to treatment at different receptors indicating that the underlying mechanisms are slightly different. Furthermore, administration of low dose antidepressants supplemented with an element is effective and can reduce unwanted side effects in different types of depression/anxiety. Copyright © 2014 Institute of Pharmacology, Polish Academy of Sciences. Published by Elsevier Urban & Partner Sp. z o.o. All rights reserved.

  20. 3D Rigid-Plastic Finite Element Analysis for Skew Rolling Process of the Stepped Part

    Institute of Scientific and Technical Information of China (English)

    Gang FANG; Pan ZENG

    2003-01-01

    Based on rigid-plastic finite element method, a skew rolling process of stepped part is simulated. Considering nodesaving and effective remeshing, the tetrahedron solid elements are used to discrete workpiece. The workpiece material adopts rigid-plastic m

  1. A Remote and Virtual Synchrotron Beamline

    Science.gov (United States)

    Jackson, J. M.; Alp, E.; Sturhahn, W.

    2012-12-01

    National facilities offer one-of-a-kind opportunities to apply state-of-the-art experimental techniques to the pressing scientific problems of today. Yet, few students are able to experience research projects at national facilities due to limited accessibility caused in part by limited involvement in the local academic institution, constrained working areas at the experimental stations, and/or travel costs. We present a virtual and remote beam-line for Earth science studies using nuclear resonant and inelastic x-ray scattering methods at Sector 3 of the Advanced Photon Source at Argonne National Laboratory. Off-site students have the capability of controlling their measurements via secure internet connections and webcams. Students can access a 'view only mode' for ease of interaction and safety-control. More experienced users have exclusive control of the experiment and can remotely change variables within the experimental setup. Students may also access the virtual aspects these experiments by simulating certain conditions with our newly developed software. We evaluate such a tool by giving "before" and "after" assignments to students at different levels. These levels include high-school students from the Pasadena and greater Los Angeles area school districts, undergraduate students from Caltech's SURF/MURF program, and graduate students at Caltech. We specifically target underrepresented groups. Our results thus far show that the capabilities offered by our remote and virtual beamline show improved knowledge and understanding of applying experimental-based studies at the synchrotron to solve problems in the Earth sciences.

  2. I18--the microfocus spectroscopy beamline at the Diamond Light Source.

    Science.gov (United States)

    Mosselmans, J Frederick W; Quinn, Paul D; Dent, Andrew J; Cavill, Stuart A; Moreno, Sofia Diaz; Peach, Andrew; Leicester, Peter J; Keylock, Stephen J; Gregory, Simon R; Atkinson, Kirk D; Rosell, Josep Roque

    2009-11-01

    The design and performance of the microfocus spectroscopy beamline at the Diamond Light Source are described. The beamline is based on a 27 mm-period undulator to give an operable energy range between 2 and 20.7 keV, enabling it to cover the K-edges of the elements from P to Mo and the L(3)-edges from Sr to Pu. Micro-X-ray fluorescence, micro-EXAFS and micro-X-ray diffraction have all been achieved on the beamline with a spot size of approximately 3 microm. The principal optical elements of the beamline consist of a toroid mirror, a liquid-nitrogen-cooled double-crystal monochromator and a pair of bimorph Kirkpatrick-Baez mirrors. The performance of the optics is compared with theoretical values and a few of the early experimental results are summarized.

  3. Microbeam MAD Beamline for Challenging Protein Crystallography in TPS

    Science.gov (United States)

    Liu, D. G.; Chao, C. H.; Chang, C. H.; Juang, J. M.; Liu, C. Y.; Chang, S. H.; Chang, C. F.; Chou, C. K.; Tseng, C. C.; Chiang, C. H.; Jean, Y. C.; Tang, M. T.; Chung, S. C.; Chang, S. L.

    2013-03-01

    The TPS-05A beamline is the first X-ray beamline at NSRRC built for micro protein crystallography experiment as well as one of the seven ID beamlines in phase I at the TPS synchrotron facility. A 2-meter in-vacuum undulator (IU22) serves as the photon source from which the harmonics #3 to #9 will provide brilliance of 1018-1020 photons s-1 mrad-2 mm-2 (0.1% bandwidth)-1 and photon flux of 1013-1014 photons s-1 (0.1% bandwidth)-1 in the required energy range of 5.7-20 keV (2.175-0.620 Å) to cover MAD phasing experiments at 1 Å and SAD phasing experiments at 2 Å. The beamline optics consists of a cryo-cooled double crystal monochromator (DCM) and a pair of focusing K-B mirrors. Requirements from the user group include a target focus size of 50 μm × 50 μm (H × V) at the sample position, photon flux greater than 2 × 1012 photons s-1 at Se K-edge (0.9795 Å), pinholes for adjusting the beam size down to 5 μm. Calculation of heat load for the first optical element, i.e. the first crystal of DCM, is included in this paper.

  4. Taking Part in Technology Education: Elements in Students' Motivation

    Science.gov (United States)

    Autio, Ossi; Hietanoro, Jenni; Ruismaki, Heikki

    2011-01-01

    The purpose of this study was to determine the elements motivating comprehensive school students to study technology education. In addition, we tried to discover how students' motivation towards technology education developed over the period leading up to their school experience and the effect this might have on their future involvement with…

  5. Beamline 9.0.1 - a high-resolution undulator beamline for gas-phase spectroscopy

    Energy Technology Data Exchange (ETDEWEB)

    Bozek, J.D.; Heimann, P.A.; Mossessian, D. [Ernest Orlando Lawrence Berkeley National Lab., CA (United States)

    1997-04-01

    Beamline 9.0.1 at the Advanced Light Source is an undulator beamline with a Spherical Grating Monochromator (SGM) which provides very high resolution and flux over the photon energy range 20-320eV. The beamline has been used primarily by the atomic and molecular science community to conduct spectroscopy experiments using electron, ion and fluorescence photon detection. A description of the beamline and its performance will be provided in this abstract.

  6. A partly and fully cracked triangular XFEM element for modeling cohesive fracture

    DEFF Research Database (Denmark)

    Mougaard, Jens Falkenskov; Poulsen, Peter Noe; Nielsen, Leif Otto

    2011-01-01

    This paper discusses the build‐up of a partly cracked cohesive crack tip element. The crack tip element is based on the principles of the eXtended Finite Element Method (XFEM) and is of Linear Strain Triangle (LST) type. The composition of the enrichment has been in focus to achieve as complete...

  7. Beamline for Schools Safety Awareness Day

    CERN Multimedia

    Photo Service, CERN

    2014-01-01

    The first two teams to participate in CERN's Beamline for Schools project spent their first day at CERN at the Safety Training Center in Prévessin. They covered amongst others radiation protection, cryogenics and fire-fighting. The teams will spend the rest of the week at the T9 beamline.

  8. BNL ATF II beamlines design

    Energy Technology Data Exchange (ETDEWEB)

    Fedurin, M. [Brookhaven National Lab. (BNL), Upton, NY (United States); Jing, Y. [Brookhaven National Lab. (BNL), Upton, NY (United States); Stratakis, D. [Brookhaven National Lab. (BNL), Upton, NY (United States); Swinson, C. [Brookhaven National Lab. (BNL), Upton, NY (United States)

    2015-05-03

    The Brookhaven National Laboratory. Accelerator Test Facility (BNL ATF) is currently undergoing a major upgrade (ATF-II). Together with a new location and much improved facilities, the ATF will see an upgrade in its major capabilities: electron beam energy and quality and CO2 laser power. The electron beam energy will be increased in stages, first to 100-150 MeV followed by a further increase to 500 MeV. Combined with the planned increase in CO2 laser power (from 1-100 TW), the ATF-II will be a powerful tool for Advanced Accelerator research. A high-brightness electron beam, produced by a photocathode gun, will be accelerated and optionally delivered to multiple beamlines. Besides the energy range (up to a possible 500 MeV in the final stage) the electron beam can be tailored to each experiment with options such as: small transverse beam size (<10 um), short bunch length (<100 fsec) and, combined short and small bunch options. This report gives a detailed overview of the ATFII capabilities and beamlines configuration.

  9. Design of the LBNF Beamline

    Energy Technology Data Exchange (ETDEWEB)

    Papadimitriou, Vaia; et al.

    2016-06-01

    The Long Baseline Neutrino Facility (LBNF) will utilize a beamline located at Fermilab to provide and aim a neutrino beam of sufficient intensity and appropriate energy range toward DUNE detectors, placed deep underground at the SURF Facility in South Dakota. The primary proton beam (60 - 120 GeV) will be extracted from the MI-10 section of Fermilab's Main Injector. Neutrinos are produced after the protons hit a solid target and produce mesons which are subsequently focused by magnetic horns into a 194 m long decay pipe where they decay into muons and neutrinos. The parameters of the facility were determined taking into account the physics goals, spacial and radiological constraints and the experience gained by operating the NuMI facility at Fermilab. The Beamline facility is designed for initial operation at a proton-beam power of 1.2 MW, with the capability to support an upgrade to 2.4 MW. LBNF/DUNE obtained CD-1 approval in November 2015. We discuss here the design status and the associated challenges as well as the R&D and plans for improvements before baselining the facility.

  10. First X-ray fluorescence CT experimental results at the SSRF X-ray imaging beamline

    Institute of Scientific and Technical Information of China (English)

    DENG Biao; YANG Qun; XIE Hong-Lan; DU Guo-Hao; XIAO Wi-Qiao

    2011-01-01

    X-ray fluorescence CT is a non-destructive technique for detecting elemental composition and distribution inside a specimen. In this paper, the first experimental results of X-ray fluorescence CT obtained at the SSRF X-ray imaging beamline (BL13W1) are described. The test samples were investigated and the 2D elemental image was reconstructed using a filtered back-projection algorithm. In the sample the element Cd was observed. Up to now, the X-ray fluorescence CT could be carried out at the SSRF X-ray imaging beamline.

  11. Time-resolved neutron imaging at ANTARES cold neutron beamline

    CERN Document Server

    Tremsin, A S; Tittelmeier, K; Schillinger, B; Schulz, M; Lerche, M; Feller, W B

    2015-01-01

    In non-destructive evaluation with X-rays light elements embedded in dense, heavy (or high-Z) matrices show little contrast and their structural details can hardly be revealed. Neutron radiography, on the other hand, provides a solution for those cases, in particular for hydrogenous materials, owing to the large neutron scattering cross section of hydrogen and uncorrelated dependency of neutron cross section on the atomic number. The majority of neutron imaging experiments at the present time is conducted with static objects mainly due to the limited flux intensity of neutron beamline facilities and sometimes due to the limitations of the detectors. However, some applications require the studies of dynamic phenomena and can now be conducted at several high intensity beamlines such as the recently rebuilt ANTARES beam line at the FRM-II reactor. In this paper we demonstrate the capabilities of time resolved imaging for repetitive processes, where different phases of the process can be imaged simultaneously and...

  12. An atomic finite element model for biodegradable polymers. Part 1. Formulation of the finite elements.

    Science.gov (United States)

    Gleadall, Andrew; Pan, Jingzhe; Ding, Lifeng; Kruft, Marc-Anton; Curcó, David

    2015-11-01

    Molecular dynamics (MD) simulations are widely used to analyse materials at the atomic scale. However, MD has high computational demands, which may inhibit its use for simulations of structures involving large numbers of atoms such as amorphous polymer structures. An atomic-scale finite element method (AFEM) is presented in this study with significantly lower computational demands than MD. Due to the reduced computational demands, AFEM is suitable for the analysis of Young's modulus of amorphous polymer structures. This is of particular interest when studying the degradation of bioresorbable polymers, which is the topic of an accompanying paper. AFEM is derived from the inter-atomic potential energy functions of an MD force field. The nonlinear MD functions were adapted to enable static linear analysis. Finite element formulations were derived to represent interatomic potential energy functions between two, three and four atoms. Validation of the AFEM was conducted through its application to atomic structures for crystalline and amorphous poly(lactide).

  13. Diagnostic X-Multi-Axis Beamline

    Energy Technology Data Exchange (ETDEWEB)

    Paul, A C

    2000-04-05

    Tomographic reconstruction of explosive events require time resolved multipal lines of sight. Considered here is a four (or eight) line of sight beam layout for a nominal 20 MeV 2000 Ampere 2 microsecond electron beam for generation of x-rays 0.9 to 5 meters from a given point, the ''firing point''. The requirement of a millimeter spatial x-ray source requires that the electron beam be delivered to the converter targets with sub-millimeter precision independent of small variations in beam energy and initial conditions. The 2 usec electron beam pulse allows for four bursts in each line, separated in time by about 500 microseconds. Each burst is divided by a electro-magnetic kicker into four (or eight) pulses, one for each beamline. The arrival time of the four (or eight) beam pulses at the x-ray target can be adjusted by the kicker timing and the sequence that the beams of each burst are switched into the different beamlines. There exists a simple conceptual path from a four beamline to a eight beamline upgrade. The eight line beamline is built up from seven unique types of sub-systems or ''blocks''. The beamline consists of 22 of these functional blocks and contains a total of 455 individual magnets, figure 1. The 22 blocks are inter-connected by a total of 30 straight line inter-block sections (IBS). Beamlines 1-4 are built from 12 blocks with conceptual layout structure shown in figure 2. Beamlines 5-8 are built with an additional 10 blocks with conceptual layout structure shown in figure 3. This beamline can be thought of as looking like a lollipop consisting of a 42 meter long stick leading to a 60 by 70 meter rectangular candy blob consisting of the eight lines of sight. The accelerator providing the electron beam is at the end of the stick and the firing point is at the center of the blob. The design allows for a two stage implementation. Beamlines 1-3 can be installed to provide a tomographic azimuthal resolution of 45

  14. Simulation of beamline alignment operations

    Energy Technology Data Exchange (ETDEWEB)

    Annese, C; Miller, M G

    1999-02-02

    The CORBA-based Simulator was a Laboratory Directed Research and Development (LDRD) project that applied simulation techniques to explore critical questions about distributed control systems. The simulator project used a three-prong approach that studied object-oriented distribution tools, computer network modeling, and simulation of key control system scenarios. The National Ignition Facility's (NIF) optical alignment system was modeled to study control system operations. The alignment of NIF's 192 beamlines is a large complex operation involving more than 100 computer systems and 8000 mechanized devices. The alignment process is defined by a detailed set of procedures; however, many of the steps are deterministic. The alignment steps for a poorly aligned component are similar to that of a nearly aligned component; however, additional operations/iterations are required to complete the process. Thus, the same alignment operations will require variable amounts of time to perform depending on the current alignment condition as well as other factors. Simulation of the alignment process is necessary to understand beamline alignment time requirements and how shared resources such as the Output Sensor and Target Alignment Sensor effect alignment efficiency. The simulation has provided alignment time estimates and other results based on documented alignment procedures and alignment experience gained in the laboratory. Computer communication time, mechanical hardware actuation times, image processing algorithm execution times, etc. have been experimentally determined and incorporated into the model. Previous analysis of alignment operations utilized average implementation times for all alignment operations. Resource sharing becomes rather simple to model when only average values are used. The time required to actually implement the many individual alignment operations will be quite dynamic. The simulation model estimates the time to complete an operation using

  15. Holographic optical elements recorded in silver halide sensitized gelatin emulsions. Part I. Transmission holographic optical elements.

    Science.gov (United States)

    Kim, J M; Choi, B S; Kim, S I; Kim, J M; Bjelkhagen, H I; Phillips, N J

    2001-02-10

    Silver halide sensitized gelatin (SHSG) holograms are similar to holograms recorded in dichromated gelatin (DCG), the main recording material for holographic optical elements (HOE's). The drawback of DCG is its low sensitivity and limited spectral response. Silver halide materials can be processed in such a way that the final hologram will have properties like a DCG hologram. Recently this technique has become more interesting since the introduction of new ultra-high-resolution silver halide emulsions. An optimized processing technique for transmission HOE's recorded in these materials is introduced. Diffraction efficiencies over 90% can be obtained for transmissive diffraction gratings. Understanding the importance of the selective hardening process has made it possible to obtain results similar to conventional DCG processing. The main advantage of the SHSG process is that high-sensitivity recording can be performed with laser wavelengths anywhere within the visible spectrum. This simplifies the manufacturing of high-quality, large-format HOE's.

  16. The BALDER Beamline at the MAX IV Laboratory

    Science.gov (United States)

    Klementiev, K.; Norén, K.; Carlson, S.; Sigfridsson Clauss, K. G. V.; Persson, I.

    2016-05-01

    X-ray absorption spectroscopy (XAS) includes well-established methods to study the local structure around the absorbing element - extended X-ray absorption fine structure (EXAFS), and the effective oxidation number or to quantitatively determine the speciation of an element in a complex matrix - X-ray absorption near-edge structure (XANES). The increased brilliance and intensities available at the new generation of synchrotron light sources makes it possible to study, in-situ and in-operando, much more dilute systems with relevance for natural systems, as well as the micro-scale variability and dynamics of chemical reactions on the millisecond time-scale. The design of the BALDER beamline at the MAX IV Laboratory 3 GeV ring has focused on a high flux of photons in a wide energy range, 2.4-40 keV, where the K-edge is covered for the elements S to La, and the L 3-edge for all elements heavier than Sb. The overall design of the beamline will allow large flexibility in energy range, beam size and data collection time. The other focus of the beamline design is the possibility to perform multi-technique analyses on samples. Development of sample environment requires focus on implementation of auxiliary methods in such a way that techniques like Fourier transform infrared (FTIR) spectroscopy, UV-Raman spectroscopy, X-ray diffraction and/or mass spectrometry can be performed simultaneously as the XAS study. It will be a flexible system where different instruments can be plugged in and out depending on the needs for the particular investigation. Many research areas will benefit from the properties of the wiggler based light source and the capabilities to perform in-situ and in-operando measurements, for example environmental and geochemical sciences, nuclear chemistry, catalysis, materials sciences, and cultural heritage.

  17. Holographic optical elements recorded in silver halide sensitized gelatin emulsions. Part 2. Reflection holographic optical elements.

    Science.gov (United States)

    Kim, Jong Man; Choi, Byung So; Choi, Yoon Sun; Kim, Jong Min; Bjelkhagen, Hans I; Phillips, Nicholas J

    2002-03-10

    Silver halide sensitized gelatin (SHSG) holograms are similar to holograms recorded in dichromated gelatin (DCG), the main recording material for holographic optical elements (HOEs). The drawback of DCG is its low energetic sensitivity and limited spectral response. Silver halide materials can be processed in such away that the final hologram will have properties like a DCG hologram. Recently this technique has become more interesting since the introduction of new ultra-fine-grain silver halide (AgHal) emulsions. In particular, high spatial-frequency fringes associated with HOEs of the reflection type are difficult to construct when SHSG processing methods are employed. Therefore an optimized processing technique for reflection HOEs recorded in the new AgHal materials is introduced. Diffraction efficiencies over 90% can be obtained repeatably for reflection diffraction gratings. Understanding the importance of a selective hardening process has made it possible to obtain results similar to conventional DCG processing. The main advantage of the SHSG process is that high-sensitivity recording can be performed with laser wavelengths anywhere within the visible spectrum. This simplifies the manufacturing of high-quality, large-format HOEs, also including high-quality display holograms of the reflection type in both monochrome and full color.

  18. Imaging beamline for high energy proton radiography

    Institute of Scientific and Technical Information of China (English)

    WEI Tao; YANG Guo-Jun; LONG Ji-Dong; WANG Shao-Heng; HE Xiao-Zhong

    2012-01-01

    Proton radiography is a new tool for advanced hydrotesting.This article will discuss the basic concept of proton radiography first,especially the magnetic lens system.Then a scenario of 50 GeV imaging beamline will be described in every particular,including the matching section,Zumbro lens system and imaging system.The simulation result shows that the scenario of imaging beamline performs well,and the influence of secondary particles can be neglected.

  19. ROCK: the new Quick-EXAFS beamline at SOLEIL

    Science.gov (United States)

    Briois, V.; La Fontaine, C.; Belin, S.; Barthe, L.; Moreno, Th; Pinty, V.; Carcy, A.; Girardot, R.; Fonda, E.

    2016-05-01

    ROCK is a new beamline at SOLEIL dedicated to Quick-EXAFS measurements. The optical layout has been optimized to get full advantage of the monochromators, which were designed at SOLEIL and successfully used at SAMBA from 2009 to 2014. ROCK has started user operations since March 2015. It is mainly employed to monitor fast kinetic processes in materials used in catalysis and energy sciences. A review of the ROCK performances and capabilities is presented. The high automation achieved for fast change of monochromators, optimization of mirrors for harmonic rejection and detectors allows the simultaneous operando characterization of different chemical elements present in a material during the same reaction.

  20. Beamline Insertions Manager at Jefferson Lab

    Energy Technology Data Exchange (ETDEWEB)

    Johnson, Michael C. [Jefferson Lab., Newport News, VA (United States)

    2015-09-01

    The beam viewer system at Jefferson Lab provides operators and beam physicists with qualitative and quantitative information on the transverse electron beam properties. There are over 140 beam viewers installed on the 12 GeV CEBAF accelerator. This paper describes an upgrade consisting of replacing the EPICS-based system tasked with managing all viewers with a mixed system utilizing EPICS and high-level software. Most devices, particularly the beam viewers, cannot be safely inserted into the beam line during high-current beam operations. Software is partly responsible for protecting the machine from untimely insertions. The multiplicity of beam-blocking and beam-vulnerable devices motivates us to try a data-driven approach. The beamline insertions application components are centrally managed and configured through an object-oriented software framework created for this purpose. A rules-based engine tracks the configuration and status of every device, along with the beam status of the machine segment containing the device. The application uses this information to decide on which device actions are allowed at any given time.

  1. [Determination of inorganic elements in different parts of Sonchus oleraceus L by flame atomic absorption spectrometry].

    Science.gov (United States)

    Wang, Nai-Xing; Cui, Xue-Gui; Du, Ai-Qin; Mao, Hong-Zhi

    2007-06-01

    Flame atomic absorption spectrometry with air-acetylene flame was used for the determination of inorganic metal elements in different parts ( flower, leaf, stem and root) of Sonchus oleraceus L. The contents of Ca, Mg, K, Na, Fe, Mn, Cu, Zn, Cr, Co, Ni, Pb and Cd in the flower, leaf, stem and root of Sonchus oleraceus L were compared. The order from high to low of the additive weight (microg x g(-1)) for the 13 kinds of metal elements is as follows: leaf (77 213.72) > flower (47 927.15) > stem(42 280.99) > root (28 131.18). From the experimental results it was found that there were considerable differences in the contents of the metal elements in different parts, and there were richer contents of Fe, Zn, Mn and Cu in root and flower, which are necessary to human health, than in other parts.

  2. Ring beamlines and instrumentation for industrial applications

    Science.gov (United States)

    Pearce, W. Jorge; Trippe, Anthony P.

    1994-08-01

    Many recently constructed storage rings are catering to the needs of industrial applications in addition to providing the traditional services required for synchrotron radiation research. The Center for Advanced Microstructures and Devices (CAMD) was established by Louisiana State University to pioneer development of microfabrication while supporting research in basic science. Maxwell Laboratories designed, built, and successfully commissioned the 1.2 GeV, 400 mA light source for CAMD. Maxwell Laboratories has completed one X-ray lithography beamline at CAMD, and two more are now being manufactured. The completed beamline system, designed for thin resists, delivers photons up to 2 keV. The two beamlines currently under construction deliver photons up to 6 keV for thick (> 50 μm) resists, which play a role in the fabrication of 3-D nanostructures. One of the thick-resist beamlines includes an aspheric mirror that collimates the synchrotron-radiation beam in the horizontal plane while focusing it in the vertical direction - creating a sharp, uniform line image at the workpiece. The other thick-resist beamline has conventional planar optics. Beam position monitors (BPMs) developed for the CAMD beamlines provide a precise vertical profile of the beam by measuring differential photocurrents generated in the BPM probes. Beam power measurements are accomplished with a fixed-aperture calorimeter. Since each calorimeter is precisely calibrated before shipment, its thermal response in the beam is an accurate means to determine beam power for setting lithography exposure times or for computing beamline energy balance.

  3. Conceptual design of NBI beamline for VEST plasma heating

    Energy Technology Data Exchange (ETDEWEB)

    Kim, T.S., E-mail: tskim@kaeri.re.kr; In, S.R.; Jeong, S.H.; Park, M.; Chang, D.H.; Jung, B.K.; Lee, K.W.

    2016-11-01

    Highlights: • VEST NBI injector is conceptually designed to support further VEST plasma experiment. • VEST NBI injector composed of 2 sets of 20 keV/25A magnetic cusp type bucket ion source, neutralizer ducts, electrostatic ion dumps, NB vessel with cryopump, and rotating calorimerter. • The vacuum vessel of the beamline is divided into two parts for high injection efficiency and different direction (co- and counter-current) of neutral beam injection. • An ion source for the VEST NBI system was also designed to deliver neutral hydrogen beams with a power of 0.3 MW. The plasma generator of the VEST NB ion source has modified TFTR bucket multi-cusp chamber. The plasma generator has twelve hair-pin shaped tungsten filaments used as a cathode and an arc chamber including a bucket and an electron dump which serve as anode. The accelerator system consists of three grids, each having extraction area of 100 mm × 320 mm and 64 shaped slits of 3 mm spacing. • The preliminary structure design and the layout of the main components of the injector have been completed. Simulation and calculation for optimization of the NB beamline design results prove that the parameters of ion source, neutralization efficiency (76%:95% equilibrium neutralization efficiency), and beam power transmission efficiency (higher than 90%) are in agreement with design targets of the VEST NB beamline. • This VEST NBI system will provide a neutral beam of ∼0.6 MW for both heating and current drive in torus plasma. - Abstract: A 10 m s-pulsed NBI (Neutral Beam Injection) system for VEST (Versatile Experiment Spherical Torus) plasma heating is designed to provide a beam power of more than 0.6 MW with 20 keV H° neutrals. The VEST NBI injector is composed of 2 sets of 20 keV/25A magnetic cusp type bucket ion source, neutralizer ducts, residual ion dump, NB vessel with a cryopump, and rotating calorimeter. The position and size of these beamline components are roughly determined with geometric

  4. P13, the EMBL macromolecular crystallography beamline at the low-emittance PETRA III ring for high- and low-energy phasing with variable beam focusing

    Science.gov (United States)

    Cianci, Michele; Bourenkov, Gleb; Pompidor, Guillaume; Karpics, Ivars; Kallio, Johanna; Bento, Isabel; Roessle, Manfred; Cipriani, Florent; Fiedler, Stefan; Schneider, Thomas R.

    2017-01-01

    The macromolecular crystallography P13 beamline is part of the European Molecular Biology Laboratory Integrated Facility for Structural Biology at PETRA III (DESY, Hamburg, Germany) and has been in user operation since mid-2013. P13 is tunable across the energy range from 4 to 17.5 keV to support crystallographic data acquisition exploiting a wide range of elemental absorption edges for experimental phase determination. An adaptive Kirk­patrick–Baez focusing system provides an X-ray beam with a high photon flux and tunable focus size to adapt to diverse experimental situations. Data collections at energies as low as 4 keV (λ = 3.1 Å) are possible due to a beamline design minimizing background and maximizing photon flux particularly at low energy (up to 1011 photons s−1 at 4 keV), a custom calibration of the PILATUS 6M-F detector for use at low energies, and the availability of a helium path. At high energies, the high photon flux (5.4 × 1011 photons s−1 at 17.5 keV) combined with a large area detector mounted on a 2θ arm allows data collection to sub-atomic resolution (0.55 Å). A peak flux of about 8.0 × 1012 photons s−1 is reached at 11 keV. Automated sample mounting is available by means of the robotic sample changer ‘MARVIN’ with a dewar capacity of 160 samples. In close proximity to the beamline, laboratories have been set up for sample preparation and characterization; a laboratory specifically equipped for on-site heavy atom derivatization with a library of more than 150 compounds is available to beamline users. PMID:28009574

  5. BAMline: the first hard X-ray beamline at BESSY II

    Energy Technology Data Exchange (ETDEWEB)

    Goerner, W.; Hentschel, M.P.; Mueller, B.R. E-mail: bernd.mueller@bam.de; Riesemeier, H.; Krumrey, M.; Ulm, G.; Diete, W.; Klein, U.; Frahm, R

    2001-07-21

    The first hard X-ray beamline at BESSY II will be installed by BAM and PTB at a superconducting 7 T wavelength shifter. The main optical elements of the beamline are a Double-Multilayer-Monochromator and a Double-Crystal-Monochromator. The two devices can be used separately or in-line. Main applications of monochromatic radiation with photon energies up to 50 keV are X-ray fluorescence analysis, micro-computed tomography, X-ray topography, detector calibration and reflectometry. Calculable undispersed radiation up to 200 keV will be available for radiometric applications.

  6. Understanding the instrumental profile of synchrotron radiation X-ray powder diffraction beamlines.

    Science.gov (United States)

    Rebuffi, Luca; Sánchez Del Río, Manuel; Busetto, Edoardo; Scardi, Paolo

    2017-05-01

    A Monte Carlo algorithm has been developed to calculate the instrumental profile function of a powder diffraction synchrotron beamline. Realistic models of all optical elements are implemented in a ray-tracing software. The proposed approach and the emerging paradigm have been investigated and verified for several existing X-ray powder diffraction beamlines. The results, which can be extended to further facilities, show a new and general way of assessing the contribution of instrumental broadening to synchrotron radiation data, based on ab initio simulations.

  7. Elements of nonlinear quantum mechanics (Part II): Triple bracket generalization of quantum mechanics

    OpenAIRE

    Czachor, Marek

    1994-01-01

    A new version of NLQM is formulated in terms of the generalized Nambu dynamics. The generalization is free from the difficulties of earlier approaches. The paper is a second part of "Elements of NLQM (I): NL Schrodinger equation and two-level atoms".

  8. Experience with Multi-Beam and Multi-Beamline FEL-Operation

    Science.gov (United States)

    Rönsch-Schulenburg, J.; Faatz, B.; Honkavaara, K.; Kuhlmann, M.; Schreiber, S.; Treusch, R.; Vogt, M.

    2017-07-01

    DESY’s free-electron laser FLASH provides soft X-ray pulses for scientific users at wavelengths down to 4nm simultaneously in two undulator beamlines. They are driven by a common linear superconducting accelerator with a beam energy of up to 1.25 GeV. The superconducting technology allows the acceleration of electron bunch trains of several hundred bunches with a spacing of 1 microsecond or more and a repetition rate of 10 Hz. A fast kickerseptum system directs one part of the bunch train to FLASH1 and the other part to FLASH2 keeping the full 10 Hz repetition rate for both. The unique setup of FLASH allows independent FEL pulse parameters for both beamlines. In April 2016, simultaneous operation of FLASH1 and FLASH2 for external users started. This paper reports on our operating experience with this type of multi-beam, multi-beamline set-up.

  9. Application of partially coherent wavefront propagation calculations for design of coherence-preserving synchrotron radiation beamlines

    Science.gov (United States)

    Chubar, Oleg; Chu, Yong S.; Kaznatcheev, Konstantine; Yan, Hanfei

    2011-09-01

    Ultra-low emittance third-generation synchrotron radiation (SR) sources, such as NSLS-II and MAX-IV, will offer excellent opportunities for further development of experimental techniques exploiting X-ray coherence. However, even in these new SR sources, the radiation produced by relativistic electrons (in undulators, wigglers and bending magnets) will remain only partially coherent in the X-ray spectral range. "Extraction" of "coherent portion" of the radiation flux and its transport to sample without loss of coherence must be performed by dedicated SR beamlines, optimized for particular types of experiments. Detailed quantitative prediction of partially coherent X-ray beam properties at propagation through optical elements, which is required for the optimization of such beamlines, can only be obtained from accurate and efficient physical-optics based numerical simulations. Examples of such simulations, made for NSLS-II beamlines, using "Synchrotron Radiation Workshop" (SRW) computer code, are presented. Special attention is paid to the numerical analysis of the basic properties of partially coherent undulator radiation beam and its distinctions from the Gaussian beam. Performance characteristics of importance for particular beamlines, such as radiation spot size and flux at sample vs size of secondary source aperture for high-resolution microscopy beamlines, are predicted by the simulations.

  10. Numerical analysis of partially coherent radiation at soft x-ray beamline.

    Science.gov (United States)

    Meng, Xiangyu; Xue, Chaofan; Yu, Huaina; Wang, Yong; Wu, Yanqing; Tai, Renzhong

    2015-11-16

    A new model for numerical analysis of partially coherent x-ray at synchrotron beamlines is presented. The model is based on statistical optics. Four-dimensional coherence function, Mutual Optical Intensity (MOI), is applied to describe the wavefront of the partially coherent light. The propagation of MOI through optical elements in the beamline is deduced with numerical calculation. The coherence of x-ray through beamlines can be acquired. We applied the model to analyze the coherence in the STXM beamline at SSRF, and got the coherence length of the beam at the endstation. To verify the theoretical results, the diffraction experiment of a single slit was performed and the diffraction pattern was simulated to get the coherence length, (31 ± 3.0) µm × (25 ± 2.1) µm (H × V), which had a good agreement with the theoretical results, (30.7 ± 0.6) µm × (31 ± 5.3) µm (H × V). The model is applicable to analyze the coherence in synchrotron beamlines.

  11. nuSTORM Pion Beamline Design Update

    Energy Technology Data Exchange (ETDEWEB)

    Liu, A. [Indiana U.; Bross, A. [Fermilab; Neuffer, D. [Fermilab; Lee, S. Y. [Indiana U.

    2013-09-01

    A facility producing neutrinos from muons that decay in a racetrack ring can provide extremely well understood neutrino beams for oscillation physics and the search for sterile neutrinos. The “neutrinos from STORed Muons” (nuSTORM) facility based on this idea has been introduced by Bross, Neuffer et al. The design of the nuSTORM facility and the particle tracking have been presented in the paper of Liu, et al. This paper demonstrates the recent optimization results of the pion beamline, with G4beamline simulations. The optimum choice of pion beam center momentum, a new algorithm on fitting bivariate Gaussian distribution to the pion phase space data at the downstream side of the horn, and the comparison of the beamline performance with the optics designed based on Graphite and Inconel targets are also described.

  12. Laser-driven electron beamlines generated by coupling laser-plasma sources with conventional transport systems

    Energy Technology Data Exchange (ETDEWEB)

    Antici, P. [Istituto Nazionale di Fisica Nucleare (INFN), Laboratori Nazionali di Frascati, Via E. Fermi, 40, 00044 Frascati (Italy); SAPIENZA, University of Rome, Dip. SBAI, Via A. Scarpa 14, 00161 Rome (Italy); INFN - Sezione di Roma, c/o Dipartimento di Fisica - SAPIENZA, University of Rome, P.le Aldo Moro, 2 - 00185 Rome (Italy); Bacci, A.; Chiadroni, E.; Ferrario, M.; Rossi, A. R. [Istituto Nazionale di Fisica Nucleare (INFN), Laboratori Nazionali di Frascati, Via E. Fermi, 40, 00044 Frascati (Italy); Benedetti, C. [University of Bologna and INFN - Bologna (Italy); Lancia, L.; Migliorati, M.; Mostacci, A.; Palumbo, L. [SAPIENZA, University of Rome, Dip. SBAI, Via A. Scarpa 14, 00161 Rome (Italy); INFN - Sezione di Roma, c/o Dipartimento di Fisica - SAPIENZA, University of Rome, P.le Aldo Moro, 2 - 00185 Rome (Italy); Serafini, L. [INFN-Milan and Department of Physics, University of Milan, Via Celoria 16, 20133 Milan (Italy)

    2012-08-15

    Laser-driven electron beamlines are receiving increasing interest from the particle accelerator community. In particular, the high initial energy, low emittance, and high beam current of the plasma based electron source potentially allow generating much more compact and bright particle accelerators than what conventional accelerator technology can achieve. Using laser-generated particles as injectors for generating beamlines could significantly reduce the size and cost of accelerator facilities. Unfortunately, several features of laser-based particle beams need still to be improved before considering them for particle beamlines and thus enable the use of plasma-driven accelerators for the multiple applications of traditional accelerators. Besides working on the plasma source itself, a promising approach to shape the laser-generated beams is coupling them with conventional accelerator elements in order to benefit from both a versatile electron source and a controllable beam. In this paper, we perform start-to-end simulations to generate laser-driven beamlines using conventional accelerator codes and methodologies. Starting with laser-generated electrons that can be obtained with established multi-hundred TW laser systems, we compare different options to capture and transport the beams. This is performed with the aim of providing beamlines suitable for potential applications, such as free electron lasers. In our approach, we have analyzed which parameters are critical at the source and from there evaluated different ways to overcome these issues using conventional accelerator elements and methods. We show that electron driven beamlines are potentially feasible, but exploiting their full potential requires extensive improvement of the source parameters or innovative technological devices for their transport and capture.

  13. Laser-driven electron beamlines generated by coupling laser-plasma sources with conventional transport systems

    Science.gov (United States)

    Antici, P.; Bacci, A.; Benedetti, C.; Chiadroni, E.; Ferrario, M.; Rossi, A. R.; Lancia, L.; Migliorati, M.; Mostacci, A.; Palumbo, L.; Serafini, L.

    2012-08-01

    Laser-driven electron beamlines are receiving increasing interest from the particle accelerator community. In particular, the high initial energy, low emittance, and high beam current of the plasma based electron source potentially allow generating much more compact and bright particle accelerators than what conventional accelerator technology can achieve. Using laser-generated particles as injectors for generating beamlines could significantly reduce the size and cost of accelerator facilities. Unfortunately, several features of laser-based particle beams need still to be improved before considering them for particle beamlines and thus enable the use of plasma-driven accelerators for the multiple applications of traditional accelerators. Besides working on the plasma source itself, a promising approach to shape the laser-generated beams is coupling them with conventional accelerator elements in order to benefit from both a versatile electron source and a controllable beam. In this paper, we perform start-to-end simulations to generate laser-driven beamlines using conventional accelerator codes and methodologies. Starting with laser-generated electrons that can be obtained with established multi-hundred TW laser systems, we compare different options to capture and transport the beams. This is performed with the aim of providing beamlines suitable for potential applications, such as free electron lasers. In our approach, we have analyzed which parameters are critical at the source and from there evaluated different ways to overcome these issues using conventional accelerator elements and methods. We show that electron driven beamlines are potentially feasible, but exploiting their full potential requires extensive improvement of the source parameters or innovative technological devices for their transport and capture.

  14. National synchrotron light source user's manual: Guide to the VUV and x-ray beamlines: Third edition

    Energy Technology Data Exchange (ETDEWEB)

    Gmuer, N.F.; Thomlinson, W.; White-DePace, S.

    1989-01-01

    This report contains information on the following topics: A Word on the Writing of Beamline Descriptions; Beamline Equipment Utilization for General Users; the Vacuum Ultraviolet (VUV) Storage Ring and Beamlines; VUV Beamline Descriptions--An Explanation; VUV Beamline Descriptions; X-Ray Storage Ring and Beamlines; X-Ray Beamline Descriptions--An Explanation; and X-Ray Beamline Descriptions.

  15. XDS: a flexible beamline for X-ray diffraction and spectroscopy at the Brazilian synchrotron.

    Science.gov (United States)

    Lima, F A; Saleta, M E; Pagliuca, R J S; Eleotério, M A; Reis, R D; Fonseca Júnior, J; Meyer, B; Bittar, E M; Souza-Neto, N M; Granado, E

    2016-11-01

    The majority of the beamlines at the Brazilian Synchrotron Light Source Laboratory (LNLS) use radiation produced in the storage-ring bending magnets and are therefore currently limited in the flux that can be used in the harder part of the X-ray spectrum (above ∼10 keV). A 4 T superconducting multipolar wiggler (SCW) was recently installed at LNLS in order to improve the photon flux above 10 keV and fulfill the demands set by the materials science community. A new multi-purpose beamline was then installed at the LNLS using the SCW as a photon source. The XDS is a flexible beamline operating in the energy range between 5 and 30 keV, designed to perform experiments using absorption, diffraction and scattering techniques. Most of the work performed at the XDS beamline concentrates on X-ray absorption spectroscopy at energies above 18 keV and high-resolution diffraction experiments. More recently, new setups and photon-hungry experiments such as total X-ray scattering, X-ray diffraction under high pressures, resonant X-ray emission spectroscopy, among others, have started to become routine at XDS. Here, the XDS beamline characteristics, performance and a few new experimental possibilities are described.

  16. New beamline dedicated to solution scattering from biological macromolecules at the ESRF

    Energy Technology Data Exchange (ETDEWEB)

    Pernot, P; Theveneau, P; Giraud, T; Fernandes, R Nogueira; Nurizzo, D; Spruce, D; Surr, J; McSweeney, S [ESRF, BP 220, Grenoble (France); Round, A; Felisaz, F; Foedinger, L; Gobbo, A; Huet, J; Villard, C; Cipriani, F, E-mail: rejma@esrf.f, E-mail: around@embl.f [EMBL Grenoble, BP 181, Grenoble (France)

    2010-10-01

    The new bio-SAXS beamline (ID14-3 at the ESRF, Grenoble, France) is dedicated exclusively to small-angle scattering experiments of biological macromolecules in solution and has been in user operation since November 2008. Originally a protein crystallography beamline, ID14-3 was refurbished, still as a part of the ESRF Structural Biology group, with the main aim to provide a facility with 'quick and easy' access to satisfy rapidly growing demands from crystallographers, biochemists and structural biologists. The beamline allows manual and automatic sample loading/unloading, data collection, processing (conversion of a 2D image to a normalized 1D X-ray scattering profile) and analysis. The users obtain on-line standard data concerning the size (radius of gyration, maximum dimension and volume) and molecular weight of samples which allow on-the fly ab-inito shape reconstruction in order to provide feedback enabling the data collection strategies to be optimized. Automation of sample loading is incorporated on the beamline using a device constructed in collaboration between the EMBL (Grenoble and Hamburg outstations) and the ESRF. Semi/automated data analysis is implemented following the model of the SAXS facility at X33, EMBL Hamburg. This paper describes the bio-SAXS beamline and set-up characteristics together with the examples of user data obtained.

  17. Soil examination for a forensic trace evidence laboratory - Part 2: Elemental analysis.

    Science.gov (United States)

    Woods, Brenda; Paul Kirkbride, K; Lennard, Chris; Robertson, James

    2014-12-01

    Laser-induced breakdown spectroscopy (LIBS), X-ray fluorescence spectroscopy (XRF) and scanning electron microscopy/energy dispersive X-ray spectroscopy (SEM/EDX) are compared in terms of their discrimination power when applied to Australian soil specimens. SEM/EDX and XRF are frequently used in forensic laboratories for the elemental analysis of paint and glass, and for miscellaneous examinations. LIBS is an emerging technique for forensic applications, with a number of researchers promoting its use for the elemental profiling of glass fragments. In this study, 29 soil specimens were analysed, with 12 specimens coming from the Canberra area and the remaining 17 specimens from other sites around Australia. As very good discrimination results were obtained for each of the analytical methods, any of these elemental analysis techniques, available in a trace evidence laboratory, could be used as part of a wider examination protocol to differentiate soil specimens.

  18. Basic design of beamline and polarization control

    Institute of Scientific and Technical Information of China (English)

    2006-01-01

    The basic concept of synchrotron radiation beamlines for vacuum ultraviolet and X-ray experiments has been introduced to beginning users and designers of beamlines. The beamline defined here is composed of a front end,pre-mirrors, and a monochromator with refocusing mirrors, which are connected by beam pipes, providing monochromatic light for the experiments. Firstly, time characteristics of the synchrotron radiation are briefly reviewed.Secondly, the basic technology is introduced as the fundamental knowledge required to both users and designers. The topics are photoabsorption by air and solids, front ends and beam pipes, mirrors, monochromators, and filters. Thirdly,the design consideration is described mainly for the designers. The topics are design principle, principle of ray tracing,optical machinery and control, and vacuum. Fourthly, polarization control is considered. The topics are polarizers,polarization diagnosis of beamline, and circularly-polarized light generation. Finally, a brief summary is given introducing some references for further knowledge of the users and the designers.

  19. Beamline for schools beam line training day

    CERN Multimedia

    Photo Service, CERN

    2014-01-01

    The first two teams to participate in CERN's Beamline for Schools project spent their second day at CERN learning the basics of beam physics, and visiting their experimental setup at the T9 beam line in CERN's East Hall on the Meyrin site.

  20. Finite element analysis of steady and transiently moving/rolling nonlinear viscoelastic structure. Part 1: Theory

    Science.gov (United States)

    Padovan, Joe

    1986-01-01

    In a three part series of papers, a generalized finite element analysis scheme is developed to handle the steady and transient response of moving/rolling nonlinear viscoelastic structure. This paper considers the development of the moving/rolling element strategy, including the effects of large deformation kinematics and viscoelasticity modelled by fractional integro-differential operators. To improve the solution strategy, a special hierarchical constraint procedure is developed for the case of steady rolling/translating as well as a transient scheme involving the use of a Grunwaldian representation of the fractional operator. In the second and third parts of the paper, 3-D extensions are developed along with transient contact strategies enabling the handling of impacts with obstructions. Overall, the various developments are benchmarked via comprehensive 2- and 3-D simulations. These are correlated with experimental data to define modelling capabilities.

  1. National Synchrotron Light Source user`s manual: Guide to the VUV and x-ray beamlines. Fifth edition

    Energy Technology Data Exchange (ETDEWEB)

    Gmuer, N.F. [ed.

    1993-04-01

    The success of the National Synchrotron Light Source is based, in large part, on the size of the user community and the diversity of the scientific and technical disciplines represented by these users. As evidence of this success, the VUV Ring has just celebrated its 10th anniversary and the X-ray Ring will do the same in 1995. In order to enhance this success, the NSLS User`s Manual: Guide to the VUV and X-Ray Beamlines - Fifth Edition, is being published. This Manual presents to the scientific community-at-large the current and projected architecture, capabilities and research programs of the various VUV and X-ray beamlines. Also detailed is the research and computer equipment a General User can expect to find and use at each beamline when working at the NSLS. The Manual is updated periodically in order to keep pace with the constant changes on these beamlines.

  2. Elastic and Piezoelectric Properties of Boron Nitride Nanotube Composites. Part II; Finite Element Model

    Science.gov (United States)

    Kim, H. Alicia; Hardie, Robert; Yamakov, Vesselin; Park, Cheol

    2015-01-01

    This paper is the second part of a two-part series where the first part presents a molecular dynamics model of a single Boron Nitride Nanotube (BNNT) and this paper scales up to multiple BNNTs in a polymer matrix. This paper presents finite element (FE) models to investigate the effective elastic and piezoelectric properties of (BNNT) nanocomposites. The nanocomposites studied in this paper are thin films of polymer matrix with aligned co-planar BNNTs. The FE modelling approach provides a computationally efficient way to gain an understanding of the material properties. We examine several FE models to identify the most suitable models and investigate the effective properties with respect to the BNNT volume fraction and the number of nanotube walls. The FE models are constructed to represent aligned and randomly distributed BNNTs in a matrix of resin using 2D and 3D hollow and 3D filled cylinders. The homogenisation approach is employed to determine the overall elastic and piezoelectric constants for a range of volume fractions. These models are compared with an analytical model based on Mori-Tanaka formulation suitable for finite length cylindrical inclusions. The model applies to primarily single-wall BNNTs but is also extended to multi-wall BNNTs, for which preliminary results will be presented. Results from the Part 1 of this series can help to establish a constitutive relationship for input into the finite element model to enable the modeling of multiple BNNTs in a polymer matrix.

  3. 10 CFR Appendix O to Part 110 - Illustrative List of Fuel Element Fabrication Plant Equipment and Components Under NRC's Export...

    Science.gov (United States)

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Illustrative List of Fuel Element Fabrication Plant... Appendix O to Part 110—Illustrative List of Fuel Element Fabrication Plant Equipment and Components Under NRC's Export Licensing Authority Note: Nuclear fuel elements are manufactured from source or...

  4. Beamline Design and Instrumentation for the Imaging and Coherence Beamline I13L at the Diamond Light Source

    Science.gov (United States)

    Wagner, U. H.; Pešić, Z. D.; De Fanis, A.; Rau, C.

    2013-03-01

    I13L is a 250 m long hard x-ray beamline (6 keV to 35 keV) at the Diamond Light Source. The beamline comprises of two independent experimental endstations: one for imaging in direct space using x-ray microscopy and one for imaging in reciprocal space using coherent diffraction based imaging techniques. In this paper we will discuss the fundamental design concepts of the beamline and explain their implications for the civil engineering of the endstation building and the beamline instrumentation. For the latter this paper will focus on the beamline mirror systems and monochromators.

  5. Machining Deformation Prediction of Thin-Walled Part Based on Finite Element Analysis

    Institute of Scientific and Technical Information of China (English)

    Hongxiang Wang; Yabin Tang; Zhanshan Liu; Shi Gao

    2015-01-01

    For the problems of machining distortion and the low accepted product during milling process of aluminum alloy thin⁃walled part, this paper starts from the analysis of initial stress state in material preparation process, the change process of residual stress within aluminum alloy pre⁃stretching plate is researched, and the distribution law of residual stress is indirectly obtained by delamination measurement methods, so the effect of internal residual stress on machining distortion is considered before finite element simulation. Considering the coupling effects of residual stress, dynamic milling force and clamping force on machining distortion, a three⁃dimensional dynamic finite element simulation model is established, and the whole cutting process is simulated from the blank material to finished product, a novel prediction method is proposed, which can availably predict the machining distortion accurately. The machining distortion state of the thin⁃walled part is achieved at different processing steps, the machining distortion of the thin⁃walled part is detected with three coordinate measuring machine tools, show that the simulation results are in good agreement with experimental data.

  6. Optical design of the NSRL undulator beamline.

    Science.gov (United States)

    Zhang, Y W; Sheng, L S; Zhang, G B; Gao, H

    1998-05-01

    The optical design of the NSRL undulator beamline is presented. The NSRL undulator has 29 periods of 9.2 cm that produce a photon energy of 7.7-124 eV with the fundamental and third harmonics at a ring energy of 800 MeV. The beamline consists of a typical Kirkpatrick-Baez prefocusing mirror system, a modified spherical-grating monochromator (SGM) and a refocusing toroidal mirror. The monochromator has two including angles of 148 and 157 degrees with two plane mirrors inserted into the entrance arm in order to cover the wide energy range with high grating diffraction efficiency. Calculation shows that the resolving power of the monochromator can be greater than 5000 with the slits fully opened and 20000 with a 20 micro m opening of the slits. The spot at the sample is about 1.5 (H) mm x 0.5 (V) mm.

  7. Depolarization in the ILC Linac-to-Ring Positron Beamline

    CERN Document Server

    Riemann, Sabine

    2012-01-01

    To achieve the physics goals of future Linear Colliders, it is important that electron and positron beams are polarized. The positron source planned for the International Linear Collider (ILC) is based on a helical undulator system and can deliver a polarised beam with positron polarization of 60%. To ensure that no significant polarization is lost during the transport of the electron and positron beams from the source to the interaction region, spin tracking has to be included in all transport elements which can contribute to a loss of polarization. These are the positron source, the damping ring, the spin rotators, the main linac and the beam delivery system. In particular, the dynamics of the polarized positron beam is required to be investigated. The results of positron spin tracking and depolarization study at the Positron-Linac-To-Ring (PLTR) beamline are presented.

  8. Implementation of Bourbaki's Elements of Mathematics in Coq: Part Two, From Natural Numbers to Real Numbers

    OpenAIRE

    José Grimm

    2016-01-01

    International audience; This paper describes a formalization of the first book of the series ``Elements of Mathematics'' by Nicolas Bourbaki, using the Coq proof assistant. In a first paper published in this journal, we presented the axioms and basic constructions (corresponding to a part of the first two chapters of book I, theory of sets). We discuss here the set of integers (third chapter of book I, theory of set), the sets Z and Q (first chapter of book II, Algebra) and the set of real nu...

  9. EIS: the scattering beamline at FERMI.

    Science.gov (United States)

    Masciovecchio, Claudio; Battistoni, Andrea; Giangrisostomi, Erika; Bencivenga, Filippo; Principi, Emiliano; Mincigrucci, Riccardo; Cucini, Riccardo; Gessini, Alessandro; D'Amico, Francesco; Borghes, Roberto; Prica, Milan; Chenda, Valentina; Scarcia, Martin; Gaio, Giulio; Kurdi, Gabor; Demidovich, Alexander; Danailov, Miltcho B; Di Cicco, Andrea; Filipponi, Adriano; Gunnella, Roberto; Hatada, Keisuke; Mahne, Nicola; Raimondi, Lorenzo; Svetina, Cristian; Godnig, Roberto; Abrami, Alessandro; Zangrando, Marco

    2015-05-01

    The Elastic and Inelastic Scattering (EIS) beamline at the free-electron laser FERMI is presented. It consists of two separate end-stations: EIS-TIMEX, dedicated to ultrafast time-resolved studies of matter under extreme and metastable conditions, and EIS-TIMER, dedicated to time-resolved spectroscopy of mesoscopic dynamics in condensed matter. The scientific objectives are discussed and the instrument layout illustrated, together with the results from first exemplifying experiments.

  10. XAFS at the Pacific Northwest Consortium-Collaborative Access Team undulator beamline.

    Science.gov (United States)

    Heald, S; Stern, E; Brewe, D; Gordon, R; Crozier, D; Jiang, D; Cross, J

    2001-03-01

    The Pacific Northwest Consortium-Collaborative Access Team (PNC-CAT) has begun operating an insertion device beamline at the Advanced Photon Source. The beamline has been extensively used for XAFS studies. This paper summarizes its capabilities, and our initial operational experience. The beamline is based on APS undulator A, and incorporates full undulator scanning. The monochromator is liquid nitrogen cooled and has both Si(111) and Si(311) crystals in a side-by-side configuration. Crystal changes only take a few minutes. The crystals cover the energy range from 3-50 keV with fluxes as high as 2x10(13) ph/sec. Microbeams can be produced using Kirkpatrick-Baez mirrors (spot size 1-3 microm) or tapered capillaries (sub-microm spots). When these optics are combined with a 13-element Ge detector, the beamline provides powerful microbeam imaging and spectroscopy capabilities. Experimental examples from the environmental field and in-situ UHV film growth will be discussed.

  11. Parmelia sulcata lichen transplants positioning towards wind direction (Part I): precipitation volumes, total element deposition and lichen element content

    NARCIS (Netherlands)

    Marques, A.P.; Freitas, M.C.; Wolterbeek, H. Th.; Verburg, T.

    2009-01-01

    Parmelia sulcata transplants were used in three different exposure systems, focused on three different influxes: free influx, horizontal influx and vertical influx. The total element deposition and the precipitation volumes were found to be positively correlated for Fe and Ni only. The element conte

  12. Main formulations of the finite element method for the problems of structural mechanics. Part 3

    Directory of Open Access Journals (Sweden)

    Ignat’ev Aleksandr Vladimirovich

    2015-01-01

    Full Text Available In this paper the author offers is the classification of the formulae of Finite Element Method. This classification help to orient in a huge number of published articles, as well as those to be published, which are dedicated to the problem of enhancing the efficiency of the most commonly used method. The third part of the article considers the variation formulations of FEM and the energy principles lying in the basis of it. If compared to the direct method, which is applied only to finite elements of a simple geometrical type, the variation formulations of FEM are applicable to the elements of any type. All the variation methods can be conventionally divided into two groups. The methods of the first group are based on the principle of energy functional stationarity - a potential system energy, additional energy or on the basis of these energies, which means the full energy. The methods of the second group are based on the variants of mathematical methods of weighted residuals for solving the differential equations, which in some cases can be handled according to the principle of possible displacements or extreme energy principles. The most widely used and multipurpose is the approach based on the use of energy principles coming from the energy conservation law: principle of possible changes in stress state, principle of possible change in stress-strain state.

  13. Main formulations of the finite element method for the problems of structural mechanics. Part 2

    Directory of Open Access Journals (Sweden)

    Ignat’ev Aleksandr Vladimirovich

    Full Text Available The author offers a classification of Finite Element formulations, which allows orienting in a great number of the published and continuing to be published works on the problem of raising the efficiency of this widespread numerical method. The second part of the article offers examination of straight formulations of FEM in the form of displacement approach, area method and classical mixed-mode method. The question of solution convergence according to FEM in the form of classical mixed-mode method is considered on the example of single-input single-output system of a beam in case of finite element grid refinement. The author draws a conclusion, that extinction of algebraic equations system of FEM in case of passage to the limit is not a peculiar feature of this method in general, but manifests itself only in some particular cases. At the same time the obtained results prove that FEM in mixed-mode form provides obtaining more stable results in case of finite element grid refinement in comparison with FEM in the form of displacement approach. It is quite obvious that the same qualities will appear also in two-dimensional systems.

  14. A comparative study of the spectra recorded at RRCAT synchrotron BL-8 dispersive EXAFS beamline with other beamlines

    Indian Academy of Sciences (India)

    Abhijeet Gaur; B D Shrivastava; S N Jha; D Bhattacharyya; A Poswal

    2013-01-01

    The aim of the present work is to make a comparative study of the EXAFS spectra recorded at the BL-8 dispersive EXAFS beamline at 2 GeV Indus-2 synchrotron source at RRCAT, Indore (India) with those recorded at other synchrotron EXAFS beamlines, viz., X-19A at NSLS, BNL (USA), EXAFS wiggler beamline 4-1 at the SSRL (USA) and beamline 11.1 at ELETTRA (Italy). For this purpose, EXAFS spectra at Cu K-edge in copper metal have been recorded at these four beamlines. Further, EXAFS spectra at Cu K-edge in a copper complex have also been recorded at BL-8 beamline and beamline 11.1 at ELETTRA (Italy). The obtained experimental () data have been background-subtracted and then normalized. The normalized data have been then converted to () data, which have been Fourier-transformed and then fitted with the theoretical model, thereby yielding different structural parameters. It has been shown that the results obtained from the EXAFS spectra recorded at the BL-8 beamline are comparable with those obtained from other synchrotron EXAFS beamlines and also with the crystallographic results reported by earlier workers. The reliability, usefulness and data quality of the BL-8 beamline have been discussed.

  15. Finite element modeling of borehole heat exchanger systems. Part 1. Fundamentals

    Science.gov (United States)

    Diersch, H.-J. G.; Bauer, D.; Heidemann, W.; Rühaak, W.; Schätzl, P.

    2011-08-01

    Single borehole heat exchanger (BHE) and arrays of BHE are modeled by using the finite element method. The first part of the paper derives the fundamental equations for BHE systems and their finite element representations, where the thermal exchange between the borehole components is modeled via thermal transfer relations. For this purpose improved relationships for thermal resistances and capacities of BHE are introduced. Pipe-to-grout thermal transfer possesses multiple grout points for double U-shape and single U-shape BHE to attain a more accurate modeling. The numerical solution of the final 3D problems is performed via a widely non-sequential (essentially non-iterative) coupling strategy for the BHE and porous medium discretization. Four types of vertical BHE are supported: double U-shape (2U) pipe, single U-shape (1U) pipe, coaxial pipe with annular (CXA) and centred (CXC) inlet. Two computational strategies are used: (1) The analytical BHE method based on Eskilson and Claesson's (1988) solution, (2) numerical BHE method based on Al-Khoury et al.'s (2005) solution. The second part of the paper focusses on BHE meshing aspects, the validation of BHE solutions and practical applications for borehole thermal energy store systems.

  16. Vibration transmission through rolling element bearings. Part III: Geared rotor system studies

    Science.gov (United States)

    Lim, T. C.; Singh, R.

    1991-11-01

    This paper extends the proposed bearing matrix formulation of Parts I and II to analyze the overall dynamics of a geared rotor system which includes a spur gear pair, shafts, rolling element bearing, a prime mover and a load (attached to the geared rotor system through flexible torsional couplings), a rigid or flexible casing, and compliant or massive mounts. Linear time-invariant, discrete dynamic models of a generic geared rotor system with proportional viscous damping are developed, by using lumped parameter and dynamic finite element techniques, which are then used to predict the vibration transmissibility through bearings and mounts, casing vibration motion, and dynamic response of the internal rotating system. Each rotating shaft is modeled as an Euler beam in the lumped parameter model and as a Timoshenko beam in the dynamic finite element model, but the gyroscopic moment is not included. Eigensolution and forced harmonic response studies due to rotating mass unbalance or kinematic transmission error excitation for the following example cases are obtained by using the formulation, and the results are compared with those of simple models currently available in the literature and/or experiment: case I, a single-stage rotor system with flexibly mounted rigid casing consisting of two bearings as a special case of the geared rotor system; case II, a spur gear pair drive supported by four bearings installed in a flexibly mounted rigid casing; and case III, an experimental set-up consisting of a high-precision gear and pinion, and four identical rolling element bearings contained in a flexible casing mounted rigidly on a massive foundation. Analytical predictions show that the theory is indeed capable of predicting bearing and mount moment transmissibilities in addition to the force transmissibilities. Also, flexural vibrations of the casing plate are predicted well as the theory is in good agreement with measurements made on case III; such predictions are not

  17. Comparing the effect of low and high emittance on synchrotron radiation and beamline design

    Directory of Open Access Journals (Sweden)

    A Gholampour Azhir

    2017-08-01

    Full Text Available In this paper, we have discussed about the role of two emittance values suggested for Iranian Light Source Facility (ILSF (3.278 and 0.476 nm.rad on different radiation features of the synchrotron light sources (bending magnet, shaker and oscillator such as spot size, divergence of the beam on light spot, brilliance and important quantities in beamline design such as photon cross-section, optical element sizes and energy resolution  

  18. Macromolecular crystallography beamline X25 at the NSLS.

    Science.gov (United States)

    Héroux, Annie; Allaire, Marc; Buono, Richard; Cowan, Matthew L; Dvorak, Joseph; Flaks, Leon; Lamarra, Steven; Myers, Stuart F; Orville, Allen M; Robinson, Howard H; Roessler, Christian G; Schneider, Dieter K; Shea-McCarthy, Grace; Skinner, John M; Skinner, Michael; Soares, Alexei S; Sweet, Robert M; Berman, Lonny E

    2014-05-01

    Beamline X25 at the NSLS is one of the five beamlines dedicated to macromolecular crystallography operated by the Brookhaven National Laboratory Macromolecular Crystallography Research Resource group. This mini-gap insertion-device beamline has seen constant upgrades for the last seven years in order to achieve mini-beam capability down to 20 µm × 20 µm. All major components beginning with the radiation source, and continuing along the beamline and its experimental hutch, have changed to produce a state-of-the-art facility for the scientific community.

  19. X-ray absorption spectroscopy investigations on radioactive matter using MARS beamline at SOLEIL synchrotron

    Energy Technology Data Exchange (ETDEWEB)

    Llorens, Isabelle; Solari, Pier Lorenzo; Sitaud, Bruno [Synchrotron SOLEIL - l' Orme des Merisiers Saint Aubin, Gif-sur-Yvette (France); and others

    2014-07-01

    The MARS beamline at the SOLEIL synchrotron is dedicated to the characterization of radioactive material samples. One great advantage of the beamline is the possibility to characterize about 380 radionuclides by different X-ray techniques in the same place. This facility is unique in Europe. A wide energy range from around 3.5 keV to 36 keV K-edges from K to Cs, and L3 edges from Cd to Am and beyond can be used. The MARS beamline is optimized for X-ray absorption spectroscopy techniques (XANES/EXAFS), powder diffraction (XRD) but X-ray fluorescence (XRF) analysis, High Energy Resolution Fluorescence Detected-XAS (HERFD-XAS), X-ray Emission (XES) and μ-XAS/XRD are also possible. A description of the beamline as well as its performances are given in a first part. Then some scientific examples of XAS studies from users are presented which cover a wide variety of topics in radiochemistry and nuclear materials.

  20. Implementation of Bourbaki's Elements of Mathematics in Coq: Part Two, From Natural Numbers to Real Numbers

    Directory of Open Access Journals (Sweden)

    José Grimm

    2016-12-01

    Full Text Available This paper describes  a formalization of the first book of the series ``Elements  of Mathematics'' by Nicolas Bourbaki, using the Coq proof assistant. In a first paper published in this journal, we presented the axioms and basic constructions (corresponding to a part of the first two chapters of book I, theory of sets. We discuss here the set of integers (third chapter of  book I, theory of set, the sets Z and Q (first chapter of book II, Algebra and the set of real numbers (Chapter 4 of  book III, General topology. We start with a comparison of the Bourbaki  approach, the Coq standard library, and the Ssreflect library, then present our implementation.

  1. Superconducting axisymmetric finite elements based on a gauged potential variational principle. Part 1: Formulation

    Science.gov (United States)

    Schuler, James J.; Felippa, Carlos A.

    1994-01-01

    The present work is part of a research program for the numerical simulation of electromagnetic (EM) fields within conventional Ginzburg-Landau (GL) superconductors. The final goal of this research is to formulate, develop and validate finite element (FE) models that can accurately capture electromagnetic thermal and material phase changes in a superconductor. The formulations presented here are for a time-independent Ginzburg-Landau superconductor and are derived from a potential-based variational principle. We develop an appropriate variational formulation of time-independent supercontivity for the general three-dimensional case and specialize it to the one-dimensional case. Also developed are expressions for the material-dependent parameters alpha and beta of GL theory and their dependence upon the temperature T. The one-dimensional formulation is then discretized for finite element purposes and the first variation of these equations is obtained. The resultant Euler equations contain nonlinear terms in the primary variables. To solve these equations, an incremental-iterative solution method is used. Expressions for the internal force vector, external force vector, loading vector and tangent stiffness matrix are therefore developed for use with the solution procedure.

  2. SASE3: soft x-ray beamline at European XFEL

    Science.gov (United States)

    La Civita, Daniele; Gerasimova, Natalia; Sinn, Harald; Vannoni, Maurizio

    2014-09-01

    The European XFEL in Hamburg will be comprised of a linear accelerator and three Free-Electron-Laser beamlines (SASE1, SASE2 and SASE3) covering the energy range from 250 eV to 24 keV. It will provide up to 2700 pulses in trains of 600 microsecond duration at a repetition rate of 10 Hz. SASE3 beamline is the soft X-ray beamline (0.25 - 3 keV) and delivers photon pulses to SQS (Small Quantum System) and SCS (Spectroscopy & Coherent Scattering) experiments. The beamline is able to operate in both monochromatic and non-monochromatic mode. The latter provides the inherent FEL bandwidth at higher intensities. The beamline from photon source to experimental station is about 450 m long. The length of the beamline is related to the optics single-shotdamage issue. The almost diffraction-limited beam is propagated along the beamline with very long (up to 800 mm clear aperture), cooled (with eutectic bath) and super-polished (50 nrad RMS slope error and less than 3 nm PV residual height error) mirrors. The VLS-PG (variable line spacing - plane grating) monochromator covers the entire beamline energy range and its optical design is guided by the optimization of the energy resolving power, the minimization of the pulse broadening and the maximization of optics damage tolerance. Grating substrates are 530 mm long, eutectic cooled and present outstanding surface quality. The VLS parameters of the blazed profile are also a real challenge under manufacturing and measuring point of view. Adaptive optics in the horizontal (the second offset mirror) and vertical (monochromator premirror) plane are foreseen in the optical layout to increase the beamline tunability and to preserve the highly coherent beam properties. Beamline optical design, expected performance and also mechanical aspects of main beamline components are reported.

