WorldWideScience

Sample records for batch cooling crystallization

  1. Batch-to-batch model improvement for cooling crystallization

    OpenAIRE

    Forgione, Marco; Birpoutsoukis, Georgios; Bombois, Xavier; Mesbah, Ali; Daudey, Peter; Van Den Hof, Paul

    2015-01-01

    © 2015 Elsevier Ltd. Two batch-to-batch model update strategies for model-based control of batch cooling crystallization are presented. In Iterative Learning Control, a nominal process model is adjusted by a non-parametric, additive correction term which depends on the difference between the measured output and the model prediction in the previous batch. In Iterative Identification Control, the uncertain model parameters are iteratively estimated using the measured batch data. Due to the diff...

  2. Process Modeling for Batch Cooling Crystallization

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    The general mathematical model for batch cooling crystallization was established based on the popula tion balance equation considering the change of slurry volume, and simulated with crystallization thermodynamics, kinetics and mass balance employing bed voidage. In the system of vitamin C-water-ethanol, reliability of this model was verified by comparison between simulation results and experimental data. The effects of operation parameters on product quality can be systematically investigated by modeling simulation.

  3. Process Modeling for Batch Cooling Crystallization

    Institute of Scientific and Technical Information of China (English)

    陈慧萍; 王静康

    2001-01-01

    The general mathematical model for batch cooling crystallization was established based on the population balance equation considering the change of slurry volume, and simulated with crystallization thermodynamics,kinetics and mass balance employing bed voidage. In the system of vitamin C-water-ethanol, reliability of this model was verified by comparison between simulation results and experimental data. The effects of operation parameters on product quality can be systematically investigated by modeling simulation.

  4. Batch Cooling Crystallization of Potassium Sulphate from Water Solution

    Directory of Open Access Journals (Sweden)

    Kalšan, M.

    2009-12-01

    Full Text Available Batch cooling crystallization, at the rotation speed of 700 min–1, of an aqueous solution of a potassium sulphate has been investigated on a laboratory scale. The effect of hydrodynamics conditions on the crystallization process were investigated by using different type of impellers. Two types of impellers were investigated; the four-pitched blade impeller which generates axi-al flow and the six-blades Rusthon turbine which generates radial flow. The experiments were performed at four different linear cooling rates in the range from 8-20 °C h–1 for both types of impeller.The influence of the cooling rates on the metastable zone width, the crystallization kinetics and the granulometric properties of the obtained crystals were investigated. The experimental data show that higher cooling rate expands the metastable zone for all the types of impeller (Fig. 2 and influences the crystal size distribution (Fig. 7 and Fig. 8.At low cooling rates, supersaturation was kept at a constant value for a longer period. It resulted in improved conditions for mass transfer and the crystals grew. Bigger crystals were obtained at lower cooling rates (Fig. 7.It is stated that radial flow (Rusthon turbine is particularly inappropriate for the nucleation process, and for crystallization. Nucleation started at a lower temperature and higher supersaturation (Fig. 3. These conditions resulted in a high nucleation’s rate and large number of nucleation centres.Also, the obtained crystals settled on the wall of the reactor, baffles and stirrer. A great part of the obtained crystals was agglomerated. The nucleation order, n and coefficient of nucleation, kn were determined for different cooling rates (Fig. 5a. The nucleation order is higher at radial flow (nucleation started at higher supersaturation. The relation between the rate of concentration drop in a solution and supersaturation has beenapproximated with a power low equation (Fig. 5b. For the used impellers

  5. Integration of Generic Multi-dimensional Model and Operational Policies for Batch Cooling Crystallization

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli; Singh, Ravendra; Sin, Gürkan;

    2011-01-01

    analysis of various crystallization operations and conditions. Furthermore, a systematic procedure for generating operational policies through available analytical crystal size distribution (CSD) estimators has been developed and verified for achieving targeted CSD consistently. The application of the...... model-based framework is highlighted for batch cooling crystallization of potassium dihydrogen phosphate (KDP) in two-dimensions, while the use of the analytical estimator is demonstrated for a potassium dichromate case study to achieve a target CSD....

  6. In-line image analysis on the effects of additives in batch cooling crystallization

    Science.gov (United States)

    Qu, Haiyan; Louhi-Kultanen, Marjatta; Kallas, Juha

    2006-03-01

    The effects of two potassium salt additives, ethylene diamine tetra acetic acid dipotassium salt (EDTA) and potassium pyrophosphate (KPY), on the batch cooling crystallization of potassium dihydrogen phosphate (KDP) were investigated. The crystal growth rates of certain crystal faces were determined from in-line images taken with a MTS particle image analysis (PIA) video microscope. An in-line image processing method was developed to characterize the size and shape of the crystals. The nucleation kinetics was studied by measurement of the metastable zone width and induction time. A significant promotion effect on both nucleation and growth of KDP was observed when EDTA was used as an additive. KPY, however, exhibited strong inhibiting impacts. The mechanism underlying the EDTA promotion effect on crystal growth was further studied with the 2-dimension nucleation model. It is shown that the presence of EDTA increased the density of adsorbed molecules of the crystallizing solute on the surface of the crystal.

  7. Systematic Procedure for Generating Operational Policies to Achieve Target Crystal Size Distribution (CSD) in Batch Cooling Crystallization

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli; Singh, Ravendra; Sin, Gürkan;

    Batch cooling crystallization is one of the important unit operations involving separation of solid-liquid phases. Usually the most common crystal product qualities are directly related to the crystal size distribution (CSD). However the main difficulty in batch crystallization is to obtain a...... uniform and reproducible CSD. Therefore supersaturation control can be applied to drive the process within the metastable zone and thereby enhance the control of the CSD. Although this approach has been shown to produce high quality crystals, the set point operating profiles for the supersaturation...... controller are usually chosen arbitrarily or by trial-and-error. Therefore there is a need for a systematic procedure to generate operational policy that guarantees the target CSD can be achieved. Furthermore, to predict the desired crystal morphology by means of model-based approaches, appropriate models...

  8. The induction time, interfacial energy and growth mechanism of maltitol in batch cooling crystallization

    Energy Technology Data Exchange (ETDEWEB)

    Hou, J.; Wu, S.; Li, R. [State Research Center for Industrialization of Crystallization Technology, School of Chemical, Engineering and Technology, Tianjin University (China); Dong, W.; Gong, J. [State Research Center for Industrialization of Crystallization Technology, School of Chemical, Engineering and Technology, Tianjin University (China); Tianjin Key Laboratory Modern Drug Delivery and High-Efficiency, Tianjin University (China)

    2012-08-15

    Maltitol is crystallized with seeds by cooling mode in industry, often with large amount of fine crystals and wide crystal size distribution. To eliminate the fine nucleation, it's necessary to understand the nucleation kinetics. In this work, the solubility of maltitol in water was measured by the gravimetric method, the nucleation kinetics of maltitol in batch cooling crystallization was investigated using focus beam reflectance measurement (FBRM), and a novel method was proposed to determine the induction time from the trend of the crystal median chord given by FBRM. Based on the relationship between the induction time and the supersaturation, the nucleation mechanism was obtained, including homogenous nucleation at high supersaturation and heterogenous nucleation at low supersaturation. Additionally, combining the classical nucleation theory (CNT) and Arrhenius' principle, the crystal-solution interfacial energy and the energy barrier of homogenous nucleation were calculated. From the scanning electron microscope (SEM) images, the growth mechanism of maltitol was identified as surface nucleation growth and the surface entropy factor calculated from the kinetic analyses of t{sub ind} data corroborated this growth mechanism. (Copyright copyright 2012 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

  9. Integration of Generic Multi-dimensional Model and Operational Policies for Batch Cooling Crystallization

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli; Singh, Ravendra; Sin, Gürkan;

    obtain the required product qualities in terms of CSD and shape. Usually the main difficulty in batch cooling crystallization is to accomplish a uniform and reproducible CSD. Usually supersaturation control has been applied to drive the process within the metastable zone to enhance the control of the CSD...... operational policy, an analytical CSD estimator has been introduced and integrated with the generic multi-dimensional model in the framework. The estimator is based on the assumptions of constant supersaturation and an operation that is dominated by size dependent growth. The generated operational policy...... provides the supersaturation set point and by maintaining the operation at this point, a target CSD is achieved. Compared to earlier works, additional information regarding the total crystal mass is also targeted here. The application of the multi-dimensional model-based framework is highlighted using a...

  10. Systematic procedure for generating operational policies to achieve target crystal size distribution (CSD) in batch cooling crystallization

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli; Singh, Ravendra; Sin, Gürkan;

    2011-01-01

    A systematic procedure to achieve a target crystal size distribution (CSD) under generated operational policies in batch cooling crystallization is presented. An analytical CSD estimator has been employed in the systematic procedure to generate the necessary operational policies to achieve the...... target CSD. Furthermore, this systematic procedure has been integrated with a generic multi-dimensional model-based framework. The generic nature of the model-based framework allows the study of a wide range of chemical systems under different operational scenarios, enabling thereby, the analysis of...... various crystallization operations and conditions. Therefore this generic multidimensional model-based framework can be used to generate “specific” models for crystallization processes and further verify the operational policies generated by the analytical CSD estimator for achieving the targeted CSD...

  11. Batch-to-batch learning for model-based control of process systems with application to cooling crystallization

    NARCIS (Netherlands)

    Forgione, M.

    2014-01-01

    From an engineering perspective, the term process refers to a conversion of raw materials into intermediate or final products using chemical, physical, or biological operations. Industrial processes can be performed either in continuous or in batch mode. There exist for instance continuous and batch

  12. Improving batch cooling seeded crystallization of an organic weed-killer using on-line ATR FTIR measurement of supersaturation

    Science.gov (United States)

    Lewiner, F.; Févotte, G.; Klein, J. P.; Puel, F.

    2001-06-01

    In previous papers, a method for the calibration of ATR FTIR measurement of dissolved solid concentration during cooling crystallizations was presented, and efficient basic procedures for the determination of solubility and metastability curves were described. The present paper reports new experimental results. The crystallization of an organic product is studied thanks to on-line FTIR measurements of supersaturation and off-line crystal size distribution (CSD) determinations. The obtained information is shown to potentially allow a deeper examination of major industrial issues such as the reduction of batch-to-batch variations and the improvement of the CSD of the final particles. A particular attention is focused on the determination of appropriate seeding parameters such as the cooling rate of seeded slurries, the temperature of introduction and the amount of seed. The results obtained demonstrate that, although any modelling approach is outside the scope of this paper, the analysis of the measured supersaturation profiles allows some interpretation of mechanisms governing the final CSD, and consequently, the proposal of improved operating parameters.

  13. Characterization of three LYSO crystal batches

    International Nuclear Information System (INIS)

    We report on three LYSO crystal batches characterized at the Caltech crystal laboratory for future HEP experiments: 25 20 cm long crystals for the SuperB experiment; 12 13 cm long crystals for the Mu2e experiment and 623 14×14×1.5 mm3 plates with five holes for a LYSO/W Shashlik matrix for a beam test at Fermilab. Optical and scintillation properties measured are longitudinal transmittance, light output and FWHM energy resolution. Correlations between these properties are also investigated

  14. Characterization of Three LYSO Crystal Batches

    International Nuclear Information System (INIS)

    We report on three LYSO crystal batches characterized at the Caltech crystal laboratory for future HEP experiments: Twenty-five 20 cm long crystals for the SuperB experiment; twelve 13 cm long crystals for the Mu2e experiment and 623 14×14×1.5 mm plates with five holes for a LYSO/W Shashlik matrix for a beam test at Fermilab. Optical and scintillation properties measured are longitudinal Transmittance, light output and FWHM energy resolution. Correlations between these properties are also investigated

  15. 间歇结晶过程的分批优化%Batch-to-batch Optimization of Batch Crystallization Processes

    Institute of Scientific and Technical Information of China (English)

    Woranee Paengjuntuek; Paisan Kittisupakorn; Amornchai Arpornwichanop

    2008-01-01

    It is the fact that several process parameters are either unknown or uncertain. Therefore, an optimal control profile calculated with developed process models with respect to such process parameters may not give an optimal performance when implemented to real processes. This study proposes a batch-to-batch optimization strat-egy for the estimation of uncertain kinetic parameters in a batch crystallization process of potassium sulfate produc-tion. The knowledge of a crystal size distribution of the product at the end of batch operation is used in the proposedmethodology. The updated kinetic parameters are applied for determining an optimal operating temperature policy for the next batch run.

  16. Monitoring and optimization of industrial batch crystallization processes using NIR and ATR UV-vis spectroscopy

    OpenAIRE

    Hsieh, Chun; Billeter, Julien; Gemperline, Paul

    2010-01-01

    In the pharmaceutical industry, batch crystallization processes at production scale are not always well understood. Several factors have a significant impact on the process of crystallization, such as the physicochemical properties (solubility curve and super-saturation level), the crystal seeding (amount, purity and specific area), the engineering design (crystallizer and propeller), and the control (heating, cooling and stirring rates) [1]. When these factors are poorly understood or insuff...

  17. Systematic Modelling and Crystal Size Distribution Control for Batch Crystallization Processes

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli; Singh, Ravendra; Sin, Gürkan;

    Analytical Technology (PAT) system needs to be available. That is, the design of process control and product monitoring system that will obtain the desired end-product properties is also needed. The generic multi-dimensional model-based framework of batch cooling crystallization processes has been developed...... desired CSD is achieved, an appropriate Process Analytical Technology (PAT) system needs to be available. That is, the design of process control and product monitoring system that will obtain the desired end-product properties is also needed.......Crystallization processes form an important class of separation methods that are frequently used in the chemical, the pharmaceutical and the food industry. The specifications of the crystal product are usually given in terms of crystal size, shape and purity. In order to predict the desired crystal...

  18. Modelling of Batch Process Operations

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli; Cameron, Ian; Gani, Rafiqul

    Here a batch cooling crystalliser is modelled and simulated as is a batch distillation system. In the batch crystalliser four operational modes of the crystalliser are considered, namely: initial cooling, nucleation, crystal growth and product removal. A model generation procedure is shown that s...

  19. Crystallization Thermodynamic and Kinetic Behaviors of Vitamin C in Batch Crystallizer

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    The bench-scale cooling crystallization for ternary solution of L-ascorbic acid (Vitamin C) was studied. The solid-liquid phase diagram of Vitamin C-water-ethanol system was obtained on the basis of differential scanning calorimeter (DSC) curves. The heat of crystallization of Vitamin C was calculated with the aid of quantitative analysis. According to the population balance equation under unsteady state, the rates of nucleation and growth were determined. The parameters of crystallization kinetics equations were estimated by regression of experimental data. Crystal morphology and size were determined with x-ray diffraction and TA Ⅱ Coulter Counter.

  20. Continuous preparation of polymer coated drug crystals by solid hollow fiber membrane-based cooling crystallization.

    Science.gov (United States)

    Chen, Dengyue; Singh, Dhananjay; Sirkar, Kamalesh K; Pfeffer, Robert

    2016-02-29

    A facile way to continuously coat drug crystals with a polymer is needed in controlled drug release. Conventional polymer coating methods have disadvantages: high energy consumption, low productivity, batch processing. A novel method for continuous polymer coating of drug crystals based on solid hollow fiber cooling crystallization (SHFCC) is introduced here. The drug acting as the host particle and the polymer for coating are Griseofulvin (GF) and Eudragit RL100, respectively. The polymer's cloud point temperature in its acetone solution was determined by UV spectrophotometry. An acetone solution of the polymer containing the drug in solution as well as undissolved drug crystals in suspension were pumped through the tube side of the SHFCC device; a cold liquid was circulated in the shell side to rapidly cool down the feed solution-suspension in the hollow-fiber lumen. The polymer precipitated from the solution and coated the suspended crystals due to rapid temperature reduction and heterogeneous nucleation; crystals formed from the solution were also coated by the polymer. Characterizations by scanning electron microscopy, thermogravimetric analysis, laser diffraction spectroscopy, X-ray diffraction, Raman spectroscopy, and dissolution tests show that a uniformly coated, free-flowing drug/product can be obtained under appropriate operating conditions without losing the drug's pharmaceutical properties and controlled release characteristics. PMID:26772536

  1. Regions of attainable particle sizes in continuous and batch crystallization processes

    OpenAIRE

    Vetter, Thomas; Burcham, Christopher L; Doherty, Michael F.

    2014-01-01

    Abstract Process alternatives for continuous crystallization, i.e., cascades of mixed suspension, mixed product removal crystallizers (MSMPRCs) and plug flow crystallizers (PFCs), as well as batch crystallizers are discussed and modeled using population balance equations. The attainable region approach that has previously been used in the design of chemical reactor networks and separation systems is applied to the above-mentioned alternatives for crystallization processes in order to identify...

  2. Batch cooling crystallization and pressure filtration of sulphathiazole

    DEFF Research Database (Denmark)

    Häkkinen, Antti; Pöllänen, Kati; Karjalainen, Milja;

    2005-01-01

    Currently there is a great interest in new process analytical approaches to increase the process understanding of pharmaceutical unit operations. In the present study, the influence of the solvent composition on the material properties and, further, on the filtration characteristics, of different...

  3. Batch crystallization of rhodopsin for structural dynamics using an X-ray free-electron laser

    Energy Technology Data Exchange (ETDEWEB)

    Wu, Wenting; Nogly, Przemyslaw; Rheinberger, Jan; Kick, Leonhard M.; Gati, Cornelius; Nelson, Garrett; Deupi, Xavier; Standfuss, Jörg; Schertler, Gebhard; Panneels, Valérie, E-mail: valerie.panneels@psi.ch [Paul Scherrer Institute, OFLC/103, 5232 Villigen-PSI (Switzerland)

    2015-06-27

    A new batch preparation method is presented for high-density micrometre-sized crystals of the G protein-coupled receptor rhodopsin for use in time-resolved serial femtosecond crystallography at an X-ray free-electron laser using a liquid jet. Rhodopsin is a membrane protein from the G protein-coupled receptor family. Together with its ligand retinal, it forms the visual pigment responsible for night vision. In order to perform ultrafast dynamics studies, a time-resolved serial femtosecond crystallography method is required owing to the nonreversible activation of rhodopsin. In such an approach, microcrystals in suspension are delivered into the X-ray pulses of an X-ray free-electron laser (XFEL) after a precise photoactivation delay. Here, a millilitre batch production of high-density microcrystals was developed by four methodical conversion steps starting from known vapour-diffusion crystallization protocols: (i) screening the low-salt crystallization conditions preferred for serial crystallography by vapour diffusion, (ii) optimization of batch crystallization, (iii) testing the crystal size and quality using second-harmonic generation (SHG) imaging and X-ray powder diffraction and (iv) production of millilitres of rhodopsin crystal suspension in batches for serial crystallography tests; these crystals diffracted at an XFEL at the Linac Coherent Light Source using a liquid-jet setup.

  4. Batch crystallization of rhodopsin for structural dynamics using an X-ray free-electron laser

    International Nuclear Information System (INIS)

    A new batch preparation method is presented for high-density micrometre-sized crystals of the G protein-coupled receptor rhodopsin for use in time-resolved serial femtosecond crystallography at an X-ray free-electron laser using a liquid jet. Rhodopsin is a membrane protein from the G protein-coupled receptor family. Together with its ligand retinal, it forms the visual pigment responsible for night vision. In order to perform ultrafast dynamics studies, a time-resolved serial femtosecond crystallography method is required owing to the nonreversible activation of rhodopsin. In such an approach, microcrystals in suspension are delivered into the X-ray pulses of an X-ray free-electron laser (XFEL) after a precise photoactivation delay. Here, a millilitre batch production of high-density microcrystals was developed by four methodical conversion steps starting from known vapour-diffusion crystallization protocols: (i) screening the low-salt crystallization conditions preferred for serial crystallography by vapour diffusion, (ii) optimization of batch crystallization, (iii) testing the crystal size and quality using second-harmonic generation (SHG) imaging and X-ray powder diffraction and (iv) production of millilitres of rhodopsin crystal suspension in batches for serial crystallography tests; these crystals diffracted at an XFEL at the Linac Coherent Light Source using a liquid-jet setup

  5. Modelling of Batch Process Operations

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli; Cameron, Ian; Gani, Rafiqul

    Here a batch cooling crystalliser is modelled and simulated as is a batch distillation system. In the batch crystalliser four operational modes of the crystalliser are considered, namely: initial cooling, nucleation, crystal growth and product removal. A model generation procedure is shown that...... Freedom (DoF) analysis, choice of variables to satisfy DoF and solution strategy. The batch distillation model for setting up and testing an operating sequence is developed and simulated. This looks at such operating policies as constant reflux ratio or set concentration of specific compound in the...

  6. Colouring cryo-cooled crystals: online microspectrophotometry

    International Nuclear Information System (INIS)

    A portable and readily aligned online microspectrophotometer that can be easily installed on macromolecular crystallography beamlines is described. It allows measurement of the spectral characteristics of macromolecular crystals prior, during, and after the X-ray diffraction experiment. X-rays can produce a high concentration of radicals within cryo-cooled macromolecular crystals. Some radicals have large extinction coefficients in the visible (VIS) range of the electromagnetic spectrum, and can be observed optically and spectrally. An online microspectrophotometer with high temporal resolution has been constructed that is capable of measuring UV/VIS absorption spectra (200–1100 nm) during X-ray data collection. The typical X-ray-induced blue colour that is characteristic of a wide range of cryo-conditions has been identified as trapped solvated electrons. Disulphide-containing proteins are shown to form disulphide radicals at millimolar concentrations, with absorption maxima around 400 nm. The solvated electrons and the disulphide radicals seem to have a lifetime in the range of seconds up to minutes at 100 K. The temperature dependence of the kinetics of X-ray-induced radical formation is different for the solvated electrons compared with the disulphide radicals. The online microspectrophotometer provides a technique complementary to X-ray diffraction for analysing and characterizing intermediates and redox states of proteins and enzymes

  7. Temperature control of bench-scaled batch reactor equipped with a monofluid heating/cooling system

    Science.gov (United States)

    Teng, Hai-peng; Song, Yi-ming

    2014-04-01

    An advanced control concept, Predictive Functional Control (PFC), is applied for temperature control of a bench-scaled batch reactor equipped with monofluid heating/cooling system. First principles process models are developed. Based on achieved models, significant process variables, which are difficult or impossible to measure online, are estimated from easily measured variables, and cascade PFC control strategy has been projected and implemented in Matlab R14. The dynamics of individual subunits is explicitly taken into consideration by internal model in the control algorithms, and model uncertainty, various process disturbances are compensated by modification of internal model. The experimental results present an excellent capability of tracking the set point, and the success of PFC technique as a process control paradigm is illustratively demonstrated.

  8. FBRM and PVM investigations of the double feed semi-batch crystallization of 6-aminopenicillanic acid

    Institute of Scientific and Technical Information of China (English)

    Min SU; Lin WANG; Hua SUN; Jingkang WANG

    2009-01-01

    6-Aminopenicillanic acid (6-APA) is a crucial pharmaceutical intermediate in the chemistry of semi-synthetic antibiotics. The focused beam reflectance measurement (FBRM) technology and particle vision measurement (PVM) technology were employed to the processes of online-monitoring of 6-APA crystallization behavior in a double-feeding semi-batch crystallizer. Experiments were carried out with four kinds of double-feeding policies and the results were compared with the traditional single-feeding. Records and analysis of FBRM indicated that the nucleation of double feeding policy was much higher than single policy, and chord length of 6-APA was almost determined and had little change after the nucleation peak. Ostwald ripening process had no significant effect on further growth of 6-APA crystal. PVM images showed that the crystal habit of 6-APA was continuously changed during the crystallization process. The development of (002) face in the final crystal for the five feeding policies were different.

  9. Sympathetic cooling in a large ion crystal

    OpenAIRE

    Lin, Guin-Dar; Duan, L.-M.

    2015-01-01

    We analyze the dynamics and steady state of a linear ion array when some of the ions are continuously laser cooled. We calculate the ions' local temperature measured by its position fluctuation under various trapping and cooling configurations, taking into account background heating due to the noisy environment. For a large system, we demonstrate that by arranging the cooling ions evenly in the array, one can suppress the overall heating considerably. We also investigate the effect of differe...

  10. Batch production of single-crystal diamond bridges and cantilevers for microelectromechanical systems

    International Nuclear Information System (INIS)

    The utilization of single-crystal diamond offers a way to achieve extreme semiconductor and mechanical properties of diamond for microelectromechanical systems (MEMS). However, current diamond MEMS devices are limited to polycrystalline or nanocrystalline films. In this paper, we report on the batch fabrication and mechanical operation of single-crystal diamond bridges/cantilevers. The bending of these bridges/cantilevers is achieved by nanoindentation with atomic force microscopy. The resonant vibration of the cantilevers is demonstrated by using a piezoelectric actuation method with direct optical readout. These bridges/cantilevers exhibit high-quality single crystal. The maximum measured Young's modulus of the diamond bridges/cantilevers is more than 1000 GPa. The air gap between the diamond bridges/cantilevers and the substrate guarantees the application of single-crystal diamond to the MEMS.

  11. Batch study of liquid-phase adsorption of Crystal Violet using Posidonia oceanica L. fibers

    International Nuclear Information System (INIS)

    This paper presents a study on the batch adsorption of crystal violet dye from aqueous solution onto Posidonia oceanica L. fibers in order to explore their potential use as low cost adsorbents for wastewater dye removal. A series of batch tests were conducted and the influence of contact time, initial dye concentration, pH of the solution and adsorbent dosage on crystal violet removal was investigated. FT-IR spectroscopy analysis of the Posidonia oceanica L. fibers before and after dye sorption was also investigated to confirm the mechanism of the removal of crystal violet. Results indicate that crystal violet uptake increased with increased initial dye concentration and decreased with increased pH values. The results showed that the highest dye adsorption capacity (11.75 mg/g) was found at pH = 6, for an adsorbent dosage of 5 g/L, initial dye concentration of 60 mg/L, under a constant temperature of 23±02 degree, and the equilibrium state was reached within 10 min of exposure time. The relatively low cost and high capabilities of Posidonia oceanica L. fibers make them potentially attractive options for dye removal from dilute industrial effluents.

  12. Effect of cooling rate on crystallization in an aluminophosphosilicate melt

    DEFF Research Database (Denmark)

    Liu, S. J.; Zhang, Yanfei; Yue, Yuanzheng

    2011-01-01

    the glass melt to the casting, pressing and fiber-drawing processes, respectively. Results show that phase separation occurs in the melt during cooling, and leads to the internal nucleation and opalescence in the studied glass. The degree of phase separation increases with decreasing the cooling rate......The effect of cooling rate on spontaneous crystallization behavior of an alumino-phospho-silicate melt is studied by means of differential scanning calorimetry, X-ray diffraction, scanning electron microscopy and viscometry. The cooling rates of 160, 2100 and 12000 K/s are attained by subjecting....... Hence, the opalescence of the glass can be tuned by adjusting the cooling rate. This makes the production of opal glasses or transparent glass ceramics more efficient and energy saving, since the conventional isothermal treatment procedure can be left out....

  13. Time-resolved crystallization of deeply cooled liquid hydrogen isotopes

    Energy Technology Data Exchange (ETDEWEB)

    Kuehnel, Matthias

    2014-02-15

    This thesis serves two main purposes: 1. The introduction of a novel experimental method to investigate phase change dynamics of supercooled liquids 2. First-time measurements for the crystallization behaviour for hydrogen isotopes under various conditions (1) The new method is established by the synergy of a liquid microjet of ∼ 5 μm diameter and a scattering technique with high spatial resolution, here linear Raman spectroscopy. Due to the high directional stability and the known velocity of the liquid filament, its traveling axis corresponds to a time axis static in space. Utilizing evaporative cooling in a vacuum environment, the propagating liquid cools down rapidly and eventually experiences a phase transition to the crystalline state. This temporal evolution is probed along the filament axis, ultimately resulting in a time resolution of 10 ns. The feasibility of this approach is proven successfully within the following experiments. (2) A main object of study are para-hydrogen liquid filaments. Raman spectra reveal a temperature gradient of the liquid across the filament. This behaviour can quantitatively be reconstructed by numerical simulations using a layered model and is rooted in the effectiveness of evaporative cooling on the surface and a finite thermal conductivity. The deepest supercoolings achieved are ∼ 30% below the melting point, at which the filament starts to solidify from the surface towards the core. With a crystal growth velocity extracted from the data the appropriate growth mechanism is identified. The crystal structure that initially forms is metastable and probably the result of Ostwald's rule of stages. Indications for a transition within the solid towards the stable equilibrium phase support this interpretation. The analog isotope ortho-deuterium is evidenced to behave qualitatively similar with quantitative differences being mass related. In further measurements, isotopic mixtures of para-hydrogen and ortho-deuterium are

  14. Crystal Ice Formation of Solution and Its Removal Phenomena From Cooled Solid Surface

    Science.gov (United States)

    Hirata, Tetsuo; Ishikawa, Masaaki; Nagasaka, Kouji

    Experimental studies for freezing phenomena of ethylene glycol solution on cooled plate have been performed. A polyvinyl chloride as well as an acrylic resin plates are used for the cooled plates. It is found that the crystal ice formed at the cooled plate is removed from the plate due to buoyancy force acting the crystal ice. It means that ice formation on a cooled plate without deposit ice layer is possible by the present method. It is shown that the cooled plate surface is under cooled about 1.0~1.5 degree below the freezing temperature of the solution during the crystal ice formation and its removal phenomena. The degree of under cooled temperature is unaffected by the cooling temperature of the plate. For higher concentration of solution, it is found that the number of the removed crystal ice per unit time is increased and the volume of each removed ice is decreased.

  15. Structural evolution in the crystallization of rapid cooling silver melt

    Energy Technology Data Exchange (ETDEWEB)

    Tian, Z.A., E-mail: ze.tian@gmail.com [School of Physics and Electronics, Hunan University, Changsha 410082 (China); Laboratory for Simulation and Modelling of Particulate Systems School of Materials Science and Engineering, University of New South Wales, Sydney, NSW 2052 (Australia); Dong, K.J.; Yu, A.B. [Laboratory for Simulation and Modelling of Particulate Systems School of Materials Science and Engineering, University of New South Wales, Sydney, NSW 2052 (Australia)

    2015-03-15

    The structural evolution in a rapid cooling process of silver melt has been investigated at different scales by adopting several analysis methods. The results testify Ostwald’s rule of stages and Frank conjecture upon icosahedron with many specific details. In particular, the cluster-scale analysis by a recent developed method called LSCA (the Largest Standard Cluster Analysis) clarified the complex structural evolution occurred in crystallization: different kinds of local clusters (such as ico-like (ico is the abbreviation of icosahedron), ico-bcc like (bcc, body-centred cubic), bcc, bcc-like structures) in turn have their maximal numbers as temperature decreases. And in a rather wide temperature range the icosahedral short-range order (ISRO) demonstrates a saturated stage (where the amount of ico-like structures keeps stable) that breeds metastable bcc clusters. As the precursor of crystallization, after reaching the maximal number bcc clusters finally decrease, resulting in the final solid being a mixture mainly composed of fcc/hcp (face-centred cubic and hexagonal-closed packed) clusters and to a less degree, bcc clusters. This detailed geometric picture for crystallization of liquid metal is believed to be useful to improve the fundamental understanding of liquid–solid phase transition. - Highlights: • A comprehensive structural analysis is conducted focusing on crystallization. • The involved atoms in our analysis are more than 90% for all samples concerned. • A series of distinct intermediate states are found in crystallization of silver melt. • A novelty icosahedron-saturated state breeds the metastable bcc state.

  16. Structural evolution in the crystallization of rapid cooling silver melt

    International Nuclear Information System (INIS)

    The structural evolution in a rapid cooling process of silver melt has been investigated at different scales by adopting several analysis methods. The results testify Ostwald’s rule of stages and Frank conjecture upon icosahedron with many specific details. In particular, the cluster-scale analysis by a recent developed method called LSCA (the Largest Standard Cluster Analysis) clarified the complex structural evolution occurred in crystallization: different kinds of local clusters (such as ico-like (ico is the abbreviation of icosahedron), ico-bcc like (bcc, body-centred cubic), bcc, bcc-like structures) in turn have their maximal numbers as temperature decreases. And in a rather wide temperature range the icosahedral short-range order (ISRO) demonstrates a saturated stage (where the amount of ico-like structures keeps stable) that breeds metastable bcc clusters. As the precursor of crystallization, after reaching the maximal number bcc clusters finally decrease, resulting in the final solid being a mixture mainly composed of fcc/hcp (face-centred cubic and hexagonal-closed packed) clusters and to a less degree, bcc clusters. This detailed geometric picture for crystallization of liquid metal is believed to be useful to improve the fundamental understanding of liquid–solid phase transition. - Highlights: • A comprehensive structural analysis is conducted focusing on crystallization. • The involved atoms in our analysis are more than 90% for all samples concerned. • A series of distinct intermediate states are found in crystallization of silver melt. • A novelty icosahedron-saturated state breeds the metastable bcc state.

  17. Effect of Cooling Rate on Crystallization Behavior of Milk Fat Fraction/Sunflower Oil Blends

    OpenAIRE

    Martini, Silvana; Herrera, M. L.; Hartel, R. W.

    2001-01-01

    The effect of cooling rate (slow: 0.1°C/min; fast: 5.5°C/min) on the crystallization kinetics of blends of a highmelting milk fat fraction and sunflower oil (SFO) was investigated by pulsed NMR and DSC. For slow cooling rate, the majority of crystallization had already occurred by the time the set crystallization temperature had been reached. For fast cooling rate, crystallization started after the samples reached the selected crystallization temperature, and the solid fat content curves were...

  18. Transparent phosphosilicate glasses containing crystals formed during cooling of melts

    DEFF Research Database (Denmark)

    Liu, S. J.; Zhang, Yanfei; He, W.;

    2011-01-01

    The effect of P2O5-SiO2 substitution on spontaneous crystallization of SiO2-Al2O3-P2O5- Na2O-MgO melts during cooling was studied by X-ray diffraction (XRD), differential scanning calorimetry (DSC), scanning electron microscopy (SEM) and rotation viscometry. Results show that addition of P2O5 leads...... to amorphous phase separation (APS), i.e., phosphate- and silicate-rich phases. It is due to the tendency of Mg2+ to form [MgO4] linking with [SiO4]. Molar substitution of P2O5 for SiO2 enhances the network polymerization of silicate-rich phase in the melts, and thereby the spontaneous...

  19. Estimating Influence of Crystallizing Latent Heat on Cooling-Crystallizing Process of a Granitic Melt and Its Geological Implications

    Institute of Scientific and Technical Information of China (English)

    ZHANG Bangtong; WU Junqi; LING Hongfei; CHEN Peirong

    2008-01-01

    Based on the theory of thermal conductivity, in this paper we derived a formula to estimate the prolongation period (AtL) of cooling-crystallization process of a granitic melt caused by latent heat of crystallization as follows: △t=QL×△tcol/TM-TC×CP where TM is initial temperature of the granite melt, Tc crystallization temperature of the granite melt,CP specific heat, △tcol cooling period of a granite melt from its initial temperature (TM) to its crystallization temperature (TC), QL latent heat of the granite melt. The cooling period of the melt for the Fanshan granodiorite from its initial temperature (900℃) to crystallization temperature (600℃) could be estimated ~210,000 years if latent heat was not considered. Calculation for the Fanshan melt using the above formula yields a AtL value of~190,000 years, which implies that the actual cooling period within the temperature range of 900℃-600℃ should be 400,000 years. This demonstrates that the latent heat produced from crystallization of the granitic melt is a key factor influencing the cooling-crystallization process of a granitic melt, prolongating the period of crystallization and resulting in the large emplacement-crystallization time difference (ECTD) in granite batholith.

  20. A generic multi-dimensional model-based system for batch cooling crystallization processes

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli; Singh, Ravendra; Sin, Gürkan; Gernaey, Krist; Gani, Rafiqul

    2011-01-01

    Highly porous deposits of flame-made aerosol nanoparticles were formed by filtration through a porous substrate (α-alumina, average pore diameter 3.7 μm). The aerosol was characterized by transmission electron microscopy (TEM) and scanning mobility particle sizer (SMPS) showing average primary an...

  1. CRC DEPLETION CALCULATIONS FOR THE RODDED ASSEMBLIES IN BATCHES 1, 2, 3, AND 1X OF CRYSTAL RIVER UNIT 3

    International Nuclear Information System (INIS)

    The purpose of this design analysis is to document the SAS2H depletion calculations of certain rodded fuel assemblies from batches 1, 2, 3, and 1X of the Crystal River Unit 3 pressurized water reactor (PWR) that are required for Commercial Reactor Critical (CRC) evaluations to support the development of the disposal criticality methodology. A rodded assembly is one that contains a control rod assembly (CRA) or an axial power shaping rod assembly (APSRA) for some period of time during its irradiation history. The objective of this analysis is to provide SAS2H calculated isotopic compositions of depleted fuel and depleted burnable poison for each fuel assembly to be used in subsequent CRC reactivity calculations containing the fuel assemblies

  2. CRC DEPLETION CALCULATIONS FOR THE NON-RODDED ASSEMBLIES IN BATCHES 1, 2, AND 3 OF CRYSTAL RIVER UNIT 3

    International Nuclear Information System (INIS)

    The purpose of this design analysis is to document the SAS2H depletion calculations of certain non-rodded fuel assemblies from batches 1, 2, and 3 of the Crystal River Unit 3 pressurized water reactor (PWR) that are required for Commercial Reactor Critical (CRC) evaluations to support development of the disposal criticality methodology. A non-rodded assembly is one which never contains a control rod assembly (CRA) or an axial power shaping rod assembly (APSRA) during its irradiation history. The objective of this analysis is to provide SAS2H generated isotopic compositions for each fuel assembly's depleted fuel and depleted burnable poison materials. These SAS2H generated isotopic compositions are acceptable for use in CRC benchmark reactivity calculations containing the various fuel assemblies

  3. CRC DEPLETION CALCULATIONS FOR THE NON-RODDED ASSEMBLIES IN BATCHES 1, 2, AND 3 OF CRYSTAL RIVER UNIT 3

    Energy Technology Data Exchange (ETDEWEB)

    Kenneth D. Wright

    1997-07-29

    The purpose of this design analysis is to document the SAS2H depletion calculations of certain non-rodded fuel assemblies from batches 1, 2, and 3 of the Crystal River Unit 3 pressurized water reactor (PWR) that are required for Commercial Reactor Critical (CRC) evaluations to support development of the disposal criticality methodology. A non-rodded assembly is one which never contains a control rod assembly (CRA) or an axial power shaping rod assembly (APSRA) during its irradiation history. The objective of this analysis is to provide SAS2H generated isotopic compositions for each fuel assembly's depleted fuel and depleted burnable poison materials. These SAS2H generated isotopic compositions are acceptable for use in CRC benchmark reactivity calculations containing the various fuel assemblies.

  4. CRC DEPLETION CALCULATIONS FOR THE NON-RODDED ASSEMBLIES IN BATCHES 4 AND 5 OF CRYSTAL RIVER UNIT 3

    Energy Technology Data Exchange (ETDEWEB)

    Kenneth D. Wright

    1997-07-30

    The purpose of this design analysis is to document the SAS2H depletion calculations of certain non-rodded fuel assemblies from batches 4 and 5 of the Crystal River Unit 3 pressurized water reactor (PWR) that are required for commercial Reactor Critical (CRC) evaluations to support the development of the disposal criticality methodology. A non-rodded assembly is one which never contains a control rod assembly (CRA) or an axial power shaping rod assembly (APSRA) during its irradiation history. The objective of this analysis is to provide SAS2H generated isotopic compositions for each fuel assembly's depleted fuel and depleted burnable poison materials. These SAS2H generated isotopic compositions are acceptable for use in CRC benchmark reactivity calculations containing the various fuel assemblies.

  5. CRC DEPLETION CALCULATIONS FOR THE NON-RODDED ASSEMBLIES IN BATCHES 4 AND 5 OF CRYSTAL RIVER UNIT 3

    International Nuclear Information System (INIS)

    The purpose of this design analysis is to document the SAS2H depletion calculations of certain non-rodded fuel assemblies from batches 4 and 5 of the Crystal River Unit 3 pressurized water reactor (PWR) that are required for commercial Reactor Critical (CRC) evaluations to support the development of the disposal criticality methodology. A non-rodded assembly is one which never contains a control rod assembly (CRA) or an axial power shaping rod assembly (APSRA) during its irradiation history. The objective of this analysis is to provide SAS2H generated isotopic compositions for each fuel assembly's depleted fuel and depleted burnable poison materials. These SAS2H generated isotopic compositions are acceptable for use in CRC benchmark reactivity calculations containing the various fuel assemblies

  6. CRC DEPLETION CALCULATIONS FOR THE RODDED ASSEMBLIES IN BATCHES 1, 2, 3, AND 1X OF CRYSTAL RIVER UNIT 3

    Energy Technology Data Exchange (ETDEWEB)

    Kenneth D. Wright

    1997-09-03

    The purpose of this design analysis is to document the SAS2H depletion calculations of certain rodded fuel assemblies from batches 1, 2, 3, and 1X of the Crystal River Unit 3 pressurized water reactor (PWR) that are required for Commercial Reactor Critical (CRC) evaluations to support the development of the disposal criticality methodology. A rodded assembly is one that contains a control rod assembly (CRA) or an axial power shaping rod assembly (APSRA) for some period of time during its irradiation history. The objective of this analysis is to provide SAS2H calculated isotopic compositions of depleted fuel and depleted burnable poison for each fuel assembly to be used in subsequent CRC reactivity calculations containing the fuel assemblies.

  7. CRC DEPLETION CALCULATIONS FOR THE NON-RODDED ASSEMBLIES IN BATCHES 8 AND 9 CRYSTAL RIVER UNIT 3

    International Nuclear Information System (INIS)

    The purpose of this design analysis is to document the SAS2H depletion calculations of certain non-rodded fuel assemblies from batches 8 and 9 of the Crystal River Unit 3 pressurized water reactor (PWR) that are required for Commercial Reactor Critical (CRC) evaluations to support the development of the disposal criticality methodology. A non-rodded assembly is one which never contains a control rod assembly (CRA) or an axial power shaping rod assembly (APSRA) during its irradiation history. The objective of this analysis is to provide SAS2H generated isotopic compositions for each fuel assembly's depleted fuel and depleted burnable poison materials. These SAS2H generated isotopic compositions are acceptable for use in CRC benchmark reactivity calculations containing the various fuel assemblies

  8. Influence of rare earth oxides on the non-isothermal crystallization of phosphosilicate melts during cooling

    DEFF Research Database (Denmark)

    Liu, S.J.; Shan, Z.T.; Fu, G.Z.;

    2014-01-01

    -isothermal melt-crystallization kinetics can be well described by the Avrami model. The activation energy Ee of crystallization in both the undoped and Yb3+/Er3+ codoped samples during cooling is determined using the differential iso-conversional method of Friedman. The Ee value decreases with crystallinity (θ...

  9. PHYSICS UPDATE: Observation of snow crystals using a chamber cooled by dry ice

    Science.gov (United States)

    Kagawa, S.; Kakehi, M.; Ito, F.; Kagawa, K.

    1999-01-01

    It is shown that microscopic observation of natural snow crystals is possible even at relatively high atmospheric temperature, around 0 °C. For this purpose, a partial cooling method was employed. That is, a snow crystal was placed in a chamber cooled by dry ice, which prevented frost production. By using this simple method, snow crystals can be observed in winter (where snow is available). This type of observational experiment is very successful in exciting students' interest in the beauty of natural forms.

  10. Feedback system of a liquid nitrogen cooled double-crystal monochromator: design and performances

    OpenAIRE

    Proux, Olivier; Nassif, Vivian; Prat, Alain; Ulrich, Olivier; Lahera, Eric; Biquard, Xavier; Menthonnex, Jean-Jacques; Hazemann, Jean-Louis

    2005-01-01

    Abstract We report on a new setup of indirect cryogenic cooling system for double-crystal monochromator running on BM30b / FAME beamline at the ESRF (Grenoble, France). This device has been conceived to limit the vibrations on the first diffracting crystal and to maintain it at a constant temperature. These points are crucial to maximize the beamline stability. Moreover, the relative angular position of the second crystal is dynamically adjusted by a piezoelectric transducer coupled with a fe...

  11. Crystal/liquid partitioning in augite - Effects of cooling rate

    Science.gov (United States)

    Gamble, R. P.; Taylor, L. A.

    1980-01-01

    The partitioning of major and minor elements between augite and melt was determined as a function of cooling rate for two high-titanium basalt compositions. The results of this study of lunar rock systems 10017 and 75055 were compared with the results of other kinetic studies of augite-liquid partitioning in other rock systems. It was found that the partitioning of major elements (i.e., Ca, Fe, Mg) is essentially rate independent and is insensitive to bulk rock composition and to the nature and order of appearance of coexisting phases for cooling rates of less than 100 C/hr. The partitioning behavior of minor elements (i.e., Al, Cr, Ti) for the same range of cooling rates is complex, being dependent on cooling rate and bulk rock composition. Consideration of these factors is important when augite chemistry and/or partitioning behavior are used in modeling certain magmatic processes or in estimating the thermal history of basaltic rocks.

  12. Neutronics and Depletion Methods for Parametric Studies of Fluoride Salt Cooled High Temperature Reactors with Slab Fuel Geometry and Multi-Batch Fuel Management Schemes

    International Nuclear Information System (INIS)

    The Advanced High Temperature Reactor (AHTR) is a 3400 MWth fluoride salt cooled high temperature reactor (FHR) that uses TRISO particle fuel compacted into slabs rather than spherical fuel pebbles or cylindrical fuel compacts. Simplified methods are required for parametric design studies such that analyzing the entire feasible design space for an AHTR is tractable. These simplifications include fuel homogenization techniques to increase the speed of neutron transport calculations in depletion analysis and equilibrium depletion analysis methods to analyze systems with multi-batch fuel management schemes. This paper presents three elements of significant novelty. First, the reactivity-equivalent physical transformation (RPT) methodology usually applied in systems with coated particle fuel in cylindrical and spherical geometries was extended to slab geometries. Secondly, based on this newly developed RPT method for slab geometries, a methodology that uses Monte Carlo depletion approaches was further developed to search for the maximum discharge burnup in a multi-batch system by iteratively estimating the beginning of equilibrium cycle composition and sampling different discharge burnups. This iterative equilibrium depletion search (IEDS) method fully defines an equilibrium fuel cycle (keff, power, flux and composition evolutions across space and time), but is computationally demanding, although feasible on single-processor workstations. Finally, an analytical method, the non-linear reactivity model, was developed by expanding the linear reactivity model to include an arbitrary number of higher order terms to extrapolate single-batch depletion results to estimate the maximum discharge burnup and BOEC keff in systems with multi-batch fuel management schemes. Results from this method were benchmarked against equilibrium depletion analysis results using the IEDS.

  13. Efficient rotational cooling of Coulomb-crystallized molecular ions by a helium buffer gas.

    Science.gov (United States)

    Hansen, A K; Versolato, O O; Kłosowski, L; Kristensen, S B; Gingell, A; Schwarz, M; Windberger, A; Ullrich, J; López-Urrutia, J R Crespo; Drewsen, M

    2014-04-01

    The preparation of cold molecules is of great importance in many contexts, such as fundamental physics investigations, high-resolution spectroscopy of complex molecules, cold chemistry and astrochemistry. One versatile and widely applied method to cool molecules is helium buffer-gas cooling in either a supersonic beam expansion or a cryogenic trap environment. Another more recent method applicable to trapped molecular ions relies on sympathetic translational cooling, through collisional interactions with co-trapped, laser-cooled atomic ions, into spatially ordered structures called Coulomb crystals, combined with laser-controlled internal-state preparation. Here we present experimental results on helium buffer-gas cooling of the rotational degrees of freedom of MgH(+) molecular ions, which have been trapped and sympathetically cooled in a cryogenic linear radio-frequency quadrupole trap. With helium collision rates of only about ten per second--that is, four to five orders of magnitude lower than in typical buffer-gas cooling settings--we have cooled a single molecular ion to a rotational temperature of 7.5(+0.9)(-0.7) kelvin, the lowest such temperature so far measured. In addition, by varying the shape of, or the number of atomic and molecular ions in, larger Coulomb crystals, or both, we have tuned the effective rotational temperature from about 7 kelvin to about 60 kelvin by changing the translational micromotion energy of the ions. The extremely low helium collision rate may allow for sympathetic sideband cooling of single molecular ions, and eventually make quantum-logic spectroscopy of buffer-gas-cooled molecular ions feasible. Furthermore, application of the present cooling scheme to complex molecular ions should enable single- or few-state manipulations of individual molecules of biological interest. PMID:24670662

  14. Design of an adaptive cooled first crystal for an X-ray monochromator

    International Nuclear Information System (INIS)

    We report here on the design of the first crystal in an x-ray monochromator for E.S.R.F. beam lines. This crystal is a thin silicon foil bonded to a cooled beryllium support. A system of piezoelectric actuators is used to counterbalance the deformations induced by synchrotron beams. This work was carried out by the C.E.A. in collaboration with the E.S.R.F. and the LASERDOT Company (Aerospatiale Group). (orig.)

  15. Probing polymer crystallization at processing-relevant cooling rates with synchrotron radiation

    International Nuclear Information System (INIS)

    Processing of polymeric materials to produce any kind of goods, from films to complex objects, involves application of flow fields on the polymer melt, accompanied or followed by its rapid cooling. Typically, polymers solidify at cooling rates which span over a wide range, from a few to hundreds of °C/s. A novel method to probe polymer crystallization at processing-relevant cooling rates is proposed. Using a custom-built quenching device, thin polymer films are ballistically cooled from the melt at rates between approximately 10 and 200 °C/s. Thanks to highly brilliant synchrotron radiation and to state-of-the-art X-ray detectors, the crystallization process is followed in real-time, recording about 20 wide angle X-ray diffraction patterns per second while monitoring the instantaneous sample temperature. The method is applied to a series of industrially relevant polymers, such as isotactic polypropylene, its copolymers and virgin and nucleated polyamide-6. Their crystallization behaviour during rapid cooling is discussed, with particular attention to the occurrence of polymorphism, which deeply impact material’s properties

  16. Probing polymer crystallization at processing-relevant cooling rates with synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Cavallo, Dario, E-mail: Dario.cavallo@unige.it [University of Genoa, Dept. of Chemistry and Industrial Chemistry, Via Dodecaneso 31, 16146 Genoa (Italy); Portale, Giuseppe [ESRF, Dubble CRG, Netherlands Organization of Scientific Research (NWO), 38043 Grenoble (France); Androsch, René [Martin-Luther-University Halle-Wittenberg, Center of Engineering Sciences, D-06099 Halle/S. (Germany)

    2015-12-17

    Processing of polymeric materials to produce any kind of goods, from films to complex objects, involves application of flow fields on the polymer melt, accompanied or followed by its rapid cooling. Typically, polymers solidify at cooling rates which span over a wide range, from a few to hundreds of °C/s. A novel method to probe polymer crystallization at processing-relevant cooling rates is proposed. Using a custom-built quenching device, thin polymer films are ballistically cooled from the melt at rates between approximately 10 and 200 °C/s. Thanks to highly brilliant synchrotron radiation and to state-of-the-art X-ray detectors, the crystallization process is followed in real-time, recording about 20 wide angle X-ray diffraction patterns per second while monitoring the instantaneous sample temperature. The method is applied to a series of industrially relevant polymers, such as isotactic polypropylene, its copolymers and virgin and nucleated polyamide-6. Their crystallization behaviour during rapid cooling is discussed, with particular attention to the occurrence of polymorphism, which deeply impact material’s properties.

  17. Igneous cooling history of olivine-phyric shergottite Yamato 980459 constrained by dynamic crystallization experiments

    Science.gov (United States)

    First, Emily; Hammer, Julia

    2016-07-01

    Dynamic crystallization experiments were performed on a liquid having the bulk composition of olivine-phyric shergottite Yamato 980459, to constrain the igneous thermal history of this meteorite. Key characteristics of the meteorite's mineralogy and texture, including several morphologically distinct olivine and pyroxene crystal populations and a glassy mesostasis devoid of plagioclase, were replicated upon cooling from 1435 to 909 °C at 1 atmosphere under reducing conditions. Three sequential cooling ramps are required to produce synthetic samples with textures and compositions matching Yamato 980459. Olivine phenocrysts formed at stage suppressed the formation of plagioclase and produced groundmass crystals, consistent with crystallization at lava flow depths of 5-7 cm. Although Y 980459 is unique among Martian meteorites (i.e., preserving a primary glassy mesostasis), its emplacement did not require unique physical conditions. Rather, the second and third cooling stages may reflect cooling within the core of a pāhoehoe-like flow and subsequent breakout on the surface of Mars.

  18. Laser-induced cooling of a Yb:YAG crystal in air at atmospheric pressure.

    Science.gov (United States)

    Soares de Lima Filho, Elton; Nemova, Galina; Loranger, Sébastien; Kashyap, Raman

    2013-10-21

    We report for the first time the experimental demonstration of optical cooling of a bulk crystal at atmospheric pressure. The use of a fiber Bragg grating (FBG) sensor to measure laser-induced cooling in real time is also demonstrated for the first time. A temperature drop of 8.8 K from the chamber temperature was observed in a Yb:YAG crystal in air when pumped with 4.2 W at 1029 nm. A background absorption of 2.9 × 10⁻⁴ cm⁻¹ was estimated with a pump wavelength at 1550 nm. Simulations predict further cooling if the pump power is optimized for the sample's dimensions. PMID:24150315

  19. Cooling rates and crystallization dynamics of shallow level pegmatite-aplite dikes, San Diego County, California

    Science.gov (United States)

    Webber, Karen L.; Simmons, William B.; Falster, Alexander U.; Foord, Eugene E.

