WorldWideScience

Sample records for aluminium alloy tubes

  1. Mechanism of Nickel-Aluminium Alloy Electroplating

    Institute of Scientific and Technical Information of China (English)

    2003-01-01

    The effect of operating conditions on the aluminium content of Ni-Al alloy deposit and the catalytic function of NaF on electrodeposition in the nonaqueous solution containing aluminium are investigated.The results indicate that the plated aluminuim content will be increased with the rise of current density in a given range.When the current density is 2.5A/dm2,nickle-aluminium alloy containing 13.1 wt% aluminium will be deposited.The plated aluminium content will be increased by 2wt% as 0.1mol/L NaF is added to the bath.

  2. Effect of hydrogen on aluminium and aluminium alloys: A review

    DEFF Research Database (Denmark)

    Ambat, Rajan; Dwarakadasa, E.S.

    1996-01-01

    in aluminium and its alloys and its effect on mechanical properties. The importance of hydrogen embrittlement over anodic dissolution to explain the stress corrosion cracking mechanism of these alloys is also examined in considerable detail. The various experimental findings concerning the link between...

  3. Electrical Conductivity of Aluminium Alloy Foams

    Institute of Scientific and Technical Information of China (English)

    凤仪; 郑海务; 朱震刚; 祖方遒

    2002-01-01

    Closed-cell aluminium alloy foams were produced using the powder metallurgical technique. The effect of porosityand cell diameter on the electrical conductivity of foams was investigated and the results were compared with anumber of models. It was found that the percolation theory can be successfully applied to describe the dependenceof the electrical conductivity of aluminium alloy foams on the relative density. The cell diameter has a negligibleeffect on the electrical conductivity of foams.

  4. New aluminium alloys with high lithium content

    Energy Technology Data Exchange (ETDEWEB)

    Schemme, K.; Velten, B.

    1989-06-01

    Since the early 80's there have been made great efforts to replace the high strength aluminium alloys for the aircraft and space industry by a new generation of aluminium-lithium alloys. The attractivity of this kind of alloys could be increased by a further reduction of their density, caused by an increasing lithium content (/ge/ 5 wt.% Li). Therefore binary high-lithium containing alloys with low density are produced and metallografically investigated. A survey of their strength and wear behavior is given by using tensile tests and pin abrasing tests. (orig.).

  5. EFFECT OF COLD DEFORMATION ON THE CORROSION BEHAVIOUR OF Mn-CONTAINING ALUMINIUM ALLOY TUBE%冷加工对含Mn铝合金管腐蚀行为的影响

    Institute of Scientific and Technical Information of China (English)

    王冠; 林晓群

    2011-01-01

    采用SEM,TEM,动电位极化和浸泡实验研究了机械冷加工变形对汽车散热器高Mn(0.22%,质量分数,下同)和低Mn(0.08%)铝合金管在0.6 mol/L NaCl(pH=6)和SWAAT(ASTM G85,pH=3)溶液中的腐蚀行为的影响.电化学极化测试表明,无形变时高Mn铝合金直管的点蚀电位最高;但冷加工能降低高Mn铝合金弯曲表面的点蚀电位,而对低Mn铝合金的点蚀电位没有明显影响.TEM观察发现,冷加工后高Mn铝合金中有大量纳米尺度的富Mn析出相,在低Mn铝合金中却没有观察到这种析出相.阴极极化测试表明,富Mn相能显著促进阴极反应,富Mn相相对Al基体为阴极相,因而是点蚀萌生的部位.添加Mn尽管有利于提高铝合金的耐蚀性,但机械冷加工会弱化这一效应.%Aluminium alloys are extensively employed as heat transfer tube materials in heat exchangers. Previous work has focused on the corrosion behaviour of tube materials in brazed heat exchangers. However, very little attention has been devoted to corrosion of tubes in mechanically-expanded heat exchangers despite the observation of some instances of early corrosion failure in bent region of aluminium alloy tube. The effects of cold deformation on the corrosion behaviour of aluminium tube materials have been studied in 0.6 mol/L NaCl and SWAAT solutions by SEM, TEM,potentiodynamic polarizations and immersion test. The results show that high Mn content (0.22%,mass fraction) can experience preferential corrosion and early failure in the bent region, but not for one with a lower Mn content (0.08%). SEM/TEM observations of the microstructure of the alloys show that each alloy has one main type of coarse intermetallic particle. However, TEM observations show that there is a distinct difference in particle morphology between the bent and straight regions of the high Mn alloy tube, the bent region has more nano-scale Mn-rich particles than the straight region,and no such effects are observed on the

  6. Investigation of the formability of aluminium alloys at elevated temperatures

    Science.gov (United States)

    Tisza, M.; Budai, D.; Kovács, P. Z.; Lukács, Zs

    2016-11-01

    Aluminium alloys are more and more widely applied in car body manufacturing. Increasing the formability of aluminium alloys are one of the most relevant tasks in todays’ research topics. In this paper, the focus will be on the investigation of the formability of aluminium alloys concerning those material grades that are more widely applied in the automotive industry including the 5xxx and 6xxx aluminium alloy series. Recently, besides the cold forming of aluminium sheets the forming of aluminium alloys at elevated temperatures became a hot research topic, too. In our experimental investigations, we mostly examined the EN AW 5754 and EN AW 6082 aluminium alloys at elevated temperatures. We analysed the effect of various material and process parameters (e.g. temperature, sheet thickness) on the formability of aluminium alloys with particular emphasis on the Forming Limit Diagrams at elevated temperatures in order to find the optimum forming conditions for these alloys.

  7. A Reaction Coating on Aluminium Alloys by Laser Processing

    NARCIS (Netherlands)

    Zhou, X.B.; Hosson, J.Th.M. De

    1993-01-01

    An aluminium oxide layer of 100 µm in thickness has been successfully coated on aluminium alloy 6061 and pure aluminium using a powder mixture of silicon oxide and aluminium by laser processing. A strong Al/Al2O3 interface was formed. The exothermic chemical reaction between SiO2 and Al may promote

  8. Friction Welding of Aluminium and Aluminium Alloys with Steel

    Directory of Open Access Journals (Sweden)

    Andrzej Ambroziak

    2014-01-01

    Full Text Available The paper presents our actual knowledge and experience in joining dissimilar materials with the use of friction welding method. The joints of aluminium and aluminium alloys with the different types of steel were studied. The structural effects occurring during the welding process were described. The mechanical properties using, for example, (i microhardness measurements, (ii tensile tests, (iii bending tests, and (iv shearing tests were determined. In order to obtain high-quality joints the influence of different configurations of the process such as (i changing the geometry of bonding surface, (ii using the interlayer, or (iii heat treatment was analyzed. Finally, the issues related to the selection of optimal parameters of friction welding process were also investigated.

  9. Steam Assisted Accelerated Growth of Oxide Layer on Aluminium Alloys

    OpenAIRE

    2013-01-01

    Corrosion resistance of aluminium alloys is related to the composition and morphology of the oxide film on the surface of aluminium. In this paper we investigated the use of steam on the surface modification of aluminium to produce boehmite films. The study reveals a detailed investigation of the effect of vapour pressure, structure of intermetallic particles and thickness of boehmite films on the corrosion behaviour of aluminium alloys.

  10. Alloys of uranium and aluminium with low aluminium content; Alliages uranium-aluminium a faible teneur en aluminium

    Energy Technology Data Exchange (ETDEWEB)

    Cabane, G.; Englander, M.; Lehmann, J. [Commissariat a l' Energie Atomique, Saclay (France). Centre d' Etudes Nucleaires

    1955-07-01

    Uranium, as obtained after spinning in phase {gamma}, presents an heterogeneous structure with large size grains. The anisotropic structure of the metal leads to an important buckling and surface distortion of the fuel slug which is incompatible with its tubular cladding for nuclear fuel uses. Different treatments have been made to obtain an isotropic structure presenting high thermal stability (laminating, hammering and spinning in phase {alpha}) without success. Alloys of uranium and aluminium with low aluminium content present important advantage in respect of non allied uranium. The introduction of aluminium in the form of intermetallic compound (UAl{sub 2}) gives a better resistance to thermal fatigue. Alloys obtained from raw casting present an improved buckling and surface distortion in respect of pure uranium. This improvement is obtained with uranium containing between 0,15 and 0,5 % of aluminium. An even more improvement in thermal stability is obtained by thermal treatments of these alloys. These new characteristics are explained by the fine dispersion of the UAl{sub 2} particles in uranium. The results after treatments obtained from an alloy slug containing 0,4 % of aluminium show no buckling or surface distortion and no elongation. (M.P.)

  11. Mechanical behaviour of aluminium-lithium alloys

    Indian Academy of Sciences (India)

    N Eswara Prasad; A A Gokhale; P Rama Rao

    2003-02-01

    Aluminium-lithium alloys hold promise of providing a breakthrough response to the crying need for lightweight alloys for use as structurals in aerospace applications. Considerable worldwide research has gone into developing a range of these alloys over the last three decades. As a result, substantial understanding has been developed of the microstructure-based micromechanisms of strengthening, of fatigue and fracture as well as of anisotropy in mechanical properties. However, these alloys have not yet greatly displaced the conventionally used denser Al alloys on account of their poorer ductility, fracture toughness and low cycle fatigue resistance. This review aims to summarise the work pertaining to study of structure and mechanical properties with a view to indicate the directions that have been and can be pursued to overcome property limitations.

  12. Friction factor of CP aluminium and aluminium–zinc alloys

    Indian Academy of Sciences (India)

    N Vidhya Sagar; K S Anand; A C Mithun; K Srinivasan

    2006-12-01

    Friction factor has been determined for CP aluminium and aluminium–zinc alloys using ring compression test at different temperatures from 303 K to 773 K. It is found that CP aluminium exhibits sticking whereas Al–Zn alloys do not exhibit sticking at elevated temperatures. Hot working of Al–Zn alloy is easier than that of CP aluminium at 773 K. As zinc content increases up to 10 wt% the friction factor decreases up to 0.02.

  13. Study of fatigue behaviour of 7475 aluminium alloy

    Indian Academy of Sciences (India)

    B B Verma; J D Atkinson; M Kumar

    2001-04-01

    Fatigue properties of a thermomechanically treated 7475 aluminium alloy have been studied in the present investigation. The alloy exhibited superior fatigue life compared to conventional structural aluminium alloys and comparable stage II crack growth rate. It was also noticed that the fatigue crack initiated from a surface grain and the crack extension was dominated by ductile striations. Analysis also revealed that this alloy possessed fracture toughness and tensile properties superior to that noticed with other structural aluminium alloys. Therefore the use of this alloy can safely reduce the overall weight of the aircraft.

  14. Combined Corrosion and Wear of Aluminium Alloy 7075-T6

    NARCIS (Netherlands)

    Liu, Y.; Mol, J.M.C.; Janssen, G.C.A.M.

    2016-01-01

    The aluminium alloy 7075-T6 is widely used in engineering. In some applications, like slurry transport, corrosion and abrasion occur simultaneously, resulting in early material failure. In the present work, we investigated the combined effect of corrosion and wear on the aluminium alloy 7075-T6. We

  15. Forming of aluminium alloy friction stir welds

    Science.gov (United States)

    Bruni, Carlo

    2016-10-01

    The present paper aims at investigating, through analytical models, numerical models and experiments, the effect of the warm deformation phase, realised with an in temperature upsetting, on the weld previously performed by friction stir lap welding on aluminium alloy blanks. The investigation allows to show the deformation zones after upsetting that determine the homogenisation of the weld section. The analytical model allows to relate the friction factor with the upsetting load. The presence on the weld of not elevated friction factor values determines the deformation and localisation levels very useful for the weld. Such methodology allows to improve the weld itself with the forming phase.

  16. Research on hydraulic forming loading paths of aluminium alloy anti-collision energy-absorbing tube%铝合金防碰撞吸能管液压成形加载路径研究

    Institute of Scientific and Technical Information of China (English)

    汪奇超; 雷君相; 骆协海

    2011-01-01

    According to the need of the double diameter tube part forming, the axial feeding compensation and hydraulic pressure loading control to the hydraulic bulging process of aluminium alloy 6061 tube were put forward. By numerical simulation method and the analysis software ABAQUS 6. 10 , aluminum alloy 6061 tube hydraulic bulging loading paths were studied. Taking eventual thickness distribution of the forming parts and forming failure control as the basis, the axial feeding and liquid pressure loading path on forming quality was analyzed. Research shows that when the axle feeding rate is 27 mm and hydraulic pressure is 85 Mpa, the max thinning rate of the anti-collision energy-absorb ing tube is 20. 5%, the quality of parts is nice and the forming of S shape transition region in a pair of mould can be fin ished.%针对防碰撞吸能管成形需要,提出了对铝合金6061圆管液压胀形过程的轴向进给补偿-液压力加载路径控制过程.通过数值模拟方法,采用分析软件ABAQUS 6.10对铝合金6061管材液压胀形的加载路径进行了研究.以成形件不发生起皱、破裂两种失效方式以及最终成形壁厚分布为依据,分析了不同轴向进给和液压力加载路径对成形件质量的影响.研究表明,采用轴向进给量为27mm,液压力为85 MPa的加载路径,获得吸能管的最大减薄率为20.5%,成形质量较好,并在一副模具中同时完成S型过渡区域的成形.

  17. Corrosion of Metal-Matrix Composites with Aluminium Alloy Substrate

    Directory of Open Access Journals (Sweden)

    B. Bobic

    2010-03-01

    Full Text Available The corrosion behaviour of MMCs with aluminium alloy matrix was presented. The corrosion characteristics of boron-, graphite-, silicon carbide-, alumina- and mica- reinforced aluminium MMCs were reviewed. The reinforcing phase influence on MMCs corrosion rate as well as on various corrosion forms (galvanic, pitting, stress corrosion cracking, corrosion fatique, tribocorrosion was discussed. Some corrosion protection methods of aluminium based MMCs were described

  18. Adhesive Bonding of Aluminium Alloy A5754 by Epoxy Resins

    Directory of Open Access Journals (Sweden)

    Ivan Michalec

    2013-01-01

    Full Text Available Joining thin sheets of aluminium and its alloys is a promising area in the field of joining materials. Nowadays, joining methods that do not melt the material itself are increasingly being utilised. This paper deals with adhesive bonding of aluminium alloy A5754 by two-component epoxy resins. Theresults show that joints bonded by Hysol 9466 have appropriate mechanical properties, but that joints bonded by Hysol 9492 have better thermal stability.

  19. A Reaction Coating on Aluminium Alloys by Laser Processing

    OpenAIRE

    1993-01-01

    An aluminium oxide layer of 100 µm in thickness has been successfully coated on aluminium alloy 6061 and pure aluminium using a powder mixture of silicon oxide and aluminium by laser processing. A strong Al/Al2O3 interface was formed. The exothermic chemical reaction between SiO2 and Al may promote the metal/oxide wetting and the formation of Al2O3 layer. This new approach of ceramic coating on metals using a chemical reaction of other ceramics with metals may be applied to other systems.

  20. A numerical analysis of empty and foam-filled aluminium conical tubes under oblique impact loading

    Science.gov (United States)

    Mat, Fauziah; Ismail, Khairul Azwan; Yaacob, Sazali

    2015-05-01

    In real impact applications, an energy absorber rarely sustains dynamic loading either axial or oblique but a combination of both. Established studies have proved that thin-walled tube is an excellent energy absorber under dynamic loading. Furthermore, the introduction of foam filling successfully enhanced the energy absorption capacity of thin-walled tube. However, the understanding of its response under oblique loading has yet been fully explored. Moreover, emerging in automotive industry has lead to increase interests on lightweight materials such as aluminium alloy. As such, this paper presents the crushing behaviour of empty and foam-filled aluminium alloy (AA6061-T6) conical tubes under oblique impact loading using a validated nonlinear finite element (FE) code, LS-DYNA. The study aims to assess the effect of foam filling on the energy absorption of AA6061-T6 tubes for variations in filler density. In fact, to the best of our knowledge, this study is the first attempt to evaluate a response of empty and foam-filled aluminum conical tube by using an experimentally validated model under oblique dynamic loading conditions. Good correlations between the numerical and experimental results were observed. The study show that initial peak force and the energy absorption increase with increasing filler density under axial and oblique loading. On the other hand, the effect of foam filling (0.534 g/cm3 aluminium foam filler) is less pronounced for the initial peak force under axial impact loading. Furthermore, the initial peak force and dynamic force of empty and foam-filled AA6061-T6 conical tubes decrease as the load angle increases from 0 deg to 20 deg hence reduces the energy absorption capacity.

  1. Local electrochemical behaviour of 7xxx aluminium alloys

    NARCIS (Netherlands)

    Andreatta, F.

    2004-01-01

    Aluminium alloys of the 7xxx series (Al-Zn-Mg-Cu) are susceptible to localized types of corrosion like pitting, intergranular corrosion and exfoliation corrosion. This represents a limitation for the application of these alloys in the aerospace components because localized corrosion might have a neg

  2. Development of Al-TiC Alloys Using Powder Metallurgy as Grain Refiners for Aluminium and Its Alloys

    Directory of Open Access Journals (Sweden)

    Abdel-Nasser .M. Omran

    2014-07-01

    Full Text Available Al-Ti-C master alloys have been widely investigated for many years as grain refiner for aluminium and its alloys. In this work, the Al-Ti-C master alloys are synthesized using powder metallurgy technique through the mixing of aluminium and TiC powders with different TiC contents 3.75 (3, 5(4, 6.25(5 and 7.5(6 Wt% TiC(Wt% Ti. The mixing powders with different contents of TiC were pressed in cylinder shape. The pressed specimens were sintered from 450 oC in a tube furnace under argon atmosphere for 2 hrs. The produced alloys before and after sintering are examined using SEM, EDX and XRD. The results indicate that, the Al-TiC alloy containing fine TiC particles dispersed in all matrix was successfully prepared. The prepared Al-TiC alloys with different contents of TiC were evaluated using the KBI test mold as grain refiner for pure aluminum and its alloys. The results indicate that the prepared Al-TiC master alloy is high grain refining efficiency for pure aluminum and its alloys.

  3. Incremental forming of aluminium alloys in cryogenic environment

    Science.gov (United States)

    Vanhove, Hans; Mohammadi, Amirahmad; Duflou, Joost R.

    2016-10-01

    Incremental Sheet Forming processes suffer from stringent forming limits, restricting the range of producible geometries. Through in-process cooling of the sheet to cryogenic level, this paper explores the potential of altering material properties benefiting the formability and residual hardness of different aluminium alloys. Global cooling of aluminium sheets with liquid nitrogen and dry ice allows to reach temperatures of 78K and 193K respectively. Extended with experiments at room temperature (293K), these tests form a base for comparison of surface quality, formability and residual hardness. As an aluminium alloy commonly used for its high strength to weight ratio, but suffering from limited formability compared to draw-quality steels, AA5083-H111 is of interest for cryogenic treatment. AA1050-H24 is included in the test campaign as a base for commercially pure aluminium.

  4. Metal-Ceramic Interfaces in Laser Coated Aluminium Alloys

    NARCIS (Netherlands)

    Zhou, X.B.; Hosson, J.Th.M. De

    1994-01-01

    A novel process was developed to firmly coat an aluminium alloy, Al6061, with α-Al2O3 by means of laser processing. In this approach a mixture of SiO2 and Al powder was used to inject in the laser melted surface of aluminium. A reaction product α-Al2O3 layer of a thickness of 100 µm was created whic

  5. China Rescinds the Export Tax on Aluminium Alloys Made by Scrap

    Institute of Scientific and Technical Information of China (English)

    2005-01-01

    <正>According to an official from the Tax Regulations Office under China’s State Council, from July 1st 2005, China will rescind the 5 per cent export tax on the aluminium alloys produced by using aluminium alloys scrap. An official from the State Council’s office said that through investigation they found that most aluminium alloys produced from aluminium scrap are not that energy consuming compared to primary aluminium. Starting from January 1st 2005, China decided to collect 5 per cent export tax on aluminium so as to control the industry development connected with high energy cost.

  6. Effects and mechanisms of grain refinement in aluminium alloys

    Indian Academy of Sciences (India)

    K T Kashyap; T Chandrashekar

    2001-08-01

    Grain refinement plays a crucial role in improving characteristics and properties of cast and wrought aluminium alloys. Generally Al–Ti and Al–Ti–B master alloys are added to the aluminium alloys to grain refine the solidified product. The mechanism of grain refinement is of considerable controversy in the scientific literature. The nucleant effects i.e. which particle and its characteristics nucleate -Al, has been the subject of intensive research. Lately the solute effect i.e. the effect of dissolved titanium on grain refinement, has come into forefront of grain refinement research. The present paper attempts to review the literature on the nucleant effects and solute effects on grain refinement and addresses the importance of dissolved titanium in promoting nucleation of -Al on nucleant particles.

  7. Steam generated conversion coating on aluminium alloys

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Jellesen, Morten Stendahl; Ambat, Rajan

    pressure steam produced by an autoclave at a temperature of 107 – 121 °C and pressure of 15 -17 psi for 10 minutes to produce a thin coating of aluminium oxide. The aim of this study is to understand the effect of high pressure steam with and without different chemical additives on surface morphology...

  8. Implants for surgery -- Metallic materials -- Part 3: Wrought titanium 6-aluminium 4-vanadium alloy

    CERN Document Server

    International Organization for Standardization. Geneva

    1996-01-01

    Specifies the characteristics of, and corresponding test methods for, the wrought titanium alloy known as titanium 6-aluminium 4-vanadium alloy (Ti 6-Al 4-V alloy) for use in the manufacture of surgical implants.

  9. TORSIONAL DEFORMATION AND FATIGUE BEHAVIOUR OF 6061 ALUMINIUM ALLOY

    Directory of Open Access Journals (Sweden)

    marini marno

    2012-02-01

    Full Text Available Torsional deformation and fatigue behaviour of both solid and thin-walled tubular specimens were made from as-received and heat treated 6061 aluminium alloy were studied. 6061 aluminium alloy have been widely used as a candidate material in automobile, aerospace, aircraft and structural application because of their superior mechanical properties such as high strength to weight ratio, good ductility and others. The differences in cyclic deformation and fatigue behaviours between round and solid specimens where a stress gradient exist, and thin-walled tubular specimens where a uniform stress state is commonly assumed, are also discussed. Von Mises and Tresca criteria has been used to predict the monotonic and cyclic deformation curve and compared to the torsional data obtained from the experiment. The S-N curve was used to present and evaluate the fatigue life of the specimens. Through fractographic analysis, failure criteria of fracture surfaces were observed and discussed. 

  10. Gas accumulation at grain boundaries during 800 MeV proton irradiation of aluminium and aluminium-alloys

    DEFF Research Database (Denmark)

    Singh, Bachu Narain; Horsewell, Andy; Sommer, W. F.;

    1986-01-01

    Samples of pure aluminium (99.9999%) and commercial Al-2.7%Mg(AlMg3) and Al-1.1%Mg-0.5%Si(Al6061) alloys were irradiated with 800 MeV protons at the Los Alamos Meson Physics Facility (LAMPF) at a temperature between 40-100°C to a maximum dose of 0.2 dpa. Transmission electron microscopy (TEM......) showed a complete absence of voids or bubbles in the grain interiors of the aluminium and the aluminium-alloys. Bubbles were clearly visible by TEM at grain boundaries in pure Al and the AlMg3 alloy; but bubbles were not visible in the Al6061 alloy. The bubble density in the AlMg3 alloy was considerably...

  11. Carbon treated commercial aluminium alloys as anodes for aluminium-air batteries in sodium chloride electrolyte

    Science.gov (United States)

    Pino, M.; Herranz, D.; Chacón, J.; Fatás, E.; Ocón, P.

    2016-09-01

    An easy treatment based in carbon layer deposition into aluminium alloys is presented to enhance the performance of Al-air primary batteries with neutral pH electrolyte. The jellification of aluminate in the anode surface is described and avoided by the carbon covering. Treated commercial Al alloys namely Al1085 and Al7475 are tested as anodes achieving specific capacities above 1.2 Ah g-1vs 0.5 Ah g-1 without carbon covering. The influence of the binder proportion in the treatment as well as different carbonaceous materials, Carbon Black, Graphene and Pyrolytic Graphite are evaluated as candidates for the covering. Current densities of 1-10 mA cm-2 are measured and the influence of the alloy explored. A final battery design of 4 cells in series is presented for discharges with a voltage plateau of 2 V and 1 Wh g-1 energy density.

  12. Recycling of Glass Fibre Reinforced Aluminium Laminates and Silicon Removal from Aerospace Al Alloy

    NARCIS (Netherlands)

    Zhu, G.

    2012-01-01

    Aerospace aluminium alloys (7xxx and 2xxx series Al alloy) is one of the important Al alloys in our life. The recycling of aerospace Al alloy plays a significant role in sustainable development of Al industry. The fibre reinforced metal laminates GLARE including 67 wt.% 2024 Al alloy was used as upp

  13. Investigation of The Amount of Energy Absorption of Aluminium Tube : Inversion and Concertina Collapse Mode

    Directory of Open Access Journals (Sweden)

    Mohd Suhairil Meon

    2012-01-01

    Full Text Available The objective of this study is to investigate the effect of variation of the tube length and the crosshead velocity on the amount of energy absorption of aluminium tubes (Al 6061 towards the inversion and concertina collapsed mode. The tests were performed on the Aluminium tubes using compression test apparatus according to ASTM E8 standard procedures. Two parameters that are included in the experiment were the crosshead velocity and tube length. The collected experimental data were organized and analysis of energy absorption was performed. Comparison was made to the values of energy absorption obtained from the experiments, and it was found that the energy absorbed by the Aluminium tube under inversion mode was increased by increasing the tube length as well as crosshead velocity. Results for the concertina type mode differ with inversion mode.

  14. Enhancement of wear and ballistic resistance of armour grade AA7075 aluminium alloy using friction stir processing

    OpenAIRE

    I. Sudhakar; V. Madhu; G. Madhusudhan Reddy; K. Srinivasa Rao

    2015-01-01

    Industrial applications of aluminium and its alloys are restricted because of their poor tribological properties. Thermal spraying, laser surfacing, electron beam welding are the most widely used techniques to alter the surface morphology of base metal. Preliminary studies reveal that the coating and layering of aluminium alloys with ceramic particles enhance the ballistic resistance. Furthermore, among aluminium alloys, 7075 aluminium alloy exhibits high strength which can be compared to tha...

  15. Hot Deformation Of 6xxx Series Aluminium Alloys

    Directory of Open Access Journals (Sweden)

    Mrówka-Nowotnik G.

    2015-06-01

    Full Text Available The hot deformation behavior of the 6xxx aluminum alloys was investigated by compression tests in the temperature range 100°C-375°C and strain rate range 10−4s−1 and 4×10−4s−1 using dilatometer DIL 805 BÄHR Thermoanalyse equipped with accessory attachment deformation allows the process to execute thermoplastic in vacuum and inert gas atmosphere. Associated microstructural changes of characteristic states of examined alloys were studied by using the transmission electron microscope (TEM. The results show that the stress level decreases with increasing deformation temperature and deformation rate. And was also found that the activation energy Q strongly depends on both, the temperature and rate of deformation. The results of TEM observation showing that the dynamic flow softening is mainly as the result of dynamic recovery and recrystallization of 6xxx aluminium alloys.

  16. Aluminium. II - A review of deformation properties of high purity aluminium and dilute aluminium alloys.

    Science.gov (United States)

    Reed, R. P.

    1972-01-01

    The elastic and plastic deformation behavior of high-purity aluminum and of dilute aluminum alloys is reviewed. Reliable property data, including elastic moduli, elastic coefficients, tensile, creep, fatigue, hardness, and impact are presented. Single crystal tensile results are discussed. Rather comprehensive reference lists, containing publications of the past 20 years, are included for each of the above categories. Defect structures and mechanisms responsible for mechanical behavior are presented. Strengthening techniques (alloys, cold work, irradiation, quenching, composites) and recovery are briefly reviewed.

  17. Optimal modifying and refining processes for A356 aluminium alloys

    Institute of Scientific and Technical Information of China (English)

    ZUO Xiu-rong; ZHONG Zhi-guo

    2006-01-01

    The influence of Ti, B, RE (cerium-rich mixtures of rare earth) and Sr, applied in modification and refining processes, on A356 aluminum alloys has been studied with the aids of OM, etc. The results show that the grain refining efficiency of Grain-Refining Aluminium Ingot (GRAI) and Al-Ti master alloys is similar. But the Ti addition from GRAI has lower costs than that with Al-Ti master alloys. So A356 aluminum alloys produced with GRAI are feasible in economy.Grain refining with GRAI with 0.01%Ti plus additional 0.03% B offers significant advantages over that from GRAI with 0.1% Ti only in A356 aluminum alloys, which made the dendrite α (Al) grain structure transform into equiaxed α (Al) grain structure, plus a partially modified eutectic silicon structure. RE addition to A356 aluminum alloys with Sr modifier is enable to achieve small DAS,reduced pores, well-refined fibrous silicon, small and dispersive eutectic colonies.

  18. Foaming of aluminium-silicon alloy using concentrated solar energy

    Energy Technology Data Exchange (ETDEWEB)

    Cambronero, L.E.G.; Ruiz-Roman, J.M. [Grupo de Materiales Hibridos, ETSIM-UPM, Madrid, Rios Rosas 21, 28003 Madrid (Spain); Canadas, I.; Martinez, D. [Plataforma Solar de Almeria, CIEMAT, P.O. Box 22, 04200 Tabernas (Almeria) (Spain)

    2010-06-15

    Solar energy is used for the work reported here as a nonconventional heating system to produce aluminium foam from Al-Si alloy precursors produced by powder metallurgy. A commercial precursor in cylindrical bars enclosed in a stainless-steel mould was heated under concentrated solar radiation in a solar furnace with varied heating conditions (heating rate, time, and temperature). Concentrated solar energy close to 300 W/cm{sup 2} on the mould is high enough to achieve complete foaming after heating for only 200 s. Under these conditions, the density and pore distribution in the foam change depending on the solar heating parameters and mould design. (author)

  19. Release Behaviour of Shock Loaded LY12 Aluminium Alloy

    Institute of Scientific and Technical Information of China (English)

    YAN Min; DAI Lan-Hong; SHEN Le-Tian

    2005-01-01

    @@ By making use of a light gas gun, a specially designed target is impacted by the LY12 flyer, and the pressure is taken in the range of 0.6-3 GPa. Based on the stress profiles measured in the buffer materials by manganese gauges, the Hugoniot curve and release curves of LY12 aluminium alloy are obtained. Meanwhile, the release curves from different initial shocked states are described in both the pressure-particle velocity plane and the pressure-specific volume plane.

  20. Role of acidic chemistries in steam treatment of aluminium alloys

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Jellesen, Morten Stendahl; Ambat, Rajan

    2015-01-01

    The effect of acidic chemistry on the accelerated growth of oxide on aluminium alloys Peraluman 706TM and AA6060 under exposure to high temperature steam was investigated. Studied chemistries were based on citrates and phosphates. Results showed that the presence of citrate and phosphate anions...... initiate doxide growth at the intermetallic particles while growth and corrosion performance of oxide was found tobe a function of anions type and their concentration. Further, steam treatment with phosphates exhibited better performance under acetic acid salt spray and filiform corrosion test whereas...

  1. The fracture of boron fibre-reinforced 6061 aluminium alloy

    Science.gov (United States)

    Wright, M. A.; Welch, D.; Jollay, J.

    1979-01-01

    The fracture of 6061 aluminium alloy reinforced with unidirectional and cross-plied 0/90 deg, 0/90/+ or - 45 deg boron fibres has been investigated. The results have been described in terms of a critical stress intensity, K(Q). Critical stress intensity factors were obtained by substituting the failure stress and the initial crack length into the appropriate expression for K(Q). Values were obtained that depended on the dimensions of the specimens. It was therefore concluded that, for the size of specimen tested, the values of K(Q) did not reflect any basic materials property.

  2. Outstanding inhibitive effect of colchicine on aluminium alloy 6061 corrosion

    Directory of Open Access Journals (Sweden)

    Mudigere Krishnegowda Pavithra

    2015-12-01

    Full Text Available The corrosion protection ability of colchicine (CC on Aluminium alloy 6061 (AA6061 in 3.5% NaCl medium was examined by potentiodynamic polarization, electrochemical impedance, and chronoamperometric techniques. About 99 % of protection efficiency was achieved by 2 mM concentration of CC in 3.5% NaCl solution.The adsorption of CC on AA6061 surface obeys Langmuir isotherm by following both physisorption and chemisorption mechanism. Variation in the surface morphology of inhibited and uninhibited metal samples was examined by scanning electron microscopy. 

  3. Fractographic analysis of fatigue damage in 7000 aluminium alloys.

    Science.gov (United States)

    Cvijović, Z; Vratnica, M; Gerić, K

    2008-12-01

    In this paper, an attempt is made to correlate the fatigue damage in 7000 aluminium alloys with different impurity contents to the microstructural features and to explain their interdependence through fractographic observations. The Paris constants of these alloys in the form of hot-forged plates subjected to the overaged T73 temper are evaluated and differences in the fatigue crack growth rate described by striation spacing measurements. Scanning electron microscopy analysis of fatigue fracture surfaces revealed that the type and morphological parameters of coarse intermetallic particles play a critical role in fatigue crack growth behaviour. The elemental distribution determined by means of energy-dispersive spectroscopy analysis showed that the fractured particles accelerating the crack advances are larger particles of Fe-rich phases. The fatigue crack growth rate increases considerably with increasing amounts of these particles. The smaller eta, S and Mg(2)Si particles contribute beneficially to fatigue life.

  4. Laser surface alloying of aluminium-transition metal alloys

    Directory of Open Access Journals (Sweden)

    Almeida, A.

    1998-04-01

    Full Text Available Laser surface alloying has been used as a tool to produce hard and corrosion resistant Al-transition metal (TM alloys. Cr and Mo are particularly interesting alloying elements to produce stable highstrength alloys because they present low diffusion coefficients and solid solubility in Al. To produce Al-TM surface alloys a two-step laser process was developed: firstly, the material is alloyed using low scanning speed and secondly, the microstructure is modified by a refinement step. This process was used in the production of Al-Cr, Al-Mo and Al-Nb surface alloys by alloying Cr, Mo or Nb powder into an Al and 7175 Al alloy substrate using a CO2 laser. This paper presents a review of the work that has been developed at Instituto Superior Tecnico on laser alloying of Al-TM alloys, over the last years.

    En el presente trabajo se estudia la aleación superficial mediante láser de aluminio con metales de transición. El cromo y el molibdeno son particularmente interesantes porque producen aleaciones de alta resistencia y por el bajo coeficiente de difusión y solución sólida en aluminio. Para producir estas aleaciones se ha seguido un procedimiento desarrollado en dos partes. En primer lugar, el material se alea usando una baja velocidad de procesado y en segundo lugar la estructura se modifica mediante un refinamiento posterior. Este procedimiento se ha empleado en la producción de aleaciones Al-Cr, Al-Mo y Al-Nb mediante aleación con láser de CO2 de polvos de Cr, Mo o Nb en aluminio y la aleación 7175. Este trabajo es una revisión del desarrollado en el Instituto Superior Técnico de Lisboa en los últimos años.