  3. Optical design and multi-length-scale scanning spectro-microscopy possibilities at the Nanoscopium beamline of Synchrotron Soleil.

    Science.gov (United States)

    Somogyi, Andrea; Medjoubi, Kadda; Baranton, Gil; Le Roux, Vincent; Ribbens, Marc; Polack, François; Philippot, Pascal; Samama, Jean Pierre

    2015-07-01

    The Nanoscopium 155 m-long beamline of Synchrotron Soleil is dedicated to scanning hard X-ray nanoprobe techniques. Nanoscopium aims to reach ≤100 nm resolution in the 5-20 keV energy range for routine user experiments. The beamline design tackles the tight stability requirements of such a scanning nanoprobe by creating an overfilled secondary source, implementing all horizontally reflecting main beamline optics, applying high mechanical stability equipment and constructing a dedicated high-stability building envelope. Multi-technique scanning imaging and tomography including X-ray fluorescence spectrometry and spectro-microscopy, absorption, differential phase and dark-field contrasts are implemented at the beamline in order to provide simultaneous information on the elemental distribution, speciation and sample morphology. This paper describes the optical concept and the first measured performance of the Nanoscopium beamline followed by the hierarchical length-scale multi-technique imaging experiments performed with dwell times down to 3 ms per pixel.

  4. Parmelia sulcata lichen transplants positioning towards wind direction (Part II): element concentrations and relationships with atmospheric element deposition

    NARCIS (Netherlands)

    Marques, A.P.; Freitas, M.C.; Wolterbeek, H.Th.; Verburg, T.

    2009-01-01

    Parmelia sulcata transplants were positioned in three different exposure systems allowing three different influxes: free influx (Fi), horizontal influx (Hi) and vertical influx (Vi). Results suggest the absence of any wind-directional effects on element accumulation within Fi and Hi systems, but und

  5. Diagnostics Beamline for the SRF Gun Project

    CERN Document Server

    Kamps, T; Goldammer, K; Krämer, Dietrich; Kuske, P; Kuszynski, J; Lipka, D; Marhauser, F; Quast, T; Richter, R

    2005-01-01

    A superconducting rf photo electron injector (SRF gun) is currently under construction by a collaboration between BESSY, DESY, FZR and MBI. The project aims at the design and setup of an CW SRF gun including a diagnostics beamline for the ELBE FEL and to address R&D issues on low emittance injectors for future light sources such as the BESSY FEL. Of critical importance for the injector performance is the control of the electron beam parameters. For this reason a compact diagnostics beamline is under development serving a multitude of operation settings ranging from low-charge (77pC), low-emittance (1 pi mm mrad) mode to high-charge (2.5nC) operation of the gun. For these operation modes beam dynamics simulations are resulting in boundary conditions for the beam instrumentation. Proven and mature technology is projected wherever possible, for example for current and beam position monitoring. The layout of the beam profile and emittance measurement systems is described. For the bunch length, which varies be...

  6. Beam Characterization at the KAERI UED Beamline

    CERN Document Server

    Setiniyaz, Sadiq; Baek, In-Hyung; Nam, Jinhee; Chae, MoonSik; Han, Byung-Heon; Gudkov, Boris; Jang, Kyu Ha; Park, Sunjeong; Miginsky, Sergey; Vinokurov, Nikolay; Jeong, Young Uk

    2016-01-01

    The UED (ultrafast electron diffraction) beamline of the KAERI's (the Korea Atomic Energy Research Institute's) WCI (World Class Institute) Center has been successfully commissioned. We have measured the beam emittance by using the quadrupole scan technique and the charge by using a novel measurement system we have developed. In the quadrupole scan, a larger drift distance between the quadrupole and the screen is preferred because it gives a better thin-lens approximation. A high bunch-charge beam, however, will undergo emittance growth in the long drift caused by the space-charge force. We present a method that mitigates this growth by introducing a quadrupole scan with a short drift and without using the thin-lens approximation. The quadrupole in this method is treated as a thick lens, and the emittance is extracted by using the thick-lens equations. Apart from being precise, our method can be readily applied without making any change to the beamline and has no need for a big drift space. For charge measure...

  7. Diagnostics Beamline for the SRF Gun Project

    Energy Technology Data Exchange (ETDEWEB)

    T. Kamps; V. Durr; K. Goldammer; D. Kramer; P. Kuske; J. Kuszynski; D. Lipka; F. Marhauser; T. Quast; D. Richter; U. Lehnert; P. Michel; J. Teichert; P. Evtushenko; I. Will

    2005-08-22

    A superconducting radio-frequency photo electron injector (SRF gun) is currently under construction by a collaboration of BESSY, DESY, FZR and MBI. The project aims at the design and setup of a CW SRF gun including a diagnostics beamline for the ELBE FEL and to address R&D issues on low emittance injectors for future light sources such as the BESSY FEL. Of critical importance for the injector performance is the control of the electron beam parameters. For this reason a compact diagnostics beamline is under development serving a multitude of operation settings ranging from low-charge (77pC), low-emittance (1 mm mrad) mode to high-charge (2.5nC) operation of the gun. For these operation modes beam dynamics simulations are resulting in boundary conditions for the beam instrumentation. Proven and mature technology is projected wherever possible, for example for current and beam position monitoring. The layout of the beam profile and emittance measurement systems is described. For the bunch length, which varies between 5 ps and 50 ps, two schemes using electro-optical sampling and Cherenkov radiation are detailed. The beam energy and energy spread is measured with a 180-degree spectrometer.

  8. A decade of user operation on the macromolecular crystallography MAD beamline ID14-4 at the ESRF

    Energy Technology Data Exchange (ETDEWEB)

    McCarthy, Andrew A., E-mail: andrewmc@embl.fr; Brockhauser, Sandor [European Molecular Biology Laboratory, 6 rue Jules Horowitz, BP 181, 38042 Grenoble (France); Unit of Virus Host Cell Interactions, UJF-EMBL-CNRS, UMI 3265, 6 rue Jules Horowitz, 38042 Grenoble Cedex 9 (France); Nurizzo, Didier; Theveneau, Pascal; Mairs, Trevor; Spruce, Darren; Guijarro, Matias; Lesourd, Marc [European Synchrotron Radiation Facility, 6 rue Jules Horowitz, BP 220, 38042 Grenoble (France); Ravelli, Raimond B. G. [European Molecular Biology Laboratory, 6 rue Jules Horowitz, BP 181, 38042 Grenoble (France); McSweeney, Sean [European Synchrotron Radiation Facility, 6 rue Jules Horowitz, BP 220, 38042 Grenoble (France)

    2009-11-01

    The improvement of the X-ray beam quality achieved on ID14-4 by the installation of new X-ray optical elements is described. ID14-4 at the ESRF is the first tunable undulator-based macromolecular crystallography beamline that can celebrate a decade of user service. During this time ID14-4 has not only been instrumental in the determination of the structures of biologically important molecules but has also contributed significantly to the development of various instruments, novel data collection schemes and pioneering radiation damage studies on biological samples. Here, the evolution of ID14-4 over the last decade is presented, and some of the major improvements that were carried out in order to maintain its status as one of the most productive macromolecular crystallography beamlines are highlighted. The experimental hutch has been upgraded to accommodate a high-precision diffractometer, a sample changer and a large CCD detector. More recently, the optical hutch has been refurbished in order to improve the X-ray beam quality on ID14-4 and to incorporate the most modern and robust optical elements used at other ESRF beamlines. These new optical elements will be described and their effect on beam stability discussed. These studies may be useful in the design, construction and maintenance of future X-ray beamlines for macromolecular crystallography and indeed other applications, such as those planned for the ESRF upgrade.

  9. G4beamline Particle Tracking in Matter Dominated Beam Lines

    Energy Technology Data Exchange (ETDEWEB)

    T.J. Roberts, K.B. Beard, S. Ahmed, D. Huang, D.M. Kaplan

    2011-03-01

    The G4beamline program is a useful and steadily improving tool to quickly and easily model beam lines and experimental equipment without user programming. It has both graphical and command-line user interfaces. Unlike most accelerator physics codes, it easily handles a wide range of materials and fields, being particularly well suited for the study of muon and neutrino facilities. As it is based on the Geant4 toolkit, G4beamline includes most of what is known about the interactions of particles with matter. We are continuing the development of G4beamline to facilitate its use by a larger set of beam line and accelerator developers. A major new feature is the calculation of space-charge effects. G4beamline is open source and freely available at http://g4beamline.muonsinc.com

  10. Design and analysis of a Be window for the APS diagnostics undulator beamline

    Energy Technology Data Exchange (ETDEWEB)

    Sheng, I.C.; Yang, B.X.; Sharma, S. [Argonne National Lab., IL (United States). Advanced Photon Source

    1997-06-01

    The design of a beryllium (Be) window for use under the extremely high heat load of an undulator beam is one of the challenges for third-generation synchrotron radiation beamlines. A novel design of a Be window is presented for the Advanced Photon Source (APS) diagnostics undulator beamline, whose beam has a peak power density of 150 W/mm{sup 2} (7 GeV/100 mA stored beam). The window has a double concave profile with a thickness of 0.5 mm at the center and is brazed to a water-cooled oxygen-free, high-conductivity (OFHC) copper manifold. Finite-element thermal analysis of the Be window is also presented.

  11. Part A - Advanced turbine systems. Part B - Materials/manufacturing element of the Advanced Turbine Systems Program

    Energy Technology Data Exchange (ETDEWEB)

    Karnitz, M.A.

    1996-06-01

    The DOE Offices of Fossil Energy and Energy Efficiency and Renewable Energy have initiated a program to develop advanced turbine systems for power generation. The objective of the Advanced Turbine Systems (ATS) Program is to develop ultra-high efficiency, environmentally superior, and cost competitive gas turbine systems for utility and industrial applications. One of the supporting elements of the ATS Program is the Materials/Manufacturing Technologies Task. The objective of this element is to address the critical materials and manufacturing issues for both industrial and utility gas turbines.

  12. Impact of Measuring Part Elements of Transformer Differential Protection on Input Signal Processing

    Directory of Open Access Journals (Sweden)

    Andreev M.V

    2017-08-01

    Full Text Available The electric power system (EPS is a large, multi-parameter, non-linear and dynamic system. The problem of calculation of relay protection (RP settings has become more urgent nowadays. The situation is exacerbated by the active implementation of renewable energy sources, FACTS, etc., which significantly change the “traditional” EPS and their operating modes. The problem can be solved by deep analysis of functioning of main elements of RP devices in the specific operating conditions and revision of coefficients used in settings calculation. That can be done using RPs detailed mathematical models and modern EPS simulators. The results of the analysis will make it possible to formulate a new methodology for setting up RP. That is a final goal. In the framework of solving this problem, the novel approach for developing RPs’ detailed mathematical models is formulated and theoretically proved. On the basis of this approach, mathematical models of the system “instrumental transformer - auxiliary transformer - analog filter” (measuring part of digital transformer differential protection for different types of auxiliary current transformers (active and passive and filters (Butterworth, Chebyshev, Bessel are developed. A comparative numerical analysis of their frequency and phase responses is carried out, including taking into account the magnetization of instrumental current transformers. Summarizing, the theoretical and practical studies presented in the article allows formulating requirements for RPs’ detailed mathematical models, which will be used in the further research.

  13. Element Partition Trees For H-Refined Meshes to Optimize Direct Solver Performance. Part I: Dynamic Programming

    KAUST Repository

    AbouEisha, Hassan M.

    2017-07-13

    We consider a class of two-and three-dimensional h-refined meshes generated by an adaptive finite element method. We introduce an element partition tree, which controls the execution of the multi-frontal solver algorithm over these refined grids. We propose and study algorithms with polynomial computational cost for the optimization of these element partition trees. The trees provide an ordering for the elimination of unknowns. The algorithms automatically optimize the element partition trees using extensions of dynamic programming. The construction of the trees by the dynamic programming approach is expensive. These generated trees cannot be used in practice, but rather utilized as a learning tool to propose fast heuristic algorithms. In this first part of our paper we focus on the dynamic programming approach, and draw a sketch of the heuristic algorithm. The second part will be devoted to a more detailed analysis of the heuristic algorithm extended for the case of hp-adaptive

  14. DEIMOS: A beamline dedicated to dichroism measurements in the 350–2500 eV energy range

    Energy Technology Data Exchange (ETDEWEB)

    Ohresser, P., E-mail: philippe.ohresser@synchrotron-soleil.fr; Otero, E.; Choueikani, F.; Chen, K.; Stanescu, S.; Deschamps, F.; Moreno, T.; Polack, F.; Lagarde, B.; Daguerre, J.-P.; Marteau, F. [Synchrotron SOLEIL, L’Orme des Merisiers, Saint-Aubin - BP 48, 91192 Gif-sur-Yvette (France); Scheurer, F.; Joly, L.; Muller, B. [Institut de Physique et Chimie des Matériaux de Strasbourg, UMR 7504 UdS-CNRS, 67034 Strasbourg Cedex 2 (France); Kappler, J.-P. [Synchrotron SOLEIL, L’Orme des Merisiers, Saint-Aubin - BP 48, 91192 Gif-sur-Yvette (France); Institut de Physique et Chimie des Matériaux de Strasbourg, UMR 7504 UdS-CNRS, 67034 Strasbourg Cedex 2 (France); Bunau, O.; Sainctavit, Ph. [Synchrotron SOLEIL, L’Orme des Merisiers, Saint-Aubin - BP 48, 91192 Gif-sur-Yvette (France); Institut de Minéralogie et de Physique des Milieux Condensés, CNRS UMR 7590, Université Pierre et Marie Curie, 75252 Paris Cedex 5 (France)

    2014-01-15

    The DEIMOS (Dichroism Experimental Installation for Magneto-Optical Spectroscopy) beamline was part of the second phase of the beamline development at French Synchrotron SOLEIL (Source Optimisée de Lumière à Energie Intermédiaire du LURE) and opened to users in March 2011. It delivers polarized soft x-rays to perform x-ray absorption spectroscopy, x-ray magnetic circular dichroism, and x-ray linear dichroism in the energy range 350–2500 eV. The beamline has been optimized for stability and reproducibility in terms of photon flux and photon energy. The main end-station consists in a cryo-magnet with 2 split coils providing a 7 T magnetic field along the beam or 2 T perpendicular to the beam with a controllable temperature on the sample from 370 K down to 1.5 K.

  15. MX: A beamline control system toolkit

    Science.gov (United States)

    Lavender, William M.

    2000-06-01

    The development of experimental and beamline control systems for two Collaborative Access Teams at the Advanced Photon Source has resulted in the creation of a portable data acquisition and control toolkit called MX. MX consists of a set of servers, application programs and libraries that enable the creation of command line and graphical user interface applications that may be easily retargeted to new and different kinds of motor and device controllers. The source code for MX is written in ANSI C and Tcl/Tk with interprocess communication via TCP/IP. MX is available for several versions of Unix, Windows 95/98/NT and DOS. It may be downloaded from the web site http://www.imca.aps.anl.gov/mx/.

  16. Elements redistribution between organic and mineral parts of microbial mats: SR-XRF research (Baikal Rift Zone)

    Energy Technology Data Exchange (ETDEWEB)

    Lazareva, E.V. [Institute of Geology and Mineralogy SB RAS, pr. Ac. Koptug, 3, 630090 Novosibirsk (Russian Federation)], E-mail: lazareva@uiggm.nsc.ru; Bryanskaya, A.V. [Institute of Cytology and Genetics SB RAS, 630090 Novosibirsk (Russian Federation); Zhmodik, S.M.; Kolmogorov, Y.P. [Institute of Geology and Mineralogy SB RAS, pr. Ac. Koptug, 3, 630090 Novosibirsk (Russian Federation); Pestunova, O.P. [Boreskov Institute of Catalysis SB RAS, Novosibirsk 630090 (Russian Federation); Barkhutova, D.D. [Institute of General and Experimental Biology SB RAS, Ulan-Ude (Russian Federation); Zolotarev, K.V.; Shaporenko, A.D. [Budker Institute of Nuclear Physics SB RAS, 630090 Novosibirsk (Russian Federation)

    2009-05-11

    In article minerals formation and elements accumulation in microbial mats of some hot springs of the Barguzin basin (Baikal Rift Zone) is discussed. The content of a wide spectrum of elements in microbial mats is studied by means of the method SR-XRF. Regularity of elements accumulation by community depending on geochemical features of hot spring's waters are discussed. These elements are distributed in different ways between organic and mineral substance of the microbial mats. The distribution of K, Mn, Ni, Cu, Zn, Fe is regular, Ca, Rb, Sr are almost totally related with the mats mineral part, while Ga, Ge and Br are accumulated in mats organic substance. Germanium element is concentrated in considerable amounts in the cyanobacterial communities, that develop in sulphideless springs with a higher radon concentration.

  17. A decade of user operation on the macromolecular crystallography MAD beamline ID14-4 at the ESRF.

    Science.gov (United States)

    McCarthy, Andrew A; Brockhauser, Sandor; Nurizzo, Didier; Theveneau, Pascal; Mairs, Trevor; Spruce, Darren; Guijarro, Matias; Lesourd, Marc; Ravelli, Raimond B G; McSweeney, Sean

    2009-11-01

    ID14-4 at the ESRF is the first tunable undulator-based macromolecular crystallography beamline that can celebrate a decade of user service. During this time ID14-4 has not only been instrumental in the determination of the structures of biologically important molecules but has also contributed significantly to the development of various instruments, novel data collection schemes and pioneering radiation damage studies on biological samples. Here, the evolution of ID14-4 over the last decade is presented, and some of the major improvements that were carried out in order to maintain its status as one of the most productive macromolecular crystallography beamlines are highlighted. The experimental hutch has been upgraded to accommodate a high-precision diffractometer, a sample changer and a large CCD detector. More recently, the optical hutch has been refurbished in order to improve the X-ray beam quality on ID14-4 and to incorporate the most modern and robust optical elements used at other ESRF beamlines. These new optical elements will be described and their effect on beam stability discussed. These studies may be useful in the design, construction and maintenance of future X-ray beamlines for macromolecular crystallography and indeed other applications, such as those planned for the ESRF upgrade.

  18. SEACAS Theory Manuals: Part III. Finite Element Analysis in Nonlinear Solid Mechanics

    Energy Technology Data Exchange (ETDEWEB)

    Laursen, T.A.; Attaway, S.W.; Zadoks, R.I.

    1999-03-01

    This report outlines the application of finite element methodology to large deformation solid mechanics problems, detailing also some of the key technological issues that effective finite element formulations must address. The presentation is organized into three major portions: first, a discussion of finite element discretization from the global point of view, emphasizing the relationship between a virtual work principle and the associated fully discrete system, second, a discussion of finite element technology, emphasizing the important theoretical and practical features associated with an individual finite element; and third, detailed description of specific elements that enjoy widespread use, providing some examples of the theoretical ideas already described. Descriptions of problem formulation in nonlinear solid mechanics, nonlinear continuum mechanics, and constitutive modeling are given in three companion reports.

  19. Design and performance of a new VIS–VUV photoluminescence beamline at UVSOR-III

    Energy Technology Data Exchange (ETDEWEB)

    Fukui, Kazutoshi, E-mail: fukui@fuee.u-fukui.ac.jp; Ikematsu, Ryu-ichi; Imoto, Yoshinori [University of Fukui, 3-9-1 Bunkyo, Fukui 910-8507 (Japan); Kitaura, Mamoru [Yamagata University, 1-4-12 Kojirakawamachi, Yamagata 990-8560 (Japan); Nakagawa, Kazumichi [Kobe University, 3-11 Tsurukabuto, Nada-ku, Kobe, Hyogo 657-8501 (Japan); Ejima, Takao [Tohoku University, 2-1-1 Katahira, Aoba-ku, Sendai, Miyagi 980-8577 (Japan); Nakamura, Eiken; Sakai, Masahiro; Hasumoto, Masami; Kimura, Shin-ichi [Institute for Molecular Science, 38 Nishigo-Naka, Myodaiji, Okazaki, Aichi 444-8585 (Japan)

    2014-01-28

    A new bending-magnet beamline with a 2.5 m normal-incidence monochromator mainly dedicated to photoluminescence measurements of solids has been constructed at the UVSOR-III. A new bending-magnet beamline with a 2.5 m normal-incidence monochromator has been constructed to serve with a light source in the visible–vacuum-ultraviolet region for photoluminescence, transmission and reflection spectroscopies of solids at the UVSOR-III 750 MeV synchrotron radiation light source. The aim is to pave the way to establishing a beamline with high photon flux, high brilliance, high energy-resolution, high linear-polarization and low higher-order light. To obtain high photon flux and brilliance, the acceptance angle of the bending-magnet radiation was designed to be 40 mrad (H) × 14 mrad (V) and the post-mirror system employed Kirkpatrick–Baez optics. The incidence angle of the incoming light to the optical elements, except to the gratings, was set to a grazing angle in order to keep a degree of linear polarization. For achieving high energy-resolution, an off-plane Eagle-type monochromator was adopted. Higher-order unwanted light in the energy range below ∼11 eV was suppressed to be less than 0.1%.

  20. D3, the new diffractometer for the macromolecular crystallography beamlines of the Swiss Light Source

    Energy Technology Data Exchange (ETDEWEB)

    Fuchs, Martin R., E-mail: mfuchs@bnl.gov [Paul Scherrer Institute, 5232 Villigen PSI (Switzerland); Brookhaven National Laboratory, Mail Stop 745, Upton, NY 11973 (United States); Pradervand, Claude; Thominet, Vincent; Schneider, Roman; Panepucci, Ezequiel; Grunder, Marcel; Gabadinho, Jose; Dworkowski, Florian S. N.; Tomizaki, Takashi; Schneider, Jörg; Mayer, Aline; Curtin, Adrian; Olieric, Vincent; Frommherz, Uli; Kotrle, Goran; Welte, Jörg; Wang, Xinyu; Maag, Stephan [Paul Scherrer Institute, 5232 Villigen PSI (Switzerland); Schulze-Briese, Clemens [DECTRIS Ltd, Neuenhoferstrasse 107, 5400 Baden (Switzerland); Wang, Meitian [Paul Scherrer Institute, 5232 Villigen PSI (Switzerland)

    2014-02-04

    A new diffractometer for microcrystallography has been developed for the three macromolecular crystallography beamlines of the Swiss Light Source. A new diffractometer for microcrystallography has been developed for the three macromolecular crystallography beamlines of the Swiss Light Source. Building upon and critically extending previous developments realised for the high-resolution endstations of the two undulator beamlines X06SA and X10SA, as well as the super-bend dipole beamline X06DA, the new diffractometer was designed to the following core design goals. (i) Redesign of the goniometer to a sub-micrometer peak-to-peak cylinder of confusion for the horizontal single axis. Crystal sizes down to at least 5 µm and advanced sample-rastering and scanning modes are supported. In addition, it can accommodate the new multi-axis goniometer PRIGo (Parallel Robotics Inspired Goniometer). (ii) A rapid-change beam-shaping element system with aperture sizes down to a minimum of 10 µm for microcrystallography measurements. (iii) Integration of the on-axis microspectrophotometer MS3 for microscopic sample imaging with 1 µm image resolution. Its multi-mode optical spectroscopy module is always online and supports in situ UV/Vis absorption, fluorescence and Raman spectroscopy. (iv) High stability of the sample environment by a mineral cast support construction and by close containment of the cryo-stream. Further features are the support for in situ crystallization plate screening and a minimal achievable detector distance of 120 mm for the Pilatus 6M, 2M and the macromolecular crystallography group’s planned future area detector Eiger 16M.

  1. A NEW STABILIZED FINITE ELEMENT METHOD FOR SOLVING THE STOKES AND NAVIER-STOKES EQUATIONS PART II. THE NONLINEAR CASE

    Institute of Scientific and Technical Information of China (English)

    DUAN Huoyuan; LIANG Guoping

    2001-01-01

    Following Part I., we study the stabilized finite element method for the incom pressible Navier-Stokes equations. It is shown that this new methodology is stable and has an optimal error estimates for all mesh Peclet number, allowing any combination of velocity and pressure interpolation.

  2. The Change of Austenitic Stainless Steel Elements Content in the Inner Parts of VVER-440 Reactor during Operation

    Science.gov (United States)

    Smutný, Vladimír; Hep, Jaroslav; Novosad, Petr

    2009-08-01

    Neutron activation induces the element transmutation in materials surrounding the reactor active core. The objective of the present paper is to calculate and evaluate the change of austenitic stainless steel 08Ch18N10T elements content through neutron induced activation, in inner parts of VVER-440 - in the baffle and in the barrel. Particularly the content changes of Mn in austenitic stainless steel. The neutron flux density and then the neutron activation of austenitic stainless steel elements in parts at the core are calculated. Neutron activation represents a measure of austenitic stainless steel elements transmutation. The power distribution is determined as an average value of several cycles power distribution in the middle of a cycle for the NPP Dukovany. The power distribution is calculated with the code MOBY-DICK [1]. The neutron flux density is calculated with the code TORT [2]. The neutron activation of austenitic stainless steel elements in the baffle and in the barrel is calculated with the system EASY-2007 containing the code FISPACT-2007 [3]. The calculation of the changing austenitic stainless steel elements content is performed depending on the moment of the supposed end of reactor operation - 40 years. There is also necessary monitoring and benchmarking of steel element content change, because the neutron flux calculation, particularly in thermal region, shows a considerable uncertainty, e.g. [4]. The motivation for this work is the study focused to stress corrosion cracking of austenitic stainless steels induced by radiation inside PWR and BWR, e.g. [5]. The paper could be a suggestion to estimation of austenitic stainless steel corrosion damage induced by neutrons in inner parts of VVER-440 reactor.

  3. Status of the crystallography beamlines at PETRA III

    Science.gov (United States)

    Burkhardt, Anja; Pakendorf, Tim; Reime, Bernd; Meyer, Jan; Fischer, Pontus; Stübe, Nicolas; Panneerselvam, Saravanan; Lorbeer, Olga; Stachnik, Karolina; Warmer, Martin; Rödig, Philip; Göries, Dennis; Meents, Alke

    2016-03-01

    Since 2013, three beamlines for macromolecular crystallography are available to users at the third-generation synchrotron PETRA III in Hamburg: P11, P13 and P14, the latter two operated by EMBL. Beamline P11 is operated by DESY and is equipped with a Pilatus 6M detector. Together with the photon flux of 2× 10^{13} ph/s provided by the very brilliant X-ray source of PETRA III, a full data set can be typically collected in less than 2min. P11 provides state-of-the-art microfocusing capabilities with beam sizes down to 1× 1 μ m2, which makes the beamline ideally suited for investigation of microcrystals and serial crystallography experiments. An automatic sample changer allows fast sample exchange in less than 20s, which enables high-throughput crystallography and fast crystal screening. For sample preparation, an S2 biosafety laboratory is available in close proximity to the beamline.

  4. Experimental stations at I13 beamline at Diamond Light Source

    Science.gov (United States)

    Pešić, Z. D.; De Fanis, A.; Wagner, U.; Rau, C.

    2013-03-01

    The I13 beamline of Diamond Light Source has been operational since December 2011. The beamline encompass two fully independent branches devoted to coherent imaging experiments (coherent x-ray diffraction, coherent diffraction imaging and ptychography) and x-ray imaging (in-line phase contrast imaging, tomography and full-field microscopy). This paper gives an overview of the current status of experimental stations on both branches and outlines planned developments.

  5. Circular dichroism beamline B23 at the Diamond Light Source.

    Science.gov (United States)

    Hussain, Rohanah; Jávorfi, Tamás; Siligardi, Giuliano

    2012-01-01

    Synchrotron radiation circular dichroism (SRCD) is a well established technique in structural biology. The first UV-VIS beamline, dedicated to circular dichroism, at Diamond Light Source Ltd, a third-generation synchrotron facility in south Oxfordshire, UK, has recently become operational and it is now available for the user community. Herein the main characteristics of the B23 SRCD beamline, the ancillary facilities available for users, and some of the recent advances achieved are summarized.

  6. A new Mtest beamline for the 1999 fixed target run

    Energy Technology Data Exchange (ETDEWEB)

    C. N. Brown and T. R. Kobilarcik

    2000-05-18

    The beamline cryogenic system for the Meson area will not be run for the 1999 fixed target run. The current MTest (MT) beamline relies on cryogenic magnets. A non-cryogenic solution is proposed which can yield up to 1 x 10{sup 6} pions per cycle at 120 GeV/c per 1 x 10{sup 11} incident protons at 800 GeV/c.

  7. Beamline for Schools 2016: How to be a CERN scientist

    CERN Multimedia

    2016-01-01

    Two teams of high-school students from the UK and Poland had the opportunity to conduct their own experiments at a fully equipped CERN beamline.   Students from the 2016 Beamline for Schools competition working on their experiment. (Image: Noemí Carabán Gonzalez/CERN) Two teams of high-school students from the UK and Poland had the opportunity to conduct their own experiments at a fully equipped CERN beamline, after winning the Beamline for Schools competition. The teams, ”Pyramid Hunters” from Poland and “Relatively Special” from the United Kingdom, spent 10 days at CERN conducting the experiments they had dreamt up in their winning proposals. The Beamline for Schools competition gives high-school students the chance to run an experiment on a fully equipped CERN beamline, in the same way researchers do at the Large Hadron Collider and other CERN facilities every day. To know more about their stay at CERN and the experiments they&r...

  8. Highlights from e-EPS: New milestone for ELI Beamlines facility

    CERN Multimedia

    Jorge Rivero González, e-EPS News

    2013-01-01

    e-EPS News is a monthly addition to the CERN Bulletin line-up, showcasing articles from e-EPS – the European Physical Society newsletter – as part of a collaboration between the two publications.   On 16 September 2013, the Extreme Light Infrastructure (ELI) Beamlines facility awarded a contract worth approximately €34.5m to Lawrence Livermore National Security LLC (LLNS, California, USA) to develop and deliver a state-of-the-art laser system that will be at the heart of the ELI Beamlines user facility. Located in the village of Dolní Břežany, Czech Republic, the ELI Beamlines facility aims to pioneer work in a number of research fields using ultra-high intensity lasers. The facility will host a cutting-edge research laser, around 100 times more powerful than any other laser in operation today. In particular, it will focus on providing users with ultra-short energetic particle beams (10 GeV) and radiation beams (up to a few MeV), produced by...

  9. Validation of Monte-Carlo simulations with measurements at the ICON beam-line at SINQ

    Energy Technology Data Exchange (ETDEWEB)

    Giller, L. [LRS, Physics Department, Ecole Polytechnique Federal de Lausanne, CH-1015 Lausanne (Switzerland); Filges, U. [LDM, NUM Department, Paul Scherrer Institut, CH-5232 Villigen PSI (Switzerland)], E-mail: uwe.filges@psi.ch; Kuehne, G. [ASQ, NUM Department, Paul Scherrer Institut, CH-5232 Villigen PSI (Switzerland); Wohlmuther, M. [ABE, GFA Department, Paul Scherrer Institut, CH-5232 Villigen PSI (Switzerland); Zanini, L. [ASQ, NUM Department, Paul Scherrer Institut, CH-5232 Villigen PSI (Switzerland)

    2008-02-11

    ICON is the new cold neutron imaging facility at the neutron spallation source SINQ. The ICON facility is placed at beam-line S52 with direct view to the cold liquid D{sub 2} moderator. The beam-line includes a 4.4 m long collimation section followed by a 11 m long flight path to the imaging system. The essential part of the collimation section is composed of six revolving drums and a variable aperture wheel. Depending on the investigated object, different apertures are used. Measurements have shown that each setup has a different spatial neutron flux distribution and specific beam profiles. Measured beam profiles have been used to validate results of simulations coupling the Monte-Carlo program MCNPX with the neutron ray-tracing program McStas. In a first step, MCNPX was used to calculate neutron spectra closed to the SINQ target, at the entrance of the collimation section. These results served as an input for McStas where the beam-line itself was simulated. In the present paper, experimental and theoretical results will be compared and discussed.

  10. Validation of Monte-Carlo simulations with measurements at the ICON beam-line at SINQ

    Science.gov (United States)

    Giller, L.; Filges, U.; Kühne, G.; Wohlmuther, M.; Zanini, L.

    2008-02-01

    ICON is the new cold neutron imaging facility at the neutron spallation source SINQ. The ICON facility is placed at beam-line S52 with direct view to the cold liquid D 2 moderator. The beam-line includes a 4.4 m long collimation section followed by a 11 m long flight path to the imaging system. The essential part of the collimation section is composed of six revolving drums and a variable aperture wheel. Depending on the investigated object, different apertures are used. Measurements have shown that each setup has a different spatial neutron flux distribution and specific beam profiles. Measured beam profiles have been used to validate results of simulations coupling the Monte-Carlo program MCNPX with the neutron ray-tracing program McStas. In a first step, MCNPX was used to calculate neutron spectra closed to the SINQ target, at the entrance of the collimation section. These results served as an input for McStas where the beam-line itself was simulated. In the present paper, experimental and theoretical results will be compared and discussed.

  11. Status of the LBNE Neutrino Beamline

    CERN Document Server

    Papadimitriou, Vaia

    2011-01-01

    The Long Baseline Neutrino Experiment (LBNE) will utilize a neutrino beamline facility located at Fermilab to carry out a compelling research program in neutrino physics. The facility will aim a beam of neutrinos toward a detector placed at the Homestake Mine in South Dakota. The neutrinos are produced in a three-step process. First, protons from the Main Injector (60-120 GeV) hit a solid target and produce mesons. Then, the charged mesons are focused by a set of focusing horns into the decay pipe, towards the far detector. Finally, the mesons that enter the decay pipe decay into neutrinos. The parameters of the facility were determined taking into account several factors including the physics goals, the Monte Carlo modeling of the facility, spacial and radiological constraints and the experience gained by operating the NuMI facility at Fermilab. The initial beam power is expected to be ~700 kW, however some of the parameters were chosen to be able to deal with a beam power of 2.3 MW. We discuss here the stat...

  12. From Beamline to Scanner with 225Ac

    Science.gov (United States)

    Robertson, Andrew K. H.; Ramogida, Caterina F.; Kunz, Peter; Rodriguez-Rodriguez, Cristina; Schaffer, Paul; Sossi, Vesna

    2016-09-01

    Due to the high linear energy transfer and short range of alpha-radiation, targeted radiation therapy using alpha-emitting pharmaceuticals that successfully target small disease clusters will kill target cells with limited harm to healthy tissue, potentially treating the most aggressive forms of cancer. As the parent of a decay chain with four alpha- and two beta-decays, 225Ac is a promising candidate for such a treatment. However, this requires retention of the entire decay chain at the target site, preventing the creation of freely circulating alpha-emitters that reduce therapeutic effect and increase toxicity to non-target tissues. Two major challenges to 225Ac pharmaceutical development exist: insufficient global supply, and the difficulty of preventing toxicity by retaining the entire decay chain at the target site. While TRIUMF works towards large-scale (C i amounts) production of 225Ac, we already use our Isotope Separation On-Line facility to provide small (overview of this research program and the journey of 225Ac from the beamline to the scanner. This research is funded by the Natural Sciences and Engineering Research Council of Canada.

  13. FLASH2: Operation, beamlines, and photon diagnostics

    Energy Technology Data Exchange (ETDEWEB)

    Plönjes, Elke, E-mail: elke.ploenjes@desy.de; Faatz, Bart; Kuhlmann, Marion; Treusch, Rolf [Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg (Germany)

    2016-07-27

    FLASH2, a major extension of the soft X-ray free-electron laser FLASH at DESY, turns FLASH into a multi-user FEL facility. A new undulator line is located in a separate accelerator tunnel and driven additionally by the FLASH linear accelerator. First lasing of FLASH2 was achieved in August 2014 with simultaneous user operation at FLASH1. The new FLASH2 experimental hall offers space for up to six experimental end stations, some of which will be installed permanently. The wide wavelength range spans from 4-60 nm and 0.8 nm in the 5{sup th} harmonic and in the future deep into the water window in the fundamental. While this is of high interest to users, it is challenging from the beamline instrumentation point of view. Online diagnostics - which are mostly pulse resolved - for beam intensity, position, wavelength, wave front, and pulse length have been to a large extent developed at FLASH(1) and have now been optimized for FLASH2. Pump-probe facilities for XUV-XUV, XUV optical and XUV-THz experiments will complete the FLASH2 user facility.

  14. Design of the LBNF Beamline Target Station

    Energy Technology Data Exchange (ETDEWEB)

    Tariq, S. [Fermilab; Ammigan, K. [Fermilab; Anderson, K.; ; Buccellato, S. A. [Fermilab; Crowley, C. F. [Fermilab; Hartsell, B. D. [Fermilab; Hurh, P. [Fermilab; Hylen, J. [Fermilab; Kasper, P. [Fermilab; Krafczyk, G. E. [Fermilab; Lee, A. [Fermilab; Lundberg, B. [Fermilab; Reitzner, S. D. [Fermilab; Sidorov, V. [Fermilab; Stefanik, A. M. [Fermilab; Tropin, I. S. [Fermilab; Vaziri, K. [Fermilab; Williams, K. [Fermilab; Zwaska, R. M. [Fermilab; Densham, C. [RAL, Didcot

    2016-10-01

    The Long Baseline Neutrino Facility (LBNF) project will build a beamline located at Fermilab to create and aim an intense neutrino beam of appropriate energy range toward the DUNE detectors at the SURF facility in Lead, South Dakota. Neutrino production starts in the Target Station, which consists of a solid target, magnetic focusing horns, and the associated sub-systems and shielding infrastructure. Protons hit the target producing mesons which are then focused by the horns into a helium-filled decay pipe where they decay into muons and neutrinos. The target and horns are encased in actively cooled steel and concrete shielding in a chamber called the target chase. The reference design chase is filled with air, but nitrogen and helium are being evaluated as alternatives. A replaceable beam window separates the decay pipe from the target chase. The facility is designed for initial operation at 1.2 MW, with the ability to upgrade to 2.4 MW, and is taking advantage of the experience gained by operating Fermilab’s NuMI facility. We discuss here the design status, associated challenges, and ongoing R&D and physics-driven component optimization of the Target Station.

  15. Synchrotron total reflection X-ray fluorescence at BL-16 microfocus beamline of Indus-2

    Science.gov (United States)

    Tiwari, M. K.; Singh, A. K.; Das, Gangadhar; Chowdhury, Anupam; Lodha, G. S.

    2014-04-01

    Determination of ultra trace elements is important in many disciplines both in basic and applied sciences. Numerous applications show their importance in medical science, environmental science, materials science, food processing and semiconductor industries and in maintaining the quality control of ultra pure chemicals and reagents. We report commissioning of a synchrotron based total reflection x-ray fluorescence (TXRF) facility on the BL-16 microfocus beamline of Indus-2. This paper describes the performance of the BL-16 TXRF spectrometer and the detailed description of its capabilities through examples of measured results.

  16. Release of Inorganic Elements during Wood Combustion. Release to the Gas Phase of Inorganic Elements during: Wood Combustion. Part 1: Development and Evaluation of Quantification Methods

    DEFF Research Database (Denmark)

    van Lith, Simone Cornelia; Alonso-Ramírez, Violeta; Jensen, Peter Arendt

    2006-01-01

    During wood combustion, inorganic elements such as alkali metals, sulfur, chlorine, and some heavy metals are partly released to the gas phase, which may cause problems in combustion facilities because of deposit formation and corrosion. Furthermore, it may cause harmful emissions of gases......) in this reactor, whereas methods B and C involved initial pyrolysis and combustion, respectively, of a large fuel sample (~5 kg) in a bench-scale fixed-bed reactor at 500 C. The methods were evaluated by comparing the data on the release of Cl, S, K, Na, Zn, and Pb from fiber board obtained by the three methods...

  17. Students on the Beamline: classroom, research, and discovery

    Science.gov (United States)

    Patry, J.; Walker, T.

    2012-12-01

    High level research is mainly the focus of trained scientists who possess a science specific background. The Canadian Light Source outreach service has developed a two stage research immersion approach which brings together students, teachers, and renowned scientists: Students on the Beamline. The first stage offers a training session for teachers to develop their professional competencies in regards to authentic science research and the synchrotron facility. During the second stage, students from classrooms apply a research protocol of their own design with the help of their teacher and synchrotron scientists. During this presentation, we will first explain the professional approach of the training. In the second part, two experiments designed by students will be presented which are geophysically based so to speak: Study of the Meteoritic Melt Sheet of the Manicouagan Basin and Effects of Olivine on the capture of NOx. Results have shown that teachers bring in the classroom a more authentic and new experience in research application. As for the students, their unique research has contributed to the increase of our knowledge and a better understanding of the scientific inquiry process.Scientist and teacher working together on the synchrotron

  18. Test design description Volume 2, Part 1. IFR-1 metal fuel irradiation test (AK-181) element as-built data

    Energy Technology Data Exchange (ETDEWEB)

    Dodds, N. E.

    1986-06-01

    The IFR-1 Test, designated as the AK-181 Test Assembly, will be the first irradiation test of wire wrapped, sodium-bonded metallic fuel elements in the Fast Flux Test Facility (FFTF). The test is part of the Integral Fast Reactor (IFR) fuels program conducted by Argonne National Laboratory (ANL) in support of the Innovative Reactor Concepts Program sponsored by the US Department of Energy (DOE). One subassembly, containing 169 fuel elements, will be irradiated for 600 full power days to achieve 10 at.% burnup. Three metal fuel alloys (U-10Zr, U-8Pu-10Zr) will be irradiated in D9 cladding tubes. The metal fuel elements have a fuel-smeared density of 75% and each contains five slugs. The enriched zone contains three slugs and is 36-in. long. One 6.5-in. long depleted uranium axial blanket slug (DU-10Zr) was loaded at each end of the enriched zone. the fuel elements were fabricated at ANL-W and delivered to Westinghouse-Hanford for wirewrapping and assembly into the test article. This Test Design Description contains relevant data on compositions, densities, dimensions and weights for the cast fuel slugs and completed fuel elements. The elements conform to the requirements in MG-22, "Users` Guide for the Irradiation of Experiments in the FTR."

  19. A new experiment station on beamline 4B7A at Beijing Synchrotron Radiation Facility

    Energy Technology Data Exchange (ETDEWEB)

    Zheng, L., E-mail: zhenglei@ihep.ac.cn; Zhao, Y.D.; Tang, K.; Ma, C.Y.; Hong, C.H.; Han, Y.; Cui, M.Q.; Guo, Z.Y.

    2014-11-01

    A new experiment station was installed on beamline 4B7A at Beijing Synchrotron Radiation Facility (BSRF), making it possible to record X-ray absorption fine structure (XAFS) spectrum in three modes over an energy range from 1750 eV to 6000 eV. A 13-element Si(Li) array detector and a single-element SDD detector were used to acquire data in partial fluorescence yield (PFY) mode. Two low-pressure noble gas ion chambers were adopted for measuring XAFS in transmission mode. In total electron yield (TEY) mode the current of sample is recorded. Solid, wet and liquid samples were suitable for this experimental station. Some representative results obtained from this station were shown and discussed. - Highlights: • A new experiment station was installed on beamline 4B7A at BSRF. • This experiment station has three modes for recording X-ray XAFS spectrum. • The energy region covers the K-edge of elements Si, P, S, Cl, K, Ca and Ti. • Solid, wet and liquid samples can be measured in this experiment station.

  20. Diamond beamline I07: a beamline for surface and interface diffraction.

    Science.gov (United States)

    Nicklin, Chris; Arnold, Tom; Rawle, Jonathan; Warne, Adam

    2016-09-01

    Beamline I07 at Diamond Light Source is dedicated to the study of the structure of surfaces and interfaces for a wide range of sample types, from soft matter to ultrahigh vacuum. The beamline operates in the energy range 8-30 keV and has two endstations. The first houses a 2+3 diffractometer, which acts as a versatile platform for grazing-incidence techniques including surface X-ray diffraction, grazing-incidence small- (and wide-) angle X-ray scattering, X-ray reflectivity and grazing-incidence X-ray diffraction. A method for deflecting the X-rays (a double-crystal deflector) has been designed and incorporated into this endstation, extending the surfaces that can be studied to include structures formed on liquid surfaces or at liquid-liquid interfaces. The second experimental hutch contains a similar diffractometer with a large environmental chamber mounted on it, dedicated to in situ ultrahigh-vacuum studies. It houses a range of complementary surface science equipment including a scanning tunnelling microscope, low-energy electron diffraction and X-ray photoelectron spectroscopy ensuring that correlations between the different techniques can be performed on the same sample, in the same chamber. This endstation allows accurate determination of well ordered structures, measurement of growth behaviour during molecular beam epitaxy and has also been used to measure coherent X-ray diffraction from nanoparticles during alloying.

  1. A study on radiation shielding and safety analysis for a synchrotron radiation beamline

    Energy Technology Data Exchange (ETDEWEB)

    Asano, Yoshihiro [Japan Atomic Energy Research Inst., Kansai Research Establishment, Synchrotron Radiation Research Center, Mikazuhi, Hyogo (Japan)

    2001-03-01

    Methods of shielding design and safety analysis are presented for a beam-line of synchrotron radiation. This paper consists of the shielding and safety study of synchrotron radiation with extremely intense and low energy photon below several hundreds keV, and the study for the behavior of remarkable high-energy photons up to 8 GeV, which can creep into beam-lines. A new shielding design code, STAC8 was developed to estimate the leakage dose outside the beam line hutch (an enclosure of the beam, optical elements or experimental instruments) easily and quickly with satisfactory accuracy. The code can calculate consistently from sources of synchrotron radiation to dose equivalent outside hutches with considering the build up effect and polarization effect. Validity of the code was verified by comparing its calculations with those of Monte Carlo simulations and measurement results of the doses inside the hutch of the BL14C of Photon Factory in the High Energy Accelerator Research Organization (KEK), showing good agreements. The shielding design calculations using STAC8 were carried out to apply to the practical beam-lines with the considering polarization effect and clarified the characteristics of the typical beam-line of the third generation synchrotron radiation facility, SPring-8. In addition, the shielding calculations were compared with the measurement outside the shield wall of the bending magnet beam-line of SPring-8, and showed fairly good agreement. The new shielding problems, which have usually been neglected in shielding designs for existing synchrotron radiation facilities, are clarified through the analysis of the beam-line shielding of SPring-8. The synchrotron radiation from the SPring-8 has such extremely high-intensity involving high energy photons that the scattered synchrotron radiation from the concrete floor of the hutch, the ground shine, causes a seriously high dose. The method of effective shielding is presented. For the estimation of the gas

  2. 33 CFR Appendix C to Part 155 - Training Elements for Oil Spill Response Plans

    Science.gov (United States)

    2010-07-01

    ... delivered to the various personnel. Further, this section of the plan must work in harmony with those sections of the plan dealing with exercises, the spill management team, and the qualified individual. 1... plan, it is necessary for the plan to convey the elements that define the program as appropriate....

  3. 33 CFR Appendix D to Part 154 - Training Elements for Oil Spill Response Plans

    Science.gov (United States)

    2010-07-01

    .... Further, this section of the plan must work in harmony with those sections of the plan dealing with exercises, the spill management team, and the qualified individual. 1.3The material in this appendix D is... the elements that define the program as appropriate. 2.2An effective spill response training...

  4. Local buckling of aluminium structures exposed to fire. Part 2: Finite element models

    NARCIS (Netherlands)

    Maljaars, J.; Soetens, F.

    2009-01-01

    A test series was carried out and reported in a corresponding paper on slender aluminium alloy sections, loaded in compression at elevated temperature. This paper gives the results of simulations of these tests with a finite element model. For this purpose, a novel constitutive model for fire expose

  5. Multi-element concentrations in plant parts and fluids of Malaysian nickel hyperaccumulator plants and some economic and ecological considerations.

    Science.gov (United States)

    van der Ent, Antony; Mulligan, David

    2015-04-01

    Information about multi-elemental concentrations in different plant parts of tropical Ni hyperaccumulator species has the potential to provide insight into their unusual metabolism relative to a range of essential and non-essential elements, but this information is scant in the literature. As Ni hyperaccumulation, and possibly co-accumulation of other toxic elements, has been hypothesized to provide herbivore (insect) protection, there is a need to quantify a range of these elements in plant tissues and transport fluids to at least verify the possibility of this explanation. In this study, multiple elements were analyzed in a range of different plant parts and transport fluids from Ni hyperaccumulator species collected from Sabah (Malaysia). The results show preferential accumulation of Ni in leaves over woody parts, but the highest concentrations were found in the phloem tissue (up to 7.9 % in Rinorea bengalensis) and phloem sap (up to 16.9 % in Phyllanthus balgooyi), visible by a bright green coloration in the field fresh material. The amount of Ni contained in one mature R. bengalensis tree was calculated at 4.77 kg. The high Ni concentration in the flowers of Phyllanthus securinegoides could affect insect floral visitors and pollination. High concentrations of Ni in the seeds of this species also could supply the seedling with Ni and aid in herbivory protection during the first stages of development. Foliar Ca and Ni in P. cf. securinegoides and R. bengalensis are positively correlated. Low accumulation of Ca is desirable for phytomining but concentrations of Ca are high in most Ni hyperaccumulators examined, and this could have consequences for the economic viability of Ni extraction from bio ore if these species were to be used as 'metal crops'.

  6. Finite Element Analysis of the Effect on Edge Distance of the Tensile Bearing Capacity of Embedded Hanging Parts

    OpenAIRE

    Meng Xian Hong; Liu Wei

    2016-01-01

    In order to explore the trend of tensile bearing capacity of embedded hanging parts when change the edge distance. Based on the finite element analysis software ABAQUS, the four simulation model was established. The buried depth and strength of concrete remain unchanged, but the edge distance was gradient change. By the load - displacement curve of every model known, the greater the edge distance, the greater the bearing capacity. When the edge distance reaches 1.5 times buried depth, the eff...

  7. Upgrading design of the 3B1A beamline for x-ray nanometre lithography of microelectronic devices at BSRF

    Institute of Scientific and Technical Information of China (English)

    Yi Fu-Ting; Ye Tian-Chun; Peng Liang-Qiang; Chen Da-Peng; Zhang Ju-Fang; Han Yong

    2004-01-01

    Beijing Synchrotron Radiation Facility is a partly dedicated synchrotron radiation source operated in either parasitic or dedicated mode. The 3B1A beamline, extracted from a bending magnet, was originally designed as a soft x-ray beamline for submicro x-ray lithography with critical lateral size just below 1μm in 1988 and no change has been made since it was built. But later the required resolution of x-ray lithography has changed from sub-micrometre to the nanometre in the critical lateral size. This beamline can longer more meet the requirement for x-ray nano lithography and has to be modified to fit the purpose. To upgrade the design of the 3B1A beamline for x-ray nano lithography, a mirror is used to reflect and scan the x-ray beam for the nano lithography station, but the mirror's grazing angle is changed to 27.9mrad in the vertical direction, and the convex curve needs to be modified to fit the change; the tiny change of mirror scanning angle is firstly considered to improve the uniformity of the x-ray spot on the wafer by controlling the convex curve.

  8. Performance of synchrotron X-ray monochromators under heat load Part 1 finite element modeling

    CERN Document Server

    Zhang, L; Migliore, J S; Mocella, V; Ferrero, C; Freund, A K

    2001-01-01

    In this paper we present the details of the finite element modeling (FEM) procedure used to calculate the thermal deformation generated by the X-ray power absorbed in silicon crystals. Different parameters were varied systematically such as the beam footprint on the crystal, the reflection order and the white beam slit settings. Moreover, the influence of various cooling parameters such as the cooling coefficient and the temperature of the coolant were studied. The finite element meshing was carefully optimized to generate a deformation output that could be easily read by a diffraction simulation code. Comparison with the experiments shows that the peak-to-valley slope error calculated by the FEM is an excellent approximation of the rocking curve width for a liquid nitrogen cooled silicon (3 3 3) crystal, and a quite good approximation for significantly deformed silicon (1 1 1) crystals.

  9. MP Salsa: a finite element computer program for reacting flow problems. Part 1--theoretical development

    Energy Technology Data Exchange (ETDEWEB)

    Shadid, J.N.; Moffat, H.K.; Hutchinson, S.A.; Hennigan, G.L.; Devine, K.D.; Salinger, A.G.

    1996-05-01

    The theoretical background for the finite element computer program, MPSalsa, is presented in detail. MPSalsa is designed to solve laminar, low Mach number, two- or three-dimensional incompressible and variable density reacting fluid flows on massively parallel computers, using a Petrov-Galerkin finite element formulation. The code has the capability to solve coupled fluid flow, heat transport, multicomponent species transport, and finite-rate chemical reactions, and to solver coupled multiple Poisson or advection-diffusion- reaction equations. The program employs the CHEMKIN library to provide a rigorous treatment of multicomponent ideal gas kinetics and transport. Chemical reactions occurring in the gas phase and on surfaces are treated by calls to CHEMKIN and SURFACE CHEMKIN, respectively. The code employs unstructured meshes, using the EXODUS II finite element data base suite of programs for its input and output files. MPSalsa solves both transient and steady flows by using fully implicit time integration, an inexact Newton method and iterative solvers based on preconditioned Krylov methods as implemented in the Aztec solver library.

  10. Positron separators in Superomega muon beamline at J-PARC

    Energy Technology Data Exchange (ETDEWEB)

    Ikedo, Y., E-mail: ikedo@post.kek.jp [Institute of Materials and Structure Science, High Energy Accelerator Research Organization, Tokai Campus, 230-1 Shirakata, Tokai, Ibaraki 319-1106 (Japan); Japan Proton Accelerator Research Complex, 2-4 Shirakata-Shirane, Tokai, Ibaraki 319-1195 (Japan); Miyake, Y.; Shimomura, K.; Strasser, P.; Kawamura, N.; Nishiyama, K.; Makimura, S.; Fujimori, H.; Koda, A.; Nakamura, J.; Nagatomo, T.; Kobayashi, Y. [Institute of Materials and Structure Science, High Energy Accelerator Research Organization, Tokai Campus, 230-1 Shirakata, Tokai, Ibaraki 319-1106 (Japan); Japan Proton Accelerator Research Complex, 2-4 Shirakata-Shirane, Tokai, Ibaraki 319-1195 (Japan); Adachi, T. [Faculty of Science, University of Tokyo, 7-3-1 Hongo, Bunkyo, Tokyo 113-0501 (Japan); Pant, A.D. [Interdisciplinary Graduate School of Medicine and Engineering, Yamanashi University, 4-3-11 Takeda, Kofu 400-8511 (Japan); Ogitsu, T.; Nakamoto, T.; Sasaki, K.; Ohata, H.; Okada, R.; Yamamoto, A. [Cryogenics Science Center, High Energy Accelerator Research Organization (KEK), 1-1 Oho, Tsukuba, Ibaraki 305-0501 (Japan); Japan Proton Accelerator Research Complex, 2-4 Shirakata-Shirane, Tokai, Ibaraki 319-1195 (Japan); and others

    2013-12-15

    Highlights: • Three stage positron separators was installed onto the U-line in the MLF/J-PARC. • The separators can be applied 400 kV to the both electrodes. • The separators were tested and were confirmed to successfully eliminate the positrons from the beam. -- Abstract: A positron separator is one of the essential components of a muon beamline to eliminate contamination in the beam, mainly positrons that have the same momentum as muons and are transported together with the beam. In order to eliminate positrons efficiently, we selected a Wien filter type three-stage positron separator for the new muon beamline, called Superomega, that is under construction in the Materials and Life Science Experimental Facility (MLF) of the Japan Accelerator Research Complex (J-PARC). The Superomega muon beamline is the second muon beamline at MLF/J-PARC, and started operation in October of 2012. Here, we report on the features and the test results of the positron separators installed in the Superomega muon beamline.

  11. The SLS Beamlines Data Acquisition and Control System

    CERN Document Server

    Krempasky, J; Vermeulen, D; Maden, D; Korhonen, T T; Portmann, W; Hunt, S; Abela, R; Muntwiler, M

    2001-01-01

    On December 15th the Swiss Light Source (SLS) produced a stored beam for the first time. This important milestone was achieved in a very tight time schedule. The fact that all major systems are controlled by Epics made this challenge feasible. In the first phase there are four beamlines: two for the surface science community, one for powder and surface diffraction and computed micro-tomography, and the last one for protein crystallography. All of them are equipped with insertion devices, which users want to treat as active sub-systems like a monochromator or experimental station. The beamline control systems are based on the same hardware and software technology as is the machine. This implies extensive use of Personal Computers running Linux RedHat 6.2 and VME systems (PowerPC). The advantage of this choice is a staightforward implementation of the insertion devices into the beamline and experiment framework. Although the experiment Application Program Interfaces differ from beamline to beamline, the standar...

  12. Optics Concept for a Pair of Undulator Beamlines for MX.

    Science.gov (United States)

    Berman, L E; Allaire, M; Chance, M R; Hendrickson, W A; Héroux, A; Jakoncic, J; Liu, Q; Orville, A M; Robinson, H H; Schneider, D K; Shi, W; Soares, A S; Stojanoff, V; Stoner-Ma, D; Sweet, R M

    2011-09-01

    We describe a concept for x-ray optics to feed a pair of macromolecular crystallography (MX) beamlines which view canted undulator radiation sources in the same storage ring straight section. It can be deployed at NSLS-II and at other low-emittance third-generation synchrotron radiation sources where canted undulators are permitted, and makes the most of these sources and beamline floor space, even when the horizontal angle between the two canted undulator emissions is as little as 1-2 mrad. The concept adopts the beam-separation principles employed at the 23-ID (GM/CA-CAT) beamlines at the Advanced Photon Source (APS), wherein tandem horizontally-deflecting mirrors separate one undulator beam from the other, following monochromatization by a double-crystal monochromator. The scheme described here would, in contrast, deliver the two tunable monochromatic undulator beams to separate endstations that address rather different and somewhat complementary purposes, with further beam conditioning imposed as required. A downstream microfocusing beamline would employ dual-stage focusing for work at the micron scale and, unique to this design, switch to single stage focusing for larger beams. On the other hand, the upstream, more highly automated beamline would only employ single stage focusing.

  13. Optics Concept for a Pair of Undulator Beamlines for MX*

    Science.gov (United States)

    Berman, L.E.; Allaire, M.; Chance, M.R.; Hendrickson, W.A.; Héroux, A.; Jakoncic, J.; Liu, Q.; Orville, A.M.; Robinson, H.H.; Schneider, D.K.; Shi, W.; Soares, A.S.; Stojanoff, V.; Stoner-Ma, D.; Sweet, R.M.

    2011-01-01

    We describe a concept for x-ray optics to feed a pair of macromolecular crystallography (MX) beamlines which view canted undulator radiation sources in the same storage ring straight section. It can be deployed at NSLS-II and at other low-emittance third-generation synchrotron radiation sources where canted undulators are permitted, and makes the most of these sources and beamline floor space, even when the horizontal angle between the two canted undulator emissions is as little as 1-2 mrad. The concept adopts the beam-separation principles employed at the 23-ID (GM/CA-CAT) beamlines at the Advanced Photon Source (APS), wherein tandem horizontally-deflecting mirrors separate one undulator beam from the other, following monochromatization by a double-crystal monochromator. The scheme described here would, in contrast, deliver the two tunable monochromatic undulator beams to separate endstations that address rather different and somewhat complementary purposes, with further beam conditioning imposed as required. A downstream microfocusing beamline would employ dual-stage focusing for work at the micron scale and, unique to this design, switch to single stage focusing for larger beams. On the other hand, the upstream, more highly automated beamline would only employ single stage focusing. PMID:21822346

  14. Links between geodiversity and cultural elements on three scale levels, a neglected part of geoconservation

    Science.gov (United States)

    van den Ancker, Hanneke; Jungerius, Pieter Dirk

    2015-04-01

    The best-known landscape map of The Netherlands is a simplified version of the first geological map of The Netherlands and was made between 1856 and 1867 by Winand Staring. It still is the basis of our vegetation districts. The main landscape units of this map are the sand landscape, the peat landscape, the river landscape, the marine landscape, the coastal dunes and the hills. On this scale level there is general awareness of the relationships between the geo aspects (geomorphology, geology, geohydrology and soil science) of the landscape and historical land use, e.g. in field patterns and other cultural elements (archaeology and historical geography). From three of these units, examples of interactions between geo-aspects and cultural elements are given for two different scale levels: first on a more regional scale level, then on site level. Especially the last level requires field study. The relationships between the geo and cultural aspects appear to be most intact and are most variable at the site level. Earth scientists as yet hardly involve themselves in geoconservation studies re these relationships, for which reason the geo-aspects of the cultural elements, especially those at the site level, often are not noticed and disappear during land development projects or gardening efforts. It also is a missed opportunity as these sites offer a chance to raise interest of a broader public for geomorphology and soils, which are in general more difficult to communicate. The development and management of cultural landscapes and sites, by Dutch law is the domain of land owners and landscape architects, who in the course of a project consult other experts. Our plea for future planning projects is to work with a team of experts including archaeologists, historical geographers, flora and fauna experts, geologists, geomorphologists and soil specialists. Although the costs of preparing a plan will be slightly higher, our experience is that it will improve the quality of

  15. 08B1-1: an automated beamline for macromolecular crystallography experiments at the Canadian Light Source.

    Science.gov (United States)

    Fodje, Michel; Grochulski, Pawel; Janzen, Kathryn; Labiuk, Shaunivan; Gorin, James; Berg, Russ

    2014-05-01

    Beamline 08B1-1 is a recently commissioned bending-magnet beamline at the Canadian Light Source. The beamline is designed for automation and remote access. Together with the undulator-based beamline 08ID-1, they constitute the Canadian Macromolecular Crystallography Facility. This paper describes the design, specifications, hardware and software of beamline 08B1-1. A few scientific results using data obtained at the beamline will be highlighted.

  16. Hard X-ray micro-focusing beamline at SSRF

    Institute of Scientific and Technical Information of China (English)

    张丽丽; 兰旭颖; 毛成文; 王娟; 蒋晖; 郑怡; 董朝晖; 曾乐勇; 李爱国; 闫帅; 蒋升; 杨科; 王华; 何上明; 梁东旭; 张玲; 何燕

    2015-01-01

    The hard X-ray micro-focusing beamline (BL15U1) of SSRF is dedicated to hard X-ray micro/nano-spectrochemical analysis consisting of X-ray fluorescence (XRF), X-ray absorption spectroscopy (XAS) and X-ray diffraction (XRD) techniques. It is one of the most versatile instruments in hard X-ray microscopy sci-ence. Since its commission in 2009, BL15U1 has allocated over 25000 h beamtime for users, and about 700 proposals have been executed. The beamline and the experimental end-station were upgraded for several times to facilitate the users’ experimental needs and make it more convenient to operate. In this paper, we give a review on the beamline, describing its characteristics, recent technical developments, and a few examples of scientific progresses achieved in recent years on BL15U1.

  17. The Materials Science beamline upgrade at the Swiss Light Source

    Energy Technology Data Exchange (ETDEWEB)

    Willmott, P. R., E-mail: philip.willmott@psi.ch; Meister, D.; Leake, S. J.; Lange, M.; Bergamaschi, A. [Swiss Light Source, Paul Scherrer Institut, CH-5232 Villigen (Switzerland); and others

    2013-07-16

    The wiggler X-ray source of the Materials Science beamline at the Swiss Light Source has been replaced with a 14 mm-period cryogenically cooled in-vacuum undulator. In order to best exploit the increased brilliance of this new source, the entire front-end and optics have been redesigned. The Materials Science beamline at the Swiss Light Source has been operational since 2001. In late 2010, the original wiggler source was replaced with a novel insertion device, which allows unprecedented access to high photon energies from an undulator installed in a medium-energy storage ring. In order to best exploit the increased brilliance of this new source, the entire front-end and optics had to be redesigned. In this work, the upgrade of the beamline is described in detail. The tone is didactic, from which it is hoped the reader can adapt the concepts and ideas to his or her needs.

  18. Atmospheric pollution in an urban environment by tree bark biomonitoring--part I: trace element analysis.

    Science.gov (United States)

    Guéguen, Florence; Stille, Peter; Lahd Geagea, Majdi; Boutin, René

    2012-03-01

    Tree bark has been shown to be a useful biomonitor of past air quality because it accumulates atmospheric particulate matter (PM) in its outermost structure. Trace element concentrations of tree bark of more than 73 trees allow to elucidate the impact of past atmospheric pollution on the urban environment of the cities of Strasbourg and Kehl in the Rhine Valley. Compared to the upper continental crust (UCC) tree barks are strongly enriched in Mn, Ni, Cu, Zn, Cd and Pb. To assess the degree of pollution of the different sites in the cities, a geoaccumulation index I(geo) was applied. Global pollution by V, Ni, Cr, Sb, Sn and Pb was observed in barks sampled close to traffic axes. Cr, Mo, Cd pollution principally occurred in the industrial area. A total geoaccumulation index I(GEO-tot) was defined; it is based on the total of the investigated elements and allows to evaluate the global pollution of the studied environment by assembling the I(geo) indices on a pollution map.

  19. COYOTE : a finite element computer program for nonlinear heat conduction problems. Part I, theoretical background.

    Energy Technology Data Exchange (ETDEWEB)

    Glass, Micheal W.; Hogan, Roy E., Jr.; Gartling, David K.

    2010-03-01

    The need for the engineering analysis of systems in which the transport of thermal energy occurs primarily through a conduction process is a common situation. For all but the simplest geometries and boundary conditions, analytic solutions to heat conduction problems are unavailable, thus forcing the analyst to call upon some type of approximate numerical procedure. A wide variety of numerical packages currently exist for such applications, ranging in sophistication from the large, general purpose, commercial codes, such as COMSOL, COSMOSWorks, ABAQUS and TSS to codes written by individuals for specific problem applications. The original purpose for developing the finite element code described here, COYOTE, was to bridge the gap between the complex commercial codes and the more simplistic, individual application programs. COYOTE was designed to treat most of the standard conduction problems of interest with a user-oriented input structure and format that was easily learned and remembered. Because of its architecture, the code has also proved useful for research in numerical algorithms and development of thermal analysis capabilities. This general philosophy has been retained in the current version of the program, COYOTE, Version 5.0, though the capabilities of the code have been significantly expanded. A major change in the code is its availability on parallel computer architectures and the increase in problem complexity and size that this implies. The present document describes the theoretical and numerical background for the COYOTE program. This volume is intended as a background document for the user's manual. Potential users of COYOTE are encouraged to become familiar with the present report and the simple example analyses reported in before using the program. The theoretical and numerical background for the finite element computer program, COYOTE, is presented in detail. COYOTE is designed for the multi-dimensional analysis of nonlinear heat conduction

  20. Current schemes for National Synchrotron Light Source UV beamlines

    Energy Technology Data Exchange (ETDEWEB)

    Williams, G.P.; Howells, M.R.; McKinney, W.R.