    1999-01-01

    Pegmatites of the Pala and Mesa Grande Pegmatite Districts, San Diego County, California are typically thin, sheet-like composite pegmatite-aplite dikes. Aplitic portions of many dikes display pronounced mineralogical layering referred to as "line rock," characterized by fine-grained, garnet-rich bands alternating with albite- and quartz-rich bands. Thermal modeling was performed for four dikes in San Diego County including the 1 m thick Himalaya dike, the 2 m thick Mission dike, the 8 m thick George Ashley dike, and the 25 m thick Stewart dike. Calculations were based on conductive cooling equations accounting for latent heat of crystallization, a melt emplacement temperature of 650 °C into 150 °C fractured, gabbroic country rock at a depth of 5 km, and an estimated 3 wt% initial H2O content in the melt. Cooling to -5 cm/s. Crystal size distribution (CSD) studies of garnet from layered aplites suggest growth rates of about 10-6 cm/s. These results indicate that the dikes cooled and crystallized rapidly, with variable nucleation rates but high overall crystal-growth rates. Initial high nucleation rates coincident with emplacement and strong undercooling can account for the millimeter-size aplite grains. Lower nucleation rates coupled with high growth rates can explain the decimeter-size minerals in the hanging walls, cores, and miarolitic cavities of the pegmatites. The presence of tourmaline and/or lepidolite throughout these dikes suggests that although the melts were initially H2O-undersaturated, high melt concentrations of incompatible (or fluxing) components such as B, F, and Li (±H2O), aided in the development of large pegmatitic crystals that grew rapidly in the short times suggested by the conductive cooling models.

  20. Composition dependence of spontaneous crystallization of phosphosilicate glass melts during cooling

    DEFF Research Database (Denmark)

    Liu, S.J.; Zhu, C.F.; Zhang, Y.F.; Xiao, Z.H.; Yue, Yuanzheng

    2012-01-01

    crystallization degree. It is found that adding NaF into the studied compositions slightly decreases melt fragility and improves both the glass-forming ability and melt workability. This effect is associated with the unique structural role of NaF compared to the other modifier oxides. It is also found that the......Crystallization behavior of alumino-phospho-silicate melts during cooling is studied by means of the differential scanning calorimetry, X-ray diffractometry and viscometry. The results show a pronounced impact of alkaline earth oxide, alkali oxide and fluoride on the crystal type and...... onset viscosity of crystallization can be used as a parameter for describing both glass-forming ability and melt workability....

  1. Combined anti-solvent and cooling method of manufacturing indomethacin-saccharin (IMC-SAC) co-crystal powders

    Science.gov (United States)

    Chun, Nan-Hee; Lee, Min-Jeong; Song, Geon-Hyung; Chang, Kwan-Young; Kim, Chang-Sam; Choi, Guang J.

    2014-12-01

    The anti-solvent approach has been demonstrated as one potential industrial method to produce pharmaceutical co-crystal powders with high purity. In this study, we combined the anti-solvent method with cooling to maximize the yield of the solution-based co-crystallization between indomethacin (IMC) and saccharin (SAC). The cooling start time was the key process parameter; other parameters were fixed based on results of preliminary work. Highly pure IMC-SAC co-crystal powders were produced via the combined method, regardless of the cooling start time, and the yield was substantially enhanced. However, some material properties, such as crystallinity and particle size, were affected by the cooling start time; i.e., whether cooling was started before nucleation (pre-nucleation cooling) or after nucleation (post-nucleation cooling). When pre-nucleation cooling was applied, a greater degree of supersaturation led to nucleation of α-IMC and IMC-SAC together. The metastable α-IMC eventually transitioned to stable IMC-SAC co-crystal particles, followed by crystal growth. When post-nucleation cooling was applied, the transient α-IMC was not detected during the entire process.

  2. Radiative cooling of solar absorbers using a visibly transparent photonic crystal thermal blackbody.

    Science.gov (United States)

    Zhu, Linxiao; Raman, Aaswath P; Fan, Shanhui

    2015-10-01

    A solar absorber, under the sun, is heated up by sunlight. In many applications, including solar cells and outdoor structures, the absorption of sunlight is intrinsic for either operational or aesthetic considerations, but the resulting heating is undesirable. Because a solar absorber by necessity faces the sky, it also naturally has radiative access to the coldness of the universe. Therefore, in these applications it would be very attractive to directly use the sky as a heat sink while preserving solar absorption properties. Here we experimentally demonstrate a visibly transparent thermal blackbody, based on a silica photonic crystal. When placed on a silicon absorber under sunlight, such a blackbody preserves or even slightly enhances sunlight absorption, but reduces the temperature of the underlying silicon absorber by as much as 13 °C due to radiative cooling. Our work shows that the concept of radiative cooling can be used in combination with the utilization of sunlight, enabling new technological capabilities. PMID:26392542

  3. Small angle neutron scattering on a fast-cooled liquid crystal: MBBA

    International Nuclear Information System (INIS)

    The medium range order was studied in the non-crystalline solid phases of the fast-cooled nematic liquid crystal MBBA by small angle scattering of neutrons. In agreement with theoretical predictions, anisotropic intensity distribution was found at 0<0.005 nmsup(-1) on the magnetic field aligned sample. Bragg-reflections were also observed around 0.037 nmsup(-1) as a consequence of the evolution of smectic-type structures connected with the gradual relaxation in these solid phases. (author)

  4. Improvement in Stability of SPring-8 Standard X-Ray Monochromators with Water-Cooled Crystals

    Science.gov (United States)

    Yamazaki, Hiroshi; Shimizu, Yasuhiro; Miura, Takanori; Tanaka, Masayuki; Kishimoto, Hikaru; Matsuzaki, Yasuhisa; Shimizu, Nobtaka; Kawano, Yoshiaki; Kumasaka, Takashi; Yamamoto, Masaki; Koganezawa, Tomoyuki; Sato, Masugu; Hirosawa, Ichiro; Senba, Yasunori; Ohashi, Haruhiko; Goto, Shunji; Ishikawa, Tetsuya

    2010-06-01

    SPring-8 standard double-crystal monochromators containing water-cooled crystals were stabilized to a sufficient level to function as a part of optics components to supply stable microfocused x-ray beams, by determining causes of the instability and then removing them. The instability was caused by two factors—thermal deformation of fine stepper stages in the monochromator, which resulted in reduction in beam intensity with time, and vibrations of coolant supply units and vacuum pumps, which resulted in fluctuation in beam intensity. We remodeled the crystal holders to maintain the stage temperatures constant with water, attached x-ray and electron shields to the stages in order to prevent their warming up, introduced accumulators in the water circuits to absorb pressure pulsation, used polyurethane tubes to stabilize water flow, and placed rubber cushions un der scroll vacuum pumps. As a result, the intensity reduction rate of the beam decreased from 26% to 1% per hour and the intensity fluctuation from 13% to 1%. The monochromators were also modified to prevent radiation damage to the crystals, materials used as a water seal, and motor cables.

  5. Improvement in Stability of SPring-8 Standard X-Ray Monochromators with Water-Cooled Crystals

    International Nuclear Information System (INIS)

    SPring-8 standard double-crystal monochromators containing water-cooled crystals were stabilized to a sufficient level to function as a part of optics components to supply stable microfocused x-ray beams, by determining causes of the instability and then removing them. The instability was caused by two factors--thermal deformation of fine stepper stages in the monochromator, which resulted in reduction in beam intensity with time, and vibrations of coolant supply units and vacuum pumps, which resulted in fluctuation in beam intensity. We remodeled the crystal holders to maintain the stage temperatures constant with water, attached x-ray and electron shields to the stages in order to prevent their warming up, introduced accumulators in the water circuits to absorb pressure pulsation, used polyurethane tubes to stabilize water flow, and placed rubber cushions under scroll vacuum pumps. As a result, the intensity reduction rate of the beam decreased from 26% to 1% per hour and the intensity fluctuation from 13% to 1%. The monochromators were also modified to prevent radiation damage to the crystals, materials used as a water seal, and motor cables.

  6. Feedback system of a liquid-nitrogen-cooled double-crystal monochromator: design and performances.

    Science.gov (United States)

    Proux, Olivier; Nassif, Vivian; Prat, Alain; Ulrich, Olivier; Lahera, Eric; Biquard, Xavier; Menthonnex, Jean Jacques; Hazemann, Jean Louis

    2006-01-01

    A new set-up is reported of an indirect cryogenic cooling system for a double-crystal monochromator which runs on the BM30b/FAME beamline at the ESRF (Grenoble, France). This device has been conceived to limit the vibrations on the first diffracting crystal and to maintain it at a constant temperature. These points are crucial for maximizing the beamline stability. Moreover, the relative angular position of the second crystal can be dynamically adjusted by a piezoelectric transducer coupled with a feedback system in order to always be at the maximum of the rocking curve during an X-ray absorption spectroscopy scan. The temperature is stabilized to an accuracy of 0.01 degrees , with two principal consequences. The energy resolution is close to the theoretical value [DeltaE/E = 5.6 x 10(-6) for Si(220)] and the precision of the energy positioning is extremely good even if the power load changes. A feedback mechanism allows a permanent and automatic optimization of the angle between the two crystals of the monochromator. The intensity of the monochromatic beam remains optimized (i) when the intensity of the electron beam decreases in the storage ring and (ii) during an energy scan. PMID:16371709

  7. An experimental study of pyroxene crystallization during rapid cooling in a thermal gradient; applications to komatiites and chondrites

    Directory of Open Access Journals (Sweden)

    S. Bouquain

    2013-03-01

    Full Text Available To investigate the crystallization of pyroxene in spinifex-textured komatiites and in chondrites we undertook a series of experiments in which compositions in the CMAS system were cooling rapidly in a thermal gradient. Cooling rates were generally between 5 to 10 °C h−1 but some runs were made at 100–200 °C h−1; thermal gradients were between 10 and 20 °C cm−1. These conditions reproduced those at various levels in the crust of komatiitic lava flow. The starting composition was chosen to have pigeonite on the liquidus and a majority of the experiments crystallized zoned pigeonite-diopside crystals like those in komatiite lavas. A~conspicuous aspect of the experimental results was their lack of reproduceability. Some experiments crystallized forsterite whereas others that were run under similar conditions crystallized two pyroxenes and no forsterite; some experiments were totally glassy but others totally crystallized to pyroxene. The degree of supercooling at the onset of pyroxene crystallization was variable, from less than 25 °C to more than 110 °C. We attribute these results to the difficulty of nucleation of pyroxene. In some cases forsterite crystallized metastably and modified the liquid composition to inhibit pyroxene crystallization; in others no nucleation took place until a large degree of supercooling was achieved, then pyroxene crystallized rapidly. Pigeonite crystallized under a wide range of conditions, at cooling rates from 3 to 100 °C h−1. The notion that this mineral only forms at low cooling rates is not correct.

  8. Performance of a directly water-cooled silicon crystal for use in high-power synchrotron radiation applications

    International Nuclear Information System (INIS)

    Results of measurements made using the Multipole Wiggler at Beamline 16 of Photon Factory are reported. Double crystal rocking curves, Si(111) and Si(333) topographs, and thermal maps of the cooled crystal surface were measured at total incident power levels up to 1600 W and power densities up to 0.7 W/mm2, for two different crystal designs. Significant crystal deformation occurred in the form of surface curvature for both designs. Finite element calculations provided a preview of the experimental results and proved very valuable in interpretation of the measurements. 16 refs., 10 figs., 5 tabs

  9. Biological treatment of thin-film transistor liquid crystal display (TFT-LCD) wastewater using aerobic and anoxic/oxic sequencing batch reactors.

    Science.gov (United States)

    Lei, Chin-Nan; Whang, Liang-Ming; Chen, Po-Chun

    2010-09-01

    The amount of pollutants produced during manufacturing processes of thin-film transistor liquid crystal display (TFT-LCD) substantially increases due to an increasing production of the opto-electronic industry in Taiwan. This study presents the treatment performance of one aerobic and one anoxic/oxic (A/O) sequencing batch reactors (SBRs) treating synthetic TFT-LCD wastewater containing dimethyl sulfoxide (DMSO), monoethanolamine (MEA), and tetra-methyl ammonium hydroxide (TMAH). The long-term monitoring results for the aerobic and A/O SBRs demonstrate that stable biodegradation of DMSO, MEA, and TMAH can be achieved without any considerably adverse impacts. The ammonium released during MEA and TMAH degradation can also be completely oxidized to nitrate through nitrification in both SBRs. Batch studies on biodegradation rates for DMSO, MEA, and TMAH under anaerobic, anoxic, and aerobic conditions indicate that effective MEA degradation can be easily achieved under all three conditions examined, while efficient DMSO and TMAH degradation can be attained only under anaerobic and aerobic conditions, respectively. The potential odor problem caused by the formation of malodorous dimethyl sulfide from DMSO degradation under anaerobic conditions, however, requires insightful consideration in treating DMSO-containing wastewater. PMID:20705321

  10. Liquid-metal-cooled, curved-crystal monochromator for Advanced Photon Source bending-magnet beamline 1-BM

    International Nuclear Information System (INIS)

    The authors describe a horizontally focusing curved-crystal monochromator that invokes a 4-point bending scheme and a liquid-metal cooling bath. The device has been designed for dispersive diffraction and spectroscopy in the 5--20 keV range, with a predicted focal spot size of ≤ 100 microm. To minimize thermal distortions and thermal equilibration time, the 355 x 32 x 0.8 mm crystal will be nearly half submerged in a bath of Ga-In-Sn-Zn alloy. The liquid metal thermally couples the crystal to the water-cooled Cu frame, while permitting the required crystal bending. Calculated thermal profiles and anticipated focusing properties are discussed

  11. Design concept for a direct water-cooled silicon crystal for use in a high-power synchrotron radiation beam

    International Nuclear Information System (INIS)

    The onset of high-power Synchrotron Radiation beams, now available at several of the Synchrotron Radiation facilities, has resulted in a search for new ways on how to handle the increased thermal load on optical components that are directly exposed to these beams. This report examines one possible way of the direct water-cooling of a silicon crystal as used in monochromators and how to get the water to the crystal with the least possible strain on the crystal. Suggestions are made on how to mount the crystal assembly in an experimental setup, so that physical properties of the crystal can be measured during direct exposure to a suitable high-power Synchrotron Radiation beam. Ways of making small correction movements to the crystal in two directions are outlined. (author)

  12. Crystallization and cooling conditions for the diogenite formation in the turbulent magma ocean of the asteroid 4 Vesta

    CERN Document Server

    Kawabata, Yusuke

    2016-01-01

    The asteroid 4 Vesta has been completely differentiated to core and mantle despite its small size, of which surface materials are howardite-eucrite-diogenite (HED) meteorites that we know the detailed petrology, and therefore, is a good target for understanding differentiation of terrestrial planets. A new differentiation model for crust formation was developed by taking magma ocean fluid dynamics, chemical equilibrium, presence of $^{26}$Al, and cooling into consideration with special care to crystal separation. The role of crystal size, thickness of the conductive lid, and fO2 are evaluated as parameters. The results show that large crystals (1cm) settle and form a km-thick cumulate layer of orthopyroxene with Mg# of 0.70-0.90 in ~20 thousand years, which almost agrees with the Mg# of diogenites, whereas thinner layers are formed if the grain size is smaller.

  13. Amplification of laser radiation in disk Yb:YAG crystals cooled down to the liquid nitrogen temperature

    International Nuclear Information System (INIS)

    The parameters of a diode-pumped Yb:YAG amplifier are calculated. The derived expressions allow one to determine the optimal doping of the YAG crystal with Yb ions, which is ∼10% for a 600-μm-thick crystal. The calculations take into account the absorption line profile and the characteristics of the pump spectrum (the shape, width, central wavelength). When the 10% Yb-doped YAG crystal is cooled down from 296 K to 80 K, the shift of the gain profile centre (∼0.3 nm) and the increase in the stimulated emission cross section (by four times) as well as the depletion of the lower working level are observed. The small-signal gain (the maximum value is 1.7, which corresponds to the gain 4.4 cm-1) is measured as a function of the absorbed pump power and well agrees with the results of theoretical calculations. (lasers)

  14. FORTRAN 77 programs for conductive cooling of dikes with temperature-dependent thermal properties and heat of crystallization

    Science.gov (United States)

    Delaney, P.T.

    1988-01-01

    Temperature histories obtained from transient heat-conduction theory are applicable to most dikes despite potential complicating effects related to magma flow during emplacement, groundwater circulation, and metamorphic reaction during cooling. Here. machine-independent FORTRAN 77 programs are presented to calculate temperatures in and around dikes as they cool conductively. Analytical solutions can treat thermal-property contrasts between the dike and host rocks, but cannot address the release of magmatic heat of crystallization after the early stages of cooling or the appreciable temperature dependence of thermal conductivity and diffusivity displayed by most rock types. Numerical solutions can incorporate these additional factors. The heat of crystallization can raise the initial temperature at the dike contact, ??c1, about 100??C above that which would be estimated if it were neglected, and can decrease the rate at which the front of solidified magma moves to the dike center by a factor of as much as three. Thermal conductivity and diffusivity of rocks increase with decreasing temperature and, at low temperatures, these properties increase more if the rocks are saturated with water. Models that treat these temperature dependencies yield estimates of ??c1 that are as much as 75??C beneath those which would be predicted if they were neglected. ?? 1988.

  15. Batch By Batch Longitudinal Emittance Blowup MD

    CERN Document Server

    Mastoridis, T; Butterworth, A; Jaussi, M; Molendijk, J

    2012-01-01

    The transverse bunch emittance increases significantly at 450 GeV from the time of injection till the ramp due to IBS. By selectively blowing up the longitudinal emittance of the incoming batch at each injection, it should be possible to reduce the transverse emittance growth rates due to IBS. An MD was conducted on April 22nd 2012 to test the feasibility and performance of the batch-by-batch longitudinal emittance blowup. There were three main goals during the MD. First, to test the developed hardware, firmware, and software for the batch-by-batch blowup. Then, to measure the transverse emittance growth rates of blown-up and "witness" batches to quantify any improvement, and finally to test the ALLInjectSequencer class, which deals with the complicated gymnastics of introducing or masking the new batch to various RF loops.

  16. Abundant Cool Magnesium-Rich Pyroxene Crystals in Comet Hale-Bopp

    Science.gov (United States)

    Wooden, D. H.

    1999-01-01

    Modeling of the observed dust emission from Comet Hale-Bopp over a large range of heliocentric distances (2.8 AU - 0.93 AU -1.7 AU) led to the discovery of Mg-rich pyroxene crystals in the coma These pyroxene crystals are apparent in the 10 micron spectrum only when the comet is close to perihelion (r(sub h) = 1.2 AU) because they are cooler than the other silicate minerals. The pyroxene crystals are cooler than the other species because of their high Mg-content. They do not absorb as efficiently as the other silicate minerals. Given the same high Mg content of Mg/(Mg + Fe) = 0.9, radiative equilibrium computations show that pyroxene crystals are expected to be 150 K cooler than olivine crystals. The pyroxene crystals are also about 10x more abundant than the other silicate mineral species. Their high Mg content and relatively large abundance are in agreement with the preponderance of pyroxene interplanetary dust particles (IDPs) and the recent reanalysis of the PUMA-I flyby of Comet Halley. Before Hale-Bopp, only olivine crystals were detected spectroscopically in comets, probably because the pyroxene crystals are less optically active, hence significantly cooler and harder to detect in contrast to the warmer silicate species. Determining the relative abundances of silicate minerals depends on their Mg contents. If the pyroxene crystals in Comet Hale-Bopp are solar nebula condensates, then they probably had to form during the early FU Orionis epoch when the inner disk was hot enough and be transported out to the region of formation of icy planetesimals without being reheated. Reheating events appear to reincorporate Fe back into the crystals or form Fe-rich rims, which are not consistent with the high-Mg-content crystals. The condensation of Mg-rich pyroxene crystals is expected from solar nebula thermal equilibrium computations. However, their subsequent transport to the outer solar nebula unaltered has yet to be theoretically demonstrated. The discovery of Mg

  17. Introduction of liquid nitrogen cryogenic cooling system and development of multi-crystal switching system on BL11XU at SPring-8

    International Nuclear Information System (INIS)

    The liquid nitrogen circulation cooling device for a double crystal monochromator was introduced, and the multi-crystal switching system was developed as part of the R and D of beamlines on the JAEA dedicated beamline 'BL11XU' at SPring-8. The cooling method using liquid nitrogen has two characteristics; (1) the coefficient of linear expansion of silicon becomes smaller, and (2) heat conductivity becomes larger by cooling silicon single crystals near to liquid nitrogen temperature. The X-ray energy range from 6 keV to 70 keV is required for researches on BL11XU. The rotation range of theta angle of the monochromator is limited from 3 to 27 degrees. In order to obtain the high flux X-ray in the required energy range, it is desirable to use both Si (111) and Si (311) crystals properly according to each experiment. However, for the monochromator equipped with the liquid nitrogen circulation cooling device, it is generally required at least for 3 - 5 days to exchange crystals. Then, we developed a new multi-crystal switching system. In this system, 2 sets of single crystals (i.e. Si(111) and Si(311)) were prepared with the same size. Then, they were arranged side by side so that the crystals could be switched easily only by changing one axis. The indium sheets were intercalated between crystals to improve of the heat transfer of the crystals. In order to prevent the vibration of crystals by liquid nitrogen circulation, unnecessary axes were removed from the monochromator. The axes and the motors were also improved. Moreover, the sheet heater was intercalated to prevent the super cooling of stages by liquid nitrogen circulation. Consequently, as compared with the previously artificial synthetic-diamond crystal, X-ray intensity became about 7.4 times larger at 14.4 keV. Furthermore, the crystal exchange and its adjustment could be attained only in 5 minutes as the needed arises. This multi-crystal switching system can be applied not only to the above-mentioned crystal

  18. Attaining 186-nm light generation in cooled beta-BaB(2)O(4) crystal.

    Science.gov (United States)

    Kouta, H; Kuwano, Y

    1999-09-01

    The transparency range of beta-BaB(2)O(4) (BBO) was expanded by means of cooling, and the resulting absorption coefficient at 193.4 nm was reduced to 0.29cm(-1) at 91 K from 1.39cm(-1) at 295 K. Further, generation of light at 186.0 nm (the measurement limit in air) by type I sum-frequency generation (SFG) based on fundamental (744-nm) and third-harmonic (248-nm) light from a Ti:sapphire laser was confirmed for cooled BBO. Calculations based on observed data for SFG wavelengths and phase-matching angles indicate a potential for cooled BBO to generate wavelengths as low as 181.7 nm. PMID:18073993

  19. Further tests on liquid-nitrogen-cooled, thin silicon-crystal monochromators using a focused wiggler synchrotron beam

    International Nuclear Information System (INIS)

    A newly designed cryogenically cooled, thin Si crystal monochromator was tested at the European Synchrotrons Radiation Facility (ESRF) beamline BL3. It exhibited less than 1 arcsec of thermal strain up to a maximum incident power of 186 W and average power density of 521 W/mm2. Data were collected for the thin (0.7 mm) portion of the crystal and for the thick (>25 mm) part. Rocking curves were measured as a function of incident power. With a low power beam, the Si(333) rocking curve at 30 keV for the thin and thick sections was < 1 arcsec FWHM at room temperature. The rocking curve of the thin section increased to 2.0 arcsec when cooled to 78 K, while the thick part was unaffected by the reduction in temperature. The rocking curve of the this section broadened to 2.5 arcsec FWHM and that of the thick section broadened to 1.7 arcsec at the highest incident power. The proven range of performance for this monochromator has been extended to the power density, but not the absorbed power, expected for the Advanced Photon Source (APS) undulator A in closed-gap operation (first harmonic at 3.27 kev) at a storage-ring current of 300 mA

  20. Calculations of thermal deformations in directly water-cooled monochromator crystals

    International Nuclear Information System (INIS)

    Computer simulations on the thermal behaviors, i.e., thermal transfer coefficient, temperature distribution and thermal deformations of monochromator crystals have been reported under the condition that they would be used in SPring-8. The calculations have been carried out on the basis of high heat load experiments by the present authors with a finite element analysis code (ANSYS). The bending-magnet (with power density of 0.27 MW/m2 on crystal surface) causes a temperature rise of 4 K and a slope error of 0.27 arcsec on the top surface of crystal. On the prototype X-ray undulator WPH-33J beamline, the crystal receives a power density of 8.1 MW/m2, having a temperature rise of 85 K and a slope error of 2.1 arcsec in the simulation. (author)

  1. The Effect of the Wall Contact and Post-Growth, Cool-Down on Defects in CdTe Crystals Grown By 'Contactless' PVT

    Science.gov (United States)

    Palosz, W.; Grasza, K.; Dudley, M.; Raghothamachar, B.; Cai, L.; Dunrose, K.; Halliday, D.; Boyall, N. M.; Rose, M. Franklin (Technical Monitor)

    2001-01-01

    To take a maximum advantage of materials processing in microgravity for understanding the effects of gravity, gravity-independent effects should be minimized. In crystal growth, the quality of the grown crystals may depend, among other factors, on their interaction with the walls of the processing container during and after growth, and on the rate of the crystal cool-down at the end of the process. To investigate the above phenomena, a series of CdTe crystal growth processes was carried out. The crystals were grown by physical vapor transport without contact with the side walls of the silica glass ampoules. To eliminate the effect of the seed quality, and to reduce the number of nuclei and related crystal grains, the Low Supersaturation Nucleation technique was applied. The source temperature was 930 C, the undercooling was a few degrees. The crystals, having the diameter of 25 mm, grew at the rate of a few mm per day. The post-growth cool-down to the room temperature was conducted at different rates, and lasted from a few minutes to four days. The crystals were characterized using chemical etching, low temperature luminescence, and Synchrotron White Beam X-ray Topography techniques. The dislocation (etch pit) density was measured and its distribution was analyzed by comparison with Poisson curves and with the Normalized Radial Distribution Correlation Function. In the regions where the crystal is in contact with silica, the materials show a considerable strain field which extends for a few mm or more from the silica-crystal interface. In the reference crystal grown with contact with the ampoule walls, and when the crystals are cooled at the highest rates, the etch pit/dislocation density is in the high 10(exp 5) per square centimeter region. Typical EPD values for lower cool-down rates are in the lower 10(exp 4) per square centimeter region. In some areas the actual dislocation density was about 10(exp 3) per square centimeter or even less. No apparent effect of

  2. Thermal deformation of cryogenically cooled silicon crystals under intense X-ray beams: measurement and finite-element predictions of the surface shape

    International Nuclear Information System (INIS)

    The shape of cryogenically cooled monochromator crystals deformed by the heat load of the X-ray beam is derived from rocking curve measurements at various vertical positions of a narrow-gap slit downstream from the monochromator. Experimentally, it is observed that the crystal shape changes from concave to convex when beam power increases. The observations are accurately modelled by finite-element analysis, showing an excellent quantitative agreement with experiments. X-ray crystal monochromators exposed to white-beam X-rays in third-generation synchrotron light sources are subject to thermal deformations that must be minimized using an adequate cooling system. A new approach was used to measure the crystal shape profile and slope of several cryogenically cooled (liquid nitrogen) silicon monochromators as a function of beam power in situ and under heat load. The method utilizes multiple angular scans across the Bragg peak (rocking curve) at various vertical positions of a narrow-gap slit downstream from the monochromator. When increasing the beam power, the surface of the liquid-nitrogen-cooled silicon crystal deforms from a concave shape at low heat load to a convex shape at high heat load, passing through an approximately flat shape at intermediate heat load. Finite-element analysis is used to calculate the crystal thermal deformations. The simulated crystal profiles and slopes are in excellent agreement with experiments. The parameters used in simulations, such as material properties, absorbed power distribution on the crystal and cooling boundary conditions, are described in detail as they are fundamental for obtaining accurate results

  3. Pro Spring Batch

    CERN Document Server

    Minella, Michael T

    2011-01-01

    Since its release, Spring Framework has transformed virtually every aspect of Java development including web applications, security, aspect-oriented programming, persistence, and messaging. Spring Batch, one of its newer additions, now brings the same familiar Spring idioms to batch processing. Spring Batch addresses the needs of any batch process, from the complex calculations performed in the biggest financial institutions to simple data migrations that occur with many software development projects. Pro Spring Batch is intended to answer three questions: *What? What is batch processing? What

  4. Properties of Bi-Te-Sb single crystals grown by the Czochralski method for thermoelectric cooling

    International Nuclear Information System (INIS)

    This paper reports on materials based on Bi, Te, Se, Sb and produced by pressing, extrusion or zone recrystallization that are used usually for the thermoelectric cooling. But by Czochralski method materials have been far less grown. Researches on growing of monocrystalline ingots on the base of combinations Bi-Se-Te and Bi-Sb-Te have been done. Thermoelectric material produced by the Czochralski method does not essentially differ from that one grown by zone recrystallization or Bridgman method

  5. Phase coexistence and transformations in field-cooled ternary piezoelectric single crystals near the morphotropic phase boundary

    International Nuclear Information System (INIS)

    Structural phase transformations in (100)-oriented Pb(In1/2Nb1/2)O3-Pb(Mg1/3Nb2/3)O3-PbTiO3 single crystals have been investigated by X-ray diffraction. A cubic (C) → tetragonal (T) → monoclinic-C (MC) transformation sequence was observed in the field-cooled condition. Two phase coexistence regions of C + T and T + MC were found. In addition to an increase in the C → T phase transition temperature and a decrease of the T → MC one, a broadening of the coexistence regions was also found with increasing field. This broadening can be explained by the presence of polar nano regions within the C, T, and MC phase regions

  6. Phase coexistence and transformations in field-cooled ternary piezoelectric single crystals near the morphotropic phase boundary

    Science.gov (United States)

    Luo, Chengtao; Wang, Yaojin; Wang, Zhiguang; Ge, Wenwei; Li, Jiefang; Luo, Haosu; Viehland, D.

    2014-12-01

    Structural phase transformations in (100)-oriented Pb(In1/2Nb1/2)O3-Pb(Mg1/3Nb2/3)O3-PbTiO3 single crystals have been investigated by X-ray diffraction. A cubic (C) → tetragonal (T) → monoclinic-C (MC) transformation sequence was observed in the field-cooled condition. Two phase coexistence regions of C + T and T + MC were found. In addition to an increase in the C → T phase transition temperature and a decrease of the T → MC one, a broadening of the coexistence regions was also found with increasing field. This broadening can be explained by the presence of polar nano regions within the C, T, and MC phase regions.

  7. Effect of titanium dioxide (TiO{sub 2}) on largely improving solar reflectance and cooling property of high density polyethylene (HDPE) by influencing its crystallization behavior

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Shichao; Zhang, Jun, E-mail: zhangjun@njtech.edu.cn

    2014-12-25

    Highlights: • HDPE/TiO{sub 2} composites have more perfect crystal structure. • Refractive index is the key factor affecting the final solar reflectance. • HDPE/TiO{sub 2} composites can achieve high solar reflectance. • The real cooling property is in accordance with solar reflectance. - Abstract: In this study, the different crystal forms of titanium dioxide (TiO{sub 2}) were added into high density polyethylene (HDPE) to fabricate cool material. Crystal structure, crystallization behavior, crystal morphology were investigated by wide angle X-ray diffraction (WAXD), differential scanning calorimetry (DSC) and polarized optical microscope (POM). Scanning electron microscope (SEM) was applied to observe dispersion of TiO{sub 2} particles in the HDPE matrix and the cross section morphology. The solar reflectance and actual cooling property were evaluated by UV–Vis–NIR spectrometer and a self-designed device. By adding TiO{sub 2} particles into HDPE matrix, the polymer chain could crystallize into more perfect and thermal stable lamella. The presence of TiO{sub 2} particles dramatically increased the number of nucleation site therefore decreased the crystal size. The subsequent solar reflectance was related to the degree of crystallinity, the spherulite size of HDPE, refractive index, and distribution of TiO{sub 2} particles in HDPE matrix. It was found the rutile TiO{sub 2} could largely improve the total solar reflectance from 28.2% to 51.1%. Finally, the temperature test showed that the composites had excellent cooling property, which was in accordance with solar reflectance result.

  8. Development of high-purity optical grade single-crystal CVD diamond for intracavity cooling

    Science.gov (United States)

    Bennett, Andrew M.; Wickham, Benjamin J.; Dhillon, Harpreet K.; Chen, Ying; Webster, Scott; Turri, Giorgio; Bass, Michael

    2014-02-01

    Microwave assisted chemical vapour deposited bulk diamond products have been used in a range of high power laser systems, due to low absorption across a range of wavelengths and exceptional thermal properties. However the application of polycrystalline products has frequently been limited to applications at longer wavelengths or thermal uses outside of the optical path due to the birefringence and scatter that are intrinsic properties of the polycrystalline materials. However, there are some solid state structures, including thin disc gain modules and amplifiers, that will gain significantly in terms of potential output powers if diamond could be used as a heat spreader in the optical path as well as a heat spreader on the rear surface of the disk. Therefore single crystal grades of diamond have been developed that overcome the limitations of the polycrystalline material, with low absorption, low scatter and low birefringence grades for demanding optical applications. We will present new data, characterising the performance of these materials across infra-red and visible wavelengths with absorption coefficient measured by laser calorimetry at a range of wavelengths from 1064 nm to 452 nm.

  9. Recurrent Batch Normalization

    OpenAIRE

    Cooijmans, Tim; Ballas, Nicolas; Laurent, César; Gülçehre, Çağlar; Courville, Aaron

    2016-01-01

    We propose a reparameterization of LSTM that brings the benefits of batch normalization to recurrent neural networks. Whereas previous works only apply batch normalization to the input-to-hidden transformation of RNNs, we demonstrate that it is both possible and beneficial to batch-normalize the hidden-to-hidden transition, thereby reducing internal covariate shift between time steps. We evaluate our proposal on various sequential problems such as sequence classification, language modeling an...

  10. Effects of micro electric current load during cooling of plant tissues on intracellular ice crystal formation behavior and pH.

    Science.gov (United States)

    Ninagawa, Takako; Kawamura, Yukio; Konishi, Tadashi; Narumi, Akira

    2016-08-01

    Cryopreservation techniques are expected to evolve further to preserve biomaterials and foods in a fresh state for extended periods of time. Long-term cryopreservation of living materials such as food and biological tissue is generally achieved by freezing; thus, intracellular freezing occurs. Intracellular freezing injures the cells and leads to cell death. Therefore, a dream cryopreservation technique would preserve the living materials without internal ice crystal formation at a temperature low enough to prevent bacterial activity. This study was performed to investigate the effect of micro electrical current loading during cooling as a new cryopreservation technique. The behavior of intracellular ice crystal formation in plant tissues with or without an electric current load was evaluated using the degree of supercooling, degree of cell deformation, and grain size and growing rate of intracellular ice crystal. Moreover, the transition of intracellular pH during plant tissue cooling with or without electric current loading was also examined using the fluorescence intensity ratio to comprehend cell activity at lower temperatures. The results indicated that micro electric current load did not only decrease the degree of cell deformation and grain size of intracellular ice crystal but also reduced the decline in intracellular pH due to temperature lowering, compared with tissues subjected to the same cooling rate without an electric current load. Thus, the effect of electric current load on cryopreservation and the potential of a new cryopreservation technique using electric current load were discussed based on these results. PMID:27343137

  11. Spring batch essentials

    CERN Document Server

    Rao, P Raja Malleswara

    2015-01-01

    If you are a Java developer with basic knowledge of Spring and some experience in the development of enterprise applications, and want to learn about batch application development in detail, then this book is ideal for you. This book will be perfect as your next step towards building simple yet powerful batch applications on a Java-based platform.

  12. Annihilation behaviour under electron irradiation of athermal ω-phase crystals formed by cooling at 131K in a β-Ti-Mo alloy

    International Nuclear Information System (INIS)

    Formation of athermal ω-phase crystals due to cooling to 131 K has been directly observed in a β-type Ti-15mass%Mo alloy. The athermal ω-phase crystals easily disappear by electron irradiation during the in-situ observation at 131 K. Incubation phenomenon of the annihilation is also recognized. The annihilation behaviour was investigated based on the dependence on electron irradiation conditions and incubation phenomena. It is concluded that the annihilation mechanism is concerned with interactive effects of temperature rise due to electron irradiation and collective oscillation resulted from inelastic scattering of electron beam.

  13. Effect of heat treatment and cooling conditions on the anisotropy parameters of drag thermo-electromotive force (TEMF) in neutron-doped silicon crystals

    International Nuclear Information System (INIS)

    The effect of high-temperature (1200 0C) annealing and quenching on the anisotropy parameters of the drag thermo-e.m.f. (M) in neutron-doped silicon crystals has been studied experimentally. Comparison is given of M in dependence on electron concentration in neutron-doped Si subjected to different annealing and cooling conditions and in phosphorus-doped n-type Si crystals. The dependences of piezoresistance and piezo-thermo-e.m.f. on uniaxial stress are also compared. Results are discussed on the basis of homogeneous distribution of dopants under neutron transmutation treatment

  14. Construcción de un Simulador Dinámico para Procesos de Cristalización por Lotes a Vacío Dynamic Simulator Construction for Vacuum Batch Crystallization Processes

    Directory of Open Access Journals (Sweden)

    Jesús Carrillo

    2008-01-01

    Full Text Available Se presenta un simulador dinámico para procesos de cristalización por lotes a vacío utilizando un modelo no lineal El modelo se basa en la ecuación de balance de población, balances de materia y energía para el interior del cristalizador, la ecuación de continuidad del vapor en la camisa de calentamiento y relaciones constitutivas. Utilizando la técnica de momentos de distribución de tamaño de cristal, la ecuación de balance de población se convierte en ecuaciones diferenciales. La construcción del simulador se realizó utilizando Visual Basic. Se propone un ejemplo y se comparan los resultados con otro simulador y con datos experimentales de un equipo piloto, obteniéndose resultados concordantes.A dynamic simulator for vacuum batch crystallization processes using a non-linear model is presented. The model is based on the equation of balance population, on mass and energy balances inside the crystallizer, on the steam continuity equation for the heating jacket and on constitutive relations. Using the technique of crystal size distribution moments, the equation of balance population is converted into a set of differential equations. The construction of simulator was done using Visual Basic. An example of its use is proposed comparing results with those of another simulator and with experimental information obtained in a pilot equipment pilot, obtaining similar results.

  15. Stacking with stochastic cooling

    International Nuclear Information System (INIS)

    Accumulation of large stacks of antiprotons or ions with the aid of stochastic cooling is more delicate than cooling a constant intensity beam. Basically the difficulty stems from the fact that the optimized gain and the cooling rate are inversely proportional to the number of particles 'seen' by the cooling system. Therefore, to maintain fast stacking, the newly injected batch has to be strongly 'protected' from the Schottky noise of the stack. Vice versa the stack has to be efficiently 'shielded' against the high gain cooling system for the injected beam. In the antiproton accumulators with stacking ratios up to 105 the problem is solved by radial separation of the injection and the stack orbits in a region of large dispersion. An array of several tapered cooling systems with a matched gain profile provides a continuous particle flux towards the high-density stack core. Shielding of the different systems from each other is obtained both through the spatial separation and via the revolution frequencies (filters). In the 'old AA', where the antiproton collection and stacking was done in one single ring, the injected beam was further shielded during cooling by means of a movable shutter. The complexity of these systems is very high. For more modest stacking ratios, one might use azimuthal rather than radial separation of stack and injected beam. Schematically half of the circumference would be used to accept and cool new beam and the remainder to house the stack. Fast gating is then required between the high gain cooling of the injected beam and the low gain stack cooling. RF-gymnastics are used to merge the pre-cooled batch with the stack, to re-create free space for the next injection, and to capture the new batch. This scheme is less demanding for the storage ring lattice, but at the expense of some reduction in stacking rate. The talk reviews the 'radial' separation schemes and also gives some considerations to the 'azimuthal' schemes

  16. Paramagnetic magnetization signals and curious metastable behaviour in field-cooled magnetization of a single crystal of superconductor 2H-NbSe2.

    Science.gov (United States)

    Kumar, Santosh; Tomy, C V; Balakrishnan, G; Paul, D McK; Grover, A K

    2015-07-29

    We present here some newer characteristics pertaining to paramagnetic Meissner effect like response in a single crystal of the low [Formula: see text] superconducting compound 2H-[Formula: see text] via a detailed study of effects of perturbation on the field-cooled magnetization response. In the temperature range, where an anomalous paramagnetic magnetization occurs, the field-cooled magnetization response is found to be highly metastable: it displays a curious tendency to switch randomly from a given paramagnetic value to a diamagnetic or to a different paramagnetic value, when the system is perturbed by an impulse of an externally applied ac magnetic field. The new facets revealed in a single crystal of 2H-[Formula: see text] surprisingly bear a marked resemblance with the characteristics of magnetization behaviour anticipated for the giant vortex states with multiple flux quanta ([Formula: see text], [Formula: see text], [Formula: see text]) predicted to occur in mesoscopic-sized superconducting specimen and possible transitions amongst such states. PMID:26154109

  17. Local thermal resonance control of GaInP photonic crystal membrane cavities using ambient gas cooling

    CERN Document Server

    Sokolov, Sergei; Yüce, Emre; Combrié, Sylvain; Lehoucq, Gaelle; De Rossi, Alfredo; Mosk, Allard P

    2015-01-01

    We perform a spatially dependent tuning of a GaInP photonic crystal cavity using a continuous wave violet laser. Local tuning is obtained by laser heating of the photonic crystal membrane. The cavity resonance shift is measured for different pump positions and for two ambient gases: helium and nitrogen. The use of high-conducting gas in combination with low-conducting semiconductor leads to a resonance control with a spatial resolution better than 4 microns.

  18. Polling with batch service

    OpenAIRE

    Boxma, O.; Van der Wal; Yechiali, U.

    2008-01-01

    This article considers a batch service polling system. We first study the case in which the server visits the queues cyclically, considering three different service regimes: gated, exhaustive, and globally gated. We subsequently analyze the case (the so-called "Israeli Queue") in which the server first visits the queue with the "oldest" customer. In both cases, queue lengths and waiting times are the main performance measures under consideration.

  19. Effect of batch and fed-batch growth modes on biofilm formation by Listeria monocytogenes at different temperatures

    OpenAIRE

    Rodrigues, Diana Alexandra Ferreira; Almeida, Marta A. S.; Teixeira, P.; Oliveira, Rosário; Azeredo, Joana

    2009-01-01

    The influence of Listeria monocytogenes (L. monocytogenes) biofilm formation feeding conditions (batch and fed-batch) at different temperatures on biofilm biomass and activity was determined. Biofilm biomass and cellular metabolic activity were assessed by Crystal Violet (CV) staining and 2,3-bis(2-methoxy-4-nitro-5-sulfophenyl)-2H-tetrazolium-5-carboxanilide inner salt (XTT) colorimetric method, respectively. Live/Dead staining was also performed in order to get microscopic visualization of ...

  20. High heat load performance of an inclined crystal monochromator with liquid gallium cooling on the CHESS-ANL undulator

    International Nuclear Information System (INIS)

    Recent results for the performance of a novel double crystal monochromator subjected to high heat loads on an APS prototype undulator at the Cornell High Energy Synchrotron Source (CHESS) are presented. The monochromator was designed to achieve symmetric diffraction from asymmetric planes to spread out the beam footprint thereby lowering the incident power density. Both crystals had (111) oriented surfaces and were arranged such that the beam was diffracted from the (11 bar 1) planes at 5 KeV. Rocking curves with minimal distortion were obtained at a ring electron current of 100 mA. This corresponded to 380 Watts total power and an average power density of 40 Watts/mm2 normal to the incident beam. These results are compared to data obtained from the same crystals in the standard geometry (diffracting planes parallel to surface). The footprint area in the inclined case was three times that of the standard case. We also obtained rocking curve data for the (333) reflection at 15 KeV for both standard and inclined cases, and these data also showed a minimal distortion only for the inclined case. In addition, thermal data were obtained via infrared pyrometry. Liquid gallium flow rates of up to 2 gallons per minute were investigated. The diffraction data revealed a dramatically improved performance for the inclined crystal case

  1. Batch-annealed dual-phase steel

    International Nuclear Information System (INIS)

    Dual-phase steel, consisting essentially of a ferrite matrix containing islands of martensite, is produced by batch annealing of hot or cold rolled steel having carbon below 0.2% and manganese below 2% and at least critical contents of copper (0.4%) and nickel (0.6%), with heat to the alpha plus gamma region, followed by slow cooling. This procedure is effective and controllable, and yields a dual-phase steel product that has high tensile strength with excellent elongation properties and that develops good yield strength upon moderate deformation

  2. Synthesis of single crystals of V2AlC phase by high-temperature solution growth and slow cooling technique

    International Nuclear Information System (INIS)

    Single-crystalline platelets of the nanolaminated V2AlC phase have been produced by high-temperature solution growth followed by a slow cooling process, with areas ranging from a few mm2 up to almost 1 cm2. Structural characterization confirms the single-crystalline character of the samples. The surface morphology of the V2AlC crystals is flat and devoid of dendrites. Well-defined steps and terraces indicate a step flow growth process. Emphasis is put on the mechanical cleavage of the samples which can be achieved in the basal plane thanks to the existence of the weakly bonded Al atomic planes. The cleavage surface exhibits terraces ending with a triangular shape and with a height equal to an integer number of half-lattice units

  3. Experimental investigation of the effects of compound angle holes on film cooling effectiveness and heat transfer performance using a transient liquid crystal thermometry technique

    Science.gov (United States)

    Seager, David J.; Liburdy, James A.

    1997-11-01

    To further understand the effect of both compound angle holes and hole shaping on film cooling, detailed heat transfer measurements were obtained using hue based thermochromic liquid crystal method. The data were analyzed to measure both the full surface adiabatic effectiveness and heat transfer coefficient. The compound angles that were evaluated consist of holes that were aligned 0 degrees, 45 degrees, 60 degrees and 90 degrees to the main cross flow direction. Hole shaping variations from the traditional cylindrical shaped hole include forward diffused and laterally diffused hole geometries. Geometric parameters that were selected were the length to diameter ratio of 3.0, and the inclination angle 35 degrees. A density ratio of 1.55 was obtained for all teste. For each set of conditions the blowing ratio was varied to be 0.88, 1.25, and 1.88. Adiabatic effectiveness was obtained using a steady state test, while an active heating surface was used to determine the heat transfer coefficient using a transient method. The experimental method provides a unique method of analyzing a three-temperature heat transfer problem by providing detailed surface transport properties. Based on these results for the different hole geometries at each blowing ratio conclusions are drawn relative to the effects of compound angle holes on the overall film cooling performance.

  4. Multi-dimensional population balance models of crystallization processes

    DEFF Research Database (Denmark)

    Meisler, Kresten Troelstrup; von Solms, Nicolas

    A generic and model-based framework for batch cooling crystallization operations has been extended to incorporate continuous and fed-batch processes. Modules for the framework have been developed, including a module for reactions, allowing the study of reactive crystallization within the framework....... A kinetic model library together with an ontology for knowledge representation has been developed, in which kinetic models and relations from the literature are stored along with the references and data. The model library connects to the generic modelling framework as well, as models can be...... parameters for the simulation can be found in the database. A procedure for parameter estimation has been illustrated based on experimental work. The identifiability of the models has been discussed in relation to parameter estimation using sensitivity analysis. Some important identifiability issues have...

  5. More on Combinatorial Batch Codes

    OpenAIRE

    Ruj, Sushmita; Roy, Bimal

    2008-01-01

    Paterson, Stinson and Wei \\cite{PSW} introduced Combinatorial batch codes, which are combinatorial description of Batch code. Batch codes were first presented by Ishai, Kushilevita, Ostrovsky and Sahai \\cite{IKOS} in STOC'04. In this paper we answer some of the questions put forward by Paterson, Stinson and Wei and give some results for the general case $t>1$ which were not studied by the authors.

  6. Stacking with stochastic cooling

    Energy Technology Data Exchange (ETDEWEB)

    Caspers, Fritz E-mail: Fritz.Caspers@cern.ch; Moehl, Dieter

    2004-10-11

    Accumulation of large stacks of antiprotons or ions with the aid of stochastic cooling is more delicate than cooling a constant intensity beam. Basically the difficulty stems from the fact that the optimized gain and the cooling rate are inversely proportional to the number of particles 'seen' by the cooling system. Therefore, to maintain fast stacking, the newly injected batch has to be strongly 'protected' from the Schottky noise of the stack. Vice versa the stack has to be efficiently 'shielded' against the high gain cooling system for the injected beam. In the antiproton accumulators with stacking ratios up to 10{sup 5} the problem is solved by radial separation of the injection and the stack orbits in a region of large dispersion. An array of several tapered cooling systems with a matched gain profile provides a continuous particle flux towards the high-density stack core. Shielding of the different systems from each other is obtained both through the spatial separation and via the revolution frequencies (filters). In the 'old AA', where the antiproton collection and stacking was done in one single ring, the injected beam was further shielded during cooling by means of a movable shutter. The complexity of these systems is very high. For more modest stacking ratios, one might use azimuthal rather than radial separation of stack and injected beam. Schematically half of the circumference would be used to accept and cool new beam and the remainder to house the stack. Fast gating is then required between the high gain cooling of the injected beam and the low gain stack cooling. RF-gymnastics are used to merge the pre-cooled batch with the stack, to re-create free space for the next injection, and to capture the new batch. This scheme is less demanding for the storage ring lattice, but at the expense of some reduction in stacking rate. The talk reviews the 'radial' separation schemes and also gives some

  7. Development of a neutron irradiation device with a cooled crystal filter: Radiation physical properties and applications in in vivo irradiations

    International Nuclear Information System (INIS)

    The radiation-physical and geometrical properties of a neutron-beam, collimated with a Bi-crystal filter were investigated at the reactor BER II. The influence of the crystal temperature as well as the actions of a reflector and a collimator on neutron flux-density and neutron field of the thermal neutrons were investigated. The dose contributions of the thermal, epithermal and fast neutrons as well as γ-radiation was determined by activation of the sample respective with TLD-measurements. The influence of irradiation and measurement geometry on the sensitivity and detection probability was investigated by means of phantom irradiations. The method prooved to be suitable, to detect changes of the Ca-content in a rat hind leg by about 10%. In investigations on animal groups of about 10 animals a threshold of detectability for changes of the ca-content is to be expected by about 4%. In a further group experiment it was found, that even in the case of multiple radiation the procedure of irradiation and measurement was not followed by a significant change in the Ca-content of the hind legs of the testing animals. (orig.)

  8. Column and Batch Experiments

    Directory of Open Access Journals (Sweden)

    Jorge L. Gardea-Torresdey

    2005-01-01

    Full Text Available Batch and column experiments were performed to determine the Cu(II binding capacity of silica-immobilized humin biomass. For column studies, 500 bed volumes of a 0.1 mM Cu(II solution were passed through humin packed columns at the flow rates of 1, 1.5, 2, and 3 mL/min. The biopolymer showed an average Cu binding capacity of 12 ± 1.5 mg/g and a Cu recovery of about 96.5 % ± 1.5. The breakthrough points for Cu(II alone were approximately 420, 390, 385, and 300 bed volumes for the flow rates of 1, 1.5, 2 and 3 mL/min, respectively. The interference studies demonstrated that at low concentrations, the hard cations Ca(II and Mg(II did not seem to represent a major interference on Cu(II binding to the humin biopolymer. The selectivity showed by this biopolymer was Cu(II>Ca(II>Mg(II. On the other hand, batch experiments showed that Ca(II + Mg(II at 100mM each reduced the Cu(II binding to 73 %. However, 1000 mM concentrations of Ca(II and Mg(II, separately and in mixture, reduced the Cu(II binding to 47 %, 44 % and 31 %, respectively. The results of this study showed that immobilized humin in a silica matrix could represent an inexpensive bio-source for Cu removal from contaminated water, even in the presence of low concentrations of the hard cations Ca(II and Mg(II.

  9. Heterogeneous batch structures in throughput scheduling

    OpenAIRE

    Weeda, P.J.

    1993-01-01

    Recently a few papers appeared on throughput scheduling, dealing with the relationship between batch structure and process structure in discrete batch production, while maximizing time-constrained throughput. Results have been concentrated on the class of homogeneous batch structures, i.e. batch structures with equal batch sizes for each process per cycle. In this paper heterogeneous batch structures are considered. By numerical examples, it is shown that heterogeneous batch structures can ou...

  10. Microalgal TAG production strategies: why batch beats repeated-batch

    OpenAIRE

    Benvenuti, G.; Lamers, P.P.; Breuer, G.; Bosma, R.; Cerar, Ana; Wijffels, R.H.; Barbosa, M. J.

    2016-01-01

    Background For a commercially feasible microalgal triglyceride (TAG) production, high TAG productivities are required. The operational strategy affects TAG productivity but a systematic comparison between different strategies is lacking. For this, physiological responses of Nannochloropsis sp. to nitrogen (N) starvation and N-rich medium replenishment were studied in lab-scale batch and repeated-batch (part of the culture is periodically harvested and N-rich medium is re-supplied) cultivation...

  11. Data-driven batch schuduling

    Energy Technology Data Exchange (ETDEWEB)

    Bent, John [Los Alamos National Laboratory; Denehy, Tim [GOOGLE; Arpaci - Dusseau, Remzi [UNIV OF WISCONSIN; Livny, Miron [UNIV OF WISCONSIN; Arpaci - Dusseau, Andrea C [NON LANL

    2009-01-01

    In this paper, we develop data-driven strategies for batch computing schedulers. Current CPU-centric batch schedulers ignore the data needs within workloads and execute them by linking them transparently and directly to their needed data. When scheduled on remote computational resources, this elegant solution of direct data access can incur an order of magnitude performance penalty for data-intensive workloads. Adding data-awareness to batch schedulers allows a careful coordination of data and CPU allocation thereby reducing the cost of remote execution. We offer here new techniques by which batch schedulers can become data-driven. Such systems can use our analytical predictive models to select one of the four data-driven scheduling policies that we have created. Through simulation, we demonstrate the accuracy of our predictive models and show how they can reduce time to completion for some workloads by as much as 80%.

  12. Cristalização e taxa crítica de resfriamento para vitrificação do poli(sebacato de decametileno) Crystallization and critical cooling rate to vitrify poly(decamethylene sebacate)

    OpenAIRE

    Luciana Maria Guimarães; Edgar Dutra Zanotto

    2003-01-01

    We synthesized Poly(decamethylene sebacate) - P10MS - and studied its overall crystallization rates in a range of temperatures using Differential Scanning Calorimetry in isothermal conditions, which enabled us to identify the crystallization mechanism by means of the Johnson-Mehl-Avrami-Kolmogorov equation. The critical cooling rate (Rc) to vitrify the P10MS was determined using a non-isothermal method proposed by Barandiarán & Colmenero (BC). The value of Rc is around 50-250 K/s, which confi...