  5. Development of Zirconium alloys (for pressure tubes)

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Young Suk; Kwon, Sang Chul; Choo, Ki Nam; Jung, Chung Hwan; Yim, Kyong Soo; Kim, Sung Soo; Baek, Jong Hyuk; Jeong, Yong Hwan; Kim, Kyong Ho; Cho, Hae Dong [Korea Atomic Energy Research Inst., Daeduk (Korea, Republic of); Hwang, S. K.; Kim, M. H. [Inha Univ., Incheon (Korea, Republic of); Kwon, S. I [Korea Univ., Seoul (Korea, Republic of); Kim, I. S. [Korea Advanced Inst. of Science and Technology, Taejon (Korea, Republic of)

    1997-09-01

    The objective of this research is to set up the basic technologies for the evaluation of pressure tube integrity and to develop improved zirconium alloys to prevent pressure tube failures due to DHC and hydride blister caused by excessive creep-down of pressure tubes. The experimental procedure and facilities for characterization of pressure tubes were developed. The basic research related to a better understanding of the in-reactor performances of pressure tubes leads to noticeable findings for the first time : the microstructural effect on corrosion and hydrogen pick-up behavior of Zr-2.5Nb pressure tubes, texture effect on strength and DHC resistance and enhanced recrystallization by Fe in zirconium alloys and etc. Analytical methodology for the assessment of pressure tubes with surface flaws was set up. A joint research is being under way with AECL to determine the fracture toughness of O-8 at the EOL (End of Life) that had been quadruple melted and was taken out of the Wolsung Unit-1 after 10 year operation. In addition, pressure tube with texture controlled is being made along with VNINM in Russia as a joint project between KAERI and Russia. Finally, we succeeded in developing 4 different kinds of zirconium alloys with better corrosion resistance, low hydrogen pickup fraction and higher creep strength. (author). 121 refs., 65 tabs., 260 figs

  6. Electrolytic deposition of aluminium-magnesium-alloys from electrolytes containing organo-aluminium complexes; Elektrolytische Abscheidung von Aluminium-Magnesium-Legierungen aus aluminiumorganischen Komplexelektrolyten

    Energy Technology Data Exchange (ETDEWEB)

    Lehmkuhl, H.; Mehler, K.; Bongard, H.; Tesche, B. [Max-Planck-Institut fuer Kohlenforschung, Muelheim an der Ruhr (Germany); Reinhold, B. [Audi AG, Ingolstadt (Germany). Technische Entwicklung

    2000-10-01

    The galvanic deposition of pure aluminium from fluoride-containing electrolytes has been developed further and for the first time aluminium and magnesium have been deposited from a toluene-solution of a halide-free organo-aluminium complex electrolyte. The rate of incorporation of magnesium can be controlled over a wide range by either adjusting the composition of the aluminium-magnesium anode or by using separate aluminium or magnesium anodic circuits. The current efficiency for both anode and cathode approaches 100%. The resulting coating is optically attractive and, depending upon the magnesium-content or the cathodic current density, can be formed as a dull or polished surface. Investigations using an electron microscope show that the surface, in contrast to that of pure aluminium, consists of spherical particles. The aluminium-magnesium coating provides excellent protection against the corrosion of magnesium components. Electrochemical investigations using, for example 25% by weight magnesium incorporation, indicate a pronounced passivity interval compared to the alloy AZ91hp. In contrast to galvanic zinc-plated and silicate-sealed examples, cyclic corrosion tests on screws simulating 10 years of exposure, show no corrosion. (orig.)

  7. The influence of alloy composition on residual stresses in heat treated aluminium alloys

    Energy Technology Data Exchange (ETDEWEB)

    Robinson, J.S., E-mail: jeremy.robinson@ul.ie [Department of Mechanical, Aeronautical and Biomedical Engineering, University of Limerick (Ireland); Redington, W. [Materials and Surface Science Institute, University of Limerick (Ireland)

    2015-07-15

    The as quenched properties of eight different heat treatable aluminium alloys are related to residual stress magnitudes with the objective being to establish if there is a relationship between the residual stress and the as quenched alloy hardness and strength. Near surface residual stresses were assessed with X-ray diffraction using both the established sin{sup 2}ψ method and the more recent cos α technique. Through thickness residual stresses were also characterised using neutron diffraction. The alloys were chosen to encompass a wide range of strengths. The low to medium strength alloys were 6060 and 6082, medium to high strength 2618A, 2014A, 7075, 7010 and two variants of 7449, while the very high strength alloy was the powder metallurgy alloy N707. To assess the as quenched strength, dynamic hardness and tensile properties were determined from samples tested immediately after quenching to minimise the influence of precipitation hardening by natural aging. In addition, hot hardness measurements were made in situ on samples cooled to simulate quench paths. Within the experimental constraints of the investigation, the distribution of residual stress through the thickness was found to follow the same pattern for all the alloys investigated, varying from tensile in the interior to surface compression. The influence of alloy strength was manifested as a change in the observed residual stress magnitudes, and surface residual stresses were found to vary linearly with as quenched hardness and strength. - Highlights: • As quenched aluminium alloys contain high magnitude residual stresses. • Surface is compressive balance by a tensile core. • As quenched surface residual stress is linear function of alloy strength. • In situ hot hardness demonstrates rapid change in intrinsic hardness during rapid cooling.

  8. The role of magnesium in the electrochemical behaviour of 5XXX aluminium-magnesium alloys

    NARCIS (Netherlands)

    Flores Ramirez, J.R.

    2006-01-01

    An investigation concerning the effects of magnesium on the intergranular corrosion susceptibility of AA5XXX aluminium alloys was carried out. In the present work, magnesium is found to be highly mobile in the bulk metal as well as in the aluminium oxide. This mobility is also found to be dependent

  9. Domestic Output of Aluminium Alloy Hub Surpassing 70 million in 2007

    Institute of Scientific and Technical Information of China (English)

    2008-01-01

    <正>According to a report from the hub branch of China Association of Automobile Manufactur- ers,China has produced a total of more than 70 million aluminium alloy hubs in 2007,a year- on-year growth over 25%,while consuming over 700,000 tons of primary aluminium the whole year.

  10. Microstructure and interfaces of a reaction coating on aluminium alloys by laser processing

    NARCIS (Netherlands)

    Zhou, X.B.; Hosson, J.Th.M. De

    1993-01-01

    This paper reports an approach to coat a ceramic layer on aluminium alloys by means of chemical reaction. The reaction product of Al2O3 layer of 100 µm in thickness has been formed using a powder mixture of silicon oxide and aluminium by laser processing. It turns out that the large amount of heat f

  11. Cold compression residual stress reduction in aluminium alloy 7010

    Energy Technology Data Exchange (ETDEWEB)

    Tanner, D.A. [Limerick Univ. (Ireland). Materials Research Centre; Robinson, J.S. [Dept. of Materials Science and Technology, Univ. of Limerick (Ireland); Cudd, R.L. [HDA Forgings Ltd., Redditch, Worchestershire (United Kingdom)

    2000-07-01

    7010 is one of the high strength aluminium alloys used mainly as plate and forgings in the aerospace industry. Its high strength is achieved through a quenching operation where the material is rapidly cooled from the solution heat treatment temperature (475 C) to room temperature. As with all rapid quenching operations, residual stresses develop, leaving the material unsuitable for further machining operations and for service. Regular shaped forgings are generally cold compressed after quenching to relieve residual stresses. The effect of friction, increasing/decreasing the amount of cold compression and applying cold compression in 'bites' on residual stress magnitudes is unknown. This paper aims to study the effect that these variables have on final residual stress patterns through use of a finite element model. (orig.)

  12. The Relationship of Aluminium and Silver to Neural Tube Defects; a Case Control

    Directory of Open Access Journals (Sweden)

    María de Jesús Ramírez-Altamirano

    2012-09-01

    Full Text Available Objective: The purpose of this study was to identify the relationship of neurotoxic inorganic elements in the hair of patients with the diagnosis of Neural Tube Defects. Our initial hypothesis was that neurotoxic inorganic elements were associated with Neural Tube Defects.Methods: Twenty-three samples of hair from newborns were obtained from the General Hospital, “Aurelio Valdivieso” in the city of Oaxaca, Mexico. The study group included 8 newborn infants with neural tube pathology. The control group was composed of 15 newborns without this pathology. The presence of inorganic elements in the hair samples was determined by inductively-coupled plasma spectroscopy(spectroscopic emission of the plasma.Findings: The population of newborns with Neural Tube Defects showed significantly higher values of the following elements than the control group: Aluminium, Neural Tube Defects 152.77±51.06 μg/g, control group 76.24±27.89 μg/g; Silver, Neural Tube Defects 1.45±0.76, control group 0.25±0.53 μg/g; Potassium,Neural Tube Defects 553.87±77.91 μg/g, control group 341.13±205.90 μg/g. Association was found at 75 percentile between aluminium plus silver, aluminium plus potassium, silver plus potassium, and potassium plus sodium.Conclusion: In the hair of newborns with Neural Tube Defects, the following metals were increased:aluminium, silver. Given the neurotoxicity of the same, and association of Neural Tube Defects with aluminum and silver, one may infer that they may be participating as factors in the development of Neural Tube Defects.

  13. Recovery of actinides from actinide-aluminium alloys by chlorination: Part I

    OpenAIRE

    Cassayre, Laurent; Soucek, Pavel; Mendes, Eric; Malmbeck, Rikard; Nourry, Christophe; Eloirdi, Rachel; Glatz, Jean-Paul

    2011-01-01

    Pyrochemical processes in molten LiCl–KCl are being developed in ITU for recovery of actinides from spent nuclear fuel. The fuel is anodically dissolved to the molten salt electrolyte and actinides are electrochemically reduced on solid aluminium cathodes forming solid actinide–aluminium alloys. A chlorination route is being investigated for recovery of actinides from the alloys. This route consists in three steps: Vacuum distillation for removal of the salt adhered on the electrode, chlorina...

  14. Experimental study of impact energy absorption in aluminium square tubes with thermal triggers

    Directory of Open Access Journals (Sweden)

    Nuno Peixinho

    2012-04-01

    Full Text Available This study presents an approach for the improvement of crashworthiness properties of aluminium tubular structures using initiators introduced through localized heating. The main objective of this approach is to improve the ability to absorb impact energy in a progressive and controlled manner by a local modification of material properties. Through a localized heating in areas previously chosen for initiation, associated with the softening of the aluminium alloy the deformation can be introduced precisely, forcing the tubular structure to deform in a mode of high energy absorption and reducing the maximum load in a controlled manner. This study presents the properties for an aluminium alloy 6061-T5 modified by thermal treatment by the use of a laser beam. Experimental results are presented of quasi-static and impact tests of tubular structures using the proposed approach. This concept appears as possible and effective in the experimental work presented.

  15. Emeraldine base as corrosion protective layer on aluminium alloy AA5182, effect of the surface microstructure

    DEFF Research Database (Denmark)

    Cecchetto, L; Ambat, Rajan; Davenport, A.J.

    2007-01-01

    AA5182 aluminium alloy cold rolled samples were coated by thin Wlms of emeraldine base (EB) obtained from a 5% solution in N-methylpyrrolidinone. Accelerated corrosion tests prove this coating very eVective for corrosion protection of aluminium alloys in neutral environment. This study underlines......: • a weak redox activity of the polymer which passivate the metal, • a proton involving self-healing process taking place at the polymer–metal interface, which contributes to delay local acidiWcation in Wrst steps of corrosion on EB coated aluminium surfaces....

  16. Microstructure and properties of hot compacted powders of aluminium alloys.

    Science.gov (United States)

    Lityńska-Dobrzyńska, L; Dutkiewicz, J; Maziarz, W; Kanciruk, A

    2009-11-01

    Atomized 6061 aluminium alloy powders with and without the addition of 2 wt% Zr were milled for 80 h in a planetary ball mill and hot pressed in vacuum. The milled powders showed microhardness of about 170 HV, which increased after hot pressing up to 260 HV and up to 280 HV for powders without and with the Zr additions, respectively. Compression tests showed the high yield stress of 300 MPa obtained for the hot-pressed sample produced from the initial powders compared with ultimate compression strength of above 800 MPa for that of the milled sample and slightly higher for that with Zr additions. The effect of hot pressing on the structure of powders was investigated using a conventional analytical and high-resolution electron microscopy and high angle annular dark-field scanning transmission electron microscopy combined with energy dispersive X-ray microanalysis. The samples of initial powders hot pressed in vacuum showed a cell structure with particles of the Mg(2)Si and AlFeSi phases in intercell areas. In the milled and hot-pressed sample, the homogeneous structure of small grains of size below 200 nm was observed. The AlFeSi and Mg(2)Si particles with size 20-100 nm were uniformly distributed as well as the Zr rich particles in the Zr containing alloy. The Zr-rich particles containing up to 80 at% Zr were identified as a metastable fcc cubic phase with lattice parameter a= 0.48 nm.

  17. Pitting corrosion of A357 aluminium alloy obtained by semisolid processing

    Energy Technology Data Exchange (ETDEWEB)

    Bastidas, J.M.; Polo, J.L.; Torres, C.L. [National Centre for Metallurgical Research (CSIC), Madrid (Spain); Forn, A.; Baile, M.T. [Polytechnic Univ. of Catalonia, Vilanova i la Geltru (Spain)

    2001-09-01

    This paper studies the pitting corrosion of a structural component of A357 aluminium alloy obtained by a semisolid metal forming process. The mechanical properties of the A357 alloy were improved by applying standard heat treatments T5 and T6. Impedance measurements were conducted at the rest potential and polarisation curves were plotted using a 3% NaCl test solution. After polarisation experiments the specimens were analysed by scanning electron microscopy. The corrosion process is favoured through the eutectic regions. The results show that T6 heat treatment improved the corrosion resistance of the A357 aluminium alloy. (orig.)

  18. Mushy Zone Properties and Castability of Aluminium Foundry Alloys

    Energy Technology Data Exchange (ETDEWEB)

    Dahle, A.K.

    1996-01-01

    The growing application and market share of aluminium castings demand better understanding of the mechanisms of defect formation during casting. Although casting is a cost-effective production route, inadequate reproducibility and quality of the cast structure often restrict the utilization of castings. This doctoral thesis aims to (1) determine how the solidification conditions affect the rheological behaviour in the partially solidified state, (2) to measure how alterations in solidification variables influence castability, and (3) to investigate the relationship between mushy zone rheology and castability. The development of mechanical strength in the mushy zone was measured as a function of chemical composition. Measurements of the dendrite coherency point provided accurate determination of the point where the dendrite network is established. The strength measurements confirm that the dendrites are largely independent and free-floating before dendrite coherency. The point and rate of strength development in the subsequently established interdendritic network strongly depend on the size and morphology of the dendrites and fraction solid. The castability investigation was limited to evaluations of fluidity and feeding. Fluidity measurements showed a complex effect of increased grain refinement. Alterations of the concentration and type of main alloying element gave a direct relationship between mushy zone rheology and fluidity. The range of the operating feeding mechanisms during solidification is directly related to the rheological properties of the mushy zone. 251 refs., 77 refs., 25 tabs.

  19. Investigation of the properties of aluminium alloys used in the construction of nuclear research reactors

    Energy Technology Data Exchange (ETDEWEB)

    Hajewska, E. [Institute of Atomic Energy, Otwock-Swierk (Poland)

    1993-11-01

    In the paper there are described the results of the studies of the properties of aluminium alloys using in the construction of research reactors, especially of the Polish alloy PAR-1 which belongs to the group of Al-Mg-Si alloys. The influence of the heat treatment on structure of the alloy as well as on the mechanical and corrosion properties was studying. In the paper the results of some properties of PAR-1 alloy after irradiation were done. (author). 27 refs, 43 figs, 9 tabs.

  20. Process parameters optimization for friction stir welding of RDE-40 aluminium alloy using Taguchi technique

    Institute of Scientific and Technical Information of China (English)

    A.K.LAKSHMINARAYANAN; V.BALASUBRAMANIAN

    2008-01-01

    Taguchi approach was applied to determine the most influential control factors which will yield better tensile strength of the joints of friction stir welded RDE-40 aluminium alloy. In order to evaluate the effect of process parameters such as tool rotational speed, traverse speed and axial force on tensile strength of friction stir welded RDE-40 aluminium alloy, Taguchi parametric design and optimization approach was used. Through the Taguchi parametric design approach, the optimum levels of process parameters were determined. The results indicate that the rotational speed, welding speed and axial force are the significant parameters in deciding the tensile strength of the joint. The predicted optimal value of tensile strength of friction stir welded RDE-40 aluminium alloy is 303 MPa. The results were confirmed by further experiments.

  1. Void growth in high strength aluminium alloy single crystals: a CPFEM based study

    Science.gov (United States)

    Asim, Umair; Siddiq, M. Amir; Demiral, Murat

    2017-04-01

    High strength aluminium alloys that are produced through forming and joining processes are widely used in aerospace components. The ductile failure in these metals occurs due to the evolution and accumulation of microscopic defects, such as microvoids and shear bands. The present work investigates the underlying physical mechanisms during ductile failure by performing a rigorous, fully-validated, three-dimensional crystal plasticity, finite element study with aluminium alloy single crystals. Representative volume element (RVE) based simulations of single crystalline aluminium alloys (AA-5xxx) with different void geometries and orientations have been performed. Both local and nonlocal crystal plasticity constitutive models have been implemented in a finite element framework and are used to seek new insights into the interrelationships among void growth, initial porosity, initial void size, plastic anisotropy, and local/nonlocal size effects.

  2. Properties of the Aluminium Alloy EN AC-51100 after Laser Surface Treatment

    Directory of Open Access Journals (Sweden)

    Tański T.

    2016-03-01

    Full Text Available In this paper, the influence of a laser surface treatment on the structure and properties of aluminium alloy has been determined. The aim of this work was to improve the tribological properties of the surface layer of the EN AC-51100 aluminium alloy by simultaneously melting and feeding silicon carbide particles into the molten pool. The silicon carbide powder was introduced into the liquid metal using a gravity feeder within a constant feed rate of 1 g/min. A high power diode laser (HPDL was used for remelting. Laser beam energies used in experiments were 1.8 kW, 2.0 kW and 2.2 kW, combined with the constant velocity of 50 mm/min. As a result of the laser treatment on the aluminium alloy, a composite layer with greater hardness and wear resistance compared to the based material was obtained.

  3. The effect of heat treatment on the corrosion behaviour of 319 aluminium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Panagopoulos, C.N.; Georgiou, E.P.; Giannakopoulos, K.I. [Laboratory of Physical Metallurgy, National Technical University of Athens, Zografos, Athens (Greece)

    2009-06-15

    The effect of various heat treatments on the corrosion behaviour of 319 T1 cast aluminium alloy was investigated. From this alloy, specimens were heat treated in T5, T6 and two steps solution heat treatment T6 conditions and afterwards were subjected to electrochemical corrosion in a 0.1 M NaCl solution (pH = 12). From the above treatments, T5 heat treatment did not improve the corrosion resistance of the as-received alloy in contrast to T6 heat treatment which improved the corrosion resistance of the same alloy. However, two steps solutionizing T6 treatment showed the best corrosion resistance of the aluminium alloy. (Abstract Copyright [2009], Wiley Periodicals, Inc.)

  4. Production of FR Tubing from Advanced ODS Alloys

    Energy Technology Data Exchange (ETDEWEB)

    Maloy, Stuart Andrew [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Lavender, Curt [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Omberg, Ron [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Lewandowski, John [Case Western Reserve Univ., Cleveland, OH (United States)

    2016-10-25

    Significant research is underway to develop LWR nuclear fuels with improved accident tolerance. One of the leading candidate materials for cladding are the FeCrAl alloys. New alloys produced at ORNL called Gen I and Gen II FeCrAl alloys possess excellent oxidation resistance in steam up to 1400°C and in parallel methods are being developed to produce tubing from these alloys. Century tubing continues to produce excellent tubing from FeCrAl alloys. This memo reports receipt of ~21 feet of Gen I FeCrAl alloy tubing. This tubing will be used for future tests including burst testing, mechanical testing and irradiation testing.

  5. Collapse Behaviour and Energy Absorption of Aluminium Tubes Filled with Wood Sawdust

    Directory of Open Access Journals (Sweden)

    Raj Kiran

    2015-10-01

    Full Text Available Experiments on filled and empty circular thin walled Aluminium AA6063 tubes with varying L/D ratios have been performed to study load compression and energy absorbed for quasi static axial and oblique loading. Dependence of deformation characteristics and energy absorption responses have been studied. Energy absorption was measured from load-displacement graph obtained from UTM using MATLAB. Tubes were clamped at the lower end and axial and oblique loads were applied by applying a force at upper end with different angles to the centreline of column. Peak loads and absorbed energies have been compared for filled and empty tubes for same L/D ratio. Experimental results are used to determine energy absorption capacity due to plastic deformation of thin walled tube. The goal of the research was to study the interaction between the forming and crash response of Al AA6063 in order to evaluate its potential for use in vehicle design for crashworthiness.

  6. MICROSTRUCTURAL AND MECHANICAL STUDY OF ALUMINIUM ALLOYS SUBMITTED TO DISTINCT SOAKING TIMES DURING SOLUTION HEAT TREATMENT

    Directory of Open Access Journals (Sweden)

    Valmir Martins Monteiro

    2014-12-01

    Full Text Available This work studies the microstructural characteristics and mechanical properties for different aluminium alloys (1100, 3104 and 8011 hot rolled sheets that were subjected to a solution heat treatment with distinct soaking times, in order to promote microstructural and mechanical changes on these alloys with solute fractions slightly above the maximum solubility limit. Scanning Electronic Microscopy (SEM / Energy Dispersive Spectroscopy X-Ray (EDS, X-Ray Diffraction (XRD and Hardness Tests were employed to observe the microstructural / compositional and mechanical evaluation. For the 1100 and 8011 alloys the more suitable soaking time occur between 1 and 2 hours, and for the 3104 alloy occurs between 2 and 3 hours.

  7. Recovery of actinides from actinide-aluminium alloys by chlorination: Part II

    Science.gov (United States)

    Souček, P.; Cassayre, L.; Eloirdi, R.; Malmbeck, R.; Meier, R.; Nourry, C.; Claux, B.; Glatz, J.-P.

    2014-04-01

    A chlorination route is being investigated for recovery of actinides from actinide-aluminium alloys, which originate from pyrochemical recovery of actinides from spent metallic nuclear fuel by electrochemical methods in molten LiCl-KCl. In the present work, the most important steps of this route were experimentally tested using U-Pu-Al alloy prepared by electrodeposition of U and Pu on solid aluminium plate electrodes. The investigated processes were vacuum distillation for removal of the salt adhered on the electrode, chlorination of the alloy by chlorine gas and sublimation of the AlCl3 formed. The processes parameters were set on the base of a previous thermochemical study and an experimental work using pure UAl3 alloy. The present experimental results indicated high efficiency of salt distillation and chlorination steps, while the sublimation step should be further optimised.

  8. Evaluation of the mechanical properties of microarc oxidation coatings and 2024 aluminium alloy substrate

    CERN Document Server

    Xue Wen Bin; Deng Zhi Wei; Chen Ru Yi; Li Yong Liang; Zhang Ton Ghe

    2002-01-01

    A determination of the phase constituents of ceramic coatings produced on Al-Cu-Mg alloy by microarc discharge in alkaline solution was performed using x-ray diffraction. The profiles of the hardness, H, and elastic modulus, E, across the ceramic coating were determined by means of nanoindentation. In addition, a study of the influence of microarc oxidation coatings on the tensile properties of the aluminium alloy was also carried out. The results show that the H-and E-profiles are similar, and both of them exhibit a maximum value at the same depth of coating. The distribution of the alpha-Al sub 2 O sub 3 phase content determines the H- and E-profiles of the coatings. The tensile properties of 2024 aluminium alloy show less change after the alloy has undergone microarc discharge surface treatment.

  9. Steam assisted oxide growth on aluminium alloys using oxidative chemistries: Part II corrosion performance

    Science.gov (United States)

    Din, Rameez Ud; Jellesen, Morten Stendahl; Ambat, Rajan

    2015-11-01

    Surface treatment of aluminium alloys using steam with oxidative chemistries, namely KMnO4 and HNO3 resulted in accelerated growth of oxide on aluminium alloys. Detailed investigation of the corrosion performance of the treated surfaces was carried out using potentiodynamic polarisation and standard industrial test methods such as acetic acid salt spray (AASS) and filiform corrosion on commercial AA6060 alloy. Barrier properties of the film including adhesion were evaluated using tape test under wet and dry conditions. Electrochemical results showed reduced cathodic and anodic activity, while the protection provided by steam treatment with HNO3 was a function of the concentration of NO3- ions. The coating generated by inclusion of KMnO4 showed highest resistance to filiform corrosion. Overall, the performance of the steam treated surfaces under filiform corrosion and AASS test was a result of the local coverage of the alloy microstructure resulting from steam containing with KMnO4 and HNO3.

  10. Galvanic corrosion of rare earth modified AM50 and AZ91D magnesium alloys coupled to steel and aluminium alloys

    Energy Technology Data Exchange (ETDEWEB)

    Mohedano, M.; Arrabal, R.; Pardo, A.; Paucar, A.; Merino, M. C.; Matykina, E.; Mingo, B.; Garces, G.

    2014-04-01

    Electrochemical and gravimetric measurements were used to examine the effects of neodymium and gadolinium additions on the galvanic corrosion behaviour of AM50 and AZ91D magnesium alloys coupled to A 570 Gr 36 carbon steel and AA2011-AA6082 aluminium alloys. Rare earth modified alloys showed Al{sub 2}Nd/Al{sub 2}Gd and Al-Mn-Nd/Al-Mn-Gd intermetallics, reduced area fraction of {beta}-Mg{sub 1}7Al{sub 1}2 phase and increased corrosion resistance due to increased surface passivity and suppression of micro-galvanic couples. Neodymium and gadolinium additions improved the galvanic corrosion resistance of AM50 alloy, but were less effective in case of the AZ91D alloy. The AA6082 alloy was the most compatible material and the AA2011 alloy was the least compatible. (Author)

  11. Surface Chemistry of Aluminium Alloy Slid against Steel Lubricated by Organic Friction Modifier in Hydrocarbon Oil

    Directory of Open Access Journals (Sweden)

    Ichiro Minami

    2012-01-01

    Full Text Available The lubrication mechanism of aluminium alloy slid against steel was investigated from the standpoint of surface chemistry. Low friction and low wear were observed using glycerol mono-olate in a hydrocarbon as lubricant. Increase in the silicon content in the aluminium alloy during rubbing was observed by surface analyses using (1 Auger electron spectroscopy, (2 scanning electron microscopy along with energy dispersive X-ray spectroscopy, and (3 X-ray photoelectron spectroscopy. Mild removal of the passive state (aluminium oxide from the uppermost surface by the additive during the running-in process was proposed as the lubrication mechanism. The importance of additive chemistry that improves the running-in process was pointed out.

  12. Interface and microstructure characteristics of SiCp/2024 aluminium alloy composite

    Institute of Scientific and Technical Information of China (English)

    罗守靖; 姜巨福; 王迎; 藤东东; 祖丽君

    2003-01-01

    Electron microscope examination of the microstructure, interface and fracture surface of SiC particulatereinforced 2024 aluminium alloy composites produced by powder mixing and semi-solid extrusion process was pres-ented. The microstructure of SiCp/2024 composites fabricated by the present method is characterized by uniformlydistributed SiC particulates in well-densified matrix. Conventional transmission electron microscopy(TEM) revealsthe interface between the SiC particulates and the aluminium matrix. It is shown that this interface provides verystrong bonding which is further evidenced by the fractographic results, and that there is no apparent chemical reac-tion. Examination of the fracture surface indicates that the bonding strength between the SiC particulates and the a-luminium alloy matrix is stronger than that of the matrix. The dimples and tearing edges on the fracture surface ofcomposites are obviously observed.

  13. INVESTIGATION OF ECOLOGICAL SAFETY OF LUBRICATIONS FOR CASTING UNDER PRESSURE OF ALUMINIUM ALLOYS

    Directory of Open Access Journals (Sweden)

    A. M. Mihaltsov

    2008-01-01

    Full Text Available The investigations of environmental safety of different lubrications for moulds for casting under pressure of aluminium alloys are carried out. The method of carrying out of experiments on determination of harmful substances, escaping from lubrication in the process of destruction, is described.

  14. Characterization of steam generated anti-corrosive oxide films on Aluminium alloys

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Jellesen, Morten Stendahl; Ambat, Rajan

    2014-01-01

    alloy surfaces were exposed to high pressure steam produced by an autoclave at a temperature of 107 – 121 °C and pressure of 15 -17 psi for 10 minutes to produce a thin coating of aluminium oxide. The aim of this study is to understand the effect of high pressure steam with and without different...

  15. Steam assisted oxide growth on aluminium alloys using oxidative chemistries: Part I Microstructural investigation

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Piotrowska, Kamila; Gudla, Visweswara Chakravarthy;

    2015-01-01

    The surface treatment of aluminium alloys under steam containing KMnO4 and HNO3resulted in the formation of an oxide layer having a thickness of up to 825 nm. The use of KMnO4 and HNO3 in the steam resulted in incorporation of the respective chemical species into the oxide layer. Steam treatment ...

  16. Effect of Pulsed Current TIG Welding Parameters on Pitting Corrosion Behaviour of AA6061 Aluminium Alloy

    Institute of Scientific and Technical Information of China (English)

    T. Senthil Kumar; V. Balasubramanian; M. Y. Sanavullah; S. Babu

    2007-01-01

    Medium strength aluminium alloy (Al-Mg-Si alloy) has gathered wide acceptance in the fabrication of light weight structures requiring a high strength-to weight ratio, such as transportable bridge girders, military vehicles, road tankers and railway transport systems. The preferred welding process for aluminium alloy is frequently TIG (tungsten inert gas) welding due to its comparatively easier applicability and better economy.In the case of single pass TIG welding of thinner section of this alloy, the pulsed current has been found beneficial due to its advantages over the conventional continuous current process. The use of pulsed current parameters has been found to improve the mechanical properties of the welds compared to those of continuous current welds of this alloy due to grain refinement occurring in the fusion zone. A mathematical model has been developed to predict pitting corrosion potential of pulsed current TIG welded AA6061 aluminium alloy.Factorial experimental design has been used to optimize the experimental conditions. Analysis of variance technique has been used to find out the significant pulsed current parameters. Regression analysis has been used to develop the model. Using the developed model pitting corrosion potential values have been estimated for different combinations of pulsed current parameters and the results are analyzed in detail.

  17. Recovery of actinides from actinide-aluminium alloys by chlorination: Part I

    Science.gov (United States)

    Cassayre, L.; Souček, P.; Mendes, E.; Malmbeck, R.; Nourry, C.; Eloirdi, R.; Glatz, J.-P.

    2011-07-01

    Pyrochemical processes in molten LiCl-KCl are being developed in ITU for recovery of actinides from spent nuclear fuel. The fuel is anodically dissolved to the molten salt electrolyte and actinides are electrochemically reduced on solid aluminium cathodes forming solid actinide-aluminium alloys. A chlorination route is being investigated for recovery of actinides from the alloys. This route consists in three steps: Vacuum distillation for removal of the salt adhered on the electrode, chlorination of the actinide-aluminium alloys by chlorine gas and sublimation of the formed AlCl 3. A thermochemical study showed thermodynamic feasibility of all three steps. On the basis of the conditions identified by the calculations, experiments using pure UAl 3 alloy were carried out to evaluate and optimise the chlorination step. The work was focused on determination of the optimal temperature and Cl 2/UAl 3 molar ratio, providing complete chlorination of the alloy without formation of volatile UCl 5 and UCl 6. The results showed high efficient chlorination at a temperature of 150 °C.

  18. Cavitation-aided grain refinement in aluminium alloys

    NARCIS (Netherlands)

    Atamanenko, T.V.

    2010-01-01

    This thesis deals with grain refinement under the influence of ultrasonic-driven cavitation in aluminium casting processes. Three major goals of this research were: (1) to identify the mechanism of the cavitation-aided grain refinement at different stages of solidification; (2) to reveal the conditi

  19. Diamond turning and polishing tests on new RSP aluminium alloys

    NARCIS (Netherlands)

    Horst, R. ter; Haan, M. de; Gubbels, G.P.H.; Senden, R.; Venrooy, B.W.H. van; Hoogstrate, A.M.

    2012-01-01

    For years now conventional aluminium 6061 T6 has widely been used for mirrors in astronomical instruments, being diamond turned or since a few years also being optically polished. This allows the development of optical systems that can be tested and operated at any temperature, without being affecte

  20. Identification of monoclinic θ-phase dispersoids in a 6061 aluminium alloy

    Science.gov (United States)

    Buchanan, Karl; Ribis, Joël; Garnier, Jérôme; Colas, Kimberly

    2016-04-01

    Intermetallic dispersoids play an important role in controlling the 6xxx alloy series' grain distribution and increasing the alloy's toughness. The dispersoid distribution in a 6061 aluminium alloy (Al-Mg-Si) was analysed by transmission electron microscopy, selected area diffraction and energy-dispersive X-ray spectroscopy. The dispersoids had three unique crystal structures: simple cubic ?, body-centred cubic ? and monoclinic (C2/m). While the SC and BCC dispersoids have been well characterized in the literature, a detailed analysis of monoclinic dispersoids has not been presented. Therefore, the current work discusses the chemical composition, crystal structure and morphology of the monoclinic dispersoids.

  1. Gating System Design for Casting thin Aluminium Alloy (Al-Si) Plates

    OpenAIRE

    Victor ANJO; Reyaz KHAN

    2013-01-01

    The main problems caused by improper gating are entrained aluminium oxide films, cuts and washes, low casting yield and entrapped gas. This study describes the design of a gating system to produce thin Aluminium cast alloy plates of different sizes and thicknesses of 4mm, 6mm, 8mm, and 10mm using the non-pressurized gating with ratio of 1:4:4 and green sand moulding technique. The gating design was based on the laws of fluid mechanics and empirical rules of gating for non ferrous metals. The ...

  2. INVESTIGATION OF POWDER-GAS EMISSIONS, FONNED AT MELTING AND REFINING OF ALUMINIUM ALLOYS IN REVERBERATING FURNACES

    Directory of Open Access Journals (Sweden)

    S. P. Zadrutskij

    2009-01-01

    Full Text Available As a result of carried out analysis of processes of aluminium alloys casting and refining in reverberating  furnaces it is determined that searching source of harmful emissions are the refining processes.