    1979-01-01

    We describe in some detail four beamlines proposed for the National Synchrotron Light Source uv ring at Brookhaven National Laboratory. Three grazing-incidence instruments, one of the plane grating Mijake type and two with toroidal gratings at grazing angles of 2-1/2/sup 0/ and 15/sup 0/ are described. Two normal incidence instruments, one using the source as entrance slit and accepting 75 milliradians horizontally are also discussed. In each case we have estimated the output fluxes expected from such beamlines.

  1. Finite element modeling of borehole heat exchanger systems. Part 2. Numerical simulation

    Science.gov (United States)

    Diersch, H.-J. G.; Bauer, D.; Heidemann, W.; Rühaak, W.; Schätzl, P.

    2011-08-01

    Single borehole heat exchanger (BHE) and arrays of BHE are modeled by using the finite element method. Applying BHE in regional discretizations optimal conditions of mesh spacing around singular BHE nodes are derived. Optimal meshes have shown superior to such discretizations which are either too fine or too coarse. The numerical methods are benchmarked against analytical and numerical reference solutions. Practical application to a borehole thermal energy store (BTES) consisting of 80 BHE is given for the real-site BTES Crailsheim, Germany. The simulations are controlled by the specifically developed FEFLOW-TRNSYS coupling module. Scenarios indicate the effect of the groundwater flow regime on efficiency and reliability of the subsurface heat storage system.

  2. Isogeometric Boundary Element Analysis with elasto-plastic inclusions. Part 1: Plane problems

    CERN Document Server

    Beer, Gernot; Zechner, Jürgen; Dünser, Christian; Fries, Thomas-Peter

    2015-01-01

    In this work a novel approach is presented for the isogeometric Boundary Element analysis of domains that contain inclusions with different elastic properties than the ones used for computing the fundamental solutions. In addition the inclusion may exhibit inelastic material behavior. In this paper only plane stress/strain problems are considered. In our approach the geometry of the inclusion is described using NURBS basis functions. The advantage over currently used methods is that no discretization into cells is required in order to evaluate the arising volume integrals. The other difference to current approaches is that Kernels of lower singularity are used in the domain term. The implementation is verified on simple finite and infinite domain examples with various boundary conditions. Finally a practical application in geomechanics is presented.

  3. Element Analysis of Ceramic Coatings under Spherical Indentation with Metallic Interlayer:Part Ⅱ Ring Crack

    Institute of Scientific and Technical Information of China (English)

    Minh-Quy LE; Seock-Sam KIM

    2006-01-01

    Spherical indentation of ceramic coatings with metallic interlayer was performed by means of axisymmetric finite element analysis(FEA). Two typical ceramic coatings with relatively high and low elastic modulus deposited on aluminum alloy and carbon steel were considered. The fracture mechanics of the ceramic coatings mechanisms due to occurrence of surface ring cracks extending traverse the coating thickness under spherical indentation are investigated within the framework of linear fracture mechanics. The J-integral associated to such cracks was computed. The evolution of J-integral vs the crack length and the indentation depth was studied. The effects of the interlayer, the coating and the substrate on the J-integral evolution were discussed. The results show that a suitable metallic interlayer can improve the fracture resistance of the coating systems under the same indentation conditions through reducing the J-integral.

  4. Implementation of Bourbaki's Elements of Mathematics in Coq: Part One, Theory of Sets

    Directory of Open Access Journals (Sweden)

    José Grimm

    2010-01-01

    Full Text Available This paper presents a formalization of the first book of the series ``Elements of Mathematics'' by Nicolas Bourbaki, using the Coq proof assistant.It discusses formalization of mathematics, and explains in which sense a computer proof of a statement corresponds to a proof in the Bourbaki sense, given that the Coq quantifiers are not defined in terms of Hilbert's epsilon function. The list of axioms and axiom schemes of Bourbaki is compared to the more usual Zermelo-Fraenkel theory, and to those proposed by Carlos Simpson, which form the basis of the Gaia software. Some basic constructions (union, intersection, product, function, equivalence and order relation are described, as well as some properties; this corresponds to Sections 1 to 6 of Chapter II, and the first two sections of Chapter III. A commented proof of Zermelo's theorem is also given. The code (including almost all exercises is available on the Web, underhttp://www-sop.inria.fr/apics/gaia.

  5. Finite Element Analysis of Ceramic Coatings under Spherical Indentation with Metallic Interlayer: Part Ⅰ Uncracked Coatings

    Institute of Scientific and Technical Information of China (English)

    Minh-Quy LE; Seock-Sam KIM

    2006-01-01

    Spherical indentation of ceramic coatings with metallic interlayer was performed by means of axisymmetric finite element analysis (FEA). Two typical ceramic coatings with relatively high and low elastic modulus deposited on aluminum alloy and carbon steel were considered. Various combinations of indenter radius-coating thickness ratios and interlayer thickness-coating thickness ratios were used in the modeling. The effects of the interlayer, the coating and the substrate on the indentation behavior, such as the radial stress distribution along the coating surface as well as the coating interface, and the plastic deformation zone evolution in the substrate were investigated in connection with the above mentioned ratios. The coating cracking dominant modes were also discussed within the context of the peak tensile stresses on the coating surface and on the coating interface.

  6. Design of a large acceptance, high efficiency energy selection system for the ELIMAIA beam-line

    Science.gov (United States)

    Schillaci, F.; Maggiore, M.; Andó, L.; Cirrone, G. A. P.; Cuttone, G.; Romano, F.; Scuderi, V.; Allegra, L.; Amato, A.; Gallo, G.; Korn, G.; Leanza, R.; Margarone, D.; Milluzzo, G.; Petringa, G.

    2016-08-01

    A magnetic chicane based on four electromagnetic dipoles is going to be realized by INFN-LNS to be used as an Energy Selection System (ESS) for laser driven proton beams up to 300 MeV and C6+ up to 70 MeV/u. The system will provide, as output, ion beams with a contrallable energy spread varying from 5% up to 20% according to the aperture slit size. Moreover, it has a very wide acceptance in order to ensure a very high transmission efficiency and, in principle, it has been designed to be used also as an active energy modulator. This system is the core element of the ELIMED (ELI-Beamlines MEDical and Multidisciplinary applications) beam transport, dosimetry and irradiation line that will be developed by INFN-LNS (It) and installed at the ELI-Beamlines facility in Prague (Cz). ELIMED will be the first user's open transport beam-line where a controlled laser-driven ion beam will be used for multidisciplinary research. The definition of well specified characteristics, both in terms of performance and field quality, of the magnetic chicane is crucial for the system realization, for the accurate study of the beam dynamics and for the proper matching with the Permanent Magnet Quadrupoles (PMQs) used as a collection system already designed. Here, the design of the magnetic chicane is described in details together with the adopted solutions in order to realize a robust system form the magnetic point of view. Moreover, the first preliminary transport simulations are also described showing the good performance of the whole beam line (PMQs+ESS).

  7. Development and tests of a new prototype detector for the XAFS beamline at Elettra Synchrotron in Trieste

    CERN Document Server

    Fabiani, S; Baldazzi, G; Bellutti, P; Bertuccio, G; Bruschi, M; Bufon, J; Carrato, S; Castoldi, A; Cautero, G; Ciano, S; Cicuttin, A; Crespo, M L; Santos, M Dos; Gandola, M; Giacomini, G; Giuressi, D; Guazzoni, C; Menk, R H; Niemela, J; Olivi, L; Picciotto, A; Piemonte, C; Rashevskaya, I; Rachevski, A; Rignanese, L P; Sbrizzi, A; Schillani, S; Vacchi, A; Garcia, V Villaverde; Zampa, G; Zampa, N; Zorzi, N

    2016-01-01

    The XAFS beamline at Elettra Synchrotron in Trieste combines X-ray absorption spectroscopy and X-ray diffraction to provide chemically specific structural information of materials. It operates in the energy range 2.4-27 keV by using a silicon double reflection Bragg monochromator. The fluorescence measurement is performed in place of the absorption spectroscopy when the sample transparency is too low for transmission measurements or the element to study is too diluted in the sample. We report on the development and on the preliminary tests of a new prototype detector based on Silicon Drift Detectors technology and the SIRIO ultra low noise front-end ASIC. The new system will be able to reduce drastically the time needed to perform fluorescence measurements, while keeping a short dead time and maintaining an adequate energy resolution to perform spectroscopy. The custom-made silicon sensor and the electronics are designed specifically for the beamline requirements.

  8. DESIGN OF VISIBLE DIAGNOSTIC BEAMLINE FOR NSLS2 STORAGE RING

    Energy Technology Data Exchange (ETDEWEB)

    Cheng, W.; Fernandes, H.; Hseuh, H.; Kosciuk, B.; Krinsky, S.; Singh, O.

    2011-03-28

    A visible synchrotron light monitor (SLM) beam line has been designed at the NSLS2 storage ring, using the bending magnet radiation. A retractable thin absorber will be placed in front of the first mirror to block the central x-rays. The first mirror will reflect the visible light through a vacuum window. The light is guided by three 6-inch diameter mirrors into the experiment hutch. In this paper, we will describe design work on various optical components in the beamline. The ultra high brightness NSLS-II storage ring is under construction at Brookhaven National Laboratory. It will have 3GeV, 500mA electron beam circulating in the 792m ring, with very low emittance (0.9nm.rad horizontal and 8pm.rad vertical). The ring is composed of 30 DBA cells with 15 fold symmetry. Three damping wigglers will be installed in long straight sections 8, 18 and 28 to lower the emittance. While electrons pass through the bending magnet, synchrotron radiation will be generated covering a wide spectrum. There are other insertion devices in the storage ring which will generate shorter wavelength radiation as well. Synchrotron radiation has been widely used as diagnostic tool to measure the transverse and longitudinal profile. Three synchrotron light beam lines dedicated for diagnostics are under design and construction for the NSLS-II storage ring: two x-ray beam lines (pinhole and CRL) with the source points from Cell 22 BM{_}A (first bending in the DBA cell) and Cell22 three-pole wiggler; the third beam line is using visible part of radiation from Cell 30 BM{_}B (second bending magnet from the cell). Our paper focuses on the design of the visible beam line - SLM.

  9. The Pharmaceutical Industry Beamline of Pharmaceutical Consortium for Protein Structure Analysis

    CERN Document Server

    Nishijima, K

    2002-01-01

    The Pharmaceutical Industry Beamline was constructed by the Pharmaceutical Consortium for Protein Structure Analysis which was established in April 2001. The consortium is composed of 22 pharmaceutical companies affiliating with the Japan Pharmaceutical Manufacturers Association. The beamline is the first exclusive on that is owned by pharmaceutical enterprises at SPring-8. The specification and equipments of the Pharmaceutical Industry Beamline is almost same as that of RIKEN Structural Genomics Beamline I and II. (author)

  10. Distributed control of protein crystallography beamline 5.0 using CORBA

    OpenAIRE

    Timossi, Chris

    1999-01-01

    The Protein Crystallography Beamline at Berkeley Lab's Advanced Light Source is a facility that is being used to solve the structure of proteins. The software that is being used to control this beamline uses Java for user interface applications which communicate via CORBA with workstations that control the beamline hardware. We describe the software architecture for the beamline and our experiences after two years of operation.

  11. Finite Element Analysis of the Effect on Edge Distance of the Tensile Bearing Capacity of Embedded Hanging Parts

    Directory of Open Access Journals (Sweden)

    Meng Xian Hong

    2016-01-01

    Full Text Available In order to explore the trend of tensile bearing capacity of embedded hanging parts when change the edge distance. Based on the finite element analysis software ABAQUS, the four simulation model was established. The buried depth and strength of concrete remain unchanged, but the edge distance was gradient change. By the load - displacement curve of every model known, the greater the edge distance, the greater the bearing capacity. When the edge distance reaches 1.5 times buried depth, the effect of increasing edge distance for improving the bearing capacity will be impaired.

  12. Oxygen, {\\alpha}-element and iron abundance distributions in the inner part of the Galactic thin disc

    CERN Document Server

    Martin, R P; Kovtyukh, V V; Korotin, S A; Yegorova, I A; Saviane, Ivo

    2015-01-01

    We derived elemental abundances in 27 Cepheids, the great majority situated within a zone of Galactocentric distances ranging from 5 to 7 kpc. One star of our sample, SU Sct, has a Galactocentric distance of about 3 kpc, and thus falls in a poorly investigated region of the inner thin disc. Our new results, combined with data on abundances in the very central part of our Galaxy taken from literature, show that iron, magnesium, silicon, sulfur, calcium and titanium LTE abundance radial distributions, as well as NLTE distribution of oxygen reveal a plateau-like structure or even positive abundance gradient in the region extending from the Galactic center to about 5 kpc.

  13. MPSalsa a finite element computer program for reacting flow problems. Part 2 - user`s guide

    Energy Technology Data Exchange (ETDEWEB)

    Salinger, A.; Devine, K.; Hennigan, G.; Moffat, H. [and others

    1996-09-01

    This manual describes the use of MPSalsa, an unstructured finite element (FE) code for solving chemically reacting flow problems on massively parallel computers. MPSalsa has been written to enable the rigorous modeling of the complex geometry and physics found in engineering systems that exhibit coupled fluid flow, heat transfer, mass transfer, and detailed reactions. In addition, considerable effort has been made to ensure that the code makes efficient use of the computational resources of massively parallel (MP), distributed memory architectures in a way that is nearly transparent to the user. The result is the ability to simultaneously model both three-dimensional geometries and flow as well as detailed reaction chemistry in a timely manner on MT computers, an ability we believe to be unique. MPSalsa has been designed to allow the experienced researcher considerable flexibility in modeling a system. Any combination of the momentum equations, energy balance, and an arbitrary number of species mass balances can be solved. The physical and transport properties can be specified as constants, as functions, or taken from the Chemkin library and associated database. Any of the standard set of boundary conditions and source terms can be adapted by writing user functions, for which templates and examples exist.

  14. MPSalsa a finite element computer program for reacting flow problems. Part 2 - user`s guide

    Energy Technology Data Exchange (ETDEWEB)

    Salinger, A.; Devine, K.; Hennigan, G.; Moffat, H. [and others

    1996-09-01

    This manual describes the use of MPSalsa, an unstructured finite element (FE) code for solving chemically reacting flow problems on massively parallel computers. MPSalsa has been written to enable the rigorous modeling of the complex geometry and physics found in engineering systems that exhibit coupled fluid flow, heat transfer, mass transfer, and detailed reactions. In addition, considerable effort has been made to ensure that the code makes efficient use of the computational resources of massively parallel (MP), distributed memory architectures in a way that is nearly transparent to the user. The result is the ability to simultaneously model both three-dimensional geometries and flow as well as detailed reaction chemistry in a timely manner on MT computers, an ability we believe to be unique. MPSalsa has been designed to allow the experienced researcher considerable flexibility in modeling a system. Any combination of the momentum equations, energy balance, and an arbitrary number of species mass balances can be solved. The physical and transport properties can be specified as constants, as functions, or taken from the Chemkin library and associated database. Any of the standard set of boundary conditions and source terms can be adapted by writing user functions, for which templates and examples exist.

  15. A new experiment station on beamline 4B7A at Beijing Synchrotron Radiation Facility

    Science.gov (United States)

    Zheng, L.; Zhao, Y. D.; Tang, K.; Ma, C. Y.; Hong, C. H.; Han, Y.; Cui, M. Q.; Guo, Z. Y.

    2014-11-01

    A new experiment station was installed on beamline 4B7A at Beijing Synchrotron Radiation Facility (BSRF), making it possible to record X-ray absorption fine structure (XAFS) spectrum in three modes over an energy range from 1750 eV to 6000 eV. A 13-element Si(Li) array detector and a single-element SDD detector were used to acquire data in partial fluorescence yield (PFY) mode. Two low-pressure noble gas ion chambers were adopted for measuring XAFS in transmission mode. In total electron yield (TEY) mode the current of sample is recorded. Solid, wet and liquid samples were suitable for this experimental station. Some representative results obtained from this station were shown and discussed.

  16. Final Technical Report on STTR Project DE-FG02-06ER86281 Particle Tracking in Matter-Dominated Beam Lines (G4beamline)

    Energy Technology Data Exchange (ETDEWEB)

    Muons, Inc.

    2011-05-19

    This project has been for software development of the G4beamline [1] program, which is a particle-tracking simulation program based on the Geant4 toolkit [2], optimized for beam lines. This program can perform more realistic simulations than most alternatives, while being significantly easier to use by physicists. This project has fostered the general acceptance of G4beamline within the muon community, and has assisted in expanding its role outside that community. During this project, the G4beamline user community has grown from about a half-dozen users to more than 200 users around the world. This project also validated our business decision to keep G4beamline an open-source program, judging that an STTR project would provide more development resources than would marketing and selling the program. G4beamline is freely available to the physics community, and has been well validated against experiments and other codes within its domain. Muons, Inc. continues to support and develop the program, and a major part of the company's continued success and growth is directly related to our expertise in applying this program to interesting applications.

  17. Small angle X-ray scattering beamline at SSRF

    Institute of Scientific and Technical Information of China (English)

    田丰; 李小芸; 缪夏然; 边风刚; 王吉力; 李秀宏; 王玉柱; 杨春明; 周平; 林金友; 曾建荣; 洪春霞; 滑文强

    2015-01-01

    Beamline BL16B1 at Shanghai Synchrotron Radiation Facility (SSRF) is dedicated to studying the mi-crostructure and dynamic processes of polymers, nanomaterials, mesoporous materials, colloids, liquid crystals, metal materials, etc. At present, SAXS, wide angle X-ray scattering (WAXS), simultaneous SAXS/WAXS, grazing incident SAXS, and anomalous SAXS techniques are available for end user to conduct diverse ex-periments at this beamline. The sample-to-detector distance is adjustable from 0.2 m to 5 m. The practicable q-range is 0.03–3.6 nm−1 at incident X-ray of 10 keV for conventional SAXS whilst a continuous q-region of 0.06–33 nm−1 can be achieved in simultaneous SAXS/WAXS mode. Time-resolved SAXS measurements in sub-second level was achieved by the beamline upgrating in 2013. This paper gives detailed descriptions about the status, performance and applications of the SAXS beamline.

  18. Third-Order Apochromatic Drift-Quadrupole Beamline

    CERN Document Server

    Balandin, V; Decking, W; Golubeva, N

    2012-01-01

    In this paper we present the design of a straight drift-quadrupole system which can transport certain beam ellipses (apochromatic beam ellipses) without influence of the second and of the third order chromatic and geometric aberrations of the beamline transfer map.

  19. The Diamond Beamline Controls and Data Acquisition Software Architecture

    Science.gov (United States)

    Rees, N.

    2010-06-01

    The software for the Diamond Light Source beamlines[1] is based on two complementary software frameworks: low level control is provided by the Experimental Physics and Industrial Control System (EPICS) framework[2][3] and the high level user interface is provided by the Java based Generic Data Acquisition or GDA[4][5]. EPICS provides a widely used, robust, generic interface across a wide range of hardware where the user interfaces are focused on serving the needs of engineers and beamline scientists to obtain detailed low level views of all aspects of the beamline control systems. The GDA system provides a high-level system that combines an understanding of scientific concepts, such as reciprocal lattice coordinates, a flexible python syntax scripting interface for the scientific user to control their data acquisition, and graphical user interfaces where necessary. This paper describes the beamline software architecture in more detail, highlighting how these complementary frameworks provide a flexible system that can accommodate a wide range of requirements.

  20. New X-ray emission spectrometer at the Rossendorf Beamline

    Energy Technology Data Exchange (ETDEWEB)

    Kvashnina, Kristina O.; Scheinost, Andreas C. [Helmholtz-Zentrum Dresden-Rossendorf e.V., Dresden (Germany). Div. Molecular Structures

    2016-07-01

    A preliminary Johann-type X-ray emission spectrometer has recently been installed and tested at the Rossendorf Beamline (ROBL). The spectrometer consists of a single spherically bent crystal analyzer and an avalanche photodiode detector positioned on the vertical Rowland cycle with 1 m diameter. The instrument has been tested at the Zr-K edge.

  1. The High Energy Materials Science Beamline (HEMS) at PETRA III

    Science.gov (United States)

    Schell, Norbert; King, Andrew; Beckmann, Felix; Ruhnau, Hans-Ulrich; Kirchhof, René; Kiehn, Rüdiger; Müller, Martin; Schreyer, Andreas

    2010-06-01

    The HEMS Beamline at the German high-brilliance synchrotron radiation storage ring PETRA III is fully tunable between 30 and 250 keV and optimized for sub-micrometer focusing. Approximately 70 % of the beamtime will be dedicated to Materials Research. Fundamental research will encompass metallurgy, physics and chemistry with first experiments planned for the investigation of the relationship between macroscopic and micro-structural properties of polycrystalline materials, grain-grain-interactions, and the development of smart materials or processes. For this purpose a 3D-microsctructure-mapper has been designed. Applied research for manufacturing process optimization will benefit from high flux in combination with ultra-fast detector systems allowing complex and highly dynamic in-situ studies of micro-structural transformations, e.g. during welding processes. The beamline infrastructure allows accommodation of large and heavy user provided equipment. Experiments targeting the industrial user community will be based on well established techniques with standardized evaluation, allowing full service measurements, e.g. for tomography and texture determination. The beamline consists of a five meter in-vacuum undulator, a general optics hutch, an in-house test facility and three independent experimental hutches working alternately, plus additional set-up and storage space for long-term experiments. HEMS is under commissioning as one of the first beamlines running at PETRA III.

  2. Remote access and automation of SPring-8 MX beamlines

    Energy Technology Data Exchange (ETDEWEB)

    Ueno, Go, E-mail: ueno@spring8.or.jp; Hikima, Takaaki; Yamashita, Keitaro; Hirata, Kunio; Yamamoto, Masaki [RIKEN SPring-8 Center, 1-1-1 Koto, Sayo-cho, Sayo-gun, Hyogo 679-5148 JAPAN (Japan); Hasegawa, Kazuya; Murakami, Hironori; Furukawa, Yukito; Mizuno, Nobuhiro; Kumasaka, Takashi [SPring-8/JASRI, 1-1-1 Koto, Sayo-cho, Sayo-gun, Hyogo 679-5198 JAPAN (Japan)

    2016-07-27

    At SPring-8 MX beamlines, a remote access system has been developed and started user operation in 2010. The system has been developed based on an automated data collection and data management architecture utilized for the confirmed scheme of SPring-8 mail-in data collection. Currently, further improvement to the remote access and automation which covers data processing and analysis are being developed.

  3. Canadian macromolecular crystallography facility: a suite of fully automated beamlines.

    Science.gov (United States)

    Grochulski, Pawel; Fodje, Michel; Labiuk, Shaunivan; Gorin, James; Janzen, Kathryn; Berg, Russ

    2012-06-01

    The Canadian light source is a 2.9 GeV national synchrotron radiation facility located on the University of Saskatchewan campus in Saskatoon. The small-gap in-vacuum undulator illuminated beamline, 08ID-1, together with the bending magnet beamline, 08B1-1, constitute the Canadian Macromolecular Crystallography Facility (CMCF). The CMCF provides service to more than 50 Principal Investigators in Canada and the United States. Up to 25% of the beam time is devoted to commercial users and the general user program is guaranteed up to 55% of the useful beam time through a peer-review process. CMCF staff provides "Mail-In" crystallography service to users with the highest scored proposals. Both beamlines are equipped with very robust end-stations including on-axis visualization systems, Rayonix 300 CCD series detectors and Stanford-type robotic sample auto-mounters. MxDC, an in-house developed beamline control system, is integrated with a data processing module, AutoProcess, allowing full automation of data collection and data processing with minimal human intervention. Sample management and remote monitoring of experiments is enabled through interaction with a Laboratory Information Management System developed at the facility.

  4. Design of 3B3 beamline control system

    Institute of Scientific and Technical Information of China (English)

    2006-01-01

    Both structure and design of the control system in BSRF-3B3 beamline, are discussed and the subsystems are described. The LabVIEW software has advantages on data collecting and real time inspecting. In the process of data collecting, some methods are taken to solve the problems that may be met.

  5. Angle-resolved electron and ion spectroscopy apparatus on the soft X-ray photochemistry beamline BL27SU at SPring-8

    CERN Document Server

    Ueda, K; Senba, Y; Okada, K; Shimizu, Y; Chiba, H; Ohashi, H; Tamenori, Y; Okumura, H; Saitô, N; Nagaoka, S; Hiraya, A; Ishiguro, E; Ibuki, T; Suzuki, I H; Koyano, I

    2001-01-01

    We have designed and constructed the apparatus for the angular distribution measurements of photoejected electrons and ions from free molecules, as a part of the endstation of the c-branch of the beamline BL27SU, a soft X-ray photochemistry beamline at SPring-8. The experimental procedures are described in combination with the use of a capability to switch the horizontal and vertical directions of the linear polarization of the light produced by the figure-8 undulator. As a typical example of the experimental results, we present angle-resolved energetic ion yield spectra in the O 1s excitation region of CO sub 2.

  6. Justification for the development of a bending magnet beamline at sector 10 at the APS.

    Energy Technology Data Exchange (ETDEWEB)

    Kemner, K. M.; Biosciences Division

    2006-09-18

    undulator beamline with an experimental station for bulk XAFS applications and x-ray microbeam applications (XRF, XAFS, and XRD) and (2) a BM beamline with an experimental station for large-sample XAFS spectroscopy and XRF elemental mapping on submillimeter to centimeter length scales.

  7. Surface and interface analysis of nanomaterials at microfocus beamline (BL-16) of Indus-2

    Science.gov (United States)

    Das, Gangadhar; Khooha, Ajay; Kane, S. R.; Singh, A. K.; Tiwari, M. K.

    2016-05-01

    Analysis of chemical nature and electronic structure at the interface of a thin film medium is important in many technological applications as well as to understand overall efficiency of a thin film device. Synchrotron radiation based x-ray spectroscopy is a promising technique to study interface nature of the nanomaterials with atomic resolutions. A combined x-ray reflectivity and grazing incidence x-ray fluorescence measurement facility has been recently constructed at the BL-16 microfocus beamline of Indus-2 synchrotron facility to accomplish surface-interface microstructural characterization of thin layered materials. It is also possible to analyze contaminates or adsorbed ad-atoms on the surface of the thin nanostructure materials. The BL-16 beamline also provides an attractive platform to perform a variety of analytical research activities especially in the field of micro x-ray fluorescence and ultra-trace elements analysis using Synchrotron radiation. We describe various salient features of the BL-16 reflectometer experimental station and the detailed description of its capabilities through the measured results, obtained for various thin layered nanomaterials.

  8. Design and performance of a new VIS-VUV photoluminescence beamline at UVSOR-III.

    Science.gov (United States)

    Fukui, Kazutoshi; Ikematsu, Ryu-ichi; Imoto, Yoshinori; Kitaura, Mamoru; Nakagawa, Kazumichi; Ejima, Takao; Nakamura, Eiken; Sakai, Masahiro; Hasumoto, Masami; Kimura, Shin-ichi

    2014-03-01

    A new bending-magnet beamline with a 2.5 m normal-incidence monochromator has been constructed to serve with a light source in the visible-vacuum-ultraviolet region for photoluminescence, transmission and reflection spectroscopies of solids at the UVSOR-III 750 MeV synchrotron radiation light source. The aim is to pave the way to establishing a beamline with high photon flux, high brilliance, high energy-resolution, high linear-polarization and low higher-order light. To obtain high photon flux and brilliance, the acceptance angle of the bending-magnet radiation was designed to be 40 mrad (H) × 14 mrad (V) and the post-mirror system employed Kirkpatrick-Baez optics. The incidence angle of the incoming light to the optical elements, except to the gratings, was set to a grazing angle in order to keep a degree of linear polarization. For achieving high energy-resolution, an off-plane Eagle-type monochromator was adopted. Higher-order unwanted light in the energy range below ∼11 eV was suppressed to be less than 0.1%.

  9. Design and performance of a new VIS–VUV photoluminescence beamline at UVSOR-III

    Science.gov (United States)

    Fukui, Kazutoshi; Ikematsu, Ryu-ichi; Imoto, Yoshinori; Kitaura, Mamoru; Nakagawa, Kazumichi; Ejima, Takao; Nakamura, Eiken; Sakai, Masahiro; Hasumoto, Masami; Kimura, Shin-ichi

    2014-01-01

    A new bending-magnet beamline with a 2.5 m normal-incidence monochromator has been constructed to serve with a light source in the visible–vacuum-ultraviolet region for photoluminescence, transmission and reflection spectroscopies of solids at the UVSOR-III 750 MeV synchrotron radiation light source. The aim is to pave the way to establishing a beamline with high photon flux, high brilliance, high energy-resolution, high linear-polarization and low higher-order light. To obtain high photon flux and brilliance, the acceptance angle of the bending-magnet radiation was designed to be 40 mrad (H) × 14 mrad (V) and the post-mirror system employed Kirkpatrick–Baez optics. The incidence angle of the incoming light to the optical elements, except to the gratings, was set to a grazing angle in order to keep a degree of linear polarization. For achieving high energy-resolution, an off-plane Eagle-type monochromator was adopted. Higher-order unwanted light in the energy range below ∼11 eV was suppressed to be less than 0.1%. PMID:24562569

  10. Initial Emittance Measurements of the Fermilab Linac Beam Using the MTA Beamline

    CERN Document Server

    Johnstone, C

    2012-01-01

    The MTA beam line has been specifically designed to facilitate measurements of the Fermilab Linac beam emittance and properties utilizing a long, 10m, element-free straight. Linac beam is extracted downstream of the 400-MeV electrostatic chopper located in the Booster injection line. This chopper cannot be utilized for MTA beam, and therefore the entire Linac beam pulse is directed into the MTA beamline. Pulse length manipulation is provided by the 750-keV electrostatic chopper at the upstream end of the Linac and, using this device, beam can be delivered from 8 {\\mu}sec up to the full 50 {\\mu}sec Linac pulse length. The 10 m emittance measurement straight exploits and begins at the 12' shield wall that separates the MTA Experimental Hall and beamline stub from the Linac enclosure. A quadrupole triplet has been installed upstream of the shield wall in order to focus a large, 1.5-2" (~95% width) beam through the shield wall and onto a profile monitor located at the exit of the shielding. Another profile monito...

  11. Strangelet search and particle production studies in Pb-Pb collisions at 158·A GeV/c with the H6 beamline spectrometer at CERN

    CERN Document Server

    Lindén, Tomas

    The charged particle beamline simulation program DECAY TURTLE (Trace Unlimited Rays Through Lumped Elements) has been modified to enable simulation of dipole magnet steering effects and simulation of hadronic interactions. These modifications together with the implementation of the measured misalignments of the magnetic elements of the H6 beamline at the CERN North Area and implementation of more accurate magnet apertures have been shown to allow a realistic simulation to be made of the complex 524 m long H6 beamline spectrometer used by NA52. The acceptance of the H6 beamline spectrometer has been computed using this modified version of DECAY TURTLE. Using these results better determined invariant differential production cross sections have been computed from the NA52 1994-1995 data, with improved error estimates. New limits for strangelet production in lead-lead collisions at 158.A GeV/c have been computed from the NA52 measurements from 1994-1995. The methods and results presented in this work can be appli...

  12. Beamline 9.3.2 - a high-resolution, bend-magnet beamline with circular polarization capability

    Energy Technology Data Exchange (ETDEWEB)

    Moler, E.J.; Hussain, Z.; Howells, M.R. [Lawrence Berkeley National Lab., CA (United States)] [and others

    1997-04-01

    Beamline 9.3.2 is a high resolution, SGM beamline on an ALS bending magnet with access to photon energies from 30-1500 eV. Features include circular polarization capability, a rotating chamber platform that allows switching between experiments without breaking vacuum, an active feedback system that keeps the beam centered on the entrance slit of the monochromator, and a bendable refocusing mirror. The beamline optics consist of horizontally and vertically focussing mirrors, a Spherical Grating Monochromator (SGM) with movable entrance and exit slits, and a bendable refocussing mirror. In addition, a movable aperature has been installed just upstream of the vertically focussing mirror which can select the x-rays above or below the plane of the synchrotron storage ring, allowing the user to select circularly or linearly polarized light. Circularly polarized x-rays are used to study the magnetic properties of materials. Beamline 9.3.2 can supply left and right circularly polarized x-rays by a computer controlled aperture which may be placed above or below the plane of the synchrotron storage ring. The degree of linear and circular polarization has been measured and calibrated.

  13. Design, fabrication and testing of elliptical crystal bender for the EXAFS beam-line at INDUS-II synchrotron source

    Indian Academy of Sciences (India)

    N C Das; S N Jha; D Bhattacharyya; A K Poswal; A K Sinha; V K Mishra

    2004-10-01

    An extended X-ray absorption fine structure (EXAFS) beam-line for X-ray absorption studies using energy dispersive geometry and position sensitive detector is being developed for the INDUS-II synchrotron source. The optical design of the beam-line has been completed based on the working principle that a single crystal bent in the shape of an ellipse by a crystal bender would act as a dispersing as well as focusing element. The heart of the beam-line is the crystal bender which has been designed on the basis of the principle of four-point bending and has been fabricated indigenously. The crystal bender is capable of producing pre-defined elliptical curvature on a crystal surface by applying different couples at the two-ends of the crystal which has variable width along its length. The focusing property of the crystal bender has been tested using a laser source and has been compared with the theoretically simulated results.

  14. Elemental distributions in surficial sediments and potential offshore mineral resources from the western continental margin of India. Part 2. Potential offshore mineral resources

    Digital Repository Service at National Institute of Oceanography (India)

    Paropkari, A.L.; Mascarenhas, A.; Rao, Ch.M.; PrakashBabu, C.; Murty, P.S.N.

    patterns of ten selected elements is surficial sediments. Part 2 projects the potential offshore mineral resources. Target areas for future exploration and indicated and exploration strategies are recommended. Appendix 1 is a compilation of the bibliography...

  15. Exploratory studies of element substitutions in synthetic tetrahedrite. Part II. Selenium and tellurium as anions in Zn-Fe tetrahedrites

    DEFF Research Database (Denmark)

    Karup-Møller, Sven; Makovicky, E.

    1999-01-01

    Composition limits of iron and/or zinc-bearing selenium tetrahedrite were explored by means of dry syntheses from pure elements at 450oC. Only the substituted compositions Cu10Zn2Sb4Se13 (a 10.833 Å) and Cu10Fe1.8Sb4Se13 (a 10.823 Å) are stable. All partly substituted and unsubstituted (i.e. Zn......-free) compositons do not materialize. The substituted Se tetrahedrite coexists with Cu3SbSe3, (iron-bearing) Cu2-xSe, Cu3SbSe4 plus/minus low Zn-sulfide melt. Selenium does not adopt the role of cation and tellurium that of anion in the tetrahedrite structure. The explanation of the severely restricted composition...

  16. Identifying shared and contested elements in climate plans as part of shaping transitions towards a Danish low carbon society

    DEFF Research Database (Denmark)

    Jørgensen, Michael Søgaard

    2011-01-01

    the Danish Society of Engineers, a renewable energy NGO, an environmental NGO and a national climate change commission. The aim is to identify shared and contested elements, which need to be addressed in attempts to establish alignment around transition efforts towards a fossil free Danish society...... in agriculture. The plans differ with respect to whether and how agricultural production and Danish food consumption should change as part of transitions towards a low carbon society. All four plans agree about a significant increase in Danish wind turbine capacity and stronger energy saving efforts in Danish...... production and consumption activities. The plans differ with respect to how big reduction of energy consumption it is possible to obtain and how big the future energy consumption will be. This has implications for how big wind turbine capacity the plans assume is necessary and possible to build, ranging from...

  17. Exploratory studies of element substitutions in synthetic tetrahedrite. Part II. Selenium and tellurium as anions in Zn-Fe tetrahedrites

    DEFF Research Database (Denmark)

    Karup-Møller, Sven; Makovicky, E.

    1999-01-01

    -free) compositons do not materialize. The substituted Se tetrahedrite coexists with Cu3SbSe3, (iron-bearing) Cu2-xSe, Cu3SbSe4 plus/minus low Zn-sulfide melt. Selenium does not adopt the role of cation and tellurium that of anion in the tetrahedrite structure. The explanation of the severely restricted composition......Composition limits of iron and/or zinc-bearing selenium tetrahedrite were explored by means of dry syntheses from pure elements at 450oC. Only the substituted compositions Cu10Zn2Sb4Se13 (a 10.833 Å) and Cu10Fe1.8Sb4Se13 (a 10.823 Å) are stable. All partly substituted and unsubstituted (i.e. Zn...

  18. Orbital stress analysis, part V: systematic approach to validate a finite element model of a human orbit.

    Science.gov (United States)

    Al-sukhun, Jehad; Penttilä, Heikki; Ashammakhi, Nureddin

    2012-05-01

    The progress in computer technology and the increased use of finite element analysis in the medical field by nonengineers and medical researchers lead us to believe that there is a need to develop a systematic approach to validate a finite element model (FEM), of a human orbit, that simulates part of the maxillofacial skeleton and to investigate the effects and the clinical significance of changing the geometry, boundary conditions, that is, muscle forces, and orthotropic material properties on the predictive outcome of an FEM of a human orbit. Forty-seven variables affecting the material properties, boundary conditions, and the geometry of an FEM of a human orbit including the globe were systematically changed, creating a number of FEMs of the orbit. The effects of the variations were quantified as differences in the principal strain magnitudes modeled by the original FEM (criterion standard), before the sensitivity analyses, and those generated by the changed FEMs. The material properties that had the biggest impact on the predicted principal strains were the shear moduli (up to 21%) and the absence of fatty tissue (up to 75%). The boundary condition properties that had the biggest impact on the predicted principal strains were the superior rectus muscle and canthal ligaments (up to 18% and 23%, respectively). Alterations to the geometry of the orbit, such as an increase in its volume, had the greatest effect on principal strain magnitudes (up to 52%). Changes in geometry, boundary conditions, and orthotropic material properties can induce significant changes in strain patterns. These values must therefore be chosen with care when using finite element modeling techniques. This study also highlights the importance of restoring the orbital fat and volume when reconstructing the orbital floor following a blunt injury. The possibility that the unrestored increase in the orbital volume and the resulting stresses may be a source of globe injuries, causing diplopia

  19. Photoelectron spectroscopy study on Li substituted NiO using PES beamline installed on Indus-1

    CERN Document Server

    Banerjee, A; Phase, D M; Dasannacharya, B A

    2003-01-01

    Photoelectron spectroscopy beamline based on a toroidal grating monochromator (TGM) is recently commissioned on Indus-1 storage ring. It has been used to carry out valence band photoemission study of Li substituted NiO. In this paper initially a brief description of the beamline components and the experimental station for angle integrated photoemission experiment is presented. The later part of this paper is devoted to studies carried out on Li sub x Ni sub 1 sub - sub x O with x=0.0, 0.35 and 0.5 samples. Thin pellets of polycrystalline samples were used for the measurements reported here. Valence band spectra recorded on polycrystalline Li sub x Ni sub 1 sub - sub x O samples show drastic changes in various features as compared to that of pure NiO. The prominent changes are: (i) change in the relative contributions of Ni-3d and O-2p emissions, (ii) change in the peak position of Ni-3d from the top of the valance band of NiO and (iii) no noticeable change in the Ni satellite peak. These results are evaluated...

  20. Monochromator development at 4W1B beamline of BSRF

    Science.gov (United States)

    Xie, Yaning; Yan, Y.; Hu, T. D.; Liu, T.; Xian, D. C.

    2001-07-01

    The 4W1B is a X-ray monochromator beamline for XAFS at BSRF. During the upgrading phase, we have redesigned the monochromator to improve the performance of the beamline. It is a goniometer based, fixed exit double crystal monochromator. A mechanical linkage is employed to adjust the distance between the surfaces of the two crystals as the Bragg angle is changed to keep the outgoing beam direction constant. The whole mechanism is driven by only one stepping motor. The testing result shows that over the scanning range of 5-30°, the shift of outgoing beam position is less then 70 μm in the vertical direction. The basic principle, the mechanical realization, and the error analysis are discussed in detail. The performance and the testing results are also presented in this paper.

  1. Advances on the Brazilian toroidal grating monochromator (TGM) beamline

    Energy Technology Data Exchange (ETDEWEB)

    Cavasso Filho, R.L. [Laboratorio Nacional de Luz Sincrotron, Box 6192, Campinas, SP 13084-971 (Brazil); Homem, M.G.P. [Laboratorio Nacional de Luz Sincrotron, Box 6192, Campinas, SP 13084-971 (Brazil); Landers, R. [Instituto de Fisica ' Gleb Wataghin' , Universidade Estadual de Campinas, Box 6165, Campinas, SP 13083-970 (Brazil); Naves de Brito, A. [Laboratorio Nacional de Luz Sincrotron, Box 6192, Campinas, SP 13084-971 (Brazil)]. E-mail: arnaldo@lnls.br

    2005-06-15

    We report on an important advance for the vacuum ultraviolet and soft X-ray TGM beamline at Laboratorio Nacional de Luz Sincrotron (LNLS). This beamline provides photons in the energy range 12-330 eV using three gratings. It is well known that TGMs deliver relatively high flux at these energies but harmonic contamination can be a serious problem. Of special interest for the users is the range between 12 and 21 eV covered by one of the gratings for studies of outer and inner valence ionization processes in gases as well as solids. Here, we report a solution to the harmonic contamination problems based on a noble gas phase filter combined with thin metal foil barriers.

  2. Elliptical multipole wiggler beamlines at the advanced photon source

    Energy Technology Data Exchange (ETDEWEB)

    Beno, M.A. E-mail: beno@anl.gov; Kurtz, C.; Munkholm, A.; Ruett, U.; Engbretson, M.; Jennings, G.; Linton, J.; Knapp, G.S.; Montano, P.A

    2001-07-21

    The Basic Energy Sciences Synchrotron Radiation Center Collaborative Access Team has built three independent beamlines, which simultaneously utilize the X-ray radiation from an elliptical multipole wiggler, located at Sector 11 of the Advanced Photon Source. This insertion device produces circularly polarized X-rays on-axis and linearly polarized X-rays above and below the ring plane. The lower linearly polarized radiation is used in the monochromatic 11ID-D station for scattering and spectroscopy experiments in the 5-40 keV range. The on-axis circularly polarized photons are used for magnetic Compton scattering experiments in the 11ID-B station. The upper linearly polarized radiation is utilized by the high-energy diffraction station, 11ID-C. We report here on the beamline optics and experimental station equipment.

  3. Low-dose, high-resolution and high-efficiency ptychography at STXM beamline of SSRF

    Science.gov (United States)

    Xu, Zijian; Wang, Chunpeng; Liu, Haigang; Tao, Xulei; Tai, Renzhong

    2017-06-01

    Ptychography is a diffraction-based X-ray microscopy method that can image extended samples quantitatively while remove the resolution limit imposed by image-forming optical elements. As a natural extension of scanning transmission X-ray microscopy (STXM) imaging method, we developed soft X-ray ptychographic coherent diffraction imaging (PCDI) method at the STXM endstation of BL08U beamline of Shanghai Synchrotron Radiation Facility. Compared to the traditional STXM imaging, the new PCDI method has resulted in significantly lower dose, higher resolution and higher efficiency imaging in our platform. In the demonstration experiments shown here, a spatial resolution of sub-10 nm was obtained for a gold nanowires sample, which is much better than the limit resolution 30 nm of the STXM method, while the radiation dose is only 1/12 of STXM.

  4. Stress distribution in the temporomandibular joint after mandibular protraction: a 3-dimensional finite element method study. Part 1.

    Science.gov (United States)

    Gupta, Anurag; Kohli, Virender S; Hazarey, Pushpa V; Kharbanda, Om P; Gunjal, Amit

    2009-06-01

    This study was designed to evaluate patterns of stress generation in the temporomandibular joint after mandibular protraction, by using a 3-dimensional finite element method. The results of the initial investigation are reported here in Part 1. The effects of varying the construction bite are reported in Part 2. A 3-dimensional computer-aided design model was developed from the magnetic resonance images of a growing boy (age, 12 years), by using I-DEAS NX (version 11.0, Siemens PLM Software, Plano, Tex). The model simulated mandibular protraction, with 5 mm of sagittal advancement and 4 mm of vertical opening. Stress distributions on the condylar neck, the glenoid fossa, and the articular disc in the anteroposterior and mediolateral directions were assessed. Tensile stresses were located on the posterosuperior aspects and compressive stresses on the anterior and anterosuperior aspects of the condylar head. Tensile stresses were found in the posterior region of the glenoid fossa near the attachment of the posterior connective tissues. These results suggest that, on mandibular protraction, the mandibular condyle experiences tensile stresses in the posterosuperior aspect that might help explain condylar growth in this direction. Similarly, on the glenoid fossa, tensile stresses are created in the region of posterior connective tissues; this might be correlated with the increased cellular activity in this region. Further study with variable vertical heights of the construction bites is needed.

  5. Successful test of SPS-to-LHC beamline

    CERN Multimedia

    Maximilien Brice

    2004-01-01

    On 23 October there was great excitement in the Prevessin control room when, on the first attempt, a beam passed over 2.5 km down the new SPS-to-LHC transfer line, TI8, to within a few metres of the LHC tunnel. Members of the AB, AT and TS departments involved in the beamline and its test, celebrate their success with the Director General, Robert Aymar, and the LHC Project Leader, Lyn Evans.

  6. Successful test of SPS-to-LHC beamline

    CERN Multimedia

    2004-01-01

    On 23 October there was great excitement in the Prevessin control room when, on the first attempt, a beam passed over 2.5 km down the new SPS-to-LHC transfer line, TI8, to within a few metres of the LHC tunnel. Above: members of the AB, AT and TS departments involved in the beamline and its test, celebrate their success with the Director General, Robert Aymar, and the LHC Project Leader, Lyn Evans.

  7. Surface science station of the infrared beamline at SPring-8

    CERN Document Server

    Sakurai, M; Kimura, H; Nishida, S; Nanba, T

    2001-01-01

    An experimental station for surface science has been constructed at the infrared beamline (BL43IR) of SPring-8, Japan. The station utilizes synchrotron radiation in the energy range of 100-20000 cm sup - sup 1 to perform infrared reflection absorption spectroscopy (IRAS) of surfaces. It consists of an experimental section, a preparation chamber, gas handling equipment and a pair of focusing optics. In situ observation of vibrational spectra is possible using both IRAS and high-resolution electron energy loss spectroscopy.

  8. Solvent Refined Coal (SRC) process: trace elements. Volume III. Pilot plant development work. Part 6. Fate of trace elements in the SRC process. [Ph. D. Thesis

    Energy Technology Data Exchange (ETDEWEB)

    Weiss, C.S.

    1980-09-01

    A study of the forms of trace elements occurring in Solvent Refined Coal has been performed by chemical separation of the Solvent Refined Coal based on differences in the functionality and molecular weight of the organic matrix. Analysis of the fractions separated for various trace elements has revealed associations of certain elements with other elements as well as with certain fractions. The analysis of Solvent Refined Coal I by these methods provided data on the distribution of Ti, V, Ca, S, Al, Mn, As, Se, Cr, Fe, Ni, Zn, Sc, and Ga in the fractions generated. Because of the low trace element content of Solvent Refined Coal II only As, Se, and Cr could be detected in the silica fractions. Based on the distributions three different groups of elements have been based on the association of elements with each other and with certain fractions. The first group is composed of As, Se, and Cr associated with silica fractions of relatively low functionality; these elements have a high percent solubility in the starting Solvent Refined Coal II oil. The second group composed of Ti, V, and to a lesser extent a second form of Cr, is associated with fractions that have a high concentration of phenolic material and is probably present as phenoxide complexes. The third group composed of Fe, Ca, K, Al, and Mg is associated with the most functional fractions and is possibly present as humic acid type complexes or as submicron size particulates. The integration of chromatographic methods with trace element analysis of the fractions generated is capable of discerning the presence of different forms of the elements. The methods used are applicable to other important geologically occurring organic matter.

  9. Design and simulation of the nuSTORM pion beamline

    Energy Technology Data Exchange (ETDEWEB)

    Liu, A., E-mail: aoliu@fnal.gov; Neuffer, D.; Bross, A.

    2015-11-21

    The nuSTORM (neutrinos from STORed Muons) proposal presents a detailed design for a neutrino facility based on a muon storage ring, with muon decay in the production straight section of the ring providing well defined neutrino beams. The facility includes a primary high-energy proton beam line, a target station with pion production and collection, and a pion beamline for pion transportation and injection into a muon decay ring. The nuSTORM design uses “stochastic injection”, in which pions are directed by a chicane, referred to as the Orbit Combination Section (OCS), into the production straight section of the storage ring. Pions that decay within that straight section provide muons within the circulating acceptance of the ring. The design enables injection without kickers or a separate pion decay transport line. The beam line that the pions traverse before being extracted from the decay ring is referred to as the pion beamline. This paper describes the design and simulation of the pion beamline, and includes full beam dynamics simulations of the system.

  10. New fast closing shutter for the PETRA III beamlines

    Science.gov (United States)

    Hahn, U.; Hesse, M.; Müller, S.; Peters, H.-B.; Timmann, B.; Wengler, R.; Zink, H.

    2008-03-01

    The conversion of the PETRA storage ring at the Deutsches Elektronen Synchrotron (DESY) to the third generation synchrotron radiation light source PETRAIII [1] poses a challenge to the design of the beamline transport system. One of these challenges is to supply 14 beamlines and experiments windowless with the extremely collimated undulator radiation from the storage ring. The windowless connection includes the risk of accidental venting of the storage ring by experiments connected to the beamlines. To stop the inrush of such an accidental venting fast closing shutter (FCS) systems with closing times in the 10msec range are mandatory. The strong radiation background in the storage ring tunnel requires the installation of all metal valves. A new small fast closing shutter with an aperture of 40mm fitting to the strong collimated undulator beams and with a closing time beam time losses for all users. The mechanical and electronic layouts as well as first experiences with the new fast closing shutter system developed for PETRAIII are presented.

  11. Performance of a novel VUV bending magnet beamline

    CERN Document Server

    Song, Y F; Hsieh, T F; Huang, L R; Chung, S C; Cheng, N F; Hsiung, G Y; Wang, D J; Chen, C T; Tsang, K L

    2001-01-01

    A novel high resolution, high flux bending magnet beamline with an energy range from 5 to 40 eV has been constructed at SRRC. This Dragon-like beamline, which horizontally collects 50 mrad of synchrotron radiation from a bending magnet source, uses four cylindrical gratings with an included angle of 140 deg. and a movable curved exit slit. The average photon flux with an energy resolving power of 1000 is about 2x10 sup 1 sup 2 photons/s, which is among the highest of all existing VUV bending magnet beamlines. An energy resolving power of 24,000 at 6.8 eV has been obtained from the Schumann-Runge bands (B sup 3 limit construction operator in a limit construction/sum L: summation operator operator End lower limit of a limit construction u lower limit End limit End sup - /leftarrow/gets A: =leftward arrow X sup 3 limit construction operator in a limit construction/sum L: summation operator operator End lower limit of a limit construction g lower limit End limit End sup -) absorption spectra of O sub 2 gas. A pho...

  12. Pulsed beam tests at the SANAEM RFQ beamline

    Science.gov (United States)

    Turemen, G.; Akgun, Y.; Alacakir, A.; Kilic, I.; Yasatekin, B.; Ergenlik, E.; Ogur, S.; Sunar, E.; Yildiz, V.; Ahiska, F.; Cicek, E.; Unel, G.

    2017-07-01

    A proton beamline consisting of an inductively coupled plasma (ICP) source, two solenoid magnets, two steerer magnets and a radio frequency quadrupole (RFQ) is developed at the Turkish Atomic Energy Authority’s (TAEA) Saraykoy Nuclear Research and Training Center (SNRTC-SANAEM) in Ankara. In Q4 of 2016, the RFQ was installed in the beamline. The high power tests of the RF power supply and the RF transmission line were done successfully. The high power RF conditioning of the RFQ was performed recently. The 13.56 MHz ICP source was tested in two different conditions, CW and pulsed. The characterization of the proton beam was done with ACCTs, Faraday cups and a pepper-pot emittance meter. Beam transverse emittance was measured in between the two solenoids of the LEBT. The measured beam is then reconstructed at the entrance of the RFQ by using computer simulations to determine the optimum solenoid currents for acceptance matching of the beam. This paper will introduce the pulsed beam test results at the SANAEM RFQ beamline. In addition, the high power RF conditioning of the RFQ will be discussed.

  13. Advanced light source vacuum policy and vacuum guidelines for beamlines and experiment endstations

    Energy Technology Data Exchange (ETDEWEB)

    Hussain, Z.

    1995-08-01

    The purpose of this document is to: (1) Explain the ALS vacuum policy and specifications for beamlines and experiment endstations. (2) Provide guidelines related to ALS vacuum policy to assist in designing beamlines which are in accordance with ALS vacuum policy. This document supersedes LSBL-116. The Advanced Light Source is a third generation synchrotron radiation source whose beam lifetime depends on the quality of the vacuum in the storage ring and the connecting beamlines. The storage ring and most of the beamlines share a common vacuum and are operated under ultra-high-vacuum (UHV) conditions. All endstations and beamline equipment must be operated so as to avoid contamination of beamline components, and must include proper safeguards to protect the storage ring vacuum from an accidental break in the beamline or endstation vacuum systems. The primary gas load during operation is due to thermal desorption and electron/photon induced desorption of contaminants from the interior of the vacuum vessel and its components. The desorption rates are considerably higher for hydrocarbon contamination, thus considerable emphasis is placed on eliminating these sources of contaminants. All vacuum components in a beamline and endstation must meet the ALS vacuum specifications. The vacuum design of both beamlines and endstations must be approved by the ALS Beamline Review Committee (BRC) before vacuum connections to the storage ring are made. The vacuum design is first checked during the Beamline Design Review (BDR) held before construction of the beamline equipment begins. Any deviation from the ALS vacuum specifications must be approved by the BRC prior to installation of the equipment on the ALS floor. Any modification that is incorporated into a vacuum assembly without the written approval of the BRC is done at the user`s risk and may lead to rejection of the whole assembly.

  14. Advanced light source vacuum policy and vacuum guidelines for beamlines and experiment endstations

    Energy Technology Data Exchange (ETDEWEB)

    Hussain, Z.

    1995-08-01

    The purpose of this document is to: (1) Explain the ALS vacuum policy and specifications for beamlines and experiment endstations. (2) Provide guidelines related to ALS vacuum policy to assist in designing beamlines which are in accordance with ALS vacuum policy. This document supersedes LSBL-116. The Advanced Light Source is a third generation synchrotron radiation source whose beam lifetime depends on the quality of the vacuum in the storage ring and the connecting beamlines. The storage ring and most of the beamlines share a common vacuum and are operated under ultra-high-vacuum (UHV) conditions. All endstations and beamline equipment must be operated so as to avoid contamination of beamline components, and must include proper safeguards to protect the storage ring vacuum from an accidental break in the beamline or endstation vacuum systems. The primary gas load during operation is due to thermal desorption and electron/photon induced desorption of contaminants from the interior of the vacuum vessel and its components. The desorption rates are considerably higher for hydrocarbon contamination, thus considerable emphasis is placed on eliminating these sources of contaminants. All vacuum components in a beamline and endstation must meet the ALS vacuum specifications. The vacuum design of both beamlines and endstations must be approved by the ALS Beamline Review Committee (BRC) before vacuum connections to the storage ring are made. The vacuum design is first checked during the Beamline Design Review (BDR) held before construction of the beamline equipment begins. Any deviation from the ALS vacuum specifications must be approved by the BRC prior to installation of the equipment on the ALS floor. Any modification that is incorporated into a vacuum assembly without the written approval of the BRC is done at the user`s risk and may lead to rejection of the whole assembly.

  15. Wavefront propagation through the beamline designed for seeding the DESY XUV FEL

    CERN Document Server

    Reininger, R; Gürtler, P; Bahrdt, J

    2001-01-01

    A beamline designed to reduce the spectral bandwidth of the DESY XUV FEL is described. The beamline is intended to cover the wavelength range from 6.4 to 50 nm with three variable line spacing gratings. A plane mirror in front of the grating is used to maintain constant magnification in the dispersion direction. The electric field generated by the first undulator at three wavelengths, 6.4, 13, and 25 nm, is propagated through the beamline. The results show that the beamline has the resolution and imaging properties required for seeding the second undulator at these wavelengths.

  16. HERMES: a soft X-ray beamline dedicated to X-ray microscopy.

    Science.gov (United States)

    Belkhou, Rachid; Stanescu, Stefan; Swaraj, Sufal; Besson, Adrien; Ledoux, Milena; Hajlaoui, Mahdi; Dalle, Didier

    2015-07-01

    The HERMES beamline (High Efficiency and Resolution beamline dedicated to X-ray Microscopy and Electron Spectroscopy), built at Synchrotron SOLEIL (Saint-Auban, France), is dedicated to soft X-ray microscopy. The beamline combines two complementary microscopy methods: XPEEM (X-ray Photo Emitted Electron Microscopy) and STXM (Scanning Transmission X-ray Microscopy) with an aim to reach spatial resolution below 20 nm and to fully exploit the local spectroscopic capabilities of the two microscopes. The availability of the two methods within the same beamline enables the users to select the appropriate approach to study their specific case in terms of sample environment, spectroscopy methods, probing depth etc. In this paper a general description of the beamline and its design are presented. The performance and specifications of the beamline will be reviewed in detail. Moreover, the article is aiming to demonstrate how the beamline performances have been specifically optimized to fulfill the specific requirements of a soft X-ray microscopy beamline in terms of flux, resolution, beam size etc. Special attention has been dedicated to overcome some limiting and hindering problems that are usually encountered on soft X-ray beamlines such as carbon contamination, thermal stability and spectral purity.

  17. A high-precision cryogenically-cooled crystal monochromator for the APS diagnostics beamline

    Energy Technology Data Exchange (ETDEWEB)

    Rotela, E.; Yang, B.; Sharma, s.; Barcikowski, A.

    2000-07-24

    A high-precision cryogenically-cooled crystal monochromator has been developed for the APS diagnostics beamline. The design permits simultaneous measurements of the particle beam size and divergence. It provides for a large rotation angle, {minus}15{degree} to 180{degree}, with a resolution of 0.0005{degree}. The roll angle of the crystal can be adjusted by up to {+-}3{degree} with a resolution of 0.0001{degree}. A vertical translational stage, with a stroke of {+-}25 mm and resolution of 8 {micro}m, is provided to enable using different parts of the same crystal or to retract the crystal from the beam path. The modular design will allow optimization of cooling schemes to minimize thermal distortions of the crystal under high heat loads.

  18. MX1: a bending-magnet crystallography beamline serving both chemical and macromolecular crystallography communities at the Australian Synchrotron

    Energy Technology Data Exchange (ETDEWEB)

    Cowieson, Nathan Philip; Aragao, David; Clift, Mark; Ericsson, Daniel J.; Gee, Christine; Harrop, Stephen J.; Mudie, Nathan; Panjikar, Santosh; Price, Jason R.; Riboldi-Tunnicliffe, Alan; Williamson, Rachel; Caradoc-Davies, Tom, E-mail: tom.caradoc-davies@synchrotron.org.au [Australian Synchrotron, 800 Blackburn Road, Clayton, Victoria 3168 (Australia)

    2015-01-01

    The macromolecular crystallography beamline MX1 at the Australian Synchrotron is described. MX1 is a bending-magnet crystallography beamline at the 3 GeV Australian Synchrotron. The beamline delivers hard X-rays in the energy range from 8 to 18 keV to a focal spot at the sample position of 120 µm FWHM. The beamline endstation and ancillary equipment facilitate local and remote access for both chemical and biological macromolecular crystallography. Here, the design of the beamline and endstation are discussed. The beamline has enjoyed a full user program for the last seven years and scientific highlights from the user program are also presented.

  19. A finite element modelling methodology for the non-linear stiffness evaluation of adhesively bonded single lap-joints. Part 2, Novel shell mesh to minimise analysis time

    OpenAIRE

    Pearson, Ian T.; Mottram, J. Toby

    2012-01-01

    A new modelling methodology is presented that enables the stiffness of adhesively bonded single lap-joints to be included in the finite element analysis of whole vehicle bodies. This work was driven by the need to significantly reduce computing resources for vehicle analysis. To achieve this goal the adhesive bond line and adherends are modelled by a relatively ‘small’ number of shell elements to replace the usual solid element mesh for a reliable analysis. Previous work in Part 1 has provide...

  20. Development of nano structured diamond windows for application in synchrotron beamlines

    Energy Technology Data Exchange (ETDEWEB)

    Campos, R.A.; Trava-Airoldi, V.J.; Corat, E.J. [Instituto Nacional de Pesquisas Espaciais (INPE), Sao Jose dos Campos, SP (Brazil); Bagnato, O.R. [Laboratorio Nacional de Luz Sincroton (LNLS), Campinas, SP (Brazil); Moro, J.R. [Instituto Federal de Educacao, Ciencia e Tecnologia de Sao Paulo (IFSP), SP (Brazil)

    2011-07-01

    Full text. Synchrotron light sources are important tools in the scientific field. In essence, they are rather like enormous super-microscopes capable of studying biological, chemical and material samples at very high resolution, down to the atomic and molecular level, by using synchrotron light. The intense synchrotron light is electromagnetic radiation produced by high-energy electrons in a particle accelerator. The configuration of the beamlines uses windows of material transparent to radiation. Beryllium (Be) is the standard material. In general, these windows serve both, as filters to absorb the photons of low energy and, as insulating barrier between the storage ring and the environment. The justification for the use of beryllium windows at synchrotron beamlines is that elements with low atomic number - (4) transmit more electromagnetic radiation. Besides all the qualities, beryllium has some drawbacks such as deterioration of spatial coherence due to surface roughness and defects. Another problem observed is the appearance of Fresnel diffraction due to manufacturing defects of the windows. In this paper, we propose the use of windows made of nano structured diamond with average roughness of 20nm, without the need to polish, with maximum thickness of around 3 {mu}m. Diamond also has a low atomic number - (6). Another quality of nano structured diamond films is its mechanical properties. It needs only 5-6% of the thickness of beryllium to withstand the same pressure gradient. The film morphology was characterized with the help of Atomic Force Microscopy (AFM) and Scanning Electron Microscopy (SEM-FEG). Diamond's quality was determined by Raman Spectroscopy

  1. Preliminary design of multi-function LIGA beamline

    Institute of Scientific and Technical Information of China (English)

    2006-01-01

    One design of multi-function LIGA beamline has been reported. In this design, two plane mirrors and a series of filters have been employed. One can choose the spectrum range of X-ray easily according to the exposure requirement by adjusting the grazing angle of mirrors and the thickness of filters. And the spot size in the horizontal direction is up to 120mm, which is large enough for exposing 5 inch silicon slice. The typical exposure time is about 1.2h, 1.8h, 0.5h, corresponding to PMMA thickness of 500 μ m, 200 μ m, 20 t m, respectively.

  2. Microfocusing at the PG1 beamline at FLASH

    Energy Technology Data Exchange (ETDEWEB)

    Dziarzhytski, Siarhei, E-mail: siarhei.dziarzhytski@desy.de [DESY, Notkestrasse 85, 22067 Hamburg (Germany); Gerasimova, Natalia [European XFEL GmbH, Albert-Einstein-Ring 19, 22761 Hamburg (Germany); Goderich, Rene [University of South Florida (United States); Mey, Tobias [Laser Laboratorium Göttingen eV, Hans-Adolf-Krebs-Weg 1, 37077 Göttingen (Germany); Reininger, Ruben [Advanced Photon Source, Argonne National Laboratory, Argonne, IL 60439 (United States); Rübhausen, Michael [University of Hamburg and Center for Free-Electron Laser Science, Notkestrasse 85, 22607 Hamburg (Germany); Siewert, Frank [Institute for Nanometre Optics and Technology at Helmholtz Zentrum Berlin/BESSY II, Albert-Einstein-Strasse 15, 12489 Berlin (Germany); Weigelt, Holger; Brenner, Günter [DESY, Notkestrasse 85, 22067 Hamburg (Germany)

    2016-01-01

    The Kirkpatrick–Baez (KB) refocusing mirrors unit at the PG1 beamline at FLASH has been newly designed, developed and fully commissioned. The vertical focal size of the KB optics is measured to be 5.8 ± 1 µm FWHM and the horizontal 6 ± 2 µm FWHM; astigmatism has been minimized to below 1 mm between waist positions. Such a tight focus is essential for the VUV double Raman spectrometer as it serves as an entrance slit for the first monochromator and defines its resolution to a very large extent. The Raman spectrometer is a permanent end-station at the PG1 beamline, dedicated to inelastic soft X-ray scattering experiments. The Kirkpatrick–Baez (KB) refocusing mirror system installed at the PG1 branch of the plane-grating monochromator beamline at the soft X-ray/XUV free-electron laser in Hamburg (FLASH) is designed to provide tight aberration-free focusing down to 4 µm × 6 µm full width at half-maximum (FWHM) on the sample. Such a focal spot size is mandatory to achieve ultimate resolution and to guarantee best performance of the vacuum-ultraviolet (VUV) off-axis parabolic double-monochromator Raman spectrometer permanently installed at the PG1 beamline as an experimental end-station. The vertical beam size on the sample of the Raman spectrometer, which operates without entrance slit, defines and limits the energy resolution of the instrument which has an unprecedented design value of 2 meV for photon energies below 70 eV and about 15 meV for higher energies up to 200 eV. In order to reach the designed focal spot size of 4 µm FWHM (vertically) and to hold the highest spectrometer resolution, special fully motorized in-vacuum manipulators for the KB mirror holders have been developed and the optics have been aligned employing wavefront-sensing techniques as well as ablative imprints analysis. Aberrations like astigmatism were minimized. In this article the design and layout of the KB mirror manipulators, the alignment procedure as well as microfocus

  3. The polariser beamline at TRIUMF for nuclear structure physics

    Science.gov (United States)

    Voss, A.; Pearson, M. R.; Levy, C. D. P.; Billowes, J.; Buchinger, F.; Chow, K. H.; Crawford, J. E.; Hossein, M. D.; Kiefl, R. F.; Macfarlane, W. A.; Mané, E.; Morris, G. D.; Parolin, T. J.; Saadaoui, H.; Salman, Z.; Shelbaya, O. T. J.; Smadella, M.; Song, Q.; Wang, D.

    2011-10-01

    Originally built to provide polarised ion beams for condensed matter experiments, the polariser beamline at TRIUMF is coupled to both beta-NMR and beta-NQR spectrometers. In addition, the beam can be passed through a radio-frequency quadrupole cooler and buncher (RFQ) providing bunched beams. Recently, a laser spectroscopy and beta-NQR program was started to investigate the ground state structure of exotic nuclei. Results from recent experiments including zero-field beta-NQR studies to determine the quadrupole moment of the halo nucleus Li-11 and laser spectroscopy to determine the charge radius of Rb-74.

  4. Mixed and Penalty Finite Element Models for the Nonlinear Behavior of Biphasic Soft Tissues in Finite Deformation: Part II - Nonlinear Examples.

    Science.gov (United States)

    Almeida, EDGARD S.; Spilker, ROBERT L.