  13. Batch compositions for cordierite ceramics

    Science.gov (United States)

    Hickman, David L.

    1994-07-26

    Ceramic products consisting principally of cordierite and a method for making them are provided, the method employing batches comprising a mineral component and a chemical component, the mineral component comprising clay and talc and the chemical component consisting essentially of a combination of the powdered oxides, hydroxides, or hydrous oxides of magnesium, aluminum and silicon. Ceramics made by extrusion and firing of the batches can exhibit low porosity, high strength and low thermal expansion coefficients.

  14. Stacking with Stochastic Cooling

    CERN Document Server

    Caspers, Friedhelm

    2004-01-01

    Accumulation of large stacks of antiprotons or ions with the aid of stochastic cooling is more delicate than cooling a constant intensity beam. Basically the difficulty stems from the fact that the optimized gain and the cooling rate are inversely proportional to the number of particles seen by the cooling system. Therefore, to maintain fast stacking, the newly injected batch has to be strongly protected from the Schottky noise of the stack. Vice versa the stack has to be efficiently shielded against the high gain cooling system for the injected beam. In the antiproton accumulators with stacking ratios up to 105, the problem is solved by radial separation of the injection and the stack orbits in a region of large dispersion. An array of several tapered cooling systems with a matched gain profile provides a continuous particle flux towards the high-density stack core. Shielding of the different systems from each other is obtained both through the spatial separation and via the revolution frequencies (filters)....

  15. BatchJobs and BatchExperiments: Abstraction Mechanisms for Using R in Batch Environments

    Directory of Open Access Journals (Sweden)

    Bernd Bischl

    2015-03-01

    Full Text Available Empirical analysis of statistical algorithms often demands time-consuming experiments. We present two R packages which greatly simplify working in batch computing environments. The package BatchJobs implements the basic objects and procedures to control any batch cluster from within R. It is structured around cluster versions of the well-known higher order functions Map, Reduce and Filter from functional programming. Computations are performed asynchronously and all job states are persistently stored in a database, which can be queried at any point in time. The second package, BatchExperiments, is tailored for the still very general scenario of analyzing arbitrary algorithms on problem instances. It extends package BatchJobs by letting the user define an array of jobs of the kind apply algorithm A to problem instance P and store results. It is possible to associate statistical designs with parameters of problems and algorithms and therefore to systematically study their influence on the results. The packages main features are: (a Convenient usage: All relevant batch system operations are either handled internally or mapped to simple R functions. (b Portability: Both packages use a clear and well-defined interface to the batch system which makes them applicable in most high-performance computing environments. (c Reproducibility: Every computational part has an associated seed to ensure reproducibility even when the underlying batch system changes. (d Abstraction and good software design: The code layers for algorithms, experiment definitions and execution are cleanly separated and enable the writing of readable and maintainable code.

  16. Applications of thin-film sandwich crystallization platforms.

    Science.gov (United States)

    Axford, Danny; Aller, Pierre; Sanchez-Weatherby, Juan; Sandy, James

    2016-04-01

    Examples are shown of protein crystallization in, and data collection from, solutions sandwiched between thin polymer films using vapour-diffusion and batch methods. The crystallization platform is optimal for both visualization and in situ data collection, with the need for traditional harvesting being eliminated. In wells constructed from the thinnest plastic and with a minimum of aqueous liquid, flash-cooling to 100 K is possible without significant ice formation and without any degradation in crystal quality. The approach is simple; it utilizes low-cost consumables but yields high-quality data with minimal sample intervention and, with the very low levels of background X-ray scatter that are observed, is optimal for microcrystals. PMID:27050266

  17. Stochastic Cooling

    Energy Technology Data Exchange (ETDEWEB)

    Blaskiewicz, M.

    2011-01-01

    Stochastic Cooling was invented by Simon van der Meer and was demonstrated at the CERN ISR and ICE (Initial Cooling Experiment). Operational systems were developed at Fermilab and CERN. A complete theory of cooling of unbunched beams was developed, and was applied at CERN and Fermilab. Several new and existing rings employ coasting beam cooling. Bunched beam cooling was demonstrated in ICE and has been observed in several rings designed for coasting beam cooling. High energy bunched beams have proven more difficult. Signal suppression was achieved in the Tevatron, though operational cooling was not pursued at Fermilab. Longitudinal cooling was achieved in the RHIC collider. More recently a vertical cooling system in RHIC cooled both transverse dimensions via betatron coupling.

  18. Physicochemical Characteristics of Transferon™ Batches

    Directory of Open Access Journals (Sweden)

    Emilio Medina-Rivero

    2016-01-01

    Full Text Available Transferon, a biotherapeutic agent that has been used for the past 2 decades for diseases with an inflammatory component, has been approved by regulatory authorities in Mexico (COFEPRIS for the treatment of patients with herpes infection. The active pharmaceutical ingredient (API of Transferon is based on polydispersion of peptides that have been extracted from lysed human leukocytes by a dialysis process and a subsequent ultrafiltration step to select molecules below 10 kDa. To physicochemically characterize the drug product, we developed chromatographic methods and an SDS-PAGE approach to analyze the composition and the overall variability of Transferon. Reversed-phase chromatographic profiles of peptide populations demonstrated batch-to-batch consistency from 10 representative batches that harbored 4 primary peaks with a relative standard deviation (RSD of less than 7%. Aminogram profiles exhibited 17 proteinogenic amino acids and showed that glycine was the most abundant amino acid, with a relative content of approximately 18%. Further, based on their electrophoretic migration, the peptide populations exhibited a molecular mass of about 10 kDa. Finally, we determined the Transferon fingerprint using a mass spectrometry tool. Because each batch was produced from independent pooled buffy coat samples from healthy donors, supplied by a local blood bank, our results support the consistency of the production of Transferon and reveal its peptide identity with regard to its physicochemical attributes.

  19. NDA BATCH 2002-02

    Energy Technology Data Exchange (ETDEWEB)

    Lawrence Livermore National Laboratory

    2009-12-09

    QC sample results (daily background checks, 20-gram and 100-gram SGS drum checks) were within acceptable criteria established by WIPP's Quality Assurance Objectives for TRU Waste Characterization. Replicate runs were performed on 5 drums with IDs LL85101099TRU, LL85801147TRU, LL85801109TRU, LL85300999TRU and LL85500979TRU. All replicate measurement results are identical at the 95% confidence level as established by WIPP criteria. Note that the batch covered 5 weeks of SGS measurements from 23-Jan-2002 through 22-Feb-2002. Data packet for SGS Batch 2002-02 generated using gamma spectroscopy with the Pu Facility SGS unit is technically reasonable. All QC samples are in compliance with established control limits. The batch data packet has been reviewed for correctness, completeness, consistency and compliance with WIPP's Quality Assurance Objectives and determined to be acceptable. An Expert Review was performed on the data packet between 28-Feb-02 and 09-Jul-02 to check for potential U-235, Np-237 and Am-241 interferences and address drum cases where specific scan segments showed Se gamma ray transmissions for the 136-keV gamma to be below 0.1 %. Two drums in the batch showed Pu-238 at a relative mass ratio more than 2% of all the Pu isotopes.

  20. Simulated Batch Production of Penicillin

    Science.gov (United States)

    Whitaker, A.; Walker, J. D.

    1973-01-01

    Describes a program in applied biology in which the simulation of the production of penicillin in a batch fermentor is used as a teaching technique to give students experience before handling a genuine industrial fermentation process. Details are given for the calculation of minimum production cost. (JR)

  1. Physicochemical Characteristics of Transferon™ Batches

    Science.gov (United States)

    Pérez-Sánchez, Gilberto; Favari, Liliana; Estrada-Parra, Sergio

    2016-01-01

    Transferon, a biotherapeutic agent that has been used for the past 2 decades for diseases with an inflammatory component, has been approved by regulatory authorities in Mexico (COFEPRIS) for the treatment of patients with herpes infection. The active pharmaceutical ingredient (API) of Transferon is based on polydispersion of peptides that have been extracted from lysed human leukocytes by a dialysis process and a subsequent ultrafiltration step to select molecules below 10 kDa. To physicochemically characterize the drug product, we developed chromatographic methods and an SDS-PAGE approach to analyze the composition and the overall variability of Transferon. Reversed-phase chromatographic profiles of peptide populations demonstrated batch-to-batch consistency from 10 representative batches that harbored 4 primary peaks with a relative standard deviation (RSD) of less than 7%. Aminogram profiles exhibited 17 proteinogenic amino acids and showed that glycine was the most abundant amino acid, with a relative content of approximately 18%. Further, based on their electrophoretic migration, the peptide populations exhibited a molecular mass of about 10 kDa. Finally, we determined the Transferon fingerprint using a mass spectrometry tool. Because each batch was produced from independent pooled buffy coat samples from healthy donors, supplied by a local blood bank, our results support the consistency of the production of Transferon and reveal its peptide identity with regard to its physicochemical attributes. PMID:27525277

  2. NGBAuth - Next Generation Batch Authentication for long running batch jobs.

    CERN Document Server

    Juto, Zakarias

    2015-01-01

    This document describes the prototyping of a new solution for the CERN batch authentication of long running jobs. While the job submission requires valid user credentials, these have to be renewed due to long queuing and execution times. Described within is a new system which will guarantee a similar level of security as the old LSFAuth while simplifying the implementation and the overall architecture. The new system is being built on solid, streamlined and tested components (notably OpenSSL) and a priority has been to make it more generic in order to facilitate the evolution of the current system such as for the expected migration from LSF to Condor as backend batch system.

  3. Use of focused beam reflectance measurement (FBRM) and process video imaging (PVI) in a modified mixed suspension mixed product removal (MSMPR) cooling crystallizer

    Science.gov (United States)

    Kougoulos, E.; Jones, A. G.; Jennings, K. H.; Wood-Kaczmar, M. W.

    2005-01-01

    The FBRM instrument is a 'powerful' tool developed by Lasentec as an 'in situ' particle monitoring technique for in-line real-time measurement of particle size. This technique was successfully used to monitor steady-state operation in a modified MSMPR crystallizer. The FBRM technique was also used to estimate crystallization kinetics. The FBRM particle size measurements were complimented by an in-line process video imaging (PVI) system developed ' in-house' (Microscopy and Microanalysis, 6 (Suppl. 2) (2000) 996-997), to visualize habit and crystal behaviour within an MSMPR crystallizer. A comparison of the steady-state crystal size distributions measured by low angle light scattering (LALLS) and FBRM was made, showing poor sensitivity of the FBRM technique to particles of less than 1 μm hence the technique was not suitable for the measurement of crystallization kinetics for this organic system.

  4. Effect of rhodium doping on the growth and characteristics of BaTiO 3 single crystals grown by step-cooling method

    Science.gov (United States)

    Madeswaran, S.; Giridharan, N. V.; Varatharajan, R.; Ravi, G.; Jayavel, R.

    2004-06-01

    Single crystals of Rh-doped BaTiO 3 have been grown by high-temperature solution growth technique. The dopant has significant effect on the growth parameters and crystal properties. Bulk single crystals of dimensions 5×5×4 mm 3 have been grown with optimized growth conditions. Layer growth and vein-like structure patterns, indicative of 2D-nucleation mechanism, have been observed on the grown crystals. The dopant level in the grown crystals was estimated by EDX analysis. The crystals possess tetragonal structure and the tetragonality decreases for higher dopant concentration. Rh doping in BaTiO 3 leads to decrease in dielectric constant and Curie temperature ( Tc) values.

  5. NDA Batch 2002-13

    Energy Technology Data Exchange (ETDEWEB)

    Hollister, R

    2009-09-17

    QC sample results (daily background check drum and 100-gram SGS check drum) were within acceptance criteria established by WIPP's Quality Assurance Objectives for TRU Waste Characterization. Replicate runs were performed on drum LL85501243TRU. Replicate measurement results are identical at the 95% confidence level as established by WIPP criteria. HWM NCAR No. 02-1000168 issued on 17-Oct-2002 regarding a partially dislodged Cd sheet filter on the HPGe coaxial detector. This physical geometry occurred on 01-Oct-2002 and was not corrected until 10-Oct-2002, during which period is inclusive of the present batch run of drums. Per discussions among the Independent Technical Reviewer, Expert Reviewer and the Technical QA Supervisor, as well as in consultation with John Fleissner, Technical Point of Contact from Canberra, the analytical results are technically reliable. All QC standard runs during this period were in control. Data packet for SGS Batch 2002-13 generated using passive gamma-ray spectroscopy with the Pu Facility SGS unit is technically reasonable. All QC samples are in compliance with establiShed control limits. The batch data packet has been reviewed for correctness, completeness, consistency and compliance with WIPP's Quality Assurance Objectives and determined to be acceptable.

  6. Optimal online-list batch scheduling

    OpenAIRE

    Paulus, JJ Jacob Jan; Ye, Deshi; Zhang, G.

    2008-01-01

    We consider the online-list batch scheduling problem. Jobs arrive one by one and have to be assigned upon arrival to a scheduled batch such that the makespan is minimized. Each batch can accommodate up to B jobs. We give a complete classification of the tractability of this online problem.

  7. Electronic Cooling in Graphene

    OpenAIRE

    Bistritzer, R.; Macdonald, A. H.

    2009-01-01

    Energy transfer to acoustic phonons is the dominant low-temperature cooling channel of electrons in a crystal.For cold neutral graphene we find that the weak cooling power of its acoustical modes relative to the heat capacity of the system leads to a power law decay of the electronic temperature when far from equilibrium. For heavily doped graphene a high electronic temperature is shown to initially decrease linearly with time at a rate proportional to n^(3/2) with n being the electronic dens...

  8. Impact of cooling condition on the crystal structure and surface quality of preferred c-axis-oriented AIN films for SAW devices

    Institute of Scientific and Technical Information of China (English)

    ZHANG Geng-yu; YANG Bao-he; ZHAO Jian; LI Cui-ping; LI Ming-ji

    2011-01-01

    AIN films with preferred c-axis orientation are deposited on Si substrates using the radio frequency (RF) magnetron sputtering method. The post-processing is carried out under the cooling conditions including high vacuum, low vacuum under deposition gas ambient and low vacuum under dynamic N2 ambient. Structures and morphologies of the films are analyzed by X-ray diffraction (XRD) and atomic force microscopy (AFM). The hardness and Young's modulus are investigated by the nanoindenter. The experimental results indicate that the (100) and (110) peak intensities decrease in the XRD spectra and the root-mean-square of roughness (Rrms) of the film decreases gradually with the increase of the cooling rate. The maximum values of the hardness and Young's modulus are obtained by cooling in low vacuum under deposition gas ambient. The reason for orientation variation of the films is explained from the perspective of the Al-N bond formation.

  9. Influence of batch or fed-batch growth on Staphylococcus epidermidis biofilm formation

    OpenAIRE

    Cerca, Nuno; Pier, Gerald B.; Vilanova, Manuel; Oliveira, Rosário; Azeredo, Joana

    2004-01-01

    Aims: To make a quantitative evaluation of the differences in biofilm formation by Staphylococcus epidermidis using batch and fed-batch growth systems and to correlate this with production of the major biofilm polysaccharide, poly-N-acetyl glucosamine (PNAG). Methods and Results: Dry weight measurements of biofilms formed in batch and fed-batch conditions were compared with haemagglutination titres, which measure the amount of PNAG produced. Strains grown in batch systems devel...

  10. Combinatorial Batch Codes with Redundancy

    OpenAIRE

    Jung, Jiyoon; Mummert, Carl; Niese, Elizabeth; Schroeder, Michael w.

    2015-01-01

    A combinatorial batch code with redundancy $r$ and parameters $(n,k,m,t)$ can be represented as a system $C$ of $m$ (not necessarily distinct) subsets of an underlying $n$-element set $F$, so that each $k$-subset of $F$ can be covered by every $(m-r)$-subset $K$ of $C$ while taking no more than $t$ elements of $F$ with each set in $K$. The sum of the cardinalities of the sets in $C$ is the weight of the code. We focus on the case $t =1$, and determine the minimal weight for several ranges of ...

  11. Spray cooling

    International Nuclear Information System (INIS)

    Spray cooling - using water spraying in air - is surveyed as a possible system for make-up (peak clipping in open circuit) or major cooling (in closed circuit) of the cooling water of the condensers in thermal power plants. Indications are given on the experiments made in France and the systems recently developed in USA, questions relating to performance, cost and environmental effects of spray devices are then dealt with

  12. High density protein crystal growth

    Science.gov (United States)

    Rouleau, Robyn (Inventor); Delucas, Lawrence (Inventor); Hedden, Douglas Keith (Inventor)

    2004-01-01

    A protein crystal growth assembly including a crystal growth cell and further including a cell body having a top side and a bottom side and a first aperture defined therethrough, the cell body having opposing first and second sides and a second aperture defined therethrough. A cell barrel is disposed within the cell body, the cell barrel defining a cavity alignable with the first aperture of the cell body, the cell barrel being rotatable within the second aperture. A reservoir is coupled to the bottom side of the cell body and a cap having a top side is disposed on the top side of the cell body. The protein crystal growth assembly may be employed in methods including vapor diffusion crystallization, liquid to liquid crystallization, batch crystallization, and temperature induction batch mode crystallization.

  13. Cool contrails

    OpenAIRE

    U. Schumann

    2012-01-01

    Contrails are cirrus clouds which warm or cool the Earth depending on flight route and weather. Hence, the climate impact of aviation can be minimised by avoiding warming contrails and allowing for cooling contrails by proper weather dependent route selection. This article summarises recent research results on this topic.

  14. Batch processing: definition and event log identification

    OpenAIRE

    Martin, Niels,; SWENNEN, Marijke; Depaire, Benoit; Jans, Mieke; CARIS, An; Vanhoof, Koen

    2015-01-01

    A resource typically executes a particular activity on a series of cases. When a resource performs an activity on several cases simultaneously, (quasi-) sequentially or concurrently, this is referred to as batch processing. Given its influence on process performance, batch processing needs to be taken into account when modeling business processes for performance evaluation purposes. This paper suggests event logs as an information source to gain insight in batching behavior. It marks a first ...

  15. Batch process design: an overview from control

    OpenAIRE

    Zuluaga Bedoya, Christian Camilo

    2015-01-01

    Abstract: batch process design: an overview from control In this work, the topic of batch process design is addressed, through an analysis of the phenomenological-based model and using set-theoretic methods to deduce process constraints and parametric effects in state controllability. A review of literature is presented about characterization of batch process from point of view of design problem. Furthermore simultaneous process and control design is also reviewed, considering the main contri...

  16. Direct transmission electron microscopy observations of martensitic transformations in Ni-rich NiTi single crystals during in situ cooling and straining

    Czech Academy of Sciences Publication Activity Database

    Kröger, A.; Dziaszyk, S.; Frenzel, J.; Somsen, Ch.; Dlouhý, Antonín; Eggeler, G.

    2008-01-01

    Roč. 481, Sp. Iss. (2008), s. 452-456. ISSN 0921-5093. [ESOMAT 2006. Bochum, 10.09.2006-15.09.2006] Institutional research plan: CEZ:AV0Z20410507 Keywords : In situ TEM * NiTi single crystal * Martensitic transformations Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 1.806, year: 2008

  17. Plutonium immobilization feed batching system concept report

    International Nuclear Information System (INIS)

    The Plutonium Immobilization Facility will encapsulate plutonium in ceramic pucks and seal the pucks inside welded cans. Remote equipment will place these cans in magazines and the magazines in a Defense Waste Processing Facility (DWPF) canister. The DWPF will fill the canister with high level waste glass for permanent storage. Feed batching is one of the first process steps involved with first stage plutonium immobilization. It will blend plutonium oxide powder before it is combined with other materials to make pucks. This report discusses the Plutonium Immobilization feed batching process preliminary concept, batch splitting concepts, and includes a process block diagram, concept descriptions, a preliminary equipment list, and feed batching development areas

  18. Sympathetic cooling of $^4$He$^+$ ions in a radiofrequency trap

    OpenAIRE

    Roth, B.(Institut für Experimentalphysik I, Ruhr–Universität Bochum, Bochum, 44780, Germany); Fröhlich, U.; S.SCHILLER

    2004-01-01

    We have generated Coulomb crystals of ultracold $^4$He$^+$ ions in a linear radiofrequency trap, by sympathetic cooling via laser--cooled $^9$Be$^+$. Stable crystals containing up to 150 localized He$^+$ ions at $\\sim$20 mK were obtained. Ensembles or single ultracold He$^+$ ions open up interesting perspectives for performing precision tests of QED and measurements of nuclear radii. The present work also indicates the feasibility of cooling and crystallizing highly charged atomic ions using ...

  19. Supervision of Fed-Batch Fermentations

    DEFF Research Database (Denmark)

    Gregersen, Lars; Jørgensen, Sten Bay

    1999-01-01

    Process faults may be detected on-line using existing measurements based upon modelling that is entirely data driven. A multivariate statistical model is developed and used for fault diagnosis of an industrial fed-batch fermentation process. Data from several (25) batches are used to develop a mo...

  20. Asymptotic Modelling of Crystallisation in Two Layers Systems. Application to Methane Hydrate Formation in Batch Reactor.

    OpenAIRE

    Cournil, Michel; Herri, Jean-Michel

    2002-01-01

    This paper proposes to re-visit the problem of gas-liquid crystallization in the framework of a two-layer model and with the help of data coming from experiments on methane hydrate crystallization in a semi-batch reactor. Preliminary quantitative discussion of the order of magnitude of different effects makes possible realistic simplifications in the theoretical models. In particular, the role of the interfacial film is clearly defined. As previous authors did, we use a formulation in terms o...

  1. Operation of a Batch Stripping Distillation Column

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    A stripping batch distillation column is preferred when the amount of the light component in the feed is small and the products are to be recovered at high purity. The operation modes of a batch stripping are believed to be the same as those of a rectifier. However, the control system of a stripper is different. In this paper, we explore three different control methods with Hysys (Hyprotech Ltd. 1997) for a batch stripper. The main difference is the control scheme for reboiler liquid level: (a) controlled by reflux flow; (b) controlled by reboiler heat duty; (c) controlled by bottom product flow. The main characteristics of operating a batch stripper with different control scheme are presented in this paper. Guidelines are provided for the startup of a batch stripper, the effects of somecontrol tuning parameters on the column performance are discussed.

  2. Analysis and modelling of the energy consumption of chemical batch plants

    Energy Technology Data Exchange (ETDEWEB)

    Bieler, P.S.

    2004-07-01

    This report for the Swiss Federal Office of Energy (SFOE) describes two different approaches for the energy analysis and modelling of chemical batch plants. A top-down model consisting of a linear equation based on the specific energy consumption per ton of production output and the base consumption of the plant is postulated. The model is shown to be applicable to single and multi-product batches for batch plants with constant production mix and multi-purpose batch plants in which only similar chemicals are produced. For multipurpose batch plants with highly varying production processes and changing production mix, the top-down model produced inaccurate results. A bottom-up model is postulated for such plants. The results obtained are discussed that show that the electricity consumption for infrastructure equipment was significant and responsible for about 50% of total electricity consumption. The specific energy consumption for the different buildings was related to the degree of automation and the production processes. Analyses of the results of modelling are presented. More detailed analyses of the energy consumption of this apparatus group show that about 30 to 40% of steam energy is lost and thus a large potential for optimisation exists. Various potentials for making savings, ranging from elimination of reflux conditions to the development of a new heating/cooling-system for a generic batch reactor, are identified.

  3. BATCH systémy

    OpenAIRE

    Beránek, Jakub

    2013-01-01

    Bakalářská práce je zaměřena na dávkové systémy. V teoretické části je stručně popsána filozofie dávkových systémů a norma ANSI/ISA 88, která je významným dokumentem v dávkovém řízení. V další části je popsáno několik programů pro řízení dávkových procesů z české i celosvětové produkce. Poslední část obsahuje přípravu, návrh a realizaci laboratorní úlohy pro řízení modelového dávkového procesu s použitím modulu COMES Batch.

  4. Batch Scheduling a Fresh Approach

    Science.gov (United States)

    Cardo, Nicholas P.; Woodrow, Thomas (Technical Monitor)

    1994-01-01

    The Network Queueing System (NQS) was designed to schedule jobs based on limits within queues. As systems obtain more memory, the number of queues increased to take advantage of the added memory resource. The problem now becomes too many queues. Having a large number of queues provides users with the capability to gain an unfair advantage over other users by tailoring their job to fit in an empty queue. Additionally, the large number of queues becomes confusing to the user community. The High Speed Processors group at the Numerical Aerodynamics Simulation (NAS) Facility at NASA Ames Research Center developed a new approach to batch job scheduling. This new method reduces the number of queues required by eliminating the need for queues based on resource limits. The scheduler examines each request for necessary resources before initiating the job. Also additional user limits at the complex level were added to provide a fairness to all users. Additional tools which include user job reordering are under development to work with the new scheduler. This paper discusses the objectives, design and implementation results of this new scheduler

  5. 27 CFR 19.748 - Dump/batch records.

    Science.gov (United States)

    2010-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2010-04-01 2010-04-01 false Dump/batch records. 19.748.../batch records. (a) Format of dump/batch records. Proprietor's dump/batch records shall contain, as... ingredients used; (10) Formula number; (11) Quantity of ingredients used in the batch that have...

  6. Flux free growth of large FeSe1/2Te1/2 superconducting single crystals by an easy high temperature melt and slow cooling method

    OpenAIRE

    Maheshwari, P. K.; Rajveer Jha; Bhasker Gahtori; Awana, V. P. S.

    2015-01-01

    We report successful growth of flux free large single crystals of superconducting FeSe1/2Te1/2 with typical dimensions of up to few cm. The AC and DC magnetic measurements revealed the superconducting transition temperature (Tc) value of around 11.5K and the isothermal MH showed typical type-II superconducting behavior. The lower critical field (Hc1) being estimated by measuring the low field isothermal magnetization in superconducting regime is found to be above 200Oe at 0K. The temperature ...

  7. Batch and Fed-Batch Fermentation System on Ethanol Production from Whey using Kluyveromyces marxianus

    Directory of Open Access Journals (Sweden)

    H Hadiyanto

    2013-10-01

    Full Text Available Nowadays reserve of fossil fuel has gradually depleted. This condition forces many researchers to  find energy alternatives which is renewable and sustainable in the future. Ethanol derived from cheese industrial waste (whey using fermentation process can be a new perspective in order to secure both energy and environment. The aim of this study was  to compare the operation modes (batch and fed-batch of fermentation system on ethanol production from whey using Kluyveromyces marxianus. The result showed that the fermentation process for ethanol production by fed-batch system was higher at some point of parameters compared with batch system. Growth rate and ethanol yield (YP/S of fed-batch fermentation were 0.122/h and 0.21 gP/gS respectively; growth rate and ethanol yield (YP/S of batch fermentation were 0.107/h, and 0.12 g ethanol/g substrate, respectively. Based on the data of biomass and ethanol concentrations, the fermentation process for ethanol production by fed-batch system were higher at some point of parameters compared to batch system. Periodic substrate addition performed on fed-batch system leads the yeast growth in low substrate concentrations and consequently  increasing their activity and ethanol productivity. Keywords: batch; ethanol; fed-batch; fermentation;Kluyveromyces marxianus, whey

  8. Cooling Vest

    Science.gov (United States)

    1983-01-01

    Because quadriplegics are unable to perspire below the level of spinal injury, they cannot tolerate heat stress. A cooling vest developed by Ames Research Center and Upjohn Company allows them to participate in outdoor activities. The vest is an adaptation of Ames technology for thermal control garments used to remove excess body heat of astronauts. The vest consists of a series of corrugated channels through which cooled water circulates. Its two outer layers are urethane coated nylon, and there is an inner layer which incorporates the corrugated channels. It can be worn as a backpack or affixed to a wheelchair. The unit includes a rechargeable battery, mini-pump, two quart reservoir and heat sink to cool the water.

  9. LSF usage for batch at CERN

    CERN Multimedia

    Schwickerath, Ulrich

    2007-01-01

    Contributed poster to the CHEP07. Original abstract: LSF 7, the latest version of Platform's batch workload management system, addresses many issues which limited the ability of LSF 6.1 to support large scale batch farms, such as the lxbatch service at CERN. In this paper we will present the status of the evaluation and deployment of LSF 7 at CERN, including issues concerning the integration of LSF 7 with the gLite grid middleware suite and, in particular, the steps taken to endure an efficient reporting of the local batch system status and usage to the Grid Information System

  10. Fractional Repetition and Erasure Batch Codes

    OpenAIRE

    Silberstein, Natalia

    2014-01-01

    Batch codes are a family of codes that represent a distributed storage system (DSS) of $n$ nodes so that any batch of $t$ data symbols can be retrieved by reading at most one symbol from each node. Fractional repetition codes are a family of codes for DSS that enable efficient uncoded repairs of failed nodes. In this work these two families of codes are combined to obtain fractional repetition batch (FRB) codes which provide both uncoded repairs and parallel reads of subsets of stored symbols...

  11. Batch Proving and Proof Scripting in PVS

    Science.gov (United States)

    Munoz, Cesar A.

    2007-01-01

    The batch execution modes of PVS are powerful, but highly technical, features of the system that are mostly accessible to expert users. This paper presents a PVS tool, called ProofLite, that extends the theorem prover interface with a batch proving utility and a proof scripting notation. ProofLite enables a semi-literate proving style where specification and proof scripts reside in the same file. The goal of ProofLite is to provide batch proving and proof scripting capabilities to regular, non-expert, users of PVS.

  12. Model Penjadwalan Batch Multi Item dengan Dependent Processing Time

    OpenAIRE

    Sukoyo Sukoyo; TMA. Ari Samadhi; Bermawi P. Iskandar; Abdul Hakim Halim

    2010-01-01

    This paper investigates a development of single machine batch scheduling for multi items with dependent processing time. The batch scheduling problem is to determine simultaneously number of batch (N), which item and its size allocated for each batch, and processing sequences of resulting batches. We use total actual flow time as the objective of schedule performance. The multi item batch scheduling problem could be formulated into a biner-integer nonlinear programming model because the numbe...

  13. Cool snacks

    DEFF Research Database (Denmark)

    Grunert, Klaus G; Brock, Steen; Brunsø, Karen;

    2016-01-01

    product requires an interdisciplinary effort where researchers with backgrounds in psychology, anthropology, media science, philosophy, sensory science and food science join forces. We present the COOL SNACKS project, where such a blend of competences was used first to obtain thorough insight into young...

  14. Cooling towers

    International Nuclear Information System (INIS)

    This paper investigates the internal elements of the typical types of cooling towers currently used, delineates their functions and shows how to upgrade them in the real world for energy savings and profitability of operation. Before and after statistics of costs and profits obtained through optimization of colder water by engineered thermal upgrading are discussed

  15. Stochastic cooling

    International Nuclear Information System (INIS)

    Stochastic cooling is the damping of betatron oscillations and momentum spread of a particle beam by a feedback system. In its simplest form, a pickup electrode detects the transverse positions or momenta of particles in a storage ring, and the signal produced is amplified and applied downstream to a kicker. The time delay of the cable and electronics is designed to match the transit time of particles along the arc of the storage ring between the pickup and kicker so that an individual particle receives the amplified version of the signal it produced at the pick-up. If there were only a single particle in the ring, it is obvious that betatron oscillations and momentum offset could be damped. However, in addition to its own signal, a particle receives signals from other beam particles. In the limit of an infinite number of particles, no damping could be achieved; we have Liouville's theorem with constant density of the phase space fluid. For a finite, albeit large number of particles, there remains a residue of the single particle damping which is of practical use in accumulating low phase space density beams of particles such as antiprotons. It was the realization of this fact that led to the invention of stochastic cooling by S. van der Meer in 1968. Since its conception, stochastic cooling has been the subject of much theoretical and experimental work. The earliest experiments were performed at the ISR in 1974, with the subsequent ICE studies firmly establishing the stochastic cooling technique. This work directly led to the design and construction of the Antiproton Accumulator at CERN and the beginnings of p anti p colliding beam physics at the SPS. Experiments in stochastic cooling have been performed at Fermilab in collaboration with LBL, and a design is currently under development for a anti p accumulator for the Tevatron

  16. Multi-objective optimization of glycopeptide antibiotic production in batch and fed batch processes

    DEFF Research Database (Denmark)

    Maiti, Soumen K.; Eliasson Lantz, Anna; Bhushan, Mani; Wangikar, Pramod P.

    2011-01-01

    as pareto optimal solutions. These solutions gives flexibility in evaluating the trade-offs and selecting the most suitable operating policy. Here, ε-constraint approach was used to generate the pareto solutions for two objectives: product concentration and product per unit cost of media, for batch...... and fed batch operations using process model for Amycolatopsis balhimycina, a glycopeptide antibiotic producer. This resulted in a set of several pareto optimal solutions with the two objectives ranging from (0.75gl−1, 3.97g$-1) to (0.44gl−1, 5.19g$-1) for batch and from (1.5gl−1, 5.46g$-1) to (1.1gl......−1, 6.34g$-1) for fed batch operations. One pareto solution each for batch and for fed batch mode was experimentally validated....

  17. Complete characterisation of the customer delay in a queueing system with batch arrivals and batch service

    OpenAIRE

    Claeys, Dieter; Laevens, Koenraad; Walraevens, Joris; Bruneel, Herwig

    2010-01-01

    Whereas the buffer content of batch-service queueing systems has been studied extensively, the customer delay has only occasionally been studied. The few papers concerning the customer delay share the common feature that only the moments are calculated explicitly. In addition, none of these surveys consider models including the combination of batch arrivals and a server operating under the full-batch service policy (the server waits to initiate service until he can serve at full capacity). In...

  18. A very cool cooling system

    CERN Multimedia

    Antonella Del Rosso

    2015-01-01

    The NA62 Gigatracker is a jewel of technology: its sensor, which delivers the time of the crossing particles with a precision of less than 200 picoseconds (better than similar LHC detectors), has a cooling system that might become the precursor to a completely new detector technique.   The 115 metre long vacuum tank of the NA62 experiment. The NA62 Gigatracker (GTK) is composed of a set of three innovative silicon pixel detectors, whose job is to measure the arrival time and the position of the incoming beam particles. Installed in the heart of the NA62 detector, the silicon sensors are cooled down (to about -20 degrees Celsius) by a microfluidic silicon device. “The cooling system is needed to remove the heat produced by the readout chips the silicon sensor is bonded to,” explains Alessandro Mapelli, microsystems engineer working in the Physics department. “For the NA62 Gigatracker we have designed a cooling plate on top of which both the silicon sensor and the...

  19. Workshop on beam cooling and related topics

    International Nuclear Information System (INIS)

    The sessions of the Workshop on Beam Cooling and Related Topics, held in Montreux from 4-8 October 1993, are reported in these Proceedings. This meeting brought together international experts in the field of accelerator beam cooling. Its purpose was to discuss the status of the different cooling techniques currently in use (stochastic, electron, ionization, heavy-ion, and laser) and their actual performances, technological implications, and future prospects. Certain theoretical principles (muon cooling, cyclotron maser cooling) were discussed and are reported on in these Proceedings. Also of interest in this Workshop was the possibility of beam crystallization in accelerators using ultimate cooling. In the first part of these Proceedings, overview talks on the various cooling techniques, their implications, present performance, and future prospects are presented. More detailed reports on all the topics are then given in the form of oral presentations or poster sessions. Finally, the chairmen and/or convenors then present summary talks. (orig.)

  20. Cooling systems

    International Nuclear Information System (INIS)

    Progress on the thermal effects project is reported with regard to physiology and distribution of Corbicula; power plant effects studies on burrowing mayfly populations; comparative thermal responses of largemouth bass from northern and southern populations; temperature selection by striped bass in Cherokee Reservoir; fish population studies; and predictive thermoregulation by fishes. Progress is also reported on the following; cause and ecological ramifications of threadfin shad impingement; entrainment project; aquaculture project; pathogenic amoeba project; and cooling tower drift project

  1. 21 CFR 211.188 - Batch production and control records.

    Science.gov (United States)

    2010-04-01

    ... 21 Food and Drugs 4 2010-04-01 2010-04-01 false Batch production and control records. 211.188... Reports § 211.188 Batch production and control records. Batch production and control records shall be prepared for each batch of drug product produced and shall include complete information relating to...

  2. 7 CFR 58.728 - Cooking the batch.

    Science.gov (United States)

    2010-01-01

    ... 7 Agriculture 3 2010-01-01 2010-01-01 false Cooking the batch. 58.728 Section 58.728 Agriculture... Procedures § 58.728 Cooking the batch. Each batch of cheese within the cooker, including the optional... cheese particles or ingredients after the cooker batch of cheese has reached the final...

  3. 40 CFR 63.1408 - Aggregate batch vent stream provisions.

    Science.gov (United States)

    2010-07-01

    ... from all aggregate batch vent streams in the compliance demonstration required for reactor batch... comply with the mass emission limit for reactor batch process vents. ... 40 Protection of Environment 11 2010-07-01 2010-07-01 true Aggregate batch vent stream...

  4. A Batch Feeder for Inhomogeneous Bulk Materials

    Science.gov (United States)

    Vislov, I. S.; Kladiev, S. N.; Slobodyan, S. M.; Bogdan, A. M.

    2016-04-01

    The work includes the mechanical analysis of mechanical feeders and batchers that find application in various technological processes and industrial fields. Feeders are usually classified according to their design features into two groups: conveyor-type feeders and non-conveyor feeders. Batchers are used to batch solid bulk materials. Less frequently, they are used for liquids. In terms of a batching method, they are divided into volumetric and weighting batchers. Weighting batchers do not provide for sufficient batching accuracy. Automatic weighting batchers include a mass controlling sensor and systems for automatic material feed and automatic mass discharge control. In terms of operating principle, batchers are divided into gravitational batchers and batchers with forced feed of material using conveyors and pumps. Improved consumption of raw materials, decreased loss of materials, ease of use in automatic control systems of industrial facilities allows increasing the quality of technological processes and improve labor conditions. The batch feeder suggested by the authors is a volumetric batcher that has no comparable counterparts among conveyor-type feeders and allows solving the problem of targeted feeding of bulk material batches increasing reliability and hermeticity of the device.

  5. Applying prior knowledge to model batch keeping-quality of cucumber batches

    NARCIS (Netherlands)

    Schouten, R.E.; Tijskens, L.M.M.; Kooten, van O.; Jongbloed, G.

    2004-01-01

    Keeping-quality of individual cucumbers is limited by the green colour; the keeping-quality of batches of cucumbers is limited by the time it takes before 5␘f the cucumbers in the batch reach a predefined colour limit. From literature concerning the synthesis and degradation of chlorophyll and a pub

  6. Quality and Batch-to-Batch Consistency of Original and Biosimilar Epoetin Products.

    Science.gov (United States)

    Halim, Liem Andhyk; Brinks, Vera; Jiskoot, Wim; Romeijn, Stefan; Haselberg, Rob; Burns, Chris; Wadhwa, Meenu; Schellekens, Huub

    2016-02-01

    Comprehensive physicochemical characterization and biological assays are essential parts in assessing quality attributes of biologicals. Here, we compared the quality of different marketed recombinant human erythropoietin (epoetin) products: originators, Eprex and NeoRecormon as well as 2 biosimilars, Retacrit and Binocrit. In addition, assessment of batch-to-batch variability was included by collecting 2 or more batches of each product. Common assays which included sodium dodecyl sulfate-polyacrylamide gel electrophoresis, high-performance size-exclusion chromatography, asymmetrical flow field-flow fractionation, capillary zone electrophoresis, and potency testing were used. Of the tested products and among batches of single products, variations in epoetin content, isoform profiles, and potency were found. Ultimately, this study demonstrated the high quality of epoetin products with some degree of variation among products and batches, confirming the "similar but not identical" paradigm of biologicals. PMID:26869417

  7. Cooling tower

    International Nuclear Information System (INIS)

    The proposal concerns the reinforcement of a cooling tower made of reinforced concrete, which has a dish-shaped supporting structure and has ribs running in the vertical direction. In order to reduce the cost for fitting the reinforcement, the dish-shaped supporting structure is made wholly or partly as an anisotropic dish. By this construction of the reinforcement (spatial grating with different thickness of beam reinforcement of vertical ribs and of the circular beams provided in the dish, site reinforcement of the areas between the beams) one achieves the anisotropy of the dish. The fixing of constructional steel mats as site reinforcement is advantageous. (UWI)

  8. Cool snacks

    DEFF Research Database (Denmark)

    Grunert, Klaus G; Brock, Steen; brunsø, karen;

    2016-01-01

    product requires an interdisciplinary effort where researchers with backgrounds in psychology, anthropology, media science, philosophy, sensory science and food science join forces. We present the COOL SNACKS project, where such a blend of competences was used first to obtain thorough insight into young...... people's snacking behaviour and then to develop and test new, healthier snacking solutions. These new snacking solutions were tested and found to be favourably accepted by young people. The paper therefore provides a proof of principle that the development of snacks that are both healthy and attractive...

  9. The practical effect of batch on genomic prediction

    OpenAIRE

    2012-01-01

    Measurements from microarrays and other high-throughput technologies are susceptible to non-biological artifacts like batch effects. It is known that batch effects can alter or obscure the set of significant results and biological conclusions in high-throughput studies. Here we examine the impact of batch effects on predictors built from genomic technologies. To investigate batch effects, we collected publicly available gene expression measurements with known outcomes, and estimated batches u...

  10. Following an Optimal Batch Bioreactor Operations Model

    DEFF Research Database (Denmark)

    Ibarra-Junquera, V.; Jørgensen, Sten Bay; Virgen-Ortíz, J.J.;

    2012-01-01

    The problem of following an optimal batch operation model for a bioreactor in the presence of uncertainties is studied. The optimal batch bioreactor operation model (OBBOM) refers to the bioreactor trajectory for nominal cultivation to be optimal. A multiple-variable dynamic optimization of fed-batch...... reactor for biomass production is studied using a differential geometry approach. The maximization problem is solved by handling both the optimal filling policy and substrate concentration in the inlet stream. In order to follow the OBBOM, a master–slave synchronization is used. The OBBOM is considered as...... the master system which includes the optimal cultivation trajectory for the feed flow rate and the substrate concentration. The “real” bioreactor, the one with unknown dynamics and perturbations, is considered as the slave system. Finally, the controller is designed such that the real bioreactor is...

  11. Systematic Methodology for Reproducible Optimizing Batch Operation

    DEFF Research Database (Denmark)

    Bonné, Dennis; Jørgensen, Sten Bay

    This contribution presents a systematic methodology for rapid acquirement of discrete-time state space model representations of batch processes based on their historical operation data. These state space models are parsimoniously parameterized as a set of local, interdependent models. The present...... contribution furthermore presents how the asymptotic convergence of Iterative Learning Control is combined with the closed-loop performance of Model Predictive Control to form a robust and asymptotically stable optimal controller for ensuring reliable and reproducible operation of batch processes. This...... controller may also be used for Optimizing control. The modeling and control performance is demonstrated on a fed-batch protein cultivation example. The presented methodologies lend themselves directly for application as Process Analytical Technologies (PAT)....

  12. Dynamic Fractional Resource Scheduling vs. Batch Scheduling

    CERN Document Server

    Casanova, Henri; Vivien, Frédéric

    2011-01-01

    We propose a novel job scheduling approach for homogeneous cluster computing platforms. Its key feature is the use of virtual machine technology to share fractional node resources in a precise and controlled manner. Other VM-based scheduling approaches have focused primarily on technical issues or on extensions to existing batch scheduling systems, while we take a more aggressive approach and seek to find heuristics that maximize an objective metric correlated with job performance. We derive absolute performance bounds and develop algorithms for the online, non-clairvoyant version of our scheduling problem. We further evaluate these algorithms in simulation against both synthetic and real-world HPC workloads and compare our algorithms to standard batch scheduling approaches. We find that our approach improves over batch scheduling by orders of magnitude in terms of job stretch, while leading to comparable or better resource utilization. Our results demonstrate that virtualization technology coupled with light...

  13. Estimation of the growth kinetics for the cooling crystallisation of paracetamol and ethanol solutions

    Science.gov (United States)

    Mitchell, Niall A.; Ó'Ciardhá, Clifford T.; Frawley, Patrick J.

    2011-08-01

    This work details the estimation of the growth kinetics of paracetamol in ethanol solutions for cooling crystallisation processes, by means of isothermal seeded batch experiments. The growth kinetics of paracetamol crystals were evaluated in isolation, with the growth rate assumed to be size independent. Prior knowledge of the Metastable Zone Width (MSZW) was required, so that supersaturation ratios of 1.7-1.1 could be induced in solution without the occurrence of nucleation. The technique involved the utilisation of two in-situ Process Analytical Techniques (PATs), with a Focused Beam Reflectance Measurement (FBRM ®) utilised to ensure that negligible nucleation occurred and an Attenuated Total Reflectance-Fourier Transform Infrared (ATR-FTIR) probe employed for online monitoring of solute concentration. Initial Particle Size Distributions (PSDs) were used in conjunction with desupersaturation profiles to determine the growth rate as a function of temperature and supersaturation. Furthermore, the effects of seed loading and size on the crystal growth rate were investigated. A numerical model, incorporating the population balance equation and the method of moments, was utilised to describe the crystal growth process. Experimental parameters were compared to the model simulation, with the accuracy of the model validated by means of the final product PSDs and solute concentration.

  14. ATLAS - Liquid Cooling Systems

    CERN Document Server

    Bonneau, P.

    1998-01-01

    Photo 1 - Cooling Unit - Side View Photo 2 - Cooling Unit - Detail Manifolds Photo 3 - Cooling Unit - Rear View Photo 4 - Cooling Unit - Detail Pump, Heater and Exchanger Photo 5 - Cooling Unit - Detail Pump and Fridge Photo 6 - Cooling Unit - Front View

  15. Optimal Control of Fed-Batch Fermenters

    OpenAIRE

    Valentinotti, S.; Cannizzaro, C; Rhiel, M.; Holmberg, U.; von Stockar, U; Bonvin, D.

    2000-01-01

    Optimal control of fed-batch fermenters S. Valentinotti† C. Cannizzaro‡ M.Rhiel‡ U. Holmberg† U. von Stockar‡ D. Bonvin† †Institut d’Automatique, EPFL, 1015 Lausanne, Switzerland ‡Institut de Genie Chimique, EPFL, 1015 Lausanne, Switzerland Fermentors are often run in a fed-batch manner to avoid the formation of overflow metabolites. At a high growth rate, the most efficient metabolic pathway(s) of certain microorganisms become saturated resulting in overflow metabolite production. These byprodu...

  16. A crystal barrel

    CERN Multimedia

    2007-01-01

    The production of crystals for the barrel of the CMS electromagnetic calorimeter has been completed. This is an important milestone for the experiment, which received the last of its 62,960 crystals on 9 March. The members of the team responsible for the crystal acceptance testing at CERN display the last crystal for the CMS electromagnetic calorimeter barrel. From left to right: Igor Tarasov, Etiennette Auffray and Hervé Cornet.One of the six machines specially developed to measure 67 different parameters on each crystal. Igor Tarasov is seen inserting the last batch of crystals into the machine. The last of the 62,960 CMS barrel crystals arrived at CERN on 9 March. Once removed from its polystyrene protection, this delicate crystal, like thousands of its predecessors, will be inserted into the last of the 36 supermodules of the barrel electromagnetic calorimeter in a few days' time. This marks the end of an important chapter in an almost 15-year-long journey by the CMS crystals team, some of whose member...

  17. Phononic crystal devices

    Science.gov (United States)

    El-Kady, Ihab F.; Olsson, Roy H.

    2012-01-10

    Phononic crystals that have the ability to modify and control the thermal black body phonon distribution and the phonon component of heat transport in a solid. In particular, the thermal conductivity and heat capacity can be modified by altering the phonon density of states in a phononic crystal. The present invention is directed to phononic crystal devices and materials such as radio frequency (RF) tags powered from ambient heat, dielectrics with extremely low thermal conductivity, thermoelectric materials with a higher ratio of electrical-to-thermal conductivity, materials with phononically engineered heat capacity, phononic crystal waveguides that enable accelerated cooling, and a variety of low temperature application devices.

  18. Cool visitors

    CERN Multimedia

    2006-01-01

    Pictured, from left to right: Tim Izo (saxophone, flute, guitar), Bobby Grant (tour manager), George Pajon (guitar). What do the LHC and a world-famous hip-hop group have in common? They are cool! On Saturday, 1st July, before their appearance at the Montreux Jazz Festival, three members of the 'Black Eyed Peas' came on a surprise visit to CERN, inspired by Dan Brown's Angels and Demons. At short notice, Connie Potter (Head of the ATLAS secretariat) organized a guided tour of ATLAS and the AD 'antimatter factory'. Still curious, lead vocalist Will.I.Am met CERN physicist Rolf Landua after the concert to ask many more questions on particles, CERN, and the origin of the Universe.

  19. Exploring the Transition From Batch to Online

    DEFF Research Database (Denmark)

    Jørgensen, Anker Helms

    2010-01-01

    truly interactive use of computers known today. The transition invoked changes in a number of areas: technological, such as hybrid forms between batch and online; organisational such as decentralization; and personal as users and developers alike had to adopt new technology, shape new organizational...

  20. Cooling off with physics

    International Nuclear Information System (INIS)

    You might think of ice cream as a delicious treat to be enjoyed on a sunny summer's day. However, to the ice-cream scientists who recently gathered in Thessaloniki in Greece for the 2nd International Ice Cream Symposium, it is a complex composite material. Ice cream consists of three dispersed phases: ice crystals, which have a mean size of 50 microns, air bubbles with a diameter of about 70 microns, and fat droplets with a size of 1 micron. These phases are held together by what is called the matrix - not a sci-fi film, but a viscous solution of sugars, milk proteins and polysaccharides. The microstructure, and hence the texture that you experience when you eat ice cream, is created in a freezing process that has remained fundamentally unchanged since the first ice-cream maker was patented in the 1840s. The ingredients - water, milk protein, fat, sugar, emulsifiers, stabilizers, flavours and a lot of air - are mixed together before being pasteurized and homogenized. They are then pumped into a cylinder that is cooled from the outside with a refrigerant. As the mixture touches the cylinder wall it freezes and forms ice crystals, which are quickly scraped off by a rotating blade. The blade is attached to a beater that disperses the ice crystals into the mixture. At the same time, air is injected and broken down into small bubbles by the shear that the beater generates. As the mixture passes along the cylinder, the number of ice crystals increases and its temperature drops. As a result, the viscosity of the mixture increases, so that more energy input is needed to rotate the beater. This energy is dissipated as heat, and when the ice cream reaches about -6 deg. C the energy input through the beater equals the energy removed as heat by the refrigerant. The process therefore becomes self-limiting and it is not possible to cool the ice cream any further. However, at -6 deg. C the microstructure is unstable. The ice cream therefore has to be removed from the freezer and

  1. Device for cooling down cooling water especially in cooling towers

    International Nuclear Information System (INIS)

    A cooling tower is described where water runs over packing plates being cooled by steaming air. In the cooling process a combination of wet and dry cooling is applied, namely by special design of the packing plates which are arranged inclined to the vertical. Spraying device and packing plates are shaped in such a way that the plates are wetted almost on one side only. 13 drawings explain the construction of the device described in detail. (UWI)

  2. Monte Carlo simulation on kinetics of batch and semi-batch free radical polymerization

    KAUST Repository

    Shao, Jing

    2015-10-27

    Based on Monte Carlo simulation technology, we proposed a hybrid routine which combines reaction mechanism together with coarse-grained molecular simulation to study the kinetics of free radical polymerization. By comparing with previous experimental and simulation studies, we showed the capability of our Monte Carlo scheme on representing polymerization kinetics in batch and semi-batch processes. Various kinetics information, such as instant monomer conversion, molecular weight, and polydispersity etc. are readily calculated from Monte Carlo simulation. The kinetic constants such as polymerization rate k p is determined in the simulation without of “steady-state” hypothesis. We explored the mechanism for the variation of polymerization kinetics those observed in previous studies, as well as polymerization-induced phase separation. Our Monte Carlo simulation scheme is versatile on studying polymerization kinetics in batch and semi-batch processes.

  3. Batch and Fed-Batch Fermentation System on Ethanol Production from Whey using Kluyveromyces marxianus

    OpenAIRE

    H Hadiyanto; D. Ariyanti; A.P. Aini; D.S. Pinundi

    2013-01-01

    Nowadays reserve of fossil fuel has gradually depleted. This condition forces many researchers to  find energy alternatives which is renewable and sustainable in the future. Ethanol derived from cheese industrial waste (whey) using fermentation process can be a new perspective in order to secure both energy and environment. The aim of this study was  to compare the operation modes (batch and fed-batch) of fermentation system on ethanol production from whey using Kluyveromyces marxianus. The r...

  4. Sojourn time distributions in a Markovian G-queue with batch arrival and batch removal

    OpenAIRE

    Yang Woo Shin

    1999-01-01

    We consider a single server Markovian queue with two types of customers; positive and negative, where positive customers arrive in batches and arrivals of negative customers remove positive customers in batches. Only positive customers form a queue and negative customers just reduce the system congestion by removing positive ones upon their arrivals. We derive the LSTs of sojourn time distributions for a single server Markovian queue with positive customers and negative customers by using the...

  5. Batch and fed-batch production of butyric acid by Clostridium butyricum ZJUCB

    Institute of Scientific and Technical Information of China (English)

    HE Guo-qing; KONG Qing; CHEN Qi-he; RUAN Hui

    2005-01-01

    The production of butyric acid by Clostridium butyricum ZJUCB at various pH values was investigated. In order to study the effect of pH on cell growth, butyric acid biosynthesis and reducing sugar consumption, different cultivation pH values ranging from 6.0 to 7.5 were evaluated in 5-L bioreactor. In controlled pH batch fermentation, the optimum pH for cell growth and butyric acid production was 6.5 with a cell yield of 3.65 g/L and butyric acid yield of 12.25 g/L. Based on these results, this study then compared batch and fed-batch fermentation of butyric acid production at pH 6.5. Maximum value (16.74 g/L) of butyric acid concentration was obtained in fed-batch fermentation compared to 12.25 g/L in batch fermentation. It was concluded that cultivation under fed-batch fermentation mode could enhance butyric acid production significantly (P<0.01) by C. butyricum ZJUCB.