  3. Application of artificial neural networks for modelling correlations in age hardenable aluminium alloys

    Directory of Open Access Journals (Sweden)

    F. Musharavati

    2010-07-01

    Full Text Available Purpose: This paper discusses some of the preliminary results of an ongoing research on the applications of artificial neural networks (ANNs in modelling, predicting and simulating correlations between mechanical properties of age hardenable aluminium alloys as a function of alloy composition.Design/methodology/approach: Appropriate combinations of inputs and outputs were selected for neural network modelling. Multilayer feedforward networks were created and trained using datasets from public literature. Influences of alloying elements, alloy composition and processing parameters on mechanical properties of aluminium alloys were predicted and simulated using ANNs models.Two sample t-tests were used to analyze the prediction accuracy of the trained ANNs.Findings: Good performances of the neural network models were achieved. The models were able to predict mechanical properties within acceptable margins of error and were able to provide relevant simulated data for correlating alloy composition and processing parameters with mechanical properties. Therefore, ANNs models are convenient and powerful tools that can provide useful information which can be used to identify desired properties in new aluminium alloys for practical applications in new and/or improved aluminium products.Research limitations/implications: Few public data bases are available for modelling properties. Minor contradictions on the experimental values of properties and alloy compositions were also observed. Future work will include further development of simulated data into property charts.Practical implications: Correlations between mechanical properties and alloy compositions can help in identifying a suitable alloy for a new or improved aluminum product application. In addition, availability of simulated structure-process-property data or charts assists in reducing the time and costs of trial and error experimental approaches by providing near-optimal values that can be used

  4. Laser beam welding of high strength aluminium-lithium alloys; Laserstrahlschweissen von hochfesten Aluminium-Lithium Legierungen

    Energy Technology Data Exchange (ETDEWEB)

    Enz, Josephin

    2012-07-01

    The present development in aircraft industry determined by the demand for a higher cost-effectiveness. Laser beam welding is one of the most promising joining technologies for the application in the aircraft industry through the considerable reduction of the production costs. Furthermore the weight of an aircraft structure can be reduced by the use of light and high strength aluminium alloys. This paper deals with the development of a process for the laser beam welding of a skin-stringer-joint where the Al-Li-alloy AA2196 is used as stringer material and the Al-Li-alloy AA2198 is used as skin and stringer material. By the use of design of experiments the optimal welding process parameters for different material combinations were determined which will be used for the welding of a 5-stringer panel. Therefore the weld seams of the joints were tested for irregularities and microstructural characteristics. In addition several mechanical tests were performed, which define the quality of the welded joint. Furthermore the influence of the oxide layer and the welding preparation on the welding performance was investigated. (orig.) [German] Die derzeitigen Entwicklungen im Flugzeugbau werden durch die allgemeine Forderung nach einer Steigerung der Wirtschaftlichkeit bestimmt. Das Laserstrahlschweissen ist dabei eines der vielversprechendsten Fuegeverfahren fuer die Anwendung im Flugzeugbau durch das die Herstellungskosten deutlich reduziert werden koennen. Zudem kann durch die Verwendung von leichten und hochfesten Aluminium-Legierungen das Gewicht einer Flugzeugstruktur zusaetzlich reduziert werden. Die vorliegende Arbeit befasst sich mit der Entwicklung eines Prozesses zum Laserstrahlschweissen einer Skin-Stringer-Verbindung aus den Aluminium-Lithium-Legierungen AA2196 (als Stringer-Werkstoff) und AA2198 (als Skin- und Stringer-Werkstoff). Unter Verwendung der statistischen Versuchsplanung wurden die optimalen Einstellungen der Schweissprozessparameter fuer die

  5. Impact toughness improvement of high strength aluminium alloy by intrinsic and extrinsic fracture mechanisms via hot roll bonding

    OpenAIRE

    Cepeda-Jiménez, C.M.; García-Infanta, J.M.; Pozuelo, M.; Ruano, Oscar Antonio; Carreño, Fernando

    2009-01-01

    A multilayer aluminium laminate comprising ten layers of Al-Zn-Mg-Cu alloy (82 vol.%) and nine layers of pure aluminium (18 vol.%) has been processed by hot rolling. The rolled laminate was characterized by electron backscattering diffraction, Charpy impact and shear tests. The multilayer laminate showed an outstanding Charpy impact toughness, being eighteen times higher than that for the as-received Al-Zn-Mg-Cu alloy. Damage tolerance improvement was due to the high volume fra...

  6. Deforming mechanism of non-mandrel drawing process of circular aluminium tube by simulation

    Institute of Scientific and Technical Information of China (English)

    QUAN Guo-zheng; ZHOU Jie; WANG Meng-han; QUAN Guo-hui; TONG Ying

    2006-01-01

    The aluminium tubes with high strength and smooth outer-surface can be produced by non-mandrel drawing process. It is an effective method to study forming mechanism of drawing process by simulation, based on which the relevant dies with reasonable dimensions can be designed to ensure tube precision. The dynamic model and elasto-plastic finite element model of the forming process were established based on FEM software Deform-3D, then the simulation was performed. The expressions about drawing load were deduced, and the influence of friction coefficient on drawing load was computed by the expressions and software respectively. Based on simulation results the deformation mechanism of drawing process without plug was expounded. According to flowing speed vector graph the law of material flowing was summarized, by which the deformation regions were partitioned.Furthermore, some potential problems of drawing process such as diameter shrinking, thickness varying were forecast and analyzed quantificationally.

  7. BEHAVIOUR OF COPPER AND ALUMINIUM ELECTRODES ON EDM OF EN-8 ALLOY STEEL

    Directory of Open Access Journals (Sweden)

    DHANANJAY PRADHAN

    2011-07-01

    Full Text Available Electrical discharge machining (EDM has been recognized as an efficient production method for precision machining of electrically conducting hardened materials. Copper and aluminium are used as electrode materials in this process with Kerosene oil as the dielectric medium. In this work, the behavior of copper and aluminium electrodes on electric discharge machining of EN-8 alloy steel had been studied. Keeping all other machining parameters same, the hardened work material was machined with the two electrodes at different values of peak current, pulse-on time & duty factor according to 23 full factorial design. It has been found that copper shows better results than aluminium in term of surface finish (μm in same dielectric media. Therefore, copper is recommended as a good electrode material.

  8. Steam assisted oxide growth on aluminium alloys using oxidative chemistries: Part I Microstructural investigation

    Science.gov (United States)

    Din, Rameez Ud; Piotrowska, Kamila; Gudla, Visweswara Chakravarthy; Jellesen, Morten Stendahl; Ambat, Rajan

    2015-11-01

    The surface treatment of aluminium alloys under steam containing KMnO4 and HNO3 resulted in the formation of an oxide layer having a thickness of up to 825 nm. The use of KMnO4 and HNO3 in the steam resulted in incorporation of the respective chemical species into the oxide layer. Steam treatment with solution containing HNO3 caused dissolution of Cu and Si from the intermetallic particles in the aluminium substrate. The growth rate of oxide layer was observed to be a function of MnO4- and NO3- ions present in the aqueous solution. The NO3- ions exhibit higher affinity towards the intermetallic particles resulting in poor coverage by the steam generated oxide layer compared to the coating formed using MnO4- ions. Further, increase in the concentration of NO3- ions in the solution retards precipitation of the steam generated aluminium hydroxide layer.

  9. Appearance of anodised aluminium: Effect of alloy composition and prior surface finish

    DEFF Research Database (Denmark)

    Aggerbeck, Martin; Canulescu, Stela; Dirscherl, Kai;

    2014-01-01

    Effect of alloy composition and prior surface finish on the optical appearance of the anodised layer on aluminium alloys was investigated. Four commercial alloys namely AA1050, Peraluman 706, AA5754, and AA6082 were used for the investigation. Microstructure and surface morphology of the substrate...... that the roughness of the as-etched surface increases with the degree of alloying due to second phase particles making the reflection more diffused, and that the as-etched surface morphology is similar to the oxide–substrate interface after anodising. Proper polishing is achieved on hard alloys and the glossy...... prior to anodising were analysed using scanning electron microscopy and atomic force microscopy. The optical appearance of the anodised surface with and without sealing was investigated using a photography setup, photospectrometry and bidirectional reflectance distribution function. It was found...

  10. Accelerated growth of oxide film on aluminium alloys under steam: Part I: Effects of alloy chemistry and steam vapour pressure on microstructure

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Gudla, Visweswara C.; Jellesen, Morten S.;

    2015-01-01

    at the top. The kinetics of formation of film understeamwas rapid; approx. 350nm thick layers were generated within 5 s of steam treatment, however increase in thickness of the oxide retarded further growth. The enrichment or depletion of different alloying elements at the surface of aluminium as a result...... of alkaline etching pre-treatment influenced the thickness and growth of theoxide. Moreover the steam treatment resulted in the partial oxidation of second phase intermetallic particles present in the aluminium alloy microstructure....

  11. Composite Ni-Co-fly ash coatings on 5083 aluminium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Panagopoulos, C.N., E-mail: chpanag@metal.ntua.gr [Laboratory of Physical Metallurgy, National Technical University of Athens, Zografos, 15780 Athens (Greece); Georgiou, E.P.; Tsopani, A.; Piperi, L. [Laboratory of Physical Metallurgy, National Technical University of Athens, Zografos, 15780 Athens (Greece)

    2011-03-15

    Ni-Co-fly ash coatings were deposited on zincate treated 5083 wrought aluminium alloy substrates with the aid of the electrodeposition technique. Structural and chemical characterization of the produced composite coatings was performed with the aid of X-ray diffraction (XRD), scanning electron microscopy (SEM) and electron dispersive X-ray analysis (EDS) techniques. The Ni-Co-fly ash coatings were found to consist of a crystalline Ni-Co solid solution with dispersed fly ash particles. In addition, chemical analysis of the Ni-Co matrix showed that it consisted of 80 wt.% Ni and 20 wt.% Co. The co-deposition of fly ash particles leads to a significant increase of the microhardness of the coating. The corrosion behaviour of the Ni-Co-fly ash/zincate coated aluminium alloy, in a 0.3 M NaCl solution (pH = 3.5), was studied by means of potentiodynamic corrosion experiments.

  12. Fatigue damage rule of LY12CZ aluminium alloy under sequential biaxial loading

    Science.gov (United States)

    Wang, YingYu; Zhang, DaChuan; Yao, WeiXing

    2014-01-01

    A series of biaxial two-level variable amplitude loading tests are conducted on smooth tubular specimens of LY12CZ aluminium alloy. The loading paths of 90° out-of-phase, 45° out-of-phase and 45° in-phase are utilized. The fatigue damage cumulative rules under two-level step loading of three loading paths are analyzed. By introducing a parameter α which is a function of the phase lag angle between the axial and the torsional loading, a new multiaxial nonlinear fatigue damage cumulative model is proposed. The proposed model is evaluated by the experimental data for two-level loading, multi-level loading of LY12CZ aluminium alloy, and multi-level loading of 45 steel. Fatigue lives predicted are within a factor of 2 scatter band.

  13. Effect of Process Parameters of Friction Stir Welded Joint for Similar Aluminium Alloys H30

    Directory of Open Access Journals (Sweden)

    Vanita S. Thete

    2015-05-01

    Full Text Available In this paper the effect of process parameters of friction stir welded joint for similar aluminium alloys H30 was studied. Taper cylindrical with three flutes all made of High speed steel was used for the friction stir welding (FSW aluminium alloy H30 and the tensile test of the welded joint were tested by universal testing method. The optimization done using detailed mathematical model is simulated by Minitab17. In this investigation, an effective approach based on Taguchi method, has been developed to determine the optimum conditions leading to higher tensile strength. Experiments were conducted on varying rotational speed, transverse speed, and axial force using L9 orthogonal array of Taguchi method. The present study aims at optimizing process parameters to achieve high tensile strength.

  14. RESEARCH OF FATIGUE AND MECHANICAL PROPERTIES AlMg1SiCu ALUMINIUM ALLOYS

    Directory of Open Access Journals (Sweden)

    Mária Mihaliková

    2015-11-01

    Full Text Available The paper is concerned with an analysis of utility and fatigue properties of industrially produced aluminium alloy, specifically EN AW 6061 (AlMg1SiCu, reinforced with the particles of SiC. The following properties were subject to evaluation: microstructure and sub-structure, mechanical characteristics. All of these mechanical properties in pre- and post- equal channel angular pressed (ECAP state have been studied. The hardness was evaluated by Vickers hardness test at the load of HV10. The significant part the thesis was devoted to the fatigue properties at cyclic load in torsion. The presented results demonstrate well that the combination of fractography and microscopy can give a significant contribution to the knowledge of initiation and propagation crack in the aluminium alloy.

  15. Braze Welding TIG of Titanium and Aluminium Alloy Type Al – Mg

    Directory of Open Access Journals (Sweden)

    Winiowski A.

    2016-03-01

    Full Text Available The article presents the course and the results of technological tests related to TIG-based arc braze welding of titanium and AW-5754 (AlMg3 aluminium alloy. The tests involved the use of an aluminium filler metal (Al99.5 and two filler metals based on Al-Si alloys (AlSi5 and AlSi12. Braze welded joints underwent tensile tests, metallographic examinations using a light microscope as well as structural examinations involving the use of a scanning electron microscope and an X-ray energy dispersive spectrometer (EDS. The highest strength and quality of welds was obtained when the Al99.5 filler metal was used in a braze welding process. The tests enabled the development of the most convenient braze welding conditions and parameters.

  16. Visual sensing of weld pool in variable polarity TIG welding of aluminium alloy

    Institute of Scientific and Technical Information of China (English)

    ZHANG Guang-jun; YAN Zhi-hong; WU Lin

    2006-01-01

    The passive visual sensing method was successfully applied to monitor the weld pool in TIG welding of aluminium alloy.In order to reduce the disturbance from the arc and acquire clear image, two techniques were used: one was the own-developed computer-controlled variable polarity power(VPP), the other was the composite filter technology. The VPP source did not have high-frequency electromagnetic interference from arc stabilizer in traditional AC welding power, and its output current wave was controlled by computer, so the imaging current and the imaging time could be adjusted easily. Filter spectral window was identified at 650 nm by analyzing the measured arc light spectral distribution. At the end, the high quality and clear images of welding pool of aluminium alloy were successfully acquired at low imaging current.

  17. High-temperature mechanical properties of aluminium alloys reinforced with boron carbide particles

    Energy Technology Data Exchange (ETDEWEB)

    Onoro, J. [Dept. Ingenieria y Ciencia de los Materiales, ETSI Industriales, Universidad Politecnica de Madrid, c/Jose Gutierrez Abascal 2, 28006 Madrid (Spain)], E-mail: javier.onoro@upm.es; Salvador, M.D. [Dept. Ingenieria Mecanica y de Materiales, ETSI Industriales, Universidad Politecnica de Valencia, Camino de Vera s/n, 46071 Valencia (Spain); Cambronero, L.E.G. [Dept. Ingenieria de Materiales, ETSI Minas, Universidad Politecnica de Madrid, c/Rios Rosas 21, 28003 Madrid (Spain)

    2009-01-15

    The mechanical properties of particulate-reinforced metal-matrix composites based on aluminium alloys (6061 and 7015) at high temperatures were studied. Boron carbide particles were used as reinforcement. All composites were produced by hot extrusion. The tensile properties and fracture analysis of these materials were investigated at room temperature and at high temperature to determine their ultimate strength and strain to failure. The fracture surface was analysed by scanning electron microscopy.

  18. Assessment of air pollutants produced by industrial activity from an aluminium alloys foundry

    Directory of Open Access Journals (Sweden)

    D. Cirtina

    2015-10-01

    Full Text Available The industrial activity in non-ferrous alloys foundries leads to the elimination of the pollutants in the atmosphere that may have adverse effects on the environment and human health. This paper presents an evaluation of the pollutantemissions resulting from an aluminium foundry starting from data on concentrations and pollutant massflow rates estimated for each phase of the technological process and on measured ambient levels for the area of influence of the objective to study.

  19. Micro-scale abrasion behaviour of electroless Ni-P-SiC coating on aluminium alloy

    OpenAIRE

    2014-01-01

    Electroless nickel (EN) and electroless nickel composite (ENC) coatings were deposited on aluminium alloy substrate, LM24. The micro abrasion test was conducted to study the wear behaviour of the coatings with the effect of SiC concentration. Microhardness of the coatings was tested also. The wear scars were analysed using optical microscope and scanning electron microscope (SEM). The wear resistance was found to be improved in composite coating that has higher microhardness as compared to pa...

  20. Heat input effect of friction stir welding on aluminium alloy AA 6061-T6 welded joint

    Directory of Open Access Journals (Sweden)

    Sedmak Aleksandar

    2016-01-01

    Full Text Available This paper deals with the heat input and maximum temperature developed during friction stir welding with different parameters. Aluminium alloy (AA 6061-T6 has been used for experimental and numerical analysis. Experimental analysis is based on temperature measurements by using infrared camera, whereas numerical analysis was based on empirical expressions and finite element method. Different types of defects have been observed in respect to different levels of heat input.

  1. Laser surface treatment of magnesium alloys with aluminium oxide powder

    Directory of Open Access Journals (Sweden)

    L.A. Dobrzański

    2009-11-01

    Full Text Available Purpose: The aim of this paper was to improve the magnesium cast alloys surface layer by laser surface treatment and to determine the laser treatment parameters.Design/methodology/approach: The laser treatment of magnesium alloys with alloying Al2O3 powder of the particle about 80μm was carried out using a high power diode laser (HPDL. The resulting microstructure in the modified surface layer was examined using scanning electron microscopy. Phase composition was determined by the X-ray diffraction method using the XPert device. The measurements of microhardness of the modified surface layer were also studied.Findings: The alloyed region has a fine microstructure with hard carbide particles. Microhardness of laser surface alloyed layer was significantly improved as compared to an alloy without laser treatment.Research limitations/implications: The investigations were conducted for cast magnesium alloys MCMgAl12Zn1, MCMgAl9Zn1, MCMgAl6Zn1, MCMgAl3Zn1 and Al2O3 powder of the particle size about 80 μm. One has used laser power in the range from 1.2to 2.0 kW.Practical implications: The results obtained in this investigation were promising comparing with the other conventional processes. High Power Diode Laser can be used as an economical substitute of Nd: YAG and CO2 to improve the surface magnesium alloy by feeding the carbide particles.Originality/value: The value of this paper is to define the influence of laser treatment parameters on quality, microstructure and microhardness of magnesium cast alloys surface layer.

  2. TEM and HRTEM studies of ball milled 6061 aluminium alloy powder with Zr addition.

    Science.gov (United States)

    Lityńska-Dobrzyńska, L; Dutkiewicz, J; Maziarz, W; Rogal, Ł

    2010-03-01

    The effect of mechanical alloying on the microstructure of atomized 6061 aluminium alloy powder and 6061 powder with a zirconium addition was studied in the work. The atomized 6061 aluminium alloy powder and 6061 powder with addition of 2 wt.% Zr were milled in a planetary ball mill and investigated using X-ray diffraction measurements, conventional and high-resolution electron microscopy (TEM/HRTEM) and high-angle annular dark field scanning transmission electron microscopy combined with energy dispersive X-ray microanalysis. An increase of stresses was observed in milled powders after the refinement of crystallites beyond 100 nm. In the powder with zirconium addition, some part of the Zr atoms diffused in aluminium forming a solid solution containing up to 0.5 wt.% Zr. The remaining was found to form Zr-rich particles containing up to 88 wt.% Zr and were identified as face centred cubic (fcc) phase with lattice constant a= 0.48 nm. That fcc phase partially transformed into the L1(2) ordered phase. Eighty-hour milling brought an increase of microhardness (measured with Vickers method) from about 50 HV (168 MPa) for the initial 6061 powder to about 170 HV (552 MPa). The addition of zirconium had no influence on the microhardness.

  3. THE EFFECT OF THE ALUMINIUM ALLOY SURFACE ROUGHNESS ON THE RESTITUTION COEFFICIENT

    Directory of Open Access Journals (Sweden)

    Stanisław Bławucki

    2015-08-01

    Full Text Available The paper presents the results of research on the effect of the surface roughness of aluminum alloy on its coefficient of restitution. It describes the current method of finishing the workpiece surface layer after cutting and innovative measuring device which was used in the research. The material used in the research was aluminium alloy EN AW 7075. The paper also presents a relationship between the coefficient of restitution and surface roughness of the milled samples as well as impressions left by bead in function of velocity and a sample surface roughness.

  4. Experimental and simulation studies on laser conduction welding of AA5083 aluminium alloys

    Science.gov (United States)

    Tobar, M. J.; Lamas, M. I.; Yáñez, A.; Sánchez-Amaya, J. M.; Boukha, Z.; Botana, F. J.

    In this paper, a three-dimensional numerical model was developed to study laser welding in an aluminium alloy (AA5083). The CFD model was used to solve the governing equations of conservation of mass, momentum and energy, so as to obtain the morphology, velocity field and temperature field of the melted zone in steady state. The predicted dimensions of the weld pool agreed well with experimental results obtained on laser conduction welding with a (CW) high power diode laser. The study allowed to determine the effect of different surface treatment (sandblasting, black painting) on the laser absorptivity of the alloy and analyze the heat transfer mechanism within the weld pool.

  5. Protection of 2024-T3 aluminium alloy by corrosion resistant phytic acid conversion coating

    Science.gov (United States)

    Shi, Hongwei; Han, En-Hou; Liu, Fuchun; Kallip, Silvar

    2013-09-01

    The corrosion protection properties of environmentally friendly phytic acid conversion coatings were studied on 2024-T3 aluminium alloy. The films were prepared under acidic conditions with various pH values and characterised by SEM, EDS, ATR-FTIR and electrochemical techniques. The results indicate that the conversion coatings obtained by immersing the alloy in phytic acid solutions at pH from 3 to 5.5 provide excellent corrosion resistance. ATR-FTIR confirms that the film is formed by deposition of reaction products between Al3+ and phosphate groups in phytic acid molecules. The conformation models of the deposition film are proposed.

  6. Aluminium Alloy AA6060 surface treatment with high temperature steam containing chemical additives

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Tabrizian, Naja; Jellesen, Morten S.

    2015-01-01

    The steam treatment process was employed to produce a conversion coating on aluminium alloy AA6060. The changes in microstructure and its effect on corrosion resistance properties were investigated. Various concentrations of KMnO4 containing Ce(NO3)3 was injected into the steam and its effect...... on the formation of steam-based conversion coating was evaluated. The use of Mn-Ce into the steam resulted in incorporation of these species into the conversion coating, which resulted in improved corrosion resistance of the alloy substrate....

  7. Microstructures and Properties of Aluminium-Magnesium Alloys with Additions of Manganese, Zirconium and Scandium

    OpenAIRE

    Johansen, Arve

    2000-01-01

    The present work reports on the effect of Mn-, Zr- and Sc-additions upon hot deformation properties, recrystallization properties and mechanical properties for different temper conditions of Al-Mg alloys. It can be stated that the addition of Mn, Zr and Sc improves the recrystallization properties and the mechanical properties of Al-Mg alloys. It should be emphasised that the precipitation of the metastable cubic Al3Zr and the stable cubic Al3(Sc,Zr) is favourable in an aluminium-magnesium ma...

  8. Microstructures and Properties of Aluminium-Magnesium Alloys with Additions of Manganese, Zirconium and Scandium

    OpenAIRE

    Johansen, Arve

    2000-01-01

    The present work reports on the effect of Mn-, Zr- and Sc-additions upon hot deformation properties, recrystallization properties and mechanical properties for different temper conditions of Al-Mg alloys.It can be stated that the addition of Mn, Zr and Sc improves the recrystallization properties and the mechanical properties of Al-Mg alloys. It should be emphasised that the precipitation of the metastable cubic Al3Zr and the stable cubic Al3(Sc,Zr) is favourable in an aluminium-magnesium mat...

  9. Fatigue behaviour of high strength AA 7012 aluminium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Di Russo, E.; Ragazzini, R.; Buratti, M.; Ferrarin, C. (Aluminia-ISML, Novara (Italy) Caproni Vizzola costruzioni aeronautiche, Somma Lombarda (Italy))

    1990-02-01

    The alloy 7012 (Al, 6.2% Zn, 2% Mg, 1% Cn, 0.13% Mn, 0.14% Zn, 0.04% Ti) belongs to the 7XXX family of high mechanical resistance alloys containing Zr as the principal additive. Produced in the form of extrusions, sheets and forgings, the alloy finds application in the defense, transportation and power industry fields. This paper presents the results of experimental fatigue tests (10/sup 7/ cycles) on 7020 in the T6 and T73 temper conditions and draws comparisons with corresponding test results on 7075 and 2024 type alloys. A comparative analysis of S-N curves obtained from plane bending and axial fatigue tests on smooth and notched specimens evidences the superior performance of 7020 in terms of higher strength and corrosion cracking resistance.

  10. A predictive fatigue life model for anodized 7050 aluminium alloy

    OpenAIRE

    Chaussumier, Michel; Mabru, Catherine; Shahzad, Majid; Chieragatti, Rémy; Rezaï-Aria, Farhad

    2013-01-01

    International audience; The objective of this study is to predict fatigue life of anodized 7050 aluminum alloy specimens. In the case of anodized 7050-T7451 alloy, fractographic observations of fatigue tested specimens showed that pickling pits were the predominant sites for crack nucleation and subsequent failure. It has been shown that fatigue failure was favored by the presence of multiple cracks. From these experimental results, a fatigue life predictive model has been developed including...

  11. Effect of Laser Feeding on Heat Treated Aluminium Alloy Surface Properties

    Directory of Open Access Journals (Sweden)

    Labisz K.

    2016-06-01

    Full Text Available In this paper are presented the investigation results concerning microstructure as well as mechanical properties of the surface layer of cast aluminium-silicon-copper alloy after heat treatment alloyed and/ or remelted with SiC ceramic powder using High Power Diode Laser (HPDL. For investigation of the achieved structure following methods were used: light and scanning electron microscopy with EDS microanalysis as well as mechanical properties using Rockwell hardness tester were measured. By mind of scanning electron microscopy, using secondary electron detection was it possible to determine the distribution of ceramic SiC powder phase occurred in the alloy after laser treatment. After the laser surface treatment carried out on the previously heat treated aluminium alloys, in the structure are observed changes concerning the distribution and morphology of the alloy phases as well as the added ceramic powder, these features influence the hardness of the obtained layers. In the structure, there were discovered three zones: the remelting zone (RZ the heat influence zone (HAZ and transition zone, with different structure and properties. In this paper also the laser treatment conditions: the laser power and ceramic powder feed rate were investigated. The surface laser structure changes in a manner, that there zones are revealed in the form of. This carried out investigations make it possible to develop, interesting technology, which could be very attractive for different branches of industry.

  12. Lubrication in Hot Tube Extrusion of Superalloys and Ti Alloys

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    Tubular products made of superalloys and titanium alloys usually work in high temperature environment and applied heavy loading. Hot extrusion is the best technology to form tubular billets with fine microstructures and good mechanical properties. Lubrication is one of the key techniques in hot extrusion, glass lubricants are most suitable for hot extrusion. Lubrication technique in hot extrusion is dealt with in this paper, the lubrication principle of hot tube extrusion is presented. Experiments of glass lubricated backward tube extrusion of titanium alloys and forward tube extrusion of superalloys are also discussed.

  13. The Effect of Laser Surface Treatment on Structure and Mechanical Properties Aluminium Alloy ENAC-AlMg9

    Directory of Open Access Journals (Sweden)

    Pakieła W.

    2016-09-01

    Full Text Available In this work, the influence of a high power diode laser surface treatment on the structure and properties of aluminium alloy has been determined. The aim of this study was to improve the mechanical and tribological properties of the surface layer of the aluminium alloy by simultaneously melting and feeding tungsten carbide particles into the molten pool. During the process was used high-power diode laser HPDL. In order to remelt the aluminium alloy surface the HPDL laser of 1.8, 2.0 and 2.2 kW laser beam power has been used. The linear laser scan rate of the beam was set 0.5 cm/s. In order to protect the liquid metal during laser treatment was used argon. As a base material was used aluminium alloy ENAC-AlMg9. To improve the surface mechanical and wear properties of the applied aluminium alloy was used biphasic tungsten carbide WC/W2C. The size of alloying powder was in the range 110-210 µm. The ceramic powder was introduced in the remelting zone by a gravity feeder at a constant rate of 8 g/m.

  14. Microstructure and Properties of Composite Coatings Obtained on Aluminium Alloys

    Directory of Open Access Journals (Sweden)

    Bara M.

    2016-09-01

    Full Text Available This paper presents methods of modifying the anode surface layers of Al2O3 by introducing carbon to their microstructure. Composite coatings were prepared using two different methods. In the first, coatings were formed by means of oxidation under constant current conditions. Anodic oxidation of aluminium was conducted in a multicomponent electrolyte with the addition of organic acids and graphite. The second method was based on the formation of oxide coatings in an electrolyte without the addition of graphite or heat treatment of the layers of succinic acid. The obtained coatings were tested using SEM, TEM, and GDOES (glow discharge optical emission spectrometry and their tribological and stereometric properties were measured. The study demonstrated the beneficial effects of the methods when used to improve the tribological properties of sliding couples.

  15. Corrosion behaviour of aluminium-magnesium alloys in molten sodium

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    The corrosion behaviour of the Al-1% Mg, A1-3% Mg, A1-5% Mg and A1-3% Mg-0.15%Zr alloys in moltensodium was investigated. The morphology of the corrosion products and the alloying element distribution of the specimenswere analyzed by using OM, SEM and EDS. The results showed that the effects of the magnesium content and the im-mersion temperature on the corrosion of the specimens are related to β phase (Mg5Al8).

  16. Experimental investigation of hardness of FSW and TIG joints of Aluminium alloys of AA7075 and AA6061

    Directory of Open Access Journals (Sweden)

    Chetan Patil

    2016-07-01

    Full Text Available This paper reports hardness testing conducted on welded butt joints by FSW and TIG welding process on similar and dissimilar aluminium alloys. FSW joints were produced for similar alloys of AA7075T651 and dissimilar alloys of AA7075T651- AA6061T6. The Friction stir welds of AA7075 & AA6061 aluminium alloy were produced at different tool rotational speeds of 650,700, 800, 900, 1000 and transverse speed of 30, 35, 40 mm/min. TIG welding was conducted along the rolling direction of similar and dissimilar aluminium plates. The Brinell hardness testing techniques were employed to conduct the tests; these tests were conducted on the welds to ascertain the joint integrity before characterization to have an idea of the quality of the welds

  17. A hybrid aluminium alloy and its zoo of interacting nano-precipitates

    Energy Technology Data Exchange (ETDEWEB)

    Wenner, Sigurd, E-mail: sigurd.wenner@ntnu.no [Department of Physics, NTNU, Høgskoleringen 5, NO-7491 Trondheim (Norway); Marioara, Calin Daniel; Andersen, Sigmund Jarle [Materials and Chemistry, SINTEF, Høgskoleringen 5, NO-7491 Trondheim (Norway); Ervik, Martin; Holmestad, Randi [Department of Physics, NTNU, Høgskoleringen 5, NO-7491 Trondheim (Norway)

    2015-08-15

    An alloy with aluminium as its base element is heat treated to form a multitude of precipitate phases known from different classes of industrial alloys: Al–Cu(–Mg), Al–Mg–Si–Cu, and Al–Zn–Mg. Nanometer-sized needle-shaped particles define the starting point of the phase nucleation, after which there is a split in the precipitation sequence into six phases of highly diverse compositions and morphologies. There are several unique effects of phases from different alloy systems being present in the same host lattice, of which we concentrate on two: the replacement of Ag by Zn on the Ω interface and the formation of combined plates of the θ′ and C phases. Using atomically resolved scanning transmission electron microscopy and energy-dispersive X-ray spectroscopy, we investigate the formation mechanisms, crystal structures and compositions of the precipitates. - Graphical abstract: Display Omitted - Highlights: • An aluminium alloy composition in-between the 2/6/7xxx systems was investigated. • Six different phases from the three systems coexist in an over-aged state. • All phases with 〈001〉{sub Al} coherencies can nucleate on 6xxx needle precipitates. • Modified theta′ and omega interfaces are observed.

  18. Analysis of wear properties of aluminium based journal bearing alloys with and without lubrication.

    Science.gov (United States)

    Mathavan, J. Joy; Patnaik, Amar

    2016-09-01

    Apart from classical bearing materials, Aluminium alloys are used as bearing materials these days because of their superior quality. In this analysis, new Aluminium based bearing materials, with filler metals Si, Ni, and Cr are prepared by metal mould casting in burnout furnace machine, and tribological properties of these alloys with and without lubrication were tested. The experiments for wear with lubrication are conducted on multiple specimen tester and experiments without lubrication is conducted on Pin on disk tribometer. The disc material used was SAE 1050 steel. Wear tests were conducted at a sliding speed of 0.785 m/s and at a normal load of 20 N. Coefficient of friction values, temperature changes and wear of the specimens were plotted on graph according to the above mentioned working conditions. Hardness and weight losses of the specimens were calculated. The obtained results demonstrate how the friction and wear properties of these samples have changed with the % addition of Silicon, Chromium and Nickel to the base metal aluminium.

  19. Study of surface interactions of ionic liquids with aluminium alloys in corrosion and erosion corrosion processes

    Science.gov (United States)

    Bermúdez, María-Dolores; Jiménez, Ana-Eva; Martínez-Nicolás, Ginés

    2007-06-01

    Surface interactions of alkylimidazolium ionic liquids (ILs) with aluminium alloy Al 2011 have been studied by immersion tests in seven neat ILs [1- n-alkyl-3-methylimidazolium X - (X = BF 4; n = 2 (IL1), 6 (IL2), 8 (IL3). X = CF 3SO 3; n = 2 (IL4). X = (4-CH 3C 6H 4SO 3); n = 2 (IL5). X = PF 6; n = 6 (IL6)] and 1-butyl-3-methylpyridinium bis(trifluoromethylsulfonyl)imide (IL7)]. Immersion tests for Al 2011 have also been carried out in 1 wt.% and 5 wt.% solutions of 1-ethyl,3-methylimidazolium tetrafluoroborate (IL1) in water. No corrosion of Al 2011 by neat ILs is observed. The highest corrosion rate for Al 2011 in water is observed in the presence of a 5 wt.% IL1 due to hydrolysis of the anion with hydrogen evolution and formation of aluminium fluoride. Erosion-corrosion processes have been studied for three aluminium alloys (Al 2011, Al 6061 and Al 7075) in a 90 wt.% IL1 solution in water in the presence of α-alumina particles. The erosion-corrosion rates are around 0.2 mm/year or lower, and increase with increasing copper content to give a corrosion resistance order of Al 6061 > Al 7075 > Al 2011. Results are discussed on the basis of scanning electron microscopy (SEM) observations, energy dispersive spectroscopy (EDS) analysis, X-ray diffraction (XRD) patterns and X-ray photoelectron spectroscopy (XPS) determinations.

  20. Gating System Design for Casting thin Aluminium Alloy (Al-Si Plates

    Directory of Open Access Journals (Sweden)

    Victor ANJO

    2013-11-01

    Full Text Available The main problems caused by improper gating are entrained aluminium oxide films, cuts and washes, low casting yield and entrapped gas. This study describes the design of a gating system to produce thin Aluminium cast alloy plates of different sizes and thicknesses of 4mm, 6mm, 8mm, and 10mm using the non-pressurized gating with ratio of 1:4:4 and green sand moulding technique. The gating design was based on the laws of fluid mechanics and empirical rules of gating for non ferrous metals. The equipments used for this experiment includes; a coal fired crucible furnace and an X-Ray machine. Materials used include; silica sand, clay, wood, glue and Aluminium alloy scraps. The experimental procedure involved: the gating design calculations, construction of wooden pattern and gating; using the wooden pattern and gating to produce the mould cavities and gating; melting, melt treatment and pouring of melt in the sand mould to produce the casting. The plate castings after removal from mould were visually examined for surface defects and after fettling and cleaning X-Ray radiography was used to find the internal soundness of the castings. From the results obtained in the experiment, it was found that there were no internal defects and quality castings were produced.

  1. Crack initiation and propagation paths in small diameter FSW 6082-T6 aluminium tubes under fatigue loading

    Directory of Open Access Journals (Sweden)

    Roberto Tovo

    2016-03-01

    Full Text Available This paper reports results of fatigue tests of friction stir welded (FSW aluminium tubes. Relatively small 38 mm diameter tubes were used and hence an automated FSW process using a retracting tool was designed for this project, as the wall thickness of the aluminium tube was similar to the diameter of the FSW tool. This is a more complex joint geometry to weld than the more usual larger diameter tube reported in the literature. S-N fatigue testing was performed using load ratios of R = 0.1 and R = -1. Crack path analysis was performed using both low magnification stereo microscopy and scanning electron microscopy, in order to identify crack initiation sites and to determine the direction of crack propagation. Work is still in progress to follow the crack path through the various microstructural zones associated with the weld. A simple statistical analysis was used to characterize the most typical crack initiation site. This work forms part of a wider project directed at determining multiaxial fatigue design rules for small diameter 6082-T6 aluminium tubes that could be of use in the ground vehicle industry.