    1998-01-01

    This two-part paper addresses finite element-based computational models for the three-dimensional (3-D) nonlinear analysis of soft hydrated tissues, such as articular cartilage in diarthrodial joints, under physiologically relevant loading conditions. A biphasic continuum description is used to represent the soft tissue as a two-phase mixture of incompressible inviscid fluid and a hyperelastic, transversely isotropic solid. Alternate mixed-penalty and velocity-pressure finite element formulations are used to solve the nonlinear biphasic governing equations, including the effects of strain-dependent permeability and a hyperelastic solid phase under finite deformation. The resulting first-order, nonlinear system of equations is discretized in time using an implicit finite difference scheme, and solved using the Newton-Raphson method. Details of the formulations were presented in Part I [1]. In Part II, the two formulations are used to develop two-dimensional (2-D) quadrilateral and triangular elements and three-dimensional (3-D) hexahedral and tetrahedral elements. Numerical examples, including those representative of soft tissue material testing and simple human joints, are used to validate the formulations and to illustrate their applications. A focus of this work is the comparison of the alternate formulations for nonlinear problems. While it is demonstrated that both formulations produce a range of converging elements, the velocity-pressure formulation is found to be more efficient computationally.

  5. Plastique: A synchrotron radiation beamline for time resolved fluorescence in the frequency domain

    Science.gov (United States)

    De Stasio, Gelsomina; Zema, N.; Antonangeli, F.; Savoia, A.; Parasassi, T.; Rosato, N.

    1991-06-01

    PLASTIQUE is the only synchrotron radiation beamline in the world that performs time resolved fluorescence experiments in frequency domain. These experiments are extremely valuable sources of information on the structure and dynamics of molecules. We describe the beamline and some initial data.

  6. CERN announces the fourth annual Beamline for Schools competition

    CERN Multimedia

    BL4S team

    2016-01-01

    CERN is pleased to announce the fourth annual Beamline for Schools (BL4S) competition. Once again, in 2017, a fully equipped beamline will be made available at CERN for students. As in previous years, two teams will be invited to the Laboratory to execute the experiments they proposed in their applications. The 2017 competition is being made possible thanks to support from the Alcoa Foundation for the second consecutive year.   The competition is open to teams of high-school students aged 16 or older who, if they win, are invited (with two supervisors) to CERN to carry out their experiment. Teams must have at least five students but there is no upper limit to a team’s size (although just nine students per winning team will be invited to CERN). Teams may be composed of pupils from a single school, or from a number of schools working together. As science-loving mega-celebrity Will.I.Am told us: “If you’re interested in science, technology, engineering or ...

  7. Dedicated Beamline Facilities for Catalytic Research. Synchrotron Catalysis Consortium (SCC)

    Energy Technology Data Exchange (ETDEWEB)

    Chen, Jingguang [Columbia Univ., New York, NY; Frenkel, Anatoly [Yeshiva Univ., New York, NY (United States); Rodriguez, Jose [Brookhaven National Lab. (BNL), Upton, NY (United States); Adzic, Radoslav [Brookhaven National Lab. (BNL), Upton, NY (United States); Bare, Simon R. [UOP LLC, Des Plaines, IL (United States); Hulbert, Steve L. [Brookhaven National Lab. (BNL), Upton, NY (United States); Karim, Ayman [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Mullins, David R. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Overbury, Steve [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

    2015-03-04

    Synchrotron spectroscopies offer unique advantages over conventional techniques, including higher detection sensitivity and molecular specificity, faster detection rate, and more in-depth information regarding the structural, electronic and catalytic properties under in-situ reaction conditions. Despite these advantages, synchrotron techniques are often underutilized or unexplored by the catalysis community due to various perceived and real barriers, which will be addressed in the current proposal. Since its establishment in 2005, the Synchrotron Catalysis Consortium (SCC) has coordinated significant efforts to promote the utilization of cutting-edge catalytic research under in-situ conditions. The purpose of the current renewal proposal is aimed to provide assistance, and to develop new sciences/techniques, for the catalysis community through the following concerted efforts: Coordinating the implementation of a suite of beamlines for catalysis studies at the new NSLS-II synchrotron source; Providing assistance and coordination for catalysis users at an SSRL catalysis beamline during the initial period of NSLS to NSLS II transition; Designing in-situ reactors for a variety of catalytic and electrocatalytic studies; Assisting experimental set-up and data analysis by a dedicated research scientist; Offering training courses and help sessions by the PIs and co-PIs.

  8. Status of the ELIMED Beamline at the ELIMAIA facility

    Science.gov (United States)

    Schillaci, F.; Cirrone, G. A. P.; Cuttone, G.; Romano, F.; Scuderi, V.; Allegra, L.; Amato, A.; Andó, L.; Costa, M.; Gallo, G.; Leanza, R.; Maggiore, M.; Milluzzo, G.; Petringa, G.; Pipek, J.; Russo, A. D.; Korn, G.; Margarone, D.; Leray, M. J.; Tasset-Maye, O.; Antoine, S.; Jehanno, P.

    2016-12-01

    Laser-target acceleration represents a very promising alternative to conventional accelerators for several potential applications, from the nuclear physics to the medical ones. However, some extreme features, not suitable for multidisciplinary applications, as the wide energy and angular spreads, characterize optically accelerated ion beams. Therefore, beyond the improvements at the laser-target interaction level, a lot of efforts have been recently devoted to the development of specific beam-transport devices in order to obtain controlled and reproducible output beams. In this framework, a three years contract has been signed between the INFN-LNS (IT) and Eli-Beamlines-IoP (CZ) to provide the design and the realization of a complete transport beam-line, named ELIMED, dedicated to the transport, diagnostics and dosimetry of laser-driven ion beams. The transport devices will be composed by a set of super-strong permanent magnet quadrupoles able to collect and focus laser driven ions up to 70 MeV/u, and a magnetic chicane made of conventional electromagnetic dipoles to select particles within a narrow energy range. Here, the actual status of the design and development of these magnetic systems is described.

  9. In situ beamline analysis and correction of active optics.

    Science.gov (United States)

    Sutter, John; Alcock, Simon; Sawhney, Kawal

    2012-11-01

    At the Diamond Light Source, pencil-beam measurements have enabled long-wavelength slope errors on X-ray mirror surfaces to be examined under ultra-high vacuum and beamline mounting without the need to remove the mirror from the beamline. For an active mirror an automated procedure has been implemented to calculate the actuator settings that optimize its figure. More recently, this in situ pencil-beam method has been applied to additional uses for which ex situ measurements would be inconvenient or simply impossible. First, it has been used to check the stability of the slope errors of several bimorph mirrors at intervals of several weeks or months. Then, it also proved useful for the adjustment of bender and sag compensation actuators on mechanically bent mirrors. Fits to the bending of ideal beams have been performed on the slope errors of a mechanically bent mirror in order to distinguish curvatures introduced by the bending actuators from gravitational distortion. Application of the optimization procedure to another mechanically bent mirror led to an improvement of its sag compensation mechanism.

  10. Design and R&D for manufacturing the beamline components of MITICA and ITER HNBs

    Energy Technology Data Exchange (ETDEWEB)

    Dalla Palma, M., E-mail: mauro.dallapalma@igi.cnr.it [Consorzio RFX, Padova (Italy); Sartori, E. [Consorzio RFX, Padova (Italy); Blatchford, P.; Chuilon, B. [CCFE, Culham Science Centre, Oxfordshire (United Kingdom); Graceffa, J. [ITER Organization, St Paul Lez Durance (France); Hanke, S. [KIT, Institute for Technical Physics, Eggenstein-Leopoldshafen (Germany); Hardie, C. [CCFE, Culham Science Centre, Oxfordshire (United Kingdom); Masiello, A. [F4E, Barcelona (Spain); Muraro, A. [Consorzio RFX, Padova (Italy); Ochoa, S. [KIT, Institute for Technical Physics, Eggenstein-Leopoldshafen (Germany); Shah, D. [ITER Organization, St Paul Lez Durance (France); Veltri, P.; Zaccaria, P.; Zaupa, M. [Consorzio RFX, Padova (Italy)

    2015-10-15

    Highlights: • Particle beam-component interaction was analysed developing and applying numerical codes. • Gas density distribution was calculated with AVOCADO code and applied for electrical analyses. • High heat flux components were designed, analysed with subcooled boiling, verified for fatigue. • Fracture behaviour of ceramics was analysed by finite element modelling and was verified. • R&D supports the design of the beamline components, especially for water-vacuum barriers. - Abstract: The design of the beamline components of MITICA, the full prototype of the ITER heating neutral beam injectors, is almost finalised and technical specifications for the procurement are under preparation. These components are the gas neutraliser, the electrostatic residual ion dump, and the calorimeter. Electron dump panels are foreseen each side of the upstream end of the neutraliser to protect the cryo-panels from electrons, created by stripping and other processes, that exit the 1 MeV accelerator. As the design of the components must fulfil requirements on the beam physics, insight on physical processes is required to identify performance trade-offs and constraints. The spatial gas distribution was simulated to verify the pumping requirements with electron dump panels and local conditions for breakdown voltage. Electrostatic analyses were carried out for the insulating elements of the RID to verify the limits of the electric field intensity. Different criteria were approached to investigate the fracture behaviour of ceramics considering the manufacturing implications and extrapolating the conditions for proof testing. Severe heating conditions will be applied steadily, as the maximum pulse duration is 1 h, and cyclically so requiring to fulfil fatigue and ratcheting verifications. High heat fluxes, up to 13 MW/m{sup 2} on the calorimeter, with enhanced heat transfer in subcooled boiling conditions will occur in the actively cooled CuCr1Zr panel elements provided with

  11. Commissioning and first results of scanning type EXAFS beamline (BL-09) at INDUS-2 synchrotron source

    Energy Technology Data Exchange (ETDEWEB)

    Poswal, A. K., E-mail: poswalashwini@gmail.com; Agrawal, A., E-mail: poswalashwini@gmail.com; Yadav, A. K., E-mail: poswalashwini@gmail.com; Nayak, C., E-mail: poswalashwini@gmail.com; Basu, S., E-mail: poswalashwini@gmail.com; Bhattachryya, D.; Jha, S. N.; Sahoo, N. K. [Atomic and Molecular Physics Division, Bhabha Atomic Research Centre, Mumbai -400085 (India); Kane, S. R.; Garg, C. K. [Indus Synchrotrons Utilization Division, Raja Ramanna Centre for Advanced Technology, Indore- 452013 (India)

    2014-04-24

    An Energy Scanning X-ray Absorption Fine Structure spectroscopy beamline has recently been installed and commissioned at BL-09 bending magnet port of INDUS-2 synchrotron source, Indore. The beamline uses an UHV compatible fixed exit double crystal monochromator (DCM) with two Si (111) crystals. Two grazing incidence cylindrical mirrors are also used in this beamline; the pre-mirror is used as a collimating mirror while the post mirror is used for vertical focusing and higher harmonic rejection. In this beamline it is possible to carry out EXAFS measurements both in transmission and fluorescence mode on various types of samples, using Ionization chamber detectors and solid state drift detector respectively. In this paper, results from first experiments of the Energy Scanning EXAFS beamline are presented.

  12. Performance of beamline 9.3.1 at the ALS: Flux and resolution measurements

    Energy Technology Data Exchange (ETDEWEB)

    Uehara, Y. [Univ. of Nevada, Las Vegas, NV (United States); Fischer, G.; Kring, J.; Perera, R.C.C. [Ernest Orlando Lawrence Berkeley National Lab., CA (United States)

    1997-04-01

    Beamline 9.3.1 at the ALS is a windowless beamline, covering the 1-6 keV photon-energy range. This beamline is the first monochromatic hard x-ray beamline in the ALS, and designed to achieve the goals of high energy resolution, and preservation of the high brightness from the ALS. It consists of a new {open_quotes}Cowan type{close_quotes} double-crystal monochromator and two toroidal mirrors which are positioned before and after the monochromator. The construction of the beamline was completed in December of 1995, with imperfect mirrors. In this report, the authors describe the experimental results of absolute flux measurements and x-ray absorption measurements of gases and solid samples using the present set of mirrors.

  13. Performance and capabilities of the Canadian Dragon: The SGM beamline at the Canadian Light Source

    Energy Technology Data Exchange (ETDEWEB)

    Regier, T. [Canadian Light Source, Inc. (CLSI), University of Saskatchewan, Saskatoon, SK (Canada)], E-mail: tom.regier@lightsource.ca; Krochak, J. [Canadian Light Source, Inc. (CLSI), University of Saskatchewan, Saskatoon, SK (Canada); Sham, T.K. [Department of Chemistry, University of Western Ontario, London, ON (Canada); Hu, Y.F. [Canadian Light Source, Inc. (CLSI), University of Saskatchewan, Saskatoon, SK (Canada); Thompson, J. [Department of Chemistry, University of Western Ontario, London, ON (Canada); Blyth, R.I.R. [Canadian Light Source, Inc.(CLSI), University of Saskatchewan, Saskatoon, SK (Canada)

    2007-11-11

    The Canadian Dragon is a Spherical Grating Monochromator (SGM) beamline for the photon energy range between 250 and 2000 eV. The high flux from the source, a 45 mm planar undulator, allows for excellent performance in the difficult 1-2 keV range. Resolving powers comparable to those of the leading spectroscopy beamlines are routinely available. The beamline design employs toroidal refocusing optics to allow for two in-line endstation areas. The upstream experimental area hosts a dedicated UHV endstation with a Scienta SES-100 photoelectron energy analyzer. The downstream experimental area is primarily used for solid sample X-ray absorption studies, but can be fitted with a number of different endstations. A 1 metre long differential pumping section between the beamline optics and the second endstation area permits the analysis of non-UHV compatible samples, making the beamline suitable for many environmental or biological experiments.

  14. Multipurpose monochromator for the Basic Energy Science Synchrotron Radiation Center Collaborative Access Team beamlines at the Advanced Photon Source x-ray facility

    Science.gov (United States)

    Ramanathan, M.; Beno, M. A.; Knapp, G. S.; Jennings, G.; Cowan, P. L.; Montano, P. A.

    1995-02-01

    The Basic Energy Science Synchrotron Radiation Center (BESSRC) Collaborative Access Team (CAT) will construct x-ray beamlines at two sectors of the Advanced Photon Source facility. In most of the beamlines the first optical element will be a monochromator, so that a standard design for this critical component is advantageous. The monochromator is a double-crystal, fixed exit scheme with a constant offset designed for ultrahigh vacuum windowless operation. In this design, the crystals are mounted on a turntable with the first crystal at the center of rotation. Mechanical linkages are used to correctly position the second crystal and maintain a constant offset. The main drive for the rotary motion is provided by a vacuum compatible Huber goniometer isolated from the main vacuum chamber. The design of the monochromator is such that it can accommodate water, gallium, or liquid-nitrogen cooling for the crystal optics.

  15. The performance of a cryogenically cooled monochromator for an in-vacuum undulator beamline.

    Science.gov (United States)

    Zhang, Lin; Lee, Wah Keat; Wulff, Michael; Eybert, Laurent

    2003-07-01

    The channel-cut silicon monochromator on beamline ID09 at the European Synchrotron Radiation Facility is indirectly cooled from the sides by liquid nitrogen. The thermal slope error of the diffracting surface is calculated by finite-element analysis and the results are compared with experiments. The slope error is studied as a function of cooling coefficients, beam size, position of the footprint and power distribution. It is found that the slope error versus power curve can be divided into three regions: (i). The linear region: the thermal slope error is linearly proportional to the power. (ii). The transition region: the temperature of the Si crystal is close to 125 K; the thermal slope error is below the straight line extrapolated from the linear curve described above. (iii). The non-linear region: the temperature of the Si crystal is higher than 125 K and the thermal slope error increases much faster than the power. Heat-load tests were also performed and the measured rocking-curve widths are compared with those calculated by finite-element modeling. When the broadening from the intrinsic rocking-curve width and mounting strain are included, the calculated rocking-curve width versus heat load is in excellent agreement with experiment.

  16. Biomechanical Evaluation of Different Fixation Methods for Mandibular Anterior Segmental Osteotomy Using Finite Element Analysis, Part One: Superior Repositioning Surgery.

    Science.gov (United States)

    Kilinç, Yeliz; Erkmen, Erkan; Kurt, Ahmet

    2016-01-01

    The aim of the current study was to comparatively evaluate the mechanical behavior of 3 different fixation methods following various amounts of superior repositioning of mandibular anterior segment. In this study, 3 different rigid fixation configurations comprising double right L, double left L, or double I miniplates with monocortical screws were compared under vertical, horizontal, and oblique load conditions by means of finite element analysis. A three-dimensional finite element model of a fully dentate mandible was generated. A 3 and 5 mm superior repositioning of mandibular anterior segmental osteotomy were simulated. Three different finite element models corresponding to different fixation configurations were created for each superior repositioning. The von Mises stress values on fixation appliances and principal maximum stresses (Pmax) on bony structures were predicted by finite element analysis. The results have demonstrated that double right L configuration provides better stability with less stress fields in comparison with other fixation configurations used in this study.

  17. Modeling of the distribution of heavy metals and trace elements in argan forest soil and parts of argan tree.

    Science.gov (United States)

    Mohammed, Faez A E; Bchitou, Rahma; Boulmane, Mohamed; Bouhaouss, Ahmed; Guillaume, Dominique

    2013-01-01

    The transfer of heavy metals and trace elements from argan forest soil into the wood, leaves, almonds, and argan oil was studied. Analyzed metals were: chromium, cadmium, copper, zinc, lead, calcium, phosphorus, potassium, and magnesium. Correlations linking different behaviors of the studied heavy metals and trace elements observed by multidimensional analysis were attributed to partial-spatial variations. Whereas the RV-coefficient of wood, leaf, almond and oil groups was high, the soil group correlated poorly with the other groups.

  18. Biomechanical Evaluation of Different Fixation Methods for Mandibular Anterior Segmental Osteotomy Using Finite Element Analysis, Part Two: Superior Repositioning Surgery With Bone Allograft.

    Science.gov (United States)

    Kilinç, Yeliz; Erkmen, Erkan; Kurt, Ahmet

    2016-01-01

    In this study, the biomechanical behavior of different fixation methods used to fix the mandibular anterior segment following various amounts of superior repositioning was evaluated by using Finite Element Analysis (FEA). The three-dimensional finite element models representing 3 and 5 mm superior repositioning were generated. The gap in between segments was assumed to be filled by block bone allograft and resignated to be in perfect contact with the mandible and segmented bone. Six different finite element models with 2 distinct mobilization rate including 3 different fixation configurations, double right L (DRL), double left L (DLL), or double I (DI) miniplates with monocortical screws, correspondingly were created. A comparative evaluation has been made under vertical, horizontal and oblique loads. The von Mises and principal maximum stress (Pmax) values were calculated by finite element solver programme. The first part of our ongoing Finite Element Analysis research has been addressed to the mechanical behavior of the same fixation configurations in nongrafted models. In comparison with the findings of the first part of the study, it was concluded that bone graft offers superior mechanical stability without any limitation of mobilization and less stress on the fixative appliances as well as in the bone.

  19. Importance of nickel in Fabaceae. Pt. 1. Comparative studies on the content of nickel and certain other elements in vegetative parts and seeds

    Energy Technology Data Exchange (ETDEWEB)

    Horak, O.

    1985-02-28

    Vegetative parts and seeds of 15 Fabaceae were analyzed with respect to concentrations of Ni as well as K, Ca, Mg, Fe, Mn, Zn, Cu and Mo. The distribution pattern of the examined elements is different. For the macronutrients and iron mostly a significant higher concentration could be found in the shoot, whilst micronutrients frequently were accumulated in the seed. Nickel is that element, which is accumulated relatively highest in the seed. This is a criterion for a specific importance of nickel, which is a compound of urease and in this function could be involved in the mobilization of nitrogen storage substances of the seed.

  20. The sub-micron resolution X-ray spectroscopy beamline at NSLS-II

    Science.gov (United States)

    De Andrade, V.; Thieme, J.; Northrup, P.; Yao, Y.; Lanzirotti, A.; Eng, P.; Shen, Q.

    2011-09-01

    For many research areas such as life, environmental, earth or material sciences, novel analytical resources have to be developed for an advance understanding of complex natural and engineered systems that are heterogeneous on the micron to the tenths of microns scale. NSLS-II at BNL will be a synchrotron radiation source with an ultra-high brilliance delivering a high current (500 mA). One of the 1st six NSLS-II beamlines will be the Sub-micron Resolution X-ray spectroscopy beamline (SRX), dedicated as an analytical tool to study complex systems on a sub-micron length scale. SRX will comprise two branches thanks to a canted setup with two undulators: the first branch using Kirkpatrick-Baez mirrors as focusing optics will cover the energy range of 4.65-23 keV, allowing for XANES experiments from the Ti to the Rh K-edge. Thanks to a horizontally deflecting double crystal monochromator with maximum stability, a set of slits located on the secondary source, and two sets of complementary and quickly interchangeable KB mirrors, spectroscopy with very high spectral and spatial resolution will be achieved. The spot size will almost fully cover a range from 60×60 to 1300×500 nm 2, providing an attractive adaptability of the observation scale. A 1.5 m long IVU21 will serve as a light source. The expected high flux in a sub-micron-spot (5×10 12 and 7×10 13 ph s -1 at maximum and lowest resolutions) will open new possibilities for spectromicroscopy of trace elements. The 2nd canted undulator will serve as an independent light source for the second branch designed for experiments with X-ray energies in the range of 2-15 keV. Using Fresnel zone plates, the spatial resolution aimed for is around 30 nm with up to 7×10 9 ph s -1 in the spot. This branch would be attractive for many biological applications from life and environmental science due to low-Z elements of interest within that energy range. In both experimental stations, X-ray fluorescence will be used for imaging

  1. Beam property studies in the PLS diagnostic beamline

    CERN Document Server

    Ko, I S; Seon, D K; Kim, C B; Lee, T Y

    1999-01-01

    A diagnostic beamline has been operated in the Pohang Light Source (PLS) storage ring for the diagnostics of electron and photon beam properties. It consists of two 1:1 imaging systems: a visible-light imaging system and a soft X-ray imaging system. We have measured the transverse and the longitudinal structures of beams by using a streak camera to obtain a visible image. Accurate transverse beam size have been measured to be 186 mu m horizontally and 43.1 mu m vertically by using soft X-ray images with minimum diffraction errors. The corresponding emittances are 11.7 nm-rad horizontally and 0.59 nm-rad vertically. By comparing the measured data with the design values, we confirmed that the PLS storage ring has reached its designed performance within an error of 3.3 % in the transverse direction.

  2. Lithography beamline design and exposure uniformity controlling and measuring

    Science.gov (United States)

    Qian, Shinan; Jiang, Dikui; Liu, Zewen; Chen, Qianhong; Kan, Ya; Liu, Wanpo

    1989-07-01

    The lithography beamline design of Hefei National Synchrotron Radiation Laboratory is presented. A scanning mirror is used to cut off short wavelength radiation and to expand the vertical exposure dimension to 50 mm. A thin beryllium window is installed before the scanning mirror to prevent the longer wavelength radiation from going through. An exposure chamber with a vacuum of 5×10E-7 Torr is located at 7 m downstream from the source point. Because there is no window at the entrance of the chamber, a differential pumping system is used. The scanning mirror is driven by a stepping motor which oscillates through a 1° angle. The required driving speed curve is determined by a computer in order to obtain a uniform exposure area. An in situ moiré fringe grating system is used to measure the uniformity of the motor speed.

  3. MX1: a bending-magnet crystallography beamline serving both chemical and macromolecular crystallography communities at the Australian Synchrotron.

    Science.gov (United States)

    Cowieson, Nathan Philip; Aragao, David; Clift, Mark; Ericsson, Daniel J; Gee, Christine; Harrop, Stephen J; Mudie, Nathan; Panjikar, Santosh; Price, Jason R; Riboldi-Tunnicliffe, Alan; Williamson, Rachel; Caradoc-Davies, Tom

    2015-01-01

    MX1 is a bending-magnet crystallography beamline at the 3 GeV Australian Synchrotron. The beamline delivers hard X-rays in the energy range from 8 to 18 keV to a focal spot at the sample position of 120 µm FWHM. The beamline endstation and ancillary equipment facilitate local and remote access for both chemical and biological macromolecular crystallography. Here, the design of the beamline and endstation are discussed. The beamline has enjoyed a full user program for the last seven years and scientific highlights from the user program are also presented.

  4. Undulator beamline of the Brockhouse sector at the Canadian Light Source.

    Science.gov (United States)

    Diaz, B; Gomez, A; Meyer, B; Duffy, A; Hallin, E; Kycia, S

    2014-08-01

    The Brockhouse project at the Canadian Light Source plans the construction of three beamlines, two wiggler beamlines, and one undulator beamline, that will be dedicated to x-ray diffraction and scattering. In this work, we will describe the undulator beamline main components and performance parameters, obtained from ray tracing using XOP-SHADOW codes. The undulator beamline will operate from 4.95 to 21 keV, using a 20 mm period hybrid undulator placed upstream of the wiggler in the same straight section. The beamline optics design was developed in cooperation with the Brazilian Synchrotron - LNLS. The beamline will have a double crystal monochromator with the options of Si(111) or Si(311) crystal pairs followed by two mirrors in the KB configuration to focus the beam at the sample position. The high brilliance of the undulator source will produce a very high flux of ~10(13) photons/s and high energy resolution into a small focus of 170 μm horizontal and 20-60 μm vertical, depending on the optical configuration and energy chosen. Two multi-axis goniometer experimental stations with area detectors and analyzers are foreseen to enable diffraction, resonant and inelastic scattering experiments, and SAXS/WAXS experiments with high resolution and time resolving capabilities.

  5. 3-D Imaging Using Row–Column-Addressed Arrays With Integrated Apodization. Part I: Apodization Design and Line Element Beamforming

    DEFF Research Database (Denmark)

    Rasmussen, Morten Fischer; Christiansen, Thomas Lehrmann; Thomsen, Erik Vilain

    2015-01-01

    -integrated apodization increased the apparent diameter of the vessel from 2.0 mm to 2.4 mm, corresponding to an increase from 67% to 80% of the true vessel diameter. The line element beamforming approach is shown to be essential for achieving correct time-of-flight calculations, and hence avoid geometrical distortions...

  6. Elements in rice on the Swedish market: part 2. Chromium, copper, iron, manganese, platinum, rubidium, selenium and zinc.

    Science.gov (United States)

    Jorhem, L; Astrand, C; Sundstrom, B; Baxter, M; Stokes, P; Lewis, J; Grawe, K P

    2008-07-01

    A survey of the levels of some essential and non-essential trace elements in different types of rice available on the Swedish retail market was carried out in 2001-03. The types of rice included long and short grain, brown, white, and parboiled white. The mean levels found were: chromium (Cr) = 0.008 mg kg(-1), copper (Cu) = 1.9 mg kg(-1), iron (Fe) = 4.7 mg kg(-1), manganese (Mn) = 16 mg kg(-1), platinum (Pt) < 0.0003 mg kg(-1), rubidium (Rb) = 3.3 mg kg(-1), selenium (Se) =0.1 mg kg(-1); and zinc (Zn) = 15 mg kg(-1). Inductively coupled plasma-mass spectrometry (ICP-MS) was used for the determination of Pt, Rb, and Se, after acid digestion. All other elements were determined using atomic absorption spectrometry (AAS) after dry ashing. Intake calculations were performed and it was concluded that rice may contribute considerably to the daily requirements of the essential elements Cu, Fe, Mn, Se, and Zn if rice consumption is high. The levels of some elements, e.g. Fe and Mn, were significantly higher in brown compared with white rice.

  7. Flooding and drying in finite-element discretizations of shallow-water equations. Part 1: One dimension

    NARCIS (Netherlands)

    Bokhove, O.

    2003-01-01

    Free boundaries in shallow-water equations demarcate the time-dependent water line between ``flooded'' and ``dry'' topography. A novel numerical algorithm to treat flooding and drying in a formally second-order explicit space discontinuous finite element discretization of the one-dimensional or symm

  8. Regular Mechanical Transformation of Rotations Into Translations: Part 2. Kinematic Synthesis of the Elements of High Kinematic Joints, Realizing the Process of Motions Transformation

    Science.gov (United States)

    Abadjieva, Emilia; Abadjiev, Valentin

    2017-09-01

    This work is developed on the basis of the illustrated main parts of the kinematic theory (theory of gearing) of the spatial rack drives in Part 1 of this study. The applied theoretical approach to their synthesis, based on the T. Olivier's second principle is defined. A study of the geometric nature of the surface of action (mesh region, respectively) of these class transmissions is shown. Research software programs for synthesis and visualization of these transmissions and their specific elements are elaborated, on the basis of the given algorithms to the synthesis of the elements of high kinematic joints (active tooth surfaces), with which the movable links of the studied gear systems are equipped.

  9. First results from the high-brightness x-ray spectroscopy beamline at ALS

    Energy Technology Data Exchange (ETDEWEB)

    Perera, R.C.C.; Ng, W.; Jones, G. [Lawrence Berkeley National Lab., CA (United States)] [and others

    1997-04-01

    Beamline 9.3.1 at the Advanced Light Source (ALS) is a windowless beamline, covering the 1-6 keV photon-energy range, designed to achieve the goal of high brightness at the sample for use in the X-ray Atomic and Molecular Spectroscopy (XAMS) science, surface and interface science, biology and x-ray optical development programs at ALS. X-ray absorption and time of flight photo emission measurements in 2 - 5 keV photon energy in argon along with the flux, resolution, spot size and stability of the beamline will be discussed. Prospects for future XAMS measurements will also be presented.

  10. XAFS at the new materials science beamline 10 at the DELTA storage ring

    Science.gov (United States)

    Lützenkirchen-Hecht, D.; Wagner, R.; Frahm, R.

    2016-05-01

    The layout and the characteristics of the hard X-ray beamline BL 10 at the superconducting asymmetric wiggler at the 1.5 GeV Dortmund Electron Accelerator DELTA are described. Equipped with a stable and robust Si(111) channel-cut monochromator, this beamline is suited for XAFS studies in the spectral range from about 4 keV to ca. 16 keV photon energy. We will illustrate the performance of the beamline, and present EXAFS data obtained from several reference compounds. XANES data measured for dilute sample systems as well as surface sensitive grazing incidence EXAFS obtained from thin film samples will also be discussed.

  11. Beam-position monitors in the X-ray undulator beamline at PETRA.

    Science.gov (United States)

    Hahn, U; Brefeld, W; Hesse, M; Schneider, J R; Schulte-Schrepping, H; Seebach, M; Werner, M

    1998-05-01

    At the 12 GeV storage ring PETRA, the first synchrotron radiation beamline uses a 4 m-long undulator. The beamline, with a length of 130 m between source and sample, delivers hard X-ray photons usable up to 300 keV. The photon beam has a total power of 7 kW. Combined with the high brilliance, the powerful beam is very critical for all beamline components. Copper, located at a distance of 26 m, hit by the full undulator beam, melts within 20 ms. Different monitors are described for stable, safe and reliable operation of beam and experiments.

  12. Imaging in real and reciprocal space at the Diamond beamline I13

    Energy Technology Data Exchange (ETDEWEB)

    Rau, C., E-mail: Christoph.rau@diamond.ac.uk [Diamond Light Source Ltd., Harwell Science and Innovation Campus, Didcot, OX 11 0DE (United Kingdom); University of Manchester, School of Materials Grosvenor St., Manchester, M1 7HS (United Kingdom); Northwestern University School of Medicine, 303 E. Chicago Avenue, Chicago, IL 60611-3008 (United States); Wagner, U. H.; Vila-Comamala, J.; Bodey, A.; Parson, A.; García-Fernández, M.; Pešić, Z. [Diamond Light Source Ltd., Harwell Science and Innovation Campus, Didcot, OX 11 0DE (United Kingdom); De Fanis, A. [Diamond Light Source Ltd., Harwell Science and Innovation Campus, Didcot, OX 11 0DE (United Kingdom); European XFEL GmbH, Notkestraße 85, 22607 Hamburg (Germany)

    2016-01-28

    The Diamond Imaging and Coherence beamline I13 consists of two independent branchlines for imaging in real and reciprocal space. Different microscopies are available providing a range of spatial resolution from 5µm to potentially 5nm. The beamline operates in the energy range of 6-35keV covering different scientific areas such as biomedicine, materials science and geophysics. Several original devices have been developed at the beamline, such as the EXCALIBUR photon counting detector and the combined robot arms for coherent X-ray diffraction.

  13. Progress of projection computed tomography by upgrading of the beamline 37XU of SPring-8

    Science.gov (United States)

    Terada, Yasuko; Suzuki, Yoshio; Uesugi, Kentaro; Miura, Keiko

    2016-01-01

    Beamline 37XU at SPring-8 has been upgraded for nano-focusing applications. The length of the beamline has been extended to 80 m. By utilizing this length, the beamline has advantages for experiments such as X-ray focusing, X-ray microscopic imaging and X-ray computed tomography. Projection computed tomography measurements were carried out at experimental hutch 3 located 80 m from the light source. CT images of a microcapsule have been successfully obtained with a wide X-ray energy range.

  14. Progress of projection computed tomography by upgrading of the beamline 37XU of SPring-8

    Energy Technology Data Exchange (ETDEWEB)

    Terada, Yasuko, E-mail: yterada@spring8.or.jp; Suzuki, Yoshio; Uesugi, Kentaro; Miura, Keiko [Japan Synchrotron Radiation Research Institute, SPring-8, 1-1-1 Koto, Sayo, Hyogo 679-5198 (Japan)

    2016-01-28

    Beamline 37XU at SPring-8 has been upgraded for nano-focusing applications. The length of the beamline has been extended to 80 m. By utilizing this length, the beamline has advantages for experiments such as X-ray focusing, X-ray microscopic imaging and X-ray computed tomography. Projection computed tomography measurements were carried out at experimental hutch 3 located 80 m from the light source. CT images of a microcapsule have been successfully obtained with a wide X-ray energy range.

  15. A Fast, Versatile Nanoprobe for Complex Materials: The Sub-micron Resolution X-ray Spectroscopy Beamline at NSLS-II (491st Brookhaven Lecture)

    Energy Technology Data Exchange (ETDEWEB)

    Thieme, Juergen [BNL Photon Sciences Directorate

    2014-02-06

    Time is money and for scientists who need to collect data at research facilities like Brookhaven Lab’s National Synchrotron Light Source (NSLS), “beamtime” can be a precious commodity. While scanning a complex material with a specific technique and standard equipment today would take days to complete, researchers preparing to use brighter x-rays and the new sub-micron-resolution x-ray spectroscopy (SRX) beamline at the National Synchrotron Light Source II (NSLS-II) could scan the same sample in greater detail with just a few hours of beamtime. Talk about savings and new opportunities for researchers! Users will rely on these tools for locating trace elements in contaminated soils, developing processes for nanoparticles to deliver medical treatments, and much more. Dr. Thieme explains benefits for next-generation research with spectroscopy and more intense x-rays at NSLS-II. He discusses the instrumentation, features, and uses for the new SRX beamline, highlighting its speed, adjustability, and versatility for probing samples ranging in size from millimeters down to the nanoscale. He will talk about complementary beamlines being developed for additional capabilities at NSLS-II as well.

  16. Recent Major Improvements to the ALS Sector 5 MacromolecularCrystallography Beamlines

    Energy Technology Data Exchange (ETDEWEB)

    Morton, Simon A.; Glossinger, James; Smith-Baumann, Alexis; McKean, John P.; Trame, Christine; Dickert, Jeff; Rozales, Anthony; Dauz,Azer; Taylor, John; Zwart, Petrus; Duarte, Robert; Padmore, Howard; McDermott, Gerry; Adams, Paul

    2007-07-01

    Although the Advanced Light Source (ALS) was initially conceived primarily as a low energy (1.9GeV) 3rd generation source of VUV and soft x-ray radiation it was realized very early in the development of the facility that a multipole wiggler source coupled with high quality, (brightness preserving), optics would result in a beamline whose performance across the optimal energy range (5-15keV) for macromolecular crystallography (MX) would be comparable to, or even exceed, that of many existing crystallography beamlines at higher energy facilities. Hence, starting in 1996, a suite of three beamlines, branching off a single wiggler source, was constructed, which together formed the ALS Macromolecular Crystallography Facility. From the outset this facility was designed to cater equally to the needs of both academic and industrial users with a heavy emphasis placed on the development and introduction of high throughput crystallographic tools, techniques, and facilities--such as large area CCD detectors, robotic sample handling and automounting facilities, a service crystallography program, and a tightly integrated, centralized, and highly automated beamline control environment for users. This facility was immediately successful, with the primary Multiwavelength Anomalous Diffraction beamline (5.0.2) in particular rapidly becoming one of the foremost crystallographic facilities in the US--responsible for structures such as the 70S ribosome. This success in-turn triggered enormous growth of the ALS macromolecular crystallography community and spurred the development of five additional ALS MX beamlines all utilizing the newly developed superconducting bending magnets ('superbends') as sources. However in the years since the original Sector 5.0 beamlines were built the performance demands of macromolecular crystallography users have become ever more exacting; with growing emphasis placed on studying larger complexes, more difficult structures, weakly diffracting or

  17. Mixed and Penalty Finite Element Models for the Nonlinear Behavior of Biphasic Soft Tissues in Finite Deformation: Part I - Alternate Formulations.

    Science.gov (United States)

    Almeida, EDGARD S.; Spilker, ROBERT L.

    1997-01-01

    This paper addresses finite element-based computational models for the three-dimensional, (3-D) nonlinear analysis of soft hydrated tissues, such as the articular cartilage in diarthrodial joints, under physiologically relevant loading conditions. A biphasic continuum description is used to represent the soft tissue as a two-phase mixture of incompressible, inviscid fluid and a hyperelastic solid. Alternate mixed-penalty and velocity-pressure finite element formulations are used to solve the nonlinear biphasic governing equations, including the effects of a strain-dependent permeability and a hyperelastic solid phase under finite deformation. The resulting first-order nonlinear system of equations is discretized in time using an implicit finite difference scheme, and solved using the Newton-Raphson method. Using a discrete divergence operator, an equivalence is shown between the mixed-penalty method and a penalty method previously derived by Suh et al. [1]. In Part II [2], the mixed-penalty and velocity-pressure formulations are used to develop two-dimensional (2-D) quadrilateral and triangular elements and 3-D hexahedral and tetrahedral elements. Numerical examples, including those representative of soft tissue material testing and simple human joints, are used to validate the formulations and to illustrate their applications. A focus of this work is the comparison of alternate formulations for nonlinear problems. While it is demonstrated that both formulations produce a range of converging elements, the velocity-pressure formulation is found to be more efficient computationally.

  18. Nonlinear incompressible finite element for simulating loading of cardiac tissue--Part I: Two dimensional formulation for thin myocardial strips.

    Science.gov (United States)

    Horowitz, A; Sheinman, I; Lanir, Y; Perl, M; Sideman, S

    1988-02-01

    A two-dimensional incompressible plane-stress finite element is formulated for the simulation of the passive-state mechanics of thin myocardial strips. The formulation employs a total Lagrangian and materially nonlinear approach, being based on a recently proposed structural material law, which is derived from the histological composition of the tissue. The ensuing finite element allows to demonstrate the mechanical properties of a single myocardial layer containing uniformly directed fibers by simulating various loading cases such as tension, compression and shear. The results of these cases show that the fiber direction is considerably stiffer than the cross-fiber direction, that there is significant coupling between these two directions, and that the shear stiffness of the tissue is lower than its tensile and compressive stiffness.

  19. Release to the Gas Phase of Inorganic Elements during Wood Combustion. Part 2: Influence of Fuel Composition

    DEFF Research Database (Denmark)

    van Lith, Simone Cornelia; Jensen, Peter Arendt; Frandsen, Flemming

    2008-01-01

    Combustion of wood for heat and power production may cause problems such as ash deposition, corrosion, and harmful emissions of gases and particulate matter. These problems are all directly related to the release of inorganic elements (in particular Cl, S, K, Na, Zn, and Pb) from the fuel...... to the gas phase. The aims of this study are to obtain quantitative data on the release of inorganic elements during wood combustion and to investigate the influence of fuel composition. Quantitative release data were obtained by pyrolyzing and subsequently combusting small samples of wood (~30 g) at various...... temperatures in the range of 500–1150 °C in a laboratory-scale tube reactor and by performing mass balance calculations based on the weight measurements and chemical analyses of the wood fuels and the residual ash samples. Four wood fuels with different ash contents and inorganic compositions were investigated...

  20. Development and demonstration of manufacturing processes for fabricating graphite/Larc-160 polyimide structural elements, part 4, paragraph C

    Science.gov (United States)

    1981-01-01

    Progress in the development of processes for production of Celion/LARC-160 graphite-polyimide materials, quality control methods, and the fabrication of Space Shuttle composite structure components is reported. The formulation and processing limits for three batches of resin are presented. Process improvements for simplification of the imidizing and autoclave cure cycles are described. Imidized and autoclave cured test panels were prepared. Celion/LARC-160 cure process verification and the fabrication of honeycomb sandwich panel elements and skin/stringer panels are described. C-scans of laminates imidized at 163 C to 218 C for periods from 30 to 180 minutes, and of process verification laminates made from different batches of prepreg are presented. Failure modes and load/strain characteristics of sandwich elements and C-scans of stringer to skin bond joints are also given.

  1. The impact of the hyperacid Ijen Crater Lake. Part I: Concentrations of elements in crops and soil.

    Science.gov (United States)

    Heikens, Alex; Widianarko, Budi; Dewi, Inge C; De Boer, Jan L M; Seinen, Willem; van Leeuwen, Kees

    2005-09-01

    In Asembagus (East Java, Indonesia) irrigation water is contaminated with effluent from the hyperacid Ijen Crater Lake resulting in a low pH and high levels of various elements. As a first step towards a risk assessment, locally produced food items (rice, maize, cassava leaf, cassava root, peanuts) were collected and concentrations of As, B, Ca, Cd, Co, Cu, Fe, Mg, Mn, Mo, Ni, Pb, V, Zn were compared to samples from a reference area and with literature values. Further, concentrations in rice were compared to total soil concentrations in paddy fields. Compared to the reference area, food items produced in the contaminated area had increased levels of Cd, Co, Ni and Mn in particular, while levels of Mo were lower. In contrast, total soil concentrations of Cd and Mn in particular have decreased whereas especially Mo was increased. In combination with the observed soil acidification, it is likely that the bioavailable concentration of most elements in the contaminated soil is higher (except for Mo) due to an increased weathering rate and/or input via the contaminated irrigation water. In terms of human health, concentrations in foods were generally within normal literature values. However, it was observed that essential elements (in particular Fe) known for their inhibitory effects on e.g. Cd and Mn toxicity did not accumulate in crops whereas Cd and Mn did.

  2. Heat transfer studies for a crystal in a synchrotron radiation beamline

    Indian Academy of Sciences (India)

    A K Sinha

    2009-04-01

    Heat load studies have been performed for the first crystal of a double crystal monochromator to be installed in a beamline of the 2·5 GeV synchrotron radiation source Indus-2. Finite element analysis (FEA) has been used to calculate the temperature distribution and the mechanical distortions on these crystals. Several cases of cooling schemes and heat loads have been studied. Based on these FEA results, the analytical relationships available in the literature have been modified. It is shown that modified analytical results compare well with the empirical results obtained from FEA. The optimisation of the cooling conditions can be achieved by doing FEA calculations for only one case. All other cases can then be calculated by using analytical relations proposed here. The proposed analytical equations are generic in nature and can be applied for any source—crystal combination and therefore would be useful for performance prediction of any new monochromator on a new synchrotron source without taking recourse to time consuming, computation-intensive FEA.

  3. Design and implementation of a robust and cost-effective double-scattering system at a horizontal proton beamline

    Science.gov (United States)

    Helmbrecht, S.; Baumann, M.; Enghardt, W.; Fiedler, F.; Krause, M.; Lühr, A.

    2016-11-01

    Purpose: particle therapy has the potential to improve radiooncology. With more and more facilities coming into operation, also the interest for research at proton beams increases. Though many centers provide beam at an experimental room, some of them do not feature a device for radiation field shaping, a so called nozzle. Therefore, a robust and cost-effective double-scattering system for horizontal proton beamlines has been designed and implemented. Materials and methods: the nozzle is based on the double scattering technique. Two lead scatterers, an aluminum ridge-filter and two brass collimators were optimized in a simulation study to form a laterally homogeneous 10 cm × 10 cm field with a spread-out Bragg-peak (SOBP). The parts were mainly manufactured using 3D printing techniques and the system was set up at OncoRay's experimental beamline. Measurement of the radiation field were carried out using a water phantom. Results: high levels of dose homogeneity were found in lateral (dose variation ΔD/D design let it appear as a valuable option for proton therapy centers intending to foster their experimental portfolio.

  4. The EIS-TIMER beamline: transient grating spectroscopy at FERMI (Conference Presentation)

    Science.gov (United States)

    Svetina, Cristian

    2016-09-01

    FERMI, the Italian Free Electron Laser user facility, provides VUV/soft x-ray photons pulses with unprecedented high brilliance and coherence. The unique design of EIS-TIMER is conceived to exploit such kind of non-linear coherent experiments to probe collective vibrational and electronic properties of matter at the nanoscale. After the proof of principle experiment successfully carried out at the DiProI beamline employing a simplified and compact setup (mini-TIMER), the EIS-TIMER beamline has been installed and commissioned. The beamlines employs 24 mirrors and three photon beams in order to create a wide set of transient grating able to reach Q vectors so far impossible to probe. In the presentation the scientific case, the commissioning results as well as the future development of the beamline will be shown. The future project nano-TIMER will be described in detail with particular attention to it's unique optical scheme mainly composed by diffraction gratings.

  5. High-throughput Toroidal Grating Beamline for Photoelectron Spectroscopy at CAMD

    Science.gov (United States)

    Kizilkaya, O; Jiles, R W; Patterson, M C; Thibodeaux, C A; Poliakoff, E D; Sprunger, P T; Kurtz, R L; Morikawa, E

    2016-01-01

    A 5 meter toroidal grating (5m-TGM) beamline has been commissioned to deliver 28 mrad of bending magnet radiation to an ultrahigh vacuum endstation chamber to facilitate angle resolved photoelectron spectroscopy. The 5m-TGM beamline is equipped with Au-coated gratings with 300, 600 and 1200 lines/mm providing monochromatized synchrotron radiation in the energy ranges 25-70 eV, 50–120 eV and 100–240 eV, respectively. The beamline delivers excellent flux (~1014-1017 photons/sec/100mA) and a combined energy resolution of 189 meV for the beamline (at 1.0 mm slit opening) and HA-50 hemispherical analyzer was obtained at the Fermi level of polycrystalline gold crystal. Our preliminary photoelectron spectroscopy results of phenol adsorption on TiO2 (110) surface reveals the metal ion (Ti) oxidation. PMID:27134636

  6. I19, the small-molecule single-crystal diffraction beamline at Diamond Light Source.

    Science.gov (United States)

    Nowell, Harriott; Barnett, Sarah A; Christensen, Kirsten E; Teat, Simon J; Allan, David R

    2012-05-01

    The dedicated small-molecule single-crystal X-ray diffraction beamline (I19) at Diamond Light Source has been operational and supporting users for over three years. I19 is a high-flux tunable-wavelength beamline and its key details are described in this article. Much of the work performed on the beamline involves structure determination from small and weakly diffracting crystals. Other experiments that have been supported to date include structural studies at high pressure, studies of metastable species, variable-temperature crystallography, studies involving gas exchange in porous materials and structural characterizations that require analysis of the diffuse scattering between Bragg reflections. A range of sample environments to facilitate crystallographic studies under non-ambient conditions are available as well as a number of options for automation. An indication of the scope of the science carried out on the beamline is provided by the range of highlights selected for this paper.

  7. Safety Analysis Report: X17B2 beamline Synchrotron Medical Research Facility

    Energy Technology Data Exchange (ETDEWEB)

    Gmuer, N.F.; Thomlinson, W.

    1990-02-01

    This report contains a safety analysis for the X17B2 beamline synchrotron medical research facility. Health hazards, risk assessment and building systems are discussed. Reference is made to transvenous coronary angiography. (LSP)

  8. Evaluation of the effect of coal cleaning of fugitive elements. Part II. Analytical methods. Final report, Phase II

    Energy Technology Data Exchange (ETDEWEB)

    Bosshart, R.E.; Price, A.A.; Ford, C.T.

    1980-03-01

    This report contains the analytical and test methods which were used routinely at Bituminous Coal Research, Inc. during the project. The procedures contained herein should aid coal industry laboratories and others, including commercial laboratories, who might be required to determine trace elements in coal. Some of the procedures have been presented in previous BCR reports; however, this report includes additional procedures which are described in greater detail. Also presented are many as the more basic coal methods which have been in use at BCR for many years, or which have been adapted or refined from other standard reference sources for coal and water. The basis for choosing specific analytical procedures for trace elements in coal is somewhat complex. At BCR, atomic absorption was selected as the basic method in the development of these procedures. The choice was based on sensitivity, selectivity, accuracy, precision, practicability, and economy. Whenever possible, the methods developed had to be both adequate and amenable for use by coal industry laboratories by virtue of relative simplicity and cost. This is not to imply that the methods described are simple or inexpensive; however, atomic abosrption techniques do meet these criteria in relation to more complex and costly methods such as neutron activation, mass spectrometry, and x-ray fluorescence, some of which require highly specialized personnel as well as access to sophisticated nuclear and computational facilities. Many of the analytical procedures for trace elements in coal have been developed or adapted specifically for the BCR studies. Their presentation is the principal purpose of this report.

  9. Summer student project report - A versatile ion source for improving the sensitivity and resolution of the CRIS beamline at ISOLDE

    CERN Document Server

    AUTHOR|(CDS)2156312

    2016-01-01

    The main part of my project involved working on the independent ion source attached to the collinear resonance ionisation spectroscopy experiment at ISOLDE. The primary aim was to increase the maximum accelerating potential from 5 kV to 30 kV, to become comparable to ion beams from the ISOLDE High Resolution Separator and to improve the resolution of hyperfine structure measurements. The new ion source allows for easy exchange between surface and plasma ion sources, as well as use as a laser ion source. The work included disassembling and rebuilding the ion optics, electronics and vacuum systems, adding new features such as a laser window. This was done in parallel with simulations of other parts of the beamline and in- volvement in online experiments. We were successful in reaching 30 kV and plan to produce beams of ions in the near future to investigate the sensitivity of various ionisation schemes.

  10. The Variable Polarization XUV Beamline P04 at PETRA III: Optics, mechanics and their performance

    Energy Technology Data Exchange (ETDEWEB)

    Viefhaus, Jens, E-mail: jens.viefhaus@desy.de [Deutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg (Germany); Scholz, Frank; Deinert, Sascha; Glaser, Leif; Ilchen, Markus; Seltmann, Jörn; Walter, Peter [Deutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg (Germany); Siewert, Frank, E-mail: frank.siewert@helmholtz-berlin.de [Helmholtz-Zentrum Berlin (HZB) für Materialien und Energie, Albert-Einstein-Straße 15, 12489 Berlin (Germany)

    2013-05-11

    The layout of the Variable Polarization XUV Beamline P04 at PETRA III is described with emphasis on selected examples of optics, mirrors and gratings. A precise characterization of the optics, their performance inside the holder and of the surrounding mechanics is presented. This also includes a detailed characterization of the different beamline mechanics as a whole (grating unit, exit slit unit, re-focusing unit) including the environment.

  11. Construction and characterization of a laser-driven proton beamline at GSI

    OpenAIRE

    Busold, Simon

    2014-01-01

    The thesis includes the first experiments with the new 100 TW laser beamline of the PHELIX laser facility at GSI Darmstadt to drive a TNSA (Target Normal Sheath Acceleration) proton source at GSI's Z6 experimental area. At consecutive stages a pulsed solenoid has been applied for beam transport and energy selection via chromatic focusing, as well as a radiofrequency cavity for energy compression of the bunch. This novel laser-driven proton beamline, representing a central experiment of the...

  12. Cold Drawn Steel Wires-Processing, Residual Stresses and Ductility-Part I: Metallography and Finite Element Analyses

    Energy Technology Data Exchange (ETDEWEB)

    Phelippeau,A.; Pommier, S.; Tsakalakos, T.; Clavel, M.; Prioul, C.

    2006-01-01

    Cold drawing steel wires lead to an increase of their mechanical strength and to a drop of their ductility. The increase of their mechanical strength has long been related to the reduction of the various material scales by plastic deformation, but the mechanisms controlling their elongation to failure have received relatively little attention. It is usually found that heavily deformed materials show a tendency to plastic strain localization and necking. However, in this paper it is shown that, though the steel wires are plastically deformed up to strain levels as high as 3.5, a significant capability of plastic deformation is preserved in as-drawn wires. This apparent contradiction is resolved by the existence of residual stresses inside the wire. Finite element analyses have been conducted in order to show that residual stresses, inherited from the drawing process, are sufficient to produce a significant hardening effect during a post-drawing tensile test, without introducing any hardening in the local material behavior. The main conclusion of this paper is that once the material has lost its hardening capabilities, residual stresses, inherited from the process, control the elongation of cold drawn wires. The finite element method allowed also the determination of the residual stress field that would lead to the best agreement between the simulated and the experimental stress strain curve of as-drawn wires.

  13. Implementation of remote monitoring and diffraction evaluation systems at the Photon Factory macromolecular crystallography beamlines

    Science.gov (United States)

    Yamada, Yusuke; pHonda, Nobuo; Matsugaki, Naohiro; Igarashi, Noriyuki; Hiraki, Masahiko; Wakatsuki, Soichi

    2008-01-01

    Owing to recent advances in high-throughput technology in macromolecular crystallography beamlines, such as high-brilliant X-ray sources, high-speed readout detectors and robotics, the number of samples that can be examined in a single visit to the beamline has increased dramatically. In order to make these experiments more efficient, two functions, remote monitoring and diffraction image evaluation, have been implemented in the macromolecular crystallography beamlines at the Photon Factory (PF). Remote monitoring allows scientists to participate in the experiment by watching from their laboratories, without having to come to the beamline. Diffraction image evaluation makes experiments easier, especially when using the sample exchange robot. To implement these two functions, two independent clients have been developed that work specifically for remote monitoring and diffraction image evaluation. In the macromolecular crystallography beamlines at PF, beamline control is performed using STARS (simple transmission and retrieval system). The system adopts a client–server style in which client programs communicate with each other through a server process using the STARS protocol. This is an advantage of the extension of the system; implementation of these new functions required few modifications of the existing system. PMID:18421163

  14. MxCuBE: a synchrotron beamline control environment customized for macromolecular crystallography experiments.

    Science.gov (United States)

    Gabadinho, José; Beteva, Antonia; Guijarro, Matias; Rey-Bakaikoa, Vicente; Spruce, Darren; Bowler, Matthew W; Brockhauser, Sandor; Flot, David; Gordon, Elspeth J; Hall, David R; Lavault, Bernard; McCarthy, Andrew A; McCarthy, Joanne; Mitchell, Edward; Monaco, Stéphanie; Mueller-Dieckmann, Christoph; Nurizzo, Didier; Ravelli, Raimond B G; Thibault, Xavier; Walsh, Martin A; Leonard, Gordon A; McSweeney, Sean M

    2010-09-01

    The design and features of a beamline control software system for macromolecular crystallography (MX) experiments developed at the European Synchrotron Radiation Facility (ESRF) are described. This system, MxCuBE, allows users to easily and simply interact with beamline hardware components and provides automated routines for common tasks in the operation of a synchrotron beamline dedicated to experiments in MX. Additional functionality is provided through intuitive interfaces that enable the assessment of the diffraction characteristics of samples, experiment planning, automatic data collection and the on-line collection and analysis of X-ray emission spectra. The software can be run in a tandem client-server mode that allows for remote control and relevant experimental parameters and results are automatically logged in a relational database, ISPyB. MxCuBE is modular, flexible and extensible and is currently deployed on eight macromolecular crystallography beamlines at the ESRF. Additionally, the software is installed at MAX-lab beamline I911-3 and at BESSY beamline BL14.1.

  15. MINE DEGASIFICATION AS BASIC SAFETY ELEMENT IN THE UNDERGROUND PARTS OF GASSY COAL MINES IN THE OSTRAVA – KARVINÁ COALFIELD

    Directory of Open Access Journals (Sweden)

    Vlastimil Hudeček

    2011-12-01

    Full Text Available In the article, degasification methods to drain the gas from the underground parts of coal mines in the Czech Republic are described. The authors are concerned with the possibilities of and new trends in ensuring safety by means of drilling operations. Examples of applications of degasification in mine plants in the Czech Republic, above all in a hard coal deposit in the Ostrava-Karviná Coalfield in the Upper Silesian Basin are presented.

  16. Oxygen, $\\alpha$-element and iron abundance distributions in the inner part of the Galactic thin disc. II

    CERN Document Server

    Andrievsky, S M; Kovtyukh, V V; Korotin, S A; Lépine, J R D

    2016-01-01

    We have derived the abundances of 36 chemical elements in one Cepheid star, ASAS 181024--2049.6, located R$_{\\rm G}= 2.53$ kpc from the Galactic center. This star falls within a region of the inner thin disc poorly sampled in Cepheids. Our spectral analysis shows that iron, magnesium, silicon, calcium and titanium LTE abundances in that star support the presence of a plateau-like abundance distribution in the thin disc within 5 kpc of the Galactic center, as previously suggested by \\cite{Maret15}. If confirmed, the flattening of the abundance gradient within that region could be the result of a decrease in the star formation rate due to dynamic effects, possibly from the central Galactic bar.

  17. Consideration on thermodynamic data for predicting solubility and chemical species of elements in groundwater. Part 1: Tc, U, Am

    Energy Technology Data Exchange (ETDEWEB)

    Yamaguchi, Tetsuji; Takeda, Seiji [Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan). Tokai Research Establishment

    1999-01-01

    The solubility determines the release of radionuclides from waste form and is used as a source term in radionuclide migration analysis in performance assessment of radioactive waste repository. Complexations of radionuclides by ligands in groundwater affect the interaction between radionuclides and geologic media, thus affect their migration behavior. Thermodynamic data for Tc, Am and U were reviewed and compiled to be used for predicting the solubility and chemical species in groundwater. Thermodynamic data were reviewed with emphasis on the hydrolysis and carbonate complexation that can dominate the speciation in typical groundwater. Thermodynamic data for other species were selected based on existing database. Thermodynamic data for other important elements are under investigation, thus shown in an appendix for temporary use. (author)

  18. High efficiency diffraction grating for EUV lithography beamline monochromator

    Science.gov (United States)

    Voronov, D. L.; Warwick, T.; Gullikson, E. M.; Salmassi, F.; Naulleau, P.; Artemiev, N. A.; Lum, P.; Padmore, H. A.

    2016-09-01

    A blazed diffraction grating for the EUV lithography Beamline 12.0.1 of the Advanced Light Source has been fabricated using optical direct write lithography and anisotropic wet etching technology. A variable line spacing pattern was recorded on a photoresist layer and transferred to a hard mask layer of the grating substrate by a plasma etch. Then anisotropic wet etching was applied to shape triangular grating grooves with precise control of the ultralow blaze angle. Variation of the groove density along the grating length was measured with a Long Trace Profiler (LTP). Fourier analysis of the LTP data confirmed high groove placement accuracy of the grating. The grating coated with a Ru coating demonstrated diffraction efficiency of 69.6% in the negative first diffraction order which is close to theoretical efficiency at the wavelength of 13.5 nm. This work demonstrates an alternative approach to fabrication of highly efficient and precise x-ray diffraction gratings with ultra-low blaze angles.

  19. Status of the Design of the LBNE Neutrino Beamline

    CERN Document Server

    Andrews, R; Childress, S C; Moore, C D; Papadimitriou, V; Campbell, M R

    2013-01-01

    The Long Baseline Neutrino Experiment (LBNE) will utilize a neutrino beamline facility located at Fermilab to carry out a compelling research program in neutrino physics. The facility will aim a beam of neutrinos toward a detector placed at the Homestake Mine in South Dakota, about 1300 km away. The neutrinos are produced as follows: First, protons extracted from the MI-10 section of the Main Injector (60-120 GeV) hit a solid target above grade and produce mesons. Then, the charged mesons are focused by a set of focusing horns into a 250 m long decay pipe, towards the far detector. Finally, the mesons that enter the decay pipe decay into neutrinos. The parameters of the facility were determined taking into account several factors including the physics goals, the modeling of the facility, spacial and radiological constraints and the experience gained by operating the NuMI facility at Fermilab. The initial beam power is expected to be ~700 kW, however some of the parameters were chosen to be able to deal with a...

  20. Current Status of the SANAEM RFQ Accelerator Beamline

    CERN Document Server

    Turemen, G; Ogur, S; Yildiz, V; Mete, O; Oz, S; Ozbey, A; Yildiz, H; Yaman, F; Akgun, Y; Alacakir, A; Bolukdemir, S; Bozbey, A; Sahin, A; Unel, G; Erhan, S

    2015-01-01

    The design and production studies of the proton beamline of SPP, which aims to acquire know-how on proton accelerator technology thru development of man power and serves as particle accelerator technologies test bench, continue at TAEK-SANAEM as a multi-phase project. For the first phase, 20 keV protons will be accelerated to 1.3 MeV by a single piece RFQ. Currently, the beam current and stability tests are ongoing for the Inductively Coupled Plasma ion source. The measured magnetic field maps of the Low Energy Beam Transport solenoids are being used for matching various beam configurations of the ion source to the RFQ by computer simulations. The installation of the low energy diagnostics box was completed in Q1 of 2015. The production of the RFQ cavity was started with aluminum 7075-T6 which will be subsequently coated by Copper to reduce the RF (Ohmic) losses. On the RF side, the development of the hybrid power supply based on solid state and tetrode amplifiers continues. All RF transmission components hav...

  1. Neutrino Flux Prediction for the NuMI Beamline

    Energy Technology Data Exchange (ETDEWEB)

    Aliaga Soplin, Leonidas [William-Mary Coll.

    2016-01-01

    The determination of the neutrino flux in any conventional neutrino beam presents a challenge for the current and future short and long baseline neutrino experiments. The uncertainties associated with the production and attenuation of the hadrons in the beamline materials along with those associated with the beam optics have a big effect in the flux spectrum knowledge. For experiments like MINERvA, understanding the flux is crucial since it enters directly into every neutrino-nucleus cross-sections measurements. The foundation of this work is predicting the neutrino flux at MINERvA using dedicated measurements of hadron production in hadron-nucleus collisions and incorporating in-situ MINERvA data that can provide additional constraints. This work also includes the prospect for predicting the flux at other detectors like the NOvA Near detector. The procedure and conclusions of this thesis will have a big impact on future hadron production experiments and on determining the fl ux for the upcoming DUNE experiment.

  2. Alignment of the photoelectron spectroscopy beamline at NSRL

    CERN Document Server

    Li, Chaoyang; Wen, Shen; Pan, Congyuan; An, Ning; Du, Xuewei; Zhu, Junfa; Wang, Qiuping

    2013-01-01

    The photoelectron spectroscopy beamline at National Synchrotron Radiation Laboratory (NSRL) is equipped with a spherical grating monochromator with the included angle of 174 deg. Three gratings with line density of 200, 700 and 1200 lines/mm are used to cover the energy region from 60 eV to 1000 eV. After several years operation, the spectral resolution and flux throughput were deteriorated, realignment is necessary to improve the performance. First, the wavelength scanning mechanism, the optical components position and the exit slit guide direction are aligned according to the design value. Second, the gratings are checked by Atomic Force Microscopy (AFM). And then the gas absorption spectrum is measured to optimize the focusing condition of the monochromator. The spectral resolving power is recovered to the designed value of 1000@244eV. The flux at the end station for the 200 lines/mm grating is about 10^10 photons/sec/200mA, which is in accordance with the design. The photon flux for the 700 lines/mm grati...

  3. Design, Installation, and Initial Commissioning of the MTA Beamline

    CERN Document Server

    Moore, Craig; Garcia, Fernanda; Gerardi, Michael; Johnstone, Carol; Kobilarcik, Thomas; Kucera, Michael; Kufer, Mathew; Newhart, Duane; Rakhno, Igor; Vogel, Gregory

    2012-01-01

    A new experimental area designed to develop, test and verify muon ionization cooling apparatus using the 400-MeV Fermilab Linac proton beam has been fully installed and is presently being commissioned. Initially, this area was used for cryogenic tests of liquid-hydrogen absorbers for the MUCOOL R&D program and, now, for high-power beam tests of absorbers, high-gradient rf cavities in the presence of magnetic fields (including gas-filled cavities), and other prototype muon-cooling apparatus. The experimental scenarios being developed for muon facilities involve collection, capture, and cooling of large-emittance, high-intensity muon beams--~10**13 muons, so that conclusive tests of the apparatus require full Linac beam, which is 1.6 x 10**13 p/pulse. To support the muon cooling facility, this new primary beamline extracts and transports beam directly from the Linac to the test facility. The design concept for the MuCool facility is taken from an earlier proposal, but modifications were necessary to accommo...

  4. Neutrino Flux Prediction for the NuMI Beamline

    Energy Technology Data Exchange (ETDEWEB)

    Soplin, Leonidas Aliaga [Coll. William and Mary

    2016-01-01

    The determination of the neutrino flux in any conventional neutrino beam presents a challenge for the current and future short and long baseline neutrino experiments. The uncertainties associated with the production and attenuation of the hadrons in the beamline materials along with those associated with the beam optics have a big effect in the flux spectrum knowledge. For experiments like MINERvA, understanding the flux is crucial since it enters directly into every neutrino-nucleus cross-sections measurements. The foundation of this work is predicting the neutrino flux at MINERvA using dedicated measurements of hadron production in hadron-nucleus collisions and incorporating in-situ MINERvA data that can provide additional constraints. This work also includes the prospect for predicting the flux at other detectors like the NOvA Near detector. The procedure and conclusions of this thesis will have a big impact on future hadron production experiments and on determining the flux for the upcoming DUNE experiment.

  5. 3-D magnetotelluric inversion including topography using deformed hexahedral edge finite elements and direct solvers parallelized on SMP computers - Part I: forward problem and parameter Jacobians

    Science.gov (United States)

    Kordy, M.; Wannamaker, P.; Maris, V.; Cherkaev, E.; Hill, G.