  6. Using Forensics to Untangle Batch Effects in TCGA Data - TCGA

    Science.gov (United States)

    Rehan Akbani, Ph.D., and colleagues at the University of Texas MD Anderson Cancer Center developed a tool called MBatch to detect, diagnose, and correct batch effects in TCGA data. Read more about batch effects in this Case Study.

  7. Optimal operation of batch membrane processes

    CERN Document Server

    Paulen, Radoslav

    2016-01-01

    This study concentrates on a general optimization of a particular class of membrane separation processes: those involving batch diafiltration. Existing practices are explained and operational improvements based on optimal control theory are suggested. The first part of the book introduces the theory of membrane processes, optimal control and dynamic optimization. Separation problems are defined and mathematical models of batch membrane processes derived. The control theory focuses on problems of dynamic optimization from a chemical-engineering point of view. Analytical and numerical methods that can be exploited to treat problems of optimal control for membrane processes are described. The second part of the text builds on this theoretical basis to establish solutions for membrane models of increasing complexity. Each chapter starts with a derivation of optimal operation and continues with case studies exemplifying various aspects of the control problems under consideration. The authors work their way from th...

  8. FBSNG - batch system for farm architecture

    International Nuclear Information System (INIS)

    FBSNG is a redesigned version of Farm Batch System (FBS), which was developed as a batch process management system for off-line Run II data processing at FNAL. FBSNG is designed for UNIX computer farms and is capable of managing up to 1000 nodes in a single farm. FBSNG allows users to start arrays of parallel processes on one or more farm computers. It uses a simplified abstract resource counting method for load balancing between computers. The resource counting approach allows FBSNG to be a simple and flexible tool for farm resource management. FBSNG scheduler features include guaranteed and controllable 'fair-share' scheduling. FBSNG is easily portable across different flavors of UNIX. The system has been successfully used at Fermilab as well as by off-site collaborators for several years on farms of different sizes and different platforms for off-line data processing, Monte-Carlo data generation and other tasks

  9. Properties of batch means from stationary ARMA time series

    OpenAIRE

    Kang, Keebom; Schmeiser, Bruce

    1986-01-01

    The batch means process arising from an arbitrary autoregressive moving-average (ARMA) process time series is derived. As side results, the variance and correlation structures of the batch means process as functions of the batch size and parameters of the original process are obtained. Except for the first-order ARMA process, for which a closed-form expression is obtained, the parameters of the batch-means process are determined numerically. Keywords: Monte Carlo method; Simulation. (Author)

  10. Exception Handling in Recipe-Based Batch Control

    OpenAIRE

    Olsson, Rasmus

    2002-01-01

    The focus of this thesis is exception handling in recipe-based batch control. Exception handling is a critical element for achieving long-term success in batch production. It is reported to constitute 40-60 percent of the batch control design and implementation effort. Correct handling of exceptions is a key element in process safety, consistent product quality, and production cost minimization. The previous work on Grafchart for sequential programming, batch process recipe handling and resou...

  11. Capacitated max -Batching with Interval Graph Compatibilities

    Science.gov (United States)

    Nonner, Tim

    We consider the problem of partitioning interval graphs into cliques of bounded size. Each interval has a weight, and the weight of a clique is the maximum weight of any interval in the clique. This natural graph problem can be interpreted as a batch scheduling problem. Solving a long-standing open problem, we show NP-hardness, even if the bound on the clique sizes is constant. Moreover, we give a PTAS based on a novel dynamic programming technique for this case.

  12. Isopropyl alcohol recovery by heteroazeotropic batch distillation

    OpenAIRE

    Van Baelen, Guy; Vreysen, Steven; Gerbaud, Vincent; Rodriguez-Donis, Ivonne; Geens, Jeroen; Janssens, Bart

    2010-01-01

    Solvent recovery is becoming a major issue in the pharmaceutical and specialty chemical industries. Solvent recovery by conventional batch distillation is limited by the frequent presence of azeotropes in the used solvent mixtures. Most distillation processes for the separation of azeotropic or difficult zeotropic mixtures involve the addition of an entrainer (homogeneous and heterogeneous azeotropic distillation or extractive distillation). In this study the recovery of IPA (isopropyl alc...

  13. A novel heat integrated batch distillation scheme

    International Nuclear Information System (INIS)

    Highlights: → We develop an internally heat integrated structure for a batch distillation. → The concentric reboiler receives heat from the rectifier operated at high pressure. → A compressor and a throttling valve are installed for pressure adjustment. → Heat integration provides a significant savings in energy as well as cost. -- Abstract: Published studies have been focused mainly on the energy integration of continuous distillation columns. In this contribution, a novel heat integrated batch distillation column (HIBDC) is proposed. Aiming to improve the thermodynamic efficiency and reduce the total annual cost (TAC), a thermally coupled column configuration is explored with introducing heat integration between the rectifying tower and concentric reboiler. A compressor is employed to provide the necessary temperature driving force for the heat transferred from the rectifier to the reboiler. Investigating the feasibility of energy integration in the simulated batch process, a number of sensitivity tests have been conducted to select the value of operating compression ratio. An economic comparison between the proposed HIBDC and the conventional stand alone column is also performed. It is observed that the HIBDC system appears overwhelmingly superior to its conventional counterpart providing about an energy savings of 56.1% and cost (TAC) savings of 40.53%.

  14. 21 CFR 80.37 - Treatment of batch pending certification.

    Science.gov (United States)

    2010-04-01

    ... 21 Food and Drugs 1 2010-04-01 2010-04-01 false Treatment of batch pending certification. 80.37... COLOR ADDITIVE CERTIFICATION Certification Procedures § 80.37 Treatment of batch pending certification. Immediately after the sample that is to accompany a request for certification of a batch of color additive...

  15. 21 CFR 80.38 - Treatment of batch after certification.

    Science.gov (United States)

    2010-04-01

    ... 21 Food and Drugs 1 2010-04-01 2010-04-01 false Treatment of batch after certification. 80.38... COLOR ADDITIVE CERTIFICATION Certification Procedures § 80.38 Treatment of batch after certification. (a) Immediately upon notification that a batch of color additive has been certified, the person...

  16. 40 CFR 63.462 - Batch cold cleaning machine standards.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 9 2010-07-01 2010-07-01 false Batch cold cleaning machine standards... National Emission Standards for Halogenated Solvent Cleaning § 63.462 Batch cold cleaning machine standards. (a) Each owner or operator of an immersion batch cold solvent cleaning machine shall comply with...

  17. 40 CFR 63.1321 - Batch process vents provisions.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 11 2010-07-01 2010-07-01 true Batch process vents provisions. 63.1321... Standards for Hazardous Air Pollutant Emissions: Group IV Polymers and Resins § 63.1321 Batch process vents provisions. (a) Batch process vents. Except as specified in paragraphs (b) through (d) of this...

  18. 40 CFR 63.1406 - Reactor batch process vent provisions.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 11 2010-07-01 2010-07-01 true Reactor batch process vent provisions... § 63.1406 Reactor batch process vent provisions. (a) Emission standards. Owners or operators of reactor... reactor batch process vent located at a new affected source shall control organic HAP emissions...

  19. A Semi-Batch Reactor Experiment for the Undergraduate Laboratory

    Science.gov (United States)

    Derevjanik, Mario; Badri, Solmaz; Barat, Robert

    2011-01-01

    This experiment and analysis offer an economic yet challenging semi-batch reactor experience. Household bleach is pumped at a controlled rate into a batch reactor containing pharmaceutical hydrogen peroxide solution. Batch temperature, product molecular oxygen, and the overall change in solution conductivity are metered. The reactor simulation…

  20. Crystallization phenomena in slags

    Science.gov (United States)

    Orrling, Carl Folke

    2000-09-01

    The crystallization of the mold slag affects both the heat transfer and the lubrication between the mold and the strand in continuous casting of steel. In order for mold slag design to become an engineering science rather than an empirical exercise, a fundamental understanding of the melting and solidification behavior of a slag must be developed. Thus it is necessary to be able to quantify the phenomena that occur under the thermal conditions that are found in the mold of a continuous caster. The double hot thermocouple technique (DHTT) and the Confocal Laser Scanning Microscope used in this study are two novel techniques for investigating melting and solidification phenomena of transparent slags. Results from these techniques are useful in defining the phenomena that occur when the slag film infiltrates between the mold and the shell of the casting. TTT diagrams were obtained for various slags and indicated that the onset of crystallization is a function of cooling rate and slag chemistry. Crystal morphology was found to be dependent upon the experimental temperature and four different morphologies were classified based upon the degree of melt undercooling. Continuous cooling experiments were carried out to develop CCT diagrams and it was found that the amount and appearance of the crystalline fraction greatly depends on the cooling conditions. The DHTT can also be used to mimic the cooling profile encountered by the slag in the mold of a continuous caster. In this differential cooling mode (DCT), it was found that the details of the cooling rate determine the actual response of the slag to a thermal gradient and small changes can lead to significantly different results. Crystal growth rates were measured and found to be in the range between 0.11 mum/s to 11.73 mum/s depending on temperature and slag chemistry. Alumina particles were found to be effective innoculants in oxide melts reducing the incubation time for the onset of crystallization and also extending

  1. Thin-Film Evaporative Cooling for Side-Pumped Laser

    Science.gov (United States)

    Stewart, Brian K. (Inventor)

    2010-01-01

    A system and method are provided for cooling a crystal rod of a side-pumped laser. A transparent housing receives the crystal rod therethrough so that an annular gap is defined between the housing and the radial surface of the crystal rod. A fluid coolant is injected into the annular gap such the annular gap is partially filled with the fluid coolant while the radial surface of the crystal rod is wetted as a thin film all along the axial length thereof.

  2. Environmental compatible cooling water treatment chemicals; Umweltvertraegliche Chemikalien in der Kuehlwasserkonditionierung

    Energy Technology Data Exchange (ETDEWEB)

    Gartiser, S.; Urich, E.

    2002-02-01

    In Germany about 32 billion m{sup 3}/a cooling water are discharged from industrial plants and power industry. These are conditioned partly with biocides, scaling and corrosion inhibitors. Within the research project the significance of cooling water chemicals was evaluated, identifying the chemicals from product information, calculating their loads from consumption data of more than 180 cooling plants and investigating the basic data needed for an environmental hazard assessment. Additionally the effects of cooling water samples and products were determined in biological test systems. Batch tests were performed under defined conditions in order to measure the inactivation of cooling water biocides. (orig.)

  3. Response variation in a batch of TLDS

    International Nuclear Information System (INIS)

    Full text: At Royal Perth Hospital, LiF thermoluminescent dosimeter rods (TLDs) are handled in batches of 50. Rods in each batch are always annealed together to ensure the same thermal history and an individual batch is used with the same type and energy of radiation. A subset of a batch is used for calibration purposes by exposing them to a range of known doses and their output is used to calculate the dose received by other rods used for a dose measurement. Variation in TLD response is addressed by calculating 95% certainty levels from the calibration rods and applying this to the dose measurement rods. This approach relies on the sensitivity of rods within each batch being similar. This work investigates the validity of this assumption and considers possible benefits of applying individual rod sensitivities. The variation in response of TLD rods was assessed using 25 TLD-100 rods (Harshaw/Bicron) which were uniformly exposed to 1 Gy using 6 MeV photons in a linear accelerator on 5 separate occasions. Rods were read with a Harshaw 5500 reader. During the read process the Harshaw reader periodically checks for noise and PMT gain drift and the data were corrected for these parameters. Replicate exposure data were analysed using 1-way Analysis of Variance (ANOVA) to determine whether the between rod variations were significantly different to the variations within a single rod. A batch of 50 rods was also exposed on three occasions using the above technique. Individual TLD rod sensitivity values were determined using the rod responses from 2 exposures and these values were applied to correct charges on a rod-by-rod basis for the third exposure. ANOVA results on the 5 exposures of 25 rods showed the variance between rods was significantly greater than the within rod variance (p < 0.001). The precision of an individual rod was estimated to have a standard deviation of 2.8%. This suggests that the 95% confidence limits for repeated measurements using the same dose and

  4. Influence of pH and method of crystallization on the solid physical form of indomethacin.

    Science.gov (United States)

    Dubbini, Alessandra; Censi, Roberta; Martena, Valentina; Hoti, Ela; Ricciutelli, Massimo; Malaj, Ledjan; Di Martino, Piera

    2014-10-01

    The purpose of this study was to investigate the effect of pH and method of crystallization on the solid physical form of indomethacin (IDM). IDM, a non steroidal anti-inflammatory drug poorly soluble in water, underwent two different crystallization methods: crystallization by solvent evaporation under reduced pressure at 50.0°C (method A), and crystallization by cooling of solution from 50.0 to 5.0°C (method B). In both cases, several aqueous ethanolic solutions of IDM of different pHs were prepared. pHs were adjusted by adding acidic solutions (HCl 2M) or alkali (NaOH or NH4OH 2M) to an aqueous ethanolic solution of IDM. Thus, several batches were recovered after crystallization. The chemical stability of IDM was verified through (1)H NMR and mass spectroscopy (FIA-ESI-MS), that revealed that IDM degraded in strong alkali media (pH ≥ 12). Crystals obtained under different crystallization conditions at pHs of 1.0, 4.5, 7.0, 8.0, 10.0 and chemically stable were thus characterized for crystal habit by scanning electron microscopy, for thermal behaviour by differential scanning calorimetry, and thermogravimetry, and for solid state by X-ray powder diffractometry. Under the Method A, IDM always crystallized into pure metastable alpha form when solutions were acidified or alkalized respectively with HCl and NH4OH. On the contrary, in presence of NaOH, IDM crystallized under a mixture of alpha and sodium trihydrate form, because the presence of the sodium counter ion orientates the crystallization towards the formation of the trihydrate salt. Under the method B, at pH of 1.0, IDM crystallized under the alpha form; at pH 4.5, IDM crystallized under the form alpha in presence of some nuclei of gamma form; at pH 7.0, 8.0, and 10.0 for NH4OH, IDM crystallized under the most stable polymorph gamma form, whereas in presence of NaOH, a mix of alpha, and salt forms was formed whatever the pH of the solution. PMID:25064728

  5. BATCH-GE: Batch analysis of Next-Generation Sequencing data for genome editing assessment

    Science.gov (United States)

    Boel, Annekatrien; Steyaert, Woutert; De Rocker, Nina; Menten, Björn; Callewaert, Bert; De Paepe, Anne; Coucke, Paul; Willaert, Andy

    2016-01-01

    Targeted mutagenesis by the CRISPR/Cas9 system is currently revolutionizing genetics. The ease of this technique has enabled genome engineering in-vitro and in a range of model organisms and has pushed experimental dimensions to unprecedented proportions. Due to its tremendous progress in terms of speed, read length, throughput and cost, Next-Generation Sequencing (NGS) has been increasingly used for the analysis of CRISPR/Cas9 genome editing experiments. However, the current tools for genome editing assessment lack flexibility and fall short in the analysis of large amounts of NGS data. Therefore, we designed BATCH-GE, an easy-to-use bioinformatics tool for batch analysis of NGS-generated genome editing data, available from https://github.com/WouterSteyaert/BATCH-GE.git. BATCH-GE detects and reports indel mutations and other precise genome editing events and calculates the corresponding mutagenesis efficiencies for a large number of samples in parallel. Furthermore, this new tool provides flexibility by allowing the user to adapt a number of input variables. The performance of BATCH-GE was evaluated in two genome editing experiments, aiming to generate knock-out and knock-in zebrafish mutants. This tool will not only contribute to the evaluation of CRISPR/Cas9-based experiments, but will be of use in any genome editing experiment and has the ability to analyze data from every organism with a sequenced genome. PMID:27461955

  6. BATCH-GE: Batch analysis of Next-Generation Sequencing data for genome editing assessment.

    Science.gov (United States)

    Boel, Annekatrien; Steyaert, Woutert; De Rocker, Nina; Menten, Björn; Callewaert, Bert; De Paepe, Anne; Coucke, Paul; Willaert, Andy

    2016-01-01

    Targeted mutagenesis by the CRISPR/Cas9 system is currently revolutionizing genetics. The ease of this technique has enabled genome engineering in-vitro and in a range of model organisms and has pushed experimental dimensions to unprecedented proportions. Due to its tremendous progress in terms of speed, read length, throughput and cost, Next-Generation Sequencing (NGS) has been increasingly used for the analysis of CRISPR/Cas9 genome editing experiments. However, the current tools for genome editing assessment lack flexibility and fall short in the analysis of large amounts of NGS data. Therefore, we designed BATCH-GE, an easy-to-use bioinformatics tool for batch analysis of NGS-generated genome editing data, available from https://github.com/WouterSteyaert/BATCH-GE.git. BATCH-GE detects and reports indel mutations and other precise genome editing events and calculates the corresponding mutagenesis efficiencies for a large number of samples in parallel. Furthermore, this new tool provides flexibility by allowing the user to adapt a number of input variables. The performance of BATCH-GE was evaluated in two genome editing experiments, aiming to generate knock-out and knock-in zebrafish mutants. This tool will not only contribute to the evaluation of CRISPR/Cas9-based experiments, but will be of use in any genome editing experiment and has the ability to analyze data from every organism with a sequenced genome. PMID:27461955

  7. On the track of fish batches in three distribution networks

    DEFF Research Database (Denmark)

    Randrup, Maria; Wu, Haiping; Jørgensen, Bo M.

    2012-01-01

    Three fish products sampled in retail shops were traced back to their origin and fish from the same batch were tracked forward towards the retailer, thereby simulating a recall situation. The resulting distribution networks were very complex, but to the extent that companies were willing to provide...... the necessary information, it was possible to locate the end destinations of the fish batches. The batch sizes and the number of companies involved clearly rose when batch joining occurred. Thus, a fault in a small batch can potentially have widespread implications. The study also underlines the...

  8. Production of ethanol in batch and fed-batch fermentation of soluble sugar

    International Nuclear Information System (INIS)

    Keeping in view of the demand and need for alternate energy source, especially liquid fuels and the availability of raw materials in Pakistan, we have carried out biochemical and technological studies for ethanol through fermentation of renewable substrates. Molasses and sugar cane have been used as substrate for yeast fermentation. Selected yeast were used in both batch and semi continuous fermentation of molasses. Clarified dilute molasses were fermented with different strains of Saccharomyces cerevisiae. Ethanol concentration after 64 hours batch fermentation reached 9.4% with 90% yield based on sugar content. During feed batch system similar results were obtained after a fermentation cycle of 48 hours resulting in higher productivity. Similarly carbohydrates in fruit juices and hydro lysates of biomass can be economically fermented to ethanol to be used as feed stock for other chemicals. (author)

  9. Kinetic Analyses of Desulfurization of Dibenzothiophene by Rhodococcus erythropolis in Batch and Fed-Batch Cultures

    OpenAIRE

    P. Wang; Krawiec, S.

    1996-01-01

    The DbtS(sup+) phenotype (which confers the ability to oxidize selectively the sulfur atom of dibenzothiophene [DBT] or dibenzothiophene sulfone [DBTO(inf2)]) of Rhodococcus erythropolis N1-36 was quantitatively characterized in batch and fed-batch cultures. In flask cultures, production of the desulfurization product, monohydroxybiphenyl (OH-BP), was maximal at pH 6.0, while specific productivity (OH-BP cell(sup-1)) was maximal at pH 5.5. Quantitative measurements in fermentors (in both batc...

  10. Fabrication of spherical fuel element for 10 MW high temperature gas-cooled reactor

    International Nuclear Information System (INIS)

    Cold quasi-isostatic molding with a silicon rubber die was used for manufacturing the spherical fuel elements of 10 MW high temperature gas-cooled reactor. 44 batches of fuel elements, about 20540 of the fuel elements, were produced. The cold properties of the graphite matrix materials satisfies the design specifications. The mean free uranium fraction in spherical fuel element from 44 batches is 4.57 x 10-5, certified products is 99%

  11. Hybrid radiator cooling system

    Energy Technology Data Exchange (ETDEWEB)

    France, David M.; Smith, David S.; Yu, Wenhua; Routbort, Jules L.

    2016-03-15

    A method and hybrid radiator-cooling apparatus for implementing enhanced radiator-cooling are provided. The hybrid radiator-cooling apparatus includes an air-side finned surface for air cooling; an elongated vertically extending surface extending outwardly from the air-side finned surface on a downstream air-side of the hybrid radiator; and a water supply for selectively providing evaporative cooling with water flow by gravity on the elongated vertically extending surface.

  12. 21 CFR 111.260 - What must the batch record include?

    Science.gov (United States)

    2010-04-01

    ... 21 Food and Drugs 2 2010-04-01 2010-04-01 false What must the batch record include? 111.260... for the Batch Production Record § 111.260 What must the batch record include? The batch production record must include the following: (a) The batch, lot, or control number: (1) Of the finished batch...

  13. Laser cooling of externally produced Mg ions in a Penning trap for sympathetic cooling of highly charged ions

    OpenAIRE

    Andelkovic, Z.; Cazan, R.; Nörtershäuser, W.(Institut für Kernchemie, Universität Mainz, D-55128 Mainz, Germany); Bharadia, S.; Segal, D. M.; Thompson, R. C.; Jöhren, R. (Raphael); Vollbrecht, J.; Hannen, V.; M. Vogel

    2012-01-01

    We have performed laser cooling of Mg ions confined in a Penning trap. The externally produced ions were captured in flight, stored and laser cooled. Laser-induced fluorescence was observed perpendicular to the cooling laser axis. Optical detection down to the single ion level together with electronic detection of the ion oscillations inside the Penning trap have been used to acquire information on the ion storage time, ion number and ion temperature. Evidence for formation of ion crystals ha...

  14. Batch-to-batch pharmacokinetic variability confounds current bioequivalence regulations: A dry powder inhaler randomized clinical trial.

    Science.gov (United States)

    Burmeister Getz, E; Carroll, K J; Jones, B; Benet, L Z

    2016-09-01

    Current pharmacokinetic (PK) bioequivalence guidelines do not account for batch-to-batch variability in study design or analysis. Here we evaluate the magnitude of batch-to-batch PK variability for Advair Diskus 100/50. Single doses of fluticasone propionate and salmeterol combinations were administered by oral inhalation to healthy subjects in a randomized clinical crossover study comparing three different batches purchased from the market, with one batch replicated across two treatment periods. All pairwise comparisons between different batches failed the PK bioequivalence statistical test, demonstrating substantial PK differences between batches that were large enough to demonstrate bio-inequivalence in some cases. In contrast, between-replicate PK bioequivalence was demonstrated for the replicated batch. Between-batch variance was ∼40-70% of the estimated residual error. This large additional source of variability necessitates re-evaluation of bioequivalence assessment criteria to yield a result that is both generalizable and consistent with the principles of type I and type II error rate control. PMID:27037630

  15. Adaptive quality prediction of batch processes based on PLS model

    Institute of Scientific and Technical Information of China (English)

    LI Chun-fu; ZHANG Jie; WANG Gui-zeng

    2006-01-01

    There are usually no on-line product quality measurements in batch and semi-batch processes,which make the process control task very difficult.In this paper,a model for predicting the end-product quality from the available on-line process variables at the early stage of a batch is developed using partial least squares (PLS)method.Furthermore,some available mid-course quality measurements are used to rectify the final prediction results.To deal with the problem that the process may change with time,recursive PLS (RPLS) algorithm is used to update the model based on the new batch data and the old model parameters after each batch.An application to a simulated batch MMA polymerization process demonstrates the effectiveness of the proposed method.

  16. Evaluation of vitrification factors from DWPF's macro-batch 1

    International Nuclear Information System (INIS)

    The Defense Waste Processing Facility (DWPF) is evaluating new sampling and analytical methods that may be used to support future Slurry Mix Evaporator (SME) batch acceptability decisions. This report uses data acquired during DWPF's processing of macro-batch 1 to determine a set of vitrification factors covering several SME and Melter Feed Tank (MFT) batches. Such values are needed for converting the cation measurements derived from the new methods to a ''glass'' basis. The available data from macro-batch 1 were used to examine the stability of these vitrification factors, to estimate their uncertainty over the course of a macro-batch, and to provide a recommendation on the use of a single factor for an entire macro-batch. The report is in response to Technical Task Request HLW/DWPF/TTR-980015

  17. TANK 50 BATCH 0 SALTSTONE FORMULATION CONFIRMATION

    Energy Technology Data Exchange (ETDEWEB)

    Langton, C.

    2006-06-05

    Savannah River National Laboratory (SRNL) personnel were requested to confirm the Tank 50 Batch 0 grout formulation per Technical Task Request, SSF-TTR-2006-0001 (task 1 of 2) [1]. Earlier Batch 0 formulation testing used a Tank 50 sample collected in September 2005 and is described elsewhere [2]. The current testing was performed using a sample of Tank 50 waste collected in May 2006. This work was performed according to the Technical Task and Quality Assurance Plan (TT/QAP), WSRC-RP-2006-00594 [3]. The salt solution collected from Tank 50 in May 2006 contained approximately 3 weight percent more solids than the sample collected in September 2005. The insoluble solids took longer to settle in the new sample which was interpreted as indicating finer particles in the current sample. The saltstone formulation developed for the September 2005 Tank 50 Batch 0 sample was confirmed for the May 2006 sample with one minor exception. Saltstone prepared with the Tank 50 sample collected in May 2006 required 1.5 times more Daratard 17 set retarding admixture than the saltstone prepared with the September In addition, a sample prepared with lower shear mixing (stirring with a spatula) had a higher plastic viscosity (57 cP) than samples made with higher shear mixing in a blender (23cP). The static gel times of the saltstone slurries made with low shear mixing were also shorter ({approx}32 minutes) than those for comparable samples made in the blender ({approx}47 minutes). The addition of the various waste streams (ETP, HEU-HCAN, and GPE-HCAN) to Tank 50 from September 2005 to May 2006 has increased the amount of set retarder, Daratard 17, required for processing saltstone slurries through the Saltstone facility. If these streams are continued to be added to Tank 50, the quantity of admixtures required to maintain the same processing conditions for the Saltstone facility will probably change and additional testing is recommended to reconfirm the Tank 50 Saltstone formulation.

  18. TANK 50 BATCH 0 SALTSTONE FORMULATION CONFIRMATION

    International Nuclear Information System (INIS)

    Savannah River National Laboratory (SRNL) personnel were requested to confirm the Tank 50 Batch 0 grout formulation per Technical Task Request, SSF-TTR-2006-0001 (task 1 of 2) [1]. Earlier Batch 0 formulation testing used a Tank 50 sample collected in September 2005 and is described elsewhere [2]. The current testing was performed using a sample of Tank 50 waste collected in May 2006. This work was performed according to the Technical Task and Quality Assurance Plan (TT/QAP), WSRC-RP-2006-00594 [3]. The salt solution collected from Tank 50 in May 2006 contained approximately 3 weight percent more solids than the sample collected in September 2005. The insoluble solids took longer to settle in the new sample which was interpreted as indicating finer particles in the current sample. The saltstone formulation developed for the September 2005 Tank 50 Batch 0 sample was confirmed for the May 2006 sample with one minor exception. Saltstone prepared with the Tank 50 sample collected in May 2006 required 1.5 times more Daratard 17 set retarding admixture than the saltstone prepared with the September In addition, a sample prepared with lower shear mixing (stirring with a spatula) had a higher plastic viscosity (57 cP) than samples made with higher shear mixing in a blender (23cP). The static gel times of the saltstone slurries made with low shear mixing were also shorter (∼32 minutes) than those for comparable samples made in the blender (∼47 minutes). The addition of the various waste streams (ETP, HEU-HCAN, and GPE-HCAN) to Tank 50 from September 2005 to May 2006 has increased the amount of set retarder, Daratard 17, required for processing saltstone slurries through the Saltstone facility. If these streams are continued to be added to Tank 50, the quantity of admixtures required to maintain the same processing conditions for the Saltstone facility will probably change and additional testing is recommended to reconfirm the Tank 50 Saltstone formulation

  19. ENGINEERING CONTRACT ON FY-2 BATCH 2 SATELLITES SIGNED

    Institute of Scientific and Technical Information of China (English)

    SunQing

    2004-01-01

    The signing ceremony of the Engineering Contract on FY-2 Batch 2 (FY-2 02) Satellites was held in Beijing by Commission of Science, Technology and Industry for National Defense (COSTIND) on August 31, 2004. The contract on the development and manufacture of FY-2 batch 2 satellites and the contract on the launch, test and control of FY-2 Batch 2 satellites were signed by China Meteorological Administration (CMA),

  20. Batch routing queuing networks with jump-over blocking

    OpenAIRE

    Boucherie, Richard J.

    1993-01-01

    This paper shows that the equilibrium distribution of a queueing network with batch routing is of product-form if a batch which cannot enter the destination stations, for example as a consequence of capacity constraints, jumps over these stations and selects a new set of destination stations according to the routing probabilities, that is if also customers in the batch who arrive at a non-saturated station jump over that station.

  1. ADVANCES ON BILINEAR MODELING OF BIOCHEMICAL BATCH PROCESSES

    OpenAIRE

    GONZÁLEZ MARTÍNEZ, JOSÉ MARÍA

    2015-01-01

    [EN] This thesis is aimed to study the implications of the statistical modeling approaches proposed for the bilinear modeling of batch processes, develop new techniques to overcome some of the problems that have not been yet solved and apply them to data of biochemical processes. The study, discussion and development of the new methods revolve around the four steps of the modeling cycle, from the alignment, preprocessing and calibration of batch data to the monitoring of batches trajectories....

  2. A Survey of Batch Cataloging Practices and Problems

    OpenAIRE

    Young, Philip

    2011-01-01

    Groups of bibliographic records are added to library catalogs with increasing frequency. Batch cataloging requires knowledge of bulk record transfer as well as current cataloging standards. While more efficient than cataloging items individually, batch cataloging requires different skills and creates new challenges. Responses to a wide-ranging online survey document the workload, tools, practices, and problems of batch cataloging. The unique characteristics of electronic resources affect many...

  3. Spatial and interannual variability in Baltic sprat batch fecundity

    DEFF Research Database (Denmark)

    Haslob, H.; Tomkiewicz, Jonna; Hinrichsen, H.H.;

    2011-01-01

    central Baltic Sea, namely the Bornholm Basin, Gdansk Deep and Southern Gotland Basin. Environmental parameters such as hydrography, fish condition and stock density were tested in order to investigate the observed variability in sprat fecundity. Absolute batch fecundity was found to be positively related...... ambient temperature explained 70% of variability in absolute batch fecundity. Oxygen content and fish condition were not related to sprat batch fecundity. Additionally, a negative effect of stock size on sprat batch fecundity in the Bornholm Basin was revealed. The obtained data and results are important...

  4. SULFATE SOLUBILITY LIMIT VERIFICATION FOR DWPF SLUDGE BATCH 7A

    Energy Technology Data Exchange (ETDEWEB)

    Billings, A.

    2011-04-19

    During processing at the Defense Waste Processing Facility (DWPF), high sulfate concentrations in the feed are a concern to DWPF as it can lead to the formation of a detrimental, sulfate-rich, molten salt phase on the surface of the glass melt pool. To avoid these issues, a sulfate concentration limit was implemented into the Product Composition Control System (PCCS). Related to SB7a frit development efforts, the Savannah River National Laboratory (SRNL) assessed the viability of using the current 0.6 wt % SO{sub 4}{sup 2-} limit set for SB6 (in glass) and the possibility of increasing the SO{sub 4}{sup 2-} solubility limit in PCCS to account for anticipated sulfur concentrations, targeted waste loadings, and inclusion of secondary streams (e.g., Actinide Removal Process (ARP)) with two recommended frits (Frit 418 and Frit 702) for SB7a processing. For a nominal SB7a blend with a 63 inch SB6 heel remaining in Tank 40 (projection SB7a-63), a 0.60 wt% SO{sub 4}{sup 2-} in glass limit was determined for waste loadings of 34 wt% up to 40 wt% with Frit 418 based on crucible melts with batched chemicals. SRNL also examined the inclusion of ARP for the same blending scenario (SB7a-63-ARP) with Frit 418 and at least a 0.6 wt% SO{sub 4}{sup 2-} level, and waste loadings of 34 wt% to 40 wt% were also acceptable. When a visible yellow and/or white sulfate salt layer was visible on the surface of any cooled glass, it was assumed to have surpassed the solubility limit of SO{sub 4}{sup 2-} for that particular composition. All of the glasses fabricated at these concentrations did not exhibit a sulfate rich salt layer on the surface of the glass melt and retained the majority of the batched SO{sub 4}{sup 2-}. At higher levels of SO{sub 4}{sup 2-} 'spiked' into the projected sludge compositions over the aforementioned interval of waste loadings, with Frit 418, low viscosity sulfur layers were observed on the surface of glass melts which confirm exceeding the solubility

  5. Batch sequential designs for computer experiments

    Energy Technology Data Exchange (ETDEWEB)

    Moore, Leslie M [Los Alamos National Laboratory; Williams, Brian J [Los Alamos National Laboratory; Loeppky, Jason L [UBC-OKANAGAN

    2009-01-01

    Computer models simulating a physical process are used in many areas of science. Due to the complex nature of these codes it is often necessary to approximate the code, which is typically done using a Gaussian process. In many situations the number of code runs available to build the Guassian process approximation is limited. When the initial design is small or the underlying response surface is complicated this can lead to poor approximations of the code output. In order to improve the fit of the model, sequential design strategies must be employed. In this paper we introduce two simple distance based metrics that can be used to augment an initial design in a batch sequential manner. In addition we propose a sequential updating strategy to an orthogonal array based Latin hypercube sample. We show via various real and simulated examples that the distance metrics and the extension of the orthogonal array based Latin hypercubes work well in practice.

  6. Maximum thermodynamic efficiency problem in batch distillation

    Directory of Open Access Journals (Sweden)

    J. C. Zavala-Loría

    2011-06-01

    Full Text Available A dynamic batch distillation study of the non-ideal mixture Ethanol-Water is presented. The objective of the study was to calculate an average thermodynamic efficiency of the process under an optimal constant reflux policy and the objective function includes a given production time in order to obtain the desired product quality (measured as the average mole fraction of the accumulated product. An expression for computing the thermodynamic efficiency is presented. The simulation of the column uses a mathematical model considering the complete dynamics of the operation and the problem of optimal control resulting in a non-linear programming problem. A dynamic optimization technique based on a SQP method was used to solve the problem. The average thermodynamic efficiency for the separation process under the conditions presented was 37.95%.

  7. Sewage sludge irradiators: Batch and continuous flow

    International Nuclear Information System (INIS)

    The potential threat to the environment imposed by high pathogenic organism content in municipal wastewater, especially the sludge and the world-wide growing aspirations for a cleaner, salubrious environment have made it mandatory for the sewage and sludge to undergo treatment, prior to their ultimate disposal to mother nature. Incapabilities associated with the conventional wastewater treatments to mitigate the problem of microorganisms have made it necessary to look for other alternatives, radiation treatment being the most reliable, rapid and environmentally sustainable of them. To promote the use of radiation for the sludge hygienization, Department of Atomic Energy has endeavoured to set up an indigenous, Sludge Hygienization Research Irradiator (SHRI) in the city of Baroda. Designed for 18.5 PBq of 60Co to disinfect the digested sludge, the irradiator has additional provision for treatment of effluent and raw sewage. From engineering standpoint, all the subsystems have been functioning satisfactorily since its commissioning in 1990. Prolonged studies, spanning over a period of six years, primarily focused on inactivation of microorganism revealed that 3 kGy dose of gamma radiation is adequate to make the sludge pathogen and odour-free. A dose of 1.6 kGy in raw sewage and 0.5 kGy in effluent reduced coliform counts down to the regulatory discharge limits. These observations reflect a possible cost-effective solution to the burgeoning problem of surface water pollution across the globe. In the past, sub 37 PBq 60Co batch irradiators have been designed and commissioned successfully for the treatment of sludge. Characterized with low dose delivery rates they are well-suited for treating low volumes of sludge in batches. Some concepts of continuous flow 60Co irradiators having larger activities, yet simple and economic in design, are presented in the paper

  8. Identification of root cause of vibration of a liquid-gallium-cooled silicon monochromator and recommendations for abatement

    International Nuclear Information System (INIS)

    Perfect single crystals of silicon are used to monochromate the high-intensity X-ray beams in the Advanced Photon Source at Argonne National Laboratory. Depending on the crystal geometry and the insertion device, the crystal may absorb anywhere from several hundred watts to in excess of a thousand watts. To minimize the thermal distortions in the crystal, this heat must be efficiently removed. Several approaches to this problem are being developed at the APSP including the use of inclined-crystal geometries, cryogenic cooling, liquid-gallium cooling, thin crystals, and the use of diamond. Most of these approaches require coolant flow within the crystals themselves. One issue of concern is the flow-induced vibrations. Two series of tests were performed earlier for a near-prototypical gallium-cooled crystal. This LS note describes a series of tests to measure the general vibration response characteristics of a complete liquid-gallium-cooled inclined-crystal monochromator system

  9. On the stochastic domination for batch-arrival, batch-service and assemble-transfer queueing networks

    OpenAIRE

    Economou, Antonis

    2003-01-01

    Stochastic monotonicity properties for various classes of queueing networks have been established in the literature mainly with the use of coupling constructions. Miyazawa and Taylor (1997) introduced a class of batch-arrival, batch-service and assemble-transfer queueing networks which can be thought of as generalized Jackson networks with batch movements. We study conditions for stochastic domination within this class of networks. The proofs are based on a certain charac...

  10. CRYSTALLIZATION KINETICS OF AMMONIUM PERCHLORATE IN AN AGITATED VESSEL

    OpenAIRE

    Nahidh Kaseer; Rafi' J. Yaqub; Ahmed Khalid

    2013-01-01

    31Overall crystal growth kinetics for ammonium perchlorate in laboratory scale batch  agitated vessel crystallizer have been determined from batch experiments performed in an integral mode. The effects of temperature between 30-60ºC, seed size 0.07, 0.120 and 0.275 mm and stirrer speed 160, 340, and 480 rpm, on the kinetics of crystal growth were investigated. Two different methods, viz. polynomial fitting and initial derivative were used to predict the kinetics expression. In general both me...

  11. Crystallization of glycine with ultrasound

    DEFF Research Database (Denmark)

    Louhi-Kultanen, Marjatta; Karjalainen, Milja; Rantanen, Jukka;

    2006-01-01

    Sonocrystallization has proved to be an efficient tool to influence the external appearance and structure of a crystalline product obtained by various crystallization methods. The present work focuses on high intensity sonocrystallization of glycine by varying amplitude of ultrasound with an...... ultrasound frequency of 20kHz at two temperature ranges 40-50 and 20-30 degrees C in a jacketed 250-ml cooling crystallizer equipped with a stirrer. The polymorph composition of the obtained crystals was analyzed with a temperature variable X-ray powder diffractometer (XRPD). XRPD results showed that...... ultrasound power. This study also showed, the higher the ultrasound amplitude the smaller the crystals obtained....

  12. Batch-to-batch uniformity of bacterial community succession and flavor formation in the fermentation of Zhenjiang aromatic vinegar.

    Science.gov (United States)

    Wang, Zong-Min; Lu, Zhen-Ming; Yu, Yong-Jian; Li, Guo-Quan; Shi, Jin-Song; Xu, Zheng-Hong

    2015-09-01

    Solid-state fermentation of traditional Chinese vinegar is a mixed-culture refreshment process that proceeds for many centuries without spoilage. Here, we investigated bacterial community succession and flavor formation in three batches of Zhenjiang aromatic vinegar using pyrosequencing and metabolomics approaches. Temporal patterns of bacterial succession in the Pei (solid-state vinegar culture) showed no significant difference (P > 0.05) among three batches of fermentation. In all the batches investigated, the average number of community operational taxonomic units (OTUs) decreased dramatically from 119 ± 11 on day 1 to 48 ± 16 on day 3, and then maintained in the range of 61 ± 9 from day 5 to the end of fermentation. We confirmed that, within a batch of fermentation process, the patterns of bacterial diversity between the starter (took from the last batch of vinegar culture on day 7) and the Pei on day 7 were similar (90%). The relative abundance dynamics of two dominant members, Lactobacillus and Acetobacter, showed high correlation (coefficient as 0.90 and 0.98 respectively) among different batches. Furthermore, statistical analysis revealed dynamics of 16 main flavor metabolites were stable among different batches. The findings validate the batch-to-batch uniformity of bacterial community succession and flavor formation accounts for the quality of Zhenjiang aromatic vinegar. Based on our understanding, this is the first study helps to explain the rationality of age-old artistry from a scientific perspective. PMID:25998816

  13. TIME-TEMPERATURE-TRANSFORMATION DIAGRAMS FOR THE SLUDGE BATCH 3 - FRIT 418 GLASS SYSTEM

    International Nuclear Information System (INIS)

    As a part of the Waste Acceptance Product Specifications (WAPS) for Vitrified High-Level Waste Forms defined by the Department of Energy - Office of Environmental Management, the phase stability must be determined for each of the projected high-level waste (HLW) types at the Savannah River Site (SRS). Specifically, WAPS 1.4.1 requires the glass transition temperature (Tg) to be defined and time-temperature-transformation (TTT) diagrams to be developed. The Tg of a glass is an indicator of the approximate temperature where the supercooled liquid converts to a solid on cooling or conversely, where the solid begins to behave as a viscoelastic solid on heating. A TTT diagram identifies the crystalline phases that can form as a function of time and temperature for a given waste type or more specifically, the borosilicate glass waste form. In order to assess durability, the Product Consistency Test (PCT) was used and the durability results compared to the Environmental Assessment (EA) glass. The measurement of glass transition temperature and the development of TTT diagrams have already been performed for the seven Defense Waste Processing Facility (DWPF) projected compositions as defined in the Waste Form Compliance Plan (WCP). These measurements were performed before DWPF start-up and the results were incorporated in Volume 7 of the Waste Form Qualification Report (WQR). Additional information exists for other projected compositions, but overall these compositions did not consider some of the processing scenarios now envisioned for DWPF to accelerate throughput. Changes in DWPF processing strategy have required this WAPS specification to be revisited to ensure that the resulting phases have been bounded. Frit 418 was primarily used to process HLW Sludge Batch 3 (SB3) at 38% waste loading (WL) through the DWPF. The Savannah River National Laboratory (SRNL) fabricated a cache of glass from reagent grade oxides to simulate the SB3-Frit 418 system at a 38 wt % WL for glass

  14. TIME-TEMPERATURE-TRANSFORMATION DIAGRAMS FOR THE SLUDGE BATCH 3 - FRIT 418 GLASS SYSTEM

    Energy Technology Data Exchange (ETDEWEB)

    Billings, A; Tommy Edwards, T

    2009-03-03

    As a part of the Waste Acceptance Product Specifications (WAPS) for Vitrified High-Level Waste Forms defined by the Department of Energy - Office of Environmental Management, the phase stability must be determined for each of the projected high-level waste (HLW) types at the Savannah River Site (SRS). Specifically, WAPS 1.4.1 requires the glass transition temperature (Tg) to be defined and time-temperature-transformation (TTT) diagrams to be developed. The Tg of a glass is an indicator of the approximate temperature where the supercooled liquid converts to a solid on cooling or conversely, where the solid begins to behave as a viscoelastic solid on heating. A TTT diagram identifies the crystalline phases that can form as a function of time and temperature for a given waste type or more specifically, the borosilicate glass waste form. In order to assess durability, the Product Consistency Test (PCT) was used and the durability results compared to the Environmental Assessment (EA) glass. The measurement of glass transition temperature and the development of TTT diagrams have already been performed for the seven Defense Waste Processing Facility (DWPF) projected compositions as defined in the Waste Form Compliance Plan (WCP). These measurements were performed before DWPF start-up and the results were incorporated in Volume 7 of the Waste Form Qualification Report (WQR). Additional information exists for other projected compositions, but overall these compositions did not consider some of the processing scenarios now envisioned for DWPF to accelerate throughput. Changes in DWPF processing strategy have required this WAPS specification to be revisited to ensure that the resulting phases have been bounded. Frit 418 was primarily used to process HLW Sludge Batch 3 (SB3) at 38% waste loading (WL) through the DWPF. The Savannah River National Laboratory (SRNL) fabricated a cache of glass from reagent grade oxides to simulate the SB3-Frit 418 system at a 38 wt % WL for glass

  15. Numerical and experimental simulation of mechanical and microstructural transformations in Batch annealing steels; Evaluacion numerical y experimental de las transformaciones mecanicas y microestrurales en aceros recocidos Batch

    Energy Technology Data Exchange (ETDEWEB)

    Monsalve, A.; Artigas, A.; Celentano, D.; Melendez, F.

    2004-07-01

    The heating and cooling curves during batch annealing process of low carbon steel have been modeled using the finite element technique. This has allowed to predict the transient thermal profile for every point of the annealed coils, particularly for the hottest and coldest ones. Through experimental measurements, the results have been adequately validated since a good agreement has been found between experimental values and those predicted by the model. Moreover, an Avrami recrystallization model. Moreover, and Avrami recrystallization model has been coupled to this thermal balance computation. Interrupted annealing experiments have been made by measuring the recrystallized fraction on the extreme points of the coil foe different times. These data gave the possibility to validate the developed recrystallization model through a reasonably good numerical-experimental fittings. (Author) 6 refs.

  16. Continuous Cellulosic Bioethanol Fermentation by Cyclic Fed-Batch Cocultivation

    OpenAIRE

    Jiang, He-Long; He, Qiang; He, Zhili; Hemme, Christopher L.; Wu, Liyou; Zhou, Jizhong

    2013-01-01

    Cocultivation of cellulolytic and saccharolytic microbial populations is a promising strategy to improve bioethanol production from the fermentation of recalcitrant cellulosic materials. Earlier studies have demonstrated the effectiveness of cocultivation in enhancing ethanolic fermentation of cellulose in batch fermentation. To further enhance process efficiency, a semicontinuous cyclic fed-batch fermentor configuration was evaluated for its potential in enhancing the efficiency of cellulose...

  17. Communication and control in small batch part manufacturing

    NARCIS (Netherlands)

    Tiemersma, J.J.; Curtis, W.; Kals, H.J.J.

    1993-01-01

    This paper reports on the development of a real-time control network as an integrated part of a shop floor control system for small batch part manufacturing. The shop floor control system is called the production control system (PCS). The PCS aims at an improved control of small batch part manufactu

  18. Batch variation between branchial cell cultures: An analysis of variance

    DEFF Research Database (Denmark)

    Hansen, Heinz Johs. Max; Grosell, M.; Kristensen, L.

    2003-01-01

    We present in detail how a statistical analysis of variance (ANOVA) is used to sort out the effect of an unexpected batch-to-batch variation between cell cultures. Two separate cultures of rainbow trout branchial cells were grown on permeable filtersupports ("inserts"). They were supposed to be...

  19. Searching CA Condensates, On-Line and Batch.

    Science.gov (United States)

    Kaminecki, Ronald M.; And Others

    Batch mode processing is compared, using cost-effectiveness, with on-line processing for computer-aided searching of chemical abstracts. Consideration for time, need, coverage, and adaptability are found to be the criteria by which a searcher selects a method, and sometimes both methods are used. There is a tradeoff between batch mode's slower…

  20. 40 CFR Table 1 to Subpart H of... - Batch Processes

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 9 2010-07-01 2010-07-01 false Batch Processes 1 Table 1 to Subpart H of Part 63 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS... Subpart H of Part 63—Batch Processes Monitoring Frequency for Equipment Other than Connectors...

  1. System Requirements for On-Line and Batch Retrieval.

    Science.gov (United States)

    American Society for Information Science, Washington, DC. Special Interest Group on Computerized Retrieval Services.

    Three papers on system requirements for on-line and batch retrieval presented at the American Society for Information Science (ASIS) annual meeting are included here. At G.D. Searle, data for records related to pharmacology screening are used in a batch system, and an on-line system is used to search information on mutagenic, carcinogenic, and…

  2. Improved batch correction in untargeted MS-based metabolomics

    NARCIS (Netherlands)

    Wehrens, Ron; Hageman, Jos A.; Eeuwijk, van Fred; Kooke, Rik; Flood, Pádraic J.; Wijnker, Erik; Keurentjes, Joost J.B.; Lommen, Arjen; Eekelen, van Henriëtte D.L.M.; Hall, Robert D.; Mumm, Roland; Vos, de Ric C.H.

    2016-01-01

    Introduction: Batch effects in large untargeted metabolomics experiments are almost unavoidable, especially when sensitive detection techniques like mass spectrometry (MS) are employed. In order to obtain peak intensities that are comparable across all batches, corrections need to be performed. S

  3. Dynamic Simulation of Batch Photocatalytic Reactor (BPR) for Wastewater Treatment

    Science.gov (United States)

    Dutta, Suman

    2012-08-01

    Reactive dyes discharged from dyehouse causes a serious environmental problem. UV/TiO2 photocatalysis has been employed effectively for these organic dyes removal from dye-house effluent. This process produces less amount of non-toxic final product. In this paper a photocatalytic reactor has been designed for Reactive red 198 (RR198) removal from aqueous solution. The reactor is operating in batch mode. After each batch, TiO2 catalyst has been separated and recycled in the next batch. Mathematical model equation of this batch photocatalytic reactor (BPR) has been developed considering Langmuir-Hinshelwood kinetics. Simulation of BPR has been carried out using fourth order Runge-Kutta (RK) method and fifth order RK method (Butcher method). This simulation results can be used to develop an automatic photocatlytic reactor for industrial wastewater treatment. Catalyst activity decay and its effect on each batch have been incorporated in this model.

  4. Mass Transfer and Kinetics Study of Heterogeneous Semi-Batch Precipitation of Magnesium Carbonate

    DEFF Research Database (Denmark)

    Han, B.; Qu, H. Y.; Niemi, H.;

    2014-01-01

    Precipitation kinetics and mass transfer of magnesium carbonate (MgCO3) hydrates from a reaction of magnesium hydroxide (Mg(OH)(2)) and CO2 were analyzed. The effect of CO2 flow rate and mixing intensity on precipitation was investigated under ambient temperature and atmospheric pressure. Raman...... spectroscopy was used to determine the composition of the solids during semi-batch crystallization. The obtained spectra revealed the dissolution of Mg(OH)(2) and the formation of MgCO3. The precipitation rate increased with higher gas flow rate. The rotation speed of the stirrer had a significant effect on...... the dissolution of Mg(OH)(2). In the researched system, the main driver of the precipitation kinetics was the mass transfer of CO2. Nesquehonite (MgCO3 center dot 3H(2)O), as needle-like crystals, was precipitated as the main product. Raman spectroscopy can serve as a potential tool to monitor the...

  5. Biodenitrification in Sequencing Batch Reactors. Final report

    Energy Technology Data Exchange (ETDEWEB)

    Silverstein, J. [Colorado Univ., Boulder, CO (United States). Dept. of Civil, Environmental, and Architectural Engineering

    1996-01-23

    One plan for stabilization of the Solar Pond waters and sludges at Rocky Flats Plant (RFP), is evaporation and cement solidification of the salts to stabilize heavy metals and radionuclides for land disposal as low-level mixed waste. It has been reported that nitrate (NO{sub 3}{sub {minus}}) salts may interfere with cement stabilization of heavy metals and radionuclides. Therefore, biological nitrate removal (denitrification) may be an important pretreatment for the Solar Pond wastewaters at RFP, improving the stability of the cement final waste form, reducing the requirement for cement (or pozzolan) additives and reducing the volume of cemented low-level mixed waste requiring ultimate disposal. A laboratory investigation of the performance of the Sequencing Batch Reactor (SBR) activated sludge process developed for nitrate removal from a synthetic brine typical of the high-nitrate and high-salinity wastewaters in the Solar Ponds at Rocky Flats Plant was carried out at the Environmental Engineering labs at the University of Colorado, Boulder, between May 1, 1994 and October 1, 1995.

  6. Biodenitrification in Sequencing Batch Reactors. Final report

    International Nuclear Information System (INIS)

    One plan for stabilization of the Solar Pond waters and sludges at Rocky Flats Plant (RFP), is evaporation and cement solidification of the salts to stabilize heavy metals and radionuclides for land disposal as low-level mixed waste. It has been reported that nitrate (NO3-) salts may interfere with cement stabilization of heavy metals and radionuclides. Therefore, biological nitrate removal (denitrification) may be an important pretreatment for the Solar Pond wastewaters at RFP, improving the stability of the cement final waste form, reducing the requirement for cement (or pozzolan) additives and reducing the volume of cemented low-level mixed waste requiring ultimate disposal. A laboratory investigation of the performance of the Sequencing Batch Reactor (SBR) activated sludge process developed for nitrate removal from a synthetic brine typical of the high-nitrate and high-salinity wastewaters in the Solar Ponds at Rocky Flats Plant was carried out at the Environmental Engineering labs at the University of Colorado, Boulder, between May 1, 1994 and October 1, 1995

  7. Bottleneck Management in Discrete Batch Production

    Directory of Open Access Journals (Sweden)

    Ferenčíková Denisa

    2012-06-01

    Full Text Available Today, production planning and scheduling becomes very important part of production management because companies have to react to dynamic market conditions and rising customers´ requirements for shorter delivery times, lower prices and better quality and services. They can use a lot of sophisticated methods and approaches to make their planning processes more efficient and thus meet growing customers´ requirements. However, using these new approaches is not so easy in all types of production systems. This paper deals with production planning and scheduling in discrete batch production that is just an example of very complicated production system. This type of production process is susceptible to demand fluctuation and facility exceptions and this implies bottleneck shifting. Therefore it is quite difficult to implement methods such as Theory of Constraints (TOC for production planning improvement in the standard way. One part of this paper is a case study wherecurrent production planning and scheduling in real factory is improved just through the use TOC principles.