  2. Effect of pulsed current welding on fatigue behaviour of high strength aluminium alloy joints

    Energy Technology Data Exchange (ETDEWEB)

    Balasubramanian, V. [Department of Manufacturing Engineering, Annamalai University, Annamalai Nagar 608 002, Tamil Nadu (India)], E-mail: visvabalu@yahoo.com; Ravisankar, V. [Department of Manufacturing Engineering, Annamalai University, Annamalai Nagar 608 002, Tamil Nadu (India); Madhusudhan Reddy, G. [Metal Joining Section, Defence Metallurgical Research Laboratory (DMRL), Kanchanbag (P.O), Hyderabad 560 058 (India)

    2008-07-01

    High strength aluminium alloys (Al-Zn-Mg-Cu alloys) have gathered wide acceptance in the fabrication of light weight structures requiring high strength-to weight ratio, such as transportable bridge girders, military vehicles, road tankers and railway transport systems. The preferred welding processes of high strength aluminium alloy are frequently gas tungsten arc welding (GTAW) process and gas metal arc welding (GMAW) process due to their comparatively easier applicability and better economy. Weld fusion zones typically exhibit coarse columnar grains because of the prevailing thermal conditions during weld metal solidification. This often results inferior weld mechanical properties and poor resistance to hot cracking. In this investigation, an attempt has been made to refine the fusion zone grains by applying pulsed current welding technique. Rolled plates of 6 mm thickness have been used as the base material for preparing single pass welded joints. Single V butt joint configuration has been prepared for joining the plates. The filler metal used for joining the plates is AA 5356 (Al-5Mg (wt%)) grade aluminium alloy. Four different welding techniques have been used to fabricate the joints and they are: (i) continuous current GTAW (CCGTAW), (ii) pulsed current GTAW (PCGTAW), (iii) continuous current GMAW (CCGMAW) and (iv) pulsed current GMAW (PCGMAW) processes. Argon (99.99% pure) has been used as the shielding gas. Fatigue properties of the welded joints have been evaluated by conducting fatigue test using rotary bending fatigue testing machine. Current pulsing leads to relatively finer and more equi-axed grain structure in gas tungsten arc (GTA) and gas metal arc (GMA) welds. In contrast, conventional continuous current welding resulted in predominantly columnar grain structures. Grain refinement is accompanied by an increase in fatigue life and endurance limit.

  3. The fatigue response of the aluminium-lithium alloy, 8090

    Science.gov (United States)

    Birt, M. J.; Beevers, C. J.

    1989-01-01

    The fatigue response of an Al-Li-Cu-Mg-Zr (8090) alloy has been studied at room temperature. The initiation and growth of small and long cracks has been examined at R = 0.1 and at a frequency of 100 Hz. Initiation was observed to occur dominantly at sub-grain boundaries. The growth of the small cracks was crystallographic in character and exhibited little evidence of retardation or arrest at the grain boundaries. The long crack data showed the alloy to have a high resistance to fatigue crack growth with underaging providing the optimum heat treatment for fatigue crack growth resistance. In general, this can be attributed to high levels of crack closure which resulted from the presence of extensive microstructurally related asperities.

  4. Surface morphology, composition and thermal behavior of tungsten-containing anodic spark coatings on aluminium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Lukiyanchuk, I.V.; Rudnev, V.S.; Kuryavyi, V.G.; Boguta, D.L.; Bulanova, S.B.; Gordienko, P.S

    2004-01-01

    Anodic spark coatings on aluminium alloy were prepared in aqueous electrolytes with sodium tungstate. The influence of boric acid addition in the electrolyte on the surface morphology, elemental and phase composition of the coatings was investigated. In both cases the coatings contained O, Al and W. The coatings obtained in electrolyte with boric acid and sodium tungstate contain also B at approximately 1 at.%. Scanning electron microscopy indicated that the coatings had three layers: the grey underlayer of anodic alumina, the second black layer of crystalline or amorphous aluminium tungstate agglomerated into fibers and the outer green layer of WO{sub 3}. It was proposed that isopoly- and heteropolyanions in the electrolyte used take part in the coating growth.

  5. Determination of lattice orientation in aluminium alloy grains by low energy gallium ion-channelling

    Science.gov (United States)

    Silk, Jonathan R.; Dashwood, Richard J.; Chater, Richard J.

    2010-06-01

    Polished sections of a fine-grained aluminium, silicon carbide metal matrix composite (MMC) alloy were prepared by sputtering using a low energy gallium ion source and column (FIB). The MMC had been processed by high temperature extrusion. Images of the polished surface were recorded using the ion-induced secondary electron emission. The metal matrix grains were distinguished by gallium ion-channelling contrast from the silicon carbide component. The variation of the contrast from the aluminium grains with tilt angle can be recorded and used to determine lattice orientation with the contrast from the silicon carbide (SiC) component as a reference. This method is rapid and suits site-specific investigations where classical methods of sample preparation fail.

  6. Enhancement of wear and ballistic resistance of armour grade AA7075 aluminium alloy using friction stir processing

    Directory of Open Access Journals (Sweden)

    I. Sudhakar

    2015-03-01

    Full Text Available Industrial applications of aluminium and its alloys are restricted because of their poor tribological properties. Thermal spraying, laser surfacing, electron beam welding are the most widely used techniques to alter the surface morphology of base metal. Preliminary studies reveal that the coating and layering of aluminium alloys with ceramic particles enhance the ballistic resistance. Furthermore, among aluminium alloys, 7075 aluminium alloy exhibits high strength which can be compared to that of steels and has profound applications in the designing of lightweight fortification structures and integrated protection systems. Having limitations such as poor bond integrity, formation of detrimental phases and interfacial reaction between reinforcement and substrate using fusion route to deposit hard particles paves the way to adopt friction stir processing for fabricating surface composites using different sizes of boron carbide particles as reinforcement on armour grade 7075 aluminium alloy as matrix in the present investigation. Wear and ballistic tests were carried out to assess the performance of friction stir processed AA7075 alloy. Significant improvement in wear resistance of friction stir processed surface composites is attributed to the change in wear mechanism from abrasion to adhesion. It has also been observed that the surface metal matrix composites have shown better ballistic resistance compared to the substrate AA7075 alloy. Addition of solid lubricant MoS2 has reduced the depth of penetration of the projectile to half that of base metal AA7075 alloy. For the first time, the friction stir processing technique was successfully used to improve the wear and ballistic resistances of armour grade high strength AA7075 alloy.

  7. Enhancement of wear and ballistic resistance of armour grade AA7075 aluminium alloy using friction stir processing

    Institute of Scientific and Technical Information of China (English)

    I. SUDHAKAR; V. MADHU; G. MADHUSUDHAN REDDY; K. SRINIVASA RAO

    2015-01-01

    Industrial applications of aluminium and its alloys are restricted because of their poor tribological properties. Thermal spraying, laser surfacing, electron beam welding are the most widely used techniques to alter the surface morphology of base metal. Preliminary studies reveal that the coating and layering of aluminium alloys with ceramic particles enhance the ballistic resistance. Furthermore, among aluminium alloys, 7075 aluminium alloy exhibits high strength which can be compared to that of steels and has profound applications in the designing of lightweight fortification structures and integrated protection systems. Having limitations such as poor bond integrity, formation of detrimental phases and interfacial reaction between reinforcement and substrate using fusion route to deposit hard particles paves the way to adopt friction stir processing for fabricating surface composites using different sizes of boron carbide particles as reinforcement on armour grade 7075 aluminium alloy as matrix in the present investigation. Wear and ballistic tests were carried out to assess the performance of friction stir processed AA7075 alloy. Significant improvement in wear resistance of friction stir processed surface composites is attributed to the change in wear mechanism from abrasion to adhesion. It has also been observed that the surface metal matrix composites have shown better ballistic resistance compared to the substrate AA7075 alloy. Addition of solid lubricant MoS2 has reduced the depth of penetration of the projectile to half that of base metal AA7075 alloy. For the first time, the friction stir processing technique was successfully used to improve the wear and ballistic resistances of armour grade high strength AA7075 alloy.

  8. Further studies of the anodic dissolution in sodium chloride electrolyte of aluminium alloys containing tin and gallium

    Science.gov (United States)

    Nestoridi, Maria; Pletcher, Derek; Wharton, Julian A.; Wood, Robert J. K.

    As part of a programme to develop a high power density, Al/air battery with a NaCl brine electrolyte, the high rate dissolution of an aluminium alloy containing tin and gallium was investigated in a small volume cell. The objective was to define the factors that limit aluminium dissolution in condition that mimic a high power density battery. In a cell with a large ratio of aluminium alloy to electrolyte, over a range of current densities the extent of dissolution was limited to ∼1000 C cm -2 of anode surface by a thick layer of loosely bound, crystalline deposit on the Al alloy anode formed by precipitation from solution. This leads to a large increase in impedance and acts as a barrier to transport of ions.

  9. Further studies of the anodic dissolution in sodium chloride electrolyte of aluminium alloys containing tin and gallium

    Energy Technology Data Exchange (ETDEWEB)

    Nestoridi, Maria; Pletcher, Derek [The School of Chemistry, University of Southampton, Highfield, Southampton SO17 1BJ (United Kingdom); Wharton, Julian A.; Wood, Robert J.K. [School of Engineering Sciences, The University, Southampton SO17 1BJ (United Kingdom)

    2009-09-05

    As part of a programme to develop a high power density, Al/air battery with a NaCl brine electrolyte, the high rate dissolution of an aluminium alloy containing tin and gallium was investigated in a small volume cell. The objective was to define the factors that limit aluminium dissolution in condition that mimic a high power density battery. In a cell with a large ratio of aluminium alloy to electrolyte, over a range of current densities the extent of dissolution was limited to {proportional_to}1000 C cm{sup -2} of anode surface by a thick layer of loosely bound, crystalline deposit on the Al alloy anode formed by precipitation from solution. This leads to a large increase in impedance and acts as a barrier to transport of ions. (author)

  10. Experimental and theoretical investigation on corrosion inhibition of AA5052 aluminium alloy by L-cysteine in alkaline solution

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Dapeng; Gao, Lixin [School of Environmental and Chemical Engineering, Shanghai University of Electric Power, Shanghai 200090 (China); Zhang, Daquan, E-mail: zhangdaquan@shiep.edu.cn [School of Environmental and Chemical Engineering, Shanghai University of Electric Power, Shanghai 200090 (China); Yang, Dong [School of Environmental and Chemical Engineering, Shanghai University of Electric Power, Shanghai 200090 (China); Wang, Hongxia; Lin, Tong [Institute for Frontier Materials, Deakin University, Geelong, VIC 3216 (Australia)

    2016-02-01

    The corrosion inhibition of L-cysteine on AA5052 aluminium alloy in 4 mol/L NaOH solution was investigated by hydrogen gas evolution experiment, polarisation curve, galvanostatic discharge, electrochemical impedance spectroscopy measurements and quantum chemical calculations. The adsorption of L-cysteine on aluminium alloy surface obeyed the amended Langmuir's adsorption isotherm. The polarisation curves indicated that L-cysteine acted as a cathodic inhibitor to inhibit cathodic reaction. The inhibition mechanism was dominated by the geometric covering effect. The galvanostatic discharge shows that the additives restrain the hydrogen evolution and increase the anodic utilization rate. Quantum chemical calculations indicated that L-cysteine molecules mainly interacted with on the carboxyl groups on the aluminium alloy surface. A strong hybridization occurred between the s-orbital and p-orbital of reactive sites in the L-cysteine molecule and the sp-orbital of Aluminium. - Highlights: • L-cysteine was used as corrosion inhibitor for Al alloy in alkaline solution. • Adsorption of L-cysteine on Al alloy surface obeyed the amended Langmuir's isotherm. • L-cysteine molecules interacted with the carboxyl groups on the Al alloy surface. • A strong orbital hybridization occurred between the reactive sites in L-cysteine and Al.

  11. Modelling the processing of aluminium alloys in the semi-solid state

    Energy Technology Data Exchange (ETDEWEB)

    Wahlen, A. [ARC Leichtmetallkompetenzzentrum Ranshofen GmbH, Ranshofen (Austria)

    2002-07-01

    Thixoforming, an innovative technique in which metals are formed in their semi-solid state, permits the cost-efficient production of components with improved properties and performance compared to conventional pressure die casting. Since this process is still relatively new, great technical advances can be expected in the near future. These advances should allow production of near-net-shape components with good mechanical properties, combined with low manufacturing cost. Due to the distinct thixotropic flow pattern of the semi-solid slurry, high production speeds similar to those of conventional pressure die casting can be achieved, yet the disadvantages of the latter are eliminated: thixoformed components possess a good combination of strength and ductility, and they are heat-treatable and weldable. The requirement for thixotropic flow behaviour is a particular microstructure in the semi-solid state. At the onset of forming, the solid phase of the material must exhibit a globular morphology, a feature that can be produced with a novel casting technique called new rheocasting (NRC). Cast billets of several aluminium alloys and resulting microstructures show the feasibility of the chosen process variant. Constitutive models for the distinct flow behaviour of thixotropic aluminium alloys in the semi-solid state are derived with respect to temperature, strain rate and microstructure. Experimental techniques such as deformation tests, backward extrusion experiments, differential thermal analysis and quantitative metallurgy provide the necessary data to calibrate the materials models. For the implementation in a special-purpose FE software package, constitutive models for the thixotropic flow stress, the specific thixotropic flow stress, the specific heat capacity and the thermal conductivity of cast and wrought aluminium alloys in the semi-solid state are provided. For the optimization of the thixoforming manufacturing process these models were implemented in the FE

  12. Prediction of flow stress of 7017 aluminium alloy under high strain rate compression at elevated temperatures

    Institute of Scientific and Technical Information of China (English)

    Ravindranadh BOBBILI; B. RAMAKRISHNA; V. MADHU; A.K. GOGIA

    2015-01-01

    An artificial neural network (ANN) constitutive model and JohnsoneCook (JeC) model were developed for 7017 aluminium alloy based on high strain rate data generated from split Hopkinson pressure bar (SHPB) experiments at various temperatures. A neural network configuration consists of both training and validation, which is effectively employed to predict flow stress. Temperature, strain rate and strain are considered as inputs, whereas flow stress is taken as output of the neural network. A comparative study on JohnsoneCook (JeC) model and neural network model was performed. It was observed that the developed neural network model could predict flow stress under various strain rates and tem-peratures. The experimental stressestrain data obtained from high strain rate compression tests using SHPB over a range of temperatures (25?e300 ?C), strains (0.05e0.3) and strain rates (1500e4500 s?1) were employed to formulate JeC model to predict the flow stress behaviour of 7017 aluminium alloy under high strain rate loading. The JeC model and the back-propagation ANN model were developed to predict the flow stress of 7017 aluminium alloy under high strain rates, and their predictability was evaluated in terms of correlation coefficient (R) and average absolute relative error (AARE). R and AARE for the J-C model are found to be 0.8461 and 10.624%, respectively, while R and AARE for the ANN model are 0.9995 and 2.58%, respectively. The predictions of ANN model are observed to be in consistent with the experimental data for all strain rates and temperatures.

  13. Accelerated growth of oxide film on aluminium alloys under steam: Part II: Effects of alloy chemistry and steam vapour pressure on corrosion and adhesion performance

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Bordo, Kirill; Jellesen, Morten Stendahl;

    2015-01-01

    The steam treatment of aluminium alloys with varying vapour pressure of steamresulted in the growth of aluminium oxyhydroxide films of thickness range between 450 - 825nm. The surface composition, corrosion resistance, and adhesion of the produced films was characterised by XPS, potentiodynamic...... of the vapour pressure of the steam. The accelerated corrosion and adhesion tests on steam generated oxide films with commercial powder coating verified that the performance of the oxide coating is highly dependent on the vapour pressure of the steam....

  14. SOLIDIFICATION CHARACTERISTIC OF TITANIUM CARBIDE PARTICULATE REINFORCED ALUMINIUM ALLOY MATRIX COMPOSITES

    Directory of Open Access Journals (Sweden)

    N. FATCHURROHMAN

    2012-04-01

    Full Text Available In this research solidification characteristic of metal matrix composites consisted of titanium carbide particulate reinforced aluminium-11.8% silicon alloy matrix is performed. Vortex mixing and permanent casting method are used as the manufacturing method to produce the specimens. Temperature measurements during the casting process are captured and solidification graphs are plotted to represent the solidification characteristic. The results show, as volume fraction of particulate reinforcement is increased, solidification time is faster. Particulate reinforcement promotes rapid solidification which will support finer grain size of the casting specimen. Hardness test is performed and confirmed that hardness number increased as more particulate are added to the system.

  15. ANN & ANFIS Models for Prediction of Abrasive Wear of 3105 Aluminium Alloy with Polyurethane Coating

    Directory of Open Access Journals (Sweden)

    H. Alimam

    2016-06-01

    Full Text Available The quest for safety and reliability has increased significantly after Industrial revolution, so is the case for coating industries. In this paper 3105 Aluminium alloy sheet is coated with organic polyurethane coating. After the implementation of coating, various processes are undergone to check its reliability under elevated conditions. ANN & ANFIS model were developed and trained with an objective to find abrasive wear during the process. ANN & ANFIS model were compared with the experimental results. It is observed that the abrasive wear of a coated specimen can be predicted accurately and precisely using ANN and ANFIS models.

  16. Parametric study of friction stir spot welding of aluminium alloy 5754

    Directory of Open Access Journals (Sweden)

    D. Klobčar

    2014-01-01

    Full Text Available The paper presents a parametric analysis of friction stir spot welding (FSSW of aluminium alloy 5754 in a lap joint. Experimental plan was done according to the response surface methodology (RSM, where tool rotation speed varied between 988 and 3511 rpm, plunge rate between 24,4 and 150 mm/min and dwell time between 1 and 3,5s. The plunge depth was held constant at 0,4 mm. The welds were tensile-shear tested and the microstructure was analysed. Mathematical models describing the relationship between welding parameters and spot strength, axial force and rotational moment were developed and the optimal FSSW parameters were found.

  17. A vertical type twin roll caster for an aluminium alloy clad strip

    OpenAIRE

    T. Haga; Nakamura, R; Kuma, S; H. Watari

    2013-01-01

    Purpose: of this paper: Twin roll casters that can cast two layers and three layers clad strip of aluminium alloys were invented. One of the purposes of this paper is to report that the two layers and three layers clad strip could be cast by the twin roll caster of this study. The investigation of the characters of these casters and the clad strips was purpose of this paper, too. The connecting at the interface between the strips was most important in the casting of the clad strip. Therefore,...

  18. Grain refining of aluminium alloys and silicon by means of boron-nitride particles

    Energy Technology Data Exchange (ETDEWEB)

    Wulf, Eric; Seitz, Jan-Marten; Schaper, Mirko; Bach, Friedrich-Wilhelm [Leibniz Univ. of Hannover, Garbsen (Germany). Inst. of Materials Science; Alphei, Lukas David; Westphal, David; Becker, Joerg August; Feldhoff, Armin [Leibniz Univ. of Hannover, Garbsen (Germany). Inst. of Physical Chemistry and Electrochemistry

    2013-03-15

    Investigations were carried out to grain refine the aluminium alloys Al-6Si (all compositions given in wt.%) and Al-12Si as well as pure silicon by means of inoculation using boron nitride nano-particles. Comparative tests were performed using both conventional grain refiners based on titanium as well as without inoculants. Analyses were performed using scanning electron microscopy, tensile testing, thermographic and metallographic techniques. In doing this, a significant effect on grain refining is verified by inoculating using boron nitride which exceeds the effect of conventional grain refiners. (orig.)

  19. Investigation of photocatalytic activity of titanium dioxide coating deposited on aluminium alloy substrate by plasma technique

    DEFF Research Database (Denmark)

    Daviðsdóttir, Svava; Soyama, Juliano; Dirscherl, Kai

    2011-01-01

    Nowadays, there is an increased need for functionalized surfaces with self-cleaning and antibacterial properties. Titanium dioxide (TiO2) in the anatase crystalline structure is one of the most powerful photocatalytic materials available today, which can provide above functionalities....... Literature consists of large number of publications on titanium dioxide coating for self-cleaning applications, with glass as the main substrate. Only little work is available on TiO2 coating of metallic alloys used for engineering applications. Engineering materials, such as light-weight aluminium and steel...

  20. Research of aluminium alloy aerospace structure aperture measurement based on 3D digital speckle correlation method

    Science.gov (United States)

    Bai, Lu; Wang, Hongbo; Zhou, Jiangfan; Yang, Rong; Zhang, Hui

    2014-11-01

    In this paper, the aperture change of the aluminium alloy aerospace structure under real load is researched. Static experiments are carried on which is simulated the load environment of flight course. Compared with the traditional methods, through experiments results, it's proved that 3D digital speckle correlation method has good adaptability and precision on testing aperture change, and it can satisfy measurement on non-contact,real-time 3D deformation or stress concentration. The test results of new method is compared with the traditional method.

  1. Influence of Process Parameters on the Quality of Aluminium Alloy EN AW 7075 Using Selective Laser Melting (SLM)

    Science.gov (United States)

    Kaufmann, N.; Imran, M.; Wischeropp, T. M.; Emmelmann, C.; Siddique, S.; Walther, F.

    Selective laser melting (SLM) is an additive manufacturing process, forming the desired geometry by selective layer fusion of powder material. Unlike conventional manufacturing processes, highly complex parts can be manufactured with high accuracy and little post processing. Currently, different steel, aluminium, titanium and nickel-based alloys have been successfully processed; however, high strength aluminium alloy EN AW 7075 has not been processed with satisfying quality. The main focus of the investigation is to develop the SLM process for the wide used aluminium alloy EN AW 7075. Before process development, the gas-atomized powder material was characterized in terms of statistical distribution: size and shape. A wide range of process parameters were selected to optimize the process in terms of optimum volume density. The investigations resulted in a relative density of over 99%. However, all laser-melted parts exhibit hot cracks which typically appear in aluminium alloy EN AW 7075 during the welding process. Furthermore the influence of processing parameters on the chemical composition of the selected alloy was determined.

  2. Property Evaluation of Friction Stir Welded Dissimilar Metals : AA6101-T6 and AA1350 Aluminium Alloys

    Directory of Open Access Journals (Sweden)

    Rajendran ASHOK KUMAR

    2017-02-01

    Full Text Available Next to copper, aluminium alloys are widely used in electrical industries, because of their high electrical conductivity. AA6101-T6 and AA1350 aluminium alloys are widely used in electrical bus bars. As these alloys are joined by mechanical fasteners in electrical bus bars, the conductive area has been reduced. To avoid this problem, they should be joined without removal of metal as well as their properties. Friction stir welding technique is mainly invented for joining similar and dissimilar aluminium alloys. In this investigation, friction stir welding of AA6101-T6 and AA1350 aluminium alloys was done by varying tool traversing speed, rotational speed and tilt angle with hexagonal pin profiled tool. The analysis of variance was employed to study the effect of above parameters on mechanical properties of welded joints. From the experimental results, it is observed that welded joint with the combination of 1070 rpm rotating speed, 78 mm/min traversing speed and 2° tilt angle provides better mechanical properties. Analysis of variance shows that most significant impact on tensile strength is made by variation in tool rotating speed while tool tilt angle makes the most significant impact on elongation and bending strength.DOI: http://dx.doi.org/10.5755/j01.ms.23.1.14132

  3. Modeling of microstructural evolution and flow stress of aluminium alloy during thermomechanical process

    Institute of Scientific and Technical Information of China (English)

    SHEN Jian(沈健); G.Gottstein

    2004-01-01

    The evolution of microstructural variables, including the densities of mobile dislocation, immobile dislocation at the cell interiors, immobile dislocation in the cell walls, as well as total dislocation density, of an Al-Mg-Si aluminium alloy during thermomechanical processing were simulated based on a three-internal-variables-model (3IVM) involving dislocation climb and interaction. Optimization was carried out to fit the calculated stress-strain curves to the experimental data of the Al-Mg-Si alloy with minimum mean deviation. Precipitations were taken into consideration of modeling. The stress-strain curves predicted by the kinetic equations of state in the 3IVM have a good agreement with the experimental data.

  4. Corrosion protection of Mg/Al alloys by thermal sprayed aluminium coatings

    Energy Technology Data Exchange (ETDEWEB)

    Pardo, A., E-mail: anpardo@quim.ucm.es [Departamento de Ciencia de Materiales, Facultad de Quimicas, Universidad Complutense, 28040 Madrid (Spain); Casajus, P.; Mohedano, M.; Coy, A.E.; Viejo, F. [Departamento de Ciencia de Materiales, Facultad de Quimicas, Universidad Complutense, 28040 Madrid (Spain); Torres, B. [Departamento de Ciencia e Ingenieria de Materiales, ESCET, Universidad Rey Juan Carlos, 28933 Mostoles, Madrid (Spain); Matykina, E. [Corrosion and Protection Centre, School of Materials, The University of Manchester, P.O. Box 88, Sackville Street, Manchester M60 1QD (United Kingdom)

    2009-05-15

    The protective features of thermal sprayed Al-coatings applied on AZ31, AZ80 and AZ91D magnesium/aluminium alloys were evaluated in 3.5 wt.% NaCl solution by electrochemical and gravimetric measurements. The changes in the morphology and corrosion behaviour of the Al-coatings induced by a cold-pressing post-treatment were also examined. The specimens were characterized by scanning electron microscopy, energy dispersive X-ray analysis and low-angle X-ray diffraction. The as-sprayed Al-coatings revealed a high degree of porosity and poor corrosion protection, which resulted in galvanic acceleration of the corrosion of the magnesium substrates. The application of a cold-pressing post-treatment produced more compact Al-coatings with better bonding at the substrate/coating interface and higher corrosion resistance regardless of the nature of the magnesium alloy.

  5. Effect of heat treatment on the inhibition of the acidic corrosion aluminium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Khamis, E. (Alexandria Univ. (Egypt). Dept. of Chemistry); El-Gamal, M. (Alexandria Univ. (Egypt). Dept. of Material Science); El-Toukhy, A. (Alexandria Univ. (Egypt). Dept. of Material Science); Atea, M. (Alexandria Univ. (Egypt). Dept. of Material Science)

    1994-12-01

    The effect of heat treatment on the inhibition of acid corrosion of duralumin has been studied using gasometry, mass loss measurements and potentiodynamic technique. All the data reveal that the duralumin generally developed good corrosion resistance after heat treatment and the corrosion rate ranked as follows: Non treated > Naturally aged > quenched. This improvement in the corrosion resistance was attributed to the structural homogeneity of the heat-treated alloys. The presence of some selected aryl and alkyl triazoline derivatives at the threshold concentration of 5 x 10[sup -3] M indicate that these compounds retard the corrosion rate of duralumin and the extent of inhibition depends on the molecular structure of the inhibitors. Polarization curves show that the triazoline compounds act as mixed-type inhibitors affecting both the cathodic and anodic processes. Moreover, there is no noticeable difference in the degree by which the triazoline derivatives inhibit the corrosion of pure aluminium and heat treated duralumin alloy. (orig.)

  6. Effects of different tempers on precipitation hardening of 6000 series aluminium alloys

    Institute of Scientific and Technical Information of China (English)

    LIU Hong; ZHAO Gang; LIU Chun-ming; ZUO Liang

    2007-01-01

    By means of Vickers hardness, mechanical property and formability tests, the effects of different tempers on precipitation hardening of 6000 series aluminium alloys for automotive body sheets were investigated. The results indicate that the short-time pre-aging at 170 ℃ makes for subsequent artificial aging precipitation hardening. With the increase of pre-aging time, the artificial aging hardenability increases. The aging hardening rate reaches the maximum when pre-aging time is up to 10 min, and then it decreases. The short-time pre-aging at 170 ℃ benefits sheets to obtain lower strength under delivery condition and consequently to improve stamping formability of automotive body sheets. The effects of different tempers on precipitation hardening are much more obvious than those of the alloying elements. It is a good treatment schedule to perform pre-aging for 5 min at 170 ℃ right after solution treatment.

  7. Investigating the Acid Failure of Aluminium Alloy in 2 M Hydrochloric Acid Using Vernonia amygdalina

    Directory of Open Access Journals (Sweden)

    Olugbenga A. Omotosho

    2012-04-01

    Full Text Available The acid failure of aluminium alloy in 2 M hydrochloric acid solution in the presence of Vernonia amygdalina extract was investigated using gasometric technique. Aluminium alloy coupons of dimension 4 cm by 1 cm were immersed in test solutions of free acid and also those containing extract volumes of 2, 3, 4 and 5 cm3 at ambient temperature for 30 minutes. The volumes of hydrogen gas evolved as a result of the rate of reaction were recorded and analyzed. Analysis revealed that maximum inhibitor efficiency which corresponds to the lowest corrosion rate was obtained at optimum inhibitor volumes of 5 cm3, with reduction in the corrosion rate observed to follow in order of increasing extract volumes. Adsorption study revealed that Temkin isotherm best described the metal surface interaction with the extract phytochemicals, with 12 minutes becoming the best exposure time for the phytochemicals to adsorb to the metal surface at all volumes. Statistical modelling of the corrosion rate yielded an important relationship suitable for estimating corrosion rate values once volumes of the extract is known. Microstructural studies, showed an indirect relationship between crack growth rates and extract volumes, while consistency of the irregular intermetallic phases increases with increasing extract volumes.

  8. Deep surface rolling for fatigue life enhancement of laser clad aircraft aluminium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Zhuang, W., E-mail: wyman.zhuang@dsto.defence.gov.au [Aerospace Division, Defence Science and Technology Organisation, 506 Lorimer Street, Fishermans Bend, Victoria 3207 (Australia); Liu, Q.; Djugum, R.; Sharp, P.K. [Aerospace Division, Defence Science and Technology Organisation, 506 Lorimer Street, Fishermans Bend, Victoria 3207 (Australia); Paradowska, A. [Australian Nuclear Science and Technology Organisation, Lucas Heights, NSW 2232 (Australia)

    2014-11-30

    Highlights: • Deep surface rolling as a post-repair enhancement technology was applied to the laser cladded 7075-T651 aluminium alloy specimens that simulated corrosion damage blend-out repair. • The residual stresses induced by the deep surface rolling process were measured. • The deep surface rolling process can introduce deep and high magnitude compressive residual stresses beyond the laser clad and substrate interface. • Spectrum fatigue test showed the fatigue life was significantly increased by deep surface rolling. - Abstract: Deep surface rolling can introduce deep compressive residual stresses into the surface of aircraft metallic structure to extend its fatigue life. To develop cost-effective aircraft structural repair technologies such as laser cladding, deep surface rolling was considered as an advanced post-repair surface enhancement technology. In this study, aluminium alloy 7075-T651 specimens with a blend-out region were first repaired using laser cladding technology. The surface of the laser cladding region was then treated by deep surface rolling. Fatigue testing was subsequently conducted for the laser clad, deep surface rolled and post-heat treated laser clad specimens. It was found that deep surface rolling can significantly improve the fatigue life in comparison with the laser clad baseline repair. In addition, three dimensional residual stresses were measured using neutron diffraction techniques. The results demonstrate that beneficial compressive residual stresses induced by deep surface rolling can reach considerable depths (more than 1.0 mm) below the laser clad surface.

  9. Effects of Moulding Sand Permeability and Pouring Temperatures on Properties of Cast 6061 Aluminium Alloy

    Directory of Open Access Journals (Sweden)

    Olawale Olarewaju Ajibola

    2015-01-01

    Full Text Available Effects of moulding sand permeabilities prepared from the combinations of four proportions of coarse and fine particle size mixtures and pouring temperatures varied from 700, 750, and 800 (±10°C were studied on the hardness, porosity, strength, and microstructure of cast aluminium pistons used in hydraulic brake master cylinder. Three sand moulds were prepared from each of the 80 : 20, 60 : 40, 40 : 60, and 20 : 80 ratios. The surfaces and microstructures of cast samples were examined using high resolution microscopic camera, metallurgical microscope with digital camera, and scanning electron microscope with EDX facilities. The best of the metallurgical properties were obtained from the combination of 80 : 20 coarse-fine sand ratio and 750 ± 10°C pouring temperature using as MgFeSi inoculant. An 8 : 25 ratio of coarse to fine grained eutectic aluminium alloy was obtained with enhanced metallographic properties. The cast alloy poured at 750 ± 1°C has a large number of fine grain formations assuming broom-resembling structures as shown in the 100 µm size SEM image.

  10. Optimisation of the rivet joints of the CFRP composite material and aluminium alloy

    Directory of Open Access Journals (Sweden)

    A. Czulak

    2007-01-01

    Full Text Available Purpose: The project included analysis of strain, cracking, and failure of riveted joints of plate elements madefrom the carbon-fibre-reinforced plastics (CFRP and from the 6061 aluminium alloy.Design/methodology/approach: The modelled static tensile strength test carried out for the plates from CFRPand from the 6061 aluminium alloy joined with the steel rivet. Computer simulation was carried out with IDEASsoftware package employing the FEM.Findings: Simulations using the mesh with a bigger number of FEM elements do not yield better accuracy ofcalculations and do not improve convergence with the results of laboratory experiments. Only the calculationtime gets longer. Computer simulation has also show that the type of contacts employed between elementsaffects the results significantly.Research limitations/implications: For the composite materials, joints between materials and computersimulation examinations are planed.Practical implications: Results obtained for the mesh with 4 and 5 FEM elements are the closest to the resultsof laboratory experiments, which is confirmed by the strain plot. Simulations using the mesh with a biggernumber of FEM elements do not yield better accuracy of calculations and do not improve convergence with theresults of laboratory experiments. Only the calculation time gets longer. Computer simulation has show that thetype of contacts employed between elements affects the results significantly.Originality/value: The paper presents influence of fibre mesh closeness on convergence of the results with laboratorytests. Simulation results were collected and compared with the laboratory static tensile strength tests results.

  11. Implementation and Testing of Numerical Models for Evolution of Microchemistry and Microstructure During Back-Annealing of Aluminium Alloys

    OpenAIRE

    Iversen, Jørgen Tandberg

    2014-01-01

    Precipal and Alsoft are two separate models for simulating the effects of back-annealing on microchemistry and microstructure, respectively, in AA3xxx-type aluminium alloys (i.e Mn containing alloys). The precipitation model simulates the precipitation and growth of dispersoids, growth of constituents, and the resulting change in the solid solution concentration. Alsoft is a physical softening model which combines the effects of recovery and recrystallization.Precipal was originally implemen...