    2016-01-01

    We have developed an algorithm, which we call HexMT, for 3-D simulation and inversion of magnetotelluric (MT) responses using deformable hexahedral finite elements that permit incorporation of topography. Direct solvers parallelized on symmetric multiprocessor (SMP), single-chassis workstations with large RAM are used throughout, including the forward solution, parameter Jacobians and model parameter update. In Part I, the forward simulator and Jacobian calculations are presented. We use first-order edge elements to represent the secondary electric field (E), yielding accuracy O(h) for E and its curl (magnetic field). For very low frequencies or small material admittivities, the E-field requires divergence correction. With the help of Hodge decomposition, the correction may be applied in one step after the forward solution is calculated. This allows accurate E-field solutions in dielectric air. The system matrix factorization and source vector solutions are computed using the MKL PARDISO library, which shows good scalability through 24 processor cores. The factorized matrix is used to calculate the forward response as well as the Jacobians of electromagnetic (EM) field and MT responses using the reciprocity theorem. Comparison with other codes demonstrates accuracy of our forward calculations. We consider a popular conductive/resistive double brick structure, several synthetic topographic models and the natural topography of Mount Erebus in Antarctica. In particular, the ability of finite elements to represent smooth topographic slopes permits accurate simulation of refraction of EM waves normal to the slopes at high frequencies. Run-time tests of the parallelized algorithm indicate that for meshes as large as 176 × 176 × 70 elements, MT forward responses and Jacobians can be calculated in ˜1.5 hr per frequency. Together with an efficient inversion parameter step described in Part II, MT inversion problems of 200-300 stations are computable with total run times

  6. Scanning Transmission X-ray Microscopy with X-ray Fluorescence Detection at the XUV Beamline P04, PETRA III, DESY

    Science.gov (United States)

    Andrianov, K.; Lühl, L.; Nisius, T.; Haidl, A.; Gnewkow, R.; Lötgering, L.; Dierks, H.; Kanngießer, B.; Wilhein, T.

    2017-06-01

    The presented scanning transmission x-ray microscope (STXM), build on top of our existing modular platform (FlexIX) for high resolution imaging experiments, allows versatile investigations of different samples. The FlexIX endstation allows to switch between a Full Field and a STXM mode. For the STXM mode we use a spatialy resolved detector together with an energy dispersive detector, this allows to investigate the morphology and the chemical or elemental distribution of the sample simultaneous. The combination of the nanoscopy endstation and the XUV beamline P04 results in a powerful tool for investigations of life science samples.

  7. SRX - a X-ray spectroscopy beamline with sub-100nm spatial resolution at NSLS-II

    Science.gov (United States)

    Thieme, J.

    2011-12-01

    J. Thieme, V. deAndrade, Y. Yao, J. Prietzel* (NSLS-II, Brookhaven National Laboratory, USA; *TU Munich, Germany) The new electron storage ring NSLS-II will be a source of synchrotron radiation with an unmatched low emittance. Such a facility is very well suited for hosting experiments in need of coherent radiation. One of first six beamlines to be constructed at NSLS-II will be a high resolution spectroscopy station, dedicated especially for environmental and geo-sciences. A canted setup of two undulators will serve as independent light sources for two branches of this beamline. One branch line is planned to address the energy range from 4.65 keV to 24 keV focusing the beam down to a small spot size with Kirkpatrick-Baez mirrors. The expected photon flux in the spot is in the range of above 10^13 phot/sec. A horizontally deflecting double crystal monochromator with maximum stability will ensure the possibility of spectroscopy with very high spectral resolution. The second branch is planned for reaching lower X-ray energies, addressing the range of 2 keV up to 15 keV, but with a higher spatial resolution. Using a Fresnel zoneplate, the spatial resolution aimed for is in the range of 30 nm. It can be expected that this branch would be attractive for more biological applications from environmental science due to the many elements of interest within that energy range. The experimental station will be designed to not only host X-ray fluorescence experiments but diffraction imaging experiments as well. The commissioning of this beamline will start in 2014, therefore a detailed design description will be presented here. As an example of what is achievable at this NSLS-II beamline we will present a spatially resolved study on the co-localization of iron and sulfur in a forest soil. The scientific topic to be addressed was to identify unambiguously the relationship between the speciation of iron and sulfur as a function of the chemical state of the surrounding soil when

  8. Stress Induced in the Periodontal Ligament under Orthodontic Loading (Part I): A Finite Element Method Study Using Linear Analysis.

    Science.gov (United States)

    Hemanth, M; Deoli, Shilpi; Raghuveer, H P; Rani, M S; Hegde, Chatura; Vedavathi, B

    2015-08-01

    Orthodontic tooth movement is a complex procedure that occurs due to various biomechanical changes in the periodontium. Optimal orthodontic forces yield maximum tooth movement whereas if the forces fall beyond the optimal threshold it can cause deleterious effects. Among various types of tooth movements intrusion and lingual root torque are associated with causing root resoprtion, especially with the incisors. Therefore in this study, the stress patterns in the periodontal ligament (PDL) were evaluated with intrusion and lingual root torque using finite element method (FEM). A three-dimensional (3D) FEM model of the maxillary incisors was generated using SOLIDWORKS modeling software. Stresses in the PDL were evaluated with intrusive and lingual root torque movements by a 3D FEM using ANSYS software using linear stress analysis. It was observed that with the application of intrusive load compressive stresses were distributed at the apex whereas tensile stress was seen at the cervical margin. With the application of lingual root torque maximum compressive stress was distributed at the apex and tensile stress was distributed throughout the PDL. For intrusive and lingual root torque movements stress values over the PDL was within the range of optimal stress value as proposed by Lee, with a given force system by Proffit as optimum forces for orthodontic tooth movement using linear properties.

  9. Upgrade of beamline BL08B at Taiwan Light Source from a photon-BPM to a double-grating SGM beamline.

    Science.gov (United States)

    Yuh, Jih Young; Lin, Shan Wei; Huang, Liang Jen; Fung, Hok Sum; Lee, Long Life; Chen, Yu Joung; Cheng, Chiu Ping; Chin, Yi Ying; Lin, Hong Ji

    2015-09-01

    During the last 20 years, beamline BL08B has been upgraded step by step from a photon beam-position monitor (BPM) to a testing beamline and a single-grating beamline that enables experiments to record X-ray photo-emission spectra (XPS) and X-ray absorption spectra (XAS) for research in solar physics, organic semiconductor materials and spinel oxides, with soft X-ray photon energies in the range 300-1000 eV. Demands for photon energy to extend to the extreme ultraviolet region for applications in nano-fabrication and topological thin films are increasing. The basic spherical-grating monochromator beamline was again upgraded by adding a second grating that delivers photons of energy from 80 to 420 eV. Four end-stations were designed for experiments with XPS, XAS, interstellar photoprocess systems (IPS) and extreme-ultraviolet lithography (EUVL) in the scheduled beam time. The data from these experiments show a large count rate in core levels probed and excellent statistics on background normalization in the L-edge adsorption spectrum.

  10. Prediction of part shape and associated material properties in hot-press forming using Unite element analysis

    Science.gov (United States)

    Kim, Hwigeon; Ha, Jinjin; Lee, Myoung-Gyu; Barlat, Frederic

    2016-08-01

    The hot-press forming of a U-channel was conducted on a boron-steel blank. The die consisted of two separate parts in order to perform the partial quenching process. The cold die was initially at 25 °C while the heated die was set to five different temperatures, namely, 25, 120, 220, 320 and 400 °C. The cooling temperature history, Vickers hardness and springback of the channel were measured. A thermo-mechanical-metallurgical model, which accounts for the prior austenite deformation effect, was successfully implemented in the LS-DYNA explicit solver to simulate the hot-press forming process under partial quenching conditions. The predicted and experimental results were compared and found in reasonable agreement.

  11. AI-BL1.0: a program for automatic on-line beamline optimization using the evolutionary algorithm.

    Science.gov (United States)

    Xi, Shibo; Borgna, Lucas Santiago; Zheng, Lirong; Du, Yonghua; Hu, Tiandou

    2017-01-01

    In this report, AI-BL1.0, an open-source Labview-based program for automatic on-line beamline optimization, is presented. The optimization algorithms used in the program are Genetic Algorithm and Differential Evolution. Efficiency was improved by use of a strategy known as Observer Mode for Evolutionary Algorithm. The program was constructed and validated at the XAFCA beamline of the Singapore Synchrotron Light Source and 1W1B beamline of the Beijing Synchrotron Radiation Facility.

  12. Geospatial risk assessment and trace element concentration in reef associated sediments, northern part of Gulf of Mannar biosphere reserve, Southeast Coast of India.

    Science.gov (United States)

    Krishnakumar, S; Ramasamy, S; Simon Peter, T; Godson, Prince S; Chandrasekar, N; Magesh, N S

    2017-08-21

    Fifty two surface sediments were collected from the northern part of the Gulf of Mannar biosphere reserve to assess the geospatial risk of sediments. We found that distribution of organic matter and CaCO3 distributions were locally controlled by the mangrove litters and fragmented coral debris. In addition, Fe and Mn concentrations in the marine sediments were probably supplied through the riverine input and natural processes. The Geo-accumulation of elements fall under the uncontaminated category except Pb. Lead show a wide range of contamination from uncontaminated-moderately contaminated to extremely contaminated category. The sediment toxicity level of the elements revealed that the majority of the sediments fall under moderately to highly polluted sediments (23.07-28.84%). The grades of potential ecological risk suggest that predominant sediments fall under low to moderate risk category (55.7-32.7%). The accumulation level of trace elements clearly suggests that the coral reef ecosystem is under low to moderate risk. Copyright © 2017. Published by Elsevier Ltd.

  13. Trace Element Abundance Measurements on Cosmic Dust Particles

    Science.gov (United States)

    Flynn, George

    1996-01-01

    The X-Ray Microprobe on beamline X-26A at the National Synchrotron Light Source (NSLS) at Brookhaven National Laboratory was used to determine the abundances of elements from Cr through Sr in individual interplanetary dust particles (IDPs) collected from the Earth's stratosphere and the Scanning Transmission X-ray Microscope (STXM) on beamline X-1A at the NSLS was used to determine the carbon abundances and spatial distributions in IDPs. In addition, modeling was performed in an attempt to associate particular types of IDPs with specific types of parent bodies, and thus to infer the chemistry, mineralogy, and structural properties of those parent bodies.

  14. MASSIF-1: a beamline dedicated to the fully automatic characterization and data collection from crystals of biological macromolecules

    Energy Technology Data Exchange (ETDEWEB)

    Bowler, Matthew W., E-mail: mbowler@embl.fr [European Molecular Biology Laboratory, Grenoble Outstation, 71 avenue des Martyrs, F-38042 Grenoble (France); Université Grenoble Alpes-EMBL-CNRS, 71 avenue des Martyrs, F-38042 Grenoble (France); Nurizzo, Didier, E-mail: mbowler@embl.fr; Barrett, Ray; Beteva, Antonia; Bodin, Marjolaine [European Synchrotron Radiation Facility, 71 avenue des Martyrs, F-38043 Grenoble (France)

    2015-10-03

    MASSIF-1 (ID30A-1) is a new beamline dedicated to the completely automatic characterization and data collection from crystals of biological macromolecules. MASSIF-1 (ID30A-1) is an ESRF undulator beamline operating at a fixed wavelength of 0.969 Å (12.8 keV) that is dedicated to the completely automatic characterization of and data collection from crystals of biological macromolecules. The first of the ESRF Upgrade MASSIF beamlines to be commissioned, it has been open since September 2014, providing a unique automated data collection service to academic and industrial users. Here, the beamline characteristics and details of the new service are outlined.

  15. Parallel three-dimensional magnetotelluric inversion using adaptive finite-element method. Part I: theory and synthetic study

    Science.gov (United States)

    Grayver, Alexander V.

    2015-07-01

    This paper presents a distributed magnetotelluric inversion scheme based on adaptive finite-element method (FEM). The key novel aspect of the introduced algorithm is the use of automatic mesh refinement techniques for both forward and inverse modelling. These techniques alleviate tedious and subjective procedure of choosing a suitable model parametrization. To avoid overparametrization, meshes for forward and inverse problems were decoupled. For calculation of accurate electromagnetic (EM) responses, automatic mesh refinement algorithm based on a goal-oriented error estimator has been adopted. For further efficiency gain, EM fields for each frequency were calculated using independent meshes in order to account for substantially different spatial behaviour of the fields over a wide range of frequencies. An automatic approach for efficient initial mesh design in inverse problems based on linearized model resolution matrix was developed. To make this algorithm suitable for large-scale problems, it was proposed to use a low-rank approximation of the linearized model resolution matrix. In order to fill a gap between initial and true model complexities and resolve emerging 3-D structures better, an algorithm for adaptive inverse mesh refinement was derived. Within this algorithm, spatial variations of the imaged parameter are calculated and mesh is refined in the neighborhoods of points with the largest variations. A series of numerical tests were performed to demonstrate the utility of the presented algorithms. Adaptive mesh refinement based on the model resolution estimates provides an efficient tool to derive initial meshes which account for arbitrary survey layouts, data types, frequency content and measurement uncertainties. Furthermore, the algorithm is capable to deliver meshes suitable to resolve features on multiple scales while keeping number of unknowns low. However, such meshes exhibit dependency on an initial model guess. Additionally, it is demonstrated

  16. CAT Guide and Beamline Directory. A key to APS Collaborative Access Teams

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1999-07-08

    The Advanced Photon Source (APS), a national user facility for synchrotrons radiation research, is located at Argonne National Laboratory, approximately 25 miles southwest of Chicago, Illinois. The APS is considered a third-generation synchrotrons radiation facility (specifically designed to accommodate insertion devices to serve as radiation sources) and is one of three such facilities in the world. Currently, it is the most brilliant source in the United States for research in such diverse fields as biology, medicine, materials science, chemistry, geology, agriculture and soil science, physics, and manufacturing technology. Researchers use the APS either as members of Collaborative Access Teams (CATS) or as Independent Investigators (IIs). CATS are responsible for designing, building, and operating beamlines in one or more sectors, each sector consisting of an insertion-device (ID) beamline and a bending-magnet (BM) beamline. Each beamline is designed to accommodate a specific type of research program(s) and is optimized accordingly. CAT members are entitled to use 75% of the available beam time to pursue CAT research goals. The remaining 25% of the available beam time must be made available to IIs. This document was written to help prospective IIs determine which beamlines are suitable for their specific experiments.

  17. Investigation of the heat handling capabilities of DIII-D neutral beamline internal components

    Energy Technology Data Exchange (ETDEWEB)

    Phillips, J.C.; Baxi, C.B.; Hong, R.

    1993-10-01

    The current DIII-D neutral beam system is a nominal five second pulse length upgrade of a previous design rated for only 500 msec operation. While the ion sources are rated for 60 sec operation, in practice pulse lengths are limited both by the beamline internal components ability to handle the fraction of the power which is scraped off, and by the power supplies ability to provide pulse lengths of greater than 5 sec. This paper examines the capability of the existing DIII-D neutral beamline heat removing components both in terms of present and desired operating parameters. To date, at 2.5 MW per ion source, pulses are limited to 3.5 sec by beamline internal components, while at lower ratings of 2.0 MW per ion source, up to 5 sec pulses have been achieved. Recent advances and demonstration of the extraction of 3.5 MW per DIII-D ion source give an even wider window of operating conditions. A full series of beamline thermocouple data has been collected to determine the heat loading and implied surface temperatures for the various DIII-D neutral beamline internal components. These data will be presented along with an analysis of the needs for specific component upgrades, given a desire for 10 sec operation.

  18. High resolution neutron imaging capabilities at BOA beamline at Paul Scherrer Institut

    Energy Technology Data Exchange (ETDEWEB)

    Tremsin, A.S., E-mail: ast@ssl.berkeley.edu [Space Sciences Laboratory, University of California at Berkeley, Berkeley, CA 94720 (United States); Morgano, M.; Panzner, T.; Lehmann, E.; Filgers, U. [Paul Scherrer Institut, 5232 Villigen PSI (Switzerland); Vallerga, J.V.; McPhate, J.B.; Siegmund, O.H.W. [Space Sciences Laboratory, University of California at Berkeley, Berkeley, CA 94720 (United States); Feller, W.B. [NOVA Scientific, Inc., 10 Picker Rd., Sturbridge, MA 01566 (United States)

    2015-06-01

    The cold neutron spectrum of the Beamline for neutron Optics and other Applications (BOA) at Paul Scherrer Institut enables high contrast neutron imaging because neutron cross sections for many materials increase with neutron wavelength. However, for many neutron imaging applications, spatial resolution can be as important as contrast. In this paper the neutron transmission imaging capabilities of an MCP/Timepix detector installed at the BOA beamline are presented, demonstrating the possibilities for studying sub-20 µm features in various samples. In addition to conventional neutron radiography and microtomography, the high degree of neutron polarization at the BOA beamline can be very attractive for imaging of magnetic fields, as demonstrated by our measurements. We also show that a collimated cold neutron beamline combined with a high resolution detector can produce image artifacts, (e.g. edge enhancements) due to neutron refraction and scattering. The results of our experiments indicate that the BOA beamline is a valuable addition to neutron imaging facilities, providing improved and sometimes unique capabilities for non-destructive studies with cold neutrons.

  19. Optimization of the design for beamline with fast polarization switching elliptically polarized undulators.

    Science.gov (United States)

    Cao, Jiefeng; Wang, Yong; Zou, Ying; Zhang, Xiangzhi; Wu, Yanqing; Tai, Renzhong

    2016-03-01

    Fast switching of X-ray polarization with a lock-in amplifier is a good method for acquiring weak signals from background noise for X-ray magnetic circular dichroism (XMCD) experiments. The usual way to obtain a beam with fast polarization switching is to use two series of elliptically polarized undulators (tandem twin EPUs). The two EPUs generate two individual beams. Each beam has a different polarization and is fast switched into the beamline. It is very important to ensure that the energy resolution, the flux and the spot size at the sample of the two beams are equal in XMCD experiments. However, it is difficult in beamline design because the distances from the two EPUs to the beamline optics are different and the beamline is not switchable. In this work, a beamline design without an entrance slit for fast polarization switching EPUs is discussed. The energy resolution of the two beams can be tuned to be equal by minor rotation of the optics in the monochromator. The flux of the two beams can be balanced through separation blades X, Y in the exit slit, and by adjusting the position of the X blades along the beam. The spot size of the two beams can be adjusted to be equal by shifting the sample as well.

  20. Development and calibration of mirrors and gratings for the soft x-ray materials science beamline at the Linac Coherent Light Source free-electron laser.

    Science.gov (United States)

    Soufli, Regina; Fernández-Perea, Mónica; Baker, Sherry L; Robinson, Jeff C; Gullikson, Eric M; Heimann, Philip; Yashchuk, Valeriy V; McKinney, Wayne R; Schlotter, William F; Rowen, Michael

    2012-04-20

    This work discusses the development and calibration of the x-ray reflective and diffractive elements for the Soft X-ray Materials Science (SXR) beamline of the Linac Coherent Light Source (LCLS) free-electron laser (FEL), designed for operation in the 500 to 2000 eV region. The surface topography of three Si mirror substrates and two Si diffraction grating substrates was examined by atomic force microscopy (AFM) and optical profilometry. The figure of the mirror substrates was also verified via surface slope measurements with a long trace profiler. A boron carbide (B4C) coating especially optimized for the LCLS FEL conditions was deposited on all SXR mirrors and gratings. Coating thickness uniformity of 0.14 nm root mean square (rms) across clear apertures extending to 205 mm length was demonstrated for all elements, as required to preserve the coherent wavefront of the LCLS source. The reflective performance of the mirrors and the diffraction efficiency of the gratings were calibrated at beamline 6.3.2 at the Advanced Light Source synchrotron. To verify the integrity of the nanometer-scale grating structure, the grating topography was examined by AFM before and after coating. This is to our knowledge the first time B4C-coated diffraction gratings are demonstrated for operation in the soft x-ray region.

  1. Light flux density threshold at which protein denaturation is induced by synchrotron radiation circular dichroism beamlines.

    Science.gov (United States)

    Miles, A J; Janes, Robert W; Brown, A; Clarke, D T; Sutherland, J C; Tao, Y; Wallace, B A; Hoffmann, S V

    2008-07-01

    New high-flux synchrotron radiation circular dichroism (SRCD) beamlines are providing important information for structural biology, but can potentially cause denaturation of the protein samples under investigation. This effect has been studied at the new CD1 dedicated SRCD beamline at ISA in Denmark, where radiation-induced thermal damage effects were observed, depending not only on the radiation flux but also on the focal spot size of the light. Comparisons with similar studies at other SRCD facilities worldwide has lead to the estimation of a flux density threshold under which SRCD beamlines should be operated when samples are to be exposed to low-wavelength vacuum ultraviolet radiation for extended periods of time.

  2. Effect of horizontal fast electron beam position feedback on the performance of ESRF beamlines

    CERN Document Server

    Pascarelli, S

    2001-01-01

    ESRF is a state of the art third generation synchrotron light source optimized to produce very bright and collimated hard X-ray beams using insertion devices. Instabilities of the electron beam, resulting in source point transverse displacements, spoil these outstanding beam qualities. At the beginning of operation a fast active feedback system was installed to damp the transverse motion of the electron beam in the vertical plane. Recently it became evident that also the relatively smaller horizontal instabilities may have specific detrimental effects on the operation of particularly sensitive beamlines. The dispersive XAS beamline (ID24) was the first to benefit from the activation of a local horizontal feedback. Optimized to perform time-resolved studies and high-pressure experiments, its operation was strongly perturbed. This paper briefly describes the work carried out to identify and solve these problems, presenting the outcome of the implementation of a fast orbit feedback on this beamline.

  3. Beamline for low-energy transport of highly charged ions at HITRAP

    Energy Technology Data Exchange (ETDEWEB)

    Andelkovic, Z., E-mail: z.andelkovic@gsi.de [GSI Helmholtzzentrum für Schwerionenforschung, Darmstadt (Germany); Herfurth, F.; Kotovskiy, N. [GSI Helmholtzzentrum für Schwerionenforschung, Darmstadt (Germany); König, K.; Maaß, B.; Murböck, T. [Technische Universität Darmstadt (Germany); Neidherr, D. [GSI Helmholtzzentrum für Schwerionenforschung, Darmstadt (Germany); Schmidt, S. [Technische Universität Darmstadt (Germany); Johannes Gutenberg-Universität Mainz (Germany); Steinmann, J. [GSI Helmholtzzentrum für Schwerionenforschung, Darmstadt (Germany); Hochschule Darmstadt (Germany); Vogel, M.; Vorobjev, G. [GSI Helmholtzzentrum für Schwerionenforschung, Darmstadt (Germany)

    2015-09-21

    A beamline for transport of highly charged ions with energies as low as a few keV/charge has been constructed and commissioned at GSI. Complementary to the existing infrastructure of the HITRAP facility for deceleration of highly charged ions from the GSI accelerator, the new beamline connects the HITRAP ion decelerator and an EBIT with the associated experimental setups. Therefore, the facility can now transport the decelerated heavy highly charged ions to the experiments or supply them offline with medium-heavy highly charged ions from the EBIT, both at energies as low as a few keV/charge. Here we present the design of the 20 m long beamline with the corresponding beam instrumentation, as well as its performance in terms of energy and transport efficiency.

  4. A double multilayer monochromator for the B16 Test beamline at the Diamond Light Source

    Science.gov (United States)

    Sawhney, K. J. S.; Dolbnya, I. P.; Scott, S. M.; Tiwari, M. K.; Preece, G. M.; Alcock, S. G.; Malandain, A. W.

    2011-09-01

    The B16 Test beamline at the Diamond Light Source is in user operation. It has been recently upgraded with the addition of a double multilayer monochromator (DMM), which provides further functionality and versatility to the beamline. The multilayer monochromator is equipped with two pairs of multilayer optics (Ni/B4C and Ru/B4C) to cover the wide photon energy range of 2 - 20 keV, with good efficiency. The DMM provides a broad bandpass / high flux operational mode for the beamline and, when used in tandem with the Si (111) double crystal monochromator, it gives a very high higher-order harmonics suppression. The design details of the DMM and the first commissioning results obtained using the DMM are presented.

  5. BEAMLINE-CONTROLLED STEERING OF SOURCE-POINT ANGLE AT THE ADVANCED PHOTON SOURCE

    Energy Technology Data Exchange (ETDEWEB)

    Emery, L.; Fystro, G.; Shang, H.; Smith, M.

    2017-06-25

    An EPICS-based steering software system has been implemented for beamline personnel to directly steer the angle of the synchrotron radiation sources at the Advanced Photon Source. A script running on a workstation monitors "start steering" beamline EPICS records, and effects a steering given by the value of the "angle request" EPICS record. The new system makes the steering process much faster than before, although the older steering protocols can still be used. The robustness features of the original steering remain. Feedback messages are provided to the beamlines and the accelerator operators. Underpinning this new steering protocol is the recent refinement of the global orbit feedback process whereby feedforward of dipole corrector set points and orbit set points are used to create a local steering bump in a rapid and seamless way.

  6. THERMAL FINITE ELEMENT ANALYSIS X9 AND X29 X-RAY RING CROTCH RADIATION ABSORBERS.

    Energy Technology Data Exchange (ETDEWEB)

    MERCADO-CORUJO,H.

    1999-08-11

    This report details the efforts by engineers at the National Synchrotron Light Source (NSLS) of Brookhaven National Laboratory (BNL) to evaluate the reliability of water-cooled radiation absorbers used in the NSLS X-ray ring. The absorbers on this report are part of the X-9 and X-29 dipole vacuum chambers. The absorbers are located at the intersection (crotch) of the beamline exit ports with the electron beam chamber, and are generally referred to as ''crotches''. The purpose of this analysis was to demonstrate the thermal reliability of the crotches under operating conditions that will be present over the expected life of the ring. The efforts described include general engineering layouts, engineering calculations, finite element analysis (FEA), results and conclusions of the analysis, and future design recommendations.

  7. High-brightness beamline for x-ray spectroscopy at the ALS

    Energy Technology Data Exchange (ETDEWEB)

    Perera, R.C.C.; Jones, G. [Ernest Orlando Lawrence Berkeley National Lab., CA (United States); Lindle, D.W. [Univ. of Nevada, Las Vegas, NV (United States)

    1997-04-01

    Beamline 9.3.1 at the Advanced Light Source (ALS) is a windowless beamline, covering the 1-6 keV photon-energy range, designed to achieve the goals of high energy resolution, high flux, and high brightness at the sample. When completed later this year, it will be the first ALS monochromatic hard x-ray beamline, and its brightness will be an order of magnitude higher than presently available in this energy range. In addition, it will provide flux and resolution comparable to any other beamline now in operation. To achieve these goals, two technical improvements, relative to existing x-ray beamlines, were incorporated. First, a somewhat novel optical design for x-rays, in which matched toroidal mirrors are positioned before and after the double-crystal monochromator, was adopted. This configuration allows for high resolution by passing a collimated beam through the monochromator, and for high brightness by focusing the ALS source on the sample with unit magnification. Second, a new {open_quotes}Cowan type{close_quotes} double-crystal monochromator based on the design used at NSLS beamline X-24A was developed. The measured mechanical precision of this new monochromator shows significant improvement over existing designs, without using positional feedback available with piezoelectric devices. Such precision is essential because of the high brightness of the radiation and the long distance (12 m) from the source (sample) to the collimating (focusing) mirror. This combination of features will provide a bright, high resolution, and stable x-ray beam for use in the x-ray spectroscopy program at the ALS.

  8. Finite Element Model to Analyze an Installation Load-based Stress-Strain State of the Parts Forming Gas Joint of a Medium-Speed Diesel Engine

    Directory of Open Access Journals (Sweden)

    N. D. Chainov

    2015-01-01

    Full Text Available The paper considers a developed computational model to study a stress-strain state of the assembly unit components of a medium-speed diesel engine of new generation, type CH26.5/31, which comprises a cylinder head, a sleeve, a gasket, a block, two mounting studs and four power studs.The developed three-dimensional finite element model presented in this article allows us to take into consideration all the components that make up a gas joint, regardless of their geometric complexity. Its use enables us to estimate the cylinder head - gasket - sleeve tightness of sealing when applying the mounting, temperature, and gas loads, to define the stress and strain components of parts, as well as to study the gasket condition, including pressure distribution across its surface.Based on the results obtained in the study the finite element model of the cylinder head was modified considering a more detailed description of its geometry, thus reducing the principal tensile stresses.

  9. Photostimulated phosphor based image plate detection system for HRVUV beamline at Indus-1 synchrotron radiation source

    OpenAIRE

    2014-01-01

    A high resolution vacuum ultraviolet (HRVUV) beamline based on a 6.65 meter off-plane Eagle spectrometer is in operation at the Indus-1 synchrotron radiation source, RRCAT, Indore, India. To facilitate position sensitive detection and fast spectral recording, a new BaFBr:Eu2+ phosphor based image plate (IP) detection system interchangeable with the existing photomultiplier (PMT) scanning system has been installed on this beamline. VUV photoabsorption studies on Xe, O2, N2O and SO2 are carried...

  10. Layout and first results of the nanotomography endstation at the P05 beamline at PETRA III

    Energy Technology Data Exchange (ETDEWEB)

    Ogurreck, M.; Greving, I.; Beckmann, F.; Wilde, F.; Müller, M. [Institute of Materials Research, Helmholtz–Zentrum Geesthacht (Germany); Marschall, F.; Vogt, H.; Last, A. [Institute of Microstructure Technology, Karlsruhe Institute of Technology (Germany); Rosario, J. J. do [Institute of Advanced Ceramics, Technical University Hamburg–Harburg (Germany); Leib, E. W. [Institute of Physical Chemistry, University of Hamburg (Germany)

    2016-01-28

    The Helmholtz-Zentrum Geesthacht operates the P05 Imaging Beamline at the DESY storage ring PETRA III. This beamline is dedicated to micro- and nanotomography with two endstations. This paper will present the nanotomography endstation layout and first results obtained from commissioning and test experiments. First tests have been performed with CRLs as X-ray objectives and newly developed rolled X-ray prism lenses as condenser optics. This setup allows a resolution of 100 nm half period with an effective detector pixel size of 15nm. A first tomograph of a photonic glass sample was measured in early 2014.

  11. CDApps: integrated software for experimental planning and data processing at beamline B23, Diamond Light Source

    Energy Technology Data Exchange (ETDEWEB)

    Hussain, Rohanah, E-mail: rohanah.hussain@diamond.ac.uk; Benning, Kristian; Javorfi, Tamas; Longo, Edoardo; Rudd, Timothy R.; Pulford, Bill; Siligardi, Giuliano, E-mail: rohanah.hussain@diamond.ac.uk [Diamond Light Source Ltd, Diamond House, Harwell Science and Innovation Campus, Didcot, Oxfordshire OX11 0DE (United Kingdom)

    2015-01-31

    CDApps software at Diamond B23 SRCD beamline is presented. The B23 Circular Dichroism beamline at Diamond Light Source has been operational since 2009 and has seen visits from more than 200 user groups, who have generated large amounts of data. Based on the experience of overseeing the users’ progress at B23, four key areas requiring the most assistance are identified: planning of experiments and note-keeping; designing titration experiments; processing and analysis of the collected data; and production of experimental reports. To streamline these processes an integrated software package has been developed and made available for the users. The subsequent article summarizes the main features of the software.

  12. Human placenta as a 'dual' biomarker for monitoring fetal and maternal environment with special reference to potentially toxic trace elements. Part 1: physiology, function and sampling of placenta for elemental characterisation.

    Science.gov (United States)

    Iyengar, G V; Rapp, A

    2001-12-03

    Choice of specimen from human subjects for monitoring pollutants proven to be detrimental to human health depends on the criteria chosen, namely real-time monitoring (RTM) or long-term monitoring (LTM). Specimens such as whole blood, urine, saliva and breast milk are commonly used from living subjects for RTM of toxic metals. However, sampling blood requires an invasive procedure. On the other hand, hair (with some limitations), bone (especially for the assessment of bone seeking elements), adipose tissue (mainly for organic pollutants) and liver (for both organic and inorganic toxicants) are used as specimens for LTM. With the exception of hair, generally these specimens are obtained at post-mortem. In context of health-related biomonitoring, placenta as a specimen has not received as much attention as it deserves. It is a unique sample requiring no invasive procedure, and offers possibilities for RTM, in particular as a dual purpose specimen for evaluating the pollutant burden exerted on the mother as well as on the fetus. Obtaining representative samples of placenta for elemental composition studies is a difficult task, because of heterogeneous mix of placental cells and decidual matter tainted with maternal and fetal blood. Therefore, the present sampling practices for placental tissue, and guidelines to safeguard the validity of the sampled material have been reviewed in part 1 with the following conclusions: medico-legal and ethical matters should be properly addressed before collecting the placenta; it is advisable to collect the entire placenta even if it includes the umbilical cord; further preparatory work is to be carried out in a clean laboratory and depends upon the purpose of the investigation; homogenising the entire sample may prove to be technically challenging but this step is crucial to obtain representative samples, handling the entire sample may be unavoidable; and an alternative method of procuring representative samples would require random

  13. Modeling the geochemical distribution of rare earth elements (REEs using multivariate statistics in the eastern part of Marvast placer, the Yazd province

    Directory of Open Access Journals (Sweden)

    Amin Hossein Morshedy

    2017-07-01

    Full Text Available Introduction Nowadays, exploration of rare earth element (REE resources is considered as one of the strategic priorities, which has a special position in the advanced and intelligent industries (Castor and Hedrick, 2006. Significant resources of REEs are found in a wide range of geological settings, including primary deposits associated with igneous and hydrothermal processes (e.g. carbonatite, (per alkaline-igneous rocks, iron-oxide breccia complexes, scarns, fluorapatite veins and pegmatites, and secondary deposits concentrated by sedimentary processes and weathering (e.g. heavy-mineral sand deposits, fluviatile sandstones, unconformity-related uranium deposits, and lignites (Jaireth et al., 2014. Recent studies on various parts of Iran led to the identification of promising potential of these elements, including Central Iran, alkaline rocks in the Eslami Peninsula, iron and apatite in the Hormuz Island, Kahnouj titanium deposit, granitoid bodies in Yazd, Azerbaijan, and Mashhad and associated dikes, and finally placers related to the Shemshak formation in Marvast, Kharanagh, and Ardekan indicate high concentration of REE in magmatogenic iron–apatite deposits in Central Iran and placers in Marvast area in Yazd (Ghorbani, 2013. Materials and methods In the present study, the geochemical behavior of rare earth elements is modeled by using multivariate statistical methods in the eastern part of the Marvast placer. Marvast is located 185 km south of the city of Yazd in central Iran between Yazd and Mehriz. This area lies within the southeastern part of the Sanandaj-Sirjan Zone (Alipour-Asll et al., 2012. The samples of 53 wells were analyzed for Whole-rock trace-element concentrations (including REE by inductively coupled plasma-mass spectrometry (ICP-MS (GSI, 2004. The clustering techniques such as multivariate statistical analysis technique can be employed to find appropriate groups in data sets. One of the main objectives of data clustering

  14. The variation of the unitary stresses occurring in the working part in relation to the type of soil, using the finite element method

    Science.gov (United States)

    Chiorescu, E.; Chiorescu, D.

    2017-08-01

    Agriculture brings a major contribution to the sustainable development of the economy, providing food to people. Because of the continuous growth of the population, there is an ever increasing need of food worldwide. For this reason, it is necessary to study the contact between the soil and the active tool of the cultivators, in relation to the type of soil and its parameters. The physical-mechanical characteristics of the soils are influenced by the moving velocity of the working part, as well as by the humidity of the soil. The humidity triggers the change of the friction coefficient at the soil-steel contact, being of significant importance for the decrease of the working resistance of the working tools and responsible for increasing exploitation costs. The model used for the soil has a non-linear plastic behavior of the Drucker Prager type, being different from the Mises model. The programming software Ansys was used for the simulation with the finite element method, allowing the study of the behavior of the active working part, the normal stress being analyzed in real conditions, at various depths and velocities for a soil with a clay-sandy texture.

  15. TIME-RESOLVED INFRARED SPECTROSCOPY IN THE U121R BEAMLINE AT THE NSLS

    Energy Technology Data Exchange (ETDEWEB)

    CARR,G.L.; LAVEIGNE,J.D.; LOBO,R.P.S.M.; REITZE,D.H.; TANNER,D.B.

    1999-07-19

    A facility for performing time-resolved infrared spectroscopy has been developed at the NSLS, primarily at beamline U12IR. The pulsed IR light from the synchrotron is used to perform pump-probe spectroscopy. The authors present here a description of the facility and results for the relaxation of photoexcitations in both a semiconductor and superconductor.

  16. Protein crystallography beamline BL2S1 at the Aichi synchrotron

    Science.gov (United States)

    Watanabe, Nobuhisa; Nagae, Takayuki; Yamada, Yusuke; Tomita, Ayana; Matsugaki, Naohiro; Tabuchi, Masao

    2017-01-01

    The protein crystallography beamline BL2S1, constructed at one of the 5 T superconducting bending-magnet ports of the Aichi synchrotron, is available to users associated with academic and industrial organizations. The beamline is mainly intended for use in X-ray diffraction measurements of single-crystals of macromolecules such as proteins and nucleic acids. Diffraction measurements for crystals of other materials are also possible, such as inorganic and organic compounds. BL2S1 covers the energy range 7–17 keV (1.8–0.7 Å) with an asymmetric-cut curved single-crystal monochromator [Ge(111) or Ge(220)], and a platinum-coated Si mirror is used for vertical focusing and as a higher-order cutoff filter. The beamline is equipped with a single-axis goniometer, a CCD detector, and an open-flow cryogenic sample cooler. High-pressure protein crystallography with a diamond anvil cell can also be performed using this beamline. PMID:28009576

  17. Protein crystallography beamline BL2S1 at the Aichi synchrotron

    Energy Technology Data Exchange (ETDEWEB)

    Watanabe, Nobuhisa; Nagae, Takayuki; Yamada, Yusuke; Tomita, Ayana; Matsugaki, Naohiro; Tabuchi, Masao (Nagoya); (Photon)

    2017-01-01

    The protein crystallography beamline BL2S1, constructed at one of the 5 T superconducting bending-magnet ports of the Aichi synchrotron, is available to users associated with academic and industrial organizations. The beamline is mainly intended for use in X-ray diffraction measurements of single-crystals of macromolecules such as proteins and nucleic acids. Diffraction measurements for crystals of other materials are also possible, such as inorganic and organic compounds. BL2S1 covers the energy range 7–17 keV (1.8–0.7 Å) with an asymmetric-cut curved single-crystal monochromator [Ge(111) or Ge(220)], and a platinum-coated Si mirror is used for vertical focusing and as a higher-order cutoff filter. The beamline is equipped with a single-axis goniometer, a CCD detector, and an open-flow cryogenic sample cooler. Lastly, high-pressure protein crystallography with a diamond anvil cell can also be performed using this beamline.

  18. One-dimensional numerical simulation of shock wave propagation induced by vacuum accidents in a beamline

    Energy Technology Data Exchange (ETDEWEB)

    Takiya, Toshio; Terada, Yukihiro; Komura, Akio [Hitachi Zosen Corp., Osaka (Japan); Higashino, Fumio; Miyajima, Shinichi; Ando, Masami

    1997-05-01

    A simulation for shock wave propagation in a vacuum tube has been conducted from the viewpoint of protection from vacuum accidents in beamlines of a synchrotron radiation facility. Inserted devices in beamlines such as absorbers, slits, masks and beryllium windows were replaced with orifices installed in a shock tube as a simulation model. One-dimensional Euler`s equations with friction terms were used for estimating the effects on shock wave decay as well as the effects of friction along a tube on shock attenuation. The results indicated that the entrance diameter of the shock tube was an important parameter for determining the strength of shock waves generated by the expansion of gases at the tube entrance and that the friction effects were too large to delay the arrival time of shock waves at the end of a long tube. Moreover, shock wave propagation in a long beamline model based on the MR beamline in the National Laboratory for High Energy Physics was simulated for designing adequate protection from vacuum accidents. The present simulation provides necessary information for the design of a protection system for vacuum accidents in other facilities. (author)

  19. Hard X-ray photoelectron spectroscopy on the GALAXIES beamline at the SOLEIL synchrotron

    Energy Technology Data Exchange (ETDEWEB)

    Céolin, D.; Ablett, J.M.; Prieur, D.; Moreno, T. [Synchrotron SOLEIL, l’Orme des Merisiers, Saint-Aubin, FR-91192 Gif-sur-Yvette Cedex (France); Rueff, J.-P. [Synchrotron SOLEIL, l’Orme des Merisiers, Saint-Aubin, FR-91192 Gif-sur-Yvette Cedex (France); Laboratoire de Chimie Physique-Matière et Rayonnement, Université Pierre et Marie Curie and CNRS UMR7614, FR-75231 Paris Cedex 05 (France); Marchenko, T.; Journel, L.; Guillemin, R.; Pilette, B.; Marin, T. [Laboratoire de Chimie Physique-Matière et Rayonnement, Université Pierre et Marie Curie and CNRS UMR7614, FR-75231 Paris Cedex 05 (France); Simon, M., E-mail: marc.simon@upmc.fr [Synchrotron SOLEIL, l’Orme des Merisiers, Saint-Aubin, FR-91192 Gif-sur-Yvette Cedex (France); Laboratoire de Chimie Physique-Matière et Rayonnement, Université Pierre et Marie Curie and CNRS UMR7614, FR-75231 Paris Cedex 05 (France)

    2013-10-15

    Highlights: ► We developed a new HAXPES endstation at the French synchrotron facility SOLEIL. ► The setup is operational for both solid state and gas phase experiments. ► Beamline performances allow working in the Auger Raman conditions. ► Beamline flux compensates for ionization cross section decrease at high photon energy. ► Spectrometer compensates for ionization cross section decrease at high photon energy. -- Abstract: We report on the newly operational HAXPES endstation located on the GALAXIES beamline of the SOLEIL French synchrotron facility. The photon energy provided by the beamline covers the 2.4–12 keV range, and electrons of kinetic energy up to 12 keV can be analyzed. The HAXPES station is comprised of a UHV analysis chamber designed for investigating both solid samples and gases for the first time at high kinetic energy, and a fully equipped preparation chamber. We present the first results of X-ray photoemission and photoabsorption collected with this setup.

  20. Photostimulated phosphor based image plate detection system for HRVUV beamline at Indus-1 synchrotron radiation source

    Science.gov (United States)

    Haris, K.; Singh, Param Jeet; Shastri, Aparna; Sunanda, K.; Babita, K.; Rao, S. V. N. Bhaskara; Ahmad, Shabbir; Tauheed, A.

    2014-12-01

    A high resolution vacuum ultraviolet (HRVUV) beamline based on a 6.65 m off-plane Eagle spectrometer is in operation at the Indus-1 synchrotron radiation source, RRCAT, Indore, India. To facilitate position sensitive detection and fast spectral recording, a new BaFBr:Eu2+ phosphor based image plate (IP) detection system interchangeable with the existing photomultiplier (PMT) scanning system has been installed on this beamline. VUV photoabsorption studies on Xe, O2, N2O and SO2 are carried out to evaluate the performance of the IP detection system. An FWHM of ~0.5 Å is achieved for the Xe atomic line at 1469.6 Å. Reproducibility of spectra is found to be within the experimental resolution. Compared to the PMT scanning system, the IP shows several advantages in terms of sensitivity, recording time and S/N ratio, which are highlighted in the paper. This is the first report of incorporation of an IP detection system in a VUV beamline using synchrotron radiation. Commissioning of the new detection system is expected to greatly enhance the utilization of the HRVUV beamline as a number of spectroscopic experiments which require fast recording times combined with a good signal to noise ratio are now feasible.

  1. CERN’s 2016 Beamline for Schools competition starts on 17 November

    CERN Multimedia

    2015-01-01

    Spread the word: CERN is offering high-school students from around the world the chance to create and perform a scientific experiment on a CERN accelerator beamline. What better way to learn about physics?    (Video: Noemi Caraban​/CERN ) Now in its third year, the Beamline for Schools competition is open to teams of at least five students aged 16 and with at least one adult supervisor or “coach”. Students can find out about the beamline and facilities via http://cern.ch/bl4s, then think of a simple, creative experiment. They can register their team from 17 November to start receiving e-mail updates. They then submit a written proposal and a short video by 31 March 2016. The winners will be announced in June and will come to CERN, preferably in September 2016. Previous winners have tested webcams and classroom-grown crystals at the beamline, others have studied how particles decay and investigated high-energy gamma rays. All participants will receive...

  2. Characterization of the high-energy neutron beam of the PRISMA beamline using a diamond detector

    Science.gov (United States)

    Cazzaniga, C.; Frost, C. D.; Minniti, T.; Schooneveld, E.; Perelli Cippo, E.; Tardocchi, M.; Rebai, M.; Gorini, G.

    2016-07-01

    The high-energy neutron component (En > 10 MeV) of the neutron spectrum of PRISMA, a beam-line at the ISIS spallation source, has been characterized for the first time. Neutron measurements using a Single-crystal Diamond Detector at a short-pulse source are obtained by a combination of pulse height and time of flight analysis. An XY scan provides a 2D map of the high-energy neutron beam which has a diameter of about 40 mm. The high neutron flux, that has been found to be (3.8 ± 0.7) · 105 cm-2s-1 for En > 10 MeV in the centre, opens up for a possible application of the beam-line as a high-energy neutron irradiation position. Results are of interest for the development of the ChipIR beam-line, which will feature an atmospheric-like neutron spectrum for chip irradiation experiment. Furthermore, these results demonstrate that diamond detectors can be used at spallation sources to investigate the transport of high-energy neutrons down instruments which is of interest in general to designers as high-energy neutrons are a source of background in thermal beamlines.

  3. The multi-purpose hard X-ray beamline BL10 at the DELTA storage ring.

    Science.gov (United States)

    Lützenkirchen-Hecht, D; Wagner, R; Szillat, S; Hüsecken, A K; Istomin, K; Pietsch, U; Frahm, Ronald

    2014-07-01

    The layout and the characteristics of the hard X-ray beamline BL10 at the superconducting asymmetric wiggler at the 1.5 GeV Dortmund Electron Accelerator DELTA are described. This beamline is equipped with a Si(111) channel-cut monochromator and is dedicated to X-ray studies in the spectral range from ∼4 keV to ∼16 keV photon energy. There are two different endstations available. While X-ray absorption studies in different detection modes (transmission, fluorescence, reflectivity) can be performed on a designated table, a six-axis kappa diffractometer is installed for X-ray scattering and reflectivity experiments. Different detector set-ups are integrated into the beamline control software, i.e. gas-filled ionization chambers, different photodiodes, as well as a Pilatus 2D-detector are permanently available. The performance of the beamline is illustrated by high-quality X-ray absorption spectra from several reference compounds. First applications include temperature-dependent EXAFS experiments from liquid-nitrogen temperature in a bath cryostat up to ∼660 K by using a dedicated furnace. Besides transmission measurements, fluorescence detection for dilute sample systems as well as surface-sensitive reflection-mode experiments are presented.

  4. The Structural Biology Center 19ID undulator beamline: facility specifications and protein crystallographic results.

    Science.gov (United States)

    Rosenbaum, Gerd; Alkire, Randy W; Evans, Gwyndaf; Rotella, Frank J; Lazarski, Krzystof; Zhang, Rong Guang; Ginell, Stephan L; Duke, Norma; Naday, Istvan; Lazarz, Jack; Molitsky, Michael J; Keefe, Lisa; Gonczy, John; Rock, Larry; Sanishvili, Ruslan; Walsh, Martin A; Westbrook, Edwin; Joachimiak, Andrzej

    2006-01-01

    The 19ID undulator beamline of the Structure Biology Center has been designed and built to take full advantage of the high flux, brilliance and quality of X-ray beams delivered by the Advanced Photon Source. The beamline optics are capable of delivering monochromatic X-rays with photon energies from 3.5 to 20 keV (3.5-0.6 A wavelength) with fluxes up to 8-18 x 10(12) photons s(-1) (depending on photon energy) onto cryogenically cooled crystal samples. The size of the beam (full width at half-maximum) at the sample position can be varied from 2.2 mm x 1.0 mm (horizontal x vertical, unfocused) to 0.083 mm x 0.020 mm in its fully focused configuration. Specimen-to-detector distances of between 100 mm and 1500 mm can be used. The high flexibility, inherent in the design of the optics, coupled with a kappa-geometry goniometer and beamline control software allows optimal strategies to be adopted in protein crystallographic experiments, thus maximizing the chances of their success. A large-area mosaic 3 x 3 CCD detector allows high-quality diffraction data to be measured rapidly to the crystal diffraction limits. The beamline layout and the X-ray optical and endstation components are described in detail, and the results of representative crystallographic experiments are presented.

  5. The variable polarization undulator beamline UE52 PGM nanocluster trap at BESSY II

    Directory of Open Access Journals (Sweden)

    Ruslan Ovsyannikov

    2017-02-01

    Full Text Available UE52 PGM nanocluster trap is a soft x-ray beamline at BESSY II that delivers an unfocussed low-divergence beam of variable polarization. Its characteristics are ideally suited for ion trap studies of magnetic properties.

  6. Front-end XY-slits assembly for the SPring-8 undulator beamlines.

    Science.gov (United States)

    Oura, M; Sakurai, Y; Kitamura, H

    1998-05-01

    A front-end XY-slits assembly has been designed for the SPring-8 undulator beamlines. This assembly can handle the high heat flux from the undulator, its grazing-incidence L-shaped configuration employing an enhanced heat-transfer technology.

  7. Investigation of collisional effects within the bending magnet region of a DIII-D neutral beamline

    Energy Technology Data Exchange (ETDEWEB)

    Kessler, D.N.; Hong, R.; Kellman, D.H.

    1993-10-01

    The region between the pole faces of the DIII-D neutral beamline residual ion bending magnets is an area of transient high gas pressure which may cause beam defocusing and increased heating of beamline internal components due to collisional effects. An investigation of these effects helps in understanding residual ion trajectories and in providing information for studying in the beamline capability for operation with increased pulse duration. Examination of collisional effects, and of the possible existence of space charge blow-up, was carried out by injecting deuterium gas into the region between the magnet pole faces with rates varying from 0 to 18 torr-{ell}/sec. Thermocouple and waterflow calorimetry data were taken to measure the beamline component heating and beam powder deposition on the magnet pole shields, magnet louvers, ion dump, beam collimators, and calorimeter. Data was also taken at gas flow rates varying from 0 to 25 torr-{ell}/sec into the neutralizer cell and is compared with the magnet region gas injection data obtained. Results show that both collisional effects and space charge blow-up play a role in magnet region component heating and that neutralizer gas flow sufficiently reduces component heating without incurring unacceptable power losses through collisional effects.

  8. Rossendorf Beamline at ESRF (ROBL-CRG). Bi-annual report 2009/2010

    Energy Technology Data Exchange (ETDEWEB)

    Scheinost, Andreas C.; Baehtz, Carsten (eds.)

    2011-07-01

    The Rossendorf Beamline (ROBL) - located at BM20 of the European Synchrotron Radiation Facility (ESRF) in Grenoble, France - is in operation since 1998. This 7th report covers the period from January 2009 to December 2010. In these two years, 67 peer- reviewed papers have been published based on experiments done at the beamline, more than in any biannual period before. Six highlight reports have been selected for this report to demonstrate the scientific strength and diversity of the experiments performed on the two end-stations of the beamline, dedicated to Radiochemistry (RCH) and Materials Research (MRH). The beamtime was more heavily overbooked than ever before, with an acceptance rate of only 25% experiments. We would like to thank our external proposal review members, Prof. Andre Maes (KU Leuven, Belgium), Prof. Laurent Charlet (UJF Grenoble, France), Dr. Andreas Leinweber (MPI Metallforschung, Stuttgart, Germany), Prof. David Rafaja (TU Bergakademie Freiberg, Germany), Prof. Dirk Meyer (TU Dresden, Germany), who evaluated the inhouse proposals in a thorough manner, thereby ensuring that beamtime was distributed according to scientific merit. The period was not only characterized by very successful science, but also by intense work on the optics upgrade. In spring 2009, a workshop was held at ROBL, assembling beamline experts from German, Spanish and Swiss synchrotrons, to evaluate the best setup for the new optics. These suggestions was used to prepare the call for tender published in July 2009. From the tender acceptance in November 2009 on, a series of design review meetings and factory acceptance tests followed. Already in July 2010, the first piece of equipment was delivered, the new double-crystal, double-multilayer monochromator. The disassembly of the old optics components started end of July, 2011, followed by the installation of the new components. As of December 2011, the new optics have seen the first test beam and thorough hot commissioning will

  9. Combustion of Biosolids in a Bubbling Fluidized Bed, Part 1: Main Ash-Forming Elements and Ash Distribution with a Focus on Phosphorus

    Science.gov (United States)

    2014-01-01

    This is the first in a series of three papers describing combustion of biosolids in a 5-kW bubbling fluidized bed, the ash chemistry, and possible application of the ash produced as a fertilizing agent. This part of the study aims to clarify whether the distribution of main ash forming elements from biosolids can be changed by modifying the fuel matrix, the crystalline compounds of which can be identified in the raw materials and what role the total composition may play for which compounds are formed during combustion. The biosolids were subjected to low-temperature ashing to investigate which crystalline compounds that were present in the raw materials. Combustion experiments of two different types of biosolids were conducted in a 5-kW benchscale bubbling fluidized bed at two different bed temperatures and with two different additives. The additives were chosen to investigate whether the addition of alkali (K2CO3) and alkaline-earth metal (CaCO3) would affect the speciation of phosphorus, so the molar ratios targeted in modified fuels were P:K = 1:1 and P:K:Ca = 1:1:1, respectively. After combustion the ash fractions were collected, the ash distribution was determined and the ash fractions were analyzed with regards to elemental composition (ICP-AES and SEM-EDS) and part of the bed ash was also analyzed qualitatively using XRD. There was no evidence of zeolites in the unmodified fuels, based on low-temperature ashing. During combustion, the biosolid pellets formed large bed ash particles, ash pellets, which contained most of the total ash content (54%–95% (w/w)). This ash fraction contained most of the phosphorus found in the ash and the only phosphate that was identified was a whitlockite, Ca9(K,Mg,Fe)(PO4)7, for all fuels and fuel mixtures. With the addition of potassium, cristobalite (SiO2) could no longer be identified via X-ray diffraction (XRD) in the bed ash particles and leucite (KAlSi2O6) was formed. Most of the alkaline-earth metals calcium and

  10. Study on pressure at top part of man's socks using finite element method%男短袜袜口压力的有限元研究

    Institute of Scientific and Technical Information of China (English)

    覃蕊; 范雪荣; 陈东生; 王强

    2011-01-01

    The key for optimal designing of a garment lies in understanding the pressure which has been brought about by the garment on the human body. 3-D body scanning instrument is used to scan the morphology of the inside part of the leg 6 cm above the ankle, and the relationship between the pressure brought about on the leg by the top of socks and the displacement is investigated using finite element method. In this study, the human body is regarded as an elastomer and the contact between the lower leg and the top part of socks is elastic contact. After using finite element analysis and fitting curves, the pressure-displacement quadratic equation can be obtained. Meanwhile, we divide the lower leg cross section into four equal regions according to the angle, and the area shrinkage of each region under pressure can be calculated. And finally, we analyze the relationship between factors that affect pressure levels, and then obtain a function formula between pressure and impact factors by principal component analysis.%人体与服装之间的压力研究是服装优化设计的关键.通过三维人体扫描仪对人体内侧脚踝点水平向上6 cm处腿部形态进行扫描,并运用有限元模拟男短袜袜口对腿部施压后压力与位移的关系.研究中,人体视为弹性体.腿部与袜口之间的接触视为弹性接触,通过有限元分析及曲线拟合,可得到压力与位移间的函数关系,同时按照角度将腿截面等分为4个区域,并计算出各区域受压后的总面积缩量.此外,还分析了影响压力水平的各因素之间关系,并通过主成分分析得到压力与各因素之间的函数关系式.

  11. Development of the XFP beamline for x-ray footprinting at NSLS-II

    Energy Technology Data Exchange (ETDEWEB)

    Bohon, Jen, E-mail: jbohon@bnl.gov; Sullivan, Michael; Abel, Don; Toomey, John; Chance, Mark R., E-mail: mark.chance@case.edu [Case Center for Synchrotron Biosciences, Center for Proteomics and Bioinformatics, Case Western Reserve University, Cleveland, OH (United States); Dvorak, Joseph [Brookhaven National Laboratory, Upton, NY (United States)

    2016-07-27

    For over a decade, synchrotron-based footprinting studies at the NSLS X28C beamline have provided unique insights and approaches for examining the solution-state structures of large macromolecular assemblies, membrane proteins, and soluble proteins, for time-resolved studies of macromolecular dynamics, and most recently for in vivo studies of RNA-protein complexes. The transition from NSLS to NSLS-II has provided the opportunity to create an upgraded facility for the study of increasingly complex systems; progress on the development of the XFP (X-ray Footprinting for In Vitro and In Vivo Structural Studies of Biological Macromolecules) beamline at NSLS-II is presented here. The XFP beamline will utilize a focused 3-pole wiggler source to deliver a high flux density x-ray beam, where dynamics can be studied on the microsecond to millisecond timescales appropriate for probing biological macromolecules while minimizing sample perturbation. The beamline optics and diagnostics enable adaptation of the beam size and shape to accommodate a variety of sample morphologies with accurate measurement of the incident beam, and the upgrades in sample handling and environment control will allow study of highly sensitive or unstable samples. The XFP beamline is expected to enhance relevant flux densities more than an order of magnitude from that previously available at X28C, allowing static and time-resolved structural analysis of highly complex samples that have previously pushed the boundaries of x-ray footprinting technology. XFP, located at NSLS-II 17-BM, is anticipated to become available for users in 2016.

  12. 7-GeV advanced photon source beamline initiative: Conceptual design report

    Energy Technology Data Exchange (ETDEWEB)

    1993-05-01

    The DOE is building a new generation 6-7 GeV Synchrotron Radiation Source known as the Advanced Photon Source (APS) at Argonne National Laboratory. This facility, to be completed in FY 1996, can provide 70 x-ray sources of unprecedented brightness to meet the research needs of virtually all scientific disciplines and numerous technologies. The technological research capability of the APS in the areas of energy, communications and health will enable a new partnership between the DOE and US industry. Current funding for the APS will complete the current phase of construction so that scientists can begin their applications in FY 1996. Comprehensive utilization of the unique properties of APS beams will enable cutting-edge research not currently possible. It is now appropriate to plan to construct additional radiation sources and beamline standard components to meet the excess demands of the APS users. In this APS Beamline Initiative, 2.5-m-long insertion-device x-ray sources will be built on four straight sections of the APS storage ring, and an additional four bending-magnet sources will also be put in use. The front ends for these eight x-ray sources will be built to contain and safeguard access to these bright x-ray beams. In addition, funds will be provided to build standard beamline components to meet scientific and technological research demands of the Collaborative Access Teams. The Conceptual Design Report (CDR) for the APS Beamline Initiative describes the scope of all the above technical and conventional construction and provides a detailed cost and schedule for these activities. The document also describes the preconstruction R&D plans for the Beamline Initiative activities and provides the cost estimates for the required R&D.

  13. Photostimulated phosphor based image plate detection system for HRVUV beamline at Indus-1 synchrotron radiation source

    Energy Technology Data Exchange (ETDEWEB)

    Haris, K. [Department of Physics, Aligarh Muslim University, Aligarh 202002 (India); Singh, Param Jeet [Atomic and Molecular Physics Division, Bhabha Atomic Research Centre, Mumbai 400085 (India); Shastri, Aparna, E-mail: ashastri@barc.gov.in [Atomic and Molecular Physics Division, Bhabha Atomic Research Centre, Mumbai 400085 (India); Sunanda, K.; Babita, K.; Rao, S.V.N. Bhaskara [Atomic and Molecular Physics Division, Bhabha Atomic Research Centre, Mumbai 400085 (India); Ahmad, Shabbir; Tauheed, A. [Department of Physics, Aligarh Muslim University, Aligarh 202002 (India)

    2014-12-11

    A high resolution vacuum ultraviolet (HRVUV) beamline based on a 6.65 m off-plane Eagle spectrometer is in operation at the Indus-1 synchrotron radiation source, RRCAT, Indore, India. To facilitate position sensitive detection and fast spectral recording, a new BaFBr:Eu{sup 2+} phosphor based image plate (IP) detection system interchangeable with the existing photomultiplier (PMT) scanning system has been installed on this beamline. VUV photoabsorption studies on Xe, O{sub 2}, N{sub 2}O and SO{sub 2} are carried out to evaluate the performance of the IP detection system. An FWHM of ∼0.5 Å is achieved for the Xe atomic line at 1469.6 Å. Reproducibility of spectra is found to be within the experimental resolution. Compared to the PMT scanning system, the IP shows several advantages in terms of sensitivity, recording time and S/N ratio, which are highlighted in the paper. This is the first report of incorporation of an IP detection system in a VUV beamline using synchrotron radiation. Commissioning of the new detection system is expected to greatly enhance the utilization of the HRVUV beamline as a number of spectroscopic experiments which require fast recording times combined with a good signal to noise ratio are now feasible. - Highlights: • Incorporation of an image plate detection system on HRVUV beamline at Indus-1. • Design and fabrication of mounting mechanisms, performance evaluation of new system. • Photoabsorption spectra of Xe, O{sub 2}, SO{sub 2} and N{sub 2}O recorded in the region 1150–2300 Å. • Sensitivity, wavelength coverage, reproducibility and resolution of IP demonstrated. • First report of IP detector for VUV photoabsorption using synchrotron radiation.

  14. Soft-X-ray ARPES facility at the ADRESS beamline of the SLS: concepts, technical realisation and scientific applications.

    Science.gov (United States)

    Strocov, V N; Wang, X; Shi, M; Kobayashi, M; Krempasky, J; Hess, C; Schmitt, T; Patthey, L

    2014-01-01

    Soft-X-ray angle-resolved photoelectron spectroscopy (ARPES) with photon energies around 1 keV combines the momentum space resolution with increasing probing depth. The concepts and technical realisation of the new soft-X-ray ARPES endstation at the ADRESS beamline of SLS are described. The experimental geometry of the endstation is characterized by grazing X-ray incidence on the sample to increase the photoyield and vertical orientation of the measurement plane. The vacuum chambers adopt a radial layout allowing most efficient sample transfer. High accuracy of the angular resolution is ensured by alignment strategies focused on precise matching of the X-ray beam and optical axis of the analyzer. The high photon flux of up to 10(13) photons s(-1) (0.01% bandwidth)(-1) delivered by the beamline combined with the optimized experimental geometry break through the dramatic loss of the valence band photoexcitation cross section at soft-X-ray energies. ARPES images with energy resolution up to a few tens of meV are typically acquired on the time scale of minutes. A few application examples illustrate the power of our advanced soft-X-ray ARPES instrumentation to explore the electronic structure of bulk crystals with resolution in three-dimensional momentum, access buried heterostructures and study elemental composition of the valence states using resonant excitation.

  15. Focusing, collimation and flux throughput at the IMCA-CAT bending-magnet beamline at the Advanced Photon Source

    Energy Technology Data Exchange (ETDEWEB)

    Koshelev, Irina; Huang, Rong; Graber, Timothy; Meron, Mati; Muir, J. Lewis; Lavender, William; Battaile, Kevin; Mulichak, Anne M.; Keefe, Lisa J.; (IIT); (UC)

    2009-09-02

    The IMCA-CAT bending-magnet beamline was upgraded with a collimating mirror in order to achieve the energy resolution required to conduct high-quality multi- and single-wavelength anomalous diffraction (MAD/SAD) experiments without sacrificing beamline flux throughput. Following the upgrade, the bending-magnet beamline achieves a flux of 8 x 10{sup 11} photons s{sup -1} at 1 {angstrom} wavelength, at a beamline aperture of 1.5 mrad (horizontal) x 86 {mu}rad (vertical), with energy resolution (limited mostly by the intrinsic resolution of the monochromator optics) {delta}E/E = 1.5 x 10{sup -4} (at 10 kV). The beamline operates in a dynamic range of 7.5-17.5 keV and delivers to the sample focused beam of size (FWHM) 240 {micro}m (horizontally) x 160 {micro}m (vertically). The performance of the 17-BM beamline optics and its deviation from ideally shaped optics is evaluated in the context of the requirements imposed by the needs of protein crystallography experiments. An assessment of flux losses is given in relation to the (geometric) properties of major beamline components.

  16. Focusing, collimation and flux throughput at the IMCA-CAT bending-magnet beamline at the Advanced Photon Source.

    Science.gov (United States)

    Koshelev, Irina; Huang, Rong; Graber, Timothy; Meron, Mati; Muir, J Lewis; Lavender, William; Battaile, Kevin; Mulichak, Anne M; Keefe, Lisa J

    2009-09-01

    The IMCA-CAT bending-magnet beamline was upgraded with a collimating mirror in order to achieve the energy resolution required to conduct high-quality multi- and single-wavelength anomalous diffraction (MAD/SAD) experiments without sacrificing beamline flux throughput. Following the upgrade, the bending-magnet beamline achieves a flux of 8 x 10(11) photons s(-1) at 1 A wavelength, at a beamline aperture of 1.5 mrad (horizontal) x 86 microrad (vertical), with energy resolution (limited mostly by the intrinsic resolution of the monochromator optics) deltaE/E = 1.5 x 10(-4) (at 10 kV). The beamline operates in a dynamic range of 7.5-17.5 keV and delivers to the sample focused beam of size (FWHM) 240 microm (horizontally) x 160 microm (vertically). The performance of the 17-BM beamline optics and its deviation from ideally shaped optics is evaluated in the context of the requirements imposed by the needs of protein crystallography experiments. An assessment of flux losses is given in relation to the (geometric) properties of major beamline components.

  17. Construction Status of the Beamline for Radio-Isotope Production in the Korea Multi-purpose Accelerator Complex

    Energy Technology Data Exchange (ETDEWEB)

    Chung, B. H.; Yoon, S. P.; Seol, K. T.; Kim, H. S.; Kwon, H. J.; Cho, Y. S. [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2015-10-15

    The 100-MeV beamline consist of 5 target room, a TR 103 as one of these is operating beamline, and a TR 101 as the other beamline is under construction as shown in Fig. 1. The TR 101 as beamline target room will be used for the high value-added medical isotope production and increased utilization of the proton accelerator. The optical system of the beamline consisted of dipole and quadrupole, and it included beam position monitor (BPM) and current transformer (CT) for beam diagnostics. The beamline was inserted into the carbon block and the aluminum collimator, the end of pipe as beam window was used for the aluminum to reduce the radioactive of materials. The target transfer equipment is being installed for RI production. The RI Beamline was aligned using the laser tracker, and vacuum leak was not detected by the helium leak detector. This facility is expected to the high value-added medical isotope production and increased utilization of the proton accelerator.

  18. 3-dimensional magnetotelluric inversion including topography using deformed hexahedral edge finite elements and direct solvers parallelized on symmetric multiprocessor computers - Part II: direct data-space inverse solution

    Science.gov (United States)

    Kordy, M.; Wannamaker, P.; Maris, V.; Cherkaev, E.; Hill, G.