  8. Cavity QED experiments with ion Coulomb crystals

    DEFF Research Database (Denmark)

    Herskind, Peter Fønss; Dantan, Aurélien; Marler, Joan; Albert, Magnus; Drewsen, Michael

    Cavity QED experimental results demonstrating collective strong coupling between ensembles of atomic ions cooled into Coulomb crystals and optical cavity fields have been achieved. Collective Zeeman coherence times of milliseconds have furthermore been obtained.......Cavity QED experimental results demonstrating collective strong coupling between ensembles of atomic ions cooled into Coulomb crystals and optical cavity fields have been achieved. Collective Zeeman coherence times of milliseconds have furthermore been obtained....

  9. Kinetic study of batch and fed-batch enzymatic saccharification of pretreated substrate and subsequent fermentation to ethanol

    Directory of Open Access Journals (Sweden)

    Gupta Rishi

    2012-03-01

    Full Text Available Abstract Background Enzymatic hydrolysis, the rate limiting step in the process development for biofuel, is always hampered by its low sugar concentration. High solid enzymatic saccharification could solve this problem but has several other drawbacks such as low rate of reaction. In the present study we have attempted to enhance the concentration of sugars in enzymatic hydrolysate of delignified Prosopis juliflora, using a fed-batch enzymatic hydrolysis approach. Results The enzymatic hydrolysis was carried out at elevated solid loading up to 20% (w/v and a comparison kinetics of batch and fed-batch enzymatic hydrolysis was carried out using kinetic regimes. Under batch mode, the actual sugar concentration values at 20% initial substrate consistency were found deviated from the predicted values and the maximum sugar concentration obtained was 80.78 g/L. Fed-batch strategy was implemented to enhance the final sugar concentration to 127 g/L. The batch and fed-batch enzymatic hydrolysates were fermented with Saccharomyces cerevisiae and ethanol production of 34.78 g/L and 52.83 g/L, respectively, were achieved. Furthermore, model simulations showed that higher insoluble solids in the feed resulted in both smaller reactor volume and shorter residence time. Conclusion Fed-batch enzymatic hydrolysis is an efficient procedure for enhancing the sugar concentration in the hydrolysate. Restricting the process to suitable kinetic regimes could result in higher conversion rates.

  10. 21 CFR 320.35 - Requirements for in vitro testing of each batch.

    Science.gov (United States)

    2010-04-01

    ... 21 Food and Drugs 5 2010-04-01 2010-04-01 false Requirements for in vitro testing of each batch... of each batch. If a bioequivalence requirement specifies a currently available in vitro test or an in... conduct the test on a sample of each batch of the drug product to assure batch-to-batch uniformity....

  11. 40 CFR 204.57-7 - Acceptance and rejection of batch sequence.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 24 2010-07-01 2010-07-01 false Acceptance and rejection of batch... § 204.57-7 Acceptance and rejection of batch sequence. (a) The manufacturer will continue to inspect consecutive batches until the batch sequence is accepted or rejected. The batch sequence will be accepted...

  12. 40 CFR 63.1322 - Batch process vents-reference control technology.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 11 2010-07-01 2010-07-01 true Batch process vents-reference control... Batch process vents—reference control technology. (a) Batch process vents. The owner or operator of a... venting to any combustion control device, and thus make the batch process vent, aggregate batch...

  13. Morphologically structured model for antitumoral retamycin production during batch and fed-batch cultivations of Streptomyces olindensis.

    Science.gov (United States)

    Giudici, Reinaldo; Pamboukian, Celso R D; Facciotti, Maria Cândida R

    2004-05-20

    A morphologically structured model is proposed to describe trends in biomass growth, substrate consumption, and antitumoral retamycin production during batch and fed-batch cultivations of Streptomyces olindensis. Filamentous biomass is structured into three morphological compartments (apical, subapical, and hyphal), and the production of retamycin, a secondary metabolite, is assumed to take place in the subapical cell compartment. Model accounts for the effect of glucose as well as complex nitrogen source on both the biomass growth and retamycin production. Laboratory data from bench-scale batch and fed-batch fermentations were used to estimate some model parameters by nonlinear regression. The predictive capability of the model was then tested for additional fed-batch and continuous experiments not used in the previous fitting procedure. The model predictions show fair agreement to the experimental data. The proposed model can be useful for further studies on process optimization and control. PMID:15112294

  14. Liquid nitrogen cooled X-ray monochromator for high total power loads

    CERN Document Server

    Rowen, M; Rabedeau, T

    2001-01-01

    A liquid nitrogen (LN) cooled X-ray monochromator has been designed and built for the high power loads of wigglers on the 500 mA SPEAR3 ring. The monochromator features two crystals sets for remote crystal changes, internally cooled first crystals with up to 10 atm LN coolant pressure, and low strain LN to vacuum seals. The system has been operated at one half the design total power with no thermal broadening of the rocking curve width.

  15. Optimised crystal morphologies for active pharmaceutical ingredients and related studies

    OpenAIRE

    Horgan, Danielle E.

    2015-01-01

    The majority of active pharmaceutical ingredients (APIs) are crystalline solids in their pure forms. Crystalline solids have definable morphologies, i.e. shape and size. Crystal morphology is determined by both the internal structure of the crystals and external factors during growth from solution. The morphology of a crystal batch can affect key processes during manufacturing. Companies generally accept whatever morphology the manufacturing process provides and deal with any subsequent probl...

  16. 40 CFR Table 6 to Subpart U of... - Group 1 Batch Front-End Process Vents and Aggregate Batch Vent Streams-Monitoring, Recordkeeping...

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 9 2010-07-01 2010-07-01 false Group 1 Batch Front-End Process Vents and Aggregate Batch Vent Streams-Monitoring, Recordkeeping, and Reporting Requirements 6 Table 6 to... 6 to Subpart U of Part 63—Group 1 Batch Front-End Process Vents and Aggregate Batch Vent...

  17. 40 CFR Table 7 to Subpart Jjj of... - Group 1 Batch Process Vents and Aggregate Batch Vent Streams-Monitoring, Recordkeeping, and...

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 11 2010-07-01 2010-07-01 true Group 1 Batch Process Vents and Aggregate Batch Vent Streams-Monitoring, Recordkeeping, and Reporting Requirements 7 Table 7 to Subpart JJJ... Table 7 to Subpart JJJ of Part 63—Group 1 Batch Process Vents and Aggregate Batch Vent...

  18. Crystal Meth

    Science.gov (United States)

    ... for: Navigation Home / Stories of Hope / Crystal meth Crystal meth Story Of Hope By giovanni January 3rd, ... about my drug addiction having to deal with Crystal meth. I am now in recovery and fighting ...

  19. Radiant Floor Cooling Systems

    DEFF Research Database (Denmark)

    Olesen, Bjarne W.

    2008-01-01

    In many countries, hydronic radiant floor systems are widely used for heating all types of buildings such as residential, churches, gymnasiums, hospitals, hangars, storage buildings, industrial buildings, and smaller offices. However, few systems are used for cooling.This article describes a floo...... cooling system that includes such considerations as thermal comfort of the occupants, which design parameters will influence the cooling capacity and how the system should be controlled. Examples of applications are presented....

  20. Water cooled nuclear reactor

    International Nuclear Information System (INIS)

    The description is given of a water cooled nuclear reactor comprising a core, cooling water that rises through the core, vertical guide tubes located inside the core and control rods vertically mobile in the guide tubes. In this reactor the cooling water is divided into a first part introduced at the bottom end of the core and rising through it and a second part introduced at the top end of the guide tubes so as to drop in them

  1. Solar absorption cooling

    OpenAIRE

    Kim, D.-S.

    2007-01-01

    As the world concerns more and more on global climate changes and depleting energy resources, solar cooling technology receives increasing interests from the public as an environment-friendly and sustainable alternative. However, making a competitive solar cooling machine for the market still remains a challenge to the academic and industrial communities. In an effort to meet this challenge, this thesis reports the R&D activities carried out for the development of a new solar cooling machine,...

  2. Characterization of ion Coulomb crystals for fundamental sciences

    Energy Technology Data Exchange (ETDEWEB)

    Okada, Kunihiro, E-mail: okada-k@sophia.ac.jp [Sophia University, Department of Physics (Japan); Ichikawa, Masanari [RIKEN Nishina Center for Accelerator-Based Science (Japan); Wada, Michiharu, E-mail: mw@riken.go.jp [Sophia University, Department of Physics (Japan)

    2015-11-15

    We performed classical molecular dynamics (MD) simulations in order to search the conditions for efficient sympathetic cooling of highly charged ions (HCIs) in a linear Paul trap. Small two-component ion Coulomb crystals consisting of laser-cooled ions and HCIs were characterized by the results of the MD simulations. We found that the spatial distribution is determined by not only the charge-to-mass ratio but also the space charge effect. Moreover, the simulation results suggest that the temperature of HCIs do not necessarily decrease with increasing the number of laser-cooled ions in the cases of linear ion crystals. We also determined the cooling limit of sympathetically cooled {sup 165}Ho{sup 14+} ions in small linear ion Coulomb crystals. The present results show that sub-milli-Kelvin temperatures of at least 10 Ho{sup 14+} ions will be achieved by sympathetic cooling with a single laser-cooled Be{sup +}.

  3. Initial Cooling Experiment (ICE)

    CERN Multimedia

    Photographic Service

    1978-01-01

    In 1977, in a record-time of 9 months, the magnets of the g-2 experiment were modified and used to build a proton/antiproton storage ring: the "Initial Cooling Experiment" (ICE). It served for the verification of the cooling methods to be used for the "Antiproton Project". Stochastic cooling was proven the same year, electron cooling followed later. Also, with ICE the experimental lower limit for the antiproton lifetime was raised by 9 orders of magnitude: from 2 microseconds to 32 hours. For its previous life as g-2 storage ring, see 7405430. More on ICE: 7711282, 7809081, 7908242.

  4. Emergency core cooling device

    International Nuclear Information System (INIS)

    The present invention provides an emergency core cooling device without using a reactor core spray device, in which the reactor core of a BWR type reactor is cooled effectively and certainly by flooding of the reactor core. That is, the emergency core cooling device comprises a high pressure core water injection system as an emergency core cooling system (ECCS) for cooling the inside of the reactor core upon loss of coolants accident (LOCA). By means of the high pressure core water injection system, water is injected from a condensate storage vessel or a suppression pool to the inside of the reactor core shroud upon LOCA. Accordingly, the reactor core is cooled effectively by reactor core flooding. In this device, cooling water can be injected to the inside of the reactor core shroud by means of the high pressure core injection system upon LOCA in which the coolants are discharged from the outside of the reactor core shroud. On the other hand, upon LOCA in which the coolants are discharged from the inside of the reactor core shroud, the cooling water can be supplied to the reactor core by means of a cooling system upon reactor isolation which injects water to the outside of the reactor core or a low pressure water injection system. (I.S.)

  5. Air cooling system

    International Nuclear Information System (INIS)

    A procedure for cooling the steam from a turbine used in conjunction with a power nuclear reactor has been described in the main patent. According to said procedure, use is made of a circuit where a two-phase mixture is circulated, said closed circuit connecting the turbine condenser to a cooling tower. According to the present addition patent, the cooling structure is provided with cooling fins previously hollowed in view of increasing the interface between the fluid and said structure, which improves the performance of the system

  6. High energy electron cooling

    Energy Technology Data Exchange (ETDEWEB)

    Parkhomchuk, V. [Budker Institute of Nuclear Physics, Novosibirsk (Russian Federation)

    1997-09-01

    High energy electron cooling requires a very cold electron beam. The questions of using electron cooling with and without a magnetic field are presented for discussion at this workshop. The electron cooling method was suggested by G. Budker in the middle sixties. The original idea of the electron cooling was published in 1966. The design activities for the NAP-M project was started in November 1971 and the first run using a proton beam occurred in September 1973. The first experiment with both electron and proton beams was started in May 1974. In this experiment good result was achieved very close to theoretical prediction for a usual two component plasma heat exchange.

  7. A New Batch Verifying Scheme for Identifying Illegal Signatures

    Institute of Scientific and Technical Information of China (English)

    Adrian Atanasiu

    2013-01-01

    The concept of batch verifying multiple digital signatures is to find a method by which multiple digital signatures can be verified simultaneously in a lower time complexity than separately verifying all the signatures.In this article,we analyze the complexity of the batch verifying schemes defined by Li,Hwang and Chen in 2010,and propose a new batch verifying multiple digital signature scheme,in two variants:one for RSA-by completing the Harn's schema with an identifying illegal signatures algorithm,and the other adapted for a modified Elliptic Curve Digital Signature Algorithm protocol.

  8. Examining the role of canister cooling conditions on the formation of nepheline from nuclear waste glasses

    Energy Technology Data Exchange (ETDEWEB)

    Christian, J. H. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL)

    2015-09-01

    Nepheline (NaAlSiO₄) crystals can form during slow cooling of high-level waste (HLW) glass after it has been poured into a waste canister. Formation of these crystals can adversely affect the chemical durability of the glass. The tendency for nepheline crystallization to form in a HLW glass increases with increasing concentrations of Al₂O₃ and Na₂O.

  9. Large improvements in application throughput of long-running multi-component applications using batch grids

    OpenAIRE

    Sundari, Sivagama M.; Vadhiyar, Sathish S.; Nanjundiah, Ravi S.

    2012-01-01

    Computational grids with multiple batch systems (batch grids) can be powerful infrastructures for executing long-running multi-component parallel applications. In this paper, we evaluate the potential improvements in throughput of long-running multi-component applications when the different components of the applications are executed on multiple batch systems of batch grids. We compare the multiple batch executions with executions of the components on a single batch system without increasing ...

  10. Liquid metal cooling of synchrotron optics

    International Nuclear Information System (INIS)

    The installation of insertion devices at existing synchrotron facilities around the world has stimulated the development of new ways to cool the optical elements in the associated x-ray beamlines. Argonne has been a leader in the development of liquid metal cooling for high heat load x-ray optics for the next generation of synchrotron facilities. The high thermal conductivity, high volume specific heat, low kinematic viscosity, and large working temperature range make liquid metals a very efficient heat transfer fluid. A wide range of liquid metals were considered in the initial phase of this work. The most promising liquid metal cooling fluid identified to date is liquid gallium, which appears to have all the desired properties and the fewest number of undesired features of the liquid metals examined. Besides the special features of liquid metals that make them good heat transfer fluids, the very low vapor pressure over a large working temperature range make liquid gallium an ideal cooling fluid for use in a high vacuum environment. A leak of the liquid gallium into the high vacuum and even into very high vacuum areas will not result in any detectable vapor pressure and may even improve the vacuum environment as the liquid gallium combines with any water vapor or oxygen present in the system. The practical use of a liquid metal for cooling silicon crystals and other high heat load applications depends on having a convenient and efficient delivery system. The requirements for a typical cooling system for a silicon crystal used in a monochromator are pumping speeds of 2 to 5 gpm (120 cc per sec to 600 cc per sec) at pressures up to 100 psi

  11. Minimizing makespan in a two-machine no-wait flow shop with batch processing machines

    OpenAIRE

    Muthuswamy, Shanthi; V??lez Gallego, Mario C??sar; Rojas Santiago, Miguel; Maya Toro, Jairo

    2012-01-01

    Given a set of jobs and two batch processing machines (BPMs) arranged in a flow shop environment,the objective is to batch the jobs and sequence the batches such that the makespan is minimized. The job sizes, ready times, and processing times on the two BPMs are knowN -- The batch processing machines can process a batch of jobs as long as the total size of all the jobs assigned to a batch does not exceed its capacity -- Once the jobs are batched, the processing time of the batch on the first ...

  12. Realisation of a novel crystal bender for a fast double crystal monochromator

    CERN Document Server

    Zaeper, R; Wollmann, R; Luetzenkirchen-Hecht, D; Frahm, R

    2001-01-01

    A novel crystal bender for an X-ray undulator beamline as part of a fast double crystal monochromator development for full EXAFS energy range was characterized. Rocking curves of the monochromator crystal system were recorded under different heat loads and bending forces of the indirectly cooled first Si(1 1 1) crystal. The monochromator development implements new piezo-driven tilt tables with wide angular range to adjust the crystals' Bragg angles and a high pressure actuated bender mechanism for the first crystal.

  13. Measure Guideline: Ventilation Cooling

    Energy Technology Data Exchange (ETDEWEB)

    Springer, D.; Dakin, B.; German, A.

    2012-04-01

    The purpose of this measure guideline on ventilation cooling is to provide information on a cost-effective solution for reducing cooling system energy and demand in homes located in hot-dry and cold-dry climates. This guideline provides a prescriptive approach that outlines qualification criteria, selection considerations, and design and installation procedures.

  14. Cooling of electronic equipment

    DEFF Research Database (Denmark)

    A. Kristensen, Anders Schmidt

    2003-01-01

    Cooling of electronic equipment is studied. The design size of electronic equipment decrease causing the thermal density to increase. This affect the cooling which can cause for example failures of critical components due to overheating or thermal induced stresses. Initially a pin fin heat sink...

  15. Coherent electron cooling

    Energy Technology Data Exchange (ETDEWEB)

    Litvinenko,V.

    2009-05-04

    Cooling intense high-energy hadron beams remains a major challenge in modern accelerator physics. Synchrotron radiation is still too feeble, while the efficiency of two other cooling methods, stochastic and electron, falls rapidly either at high bunch intensities (i.e. stochastic of protons) or at high energies (e-cooling). In this talk a specific scheme of a unique cooling technique, Coherent Electron Cooling, will be discussed. The idea of coherent electron cooling using electron beam instabilities was suggested by Derbenev in the early 1980s, but the scheme presented in this talk, with cooling times under an hour for 7 TeV protons in the LHC, would be possible only with present-day accelerator technology. This talk will discuss the principles and the main limitations of the Coherent Electron Cooling process. The talk will describe the main system components, based on a high-gain free electron laser driven by an energy recovery linac, and will present some numerical examples for ions and protons in RHIC and the LHC and for electron-hadron options for these colliders. BNL plans a demonstration of the idea in the near future.

  16. The final cool down

    CERN Multimedia

    Thursday 29th May, the cool-down of the final sector (sector 4-5) of LHC has begun, one week after the start of the cool-down of sector 1-2. It will take five weeks for the sectors to be cooled from room temperature to 5 K and a further two weeks to complete the cool down to 1.9 K and the commissioning of cryogenic instrumentation, as well as to fine tune the cryogenic plants and the cooling loops of cryostats.Nearly a year and half has passed since sector 7-8 was cooled for the first time in January 2007. For Laurent Tavian, AT/CRG Group Leader, reaching the final phase of the cool down is an important milestone, confirming the basic design of the cryogenic system and the ability to operate complete sectors. “All the sectors have to operate at the same time otherwise we cannot inject the beam into the machine. The stability and reliability of the cryogenic system and its utilities are now very important. That will be the new challenge for the coming months,” he explains. The status of the cool down of ...

  17. Passive evaporative cooling

    NARCIS (Netherlands)

    Tzoulis, A.

    2011-01-01

    This "designers' manual" is made during the TIDO-course AR0531 Smart & Bioclimatic Design. Passive techniques for cooling are a great way to cope with the energy problem of the present day. This manual introduces passive cooling by evaporation. These methods have been used for many years in traditi

  18. DOAS, Radiant Cooling Revisited

    Energy Technology Data Exchange (ETDEWEB)

    Hastbacka, Mildred; Dieckmann, John; Bouza, Antonio

    2012-12-01

    The article discusses dedicated outdoor air systems (DOAS) and radiant cooling technologies. Both of these topics were covered in previous ASHRAE Journal columns. This article reviews the technologies and their increasing acceptance. The two steps that ASHRAE is taking to disseminate DOAS information to the design community, available energy savings and the market potential of radiant cooling systems are addressed as well.

  19. Data center cooling method

    Science.gov (United States)

    Chainer, Timothy J.; Dang, Hien P.; Parida, Pritish R.; Schultz, Mark D.; Sharma, Arun

    2015-08-11

    A method aspect for removing heat from a data center may use liquid coolant cooled without vapor compression refrigeration on a liquid cooled information technology equipment rack. The method may also include regulating liquid coolant flow to the data center through a range of liquid coolant flow values with a controller-apparatus based upon information technology equipment temperature threshold of the data center.

  20. Solar absorption cooling

    NARCIS (Netherlands)

    Kim, D.-S.

    2007-01-01

    As the world concerns more and more on global climate changes and depleting energy resources, solar cooling technology receives increasing interests from the public as an environment-friendly and sustainable alternative. However, making a competitive solar cooling machine for the market still remain

  1. Gas-cooled reactors

    International Nuclear Information System (INIS)

    The present study is the second part of a general survey of Gas Cooled Reactors (GCRs). In this part, the course of development, overall performance and present development status of High Temperature Gas Cooled Reactors (HTCRs) and advances of HTGR systems are reviewed. (author)

  2. Xylitol production by Candida parapsilosis under fed-batch culture

    OpenAIRE

    Furlan Sandra A.; Castro Heizir F. de

    2001-01-01

    Xylitol production by Candida parapsilosis was investigated under fed-batch cultivation, using single (xylose) or mixed (xylose and glucose) sugars as substrates. The presence of glucose in the medium induced the production of ethanol as secondary metabolite and improved specific rates of growth, xylitol formation and substrate consumption. Fractionated supply of the feed medium at constant sugar concentration did not promote any increase on the productivity compared to the single batch culti...

  3. Statistical strategies for microRNAseq batch effect reduction

    OpenAIRE

    Guo, Yan; Zhao, Shilin; Su, Pei-Fang; Li, Chung-I; Ye, Fei; Flynn, Charles R.; Shyr, Yu

    2014-01-01

    RNAseq technology is replacing microarray technology as the tool of choice for gene expression profiling. While providing much richer data than microarray, analysis of RNAseq data has been much more challenging. Among the many difficulties of RNAseq analysis, correctly adjusting for batch effect is a pivotal one for large-scale RNAseq based studies. The batch effect of RNAseq data is most obvious in microRNA (miRNA) sequencing studies. Using real miRNA sequencing (miRNAseq) dat...

  4. Optimal configuration, design and operation of batch distillation processes

    OpenAIRE

    Low, K. H.

    2003-01-01

    The overall objective of this thesis is to study the optimal configuration. design and operating policy of batch distillation processes in different separation scenarios. In so doing, this work also aims to provide conceptual insights and compare the performance of the traditional regular column against unconventional columns. In the first part of the thesis, the optimal operation of extractive batch distillation is investigated. A rigorous dynamic optimisation approach based o...

  5. APPLICATION OF MODEL PREDICTIVE CONTROL TO BATCH POLYMERIZATION REACTOR

    OpenAIRE

    N.M. Ghasem; Hussain, M. A.; S. A. Sata

    2006-01-01

    The absence of a stable operational state in polymerization reactors that operates in batches is factor that determine the need of a special control system. In this study, advanced control methodology is implemented for controlling the operation of a batch polymerization reactor for polystyrene production utilizingmodel predictive control. By utilizing a model of the polymerization process, the necessary operational conditions were determined for producing the polymer within the desired chara...

  6. Dynamic Extensions of Batch Systems with Cloud Resources

    International Nuclear Information System (INIS)

    Compute clusters use Portable Batch Systems (PBS) to distribute workload among individual cluster machines. To extend standard batch systems to Cloud infrastructures, a new service monitors the number of queued jobs and keeps track of the price of available resources. This meta-scheduler dynamically adapts the number of Cloud worker nodes according to the requirement profile. Two different worker node topologies are presented and tested on the Amazon EC2 Cloud service.

  7. Fault Diagnosis of Batch Reactor Using Machine Learning Methods

    OpenAIRE

    2014-01-01

    Fault diagnosis of a batch reactor gives the early detection of fault and minimizes the risk of thermal runaway. It provides superior performance and helps to improve safety and consistency. It has become more vital in this technical era. In this paper, support vector machine (SVM) is used to estimate the heat release (Qr) of the batch reactor both normal and faulty conditions. The signature of the residual, which is obtained from the difference between nominal and estimated faulty Qr values,...

  8. Muon cooling channels

    International Nuclear Information System (INIS)

    Parameters of muon cooling channels are discussed that achieve cooling of a muon beam from initial to final emittances in all three degrees of freedom in a given length. Published theories of ionisation cooling yield equilibrium emittances from multiple scattering and energy straggling, and partition numbers. Limits are obtained on the amplitude functions in all three degrees of freedom. Parameters of wedge-shaped absorbers and partition numbers are derived for simultaneous longitudinal and transverse cooling. Limits on length and material of absorbers, and dispersion at the wedge-shaped absorbers are obtained. Parameters are presented for the RF system, e.g. peak voltage, frequency, and stable phase angle. The properties of the magnetic lattice which satisfies the conditions imposed by the longitudinal dynamics are studied. The consequences of changes in the assumed performance of the cooling channel on its parameters are discussed

  9. INITIAL COOLING EXPERIMENT (ICE)

    CERN Multimedia

    1978-01-01

    ICE was built in 1977, in a record time of 9 months, using the modified bending magnets of the g-2 muon storage ring. Its purpose was to verify the validity of stochastic and electron cooling for the antiproton project, to be launched in 1978. Already early in 1978, stochastic cooling proved a resounding success, such that the antiproton (p-pbar)project was entirely based on it. Tests of electron cooling followed later: protons of 46 MeV kinetic energy were cooled with an electron beam of 26 kV and 1.3 A. The cage seen prominently in the foreground houses the HV equipment, adjacent to the "cooler" installed in a straight section of the ring. With some modifications, the cooler was later transplanted into LEAR (Low Energy Antiproton Ring) and then, with further modifications, into the AD (Antiproton Decelerator), where it cools antiprotons to this day (2006). See also: 7711282, 7802099, 7908242.

  10. INITIAL COOLING EXPERIMENT (ICE)

    CERN Multimedia

    1979-01-01

    ICE was built in 1977, using the modified bending magnets of the g-2 muon storage ring (see 7405430). Its purpose was to verify the validity of stochastic and electron cooling for the antiproton project. Stochastic cooling proved a resounding success early in 1978 and the antiproton project could go ahead, now entirely based on stochastic cooling. Electron cooling was experimented with in 1979. The 26 kV equipment is housed in the cage to the left of the picture, adjacent to the "e-cooler" located in a straight section of the ring. With some modifications, the cooler was later transplanted into LEAR (Low Energy Antiproton Ring) and then, with further modifications, into the AD (Antiproton Decelerator), where it cools antiprotons to this day (2006). See also: 7711282, 7802099, 7809081.

  11. A Study of the Batch Annealing of Cold-Rolled HSLA Steels Containing Niobium or Titanium

    Science.gov (United States)

    Fang, Chao; Garcia, C. Isaac; Choi, Shi-Hoon; DeArdo, Anthony J.

    2015-08-01

    The batch annealing behavior of two cold-rolled, microalloyed HSLA steels has been studied in this program. One steel was microalloyed with niobium while the other with titanium. A successfully batch annealed steel will exhibit minimum variation in properties along the length of the coil, even though the inner and outer wraps experience faster heating and cooling rates and lower soaking temperatures, i.e., the so-called "cold spot" areas, than the mid-length portion of the coil, i.e., the so-called "hot spot" areas. The variation in strength and ductility is caused by differences in the extent of annealing in the different areas. It has been known for 30 years that titanium-bearing HSLA steels show more variability after batch annealing than do the niobium-bearing steels. One of the goals of this study was to try to explain this observation. In this study, the annealing kinetics of the surface and center layers of the cold-rolled sheet were compared. The surface and center layers of the niobium steel and the surface layer of the titanium steel all showed similar annealing kinetics, while the center layer of the titanium steel exhibited much slower kinetics. Metallographic results indicate that the stored energy of the cold-rolled condition, as revealed by grain center sub-grain boundary density, appeared to strongly influence the annealing kinetics. The kinetics were followed by the Kernel Average Misorientation reconstruction of the microstructure at different stages on annealing. Possible pinning effects caused by microalloy precipitates were also considered. Methods of improving uniformity and increasing kinetics, involving optimizing both hot-rolled and cold-rolled microstructure, are suggested.

  12. [Characteristic of Particulate Emissions from Concrete Batching in Beijing].

    Science.gov (United States)

    Xue, Yi-feng; Zhou, Zhen; Zhong, Lian-hong; Yan, Jing; Qu, Song; Huang, Yu-hu; Tian, He- zhong; Pan, Tao

    2016-01-15

    With the economic development and population growth in Beijing, there is a strong need for construction and housing, which leads to the increase of the construction areas. Meanwhile, as a local provided material, the production of concrete has been raised. In the process of concrete production by concrete batching, there are numerous particulates emitted, which have large effect on the atmospheric environment, however, systematic study about the tempo-spatial characteristics of pollutant emission from concrete batching is still rare. In this study, we estimated the emission of particulates from concrete batching from 1991 to 2012 using emission factor method, analyzed the tempo-spatial characteristics of pollutant emission, established the uncertainty range by adopting Monte-Carlo method, and predicted the future emission in 2020 based on the relative environmental and economical policies. The results showed that: (1) the emissions of particulates from concrete batching showed a trend of "first increase and then decrease", reaching the maximum in 2005, and then decreased due to stricter emission standard and enhanced environmental management. (2) according to spatial distribution, the emission of particulates from concrete batch mainly concentrated in the urban area with more human activities, and the area between the fifth ring and the sixth ring contributed the most. (3) through scenarios analysis, for further reducing the emission from concrete batching in 2020, more stricter standard for green production as well as powerful supervision is needed. PMID:27078945

  13. Batch process monitoring based on multilevel ICA-PCA

    Institute of Scientific and Technical Information of China (English)

    Zhi-qiang GE; Zhi-huan SONG

    2008-01-01

    In this paper,we describe a new batch process monitoring method based on multilevel independent component analysis and principal component analysis (MLICA-PCA).Unlike the conventional multi-way principal component analysis (MPCA) method,MLICA-PCA provides a separated interpretation for multilevel batch process data.Batch process data are partitioned into two levels:the within-batch level and the between-batch level.In each level,the Gaussian and non-Ganssian components of process information can be separately extracted.I2,T2 and SPE statistics are individually built and monitored.The new method facilitates fault diagnosis.Since the two variation levels arc decomposed,the variables responsible for faults in each level can be identified and interpreted more easily.A case study of the Dupont benchmark process showed that the proposed method was more efficient and interpretable in fault detection and diagnosis,compared to the alternative batch process monitoring method.

  14. OPLS in batch monitoring - Opens up new opportunities.

    Science.gov (United States)

    Souihi, Nabil; Lindegren, Anders; Eriksson, Lennart; Trygg, Johan

    2015-02-01

    In batch statistical process control (BSPC), data from a number of "good" batches are used to model the evolution (trajectory) of the process and they also define model control limits, against which new batches may be compared. The benchmark methods used in BSPC include partial least squares (PLS) and principal component analysis (PCA). In this paper, we have used orthogonal projections to latent structures (OPLS) in BSPC and compared the results with PLS and PCA. The experimental study used was a batch hydrogenation reaction of nitrobenzene to aniline characterized by both UV spectroscopy and process data. The key idea is that OPLS is able to separate the variation in data that is correlated to the process evolution (also known as 'batch maturity index') from the variation that is uncorrelated to process evolution. This separation of different types of variations can generate different batch trajectories and hence lead to different established model control limits to detect process deviations. The results demonstrate that OPLS was able to detect all process deviations and provided a good process understanding of the root causes for these deviations. PCA and PLS on the other hand were shown to provide different interpretations for several of these process deviations, or in some cases they were unable to detect actual process deviations. Hence, the use of OPLS in BSPC can lead to better fault detection and root cause analysis as compared to existing benchmark methods and may therefore be used to complement the existing toolbox. PMID:25604817

  15. Shortcut Algorithm for Simulation of Batch Extractive Distillation

    Institute of Scientific and Technical Information of China (English)

    WU Huixiong; XU Shimin; HU Hui; XIAO Bin

    2007-01-01

    The batch extractive distillation (BED) process has the advantages of both batch and extractive distillation. It is one of the most promising means for the separation of azeotropic and close-boiling point systems. However, so far this process has not been applied in industry due to its over-complexity. A new shortcut model was proposed to simulate the operation of the batch extractive distillation operations. This algorithm is based on the assumption that the batch extractive distillation column can be considered as a continuous extractive distillation column with changing feed at anytime. Namely, the whole batch process is simulated as a succession of a finite number of steady states of short duration, in which holdup is considered as constant mole. For each period of time the batch extractive distillation process is solved through the algorithm for continuous extractive distillation. Finally, the practical implementation of the shortcut model is discussed and data from the lab-oratory and literature are presented. It is found that this model has better adaptability, more satisfactory accuracy and less calculative load than previous rigorous model. Hence the algorithm for simulating BED is verified.

  16. Numerical and experimental simulation of mechanical and microstructural transformations in Batch annealing steels

    International Nuclear Information System (INIS)

    The heating and cooling curves during batch annealing process of low carbon steel have been modeled using the finite element technique. This has allowed to predict the transient thermal profile for every point of the annealed coils, particularly for the hottest and coldest ones. Through experimental measurements, the results have been adequately validated since a good agreement has been found between experimental values and those predicted by the model. Moreover, an Avrami recrystallization model. Moreover, and Avrami recrystallization model has been coupled to this thermal balance computation. Interrupted annealing experiments have been made by measuring the recrystallized fraction on the extreme points of the coil foe different times. These data gave the possibility to validate the developed recrystallization model through a reasonably good numerical-experimental fittings. (Author) 6 refs

  17. Nepheline Formation Potential in Sludge Batch 4 (SB4)

    International Nuclear Information System (INIS)

    The effect of crystallization on glass durability is complex and depends on several interrelated factors including the change in residual glass composition, the formation of internal stress or microcracks, and the preferential attack at the glass-crystal interface. Perhaps one of the most significant effects is the type and extent (or fraction) of crystallization and the resulting change to the residual glass composition. A strong increase in glass dissolution (or decrease in durability) has been observed in previous studies in glasses that formed aluminum-containing crystals, such as NaAlSiO4 (nepheline) and LiAlSi2O6, and crystalline SiO2. Although the addition of Al2O3 to borosilicate glasses enhances the durability of the waste form (through creation of network-forming tetrahedral Na+-[AlO4/2]- pairs), the combination of high Al2O3 and Na2O can lead to the formation of nepheline (NaAlSiO4). Given the projected high concentration of Al2O3 in SB4 and the potential use of a high Na2O based glass (as a result of the use of a high Na2O frit and/or a less washed sludge) to improve melt rate, the potential formation of nepheline in various SB4 systems is being assessed. Li et al. (2003) indicate that sodium alumino-borosilicate glasses are prone to nepheline crystallization if their compositions projected on the Na2O-Al2O3-SiO2 ternary fall within the nepheline primary phase field. In particular, durable glasses with SiO2/(SiO2+Na2O+ Al2O3) > 0.62, where the oxides are expressed as mass fractions in the glass, do not precipitate nepheline as their primary phase. Twelve SB4-based glasses have been identified or classified as ''prone to nepheline formation'' using a ''less conservative'' discriminator value of 0.65. Ten of the 12 glasses are Frit 320 based, and 8 of these 10 target a 40% WL-independent of the SB4 blending scenario used. This is not unexpected due to the higher alkali content of Frit 320 (12% Na2O) relative to Frit 418 (8% Na2O) and the fact that as WLs

  18. Morphology and antimony segregation of spangles on batch hot-dip galvanized coatings

    International Nuclear Information System (INIS)

    Spangles produced by batch hot-dip galvanizing process have a rougher surface and a greater surface segregation of alloying element compared with those in continuous hot-dip galvanizing line (CGL), owing to the cooling rate of the former is much smaller than that of the later. Therefore, typical spangles on a batch hot-dipped Zn-0.05Al-0.2Sb alloy coating were investigated. The chemical, morphological characterization and identification of the phases on the spangles were examined by scanning electron microscopy (SEM), backscattered electron imaging (BSE), atomic force microscopy (AFM), energy dispersive spectroscopy (EDS) and X-ray diffraction analysis (XRD). The results showed that the coating surface usually exhibited three kinds of spangles: shiny, feathery and dull spangle, of which extensively antimony surface segregation was detected. The nature of precipitate on the coating surface was identified as β-Sb3Zn4, The precipitated β-Sb3Zn4 particles distributed randomly on the shiny spangle surface, both β-Sb3Zn4 particles and dentritic segregation of antimony dispersed in the dendritic secondary arm spacings of the feathery spangle and on the whole dull spangle surface. The dentritic segregation of antimony and precipitation of Sb3Zn4 compound are discussed by a proposed model.

  19. Cooling Crystallization Kinetics of Potassium Nitrate in K+, +4NH//Cl-, 3NO--H2O System%+K 、+4NH//Cl-、NO-3-H2O体系硝酸钾冷却结晶动力学研究

    Institute of Scientific and Technical Information of China (English)

    陈丽芳; 么佳; 朱华兵; 詹志斌; 党来芳; 陈侠

    2015-01-01

    The cooling crystallization process of potassium nitrate in K+, +4NH //Cl-, 3NO--H2O system was studied via intermittent dynamic method. The moment transform method was applied to the experiment data,from which the kinetic parameters were obtained with the least square method. The corresponding equations of the nucleation rate and the crystal growth rate thus obtained during the crystallization process of potassium nitrate in this system are 0 12B =1.13×10 ⋅4 4.68 0.41 0.50 Tp 6.34 10 exp( )C MNRT×−Δand 5 6 3.791.14 10 4.89 10 exp( )GCRT×=×−Δ. Finally,the effects of the operation parame-ters were analyzed against these model equations. For the process of potassium nitrate produced through double decomposi-tion reaction from potassium chloride and ammonium nitrate,the experimental results can provide basic data for crystallizer design,and have some guiding significance for the optimization of crystallization operation.%采用间歇动态法研究了 K+、+4NH //Cl-、3NO-–H2O 体系中硝酸钾冷却结晶动力学,通过矩量变换法处理实验数据,回归拟合求得动力学参数,建立了该体系硝酸钾成核速率和生长速率动力学方程,分别为012B =1.13×10⋅44.680.410.50 Tp 6.3410 exp()CMNRT ×−Δ、563.791.14104.8910 exp()GCRT×=×−Δ,简要分析了硝酸钾冷却结晶过程的影响因素.实验结果可以为氯化钾–硝酸铵复分解法生产硝酸钾结晶器设计提供基础数据,对结晶操作的优化具有指导意义.

  20. Deposit control in process cooling water systems

    International Nuclear Information System (INIS)

    In order to achieve efficient heat transfer in cooling water systems, it is essential to control the fouling of heat exchanger surfaces. Solubilities of scale forming salts, their growth into crystals, and the nature of the surfaces play important roles in the deposition phenomenon. Condensed phosphates, organic polymers and compounds like phosphates are effective in controlling deposition of scale forming salts. The surface active agents inhibit crystal growth and modify the crystals of the scale forming salts, and thus prevent deposition of dense, uniformly structured crystalline mass on the heat transfer surface. Understanding the mechanism of biofouling is essential to control it by surface active agents. Certain measures taken in the plant, such as back flushing, to control scaling, sometimes may not be effective and can be detrimental to the system itself. (author)

  1. Evaporation from porous building materials and its cooling potential

    OpenAIRE

    Gonçalves, Teresa; Brito, Vânia; Vidigal, Filipa; Matias, Luís; Faria, Paulina

    2015-01-01

    Evaporative cooling is a traditional strategy to improve summer comfort, which has gained renewed relevance in the context of the transition to a greener economy. Here, the potential for evaporative cooling of two common porous building materials, natural stone and ceramic brick, was evaluated. The work has relevance also to the protection of built heritage becauseevaporation underlies the problems of dampness and salt crystallization, which are so harmful and frequent in this heritage. It wa...

  2. Design and Application of Software Sensors in Batch and Fed-batch Cultivations during Recombinant Protein Expression in Escherichia coli

    OpenAIRE

    Warth, Benedikt

    2008-01-01

    Software sensors are a potent tool to improve biotechnological real time process monitoring and control. In the current project, algorithms for six partly novel, software sensors were established and tested in a microbial reactor system. Eight batch and two fed-batch runs were carried out with a recombinant Escherichia coli to investigate the suitability of the different software sensor models in diverse cultivation stages. Special respect was given to effects on the sensors after recombinant...

  3. SLUDGE BATCH VARIABILITY STUDY WITH FRIT 418

    Energy Technology Data Exchange (ETDEWEB)

    Johnson, F.; Edwards, T.

    2010-11-29

    The Defense Waste Processing Facility (DWPF) initiated processing Sludge Batch 6 (SB6) in the summer of 2010. In support of processing, the Savannah River National Laboratory (SRNL) provided a recommendation to utilize Frit 418 to process SB6. This recommendation was based on assessments of the compositional projections for SB6 available at the time from the Liquid Waste Organization (LWO) and SRNL (using a model-based approach). To support qualification of SB6, SRNL executed a variability study to assess the applicability of the current durability models for SB6. The durability models were assessed over the expected Frit 418-SB6 composition range. Seventeen glasses were selected for the variability study based on the sludge projections used in the frit recommendation. Five of the glasses are based on the centroid of the compositional region, spanning a waste loading (WL) range of 32 to 40%. The remaining twelve glasses are extreme vertices (EVs) of the sludge region of interest for SB6 combined with Frit 418 and are all at 36% WL. These glasses were fabricated and characterized using chemical composition analysis, X-ray diffraction (XRD) and the Product Consistency Test (PCT). After initiating the SB6 variability study, the measured composition of the SB6 Tank 51 qualification glass produced at the SRNL Shielded Cells Facility indicated that thorium was present in the glass at an appreciable concentration (1.03 wt%), which made it a reportable element for SB6. This concentration of ThO{sub 2} resulted in a second phase of experimental studies. Five glasses were formulated that were based on the centroid of the new sludge compositional region combined with Frit 418, spanning a WL range of 32 to 40%. These glasses were fabricated and characterized using chemical composition analysis and the PCT. Based on the measured PCT response, all of the glasses (with and without thorium) were acceptable with respect to the Environmental Assessment (EA) reference glass

  4. SLUDGE BATCH 7B GLASS VARIABILITY STUDY

    Energy Technology Data Exchange (ETDEWEB)

    Johnson, F.; Edwards, T.

    2011-10-25

    The Defense Waste Processing Facility (DWPF) is preparing to initiate processing Sludge Batch 7b (SB7b). In support of the upcoming processing, the Savannah River National Laboratory (SRNL) provided a recommendation to utilize Frits 418 with a 6% Na{sub 2}O addition (26 wt% Na{sub 2}O in sludge) and 702 with a 4% Na{sub 2}O addition (24 wt% Na{sub 2}O in sludge) to process SB7b. This recommendation was based on assessments of the compositional projections for SB7b available at the time from the Savannah River Remediation (SRR). To support qualification of SB7b, SRNL executed a variability study to assess the applicability of the current durability models for SB7b. The durability models were assessed over the expected composition range of SB7b, including potential caustic additions, combined with Frits 702 and 418 over a 32-40% waste loading (WL) range. Thirty four glasses were selected based on Frits 418 and 702 coupled with the sludge projections with an additional 4-6% Na{sub 2}O to reflect the potential caustic addition. Six of these glasses, based on average nominal sludge compositions including the appropriate caustic addition, were developed for both Frit 418 and Frit 702 at 32, 36 and 40% WL to provide coverage in the center of the anticipated SB7b glass region. All glasses were fabricated and characterized using chemical composition analysis, X-ray diffraction (XRD) and the Product Consistency Test (PCT). To comply with the DWPF Glass Product Control Program, a total of thirty four glasses were fabricated to assess the applicability of the current DWPF PCCS durability models. Based on the measured PCT response, all of the glasses were acceptable with respect to the Environmental Assessment (EA) benchmark glass regardless of thermal history. The NL[B] values of the SB7b variability study glasses were less than 1.99 g/L as compared to 16.695 g/L for EA. A small number of the D-optimally selected 'outer layer' extreme vertices (EV) glasses were not

  5. Sludge Batch Variability Study With Frit 418

    International Nuclear Information System (INIS)

    The Defense Waste Processing Facility (DWPF) initiated processing Sludge Batch 6 (SB6) in the summer of 2010. In support of processing, the Savannah River National Laboratory (SRNL) provided a recommendation to utilize Frit 418 to process SB6. This recommendation was based on assessments of the compositional projections for SB6 available at the time from the Liquid Waste Organization (LWO) and SRNL (using a model-based approach). To support qualification of SB6, SRNL executed a variability study to assess the applicability of the current durability models for SB6. The durability models were assessed over the expected Frit 418-SB6 composition range. Seventeen glasses were selected for the variability study based on the sludge projections used in the frit recommendation. Five of the glasses are based on the centroid of the compositional region, spanning a waste loading (WL) range of 32 to 40%. The remaining twelve glasses are extreme vertices (EVs) of the sludge region of interest for SB6 combined with Frit 418 and are all at 36% WL. These glasses were fabricated and characterized using chemical composition analysis, X-ray diffraction (XRD) and the Product Consistency Test (PCT). After initiating the SB6 variability study, the measured composition of the SB6 Tank 51 qualification glass produced at the SRNL Shielded Cells Facility indicated that thorium was present in the glass at an appreciable concentration (1.03 wt%), which made it a reportable element for SB6. This concentration of ThO2 resulted in a second phase of experimental studies. Five glasses were formulated that were based on the centroid of the new sludge compositional region combined with Frit 418, spanning a WL range of 32 to 40%. These glasses were fabricated and characterized using chemical composition analysis and the PCT. Based on the measured PCT response, all of the glasses (with and without thorium) were acceptable with respect to the Environmental Assessment (EA) reference glass regardless of

  6. Second sector cool down

    CERN Multimedia

    2007-01-01

    At the beginning of July, cool-down is starting in the second LHC sector, sector 4-5. The cool down of sector 4-5 may occasionally generate mist at Point 4, like that produced last January (photo) during the cool-down of sector 7-8.Things are getting colder in the LHC. Sector 7-8 has been kept at 1.9 K for three weeks with excellent stability (see Bulletin No. 16-17 of 16 April 2007). The electrical tests in this sector have got opt to a successful start. At the beginning of July the cryogenic teams started to cool a second sector, sector 4-5. At Point 4 in Echenevex, where one of the LHC’s cryogenic plants is located, preparations for the first phase of the cool-down are underway. During this phase, the sector will first be cooled to 80 K (-193°C), the temperature of liquid nitrogen. As for the first sector, 1200 tonnes of liquid nitrogen will be used for the cool-down. In fact, the nitrogen circulates only at the surface in the ...

  7. MEIC electron cooling program

    International Nuclear Information System (INIS)

    Cooling of proton and ion beams is essential for achieving high luminosities (up to above 1034 cm-2s-1) for MEIC, a Medium energy Electron-Ion Collider envisioned at JLab [1] for advanced nuclear science research. In the present conceptual design, we utilize the conventional election cooling method and adopted a multi-staged cooling scheme for reduction of and maintaining low beam emittances [2,3,4]. Two electron cooling facilities are required to support the scheme: one is a low energy (up to 2 MeV) DC cooler installed in the MEIC ion pre-booster (with the proton kinetic energy up to 3 GeV); the other is a high electron energy (up to 55 MeV) cooler in the collider ring (with the proton kinetic energy from 25 to 100 GeV). The high energy cooler, which is based on the ERL technology and a circulator ring, utilizes a bunched electron beam to cool bunched proton or ion beams. To complete the MEIC cooling concept and a technical design of the ERL cooler as well as to develop supporting technologies, an R&D program has been initiated at Jefferson Lab and significant progresses have been made since then. In this study, we present a brief description of the cooler design and a summary of the progress in this cooling R&D

  8. Dry well cooling device

    International Nuclear Information System (INIS)

    A plurality of blowing ports with introduction units are disposed to a plurality of ducts in a dry well, and a cooling unit comprising a cooler, a blower and an isolating valve is disposed outside of the dry well. Cooling air and the atmosphere in the dry well are mixed to form a cooling gas and blown into the dry well to control the temperature. Since the cooling unit is disposed outside of the dry well, the maintenance of the cooling unit can be performed even during the plant operation. In addition, since dampers opened/closed depending on the temperature of the atmosphere are disposed to the introduction units for controlling the temperature of the cooling gas, the temperature of the atmosphere in the dry well can be set to a predetermined level rapidly. Since an axial flow blower is used as the blower of the cooling unit, it can be contained in a ventilation cylinder. Then, the atmosphere in the dry well flowing in the ventilation cylinder can be prevented from leaking to the outside. (N.H.)

  9. Batch and Pulsed Fed-Batch Cultures of Aspergillus flavipes FP-500 Growing on Lemon Peel at Stirred Tank Reactor.

    Science.gov (United States)

    Wolf-Márquez, V E; García-García, E; García-Rivero, M; Aguilar-Osorio, G; Martínez Trujillo, M A

    2015-11-01

    Aspergillus flavipes FP-500 grew up on submerged cultures using lemon peel as the only carbon source, developing several batch and pulsed fed-batch trials on a stirred tank reactor. The effect of carbon source concentration, reducing sugar presence and initial pH on exopectinase and endopectinase production, was analyzed on batch cultures. From this, we observed that the highest substrate concentration favored biomass (X max) but had not influence on the corresponding specific production (q p) of both pectinases; the most acid condition provoked higher endopectinase-specific productions but had not a significant effect on those corresponding to exopectinases; and reducing sugar concentrations higher than 1.5 g/L retarded pectinase production. On the other hand, by employing the pulsed fed-batch operation mode, we observed a prolonged growth phase, and an increase of about twofold on endopectinase production without a significant raise on biomass concentration. So, pulsed fed-batch seems to be a good alternative for obtaining higher endopectinase titers by using high lemon peel quantities without having mixing and repression problems to the system. The usefulness of unstructured kinetic models for explaining, under a theoretic level, the behavior of the fungus along the batch culture with regard to pectinase production was evident. PMID:26304128

  10. A study on clavulanic acid production by Streptomyces clavuligerus in batch, fed-batch and continuous processes

    Directory of Open Access Journals (Sweden)

    A. B. Neto

    2005-12-01

    Full Text Available Clavulanic acid (CA is a potent inhibitor of beta-lactamases, enzymes that are responsible for the hydrolysis of beta-lactam antibiotics. It is a secondary metabolite produced by the filamentous aerobic bacterium Streptomyces clavuligerus in submerged cultivations. In the present work clavulanic acid production in batch, fed-batch and continuous bioreactors was studied with the objective of increasing productivity. The operating conditions: temperature, aeration and agitation, were the same in all cases, 28º C, 0.5 vvm and 800 rpm, respectively. The CA concentration obtained in the fed-batch culture, 404 mg L-1, was ca twice the value obtained in the batch culture, 194 mg L-1, while 293 mg L-1 was obtained in the continuous culture. The highest productivity was obtained in the continuous cultivation, 10.6 mg L-1 h-1, as compared with 8.8 mg L-1 h-1 in the fed-batch process and 3.5 mg L-1 h-1 in the batch process, suggesting that continuous culture of Streptomyces clavuligerus is a promising strategy for clavulanic acid production.

  11. Simulation of molecular dynamics of silver subcritical nuclei and crystal clusters during solidification

    Institute of Scientific and Technical Information of China (English)

    2010-01-01

    Molecular dynamics simulation is carried out to investigate the effects of cooling rate on the final configurations of silver after rapid solidification. The cooling rate for the formation of a silver amorphous phase is determined by analyzing its pair distribution function, H-A bond index, and the largest crystal cluster. Further, the equilibrium structures of the subcritical nuclei and crystal clusters are studied. The results show that the solidified microstructure is composed of a mixture of crystal clusters and amorphous phases at a certain cooling rate range. The size of the largest crystal cluster decreases with the increasing cooling rate, and it completely disappears when the cooling rate exceeds a critical value. The structures of the subcritical nuclei and the largest crystal cluster are composed of lamellar structures of fcc and hcp atoms, indicating that the lamellar structure of fcc and hcp atoms in the silver crystal originates from nucleation, and not from the growth of crystals.

  12. Feedback cooling of currents

    Science.gov (United States)

    Washburn, Sean

    1989-02-01

    Just as feedback can be used to correct errors in the output voltages of amplifiers, it can also be used to remove noise from the current through a resistor. Such a feedback amplifier behaves as a refrigerator cooling the electrons in a resistor connnected to it. This principle has been recognized since the 1940s but has been largely ignored because the cooling power available from such refrigerators is miniscule. It is pointed out here that the method might be practical for cooling the currents in the microscopic circuits that are typical of modern electrical engineering and recent studies in transport physics.

  13. Cooling System Analysis

    OpenAIRE

    Almeida, Fernando Jorge Gonçalves; Cruz, João Pedro Brás da

    2012-01-01

    ABSTRACT This master thesis report describes the behavior of a cooling system based on the power consumption and power losses during the velocity range. The thesis is a report of the behavior of the cooling system to understand were we having more needs to cold down the system. It was used a excel sheet to describe the values of power, losses and efficiencies of the various components of the cooling. With the excel sheets built we studied various cases in the system to show ...

  14. Personal Cooling System

    Science.gov (United States)

    1986-01-01

    Cool Head, a personal cooling system for use in heat stress occupations, is a spinoff of a channeled cooling garment for space wear. It is portable and includes a heat exchanger, control display unit, liquid reservoir and temperature control unit. The user can eliminate 40 to 60 percent of his body's heat storage and lower heart rate by 50 to 80 beats a minute. The system is used by the Army, Navy, crop dusting pilots, heavy equipment operators and auto racing drivers and is marketed by Life Enhancement Technologies, LLC. Further applications are under consideration.