  12. Positron annihilation spectroscopy as a tool to develop self healing in aluminium alloys

    Energy Technology Data Exchange (ETDEWEB)

    Hautakangas, S.; Schut, H. [Faculty of Applied Physics, section NPM2, Delft University of Technology, Mekelweg 15, 2629 JB, Delft (Netherlands); Zwaag, S. van der; Rivera Diaz del Castillo, P.E.J. [Faculty of Aerospace Engineering, Section Fundamentals of Advanced Materials, Delft University of Technology, Kluyverweg 1, 2629 HS Delft (Netherlands); Dijk, N.H. van [Faculty of Applied Physics, Section FAME, Delft University of Technology, Mekelweg 15, 2629 JB, Delft (Netherlands)

    2007-07-01

    Positron lifetime and Doppler broadening spectroscopy have been applied to probe the free volume generation (vacancies, dislocations and nano-cracks) during plastic deformation of a commercial aluminium AA2024 (T3) alloy. Aim of the total program is to study how solute atoms can be driven to the areas where initial cracking may occur in order to prevent the failure of the specimen. The phenomenon of closing the nano-crack is called Self Healing, and can provide extra strength and ductility to the alloy under some loading conditions. Plastic deformation of over-aged aluminum alloy at room temperature increases the average positron lifetime from initial value of 190 ps to 203 ps. The low momentum parameter S increases in agreement with the increase of open volume defects. The elastic deformation of the sample does not have a recordable effect on the positron annihilation data. It is also shown that the induced damage does not recover after loading the sample, i.e. the AA2024 in the T3 state is non self healing material, as expected, providing important first state result in the research of self healing Al alloys. (copyright 2007 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

  13. Comparative Study of the Energy Absorption Capacities of XPS and XPE Foam Filled Aluminium Square Tubes under Quasi-Static Axial Compression

    Directory of Open Access Journals (Sweden)

    Suman Bargav. R

    2015-07-01

    Full Text Available :Quasi-static compression tests were performed on empty and foam filled Aluminium square tubes. Two different foam types: Extended Polystyrene (XPS and Extended Polyethylene (XPE were used to fill the empty tubes. In this paper experimental and numerical simulations were performed to investigate the effect of foam filling on crashworthiness parameters

  14. Characterization of semi-solid processing of aluminium alloy 7075 with Sc and Zr additions

    Energy Technology Data Exchange (ETDEWEB)

    Rogal, Ł., E-mail: l.rogal@imim.pl [Institute of Metallurgy and Materials Science of the Polish Academy of Sciences, 25 Reymonta St., 30-059 Krakow (Poland); Dutkiewicz, J. [Institute of Metallurgy and Materials Science of the Polish Academy of Sciences, 25 Reymonta St., 30-059 Krakow (Poland); Atkinson, H.V. [The University of Leicester, Department of Engineering University Road, Leicester, LE1 7RH (United Kingdom); Lityńska-Dobrzyńska, L.; Czeppe, T. [Institute of Metallurgy and Materials Science of the Polish Academy of Sciences, 25 Reymonta St., 30-059 Krakow (Poland); Modigell, M. [RWTH Aachen—Department of Mechanical Process Engineering, 55 Templergraben St., Aachen (Germany)

    2013-09-15

    For thixoforming (semi-solid processing) it is necessary to have a fine globular microstructure in a semi-solid range. Here this has been obtained for 7075 aluminium alloy by addition of modifying agents: 0.5 weight % of scandium and zirconium. The thixoforming process was carried out at 632 °C which gave about 23 volume % of liquid phase. The microstructure of the thixo-formed part (a rotor) consisted of globular grains surrounded by precipitates of secondary phase. The average hardness of thixo-formed parts was 105 HV{sub 5} and the tensile strength 300 MPa. T6 heat treatments were performed with solutionisation at 450 °C for 30 min and 10 h. In both cases the ageing time was set as 18 h at 120 °C. The heat treatments led to an increase in average tensile strength up to 495 MPa. Transmission Electron Microscopy (TEM) analysis enabled the identification of precipitates of the metastable dispersoids of L1{sub 2}–Al{sub 3} (Zr, Sc) and η′ (MgZn{sub 2}) phases in the alloy after the thixoforming and T6 treatment. The measurements of rheological properties of 7075Al alloy with Sc and Zr additions in the semi-solid range indicated an increase of particle size and spheroidization leading to an observable decrease of viscosity during isothermal shearing. A shear rate jump experiment showed that with increasing shear rate the viscosity rapidly falls.

  15. Flux-free brazing of Mg-containing aluminium alloys by means of cold spraying

    Institute of Scientific and Technical Information of China (English)

    Kirsten BOBZIN; Lidong ZHAO; Felix ERNST; Katharina RICHARDT

    2008-01-01

    In the present study, AlSi12 and AlSi10Cu4 were deposited onto Mg-containing aluminium alloys 6063 and 5754 by cold spraying. The influences of the two brazing alloys and spray parameters on coating formation were investigated. The microstructure of the coatings was characterized. Some coated samples were heat-treated at 590℃ and 560℃ in air to investigate the effect of the rupture of oxide scales on the diffusion of elements during heat-treatment. Some coated samples were brazed under argon atmosphere without any fluxes. The results show that AlSi12 had much better deposition behaviour than AlSi10Cu4. Due to the rupture of oxide scales, Cu and Si diffused into the substrate and a metal-lurgical bond formed between the brazing alloys and the substrates during heat-treatment. The coated samples could be brazed without any fluxes. Because the oxide scales prevented the formation of a metallurgical bond locally, the brazed samples had relatively low shear strengths of up to 43 MPa.

  16. Influence of friction stir welding parameters on properties of 2024 T3 aluminium alloy joints

    Directory of Open Access Journals (Sweden)

    Eramah Abdsalam M.

    2014-01-01

    Full Text Available The aim of this work is to analyse the process of friction stir welding (FSW of 3mm thick aluminium plates made of high strength aluminium alloy - 2024 T3, as well as to assess the mechanical properties of the produced joints. FSW is a modern procedure which enables joining of similar and dissimilar materials in the solid state, by the combined action of heat and mechanical work. This paper presents an analysis of the experimental results obtained by testing the butt welded joints. Tensile strength of the produced joints is assessed, as well as the distribution of hardness, micro-and macrostructure through the joints (in the base material, nugget, heat affected zone and thermo-mechanically affected zone. Different combinations of the tool rotation speed and the welding speed are used, and the dependence of the properties of the joints on these parameters of welding technology is determined. [Projekat Ministarstva nauke Republike Srbije, br. TR 34018 i br. TR 35006

  17. Multi response optimization of wire-EDM process parameters of ballistic grade aluminium alloy

    Directory of Open Access Journals (Sweden)

    Ravindranadh Bobbili

    2015-12-01

    Full Text Available In the current investigation, a multi response optimization technique based on Taguchi method coupled with Grey relational analysis is planned for wire-EDM operations on ballistic grade aluminium alloy for armour applications. Experiments have been performed with four machining variables: pulse-on time, pulse-off time, peak current and spark voltage. Experimentation has been planned as per Taguchi technique. Three performance characteristics namely material removal rate (MRR, surface roughness (SR and gap current (GC have been chosen for this study. Results showed that pulse-on time, peak current and spark voltage were significant variables to Grey relational grade. Variation of performance measures with process variables was modelled by using response surface method. The confirmation tests have also been performed to validate the results obtained by Grey relational analysis and found that great improvement with 6% error is achieved.

  18. Microstructure of friction stir welded joints of 2017A aluminium alloy sheets.

    Science.gov (United States)

    Mroczka, K; Dutkiewicz, J; Pietras, A

    2010-03-01

    The present study examines a friction stir welded 2017A aluminium alloy. Transmission electron microscope investigations of the weld nugget revealed the average grain size of 5 microm, moderate density of dislocations as well as the presence of nanometric precipitates located mostly in grains interiors. Scanning electron microscope observations of fractures showed the presence of ductile fracture in the region of the weld nugget with brittle precipitates in the lower part. The microhardness analysis performed on the cross-section of the joints showed fairly small changes; however, after the artificial ageing process an increase in hardness was observed. The change of the joint hardness subject to the ageing process indicates partial supersaturation in the material during friction stir welding and higher precipitation hardening of the joint.

  19. Hot-crack test for aluminium alloys welds using TIG process

    Directory of Open Access Journals (Sweden)

    Deschaux-beaume F.

    2010-06-01

    Full Text Available Hot cracking is a critical defect frequently observed during welding of aluminium alloys. In order to better understand the interaction between cracking phenomenon, process parameters, mechanical factors and microstructures resulting from solidification after welding, an original hot-cracking test during welding is developed. According to in-situ observations and post mortem analyses, hot cracking mechanisms are investigated, taking into account the interaction between microstructural parameters, depending on the thermal cycles, and mechanical parameters, depending on geometry and clamping conditions of the samples and on the thermal field on the sample. Finally, a process map indicating the limit between cracking and non-cracking zones according to welding parameters is presented.

  20. Optimization of process parameters in CNC turning of aluminium alloy using hybrid RSM cum TLBO approach

    Science.gov (United States)

    Rudrapati, R.; Sahoo, P.; Bandyopadhyay, A.

    2016-09-01

    The main aim of the present work is to analyse the significance of turning parameters on surface roughness in computer numerically controlled (CNC) turning operation while machining of aluminium alloy material. Spindle speed, feed rate and depth of cut have been considered as machining parameters. Experimental runs have been conducted as per Box-Behnken design method. After experimentation, surface roughness is measured by using stylus profile meter. Factor effects have been studied through analysis of variance. Mathematical modelling has been done by response surface methodology, to made relationships between the input parameters and output response. Finally, process optimization has been made by teaching learning based optimization (TLBO) algorithm. Predicted turning condition has been validated through confirmatory experiment.

  1. Plastic anisotropy of ultrafine grained aluminium alloys produced by accumulative roll bonding

    Energy Technology Data Exchange (ETDEWEB)

    Beausir, B., E-mail: benoit.beausir@univ-metz.fr [Institut fuer Strukturphysik, Technische Universitaet Dresden, D-01062 Dresden (Germany); Scharnweber, J. [Institut fuer Strukturphysik, Technische Universitaet Dresden, D-01062 Dresden (Germany); Jaschinski, J. [Institut fuer Leichtbau und Kunststofftechnik, Technische Universitaet Dresden, D-01062 Dresden (Germany); Brokmeier, H.-G. [GKSS Forschungszentrum, Max-Planck-Strasse, D-21494 Geesthacht (Germany); Oertel, C.-G.; Skrotzki, W. [Institut fuer Strukturphysik, Technische Universitaet Dresden, D-01062 Dresden (Germany)

    2010-05-25

    The plastic anisotropy of ultrafine grained aluminium alloys AA1050 and AA6016 produced by accumulative roll bonding (ARB) has been investigated by tensile deformation via the Lankford parameter. The average normal and planar anisotropies slightly increase (from 0.6 to 0.9) and decrease (from 0.6 to -0.7) as a function of ARB cycles, respectively. The global textures measured by neutron diffraction are used to simulate the Lankford and anisotropy parameters of the plates after 0, 2, 4, 6 and 8 ARB cycles with the help of the viscoplastic polycrystal self-consistent model. Simulation results are compared with those from experiment and discussed with regard to texture, strain rate sensitivity, grain shape and slip system activity.

  2. QUANTIFICATION OF SHEAR DAMAGE EVOLUTION IN ALUMINIUM ALLOY 2024T3

    Institute of Scientific and Technical Information of China (English)

    Tang Chak-yin; Fan Jianping; Tsui Chi-pong; Lee Tai-chiu; Chan Luen-chow; Rao Bin

    2007-01-01

    Shear damage may occur in the process of metal machining such as blanking and cutting, where localized shear deformation is developed. Experimental findings indicate that microscopic shear damage evolution in aluminium alloy 2024T3 (Al 2024T3) is a multi-stage mechanism, including particle cracking, micro-shear banding, matrix microcracking and coalescence of microcracks. This study is an attempt to use a set of equations to describe the multi-stage shear damage evolution in Al 2024T3. The shear damage variables in terms of multi-couple parameters of a power-law hardening material have been defined. An evolution curve of shearing damage has been calculated from experimental data. The values of the shear damage variable at different stages of damage have also been calculated. By making use of the findings, the relation between the microscopic shear damage evolution and the macroscopic shear response of the material has been discussed.

  3. Flow and failure of an aluminium alloy from low to high temperature and strain rate

    Directory of Open Access Journals (Sweden)

    Sancho Rafael

    2015-01-01

    Full Text Available The mechanical behaviour of an aluminium alloy is presented in this paper. The study has been carried out to analyse the flow and failure of the aluminium alloy 7075-T73. An experimental study has been planned performing tests of un-notched and notched tensile specimens at low strain rates using a servo-hydraulic machine. High strain rate tests have been carried out using the same geometry in a Hopkinson Split Tensile Bar. The dynamic experiments at low temperature were performed using a cryogenic chamber, and the high temperature ones with a furnace, both incorporated to the Hopkinson bar. Testing temperatures ranged from − 50 ∘C to 100 ∘C and the strain rates from 10−4 s−1 to 600 s−1. The material behaviour was modelled using the Modified Johnson-Cook model and simulated using LS-DYNA. The results show that the Voce type of strain hardening is the most accurate for this material, while the traditional Johnson-Cook is not enough accurate to reproduce the necking of un-notched specimens. The failure criterion was obtained by means of the numerical simulations using the analysis of the stress triaxiality versus the strain to failure. The diameters at the failure time were measured using the images taken with an image camera, and the strain to failure was computed for un-notched and notched specimens. The numerical simulations show that the analysis of the evolution of the stress triaxiality is crucial to achieve accurate results. A material model using the Modified Johnson-Cook for flow and failure is proposed.

  4. Influences of post weld heat treatment on tensile properties of friction stir welded AA2519-T87 aluminium alloy joints

    Science.gov (United States)

    Sabari, S. Sree; Balasubramanian, V.; Malarvizhi, S.; Reddy, G. Madusudhan

    2015-12-01

    AA 2519-T87 is an aluminium alloy that principally contains Cu as an alloying element and is a new grade of Al-Cu alloy system. This material is a potential candidate for light combat military vehicles. Fusion welding of this alloy leads to hot cracking, porosity and alloy segregation in the weld metal region. Friction stir welding (FSW) is a solid state joining process which can overcome the above mentioned problems. However, the FSW of age hardenable aluminium alloys results in poor tensile properties in the as-welded condition (AW). Hence, post weld heat treatment (PWHT) is used to enhance deteriorated tensile properties of FSW joints. In this work, the effect of PWHT, namely artificial ageing (AA) and solution treatment (ST) followed by ageing (STA) on the microstructure, tensile properties and microhardness were systematically investigated. The microstructural features of the weld joints were characterised using an optical microscope (OM), scanning electron microscope (SEM) and transmission electron microscope (TEM). The tensile strength and microhardness of the joints were correlated with the grain size, precipitate size, shape and its distribution. From the investigation, it was found that STA treatment is beneficial in enhancing the tensile strength of the FSW joints of AA2519-T87 alloy and this is mainly due to the presence of fine and densely distributed precipitates in the stir zone.

  5. Evaluation of roll-extruded Alloy 718 tubing

    Energy Technology Data Exchange (ETDEWEB)

    Smolik, G R; Korth, G E

    1978-05-01

    A sample of roll-extruded Alloy 718 tubing, a product identified for use in the Clinch River Breeder Reactor, was evaluated. The tubing satisfied AMS 5589 requirements for seamless tubing, and had tensile and fatigue properties comparable to plate for the conventional 955/sup 0/C (1750/sup 0/F) heat treatment. Recrystallization was retarded in this product and bands of very small grains resulted from the conventional heat treatment. Both as-roll-extruded and directly aged material showed the results of thermomechanical processing in high strengths and reductions in area. It is recommended that work continue toward realizing improved fatigue and stress rupture properties in this product by means of ''Minigrain'' and thermomechanical processing. 10 figures, 6 tables.

  6. Influence of tube spinning on formability of friction stir welded aluminum alloy tubes for hydroforming application

    Energy Technology Data Exchange (ETDEWEB)

    Wang, X.S. [State Key Laboratory of Advanced Welding and Joining, Harbin Institute of Technology, Harbin 150001 (China); Hu, Z.L., E-mail: zhilihuhit@163.com [State Key Laboratory of Advanced Welding and Joining, Harbin Institute of Technology, Harbin 150001 (China); Hubei Key Laboratory of Advanced Technology of Automobile Parts, Wuhan University of Technology, Wuhan 430070 (China); State Key Laboratory of Materials Processing and Die and Mould Technology, Huazhong University of Science and Technology (China); Yuan, S.J. [State Key Laboratory of Advanced Welding and Joining, Harbin Institute of Technology, Harbin 150001 (China); Hua, L. [Hubei Key Laboratory of Advanced Technology of Automobile Parts, Wuhan University of Technology, Wuhan 430070 (China)

    2014-06-01

    Due to economic and ecological reasons, the application of tailor-welded blanks of aluminum alloy has gained more and more attention in manufacturing lightweight structures for automotives and aircrafts. In the study, the research was aimed to highlight the influence of spinning on the formability of FSW tubes. The microstructural characteristics of the FSW tubes during spinning were studied by electron backscattered diffraction (EBSD) and transmission electron microscopy (TEM). The formability of the FSW tubes with different spinning reduction was assessed by hydraulic bulge test. It is found that the spinning process shows a grain refinement of the tube. The grains of the FSW tube decrease with increasing thickness reduction, and the effect of grain refinement is more obvious for the BM compared to that of the weld. The difference of grain size and precipitates between the weld and BM leads to an asymmetric W-type microhardness distribution after spinning. The higher thickness reduction of the tube, the more uniform distribution of grains and precipitates it shows, and consequently results in more significant increase of strength. As compared with the result of tensile test, the tube after spinning shows better formability when the stress state changes from uniaxial to biaxial stress state.

  7. Surface nanocrystallization of 7A04 aluminium alloy induced by circulation rolling plastic deformation

    Institute of Scientific and Technical Information of China (English)

    YE Hui-qiong; FAN Xin-min

    2006-01-01

    The surface nanocrystalline microstructures of 7A04 aluminium alloy was obtained by means of circulation rolling plastic deformation(CRPD),the grain refinement behavior and the hardness variation were examined. X-ray diffraction(XRD) and transmission electron microscopy(TEM) were applied to characterize the microstructure of the surface layer. The experimental evidences show that,after the CRPD treatment,the mean grain size in the surface layer is about 50 nm. The microhardness of the nanostructured surface layers is enhanced significantly after CRPD compared with that of the matrix,which can be attributed primarily to the grain refinement. The microhardness at the top surface can reach about HV0.05335,while the value of the matrix is HV0.05160 or so. The surface hardening effect is obtained obviously. Besides,the thermal stability of nanocrystalline layer was investigated. The results of the XRD analysis and the microhardness measurement show that the nanocrystalline layer has better thermal-stability than the matrix. And the DSC measurement shows that the synthesis of nanostructured surface layer has influence on the phase transformation of 7A04 aluminum alloy.

  8. Oxide growth on aluminium alloys in the presence of ammonium fluoborate

    Energy Technology Data Exchange (ETDEWEB)

    Oliver, J.; Paterson, P.; Flavell, T. [Royal Melbourne Inst. of Tech., VIC (Australia); Biddle, G. [Alcoa Rolled Products (Australia)

    1996-12-31

    The aim of this study as to determine the mechanisms involved in using ammonium fluoborate as a reducing atmosphere when preheating a high magnesium content aluminium alloy. Rutherford Backscattering (RBS) has been the major technique used in the analysis of samples, it revealed significant reduction in both the diffusion of magnesium to the surface and the calculated oxide thickness in the presence of NH{sub 4}BF{sub 4}. At temperatures above 500 deg C in air, SEM images revealed depressions and voids due to incipient melting at various stages, around the grain boundaries. Grain boundaries effectively acted as pipes aiding the diffusion of magnesium to the surface. These results have been verified through compositional analysis with both RBS and auger electron spectroscopy (AES). Results from NH{sub 4}BF{sub 4} atmosphere preheat conditions showed significant improvements. It was verified experimentally that above 500 deg C , AA5182 alloys undergo incipient melting at the grain boundaries with magnesium diffusing through to the surface. 5 refs., 1 fig.

  9. Comparison of RSM with ANN in predicting tensile strength of friction stir welded AA7039 aluminium alloy joints

    Institute of Scientific and Technical Information of China (English)

    A. K. LAKSHMINARAYANAN; V. BALASUBRAMANIAN

    2009-01-01

    Friction stir welding(FSW) is an innovative solid state joining technique and has been employed in aerospace, rail, automotive and marine industries for joining aluminium, magnesium, zinc and copper alloys. The FSW process parameters such as tool rotational speed, welding speed, axial force, play a major role in deciding the weld quality. Two methods, response surface methodology and artificial neural network were used to predict the tensile strength of friction stir welded AA7039 aluminium alloy. The experiments were conducted based on three factors, three-level, and central composite face centered design with full replications technique, and mathematical model was developed. Sensitivity analysis was carried out to identify critical parameters. The results obtained through response surface methodology were compared with those through artificial neural networks.

  10. Modified Layer-Removal Method for Measurement of Residual Stress in Pre-stretched Aluminium Alloy Plate

    Institute of Scientific and Technical Information of China (English)

    Liangbao Liu; Jianfei Sun; Wuyi Chen; Pengfei Sun

    2015-01-01

    Residual stress is one of the factors affecting the machining deformation of monolithic structure parts in the aviation industry. Thus, the studies on machining deformation rules induced by residual stresses largely depend on correctly and efficiently measuring the residual stresses of workpieces. A modified layer⁃removal method is proposed to measure residual stress by analysing the characteristics of a traditional layer⁃removal method. The coefficients of strain release are then deduced according to the simulation results using the finite element method ( FEM) . Moreover, the residual stress in a 7075T651 aluminium alloy plate is measured using the proposed method, and the results are then analyzed and compared with the data obtained by the traditional methods. The analysis indicates that the modified layer⁃removal method is effective and practical for measuring the residual stress distribution in pre⁃stretched aluminium alloy plates.

  11. Insight of the interface of electroless Ni-P/SiC composite coating on aluminium alloy, LM24

    OpenAIRE

    2015-01-01

    Electroless nickel composite coatings with silicon carbide, SiC, as reinforcing particles deposited with Ni–P onto aluminium alloy, LM24, having zincating as under layer were subjected to heat treatment using air furnace. The changes at the interface were investigated using scanning electron microscope (SEM) and energy dispersive X-ray (EDX) to probe the chemistry changes upon heat treatment. Microhardness tester with various loads using both Knoop and Vickers indenters was used to study the ...

  12. Probabilistic thermal-mechanical fatigue criterion for lost foam casting aluminium alloys based on 2D/3D porosities distribution

    OpenAIRE

    Szmytka F.; Limodin N.; Wang L; Osmond P.; Adrien J.; Charkaluk E.; Buffiere J.Y.

    2014-01-01

    A thermal-mechanical fatigue criterion is proposed to assess the lifetime of aluminium alloys produced by a lost foam casting process. It is based on the observed size distribution of pores sizes which are considered as critical zones for cracks initiation and gives reliable results when both pores sizes are identified from X-ray tomography and mean stresses are taken into account. Lifetime probabilities are finally successfully compared with experimental results.

  13. Probabilistic thermal-mechanical fatigue criterion for lost foam casting aluminium alloys based on 2D/3D porosities distribution

    Directory of Open Access Journals (Sweden)

    Szmytka F.

    2014-06-01

    Full Text Available A thermal-mechanical fatigue criterion is proposed to assess the lifetime of aluminium alloys produced by a lost foam casting process. It is based on the observed size distribution of pores sizes which are considered as critical zones for cracks initiation and gives reliable results when both pores sizes are identified from X-ray tomography and mean stresses are taken into account. Lifetime probabilities are finally successfully compared with experimental results.

  14. Influence of welding speed on corrosion behaviour of friction stir welded AA5086 aluminium alloy

    Institute of Scientific and Technical Information of China (English)

    Kamran Amini; Farhad Gharavi

    2016-01-01

    The plates of AA5086 aluminium alloy were joined together by friction stir welding at a fixed rotation speed of 1000 r/min various welding speeds ranging from 63 to 100 mm/min. Corrosion behavior of the parent alloy (PA), the heat affected zone (HAZ), and the weld nugget zone (WNZ) of the joints were studied in 3.5% (mass fraction) aerated aqueous NaCl solution by potentiodynamic polarization and electrochemical impedance spectroscopy (EIS). The corrosion susceptibility of the weldments increases when the welding speed increases to 63 and 100 mm/min. However, the value of corrosion rate in the weldments is lower than that in the PA. Additionally, the corrosion current density increases with increasing the welding speed in the HAZ and the WNZ. On the contrary, the corrosion potential in the WNZ appears more positive than in the HAZ with decreasing the welding speed. The WNZ exhibits higher resistance compared to the HAZ and the PA as the welding speed decreases. The results obtained from the EIS measurements suggest that the weld regions have higher corrosion resistance than the parent alloy. With increasing the welding speed, the distribution and extent of the corroded areas in the WNZ region are lower than those of the HAZ region. In the HAZ region, in addition to the pits in the corroded area, some cracks can be seen around the corroded areas, which confirms that intergranular corrosion is formed in this area. The alkaline localized corrosion and the pitting corrosion are the main corrosion mechanisms in the corroded areas within the weld regions. Crystallographic pits are observed within the weld regions.

  15. Evaluation of the mechanical properties and corrosion behaviour of coconut shell ash reinforced aluminium (6063 alloy composites

    Directory of Open Access Journals (Sweden)

    Oluyemi O. DARAMOLA

    2015-12-01

    Full Text Available Aluminium 6063/Coconut shell ash (CSAp composites having 3-12 weight percent (wt% coconut shell ash were fabricated by double stir-casting method. The microstructure, ultimate tensile strength, hardness values, density and corrosion behaviour in 0.3M H2SO4 and 3.5wt% NaCl solution of the composites were evaluated. The density of the composites exhibit a linear and proportional decreased as the percentage of coconut shell ash increases in the aluminium alloy. It implies that composites with lower weight component can be produced by adding CSAp. The microstructural analysis showed uniform distribution of coconut shell ash particles in the aluminium alloy matrix. Significant improvement in hardness and ultimate tensile strength values was noticeable as the wt% of the coconut shell ash increased in the alloy, although this occur at the expense of ductility of the composites as the modulus of elasticity of the composites decreases as the percentage of CSAp increases. Hence, this work has established that incorporation of coconut shell particles in aluminum matrix can lead to the production of low cost aluminum composites with improved hardness and tensile strength values.

  16. Optimizing pulsed current gas tungsten arc welding parameters of AA6061 aluminium alloy using Hooke and Jeeves algorithm

    Institute of Scientific and Technical Information of China (English)

    S. BABU; T. SENTHIL KUMAR; V. BALASUBRAMANIAN

    2008-01-01

    Though the preferred welding process to weld aluminium alloy is frequently constant current gas tungsten arc welding (CCGTAW), it resulted in grain coarsening at the fusion zone and heat affected zone(HAZ). Hence, pulsed current gas tungsten arc welding(PCGTAW) was performed, to yield finer fusion zone grains, which leads to higher strength of AA6061 (Al-Mg-Si) aluminium alloy joints. In order to determine the most influential control factors which will yield minimum fusion zone grain size and maximum tensile strength of the joints, the traditional Hooke and Jeeves pattern search method was used. The experiments were carried out based on central composite design with 31 runs and an algorithm was developed to optimize the fusion zone grain size and the tensile strength of pulsed current gas tungsten arc welded AA6061 aluminium aUoy joints. The results indicate that the peak current (Ip) and base current (IB) are the most significant parameters, to decide the fusion zone grain size and the tensile strength of the AA6061 aluminum alloy joints.

  17. Study of the Fatigue Life and Weight Optimization of an Automobile Aluminium Alloy Part under Random Road Excitation

    Directory of Open Access Journals (Sweden)

    A. Saoudi

    2010-01-01

    Full Text Available Weight optimization of aluminium alloy automobile parts reduces their weight while maintaining their natural frequency away from the frequency range of the power spectral density (PSD that describes the roadway profile. We present our algorithm developed to optimize the weight of an aluminium alloy sample relative to its fatigue life. This new method reduces calculation time; It takes into account the multipoint excitation signal shifted in time, giving a tangle of the constraint signals of the material mesh elements; It also reduces programming costs. We model an aluminium alloy lower vehicle suspension arm under real conditions. The natural frequencies of the part are inversely proportional to the mass and proportional to flexural stiffness, and assumed to be invariable during the process of optimization. The objective function developed in this study is linked directly to the notion of fatigue. The method identifies elements that have less than 10% of the fatigue life of the part's critical element. We achieved a weight loss of 5 to 11% by removing the identified elements following the first iteration.

  18. Sintering behaviour of Alumix 321 and 6061 aluminium alloys; Sinterizacion de las aleaciones Alumix 321 y 6061

    Energy Technology Data Exchange (ETDEWEB)

    Romano, P.; Fogagnolo, J. B.; Garcia, A.; Ruiz-Navas, E. M.

    2005-07-01

    The sintering behaviour of two aluminium alloys, Alumix 321 and 6061, was studied in this paper. Both have a similar Mg, Cu and Si contents, but have been obtained by different methods. the Alumix 321 alloy is produced by mixing the initial elements as powders and the 6061 is obtained by water atomization. The work carried out includes the study of the green properties, the determination of the compressibility and green strength curves as well as the microstructural characterization of the powders. Thermal analyses (DTAs and Dilatometries) were performed in order to study the behaviour of both alloys with temperature. furthermore, different sintering temperatures were studied by characterizing the mechanical properties of the sintered materials. It can be concluded that the 6061 alloys has better properties than the Alumix 321, when both were sintered at 600 degree centigree. (Author) 27 refs.

  19. Anodisation of Aluminium Alloys by Micro-Capillary Technique as a Tool for Reliable, Cost-Efficient, and Quick Process Parameter Determination

    Directory of Open Access Journals (Sweden)

    Daniela Nickel

    2016-01-01

    Full Text Available Anodisation is essential for improving surface properties of aluminium alloys and composites regarding wear and corrosion behaviour. Optimisation of the anodising process depends on microstructural constituents contained in aluminium alloys and represents a key task, consisting of the control of process parameters and electrolyte formulation. We applied the micro-capillary technique known from corrosion studies and modified it to form anodic aluminium oxide films on high-strength aluminium alloys in comparison to pure aluminium in sulphuric acid. A glass capillary with an opening of 800 μm in diameter was utilized. Corresponding electrochemical measurements during potentiodynamic and potentiostatic anodisation revealed anodic current responses similar to conventional anodisation. The measurement of film thickness was adapted to the thin anodised spots using ellipsometry and energy dispersive X-ray analysis. Cross sections prepared by focused ion beam milling confirm the thickness results and show the behaviour of intermetallic phases depending on the anodising potential. Consequently, micro-capillary anodising proved to be an effective tool for developing appropriate anodisation conditions for aluminium alloys and composites because it allows quick variation of electrolyte composition by applying low electrolyte volumes and rapid film formation due to short process durations at small areas and more flexible variation of process parameters due to the used set-up.

  20. EVALUATION OF PARAMETERS OF FRICTION STIR WELDING FOR ALUMINIUM AA6351 ALLOY

    Directory of Open Access Journals (Sweden)

    AHMED KHALID HUSSAIN

    2010-10-01

    Full Text Available Friction Stir Welding (FSW is a solid state welding process in which the relative motion between the tool and the work piece produces heat which makes the material of two edges being joined by plastic atomicdiffusion. This method relies on the direct conversion of mechanical energy to thermal energy to form the weld without the application of heat from conventional source. The rotational speed of the tools, the axial pressure and welding speed and the (weld time are the principal variables that are controlled in order to provide the necessary combination of heat and pressure to form the weld. These parameters are adjusted so that the interface is heated into the plastic temperature range (plastic state where welding can take place. During the last stage of welding process, atomic diffusion occurs while the interfaces are in contact, allowing metallurgical bond to form between the two materials. The functional behaviour of the weldments is substantially determined by the nature of the weld strength characterized by the tensile strength, metallurgical behavior, surface roughness, weld hardness and micro hardness. In this project an attempt is made to determine and evaluate the influence of the process parameters of FSW on the weldments. The Vickers hardness, tensile strength and radiography are considered for investigation by varying tool speed, tool feed and maintaining onstant depth of penetration of weld. Experiments were conducted on AA6351 Aluminium alloy in a CNC Vertical Machining Centre. Theoutput factors are measured in UTM, Vickers hardness tester and Radiography equipment. Results show strong relation and robust comparison between the weldment strength and process parameters. Hence FSW process variable data base is to be developed for wide variety of metals and alloys for selection of optimum process parameters for efficient weld.

  1. Soudage homogène MIG de l'alliage d'aluminium 6061 MIG homogeneous welding of 6061 aluminium alloy

    Directory of Open Access Journals (Sweden)

    Benoit Alexandre

    2013-11-01

    Full Text Available Le soudage homogène (métal d'apport identique au métal de base de l'alliage d'aluminium 6061 avec un procédé dit semi-automatique (MIG n'a jamais été reporté jusqu'à maintenant dans la littérature. Nous montrons ici que l'utilisation d'un dérivé du procédé de soudage MIG, le MIG CMT (Cold Metal Transfer permet d'obtenir des cordons de soudures sains (sans fissuration à chaud. De plus des traitements thermiques ont permis de retrouver partiellement ou de restaurer totalement les propriétés de la soudure. Nos résultats sont comparés à des essais de soudage MIG CMT avec le métal d'apport préconisé pour le soudage de l'alliage 6061. The homogeneous welding (same filler metal as base metal of the 6061 aluminium alloy with MIG process has never been reported in the open access literature. This work shows that the CMT (Cold Metal Transfer MIG, a derivative of MIG, allows producing welds without hot-cracking. Moreover, further heat treatments partially increased or fully restore the mechanical properties of the weld. These results are compared with 6061 heterogeneous welds usually met in the industry.

  2. Matrix effect on leaching of Bisphenol A diglycidyl ether (BADGE) from epoxy resin based inner lacquer of aluminium tubes into semi-solid dosage forms.

    Science.gov (United States)

    Lipke, Uwe; Haverkamp, Jan Boris; Zapf, Thomas; Lipperheide, Cornelia

    2016-04-01

    To study the impact of different semi-solid dosage form components on the leaching of Bisphenol A (BPA) and Bisphenol A diglycidyl ether (BADGE) from the epoxy resin-based inner lacquer of aluminium tubes, the tubes were filled with different matrix preparations and stored at an elevated temperature. Despite compliance with the European Standards EN 15348 and EN 15766 on porosity and polymerisation of internal coatings of aluminium tubes, the commercially available tubes used in the study contained an increased amount of polymerisation residues, such as unbound BPA, BADGE and BADGE derivatives in the lacquer, as determined by acetonitrile extraction. Storage of Macrogol ointments in these tubes resulted in an almost quantitative migration of the unbound polymerisation residues from the coating into the ointment. In addition, due to alterations observed in the RP-HPLC chromatograms of the matrix spiked with BADGE and BADGE derivatives it is supposed that the leachates can react with formulation components. The contamination of the medicinal product by BPA, BADGE and BADGE derivatives can be precluded by using aluminium tubes with an internal lacquer with a low degree of unbound polymerisation residues.

  3. Microstructure and high temperature deformation of an ultra-fine grained ECAP AA7075 aluminium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Malek, Premysl; Turba, Krystof; Cieslar, Miroslav; Harcuba, Petr [Charles Univ., Prague (Czech Republic). Dept. of Physics of Materials

    2013-01-15

    An AA 7075 aluminium alloy with an ultra-fine grained structure was prepared through equal channel angular pressing (ECAP) at pressing temperatures T ECAP of 120, 170, and 220 C. A decrease in T{sub ECAP} from 220 to 120 C was found to lead to a more pronounced refinement of the microstructure and to worse stability of the microstructure - the onset of grain coarsening was displaced to lower temperatures. The material pressed with the highest T{sub ECAP} exhibited superplastic behaviour at temperatures close to 400 C and grain boundary sliding was identified as the dominant operating deformation mechanism. The materials prepared with both of the lower T{sub ECAP} exhibited only enhanced ductility of about 200%, however this behaviour was observed at temperatures as low as 200 C. It was found that this 'low temperature superplasticity' resulted from a combined operation of grain boundary sliding at selected grain boundaries and glide of lattice dislocations. (orig.)

  4. Spectroscopic study of plasma during electrolytic oxidation of magnesium-aluminium alloys

    Science.gov (United States)

    Jovović, J.