    2016-01-01

    Following the creation described in Part I of a deformable edge finite-element simulator for 3-D magnetotelluric (MT) responses using direct solvers, in Part II we develop an algorithm named HexMT for 3-D regularized inversion of MT data including topography. Direct solvers parallelized on large-RAM, symmetric multiprocessor (SMP) workstations are used also for the Gauss-Newton model update. By exploiting the data-space approach, the computational cost of the model update becomes much less in both time and computer memory than the cost of the forward simulation. In order to regularize using the second norm of the gradient, we factor the matrix related to the regularization term and apply its inverse to the Jacobian, which is done using the MKL PARDISO library. For dense matrix multiplication and factorization related to the model update, we use the PLASMA library which shows very good scalability across processor cores. A synthetic test inversion using a simple hill model shows that including topography can be important; in this case depression of the electric field by the hill can cause false conductors at depth or mask the presence of resistive structure. With a simple model of two buried bricks, a uniform spatial weighting for the norm of model smoothing recovered more accurate locations for the tomographic images compared to weightings which were a function of parameter Jacobians. We implement joint inversion for static distortion matrices tested using the Dublin secret model 2, for which we are able to reduce nRMS to ˜1.1 while avoiding oscillatory convergence. Finally we test the code on field data by inverting full impedance and tipper MT responses collected around Mount St Helens in the Cascade volcanic chain. Among several prominent structures, the north-south trending, eruption-controlling shear zone is clearly imaged in the inversion.

  19. Thermal treatment of stabilized air pollution control residues in a waste incinerator pilot plant. Part 1: Fate of elements and dioxins.

    Science.gov (United States)

    Bergfeldt, Brita; Jay, Klaus; Seifert, Helmuth; Vehlow, Jürgen; Christensen, Thomas H; Baun, Dorthe L; Mogensen, Erhardt P B

    2004-02-01

    Air pollution control (APC) residues from municipal solid waste incinerator plants that are treated by means of the Ferrox process can be more safely disposed of due to reduction of soluble salts and stabilization of heavy metals in an iron oxide matrix. Further stabilization can be obtained by thermal treatment inside a combustion chamber of a municipal solid waste incinerator. The influence of the Ferrox products on the combustion process, the quality of the residues, and the partitioning of heavy metals between the various solids and the gas have been investigated in the Karlsruhe TAM-ARA pilot plant for waste incineration. During the experiments only few parameters were influenced. An increase in the SO2 concentration in the raw gas and slightly lower temperatures in the fuel bed could be observed compared with reference tests. Higher contents of Fe and volatile heavy metals such as Zn, Cd, Pb and partly Hg in the Ferrox products lead to increased concentration of these elements in the solid residues of the co-feeding tests. Neither the burnout nor the PCDD/F formation was altered by the addition of the Ferrox products. Co-feeding of treated APC residues seems to be a feasible approach for obtaining a single solid residue from waste incineration.

  20. ARF-B2: A Protein Complex that Specifically Binds to Part of the Anaerobic Response Element of Maize Adh 11

    Science.gov (United States)

    Ferl, Robert J.

    1990-01-01

    Crude whole cell extracts from maize (Zea mays L.) suspension cells were examined for DNA binding proteins that specifically interact with a portion of the maize Adh 1 promoter that was previously shown to be in contact with a trans-acting factor in vivo. A 17 base pair, double-stranded oligonucleotide probe was constructed that centered around a strong in vivo dimethylsulfate footprint (B2) that coincides with part of the anaerobic response element (ARE). Gel retardation assays were used to characterize a major, specific DNA binding protein activity found in the crude extracts. The activity is present in both aerobic and hypoxically treated cultures and has been designated ARF-B2 (ARE binding factor). ARF-B2 appears to be a multicomponent complex, with a 54 kilodalton subunit termed ARF-B2α in primary contact with the target DNA. Images Figure 2 Figure 3 Figure 4 Figure 5 Figure 6 Figure 7 Figure 8 Figure 9 PMID:16667563

  1. SEVERAL ELEMENTS OF THE MULTI-RESOLUTION WAVELET ANALYSIS. Part 1: BASICS OF THE WAVELETS AND THE MULTI-RESOLUTION WAVELET ANALYSIS

    Directory of Open Access Journals (Sweden)

    Akimov Pavel Alekseevich

    2012-10-01

    Full Text Available Part 1 of this paper represents an introduction into the multi-resolution wavelet analysis. The wavelet-based analysis is an exciting new problem-solving tool used by mathematicians, scientists and engineers. In the paper, the authors try to present the fundamental elements of the multi-resolution wavelet analysis in a way that is accessible to an engineer, a scientist and an applied mathematician both as a theoretical approach and as a potential practical method of solving problems (particularly, boundary problems of structural mechanics and mathematical physics. The main goal of the contemporary wavelet research is to generate a set of basic functions (or general expansion functions and transformations that will provide an informative, efficient and useful description of a function or a signal. Another central idea is that of multi-resolution whereby decomposition of a signal represents the resolution of the detail. The multi-resolution decomposition seems to separate components of a signal in a way that is superior to most other methods of analysis, processing or compression. Due to the ability of the discrete wavelet transformation technique to decompose a signal at different independent scaling levels and to do it in a very flexible way, wavelets can be named "the microscopes of mathematics". Indeed, the use of the wavelet analysis and wavelet transformations requires a new point of view and a new method of interpreting representations.

  2. Measurement of the polarization for soft x-ray magnetic circular dichroism at the BSRF beamline 4B7B

    CERN Document Server

    Zhi-Ying, Guo; Jing-Tao, Zhu; YI-Dong, Zhao; Lei, Zheng; Cai-Hao, Hong; Kun, Tang; Dong-Liang, Yang; Ming-Qi, Cui

    2012-01-01

    Three ultra-short-period W/B4C multilayers (1.244nm, 1.235nm and 1.034nm) have been fabricated and used for polarization measurement at the 4B7B Beamline of Beijing Synchrotron Radiation Facility (BSRF). By rotating analyzer ellipsometry method, the linear polarization degree of light emerging from this beamline has been measured and the circular polarization evaluated for 700eV-860eV. The first soft x-ray magnetic circular dichroism measurements are carried out at BSRF by positioning the beamline aperture out of the plane of the electron storage ring.

  3. MASSIF-1: a beamline dedicated to the fully automatic characterization and data collection from crystals of biological macromolecules

    Science.gov (United States)

    Bowler, Matthew W.; Nurizzo, Didier; Barrett, Ray; Beteva, Antonia; Bodin, Marjolaine; Caserotto, Hugo; Delagenière, Solange; Dobias, Fabian; Flot, David; Giraud, Thierry; Guichard, Nicolas; Guijarro, Mattias; Lentini, Mario; Leonard, Gordon A.; McSweeney, Sean; Oskarsson, Marcus; Schmidt, Werner; Snigirev, Anatoli; von Stetten, David; Surr, John; Svensson, Olof; Theveneau, Pascal; Mueller-Dieckmann, Christoph

    2015-01-01

    MASSIF-1 (ID30A-1) is an ESRF undulator beamline operating at a fixed wavelength of 0.969 Å (12.8 keV) that is dedicated to the completely automatic characterization of and data collection from crystals of biological macromolecules. The first of the ESRF Upgrade MASSIF beamlines to be commissioned, it has been open since September 2014, providing a unique automated data collection service to academic and industrial users. Here, the beamline characteristics and details of the new service are outlined. PMID:26524320

  4. Executive summary of major NuMI lessons learned: a review of relevant meetings of Fermilab's DUSEL Beamline Working Group

    Energy Technology Data Exchange (ETDEWEB)

    Andrews, Mike; Appel, Jeffrey A.; Bogert, Dixon; Childress, Sam; Cossairt, Don; Griffing, William; Grossman, Nancy; Harding, David; Hylen, Jim; Kuchler, Vic; Laughton, Chris; /Fermilab /Argonne /Brookhaven /LBL, Berkeley

    2009-05-01

    We have gained tremendous experience with the NuMI Project on what was a new level of neutrino beams from a high power proton source. We expect to build on that experience for any new long baseline neutrino beam. In particular, we have learned about some things which have worked well and/or where the experience is fairly directly applicable to the next project (e.g., similar civil construction issues including: tunneling, service buildings, outfitting, and potential claims/legal issues). Some things might be done very differently (e.g., decay pipe, windows, target, beam dump, and precision of power supply control/monitoring). The NuMI experience does lead to identification of critical items for any future such project, and what issues it will be important to address. The DUSEL Beamline Working Group established at Fermilab has been meeting weekly to collect and discuss information from that NuMI experience. This document attempts to assemble much of that information in one place. In this Executive Summary, we group relevant discussion of some of the major issues and lessons learned under seven categories: (1) Differences Between the NuMI Project and Any Next Project; (2) The Process of Starting Up the Project; (3) Decision and Review Processes; (4) ES&H: Environment, Safety, and Health; (5) Local Community Buy-In; (6) Transition from Project Status to Operation; and (7) Some Lessons on Technical Elements. We concentrate here on internal project management issues, including technical areas that require special attention. We cannot ignore, however, two major external management problems that plagued the NuMI project. The first problem was the top-down imposition of an unrealistic combination of scope, cost, and schedule. This situation was partially corrected by a rebaselining. However, the full, desirable scope was never achievable. The second problem was a crippling shortage of resources. Critical early design work could not be done in a timely fashion, leading to

  5. X-ray absorption spectroscopy of diluted system by undulator photon source and multi-element solid-state detector

    CERN Document Server

    Tanida, H

    2001-01-01

    In order to measure the extended X-ray absorption fine structure (EXAFS) spectrum of an ultra-diluted system, an optics and detector control system for a synchrotron radiation beamline is developed. The undulator gap width is continuously tuned to obtain the maximum X-ray photon flux during the energy scan for the EXAFS measurement. A piezoelectric translator optimizes the parallelism of the double crystal in a monochromator at each measurement point to compensate for mechanical errors of the monochromator, resulting in a smooth and intense X-ray photon flux during the measurement. For a detection of a weak fluorescence signal from diluted samples, a 19-element solid-state detector and digital signal processor are used. A K-edge EXAFS spectrum of iron in a myoglobin aqueous solution with a concentration of 5.58 parts per million was obtained by this system.

  6. A dedicated superbend x-ray microdiffraction beamline for materials, geo-, and environmental sciences at the advanced light source

    Energy Technology Data Exchange (ETDEWEB)

    Advanced Light Source; Kunz, Martin; Tamura, Nobumichi; Chen, Kai; MacDowell, Alastair A.; Celestre, Richard S.; Church, Matthew M.; Fakra, Sirine; Domning, Edward E.; Glossinger, James M.; Kirschman, Jonathan L.; Morrison, Gregory Y.; Plate, Dave W.; Smith, Brian V.; Warwick, Tony; Padmore, Howard A.; Ustundag, Ersan; Yashchuk, Valeriy V.

    2009-03-24

    A new facility for microdiffraction strain measurements and microfluorescence mapping has been built on beamline 12.3.2 at the advanced light source of the Lawrence Berkeley National Laboratory. This beamline benefits from the hard x-radiation generated by a 6 T superconducting bending magnet (superbend) This provides a hard x-ray spectrum from 5 to 22 keV and a flux within a 1 mu m spot of ~;;5x109 photons/ s (0.1percent bandwidth at 8 keV). The radiation is relayed from the superbend source to a focus in the experimental hutch by a toroidal mirror. The focus spot is tailored bytwo pairs of adjustable slits, which serve as secondary source point. Inside the lead hutch, a pair of Kirkpatrick-Baez (KB) mirrors placed in a vacuum tank refocuses the secondary slit source onto the sample position. A new KB-bending mechanism with active temperature stabilization allows for more reproducible and stable mirror bending and thus mirror focusing. Focus spots around 1 um are routinely achieved and allow a variety of experiments, which have in common the need of spatial resolution. The effective spatial resolution (~;;0.2 mu m) is limited by a convolution of beam size, scan-stage resolution, and stage stability. A four-bounce monochromator consisting of two channel-cut Si(111) crystals placed between the secondary source and KB-mirrors allows for easy changes between white-beam and monochromatic experiments while maintaining a fixed beam position. High resolution stage scans are performed while recording a fluorescence emission signal or an x-ray diffraction signal coming from either a monochromatic or a white focused beam. The former allows for elemental mapping, whereas the latter is used to produce two-dimensional maps of crystal-phases, -orientation, -texture, and -strain/stress. Typically achieved strain resolution is in the order of 5x10-5 strain units. Accurate sample positioning in the x-ray focus spot is achieved with a commercial laser-triangulation unit. A Si

  7. Ultra-high performance mirror systems for the imaging and coherence beamline I13 at the Diamond Light Source

    Science.gov (United States)

    Wagner, U. H.; Alcock, S.; Ludbrook, G.; Wiatryzk, J.; Rau, C.

    2012-05-01

    I13L is a 250m long hard x-ray beamline (6 keV to 35 keV) currently under construction at the Diamond Light Source. The beamline comprises of two independent experimental endstations: one for imaging in direct space using x-ray microscopy and one for imaging in reciprocal space using coherent diffraction based imaging techniques. To minimise the impact of thermal fluctuations and vibrations onto the beamline performance, we are developing a new generation of ultra-stable beamline instrumentation with highly repeatable adjustment mechanisms using low thermal expansion materials like granite and large piezo-driven flexure stages. For minimising the beam distortion we use very high quality optical components like large ion-beam polished mirrors. In this paper we present the first metrology results on a newly designed mirror system following this design philosophy.

  8. Stable Isotope and Trace Element Records of Parts of MIS 5 and MIS 6 from Stalagmites from Lehman Cave, Nevada, USA

    Science.gov (United States)

    Cross, M.; McGee, D.; Broecker, W. S.; Quade, J.; Cheng, H.; Edwards, R. L.

    2014-12-01

    Recent years have seen the advent of high-resolution speleothem paleoclimate records from the Great Basin, adding to and refining our knowledge of the timing, duration, and nature of glacial/interglacial periods and transitions in Western North America from lake records and other archives of paleoclimatic change. Here we present a record of isotopic and geochemical change in stalagmites from Lehman Cave, (39.01°N, 114.22°W), a well-decorated cave on the western edge of the Bonneville Basin. These slow-growth stalagmites are 230Th dated to portions of Marine Isotope Stages 5 and 6. They replicate, at least in part, an orbitally-consistent Termination II (T-II) at 131 + 2 ka, first demonstrated in Great Basin speleothems by Shakun et al. (2011). T-II is expressed in our record as a +5.5‰ (from -7.5 to -2 ‰) and nearly +4‰ (from -14.4 to -10.5‰, when corrected for sea level) shift in δ13C and δ18O, respectively. There are notable similarities and differences among our record and other Great Basin records, Devils Hole (Winograd et al. 1992) and the recent speleothem records by Lachniet et al. (2014) and Denniston et al. (2007). Our record, for example, does not agree with the early timing of T-II in Devils Hole. However, during the latter portion of MIS 5, our record exhibits oxygen isotope values (-13 to -14‰ VPDB) significantly lighter than those in MIS 5e (-10.5 to -11‰ VPDB), similar to Devils Hole and Goshute Cave. In contrast, correlative values in Leviathan Cave (Lachniet et al., 2014) during the latter part of MIS5 are up to 3‰ heavier: -10.5‰ VPDB, matching MIS 5e values. Additionally, the lowest MIS 6 oxygen isotopic values in our record are reached at approximately 137.5 ± 2 ka, about 4 ka earlier than in the Lehman Cave sample presented in the Lachniet et al. record. We evaluate several potential explanations for these offsets in the MIS 5 samples, for example, variable degrees of isotopic enrichment. As a step towards reconciling these

  9. Anatomy of a cluster IDP. Part 2: Noble gas abundances, trace element geochemistry, isotopic abundances, and trace organic chemistry of several fragments from L2008#5

    Science.gov (United States)

    Thomas, K. L.; Clemett, S. J.; Flynn, G. J.; Keller, L. P.; Mckay, David S.; Messenger, S.; Nier, A. O.; Schlutter, D. J.; Sutton, S. R.; Walker, R. M.

    1994-01-01

    The topics discussed include the following: noble gas content and release temperatures; trace element abundances; heating summary of cluster fragments; isotopic measurements; and trace organic chemistry.

  10. A new dynamic-XPS end-station for beamline P04 at PETRA III/DESY

    Energy Technology Data Exchange (ETDEWEB)

    Babenkov, Sergey V., E-mail: sergey.babenkov@desy.de [Deutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg (Germany); Aristov, Victor Y. [Institute of Solid State Physics of Russian Academy of Sciences, Chernogolovka 142432 (Russian Federation); Institut für Theoretische Physik, Universität Hamburg, Jungiusstraße 9, D-20355 Hamburg (Germany); Molodtsova, Olga V. [Deutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg (Germany); Winkler, Konrad [Omicron NanoTechnology GmbH, Limburgerstr. 75, 65232 Taunusstein (Germany); Glaser, Leif; Shevchuk, Ivan; Scholz, Frank; Seltmann, Jörn; Viefhaus, Jens [Deutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg (Germany)

    2015-03-21

    We report on a new dynamic-XPS end-station for real-time investigations of advanced materials. The end-station is based on a new Argus hemispherical electron spectrometer with high speed detection system. In combination with the high brilliance XUV beamline P04 at PETRA III it provides users at PETRA III a unique tool for fast (down to 0.1 s/spectrum) and detailed investigations compared to existing XPS devices at other beamlines.

  11. Initial performances of first undulator-based hard x-ray beamlines of NSLS-II compared to simulations

    Energy Technology Data Exchange (ETDEWEB)

    Chubar, Oleg, E-mail: chubar@bnl.gov; Chu, Yong S.; Huang, Xiaojing; Kalbfleisch, Sebastian; Yan, Hanfei; Shaftan, Timur; Wang, Guimei; Cai, Yong Q.; Suvorov, Alexey; Fluerasu, Andrei; Wiegart, Lutz; Chen-Wiegart, Yu-chen Karen; Thieme, Juergen; Williams, Garth; Idir, Mourad; Tanabe, Toshiya; Zschack, Paul; Shen, Qun [National Synchrotron Light Source II, Brookhaven National Laboratory, Upton, NY 11973 (United States)

    2016-07-27

    Commissioning of the first X-ray beamlines of NSLS-II included detailed measurements of spectral and spatial distributions of the radiation at different locations of the beamlines, from front-ends to sample positions. Comparison of some of these measurement results with high-accuracy calculations of synchrotron (undulator) emission and wavefront propagation through X-ray transport optics, performed using SRW code, is presented.

  12. Jefferson Lab Hall A Beamline Instrumentation and Calibration for GMP experiment

    Science.gov (United States)

    Gautam, Thir Narayan

    2015-10-01

    The nucleon electromagnetic form factors characterize the distributions of electric charge and magnetization current inside the nucleon and thus reflect the internal structure determined by Quantum Chromodynamics. The GMp experiment is a first experiment run in Hall A at Jefferson Lab after the upgrade to double the beam energy with the goal to precisely measure electron-proton elastic cross section in the Q2 range of 7 to 17 GeV2 with an accuracy of better than 2%; several time better than existing data at the highest Q2. In order to achieve this accuracy, a determination of the accumulated beam charge of better than 0.5% is required. The new 12 GeV beamline was commissioned during the spring of 2015, with the main instrumentation consisting of beam charge and position monitors. In this talk, the procedures and the results of the calibrations of these beamline components will be presented.

  13. Vertical synchrotron radiation beamline for proximity X-ray lithography: Theoretical analysis

    Science.gov (United States)

    Bukreeva, Inna N.; Kozhevnikov, Igor V.

    1997-02-01

    The general physical principles of operation of the vertical beamline of synchrotron radiation (SR) intended for proximity X-ray lithography are considered. An optical system provides a deflection of the SR beam to the vertical plane, a cutoff of the hard X-rays, a uniform illumination of a wafer, a normal incidence of X-ray beam onto a mask, and a small enough divergency of the radiation. A vertical SR beamline makes it possible to circumvent the expensive development of vertical-plane displacement steppers and to use the conventional horizontal ones, to exclude the scanning of the SR beam across the mask and to reduce the requirements imposed on the accuracy of alignment of a gap between the mask and the wafer.

  14. A Superbend X-Ray Microdiffraction Beamline at the Advanced Light Source

    Energy Technology Data Exchange (ETDEWEB)

    Tamura, N.; Kunz, M.; Chen, K.; Celestre, R.S.; MacDowell, A.A.; Warwick, T.

    2009-03-10

    Beamline 12.3.2 at the Advanced Light Source is a newly commissioned beamline dedicated to x-ray microdiffraction. It operates in both monochromatic and polychromatic radiation mode. The facility uses a superconducting bending magnet source to deliver an X-ray spectrum ranging from 5 to 22 keV. The beam is focused down to {approx} 1 um size at the sample position using a pair of elliptically bent Kirkpatrick-Baez mirrors enclosed in a vacuum box. The sample placed on high precision stages can be raster-scanned under the microbeam while a diffraction pattern is taken at each step. The arrays of diffraction patterns are then analyzed to derive distribution maps of phases, strain/stress and/or plastic deformation inside the sample.

  15. Recent developments on techniques for differential phase imaging at the medical beamline of ELETTRA

    Science.gov (United States)

    Arfelli, F.; Pelliccia, D.; Cedola, A.; Astolfo, A.; Bukreeva, I.; Cardarelli, P.; Dreossi, D.; Lagomarsino, S.; Longo, R.; Rigon, L.; Sodini, N.; Menk, R. H.

    2013-06-01

    Over the last decade different phase contrast approaches have been exploited at the medical beamline SYRMEP of the synchrotron radiation facility Elettra in Trieste, Italy. In particular special focus has been drawn to analyzer based imaging and the associated imaging theory and processing. Analyzer based Imaging (ABI) and Diffraction Enhanced Imaging (DEI) techniques have been successfully applied in several biomedical applications. Recently it has been suggested to translate the acquired knowledge in this field towards a Thomson Backscattering Source (TBS), which is presently under development at the Frascati National Laboratories of INFN (Istituto Nazionale di Fisica Nucleare) in Rome, Italy. Such source is capable of producing intense and quasi-monochromatic hard X-ray beams. For the technical implementation of biomedical phase imaging at the TBS a grating interferometer for differential phase contrast imaging has been designed and successfully tested at SYRMEP beamline.

  16. Small-angle X-ray scattering at the ESRF high-brillance beamline

    Energy Technology Data Exchange (ETDEWEB)

    Boesecke, P.; Diat, O. [European Synchrotron Radiation Facility (ESRF), 38 -Grenoble (France)

    1997-10-01

    The high-brilliance beamline (BL4/ID2) at the European synchrotron radiation facility (ESRF) in Grenoble has been constructed with the emphasis on time-resolved small-angle X-ray scattering and macromolecular crystallography. It has been open to users for two years. The beamline has opened up new areas in small-angle scattering research, facilitating (a) small-angle crystallography on structures with unit cells of several hundredths of nanometres, (b) overlap with the light scattering range for the study of optical systems, (c) high photon flux for time-resolved experiments and (d) a high spatial coherence allowing submicrometre imaging with X-rays. The set-up and the detector system of the small-angle scattering station are presented. A method for obtaining absolute scattering intensities is described. The parasitic background at the station is discussed in terms of absolute scattering intensities. (orig.). 22 refs.

  17. UV-CD12: synchrotron radiation circular dichroism beamline at ANKA.

    Science.gov (United States)

    Bürck, Jochen; Roth, Siegmar; Windisch, Dirk; Wadhwani, Parvesh; Moss, David; Ulrich, Anne S

    2015-05-01

    Synchrotron radiation circular dichroism (SRCD) is a rapidly growing technique for structure analysis of proteins and other chiral biomaterials. UV-CD12 is a high-flux SRCD beamline installed at the ANKA synchrotron, to which it had been transferred after the closure of the SRS Daresbury. The beamline covers an extended vacuum-UV to near-UV spectral range and has been open for users since October 2011. The current end-station allows for temperature-controlled steady-state SRCD spectroscopy, including routine automated thermal scans of microlitre volumes of water-soluble proteins down to 170 nm. It offers an excellent signal-to-noise ratio over the whole accessible spectral range. The technique of oriented circular dichroism (OCD) was recently implemented for determining the membrane alignment of α-helical peptides and proteins in macroscopically oriented lipid bilayers as mimics of cellular membranes. It offers improved spectral quality dichroism artifacts.

  18. In-vacuum sensors for the beamline components of the ITER neutral beam test facility

    Science.gov (United States)

    Dalla Palma, M.; Pasqualotto, R.; Sartori, E.; Spagnolo, S.; Spolaore, M.; Veltri, P.

    2016-11-01

    Embedded sensors have been designed for installation on the components of the MITICA beamline, the prototype ITER neutral beam injector (Megavolt ITER Injector and Concept Advancement), to derive characteristics of the particle beam and to monitor the component conditions during operation for protection and thermal control. Along the beamline, the components interacting with the particle beam are the neutralizer, the residual ion dump, and the calorimeter. The design and the positioning of sensors on each component have been developed considering the expected beam-surface interaction including non-ideal and off-normal conditions. The arrangement of the following instrumentation is presented: thermal sensors, strain gages, electrostatic probes including secondary emission detectors, grounding shunt for electrical currents, and accelerometers.

  19. Fast X-ray imaging at beamline I13L at Diamond Light Source

    Science.gov (United States)

    De Fanis, A.; Pešić, Z. D.; Wagner, U.; Rau, C.

    2013-03-01

    The imaging branch of the dual-branch beamline I13L at Diamond Light Source has been operational since April 2012. This branch is dedicated to hard X-ray imaging (in-line phase contrast radiography and tomography, and full-field microscopy), with energies in the ranges 6-30keV. At present we aim to achieve spatial resolution of the order of 1 μm over a field of view of l-20mm2. This branch aims to excel at imaging experiment of fast dynamic processes, where it is of interest to have short exposure times and high frame rates. To accommodate for this, we prepared for the beamline to operate with "pink" beam to provide higher flux, an efficient detection system, and rapid data acquisition, transfer, and saving to storage. This contributed paper describes the present situation and illustrate the author's goal for the mid-future.

  20. Undulator beamline optimization with integrated chicanes for X-ray free-electron-laser facilities.

    Science.gov (United States)

    Prat, Eduard; Calvi, Marco; Ganter, Romain; Reiche, Sven; Schietinger, Thomas; Schmidt, Thomas

    2016-07-01

    An optimization of the undulator layout of X-ray free-electron-laser (FEL) facilities based on placing small chicanes between the undulator modules is presented. The installation of magnetic chicanes offers the following benefits with respect to state-of-the-art FEL facilities: reduction of the required undulator length to achieve FEL saturation, improvement of the longitudinal coherence of the FEL pulses, and the ability to produce shorter FEL pulses with higher power levels. Numerical simulations performed for the soft X-ray beamline of the SwissFEL facility show that optimizing the advantages of the layout requires shorter undulator modules than the standard ones. This proposal allows a very compact undulator beamline that produces fully coherent FEL pulses and it makes possible new kinds of experiments that require very short and high-power FEL pulses.

  1. PARALLEL MEASUREMENT AND MODELING OF TRANSPORT IN THE DARHT II BEAMLINE ON ETA II

    Energy Technology Data Exchange (ETDEWEB)

    Chambers, F W; Raymond, B A; Falabella, S; Lee, B S; Richardson, R A; Weir, J T; Davis, H A; Schultze, M E

    2005-05-31

    To successfully tune the DARHT II transport beamline requires the close coupling of a model of the beam transport and the measurement of the beam observables as the beam conditions and magnet settings are varied. For the ETA II experiment using the DARHT II beamline components this was achieved using the SUICIDE (Simple User Interface Connecting to an Integrated Data Environment) data analysis environment and the FITS (Fully Integrated Transport Simulation) model. The SUICIDE environment has direct access to the experimental beam transport data at acquisition and the FITS predictions of the transport for immediate comparison. The FITS model is coupled into the control system where it can read magnet current settings for real time modeling. We find this integrated coupling is essential for model verification and the successful development of a tuning aid for the efficient convergence on a useable tune. We show the real time comparisons of simulation and experiment and explore the successes and limitations of this close coupled approach.

  2. Calibration and standards beamline 6.3.2 at the ALS

    Energy Technology Data Exchange (ETDEWEB)

    Underwood, J.H.; Gullikson, E.M.; Koike, M. [Ernest Orlando Lawrence Berkeley National Lab., CA (United States)] [and others

    1997-04-01

    More sophisticated optics for the x-ray, soft x-ray and far ultraviolet spectral regions being developed for synchrotron radiation research and many other applications, require accurate calibration and standards facilities for measuring reflectivity of mirrors and multilayer coatings, transmission of thin films, bandpass of multilayers, efficiency of gratings or detectors, etc. For this purpose beamline 6.3.2 was built at the ALS. Its energy coverage, versatility, simplicity and convenience also make it useful for a wide range of other experiments. The paper describes the components of this beamline, consisting of: a four jaw aperture; a horizontal focusing mirror; a monochromator; exit slit; vertical focusing mirror; mechanical and vacuum system; reflectometer; filter wheels; and data acquisition system.

  3. ROBL - a CRG beamline for radiochemistry and materials research at the ESRF

    Energy Technology Data Exchange (ETDEWEB)

    Matz, W.; Schell, N.; Bernhard, G.; Claussner, J.; Oehme, W.; Prokert, F.; Reich, T.; Schlenk, R.; Proehl, D.; Funke, H.; Eichhorn, F.; Betzl, M.; Dienel, S.; Brendler, V.; Denecke, M.A.; Krug, H.; Neumann, W.; Huettig, G.; Reichel, P.; Strauch, U.

    1999-04-01

    The paper describes the Rossendorf Beamline (ROBL) built by the Forschungszentrum Rossendorf at th ESRF. ROBL comprises two different and independently operating experimental stations: a radiochemistry laboratory for X-ray absorption spectroscopy of non-sealed radioactive samples and a general purpose materials research station for X-ray diffraction and reflectometry mainly of thin films and interfaces modified by ion beam techniques. The radiochemistry set-up is worldwide a unique installation at a modern synchrotron radiation source. (orig.) [Deutsch] Der Bericht beschreibt die Rossendorfer Beamline (ROBL), die vom Forschungszentrum Rossendorf an der ESRF errichtet wurde. ROBL besteht aus zwei unabhaengigen Messplaetzen: einem kleinen radiochemischen Labor fuer Roentgen-Adsorptionsspektroskopie an offenen radioaktiven Proben und einem Vielzweckmessplatz fuer Materialuntersuchungen insbesondere mit Roentgendiffraktion und Reflektometrie. Der Radiochemie-Messplatz ist eine weltweit unikale Einrichtung an einer modernen Synchrontronstrahlungsquelle. (orig.)

  4. Optimizing the Stark-decelerator beamline for the trapping of cold molecules using evolutionary strategies

    CERN Document Server

    Gilijamse, J J; Hoekstra, S; De van Meerakker, S Y T; Meijer, G; Gilijamse, Joop J.; K\\"upper, Jochen; Hoekstra, Steven; Meerakker, Sebastiaan Y. T. van de; Meijer, Gerard

    2006-01-01

    We demonstrate feedback control optimization for the Stark deceleration and trapping of neutral polar molecules using evolutionary strategies. In a Stark-decelerator beamline pulsed electric fields are used to decelerate OH radicals and subsequently store them in an electrostatic trap. The efficiency of the deceleration and trapping process is determined by the exact timings of the applied electric field pulses. Automated optimization of these timings yields an increase of 40 % of the number of trapped OH radicals.

  5. Pulse generation and preamplification for long pulse beamlines of Orion laser facility.

    Science.gov (United States)

    Hillier, David I; Winter, David N; Hopps, Nicholas W

    2010-06-01

    We describe the pulse generation, shaping, and preamplification system for the nanosecond beamlines of the Orion laser facility. The system generates shaped laser pulses of up to approximately 1 J of 100 ps-5 ns duration with a programmable temporal profile. The laser has a 30th-power supergaussian spatial profile and is diffraction limited. The system is capable of imposing 2D smoothing by spectral dispersion upon the beam, which will produce a nonuniformity of 10% rms at the target.

  6. High-throughput beamline for attosecond pulses based on toroidal mirrors with microfocusing capabilities

    Energy Technology Data Exchange (ETDEWEB)

    Frassetto, F.; Poletto, L., E-mail: poletto@dei.unipd.it [National Research Council, Institute of Photonics and Nanotechnologies, via Trasea 7, 35131 Padova (Italy); Trabattoni, A.; Anumula, S.; Sansone, G. [Department of Physics, Politecnico di Milano, Piazza L. Da Vinci 32, 20133 Milano (Italy); Calegari, F. [National Research Council, Institute of Photonics and Nanotechnologies, Piazza L. da Vinci 32, 20133 Milano (Italy); Nisoli, M. [Department of Physics, Politecnico di Milano, Piazza L. Da Vinci 32, 20133 Milano (Italy); National Research Council, Institute of Photonics and Nanotechnologies, Piazza L. da Vinci 32, 20133 Milano (Italy)

    2014-10-15

    We have developed a novel attosecond beamline designed for attosecond-pump/attosecond probe experiments. Microfocusing of the Extreme-ultraviolet (XUV) radiation is obtained by using a coma-compensated optical configuration based on the use of three toroidal mirrors controlled by a genetic algorithm. Trains of attosecond pulses are generated with a measured peak intensity of about 3 × 10{sup 11} W/cm{sup 2}.

  7. High-throughput beamline for attosecond pulses based on toroidal mirrors with microfocusing capabilities.

    Science.gov (United States)

    Frassetto, F; Trabattoni, A; Anumula, S; Sansone, G; Calegari, F; Nisoli, M; Poletto, L

    2014-10-01

    We have developed a novel attosecond beamline designed for attosecond-pump/attosecond probe experiments. Microfocusing of the Extreme-ultraviolet (XUV) radiation is obtained by using a coma-compensated optical configuration based on the use of three toroidal mirrors controlled by a genetic algorithm. Trains of attosecond pulses are generated with a measured peak intensity of about 3 × 10(11) W/cm(2).

  8. Fast continuous energy scan with dynamic coupling of the monochromator and undulator at the DEIMOS beamline.

    Science.gov (United States)

    Joly, L; Otero, E; Choueikani, F; Marteau, F; Chapuis, L; Ohresser, P

    2014-05-01

    In order to improve the efficiency of X-ray absorption data recording, a fast scan method, the Turboscan, has been developed on the DEIMOS beamline at Synchrotron SOLEIL, consisting of a software-synchronized continuous motion of the monochromator and undulator motors. This process suppresses the time loss when waiting for the motors to reach their target positions, as well as software dead-time, while preserving excellent beam characteristics.

  9. Radiation field characterization and shielding studies for the ELI Beamlines facility

    Science.gov (United States)

    Ferrari, A.; Amato, E.; Margarone, D.; Cowan, T.; Korn, G.

    2013-05-01

    The ELI (Extreme Light Infrastructure) Beamlines facility in the Czech Republic, which is planned to complete the installation in 2015, is one of the four pillars of the ELI European project. Several laser beamlines with ultrahigh intensities and ultrashort pulses are foreseen, offering versatile radiation sources in an unprecedented energy range: laser-driven particle beams are expected to range between 1 and 50 GeV for electrons and from 100 MeV up to 3 GeV for protons. The number of particles delivered per laser shot is estimated to be 109-1010 for the electron beams and 1010-1012 for the proton beams. The high energy and current values of the produced particles, together with the potentiality to operate at 10 Hz laser repetition rate, require an accurate study of the primary and secondary radiation fields to optimize appropriate shielding solutions: this is a key issue to minimize prompt and residual doses in order to protect the personnel, reduce the radiation damage of electronic devices and avoid strong limitations in the operational time. A general shielding study for the 10 PW (0.016 Hz) and 2 PW (10 Hz) laser beamlines is presented here. Starting from analytical calculations, as well as from dedicated simulations, the main electron and proton fields produced in the laser-matter interaction have been described and used to characterize the "source terms" in full simulations with the Monte Carlo code FLUKA. The secondary radiation fields have been then analyzed to assess a proper shielding. The results of this study and the proposed solutions for the beam dumps of the high energy beamlines, together with a cross-check analysis performed with the Monte Carlo code GEANT4, are presented.

  10. Ultrahigh contrast from a frequency-doubled chirped-pulse-amplification beamline.

    Science.gov (United States)

    Hillier, David; Danson, Colin; Duffield, Stuart; Egan, David; Elsmere, Stephen; Girling, Mark; Harvey, Ewan; Hopps, Nicholas; Norman, Michael; Parker, Stefan; Treadwell, Paul; Winter, David; Bett, Thomas

    2013-06-20

    This paper describes frequency-doubled operation of a high-energy chirped-pulse-amplification beamline. Efficient type-I second-harmonic generation was achieved using a 3 mm thick 320 mm aperture KDP crystal. Shots were fired at a range of energies achieving more than 100 J in a subpicosecond, 527 nm laser pulse with a power contrast of 10(14).

  11. Characterization of a next-generation piezo bimorph X-ray mirror for synchrotron beamlines

    Energy Technology Data Exchange (ETDEWEB)

    Alcock, Simon G., E-mail: simon.alcock@diamond.ac.uk; Nistea, Ioana; Sutter, John P.; Sawhney, Kawal [Diamond Light Source, Harwell Science and Innovation Campus, Didcot, Oxfordshire OX11 0DE (United Kingdom); Fermé, Jean-Jacques; Thellièr, Christophe; Peverini, Luca [Thales-SESO, 305 rue Louis Armand, Pôle d’Activités d’Aix les Milles, Aix-en-Provence (France)

    2015-01-01

    A next-generation bimorph mirror with piezos bonded to the side faces of a monolithic substrate was created. When replacing a first-generation bimorph mirror suffering from the junction effect, the new type of mirror significantly improved the size and shape of the reflected synchrotron X-ray beam. No evidence of the junction effect was observed even after eight months of continuous beamline usage. Piezo bimorph mirrors are versatile active optics used on many synchrotron beamlines. However, many bimorphs suffer from the ‘junction effect’: a periodic deformation of the optical surface which causes major aberrations to the reflected X-ray beam. This effect is linked to the construction of such mirrors, where piezo ceramics are glued directly below the thin optical substrate. In order to address this problem, a next-generation bimorph with piezos bonded to the side faces of a monolithic substrate was developed at Thales-SESO and optimized at Diamond Light Source. Using metrology feedback from the Diamond-NOM, the optical slope error was reduced to ∼0.5 µrad r.m.s. for a range of ellipses. To maximize usability, a novel holder was built to accommodate the substrate in any orientation. When replacing a first-generation bimorph on a synchrotron beamline, the new mirror significantly improved the size and shape of the reflected X-ray beam. Most importantly, there was no evidence of the junction effect even after eight months of continuous beamline usage. It is hoped that this new design will reinvigorate the use of active bimorph optics at synchrotron and free-electron laser facilities to manipulate and correct X-ray wavefronts.

  12. Beamline X29: a novel undulator source for X-ray crystallography.

    Science.gov (United States)

    Shi, Wuxian; Robinson, Howard; Sullivan, Michael; Abel, Don; Toomey, John; Berman, Lonny E; Lynch, Don; Rosenbaum, Gerd; Rakowsky, George; Rock, Larry; Nolan, Bill; Shea-McCarthy, Grace; Schneider, Dieter; Johnson, Erik; Sweet, Robert M; Chance, Mark R

    2006-09-01

    A high-flux insertion device and beamline for macromolecular crystallography has been built at the National Synchrotron Light Source (NSLS) that employs a mini-gap undulator source developed by the NSLS. The mini-gap undulator at beamline X29 is a hybrid-magnet device of period 12.5 mm operating at proven gaps of 3.3-10 mm. The beamline provides hard X-rays for macromolecular crystallography experiments from the second and third harmonics over an energy range of 5-15 keV. The X-ray optics is designed to deliver intense and highly collimated X-rays. Horizontal focusing is achieved by a cryogenically cooled sagittally focusing double-crystal monochromator with approximately 4.1:1 demagnification. A vertical focusing mirror downstream of the monochromator is used for harmonic rejection and vertical focusing. The experimental station hosts an Area Detector Systems Quantum 315 CCD detector with 2.2 s readout time between exposures and Crystal Logic goniostat for crystal rotation and detector positioning. An auto-mounter crystal changer has been installed to facilitate the high-throughput data collection required by the major users, which includes structural genomics projects and the Macromolecular Crystallography Research Resource mail-in program. X29 is 10(3) times brighter than any existing bending-magnet beamline at NSLS with an actual flux of 2.5 x 10(11) photons s(-1) through a 0.12 mm square aperture at 11.271 keV.

  13. Accelerator SIMS, a technique for the determination of stable trace elements in ultrapure materials

    Energy Technology Data Exchange (ETDEWEB)

    Ender, R.M.; Suter, M. [Eidgenoessische Technische Hochschule, Zurich (Switzerland); Doebeli, M.; Synal, H.A. [Paul Scherrer Inst. (PSI), Villigen (Switzerland)

    1997-09-01

    A new sputtering chamber with special precautions against sample contamination from the surroundings of the sample has been added to the AMS beamline of the tandem accelerator. This allows the detection of trace element concentrations in ultrapure materials below the ppb range in many cases. (author) 1 fig., 2 refs.

  14. Suite of three protein crystallography beamlines with single superconducting bend magnet as the source

    Energy Technology Data Exchange (ETDEWEB)

    MacDowell, Alastair A.; Celestre, Richard S.; Howells, Malcolm; McKinney, Wayne; Krupnick, James; Cambie, Daniella; Domning, Edward E; Duarte, Robert M.; Kelez, Nicholas; Plate, David W.; Cork, Carl W.; Earnest, Thomas N.; Dickert, Jeffery; Meigs, George; Ralston, Corie; Holton, James M.; Alber, Thomas; Berger, James M.; Agard, David A.; Padmore, Howard A.

    2004-08-01

    At the Advanced Light Source (ALS), three protein crystallography (PX) beamlines have been built that use as a source one of the three 6 Tesla single pole superconducting bending magnets (superbends) that were recently installed in the ring. The use of such single pole superconducting bend magnets enables the development of a hard x-ray program on a relatively low energy 1.9 GeV ring without taking up insertion device straight sections. The source is of relatively low power, but due to the small electron beam emittance, it has high brightness. X-ray optics are required to preserve the brightness and to match the illumination requirements for protein crystallography. This was achieved by means of a collimating premirror bent to a plane parabola, a double crystal monochromator followed by a toroidal mirror that focuses in the horizontal direction with a 2:1 demagnification. This optical arrangement partially balances aberrations from the collimating and toroidal mirrors such that a tight focused spot size is achieved. The optical properties of the beamline are an excellent match to those required by the small protein crystals that are typically measured. The design and performance of these new beamlines are described.

  15. Commissioning of the off-axis neutral beamline on the DIII-D tokamak

    Science.gov (United States)

    Scoville, J. T.; Murphy, C. J.; Hong, R. M.

    2011-10-01

    One of the four neutral beam injection systems on DIII-D has recently been rebuilt to allow off-axis injection. A system of hydraulically operated pistons was fit to the beamline to allow tilting up to an angle of 16.5 deg, enabling injection of 5 MW of neutral beam power up to 40 cm below the plasma centroid. Off-axis injection required rebuilding the two ion sources to produce more strongly focused and narrower beams that can inject the power at an angle through the port box of the vacuum vessel. The internal beamline collimation system was replaced with a new system compatible with the stronger focused sources. An extensive alignment process was carried out for all beamline internal components and ion sources. Extensive analysis has been carried out using thermocouple and calorimetry data to document the performance of the collimation system, leading to an extension of the allowable pulse length. We present a description of the modifications that were made to the ion sources and collimation systems and the results of heating and performance studies for the off-axis beam injection system. Work supported by U.S. DOE under DE-FC02-04ER54698.

  16. Coherence Length and Vibrations of the Coherence Beamline I13 at the Diamond Light Source

    Science.gov (United States)

    Wagner, U. H.; Parson, A.; Rau, C.

    2017-06-01

    I13 is a 250 m long hard x-ray beamline for imaging and coherent diffraction at the Diamond Light Source. The beamline (6 keV to 35 keV) comprises two independent experimental endstations: one for imaging in direct space using x-ray microscopy and one for imaging in reciprocal space using coherent diffraction based imaging techniques [1]. In particular the coherence experiments pose very high demands on the performance on the beamline instrumentation, requiring extensive testing and optimisation of each component, even during the assembly phase. Various aspects like the quality of optical components, the mechanical design concept, vibrations, drifts, thermal influences and the performance of motion systems are of particular importance. In this paper we study the impact of the front-end slit size (FE slit size), which determines the horizontal source size, onto the coherence length and the detrimental impact of monochromator vibrations using in-situ x-ray metrology in conjunction with fringe visibility measurements and vibration measurements, based on centroid tracking of an x-ray pencil beam with a photon-counting detector.

  17. Upgrades to the XRD1 beamline optics and endstation at the LNLS

    Science.gov (United States)

    Canova, H.; Fontoura, A.; Neuenschwander, R. T.; Diaz, B.; Rodella, C. B.

    2014-03-01

    XRD1 was the first X-ray diffraction beamline to be built at the LNLS and after approximately 12 years of operation it was substantially updated to improve beam stability, increase the reliability of the monochromator movement as well as provide an experimental hutch that would meet the demands of users. The improvements included the construction of an independent concrete slab below the mirror and monochromator to minimize the vibrations originating from the floor. In addition, the installation of new monochromator mechanisms as well as the replacement of the two Si(111) crystals were performed in order to attain higher precision, stability and reproducibility during operation. Moreover, the diffractometer was replaced by a 3-circle heavy duty diffractometer from Newport to collect XRD patterns primarily in capillary geometry. A robotic arm was installed for fast and automated replacement of samples as well as to secure a cryojet or a hot air blower in front of the sample during measurements. In addition, a housing equipped with 24 Mythen detectors was installed at the beamline allowing for extremely fast data acquisition. Another upgrade was the integration of motors and control systems from PXI National Instruments and Galil controllers with Phytron. These systems are crucial for the next upgrade that is underway at the beamline: enabling remote access for users to collect their measurements without the need to travel to the LNLS.

  18. The status of the macromolecular crystallography beamlines at the European Synchrotron Radiation Facility

    Science.gov (United States)

    Mueller-Dieckmann, Christoph; Bowler, Matthew W.; Carpentier, Philippe; Flot, David; McCarthy, Andrew A.; Nanao, Max H.; Nurizzo, Didier; Pernot, Petra; Popov, Alexander; Round, Adam; Royant, Antoine; de Sanctis, Daniele; von Stetten, David; Leonard, Gordon A.

    2015-04-01

    The European Synchrotron Radiation Facility (ESRF) is the oldest and most powerful 3rd generation synchrotron in Europe, providing X-rays to more than 40 experimental stations welcoming several thousand researchers per year. A major success story has been the ESRF's facilities for macromolecular crystallography (MX). These are grouped around 3 straight sections: On ID23 canted undulators accommodate ID23-1, a mini-focus tuneable energy end station and ID23-2, the world's first micro-focus beamline dedicated to MX; ID29 houses a single, mini-focus, tuneable energy end station; ID30 will provide three end stations for MX due in operation from mid-2014 to early 2015. Here, one branch of a canted X-ray source feeds two fixed-energy end stations (MASSIF-1, MASSIF-3). The second feeds ID30B, a variable focus, tuneable energy beamline. MASSIF-1 is optimised for automatic high-throughput experiments requiring a relatively large beam size at the sample position, MASSIF-3 is a high-intensity, micro-focus facility designed to complement ID23-2. All end stations are highly automated, equipped with sample mounting robots and large area, fast-readout photon-counting detectors. Experiment control and tracking is achieved via a combination of the MXCuBE2 graphical user interface and the ISPyB database, the former allowing user-friendly control of all beamline components, the latter providing data tracking before, after and during experiments.

  19. Optimization of a general-purpose, actively scanned proton beamline for ocular treatments: Geant4 simulations.

    Science.gov (United States)

    Piersimoni, Pierluigi; Rimoldi, Adele; Riccardi, Cristina; Pirola, Michele; Molinelli, Silvia; Ciocca, Mario

    2015-03-08

    The Italian National Center for Hadrontherapy (CNAO, Centro Nazionale di Adroterapia Oncologica), a synchrotron-based hospital facility, started the treatment of patients within selected clinical trials in late 2011 and 2012 with actively scanned proton and carbon ion beams, respectively. The activation of a new clinical protocol for the irradiation of uveal melanoma using the existing general-purpose proton beamline is foreseen for late 2014. Beam characteristics and patient treatment setup need to be tuned to meet the specific requirements for such a type of treatment technique. The aim of this study is to optimize the CNAO transport beamline by adding passive components and minimizing air gap to achieve the optimal conditions for ocular tumor irradiation. The CNAO setup with the active and passive components along the transport beamline, as well as a human eye-modeled detector also including a realistic target volume, were simulated using the Monte Carlo Geant4 toolkit. The strong reduction of the air gap between the nozzle and patient skin, as well as the insertion of a range shifter plus a patient-specific brass collimator at a short distance from the eye, were found to be effective tools to be implemented. In perspective, this simulation toolkit could also be used as a benchmark for future developments and testing purposes on commercial treatment planning systems.

  20. Characterization of a next-generation piezo bimorph X-ray mirror for synchrotron beamlines.

    Science.gov (United States)

    Alcock, Simon G; Nistea, Ioana; Sutter, John P; Sawhney, Kawal; Fermé, Jean Jacques; Thellièr, Christophe; Peverini, Luca

    2015-01-01

    Piezo bimorph mirrors are versatile active optics used on many synchrotron beamlines. However, many bimorphs suffer from the `junction effect': a periodic deformation of the optical surface which causes major aberrations to the reflected X-ray beam. This effect is linked to the construction of such mirrors, where piezo ceramics are glued directly below the thin optical substrate. In order to address this problem, a next-generation bimorph with piezos bonded to the side faces of a monolithic substrate was developed at Thales-SESO and optimized at Diamond Light Source. Using metrology feedback from the Diamond-NOM, the optical slope error was reduced to ∼ 0.5 µrad r.m.s. for a range of ellipses. To maximize usability, a novel holder was built to accommodate the substrate in any orientation. When replacing a first-generation bimorph on a synchrotron beamline, the new mirror significantly improved the size and shape of the reflected X-ray beam. Most importantly, there was no evidence of the junction effect even after eight months of continuous beamline usage. It is hoped that this new design will reinvigorate the use of active bimorph optics at synchrotron and free-electron laser facilities to manipulate and correct X-ray wavefronts.

  1. Photostimulated phosphor based image plate detection system for HRVUV beamline at Indus-1 synchrotron radiation source

    CERN Document Server

    Haris, K; Shastri, Aparna; K., Sunanda; K., Babita; Rao, S V N Bhaskara; Ahmad, Shabbir; Tauheed, A

    2014-01-01

    A high resolution vacuum ultraviolet (HRVUV) beamline based on a 6.65 meter off-plane Eagle spectrometer is in operation at the Indus-1 synchrotron radiation source, RRCAT, Indore, India. To facilitate position sensitive detection and fast spectral recording, a new BaFBr:Eu2+ phosphor based image plate (IP) detection system interchangeable with the existing photomultiplier (PMT) scanning system has been installed on this beamline. VUV photoabsorption studies on Xe, O2, N2O and SO2 are carried out to evaluate the performance of the IP detection system. An FWHM of ~ 0.5 {\\AA} is achieved for the Xe atomic line at 1469.6 {\\AA}. Reproducibility of spectra is found to be within the experimental resolution. Compared to the PMT scanning system, the IP shows several advantages in terms of sensitivity, recording time and S/N ratio, which are highlighted in the paper. This is the first report of incorporation of an IP detection system in a VUV beamline using synchrotron radiation. Commissioning of the new detection sys...

  2. Instrumental neutron activation analysis of different products from the sugarcane industry in Pakistan--part 1: essential elements for nutritional adequacy.

    Science.gov (United States)

    Waheed, Shahida; Ahmad, Shujaat

    2008-01-01

    Jaggery, brown sugar, white sugar, and molasses collected from the local sugarcane industry of Pakistan have been analyzed for essential elements in order to estimate their nutritional adequacy. Instrumental neutron activation analysis was used to determine Ca, CI, Co, Cr, Fe, K, Mg, Mn, Na, and Zn through sequential, short, medium, and long irradiation times. Maximum concentrations for most of these elements were determined in molasses, with lower concentrations determined in jaggery and brown sugar; white sugar contained trace amounts of all essential elements. Contributions to the weekly Recommended Dietary Allowance (RDA) values for the elements were estimated only for jaggery, brown sugar, and white sugar because molasses in Pakistan is not consumed as a dietary item. Jaggery contributes the highest percentages of Cr, Mg, Mn, and Zn, whereas the highest percentages of Cl, Fe, K, and Na can be acquired from brown sugar. The contribution of white sugar to the weekly RDAs for these elements is negligible, indicating that white sugar is a poor source of the essential elements. However, the introduction of molasses to the diet can contribute to an adequate intake of these elements.

  3. Damage and fatigue crack growth of Eurofer steel first wall mock-up under cyclic heat flux loads. Part 2: Finite element analysis of damage evolution

    Energy Technology Data Exchange (ETDEWEB)

    You, Jeong-Ha, E-mail: you@ipp.mpg.de

    2014-04-15

    Highlights: • The surface heat flux load of 3.5 MW/m{sup 2} produced substantial stresses and inelastic strains in the heat-loaded surface region, especially at the notch root. • The notch root exhibited a typical notch effect such as stress concentration and localized inelastic yield leading to a preferred damage development. • The predicted damage evolution feature agrees well with the experimental observation. • The smooth surface also experiences considerable stresses and inelastic strains. However, the stress intensity and the amount of inelastic deformation are not high enough to cause any serious damage. • The level of maximum inelastic strain is higher at the notch root than at the smooth surface. On the other hand, the amplitude of inelastic strain variation is comparable at both positions. • The amount of inelastic deformation is significantly affected by the length of pulse duration time indicating the important role of creep. - Abstract: In the preceding companion article (part 1), the experimental results of the high-heat-flux (3.5 MW/m{sup 2}) fatigue tests of a Eurofer bare steel first wall mock-up was presented. The aim was to investigate the damage evolution and crack initiation feature. The mock-up used there was a simplified model having only basic and generic structural feature of an actively cooled steel FW component for DEMO reactor. In that study, it was found that microscopic damage was formed at the notch root already in the early stage of the fatigue loading. On the contrary, the heat-loaded smooth surface exhibited no damage up to 800 load cycles. In this paper, the high-heat-flux fatigue behavior is investigated with a finite element analysis to provide a theoretical interpretation. The thermal fatigue test was simulated using the coupled damage-viscoplastic constitutive model developed by Aktaa. The stresses, inelastic deformation and damage evolution at the notch groove and at the smooth surface are compared. The different

  4. Nonlinear incompressible finite element for simulating loading of cardiac tissue--Part II: Three dimensional formulation for thick ventricular wall segments.

    Science.gov (United States)

    Horowitz, A; Sheinman, I; Lanir, Y

    1988-02-01

    A three dimensional incompressible and geometrically as well as materially nonlinear finite element is formulated for future implementation in models of cardiac mechanics. The stress-strain relations in the finite element are derived from a recently proposed constitutive law which is based on the histological composition of the myocardium. The finite element is formulated for large deformations and considers incompressibility by introducing the hydrostatic pressure as an additional variable. The results of passive loading cases simulated by this element allow to analyze the mechanical properties of ventricular wall segments, the main of which are that the circumferential direction is stiffer than the longitudinal one, that its shear stiffness is considerably lower than its tensile and compressive stiffness and that, due to its mechanically prominent role, the collagenous matrix may affect the myocardial perfusion.

  5. Best practices for single-laboratory validation of chemical methods for trace elements in foods. Part I--background and general considerations.

    Science.gov (United States)

    Murphy, Cory J; MacNeil, James D; Capar, Stephen G

    2013-01-01

    The metals subgroup of AOAC INTERNATIONAL's Community on Chemical Contaminants and Residues in Food has been engaged for the past several years in discussions concerning the requirements for the single-laboratory validation (SLV) of methods for the determination of trace elements in foods. This paper reviews the general guidance currently available related to validation of chemical analytical methods and current typical validation practices found in publications on the analysis of elements in food and other matrixes, such as environmental and clinical samples. Based on the available guidance on SLV requirements and a review of current practices in elemental analysis, a general approach based on best practices is proposed for SLV of a method for elements in food to demonstrate the method as "fit-for-purpose."

  6. Seasonal variations in the chemical composition of particulate matter: a case study in the Po Valley. Part II: concentration and solubility of micro- and trace-elements.

    Science.gov (United States)

    Canepari, S; Astolfi, M L; Farao, C; Maretto, M; Frasca, D; Marcoccia, M; Perrino, C

    2014-03-01

    Size distribution (fine and coarse fraction) and solubility distribution (extracted and residual fraction) of 20 elements (As, Ba, Be, Cd, Co, Cu, Fe, Li, Mn, Pb, Ni, Rb, S, Sb, Se, Sn, Sr, Ti, Tl, V) in atmospheric particulate matter (PM) were determined during a 5-year field study carried out in the Po Valley (peri-urban area of Ferrara, in Northern Italy). By studying the contribution of the two size fractions and the two solubility fractions to the atmospheric concentration of each element, it was possible to obtain interesting information about the variability of PM sources, to assess the role played by atmospheric stability in determining pollution episodes, and to obtain an estimate of the bio-accessible fraction. Atmospheric stability is confirmed to be one of the main causes of atmospheric pollution in this area and is to be responsible for the pronounced winter increase in both PM and elemental concentration. Long-range transport of natural and polluted air masses caused temporary increases in PM and elemental concentration, while local industrial emission seemed to play a secondary role. Regulated elements were well below their concentration limit, but many toxic elements were in the form of fine particles and soluble chemical species, more accessible to the environment, and the human body.

  7. The Heavy Photon Search beamline and its performance

    Science.gov (United States)

    Baltzell, N.; Egiyan, H.; Ehrhart, M.; Field, C.; Freyberger, A.; Girod, F.-X.; Holtrop, M.; Jaros, J.; Kalicy, G.; Maruyama, T.; McKinnon, B.; Moffeit, K.; Nelson, T.; Odian, A.; Oriunno, M.; Paremuzyan, R.; Stepanyan, S.; Tiefenback, M.; Uemura, S.; Ungaro, M.; Vance, H.

    2017-07-01

    The Heavy Photon Search (HPS) is an experiment to search for a hidden sector photon, aka a heavy photon or dark photon, in fixed target electroproduction at the Thomas Jefferson National Accelerator Facility (JLab). The HPS experiment searches for the e+e- decay of the heavy photon with bump hunt and detached vertex strategies using a compact, large acceptance forward spectrometer, consisting of a silicon microstrip detector (SVT) for tracking and vertexing, and a PbWO4 electromagnetic calorimeter for energy measurement and fast triggering. To achieve large acceptance and good vertexing resolution, the first layer of silicon detectors is placed just 10 cm downstream of the target with the sensor edges only 500 μm above and below the beam. Placing the SVT in such close proximity to the beam puts stringent requirements on the beam profile and beam position stability. As part of an approved engineering run, HPS took data in 2015 and 2016 at 1.05 GeV and 2.3 GeV beam energies, respectively. This paper describes the beam line and its performance during that data taking.

  8. The Heavy Photon Search beamline and its performance

    Energy Technology Data Exchange (ETDEWEB)

    Baltzell, N.; Egiyan, H.; Ehrhart, M.; Field, C.; Freyberger, A.; Girod, F. -X.; Holtrop, M.; Jaros, J.; Kalicy, G.; Maruyama, T.; McKinnon, B.; Moffeit, K.; Nelson, T.; Odian, A.; Oriunno, M.; Paremuzyan, R.; Stepanyan, S.; Tiefenback, M.; Uemura, S.; Ungaro, M.; Vance, H.

    2017-04-04

    The Heavy Photon Search (HPS) is an experiment to search for a hidden sector photon, aka a heavy photon or dark photon, in fixed target electroproduction at the Thomas Jefferson National Accelerator Facility (JLab). The HPS experiment searches for the e+e- decay of the heavy photon with bump hunt and detached vertex strategies using a compact, large acceptance forward spectrometer, consisting of a silicon microstrip detector (SVT) for tracking and vertexing, and a PbWO4 electromagnetic calorimeter for energy measurement and fast triggering. To achieve large acceptance and good vertexing resolution, the first layer of silicon detectors is placed just 10 cm downstream of the target with the sensor edges only 500 μm above and below the beam. Placing the SVT in such close proximity to the beam puts stringent requirements on the beam profile and beam position stability. As part of an approved engineering run, HPS took data in 2015 and 2016 at 1.05 GeV and 2.3 GeV beam energies, respectively. This paper describes the beam line and its performance during that data taking.

  9. Semianalytical analysis of shear walls with the use of discrete-continual finite element method. Part 2: Numerical examples, future development

    Directory of Open Access Journals (Sweden)

    Akimov Pavel

    2016-01-01

    Full Text Available The distinctive paper is devoted to the two-dimensional semi-analytical solution of boundary problems of analysis of shear walls with the use of discrete-continual finite element method (DCFEM. This approach allows obtaining the exact analytical solution in one direction (so-called “basic” direction, also decrease the size of the problem to one-dimensional common finite element analysis. Two numerical examples of structural analysis with the use of DCFEM are considered, conventional finite element method (FEM is used for verification purposes. The presented examples show some of the advantages of the suggested approach to semianalytical analysis of the shear wall. Future development of DCFEM, particularly associated with multigrid approach, is under consideration as well.

  10. ℎ- Spectral element methods for three dimensional elliptic problems on non-smooth domains, Part-II: Proof of stability theorem

    Indian Academy of Sciences (India)

    P Dutt; Akhlaq Husain; A S Vasudeva Murthy; C S Upadhyay

    2015-08-01

    This is the second of a series of papers devoted to the study of ℎ- spectral element methods for three dimensional elliptic problems on non-smooth domains. The present paper addresses the proof of the main stability theorem.We assume that the differential operator is a strongly elliptic operator which satisfies Lax–Milgram conditions. The spectral element functions are non-conforming. The stability estimate theorem of this paper will be used to design a numerical scheme which give exponentially accurate solutions to three dimensional elliptic problems on non-smooth domains and can be easily implemented on parallel computers.

  11. Trace Element Geochemistry of Zhaertai Group in the Middle Part of Inner Mongolia%内蒙古中部渣尔泰山群微量元素地球化学特征

    Institute of Scientific and Technical Information of China (English)

    赵帅; 刘峰; 张成江

    2009-01-01

    通过对内蒙古中部渣尔泰山群各层位岩石采样,对该山群中共43个微量元素(含稀土元素)与地壳丰度进行了对比分析,总结了该山群微量元素的地球化学特征.研究表明,该山群富集W、Re、Cu、Pb、Co等元素,而In、V、Cr、Ni等元素亏损较严重;微量元素在板岩和云母石英片岩中相对含量较高,在灰岩中相对贫化;此外,该山群稀土元素地球化学特征表现为轻稀土富集,重稀土亏损;具有明显的Eu的负异常,Ce的弱正异常.%With collecting the rock samples of different layers in Zhaertai Group in the Middle Part of Inner Mongolia, 43 trace elements ( contains rare-earth elements) were analysed, which has compared with crustal abundance, trying to summarize the trace elements geochemistry of this Group. The study shows that this group is prolific of elements such as W, Re, Cu, Pb, Co, and there are many severely depleted elements, like In, V, Cr, Ni. The trace elements is relatively higher in slate and mica quartz schist, and lower in limestone; Moreover, the rare- earth elements geochemistry exposes that Zhaertai Group is prolific of LREE, in opposite, HREE are depleted elements; this group takes on a obvious negative anomaly of Eu, and a weakly positive anomaly of Ce.

  12. The Extreme Conditions Beamline P02.2 and the Extreme Conditions Science Infrastructure at PETRA III

    Energy Technology Data Exchange (ETDEWEB)

    Liermann, H.-P., E-mail: hanns-peter.liermann@desy.de; Konôpková, Z. [Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany); Morgenroth, W. [University of Frankfurt, Frankfurt (Germany); Glazyrin, K.; Bednarčik, J.; McBride, E. E. [Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany); Petitgirard, S. [Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany); University of Bayreuth, Bayreuth (Germany); Delitz, J. T.; Wendt, M.; Bican, Y.; Ehnes, A.; Schwark, I.; Rothkirch, A.; Tischer, M.; Heuer, J.; Schulte-Schrepping, H.; Kracht, T.; Franz, H. [Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)

    2015-06-19

    Performance description of the Extreme Conditions Beamline (ECB, P02.2) at PETRA III that is optimized for micro-diffraction at simultaneous high pressure and high and low temperatures created in different diamond anvil cells environments. Additional information of the capabilities of the Extreme Conditions Science Infrastructure for DAC work is provided. A detailed description is presented of the Extreme Conditions Beamline P02.2 for micro X-ray diffraction studies of matter at simultaneous high pressure and high/low temperatures at PETRA III, in Hamburg, Germany. This includes performance of the X-ray optics and instrumental resolution as well as an overview of the different sample environments available for high-pressure studies in the diamond anvil cell. Particularly emphasized are the high-brilliance and high-energy X-ray diffraction capabilities of the beamline in conjunction with the use of fast area detectors to conduct time-resolved compression studies in the millisecond time regime. Finally, the current capability of the Extreme Conditions Science Infrastructure to support high-pressure research at the Extreme Conditions Beamline and other PETRA III beamlines is described.

  13. DCS - A High Flux Beamline for Time Resolved Dynamic Compression Science – Design Highlights

    Energy Technology Data Exchange (ETDEWEB)

    Capatina, D. [Argonne National Lab. (ANL), Argonne, IL (United States); D' Amico, Kevin L. [Argonne National Lab. (ANL), Argonne, IL (United States); Nudell, J. [Argonne National Lab. (ANL), Argonne, IL (United States); Collins, J. [Argonne National Lab. (ANL), Argonne, IL (United States); Schmidt, Oliver [Argonne National Lab. (ANL), Argonne, IL (United States)

    2016-07-27

    The Dynamic Compression Sector (DCS) beamline, a national user facility for time resolved dynamic compression science supported by the National Nuclear Security Administration (NNSA) of the Department of Energy (DOE), has recently completed construction and is being commissioned at Sector 35 of the Advanced Photon Source (APS) at Argonne National Laboratory (ANL). The beamline consists of a First Optics Enclosure (FOE) and four experimental enclosures. A Kirkpatrick–Baez focusing mirror system with 2.2 mrad incident angles in the FOE delivers pink beam to the experimental stations. A refocusing Kirkpatrick–Baez mirror system is situated in each of the two most downstream enclosures. Experiments can be conducted in either white, monochromatic, pink or monochromatic-reflected beam mode in any of the experimental stations by changing the position of two interlocked components in the FOE. The beamline Radiation Safety System (RSS) components have been designed to handle the continuous beam provided by two in-line revolver undulators with periods of 27 and 30 mm, at closed gap, 150 mA beam current, and passing through a power limiting aperture of 1.5 x 1.0 mm2. A novel pink beam end station stop [1] is used to stop the continuous and focused pink beam which can achieve a peak heat flux of 105 kW/mm2. A new millisecond shutter design [2] is used to deliver a quick pulse of beam to the sample, synchronized with the dynamic event, the microsecond shutter, and the storage ring clock.