  15. Neutron batch size optimisation methodology for Monte Carlo criticality calculations

    International Nuclear Information System (INIS)

    Highlights: • A method is suggested for improving efficiency of MC criticality calculations. • The method optimises the number of neutrons simulated per cycle. • The optimal number of neutrons per cycle depends on allocated computing time. - Abstract: We present a methodology that improves the efficiency of conventional power iteration based Monte Carlo criticality calculations by optimising the number of neutron histories simulated per criticality cycle (the so-called neutron batch size). The chosen neutron batch size affects both the rate of convergence (in computing time) and magnitude of bias in the fission source. Setting a small neutron batch size ensures a rapid simulation of criticality cycles, allowing the fission source to converge fast to its stationary state; however, at the same time, the small neutron batch size introduces a large systematic bias in the fission source. It follows that for a given allocated computing time, there is an optimal neutron batch size that balances these two effects. We approach this problem by studying the error in the cumulative fission source, i.e. the fission source combined over all simulated cycles, as all results are commonly combined over the simulated cycles. We have deduced a simplified formula for the error in the cumulative fission source, taking into account the neutron batch size, the dominance ratio of the system, the error in the initial fission source and the allocated computing time (in the form of the total number of simulated neutron histories). Knowing how the neutron batch size affects the error in the cumulative fission source allows us to find its optimal value. We demonstrate the benefits of the method on a number of numerical test calculations

  16. Different cooling configurations for a high average power longitudinally diode-pumped Yb:YAG amplifier.

    Science.gov (United States)

    Yu, Haiwu; Bourdet, Gilbert

    2006-08-20

    We analyze the temperature distribution in several Yb:YAG longitudinally pumped amplifier crystals by using various cooling configurations. The crystal designs are (i) a composite crystal made of a thin sheet of high-doped Yb:YAG bonded on a bulk piece of undoped YAG and (ii) a thick piece of low-doped Yb:YAG crystal. The cooling configurations investigated here include those both from the rear face or from the rear and side faces together. In every case we determine the average temperature rise, the longitudinal and radial temperature gradient, and the resulting crystal bending and optical phase distortion. We optimize the best cooling configuration and crystal design by compromising the average temperature, thermodeformation, and optical phase distortion. The experimental results also indicate that a thin sheet of gain medium (1.6 mm thick at 10 at. % doping) suffers from a notable bending deformation, which results in an unexpected decrease of the output energy. PMID:16892125

  17. Recent progress on batch processed large size LRE-123 bulk superconductors using a novel thin film Nd-123 seed

    International Nuclear Information System (INIS)

    Highlights: ► We developed a batch production of large grain c-axis oriented GdBa2Cu3Oy and SmBa2Cu3Oy. ► The NdBa2Cu3Oy thin film made on MgO seeds can withstand temperatures >1100 °C. ► More than 50 mm in size GdBa2Cu3Oy superconductors can be fabricated by cold seeding. ► The experimental results indicated that sample quality is excellent. -- Abstract: We developed a batch production of large grain c-axis oriented GdBa2Cu3Oy and SmBa2Cu3Oy bulk superconductors by using a cold seeding method in air. Novel thin film Nd-123 seeds grown on MgO crystals were used as a seed crystal for the batch process. Four pieces of single domain Gd-123 samples with 50 mm in diameter were successfully fabricated in single run. Magnetization results confirmed that the samples have a sharp superconducting transition with the onset Tc around 93 K. On the other hand Sm-123 system was studied as a function of varying amounts of BaO2 to reduce the Sm/Ba solid state substation and batch production in air. The magnetization results indicated that superconducting transition was increased with increasing the BaO2 concentration from 91.5 K for 0 wt% to 93 K for 0.2 and 0.3 wt%. Moreover, the maximum trapped field of 2.1 T and 1.5 T at 20 K was recorded 16 mm in diameter Sm-123 with 3 and 1 wt% BaO2 addition

  18. Bunched beam stochastic cooling

    Energy Technology Data Exchange (ETDEWEB)

    Wei, Jie

    1992-09-01

    The scaling laws for bunched-beam stochastic cooling has been derived in terms of the optimum cooling rate and the mixing condition. In the case that particles occupy the entire sinusoidal rf bucket, the optimum cooling rate of the bunched beam is shown to be similar to that predicted from the coasting-beam theory using a beam of the same average density and mixing factor. However, in the case that particles occupy only the center of the bucket, the optimum rate decrease in proportion to the ratio of the bunch area to the bucket area. The cooling efficiency can be significantly improved if the synchrotron side-band spectrum is effectively broadened, e.g. by the transverse tune spread or by using a double rf system.

  19. Bunched beam stochastic cooling

    Energy Technology Data Exchange (ETDEWEB)

    Wei, Jie.

    1992-01-01

    The scaling laws for bunched-beam stochastic cooling has been derived in terms of the optimum cooling rate and the mixing condition. In the case that particles occupy the entire sinusoidal rf bucket, the optimum cooling rate of the bunched beam is shown to be similar to that predicted from the coasting-beam theory using a beam of the same average density and mixing factor. However, in the case that particles occupy only the center of the bucket, the optimum rate decrease in proportion to the ratio of the bunch area to the bucket area. The cooling efficiency can be significantly improved if the synchrotron side-band spectrum is effectively broadened, e.g. by the transverse tune spread or by using a double rf system.

  20. Sisyphus Cooling of Lithium

    CERN Document Server

    Hamilton, Paul; Kim, Geena; Mukherjee, Biswaroop; Tiarks, Daniel; Müller, Holger

    2013-01-01

    Laser cooling to sub-Doppler temperatures by optical molasses is thought to be inhibited in atoms with unresolved, near-degenerate hyperfine structure in the excited state. We demonstrate that such cooling is possible in one to three dimensions, not only near the standard D2 line for laser cooling, but over a range extending to the D1 line. Via a combination of Sisyphus cooling followed by adiabatic expansion, we reach temperatures as low as 40 \\mu K, which corresponds to atomic velocities a factor of 2.6 above the limit imposed by a single photon recoil. Our method requires modest laser power at a frequency within reach of standard frequency locking methods. It is largely insensitive to laser power, polarization and detuning, magnetic fields, and initial hyperfine populations. Our results suggest that optical molasses should be possible with all alkali species.

  1. CONFERENCE: Electron cooling

    International Nuclear Information System (INIS)

    ECOOL 84, held at the Kernforschungszentrum Karlsruhe (KfK) last year, was the first international meeting on electron cooling and related applications and reflected the increasing interest in this area of particle beam physics

  2. Radiant Floor Cooling Systems

    DEFF Research Database (Denmark)

    Olesen, Bjarne W.

    2008-01-01

    In many countries, hydronic radiant floor systems are widely used for heating all types of buildings such as residential, churches, gymnasiums, hospitals, hangars, storage buildings, industrial buildings, and smaller offices. However, few systems are used for cooling.This article describes a floo...... cooling system that includes such considerations as thermal comfort of the occupants, which design parameters will influence the cooling capacity and how the system should be controlled. Examples of applications are presented.......In many countries, hydronic radiant floor systems are widely used for heating all types of buildings such as residential, churches, gymnasiums, hospitals, hangars, storage buildings, industrial buildings, and smaller offices. However, few systems are used for cooling.This article describes a floor...

  3. LHC cooling gains ground

    CERN Multimedia

    Huillet-Miraton Catherine

    The nominal cryogenic conditions of 1.9 K have been achieved in sectors 5-6 and 7-8. This means that a quarter of the machine has reached the nominal conditions for LHC operation, having attained a temperature of below 2 K (-271°C), which is colder than interstellar space! Elsewhere, the cryogenic system in Sector 8-1 has been filled with liquid helium and cooled to 2K and will soon be available for magnet testing. Sectors 6-7 and 2-3 are being cooled down and cool-down operations have started in Sector 3-4. Finally, preparations are in hand for the cool-down of Sector 1-2 in May and of Sector 4-5, which is currently being consolidated. The LHC should be completely cold for the summer. For more information: http://lhc.web.cern.ch/lhc/Cooldown_status.htm.

  4. Waveguide cooling system

    Science.gov (United States)

    Chen, B. C. J.; Hartop, R. W. (Inventor)

    1981-01-01

    An improved system is described for cooling high power waveguides by the use of cooling ducts extending along the waveguide, which minimizes hot spots at the flanges where waveguide sections are connected together. The cooling duct extends along substantially the full length of the waveguide section, and each flange at the end of the section has a through hole with an inner end connected to the duct and an opposite end that can be aligned with a flange hole in another waveguide section. Earth flange is formed with a drainage groove in its face, between the through hole and the waveguide conduit to prevent leakage of cooling fluid into the waveguide. The ducts have narrowed sections immediately adjacent to the flanges to provide room for the installation of fasteners closely around the waveguide channel.

  5. Cooling of wood briquettes

    Directory of Open Access Journals (Sweden)

    Adžić Miroljub M.

    2013-01-01

    Full Text Available This paper is concerned with the experimental research of surface temperature of wood briquettes during cooling phase along the cooling line. The cooling phase is an important part of the briquette production technology. It should be performed with care, otherwise the quality of briquettes could deteriorate and possible changes of combustion characteristics of briquettes could happen. The briquette surface temperature was measured with an IR camera and a surface temperature probe at 42 sections. It was found that the temperature of briquette surface dropped from 68 to 34°C after 7 minutes spent at the cooling line. The temperature at the center of briquette, during the 6 hour storage, decreased to 38°C.

  6. Batch Scheduling on Two-Machine Flowshop with Machine-Dependent Setup Times

    OpenAIRE

    Daniel Oron; Gur Mosheiov; Lika Ben-Dati

    2009-01-01

    We study a batch scheduling problem on a 2-machine flowshop. We assume unit processing time jobs, batch availability, and machine-dependent setup times. The objective is to find a job allocation to batches of integer size and a batch schedule that minimize makespan. We introduce a very efficient closed form solution for the problem.

  7. 40 CFR 63.486 - Batch front-end process vent provisions.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 9 2010-07-01 2010-07-01 false Batch front-end process vent provisions... Batch front-end process vent provisions. (a) Batch front-end process vents. Except as specified in paragraph (b) of this section, owners and operators of new and existing affected sources with batch...

  8. 40 CFR 63.1327 - Batch process vents-reporting requirements.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 11 2010-07-01 2010-07-01 true Batch process vents-reporting... Batch process vents—reporting requirements. (a) The owner or operator of a batch process vent or aggregate batch vent stream at an affected source shall submit the information specified in paragraphs...

  9. 40 CFR 63.1326 - Batch process vents-recordkeeping provisions.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 11 2010-07-01 2010-07-01 true Batch process vents-recordkeeping... Batch process vents—recordkeeping provisions. (a) Group determination records for batch process vents... batch process vent subject to the group determination procedures of § 63.1323. Except for paragraph...

  10. 40 CFR Table 3 to Subpart Ooo of... - Batch Process Vent Monitoring Requirements

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 11 2010-07-01 2010-07-01 true Batch Process Vent Monitoring... Resins Pt. 63, Subpt. OOO, Table 3 Table 3 to Subpart OOO of Part 63—Batch Process Vent Monitoring... the batch process vents or aggregate batch vent streams are not introduced with or used as the...

  11. 21 CFR 111.255 - What is the requirement to establish a batch production record?

    Science.gov (United States)

    2010-04-01

    ... 21 Food and Drugs 2 2010-04-01 2010-04-01 false What is the requirement to establish a batch... System: Requirements for the Batch Production Record § 111.255 What is the requirement to establish a batch production record? (a) You must prepare a batch production record every time you manufacture...

  12. 40 CFR 63.492 - Batch front-end process vents-reporting requirements.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 9 2010-07-01 2010-07-01 false Batch front-end process vents-reporting... Batch front-end process vents—reporting requirements. (a) The owner or operator of a batch front-end process vent or aggregate batch vent stream at an affected source shall submit the information...

  13. Horizontal-vertical coupling for three dimensional laser cooling

    International Nuclear Information System (INIS)

    In order to achieve three dimensional crystal beam, laser cooling forces are required not only in the longitudinal direction, but also in the transverse directions. With the resonance coupling method, transverse temperature is transmitted into longitudinal direction, and we have already demonstrated the horizontal laser cooling experimentally. In the present paper, we will describe an approach to extend this result to three dimensional cooling. The vertical cooling requires that the horizontal oscillation couples with the vertical oscillation. For achieving horizontal-vertical coupling, the solenoid in electron beam cooling apparatus is utilized with an experiment (νx =2.07, νy=1.07). For various solenoidal magnetic fields from 0 to 100 Gauss, horizontal and vertical betatron tunes are measured by beam transfer function. For a certain region of the solenoidal magnetic field, these tunes are mixed up each other. (author)

  14. Electron cooling for RHIC

    International Nuclear Information System (INIS)

    Electron cooling of completely stripped gold ions 197Au79+ in RHIC is considered for the store energy, γ=108. The optimal parameters of the required electron storage ring are discussed and proposed. The cooling time is calculated as 15 min, which would allow not only to avoid the beam loss due to the intra-beam scattering, but also reduce the transverse emittance and increase the luminosity several times

  15. Cooling with Superfluid Helium

    CERN Document Server

    Lebrun, P

    2014-01-01

    The technical properties of helium II (‘superfluid’ helium) are presented in view of its applications to the cooling of superconducting devices, particularly in particle accelerators. Cooling schemes are discussed in terms of heat transfer performance and limitations. Large-capacity refrigeration techniques below 2 K are reviewed, with regard to thermodynamic cycles as well as process machinery. Examples drawn from existing or planned projects illustrate the presentation. Keywords: superfluid helium, cryogenics

  16. Pressure effect on subtilisin crystallization and solubility

    Science.gov (United States)

    Webb, J. N.; Waghmare, R. Y.; Carpenter, J. F.; Glatz, C. E.; Randolph, T. W.

    1999-09-01

    High pressures (135 and 200 MPa) arrested the crystallization process in unseeded batch crystallizations of subtilisin conducted at 25°C over a period of seven days. Crystallization resumed at the normal atmospheric pressure rate once batches were depressurized and the active soluble enzyme concentration decayed to the same value as seen in atmospheric crystallizations. Solubility experiments conducted at 25°C showed an exponential increase in apparent solubility with pressure. The solubility increased approximately five-fold at 200 MPa. The partial molar volume change of crystallization for this increase in solubility with pressure is +21±1 ml/mol. Solubility changes with pressure are largely responsible for the arrest in crystallization rate at high pressure. Experiments on pH-pressure and ionic strength-pressure interactions showed that the change in apparent solubility is not due to pressure-induced changes in pH and ionic strength. For comparative purposes, solubility data as a function of pressure were collected on lysozyme. A linear dependence of lysozyme solubility with pressure was observed, with a 40% increase in apparent solubility after incubation for seven days at 210 MPa and 25°C.

  17. Alternative Room Cooling System

    Directory of Open Access Journals (Sweden)

    Md. Fazle Rabbi

    2015-06-01

    Full Text Available The rapidly growing population results in an increasing demand for much more residential and commercial buildings, which leads to vertical growth of the buildings and needs proper ventilation of those buildings. Natural air ventilation system is not sufficient for conventional building structures. Hence fans and air-conditioners are must to meet the requirement of proper ventilation as well as space conditioning. Globally building sector consumes largest energy in heating, cooling, ventilation and space conditioning. This load can be minimized by the application of solar chimney and modification in building structure for heating, cooling, ventilation and space conditioning. Passive solar cooling is a subject of interest to provide cooling by using the sun, a powerful energy source. This is done for ensuring human comfort in hot climates. ASHRAE (American Society of Heating, Refrigerating and Air Conditioning Engineers defines Comfort as ‘that state of mind which expresses satisfaction with the thermal environment.’ The present paper describes the development of a solar passive cooling system, which can provide thermal cooling throughout the summer season in hot and humid climates. The constructed passive system works on natural convection mode of air. Such system reduces the inside temperature of up to 5°C from the atmospheric temperature. Temperature can further be reduced by the judicious use of night ventilation.

  18. Microfabricated phononic crystal devices and applications

    International Nuclear Information System (INIS)

    Phononic crystals are the acoustic wave analogue of photonic crystals. Here a periodic array of scattering inclusions located in a homogeneous host material forbids certain ranges of acoustic frequencies from existence within the crystal, thus creating what are known as acoustic bandgaps. The majority of previously reported phononic crystal devices have been constructed by hand, assembling scattering inclusions in a viscoelastic medium, predominantly air, water or epoxy, resulting in large structures limited to frequencies below 1 MHz. Recently, phononic crystals and devices have been scaled to VHF (30–300 MHz) frequencies and beyond by utilizing microfabrication and micromachining technologies. This paper reviews recent developments in the area of micro-phononic crystals including design techniques, material considerations, microfabrication processes, characterization methods and reported device structures. Micro-phononic crystal devices realized in low-loss solid materials are emphasized along with their potential application in radio frequency communications and acoustic imaging for medical ultrasound and nondestructive testing. The reported advances in batch micro-phononic crystal fabrication and simplified testing promise not only the deployment of phononic crystals in a number of commercial applications but also greater experimentation on a wide variety of phononic crystal structures. (topical review)

  19. Crystals in crystals

    DEFF Research Database (Denmark)

    Christensen, Claus H.; Schmidt, I.; Carlsson, A.;

    2005-01-01

    the outer surface of the zeolite particles, particularly after thermal treatment. When using mesoporous zeolites, the particles were evenly distributed throughout the mesopore system of the zeolitic support, even after calcination, leading to nanocrystals within mesoporous zeolite single crystals........ As representative examples, a metal (Pt), an alloy (PtSn), and a metal carbide (beta-Mo2C) were supported on conventional and mesoporous zeolite carriers, respectively, and the degree of particle dispersion was compared by TEM imaging. On conventional zeolites, the supported material aggregated on...

  20. Virtual Crystallizer

    Energy Technology Data Exchange (ETDEWEB)

    Land, T A; Dylla-Spears, R; Thorsness, C B

    2006-08-29

    Large dihydrogen phosphate (KDP) crystals are grown in large crystallizers to provide raw material for the manufacture of optical components for large laser systems. It is a challenge to grow crystal with sufficient mass and geometric properties to allow large optical plates to be cut from them. In addition, KDP has long been the canonical solution crystal for study of growth processes. To assist in the production of the crystals and the understanding of crystal growth phenomena, analysis of growth habits of large KDP crystals has been studied, small scale kinetic experiments have been performed, mass transfer rates in model systems have been measured, and computational-fluid-mechanics tools have been used to develop an engineering model of the crystal growth process. The model has been tested by looking at its ability to simulate the growth of nine KDP boules that all weighed more than 200 kg.

  1. Comparing Social Stories™ to Cool versus Not Cool

    Science.gov (United States)

    Leaf, Justin B.; Mitchell, Erin; Townley-Cochran, Donna; McEachin, John; Taubman, Mitchell; Leaf, Ronald

    2016-01-01

    In this study we compared the cool versus not cool procedure to Social Stories™ for teaching various social behaviors to one individual diagnosed with autism spectrum disorder. The researchers randomly assigned three social skills to the cool versus not cool procedure and three social skills to the Social Stories™ procedure. Naturalistic probes…

  2. Environmental assessment of cooling reservoirs

    International Nuclear Information System (INIS)

    The environmental impacts, both adverse and beneficial, of cooling reservoirs are compared to cooling towers as an alternative closed cycle cooling system. Generally, the impacts associated with the construction of a cooling reservoir system are greater than for a comparable cooling tower system. Operational impacts are generally greater for cooling towers due to their visual impact, plus icing, fogging, and noise problems. The principle advantages of cooling reservoirs are their lower operating and maintenance costs, greater reliability, greater cooling efficiency, reduced water consumption in areas where cooling water storage is required, and their multiple use potential. A review of pertinent literature on cooling reservoir ecosystems, has revealed that entrainment, thermal, and chemical effects generally result in reduced populations of phytoplankton, zooplankton, and benthos in the vicinity of the power plant discharge. Adverse far field effects are generally less significant and are sometimes stimulatory. The overall effects of a power plant on the fish populations of cooling reservoirs appear to be minor. Based on the thermal characteristics of a model 6400 acre cooling reservoir with four 1150 MWe reactors, the ecological characteristics of the reservoir were predicted. The multiple use possibilities of cooling reservoirs provide their most significant beneficial aspect when compared to cooling towers. In addition, the cage culture of food fishes in cooling reservoirs provides an economical and practical method of commercially utilizing the waste heat discharged by power plants. For many areas of the country, cooling reservoirs appear to provide an environmentally and socially desirable alternative to cooling towers

  3. From Fed-batch to Continuous Enzymatic Biodiesel Production

    DEFF Research Database (Denmark)

    Price, Jason Anthony; Nordblad, Mathias; Woodley, John M.;

    2015-01-01

    In this this paper, we use mechanistic modelling to guide the development of acontinuous enzymatic process that is performed as a fed-batch operation. In this workwe use the enzymatic biodiesel process as a case study. A mechanistic model developedin our previous work was used to determine...... measured components (triglycerides, diglycerides, monoglycerides, free fatty acid and fatty acid methyl esters(biodiesel)) much better than using fed-batch data alone given the smaller residuals. We also observe a reduction in the correlation between the parameters.The model was then used to predict that 5...... reactors are required (with a combined residence time of 30 hours) to reach a final biodiesel concentration within 2 % of the95.6 mass % achieved in a fed-batch operation, for 24 hours....

  4. Biogas plasticization coupled anaerobic digestion: batch test results.

    Science.gov (United States)

    Schimel, Keith A

    2007-06-01

    Biogas has unique properties for improving the biodegradability of biomass solids during anaerobic digestion (AD). This report presents batch test results of the first investigation into utilizing biogas plasticization to "condition" organic polymers during active digestion of waste activated sludge (WAS). Preliminary design calculations based on polymer diffusion rate limitation are presented. Analysis of the 20 degrees C batch test data determined the first order (k(1)) COD conversion coefficient to be 0.167 day(-1) with a maximum COD utilization rate of 11.25 g L(-1) day(-1). Comparison of these batch test results to typical conventional AD performance parameters showed orders of magnitude improvement. These results show that biogas plasticization during active AD could greatly improve renewable energy yields from biomass waste materials such as MSW RDF, STP sludges, food wastes, animal manure, green wastes, and agricultural crop residuals. PMID:17054122

  5. A new titanium-bearing calcium aluminosilicate phase. 2: Crystallography and crystal chemistry of grains formed in slowly cooled melts with bulk compositions of calcium-aluminium-rich inclusions

    Science.gov (United States)

    Barber, David J.; Beckett, John R.; Paque, Julie M.; Stolper, Edward

    1994-01-01

    The crystallography and crystal chemistry of a new calcium- titanium-aluminosilicate mineral (UNK) observed in synthetic analogs to calcium-aluminum-rich inclusions (CAIs) from carbonaceous chondrites was studied by electron diffraction techniques. The unit cell is primitive hexagonal or trigonal, with a = 0.790 +/- 0.02 nm and c = 0.492 +/- 0.002 nm, similar to the lattice parameters of melilite and consistent with cell dimensions for crystals in a mixer furnace slag described by Barber and Agrell (1994). The phase frequently displays an epitactic relationship in which melilite acts as the host, with (0001)(sub UNK) parallel (001)(sub mel) and zone axis group 1 0 -1 0(sub UNK) parallel zone axis group 1 0 0(sub mel). If one of the two space groups determined by Barber and Agrell (1994) for their sample of UNK is applicable (P3m1 or P31m), then the structure is probably characterized by puckered sheets of octahedra and tetrahedra perpendicular to the c-axis with successive sheets coordinated by planar arrays of Ca. In this likely structure, each unit cell contains three Ca sites located in mirror planes, one octahedrally coordinated cation located along a three-fold axis and five tetrahedrally coordinated cations, three in mirrors and two along triads. The octahedron contains Ti but, because there are 1.3-1.9 cations of Ti/formula unit, some of the Ti must also be in tetrahedral coordination, an unusual but not unprecedented situation for a silicate. Tetrahedral sites in mirror planes would contain mostly Si, with lesser amounts of Al while those along the triads correspondingly contain mostly Al with subordinate Ti. The structural formula, therefore, can be expressed as Ca(sub 3)(sup VIII)(Ti,Al)(sup VI)(Al,Ti,Si)(sub 2)(sup IV)(Si,Al)(sub 3)(sup IV)O14 with Si + Ti = 4. Compositions of meteoritic and synthetic Ti-bearing samples of the phase can be described in terms of a binary solid solution between the end-members Ca3TiAl2Si3O14 and Ca3Ti(AlTi)(AlSi2)O14. A Ti

  6. Measuring the coolness of interactive products: the COOL questionnaire

    DEFF Research Database (Denmark)

    Bruun, Anders; Raptis, Dimitrios; Kjeldskov, Jesper;

    2016-01-01

    is the COOL questionnaire. We based the creation of the questionnaire on literature suggesting that perceived coolness is decomposed to outer cool (the style of a product) and inner cool (the personality characteristics assigned to it). In this paper, we focused on inner cool, and we identified 11...... inner cool characteristics. These were used to create an initial pool of question items and 2236 participants were asked to assess 16 mobile devices. By performing exploratory and confirmatory factor analyses, we identified three factors that can measure the perceived inner coolness of interactive...

  7. Formation of Piroxicam Polymorphism in Solution Crystallization

    DEFF Research Database (Denmark)

    Bruun Hansen, Thomas; Qu, Haiyan

    2015-01-01

    Recently, new insights into crystallization prior to actual nucleation have shown interesting results for drugs showing differences in hydrogen bonding or orientation in various polymorphic forms. On the basis of this concept, piroxicam was chosen as a model compound because the two common forms, I...... and II, show hydrogen bonding between different parts of the molecules and differences in the orientation of molecules in the crystal lattice. The goal of this work is to explore how various methods of controlling polymorphism during production could be employed. The mechanisms behind the nucleation...... were also explored, and new insights into polymorphic control are documented and discussed. The crystal landscape was mapped for cooling crystallization of piroxicam from acetone/water mixtures (0.5 K/min) and for antisolvent crystallization from acetone with water as the antisolvent. Varying cooling...

  8. Cooled optical luminescence dosimetry in plastic matrices

    International Nuclear Information System (INIS)

    Large-scale dosimetry services such as Landauer, Inc., require cost-effective, easy-to-manufacture dosemeters that are available in high volume with good precision and uniformity between batches. The ability to re-analyse a dosemeter and to perform necessary exposure diagnostics familiar to film dosimetrists are also desirable qualities of a dosimetric system. Battelle has developed a cooled optical luminescence dosimetry (COLD) system that allows all these features to be combined into one practical dosimetry system. COLD technology uses an extremely sensitive phototransfer mechanism manifested in certain solid state materials. Modest cooling below room temperature is required during the readout of the COLD detectors. Excitation with a laser or other light source is required to initiate the phototransfer process. Warming to near room temperature liberates the luminescence that is proportional to the radiation exposure. Due to the low readout temperatures, COLD phosphor materials can be packaged in polymers without fear of melting the polymer matrix, as would occur using a thermoluminescent process. Besides extreme sensitivity (minimum detectable exposure levels of 0.1 μSv are possible), the detectors can be reanalysed with minimal loss of signal. An imaging film is created by the mixture of small grains of COLD phosphor in the polymer matrix. A sensitive CCD or microchannel PMT device acquires a two-dimensional image of the dosemeter luminescence. The resulting digital image can then be mathematically interrogated to determine exposure diagnostics in the same way that film is currently used. (author)

  9. Seed selections for crystallization of calcium phosphate for phosphorus recovery

    Institute of Scientific and Technical Information of China (English)

    SONG Yong-hui; Dietfried DONNERT; Ute BERG; Peter G. WEIDLER; Rolf NUEESCH

    2007-01-01

    Seed induces and promotes the crystallization of calcium phosphate, and acts as carrier of the recovered phosphorus (P). In order to select suitable seed for P recovery from wastewater, three seeds including Apatite (AP), Juraperle (JP) and phosphate-modified Juraperle (M-JP) were tested and compared. Batch and fixed-bed column experiments of seeded crystallization of calcium phosphate were undertaken by using synthetic wastewater with 10 mg/L P phosphate. It shows that AP has bad enduring property in the crystallization process, while JP has better performance for multiple uses, and M-JP is a hopeful seed for P recovery by crystallization of calcium phosphate.

  10. Batch-related sterile endophthalmitis following intravitreal injection of bevacizumab

    Directory of Open Access Journals (Sweden)

    Morteza Entezari

    2014-01-01

    Full Text Available Background: To report a series of patients with sterile endophthalmitis after intravitreal bevacizumab (IVB injection from 2 different batches of bevacizumab. Materials and Methods: Records of 11 eyes with severe inflammation after IVB injections from two different batches (7 eyes from one and 4 from the other on two separate days were evaluated. Fifteen eyes of 15 patients in one day were treated with one batch and 18 eyes of 17 patients were treated another day using another batch injected for different retinal diseases. Each batch was opened on the day of injection. We used commercially available bevacizumab (100 mg/4 ml kept at 4°C. Severe cases with hypopyon were admitted to the ward and underwent anterior chamber and vitreous tap for direct smear and culture. Results: Pain, redness and decreased vision began after 11-17 days. All had anterior chamber and vitreous reactions and 5 had hypopyon. Antibiotics and corticosteroids were initiated immediately, but the antibiotics were discontinued after negative culture results. Visual acuity returned to pre-injection levels in 10 eyes after 1 month and only in one eye pars plana vitrectomy was performed. Mean VA at the time of presentation with inflammation (1.76 ± 0.78 logMAR decreased significantly (P = 0.008 compared to the initial mean corrected VA (1.18 ± 0.55 logMAR; however, final mean corrected VA (1.02 ± 0.48 logMAR improved in comparison with the baseline but not to a significant level (P = 0.159. Conclusions: We report a cluster of sterile endophthalmitis following intravitreal injection of bevacizumab from the same batch of bevacizumab that has a favorable prognosis.

  11. Crystallization of ornithine acetyltransferase from yeast by counter-diffusion and preliminary X-ray study

    Energy Technology Data Exchange (ETDEWEB)

    Maes, Dominique, E-mail: dominique.maes@vub.ac.be; Crabeel, Marjolaine [Laboratorium voor Ultrastructuur, Vrije Universiteit Brussel (VUB) and Vlaams Interuniversitair Instituut voor Biotechnologie (VIB), Pleinlaan 2, B-1050 Brussels (Belgium); Van de Weerdt, Cécile; Martial, Joseph [Laboratoire de Biologie Moléculaire et de Génie Génétique, Université de Liège, Allée de la Chimie 3, B-4000 Liège (Belgium); Peeters, Eveline; Charlier, Daniël [Erfelijkheidsleer en Microbiologie, Vrije Universiteit Brussel (VUB), Pleinlaan 2, B-1050 Brussels (Belgium); Decanniere, Klaas; Vanhee, Celine; Wyns, Lode; Zegers, Ingrid [Laboratorium voor Ultrastructuur, Vrije Universiteit Brussel (VUB) and Vlaams Interuniversitair Instituut voor Biotechnologie (VIB), Pleinlaan 2, B-1050 Brussels (Belgium)

    2006-12-01

    A study on the crystallization of ornithine acetyltransferase from yeast, catalysing the fifth step in microbial arginine synthesis, is presented. The use of the counter-diffusion technique removes the disorder present in one dimension in crystals grown by either batch or hanging-drop techniques. A study is presented on the crystallization of ornithine acetyltransferase from yeast, which catalyzes the fifth step in microbial arginine synthesis. The use of the counter-diffusion technique removes the disorder present in one dimension in crystals grown by either the batch or hanging-drop techniques. This makes the difference between useless crystals and crystals that allow successful determination of the structure of the protein. The crystals belong to space group P4, with unit-cell parameters a = b = 66.98, c = 427.09 Å, and a data set was collected to 2.76 Å.

  12. Crystallization of ornithine acetyltransferase from yeast by counter-diffusion and preliminary X-ray study

    International Nuclear Information System (INIS)

    A study on the crystallization of ornithine acetyltransferase from yeast, catalysing the fifth step in microbial arginine synthesis, is presented. The use of the counter-diffusion technique removes the disorder present in one dimension in crystals grown by either batch or hanging-drop techniques. A study is presented on the crystallization of ornithine acetyltransferase from yeast, which catalyzes the fifth step in microbial arginine synthesis. The use of the counter-diffusion technique removes the disorder present in one dimension in crystals grown by either the batch or hanging-drop techniques. This makes the difference between useless crystals and crystals that allow successful determination of the structure of the protein. The crystals belong to space group P4, with unit-cell parameters a = b = 66.98, c = 427.09 Å, and a data set was collected to 2.76 Å

  13. Optimization of ectoine synthesis through fed-batch fermentation of Brevibacterium epidermis.

    Science.gov (United States)

    Onraedt, Annelies E; Walcarius, Bart A; Soetaert, Wim K; Vandamme, Erick J

    2005-01-01

    A production process for ectoine has been developed, using Brevibacterium epidermis DSM20659 as the producer strain. First, the optimal conditions for intracellular synthesis of ectoine were determined. The size of the intracellular ectoine pool is shown to be dependent on the external salt concentration, type of carbon source, and yeast extract concentration. Under the optimized conditions of 1 M NaCl, 50 g/L monosodium glutamate, and 2.5 g/L yeast extract, a maximum concentration of intracellular ectoine of 0.9 g/L was obtained in shake flask cultures. After optimizing the batch fermentation parameters of temperature, pH, agitation, and aeration, the yield could be further increased by applying the fed-batch fermentation principle in 1.5- to 2-L fermentors. Glutamate and yeast extract were fed to the bacterial cells such that the total glutamate concentration in the broth remained constant. A total yield of 8 g ectoine/L fermentation broth was obtained with a productivity of 2 g ectoine/L/day. After the bacterial cells were harvested from the culture broth, the ectoine was recovered from them by a two-step extraction with water and ethanol. Crystallization of the product was obtained after concentration of the extract via evaporation under reduced pressure. After this downstream process, 55% of the ectoine produced in the fermentor could be crystallized in four fractions. The first fractions were of very high purity (98%). This production process can compete with other described production processes for ectoine in productivity and simplicity. Further advantages are the relatively low amounts of NaCl needed and the absence of hydroxyectoine, often a byproduct, in the final product. PMID:16080703

  14. Production of tea vinegar by batch and semicontinuous fermentation

    OpenAIRE

    Pardeep KAUR; Kocher, G. S.; Phutela, R. P.

    2010-01-01

    The fermented tea vinegar combines the beneficial properties of tea and vinegar. The complete fermentation takes 4 to 5 weeks in a batch culture and thus can be shortened by semi continuous/ continuous fermentation using immobilized bacterial cells. In the present study, alcoholic fermentation of 1.0 and 1.5% tea infusions using Saccharomyces cerevisae G was carried out that resulted in 84.3 and 84.8% fermentation efficiency (FE) respectively. The batch vinegar fermentation of these wines wit...

  15. JAVA Implementation of the Batched iLab Shared Architecture

    OpenAIRE

    Lenard Payne; Mark Schulz

    2013-01-01

    The MIT iLab Shared Architecture is limited currently to running on the Microsoft Windows platform. A JAVA implementation of the Batched iLab Shared Architecture has been developed that can be used on other operating systems and still interoperate with the existing Microsoft .NET web services of MIT’s iLab ServiceBroker. The Batched iLab Shared Architecture has been revised and separates the Labserver into a LabServer that handles experiment management and a LabEquipment that handles experime...

  16. Stochastic growth logistic model with aftereffect for batch fermentation process

    Energy Technology Data Exchange (ETDEWEB)

    Rosli, Norhayati; Ayoubi, Tawfiqullah [Faculty of Industrial Sciences and Technology, Universiti Malaysia Pahang, Lebuhraya Tun Razak, 26300 Gambang, Pahang (Malaysia); Bahar, Arifah; Rahman, Haliza Abdul [Department of Mathematical Sciences, Faculty of Science, Universiti Teknologi Malaysia, 81310 Johor Bahru, Johor (Malaysia); Salleh, Madihah Md [Department of Biotechnology Industry, Faculty of Biosciences and Bioengineering, Universiti Teknologi Malaysia, 81310 Johor Bahru, Johor (Malaysia)

    2014-06-19

    In this paper, the stochastic growth logistic model with aftereffect for the cell growth of C. acetobutylicum P262 and Luedeking-Piret equations for solvent production in batch fermentation system is introduced. The parameters values of the mathematical models are estimated via Levenberg-Marquardt optimization method of non-linear least squares. We apply Milstein scheme for solving the stochastic models numerically. The effciency of mathematical models is measured by comparing the simulated result and the experimental data of the microbial growth and solvent production in batch system. Low values of Root Mean-Square Error (RMSE) of stochastic models with aftereffect indicate good fits.

  17. Stochastic growth logistic model with aftereffect for batch fermentation process

    International Nuclear Information System (INIS)

    In this paper, the stochastic growth logistic model with aftereffect for the cell growth of C. acetobutylicum P262 and Luedeking-Piret equations for solvent production in batch fermentation system is introduced. The parameters values of the mathematical models are estimated via Levenberg-Marquardt optimization method of non-linear least squares. We apply Milstein scheme for solving the stochastic models numerically. The effciency of mathematical models is measured by comparing the simulated result and the experimental data of the microbial growth and solvent production in batch system. Low values of Root Mean-Square Error (RMSE) of stochastic models with aftereffect indicate good fits

  18. Preparation and evaluation of mercuric iodide for crystal growth

    Energy Technology Data Exchange (ETDEWEB)

    Skinner, N.L.; Ortale, C.; Schieber, M.M.

    1988-01-01

    Large quantities, on the order of several hundred, of consistent, high quality mercuric iodide for crystal growth have not been commercially available. The hydrocarbon, anion, and cation impurity levels varied considerably, occasionally preventing crystal growth. This occurred even though the starting materials was from the same vendor and was subjected to the same purification treatment. This paper will describe an aqueous precipitation process of mercuric iodide preparation in batches of 3 kg using Hg(NO/sub 3/)/sub 2/ or HgCl/sub 2/and KI. Since these salts are produced in much larger quantities than mercuric iodide, more consistent quality is available. The impurity content of these batched and single crystals are compared. Some of the single crystals grown using the in-house prepared mercuric iodide have yielded a large number of spectroscopy grade nuclear radiation detectors. The influence of the major impuritites are discussed. 13 refs., 4 figs., 1 tab.

  19. Cool WISPs for stellar cooling excesses

    Science.gov (United States)

    Giannotti, Maurizio; Irastorza, Igor; Redondo, Javier; Ringwald, Andreas

    2016-05-01

    Several stellar systems (white dwarfs, red giants, horizontal branch stars and possibly the neutron star in the supernova remnant Cassiopeia A) show a mild preference for a non-standard cooling mechanism when compared with theoretical models. This exotic cooling could be provided by Weakly Interacting Slim Particles (WISPs), produced in the hot cores and abandoning the star unimpeded, contributing directly to the energy loss. Taken individually, these excesses do not show a strong statistical weight. However, if one mechanism could consistently explain several of them, the hint could be significant. We analyze the hints in terms of neutrino anomalous magnetic moments, minicharged particles, hidden photons and axion-like particles (ALPs). Among them, the ALP or a massless HP represent the best solution. Interestingly, the hinted ALP parameter space is accessible to the next generation proposed ALP searches, such as ALPS II and IAXO and the massless HP requires a multi TeV energy scale of new physics that might be accessible at the LHC.

  20. Diffusion-Cooled Tantalum Hot-Electron Bolometer Mixers

    Science.gov (United States)

    Skalare, Anders; McGrath, William; Bumble, Bruce; LeDuc, Henry

    2004-01-01

    A batch of experimental diffusion-cooled hot-electron bolometers (HEBs), suitable for use as mixers having input frequencies in the terahertz range and output frequencies up to about a gigahertz, exploit the superconducting/normal-conducting transition in a thin strip of tantalum. The design and operation of these HEB mixers are based on mostly the same principles as those of a prior HEB mixer that exploited the superconducting/normal- conducting transition in a thin strip of niobium and that was described elsewhere.

  1. Sulfate Solubility Limit Verification For DWPF Sludge Batch 7B

    International Nuclear Information System (INIS)

    The objective of this study was to determine a sulfate solubility limit in glass for Sludge Batch 7b (SB7b). The SB7b composition projection provided by Savannah River Remediation (SRR) on May 25, 2011 was used as the basis for formulating glass compositions to determine the sulfate limit. Additions of Na2O to the projected sludge composition were made by the Savannah River National Laboratory (SRNL) due to uncertainty in the final concentration of Na2O for SB7b, which is dependent on washing effectiveness and the potential need to add NaOH to ensure an acceptable projected operating window. Additions of 4, 6, and 8 wt % Na2O were made to the nominal May 25, 2011 composition projection. An updated SB7b composition projection was received from SRR on August 4, 2011. Due to compositional similarities, no additional experimental work using the August 4, 2011 compositions was considered to be necessary for this study. Both Frit 418 and Frit 702 were included in this study. The targeted sulfate (SO42-) concentrations of the study glasses were selected within the range of 0.6 to 0.9 wt % in glass. A total of 52 glass compositions were selected based on the compositional variables of Na2O addition, Actinide Removal Process (ARP) stream addition, waste loading, frit composition, and sulfate concentration. The glasses were batched, melted, and characterized following SRNL procedures. Visual observations were recorded for each glass after it cooled and used as in indicator of sulfur retention. Representative samples of each of the glasses fabricated were subjected to chemical analysis to determine whether the targeted compositions were met, as well as to determine the quantity of sulfate that was retained after melting. In general, the measured composition data showed that there were only minor issues in meeting the targeted compositions for the study glasses, and the measured sulfate concentrations for each study glass were within 10% of the targeted values. The results for

  2. SULFATE SOLUBILITY LIMIT VERIFICATION FOR DWPF SLUDGE BATCH 7B

    Energy Technology Data Exchange (ETDEWEB)

    Fox, K.

    2011-10-03

    The objective of this study was to determine a sulfate solubility limit in glass for Sludge Batch 7b (SB7b). The SB7b composition projection provided by Savannah River Remediation (SRR) on May 25, 2011 was used as the basis for formulating glass compositions to determine the sulfate limit. Additions of Na{sub 2}O to the projected sludge composition were made by the Savannah River National Laboratory (SRNL) due to uncertainty in the final concentration of Na{sub 2}O for SB7b, which is dependent on washing effectiveness and the potential need to add NaOH to ensure an acceptable projected operating window. Additions of 4, 6, and 8 wt % Na{sub 2}O were made to the nominal May 25, 2011 composition projection. An updated SB7b composition projection was received from SRR on August 4, 2011. Due to compositional similarities, no additional experimental work using the August 4, 2011 compositions was considered to be necessary for this study. Both Frit 418 and Frit 702 were included in this study. The targeted sulfate (SO{sub 4}{sup 2-}) concentrations of the study glasses were selected within the range of 0.6 to 0.9 wt % in glass. A total of 52 glass compositions were selected based on the compositional variables of Na{sub 2}O addition, Actinide Removal Process (ARP) stream addition, waste loading, frit composition, and sulfate concentration. The glasses were batched, melted, and characterized following SRNL procedures. Visual observations were recorded for each glass after it cooled and used as in indicator of sulfur retention. Representative samples of each of the glasses fabricated were subjected to chemical analysis to determine whether the targeted compositions were met, as well as to determine the quantity of sulfate that was retained after melting. In general, the measured composition data showed that there were only minor issues in meeting the targeted compositions for the study glasses, and the measured sulfate concentrations for each study glass were within 10% of

  3. Crystallization of ornithine acetyltransferase from yeast by counter-diffusion and preliminary X-ray study

    OpenAIRE

    Maes, Dominique; Crabeel, Marjolaine; Van de Weerdt, Cécile; Martial, Joseph; Peeters, Eveline; Charlier, Daniël; Decanniere, Klaas; Vanhee, Celine; Wyns, Lode; Zegers, Ingrid

    2006-01-01

    A study on the crystallization of ornithine acetyltransferase from yeast, catalysing the fifth step in microbial arginine synthesis, is presented. The use of the counter-diffusion technique removes the disorder present in one dimension in crystals grown by either batch or hanging-drop techniques.

  4. Monitoring Cray Cooling Systems

    Energy Technology Data Exchange (ETDEWEB)

    Maxwell, Don E [ORNL; Ezell, Matthew A [ORNL; Becklehimer, Jeff [Cray, Inc.; Donovan, Matthew J [ORNL; Layton, Christopher C [ORNL

    2014-01-01

    While sites generally have systems in place to monitor the health of Cray computers themselves, often the cooling systems are ignored until a computer failure requires investigation into the source of the failure. The Liebert XDP units used to cool the Cray XE/XK models as well as the Cray proprietary cooling system used for the Cray XC30 models provide data useful for health monitoring. Unfortunately, this valuable information is often available only to custom solutions not accessible by a center-wide monitoring system or is simply ignored entirely. In this paper, methods and tools used to harvest the monitoring data available are discussed, and the implementation needed to integrate the data into a center-wide monitoring system at the Oak Ridge National Laboratory is provided.

  5. Core cooling systems

    International Nuclear Information System (INIS)

    The reactor cooling system transports the heat liberated in the reactor core to the component - heat exchanger, steam generator or turbine - where the energy is removed. This basic task can be performed with a variety of coolants circulating in appropriately designed cooling systems. The choice of any one system is governed by principles of economics and natural policies, the design is determined by the laws of nuclear physics, thermal-hydraulics and by the requirement of reliability and public safety. PWR- and BWR- reactors today generate the bulk of nuclear energy. Their primary cooling systems are discussed under the following aspects: 1. General design, nuclear physics constraints, energy transfer, hydraulics, thermodynamics. 2. Design and performance under conditions of steady state and mild transients; control systems. 3. Design and performance under conditions of severe transients and loss of coolant accidents; safety systems. (orig./RW)

  6. Doppler cooling a microsphere

    CERN Document Server

    Barker, P F

    2010-01-01

    Doppler cooling the center-of-mass motion of an optically levitated microsphere via the velocity dependent scattering force from narrow whispering gallery mode (WGM) resonances is described. Light that is red detuned from the WGM resonance can be used to damp the center-of-mass motion in a process analogous to the Doppler cooling of atoms. Leakage of photons out of the microsphere when the incident field is near resonant with the narrow WGM resonance acts to damp the motion of the sphere. The scattering force is not limited by saturation, but can be controlled by the incident power. Cooling times on the order of seconds are calculated for a 20 micron diameter silica microsphere trapped within optical tweezers, with a Doppler temperature limit in the microKelvin regime.

  7. Passive containment cooling system

    Science.gov (United States)

    Billig, Paul F.; Cooke, Franklin E.; Fitch, James R.

    1994-01-01

    A passive containment cooling system includes a containment vessel surrounding a reactor pressure vessel and defining a drywell therein containing a non-condensable gas. An enclosed wetwell pool is disposed inside the containment vessel, and a gravity driven cooling system (GDCS) pool is disposed above the wetwell pool in the containment vessel and is vented to the drywell. An isolation pool is disposed above the GDCS pool and includes an isolation condenser therein. The condenser has an inlet line disposed in flow communication with the drywell for receiving the non-condensable gas along with any steam released therein following a loss-of-coolant accident (LOCA). The condenser also has an outlet line disposed in flow communication with the drywell for returning to the drywell both liquid condensate produced upon cooling of the steam and the non-condensable gas for reducing pressure within the containment vessel following the LOCA.

  8. Lipid production in batch and fed-batch cultures of Rhodosporidium toruloides from 5 and 6 carbon carbohydrates

    Directory of Open Access Journals (Sweden)

    Wiebe Marilyn G

    2012-05-01

    Full Text Available Abstract Background Microbial lipids are a potential source of bio- or renewable diesel and the red yeast Rhodosporidium toruloides is interesting not only because it can accumulate over 50% of its dry biomass as lipid, but also because it utilises both five and six carbon carbohydrates, which are present in plant biomass hydrolysates. Methods R. toruloides was grown in batch and fed-batch cultures in 0.5 L bioreactors at pH 4 in chemically defined, nitrogen restricted (C/N 40 to 100 media containing glucose, xylose, arabinose, or all three carbohydrates as carbon source. Lipid was extracted from the biomass using chloroform-methanol, measured gravimetrically and analysed by GC. Results Lipid production was most efficient with glucose (up to 25 g lipid L−1, 48 to 75% lipid in the biomass, at up to 0.21 g lipid L−1 h−1 as the sole carbon source, but high lipid concentrations were also produced from xylose (36 to 45% lipid in biomass. Lipid production was low (15–19% lipid in biomass with arabinose as sole carbon source and was lower than expected (30% lipid in biomass when glucose, xylose and arabinose were provided simultaneously. The presence of arabinose and/or xylose in the medium increased the proportion of palmitic and linoleic acid and reduced the proportion of oleic acid in the fatty acids, compared to glucose-grown cells. High cell densities were obtained in both batch (37 g L−1, with 49% lipid in the biomass and fed-batch (35 to 47 g L−1, with 50 to 75% lipid in the biomass cultures. The highest proportion of lipid in the biomass was observed in cultures given nitrogen during the batch phase but none with the feed. However, carbohydrate consumption was incomplete when the feed did not contain nitrogen and the highest total lipid and best substrate consumption were observed in cultures which received a constant low nitrogen supply. Conclusions Lipid production in R. toruloides was lower from arabinose and mixed

  9. Ethanol production from Sorghum bicolor using both separate and simultaneous saccharification and fermentation in batch and fed batch systems

    DEFF Research Database (Denmark)

    Mehmood, Sajid; Gulfraz, M.; Rana, N. F.;

    2009-01-01

    were used in order to increase the monomeric sugar during enzymatic hydrolysis and it has been observed that the addition of these surfactants contributed significantly in cellulosic conversion but no effect was shown on hemicellulosic hydrolysis. Fermentability of hydrolyzate was tested using...... Saccharomyces cerevisiae Ethanol Red (TM) and it was observed that simultaneous saccharification and fermentation ( SSF) with both batch and fed batch resulted in better ethanol yield as compared to separate hydrolysis and fermentation ( SHF). Detoxification of furan during SHF facilitated reduction in...

  10. Heat transport through ion crystals

    Science.gov (United States)

    Freitas, Nahuel; Martinez, Esteban A.; Paz, Juan Pablo

    2016-01-01

    We study the thermodynamical properties of crystals of trapped ions which are laser cooled to two different temperatures in two separate regions. We show that these properties strongly depend on the structure of the ion crystal. Such structure can be changed by varying the trap parameters and undergoes a series of phase transitions from linear to zig-zag or helicoidal configurations. Thus, we show that these systems are ideal candidates to observe and control the transition from anomalous to normal heat transport. All structures behave as ‘heat superconductors’, with a thermal conductivity increasing linearly with system size and a vanishing thermal gradient inside the system. However, zig-zag and helicoidal crystals turn out to be hyper sensitive to disorder having a linear temperature profile and a length independent conductivity. Interestingly, disordered 2D ion crystals are heat insulators. Sensitivity to disorder is much smaller in the 1D case.

  11. NEPHELINE FORMATION POTENTIAL IN SLUDGE BATCH 4 AND ITS IMPACT ON DURABILITY: SELECTING GLASSES FOR A PHASE 3 STUDY

    Energy Technology Data Exchange (ETDEWEB)

    Fox, K

    2006-01-27

    -3 are to batched and fabricated using standard procedures. Visual observations and other analytical techniques are to be used, as needed, to assess the presence of crystals with specific interest in the nepheline primary phase. The durability of these glasses (for both quenched and centerline canister cooled versions) is to be measured using the ASTM PCT Method A. The results from these efforts are to be documented in a subsequent report. The results of this study will provide valuable input for the frit development efforts and subsequent feedback to the CBU regarding the relative viability of the current SB4 option under consideration. The refined nepheline discriminator value will provide a guideline for the avoidance of nepheline crystallization in SB4 glasses and aid in down-selection of frit compositions. These data will be combined with the results of melt rate studies and a paper study of the frits robustness with regard to variability in the sludge composition to provide an optimized frit recommendation to DWPF for immobilization of SB4.

  12. Anomalous law of cooling

    Energy Technology Data Exchange (ETDEWEB)

    Lapas, Luciano C., E-mail: luciano.lapas@unila.edu.br [Universidade Federal da Integração Latino-Americana, Caixa Postal 2067, 85867-970 Foz do Iguaçu, Paraná (Brazil); Ferreira, Rogelma M. S., E-mail: rogelma.maria@gmail.com [Centro de Ciências Exatas e Tecnológicas, Universidade Federal do Recôncavo da Bahia, 44380-000 Cruz das Almas, Bahia (Brazil); Rubí, J. Miguel, E-mail: mrubi@ub.edu [Departament de Física Fonamental, Facultat de Física, Universitat de Barcelona, Av. Diagonal 647, 08028 Barcelona (Spain); Oliveira, Fernando A., E-mail: fernando.oliveira@pq.cnpq.br [Instituto de Física and Centro Internacional de Física da Matéria Condensada, Universidade de Brasília, Caixa Postal 04513, 70919-970 Brasília, Distrito Federal (Brazil)

    2015-03-14

    We analyze the temperature relaxation phenomena of systems in contact with a thermal reservoir that undergoes a non-Markovian diffusion process. From a generalized Langevin equation, we show that the temperature is governed by a law of cooling of the Newton’s law type in which the relaxation time depends on the velocity autocorrelation and is then characterized by the memory function. The analysis of the temperature decay reveals the existence of an anomalous cooling in which the temperature may oscillate. Despite this anomalous behavior, we show that the variation of entropy remains always positive in accordance with the second law of thermodynamics.

  13. Superconductor rotor cooling system

    Energy Technology Data Exchange (ETDEWEB)

    Gamble, Bruce B.; Sidi-Yekhlef, Ahmed; Schwall, Robert E.; Driscoll, David I.; Shoykhet, Boris A.

    2004-11-02

    A system for cooling a superconductor device includes a cryocooler located in a stationary reference frame and a closed circulation system external to the cryocooler. The closed circulation system interfaces the stationary reference frame with a rotating reference frame in which the superconductor device is located. A method of cooling a superconductor device includes locating a cryocooler in a stationary reference frame, and transferring heat from a superconductor device located in a rotating reference frame to the cryocooler through a closed circulation system external to the cryocooler. The closed circulation system interfaces the stationary reference frame with the rotating reference frame.

  14. Multiphase cooling flows

    OpenAIRE

    Thomas, Peter A.

    1996-01-01

    I discuss the multiphase nature of the intracluster medium whose neglect can lead to overestimates of the baryon fraction of clusters by up to a factor of two. The multiphase form of the cooling flow equations are derived and reduced to a simple form for a wide class of self-similar density distributions. It is shown that steady-state cooling flows are \\emph{not} consistent with all possible emissivity profiles which can therefore be used as a test of the theory. In combination, they provide ...