    2014-12-01

    Plasma during Electrolytic Oxidation (PEO) of magnesium-aluminium alloys is studied in this work by means of Optical Emission Spectroscopy (OES). Spectral line shapes of the Hβ, Al II 704.21 nm and Mg II 448.11 nm line are analyzed to measure plasma electron number density Ne. From the Hβ line profile, two PEO processes characterized by relatively low electron number densities Ne ≈ 1015 cm-3 and Ne ≈ 2 × 1016 cm-3 were discovered while the shape and shift of Al II and Mg II lines revealed the third process characterized by large electron density Ne = (1-2) × 1017 cm-3. Low Ne processes, related with breakdown in gas bubbles and on oxide surface, are not influenced by anode material or electrolyte composition. The ejection of evaporated anode material through oxide layer is designated here as third PEO process. Using the Boltzmann plot technique, electron temperature of 4000 K and 33000 K is determined from relative intensities of Mg I and O II lines, respectively. Several difficulties in the analysis of spectral line shapes are met during this study and the ways to overcome some of the obstacles are demonstrated.

  5. Thermal Analysis on Butt Welded Aluminium Alloy AA7075 Plate Using FEM

    Directory of Open Access Journals (Sweden)

    M. Pal Pandi

    2014-03-01

    Full Text Available Thermo-mechanical finite element analysis has been performed to assess the residual stress in the butt weld joints of aluminium Alloy AA7075 plates by utilizing the commercial software package ABAQUS. This paper presents an efficient FE technique using equivalent load to precisely predict welding deformations and residual stresses in butt joints. The radial heat flux distribution is considered on the top surface of the weldment. Convective and radiative heat losses are taken into account through boundary conditions for the outward heat flux. Linear FE transient thermal analysis is performed using surface heat source model with Gaussian distribution to compute highest temperature in AA7075 plates. The objective of this project is to simulate the welding process by using the finite element method. After the model is built and verified, the main objective of this project is to study the effects of varying the welding process parameters on the thermo-mechanical responses. In addition to that, the aim of this research is also to find a relationship between welding parameters and the responses of single pass butt welding are evaluated through the finite element analysis. The study of this paper covers the effects of varying heat input, welding speed on the thermo-mechanical responses of the weldment after cooling down to room temperature.

  6. Effect of Negatively Charged Ions on the Formation of Microarc Oxidation Coating on 2024 Aluminium Alloy

    Institute of Scientific and Technical Information of China (English)

    Wei Yang; Bailing Jiang; Aiying Wang; Huiying Shi

    2012-01-01

    The present study deals with the effect of negatively charged ions on the ceramic coating formation on 2024 aluminium alloy during microarc oxidation (MAO) process. On the basis of the experimental results, two steps (the formation of an incipient film without arc presence and the growth of a ceramic coating with arc discharge) of MAO process have been observed. For comparison, four different negatively charged ions studied. It is proved that negatively charged ions strongly participated in the formation of an incipient film with high impedance value at the first step. The growth of ceramic coating depends on the combination between AI of the substrate and O from the electrolyte, and the negatively charged ions are little consumed. As an anodic oxide coating is prepared on the sample surface instead of the incipient film, the first step occurs easily and the growth of ceramic coating is accelerated. Furthermore, the mechanism of negatively charged ions in the formation of the MAO coating has been proposed.

  7. Ductile damage in aluminium alloy thin sheets: Correlation between micro-tomography observations and mechanical modeling

    Energy Technology Data Exchange (ETDEWEB)

    Thuillier, S., E-mail: sandrine.thuillier@univ-ubs.fr [LIMATB, Universite de Bretagne-Sud-rue de Saint Maude BP 92116 56321 Lorient Cedex (France); Maire, E. [MATEIS CNRS UMR 5510, INSA Lyon-7 avenue Jean Capelle 69621 Villeurbanne Cedex (France); Brunet, M. [LaMCoS CNRS UMR 5259, INSA Lyon-7 avenue Jean Capelle 69621 Villeurbanne Cedex (France)

    2012-12-15

    This work deals with the characterization of ductile damage in an aluminium alloy AA6016-T4 by X-ray micro-tomography, as a function of anisotropy and triaxiality. Interrupted tensile tests on notched samples with three different geometries were performed and the void volume fraction was measured for different strain values, up to rupture. It was shown that void volume fraction evolution with the strain is rather similar at 0 Degree-Sign and 90 Degree-Sign to RD but at 45 Degree-Sign to RD it shows a more rapid evolution. Moreover, for the same strain level, a higher void volume fraction was recorded for a higher triaxiality ratio. Whatever the orientation and the stress triaxiality ratio, void volume fraction values range from 5 Multiplication-Sign 10{sup -4} up to 0.04. A numerical model based on Gurson-Tvergaard-Needleman constitutive equations was used to simulate the different tests. Hardening of the material was identified from macroscopic tensile test nucleation material parameters were identified by a direct method from void volume fraction evolution. It can be seen that the influence of triaxiality on void volume fraction is underestimated, though void growth is nicely predicted for the highest triaxiality ratio, for strains below 0.5. The load level was correctly predicted, except for high strain, where coalescence seems necessary to be taken into account.

  8. Material modelling for creep-age forming of aluminium alloy 7B04

    Directory of Open Access Journals (Sweden)

    Lam Aaron C.L.

    2015-01-01

    Full Text Available This paper presents a study on the creep-ageing behaviour of a peak-aged aluminium alloy 7B04 under different tensile loads at 115oC and subsequently modelling it for creep-age forming (CAF applications. Mechanical properties and microstructural evolutions of creep-aged specimens were investigated. The material was modelled using a set of unified constitutive equations, which not only captures the material's creep deformation but also takes into account yield strength contributions from solid solution hardening, age hardening and dislocation hardening during creep-ageing. A possible application of the present work is demonstrated by implementing the determined material model into a commercial finite element analysis solver via a user-defined subroutine for springback prediction of creep-age formed plates. A good agreement is observed between the simulated springback values and experimental results. This material model now enables further investigations of 7B04 under various CAF scenarios to be conducted inexpensively via computational modelling.

  9. Effects of heat treatments on the microstructure and mechanical properties of a 6061 aluminium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Maisonnette, D. [Universite de Lyon, CNRS, INSA-Lyon, LaMCoS UMR5259, F-69621 (France); Suery, M. [Universite de Grenoble, SIMaP, UMR CNRS 5266, BP46, Domaine Universitaire, 38402 Saint Martin d' Heres Cedex (France); Nelias, D., E-mail: daniel.nelias@insa-lyon.fr [Universite de Lyon, CNRS, INSA-Lyon, LaMCoS UMR5259, F-69621 (France); Chaudet, P. [Universite de Lyon, CNRS, INSA-Lyon, LaMCoS UMR5259, F-69621 (France); Epicier, T. [Universite de Lyon, CNRS, INSA-Lyon, Mateis UMR5510, F-69621 (France)

    2011-03-15

    Research highlights: {yields} Description of the mechanical behavior of AA6061-T6 at RT after various thermal histories. {yields} A fast-heating device has been designed to reproduce those thermal histories on tensile specimens. {yields} The thermal loadings are representative of the temperature change observed in the HAZ during welding. {yields} The variation of mechanical properties is the result of metallurgical evolution observed by TEM. {yields} The yield stress at RT decreases with the maximum temperature reached during the thermal cycle. - Abstract: This paper describes the mechanical behavior of the 6061-T6 aluminium alloy at room temperature for various previous thermal histories representative of an electron beam welding. A fast-heating device has been designed to control and apply thermal loadings on tensile specimens. Tensile tests show that the yield stress at ambient temperature decreases if the maximum temperature reached increases or if the heating rate decreases. This variation of the mechanical properties is the result of microstructural changes which have been observed by Transmission Electron Microscopy (TEM).

  10. Inhibition of localized attack on the aluminium alloy AA 6351 in glycol/water solutions

    Energy Technology Data Exchange (ETDEWEB)

    Monticelli, C.; Brunoro, G.; Zucchi, F.; Fagioli, F.

    1989-06-01

    The objective of this work was to examine the feasibility of enhancing pitting resistance of AA 6351 (nominal composition: 1% Si, 0.6% Mg, 0.3% Mn, balance Al) by adding suitable inhibitors to the solutions. The compounds used were two inorganic salts: sodium molybdate and sodium tungstate and two derivatives of pyrimidine: 2-aminopyrimidine (2AP) and 2-hydroxypyrimidine (2HP). The inhibiting efficiencies of these substances were tested by both short-time electrochemical tests (galvanic coupling tests and polarization curves) and long-time immersions under experimental conditions causing the localized attack. Molybdate, tungstate and, to some extent, also 2AP efficiently inhibit AA 6351 localized corrosion in degraded solutions at 80/sup 0/C and in pure boiling solutions, for long exposure periods. The short-time electrochemical tests suggest that molybdate and tungstate are able to retard the electrochemical processes occurring on both the aluminium alloy and the small copper cathodic area produced by copper deposition. On the other hand, the 2AP efficiency is attributed to some complexing capability of this pyrimidine derivative towards dissolved copper ions, that are stabilized in solution. 2HP does not prevent AA 6351 localized attack. (orig./MM).

  11. Natural aging behaviour of friction stir welded 6005A-T6 aluminium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Dong, Peng; Sun, Daqian; Li, Hongmei, E-mail: lihongmei@jlu.edu.cn

    2013-08-01

    By local thermal cycles and hardness measurements, supported by transmission electron microscopy, the post-weld natural aging behaviour of friction stir welded 6005A-T6 aluminium alloy was investigated. The results show that the softening in the nugget zone and thermo-mechanically affected zone immediately after welding is mainly caused by the high peak temperatures and rapid cooling rates, resulting in the original β″ precipitates dissolving and restraining re-precipitation. On the one hand, the hardness recovery in both microstructural zones during post-weld natural aging is attributed to the formation of clusters or GP zones depending on the natural aging time. On the other hand, the softening in the heat-affected zone after welding is due to the transformation of the β′′ to β′ precipitates and the precipitation of Q′. Natural aging has little effect on the microstructure and hardness of the heat-affected zone. The mechanism of natural aging behaviour was discussed.

  12. Effect of Mg on microstructures and properties of Al-Mg-Si-Cu aluminium alloys for automotive body sheets

    Institute of Scientific and Technical Information of China (English)

    LIU Hong; SONG Wen-ju; ZHAO Gang; LIU Chun-ming; ZUO Liang

    2005-01-01

    The effects of variation of Mg content on microstructures,the tensile properties and the formability of Al-Mg-Si-Cu alloys for automotive body sheets were investigated by means of scan electron microscopy,optical metallographic analysis,tensile and Ericsson tests.The results show that for Al-Mg-Si-Cu aluminium alloys with excessive Si,with an increment of Mg content,the strength enhances,the specific elongation and Erisson values of alloys decrease,and the number of Mg2 Si constituent increases and that of Al(MnFe)Si type constituents reduces.Al-MgSi-Cu aluminium alloys with excessive Si for automotive body sheets can present obviously the paint bake hardenability during the paint bake cycle (I.e.artificial aging at 170 ℃ for 30 min immediately after the solution treatment and quenching).Suitable Mg content should be controlled in the range of 0.8% and 1.2 % (mass fraction).

  13. Experimental investigations of visco-plastic properties of the aluminium and tungsten alloys used in KE projectiles

    Directory of Open Access Journals (Sweden)

    Magier M.

    2012-08-01

    Full Text Available The main aim of studies on dynamic behaviour of construction materials at high strain rates is to determine the variation of mechanical properties (strength, plasticity in function of the strain rate and temperature. On the basis of results of dynamic tests on the properties of constructional materials the constitutive models are formulated to create numerical codes applied to solve constructional problems with computer simulation methods. In the case of military applications connected with the phenomena of gunshot and terminal ballistics it’s particularly important to develop a model of strength and armour penetration with KE projectile founded on reliable results of dynamic experiments and constituting the base for further analyses and optimization of projectile designs in order to achieve required penetration depth. Static and dynamic results of strength investigations of the EN AW-7012 aluminium alloy (sabot and tungsten alloy (penetrator are discussed in this paper. Static testing was carried out with the INSTRON testing machine. Dynamic tests have been conducted using the split Hopkinson pressure bars technique at strain rates up to 1,2 ⋅ 104s−1 (for aluminium alloy and 6 ⋅ 103s−1 (for tungsten alloy.

  14. Energy absorption of aluminum alloy thin-walled tubes under axial impact

    Energy Technology Data Exchange (ETDEWEB)

    Sun, Hongtu; Wang, Jian [Ludong University, Yantai (China); Shen, Guozhe; Hu, Ping [Dalian University of Technology, Dalian (China)

    2016-07-15

    Aluminum alloys are important technological materials for achieving the lightweight design of automotive structures. Many works have reported on the deformation and energy absorption of thin-walled tubes. Multicorner tubes with extra concave corners in the cross section were presented in this study to improve the energy absorption efficiency of aluminum alloy thin-walled tubes. The axial crushing of square and multicorner thin-walled tubes was simulated with the same cross-sectional perimeter. The method of folding element was applied to predict the crushing behavior of the thin-walled tubes under axial impact. The corners on the cross section were discussed to determine their effect on the energy absorption performance of thin-walled tubes. Results showed that the increasing performance of energy absorption of aluminum alloy thin-walled tubes was caused by the increasing number of corners on the cross section of multicorner tubes. Both the number and size of corners had an important effect on the crushing force efficiency of multicorner tubes. The maximum crushing force efficiency of multicorner tubes was 11.6% higher than that of square tubes with the same material consumption of thin-walled tubes. The multicorner tubes with 12 corners showed better energy absorption performance than the tubes with more than 12 corners; this high number of corners could lead to the small size of corners or unstable deformations. The high energy absorption performance of multicorner tubes prefers increasing the corner number and corner size of adjacent sides at the same time.

  15. Modification of aluminium alloys with rare metals – the basis for advanced materials in construction and transport

    Directory of Open Access Journals (Sweden)

    Skachkov Vladimir Mikchaylovich

    2016-06-01

    Full Text Available The method of process powder injection into aluminum melt shows much promise. Scandium is injected by the high-temperature exchange reaction between the salt melt and aluminum. The best salt compositions were selected. The results of the process are considered to depend on the initial salts. A series of fusions was performed under production conditions at the Kamensk-Uralskii metallurgical plant. It was shown that the injection method for production of aluminoscandium master alloys is technologically feasible. To protect intellectual property of authors, employees of the Institute of Solid State Chemistry, Ural branch of RAS (Russia a patent «Method of alloying of aluminium or alloys on its basis» RU № 2534182 of 27.11.2014 was registered.

  16. Residual stresses in shape memory alloy fiber reinforced aluminium matrix composite

    Science.gov (United States)

    Tsz Loong, Tang; Jamian, Saifulnizan; Ismail, Al Emran; Nur, Nik Hisyammudin Muhd; Watanabe, Yoshimi

    2017-01-01

    Process-induced residual stress in shape memory alloy (SMA) fiber reinforced aluminum (Al) matrix composite was simulated by ANSYS APDL. The manufacturing process of the composite named as NiTi/Al is start with loading and unloading process of nickel titanium (NiTi) wire as SMA to generate a residual plastic strain. Then, this plastic deformed NiTi wire would be embedded into Al to become a composite. Lastly, the composite is heated form 289 K to 363 K and then cooled back to 300 K. Residual stress is generated in composite because of shape memory effect of NiTi and mismatch of thermal coefficient between NiTi wire and Al matrix of composite. ANSYS APDL has been used to simulate the distribution of residual stress and strain in this process. A sensitivity test has been done to determine the optimum number of nodes and elements used. Hence, the number of nodes and elements used are 15680 and 13680, respectively. Furthermore, the distribution of residual stress and strain of nickel fiber reinforced aluminium matrix composite (Ni/Al) and titanium fiber reinforced aluminium matrix composite (Ti/Al) under same simulation process also has been simulated by ANSYS APDL as comparison to NiTi/Al. The simulation results show that compressive residual stress is generated on Al matrix of Ni/Al, Ti/Al and NiTi/Al during heating and cooling process. Besides that, they also have similar trend of residual stress distribution but difference in term of value. For Ni/Al and Ti/Al, they are 0.4% difference on their maximum compressive residual stress at 363K. At same circumstance, NiTi/Al has higher residual stress value which is about 425% higher than Ni/Al and Ti/Al composite. This implies that shape memory effect of NiTi fiber reinforced in composite able to generated higher compressive residual stress in Al matrix, hence able to enhance tensile property of the composite.

  17. The effect of cutting process on surface microstructure and hardness of pure and Al 6061 aluminium alloy

    Directory of Open Access Journals (Sweden)

    Adnan Akkurt

    2015-09-01

    Full Text Available In this study pure aluminium and Al 6061 aluminium alloy material had been cut with saw, milling, submerged plasma, plasma, laser, wire electric discharge machining, oxyfuel and Abrasive water jet. Microstructures and hardness variations of cut surfaces which obtained with different processes have been investigated. Results of the study show that the hardness and surface quality of the cut surface is affected from the kind of cutting process. Microstructure of cut surfaces is affected from the kind of cutting process. Microstructural changes during cutting of the materials are observed with all of the cutting process other than Abrasive water jet. Abrasive water jet method can be effectively used in industrial applications where no microstructural changes and hardness reduction is essential.

  18. Effect of friction time on the properties of friction welded YSZ‐alumina composite and 6061 aluminium alloy

    Directory of Open Access Journals (Sweden)

    Uday M. Basheer

    2012-03-01

    Full Text Available The aim of this work was to study the effect of friction time on the microstructure and mechanical properties of alumina 0, 25, 50 wt% yttria stabilized zirconia (YSZ composite and 6061 aluminium alloy joints formed by friction welding. The alumina-YSZ composites were prepared through slip casting in plaster of Paris molds (POP and subsequently sintered at 1600°C, while the aluminium rods were machined down using a lathe machine to the dimension required. The welding process was carried out under different rotational speeds and friction times, while friction force (0.5 ton-force was kept constant. Scanning electron microscopy was used to characterize the interface of the joints structure. The experimental results showed that the friction time has a significant effect on joint structure and mechanical properties.

  19. Microstructural evolution of aluminium/Al–Ni–Sm glass forming alloy laminates obtained by Controlled Accumulative Roll Bonding

    Energy Technology Data Exchange (ETDEWEB)

    Anghelus, Adrian, E-mail: anghelus.adrian@yahoo.com; Avettand-Fènoël, Marie-Noëlle, E-mail: marie-noelle.avettand-fenoel@univ-lille1.fr; Cordier, Catherine, E-mail: catherine.cordier@univ-lille1.fr; Taillard, Roland, E-mail: roland.taillard@univ-lille1.fr

    2015-05-15

    Highlights: • Elaboration of a UFG material by controlled ARB of Al/glass forming alloy multilayers. • Effect of the crystalline or amorphous nature of the reinforcement on the formability. • Investigation of the thermo-mechanical stability of the metallic glass. - Abstract: The current work deals with the early steps of the unprecedented elaboration of aluminium/Al based glass forming alloy laminates by only accumulative rolling at room temperature. The Al{sub 1−(x+y)}Ni{sub x}Sm{sub y} metallic glass forming alloy was introduced either in its original amorphous state or after total crystallization. This change of atomic structure, and therefore of both thermal and thermo-mechanical stability and mechanical behaviour, is shown to govern at once the processing parameters, the uniformity of the laminates microstructure and the bond strength at the matrix-reinforcement interfaces. The potential of the process so as to synthesize composite materials with a stable ultrafine structure is finally outlined.

  20. Effects of Hard Surface Grinding and Activation on Electroless-Nickel Plating on Cast Aluminium Alloy Substrates

    Directory of Open Access Journals (Sweden)

    Olawale Olarewaju Ajibola

    2014-01-01

    Full Text Available This work examined effects of hard surface polishing grits and activation on electroless-nickel (EN plating on cast aluminium alloy substrates in sodium hypophosphite baths. As-received aluminium alloy sample sourced from automobile hydraulic brake master cylinder piston was melted in electric furnace and sand cast into rod. The cast samples were polished using different grits (60 μm–1200 μm before plating. The effects on adhesion, appearance, and quantity of EN deposits on substrates were studied. Observation shows that the quantity of EN deposit is partly dependent on the alloy type and roughness of the surface of the substrates, whereas the adhesion and brightness are not solely controlled by the degree of surface polishing. The best yield in terms of adhesion and appearance was obtained from the activation in zincate and palladium chloride solutions. Higher plating rates (g/mm2/min of 3.01E-05, 2.41E-05, and 2.90E-05 were obtained from chromate, zincate, and chloride than 8.49E-06, 8.86E-06, and 1.69E-05 as obtained from HCl etched, NaOH, and H2O activated surfaces, respectively.

  1. Effect of pulsed current and post weld aging treatment on tensile properties of argon arc welded high strength aluminium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Balasubramanian, V. [Department of Manufacturing Engineering, Annamalai University, Annamalai Nagar, Tamil Nadu 608002 (India)], E-mail: visvabalu@yahoo.com; Ravisankar, V. [Department of Manufacturing Engineering, Annamalai University, Annamalai Nagar, Tamil Nadu 608002 (India); Reddy, G. Madhusudhan [Metal Joining Section, Defence Metallurgical Research Laboratory, Kanchanbag (P.O.), Hyderabad 560058 (India)

    2007-06-25

    This paper reveals the effect of pulsed current and post weld aging treatment on tensile properties of argon arc welded AA7075 aluminium alloy. This alloy has gathered wide acceptance in the fabrication of light weight structures requiring high strength-to-weight ratio, such as transportable bridge girders, military vehicles, road tankers and railway transport systems. The preferred welding processes of high strength aluminium alloy are frequently gas tungsten arc welding (GTAW) process and gas metal arc welding (GMAW) process due to their comparatively easier applicability and better economy. Weld fusion zones typically exhibit coarse columnar grains because of the prevailing thermal conditions during weld metal solidification. This often results inferior weld mechanical properties and poor resistance to hot cracking. In this investigation, an attempt has been made to refine the fusion zone grains by applying pulsed current welding technique. Four different welding techniques have been used to fabricate the joints and they are: (i) continuous current GTAW (CCGTAW), (ii) pulsed current GTAW (PCGTAW), (iii) continuous current GMAW (CCGMAW) and (iv) pulsed current GMAW (PCGMAW) processes. As welded joint strength is much lower than the base metal strength and hence, a simple aging treatment has been given to improve the tensile strength of the joints. Current pulsing leads to relatively finer and more equi-axed grain structure in GTA and GMA welds. In contrast, conventional continuous current welding resulted in predominantly columnar grain structures. Post weld aging treatment is accompanied by an increase in tensile strength and tensile ductility.

  2. Analysis of the tool plunge in friction stir welding - comparison of aluminium alloys 2024 T3 and 2024 T351

    Directory of Open Access Journals (Sweden)

    Veljić Darko

    2016-01-01

    Full Text Available Temperature, plastic strain and heat generation during the plunge stage of the friction stir welding (FSW of high-strength aluminium alloys 2024 T3 and 2024 T351 are considered in this work. The plunging of the tool into the material is done at different rotating speeds. A three-dimensional finite element (FE model for thermomechanical simulation is developed. It is based on arbitrary Lagrangian-Eulerian formulation, and Johnson-Cook material law is used for modelling of material behaviour. From comparison of the numerical results for alloys 2024 T3 and 2024 T351, it can be seen that the former has more intensive heat generation from the plastic deformation, due to its higher strength. Friction heat generation is only slightly different for the two alloys. Therefore, temperatures in the working plate are higher in the alloy 2024 T3 for the same parameters of the plunge stage. Equivalent plastic strain is higher for 2024 T351 alloy, and the highest values are determined under the tool shoulder and around the tool pin. For the alloy 2024 T3, equivalent plastic strain is the highest in the influence zone of the tool pin. [Projekat Ministarstva nauke Republike Srbije, br. TR 34016 i br. TR 35006

  3. Production and some properties of Si3N4 reinforced aluminium alloy composites

    Directory of Open Access Journals (Sweden)

    Pardeep Sharma

    2015-09-01

    Full Text Available The present research work focuses on the production of aluminium (AA6082-T6 matrix composites reinforced with various weight percentage of silicon nitride particles by conventional stir casting route. The percentage of reinforcement is varied from 0 wt.% to 12 wt.% in a stage of 3%. The microstructures and mechanical properties of the fabricated aluminium matrix composites are investigated. The scanning electron microstructure images reveal the presence of Si3N4 particles in the aluminium matrix. The distribution of Si3N4 particles has also been recognized with X-ray diffraction technique. The mechanical properties such as ultimate tensile strength and hardness have improved at the cost of reduction in ductility with increase in weight percentage of silicon nitride particulates in the aluminium metal matrix. The density and porosity of the composites also show an increasing trend with increase in volume fraction of Si3N4 particles in the aluminium matrix.

  4. Fracture criteria for automobile crashworthiness simulation of wrought aluminium alloy components

    Energy Technology Data Exchange (ETDEWEB)

    El-Magd, E. [RWTH Aachen (Germany); Gese, H. [MATFEM, Munich (Germany); Tham, R. [Fraunhofer Inst. fuer Kurzzeitdynamik, Freiburg (Germany); Hooputra, H.; Werner, H. [BMW Group, Munich (Germany)

    2001-09-01

    In automobile crashworthiness simulation, the prediction of plastic deformation and fracture of each significant, single component is critical to correctly represent the transient energy absorption through the car structure. There is currently a need, in the commercial FEM community, for validated material fracture models which adequately represent this phenomenon. The aim of this paper is to compare and to validate existing numerical approaches to predict failure with test data. All studies presented in this paper were carried out on aluminium wrought alloys: AlMgSi1.F31 and AlMgSiCu-T6. A viscoplastic material law, whose parameters are derived from uniaxial tensile and compression tests at various strain rates, is developed and presented herein. Fundamental ductile fracture mechanisms such as void nucleation, void growth, and void coalescence as well as shear band fracture are present in the tested samples and taken into consideration in the development of the fracture model. Two approaches to the prediction of fracture initiation are compared. The first is based on failure curves expressed by instantaneous macroscopic stresses and strains (i.e. maximum equivalent plastic strain vs. stress triaxiality). The second approach is based on the modified Gurson model and uses state variables at the mesoscopic scale (i.e. critical void volume fraction). Notched tensile specimens with varying notch radii and axisymmetric shear specimens were used to produce ductile fractures and shear band fractures at different stress states. The critical macroscopic and mesoscopic damage values at the fracture initiation locations were evaluated using FEM simulations of the different specimens. The derived fracture criteria (macroscopic and mesoscopic) were applied to crashworthiness experiments with real components. The quality of the prediction on component level is discussed for both types of criteria. (orig.)

  5. Nanocomposite TiC/a-C:H film prepared on titanium aluminium alloy substrates by PSII assistant MW-ECRCVD

    Institute of Scientific and Technical Information of China (English)

    Ma Guo-Jia; Liu Xi-Liang; Zhang Hua-Fang; Wu Hong-Chen; Peng Li-Ping

    2007-01-01

    Thin films of titanium carbide and amorphous hydrogenated carbon have been synthesized on titanium aluminium alloy substrates by PSII assisted MW-ECRCVD with a mirror field. The microstructure, chemical composition and nanometre grains (namely, the so-called nanocomposite structure). The size of TiC grains of nanocomposite TiC/DLC film is about 5 nm. The nanocomposite structure has obvious improvement in the mechanical properties of DLC film.the coherent strength is also obviously enhanced at the critical load of about 35N.

  6. Optimization of squeeze casting parameters for non symmetrical AC2A aluminium alloy castings through Taguchi method

    Energy Technology Data Exchange (ETDEWEB)

    Senthil, P. [Coimbatore Institute of Engineering and Technology, Coimbatore (India); Amirthagadeswaran, K. S. [Government College of Technology, Coimbatore (India)

    2012-04-15

    This paper reports a research in which an attempt was made to prepare AC2A aluminium alloy castings of a non symmetrical component through squeeze casting process. The primary objective was to investigate the influence of process parameters on mechanical properties of the castings. Experiments were conducted based on orthogonal array suggested in Taguchi's offline quality control concept. The experimental results showed that squeeze pressure, die preheating temperature and compression holding time were the parameters making significant improvement in mechanical properties. The optimal squeeze casting condition was found and mathematical models were also developed for the process.

  7. Identification of mechanical properties of weld joints of AlMgSi07.F25 aluminium alloy

    Directory of Open Access Journals (Sweden)

    P. Kopas

    2017-01-01

    Full Text Available The aim of this paper is to present the analysis of selected mechanical properties of weld joints of AlMgSi07.F25 aluminium alloy. We will focus on the influence of the test bar neck shape on the tensile strength characteristics and the course of hardness in the weld joint cross-section. For the welding process using TIG (Tungsten Inert Gas technology we considered AlSi5 as the additive material. This paper also includes a short study of numerical modelling of the test bar welding.

  8. Effect of post weld heat treatment on tensile properties and microstructure characteristics of friction stir welded armour grade AA7075-T651 aluminium alloy

    Institute of Scientific and Technical Information of China (English)

    P. SIVARAJ; D. KANAGARAJAN; V. BALASUBRAMANIAN

    2014-01-01

    This paper reports the effects of post weld heat treatments, namely artificial ageing and solution treatment followed by artificial ageing, on microstructure and mechanical properties of 12 mm thick friction stir welded joints of precipitation hardenable high strength armour grade AA7075-T651 aluminium alloy. The tensile properties, such as yield strength, tensile strength, elongation and notch tensile strength, are evaluated and correlated with the microhardness and microstructural features. The scanning electron microscope is used to characterie the fracture surfaces. The solution treatment followed by ageing heat treatment cycle is found to be marginally beneficial in improving the tensile properties of friction stir welds of AA7075-T651 aluminium alloy.

  9. Experimental and numerical investigation of the residual yield strength of aluminium alloy EN AW-2024-T3 affected by artificially produced pitting corrosion

    Science.gov (United States)

    Pippig, R.; Schmidl, E.; Steinert, P.; Schubert, A.; Lampke, T.

    2017-03-01

    In this study, the behaviour of the residual yield strength of aluminium alloy EN AW-2024-T3 affected by the morphology and numbers of corrosion pits (defects) is presented. Since specific defect structures are not reproducible during experimental corrosion tests, metal sheets with different numbers of pits and pit shapes are produced using laser micro structuring. The defect structures are measured using laser scanning microscopy. To compare the stress states of the micro structured and real corroded metal sheets, FE-analysis is used. Afterwards, uniaxial tensile tests are carried out and critical defect parameters in terms of yield strength reduction of the investigated aluminium alloy are detected.

  10. Inhibitive effect of Ce(III) and La(III) cations for AA2219 aluminium alloy corrosion in sodium chloride medium

    Energy Technology Data Exchange (ETDEWEB)

    Venkatasubramanian, G., E-mail: venkatguru_1966@yahoo.co.in [Department of Chemistry, Sathyabama University, Jeppiaar Nagar, Chennai 600119 (India); Sheik Mideen, A. [Department of Chemistry, Sathyabama University, Jeppiaar Nagar, Chennai 600119 (India); Jha, Abhay K. [Materials Processing Division, Vikram Sarabhai Space Centre, Indian Space Research Organisation, Thiruvananthapuram 695022 (India); Kulandainathan, M. Anbu [Electro Organic Chemistry Division, Central Electrochemical Research Institute, Karaikudi 630006 (India)

    2014-11-14

    In this paper, the rare earth chlorides were used to mitigate the dealloying of Al{sub 2}Cu intermetallic particles in aluminium alloy 2219-T87 plate exposed to 0.6 M NaCl solution. The negative shift of cathodic branches of potentiodynamic polarisation curves revealed the cathodic inhibition towards intermetallic dealloying. The low and high frequency time constants obtained from electrochemical impedance spectra revealed an increase in the corrosion resistance due to precipitation of rare earth oxides/hydroxides on the porous surface of native oxide film of aluminium alloy. Scanning electron microscopy coupled with energy dispersive X-ray analysis and atomic force microscopy revealed that intermetallic inclusions are the sites for the formation of cerium and lanthanum deposits which suppress copper redeposition and minimise galvanic interactions between the matrix and Al{sub 2}Cu particles. - Graphical abstract: Scanning electron microscopy and atomic force microscopy reveal the intermetallic inclusions, the sites for the formation of cerium and lanthanum oxide/hydroxide precipitates which prevent intermetallic de-alloying, suppress copper redeposition and minimise galvanic interactions in aluminium alloy 2219-T87 plate. - Highlights: • Ce{sup 3+} and La{sup 3+} act as cathodic inhibitors for AA2219-T87 aluminium alloy in 0.6 M NaCl. • Al{sub 2}Cu intermetallic particles are the sites for the formation of Ce and La precipitates. • The decrease in surface potential by rare earth chlorides confirms their inhibition.

  11. Ultrahigh performance of Ti-based glassy alloy tube sensor for Coriolis mass flowmeter

    Institute of Scientific and Technical Information of China (English)

    MA Chao-li; A. INOUE; ZHANG Tao

    2006-01-01

    Bulk metallic glasses (BMGs) have potential applications for both structural and functional components owing to their good mechanical properties. With the aim of demonstrating great engineering value of BMGs, a direct melt-forming technique based on suction casting for the production of glassy alloy tubes was developed. The fabrication, structure, geometry, properties and sensor performance of the tubes were examined. The results show that the Coriolis mass flowmeters using the Ti-based glassy alloy sensor tube exhibit excellent measurement sensitivity, viz. 28.5 times higher than that of the conventional flowmeter manufactured using stainless steel (SUS316) tube.

  12. On the influence of manufacturing practices on the SCC behavior of Alloy 690 steam generator tubing

    Energy Technology Data Exchange (ETDEWEB)

    Doherty, P.E.; Doyle, D.M. [Babcock and Wilcox International Div., Cambridge, Ontario (Canada); Sarver, J.M.; Miglin, B.P. [Babcock and Wilcox Research Div., Alliance, OH (United States)

    1996-12-31

    Thermally treated (TT) Alloy 690 is the tubing materials of choice for replacement steam generators (RSGs) throughout the world. It is manufactured using a variety of processing methods with regards to melt practice and thermomechanical forming. Studies assessing the IGSCC resistance of Alloy 690 TT SG tubing have identified a variability in the corrosion performance of nominally identical alloys. While tubing of comparable bulk chemistry may exhibit variations in microchemistry as a result of different melt practice, the correlation between melt practice and SCC resistance is difficult to assess due to other contributing factors. The other contributing factors are identified in this investigation as microstructural features whose generation is dependent on features of particular strain-anneal forming methods by which SG tubes are fabricated. In this study the microstructural characteristics which appear to affect inservice corrosion performance of Alloy 690 TT SG tubes were evaluated. The studies included extensive microstructural examinations in addition to CERT tests performed on actual Alloy 690 TT nuclear SG tubing. The CERT test results indicate that Alloy 690 TT tubing processed at higher mill anneal temperatures display the highest degree of stress corrosion cracking (SCC) resistance. This observation is discussed with reference to carbide distributions, textural aspects and grain boundary orientation character.

  13. Study of Residual Stress Tensors in High-Speed Milled Specimens of Aluminium Alloys Using a Method of Indent Pairs

    Directory of Open Access Journals (Sweden)

    Felipe Víctor Díaz

    2010-12-01

    Full Text Available From data obtained using a method of indent pairs it was possible to analyse different residual stress states generated in high-speed milled specimens of AA 6082-T6 and AA 7075-T6 aluminium alloys. The present method integrates a special device of indentation into a universal measuring machine, allowing the introduction of elongated indents to significantly reduce the absolute error of measurement. Diverse protocols for operations of high-speed face milling allow us to compare residual stress tensors inherent to climb and conventional cutting zones. Through an exhaustive analysis of the Mohr’s circles corresponding to those zones, a relationship was detected, which expresses the sensitivity of both alloys to develop surface residual stresses.