  14. DCS - A high flux beamline for time resolved dynamic compression science – Design highlights

    Energy Technology Data Exchange (ETDEWEB)

    Capatina, D., E-mail: capatina@aps.anl.gov; D’Amico, K., E-mail: kdamico@aps.anl.gov; Nudell, J., E-mail: jnudell@aps.anl.gov; Collins, J., E-mail: collins@aps.anl.gov; Schmidt, O., E-mail: oschmidt@aps.anl.gov [Advanced Photon Source, Argonne National Laboratory, 9700 S. Cass Avenue, Lemont, IL 60439 (United States)

    2016-07-27

    The Dynamic Compression Sector (DCS) beamline, a national user facility for time resolved dynamic compression science supported by the National Nuclear Security Administration (NNSA) of the Department of Energy (DOE), has recently completed construction and is being commissioned at Sector 35 of the Advanced Photon Source (APS) at Argonne National Laboratory (ANL). The beamline consists of a First Optics Enclosure (FOE) and four experimental enclosures. A Kirkpatrick–Baez focusing mirror system with 2.2 mrad incident angles in the FOE delivers pink beam to the experimental stations. A refocusing Kirkpatrick–Baez mirror system is situated in each of the two most downstream enclosures. Experiments can be conducted in either white, monochromatic, pink or monochromatic-reflected beam mode in any of the experimental stations by changing the position of two interlocked components in the FOE. The beamline Radiation Safety System (RSS) components have been designed to handle the continuous beam provided by two in-line revolver undulators with periods of 27 and 30 mm, at closed gap, 150 mA beam current, and passing through a power limiting aperture of 1.5 x 1.0 mm{sup 2}. A novel pink beam end station stop [1] is used to stop the continuous and focused pink beam which can achieve a peak heat flux of 105 kW/mm{sup 2}. A new millisecond shutter design [2] is used to deliver a quick pulse of beam to the sample, synchronized with the dynamic event, the microsecond shutter, and the storage ring clock.

  15. The test beamline of the European Spallation Source - Instrumentation development and wavelength frame multiplication

    DEFF Research Database (Denmark)

    Woracek, R.; Hofmann, T.; Bulat, M.

    2016-01-01

    The European Spallation Source (ESS), scheduled to start operation in 2020, is aiming to deliver the most intense neutron beams for experimental research of any facility worldwide. Its long pulse time structure implies significant differences for instrumentation compared to other spallation sources...... which, in contrast, are all providing short neutron pulses. In order to enable the development of methods and technology adapted to this novel type of source well in advance of the first instruments being constructed at ESS, a test beamline (TBL) was designed and built at the BER II research reactor...

  16. The Rossendorf Beamline at ESRF (ROBL-CRG). Bi-annual report 2003/04

    Energy Technology Data Exchange (ETDEWEB)

    Scheinost, A.C.; Schell, N. (eds.)

    2005-01-01

    In this report the work performed at the Rossendorf beam-line at the ESRF is described. It concerns neptunium (IV) uptake by iron metalloproteins, in-situ speciation of actinides using a newly developed spectro-electrochemical cell, quantitative antimony speciation in Swiss shooting-range soils, in-situ studies of ITO film properties and structure during annealing in vacuum, high-temperature investigations of Si/SiGe based quantum cascade structures using X-ray diffraction and reflectivity, and in-situ characterization of stress states in copper dual inlaid interconnects at high temperatures by synchrotron X-ray diffraction. (HSI)

  17. SYNCH: A program for design and analysis of synchrotrons and beamlines -- user`s guide

    Energy Technology Data Exchange (ETDEWEB)

    Garren, A.A.; Kenney, A.S.; Courant, E.D.; Russell, A.D.; Syphers, M.J.

    1993-12-31

    SYNCH is a computer program for use in the design and analysis of synchrotrons, storage rings, and beamlines. It has a large repertoire of commands that can be accessed in a flexible way. The input statements and the results of the calculations they invoke are saved in an internal database so that this information may be shared by other statements. SYNCH is the first accelerator program to organize its input in the form of a language. The statements, which resemble sentences, provide a natural way of describing lattices and invoking relevant calculations. The organization of the program is modular, so that it has been possible to expand its capabilities progressively.

  18. Target and orbit feedback simulations of a muSR beamline at BNL

    Energy Technology Data Exchange (ETDEWEB)

    MacKay, W. W. [Residence, 25 Rhododendron Circle, Asheville, NC (United States); Fischer, W. [Brookhaven National Lab. (BNL), Upton, NY (United States); Blaskiewicz, M. [Brookhaven National Lab. (BNL), Upton, NY (United States); Pile, P. [Brookhaven National Lab. (BNL), Upton, NY (United States)

    2015-05-03

    Well-polarized positive surface muons are a tool to measure the magnetic properties of materials since the precession rate of the spin can be determined from the observation of the positron directions when the muons decay. The use of the AGS complex at BNL has been explored for a muSR facility previously. Here we report simulations of a beamline with a target inside a solenoidal field, and of an orbit feed-back system with single muon beam positioning monitors based on technology available today

  19. SUNY beamline facilities at the National Synchrotron Light Source (Final Report)

    Energy Technology Data Exchange (ETDEWEB)

    Coppens, Philip

    2003-06-22

    The DOE sponsored SUNY synchrotron project has involved close cooperation among faculty at several SUNY campuses. A large number of students and postdoctoral associates have participated in its operation which was centered at the X3 beamline of the National Synchrotron Light Source at Brookhaven National Laboratory. Four stations with capabilities for Small Angle Scattering, Single Crystal and Powder and Surface diffraction and EXAFS were designed and operated with capability to perform experiments at very low as well as elevated temperatures and under high vacuum. A large amount of cutting-edge science was performed at the facility, which in addition provided excellent training for students and postdoctoral scientists in the field.

  20. Target and orbit feedback simulations of a muSR beamline at BNL

    Energy Technology Data Exchange (ETDEWEB)

    MacKay, W. W. [Residence, 25 Rhododendron Circle, Asheville, NC (United States); Fischer, W. [Brookhaven National Lab. (BNL), Upton, NY (United States); Blaskiewicz, M. [Brookhaven National Lab. (BNL), Upton, NY (United States); Pile, P. [Brookhaven National Lab. (BNL), Upton, NY (United States)

    2015-05-03

    Well-polarized positive surface muons are a tool to measure the magnetic properties of materials since the precession rate of the spin can be determined from the observation of the positron directions when the muons decay. The use of the AGS complex at BNL has been explored for a muSR facility previously. Here we report simulations of a beamline with a target inside a solenoidal field, and of an orbit feed-back system with single muon beam positioning monitors based on technology available today

  1. Fast helicity switching of x-ray circular polarization at beamline P09 at PETRA III

    Energy Technology Data Exchange (ETDEWEB)

    Strempfer, J., E-mail: Joerg.Strempfer@desy.de; Mardegan, J. R. L.; Francoual, S.; Veiga, L. S. I.; Spitzbart, T.; Zink, H. [Deutsches Elektronen Synchrotron (DESY), Notkestrasse 85, 22603 Hamburg (Germany); Bouchenoire, L. [XMaS, ESRF, 6 rue Jules Horowitz, BP220, Grenoble 38043 (France); Department of Physics, University of Liverpool, Liverpool, L69 7ZE (United Kingdom)

    2016-07-27

    At the resonant scattering and diffraction beamline P09 at PETRA III/DESY, polarization manipulation in the X-ray energy range 3-13 keV is possible using wave-plates. Recently, fast flipping of circular polarization helicity using the Raspberry Pi controlled FPGA (PiLC) device developed at DESY and dedicated piezo-electric flippers has been commissioned. Functionality of the PiLC for XMCD and first XMCD measurements at the Fe K-and Dy-L{sub 3} absorption edges are presented.

  2. Advanced Beamline Design for Fermilab's Advanced Superconducting Test Accelerator

    Energy Technology Data Exchange (ETDEWEB)

    Prokop, Christopher [Northern Illinois Univ., DeKalb, IL (United States)

    2014-01-01

    The Advanced Superconducting Test Accelerator (ASTA) at Fermilab is a new electron accelerator currently in the commissioning stage. In addition to testing superconducting accelerating cavities for future accelerators, it is foreseen to support a variety of Advanced Accelerator R&D (AARD) experiments. Producing the required electron bunches with the expected flexibility is challenging. The goal of this dissertation is to explore via numerical simulations new accelerator beamlines that can enable the advanced manipulation of electron bunches. The work especially includes the design of a low-energy bunch compressor and a study of transverse-to-longitudinal phase space exchangers.

  3. CDApps: integrated software for experimental planning and data processing at beamline B23, Diamond Light Source.

    Science.gov (United States)

    Hussain, Rohanah; Benning, Kristian; Javorfi, Tamas; Longo, Edoardo; Rudd, Timothy R; Pulford, Bill; Siligardi, Giuliano

    2015-03-01

    The B23 Circular Dichroism beamline at Diamond Light Source has been operational since 2009 and has seen visits from more than 200 user groups, who have generated large amounts of data. Based on the experience of overseeing the users' progress at B23, four key areas requiring the most assistance are identified: planning of experiments and note-keeping; designing titration experiments; processing and analysis of the collected data; and production of experimental reports. To streamline these processes an integrated software package has been developed and made available for the users. The subsequent article summarizes the main features of the software.

  4. Beamline I11 at Diamond: a new instrument for high resolution powder diffraction.

    Science.gov (United States)

    Thompson, S P; Parker, J E; Potter, J; Hill, T P; Birt, A; Cobb, T M; Yuan, F; Tang, C C

    2009-07-01

    The performance characteristics of a new synchrotron x-ray powder diffraction beamline (I11) at the Diamond Light Source are presented. Using an in-vacuum undulator for photon production and deploying simple x-ray optics centered around a double-crystal monochromator and a pair of harmonic rejection mirrors, a high brightness and low bandpass x-ray beam is delivered at the sample. To provide fast data collection, 45 Si(111) analyzing crystals and detectors are installed onto a large and high precision diffractometer. High resolution powder diffraction data from standard reference materials of Si, alpha-quartz, and LaB6 are used to characterize instrumental performance.

  5. 100-J level amplifier concepts for HiLASE and ELI-Beamlines

    Science.gov (United States)

    Sikocinski, P.; Divoky, M.; Lucianetti, A.; Sawicka, M.; Novak, J.; Rus, B.; Mocek, T.

    2012-07-01

    We present comparison of two alternative layouts of a 100 J cryogenically cooled Yb:YAG multi-slab laser system operating at 10 Hz for HiLASE and ELI Beamlines projects. In the first approach, the 100 J slab amplifier consists of a preamplifier and power amplifier, while in the second approach it uses single power amplifier with two amplifier heads. These two concepts are compared, with respect to output power, B-integral, accumulated B-integral, and peak fluence. Results are obtained by simulating beam propagation in MIRÓ code and calculating stored energy in the amplifier by homemade ray-tracing MATLAB code for amplified spontaneous emission evaluation.

  6. SYNCH: A program for design and analysis of synchrotrons and beamlines -- user`s guide

    Energy Technology Data Exchange (ETDEWEB)

    Garren, A.A.; Kenney, A.S.; Courant, E.D.; Russell, A.D.; Syphers, M.J.

    1993-12-31

    SYNCH is a computer program for use in the design and analysis of synchrotrons, storage rings, and beamlines. It has a large repertoire of commands that can be accessed in a flexible way. The input statements and the results of the calculations they invoke are saved in an internal database so that this information may be shared by other statements. SYNCH is the first accelerator program to organize its input in the form of a language. The statements, which resemble sentences, provide a natural way of describing lattices and invoking relevant calculations. The organization of the program is modular, so that it has been possible to expand its capabilities progressively.

  7. In crystallo optical spectroscopy (icOS) as a complementary tool on the macromolecular crystallography beamlines of the ESRF.

    Science.gov (United States)

    von Stetten, David; Giraud, Thierry; Carpentier, Philippe; Sever, Franc; Terrien, Maxime; Dobias, Fabien; Juers, Douglas H; Flot, David; Mueller-Dieckmann, Christoph; Leonard, Gordon A; de Sanctis, Daniele; Royant, Antoine

    2015-01-01

    The analysis of structural data obtained by X-ray crystallography benefits from information obtained from complementary techniques, especially as applied to the crystals themselves. As a consequence, optical spectroscopies in structural biology have become instrumental in assessing the relevance and context of many crystallographic results. Since the year 2000, it has been possible to record such data adjacent to, or directly on, the Structural Biology Group beamlines of the ESRF. A core laboratory featuring various spectrometers, named the Cryobench, is now in its third version and houses portable devices that can be directly mounted on beamlines. This paper reports the current status of the Cryobench, which is now located on the MAD beamline ID29 and is thus called the ID29S-Cryobench (where S stands for `spectroscopy'). It also reviews the diverse experiments that can be performed at the Cryobench, highlighting the various scientific questions that can be addressed.

  8. Obtaining local reciprocal lattice vectors from finite-element analysis.

    Science.gov (United States)

    Sutter, John P; Connolley, Thomas; Hill, Tim P; Huang, Houcheng; Sharp, Doug W; Drakopoulos, Michael

    2008-11-01

    Finite-element analysis is frequently used by engineers at synchrotron beamlines to calculate the elastic deformation of a single crystal undergoing mechanical bending or thermal load. ANSYS Workbench software is widely used for such simulations. However, although ANSYS Workbench software provides useful information on the displacements, strains and stresses within the crystal, it does not yield the local reciprocal lattice vectors that would be required for X-ray diffraction calculations. To bridge this gap, a method based on the shape functions and interpolation procedures of the software itself has been developed. An application to the double-crystal bent Laue monochromator being designed for the I12 (JEEP) wiggler beamline at the Diamond Light Source is presented.

  9. Study of 3-D stress development in parent and twin pairs of a hexagonal close-packed polycrystal: Part II - Crystal plasticity finite element modeling

    DEFF Research Database (Denmark)

    Abdolvand, Hamidreza; Majkut, Marta; Oddershede, Jette

    2015-01-01

    -of-mass positions and volumes as measured by three-dimensional X-ray diffraction (3DXRD) microscopy. The constructed microstructure is meshed with different element densities and for different numbers of grains. Then a selected group of twin and parent pairs are studied. It is shown that the measured average stress...... each grain, stresses in the parent and twin are quite different if they are plotted in the global coordinate system. However, if the stress tensor is rotated into the local coordinate system of the twin habit plane, all the stress components averaged over the presented population are close, except......Stress heterogeneity within each individual grain of polycrystalline Zircaloy-2 is studied using a crystal plasticity finite element (CPFE) model. For this purpose, the weighted Voronoi tessellation method is used to construct 3D geometries of more than 2600 grains based on their center...

  10. A cavity ring-down spectroscopy sensor for measurements of gaseous elemental mercury – Part 1: Development for high time resolution measurements in ambient air

    OpenAIRE

    X. Faïn; D. Obrist; H. Moosmüller; Pierce, A; Moore, C.

    2012-01-01

    The ability to make high time resolution measurements of gaseous elemental mercury (GEM) concentrations in air is imperative for the understanding of mercury cycling. Here we describe further development and field implementation of a laboratory prototype pulsed cavity ring-down spectroscopy (CRDS) system for high time resolution, continuous and automated measurement of GEM concentrations in ambient air. In particular, we present use of an external, isotopically enriched Hg cell for automated ...

  11. Optical design and performance of the phase II inelastic scattering beamline at the National Synchrotron Light Source

    Energy Technology Data Exchange (ETDEWEB)

    Caliebe, W.A.; Kao, C.-C.; Oversluizen, T.; Montanez, P.; Hastings, J.B. [National Synchrotron Light Source, Brookhaven National Laboratory, Upton New York, 11973 (United States); Caliebe, W.A. [Hamburger Synchrotronstrahlungslabor HASYLAB, Deutsches Elektronen-Synchrotron DESY, 22603Hamburg (Germany)] Krisch, M. [European Synchrotron Radiation Facility, F-38043Grenoble Cedex (France)

    1997-07-01

    We report the optical design and performance of the phase II inelastic scattering beamline at the National Synchrotron Light Source. The new beamline consists of a four-crystal Si(220) monochromator followed by a bent cylinder mirror. The monochromator is tunable from 5 to 10 keV with about 0.2 eV energy resolution throughout the tuning range. The size of the focused beam is about 0.5mm(H){times}0.3mm(V). {copyright} {ital 1997 American Institute of Physics.}

  12. Facilitating best practices in collecting anomalous scattering data for de novo structure solution at the ESRF Structural Biology Beamlines

    Science.gov (United States)

    de Sanctis, Daniele; Oscarsson, Marcus; Popov, Alexander; Svensson, Olof; Leonard, Gordon

    2016-01-01

    The constant evolution of synchrotron structural biology beamlines, the viability of screening protein crystals for a wide range of heavy-atom derivatives, the advent of efficient protein labelling and the availability of automatic data-processing and structure-solution pipelines have combined to make de novo structure solution in macromolecular crystallography a less arduous task. Nevertheless, the collection of diffraction data of sufficient quality for experimental phasing is still a difficult and crucial step. Here, some examples of good data-collection practice for projects requiring experimental phasing are presented and recent developments at the ESRF Structural Biology beamlines that have facilitated these are illustrated. PMID:26960128

  13. Analysis of Power Distribution on Beamline Components at Different Neutralization Efficiencies on NBI Test Stand

    Science.gov (United States)

    Li, Xiang; Xu, Yongjian; Yu, Ling; Chen, Yu; Hu, Chundong; Tao, Ling

    2016-12-01

    Neutral beam injection is recognized as one of the most effective means for plasma heating. According to the research plan of the EAST physics experiment, two sets of neutral beam injector (4-8 MW, 10-100 s) were built and operated in 2014. Neutralization efficiency is one of the important parameters for neutral beam. High neutralization efficiency can not only improve injection power at the same beam energy, but also decrease the power deposited on the heat-load components in the neutral beam injector (NBI). This research explores the power deposition distribution at different neutralization efficiencies on the beamline components of the NBI device. This work has great significance for guiding the operation of EAST-NBI, especially in long pulse and high power operation, which can reduce the risk of thermal damage of the beamline components and extend the working life of the NBI device. supported by the International Science and Technology Cooperation Program of China (No. 2014DFG61950), National Natural Science Foundation of China (No. 11405207) and the Foundation of ASIPP (No. DSJJ-15-GC03)

  14. Optimization of a dedicated bio-imaging beamline at the European X-ray FEL

    CERN Document Server

    Geloni, Gianluca; Saldin, Evgeni

    2012-01-01

    We recently proposed a basic concept for design and layout of the undulator source for a dedicated bio-imaging beamline at the European XFEL. The goal of the optimized scheme proposed here is to enable experimental simplification and performance improvement. The core of the scheme is composed by soft and hard X-ray self-seeding setups. Based on the use of an improved design for both monochromators it is possible to increase the design electron energy up to 17.5 GeV in photon energy range between 2 keV and 13 keV, which is the most preferable for life science experiments. An advantage of operating at such high electron energy is the increase of the X-ray output peak power. Another advantage is that 17.5 GeV is the preferred operation energy for SASE1 and SASE2 beamline users. Since it will be necessary to run all the XFEL lines at the same electron energy, this choice will reduce the interference with other undulator lines and increase the total amount of scheduled beam time. In this work we also propose a stu...

  15. First tests of the ion irradiation and implantation beamline at the CMAM

    Science.gov (United States)

    Jiménez-Rey, D.; Benedicto, M.; Muñoz-Martín, A.; Bachiller-Perea, D.; Olivares, J.; Climent-Font, A.; Gómez-Ferrer, B.; Rodríguez, A.; Narros, J.; Maira, A.; Álvarez, J.; Nakbi, A.; Zucchiatti, A.; de Aragón, F.; García, J. M.; Vila, R.

    2014-07-01

    The implantation and irradiation beamline of the Tandem ion accelerator of the Centro de Micro Análisis de Materiales (CMAM), in Madrid, has been recently completed with a beam sweep and monitoring system, and a cryostat/furnace. These new implementations convert the beamline into a versatile tool to implant ions, between H and Au2, in different materials with precise control of the sample temperature, which may be varied between -180 °C and 600 °C. The size of the swept area on target may be as large as 10 × 10 cm2. The implantation chamber also allows carrying out in situ or/and on line analyses during the irradiations by means of advanced optical measurements, as well as ion beam analyses (IBA). These advancements can be employed in novel applications such as the fabrication of optical waveguides and irradiation tests of structural and functional materials for future fusion reactors. The results of beam tests and first experiments are shown.

  16. Beamline and exposure station for deep x-ray lithography at the Advanced Photon Source

    Energy Technology Data Exchange (ETDEWEB)

    Lai, B.; Mancini, D.C.; Yun, W.; Gluskin, E.

    1996-12-31

    APS is a third-generation synchrotron radiation source. With an x-ray energy of 19.5 keV and highly collimated beam (<0.1 mrad), APS is well suited for producing high-aspect-ratio microstructures in thick resist films (> 1 mm) using deep x-ray lithography (DXRL). The 2-BM beamline was constructed and will be used for DXRL at APS. Selection of appropriate x-ray energy range is done through a variable-angle mirror and various filters in the beamline. At the exposure station, the beam size will be 100(H) x 5(V) mm{sup 2}. Uniform exposure will be achieved by a high-speed (100 mm/sec) vertical scanner, which allows precise angular ({approximately}0.1 mrad) and positional (< 1 {mu}m) control of the sample, allowing full use of the highly collimated beam for lateral accuracy and control of sidewall slopes during exposure of thick resists, as well as generation of conicals and other profiles. For 1-mm-thick PMMA, a 100 x 25 mm{sup 2} area can be fully exposed in about 1/2 hr, while even 10-mm-thick PMMA will require only 2-3 hours.

  17. Commissioning of the soft x-ray undulator beamline at the Siam Photon Laboratory

    Energy Technology Data Exchange (ETDEWEB)

    Nakajima, Hideki, E-mail: hideki@slri.or.th; Chaichuay, Sarunyu; Sudmuang, Porntip; Rattanasuporn, Surachet; Jenpiyapong, Watcharapon; Supruangnet, Ratchadaporn; Chanlek, Narong [Synchrotron Light Research Institute, Muang, Nakhon Ratchasima 30000 (Thailand); Songsiriritthigul, Prayoon [School of Physics, Suranaree University of Technology, Muang, Nakhon Ratchasima 30000 (Thailand)

    2016-07-27

    The synchrotron radiation from the first undulator at the Siam Photon Laboratory was characterized with the photon beam position monitors (BPMs) and grating monochromator. The soft x-ray undulator beamline employs a varied line-spacing plane grating monochromator with three interchangeable gratings. Since 2010, the beamline has delivered photons with energy of 40-160 and 220-1040 eV at the resolving power of 10,000 for user services at the two end- stations that utilize the photoemission electron spectroscopy and microscopy techniques. The undulator power-density distributions measured by the 0.05-mm wire-scan BPM were in good agreement with those in simulation. The flux-density distributions were evaluated in the red-shift measurements, which identify the central cone of radiation and its distribution. Since 2014, the operation of the other insertion devices in the storage ring has started, and consequently bought about the increases in the emittance from 41 to 61 nm·rad and the coupling constant from 4 to 11%. The local electron-orbit correction greatly improved the alignment of the electron beam in the undulator section resulting in the improvements of the photon flux and harmonics peaks of the undulator radiation.

  18. First tests of the ion irradiation and implantation beamline at the CMAM

    Energy Technology Data Exchange (ETDEWEB)

    Jiménez-Rey, D. [Centro de Micro-Análisis de Materiales, Universidad Autónoma de Madrid, C/Faraday 3, Madrid 28049 (Spain); Laboratorio Nacional de Fusión, EURATOM/CIEMAT, CIEMAT, Avda. Complutense 40, Madrid 28040 (Spain); Benedicto, M.; Muñoz-Martín, A. [Centro de Micro-Análisis de Materiales, Universidad Autónoma de Madrid, C/Faraday 3, Madrid 28049 (Spain); Bachiller-Perea, D. [Centro de Micro-Análisis de Materiales, Universidad Autónoma de Madrid, C/Faraday 3, Madrid 28049 (Spain); Dpto. de Física Aplicada, Universidad Autónoma de Madrid, Ciudad Universitaria de Cantoblanco, Madrid 28049 (Spain); Olivares, J. [Centro de Micro-Análisis de Materiales, Universidad Autónoma de Madrid, C/Faraday 3, Madrid 28049 (Spain); Dpto. de Física Aplicada, Universidad Autónoma de Madrid, Ciudad Universitaria de Cantoblanco, Madrid 28049 (Spain); Laboratorio Nacional de Fusión, EURATOM/CIEMAT, CIEMAT, Avda. Complutense 40, Madrid 28040 (Spain); Instituto de Óptica, CSIC, Calle Serrano 121, Madrid 28006 (Spain); Climent-Font, A. [Centro de Micro-Análisis de Materiales, Universidad Autónoma de Madrid, C/Faraday 3, Madrid 28049 (Spain); Dpto. de Física Aplicada, Universidad Autónoma de Madrid, Ciudad Universitaria de Cantoblanco, Madrid 28049 (Spain); and others

    2014-07-15

    The implantation and irradiation beamline of the Tandem ion accelerator of the Centro de Micro Análisis de Materiales (CMAM), in Madrid, has been recently completed with a beam sweep and monitoring system, and a cryostat/furnace. These new implementations convert the beamline into a versatile tool to implant ions, between H and Au{sub 2}, in different materials with precise control of the sample temperature, which may be varied between −180 °C and 600 °C. The size of the swept area on target may be as large as 10 × 10 cm{sup 2}. The implantation chamber also allows carrying out in situ or/and on line analyses during the irradiations by means of advanced optical measurements, as well as ion beam analyses (IBA). These advancements can be employed in novel applications such as the fabrication of optical waveguides and irradiation tests of structural and functional materials for future fusion reactors. The results of beam tests and first experiments are shown.

  19. XAS at the materials science X-ray beamline BL8 at the DELTA storage ring

    Energy Technology Data Exchange (ETDEWEB)

    Frahm, R; Wagner, R; Luetzenkirchen-Hecht, D [Fachbereich C - Physik, Bergische Universitaet Wuppertal, Gaussstrasse 20, 42097 Wuppertal (Germany); Herdt, A, E-mail: frahm@uni-wuppertal.d [Fachbereich Physik/DELTA, Technische Universitaet Dortmund, Maria-Goeppert-Mayer-Strasse 2, 44221 Dortmund (Germany)

    2009-11-15

    The hard X-ray beamline BL 8 at the 1.5 GeV electron storage ring DELTA is described, and experimental data of different fields of research are presented. Making use of the intense X-ray beam emitted by a superconducting wiggler, the beamline is dedicated to X-ray absorption experiments. Three different monochromator crystal pairs are permanently available for experiments in the spectral range from about 1 keV to ca. 25 keV photon energy. Results of reference materials show that high quality EXAFS data can be obtained using Si(111) and Si(311) monochromators. First measurements in the energy range between 1.2 and 5 keV have been accomplished using YB{sub 66}(400) monochromator crystals. The experimental hutch accommodates a unique 6-axis diffractometer which is well suited for all kinds of diffraction and absorption experiments, including the grazing incidence geometry. The diffractometer can carry heavy loads related to non-ambient sample environments such as e.g. ultrahigh vacuum sample stages or cryostats. Here we present typical results obtained at BL8 in different areas of materials science including investigations of dilute alloys by fluorescence mode EXAFS and the study of the structural changes associated with temperature induced spin transitions of metallo-supramolecular polyelectrolyte-amphiphile-complexes.

  20. Micro- and nano-imaging at the diamond beamline I13L-imaging and coherence

    Energy Technology Data Exchange (ETDEWEB)

    Rau, C., E-mail: Christoph.rau@diamond.ac.uk [Diamond Light Source Ltd., Harwell Science and Innovation Campus, Didcot, OX 11 0DE (United Kingdom); University of Manchester, School of Materials Grosvenor St., Manchester, M1 7HS (United Kingdom); Northwestern University School of Medicine, 303 E. Chicago Avenue, Chicago, IL 60611-3008 (United States); Wagner, U. H.; Vila-Comamala, J.; Bodey, A.; Parson, A.; García-Fernández, M.; Pešić, Z.; Zanette, I. [Diamond Light Source Ltd., Harwell Science and Innovation Campus, Didcot, OX 11 0DE (United Kingdom); De Fanis, A. [Diamond Light Source Ltd., Harwell Science and Innovation Campus, Didcot, OX 11 0DE (United Kingdom); European XFEL GmbH, Notkestraße 85, 22607 Hamburg (Germany); Zdora, M. [Diamond Light Source Ltd., Harwell Science and Innovation Campus, Didcot, OX 11 0DE (United Kingdom); Department of Physics and Astronomy, University College London, London, WC1E 6BT (United Kingdom)

    2016-07-27

    The Diamond Beamline I13L is dedicated to imaging on the micron- and nano-lengthscale, operating in the energy range between 6 and 30 keV. For this purpose two independent stations have been built. The imaging branch is fully operational for micro-tomography and in-line phase contrast imaging with micrometer resolution. Currently a full-field microscope providing 50nm spatial resolution over a field of view of 100 µm is being tested. On the coherence branch, coherent diffraction imaging techniques such as ptychography and coherent X-ray Bragg diffraction are currently developed. The beamline contains a number of unique features. The machine layout has been modified to the so-called mini-beta scheme, providing significantly increased flux from the two canted undulators. New instrumental designs such as a robot arm for the detector in diffraction experiments have been employed. The imaging branch is operated in collaboration with Manchester University, called therefore the Diamond-Manchester Branchline.

  1. New ambient pressure photoemission endstation at Advanced Light Source beamline 9.3.2

    KAUST Repository

    Grass, Michael E.

    2010-01-01

    During the past decade, the application of ambient pressure photoemission spectroscopy (APPES) has been recognized as an important in situ tool to study environmental and materials science, energy related science, and many other fields. Several APPES endstations are currently under planning or development at the USA and international light sources, which will lead to a rapid expansion of this technique. The present work describes the design and performance of a new APPES instrument at the Advanced Light Source beamline 9.3.2 at Lawrence Berkeley National Laboratory. This new instrument, Scienta R4000 HiPP, is a result of collaboration between Advanced Light Source and its industrial partner VG-Scienta. The R4000 HiPP provides superior electron transmission as well as spectromicroscopy modes with 16 μm spatial resolution in one dimension and angle-resolved modes with simulated 0.5° angular resolution at 24° acceptance. Under maximum transmission mode, the electron detection efficiency is more than an order of magnitude better than the previous endstation at beamline 9.3.2. Herein we describe the design and performance of the system, which has been utilized to record spectra above 2 mbar. © 2010 American Institute of Physics.

  2. I12: the Joint Engineering, Environment and Processing (JEEP) beamline at Diamond Light Source

    Energy Technology Data Exchange (ETDEWEB)

    Drakopoulos, Michael, E-mail: michael.drakopoulos@diamond.ac.uk; Connolley, Thomas; Reinhard, Christina; Atwood, Robert; Magdysyuk, Oxana; Vo, Nghia; Hart, Michael; Connor, Leigh; Humphreys, Bob; Howell, George; Davies, Steve; Hill, Tim; Wilkin, Guy; Pedersen, Ulrik; Foster, Andrew; De Maio, Nicoletta; Basham, Mark; Yuan, Fajin; Wanelik, Kaz [Diamond Light Source Ltd, Harwell Science and Innovation Campus, Didcot, Oxfordshire OX11 0DE (United Kingdom)

    2015-04-08

    JEEP is a high-energy (50–150 keV) multi-purpose beamline offering polychromatic and monochromatic modes. It can accommodate large samples and experimental rigs, enabling in situ studies using radiography, tomography, energy-dispersive diffraction, monochromatic and white-beam two-dimensional diffraction/scattering and small-angle X-ray scattering. I12 is the Joint Engineering, Environmental and Processing (JEEP) beamline, constructed during Phase II of the Diamond Light Source. I12 is located on a short (5 m) straight section of the Diamond storage ring and uses a 4.2 T superconducting wiggler to provide polychromatic and monochromatic X-rays in the energy range 50–150 keV. The beam energy enables good penetration through large or dense samples, combined with a large beam size (1 mrad horizontally × 0.3 mrad vertically). The beam characteristics permit the study of materials and processes inside environmental chambers without unacceptable attenuation of the beam and without the need to use sample sizes which are atypically small for the process under study. X-ray techniques available to users are radiography, tomography, energy-dispersive diffraction, monochromatic and white-beam two-dimensional diffraction/scattering and small-angle X-ray scattering. Since commencing operations in November 2009, I12 has established a broad user community in materials science and processing, chemical processing, biomedical engineering, civil engineering, environmental science, palaeontology and physics.

  3. A small and robust active beamstop for scattering experiments on high-brilliance undulator beamlines.

    Science.gov (United States)

    Blanchet, Clement E; Hermes, Christoph; Svergun, Dmitri I; Fiedler, Stefan

    2015-03-01

    A small active in-vacuum beamstop has been developed to monitor the flux of intense third-generation synchrotron X-ray beams protecting the downstream detector from the direct beam. Standard active beamstops, where a built-in diode directly absorbs the beam, have limitations in size and lifetime. In the present design, a silicon PIN diode detects the photons back-scattered from a cavity in the beamstop. This approach drastically reduces the radiation dose on the diode and thus increases its lifetime. The beamstop with a diameter of 2 mm has been fabricated to meet the requirements for the P12 bioSAXS beamline of EMBL Hamburg at PETRA III (DESY). The beamstop is in regular user operation at the beamline and displays a good response over the range of energies tested (6-20 keV). Further miniaturization of the diode is easily possible as its size is not limited by the PIN diode used.

  4. Support for the Advanced Polymers Beamline at the National Synchrotron Light Source

    Energy Technology Data Exchange (ETDEWEB)

    Hsiao, Benjamin S. [State Univ. of New York (SUNY), Stonybrook, NY (United States)

    2008-10-01

    The primary focus of the X27C beamline is to investigate frontier polymer science and engineering problems with emphasis on real-time studies of structures, morphologies and dynamics from atomic, nanoscopic, microscopic to mesoscopic scales using simultaneous small-angle X-ray scattering (SAXS) and wide-angle X-ray diffraction (WAXD) techniques. The scientific merit of this project is as follows. Currently, many unique sample chambers for in-situ synchrotron studies, developed by the PI (B. Hsiao) and Co-PI (B. Chu), are available for general users of X27C at NSLS. These instruments include a gel/melt spinning apparatus, a continuous fiber drawing apparatus, a tensile stretching apparatus, a high pressure X-ray cell using supercritical carbon dioxide, a parallel plate strain-controlled shear stage and a dynamic rheometer for small-strain oscillatory deformation study. Based on the use of these instruments in combination with synchrotron X-rays, many new insights into the relationships between processing and structure have been obtained in recent years. The broader impact of this project is as follows. The X27C beamline is the first synchrotron facility in the United States dedicated to chemistry/materials research (with emphasis on polymers). The major benefit of this facility to the materials community is that no extensive synchrotron experience and equipment preparation are required from general users to carry out cutting-edge experiments.

  5. Development and Manufacturing of Devices for the Experimental Samples Multi-element Analysis of the Composition of Matter in Real Time as Part of the Mass Spectrometer

    Directory of Open Access Journals (Sweden)

    A.V. Kosulya

    2016-11-01

    Full Text Available The paper discloses advantages of the LSI assembly on a flexible carrier. The paper develops the topology of the flexible carrier and manufacturing of a flexible carrier. LSI samples have been composed on flexible carrier represented by a crystal attached by a dielectric on a thin flexible board with aluminium tracks located on polyimide basis. There are determined manufacturing specifications and the assembly sequence for experimental device samples. The authors constructed the experimental samples of devices for real time multi-element analysis of substances as a component of the mass-spectrometer.

  6. A practical approach to extract symplectic transfer maps numerically for arbitrary magnetic elements

    CERN Document Server

    Li, Yongjun

    2015-01-01

    We introduce a practical approach to extract the symplectic transfer maps for arbitrary magnetic beam-line elements. Beam motion in particle accelerators depends on linear and nonlinear magnetic fields of the beam-line elements. These elements are usually modeled as magnetic multipoles with constant field strengths in the longitudinal direction (i.e., hard-edge model) in accelerator design and modeling codes. For magnets with complicated structures such as insertion devices or fields with significant longitudinal variation effects, the simplified models may not be sufficient to char- acterize beam dynamics behaviors accurately. A numerical approach has been developed to extract symplectic transfer maps from particle trajectory tracking simulation that uses magnetic field data provided by three-dimensional magnetic field modeling codes or experimental measurements. The extracted transfer maps can be used in linear optics design and nonlinear dynamics optimization to achieve more realistic results.

  7. Cyclostationarity and the cepstrum for operational modal analysis of MIMO systems—Part II: Obtaining scaled mode shapes through finite element model updating

    Science.gov (United States)

    Hanson, D.; Randall, R. B.; Antoni, J.; Waters, T. P.; Thompson, D. J.; Ford, R. A. J.

    2007-08-01

    This paper presents a new technique for scaling mode shapes, obtained from cepstrum-based operational modal analysis (OMA) techniques, such as that described in the companion paper, using finite element model updating. This OMA technique estimated frequency response functions (FRFs) between a cyclostationary input and response measurements. If the input is frequentially white, the resulting FRFs can be obtained up to an overall scaling constant using the in-band poles and zeros identified in the OMA process and employing the response autospectrum as a reference to correct for the effect of out of band modes. In this way, the mode shapes would be scaled correctly relative to each other but would still have arbitrary overall magnitude. If the input is not white, then no reference is available to correct FRF regenerated from in-band poles and zeros, and so these FRFs will exhibit both an overall slope resulting from the effect of out-of-band poles and zeros, and an arbitrary magnitude. This overall slope will differ between measurement locations so even the relative scaling between the mode shapes will be lost. This paper describes a simple technique for recovering both the relative and overall scaling of the FRFs, and hence the mode shapes, based on finite element model updating.

  8. Fe-15Ni-13Cr austenitic stainless steels for fission and fusion reactor applications - Part II: Effects of minor elements on precipitate phase stability during thermal aging

    Science.gov (United States)

    Lee, E. H.; Mansur, L. K.

    2000-01-01

    The precipitate phase stability in Fe-15Ni-13Cr base austenitic alloys was investigated as a function of minor alloying additions after thermally aging at 600°C and 675°C for times ranging from 24 h to one year. Seven major precipitate phases were found in aged specimens, including M 23C 6, Laves, Eta (η), TiO, NbC, MC, and M 2P. The types and amounts of precipitate phases varied with alloying element additions, aging temperature, and aging time. By analyzing the composition of each individual particle, it was possible to determine the essential constituent elements for each phase. From this information, a strategy to promote or suppress certain precipitate phases was developed. Among the seven phases, the most desirable precipitate phases were considered to be MC and M 2P, because these particles form on a fine scale with a high number density and, therefore, can serve as effective gas atom trap sites under irradiation.

  9. Explicit Finite Element Modeling of Multilayer Composite Fabric for Gas Turbine Engine Containment Systems, Phase II. Part 3; Material Model Development and Simulation of Experiments

    Science.gov (United States)

    Simmons, J.; Erlich, D.; Shockey, D.

    2009-01-01

    A team consisting of Arizona State University, Honeywell Engines, Systems & Services, the National Aeronautics and Space Administration Glenn Research Center, and SRI International collaborated to develop computational models and verification testing for designing and evaluating turbine engine fan blade fabric containment structures. This research was conducted under the Federal Aviation Administration Airworthiness Assurance Center of Excellence and was sponsored by the Aircraft Catastrophic Failure Prevention Program. The research was directed toward improving the modeling of a turbine engine fabric containment structure for an engine blade-out containment demonstration test required for certification of aircraft engines. The research conducted in Phase II began a new level of capability to design and develop fan blade containment systems for turbine engines. Significant progress was made in three areas: (1) further development of the ballistic fabric model to increase confidence and robustness in the material models for the Kevlar(TradeName) and Zylon(TradeName) material models developed in Phase I, (2) the capability was improved for finite element modeling of multiple layers of fabric using multiple layers of shell elements, and (3) large-scale simulations were performed. This report concentrates on the material model development and simulations of the impact tests.

  10. Neutral Kaon Mixing Beyond the Standard Model with $n_f=2+1$ Chiral Fermions Part 1: Bare Matrix Elements and Physical Results

    CERN Document Server

    Garron, Nicolas; Lytle, Andew T

    2016-01-01

    We compute the hadronic matrix elements of the four-quark operators relevant for $K^0-{\\bar K^0}$ mixing beyond the Standard Model. Our results are from lattice QCD simulations with $n_f=2+1$ flavours of domain-wall fermion, which exhibit continuum-like chiral-flavour symmetry. The simulations are performed at two different values of the lattice spacing ($a\\sim0.08$ and $a\\sim 0.11 \\, \\fm $) and with lightest unitary pion mass $\\sim 300\\, \\MeV$. For the first time, the full set of relevant four-quark operators is renormalised non-perturbatively through RI-SMOM schemes; a detailed description of the renormalisation procedure is presented in a companion paper. We argue that the intermediate renormalisation scheme is responsible for the discrepancies found by different collaborations. We also study different normalisations and determine the matrix elements of the relevant four-quark operators with a precision of $\\sim 5\\%$ or better.

  11. Spatial risk assessment and trace element concentration in reef associated sediments of Van Island, southern part of the Gulf of Mannar, India.

    Science.gov (United States)

    Krishnakumar, S; Ramasamy, S; Chandrasekar, N; Peter, T Simon; Godson, Prince S; Gopal, V; Magesh, N S

    2017-02-15

    Forty eight surface sediment samples were collected from the vicinity of Van Island in order to assess the sediment pollution level and potential ecological risk on coral reef ecosystem. The analytical and correlation results indicate a distribution of elements is chiefly controlled by the CaCO3 and OM. The enrichment factor and geoaccumulation index show the elevated level of Pb in the surface sediments is due to application of lead petrol and coal incinerating power plants. The sediment pollution index reveals that majority of the sediments falling under highly polluted sediment category (35.4%) followed by moderately polluted (25%) and dangerous sediment category (14.58%). The potential ecological risk suggests that nearly 66.6% of the samples falling under the low risk category, moderate risk category (20.8%) followed by considerable risk category (8.33%) and very high risk category (4.1%). The accumulation level of trace elements clearly suggests that the coral reef ecosystem is under low risk. Copyright © 2016 Elsevier Ltd. All rights reserved.

  12. ℎ- Spectral element methods for three dimensional elliptic problems on non-smooth domains, Part-I: Regularity estimates and stability theorem

    Indian Academy of Sciences (India)

    P Dutt; Akhlaq Husain; A S Vasudeva Murthy; C S Upadhyay

    2015-05-01

    This is the first of a series of papers devoted to the study of ℎ- spectral element methods for solving three dimensional elliptic boundary value problems on non-smooth domains using parallel computers. In three dimensions there are three different types of singularities namely; the vertex, the edge and the vertex-edge singularities. In addition, the solution is anisotropic in the neighbourhoods of the edges and vertex-edges. To overcome the singularities which arise in the neighbourhoods of vertices, vertex-edges and edges, we use local systems of coordinates. These local coordinates are modified versions of spherical and cylindrical coordinate systems in their respective neighbourhoods. Away from these neighbourhoods standard Cartesian coordinates are used. In each of these neighbourhoods we use a geometrical mesh which becomes finer near the corners and edges. The geometrical mesh becomes a quasi-uniform mesh in the new system of coordinates. We then derive differentiability estimates in these new set of variables and state our main stability estimate theorem using a non-conforming ℎ- spectral element method whose proof is given in a separate paper.

  13. Characterization of the Etna volcanic emissions through an active biomonitoring technique (moss-bags): part 1--major and trace element composition.

    Science.gov (United States)

    Calabrese, S; D'Alessandro, W; Bellomo, S; Brusca, L; Martin, R S; Saiano, F; Parello, F

    2015-01-01

    Active biomonitoring using moss-bags was applied to an active volcanic environment for the first time. Bioaccumulation originating from atmospheric deposition was evaluated by exposing mixtures of washed and air-dried mosses (Sphagnum species) at 24 sites on Mt. Etna volcano (Italy). Concentrations of major and a large suite of trace elements were analysed by inductively coupled mass and optical spectrometry (ICP-MS and ICP-OES) after total acid digestion. Of the 49 elements analysed those which closely reflect summit volcanic emissions were S, Tl, Bi, Se, Cd, As, Cu, B, Na, Fe, Al. Enrichment factors and cluster analysis allowed clear distinction between volcanogenic, geogenic and anthropogenic inputs that affect the local atmospheric deposition. This study demonstrates that active biomonitoring with moss-bags is a suitable and robust technique for implementing inexpensive monitoring in scarcely accessible and harsh volcanic environments, giving time-averaged quantitative results of the local exposure to volcanic emissions. This task is especially important in the study area because the summit area of Mt. Etna is visited by nearly one hundred thousand tourists each year who are exposed to potentially harmful volcanic emissions. Copyright © 2014 Elsevier Ltd. All rights reserved.

  14. Neutral kaon mixing beyond the Standard Model with n{sub f}=2+1 chiral fermions. Part 1: bare matrix elements and physical results

    Energy Technology Data Exchange (ETDEWEB)

    Garron, Nicolas [Theoretical Physics Division, Department of Mathematical Sciences, University of Liverpool,Brownlow Hill, Liverpool, L69 3BX (United Kingdom); Hudspith, Renwick J. [Department of Physics and Astronomy, York University,4700 Keele Street, Toronto, Ontario, M3J 1P3 (Canada); Lytle, Andrew T. [SUPA, School of Physics and Astronomy, University of Glasgow,University Avenue, Glasgow, G12 8QQ (United Kingdom); Collaboration: The RBC/UKQCD collaboration

    2016-11-02

    We compute the hadronic matrix elements of the four-quark operators relevant for K{sup 0}−K̄{sup 0} mixing beyond the Standard Model. Our results are from lattice QCD simulations with n{sub f}=2+1 flavours of domain-wall fermion, which exhibit continuum-like chiral-flavour symmetry. The simulations are performed at two different values of the lattice spacing (a∼0.08 and a∼0.11 fm) and with lightest unitary pion mass ∼300 MeV. For the first time, the full set of relevant four-quark operators is renormalised non-perturbatively through RI-SMOM schemes; a detailed description of the renormalisation procedure is presented in a companion paper. We argue that the intermediate renormalisation scheme is responsible for the discrepancies found by different collaborations. We also study different normalisations and determine the matrix elements of the relevant four-quark operators with a precision of ∼5% or better.

  15. [Monitoring of contamination of foodstuffs with elements noxious to human health. Part II. Mineral waters, soft drinks, fruits, nuts, rice, soybeans, fish and seafood].

    Science.gov (United States)

    Wojciechowska-Mazurek, Maria; Starska, Krystyna; Mania, Monika; Brulińska-Ostrowska, Elzbieta; Biernat, Urszula; Karłowski, Kazimierz

    2010-01-01

    Results of the 5-years cycle (2004-2008) monitoring investigations on food contamination with elements noxious to human health, involving testing of mineral waters and soft drinks (226 samples), fruits (467 samples), rice (234 samples), soybeans (236 samples), nuts and peanuts (237 samples), fish and seafood (237 samples) are discussed. The parties involved in testing were: laboratories of State Sanitary Inspection and the national reference laboratory of the Department of Food and Consumer Articles Research of National Institute of Public Health - National Institute of Hygiene. The reported metals contents did not give rise to health concerns, remaining generally below the levels set forth in food legislation and being comparable with contamination levels reported in other European countries; and for cadmium--often lower. Health hazard assessment was performed taking into account the mean contamination levels obtained and average domestic consumption of these food products groups in Poland. The highest intake expressed as the percentage of provisional tolerable weekly intake (PTWI) was obtained for mercury in fish, which has reached mean 3.2% PTWI. Controlled fish consumption recommendations should be adhered to by prospective mothers, pregnant women, breast-feeding women and young children. Lead and arsenic intake with mineral waters and soft drinks comprises approx. 15% of total intake of these elements with food.

  16. Fuel Element Technical Manual

    Energy Technology Data Exchange (ETDEWEB)

    Burley, H.H. [ed.

    1956-08-01

    It is the purpose of the Fuel Element Technical Manual to Provide a single document describing the fabrication processes used in the manufacture of the fuel element as well as the technical bases for these processes. The manual will be instrumental in the indoctrination of personnel new to the field and will provide a single data reference for all personnel involved in the design or manufacture of the fuel element. The material contained in this manual was assembled by members of the Engineering Department and the Manufacturing Department at the Hanford Atomic Products Operation between the dates October, 1955 and June, 1956. Arrangement of the manual. The manual is divided into six parts: Part I--introduction; Part II--technical bases; Part III--process; Part IV--plant and equipment; Part V--process control and improvement; and VI--safety.

  17. An alkaline element

    Energy Technology Data Exchange (ETDEWEB)

    Arita, T.; Murakami, K.; Okha, K.

    1983-04-28

    A cathode with a dual layer active mass is installed in the disk shaped alkaline silver and zinc element. The first layer, which is turned towards the anode, contains 85 parts Ag2O, 5 parts electrolytic MnO2 and 10 parts graphite. The second layer, which contacts the bottom of the element, contains 35 parts Ag2O, 60 parts electrolytic MnO2 and 5 parts graphite. The electrical capacity of the first and second layers is 60 and 40, respectively. The first layer may be discharged with a high current density and the second layer with less current density. The element has high characteristics with comparatively low cost.

  18. Chemical composition of modern and fossil hippopotamid teeth and implications for paleoenvironmental reconstructions and enamel formation - Part 2: Alkaline earth elements as tracers of watershed hydrochemistry and provenance

    Science.gov (United States)

    Brügmann, G.; Krause, J.; Brachert, T. C.; Stoll, B.; Weis, U.; Kullmer, O.; Ssemmanda, I.; Mertz, D. F.

    2012-11-01

    This study demonstrates that alkaline earth elements in enamel of hippopotamids, in particular Ba and Sr, are tracers for water provenance and hydrochemistry in terrestrial settings. The studied specimens are permanent premolar and molar teeth found in modern and fossil lacustrine sediments of the Western Branch of the East African Rift system (Lake Kikorongo, Lake Albert, and Lake Malawi) and from modern fluvial environments of the Nile River. Concentrations in enamel vary by two orders of magnitude for Ba (120-9336 μg g-1) as well as for Sr (9-2150 μg g-1). The variations are partially induced during post-mortem alteration and during amelogenesis, but the major contribution originates ultimately from the variable water chemistry in the habitats of the hippopotamids which is controlled by the lithologies and weathering processes in the watershed areas. Amelogenesis causes a distinct distribution of MgO, Ba and Sr in modern and fossil enamel, in that element concentrations increase along profiles from the outer rim towards the enamel-dentin junction by a factor of 1.3-1.9. These elements are well correlated in single specimens, thus suggesting that their distribution is determined by a common, single process, which can be described by closed system Rayleigh crystallization of bioapatite in vivo. Enamel from most hippopotamid specimens has Sr/Ca and Ba/Ca which are typical for herbivores. However, Ba/Sr ranges from 0.1 to 3 and varies on spatial and temporal scales. Thus, Sr concentrations and Ba/Sr in enamel differentiate between habitats having basaltic mantle rocks or Archean crustal rocks as the ultimate sources of Sr and Ba. This provenance signal is modulated by climate change. In Miocene to Pleistocene enamel from the Lake Albert region, Ba/Sr decreases systematically with time from 2 to 0.5. This trend can be correlated with changes in climate from humid to arid, in vegetation from C3 to C4 biomass as well as with increasing evaporation of the lake water

  19. An atomic finite element model for biodegradable polymers. Part 2. A model for change in Young's modulus due to polymer chain scission.

    Science.gov (United States)

    Gleadall, Andrew; Pan, Jingzhe; Kruft, Marc-Anton

    2015-11-01

    Atomic simulations were undertaken to analyse the effect of polymer chain scission on amorphous poly(lactide) during degradation. Many experimental studies have analysed mechanical properties degradation but relatively few computation studies have been conducted. Such studies are valuable for supporting the design of bioresorbable medical devices. Hence in this paper, an Effective Cavity Theory for the degradation of Young's modulus was developed. Atomic simulations indicated that a volume of reduced-stiffness polymer may exist around chain scissions. In the Effective Cavity Theory, each chain scission is considered to instantiate an effective cavity. Finite Element Analysis simulations were conducted to model the effect of the cavities on Young's modulus. Since polymer crystallinity affects mechanical properties, the effect of increases in crystallinity during degradation on Young's modulus is also considered. To demonstrate the ability of the Effective Cavity Theory, it was fitted to several sets of experimental data for Young's modulus in the literature.

  20. Evaluation of SNS Beamline Shielding Configurations using MCNPX Accelerated by ADVANTG

    Energy Technology Data Exchange (ETDEWEB)

    Risner, Joel M [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Johnson, Seth R. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Remec, Igor [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Bekar, Kursat B. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

    2015-01-01

    Shielding analyses for the Spallation Neutron Source (SNS) at Oak Ridge National Laboratory pose significant computational challenges, including highly anisotropic high-energy sources, a combination of deep penetration shielding and an unshielded beamline, and a desire to obtain well-converged nearly global solutions for mapping of predicted radiation fields. The majority of these analyses have been performed using MCNPX with manually generated variance reduction parameters (source biasing and cell-based splitting and Russian roulette) that were largely based on the analyst's insight into the problem specifics. Development of the variance reduction parameters required extensive analyst time, and was often tailored to specific portions of the model phase space. We previously applied a developmental version of the ADVANTG code to an SNS beamline study to perform a hybrid deterministic/Monte Carlo analysis and showed that we could obtain nearly global Monte Carlo solutions with essentially uniform relative errors for mesh tallies that cover extensive portions of the model with typical voxel spacing of a few centimeters. The use of weight window maps and consistent biased sources produced using the FW-CADIS methodology in ADVANTG allowed us to obtain these solutions using substantially less computer time than the previous cell-based splitting approach. While those results were promising, the process of using the developmental version of ADVANTG was somewhat laborious, requiring user-developed Python scripts to drive much of the analysis sequence. In addition, limitations imposed by the size of weight-window files in MCNPX necessitated the use of relatively coarse spatial and energy discretization for the deterministic Denovo calculations that we used to generate the variance reduction parameters. We recently applied the production version of ADVANTG to this beamline analysis, which substantially streamlined the analysis process. We also tested importance function

  1. Conceptual design of an undulator system for a dedicated bio-imaging beamline at the European X-ray FEL

    CERN Document Server

    Geloni, Gianluca; Saldin, Evgeni

    2012-01-01

    We describe a future possible upgrade of the European XFEL consisting in the construction of an undulator beamline dedicated to life science experiments. The availability of free undulator tunnels at the European XFEL facility offers a unique opportunity to build a beamline optimized for coherent diffraction imaging of complex molecules, like proteins and other biologically interesting structures. Crucial parameters for such bio-imaging beamline are photon energy range, peak power, and pulse duration. Key component of the setup is the undulator source. The peak power is maximized in the photon energy range between 3 keV and 13 keV by the use of a very efficient combination of self-seeding, fresh bunch and tapered undulator techniques. The unique combination of ultra-high peak power of 1 TW in the entire energy range, and ultrashort pulse duration tunable from 2 fs to 10 fs, would allow for single shot coherent imaging of protein molecules with size larger than 10 nm. Also, the new beamline would enable imagin...

  2. Research at and Operation of the Materials Science Beamline (X-11) at the National Synchrotron Light Source. Final Report

    Energy Technology Data Exchange (ETDEWEB)

    Sayers, Dale E.

    2003-10-15

    This is the final report for DOE DE-FG02-89ER45384. An overview of the operational history and status of beamline X-11A at the end of the contract period, and a brief review of the core science program at NCSU and the scientific results of X-11A since the last progress report is also presented.

  3. Chemical composition of modern and fossil Hippopotamid teeth and implications for paleoenvironmental reconstructions and enamel formation - Part 1: Major and minor element variation

    Science.gov (United States)

    Brügmann, G.; Krause, J.; Brachert, T. C.; Kullmer, O.; Schrenk, F.; Ssemmanda, I.; Mertz, D. F.

    2012-01-01

    Bioapatite in mammalian teeth is readily preserved in continental sediments and represents a very important archive for reconstructions of environment and climate evolution. This project provides a comprehensive data base of major, minor and trace element and isotope tracers for tooth apatite using a variety of microanalytical techniques. The aim is to identify specific sedimentary environments and to improve our understanding on the interaction between internal metabolic processes during tooth formation and external nutritional control and secondary alteration effects. Here, we use the electron microprobe to determine the major and minor element contents of fossil and modern molar enamel, cement and dentin from Hippopotamids. Most of the studied specimens are from different ecosystems in Eastern Africa, representing modern and fossil lacustrine (Lake Kikorongo, Lake Albert, and Lake Malawi) and modern fluvial environments of the Nile River system. Secondary alteration effects - in particular FeO, MnO, SO3 and F concentrations - are 2 to 10 times higher in fossil than in modern enamel; the secondary enrichment of these components in fossil dentin and cement is even higher. In modern and fossil enamel, along sections perpendicular to the enamel-dentin junction (EDJ) or along cervix-apex profiles, P2O5 and CaO contents and the CaO/P2O5 ratios are very constant (StdDev ∼1%). Linear regression analysis reveals tight control of the MgO (R2∼0.6), Na2O and Cl variation (for both R2>0.84) along EDJ-outer enamel rim profiles, despite large concentration variations (40% to 300%) across the enamel. These minor elements show well defined distribution patterns in enamel, similar in all specimens regardless of their age and origin, as the concentration of MgO and Na2O decrease from the enamel-dentin junction (EDJ) towards the outer rim, whereas Cl displays the opposite trend. Fossil enamel from Hippopotamids which lived in the saline Lake Kikorongo have a much higher MgO/Na2

  4. A finite-element-based perturbation model for the rotordynamic analysis of shrouded pump impellers: Part 1: Model development and applications

    Science.gov (United States)

    Baskharone, Erian A.

    1993-09-01

    This study concerns the rotor dynamic characteristics of fluid-encompassed rotors, with special emphasis on shrouded pump impellers. The core of the study is a versatile and categorically new finite-element-based perturbation model, which is based on a rigorous flow analysis and what we have generically termed the 'virtually' deformable finite-element approach. The model is first applied to the case of a smooth annular seal for verification purposes. The rotor excitation components, in this sample problem, give rise to a purely cylindrical, purely conical, and a simultaneous cylindrical/conical rotor whirl around the housing centerline. In all cases, the computed results are compared to existing experimental and analytical data involving the same seal geometry and operating conditions. Next, two labyrinth-seal configurations, which share the same tooth-to-tooth chamber geometry but differ in the total number of chambers, were investigated. The results, in this case, are compared to experimental measurements for both seal configurations. The focus is finally shifted to the shrouded-impeller problem, where the stability effects of the leakage flow in the shroud-to-housing secondary passage are investigated. To this end, the computational model is applied to a typical shrouded-impeller pump stage, fabricated and rotor dynamically tested by Sulzer Bros., and the results compared to those of a simplified 'bulk-flow' analysis and Sulzer Bros.' test data. In addition to assessing the computed rotor dynamic coefficients, the shrouded-impeller study also covers a controversial topic, namely that of the leakage-passage inlet swirl, which was previously cited as the origin of highly unconventional (resonance-like) trends of the fluid-exerted forces. In order to validate this claim, a 'microscopic' study of the fluid/shroud interaction mechanism is conducted, with the focus being on the structure of the perturbed flow field associated with the impeller whirl. The conclusions

  5. A finite-element-based perturbation model for the rotordynamic analysis of shrouded pump impellers: Part 1: Model development and applications

    Science.gov (United States)

    Baskharone, Erian A.

    1993-01-01

    This study concerns the rotor dynamic characteristics of fluid-encompassed rotors, with special emphasis on shrouded pump impellers. The core of the study is a versatile and categorically new finite-element-based perturbation model, which is based on a rigorous flow analysis and what we have generically termed the 'virtually' deformable finite-element approach. The model is first applied to the case of a smooth annular seal for verification purposes. The rotor excitation components, in this sample problem, give rise to a purely cylindrical, purely conical, and a simultaneous cylindrical/conical rotor whirl around the housing centerline. In all cases, the computed results are compared to existing experimental and analytical data involving the same seal geometry and operating conditions. Next, two labyrinth-seal configurations, which share the same tooth-to-tooth chamber geometry but differ in the total number of chambers, were investigated. The results, in this case, are compared to experimental measurements for both seal configurations. The focus is finally shifted to the shrouded-impeller problem, where the stability effects of the leakage flow in the shroud-to-housing secondary passage are investigated. To this end, the computational model is applied to a typical shrouded-impeller pump stage, fabricated and rotor dynamically tested by Sulzer Bros., and the results compared to those of a simplified 'bulk-flow' analysis and Sulzer Bros.' test data. In addition to assessing the computed rotor dynamic coefficients, the shrouded-impeller study also covers a controversial topic, namely that of the leakage-passage inlet swirl, which was previously cited as the origin of highly unconventional (resonance-like) trends of the fluid-exerted forces. In order to validate this claim, a 'microscopic' study of the fluid/shroud interaction mechanism is conducted, with the focus being on the structure of the perturbed flow field associated with the impeller whirl. The conclusions

  6. Conceptual design of an undulator system for a dedicated bio-imaging beamline at the European X-ray FEL

    Energy Technology Data Exchange (ETDEWEB)

    Geloni, Gianluca [European XFEL GmbH, Hamburg (Germany); Kocharyan, Vitali; Saldin, Evgeni [Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)

    2012-05-15

    We describe a future possible upgrade of the European XFEL consisting in the construction of an undulator beamline dedicated to life science experiments. The availability of free undulator tunnels at the European XFEL facility offers a unique opportunity to build a beamline optimized for coherent diffraction imaging of complex molecules, like proteins and other biologically interesting structures. Crucial parameters for such bio-imaging beamline are photon energy range, peak power, and pulse duration. Key component of the setup is the undulator source. The peak power is maximized in the photon energy range between 3 keV and 13 keV by the use of a very efficient combination of self-seeding, fresh bunch and tapered undulator techniques. The unique combination of ultra-high peak power of 1 TW in the entire energy range, and ultrashort pulse duration tunable from 2 fs to 10 fs, would allow for single shot coherent imaging of protein molecules with size larger than 10 nm. Also, the new beamline would enable imaging of large biological structures in the water window, between 0.3 keV and 0.4 keV. In order to make use of standardized components, at present we favor the use of SASE3-type undulator segments. The number segments, 40, is determined by the tapered length for the design output power of 1 TW. The present plan assumes the use of a nominal electron bunch with charge of 0.1 nC. Experiments will be performed without interference with the other three undulator beamlines. Therefore, the total amount of scheduled beam time per year is expected to be up to 4000 hours.

  7. Advanced photoelectric effect experiment beamline at Elettra: A surface science laboratory coupled with Synchrotron Radiation.

    Science.gov (United States)

    Panaccione, G; Vobornik, I; Fujii, J; Krizmancic, D; Annese, E; Giovanelli, L; Maccherozzi, F; Salvador, F; De Luisa, A; Benedetti, D; Gruden, A; Bertoch, P; Polack, F; Cocco, D; Sostero, G; Diviacco, B; Hochstrasser, M; Maier, U; Pescia, D; Back, C H; Greber, T; Osterwalder, J; Galaktionov, M; Sancrotti, M; Rossi, G

    2009-04-01

    We report the main characteristics of the advanced photoelectric effect experiments beamline, operational at Elettra storage ring, featuring a fully independent double branch scheme obtained by the use of chicane undulators and able to keep polarization control in both linear and circular mode. The paper describes the novel technical solutions adopted, namely, (a) the design of a quasiperiodic undulator resulting in optimized suppression of higher harmonics over a large photon energy range (10-100 eV), (b) the thermal stability of optics under high heat load via cryocoolers, and (c) the end station interconnected setup allowing full access to off-beam and on-beam facilities and, at the same time, the integration of users' specialized sample growth chambers or modules.

  8. Achieving Vibration Stability of the NSLS-II Hard X-ray Nanoprobe Beamline

    Energy Technology Data Exchange (ETDEWEB)

    Simos, N.

    2010-08-30

    The Hard X-ray Nanoprobe (HXN) Beamline of National Synchrotron Light Source II (NSLS-lI) requires high levels of stability in order to achieve the desired instrument resolution. To ensure that the design of the endstation helps meet the stringent criteria and that natural and cultural vibration is mitigated both passively and actively, a comprehensive study complimentary to the design process has been undertaken. Vibration sources that have the potential to disrupt sensitive experiments such as wind, traffic and NSLS II operating systems have been studied using state of the art simulations and an array of field data. Further, final stage vibration isolation principles have been explored in order to be utilized in supporting endstation instruments. This paper presents results of the various study aspects and their influence on the HXN design optimization.

  9. An in-situ heater for the XAS beamline (12-ID) in Australia

    Science.gov (United States)

    Johannessen, B.; Hussain, Z. S.; East, D. R.; Gibson, M. A.

    2013-04-01

    To accommodate for a growing number of requests by our user community an in-situ heater has been commissioned for the X-ray absorption spectroscopy (XAS) beamline 12-ID at the Australian Synchrotron. Here, we present an in-situ method for calibrating the temperature of the heating stage based on an anharmonic, correlated Einstein model. Specifically, we show that a temperature-dependant study of a bulk metallic foil (7.5 μm Cu) can be used to accurately calibrate the temperature of the heater. We also present the temperature-dependant coordination number, bond length, Debye-Waller factor, and third order cumulant to the bond length distribution function of the material from 18K to 1074K. At the higher temperatures we find that the atomic structure is comparable to that of an amorphous or liquid material indicating a gradual transition from crystalline to disordered atomic structure.

  10. The sapphire backscattering monochromator at the Dynamics beamline P01 of PETRA III

    Science.gov (United States)

    Alexeev, P.; Asadchikov, V.; Bessas, D.; Butashin, A.; Deryabin, A.; Dill, F.-U.; Ehnes, A.; Herlitschke, M.; Hermann, R. P.; Jafari, A.; Prokhorov, I.; Roshchin, B.; Röhlsberger, R.; Schlage, K.; Sergueev, I.; Siemens, A.; Wille, H.-C.

    2016-12-01

    We report on a high resolution sapphire backscattering monochromator installed at the Dynamics beamline P01 of PETRA III. The device enables nuclear resonance scattering experiments on Mössbauer isotopes with transition energies between 20 and 60 keV with sub-meV to meV resolution. In a first performance test with 119Sn nuclear resonance at a X-ray energy of 23.88 keV an energy resolution of 1.34 meV was achieved. The device extends the field of nuclear resonance scattering at the PETRA III synchrotron light source to many further isotopes like 151Eu, 149Sm, 161Dy, 125Te and 121Sb.

  11. Commissioning of a UV/time-resolved-FTIR beamline at the Duke FEL laboratory

    CERN Document Server

    Hutson, M S; Chang, M S; Gillikin, A; Litvinenko, V N; Edwards, G

    2002-01-01

    We describe the commissioning of a novel two-color beamline at the Duke Free Electron Laser Laboratory, designed to perform time-resolved FTIR spectroscopy in a pump-probe scheme with sub-nanosecond resolution to measure dynamical processes with durations as long as 10 ns. The UV pump pulses are produced by the tunable (193-700 nm) output of the OK-4 Storage-Ring FEL. The broadband, infrared probe pulses are generated as synchrotron radiation in a bending magnet downstream of the OK-4 wiggler. The repetition rate of the light source (2.79 MHz) is ideal for operating the interferometer in the rapid-scan, asynchronous sampling mode. An investigation of DNA photolyase is proposed.