  15. Anomalous law of cooling

    International Nuclear Information System (INIS)

    We analyze the temperature relaxation phenomena of systems in contact with a thermal reservoir that undergoes a non-Markovian diffusion process. From a generalized Langevin equation, we show that the temperature is governed by a law of cooling of the Newton’s law type in which the relaxation time depends on the velocity autocorrelation and is then characterized by the memory function. The analysis of the temperature decay reveals the existence of an anomalous cooling in which the temperature may oscillate. Despite this anomalous behavior, we show that the variation of entropy remains always positive in accordance with the second law of thermodynamics

  16. Doppler Cooling a Microsphere

    OpenAIRE

    Barker, P F

    2010-01-01

    Doppler cooling the center-of-mass motion of an optically levitated microsphere via the velocity dependent scattering force from narrow whispering gallery mode (WGM) resonances is described. Light that is red detuned from the WGM resonance can be used to damp the center-of-mass motion in a process analogous to the Doppler cooling of atoms. Leakage of photons out of the microsphere when the incident field is near resonant with the narrow WGM resonance acts to damp the motion of the sphere. The...

  17. Anomalous law of cooling

    Science.gov (United States)

    Lapas, Luciano C.; Ferreira, Rogelma M. S.; Rubí, J. Miguel; Oliveira, Fernando A.

    2015-03-01

    We analyze the temperature relaxation phenomena of systems in contact with a thermal reservoir that undergoes a non-Markovian diffusion process. From a generalized Langevin equation, we show that the temperature is governed by a law of cooling of the Newton's law type in which the relaxation time depends on the velocity autocorrelation and is then characterized by the memory function. The analysis of the temperature decay reveals the existence of an anomalous cooling in which the temperature may oscillate. Despite this anomalous behavior, we show that the variation of entropy remains always positive in accordance with the second law of thermodynamics.

  18. Stochastic cooling for beginners

    International Nuclear Information System (INIS)

    These two lectures have been prepared to give a simple introduction to the principles. In Part I we try to explain stochastic cooling using the time-domain picture which starts from the pulse response of the system. In Part II the discussion is repeated, looking more closely at the frequency-domain response. An attempt is made to familiarize the beginners with some of the elementary cooling equations, from the 'single particle case' up to equations which describe the evolution of the particle distribution. (orig.)

  19. Continuous cellulosic bioethanol fermentation by cyclic fed-batch cocultivation.

    Science.gov (United States)

    Jiang, He-Long; He, Qiang; He, Zhili; Hemme, Christopher L; Wu, Liyou; Zhou, Jizhong

    2013-03-01

    Cocultivation of cellulolytic and saccharolytic microbial populations is a promising strategy to improve bioethanol production from the fermentation of recalcitrant cellulosic materials. Earlier studies have demonstrated the effectiveness of cocultivation in enhancing ethanolic fermentation of cellulose in batch fermentation. To further enhance process efficiency, a semicontinuous cyclic fed-batch fermentor configuration was evaluated for its potential in enhancing the efficiency of cellulose fermentation using cocultivation. Cocultures of cellulolytic Clostridium thermocellum LQRI and saccharolytic Thermoanaerobacter pseudethanolicus strain X514 were tested in the semicontinuous fermentor as a model system. Initial cellulose concentration and pH were identified as the key process parameters controlling cellulose fermentation performance in the fixed-volume cyclic fed-batch coculture system. At an initial cellulose concentration of 40 g liter(-1), the concentration of ethanol produced with pH control was 4.5-fold higher than that without pH control. It was also found that efficient cellulosic bioethanol production by cocultivation was sustained in the semicontinuous configuration, with bioethanol production reaching 474 mM in 96 h with an initial cellulose concentration of 80 g liter(-1) and pH controlled at 6.5 to 6.8. These results suggested the advantages of the cyclic fed-batch process for cellulosic bioethanol fermentation by the cocultures. PMID:23275517

  20. Discrete time analysis of batch processes in material flow systems

    OpenAIRE

    Schleyer, Marc

    2007-01-01

    Scope of this work is the development of appropriate models for the evaluation of batch processes in material flow systems. The presented analytical methods support the long range planning in an early planning stage, in which capacities are determined to minimize the facility costs under the condition of cycle time targets.

  1. Batch immunoextraction method for efficient purification of aromatic cytokinins

    Czech Academy of Sciences Publication Activity Database

    Hauserová, Eva; Swaczynová, Jana; Doležal, Karel; Lenobel, René; Popa, Igor; Hajdúch, M.; Vydra, D.; Fuksová, Květoslava; Strnad, Miroslav

    2005-01-01

    Roč. 1100, č. 1 (2005), s. 116-125. ISSN 0021-9673 R&D Projects: GA AV ČR IBS4055304 Institutional research plan: CEZ:AV0Z50380511; MSM6198959216 Keywords : antibody * 6-benzylaminopurine * batch immunoextraction Subject RIV: ED - Physiology Impact factor: 3.096, year: 2005

  2. Batch production of YBCO disks for levitation applications

    Czech Academy of Sciences Publication Activity Database

    Plecháček, V.; Jirsa, Miloš; Rameš, Michal; Muralidhar, M.

    2012-01-01

    Roč. 36, č. 2012 (2012), s. 538-543. ISSN 1875-3892 R&D Projects: GA MŠk(CZ) ME10069 Institutional research plan: CEZ:AV0Z10100520 Keywords : YBCO disk * batch production * levitation * levitation force * rapped magnetic field * critical current density Subject RIV: BM - Solid Matter Physics ; Magnetism

  3. Batch profiling calibration for robust NMR metabonomic data analysis.

    Science.gov (United States)

    Fages, Anne; Pontoizeau, Clément; Jobard, Elodie; Lévy, Pierre; Bartosch, Birke; Elena-Herrmann, Bénédicte

    2013-11-01

    Metabonomic studies involve the analysis of large numbers of samples to identify significant changes in the metabolic fingerprints of biological systems, possibly with sufficient statistical power for analysis. While procedures related to sample preparation and spectral data acquisition generally include the use of independent sample batches, these might be sources of systematic variation whose effects should be removed to focus on phenotyping the relevant biological variability. In this work, we describe a grouped-batch profile (GBP) calibration strategy to adjust nuclear magnetic resonance (NMR) metabolomic data-sets for batch effects either introduced during NMR experiments or samples work-up. We show how this method can be applied to data calibration in the context of a large-scale NMR epidemiological study where quality control samples are available. We also illustrate the efficiency of a batch profile correction for NMR metabonomic investigation of cell extracts, where GBP can significantly improve the predictive power of multivariate statistical models for discriminant analysis of the cell infection status. The method is applicable to a broad range of NMR metabolomic/metabonomic cohort studies. PMID:23975089

  4. Adaptation to high throughput batch chromatography enhances multivariate screening.

    Science.gov (United States)

    Barker, Gregory A; Calzada, Joseph; Herzer, Sibylle; Rieble, Siegfried

    2015-09-01

    High throughput process development offers unique approaches to explore complex process design spaces with relatively low material consumption. Batch chromatography is one technique that can be used to screen chromatographic conditions in a 96-well plate. Typical batch chromatography workflows examine variations in buffer conditions or comparison of multiple resins in a given process, as opposed to the assessment of protein loading conditions in combination with other factors. A modification to the batch chromatography paradigm is described here where experimental planning, programming, and a staggered loading approach increase the multivariate space that can be explored with a liquid handling system. The iterative batch chromatography (IBC) approach is described, which treats every well in a 96-well plate as an individual experiment, wherein protein loading conditions can be varied alongside other factors such as wash and elution buffer conditions. As all of these factors are explored in the same experiment, the interactions between them are characterized and the number of follow-up confirmatory experiments is reduced. This in turn improves statistical power and throughput. Two examples of the IBC method are shown and the impact of the load conditions are assessed in combination with the other factors explored. PMID:25914370

  5. Design of common heat exchanger network for batch processes

    International Nuclear Information System (INIS)

    Heat integration of energy streams is very important for the efficient energy recovery in production systems. Pinch technology is a very useful tool for heat integration and maximizing energy efficiency. Creating of heat exchangers network as a common solution for systems in batch mode that will be applicable in all existing time slices is very difficult. This paper suggests a new methodology for design of common heat exchanger network for batch processes. Heat exchanger network designs were created for all determined repeatable and non-repeatable time periods – time slices. They are the basis for creating the common heat exchanger network. The common heat exchanger network as solution, satisfies all heat-transfer needs for each time period and for every existing combination of selected streams in the production process. This methodology use split of some heat exchangers into two or more heat exchange units or heat exchange zones. The reason for that is the multipurpose use of heat exchangers between different pairs of streams in different time periods. Splitting of large heat exchangers would maximize the total heat transfer usage of heat exchange units. Final solution contains heat exchangers with the minimum heat load as well as the minimum need of heat transfer area. The solution is applicable for all determined time periods and all existing stream combinations. - Highlights: •Methodology for design of energy efficient systems in batch processes. •Common Heat Exchanger Network solution based on designs with Pinch technology. •Multipurpose use of heat exchangers in batch processes

  6. Reprocessing of spent fuel from AHWR: preliminary batch studies

    International Nuclear Information System (INIS)

    Scheme for the reprocessing of spent fuel from advanced heavy water reactor (AHWR) is under development. Present paper describes the results of some of the preliminary batch studies carried out to collect the data required for conducting counter-current studies. Studies are carried out using simulated solutions and include data on extraction as well as stripping. (author)

  7. Research of an Efficient Variant of Batch RSA Algorithm%一种有效的Batch RSA算法的研究

    Institute of Scientific and Technical Information of China (English)

    李云飞; 柳青; 李彤; 郝林

    2011-01-01

    提出了一种改进的Batch RSA算法来提升Batch RSA算法的解密性能.该改进算法结合了负载转移技术和Multi-Power RSA技术,在Batch RSA算法的指数计算阶段提升Batch RSA算法的解密性能.实验结果和理论分析表明,该改进算法使得Batch RSA算法的解密性能得到显著提升,且易于并行实现,可使基于多核平台的Batch RSA算法的整体性能得到进一步提升.%This paper aimed at speeding up Batch RSA decryption. An efficient variant of Batch RSA was proposed to improve the Batch RSA decryption performance. The improved Batch RSA variant speeds up decryption by combining the load transferring technique and multi-power RSA technique in the exponentiation phase. The experimental result and the theoretical values show that the speed of the decryption is substantially improved and the variant can be efficiently implemented in parallel and parallel implementation of the variant on multi-core devices can further improve the overall performance of Batch RSA algorithm.

  8. Cooling tower and environment

    International Nuclear Information System (INIS)

    The influence of a cooling tower on the environment, or rather the influence of the environment on the cooling tower stands presently -along with the cooling water supply - in the middle of much discussion. The literature on these questions can hardly be overlooked by the experts concerned, especially not by the power station designers and operators. The document 'Cooling Tower and Environment' is intented to give a general idea of the important publications in this field, and to inform of the present state of technology. In this, the explanations on every section make it easier to get to know the specific subject area. In addition to older standard literature, this publication contains the best-known literature of recent years up to spring 1975, including some articles written in English. Further English literature has been collected by the ZAED (KFK) and is available at the VGB-Geschaefsstelle. Furthermore, The Bundesumweltamt compiles the literature on the subject of 'Environmental protection'. On top of that, further documentation centres are listed at the end of this text. (orig.)

  9. Measure Guideline: Ventilation Cooling

    Energy Technology Data Exchange (ETDEWEB)

    Springer, D. [Alliance for Residential Building Innovation (ARBI), David, CA (United States); Dakin, B. [Alliance for Residential Building Innovation (ARBI), David, CA (United States); German, A. [Alliance for Residential Building Innovation (ARBI), David, CA (United States)

    2012-04-01

    The purpose of this measure guideline is to provide information on a cost-effective solution for reducing cooling system energy and demand in homes located in hot-dry and cold-dry climates. This guideline provides a prescriptive approach that outlines qualification criteria, selection considerations, and design and installation procedures.

  10. Elementary stochastic cooling

    International Nuclear Information System (INIS)

    Major headings in this review include: proton sources; antiproton production; antiproton sources and Liouville, the role of the Debuncher; transverse stochastic cooling, time domain; the accumulator; frequency domain; pickups and kickers; Fokker-Planck equation; calculation of constants in the Fokker-Planck equation; and beam feedback

  11. Computer Simulation of Batch Grinding Process Based on Simulink 5.0

    Institute of Scientific and Technical Information of China (English)

    LI Xia; YANG Ying-jie; DENG Hui-yong; HUANG Guang-yao

    2005-01-01

    How to use Simulink software in grinding system was studied. The method of designing batch grinding subsystem and the steps of building batch grinding blockset were introduced. Based on batch grinding population balance model, batch grinding was simulated with Simulink. The results show that the simulation system designed with Simulink explain reasonably the impersonal rule of batch grinding. On the basis of batch grinding simulation, the computer simulation of mineral processing system with Simulink of grinding and classification, comminution, etc, can be properly explored.

  12. MASS PRODUCTION OF THE BENEFICIAL NEMATODE STEINERNEMA CARPOCAPSAE UTILIZING A FED-BATCH CULTURING PROCESS

    OpenAIRE

    Leonard D. Holmes; Inman III, Floyd L.; Sivanadane Mandjiny; Rinu Kooliyottil; Devang Upadhyay

    2013-01-01

    The present study deals with the batch and fed-batch mass production of Steinernema carpocapsae. S. carpocapsae is an entomoparasitic nematode that is used as a biological control agent of soil-borne crop insect pests. The ability and efficiency of fed-batch culture process was successful through the utilization of the nematode’s bacterial symbiont Xenorhabdus nematophila. Results from the fed-batch process were compared to those obtain from the standard batch process. The fed-batch process s...

  13. The Effect of Temperature and Solution pH on the Nucleation of Tetragonal Lysozyme Crystals

    Science.gov (United States)

    Judge, Russell A.; Jacobs, Randolph S.; Frazier, Tyralynn; Snell, Edward H.; Pusey, Marc L.

    1999-01-01

    Part of the challenge of macromolecular crystal growth for structure determination is obtaining crystals with a volume suitable for x-ray analysis. In this respect an understanding of the effect of solution conditions on macromolecule nucleation rates is advantageous. This study investigated the effects of supersaturation, temperature, and pH on the nucleation rate of tetragonal lysozyme crystals. Batch crystallization plates were prepared at given solution concentrations and incubated at set temperatures over 1 week. The number of crystals per well with their size and axial ratios were recorded and correlated with solution conditions. Crystal numbers were found to increase with increasing supersaturation and temperature. The most significant variable, however, was pH; crystal numbers changed by two orders of magnitude over the pH range 4.0-5.2. Crystal size also varied with solution conditions, with the largest crystals obtained at pH 5.2. Having optimized the crystallization conditions, we prepared a batch of crystals under the same initial conditions, and 50 of these crystals were analyzed by x-ray diffraction techniques. The results indicate that even under the same crystallization conditions, a marked variation in crystal properties exists.

  14. Protein Crystallization

    Science.gov (United States)

    Chernov, Alexander A.

    2005-01-01

    Nucleation, growth and perfection of protein crystals will be overviewed along with crystal mechanical properties. The knowledge is based on experiments using optical and force crystals behave similar to inorganic crystals, though with a difference in orders of magnitude in growing parameters. For example, the low incorporation rate of large biomolecules requires up to 100 times larger supersaturation to grow protein, rather than inorganic crystals. Nucleation is often poorly reproducible, partly because of turbulence accompanying the mixing of precipitant with protein solution. Light scattering reveals fluctuations of molecular cluster size, its growth, surface energies and increased clustering as protein ages. Growth most often occurs layer-by-layer resulting in faceted crystals. New molecular layer on crystal face is terminated by a step where molecular incorporation occurs. Quantitative data on the incorporation rate will be discussed. Rounded crystals with molecularly disordered interfaces will be explained. Defects in crystals compromise the x-ray diffraction resolution crucially needed to find the 3D atomic structure of biomolecules. The defects are immobile so that birth defects stay forever. All lattice defects known for inorganics are revealed in protein crystals. Contribution of molecular conformations to lattice disorder is important, but not studied. This contribution may be enhanced by stress field from other defects. Homologous impurities (e.g., dimers, acetylated molecules) are trapped more willingly by a growing crystal than foreign protein impurities. The trapped impurities induce internal stress eliminated in crystals exceeding a critical size (part of mni for ferritin, lysozyme). Lesser impurities are trapped from stagnant, as compared to the flowing, solution. Freezing may induce much more defects unless quickly amorphysizing intracrystalline water.

  15. Glucoamylase production in batch, chemostat and fed-batch cultivations by an industrial strain of Aspergillus niger

    DEFF Research Database (Denmark)

    Pedersen, Henrik; Beyer, Michael; Nielsen, Jens

    2000-01-01

    The Aspergillus niger strain BO-1 was grown in batch, continuous (chemostat) and fed-batch cultivations in order to study the production of the extracellular enzyme glucoamylase under different growth conditions. In the pH range 2.5-6.0, the specific glucoamylase productivity and the specific...... growth rate of the fungus were independent of pH when grown in batch cultivations. The specific glucoamylase productivity increased linearly with the specific growth rate in the range 0-0.1 h(-1) and was constant in the range 0.1-0.2 h(-1) Maltose and maltodextrin were non-inducing carbon sources...... compared to glucose, and the maximum specific growth rate was 0.19 +/- 0.02 h(-1) irrespective of whether glucose or maltose was the carbon source. In fed-batch cultivations, glucoamylase titres of up to 6.5 g 1(-1) were obtained even though the strain contained only one copy of the glaA gene....

  16. Computational crystallization.

    Science.gov (United States)

    Altan, Irem; Charbonneau, Patrick; Snell, Edward H

    2016-07-15

    Crystallization is a key step in macromolecular structure determination by crystallography. While a robust theoretical treatment of the process is available, due to the complexity of the system, the experimental process is still largely one of trial and error. In this article, efforts in the field are discussed together with a theoretical underpinning using a solubility phase diagram. Prior knowledge has been used to develop tools that computationally predict the crystallization outcome and define mutational approaches that enhance the likelihood of crystallization. For the most part these tools are based on binary outcomes (crystal or no crystal), and the full information contained in an assembly of crystallization screening experiments is lost. The potential of this additional information is illustrated by examples where new biological knowledge can be obtained and where a target can be sub-categorized to predict which class of reagents provides the crystallization driving force. Computational analysis of crystallization requires complete and correctly formatted data. While massive crystallization screening efforts are under way, the data available from many of these studies are sparse. The potential for this data and the steps needed to realize this potential are discussed. PMID:26792536

  17. ELECTRON COOLING STUDY FOR MEIC

    Energy Technology Data Exchange (ETDEWEB)

    He, Zhang [Jefferson Lab, Newport News, VA; Douglas, David R. [Jefferson Lab, Newport News, VA; Derbenev, Yaroslav S. [Jefferson Lab, Newport News, VA; Zhang, Yuhong [Jefferson Lab, Newport News, VA

    2015-09-01

    Electron cooling of the ion beams is one critical R&D to achieve high luminosities in JLab's MEIC proposal. In the present MEIC design, a multi-staged cooling scheme is adapted, which includes DC electron cooling in the booster ring and bunched beam electron cooling in the collider ring at both the injection energy and the collision energy. We explored the feasibility of using both magnetized and non-magnetized electron beam for cooling, and concluded that a magnetized electron beam is necessary. Electron cooling simulation results for the newly updated MEIC design is also presented.

  18. MASS PRODUCTION OF THE BENEFICIAL NEMATODE STEINERNEMA CARPOCAPSAE UTILIZING A FED-BATCH CULTURING PROCESS

    Directory of Open Access Journals (Sweden)

    Leonard D. Holmes

    2013-04-01

    Full Text Available The present study deals with the batch and fed-batch mass production of Steinernema carpocapsae. S. carpocapsae is an entomoparasitic nematode that is used as a biological control agent of soil-borne crop insect pests. The ability and efficiency of fed-batch culture process was successful through the utilization of the nematode’s bacterial symbiont Xenorhabdus nematophila. Results from the fed-batch process were compared to those obtain from the standard batch process. The fed-batch process successively improved the mass production process of S. carpocapsae employing liquid medium technology. Within the first week of the fed-batch process (day six, the nematode density obtained was 202,000 nematodes mL−1; whereas on day six, batch culture mode resulted in a nematode density of 23,000 nematodes mL−1. The fed-batch process was superior to that of batch production with a yield approximately 8.8-fold higher. In fed-batch process, the nematode yield was improved 88.6 % higher within a short amount of time compared to the batch process. Fed-batch seems to make the process more efficient and possibly economically viable.

  19. Control of crystal phase and morphology in hydrothermal synthesis of BiFeO3 crystal

    Science.gov (United States)

    Xu, Xuqing; Xu, Qianrui; Huang, Yajun; Hu, Xiuxiu; Huang, Yuqing; Wang, Gaoyu; Hu, Xiaolin; Zhuang, Naifeng

    2016-03-01

    Bismuth ferrite crystal is synthesized by hydrothermal method. The effect of hydrothermal temperature, KOH concentration, supersaturation, cooling rate, and compactedness on the crystal phase and the morphology of product were investigated. The results indicated that BiFeO3 microcrystalline with good quality could been synthesized at 140-240 °C with KOH concentration of 4-14 mol L-1. In addition, it is favorable for improving the crystal quality to reduce the supersaturation and decrease the cooling rate. With the increasing of the compactedness, surface holes and cracks of the as-grown crystals would be reduced. The optimization of hydrothermal condition provides guidance to grow BiFeO3 crystal with a large size and high quality for practical application.

  20. Formation of a crystallization courtyard in eutectic systems and crystal growth

    Science.gov (United States)

    Gurin, V. N.; Osipov, V. N.; Derkachenko, L. I.; Korchunov, B. N.; Popova, T. B.

    2014-03-01

    The so-called crystallization courtyard is investigated that forms in processes of mass crystallization around the Ge and Si crystals and their solid solutions (Ge+Si) during cooling of hypereutectic alloys in the Ge-Al, Si-Al, and (Ge+Si)-Al eutectic systems. For the first time, data on the composition and microhardness of this crystallization courtyard are given and its role is shown as a stopper of cracking in an Al-(Ge,Si) system during rapid cooling after the heating system is turned off. For the first time, it is suggested that a crystallization courtyard forms in all hypereutectic systems (including every system in which the amount of the taken solvent does not correspond to the eutectic point).

  1. Radiation effects on Yb:YLF crystals used in cryogenic optical refrigerators

    Science.gov (United States)

    Martin, K. W.; Melgaard, S.; Cowan, V. M.; Hubbs, J.; Fraser, T.; Sheik-Bahae, M.

    2015-09-01

    Optical cooling of solids is a promising and innovative method to provide cryogenic cooling to infrared sensors. Currently insulator crystals, specifically ytterbium-doped yttrium- lithium-fluoride (Yb:YLF), have shown the most promise for cooling to low temperatures. This method has demonstrated cooling below the National Institute of Standards and Technology (NIST) cryogenic temperature definition of less than 123 K. Optical refrigeration utilizes a phenomenon called anti-Stokes fluorescence to generate cooling power. Incident laser light is absorbed by the cooling crystal and photons are spontaneously emitted at a higher, and thus more energetic, frequency. The difference in frequency is proportional to the cooling power of the crystal. Anti-Stokes cooling is highly dependent on doping percentages and YLF crystal purity and structure. Space based infrared sensors and their coolers are operated in a radiation environment where protons, gamma, rays, heavy ions, and other radiation species are common and of varying severities depending on operational orbit. To ensure that radiative effects on cooling crystal performance are minimal, we irradiated two samples with 63 MeV protons to a total of ionized dose of 100 Krad (Si) and 1 Mrad (Si), and compared cooling crystal efficiency parameters before and after dosing.

  2. [Analysis of the transcriptional profiling of cell cycle regulatory networks of recombinant Chinese hamster ovary cells in batch and fed-batch cultures].

    Science.gov (United States)

    Liu, Xingmao; Ye, Lingling; Liu, Hong; Li, Shichong; Wang, Qiwei; Wu, Benchuan; Chen, Zhaolie

    2011-08-01

    In the light of Chinese hamster ovary (CHO) cell line 11G-S expressing human recombinant pro-urokinase, the differences of gene expression levels of the cells in different growth phases in both batch and fed-batch cultures were revealed by using gene chip technology. Then, based on the known cell cycle regulatory networks, the transcriptional profiling of the cell cycle regulatory networks of the cells in batch and fed-batch cultures was analyzed by using Genmapp software. Among the approximate 19 191 target genes in gene chip, the number of down-regulated genes was more than those of up-regulated genes of the cells in both batch and fed-batch cultures. The number of down-regulated genes of the cells in the recession phase in fed-batch culture was much more than that of the cells in batch culture. Comparative transcriptional analysis of the key cell cycle regulatory genes of the cells in both culture modes indicated that the cell proliferation and cell viability of the cells in both batch and fed-batch cultures were mainly regulated through down-regulating Cdk6, Cdk2, Cdc2a, Ccne1, Ccne2 genes of CDKs, Cyclin and CKI family and up-regulating Smad4 gene. PMID:22097809

  3. High performance batch production of LREBa2Cu3Oy using novel thin film Nd-123 seed

    International Nuclear Information System (INIS)

    A batch production for fabrication of LREBa2Cu3Oy (LRE: Sm, Gd, NEG) 'LRE-123' pellets are developed in air and Ar-1% O2 using a novel thin film Nd-123 seeds grown on MgO crystals. The SEM and XRD results conformed that the quality and orientation of the seed crystals are excellent. On the other hand, new seeds can withstand temperatures >1100 deg. C, as a result, the cold seeding process was applied even to grow Sm-123 material in Air. The trapped field observed in the best 45 mm single-grain puck of Gd-123 was in the range of 1.35 T and 0.35 T at 77.3 K and 87.3 K, respectively. The average trapped field at 77.3 K in the 24 mm diameter NEG-123 samples batch lies between 0.9 and 1 T. The maximum trapped field of 1.2 T was recorded at the sample surface. Further, the maximum trapped field of 0.23 T at 77 K was recorded in a sample with 16 mm diameter of Sm-123 with 3 mol% BaO2 addition. As a result we made more then 130 single grain pucks within a couple of months. Taking advantage of the single grain batch processed material, we constructed self-made chilled levitation disk, which was used on the open day of railway technical research Institute. More then 150 children stood on the levitation disk and revel the experience of levitation. The present results prove that a high-performance good-quality class of LREBa2Cu3Oy material can be made by using a novel thin film Nd-123 seeds.

  4. 间歇结晶过程的分析%Analyses of batch crystallization

    Institute of Scientific and Technical Information of China (English)

    林丹; 罗建军; 王胜春; 杨帆

    2001-01-01

    本文概要地介绍了用于研究在间歇悬浮结晶器中的结晶动力学和晶体粒度分布(CSD)的实验技术和数据分析的新进展,讨论了包括最大CSD的特征化、累积CSD方法、热响应技术、最大允许成长速率在内的几个简单而有用的方法.

  5. Crystal Data

    Science.gov (United States)

    SRD 3 NIST Crystal Data (PC database for purchase)   NIST Crystal Data contains chemical, physical, and crystallographic information useful to characterize more than 237,671 inorganic and organic crystalline materials. The data include the standard cell parameters, cell volume, space group number and symbol, calculated density, chemical formula, chemical name, and classification by chemical type.

  6. On the choice of batch mode in order to maximize throughput

    OpenAIRE

    Weeda, P.J.

    1990-01-01

    An analysis of serial process configurations consisting of three processes and two machines shows interesting relations between the choice of batch mode (or batch structure), utilization of capacities and maximum throughput.

  7. STOCHASTIC COOLING FOR BUNCHED BEAMS.

    Energy Technology Data Exchange (ETDEWEB)

    BLASKIEWICZ, M.

    2005-05-16

    Problems associated with bunched beam stochastic cooling are reviewed. A longitudinal stochastic cooling system for RHIC is under construction and has been partially commissioned. The state of the system and future plans are discussed.

  8. Thermal Stability of RP-2 for Hydrocarbon Boost Regenerative Cooling

    Science.gov (United States)

    Kleinhenz, Julie E.; Deans, Matthew C.; Stiegemeier, Benjamin R.; Psaras, Peter M.

    2013-01-01

    A series of tests were performed in the NASA Glenn Research Centers Heated Tube Facility to study the heat transfer and thermal stability behavior of RP-2 under conditions similar to those found in rocket engine cooling channels. It has long been known that hydrocarbon fuels, such as RP-2, can decompose at high temperature to form deposits (coke) which can adversely impact rocket engine cooling channel performance. The heated tube facility provides a simple means to study these effects. Using resistively heated copper tubes in a vacuum chamber, flowing RP-2 was heated to explore thermal effects at a range of test conditions. Wall temperature (850-1050F) and bulk fluid temperature (300-500F) were varied to define thermal decomposition and stability at each condition. Flow velocity and pressure were fixed at 75 fts and 1000 psia, respectively. Additionally, five different batches of RP-2 were tested at identical conditions to examine any thermal stability differences resulting from batch to batch compositional variation. Among these tests was one with a potential coke reducing additive known as 1,2,3,4-Tetrahydroquinoline (THQ). While copper tubes were used for the majority of tests, two exploratory tests were performed with a copper alloy known as GRCop-42. Each tube was instrumented with 15 thermocouples to examine the temperature profile, and carbon deposition at each thermocouple location was determined post-test in an oxidation furnace. In many tests, intermittent local temperature increases were observed visually and in the thermocouple data. These hot spots did not appear to correspond with a higher carbon deposition.

  9. Cooling pond temperature prediction

    International Nuclear Information System (INIS)

    A model is described which predicts temperature responses in the environment that are associated with the operation of a natural gas fueled thermoelectric power generation station. The model is a piecewise computer simulation, limited at present to closed cooling water systems. However, the techniques developed should be applicable to a much larger class of cooling system. The problem encountered consists of two parts: (1) data characterization and (2) modeling. An efficient characterization scheme for the environmental variables greatly simplifies the task of modeling. Methods borrowed from signal theory, but not yet applied to this field are applicable to and greatly simplify the digital computer investigation of environmental data. An optimal data set, from the point of view of information per unit cost, is described for the model

  10. Water Cooled Mirror Design

    Energy Technology Data Exchange (ETDEWEB)

    Dale, Gregory E. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Holloway, Michael Andrew [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Pulliam, Elias Noel [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2015-03-30

    This design is intended to replace the current mirror setup being used for the NorthStar Moly 99 project in order to monitor the target coupon. The existing setup has limited movement for camera alignment and is difficult to align properly. This proposed conceptual design for a water cooled mirror will allow for greater thermal transfer between the mirror and the water block. It will also improve positioning of the mirror by using flexible vacuum hosing and a ball head joint capable of a wide range of motion. Incorporating this design into the target monitoring system will provide more efficient cooling of the mirror which will improve the amount of diffraction caused by the heating of the mirror. The process of aligning the mirror for accurate position will be greatly improved by increasing the range of motion by offering six degrees of freedom.

  11. Magnetic entropy and cooling

    DEFF Research Database (Denmark)

    Hansen, Britt Rosendahl; Kuhn, Luise Theil; Bahl, Christian Robert Haffenden

    2010-01-01

    Some manifestations of magnetism are well-known and utilized on an everyday basis, e.g. using a refrigerator magnet for hanging that important note on the refrigerator door. Others are, so far, more exotic, such as cooling by making use of the magnetocaloric eect. This eect can cause a change in...... the temperature of a magnetic material when a magnetic eld is applied or removed. For many years, experimentalists have made use of dilute paramagnetic materials to achieve milliKelvin temperatures by use of the magnetocaloric eect. Also, research is done on materials, which might be used for hydrogen......, helium or nitrogen liquefaction or for room-temperature cooling. The magnetocaloric eect can further be used to determine phase transition boundaries, if a change in the magnetic state occurs at the boundary.In this talk, I will introduce the magnetocaloric eect (MCE) and the two equations, which...

  12. Synthesis and characterization of tetraethylammonium tetrachlorocobaltate crystals

    Indian Academy of Sciences (India)

    M A Kandhaswamy; V Srinivasan

    2002-02-01

    Single crystals of tetraethylammonium tetrachlorocobaltate were grown by solution method and characterized through single crystal X-ray diffraction, thermogravimetric analysis (TGA), differential scanning calorimetric studies (DSC) and infrared spectroscopic technique (IR). The crystals were bright, transparent and blue coloured. The unit cell parameters were found to be = = 9.0363 Å and = 14.9879 Å and = = = 90°, showing tetragonal lattice from the XRD data. Thermogravimetric analysis showed a loss of weight at 683 K from which the decomposition reaction was formulated. Thermal anomalies were found for this crystal at temperatures 200 K, 220 K in the cooling cycle and at temperatures 200 K, 240 K in the heating cycle, respectively which showed that this crystal was associated with first order phase transition. All the vibrational frequencies corresponding to (TEA)+ ions and CoCl$^{2-}_4$ ions were assigned from the IR spectral data of this crystal.

  13. Cool Stars in Hot Places

    OpenAIRE

    Megeath, S. T.; Gaidos, E.; Hester, J. J.; Adams, F. C.; Bally, J.; Lee, J. -E.; Wolk, S.

    2007-01-01

    During the last three decades, evidence has mounted that star and planet formation is not an isolated process, but is influenced by current and previous generations of stars. Although cool stars form in a range of environments, from isolated globules to rich embedded clusters, the influences of other stars on cool star and planet formation may be most significant in embedded clusters, where hundreds to thousands of cool stars form in close proximity to OB stars. At the cool stars 14 meeting, ...

  14. New materials for cooling systems

    International Nuclear Information System (INIS)

    New materials based on rubber-vulcanite compounds and used for manufacturing cooling tower elements and coating's of hydraulic structure surfaces are proposed and their production technology is described. A series of studies on physicomechanical and chemical characteristics and hydroaerothermal parameters of cooling tower elements and coatings revealed an obvious advantage of these materials over existing ones. The materials proposed provide high efficiency of cooling tower elements, hydraulic structures and the cooling tower as a whole

  15. Sorting Olive Batches for the Milling Process Using Image Processing

    Directory of Open Access Journals (Sweden)

    Daniel Aguilera Puerto

    2015-07-01

    Full Text Available The quality of virgin olive oil obtained in the milling process is directly bound to the characteristics of the olives. Hence, the correct classification of the different incoming olive batches is crucial to reach the maximum quality of the oil. The aim of this work is to provide an automatic inspection system, based on computer vision, and to classify automatically different batches of olives entering the milling process. The classification is based on the differentiation between ground and tree olives. For this purpose, three different species have been studied (Picudo, Picual and Hojiblanco. The samples have been obtained by picking the olives directly from the tree or from the ground. The feature vector of the samples has been obtained on the basis of the olive image histograms. Moreover, different image preprocessing has been employed, and two classification techniques have been used: these are discriminant analysis and neural networks. The proposed methodology has been validated successfully, obtaining good classification results.

  16. Empirical State Error Covariance Matrix for Batch Estimation

    Science.gov (United States)

    Frisbee, Joe

    2015-01-01

    State estimation techniques effectively provide mean state estimates. However, the theoretical state error covariance matrices provided as part of these techniques often suffer from a lack of confidence in their ability to describe the uncertainty in the estimated states. By a reinterpretation of the equations involved in the weighted batch least squares algorithm, it is possible to directly arrive at an empirical state error covariance matrix. The proposed empirical state error covariance matrix will contain the effect of all error sources, known or not. This empirical error covariance matrix may be calculated as a side computation for each unique batch solution. Results based on the proposed technique will be presented for a simple, two observer and measurement error only problem.

  17. Plutonium immobilization ceramic feed batching component test report

    International Nuclear Information System (INIS)

    The Plutonium Immobilization Facility will encapsulate plutonium in ceramic pucks and seal the pucks inside welded cans. Remote equipment will place these cans in magazines and the magazines in a Defense Waste Processing Facility (DWPF) canister. The DWPF will fill the canister with high level waste glass for permanent storage. Ceramic feed batching (CFB) is one of the first process steps involved with first stage plutonium immobilization. The CFB step will blend plutonium oxide powder before it is combined with other materials to make pucks. This report discusses the Plutonium Immobilization CFB process preliminary concept (including a process block diagram), batch splitting component test results, CFB development areas, and FY 1999 and 2000 CFB program milestones

  18. APPLICATION OF MODEL PREDICTIVE CONTROL TO BATCH POLYMERIZATION REACTOR

    Directory of Open Access Journals (Sweden)

    N.M. Ghasem

    2006-06-01

    Full Text Available The absence of a stable operational state in polymerization reactors that operates in batches is factor that determine the need of a special control system. In this study, advanced control methodology is implemented for controlling the operation of a batch polymerization reactor for polystyrene production utilizingmodel predictive control. By utilizing a model of the polymerization process, the necessary operational conditions were determined for producing the polymer within the desired characteristics. The maincontrol objective is to bring the reactor temperature to its target temperature as rapidly as possible with minimal temperature overshoot. Control performance for the proposed method is encouraging. It has been observed that temperature overshoot can be minimized by the proposed method with the use of both reactor and jacket energy balance for reactor temperature control.

  19. JAVA Implementation of the Batched iLab Shared Architecture

    Directory of Open Access Journals (Sweden)

    Lenard Payne

    2013-04-01

    Full Text Available The MIT iLab Shared Architecture is limited currently to running on the Microsoft Windows platform. A JAVA implementation of the Batched iLab Shared Architecture has been developed that can be used on other operating systems and still interoperate with the existing Microsoft .NET web services of MIT’s iLab ServiceBroker. The Batched iLab Shared Architecture has been revised and separates the Labserver into a LabServer that handles experiment management and a LabEquipment that handles experiment execution. The JAVA implementation provides a 3-tier code development model that allows code to be reused and to develop only the code that is specific to each experiment.

  20. Conduction cooled tube supports

    Science.gov (United States)

    Worley, Arthur C.; Becht, IV, Charles

    1984-01-01

    In boilers, process tubes are suspended by means of support studs that are in thermal contact with and attached to the metal roof casing of the boiler and the upper bend portions of the process tubes. The support studs are sufficiently short that when the boiler is in use, the support studs are cooled by conduction of heat to the process tubes and the roof casing thereby maintaining the temperature of the stud so that it does not exceed 1400.degree. F.

  1. On-line Scheduling Algorithm for Penicillin Fed-batch Fermentation

    Institute of Scientific and Technical Information of China (English)

    XUE Yao-feng; YUAN Jing-qi

    2005-01-01

    An on-line scheduling algorithm to maximize gross profit of penicillin fed-batch fermentation is proposed. According to the on-line classification method, fed-batch fermentation batches are classified into three categories. Using the scheduling strategy, the optimal termination sequence of batches is obtained. Pseudo on-line simulations for testing the proposed algorithm with the data from industrial scale penicillin fermentation are carried out.

  2. Health advantages of transition to batch management system in farrow-to-finish pig herds

    OpenAIRE

    Vangroenweghe, F; Suls, L; Van Driessche, E.; Maes, Dominiek; De Graef, E.

    2012-01-01

    Sow batch management systems have become more popular due to advantages in labour planning, piglet batch sizes, all-in all-out practices and health management. The present study investigated the potential health advantages of 10 selected farrow-to-finish pig herds before and after transition from a one week batch management system to a four or five week batch management system. Five different animal categories (gilts, sows, piglets, growers and finishers) were sampled at three time points (T0...

  3. vFlow: A GUI-Based Tool for Building Batch Applications for Cloud Computing

    OpenAIRE

    Gobjuka, Hassan; Ahmat, Kamal

    2011-01-01

    In this paper we introduce vFlow - A framework for rapid designing of batch processing applications for Cloud Computing environment. vFlow batch processing system extracts tasks from the vPlans diagrams, systematically captures the dynamics in batch application management tasks, and translates them to Cloud environment API, named vDocuments, that can be used to execute batch processing applications. vDocuments do not only enable the complete execution of low-level configuration management tas...

  4. Low mass integrated cooling

    CERN Document Server

    Mapelli, Alessandro

    2014-01-01

    Low mass on - detec tor cooling systems are being developed and stud ied by the Detector Technology group (PH - DT) in the CERN Physics Department in close collaboration with LHC and non - LHC experiments . Two approaches are currently being investigated. The first approach, for barrel configurations, consists in integrating the cooli ng apparatus in light mechanical structures support ing the detectors. In this case , the thermal management can be achieved either with light cooling pipes and thin plates or with a network of microchannels embedded in thin strips of silicon or polyimide . Both configuratio ns are being investigated in the context of the 2018 upgrade program of the ALICE Inner Tracking System (ITS). Moreover, it is also possible to use a s ilicon microchannel cooling device itself as structural support for the detectors and electronics. Such a configur ation has been adopted by the NA62 collaboration for the ir GigaTracKer (GTK) as well as by the LHCb collaboration for the 2018 major upgrade of...

  5. Project S'COOL

    Science.gov (United States)

    Green, Carolyn J.; Chambers, Lin H.

    1998-01-01

    The Students Clouds Observations On-Line or S'COOL project was piloted in 1997. It was created with the idea of using students to serve as one component of the validation for the Clouds and the Earth's Radiant Energy System (CERES) instrument which was launched with the Tropical Rainfall Measuring Mission (TRMM) in November, 1997. As part of NASA's Earth Science Enterprise CERES is interested in the role clouds play in regulating our climate. Over thirty schools became involved in the initial thrust of the project. The CERES instrument detects the location of clouds and identifies their physical properties. S'COOL students coordinate their ground truth observations with the exact overpass of the satellite at their location. Their findings regarding cloud type, height, fraction and opacity as well as surface conditions are then reported to the NASA Langley Distributed Active Archive Center (DAAC). The data is then accessible to both the CERES team for validation and to schools for educational application via the Internet. By March of 1998 ninety-three schools, in nine countries had enrolled in the S'COOL project. Joining the United States participants were from schools in Australia, Canada, France, Germany, Norway, Spain, Sweden, and Switzerland. The project is gradually becoming the global project envisioned by the project s creators. As students obtain the requested data useful for the scientists, it was hoped that students with guidance from their instructors would have opportunity and motivation to learn more about clouds and atmospheric science as well.

  6. Electron Cooling of RHIC

    CERN Document Server

    Ben-Zvi, Ilan; Barton, Donald; Beavis, Dana; Blaskiewicz, Michael; Bluem, Hans; Brennan, Joseph M; Bruhwiler, David L; Burger, Al; Burov, Alexey; Burrill, Andrew; Calaga, Rama; Cameron, Peter; Chang, Xiangyun; Cole, Michael; Connolly, Roger; Delayen, Jean R; Derbenev, Yaroslav S; Eidelman, Yury I; Favale, Anthony; Fedotov, Alexei V; Fischer, Wolfram; Funk, L W; Gassner, David M; Hahn, Harald; Harrison, Michael; Hershcovitch, Ady; Holmes, Douglas; Hseuh Hsiao Chaun; Johnson, Peter; Kayran, Dmitry; Kewisch, Jorg; Kneisel, Peter; Koop, Ivan; Lambiase, Robert; Litvinenko, Vladimir N; MacKay, William W; Mahler, George; Malitsky, Nikolay; McIntyre, Gary; Meng, Wuzheng; Merminga, Lia; Meshkov, Igor; Mirabella, Kerry; Montag, Christoph; Nagaitsev, Sergei; Nehring, Thomas; Nicoletti, Tony; Oerter, Brian; Parkhomchuk, Vasily; Parzen, George; Pate, David; Phillips, Larry; Preble, Joseph P; Rank, Jim; Rao, Triveni; Rathke, John; Roser, Thomas; Russo, Thomas; Scaduto, Joseph; Schultheiss, Tom; Sekutowicz, Jacek; Shatunov, Yuri; Sidorin, Anatoly O; Skrinsky, Aleksander Nikolayevich; Smirnov, Alexander V; Smith, Kevin T; Todd, Alan M M; Trbojevic, Dejan; Troubnikov, Grigory; Wang, Gang; Wei, Jie; Williams, Neville; Wu, Kuo-Chen; Yakimenko, Vitaly; Zaltsman, Alex; Zhao, Yongxiang; ain, Animesh K

    2005-01-01

    We report progress on the R&D program for electron-cooling of the Relativistic Heavy Ion Collider (RHIC). This electron cooler is designed to cool 100 GeV/nucleon at storage energy using 54 MeV electrons. The electron source will be a superconducting RF photocathode gun. The accelerator will be a superconducting energy recovery linac. The frequency of the accelerator is set at 703.75 MHz. The maximum electron bunch frequency is 9.38 MHz, with bunch charge of 20 nC. The R&D program has the following components: The photoinjector and its photocathode, the superconducting linac cavity, start-to-end beam dynamics with magnetized electrons, electron cooling calculations including benchmarking experiments and development of a large superconducting solenoid. The photoinjector and linac cavity are being incorporated into an energy recovery linac aimed at demonstrating ampere class current at about 20 MeV. A Zeroth Order Design Report is in an advanced draft state, and can be found on the web at http://www.ags...

  7. Batch gating for data association in monocular SLAM

    OpenAIRE

    Guerra Paradas, Edmundo; Munguía Alcalá, Rodrigo Francisco; Bolea Monte, Yolanda; Grau Saldes, Antoni

    2013-01-01

    This work describes the development and implementation of a single-camera SLAM system, introducing a novel data validation algorithm. A 6-DOF monocular SLAM method developed is based on the Delayed Inverse-Depth (DI-D) Feature Initialization, with the addition of a new data association batch validation technique, the Highest Order Hypothesis Compatibility Test, HOHCT. The DI-D initializes new features in the system defining single hypothesis for the initial depth of features by stoch...

  8. Feasibility of extractive distillation process variants in batch rectifier column

    OpenAIRE

    Stéger, Csaba; Varga, Viktoria; Horvath, Laszlo; Rev, Endre; Fonyo, Zsolt; Meyer, Michel; Lelkes, Zoltan

    2005-01-01

    A systematic comparison is presented about the separation tasks of azeotropic and close-boiling mixtures applying batch extractive distillation (BED) in rectifier. All the eight possible mixture types with at most a single azeotrope (minimum and maximum boiling azeotropes with heavy, light, and intermediate boiling entrainers; and close boiling mixtures with heavy and light entrainers) are compared. The main results of the feasibility studies on the hitherto unpublished cases are presented. A...

  9. Optimization of Recipe Based Batch Control Systems Using Neural Networks

    OpenAIRE

    Šoštarec, A.; Gosak, D.; Hlupić, N.

    2012-01-01

    In the modern pharmaceutical industry many flexible batch plants operate under an integrated business and production system, using ISA S95 and ISA S88 standards for models and terminology, and implementing flexible recipe-based production. In the environment of constantly changing market conditions, adjustment to surroundings is a business necessity. To support necessary production improvement, regulatory authorities have introduced the risk based approach for the control of process dev...

  10. Mathematical modeling of recombinant Escherichia coli aerobic batch fermentations

    OpenAIRE

    Costa, Rafael S; Rocha, I; Ferreira, E. C.

    2008-01-01

    In this work, three competing unstructured mathematical models for the biomass growth by recombinant E. coli strains with different acetate inhibition kinetics terms were evaluated for batch processes at constant temperature and pH. The models considered the dynamics of biomass growth, acetate accumulation, substrate consumption, Green Fluorescence Protein (GFP) production and three metabolic pathways for E. coli. Parameter estimation and model validation was carried out usi...

  11. Integration of virtualized worker nodes in standard batch systems

    International Nuclear Information System (INIS)

    Current experiments in HEP only use a limited number of operating system flavours. Their software might only be validated on one single OS platform. Resource providers might have other operating systems of choice for the installation of the batch infrastructure. This is especially the case if a cluster is shared with other communities, or communities that have stricter security requirements. One solution would be to statically divide the cluster into separated sub-clusters. In such a scenario, no opportunistic distribution of the load can be achieved, resulting in a poor overall utilization efficiency. Another approach is to make the batch system aware of virtualization, and to provide each community with its favoured operating system in a virtual machine. Here, the scheduler has full flexibility, resulting in a better overall efficiency of the resources. In our contribution, we present a lightweight concept for the integration of virtual worker nodes into standard batch systems. The virtual machines are started on the worker nodes just before jobs are executed there. No meta-scheduling is introduced. We demonstrate two prototype implementations, one based on the Sun Grid Engine (SGE), the other using Maui/Torque as a batch system. Both solutions support local job as well as Grid job submission. The hypervisors currently used are Xen and KVM, a port to another system is easily envisageable. To better handle different virtual machines on the physical host, the management solution VmImageManager is developed. We will present first experience from running the two prototype implementations. In a last part, we will show the potential future use of this lightweight concept when integrated into high-level (i.e. Grid) work-flows.

  12. Voronoi model learning for batch mode reinforcement learning

    OpenAIRE

    Fonteneau, Raphaël; Ernst, Damien

    2010-01-01

    We consider deterministic optimal control problems with continuous state spaces where the information on the system dynamics and the reward function is constrained to a set of system transitions. Each system transition gathers a state, the action taken while being in this state, the immediate reward observed and the next state reached. In such a context, we propose a new model learning--type reinforcement learning (RL) algorithm in batch mode, finite-time and deterministic setting. The algori...

  13. Industrial and Municipal Wastewater Treatment in the Sequencing Batch Reactor

    OpenAIRE

    Vrtovsek, J.; Ros, M.

    2008-01-01

    A mixture of Industrial wastewater from chemical industry (varnish, paint and pigments production) and municipal wastewater was treated in pilot sequencing batch reactor (SBR). Results of the pilot experiments show that the foaming problem has great influence on the behavior of SBR, especially when the ratio between industrial and municipal wastewater is very high. Foaming problem was negligible when the mixture with φ; 20 % of the industrial wastewater and j = 80 % of the municipal wastewate...

  14. SEQUENCING BATCH REACTOR: A PROMISING TECHNOLOGY IN WASTEWATER TREATMENT

    OpenAIRE

    A.H Mahvi

    2008-01-01

    Discharge of domestic and industrial wastewater to surface or groundwater is very dangerous to the environment. Therefore treatment of any kind of wastewater to produce effluent with good quality is necessary. In this regard choosing an effective treatment system is important. Sequencing batch reactor is a modification of activated sludge process which has been successfully used to treat municipal and industrial wastewater. The process could be applied for nutrients removal, high biochemical ...

  15. EFFECT OF DYE CONCENTRATION ON SEQUENCING BATCH REACTOR PERFORMANCE

    OpenAIRE

    A. A. Vaigan ، M. R. Alavi Moghaddam ، H. Hashemi

    2009-01-01

    Reactive dyes have been identified as problematic compounds in textile industries wastewater as they are water soluble and cannot be easily removed by conventional aerobic biological treatment systems. The treatability of a reactive dye (Brill Blue KN-R) by sequencing batch reactor and the influence of the dye concentration on system performance were investigated in this study. Brill Blue KN-R is one of the main dyes that are used in textile industries in Iran. Four cylindrical Plexiglas reac...

  16. Transition to four batch loading scheme in Loviisa NPP

    International Nuclear Information System (INIS)

    The WWER-440 reactors of Loviisa NPP are operated with 1500 MWth power and reduced core. During recent years a 3-batch loading scheme has been used. Loviisa-1 is currently running with BNFL fuel equilibrium cycle and Loviisa-2 with TVEL fuel equilibrium cycle. Our goal is to move to a 4-batch scheme with TVEL fuel for both reactors. To achieve this goal the U-235 enrichment has to be increased from the current designs used. The fuel to be used in the near future is 4.37 % enriched fuel with six Gd2O3 doped rods. The characteristics and consequences of the core consisting of Gd-fuel are discussed based on our target equilibrium loading pattern. With the 4-batch loading scheme the discharge burnups exceed the current assembly burnup limit with a clear margin. Thus, we also have to prepare an application for the safety authority to increase the assembly average burnup limit from the current 45 MWd/kgU to about 56 MWd/kgU. First Gd-fuel assemblies are loaded into Loviisa-1 core in September 2009 and into Loviisa-2 core in October 2010. The reload batch of Loviisa-1 in 2009 consists of 60 Gd-assemblies and 24 non-Gd-assemblies plus 12 followers. In this paper some results are presented from Loviisa-1 zero power startup experiments and the first days of power operation. Among other aspects the six Gd2O3 doped pins used in the assembly have an effect on the pin power profile of the assembly during the first half of the cycle. The influence of the changing pin power profile on the outlet temperature measurements is briefly discussed based on expected effect and measurement (Authors)

  17. Biological Treatment of Dairy Wastewater by Sequencing Batch Reactor

    OpenAIRE

    A Mohseni-Bandpi, H Bazari

    2004-01-01

    A bench scale aerobic Sequencing Batch Reactor (SBR) was investigated to treat the wastewater from an industrial milk factory. The reactor was constructed from plexi glass material and its volume was 22.5 L. The reactor was supplied with oxygen by fine bubble air diffuser. The reactor was fed with milk factory and synthetic wastewater under different operational conditions. The COD removal efficiency was achieved more than 90%, whereas COD concentration varied from 400 to 2500 mg/l. The optim...

  18. Optimal parametric sensitivity control for a fed-batch reactor

    OpenAIRE

    Stigter, J.D.; Keesman, K. J.

    2001-01-01

    The paper presents a method to derive an optimal parametric sensitivity controller for optimal estimation of a set of parameters in an experiment. The method is demonstrated for a fed batch bio-reactor case study for optimal estimation of the saturation constant Ks and, albeit intuitively, the parameter combination "mu-max X/Y" where mu-max is the maximum growth rate [g/min], Y is the yield coefficient [g/g], and X is the (constant) biomass [g].