  14. Study of surface interactions of ionic liquids with aluminium alloys in corrosion and erosion-corrosion processes

    Energy Technology Data Exchange (ETDEWEB)

    Bermudez, Maria-Dolores [Grupo de Ciencia de Materiales e Ingenieria Metalurgica, Departamento de Ingenieria de Materiales y Fabricacion, Universidad Politecnica de Cartagena, C/ Doctor Fleming s/n, Campus Muralla del Mar, 30202 Cartagena (Spain)]. E-mail: mdolores.bermudez@upct.es; Jimenez, Ana-Eva [Grupo de Ciencia de Materiales e Ingenieria Metalurgica, Departamento de Ingenieria de Materiales y Fabricacion, Universidad Politecnica de Cartagena, C/ Doctor Fleming s/n, Campus Muralla del Mar, 30202 Cartagena (Spain); Martinez-Nicolas, Gines [Grupo de Ciencia de Materiales e Ingenieria Metalurgica, Departamento de Ingenieria de Materiales y Fabricacion, Universidad Politecnica de Cartagena, C/ Doctor Fleming s/n, Campus Muralla del Mar, 30202 Cartagena (Spain)

    2007-06-30

    Surface interactions of alkylimidazolium ionic liquids (ILs) with aluminium alloy Al 2011 have been studied by immersion tests in seven neat ILs [1-n-alkyl-3-methylimidazolium X{sup -} (X = BF{sub 4}; n = 2 (IL1), 6 (IL2), 8 (IL3). X = CF{sub 3}SO{sub 3}; n = 2 (IL4). X = (4-CH{sub 3}C{sub 6}H{sub 4}SO{sub 3}); n = 2 (IL5). X PF{sub 6}; n = 6 (IL6)] and 1-butyl-3-methylpyridinium bis(trifluoromethylsulfonyl)imide (IL7)]. Immersion tests for Al 2011 have also been carried out in 1 wt.% and 5 wt.% solutions of 1-ethyl,3-methylimidazolium tetrafluoroborate (IL1) in water. No corrosion of Al 2011 by neat ILs is observed. The highest corrosion rate for Al 2011 in water is observed in the presence of a 5 wt.% IL1 due to hydrolysis of the anion with hydrogen evolution and formation of aluminium fluoride. Erosion-corrosion processes have been studied for three aluminium alloys (Al 2011, Al 6061 and Al 7075) in a 90 wt.% IL1 solution in water in the presence of {alpha}-alumina particles. The erosion-corrosion rates are around 0.2 mm/year or lower, and increase with increasing copper content to give a corrosion resistance order of Al 6061 > Al 7075 > Al 2011. Results are discussed on the basis of scanning electron microscopy (SEM) observations, energy dispersive spectroscopy (EDS) analysis, X-ray diffraction (XRD) patterns and X-ray photoelectron spectroscopy (XPS) determinations.

  15. Contribution on Taguchi's Method Application on the Surface Roughness Analysis in End Milling Process on 7136 Aluminium Alloy

    Science.gov (United States)

    ȚÎȚU, M. A.; POP, A. B.

    2016-11-01

    The resulting surface quality after the cutting process is one of the most important characteristics of product quality and also the most frequent customer requirement. Previous research was focused on the effect investigation of machining parameters: cutting speed [1] and feed per tooth [2] on surface roughness. This paper is in itself a continuation of a previous research [3], in which, with Taguchi's method it was determined the level of influence of the cutting parameters on surface roughness of 7136 aluminium alloy in end milling process. The purpose of this paper is to highlight the importance of Taguchi's method use to analyse the surface roughness of 7136 aluminium alloy in end milling process. To conduct the experiments, three cutting parameters were used: cutting speed, feed per tooth and cutting depth. To analyse the surface quality, the surface roughness Ra (the arithmetic average of the absolute values) was measured. It was determined the recommended configuration regarding the optimum values of each machining parameter and the interactions between them, in order to obtain the better cutting process performance and to reduce the surface roughness sensitivity to uncontrollable factors. Based on a full factorial experiment were confirmed the obtained results by applying the Taguchi's method. Final results are a starting point for further research.

  16. Experimental and numerical investigation on under-water friction stir welding of armour grade AA2519-T87 aluminium alloy

    Directory of Open Access Journals (Sweden)

    S. Sree Sabari

    2016-08-01

    Full Text Available Friction stir welding (FSW is a promising welding process that can join age hardenable aluminium alloys with high joint efficiency. However, the thermal cycles experienced by the material to be joined during FSW resulted in the deterioration of mechanical properties due to the coarsening and dissolution of strengthening precipitates in the thermo-mechanical affected zone (TMAZ and heat affected zone (HAZ. Under water friction stir welding (UWFSW is a variant of FSW process which can maintain low heat input as well as constant heat input along the weld line. The heat conduction and dissipation during UWFSW controls the width of TMAZ and HAZ and also improves the joint properties. In this investigation, an attempt has been made to evaluate the mechanical properties and microstructural characteristics of AA2519-T87 aluminium alloy joints made by FSW and UWFSW processes. Finite element analysis has been used to estimate the temperature distribution and width of TMAZ region in both the joints and the results have been compared with experimental results and subsequently correlated with mechanical properties.

  17. Study of twin-roll cast Aluminium alloys subjected to severe plastic deformation by equal channel angular pressing

    Science.gov (United States)

    Poková, M.; Cieslar, M.

    2014-08-01

    Aluminium alloys prepared by twin-roll casting method become widely used in industry applications. Their high solid solution supersaturation and finer grains ensure better mechanical properties when compared with the direct-chill cast ones. One of the possibilities how to enhance their thermal stability is the addition of zirconium. After heat treatment Al3Zr precipitates form and these pin moving grain boundaries when the material is exposed to higher temperatures. In the present work twin-roll cast aluminium alloys based on AA3003 with and without Zr addition were annealed for 8 hours at 450 °C to enable precipitation of Al3Zr phase. Afterwards they were subjected to severe plastic deformation by equal channel angular pressing, which led to the reduction of average grain size under 1 μm. During subsequent isochronal annealing recovery and recrystallization took place. These processes were monitored by microhardness measurements, light optical microscopy and in-situ transmission electron microscopy. The addition of Zr stabilizes the grain size and increases the recrystallization temperature by 100 °C.

  18. Tube extrusion of AZ31 alloy with Sr additions

    Energy Technology Data Exchange (ETDEWEB)

    Sadeghi, Alireza, E-mail: Alireza.Sadeghi@mail.mcgill.ca [McGill University, Department of Mining and Materials Science, Montreal, Quebec (Canada); Hoseini, Majid; Pekguleryuz, Mihriban [McGill University, Department of Mining and Materials Science, Montreal, Quebec (Canada)

    2012-05-15

    Highlights: Black-Right-Pointing-Pointer Bending and unbending of material flow during extrusion tilts the basal pole from the center of the pole figure. Black-Right-Pointing-Pointer Circumferential movement of material inside the welding zone forms two extra texture components. Black-Right-Pointing-Pointer Addition of Sr removes Al from {alpha}-Mg as a result grains could deform more easily in the circumferential directions. Black-Right-Pointing-Pointer By increasing level of Sr, maximum intensity of the ODFs decreases while the extra texture components strengthen. - Abstract: Three Mg alloys (AZ31, and AZ31 + 0.4 and 0.8 wt%Sr) were successfully hot extruded into tubes at 400 Degree-Sign C through a porthole die. Strontium (Sr) additions to AZ31 alloy reduced twining and the dynamically recrystallized grain size. However, Sr also increased the surface cracking tendency during extrusion. It was noted that the complex deformation path in the porthole die distributes the Sr-rich precipitates homogeneously across the microstructure and stringer formation is effectively avoided. The material flow in the die resembles that seen in multiple equal channel angular pressing (ECAP) routes and similar and significant effects on the final texture are observed. The material flow curvatures in the extrusion direction rotate the basal poles 25 Degree-Sign from the radial direction. Two other texture components ({delta}{sub 1}, {delta}{sub 2}) are also formed in the welding zone by the circumferential flow of material. The maximum intensity of the orientation distribution function (ODF) is reduced with increasing level of Sr. Noteworthy, the maximum intensity in AZ31 + 0.8Sr occurs at the {delta}{sub 1} component while for AZ31 and AZ31 + 0.4Sr, the maximum intensity is located at the basal components. With Sr, alloying, Al is depleted from Mg solid solution and grains deform more easily in the circumferential direction. As a result, selective workhardening

  19. Effect of alloying with zinc on SFE of aluminium by study of lattice imperfections in cold worked Al–Zn alloys

    Indian Academy of Sciences (India)

    G Karmakar; R Sen; S K Chattopadhyay; A K Meikap; S K Chatterjee

    2002-08-01

    A detailed X-ray Fourier line shape analysis has been performed on three compositions of Al–Zn alloys viz. Al–3 55 wt% Zn, Al–14 7 wt% Zn and Al–19 3 wt% Zn in fcc phase. It has been found that deformation stacking faults, both intrinsic ' and extrinsic '' are absent in the cold worked state and twin fault is found to be slightly present in the deformed lattice of the two initial compositions of the alloys. Similar to the effect of solute germanium and copper, respectively in Al–Ge and Al–Cu systems, hexagonal zinc also fails to impart faulting in fcc Al–Zn system. This corroborates the fact that aluminium has high stacking fault energy.

  20. Electrochemical Behavior and Microstructure of Recyclable Aluminium-magmesium Alloy Hot-dip Coating Deposited on Low Carbon Steel Substrates

    Institute of Scientific and Technical Information of China (English)

    Panomkorn KWAKHONG; Apichart ARTNASEAW; Chaiyaput KRUEHONG

    2015-01-01

    With the abundance and good corrosion resistance of aluminium, hot-dip technique was used to prepare the recycled Al with 8.2 mass% Mg alloy coating on low carbon steel substrates. Electrochemical behavior of this coating was investigated by an-odic polarization and open circuit potential measurement. Its microstructure and composition were observed by scanning electron microscope and energy-dispersive X-ray spectrometry, respectively. The long lasting corrosion performance of coated steels was in-vestigated under the salt fog spray test. From anodic polarization curves and open circuit potential, recycled Al with 8.2 mass% Mg coating performed adequate sacriifcial ability. At 0.40 V, current density of recycled Al with 8.2 mass% Mg alloy coating was about 200 000 times higher than that of pure recycled Al coating, and was about 0.5 times lower than that of Zn coating. The microstruc-ture of recycled Al with 8.2 mass% Mg alloy coating on the steel substrate consisted of Al3Mg2, Al-Fe intermetallic compound and Al matrix. The results from salt fog spray test showed that recycled Al with 8.2 mass% Mg alloy coated steel had similar corrosion resistance ability to Zn coated steel.

  1. Thin-walled aluminum alloy tube NC precision bending based on finite element simulation

    Institute of Scientific and Technical Information of China (English)

    GU Rui-jie; YANG He; ZHAN Mei; LI Heng

    2006-01-01

    Elongation and springback are the bottleneck problems of thin-walled aluminum alloy tube NC precision bending. So thin-walled aluminum alloy tube NC precision bending based on finite element simulation is put forward. The finite element model of thin-walled aluminum alloy tube NC bending is established based on the DYNAFORM platform. The process of thin-walled aluminum alloy tube NC precision bending is simulated with the model and the elongation and springback of tube bending can be is put forward and the computing equations of bending angle, bending radius, blanking length and initial bending section based on elongation and springback angle are derived. The bending angle, bending radius, blanking length and initial bending section of tube bending can be gained with these equations based on the elongation and springback angle from the simulation. The study can be used to control the quality of thin-walled aluminum alloy tube NC bending so that precision bending without redundance can be realized.

  2. Characterization of Tubing from Advanced ODS alloy (FCRD-NFA1)

    Energy Technology Data Exchange (ETDEWEB)

    Maloy, Stuart Andrew [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Aydogan, Eda [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Anderoglu, Osman [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Lavender, Curt [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Anderson, Iver [Ames Lab., Ames, IA (United States); Rieken, Joel [Ames Lab., Ames, IA (United States); Lewandowski, John [Case Western Reserve Univ., Cleveland, OH (United States); Hoelzer, Dave [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Odette, George R. [Univ. of California, Santa Barbara, CA (United States)

    2016-09-20

    Fabrication methods are being developed and tested for producing fuel clad tubing of the advanced ODS 14YWT and FCRD-NFA1 ferritic alloys. Three fabrication methods were based on plastically deforming a machined thick wall tube sample of the ODS alloys by pilgering, hydrostatic extrusion or drawing to decrease the outer diameter and wall thickness and increase the length of the final tube. The fourth fabrication method consisted of the additive manufacturing approach involving solid-state spray deposition (SSSD) of ball milled and annealed powder of 14YWT for producing thin wall tubes. The details of these fabrication methods are described in ORNL/TM-2015/499 “Status of producing 5 inch long clad tubing of ODS ferritic alloys.” Of the four fabrication methods, two methods were successful at producing tubing for further characterization: production of tubing by High velocity oxy-fuel spray forming and production of tubing using high temperature hydrostatic extrusion. The characterization described in the following report shows through neutron diffraction the texture produced during extrusion while maintaining the beneficial oxide dispersion. Future work will center on extending these processes to producing longer tubing for characterization and irradiation testing.

  3. Small Crack Growth and Fatigue Life Predictions for High-Strength Aluminium Alloys. Part 1; Experimental and Fracture Mechanics Analysis

    Science.gov (United States)

    Wu, X. R.; Newman, J. C.; Zhao, W.; Swain, M. H.; Ding, C. F.; Phillips, E. P.

    1998-01-01

    The small crack effect was investigated in two high-strength aluminium alloys: 7075-T6 bare and LC9cs clad alloy. Both experimental and analytical investigations were conducted to study crack initiation and growth of small cracks. In the experimental program, fatigue tests, small crack and large crack tests A,ere conducted under constant amplitude and Mini-TWIST spectrum loading conditions. A pronounced small crack effect was observed in both materials, especially for the negative stress ratios. For all loading conditions, most of the fatigue life of the SENT specimens was shown to be crack propagation from initial material defects or from the cladding layer. In the analysis program, three-dimensional finite element and A weight function methods were used to determine stress intensity factors and to develop SIF equations for surface and corner cracks at the notch in the SENT specimens. A plastisity-induced crack-closure model was used to correlate small and large crack data, and to make fatigue life predictions, Predicted crack-growth rates and fatigue lives agreed well with experiments. A total fatigue life prediction method for the aluminum alloys was developed and demonstrated using the crack-closure model.

  4. Gas Quenching during Age Hardening of the Aluminium Casting Alloy AI-7Si-0.3Mg

    Institute of Scientific and Technical Information of China (English)

    A. Rose; O. Kessler; F. Hoffmann; H.W. Zoch

    2004-01-01

    For quenching of age hardenable aluminium alloys today predominantly aqueous quenching media are used.which can lead due to the Leidenfrost phenomenon to a non-uniform cooling of the parts and thus to thermal stresses.Particularly at thin-walled or complex shaped parts local plastic deformations can occur by the uneven thermal stresses. In relation to the conventional quenching procedures in aqueous media, gas quenching exhibits a number of technological.ecological and economical advantages. In comparison to liquid quenching media, gas does not change its phase during quenching. Moreover, the cleaning problem of the parts can be avoided. The quenching intensity can be adjusted by the variable parameters gas pressure and gas speed as well as the kind of gas and thus can be adapted to the requirements of the alloy. By the higher uniformity and the better reproducibility, gas quenching offers a high potential to reduce distortion. The goal of these investigations is to clarify, if the cooling rate during gas quenching is sufficient to obtain the specific required strength after age hardening of the alloy A1-7Si-0.3Mg. For this purpose different tests in high-pressure gas quenching facilities, gas nozzle fields and water quenching baths were performed.

  5. EVALUATION & COMPARISION OF MECHANICAL PROPERTIES OF ALUMINIUM ALLOY 5052 REINFORCED WITH SILICONCARBIDE, GRAPHITE AND FLY ASH HYBRID METAL MATRIX COMPOSITES

    Directory of Open Access Journals (Sweden)

    ANKUSH SACHDEVA

    2013-10-01

    Full Text Available The engineering fraternity has always been looking forward to develop an outstanding and wonder-materials which would fit the ever-changing demands of the world. In order to fullfill the demands various newdiscoveries have been made by scientists, engineers and resrearchers. In todays competitive world many, materials have been tried for various unexplored conditions , but the never ending demand of the world encourages the researchers to develop the new material. Now the researchers are preparing the material by the combination of different materials called hybrid composite material.. Metal Matrix Composites (MMCs have emerged as a class of materials suitable for structural, aerospace, automotive, electronic, thermal and wearapplications owing to their advantages over the conventional materials. The present study was taken up to explore the possibility of using different reinforcements (silicon carbide, fly ash and graphite to enhance the properties of aluminium alloy (Al5052 composites. Different samples were prepared from the aluminium withvarying reinforcement composition. The mechanical properties studied after the experiment were strength, hardness and elongation.Further, these composites were characterized with the help of, mechanical testing and scanning electron microscopy.

  6. Modelling of plastic flow localization and damage development in friction stir welded 6005A aluminium alloy using physics based strain hardening law

    DEFF Research Database (Denmark)

    Nielsen, Kim Lau; Pardoen, Thomas; Tvergaard, Viggo

    2010-01-01

    Plastic flow localisation and ductile failure during tensile testing of friction stir welded aluminium spec- imens are investigated with a specific focus on modelling the local, finite strain, hardening response. In the experimental part, friction stir welds in a 6005A-T6 aluminium alloy were...... of fracture as determined by the void coalescence criterion. Furthermore, the presence of a second population of voids was concluded to strongly affect the fracture strain of the high strength regions of the welds. This modelling effort links the microstructure and process parameters to macroscopic parameters...

  7. Foundry Technology of GIS Aluminium Alloy Tank%GIS铝合金罐体的铸造技术

    Institute of Scientific and Technical Information of China (English)

    丁苏沛; 康敬乐; 史学谦; 毕建峰; 郭小花

    2011-01-01

    The involved equipment, die and mold as well as technological essentials for casting of aluminium alloy tank with foundry method such as sand casting, low pressure sand casting, low pressure permanent die casting with sand core, low pressure permanent die casting and Vacuum sealed molding process have been analysed and discussed.%本文就铝合金罐体的主要铸造方法(即砂型铸造、砂型低压铸造、金属型砂芯低压铸造、金属型低压铸造和V法铸造)所涉及的设备、模具和工艺方面的技术要点进行分析和探讨.

  8. Characterization of AA7050 aluminium alloy processed by ECAP; Caracterizacao da liga de aluminio AA7050 processada por ECAP

    Energy Technology Data Exchange (ETDEWEB)

    Cardoso, K.R.; Guido, V. [Universidade do Vale do Paraiba (UNIVAP), Sao Jose dos Campos, SP (Brazil). Inst. de Pesquisa e Desenvolvimento; Travessa, D.N. [Empresa Brasileira de Aeronautica (EMBRAER), Sao Jose dos Campos, SP (Brazil); Jorge Junior, A.M. [Universidade Federal de Sao Carlos (DEMa/UFSCar), SP (Brazil). Dept. de Engenharia de Materiais

    2010-07-01

    The commercial AA7050 aluminium alloy in the solution heat treated condition (W) was processed by ECAP through route A. Two pressing temperatures (room and 150 deg C and velocities (5 and 30mm/min) were used, as well as different number of passes. The effect of such variables on the microstructure evolution was evaluated using optical and transmission electron microscopy with EDX microanalysis, and xray diffraction. It was found that the microstructure has been refined by ECAP, as a result of subgrains formed within deformation bands. ECAP at 150 deg C resulted in intense precipitation of plate like {eta} phase, which evolves to equiaxial morphology as the number of passes increases. (author)

  9. Multi-Objective Optimization of Friction Stir Welding of Aluminium Alloy Using Grey Relation Analysis with Entropy Measurement Method

    Directory of Open Access Journals (Sweden)

    SAURABH KUMAR GUPTA

    2015-01-01

    Full Text Available The present research focus on optimization of Friction Stir Welding (FSW process parameters for joining of AA6061 aluminium alloy using hybrid approach. The FSW process parameters considered are tool rotational speed, welding speed and axial force. The quality characteristics considered are tensile strength (TS and percentage of tensile elongation (TE. Taguchi based experimental design L9 orthogonal array is used for determining the experimental results. The value of weights corresponding to each quality characteristic is determined by using the entropy measurement method so that their importance can be properly explained. Analysis of Variance (ANOVA is used to determine the contribution of FSW process parameters. The confirmation tests also have been done for verifying the results.

  10. Effect of Process Parameters on Tensile Strength of Friction Stir Welded Cast LM6 Aluminium Alloy Joints

    Institute of Scientific and Technical Information of China (English)

    M. Jayaraman; R.Sivasubramanian; V. Balasubramanian

    2009-01-01

    This paper reports the effect of friction stir welding (FSW) process parameters on tensile strength of cast LM6 aluminium alloy. Joints were made by using different combinations of tool rotation speed, welding speed and axial force each at four levels. The quality of weld zone was investigated using macrostructure and microstructure analysis. Tensile strength of the joints were evaluated and correlated with the weld zone hardness and microstructure. The joint fabricated using a rotational speed of 900 r/min, a welding speed of 75 mm/min and an axial force of 3 kN showed superior tensile strength compared with other joints. The tensile strength and microhardness of the welded joints for the optimum conditions were 166 MPa and 64.8 Hv respectively.

  11. Determination of Optimal Parameters for Diffusion Bonding of Semi-Solid Casting Aluminium Alloy by Response Surface Methodology

    Directory of Open Access Journals (Sweden)

    Kaewploy Somsak

    2015-01-01

    Full Text Available Liquid state welding techniques available are prone to gas porosity problems. To avoid this solid state bonding is usually an alternative of preference. Among solid state bonding techniques, diffusion bonding is often employed in aluminium alloy automotive parts welding in order to enhance their mechanical properties. However, there has been no standard procedure nor has there been any definitive criterion for judicious welding parameters setting. It is thus a matter of importance to find the set of optimal parameters for effective diffusion bonding. This work proposes the use of response surface methodology in determining such a set of optimal parameters. Response surface methodology is more efficient in dealing with complex process compared with other techniques available. There are two variations of response surface methodology. The one adopted in this work is the central composite design approach. This is because when the initial upper and lower bounds of the desired parameters are exceeded the central composite design approach is still capable of yielding the optimal values of the parameters that appear to be out of the initially preset range. Results from the experiments show that the pressing pressure and the holding time affect the tensile strength of jointing. The data obtained from the experiment fits well to a quadratic equation with high coefficient of determination (R2 = 94.21%. It is found that the optimal parameters in the process of jointing semi-solid casting aluminium alloy by using diffusion bonding are the pressing pressure of 2.06 MPa and 214 minutes of the holding time in order to achieve the highest tensile strength of 142.65 MPa

  12. Recovery in aluminium

    DEFF Research Database (Denmark)

    Gundlach, Carsten

    2006-01-01

    In the present thesis the development of a unique experimental method for volume characterisation of individual embedded crystallites down to a radius of 150 nm is presented. This method is applied to in-situ studies of recovery in aluminium. The method is an extension of 3DXRD microscopy, an X...... are represented as strings. To identify the strings a combination of a 5D connected component type algorithm and multi-peak fitting was found to be superior. The first use of the method was a study of recovery of a deformed aluminium alloy (AA1050). The aluminium alloy was deformed by cold rolling to a thickness...

  13. 铝合金方管开孔柱轴压性能研究%RESEARCH ON BEHAVIOR OF ALUMINIUM ALLOY SHS COLUMNS WITH HOLES UNDER AXIAL COMPRESSION

    Institute of Scientific and Technical Information of China (English)

    冯然; 马义红; 张长锐

    2016-01-01

    采用试验研究和有限元数值分析方法,对6061-T6系列的铝合金方管开孔柱的轴心受压性能进行研究,建立了同时考虑材料非线性和几何非线性的有限元数值模型,对短柱和中长柱的屈曲模式进行模拟,并通过数值模拟结果提出了开孔柱极限承载力的计算方法。利用该有限元模型针对孔洞的存在、大小、数目、位置对铝合金开孔柱的承载力和屈曲模式的影响进行了全面的分析,并通过对比铝合金未开孔轴心受压构件的计算方法与冷弯薄壁型钢开孔轴心受压构件的计算方法,结合数值模拟结果,提出了铝合金开孔轴心受压构件的计算公式。%The experimental study and FE numerical analysis were conducted on 6061-T6 aluminium alloy square hollow section ( SHS) columns with hole under axial compression. Both material and geometrical nonlinearities were considered in the finite element analysis. The accurate finite element models were developed for the buckling analysis of aluminium alloy stub and intermediate columns. Based on the numerical results, the design rules were proposed for the load carrying capacity of aluminium alloy SHS columns with holes. The effects of the existence, size, amount and location of the holes on the load carrying capacity and buckling modes of aluminium alloy SHS columns were evaluated. The design formulas were derived for the aluminium alloy axially compressed members with holes based on the design rules of aluminium alloy structural members and cold-formed steel thin-walled perforated members.

  14. Regarding to the Variance Analysis of Regression Equation of the Surface Roughness obtained by End Milling process of 7136 Aluminium Alloy

    Science.gov (United States)

    POP, A. B.; ȚÎȚU, M. A.

    2016-11-01

    In the metal cutting process, surface quality is intrinsically related to the cutting parameters and to the cutting tool geometry. At the same time, metal cutting processes are closely related to the machining costs. The purpose of this paper is to reduce manufacturing costs and processing time. A study was made, based on the mathematical modelling of the average of the absolute value deviation (Ra) resulting from the end milling process on 7136 aluminium alloy, depending on cutting process parameters. The novel element brought by this paper is the 7136 aluminium alloy type, chosen to conduct the experiments, which is a material developed and patented by Universal Alloy Corporation. This aluminium alloy is used in the aircraft industry to make parts from extruded profiles, and it has not been studied for the proposed research direction. Based on this research, a mathematical model of surface roughness Ra was established according to the cutting parameters studied in a set experimental field. A regression analysis was performed, which identified the quantitative relationships between cutting parameters and the surface roughness. Using the variance analysis ANOVA, the degree of confidence for the achieved results by the regression equation was determined, and the suitability of this equation at every point of the experimental field.

  15. Safety-relevant components made of low-iron, Al-base die-casting alloys; Sicherheitsbauteile aus eisenarmen Aluminium-Druckgusslegierungen

    Energy Technology Data Exchange (ETDEWEB)

    Hielscher, U. [Aluminium Rheinfelden GmbH, Rheinfelden (Germany)

    1999-07-01

    The modern automotive engineering requirements to be met by die-casting aluminium alloys with respect to the microstructure, casting process, compatibility with operating media, and weldability are such that they cannot be met by conventional alloys. Therefore, there was a quest for novel alloys, which at the Aluminium Rheinfelden company has led to the development of two low-iron alloys: Silafont-36 (AlSi9MgMnSr), and Magsimal-59 (AlMg5Si2Mn). The materials properties and some applications are explained. (orig./MM) [German] Von der Automobilindustrie werden an die Aluminiumguss-Legierungen folgende Anforderungen gestellt: 1. sehr duktiles Gefuege, 2. gute Giessbarkeit fuer das Druckgiessverfahren, 3. Vertraeglichkeit mit den Eisenwerkstoffen der Giesswerkzeuge sowie Trenn- und Schmierstoffen, 4. gute Schweissbarkeit und gute Boerdelbarkeit. Die herkoemmlichen Gusslegierungen erfuellen diese Anforderungen nicht; der Aluminium Rheinfelden gelang die Entwicklung von zwei eisenarmen Legierungen: Silafont-36 (AlSi9MgMnSr) und Magsimal-59 (AlMg5Si2Mn). (orig.)

  16. A study of the influence of precipitate-free zones on the strain localization and failure of the aluminium alloy AA7075-T651

    Science.gov (United States)

    Fourmeau, M.; Marioara, C. D.; Børvik, T.; Benallal, A.; Hopperstad, O. S.

    2015-10-01

    Age-hardened aluminium alloys have various degrees of precipitate-free zones (PFZs) along grain boundaries (GBs). The PFZs are weak zones and their existence promotes combined transgranular and intergranular fracture, thus reducing the ductility of the alloy. In this study, transmission electron microscopy (TEM) is used to display the geometrical properties and the chemical composition of the PFZs in the AA7075-T651 aluminium alloy. PFZs are found along grain and sub-GBs and their widths are about 40 and 20 nm, respectively. The PFZs are depleted of alloying elements compared with the nominal composition due to GB precipitation, but still they contain a certain amount of such elements in solid solution which will contribute to increase the yield strength and the work hardening compared to pure aluminium. Based on the results from the TEM study, a micromechanical finite element model of an idealized microstructure including grains and soft zones along the GBs is established. The Gurson model was used to represent the behaviour of the material in the grains and in the soft zones, using different initial void volume fractions to account for GB precipitation. Several loading conditions were applied to the micromechanical model in order to evaluate the localization of strains inside the soft zones and thus to get a better understanding of the role of the PFZs in ductile fracture of age-hardened aluminium alloys. It was found that the global failure strain varies non-monotonically with the global stress triaxiality due to the heterogeneity of the idealized microstructure.

  17. Hydrogen generation by the hydrolysis reaction of ball-milled aluminium-lithium alloys

    Science.gov (United States)

    Chen, Xingyu; Zhao, Zhongwei; Liu, Xuheng; Hao, Mingming; Chen, Ailiang; Tang, Zhongyang

    2014-05-01

    The addition of Li can prevent an inert alumina film from forming on the surface of Al alloy particles, allowing the rapid hydrogen generation of Al alloys to be achieved. However, because the Li content is less than 10%, the hydrogen generation rate and hydrogen yield of Al-Li alloys are significantly decreased. In this work, NaCl is introduced to prepare Al-Li alloys with low Li contents by ball milling. The research results show that by increasing the amount of NaCl added, the ball milling time and Li content can effectively improve the hydrogen generation of the alloys. Under optimal preparation conditions, the ultimate hydrogen yield of Al-Li alloys can reach 100%. The initial water temperature has almost no effect on the generation of hydrogen, even at 0 °C. Ca2+ and Mg2+ can combine with OH- to form the insoluble compounds Ca(OH)2 and Mg(OH)2, which can prevent hydrogen generation. NO3- reacts with Al to form ammonia and reduce the hydrogen yield of the alloys. Therefore, Al-Li alloys should be prevented from reacting with water containing Ca2+, Mg2+ and NO3-. Al-Li alloys must be stored in isolation from air to maintain good hydrogen-generation performances.

  18. Corrosion properties of plasma electrolytic oxidation coatings on an aluminium alloy – The effect of the PEO process stage

    Energy Technology Data Exchange (ETDEWEB)

    Dehnavi, Vahid, E-mail: vdehnavi@uwo.ca [Department of Chemical and Biochemical Engineering, University of Western Ontario, London, N6A 5B9 ON (Canada); Shoesmith, David W., E-mail: dwshoesm@uwo.ca [Surface Science Western, Department of Chemistry, University of Western Ontario, London, N6A 5B7 ON (Canada); Luan, Ben Li, E-mail: Ben.Luan@nrc-cnrc.gc.ca [National Research Council Canada, 800 Collip Circle, London, N6G4X8 ON (Canada); Department of Chemistry, University of Western Ontario, London, N6A 5B7 ON (Canada); Yari, Mehdi, E-mail: myari@uwo.ca [Department of Chemistry, University of Western Ontario, London, N6A 5B7 ON (Canada); Liu, Xing Yang, E-mail: XingYang.Liu@nrc-cnrc.gc.ca [National Research Council Canada, 800 Collip Circle, London, N6G4X8 ON (Canada); Rohani, Sohrab, E-mail: srohani@uwo.ca [Department of Chemical and Biochemical Engineering, University of Western Ontario, London, N6A 5B9 ON (Canada)

    2015-07-01

    Plasma electrolytic oxidation (PEO) coatings were grown on an aluminium alloy substrate using different processing parameters which enabled samples to be coated to different stages of the PEO process. Electrochemical impedance spectroscopy (EIS) and linear polarization resistance (LPR) techniques were employed to investigate the impedance properties of the resulting oxide coatings which will determine the corrosion performance of the coated alloy. Scanning electron microscopy was used to relate the morphology of the coatings with their corrosion performance. A direct relationship was found between the stage of the PEO process, which affects the microstructure of the coatings, and the corrosion performance. Coating thickness and phase composition did not have any measurable influence on coating corrosion performance. To some degree corrosion performance could be tailored by the processing parameters. - Highlights: • Corrosion performance of PEO coatings was found to be dependent on coating stage. • The PEO stage determined by the process parameters controlled coatings morphology. • Samples coated at the end of stage 3 demonstrated better corrosion properties. • Coating thickness and phase composition showed no influence on corrosion resistance.

  19. MICROSTRUCTURAL CHARACTERISATION AND CORROSION BEHAVIOUR OF TOP SURFACE OF TIG WELDED 2219−T87 ALUMINIUM ALLOY

    Directory of Open Access Journals (Sweden)

    G. Venkatasubramanian

    2013-03-01

    Full Text Available The microstructural characterisation and corrosion behaviour of top surface of tungsten inert gas (TIG welded 2219−T87 aluminium alloy (AA2219–T87 in 0.6 M NaCl solution was studied by optical microscopy, scanning electron microscopy (SEM, potentiodynamic polarisation, and electrochemical impedance spectroscopy (EIS. The optical microscopy and SEM analyses revealed that the welding of base metal (BM with ER2319 filler alloy caused the formation of micro pores and micro cracks on the surface of weld zone (WZ while the welding heat caused the dissolution and segregation of CuAl2 intermetallic particles along the grain boundaries in the heat affected zone (HAZ. The anodic and cathodic branches of polarisation curves showed that the HAZ has lower corrosion resistance than WZ and BM. The decrease of charge transfer resistance of HAZ when comparedto WZ and BM obtained by electrochemical impedance spectroscopy (EIS further confirmed its higher corrosion rate in 0.6 M NaCl solution.

  20. Effect of Mg, Si and Cu content on the microstructure of dilute 6000 series aluminium alloys

    Energy Technology Data Exchange (ETDEWEB)

    Jaafar, Aiza, E-mail: cnaizza@gmail.com [School of Materials and Mineral Resources Engineering, Universiti Sains Malaysia, 14300 Nibong Tebal, Penang (Malaysia); Rahmat, Azmi [School of Materials Engineering, Universiti Malaysia Perlis, Taman Muhibah, 02600 Jejawi, Arau Perlis (Malaysia); Hussain, Zuhailawati [School of Materials and Mineral Resources Engineering, Universiti Sains Malaysia, 14300 Nibong Tebal, Penang (Malaysia); Zainol, Ismail [Chemistry Department, Faculty of Science and Mathematics, Universiti Pendidikan Sultan Idris, 35900 Tanjung Malim, Perak (Malaysia)

    2011-09-01

    Highlights: > The main precipitates formed in the artificially aged dilute alloys are needle-shaped. > The ageing temperature of 100 deg. C is found to be too low to form precipitates. > The number density of precipitates increases with increasing solute contents. > There is a correlation between Mg{sub 2}Si, Si and Cu content and alloys microstructure. > The precipitates kinetics is faster in the less dilute alloys. - Abstract: The effect of Mg, Si and Cu content on the microstructural development during ageing treatment of dilute 6000 series alloys have been investigated using transmission electron microscopy (TEM). Four dilute alloys were used in this study. These alloys were subjected to quenching and artificial ageing at 100 deg. C, 185 deg. C and 300 deg. C. The microstructural developments of the precipitates formed were monitored by TEM. The ageing temperature of 100 deg. C was found to be too low to form precipitates. It was found that needle or rod-shaped precipitates were formed in the alloys after ageing at 185 and 300 deg. C. Prolong ageing up to 1000 h at 300 deg. C resulted in the formation of Mg{sub 2}Si precipitate that coexists with the type of AlFeSi and Si precipitates. The results show a correlation between the Mg{sub 2}Si, Si and Cu content on the microstructure of the four dilute alloys after ageing treatment.