  12. A Johann-type X-ray emission spectrometer at the Rossendorf beamline.

    Science.gov (United States)

    Kvashnina, Kristina O; Scheinost, Andreas C

    2016-05-01

    This paper gives a detailed description, including equations, of the Johann-type X-ray emission spectrometer which has been recently installed and tested at the Rossendorf beamline (ROBL) of the European Synchrotron Radiation Facility. The spectrometer consists of a single spherically bent crystal analyzer and an avalanche photodiode detector positioned on the vertical Rowland cycle of 1 m diameter. The hard X-ray emission spectrometer (∼3.5-25 keV) operates at atmospheric pressure and covers the Bragg angles of 65°-89°. The instrument has been tested at high and intermediate incident energies, i.e. at the Zr K-edge and at the Au L3-edge, in the second experimental hutch of ROBL. The spectrometer is dedicated for studying actinides in materials and environmental samples by high-energy-resolution X-ray absorption and X-ray emission spectroscopies.

  13. Upgrading of the PETRA-2 beamline at HASYLAB for materials science analyses

    CERN Document Server

    Kampmann, R; Burmester, J; Santos, J F D; Franz, H; Haese-Seiller, M; Marmotti, M

    2001-01-01

    The high energy synchrotron radiation beamline PETRA-2 at HASYLAB has been extended by two 2D-position sensitive multi-wire Xe/CO sub 2 detectors with an active area of (300 mm) sup 2 and a detection probability of approx 10% for 100 keV photons. The detectors may be placed at distances between approx 1 m and 8 m from the sample in order to cover large space angles or to measure with high resolution, respectively. Fast 3D-data acquisition systems allow for analyses of continuous processes with excellent time resolution and sample movements during measurements with continuously operating detectors. The experimental set up will be especially used for analyses of residual stresses, local textures and kinetics of phase transformations.

  14. Stress mitigation of x-ray beamline monochromators using topography test unit.

    Energy Technology Data Exchange (ETDEWEB)

    Maj, J.; Waldschmidt, G.; Baldo, P.; Macrander, A.; Koshelev, I.; Huang, R.; Maj, L.; Maj, A.; Univ. of Chicago; Northeastern Ohio Univ. Coll. of Medicine; Rosalind Franklin Univ. of Medicine and Science

    2007-01-01

    Silicon and diamond monochromators (crystals), often used in the Advanced Photon Source X-ray beamlines, require a good quality surface finish and stress-free installation to ensure optimal performance. The device used to mount the crystal has been shown to be ajor contributing source of stress. In this case, an adjustable mounting device is an effective method of reducing stresses and improve the rocking curve to levels much closer to ideal. Analysis by a topography test unit has been used to determine the distribution of stresses and to measure the rocking curve, as well as create CCD images of the crystal. This paper describes the process of measuring these stresses and manipulating the mounting device and crystal to create a substantially improved monochromator.

  15. A new diffractometer for materials science and imaging at HASYLAB beamline G3

    CERN Document Server

    Wróblewski, T; Crostack, H A; Ertel, A; Fandrich, F; Genzel, C; Hradil, K; Ternes, W; Woldt, E

    1999-01-01

    A 4-circle diffractometer equipped with a novel imaging system has been installed at HASYLAB beamline G3. The imaging system comprising a microchannel plate (MCP) in front of a CCD detector allows position-resolved X-ray diffraction investigations of polycrystalline materials. Alternatively, a scintillation counter behind a Soller collimator can be used. Material properties like strain and/or texture can thus be determined either position resolved using the MCP/CCD system or in an averaging mode using the Soller/scintillator combination. The field of view of the MCP/CCD system is larger than 1 cm sup 2 with a spatial resolution down to 12 mu m. Both detection systems applied are aberration free. The spatial information can be directly extracted from pictures taken by the imaging system. Together with the wide field of view this method is especially suited for the investigation of dynamical processes in polycrystalline materials.

  16. ELIMED: MEDICAL APPLICATION AT ELI-BEAMLINES. STATUS OF THE COLLABORATION AND FIRST RESULTS

    Directory of Open Access Journals (Sweden)

    Francesco Schillaci

    2014-08-01

    Full Text Available ELI-Beamlines is one of the four pillars of the ELI (Extreme Light Infrastructure pan-European project. It will be an ultrahigh-intensity, high repetition-rate, femtosecond laser facility whose main goal is to generate and apply high-brightness X-ray sources and accelerated charged particles. In particular, medical applications are treated by the ELIMED task force, which has been launched by collaboration between ELI and INFN researchers. ELIMED aims to demonstrate the clinical applicability of laser accelerated ions. In this article, the state of the ELIMED project and the first scientific results are reported. The design and realisation of a preliminary beam handling system and of an advanced spectrometer for diagnostics of high energy (multi-MeV laser-accelerated ion beams will also be briefly presented.

  17. Three-dimensional finite element analysis of posterior fiber-reinforced composite fixed partial denture Part 2: influence of fiber reinforcement on mesial and distal connectors.

    Science.gov (United States)

    Aida, Nobuhisa; Shinya, Akikazu; Yokoyama, Daiichiro; Lassila, Lippo V J; Gomi, Harunori; Vallittu, Pekka K; Shinya, Akiyoshi

    2011-01-01

    The aim of this study was to evaluate the influence of connectors under two different loading conditions on displacement and stress distribution generated in isotropic hybrid composite fixed partial denture (C-FPD) and partially anisotropic fiber-reinforced hybrid composite fixed partial denture (FRC-FPD). To this end, two three-dimensional finite element (FE) models of three-unit FPD from mandibular second premolar to mandibular second molar - intended to replace the mandibular first molar - were developed. The two loading conditions employed were a vertical load of 629 N (applied to eight points on the occlusal surface) and a lateral load of 250 N (applied to three points of the pontic). The results suggested that the reinforcing fibers in FRC framework significantly improved the rigidity of the connectors against any twisting and bending moments induced by loading. Consequently, maximum principal stress and displacement generated in the connectors of FRC-FPD were significantly reduced because stresses generated by vertical and lateral loading were transferred to the reinforcing fibers.

  18. Evaluation of the effect of the residual bone angulation on implant-supported fixed prosthesis in mandibular posterior edentulism. Part II: 3-D finite element stress analysis.

    Science.gov (United States)

    Akça, K; Iplikçioğlu, H

    2001-01-01

    Buccolingual angulation of the mandibular posterior edentulous region may affect the prosthetic load conditions, so as to cause high stress concentrated areas that may easily lead to failure. The aim of this study was to evaluate the effect of various predetermined buccolingual angulation values on stress distribution in the mandibular posterior edentulous region restored with implant-supported fixed partial dentures, using three-dimensional finite element analysis. Stress analyses were performed applying 400N oblique force to implant-supported fixed prosthesis. Stress analyses indicated tensile stress values on the buccal surface and compressive stress values on the lingual surface of cortical bone were increased as the angulation of the edentulous bone increased (especially corresponding to the cervical region of the implants). Compressive stress values, observed where two implants were placed at the second premolar and second molar regions (5-7 design) and first and second molar regions (6-7 design), respectively, were very close to or even exceeded the ultimate compressive strength of bone. It is concluded that when a definite buccolingual angulation is added to other existing risk factors such as bruxism, placing an implant for every missing tooth might reduce the high stress concentration areas.

  19. Finite element analysis of equine incisor teeth. Part 2: investigation of stresses and strain energy densities in the periodontal ligament and surrounding bone during tooth movement.

    Science.gov (United States)

    Schrock, P; Lüpke, M; Seifert, H; Staszyk, C

    2013-12-01

    This study investigated the hypothetical contribution of biomechanical loading to the onset of equine odontoclastic tooth resorption and hypercementosis (EOTRH) and to elucidate the physiological age-related positional changes of the equine incisors. Based on high resolution micro-computed tomography (μCT) datasets, 3-dimensional models of entire incisor arcades and the canine teeth were constructed representing a young and an old incisor dentition. Special attention was paid to constructing an anatomically correct model of the periodontal ligament (PDL). Using previously determined Young's moduli for the equine incisor PDL, finite element (FE) analysis was performed. Resulting strains, stresses and strain energy densities (SEDs), as well as the resulting regions of tension and compression within the PDL and the surrounding bone were investigated during occlusion. The results showed a distinct distribution pattern of high stresses and corresponding SEDs in the PDL and bone. Due to the tooth movement, peaks of SEDs were obtained in the PDL as well as in the bone on the labial and palatal/lingual sides of the alveolar crest. At the root, highest SEDs were detected in the PDL on the palatal/lingual side slightly occlusal of the root tip. This distribution pattern of high SEDs within the PDL coincides with the position of initial resorptive lesions in EOTRH affected teeth. The position of high SEDs in the bone can explain the typical age-related alteration of shape and angulation of equine incisors.

  20. RATIONAL STRUCTURES OF POLITICS IN MONTESQUIEU’S THE SPIRIT OF THE LAWS. PART I: THE KEY ELEMENTS LEGITIMATING THE POWER AND ITS SOURCES

    Directory of Open Access Journals (Sweden)

    MARIUS DUMITRESCU

    2013-05-01

    Full Text Available In The Spirit of the Laws, Montesquieu tried not to discuss about laws, but in fact, about the type of power hiding behind them. Inspired by Plato and Aristotle, he built his own vision on the palingenesis of the political forms and of the principles governing them. Baron de La Brède started from ideas, from spiritual structures, that have the role to create certain social behaviors, and identified three types of government forms, each characterized by its own nature and principle: monarchy, democracy, and despotism. The French philosopher tried to understand, besides the principles ensuring the nature of each government, the key elements legitimating the power and also its sources. The monarchy is seen by Montesquieu as the most suitable regime, for his time, to rule free societies. The aristocracy helps to the maintenance of freedom in royalty by resisting to any attempt of the crown to exceed its constitutional prerogatives. The transition from one form of government to another is done because of the alteration of principles. Democracy is maybe the most exposed to alteration as its excess of freedom leads to the affirmation of the spirit of endless equality that makes everybody wanting to be the equals to the rulers. Montesquieu sees no other solution to replace the degraded forms of political organization than the confederative republic. Such a political organization would answer the need for permanent political flexibility.

  1. Preliminary measurements on the new TOF system installed at the AMS beamline of INFN-LABEC

    Energy Technology Data Exchange (ETDEWEB)

    Palla, L., E-mail: palla@fi.infn.it [Dipartimento di Fisica, Università di Pisa, e INFN Sezione di Pisa (Italy); Castelli, L. [INFN Sezione di Firenze (Italy); Czelusniak, C. [INFN Sezione di Firenze (Italy); Dipartimento di Fisica e Astronomia, Università di Firenze (Italy); Fedi, M.E. [INFN Sezione di Firenze (Italy); Giuntini, L. [INFN Sezione di Firenze (Italy); Dipartimento di Fisica e Astronomia, Università di Firenze (Italy); Liccioli, L. [INFN Sezione di Firenze (Italy); Dipartimento di Chimica Ugo Schiff, Università di Firenze (Italy); Mandò, P.A. [INFN Sezione di Firenze (Italy); Dipartimento di Fisica e Astronomia, Università di Firenze (Italy); Martini, M. [Dipartimento di Scienza dei Materiali, Università di Milano Bicocca, e INFN Sezione di Milano Bicocca, Milano (Italy); Mazzinghi, A. [INFN Sezione di Firenze (Italy); Dipartimento di Fisica e Astronomia, Università di Firenze (Italy); Ruberto, C. [INFN Sezione di Firenze (Italy); Dipartimento di Chimica Ugo Schiff, Università di Firenze (Italy); Schiavulli, L. [Dipartimento di Fisica, Università di Bari, e INFN Sezione di Bari (Italy); Sibilia, E. [Dipartimento di Scienza dei Materiali, Università di Milano Bicocca, e INFN Sezione di Milano Bicocca, Milano (Italy); Taccetti, F. [INFN Sezione di Firenze (Italy)

    2015-10-15

    A high resolution time of flight (TOF) system has been developed at LABEC, the 3 MV Tandem accelerator laboratory in Florence, in order to improve the sensitivity of AMS measurements on carbon samples with ultra-low concentration and also to measure other isotopes, such as {sup 129}I. The system can be employed to detect and identify residual interfering particles originated from the break-up of molecular isobars. The set-up has been specifically designed for low energy heavy ions: it consists of two identical time pick-off stations, each made up of a thin conductive foil and a Micro-Channel Plate (MCP) multiplier. The beamline is also equipped with a silicon detector, installed downstream the stop TOF station. In this paper the design of the new system and the implemented readout electronics are presented. The tests performed on the single time pick-off station are reported: they show that the maximum contribution to the timing resolution given by both the intrinsic MCP resolution and the electronics is ⩽500 ps (FWHM). For these tests, single particle pulsed beams of 2–5 MeV protons and 10 MeV {sup 12}C{sup 3+} ions, to simulate typical AMS conditions, were used. The preliminary TOF and TOF-E (TOF-energy) measurements performed with carbon beams after the installation of the new system on the AMS beam line are also discussed. These measurements were performed using the foil–MCP as the start stage and a silicon detector as the stop stage. The spectra acquired with carbon ions suggest the presence of a small residual background from neighboring masses reaching the end of the beamline with the same energy as the rare isotope.

  2. Universal imaging: Dissociative ionization of polyatomic molecules, chemical dynamics beamline 9.0.2

    Energy Technology Data Exchange (ETDEWEB)

    Ahmed, M.; Chen, D.; Suits, A.G. [Ernest Orlando Lawrence Berkeley National Lab., CA (United States)

    1997-04-01

    A third endstation was recently added to the Chemical Dynamics beamline, designed to exploit the high flux broadband undulator light for a range of studies of reactive scattering, photochemistry and photoionization processes using time-of-flight mass spectroscopy coupled with position-sensitive detection. Two molecular beam sources are fixed at right angles, with the undulator light, or laser beams, intersecting the molecular beams at 45{degrees}. To date, beamline experiments have included a study of dissociative photoionization of a variety of molecules including N{sub 2}O and SF{sub 6}. In this mode, a single molecular beam source is used, with the tunable undulator light inducing, in SF{sub 6} for example, the process SF{sub 6} {r_arrow} SF{sub 6}{sup +} + e{sup {minus}} {r_arrow} SF{sub 5}{sup +} + F + e{sup {minus}}. The SF{sub 5}{sup +} ions are accelerated up the flight tube, mass selected and detected as a function of position on a phosphor screen viewed by a CCD camera. The position directly reveals the recoil speed (or translational energy release) and angular distribution for the dissociative ionization process. Furthermore, this measurement is obtained for all recoil speeds and angles simultaneously. Such detailed angular information has not previously been obtained for dissociative ionization processes; typically ion time-of-flight profiles are deconvoluted to yield rough insight into the angular distributions. The recorded image is actually a 2-dimensional projection of the nascent 3-dimensional velocity distribution, but established tomographic techniques enable the authors to reconstruct the 3-D distribution.

  3. Optimized beamline design for macromolecular crystallography at the Cornell High Energy Synchrotron Source (CHESS) (abstract)

    Science.gov (United States)

    Schildkamp, Wilfried; Bilderback, Donald; Moffat, Keith

    1989-07-01

    The A1 station on the CHESS wiggler beamline has been the workhorse for most macromolecular crystallographic experiments. This station is equipped with a fixed energy focusing germanium (111) monochromator and a focusing total reflection mirror. Our macromolecular crystallographers made full use of the high flux of more than 1012 photons/s/mm2 and the stable beam conditions, both in position and energy resolution. As a result, the A1 station was heavily oversubscribed. CHESS is presently expanding its capabilities and a new diffraction station for macromolecular crystallography is under construction. This beamline will be powered by a 24-pole hybrid permanent magnet wiggler with a critical energy of 25 keV. A focusing monochromator, which handles a specific heat load of 10 W/mm2, will have a range of tunability which covers all relevant absorption edges from 7 to 15 keV using a Ge(111) crystal. The energy resolution and the focusing properties remain constant within a factor of 2 over the entire tunability range. We expect a brilliance of about 1013 photons/s/mm2/mrad2/0.1% bandpass. The diffraction station will be equipped with an oscillation camera which can be used with x-ray film of 5×5 or 8×10 in. size or alternatively with Kodak storage phosphors. A wide variety of clamp-on accessories, like crystal coolers, fast shutters, helium pathways, polarimeter, etc. are available. The station will contain a beampipe system, which can also be used for small angle scattering experiments with sample-to-detector distances of up to 3000 mm. The entire diffraction station, its control area, a biological preparation area, and a darkroom are to be embedded in a biological safety containment of the level BL3. This will allow diffraction studies of virulent strains of viruses and other biohazards, which could not previously be studied at synchrotron radiation sources before without causing major disruption to the normal laboratory procedure.

  4. The EIS beamline at the seeded free-electron laser FERMI

    Science.gov (United States)

    Simoncig, A.; Mincigrucci, R.; Principi, E.; Bencivenga, F.; Calvi, A.; Foglia, L.; Kurdi, G.; Raimondi, L.; Manfredda, M.; Mahne, N.; Gobessi, R.; Gerusina, S.; Fava, C.; Zangrando, M.; Matruglio, A.; Dal Zilio, S.; Masciotti, V.; Masciovecchio, C.

    2017-05-01

    Among the fourth-generation light sources, the Italian free-electron laser (FEL) FERMI is the only one operating in the high-gain harmonic generation (HGHG) seeding mode. FERMI delivers pulses characterized by a quasi transform limited temporal structure, photon energies lying in the extreme ultra-violet (EUV) region, supreme transversal and longitudinal coherences, high peak brilliance, and full control of the polarization. Such state of the art performances recently opened the doors to a new class of time-resolved spectroscopies, difficult or even impossible to be performed using self-amplified spontaneous sources (SASE) light sources. FERMI is currently equipped with three operating beamlines opened to external users (DiProI, LDM and EIS), while two more are under commissioning (MagneDYN and TeraFERMI). Here, we present the recent highlights of the EIS (Elastic and Inelastic Scattering) beamline, which has been purposely designed to take full advantage from the coherence, the intensity, the harmonics content, and the temporal duration of the pulses. EIS is a flexible experimental facility for time-resolved EUV scattering experiments on condensed matter systems, consisting of two independent end-stations. The first one (EIS-TIMEX) aims to study materials in metastable and warm dense matter (WDM) conditions, while the second end-station (EIS-TIMER) is fully oriented to the extension of four-wave mixing (FWM) spectroscopies towards the EUV spectral regions, trying to reveal the behavior of matter in portions of the mesoscopic regime of exchanged momentum impossible to be probed using conventional light sources.

  5. Innovations in the design of mechanical components for a beamline -- The SRl`95 Workshop 2 summary

    Energy Technology Data Exchange (ETDEWEB)

    Kuzay, T.M. [Argonne National Lab., IL (United States); Warwick, T. [Lawrence Berkeley Lab., CA (United States)

    1995-12-31

    The Synchrotron Radiation Instrumentation 1995 Conference (SRI`95) was hosted by the Advanced Photon Source (APS) at Argonne National Laboratory (ANL). Of the many workshops within the conference, the SRI`95 Workshop 2 was ``Innovations in the Design of Mechanical Components of a Beamline``. The workshop was attended well with over 140 registrants. The following topics were discussed. Industry`s perspective on the status and future was provided by Huber Diffrationtechnik, Oxford Instruments, and Kohzu Seiko Ltd. on goniometers/diffractometers, advanced manufacturing technique of high heat load components, such as the APS photon shutter, and the specialties of monochromators provided to the third-generation synchrotrons, respectively. This was followed by a description of the engineering of a dual function monochromator design for water-cooled diamond or cryogenically cooled silicon monochromators by CMC CAT/APS. Another category was the nagging problem of sensitivity of the photon beam position monitors (XBPM) to bending magnet radiation (``BM contamination``) and the undulator magnet gap changes. Problem descriptions and suggested solutions were provided by both the Advanced Light Source (ALS) and the APS. Other innovative ideas were the cooling schemes (enhanced cooling of beamline components using metallic porous meshes including cryo-cooled applications); Glidcop photon shutter design using microchannels at the ALS; and window/filter design, manufacture and operational experiences at CHESS and PETRA/HASYLAB. Additional discussions were held on designing for micromotions and precision in the optical support systems and smart user filter schemes. This is a summary of the presentations at the Workshop. 5 refs., 5 figs.

  6. Characterization of regional cold-hydrothermal inflows enriched in arsenic and associated trace-elements in the southern part of the Duero Basin (Spain), by multivariate statistical analysis.

    Science.gov (United States)

    Giménez-Forcada, Elena; Vega-Alegre, Marisol; Timón-Sánchez, Susana

    2017-09-01

    Naturally occurring arsenic in groundwater exceeding the limit for potability has been reported along the southern edge of the Cenozoic Duero Basin (CDB) near its contact with the Spanish Central System (SCS). In this area, spatial variability of arsenic is high, peaking at 241μg/L. Forty-seven percent of samples collected contained arsenic above the maximum allowable concentration for drinking water (10μg/L). Correlations of As with other hydrochemical variables were investigated using multivariate statistical analysis (Hierarchical Cluster Analysis, HCA and Principal Component Analysis, PCA). It was found that As, V, Cr and pH are closely related and that there were also close correlations with temperature and Na(+). The highest concentrations of arsenic and other associated Potentially Toxic Geogenic Trace Elements (PTGTE) are linked to alkaline NaHCO3 waters (pH≈9), moderate oxic conditions and temperatures of around 18°C-19°C. The most plausible hypothesis to explain the high arsenic concentrations is the contribution of deeper regional flows with a significant hydrothermal component (cold-hydrothermal waters), flowing through faults in the basement rock. Water mixing and water-rock interactions occur both in the fissured aquifer media (igneous and metasedimentary bedrock) and in the sedimentary environment of the CDB, where agricultural pollution phenomena are also active. A combination of multivariate statistical tools and hydrochemical analysis enabled the distribution pattern of dissolved As and other PTGTE in groundwaters in the study area to be interpreted, and their most likely origin to be established. This methodology could be applied to other sedimentary areas with similar characteristics and problems. Copyright © 2017 Elsevier B.V. All rights reserved.

  7. A study on an efficient prediction of welding deformation for T-joint laser welding of sandwich panel Part II : Proposal of a method to use shell element model

    Directory of Open Access Journals (Sweden)

    Kim Jae Woong

    2014-06-01

    Full Text Available I-core sandwich panel that has been used more widely is assembled using high power CO₂laser welding. Kim et al. (2013 proposed a circular cone type heat source model for the T-joint laser welding between face plate and core. It can cover the negative defocus which is commonly adopted in T-joint laser welding to provide deeper penetration. In part I, a volumetric heat source model is proposed and it is verified thorough a comparison of melting zone on the cross section with experiment results. The proposed model can be used for heat transfer analysis and thermal elasto-plastic analysis to predict welding deformation that occurs during laser welding. In terms of computational time, since the thermal elasto-plastic analysis using 3D solid elements is quite time consuming, shell element model with multi-layers have been employed instead. However, the conventional layered approach is not appropriate for the application of heat load at T-Joint. This paper, Part II, suggests a new method to arrange different number of layers for face plate and core in order to impose heat load only to the face plate.

  8. A study on an efficient prediction of welding deformation for T-joint laser welding of sandwich panel Part II : Proposal of a method to use shell element model

    Science.gov (United States)

    Kim, Jae Woong; Jang, Beom Seon; Kang, Sung Wook

    2014-06-01

    I-core sandwich panel that has been used more widely is assembled using high power CO-laser welding. Kim et al. (2013) proposed a circular cone type heat source model for the T-joint laser welding between face plate and core. It can cover the negative defocus which is commonly adopted in T-joint laser welding to provide deeper penetration. In part I, a volumetric heat source model is proposed and it is verified thorough a comparison of melting zone on the cross section with experiment results. The proposed model can be used for heat transfer analysis and thermal elasto-plastic analysis to predict welding deformation that occurs during laser welding. In terms of computational time, since the thermal elasto-plastic analysis using 3D solid elements is quite time consuming, shell element model with multi-layers have been employed instead. However, the conventional layered approach is not appropriate for the application of heat load at T-Joint. This paper, Part II, suggests a new method to arrange different number of layers for face plate and core in order to impose heat load only to the face plate.

  9. {mu}-Synchrotron radiation excited X-ray fluorescence microprobe trace element studies on spherules of the Cretaceous/Tertiary boundary transitions of NE-Mexico and Haiti samples

    Energy Technology Data Exchange (ETDEWEB)

    Kramar, Utz [Universitaet Karlsruhe (Thailand), Institut fuer Mineralogie und Geochemie, Kaiserstrasse 12, D-76128 Karlsruhe (Germany)], E-mail: utz.kramar@img.uni-karlsruhe.de; Harting, Markus [Utrecht University, Department of Earthsciences, Budapestlaan 4, 3508 TA Utrecht (Netherlands); Rickers, Karen [Hamburger Synchrotronstrahlungslabor HASYLAB at Deutsches Elektronen-Synchrotron DESY, Notkestrasse 85, 22607 Hamburg (Germany); GeoForschungsZentrum Potsdam, Division 4.1, Telegrafenberg, 14473 Potsdam (Germany); Stueben, Doris [Universitaet Karlsruhe (Thailand), Institut fuer Mineralogie und Geochemie, Kaiserstrasse 12, D-76128 Karlsruhe (Germany)

    2007-08-15

    Synchrotron radiation, collimated to a {mu}m scale was used for the determination of trace elements in micro-tektites and spherule material for the first time. The experimental set-up of the SXRF microprobe at beamline L at HASYLAB at DESY offers a suitable method for performing non-destructive in situ multi-element analysis focusing on spatial trace element distributions and mineral phases of the melted ejecta material from the Cretaceous/Tertiary boundary. The spatial distribution of trace elements was determined in melt inclusions as well as in phase transitions in selected parts of chlorite-smectite spherules and tektite glass material by using a beam with a diameter of 15 {mu}m collimated with a glass capillary for line- and area scans as well as for single point measurements for elements with Z between 19 and 92. The analyzed spherules show alteration features but also zonation and carbonate inclusions, originating from the Chicxulub impact event. These initial results demonstrate the potential of {mu}-SXRF analysis for the discrimination of alteration and primary signals of the spherules and re-construction of their genetic evolution. It could be shown that the spherules represent a complex mixture of different materials from the subsurface at the Chicxulub impact site.

  10. Finite element procedures

    CERN Document Server

    Bathe, Klaus-Jürgen

    2015-01-01

    Finite element procedures are now an important and frequently indispensable part of engineering analyses and scientific investigations. This book focuses on finite element procedures that are very useful and are widely employed. Formulations for the linear and nonlinear analyses of solids and structures, fluids, and multiphysics problems are presented, appropriate finite elements are discussed, and solution techniques for the governing finite element equations are given. The book presents general, reliable, and effective procedures that are fundamental and can be expected to be in use for a long time. The given procedures form also the foundations of recent developments in the field.

  11. Thermal stability of solid lubricant element MoS{sub 2} in injection molded parts of 17-4 PH stainless steel

    Energy Technology Data Exchange (ETDEWEB)

    Furlan, K.P.; Binder, C.; Klein, A.N., E-mail: kalinefurlan@yahoo.com.br, E-mail: ctbinder@emc.ufsc.br, E-mail: klein@emc.ufsc.br [Universidade Federal de Santa Catarina (LabMat/UFSC), Florianopolis, SC (Brazil). Depto. de Engenharia Mecanica. Laboratorio de Materiais

    2009-07-01

    Sintered copper-based parts with self-lubricating properties are, nowadays, extensively employed, e.g. in automotive bushes. However, in such components, the liquid lubricant is added after the sintering stage. Recent developments have attempted to substitute the liquid lubricant for a solid one (which is incorporated during the mixing step), aiming operations under extreme conditions where liquids may be ineffective. For powder injection molding (PIM) market, stainless steels are the widest-ranging application group. In this study composites of 17-4 PH stainless steel with 10% vol. of molybdenum disulfide solid lubricant were prepared by PIM. The sintering of the compacts was carried out at various temperatures ranging from 650 to 1300 deg C. The composite structure was analyzed by SEM/EDS, and the phases formed were identified by XRD. Results indicated decomposition of MoS{sub 2} during the sintering cycle, for temperatures above 650 deg C, with formation of others sulfides and supplementary diffusion of molybdenum into the matrix. (author)

  12. Behaviour of high stretch bolts in tension working as part of elements of steel structures, and their tendency to delayed fracturing

    Directory of Open Access Journals (Sweden)

    Moyseychik Evgeniy Alekseevich

    2014-12-01

    Full Text Available In the article, the author has proven that manufacturing and installation errors, as well as contact deformations of high strength bolts, if analyzed as part of tensile connections of steel structures, work in eccentric tension. In pursuance of the effective state standards, the analysis of these bolts is based on the axial tension. The author has analyzed the failure of a steel structure, caused by the fracture of eccentrically loaded bolts made of steel grade XC 42 (France, or C40 (Germany, that later followed the delayed fracturing pattern. The author provides the findings of the lab tests, whereby the above bolts were tested in the presence of an angle washer. The author has also analyzed the findings of low-temperature tests of bolts in tension. The author demonstrates that the strength of high strength bolts is driven by the material, the structure shape, and the thermal treatment pattern. Eccentric tension tests of bolts have proven that cracks emerge in the areas of maximal concentration of stresses (holes in shafts, etc. that coincide with the areas where fibers are in tension; cracks tend to follow the delayed fracturing pattern, and their development is accompanied by the deformation-induced metal heating in the fracture area. Therefore, the analysis of high strength bolts shall concentrate on the eccentric tension with account for contact-induced loads, while the tendency to delayed fracturing may be adjusted through the employment of both metallurgical and process techniques.

  13. New beamline optics of the x-ray undulator BW1 at DORIS

    Energy Technology Data Exchange (ETDEWEB)

    Hahn, U.; Frahm, R.; Guertler, P.; Schulte-Schrepping, H. [Deutsches Elektronen-Synchrotron, Hamburg (Germany). Hamburger Synchrotronstrahlungslabor

    1996-12-31

    The X-ray undulator BW1 at the storage ring DORIS is a high brightness source for the spectral range from 2 to 20 keV. The undulator beam is used by three experiments with different distances to the source. The new optical elements allow the adaptation of the focal lengths to the needs of the experimental set-ups. The optical concept consists of a premirror with different optical surfaces, a double crystal monochromator and a focusing second mirror. Sagittal focusing is achieved either by using the cylindrical part of the premirror or by a bend crystal for a monochromatic beam, meridional focusing is done with a pneumatic driven mirror bender for the second mirror.

  14. Toxic Elements

    DEFF Research Database (Denmark)

    Hajeb, Parvaneh; Shakibazadeh, Shahram; Sloth, Jens Jørgen

    2016-01-01

    Food is considered the main source of toxic element (arsenic, cadmium, lead, and mercury) exposure to humans, and they can cause major public health effects. In this chapter, we discuss the most important sources for toxic element in food and the foodstuffs which are significant contributors...... to human exposure. The occurrence of each element in food classes from different regions is presented. Some of the current toxicological risk assessments on toxic elements, the human health effect of each toxic element, and their contents in the food legislations are presented. An overview of analytical...... techniques and challenges for determination of toxic elements in food is also given....

  15. From the meso to the nanoscopic scale through synchrotron imaging approaches: advances and near future at the NSLS-II SRX beamline

    Science.gov (United States)

    De Andrade, V.; Thieme, J.; Ganne, J.; Beck, P.; Fayard, B.; Salomé, M.

    2012-12-01

    Earth and planetary samples are commonly complex polycrystalline systems with various scale-level chemical and structural heterogeneities. They can present various crystallinity states, fine mechanical mixings of phases within a micrometer cube, micro-domains differentially affected by diverse geodynamic events. During the last decade, many questions in Earth Sciences were addressed with synchrotron techniques. Indeed, these big instruments now worldwide spreads are well equipped for unraveling the wealth of information stored in geomaterials. A large spectrum of cutting edge techniques (enabling phase identification, 3D chemical imaging, elemental speciation determination…) is available with mm to ~10 nm large X-ray beams, with sensitivity in some cases below the ppm. In this presentation, we will first underscore the predominant contribution of a newly developed synchrotron imaging technique[1] to metamorphic rocks studies. The technique allows to perform hard X-rays full-field imaging spectroscopy with high spectral and spatial resolution (Thieme, J, et al., "The sub-micron resolution X-ray spectroscopy beamline at NSLS-II", Nuclear Instruments and Methods in Physics Research Section A, 649(1), 46-48 (2011).

  16. An element

    Energy Technology Data Exchange (ETDEWEB)

    Nakamura, K.; Iidzima, K.

    1983-03-30

    An anode of a light metal is used in the element, along with an electrolyte which consists of an ether solvent and an ionogenic additive in the form of a salt of dithiocarbamic acid. The element has good discharge characteristics.

  17. The BioCAT undulator beamline 18ID: a facility for biological non-crystalline diffraction and X-ray absorption spectroscopy at the Advanced Photon Source.

    Science.gov (United States)

    Fischetti, R; Stepanov, S; Rosenbaum, G; Barrea, R; Black, E; Gore, D; Heurich, R; Kondrashkina, E; Kropf, A J; Wang, S; Zhang, Ke; Irving, T C; Bunker, G B

    2004-09-01

    The 18ID undulator beamline of the Biophysics Collaborative Access Team at the Advanced Photon Source, Argonne, IL, USA, is a high-performance instrument designed for, and dedicated to, the study of partially ordered and disordered biological materials using the techniques of small-angle X-ray scattering, fiber diffraction, and X-ray absorption spectroscopy. The beamline and associated instrumentation are described in detail and examples of the representative experimental results are presented.

  18. Design and performance of high-pressure PLANET beamline at pulsed neutron source at J-PARC

    Energy Technology Data Exchange (ETDEWEB)

    Hattori, T.; Sano-Furukawa, A. [J-PARC Center, Japan Atomic Energy Agency, Tokai, Naka, Ibaraki 319-1195 (Japan); Quantum Beam Science Center, Japan Atomic Energy Agency, Tokai, Naka, Ibaraki 319-1195 (Japan); Arima, H. [Institute for Materials Research, Tohoku University, Sendai 980-8577 (Japan); Komatsu, K. [Geochemical Research Center, Graduate School of Science, The University of Tokyo, Tokyo 113-0033 (Japan); Yamada, A. [University of Shiga Prefecture, Shiga 522-8533 (Japan); Inamura, Y.; Nakatani, T. [J-PARC Center, Japan Atomic Energy Agency, Tokai, Naka, Ibaraki 319-1195 (Japan); Seto, Y. [Graduate School of Science, Kobe University, Kobe 657-8501 (Japan); Nagai, T. [Faculty of Science, Hokkaido University, Sapporo 060-0810 (Japan); Utsumi, W. [Quantum Beam Science Center, Japan Atomic Energy Agency, Tokai, Naka, Ibaraki 319-1195 (Japan); Iitaka, T. [Computational Astrophysics Laboratory, RIKEN, Saitama 351-0198 (Japan); Kagi, H. [Geochemical Research Center, Graduate School of Science, The University of Tokyo, Tokyo 113-0033 (Japan); Katayama, Y. [Quantum Beam Science Center, Japan Atomic Energy Agency, Tokai, Naka, Ibaraki 319-1195 (Japan); Inoue, T. [Geodynamic Research Center, Ehime University, Matsuyama 790-8577 (Japan); Otomo, T. [J-PARC Center, Japan Atomic Energy Agency, Tokai, Naka, Ibaraki 319-1195 (Japan); Institute of Materials Structure Science, High Energy Accelerator Research Organization (KEK), Tsukuba, Ibaraki 205-001 (Japan); Suzuya, K. [J-PARC Center, Japan Atomic Energy Agency, Tokai, Naka, Ibaraki 319-1195 (Japan); Kamiyama, T. [J-PARC Center, Japan Atomic Energy Agency, Tokai, Naka, Ibaraki 319-1195 (Japan); Institute of Materials Structure Science, High Energy Accelerator Research Organization (KEK), Tsukuba, Ibaraki 205-001 (Japan); Arai, M. [J-PARC Center, Japan Atomic Energy Agency, Tokai, Naka, Ibaraki 319-1195 (Japan); Yagi, T. [Geochemical Research Center, Graduate School of Science, The University of Tokyo, Tokyo 113-0033 (Japan)

    2015-04-21

    PLANET is a time-of-flight (ToF) neutron beamline dedicated to high-pressure and high-temperature experiments. The large six-axis multi-anvil high-pressure press designed for ToF neutron diffraction experiments enables routine data collection at high pressures and high temperatures up to 10 GPa and 2000 K, respectively. To obtain clean data, the beamline is equipped with the incident slits and receiving collimators to eliminate parasitic scattering from the high-pressure cell assembly. The high performance of the diffractometer for the resolution (Δd/d~0.6%) and the accessible d-spacing range (0.2–8.4 Å) together with low-parasitic scattering characteristics enables precise structure determination of crystals and liquids under high pressure and temperature conditions.

  19. Grazing incidence X-ray absorption spectroscopy under non-ambient conditions: Investigations of liquid surfaces at DELTA beamline 8

    Science.gov (United States)

    Lützenkirchen-Hecht, D.; Wagner, R.; Bieder, S.; Frahm, R.

    2013-03-01

    A setup for the investigation of liquid surfaces using grazing incidence X-ray absorption spectroscopy has been installed at the hard X-ray beamline BL 8 at the 1.5 GeV electron storage ring DELTA. While the 6-axis diffractometer endstation of the beamline accommodates a Langmuir trough, the double mirror device which is originally used for the harmonic rejection of low energy beams was used to deflect the beam downwards, defining thereby the incidence angle for the reflection and fluorescence mode EXAFS experiments in a Θ-Θ-geometry. Results obtained during the biomineralization of iron oxides on a Langmuir film of stearic acid show the feasibility of grazing incidence EXAFS measurements that may provide valuable information about the molecular structure of the formed iron oxide phases.

  20. Development of sample exchange robot PAM-HC for beamline BL-1A at the photon factory

    Energy Technology Data Exchange (ETDEWEB)

    Hiraki, Masahiko, E-mail: masahiko.hiraki@kek.jp [Mechanical Engineering Center, Applied Research Laboratory, KEK (High Energy Accelerator Research Organization), 1-1 Oho, Tsukuba, Ibaraki 305-0801 Japan (Japan); Department of Accelerator Science, SOKENDAI (the Graduate University for Advanced Studies), 1-1 Oho, Tsukuba, Ibaraki 305-0801 Japan (Japan); Matsugaki, Naohiro; Yamada, Yusuke; Senda, Toshiya [Structural Biology research Center, Institute of Materials Structure Science, KEK (Japan); Department of Materials Structure Science, SOKENDAI (Japan)

    2016-07-27

    A macromolecular crystallography beamline, BL-1A, has been built at the Photon Factory (PF) for low energy experiments and has been operational since 2010. We have installed a sample exchange robot, PAM (PF Automated Mounting system), similar to other macromolecular crystallography beamlines. However, following the installation of a helium chamber to reduce the absorption of the diffraction signal by air, we developed a new sample exchange robot to replace PAM. The new robot, named PAM-HC (Helium Chamber), is designed with the goal of minimizing leakage of helium gas from the chamber. Here, the PAM-HC hardware and the flow of its movement are described. Furthermore, measurements of temperature changes during sample exchange are presented in this paper.

  1. Measuring circular dichroism in a capillary cell using the b23 synchrotron radiation CD beamline at diamond light source.

    Science.gov (United States)

    Jávorfi, Tamás; Hussain, Rohanah; Myatt, Daniel; Siligardi, Giuliano

    2010-01-01

    Synchrotron radiation circular dichroism (SRCD) is a well-established method in structural biology. The first UV-VIS beamline dedicated to circular dichroism at Diamond Light Source, a third generation synchrotron facility in South Oxfordshire, has recently become operational and it is now available for the user community. Herein we present an important application of SRCD: the CD measurement of protein solutions in fused silica rectangular capillary cells. This was achieved without the use of any lens between the photoelastic modulator and the photomultiplier tube detectors by exploiting the high photon flux of the collimated beam that can be as little as half a millimeter squared. Measures to minimize or eliminate vacuum-UV protein denaturation effects are discussed. The CD spectra measured in capillaries is a proof of principle to address CD measurements in microdevice systems using the new B23 SRCD beamline.

  2. Design, Build & Test of a Double Crystal Monochromator for Beamlines I09 & I23 at the Diamond Light Source

    Science.gov (United States)

    Kelly, J.; Lee, T.; Alcock, S.; Patel, H.

    2013-03-01

    A high stability Double Crystal Monochromator has been developed at The Diamond Light Source for beamlines I09 and I23. The design specification was a cryogenic, fixed exit, energy scanning monochromator, operating over an energy range of 2.1 - 25 keV using a Si(111) crystal set. The novel design concepts are the direct drive, air bearing Bragg axis, low strain crystal mounts and the cooling scheme. The instrument exhibited superb stability and repeatability on the B16 Test Beamline. A 20 keV Si(555), 1.4 μrad rocking curve was demonstrated. The DCM showed good stability without any evidence of vibration or Bragg angle nonlinearity.

  3. Recent progress in vacuum-ultraviolet polarization modulation spectroscopy using polarizing undulator at the TERAS BL5 beamline.

    Science.gov (United States)

    Yagi-Watanabe, Kazutoshi; Tanaka, Masahito; Kaneko, Fusae; Nakagawa, Kazumichi

    2007-12-01

    Polarization modulation spectroscopy using an Onuki-type undulator is a useful technique for circular dichroism study in the vacuum-ultraviolet region. We have been developing the vacuum-ultraviolet circular dichroism (vuv-CD) spectroscopy in TERAS BL5 beamline at AIST. This paper describes recent improvements in our instrumentation and methods of analysis to achieve precise and absolute measurements. The CD signal is usually accompanied by experimental artifacts, and elimination of all possible artifacts is the key issue for making reliable measurements. After improving beamline optical system, light flux monitor, and undulator operation method, the base line shift of the CD spectrum is suppressed less than 3x10(-4). Sample manipulation and data processing procedures are also described and absolute CD spectrum can be obtained even for linear anisotropic sample. These progresses lead to more quantitative comparison of experimental with calculation on vuv-CD spectrum.

  4. Present status of vacuum ultraviolet natural circular dichroism measurement system using polarizing undulator at TERAS BL5 beamline

    Energy Technology Data Exchange (ETDEWEB)

    Tanaka, Masahito, E-mail: masahito-tanaka@aist.go.j [Research Institute of Instrumentation Frontier, National Institute of Advanced Industrial Science and Technology (AIST), Central 2, Umezono 1-1-1, Tsukuba, Ibaraki 305-8568 (Japan); Yagi-Watanabe, Kazutoshi; Kaneko, Fusae [Research Institute of Instrumentation Frontier, National Institute of Advanced Industrial Science and Technology (AIST), Central 2, Umezono 1-1-1, Tsukuba, Ibaraki 305-8568 (Japan); Nakagawa, Kazumichi [Graduate School of Human Development and Environment, Kobe University, Tsurukabuto 3-11, Nada-ku, Kobe 657-8501 (Japan)

    2010-08-15

    The study of natural circular dichroism (CD) in the vacuum and extreme ultraviolet (VUV and EUV) regions has been providing us with chirality and structural information on biomolecules. We have developed the beamline BL5 at TERAS, Tsukuba, which is equipped with a compact Onuki-type polarizing undulator. This beamline is dedicated to measuring the CD spectra in the VUV and EUV regions for the photon energy region of 5-40 eV. The use of a polarization modulation technique with a polarizing undulator is essential for detecting a weak CD signal. Using this CD system, the natural CD spectrum has been measured in the EUV region up to 40 eV for the first time. In addition, the differences and the similarities between the CD spectra of four amino acid films (alanine, valine, leucine, and phenylalanine) in the VUV region up to 9.5 eV are determined.

  5. New Developments at the ALS High-Pressure Beamline 12.2.2

    Science.gov (United States)

    Kunz, M.; MacDowell, A. A.; Yan, J.; Beavers, C. C. G.; Doran, A.; Williams, Q. C.

    2015-12-01

    ALS-beamline 12.2.2 celebrated its 10-year anniversary as a beamline collaboratively operated by the ALS and COMPRES. The anniversary coincided with a major rebuild and expansion of its capabilities for in-situ high-pressure and high-temperature X-ray diffraction. A rebuild of the 12.2.2 laser heating table was completed and commissioned in the past year. The new design relies on a vertically positioned small (~1m x 1m) breadboard that is placed perpendicularly to the incident X-ray beam next to the sample stage. Upstream and downstream viewing-, IR-laser and pyrometry-optics are mounted on opposite surfaces of the breadboard. On-line ruby fluorescence optics including a blue diode laser are also mounted on the upstream surface. The much reduced dimensions of the design lead to smaller mechanical lever arms and thus to a significant suppression of vibrations. This was confirmed in the commissioning phase with high-quality optical images (~ 2 μm resolution) as well as a very stable hotspot in DAC samples. A further optimized pyrometry code was cross-calibrated against thermal expansions of Pt and Ta, and was found to agree with those values within experimental uncertainties. Pyrometry relies on imaging the full hot-spot onto a spectrometer and combining the thus obtained average temperature with an intensity map collected at 700 nm to produce a temperature contour map of the entire sample chamber. Besides axial laser heating, double-sided radial laser heating is also being developed and commissioned. The X-ray source of 12.2.2 makes it an ideal station to focus on high-pressure single crystal diffraction. The present set-up operates parasitically with a single rotation axis on the in-situ laser heating powder diffraction sample stage in concert with a fast (15 fps) amorphous silicon/diode array detector. Although this set-up poses limitations with respect to accessible reciprocal space, high pressure single crystal structure solution and refinements of organic

  6. Multi-objective Optimizations of a Novel Cryo-cooled DC Gun Based Ultra Fast Electron Diffraction Beamline

    OpenAIRE

    Gulliford, C.; Bartnik, A.; Bazarov, I.

    2015-01-01

    We present the results of multi-objective genetic algorithm optimizations of a potential single shot ultra fast electron diffraction beamline utilizing a 225 kV dc gun with a novel cryocooled photocathode system and buncher cavity. Optimizations of the transverse projected emittance as a function of bunch charge are presented and discussed in terms of the scaling laws derived in the charge saturation limit. Additionally, optimization of the transverse coherence length as a function of final r...

  7. A new method to suppress high-order harmonics for synchrotron radiation soft x-ray beamline

    CERN Document Server

    Guo, Zhi-Ying; Xing, Hai-Ying; Tang, Kun; Han, Yong; Chen, Dong-Liang; Zhao, Yi-Dong

    2014-01-01

    A feasible and convenient method has been proposed to suppress higher-harmonics for varied-line-spacing (VLS) plane grating monochromator in soft x-ray region. Related calculations and experiments demonstrate that decreasing the included angle slightly by changing the parameter of exit arm length can significantly improve light purity. This method is suitable and has been used for experiments of detector calibration in beamline 4B7B at Beijing Synchrotron Radiation Facility (BSRF).

  8. The CG-1D Neutron Imaging Beamline at the Oak Ridge National Laboratory High Flux Isotope Reactor

    Science.gov (United States)

    Santodonato, Lou; Bilheux, Hassina; Bailey, Barton; Bilheux, Jean; Nguyen, Phong; Tremsin, Anton; Selby, Doug; Walker, Lakeisha

    The Oak Ridge National Laboratory Neutron Sciences Directorate has installed a neutron imaging beamline at the High Flux Isotope Reactor (HFIR) cold guide hall. CG-1D is one of the three instruments that make up the CG1 instrument suite. The beamline optics and detector have recently been upgraded to meet the needs of the neutron imaging community (better "smoothing" of guide system artifacts, higher flux or spatial resolution). These upgrades comprise a new diffuser/aperture system, two new detectors, a He-filled flight tube and silicon (Si) windows. Shielding inside the flight tube, beam scrapers and a beam stop ensure that biological dose is less than 50 μSv/hr outside of the radiation boundary. A set of diffusers and apertures (pinhole geometry) has been installed at the exit of the guide system to allow motorized L/D variation. Samples sit on a translation/rotation stage for alignment and tomography purposes. Detectors for the CG-1D beamline are (1) an ANDOR DW936 charge coupled device (CCD) camera with a field of view of approximately 7 cm x 7 cm and ∼ 80 microns spatial resolution and 1 frame per second time resolution, (2) a new Micro-Channel Plate (MCP) detector with a 2.8 cm x 2.8 cm field of view and 55 microns spatial resolution, and 5 μs timing capability. 6LiF/ZnS scintillators of thickness varying from 50 to 200 microns are being used at this facility. An overview of the beamline upgrade and preliminary data is presented here.

  9. Opportunities of research in multiferroic materials using Angle Dispersive X-ray Diffraction (ADXRD) beamline on Indus-2 synchrotron source

    Science.gov (United States)

    Sinha, A. K.; Singh, M. N.; Upadhyay, A.; Sagdeo, A.

    2016-10-01

    Synchrotron beamlines have advantages of higher flux and wide tunability of photon beam compared to laboratory based equipment for performing x-ray diffraction and x- ray absorption spectroscopy (XAS). In this paper we report capabilities of angle dispersive x- ray diffraction beamline (BL-12) on Indus-2 synchrotron source for structural and spectroscopic characterisation of multiferroic materials. Brief description of the beamline along with the photon beam specifications at the experimental station is given. Results on low temperature XRD measurements on mixed spinel system (Fe1.5Co1.5O4) between 30K and 300K and subsequent Reitveld refinement reveal that there are no phase changes but the lattice parameter show anomalous changes between 100 and 150K. It has been explained how XANES spectra on a type II multiferroic, Co3TeO6, and Fe1.5Co1.5O4 can be used for the determination of charge and spin states of transition metal ions.

  10. Medical research and multidisciplinary applications with laser-accelerated beams: the ELIMED netwotk at ELI-Beamlines

    Science.gov (United States)

    Tramontana, A.; Anzalone, A.; Candiano, G.; Carpinelli, M.; Cirrone, G. A. P.; Cuttone, G.; Korn, G.; Licciardello, T.; Maggiore, M.; Manti, L.; Margarone, D.; Musumarra, A.; Perozziello, F.; Pisciotta, P.; Raffaele, L.; Romano, F.; Romano, F. P.; Stancampiano, C.; Schillaci, F.; Scuderi, V.; Torrisi, L.; Tudisco, S.

    2014-04-01

    Laser accelerated proton beams represent nowadays an attractive alternative to the conventional ones and they have been proposed in different research fields. In particular, the interest has been focused in the possibility of replacing conventional accelerating machines with laser-based accelerators in order to develop a new concept of hadrontherapy facilities, which could result more compact and less expensive. With this background the ELIMED (ELIMED: ELI-Beamlines MEDical applications) research project has been launched by LNS-INFN researchers (Laboratori Nazionali del Sud-Istituto Nazionale di Fisica Nucleare, Catania, IT) and ASCR-FZU researchers (Academy of Sciences of the Czech Republic-Fyzikální ústar, Prague, Cz), within the pan-European ELI-Beamlines facility framework. Its main purposes are the demonstration of future applications in hadrontherapy of optically accelerated protons and the realization of a laser-accelerated ion transport beamline for multidisciplinary applications. Several challenges, starting from laser-target interaction and beam transport development, up to dosimetric and radiobiological issues, need to be overcome in order to reach the final goals. The design and the realization of a preliminary beam handling and dosimetric system and of an advanced spectrometer for high energy (multi-MeV) laser-accelerated ion beams will be shortly presented in this work.

  11. A BEAMLINE FOR HIGH PRESSURE STUDIES AT THE ADVANCED LIGHT SOURCE WITH A SUPERCONDUCTING BENDING MAGNET AS THE SOURCE

    Energy Technology Data Exchange (ETDEWEB)

    Kunz, M; MacDowell, A A; Caldwell, W A; Cambie, D; Celestre, R S; Domning, E E; Duarte, R M; Gleason, A; Glossinger, J; Kelez, N; Plate, D W; Yu, T; Zaug, J M; Padmore, H A; Jeanloz, R; Alivisatos, A P; Clark, S M

    2005-04-19

    A new facility for high-pressure diffraction and spectroscopy using diamond anvil high-pressure cells has been built at the Advanced Light Source on Beamline 12.2.2. This beamline benefits from the hard X-radiation generated by a 6 Tesla superconducting bending magnet (superbend). Useful x-ray flux is available between 5 keV and 35 keV. The radiation is transferred from the superbend to the experimental enclosure by the brightness preserving optics of the beamline. These optics are comprised of: a plane parabola collimating mirror (M1), followed by a Kohzu monochromator vessel with a Si(111) crystals (E/{Delta}E {approx} 7000) and a W/B{sub 4}C multilayer (E/{Delta}E {approx} 100), and then a toroidal focusing mirror (M2) with variable focusing distance. The experimental enclosure contains an automated beam positioning system, a set of slits, ion chambers, the sample positioning goniometry and area detectors (CCD or image-plate detector). Future developments aim at the installation of a second end station dedicated for in situ laser-heating on one hand and a dedicated high-pressure single-crystal station, applying both monochromatic as well as polychromatic techniques.

  12. A Beamline for High-Pressure Studies at the Advanced Light Sourcewith a Superconducting Bending Magnet as the Source

    Energy Technology Data Exchange (ETDEWEB)

    Kunz, Martin; MacDowell, Alastair A.; Caldwell, Wendel A.; Cambie, Daniella; Celestre, Richard S.; Domning, Edward E.; Duarte,Robert M.; Gleason, Arianna E.; Glossinger, James M.; Kelez, Nicholas; Plate, David W.; Yu, Tony; Zaug, Joeseph M.; Padmore, Howard A.; Jeanloz,Raymond; Alivisatos, A. Paul; Clark, Simon M.

    2005-06-30

    A new facility for high-pressure diffraction and spectroscopy using diamond anvil high-pressure cells has been built at the Advanced Light Source on Beamline 12.2.2. This beamline benefits from the hard X-radiation generated by a 6 Tesla superconducting bending magnet (superbend). Useful x-ray flux is available between 5 keV and 35 keV. The radiation is transferred from the superbend to the experimental enclosure by the brightness preserving optics of the beamline. These optics are comprised of: a plane parabola collimating mirror (M1), followed by a Kohzu monochromator vessel with a Si(111) crystals (E/DE {approx}7000) and a W/B4C multilayers (E/DE {approx} 100), and then a toroidal focusing mirror (M2) with variable focusing distance. The experimental enclosure contains an automated beam positioning system, a set of slits, ion chambers, the sample positioning goniometry and area detectors (CCD or image-plate detector). Future developments aim at the installation of a second end station dedicated for in situ laser-heating on one hand and a dedicated high-pressure single-crystal station, applying both monochromatic as well as polychromatic techniques.

  13. JBluIce-EPICS: a fast and flexible open-source beamline control system for macromolecular crystallography

    Science.gov (United States)

    Stepanov, S.; Hilgart, M.; Makarov, O.; Pothineni, S. B.; Yoder, D.; Ogata, C.; Sanishvili, R.; Venugopalan, N.; Becker, M.; Clift, M.; Smith, J. L.; Fischetti, R. F.

    2013-03-01

    This paper overviews recent advances in the JBluIce-EPICS open-source control system designed at the macromolecular crystallography beamlines of the National Institute of General Medical Sciences and National Cancer Institute at the Advanced Photon Source (GM/CA@APS). We discuss some technical highlights of this system distinguishing it from the competition, such as reduction of software layers to only two, possibility to operate JBluIce in parallel with other beamline controls, plugin-enabled architecture where the plugins can be written in any programming language, and utilization of the whole power of the Java integrated development environment in the Graphical User Interface. Then, we demonstrate how these highlights help to make JBluIce fast, easily adaptable to new beamline developments, and intuitive for users. In particular, we discuss several recent additions to the system including a bridge between crystal rastering and data collection, automatic detection of raster polygons from optical crystal centering, background data processing, and a pathway to a fully automated pipeline from crystal screening to solving crystal structure.

  14. High-throughput operation of sample-exchange robots with double tongs at the Photon Factory beamlines

    Science.gov (United States)

    Hiraki, Masahiko; Watanabe, Shokei; pHonda, Nobuo; Yamada, Yusuke; Matsugaki, Naohiro; Igarashi, Noriyuki; Gaponov, Yurii; Wakatsuki, Soichi

    2008-01-01

    Sample-exchange robots that can exchange cryo-pins bearing protein crystals out of experimental hutches according to user instructions have been developed. The robots were designed based on the SAM (Stanford Synchrotron Research Laboratory automated mounting) system. In order to reduce the time required for the sample exchange, the single tongs of the SAM system were modified and a double-tongs system that can hold two cryo-pins at the same time was developed. Robots with double tongs can move to the goniometer head holding the next cryo-pin with one set of tongs, dismount the experimented cryo-pin with the other set, and then mount the next pin onto the goniometer head without leaving the diffractometer area. Two different types of tongs have been installed: single tongs at beamlines BL-5A and AR-NW12A, and a double-tongs system at beamline BL-17A of the Photon Factory. The same graphical user interface software for operation of the sample-exchange robots is used at all beamlines, however, so that users do not need to consider differences between the systems. In a trial, the robot with double tongs could exchange samples within 10 s. PMID:18421164

  15. SAMRAI: a novel variably polarized angle-resolved photoemission beamline in the VUV region at UVSOR-II.

    Science.gov (United States)

    Kimura, Shin-Ichi; Ito, Takahiro; Sakai, Masahiro; Nakamura, Eiken; Kondo, Naonori; Horigome, Toshio; Hayashi, Kenji; Hosaka, Masahito; Katoh, Masahiro; Goto, Tomohiro; Ejima, Takeo; Soda, Kazuo

    2010-05-01

    A novel variably polarized angle-resolved photoemission spectroscopy beamline in the vacuum-ultraviolet (VUV) region has been installed at the UVSOR-II 750 MeV synchrotron light source. The beamline is equipped with a 3 m long APPLE-II type undulator with horizontally/vertically linear and right/left circular polarizations, a 10 m Wadsworth type monochromator covering a photon energy range of 6-43 eV, and a 200 mm radius hemispherical photoelectron analyzer with an electron lens of a +/-18 degrees acceptance angle. Due to the low emittance of the UVSOR-II storage ring, the light source is regarded as an entrance slit, and the undulator light is directly led to a grating by two plane mirrors in the monochromator while maintaining a balance between high-energy resolution and high photon flux. The energy resolving power (hnu/Deltahnu) and photon flux of the monochromator are typically 1 x 10(4) and 10(12) photons/s, respectively, with a 100 microm exit slit. The beamline is used for angle-resolved photoemission spectroscopy with an energy resolution of a few meV covering the UV-to-VUV energy range.

  16. Overview of the conceptual design of the future VENUS beamline at the Spallation Neutron Source

    Energy Technology Data Exchange (ETDEWEB)

    Bilheux, Hassina Z [ORNL; Herwig, Kenneth W [ORNL; Keener, Wylie S [ORNL; Davis, Larry E [ORNL

    2015-01-01

    VENUS will be a world-class neutron-imaging instrument that will uniquely utilize the Spallation Neutron Source (SNS) time-of-flight (TOF) capabilities to measure and characterize objects across several length scales (mm to m). When completed, VENUS will provide academia, industry and government laboratories with the opportunity to advance scientific research in areas such as energy, materials, additive manufacturing, geosciences, transportation, engineering, plant physiology, biology, etc. It is anticipated that a good portion of the VENUS user community will have a strong engineering/industrial research focus. Installed at Beamline 10 (BL10), VENUS will be a 25-m neutron imaging facility with the capability to fully illuminate (i.e., umbra illumination) a 20 cm x 20 cm detector area. The design allows for a 28 cm x 28 cm field of view when using the penumbra to 80% of the full illumination flux. A sample position at 20 m will be implemented for magnification measurements. The optical components are comprised of a series of selected apertures, T0 and bandwidth choppers, beam scrapers, a fast shutter to limit sample activation, and flight tubes filled with Helium. Techniques such as energy selective, Bragg edge and epithermal imaging will be available at VENUS

  17. Fiber diffraction using the BioCAT undulator beamline at the Advanced Photon Source

    Science.gov (United States)

    Irving, T. C.; Fischetti, R.; Rosenbaum, G.; Bunker, G. B.; Biophysics Collaborative Access Team (BioCAT)

    2000-06-01

    The BioCAT undulator-based beamline at the Advanced Photon Source, Argonne IL, USA is designed to be a state-of-the-art instrument for biological non-crystalline diffraction and X-ray absorption spectroscopy. The optics consist of double crystal monochromators with sagitally focussing second crystals followed by a vertically focussing mirror which allow independent focussing of the beam in the vertical and horizontal directions virtually anywhere along the length of the 12 m experimental enclosure. When configured for a 2 m fiber diffraction camera, a focal spot of less than 40×200 μm (FWHM) has been observed which contained essentially all of the 1.5-2.5×10 13 ph/s delivered by the cryogenically-cooled Si(1 1 1) double crystal monochromator. This combination of highly demagnifying optics and the very low divergence of the very small source have yielded excellent quality patterns from various muscle specimens and collagen-containing tissues. Detectors available include a Fuji BAS2500 image plate scanner and a 1 k×1 k CCD detector optimized for small-angle applications. Future developments will include, in vacuum beam monitoring, longer camera lengths (6-8 m), and optimizations to improve first-order resolution in small-angle applications.

  18. Fiber diffraction using the BioCAT undulator beamline at the Advanced Photon Source

    CERN Document Server

    Irving, T C; Rosenbaum, G; Bunker, G B

    2000-01-01

    The BioCAT undulator-based beamline at the Advanced Photon Source, Argonne IL, USA is designed to be a state-of-the-art instrument for biological non-crystalline diffraction and X-ray absorption spectroscopy. The optics consist of double crystal monochromators with sagitally focussing second crystals followed by a vertically focussing mirror which allow independent focussing of the beam in the vertical and horizontal directions virtually anywhere along the length of the 12 m experimental enclosure. When configured for a 2 m fiber diffraction camera, a focal spot of less than 40x200 mu m (FWHM) has been observed which contained essentially all of the 1.5-2.5x10 sup 1 sup 3 ph/s delivered by the cryogenically-cooled Si(1 1 1) double crystal monochromator. This combination of highly demagnifying optics and the very low divergence of the very small source have yielded excellent quality patterns from various muscle specimens and collagen-containing tissues. Detectors available include a Fuji BAS2500 image plate sc...

  19. Direct detection of antiprotons with the Timepix3 in a new electrostatic selection beamline

    Energy Technology Data Exchange (ETDEWEB)

    Pacifico, N., E-mail: nicola.pacifico@cern.ch [Institute of Physics and Technology, University of Bergen, Allgaten 55, 5007 Bergen (Norway); Aghion, S. [Politecnico of Milano, Piazza Leonardo da Vinci 32, 20133 Milano (Italy); INFN Milano, via Celoria 16, 20133 Milano (Italy); Alozy, J. [Physics Department, CERN, 1211 Geneva 23 (Switzerland); Amsler, C.; Ariga, A.; Ariga, T. [Laboratory for High Energy Physics, Albert Einstein Center for Fundamental Physics, University of Bern, 3012 Bern (Switzerland); Bonomi, G. [Department of Mechanical and Industrial Engineering, University of Brescia, via Branze 38, 25123 Brescia (Italy); INFN Pavia, via Bassi 6, 27100 Pavia (Italy); Bräunig, P. [Kirchhoff-Institute for Physics, Heidelberg University, Im Neuenheimer Feld 227, 69120 Heidelberg (Germany); Bremer, J. [Physics Department, CERN, 1211 Geneva 23 (Switzerland); Brusa, R.S. [Department of Physics, University of Trento, via Sommarive 14, 38123 Povo, Trento (Italy); TIFPA/INFN Trento, via Sommarive 14, 38123 Povo, Trento (Italy); Cabaret, L. [Laboratory Aimé Cotton, University of Paris-Sud, ENS Cachan, CNRS, University Paris-Saclay, 91405 Orsay Cedex (France); Caccia, M. [INFN Milano, via Celoria 16, 20133 Milano (Italy); Department of Science, University of Insubria, Via Valleggio 11, 22100 Como (Italy); Campbell, M. [Physics Department, CERN, 1211 Geneva 23 (Switzerland); Caravita, R. [Department of Physics, University of Genova, via Dodecaneso 33, 16146 Genova (Italy); INFN Genova, via Dodecaneso 33, 16146 Genova (Italy); Castelli, F. [INFN Milano, via Celoria 16, 20133 Milano (Italy); Department of Physics, University of Milano, via Celoria 16, 20133 Milano (Italy); Cerchiari, G. [Max Planck Institute for Nuclear Physics, Saupfercheckweg 1, 69117 Heidelberg (Germany); Chlouba, K. [Czech Technical University, Prague, Brehov 7, 11519 Prague 1 (Czech Republic); and others

    2016-09-21

    We present here the first results obtained employing the Timepix3 for the detection and tagging of annihilations of low energy antiprotons. The Timepix3 is a recently developed hybrid pixel detector with advanced Time-of-Arrival and Time-over-Threshold capabilities and has the potential of allowing precise kinetic energy measurements of low energy charged particles from their time of flight. The tagging of the characteristic antiproton annihilation signature, already studied by our group, is enabled by the high spatial and energy resolution of this detector. In this study we have used a new, dedicated, energy selection beamline (GRACE). The line is symbiotic to the AEgIS experiment at the CERN Antiproton Decelerator and is dedicated to detector tests and possibly antiproton physics experiments. We show how the high resolution of the Timepix3 on the Time-of-Arrival and Time-over-Threshold information allows for a precise 3D reconstruction of the annihilation prongs. The presented results point at the potential use of the Timepix3 in antimatter-research experiments where a precise and unambiguous tagging of antiproton annihilations is required.

  20. Current status of the CXI beamline at the PAL-XFEL

    Science.gov (United States)

    Park, Jaehyun; Kim, Sangsoo; Nam, Ki-Hyun; Kim, Bongsoo; Ko, In Soo

    2016-09-01

    The Pohang Accelerator Laboratory's X-ray free electron laser (PAL-XFEL) is a research facility currently under construction. It will provide ultra-bright (1 × 1012 photons/pulse at 12.4 keV) and ultra-short (10 - 60 femtosecond) X-ray pulses. The CXI (coherent X-ray imaging) hard X-ray experimental station is designed to deliver brilliant hard X-rays (2 - 20.4 keV) and to measure diffraction signals with a forward scattering geometry. It will not only offer imaging studies of biological, chemical and physical samples with the "diffraction-before-destruction" scheme, but also be helpful in high-field hard X-ray physics and material science. The scientific programs are currently aimed at serial femtosecond crystallography (SFX) and coherent diffraction imaging (CDI) for bio specimens, nano materials, etc. In this paper, we describe the beamline layout, beam diagnostics, X-ray focusing optics, sample environments and detector system at the CXI experimental hutch.