  19. Conduction cooling: multicrate fastbus hardware

    International Nuclear Information System (INIS)

    Described is a new and novel approach for cooling nuclear instrumentation modules via heat conduction. The simplicity of liquid cooled crates and ease of thermal management with conduction cooled modules are described. While this system was developed primarily for the higher power levels expected with Fastbus electronics, it has many general applications

  20. SLUDGE BATCH 4 SIMULANT FLOWSHEET STUDIES: PHASE II RESULTS

    Energy Technology Data Exchange (ETDEWEB)

    Stone, M; David Best, D

    2006-09-12

    The Defense Waste Processing Facility (DWPF) will transition from Sludge Batch 3 (SB3) processing to Sludge Batch 4 (SB4) processing in early fiscal year 2007. Tests were conducted using non-radioactive simulants of the expected SB4 composition to determine the impact of varying the acid stoichiometry during the Sludge Receipt and Adjustment Tank (SRAT) process. The work was conducted to meet the Technical Task Request (TTR) HLW/DWPF/TTR-2004-0031 and followed the guidelines of a Task Technical and Quality Assurance Plan (TT&QAP). The flowsheet studies are performed to evaluate the potential chemical processing issues, hydrogen generation rates, and process slurry rheological properties as a function of acid stoichiometry. Initial SB4 flowsheet studies were conducted to guide decisions during the sludge batch preparation process. These studies were conducted with the estimated SB4 composition at the time of the study. The composition has changed slightly since these studies were completed due to changes in the sludges blended to prepare SB4 and the estimated SB3 heel mass. The following TTR requirements were addressed in this testing: (1) Hydrogen and nitrous oxide generation rates as a function of acid stoichiometry; (2) Acid quantities and processing times required for mercury removal; (3) Acid quantities and processing times required for nitrite destruction; and (4) Impact of SB4 composition (in particular, oxalate, manganese, nickel, mercury, and aluminum) on DWPF processing (i.e. acid addition strategy, foaming, hydrogen generation, REDOX control, rheology, etc.).

  1. Analyzing data flows of WLCG jobs at batch job level

    Science.gov (United States)

    Kuehn, Eileen; Fischer, Max; Giffels, Manuel; Jung, Christopher; Petzold, Andreas

    2015-05-01

    With the introduction of federated data access to the workflows of WLCG, it is becoming increasingly important for data centers to understand specific data flows regarding storage element accesses, firewall configurations, as well as the scheduling of batch jobs themselves. As existing batch system monitoring and related system monitoring tools do not support measurements at batch job level, a new tool has been developed and put into operation at the GridKa Tier 1 center for monitoring continuous data streams and characteristics of WLCG jobs and pilots. Long term measurements and data collection are in progress. These measurements already have been proven to be useful analyzing misbehaviors and various issues. Therefore we aim for an automated, realtime approach for anomaly detection. As a requirement, prototypes for standard workflows have to be examined. Based on measurements of several months, different features of HEP jobs are evaluated regarding their effectiveness for data mining approaches to identify these common workflows. The paper will introduce the actual measurement approach and statistics as well as the general concept and first results classifying different HEP job workflows derived from the measurements at GridKa.

  2. Fault Diagnosis of Batch Reactor Using Machine Learning Methods

    Directory of Open Access Journals (Sweden)

    Sujatha Subramanian

    2014-01-01

    Full Text Available Fault diagnosis of a batch reactor gives the early detection of fault and minimizes the risk of thermal runaway. It provides superior performance and helps to improve safety and consistency. It has become more vital in this technical era. In this paper, support vector machine (SVM is used to estimate the heat release (Qr of the batch reactor both normal and faulty conditions. The signature of the residual, which is obtained from the difference between nominal and estimated faulty Qr values, characterizes the different natures of faults occurring in the batch reactor. Appropriate statistical and geometric features are extracted from the residual signature and the total numbers of features are reduced using SVM attribute selection filter and principle component analysis (PCA techniques. artificial neural network (ANN classifiers like multilayer perceptron (MLP, radial basis function (RBF, and Bayes net are used to classify the different types of faults from the reduced features. It is observed from the result of the comparative study that the proposed method for fault diagnosis with limited number of features extracted from only one estimated parameter (Qr shows that it is more efficient and fast for diagnosing the typical faults.

  3. Spectrophotometric determination of fluoxetine by batch and flow injection methods.

    Science.gov (United States)

    Afkhami, Abbas; Madrakian, Tayyebeh; Khalafi, Lida

    2006-12-01

    A rapid, simple, and accurate spectrophotometric method is presented for the determination of fluoxetine by batch and flow injection analysis methods. The method is based on fluoxetine competitive complexation reaction with phenolphthalein-beta-cyclodextrin (PHP-beta-CD) inclusion complex. The increase in the absorbance of the solution at 554 nm by the addition of fluoxetine was measured. The formation constant for fluoxetin-beta-CD was calculated by non-linear least squares fitting. Fluoxetine can be determined in the range 7.0 x 10(-6)-2.4 x 10(-4) mol l(-1) and 5.0 x 10(-5)-1.0 x 10(-2) mol l(-1) by batch and flow methods, respectively. The limit of detection and limit of quantification were respectively 4.13 x 10(-6) mol l(-1) and 1.38 x 10(-5) mol l(-1) for batch and 2.46 x 10(-5) mol l(-1) and 8.22 x 10(-5) mol l(-1) for flow method. The sampling rate in flow injection analysis method was 80+/-5 samples h(-1). The method was applied to the determination of fluoxetine in pharmaceutical formulations and after addition to human urine samples. PMID:17139097

  4. Non-isothermal Crystallization Kinetics of Kaolin Modified Polyester

    Institute of Scientific and Technical Information of China (English)

    ZHANG Ruixin; GU Mingbo; CHEN Guoqiang

    2011-01-01

    Fiber-class modified kaolin and PET have been blended in the twin-screw and granulated to chips containing 4 wt% of kaolin.Non-isothermal crystallization process of kaolin modified polyester was investigated using a differential scanning calorimetry (DSC),and the addition of kaolin enhances either the melting temperature (Tm) or the crystallization temperature (Tc).The morphology of kaolin modified polyester,the melt of which is cooled at different cooling rate,was observed by scanning electron microscope (SEM).The relationship between Tc and cooling rate F was studied.Semi-crystalline phase t1/2 makes an exponential decline with increasing F,and the higher the cooling rate,the shorter the time of crystallization completion.Non-isothermal crystallization kinetics parameters and the activation energy were calculated,indicating that the higher rate of cooling needs the higher relative crystallinity in the unit crystallization time,the crystallization rate increased while speeding up the temperature reduction,and the activation energy AE was calculated to be -204.1566 kJ/mol for the non-isothermal crystallization processes by the Kissinger's methods.

  5. 40 CFR 1065.546 - Validation of minimum dilution ratio for PM batch sampling.

    Science.gov (United States)

    2010-07-01

    ... for PM batch sampling. 1065.546 Section 1065.546 Protection of Environment ENVIRONMENTAL PROTECTION... Specified Duty Cycles § 1065.546 Validation of minimum dilution ratio for PM batch sampling. Use continuous... dilution ratios for PM batch sampling as specified in § 1065.140(e)(2) over the test interval. You may...

  6. 40 CFR Table 2 to Subpart Vvvvvv... - Emission Limits and Compliance Requirements for Batch Process Vents

    Science.gov (United States)

    2010-07-01

    ... Requirements for Batch Process Vents 2 Table 2 to Subpart VVVVVV of Part 63 Protection of Environment... of Part 63—Emission Limits and Compliance Requirements for Batch Process Vents As required in § 63.11496, you must comply with the requirements for batch process vents as shown in the following...

  7. 21 CFR 226.102 - Master-formula and batch-production records.

    Science.gov (United States)

    2010-04-01

    ... 21 Food and Drugs 4 2010-04-01 2010-04-01 false Master-formula and batch-production records. 226... Records and Reports § 226.102 Master-formula and batch-production records. (a) For each Type A medicated... batch size, or of appropriate size in the case of continuous systems to be produced from the...

  8. 40 CFR 63.1036 - Alternative means of emission limitation: Batch processes.

    Science.gov (United States)

    2010-07-01

    ... limitation: Batch processes. 63.1036 Section 63.1036 Protection of Environment ENVIRONMENTAL PROTECTION... § 63.1036 Alternative means of emission limitation: Batch processes. (a) General requirement. As an... operator of a batch process that operates in regulated material service during the calendar year may...

  9. 40 CFR 65.117 - Alternative means of emission limitation: Batch processes.

    Science.gov (United States)

    2010-07-01

    ... limitation: Batch processes. 65.117 Section 65.117 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY... of emission limitation: Batch processes. (a) General requirement. As an alternative to complying with the requirements of §§ 65.106 through 65.114 and § 65.116, an owner or operator of a batch...

  10. 40 CFR 63.178 - Alternative means of emission limitation: Batch processes.

    Science.gov (United States)

    2010-07-01

    ... limitation: Batch processes. 63.178 Section 63.178 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY... Alternative means of emission limitation: Batch processes. (a) As an alternative to complying with the requirements of §§ 63.163 through 63.171 and §§ 63.173 through 63.176, an owner or operator of a batch...

  11. 40 CFR 1065.545 - Validation of proportional flow control for batch sampling.

    Science.gov (United States)

    2010-07-01

    ... control for batch sampling. 1065.545 Section 1065.545 Protection of Environment ENVIRONMENTAL PROTECTION... Specified Duty Cycles § 1065.545 Validation of proportional flow control for batch sampling. For any proportional batch sample such as a bag or PM filter, demonstrate that proportional sampling was...

  12. 40 CFR 63.487 - Batch front-end process vents-reference control technology.

    Science.gov (United States)

    2010-07-01

    ... § 63.487 Batch front-end process vents—reference control technology. (a) Batch front-end process vents... process vent, reduce organic HAP emissions for the batch cycle by 90 weight percent using a control device... control device as it relates to continuous front-end process vents shall be used. Furthermore,...

  13. 40 CFR 63.1407 - Non-reactor batch process vent provisions.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 11 2010-07-01 2010-07-01 true Non-reactor batch process vent... § 63.1407 Non-reactor batch process vent provisions. (a) Emission standards. (1) Owners or operators of non-reactor batch process vents located at new or existing affected sources with 0.25 tons per year...

  14. 40 CFR 63.491 - Batch front-end process vents-recordkeeping requirements.

    Science.gov (United States)

    2010-07-01

    ... reactor for that recipe. (2) A description of, and an emission estimate for, each batch emission episode... 40 Protection of Environment 9 2010-07-01 2010-07-01 false Batch front-end process vents... § 63.491 Batch front-end process vents—recordkeeping requirements. (a) Group determination records...

  15. OSAT: a tool for sample-to-batch allocations in genomics experiments

    Directory of Open Access Journals (Sweden)

    Yan Li

    2012-12-01

    Full Text Available Abstract Background Batch effect is one type of variability that is not of primary interest but ubiquitous in sizable genomic experiments. To minimize the impact of batch effects, an ideal experiment design should ensure the even distribution of biological groups and confounding factors across batches. However, due to the practical complications, the availability of the final collection of samples in genomics study might be unbalanced and incomplete, which, without appropriate attention in sample-to-batch allocation, could lead to drastic batch effects. Therefore, it is necessary to develop effective and handy tool to assign collected samples across batches in an appropriate way in order to minimize the impact of batch effects. Results We describe OSAT (Optimal Sample Assignment Tool, a bioconductor package designed for automated sample-to-batch allocations in genomics experiments. Conclusions OSAT is developed to facilitate the allocation of collected samples to different batches in genomics study. Through optimizing the even distribution of samples in groups of biological interest into different batches, it can reduce the confounding or correlation between batches and the biological variables of interest. It can also optimize the homogeneous distribution of confounding factors across batches. It can handle challenging instances where incomplete and unbalanced sample collections are involved as well as ideally balanced designs.

  16. Cooling lubricants; Kuehlschmierstoffe

    Energy Technology Data Exchange (ETDEWEB)

    Pfeiffer, W. [Berufsgenossenschaftliches Inst. fuer Arbeitssicherheit, St. Augustin (Germany); Breuer, D. [Berufsgenossenschaftliches Inst. fuer Arbeitssicherheit, St. Augustin (Germany); Blome, H. [Berufsgenossenschaftliches Inst. fuer Arbeitssicherheit, St. Augustin (Germany); Deininger, C. [Berufsgenossenschaftliches Inst. fuer Arbeitssicherheit, St. Augustin (Germany); Hahn, J.U. [Berufsgenossenschaftliches Inst. fuer Arbeitssicherheit, St. Augustin (Germany); Kleine, H. [Berufsgenossenschaftliches Inst. fuer Arbeitssicherheit, St. Augustin (Germany); Nies, E. [Berufsgenossenschaftliches Inst. fuer Arbeitssicherheit, St. Augustin (Germany); Pflaumbaum, W. [Berufsgenossenschaftliches Inst. fuer Arbeitssicherheit, St. Augustin (Germany); Stockmann, R. [Berufsgenossenschaftliches Inst. fuer Arbeitssicherheit, St. Augustin (Germany); Willert, G. [Berufsgenossenschaftliches Inst. fuer Arbeitssicherheit, St. Augustin (Germany); Sonnenschein, G. [Maschinenbau- und Metall-Berufsgenossenschaft, Duesseldorf (Germany)

    1996-08-01

    As a rule, the base substances used are certain liquid hydrocarbons from mineral oils as well as from native and synthetic oils. Through the addition of further substances the cooling lubricant takes on the particular qualities required for the use in question. Employees working with cooling lubricants are exposed to various hazards. The assessment of the concentrations at the work station is carried out on the basis of existing technical rules for contact with hazardous substances. However, the application/implementation of compulsory investigation and supervision in accordance with these rules is made difficult by the fact that cooling lubricants are, as a rule, made up of complicated compound mixtures. In addition to protecting employees from exposure to mists and vapours from the cooling lubricants, protection for the skin is also of particular importance. Cooling lubricants should not, if at all possible, be brought into contact with the skin. Cleansing the skin and skin care is just as important as changing working clothes regularly, and hygiene and cleanliness at the workplace. Unavoidable emissions are to be immediately collected at the point where they arise or are released and safely disposed of. This means taking into account all sources of emissions. The programme presented in this report therefore gives a very detailed account of the individual protective measures and provides recommendations for the design of technical protection facilities. (orig./MG) [Deutsch] Als Basisstoffe dienen in der Regel bestimmte fluessige Kohlenwasserstoffverbindungen aus Mineraloelen sowie aus nativen oder synthetischen Oelen. Durch die Zugabe von weiteren Stoffen erlangt der Kuehlschmierstoff seine fuer den jeweiligen Anwendungsabfall geforderten Eigenschaften. Beschaeftigte, die mit Kuehlschmierstoffen umgehen, sind unterschiedliche Gefahren ausgesetzt. Die Beurteilung der Kuehlschmierstoffkonzentrationen in der Luft am Arbeitsplatz erfolgt auf der Grundlage bestehender

  17. Elucidating the Short Term Loss Behavior of Markovian-Modulated Batch-Service Queueing Model with Discrete-Time Batch Markovian Arrival Process

    OpenAIRE

    Yung-Chung Wang; Dong-Liang Cai; Li-Hsin Chiang; Cheng-Wei Hu

    2014-01-01

    This paper applies a matrix-analytical approach to analyze the temporal behavior of Markovian-modulated batch-service queue with discrete-time batch Markovian arrival process (DBMAP). The service process is correlated and its structure is presented through discrete-time batch Markovian service process (DBMSP). We examine the temporal behavior of packet loss by means of conditional statistics with respect to congested and noncongested periods that occur in an alternating manner. The congested ...

  18. Laser cooling of organic-inorganic lead halide perovskites

    Science.gov (United States)

    Ha, Son-Tung; Shen, Chao; Zhang, Jun; Xiong, Qihua

    2016-02-01

    Optical irradiation with suitable energy can cool solids, a phenomenon known as optical refrigeration, first proposed in 1929 and experimentally achieved in ytterbium-doped glasses in 1995. Since then, considerable progress has been made in various rare earth element-doped materials, with a recent record of cooling to 91 K directly from ambient temperatures. For practical use and to suit future applications of optical refrigeration, the discovery of materials with facile and scalable synthesis and high cooling power density will be required. Herein we present the realization of a net cooling of 23.0 K in micrometre-thick 3D CH3NH3PbI3 (MAPbI3) and 58.7 K in exfoliated 2D (C6H5C2H4NH3)2PbI4 (PhEPbI4) perovskite crystals directly from room temperature. We found that the perovskite crystals exhibit strong photoluminescence upconversion and near unity external quantum efficiency, properties that are responsible for the realization of net laser cooling. Our findings indicate that solution-processed perovskite thin films may be a highly suitable candidate for constructing integrated optical cooler devices.

  19. Liquid crystal tunable photonic crystal dye laser

    OpenAIRE

    Buss, Thomas; Christiansen, Mads Brøkner; Smith, Cameron; Kristensen, Anders

    2010-01-01

    We present a dye-doped liquid crystal laser using a photonic crystal cavity. An applied electric field to the liquid crystal provides wavelength tunability. The photonic crystal enhances resonant interaction with the gain medium.

  20. Abnormal correlation between phase transformation and cooling rate for pure metals.

    Science.gov (United States)

    Han, J J; Wang, C P; Liu, X J; Wang, Y; Liu, Z-K; Zhang, T-Y; Jiang, J Z

    2016-01-01

    This work aims to achieve deep insight into the phenomenon of phase transformation upon rapid cooling in metal systems and reveal the physical meaning of scatter in the time taken to reach crystallization. The total number of pure metals considered in this work accounts for 14. Taking pure copper as an example, the correlation between phase selection of crystal or glass and cooling rate was investigated using molecular dynamic simulations. The obtained results demonstrate that there exists a cooling rate region of 6.3 × 10(11)-16.6 × 10(11) K/s, in which crystalline fractions largely fluctuate along with cooling rates. Glass transformation in this cooling rate region is determined by atomic structure fluctuation, which is controlled by thermodynamic factors. According to the feature of bond-orientation order at different cooling rates, we propose two mechanisms of glass formation: (i) kinetic retardation of atom rearrangement or structural relaxation at a high cooling rate; and (ii) competition of icosahedral order against crystal order near the critical cooling rate. PMID:26939584

  1. Batch Preheat for glass and related furnace processing operations

    Energy Technology Data Exchange (ETDEWEB)

    Energy & Environmental Resources, Inc

    2002-08-12

    The objectives that our development work addressed are: (1) Establish through lab tests a salt eutectic with a melting point of about 250 F and a working range of 250 to 1800 F. (2) Establish the most economical material of construction for the screened salt eutectics identified in the first objective. (3) Establish the material of construction for the salt heater liner. Objectives 2 and 3 were determined through corrosion tests using selected metallurgical samples. Successful completion of the above-stated goals will be incorporated in a heat recovery design that can be used in high temperature processes and furnaces, typical of which is the glass melting process. The process design incorporates the following unit operations: a vertical batch heater (whereby the batch flows down through tubes in a shell and tube exchanger; a molten salt eutectic is circulated on the shell side); a molten salt heater utilizing furnace flue gas in a radiation type heater (molten salt is circulated in the annular space between the inner and outer shells of the vertical heater, and flue gas passes from the furnace exhaust through the inner shell of the heater); a cantilever type molten salt circulating pump; and a jacketed mixer/conveyor to drive off moisture from the batch prior to feeding the batch to the vertical batch heater. Historically, radiation heaters, when applied to glass or fiberglass furnace recuperation, have experienced failures due to uneven heat flux rates, which increases internal stresses and spot overheating conditions. Low heat transfer coefficients result in requirements for large heat transfer surface areas in gas to gas or gas to air exchangers. Fouling is another factor that results in lower unit availability and reduced performance. These factors are accommodated in this process by the incorporation of several design features. The salt heater will be a vertical double wall radiation design, similar to radiation air heaters used in high temperature heat

  2. Molecular Crystals

    Science.gov (United States)

    Wright, John D.

    1995-02-01

    This book describes the chemical and physical structure of molecular crystals, their optical and electronic properties, and the reactions between neighboring molecules in crystals. In the second edition, the author has taken into account research that has undergone extremely rapid development since the first edition was published in 1987. For instance, he gives extensive coverage to the applications of molecular materials in high-technology devices (e.g. optical communications, laser printers, photocopiers, liquid crystal displays, solar cells, and more). There is also an entirely new chapter on the recently discovered Buckminsterfullerene carbon molecule (C60) and organic non-linear optic materials.

  3. Kinetic study of batch and fed-batch enzymatic saccharification of pretreated substrate and subsequent fermentation to ethanol

    OpenAIRE

    Gupta Rishi; Kumar Sanjay; Gomes James; Kuhad Ramesh

    2012-01-01

    Abstract Background Enzymatic hydrolysis, the rate limiting step in the process development for biofuel, is always hampered by its low sugar concentration. High solid enzymatic saccharification could solve this problem but has several other drawbacks such as low rate of reaction. In the present study we have attempted to enhance the concentration of sugars in enzymatic hydrolysate of delignified Prosopis juliflora, using a fed-batch enzymatic hydrolysis approach. Results The enzymatic hydroly...

  4. Liquid crystal tunable photonic crystal dye laser

    DEFF Research Database (Denmark)

    Buss, Thomas; Christiansen, Mads Brøkner; Smith, Cameron;

    2010-01-01

    We present a dye-doped liquid crystal laser using a photonic crystal cavity. An applied electric field to the liquid crystal provides wavelength tunability. The photonic crystal enhances resonant interaction with the gain medium.......We present a dye-doped liquid crystal laser using a photonic crystal cavity. An applied electric field to the liquid crystal provides wavelength tunability. The photonic crystal enhances resonant interaction with the gain medium....

  5. Laser Cooling of Molecular Anions

    CERN Document Server

    Yzombard, Pauline; Gerber, Sebastian; Doser, Michael; Comparat, Daniel

    2015-01-01

    We propose a scheme for laser cooling of negatively charged molecules. We briefly summarise the requirements for such laser cooling and we identify a number of potential candidates. A detailed computation study with C$\\_2^-$, the most studied molecular anion, is carried out. Simulations of 3D laser cooling in a gas phase show that this molecule could be cooled down to below 1 mK in only a few tens of milliseconds, using standard lasers. Sisyphus cooling, where no photo-detachment process is present, as well as Doppler laser cooling of trapped C$\\_2^-$, are also simulated. This cooling scheme has an impact on the study of cold molecules, molecular anions, charged particle sources and antimatter physics.

  6. Macromolecular Crystal Growth by Means of Microfluidics

    Science.gov (United States)

    vanderWoerd, Mark; Ferree, Darren; Spearing, Scott; Monaco, Lisa; Molho, Josh; Spaid, Michael; Brasseur, Mike; Curreri, Peter A. (Technical Monitor)

    2002-01-01

    We have performed a feasibility study in which we show that chip-based, microfluidic (LabChip(TM)) technology is suitable for protein crystal growth. This technology allows for accurate and reliable dispensing and mixing of very small volumes while minimizing bubble formation in the crystallization mixture. The amount of (protein) solution remaining after completion of an experiment is minimal, which makes this technique efficient and attractive for use with proteins, which are difficult or expensive to obtain. The nature of LabChip(TM) technology renders it highly amenable to automation. Protein crystals obtained in our initial feasibility studies were of excellent quality as determined by X-ray diffraction. Subsequent to the feasibility study, we designed and produced the first LabChip(TM) device specifically for protein crystallization in batch mode. It can reliably dispense and mix from a range of solution constituents into two independent growth wells. We are currently testing this design to prove its efficacy for protein crystallization optimization experiments. In the near future we will expand our design to incorporate up to 10 growth wells per LabChip(TM) device. Upon completion, additional crystallization techniques such as vapor diffusion and liquid-liquid diffusion will be accommodated. Macromolecular crystallization using microfluidic technology is envisioned as a fully automated system, which will use the 'tele-science' concept of remote operation and will be developed into a research facility for the International Space Station as well as on the ground.

  7. Stability of Amorphous Pharmaceutical Solids: Crystal Growth Mechanisms and Effect of Polymer Additives

    OpenAIRE

    Sun, Ye; Zhu, Lei; Wu, Tian; Cai, Ting; Gunn, Erica M.; Yu, Lian

    2012-01-01

    We review recent progress toward understanding and enhancing the stability of amorphous pharmaceutical solids against crystallization. As organic liquids are cooled to become glasses, fast modes of crystal growth can emerge. One such growth mode, the glass-to-crystal or GC mode, occurs in the bulk, and another exists at the free surface, both leading to crystal growth much faster than predicted by theories that assume diffusion defines the kinetic barrier of crystallization. These phenomena h...

  8. Solid state crystal physics at very low temperatures

    Science.gov (United States)

    Davis, W.; Krack, K.; Richard, J. P.; Weber, J.

    1980-01-01

    The properties of nearly perfect crystals was studied at cryogenic temperatures. A large Helium 3 and Helium 4 dilution refrigerator has been assembled, and is described. A cryostat suitable for cooling a 35 liter volume to .020 Kelvin was designed and constructed, together with instrumentation to observe the properties of nearly perfect crystals.

  9. Water cooled nuclear reactor

    International Nuclear Information System (INIS)

    In the reactor operating with supercritical pressure and temperature part of the water flowing through the moderator tubes is deflected at the outlet and mixed with a residual partial flow of the coolant fed into the core as well as passed along the fuel rods in opposite direction. By special guiding of the flow downward through the guide tubes of the control rods insertion of the control rods is simplified because of reduced frictional forces. By this means it is also achieved to design less critical the control rod cooling with respect to flow rate control and operating behavior in case of a scram. (orig.)

  10. Rotary engine cooling system

    Science.gov (United States)

    Jones, Charles (Inventor); Gigon, Richard M. (Inventor); Blum, Edward J. (Inventor)

    1985-01-01

    A rotary engine has a substantially trochoidal-shaped housing cavity in which a rotor planetates. A cooling system for the engine directs coolant along a single series path consisting of series connected groups of passages. Coolant enters near the intake port, passes downwardly and axially through the cooler regions of the engine, then passes upwardly and axially through the hotter regions. By first flowing through the coolest regions, coolant pressure is reduced, thus reducing the saturation temperature of the coolant and thereby enhancing the nucleate boiling heat transfer mechanism which predominates in the high heat flux region of the engine during high power level operation.

  11. Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol

    Institute of Scientific and Technical Information of China (English)

    Gregory F.L.Koay; Teong-Guan Chuah; Sumaiya Zainal-Abidin; Salmiah Ahmad; Thomas S.Y.Choong

    2012-01-01

    Palm-based dihydroxystearic acid of 69.55% purity was produced in a 500-kg-per-batch operation pilot plant and purified through solvent crystallization in a custom fabricated simultaneous batch crystallizer unit.The effects of temperature and solvent concentration on yield,particle size distribution and purity were studied.The purity was higher,while the yield and particle size were lower and smaller,respectively,at higher temperature and solvent concentration.The solvent crystallization process efficiency was rated at 66-69% when carried out with 70-80% isopropyl alcohol at 20 ℃.

  12. Cooled spool piston compressor

    Science.gov (United States)

    Morris, Brian G. (Inventor)

    1993-01-01

    A hydraulically powered gas compressor receives low pressure gas and outputs a high pressure gas. The housing of the compressor defines a cylinder with a center chamber having a cross-sectional area less than the cross-sectional area of a left end chamber and a right end chamber, and a spool-type piston assembly is movable within the cylinder and includes a left end closure, a right end closure, and a center body that are in sealing engagement with the respective cylinder walls as the piston reciprocates. First and second annual compression chambers are provided between the piston enclosures and center housing portion of the compressor, thereby minimizing the spacing between the core gas and a cooled surface of the compressor. Restricted flow passageways are provided in the piston closure members and a path is provided in the central body of the piston assembly, such that hydraulic fluid flows through the piston assembly to cool the piston assembly during its operation. The compressor of the present invention may be easily adapted for a particular application, and is capable of generating high gas pressures while maintaining both the compressed gas and the compressor components within acceptable temperature limits.

  13. ASTROMAG coil cooling study

    Science.gov (United States)

    Maytal, Ben-Zion; Vansciver, Steven W.

    1990-01-01

    ASTROMAG is a planned particle astrophysics magnetic facility. Basically it is a large magnetic spectrometer outside the Earth's atmosphere for an extended period of time in orbit on a space station. A definition team summarized its scientific objectives assumably related to fundamental questions of astrophysics, cosmology, and elementary particle physics. Since magnetic induction of about 7 Tesla is desired, it is planned to be a superconducting magnet cooled to liquid helium 2 temperatures. The general structure of ASTROMAG is based on: (1) two superconducting magnetic coils, (2) dewar of liquid helium 2 to provide cooling capability for the magnets; (3) instrumentation, matter-anti matter spectrometer (MAS) and cosmic ray isotope spectrometer (CRIS); and (4) interfaces to the shuttle and space station. Many configurations of the superconducting magnets and the dewar were proposed and evaluated, since those are the heart of the ASTROMAG. Baseline of the magnet configuration and cryostat as presented in the phase A study and the one kept in mind while doing the present study are presented. ASTROMAG's development schedule reflects the plan of launching to the space station in 1995.

  14. Cooling Performance of an Impingement Cooling Device Combined with Pins

    Institute of Scientific and Technical Information of China (English)

    Dongliang QUAN; Songling LIU; Jianghai LI; Gaowen LIU

    2005-01-01

    Experimental study and one dimensional model analysis were conducted to investigate cooling performance of an integrated impingement and pin fin cooling device. A typical configuration specimen was made and tested in a large scale low speed closed-looped wind tunnel. Detailed two-dimensional contour maps of the temperature and cooling effectiveness were obtained for different pressure ratios and therefore different coolant flow-rates through the tested specimen. The experimental results showed that very high cooling effectiveness can be achieved by this cooling device with relatively small amount of coolant flow. Based on the theory of transpiration cooling in porous material, a one dimensional heat transfer model was established to analyze the effect of various parameters on cooling effectiveness. It was found from this model that the variation of heat transfer on the gas side, including heat transfer coefficient and film cooling effectiveness, of the specimen created much more effect on its cooling effectiveness than that of the coolant side. The predictions of the one-dimensional mode were compared and agreed well with the experimental data.

  15. [Kinetics model for batch culture of white rot fungus].

    Science.gov (United States)

    Xiong, Xiao-ping; Wen, Xiang-hua; Xu, Kang-ning; Bian, Bing-hui

    2008-02-01

    In order to understand ligninolytic enzymes production process during culture of white rot fungus, accordingly to direct the design of fermentation process, a kinetics model was built for the batch culture of Phanerochaete chrysosporium. The parameters in the model were calibrated based on the experimental data from free and immobilized culture separately. The difference between each variable's values calculated based on kinetics model and experimental data is within 15%. Comparing parameters for the free and the immobilized culture, it is found that maximum biomass concentrations are both 1.78 g/L; growth rate ratio of immobilized culture (0.6683 d(-1)) is larger than that of free culture (0.5144 d(-1)); very little glucose is consumed for biomass growth in free culture while in immobilized culture much glucose is used and ammonium nitrogen is consumed at a greater rate. Ligninolytic enzymes production process is non-growth related; fungal pellets can produce MnP (231 U/L) in free culture with a production rate of 115.8 U x (g x d)(-1) before peak and 26.1 U x (g x d)(-1) after peak, thus fed-batch is a possible mode to improve MnP production and fermentation efficiency. MnP (410 U/L) and LiP (721 U/L) can be produced in immobilized culture, but MnP and LiP production rate decrease from 80.1 U x (g x d)(-1) and 248.9 U x (g x d)(-1) to 6.04 U x (g x d)(-1) and 0 U x (g x d)(-1), respectively, indicating a proper feed moment is before the enzymes peak during fed-batch culture. PMID:18613526

  16. A design algorithm for batch stirred tank transesterification reactors

    International Nuclear Information System (INIS)

    Highlights: ► Simplified algorithm for batch biodiesel reactor design was developed. ► C Sharp software tool for implementing the algorithm was also developed. ► 50 L/batch reactor was constructed and used to process neem oil biodiesel. ► Results showed that the produced neem biodiesel is a fuel grade product. ► Scale-up of the reactor was carried out using the developed software. - Abstract: A 50 L per batch, stirred tank reactor, suitable for carrying out transesterification of vegetable oils was designed and constructed. The major design assumptions included stainless steel plate thickness of 2 mm, reaction temperature of 60–65 °C and an initial/final fluid temperature of 25/70 °C. The calculated impeller Reynolds number was in the mixed regime zone of 10–104; the power number was varied between 1 and 5, while a typical propeller speed of 22.5 rev/s (or 1350 rev/min) was adopted. The limiting design conditions were maximum reactor diameter of 1.80 m, straight side height-to-diameter ratio in the range of 0.75–1.5 and minimum agitator motor power of 746 W (1 Hp). Based upon the design, a simple algorithm was developed and interpreted into Microsoft C Sharp computer programming language to enable scale up of the reactor. Performance testing of the realized reactor was carried out while using it to produce Neem oil biodiesel via base – catalyzed methanolysis, which yielded high quality fuel product.

  17. Moving from batch towards continuous organic‐chemical pharmaceutical production

    OpenAIRE

    Cervera Padrell, Albert Emili; Gernaey, Krist; Gani, Rafiqul; Kiil, Søren

    2011-01-01

    Farmaceutiske ingredienser er traditionelt blevet fremstillet i batch reaktorer, dvs i ’multipurpose’ omrørte tanke. Reaktioner og separationer har typisk været skræddersyet til disse enheder, og der har typisk været flere begrænsninger, når der overføres en organisk syntese fra laboratoriet til industriel skala. Opskalering resulterede dermed i mange tilfælde i et lavt udbytte og en relativt ineffektiv separation. Disse begrænsninger blev dog opvejet af en relativt hurtig implementering af p...

  18. Batch Mode Data Analysis at ORNL for Radiation Portal Monitoring

    International Nuclear Information System (INIS)

    The Global Nuclear Security Technology Division at Oak Ridge National Laboratory (ORNL) has developed two batch-mode data analysis tools to address the volume of data generated by radiation portal monitors (RPMs) deployed by the Second Line of Defense (SLD). The first of these tools, the ORNL Data Portal (ORNLDP), serves as both a repository and an analysis environment for the data generated by RPMs. The second tool, the In-Country Analysis Tool (ICAT), is portable and serves primarily as a small-scale analysis environment.

  19. Bounded Parallel-Batch Scheduling on Unrelated Parallel Machines

    Science.gov (United States)

    Miao, Cuixia; Zhang, Yuzhong; Wang, Chengfei

    In this paper, we consider the bounded parallel-batch scheduling problem on unrelated parallel machines. Problems R m |B|F are NP-hard for any objective function F. For this reason, we discuss the special case with p ij = p i for i = 1, 2, ⋯ , m , j = 1, 2, ⋯ , n. We give optimal algorithms for the general scheduling to minimize total weighted completion time, makespan and the number of tardy jobs. And we design pseudo-polynomial time algorithms for the case with rejection penalty to minimize the makespan and the total weighted completion time plus the total penalty of the rejected jobs, respectively.

  20. REAL WASTE TESTING OF SLUDGE BATCH 5 MELTER FEED RHEOLOGY

    Energy Technology Data Exchange (ETDEWEB)

    Reboul, S.; Stone, M.

    2010-03-17

    Clogging of the melter feed loop at the Defense Waste Processing Facility (DWPF) has reduced the throughput of Sludge Batch 5 (SB5) processing. After completing a data review, DWPF attributed the clogging to the rheological properties of the Slurry Mix Evaporator (SME) project. The yield stress of the SB5 melter feed material was expected to be high, based on the relatively high pH of the SME product and the rheological results of a previous Chemical Process Cell (CPC) demonstration performed at the Savannah River National Laboratory (SRNL).

  1. Deposition of TiN films in a batch reactor

    OpenAIRE

    Hasper, Albert; Snijders, Gert-Jan; Vandezande, Lieve; De Blank, Marinus J.; Bankras, Radko Gerard

    2006-01-01

    Titanium nitride (TiN) films are formed in a batch reactor using titanium chloride (TiCl4) and ammonia (NH3) as precursors. The TiCl4 is flowed into the reactor in temporally separated pulses. The NH3 can also be flowed into the reactor in temporally spaced pulses which alternate with the TiCl4 pulses, or the NH3 can be flowed continuously into the reactor while the TiCl4 is introduced in pulses. The resulting TiN films exhibit low resistivity and good uniformity.

  2. Modelization of cooling system components

    International Nuclear Information System (INIS)

    In the site evaluation study for licensing a new nuclear power facility, the criteria involved could be grouped in health and safety, environment, socio-economics, engineering and cost-related. These encompass different aspects such as geology, seismology, cooling system requirements, weather conditions, flooding, population, and so on. The selection of the cooling system is function of different parameters as the gross electrical output, energy consumption, available area for cooling system components, environmental conditions, water consumption, and others. Moreover, in recent years, extreme environmental conditions have been experienced and stringent water availability limits have affected water use permits. Therefore, modifications or alternatives of current cooling system designs and operation are required as well as analyses of the different possibilities of cooling systems to optimize energy production taking into account water consumption among other important variables. There are two basic cooling system configurations: - Once-through or Open-cycle; - Recirculating or Closed-cycle. In a once-through cooling system (or open-cycle), water from an external water sources passes through the steam cycle condenser and is then returned to the source at a higher temperature with some level of contaminants. To minimize the thermal impact to the water source, a cooling tower may be added in a once-through system to allow air cooling of the water (with associated losses on site due to evaporation) prior to returning the water to its source. This system has a high thermal efficiency, and its operating and capital costs are very low. So, from an economical point of view, the open-cycle is preferred to closed-cycle system, especially if there are no water limitations or environmental restrictions. In a recirculating system (or closed-cycle), cooling water exits the condenser, goes through a fixed heat sink, and is then returned to the condenser. This configuration

  3. Non-isothermal crystallization kinetics of polyethylene–clay nanocomposites prepared by high-energy ball milling

    Indian Academy of Sciences (India)

    Maryam Abareshi; Seyed Mojtaba Zebarjad; Elaheh K Goharshadi

    2014-08-01

    Non-isothermal crystallization kinetics of pure medium density polyethylene (MDPE) and MDPE–clay nanocomposites have been investigated by differential scanning calorimeter. The modified Avrami, Ozawa, Liu and Ziabicki equations have been applied to describe non-isothermal crystallization process. The results of Avrami analysis showed a very complicated crystallization mechanism. Although, Ozawa equation failed to provide an adequate description for non-isothermal crystallization process, Liu equation could describe it well. The data showed the crystallization rate of MDPE and nanocomposites raises with increasing cooling rate and the crystallization rate of nanocomposite is faster than that of MDPE at a given cooling rate. Ziabicki’s kinetic crystallizability index showed that clay can increase the ability of MDPE to crystallize, when it is cooled at unit cooling rate. The activation energy of samples has been evaluated by Kissinger method. The results showed that the activation energy of nanocomposite was lower than that of MDPE.

  4. High-heat-load synchrotron tests of room-temperature, silicon crystal monochromators at the CHESS F-2 wiggler station

    International Nuclear Information System (INIS)

    This note summarizes the results of the single crystal monochromator high-heat-load tests performed at the CHESS F-2 wiggler station. The results from two different cooling geometries are presented: (1) the ''pin-post'' crystal and (2) the ''criss-cross'' crystal. The data presented were taken in August 1993 (water-cooled pin-post) and in April 1995 (water- and gallium-cooled pin-post crystal and gallium-cooled criss-cross crystal). The motivation for trying these cooling (or heat exchanger) geometries is to improve the heat transfer efficiency over that of the conventional slotted crystals. Calculations suggest that the pin-post or the microchannel design can significantly improve the thermal performance of the crystal. The pin-post crystal used here was fabricated by Rocketdyne Albuquerque Operations. From the performance of the conventional slotted crystals, it was thought that increased turbulence in the flow pattern may also enhance the heat transfer. The criss-cross crystal was a simple attempt to achieve the increased flow turbulence. The criss-cross crystal was partly fabricated in-house (cutting, etching and polishing) and bonded by RAO. Finally, a performance comparison among all the different room temperature silicon monochromators that have been tested by the APS is presented. The data includes measurements with the slotted crystal and the core-drilled crystals. Altogether, the data presented here were taken at the CHESS F-2 wiggler station between 1991 and 1995

  5. Electronic cooling using thermoelectric devices

    Energy Technology Data Exchange (ETDEWEB)

    Zebarjadi, M., E-mail: m.zebarjadi@rutgers.edu [Department of Mechanical and Aerospace Engineering, Rutgers University, Piscataway, New Jersey 08854 (United States); Institute of Advanced Materials, Devices, and Nanotechnology, Rutgers University, Piscataway, New Jersey 08854 (United States)

    2015-05-18

    Thermoelectric coolers or Peltier coolers are used to pump heat in the opposite direction of the natural heat flux. These coolers have also been proposed for electronic cooling, wherein the aim is to pump heat in the natural heat flux direction and from hot spots to the colder ambient temperature. In this manuscript, we show that for such applications, one needs to use thermoelectric materials with large thermal conductivity and large power factor, instead of the traditionally used high ZT thermoelectric materials. We further show that with the known thermoelectric materials, the active cooling cannot compete with passive cooling, and one needs to explore a new set of materials to provide a cooling solution better than a regular copper heat sink. We propose a set of materials and directions for exploring possible materials candidates suitable for electronic cooling. Finally, to achieve maximum cooling, we propose to use thermoelectric elements as fins attached to copper blocks.

  6. Stochastic cooling of particle beams

    Energy Technology Data Exchange (ETDEWEB)

    Moehl, Dieter [European Organization for Nuclear Research (CERN), Geneva (Switzerland)

    2013-02-01

    First topical monograph on this subject matter. Provides conceptual and theoretical introduction. Introduces modern cooling schemes. This lecture note describes the main analytical approaches to stochastic cooling. The first is the time-domain picture, in which the beam is rapidly sampled at a high rate and a statistical analysis is used to describe the cooling behaviour. The second is the frequency-domain picture, which is particularly useful since the observations made on the beam and the numerical cooling simulations are mainly in this domain. This second picture is developed in detail to assess key components of modern cooling theory like mixing and signal shielding and to illustrate some of the diagnostic methods. Finally the use of a distribution function and the Fokker-Plank equation, which offer the most complete description of the beam during the cooling, are discussed.

  7. Liquid Crystals

    Science.gov (United States)

    1990-01-01

    Thermochromic liquid crystals, or TLCs, are a type of liquid crystals that react to changes in temperature by changing color. The Hallcrest/NASA collaboration involved development of a new way to visualize boundary layer transition in flight and in wind tunnel testing of aircraft wing and body surfaces. TLCs offered a new and potentially better method of visualizing the boundary layer transition in flight. Hallcrest provided a liquid crystal formulation technique that afforded great control over the sensitivity of the liquid crystals to varying conditions. Method is of great use to industry, government and universities for aerodynamic and hydrodynamic testing. Company's principal line is temperature indicating devices for industrial use, such as non-destructive testing and flaw detection in electric/electronic systems, medical application, such as diagnostic systems, for retail sale, such as room, refrigerator, baby bath and aquarium thermometers, and for advertising and promotion specials. Additionally, Hallcrest manufactures TLC mixtures for cosmetic applications, and liquid crystal battery tester for Duracell batteries.

  8. Crystallization of polyethylenes at very high supercooling

    Science.gov (United States)

    Wagner, John Edward

    The crystallization behavior of a series of ethylene-octene copolymers synthesized using metallocene catalysts has been studied using the Ding-Spruiell method of rapid cooling. In conventional crystallization experiments it was found, as expected, that the spherulite growth rates varied with octene content and molecular weight. When studied at rapid cooling rates the polymers generate their own pseudo-isothermal crystallization temperatures, in agreement with Ding-Spruiell's studies on other systems, however, at the lowest temperatures of crystallization, the spherulite growth rates of all the copolymers studied merge. The WAXD results indicate at the faster crystallization rates that the size of the unit cell unit decreases with decreasing crystallization temperature. A resulting increase in the surface free energy plays a role in the behavior of the copolymers such that spherulitic growth rates of copolymers begin to surpass that of the linear polyethylene at very high supercooling. This is a change in the behavior of the copolymers that should be of considerable relevance to polymer processing conditions. Spinodal transformation could play of role in the leveling off of growth rates at high supercooling. The crystallization and morphology of four LLDPE samples produced using metallocene catalysts through the copolymerization of ethylene and octene has been studied. The second part of the study is primarily concerned with the growth kinetics obtained through experimentally determined growth rates at different crystallization temperatures of low and high molecular weight samples. Using experimentally determined equilibrium melting points secondary nucleation behavior is studied in detail. Three Regimes are seen for a molecular weight 101,000 with no branching and at 60,000 with branching at 4 octenes per 1000 carbons. Two Regimes have been obtained for a sample of similar molecular weight but with branching at 17 octenes per 1000 carbons. Lamellar thickness data

  9. To Be Cool or Uncool?

    Institute of Scientific and Technical Information of China (English)

    袁会珍

    2007-01-01

    The western world has always been divided into two types of people-the cool and the uncool. It is a division that __1__ in school. The cool kids are good at __2__. They are __3__ with the opposite sex. They are good-looking and people want to __4__ their style. They can do their homework but they don't make a big effort. That would __5__ be cool.

  10. Electron cooling experiments in CSR

    Institute of Scientific and Technical Information of China (English)

    PARKHOMCHUK; Vasily; REVA; Vladimir

    2011-01-01

    The six species heavy ion beam was accumulated with the help of electron cooling in the main ring of Cooler Storage Ring of Heavy Ion Research Facility in Lanzhou (HIRFL-CSR). The ion beam accumulation dependence on the parameters of cooler was investigated experimentally. The 400 MeV/u 12C6+ and 200 MeV/u 129Xe54+ were stored and cooled in the experimental ring CSRe, and the cooling force was measured in different conditions.

  11. Electron Cooling Experiments in CSR

    CERN Document Server

    Xiaodong, Yang

    2011-01-01

    The six species heavy ion beam was accumulated with the help of electron cooling in the main ring of Cooler Storage Ring of Heavy Ion Research Facility in Lanzhou(HIRFL-CSR), the ion beam accumulation dependence on the parameters of cooler was investigated experimentally. The 400MeV/u 12C6+ and 200MeV/u 129Xe54+ was stored and cooled in the experimental ring CSRe, the cooling force was measured in different condition.

  12. Film cooling from two rows of holes with opposite orientation angles: injectant behavior and adiabatic film cooling effectiveness

    International Nuclear Information System (INIS)

    The present paper is aiming at describing the injectant behaviors from two rows of film cooling holes with opposite orientation angles. Boundary layer temperature distributions were measured in the streamwise normal plane to illustrate the interaction between the injectant from the holes in the upstream row and from the downstream row. Detailed adiabatic film cooling effectiveness distributions were also measured using thermochromic liquid crystal to investigate how well the injectant covers the film cooled surface. Four film cooling hole arrangements were considered including inline and staggered ones. And three blowing ratios of 0.5, 1.0 and 2.0 were studied. At the blowing ratio of 0.5, the injectant is centered near film cooled surface irrespective of hole configurations to show high film cooling effectiveness. When the blowing ratio exceeds unity the injectant tends to lift off from the wall due to the increase of the wall normal momentum. With the inline configuration, not like other configurations, the injectant is still well attached to the wall with the help of the downwash flow formed at the hole exit

  13. Direct cooled power electronics substrate

    Science.gov (United States)

    Wiles, Randy H [Powell, TN; Wereszczak, Andrew A [Oak Ridge, TN; Ayers, Curtis W [Kingston, TN; Lowe, Kirk T [Knoxville, TN

    2010-09-14

    The disclosure describes directly cooling a three-dimensional, direct metallization (DM) layer in a power electronics device. To enable sufficient cooling, coolant flow channels are formed within the ceramic substrate. The direct metallization layer (typically copper) may be bonded to the ceramic substrate, and semiconductor chips (such as IGBT and diodes) may be soldered or sintered onto the direct metallization layer to form a power electronics module. Multiple modules may be attached to cooling headers that provide in-flow and out-flow of coolant through the channels in the ceramic substrate. The modules and cooling header assembly are preferably sized to fit inside the core of a toroidal shaped capacitor.

  14. Cooling of rectangular bars

    International Nuclear Information System (INIS)

    A solution of the time-transient Heat Transfer Differential Equation in rectangular coordinates is presented, leading to a model which describes the temperature drop with time in rectangular bars. It is similar to an other model for cilindrical bars which has been previously developed in the Laboratory of Mechanical Metallurgy of UFRGS. Following these models, a generalization has been made, which permits cooling time evaluation for all profiles. These results are compared with experimental laboratory data in the 1200 to 8000C range. Some other existing models were also studied which have the purpose of studing the same phenomenon. Their mathematical forms and their evaluated values are analyzed and compared with experimental ones. (Author)

  15. ATLAS' major cooling project

    CERN Document Server

    2005-01-01

    In 2005, a considerable effort has been put into commissioning the various units of ATLAS' complex cryogenic system. This is in preparation for the imminent cooling of some of the largest components of the detector in their final underground configuration. The liquid helium and nitrogen ATLAS refrigerators in USA 15. Cryogenics plays a vital role in operating massive detectors such as ATLAS. In many ways the liquefied argon, nitrogen and helium are the life-blood of the detector. ATLAS could not function without cryogens that will be constantly pumped via proximity systems to the superconducting magnets and subdetectors. In recent weeks compressors at the surface and underground refrigerators, dewars, pumps, linkages and all manner of other components related to the cryogenic system have been tested and commissioned. Fifty metres underground The helium and nitrogen refrigerators, installed inside the service cavern, are an important part of the ATLAS cryogenic system. Two independent helium refrigerators ...

  16. Fluid cooled electrical assembly

    Science.gov (United States)

    Rinehart, Lawrence E.; Romero, Guillermo L.

    2007-02-06

    A heat producing, fluid cooled assembly that includes a housing made of liquid-impermeable material, which defines a fluid inlet and a fluid outlet and an opening. Also included is an electrical package having a set of semiconductor electrical devices supported on a substrate and the second major surface is a heat sink adapted to express heat generated from the electrical apparatus and wherein the second major surface defines a rim that is fit to the opening. Further, the housing is constructed so that as fluid travels from the fluid inlet to the fluid outlet it is constrained to flow past the opening thereby placing the fluid in contact with the heat sink.

  17. Comparison of growth, acetate production, and acetate inhibition of Escherichia coli strains in batch and fed-batch fermentations.

    Science.gov (United States)

    Luli, G W; Strohl, W R

    1990-04-01

    The growth characteristics and acetate production of several Escherichia coli strains were compared by using shake flasks, batch fermentations, and glucose-feedback-controlled fed-batch fermentations to assess the potential of each strain to grow at high cell densities. Of the E. coli strains tested, including JM105, B, W3110, W3100, HB101, DH1, CSH50, MC1060, JRG1046, and JRG1061, strains JM105 and B were found to have the greatest relative biomass accumulation, strain MC1060 accumulated the highest concentrations of acetic acid, and strain B had the highest growth rates under the conditions tested. In glucose-feedback-controlled fed-batch fermentations, strains B and JM105 produced only 2 g of acetate.liter-1 while accumulating up to 30 g of biomass.liter-1. Under identical conditions, strains HB101 and MC1060 accumulated less than 10 g of biomass.liter-1 and strain MC1060 produced 8 g of acetate.liter-1. The addition of various concentrations of sodium acetate to the growth medium resulted in a logarithmic decrease, with respect to acetate concentration, in the growth rates of E. coli JM105, JM105(pOS4201), and JRG1061. These data indicated that the growth of the E. coli strains was likely to be inhibited by the acetate they produced when grown on media containing glucose. A model for the inhibition of growth of E. coli by acetate was derived from these experiments to explain the inhibition of acetate on E. coli strains at neutral pH. PMID:2187400

  18. Crystallization, flow and thermal histories of lunar and terrestrial compositions

    Science.gov (United States)

    Uhlmann, D. R.

    1979-01-01

    Contents: a kinetic treatment of glass formation; effects of nucleating heterogeneities on glass formation; glass formation under continuous cooling conditions; crystallization statistics; kinetics of crystal nucleation; diffusion controlled crystal growth; crystallization of lunar compositions; crystallization between solidus and liquidus; crystallization on reheating a glass; temperature distributions during crystallization; crystallization of anorthite and anorthite-albite compositions; effect of oxidation state on viscosity; diffusive creep and viscous flow; high temperature flow behavior of glass-forming liquids, a free volume interpretation; viscous flow behavior of lunar compositions; thermal history of orange soil material; breccias formation by viscous sintering; viscous sintering; thermal histories of breccias; solute partitioning and thermal history of lunar rocks; heat flow in impact melts; and thermal histories of olivines.

  19. Cryogenics for the MuCool Test Area (MTA)

    Science.gov (United States)

    Darve, Christine; Norris, Barry; Pei, Liujin

    2006-03-01

    MuCool Test Area (MTA) is a complex of buildings at Fermi National Accelerator Laboratory, which are dedicated to operate components of a cooling cell to be used for Muon Collider and Neutrino Factory R&D. The long-term goal of this facility is to test ionization cooling principles by operating a 25-liter liquid hydrogen (LH2) absorber embedded in a 5 Tesla superconducting solenoid magnet. The MTA solenoid magnet will be used with RF cavities exposed to a high intensity beam. Cryogens used at the MTA include LHe, LN2 and LH2. The latter dictates stringent system design for hazardous locations. The cryogenic plant is a modified Tevatron refrigerator based on the Claude cycle. The implementation of an in-house refrigerator system and two 300 kilowatt screw compressors is under development. The helium refrigeration capacity is 500 W at 14 K. In addition the MTA solenoid magnet will be batch-filled with LHe every 2 days using the same cryo-plant. This paper reviews cryogenic systems used to support the Muon Collider and Neutrino Factory R&D programs and emphasizes the feasibility of handling cryogenic equipment at MTA in a safe manner.

  20. Modeling and Simulation of Thermal Transfer in Batch Reactor

    Directory of Open Access Journals (Sweden)

    Baghli, H.

    2006-01-01

    Full Text Available Batch reactors are frequently used in chemical, petrochemical or biochemical industry, for the production of various quality products. Processes used are discontinuous and varied. Indeed, they are characterized by non stationary and non linear systems. An optimal control of the process; requires a modeling and a simulation of the thermal behaviors inside the agitated jacketed reactor in view of the improvement of a high product quality and conditions of security. In certain fields, where the cost and the difficulty of tests are limiting factors, it is advantageous to develop the numeric simulations of these chemical processes. Thus, this study concerns the modeling and simulation of the thermal transfer in an agitated jacketed batch reactor, it is based on a model developed from the global energy balance and empiric correlations which give relationships between thermal transfer coefficients and the stirrer speed. We have achieved the validation of the model by confronting model results with several sets of experiences; for two types of stirrers.