  1. Corrosion of boiler tube alloys in refuse firing: Shredded vs bulk refuse

    Energy Technology Data Exchange (ETDEWEB)

    Krause, H.H. (Battelle, Columbus, OH (United States)); Daniel, P.L.; Blue, J.D. (Babcock Wilcox, Barberton, OH (United States))

    1994-08-01

    Results of corrosion probe exposures at two mass burning incinerators were compared with those conducted in a unit burning refuse-derived fuel. Tests were conducted with carbon steel, low-alloy steels, stainless steels, and high nickel-chromium alloys. Corrosion rates at similar metal and gas temperatures were essentially the same for both types of fuel. Boiler tube performance in the waterwalls of other incinerators confirmed these results. Boiler design and operating conditions appear to be more important factors in tube wastage than the extent of refuse processing.

  2. Effect of post weld heat treatment on tensile properties and microstructure characteristics of friction stir welded armour grade AA7075-T651 aluminium alloy

    Directory of Open Access Journals (Sweden)

    P. Sivaraj

    2014-03-01

    Full Text Available This paper reports the effects of post weld heat treatments, namely artificial ageing and solution treatment followed by artificial ageing, on microstructure and mechanical properties of 12 mm thick friction stir welded joints of precipitation hardenable high strength armour grade AA7075-T651 aluminium alloy. The tensile properties, such as yield strength, tensile strength, elongation and notch tensile strength, are evaluated and correlated with the microhardness and microstructural features. The scanning electron microscope is used to characterie the fracture surfaces. The solution treatment followed by ageing heat treatment cycle is found to be marginally beneficial in improving the tensile properties of friction stir welds of AA7075-T651 aluminium alloy.

  3. XPS Study of Chemical Changes on the La/Ce Treated Surface of A361 Aluminium Alloy Exposed to Air at Temperatures up to 500∘C

    Directory of Open Access Journals (Sweden)

    A. Pardo

    2009-01-01

    Full Text Available The chemical changes that take place on the rare earth treated surface of the A361 aluminium alloy exposed to air at temperatures between 100 and 500∘C have been examined using X-ray photoelectron spectroscopy (XPS. The most notable features discussed in this work are the disappearance of Mg and Si signals at the tested temperatures and disappearance of the Ce signal at temperatures of 400–500∘C. The biphasic microstructure of the A361 alloy, constituted by close to 12 wt% Si and the Al matrix, plays an important role in many of the results obtained. The notable growth of aluminium oxide across the conversion coating in the case of the Ce-treated surface is related to the structural transformation experienced by the cerium oxide coating at 400–500∘C.

  4. Investigating of the Effect of Rectangular and Trapezium Cross Section of Gating System by CFD Simulation in Cooling of Aluminium Alloy in a Permanent Mould Casting

    Directory of Open Access Journals (Sweden)

    N. A. Chowdhury

    2012-01-01

    Full Text Available This paper presents a systemic study of the effect of different cross section of gate in permanent mould casting of aluminium alloy. To ensure best quality of the product the mould cavity must be filled with clean metal in a controlled manner to ensure smooth, uniform and complete filling. A gating system controls smooth, uniform and complete filling of the cavity by the molten metal. In this paper, CFD models illustrating the effect of rectangular and trapezium cross sections of gating on cooling of Aluminium alloy in a permanent mould casting were investigated. Same hydraulic diameter was assigned for each of the cross section of gating systems. Bottom gating system is used for its low gas entrapment and less surface defect characteristics. By analyzing it has been observed that in rectangular cross section the cooling is more rapid than trapezium cross sections considered in the investigation.

  5. Impact of M2-Hss Tool Pin Profile in Fsw Welded Joints On Mechanical Properties Of Aa7075-T6 Aluminium Alloy

    Directory of Open Access Journals (Sweden)

    Venugopal S

    2014-05-01

    Full Text Available Friction stir, “welding is a solid state joining process and is widely being considered for aluminium alloys. The main advantage of FSW is the material that is being welded undergoes only localized changes. The welding parameter and tool pin profile play a major role in deciding the weld quality. In this work an effort has been made to analyze microstructure of aluminium AA 7075-T6 alloy. Three different tool profiles (Taper Threaded, cylindrical and square have been used to construct the joints in particular rotational speed. Tensile, Impact, micro hardness of mechanical properties of the joints have been evaluated and the formation of FSP zone has been analyzed microscopically. From the investigation it is found that the threaded cylindrical profile produces highly (defined Strength in welds.

  6. Evaluating the Applicability of GTN Damage Model in Forward Tube Spinning of Aluminum Alloy

    Directory of Open Access Journals (Sweden)

    Xianxian Wang

    2016-06-01

    Full Text Available Tube spinning is an effective plastic-forming technology for forming light-weight, high-precision and high-reliability components in high-tech fields, such as aviation and aerospace. However, cracks commonly occur in tube spinning due to the complexity of stress state, which severely restricts the improvement of the forming quality and forming limit of components. In this study, a finite element (FE model coupled with Gurson-Tvergaard-Needleman (GTN damage model for forward tube spinning of 3A21-O aluminum alloy is established and its applicability is evaluated by experiment. Meanwhile, the GTN damage model is employed to study the damage evolution for forward tube spinning of 3A21-O aluminum alloy. The results show that the FE model is appropriate for predicting the macroscopic crack appearing in uplift area for forward tube spinning, while the damage evolution in deformation area could not be predicted well due to the negative stress triaxiality and the neglect of shear deformation. Accumulation of damage in forward tube spinning occurs mainly in the uplift area. Void volume fraction (VVF in the outer surface of the tube is higher than that in the inner surface. In addition, it is prone to cracking in the outer surface of tube in the material uplift area.

  7. Al-Ti-C中间合金的制备及其在4032铝合金中的应用%Synthesis of Al-Ti-C master alloy and its application in 4032 aluminium alloy

    Institute of Scientific and Technical Information of China (English)

    张静; 赵婧婧; 杜勇

    2014-01-01

    采用元素直接合成法,以工业纯铝、钛屑及石墨颗粒为原料制备Al-Ti-C中间合金,研究和评价了Al-Ti-C中间合金的显微组织及其对4032铝合金铸态组织和活塞模锻件组织的影响。结果表明,制备的Al-Ti-C中间合金由Al基体、长条状Al3 Ti相和细小粒状TiC相,以及少量的游离 C组成。将其应用于4032铝合金中,起到了明显的铸态晶粒细化效果。用该合金制备的活塞模锻件,显微组织和性能优良。%Al-Ti-C master alloy were synthesized by commercial-purity Al billet , Ti powder and graphite particles .The microstructure of the Al-Ti-C master alloy was studied .The grain refinement effects of the master alloy on the as-cast microstructure of 4032 aluminium alloy and the microstructure of mould forging piston fabricated by 4032 aluminium alloy were evaluated .The results show that Al-Ti-C master alloy is composed of Al matrix, long lath Al3Ti phase, fine TiC particles, and small amount of free carbon.With the addition of the master alloy, the as-cast microstructure of 4032 aluminium alloy is observed to be dramatically refined .The modified alloy was used to fabricate mould forging piston.It is found the piston manifests excellent microstructure and properties .

  8. Fatigue behavior of GMAW welded Aluminium alloy AA7020; Comportamiento a fatiga de uniones soldadas GMAW de la aleacion de aluminio AA 7020

    Energy Technology Data Exchange (ETDEWEB)

    Bloem, C. A.; Salvador, M. D.; Amigo, V.; Vicente, A.

    2007-07-01

    The aim of this investigation is to evaluate the influence on the fatigue behavior by the finishing of the bulge in a welded aluminium-zinc-magnesium alloy AA7020. It was determined that total or partial elimination of the bulge has very little influence on its behavior, giving a very similar result on both cases, where one is better than the other by only 3%. (Author) 20 refs.

  9. Correlation of seawater corrosion and processing of Cu-Ni alloy tubes

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    The investigetions on the effect of the initial surface and microstructure on the seawater corrosion of Cu-Ni al-loy tubes were carried out by processing, electrochemical methods and natural seawater exposure as well as SEM. Defor-mation had more impact on the final microstructure of the tubes than the annealing time did, and at the deformation of32% and annealing temperature 550~ 600 ℃ for 1 h the tubes was completely recrystallized microstructure. As increasingthe volume fraction of recrystallization, the homogeneity of microstructure and the corrosion resistance increased. Theresidual carbon film produced on the inner surface of the tubes during the processing, had higher corrosion potential thanthe alloy subatrate and good electronic conductivity, so accelerating the dissolution of the substrate in seawater, and thenon-protective and loose corrosion product film formed. Immersed in natural seawater, the tubes of incomplete recrystal-lization, consisting of deformed and recrystallized grains, displayed intergranular corrosion, which resulted from corrosionmicro-cells built between deformed and recrystallized grains and the preferable transportation of electrons on the boundariesof both the grains. In contrast, the recrystallized alloy tubes formed the uniform and compact corrosion product film underwhich no corrosion was found

  10. Influence of Various Process Parameters on the Density of Sintered Aluminium Alloys

    Directory of Open Access Journals (Sweden)

    Mateusz Laska

    2012-01-01

    Full Text Available This paper presents the results of density measurements carried out on Alumix sintered parts. ECKA Alumix aluminium powders were used because of their wide application in the powder metallurgy industry. The compacts were produced using a wide range of compaction pressures for three different chemical compositions. The compacts were then sintered under a pure dry nitrogen atmosphere at three different temperatures. The heating and cooling rates were the same throughout the entire test. The results showed that the green density increases with compaction pressure, but that sintered density is independent of green density (compaction pressure for each sintering temperature.

  11. Comparative Investigation on Modal analysis of LM25 Aluminium alloy with other Aluminim alloys using Finite element analysis software

    Science.gov (United States)

    Arunkumar, S.; Baskaralal, V. P. M.; Muthuraman, V.

    2017-03-01

    The rudimentary steps of the modal analysis and simulation are carried out. The modal analysis is carried out on the different Aluminum Alloys cantilever beam. The cantilever beam is designed in the graphical environment of the ANSYS. The cantilever beam was fine-tuned on one end with all degree of liberation on this end were taken, beam cannot move and rotate. Mode shapes and natural frequencies are premeditated in platforms ANSYS with arithmetical formulation of the direct solver including the block Lanczos method. Aluminum alloys are widely utilized in much application due to their estimable weight to vigor property. Many examination works have been distributed out to make developments the mechanical properties of aluminum alloys. The composition of alloying elements plays a consequential role in deciding the properties of an alloy. In this study a numerical analysis implement i.e., finite element analysis (FEA) is utilized. The work obtainable in this paper is aimed at the study of effect of modal analysis of different aluminum alloys. The modeling and analysis is carried out utilizing ANSYS FEA software. A modal analysis is carried out to understand the modes of frequency demeanor of the material considered. The modal analysis play a vital role in the design of components subjected to high vibration.

  12. Ballistic behavior of boron carbide reinforced AA7075 aluminium alloy using friction stir processing–An experimental study and analytical approach

    Institute of Scientific and Technical Information of China (English)

    I. SUDHAKAR; G. MADHUSUDHAN REDDY; K. SRINIVASA RAO

    2016-01-01

    High strength-to-weight ratio of non-ferrous alloys, such as aluminium, magnesium and titanium alloys, are considered to be possible replacement of widely accepted steels in transportation and automobile sectors. Among these alloys, magnesium is self explosive and titanium is costlier, and aluminium is most likely to replace steels. Application of aluminium or its alloys is also thought of as an appropriate replacement in defence field, especially to enhance the easiness in mobility of combat vehicles while maintaining the same standard as that of conventional armour grade steels. Hence most of the investigations have been confined to aluminium or its alloys as base material and open an era of developing the newer composite materials to address the major limitation, i.e. tribological properties. The surface composites can be fabricated by incorporating the ceramic carbides like silicon carbide, carbides of transition metals and oxides of aluminium using surface modification techniques, such as high energy laser melt treatment, high energy electron beam irradiation and thermal spray process which are based on fusion route. These techniques yield the fusion related problems, such as interfacial reaction, pin holes, shrinkage cavities or voids and other casting related defects, and pave the way to need of an efficient technique which must be based on solid state. Recently developed friction stir processing technique was used in the present investigation for surface modification of AA7075 aluminum alloy, which is an alternative to steels. In the present investigation, 160μm sized boron carbide powder was procured and was reduced to 60μm and 30μm using high energy ball mill. Subsequently these powders were used to fabricate the surface composites using friction stir processing. Ballistic performance testing as per the military standard (JIS.0108.01) was carried out. In the present work, an analytical method of predicting the ballistic behavior of surface composites

  13. Fabrication of Aluminum Tubes Filled with Aluminum Alloy Foam by Friction Welding

    Directory of Open Access Journals (Sweden)

    Yoshihiko Hangai

    2015-10-01

    Full Text Available Aluminum foam is usually used as the core of composite materials by combining it with dense materials, such as in Al foam core sandwich panels and Al-foam-filled tubes, owing to its low tensile and bending strengths. In this study, all-Al foam-filled tubes consisting of ADC12 Al-Si-Cu die-cast aluminum alloy foam and a dense A1050 commercially pure Al tube with metal bonding were fabricated by friction welding. First, it was found that the ADC12 precursor was firmly bonded throughout the inner wall of the A1050 tube without a gap between the precursor and the tube by friction welding. No deformation of the tube or foaming of the precursor was observed during the friction welding. Next, it was shown that by heat treatment of an ADC12-precursor-bonded A1050 tube, gases generated by the decomposition of the blowing agent expand the softened ADC12 to produce the ADC12 foam interior of the dense A1050 tube. A holding time during the foaming process of approximately tH = 8.5 min with a holding temperature of 948 K was found to be suitable for obtaining a sound ADC12-foam-filled A1050 tube with sufficient foaming, almost uniform pore structures over the entire specimen, and no deformation or reduction in the thickness of the tube.

  14. CROSS-ROLL FLOW FORMING OF ODS ALLOY HEAT EXCHANGER TUBES FOR HOOP CREEP ENHANCEMENT

    Energy Technology Data Exchange (ETDEWEB)

    Bimal K. Kad

    2004-08-31

    Mechanically alloyed oxide dispersion strengthened (ODS) Fe-Cr-Al alloy thin walled tubes and sheets, produced via powder processing and consolidation methodologies, are promising materials for eventual use at temperatures up to 1200 C in the power generation industry, far above the temperature capabilities of conventional alloys. Target end-uses range from gas turbine combustor liners to high aspect ratio (L/D) heat exchanger tubes. Grain boundary creep processes at service temperatures, particularly those acting in the hoop direction, are the dominant failure mechanisms for such components. The processed microstructure of ODS alloys consists of high aspect ratio grains aligned parallel to the tube axis, a result of dominant axial metal flow which aligns the dispersoid particles and other impurities in the longitudinal direction. The dispersion distribution is unaltered on a micro scale by recrystallization thermal treatments, but the high aspect ratio grain shape typically obtained limits transverse grain spacing and consequently the hoop creep response. Improving hoop creep in ODS-alloy components will require understanding and manipulating the factors that control the recrystallization behavior, and represents a critical materials design and development challenge that must be overcome in order to fully exploit the potential of ODS alloys. The objectives of this program are to (1) increase creep-strength at temperature in ODS-alloy tube and liner components by 100% via, (2) preferential cross-roll flow forming and grain/particle fibering in the critical hoop direction. Recent studies in cross-rolled ODS-alloy sheets (produced from flattened tubes) indicate that transverse creep is significantly enhanced via controlled transverse grain fibering, and similar improvements are expected for cross-rolled tubes. The research program outlined here is iterative in nature and is intended to systematically (i) prescribe extrusion consolidation methodologies via detailed

  15. CROSS-ROLL FLOW FORMING OF ODS ALLOY HEAT EXCHANGER TUBES FOR HOOP CREEP ENHANCEMENT

    Energy Technology Data Exchange (ETDEWEB)

    Bimal K. Kad

    2004-03-31

    Mechanically alloyed oxide dispersion strengthened (ODS) Fe-Cr-Al alloy thin walled tubes and sheets, produced via powder processing and consolidation methodologies, are promising materials for eventual use at temperatures up to 1200 C in the power generation industry, far above the temperature capabilities of conventional alloys. Target end-uses range from gas turbine combustor liners to high aspect ratio (L/D) heat exchanger tubes. Grain boundary creep processes at service temperatures, particularly those acting in the hoop direction, are the dominant failure mechanisms for such components. The processed microstructure of ODS alloys consists of high aspect ratio grains aligned parallel to the tube axis, a result of dominant axial metal flow which aligns the dispersoid particles and other impurities in the longitudinal direction. The dispersion distribution is unaltered on a micro scale by recrystallization thermal treatments, but the high aspect ratio grain shape typically obtained limits transverse grain spacing and consequently the hoop creep response. Improving hoop creep in ODS-alloy components will require understanding and manipulating the factors that control the recrystallization behavior, and represents a critical materials design and development challenge that must be overcome in order to fully exploit the potential of ODS alloys. The objectives of this program are to (1) increase creep-strength at temperature in ODS-alloy tube and liner components by 100% via, (2) preferential cross-roll flow forming and grain/particle fibering in the critical hoop direction. Recent studies in cross-rolled ODS-alloy sheets (produced from flattened tubes) indicate that transverse creep is significantly enhanced via controlled transverse grain fibering, and similar improvements are expected for cross-rolled tubes. The research program outlined here is iterative in nature and is intended to systematically (1) prescribe extrusion consolidation methodologies via detailed

  16. CROSS-ROLL FLOW FORMING OF ODS ALLOY HEAT EXCHANGER TUBES FOR HOOP CREEP ENHANCEMENT

    Energy Technology Data Exchange (ETDEWEB)

    Bimal K. Kad

    2004-05-31

    Mechanically alloyed oxide dispersion strengthened (ODS) Fe-Cr-Al alloy thin walled tubes and sheets, produced via powder processing and consolidation methodologies, are promising materials for eventual use at temperatures up to 1200 C in the power generation industry, far above the temperature capabilities of conventional alloys. Target end-uses range from gas turbine combustor liners to high aspect ratio (L/D) heat exchanger tubes. Grain boundary creep processes at service temperatures, particularly those acting in the hoop direction, are the dominant failure mechanisms for such components. The processed microstructure of ODS alloys consists of high aspect ratio grains aligned parallel to the tube axis, a result of dominant axial metal flow which aligns the dispersoid particles and other impurities in the longitudinal direction. The dispersion distribution is unaltered on a micro scale by recrystallization thermal treatments, but the high aspect ratio grain shape typically obtained limits transverse grain spacing and consequently the hoop creep response. Improving hoop creep in ODS-alloy components will require understanding and manipulating the factors that control the recrystallization behavior, and represents a critical materials design and development challenge that must be overcome in order to fully exploit the potential of ODS alloys. The objectives of this program are to (1) increase creep-strength at temperature in ODS-alloy tube and liner components by 100% via, (2) preferential cross-roll flow forming and grain/particle fibering in the critical hoop direction. Recent studies in cross-rolled ODS-alloy sheets (produced from flattened tubes) indicate that transverse creep is significantly enhanced via controlled transverse grain fibering, and similar improvements are expected for cross-rolled tubes. The research program outlined here is iterative in nature and is intended to systematically (1) prescribe extrusion consolidation methodologies via detailed

  17. CROSS-ROLL FLOW FORMING OF ODS ALLOY HEAT EXCHANGER TUBES FOR HOOP CREEP ENHANCEMENT

    Energy Technology Data Exchange (ETDEWEB)

    Bimal K. Kad

    2004-11-30

    Mechanically alloyed oxide dispersion strengthened (ODS) Fe-Cr-Al alloy thin walled tubes and sheets, produced via powder processing and consolidation methodologies, are promising materials for eventual use at temperatures up to 1200 C in the power generation industry, far above the temperature capabilities of conventional alloys. Target end-uses range from gas turbine combustor liners to high aspect ratio (L/D) heat exchanger tubes. Grain boundary creep processes at service temperatures, particularly those acting in the hoop direction, are the dominant failure mechanisms for such components. The processed microstructure of ODS alloys consists of high aspect ratio grains aligned parallel to the tube axis, a result of dominant axial metal flow which aligns the dispersoid particles and other impurities in the longitudinal direction. The dispersion distribution is unaltered on a micro scale by recrystallization thermal treatments, but the high aspect ratio grain shape typically obtained limits transverse grain spacing and consequently the hoop creep response. Improving hoop creep in ODS-alloy components will require understanding and manipulating the factors that control the recrystallization behavior, and represents a critical materials design and development challenge that must be overcome in order to fully exploit the potential of ODS alloys. The objectives of this program are to (1) increase creep-strength at temperature in ODS-alloy tube and liner components by 100% via, (2) preferential cross-roll flow forming and grain/particle fibering in the critical hoop direction. Recent studies in cross-rolled ODS-alloy sheets (produced from flattened tubes) indicate that transverse creep is significantly enhanced via controlled transverse grain fibering, and similar improvements are expected for cross-rolled tubes. The research program outlined here is iterative in nature and is intended to systematically (i) prescribe extrusion consolidation methodologies via detailed

  18. CROSS-ROLL FLOW FORMING OF ODS ALLOY HEAT EXCHANGER TUBES FOR HOOP CREEP ENHANCEMENT

    Energy Technology Data Exchange (ETDEWEB)

    Bimal K. Kad

    2005-02-28

    Mechanically alloyed oxide dispersion strengthened (ODS) Fe-Cr-Al alloy thin walled tubes and sheets, produced via powder processing and consolidation methodologies, are promising materials for eventual use at temperatures up to 1200 C in the power generation industry, far above the temperature capabilities of conventional alloys. Target end-uses range from gas turbine combustor liners to high aspect ratio (L/D) heat exchanger tubes. Grain boundary creep processes at service temperatures, particularly those acting in the hoop direction, are the dominant failure mechanisms for such components. The processed microstructure of ODS alloys consists of high aspect ratio grains aligned parallel to the tube axis, a result of dominant axial metal flow which aligns the dispersoid particles and other impurities in the longitudinal direction. The dispersion distribution is unaltered on a micro scale by recrystallization thermal treatments, but the high aspect ratio grain shape typically obtained limits transverse grain spacing and consequently the hoop creep response. Improving hoop creep in ODS-alloy components will require understanding and manipulating the factors that control the recrystallization behavior, and represents a critical materials design and development challenge that must be overcome in order to fully exploit the potential of ODS alloys. The objectives of this program are to (1) increase creep-strength at temperature in ODS-alloy tube and liner components by 100% via, (2) preferential cross-roll flow forming and grain/particle fibering in the critical hoop direction. Recent studies in cross-rolled ODS-alloy sheets (produced from flattened tubes) indicate that transverse creep is significantly enhanced via controlled transverse grain fibering, and similar improvements are expected for cross-rolled tubes. The research program outlined here is iterative in nature and is intended to systematically (i) prescribe extrusion consolidation methodologies via detailed

  19. Interfacial heat-transfer between A356-aluminium alloy and metal mould

    Institute of Scientific and Technical Information of China (English)

    Zhao Jianhua; Tian Jun; Qian Hancheng

    2009-01-01

    The interracial heat-transfer coefficient at casting/mould interface is a key factor that impacts the simulation accuracy of solidification progress. At present, the simulation result of using available data is comparatively different from the practice. In the current study, the methods of radial heating and electricity measurement under steady-state condition were employed to study the nature of interfacial heat-transfer between A356 Aluminum alloy and metal mould. The experimental results show that the interracial heat-transfer between A356 Aluminum alloy and the outer mould drops linearly with time while that of A356 aluminum alloy and the inner mould increases with time during cooling. The interracial heat-transfer coefficient between A356 aluminum alloy and mould is inversely proportional to the electrical resistance.

  20. Evaluation of pitting corrosion with electrochemical impedance spectroscopy (EIS) for alumina/aluminium alloys composites

    Energy Technology Data Exchange (ETDEWEB)

    Odegard, C.; Bronson, A. [Univ. of Texas, El Paso, TX (United States)

    1998-12-31

    The pitting susceptibility of monolithic aluminum 6061 alloy and alumina/aluminum alloy composites has been analyzed by using electrochemical impedance spectroscopy and subsequent comparison with their polarization scans. The composites consisting of 0.10 and 0.15 volume fraction of alumina particles (VFAP) and the monolith as cylindrical electrodes were rotated at 1500 rpm while immersed in NaCl solution. The passive currents of the composites were greater than that of the monolith as per the polarization scans. The impedance spectra were acquired at constant potential increments along the passive region up to the pitting potential. The impedance spectra represented by semicircles on a Nyquist plot acquired above the pitting potential collapsed underneath the spectra obtained in the passive region near the corrosion potential for the monolithic alloy and composites. The impedance spectra modeled with a simplified equivalent circuit indicate that the effective capacitance for the composites is greater than that of the monolithic alloy.

  1. Computer simulations of martensitic transformations in iron-nickel and nickel-aluminium alloys

    CERN Document Server

    Meyer, R J

    1998-01-01

    This thesis focuses on the martensitic transformations in iron-nickel and nickel-aluminum alloys. Molecular-dynamics simulations have been done, employing potentials based on the so-called embedded-atom method (EAM). These potentials were obtained by a fit of parameterized functions to experimental data of the elements iron, nickel, and aluminum as well as the intermetallic compound NiAl. Many aspects of the austenitic transformation in iron-nickel alloys and both, the martensitic and austenitic transformations, in nickel-aluminum alloys were reproduced well by the simulations. The results allow to draw conclusions on the reasons of differences and similarities in the behavior of both alloy systems.

  2. APPLICATION OF CHEMICAL PRE-TREATMENT ON THE POLISHED SURFACE OF ALUMINIUM ALLOYS

    Directory of Open Access Journals (Sweden)

    Pavel Kraus

    2016-12-01

    Full Text Available This paper reports the preparation and characterization of thin transparent nanolayers with phase composition ZrF4 and different modification of SiO2 with special focus on affecting the surface roughness of the material and the way of exclusion of the thin nanolayer on the surface of the polished aluminium material. The thin nanolayer was prepared by the sol-gel method. The final treatment based on PTFE was applied on the surface of some samples. This treatment is suitable for increasing wear resistance. The films were characterized with help of SEM microscopy and EDS analysis. The surface roughness was measured with classical surface roughness tester. The results on this theme have already published but not on the polished surface of the aluminium material. The results from the experiment show the problems with application of these nanolayers because a cracks were found on the surface of the material and deformations of the layer after application of the PTFE final layer. The surface layer formation is discussed.

  3. INTRODUCTION TO INCONEL ALLOY 740: AN ALLOY DESIGNED FOR SUPERHEATER TUBING IN COAL-FIRED ULTRA SUPERCRITICAL BOILERS

    Institute of Scientific and Technical Information of China (English)

    S.J. Patel

    2005-01-01

    Chinese utilities as well as those worldwide are facingincreased demand for additional electric-ity, reduced plant emissions and greater efficiency.To meet this challenge willrequire increas-ing boiler temperature,pressure and coal ashcorrosion resistance of the materials of boiler construction of future coal-fired boilers. A new nickel-based tube alloy, INCONELRalloy 740,is described aiming at meeting this challenge. Emphasis will be on describing the alloy s mechanical properties, coal-ash and steam corrosion resistance.Microstructural stability as a function of temperature and time is addressed as well as some of the early methodology employed to arrive at the current chemical composition.

  4. Recent developments of the aluminium-lithium system alloys for aircraft uses; Recentes desenvolvimentos das ligas do sistema aluminio-litio para fins aeronauticos

    Energy Technology Data Exchange (ETDEWEB)

    Goncalves, Marcelo; Plaut, Ronald Lesley

    1992-12-31

    A brief review is made of the latest developments in the production of Aluminium-Lithium alloys. The necessity for new materials in the field of aeronautics has speeded up research on metallic and non-metallic materials. Lately, a good part of the research in the field of metallic components has been directed at Al-Li alloys. More recently, with the development of quaternary alloys Al-Li-X-X, the old problem of low toughness was overcome. The finality of this study is to cover the developments of the mentioned alloys, including the fundamentals of physical metallurgy of the complex system recently developed Al-Li-Cu-Mg. (author) 27 refs., 2 figs., 4 tabs.

  5. Synergism between cerium nitrate and sodium dodecylbenzenesulfonate on corrosion of AA5052 aluminium alloy in 3 wt.% NaCl solution

    Science.gov (United States)

    Liu, Jie; Wang, Dapeng; Gao, Lixin; Zhang, Daquan

    2016-12-01

    The synergistic inhibition effect of rare earth cerium nitrate and sodium dodecylbenzenesulfonate (DBS) on corrosion of AA5052 aluminium alloy in 3 wt.% NaCl solution was investigated by electrochemical impedance spectroscopy (EIS), potentiodynamic polarization curve, scanning electron microscope (SEM) and Fourier transform infrared spectroscopy (FT-IR). The results show that the single cerium nitrate or DBS has a limited inhibition effect against corrosion of AA5052 alloy. The combination cerium ions with DBS produced strong synergistic effect on corrosion inhibition for AA5052 alloy and rendered a negaitve shift of the corrosion potential. The formation of the complex of Al(DBS)3 and Ce(DBS)3 stabilized the passive film of Al2O3 and CeO2, retarding both the cathodic and anodic processes of AA5052 alloy corrosion reaction significantly.

  6. Effect of thermal exposure on mechanical properties hypo eutectic aerospace grade aluminium-silicon alloy

    Science.gov (United States)

    Nagesh Kumar, R.; Ram Prabhu, T.; Siddaraju, C.

    2016-09-01

    The effect of thermal exposure on the mechanical properties of a C355.0 aerospace grade aluminum-silicon alloy (5% Si - 1.2% Cu - 0.5% Mg) was investigated in the present study. The alloy specimens were subjected to T6 (solution treatment and artificial ageing treatment) temper treatment to enhance the strength properties through precipitation hardening. The T6 temper treatment involved solution heat treatment at 520oC for 6h, followed by water quenching and ageing at 150oC. After the heat treatment, the specimens were exposed to various temperatures (50oC, 100oC, 150oC, 200oC and 250oC) for 5 and 10 h to study the structural applications of this alloy to the various Mach number military aircrafts. After the thermal exposure, specimens were tested for tensile, hardness and impact properties (Charpy). The microstructure of the thermal exposed specimens was examined in the optical microscopes and correlated with the mechanical properties results. In summary, an increase of exposure time has a different effect on the tensile and hardness properties of the alloy. For the exposure time 5h, the tensile and hardness properties increase upto 100oC and later decrease with an increase of temperature. In contrast, the tensile and hardness properties linearly decrease with an increase of temperature. Several factors such as matrix grain growth, diffusion rate, Si particles size and distribution, precipitate stability play a key role on deciding the tensile properties of the alloy. Comparing the relative effects of temperature and time, the temperature effects dominate more in deteriorating tensile properties of the alloy. There are no effects of exposure temperature and/or time on the impact properties of the alloy.

  7. NUMERICAL SIMULATION OF INDUCTION SKULL MELTING PROCESS FOR TITANIUM-ALUMINIUM BASE ALLOY

    Institute of Scientific and Technical Information of China (English)

    Z.Y. Chen; L.J. Xu; F.T. Kong; Q. Shu; Y.Y. Chen

    2004-01-01

    The mathematics model for temperature field of water-cooling copper crucible induction skull melting process was established. The program for simulating temperature field of melting process was developed with finite element method. The temperature field of the melting process for Ti-47Al-2Cr-2Nb alloy was calculated. During melting period, the temperature is raised gradually along radius augmentation direction. The elements of the charge near the crucible wall are molten first. The center elements of the charge are molten last. The melting time of the center element is just that of all the charge melting. The melting time of Ti-47Al-2Cr-2Nb alloy is 15min. In which, the charge was heated by low power 80kW for 9min and by high power 300kW for 6min. When melting Ti-47Al-2Cr-2Nb alloy,the loading power is nearly direct proportion to melt temperature. Increasing loading power may raise melt temperature. The best melting power of Ti-47Al-2Cr-2Nb alloy is 305-310kW. This is identical with the melting test and has guidance sense to the melting process of actual titanium alloy.

  8. Determination of Aluminium in lead-calcium-aluminium ternary alloy by chrome azurol Sphotometry%铬天青S光度法测定铅钙铝三元合金中铝

    Institute of Scientific and Technical Information of China (English)

    丁林立

    2001-01-01

    In the medium of hexamethylenetetramine buffer solution(pH 5-6) aluminium reacts with chrome azurol S to produce a water dissoluble purple complex.The absorption maximeum is at 545nm. This method has higher senitivity and better repeatability than that aluminon method. The proposed method is suitable for the determination of aluminium in the range of 0.01%-5% in Lead-Calcium-aluminium ternary alloy.%在六次甲基四胺缓冲溶液(pH5~6)介质中,铝与铬天青S生成 水溶性的紫红色络合物,其λmax=545nm。本法较铝试剂法具有较高 的灵敏度,并重复性好,适用于铅钙铝三元合金中0.01%~5%铝的 测定。

  9. An improved statistical model for predicting the deuterium ingress in zirconium alloy pressure tubes

    Energy Technology Data Exchange (ETDEWEB)

    Pandey, M.D., E-mail: mdpandey@uwaterloo.ca [Department of Civil and Environmental Engineering University of Waterloo, Waterloo, Ontario, N2L 3G1 (Canada); Xin, L. [Department of Civil and Environmental Engineering University of Waterloo, Waterloo, Ontario, N2L 3G1 (Canada)

    2012-09-15

    In the CANDU pressurized heavy water reactor (PHWR), the nuclear fuel is contained in hundreds of Zr-2.5 Nb alloy pressure tubes. The corrosion of zirconium alloy produces deuterium that is absorbed by the body of the pressure tube. The presence of this deuterium causes hydrogen embrittlement of zirconium alloy with an adverse effect on the integrity of the pressure tube. An accurate prediction of deuterium accumulation over time is an important step for ensuring the fitness-for-service of pressure tubes. Deuterium ingress data collected from in-service inspection of pressure tubes exhibit heteroscedasticity, i.e., the variance of deuterium concentration is dependent on operating time (or exposure) and temperature. The currently used model by the nuclear industry involves a logarithmic regression of deuterium content over time and temperature. Since this approach does not deal with heteroscedasticity precisely, it results in a conservative prediction of the deuterium ingress. The paper presents a new approach for predicting deuterium ingress based on a weighted least-squares (WLS) regression that overcomes the limitations of the existing model, and it provides realistic prediction bounds of deuterium ingress.

  10. Investigations on temperature distribution in welding of Aluminium alloys to steel using FEM

    Directory of Open Access Journals (Sweden)

    K. S. Ashraff Ali

    2015-01-01

    Full Text Available This research study focuses on the objective to establish an analytical model for determining the thermal distribution during friction stir welding (FSW, based on different assumptions of the contact condition between the rotating tool surface and the weld piece. The material flow and heat generation are characterized by the contact conditions at the interface, and are described as sliding, sticking or partial sliding/sticking. The analytical expression for the heat generation is a modification of previous analytical models known from the literature and accounts for both conical surfaces and different contact conditions. Aluminium metal matrix composites and steel 304 (dissimilar material joining is being used for this study. Three dimensional Finite Element Models have been developed to visualize the temperature distribution across the butt ends of the plates. The results are validated with the experimental results reported in the literature. The result reveals that there exists a good coherence between experimental and simulated results.

  11. Effects of as-cast and wrought Cobalt-Chrome-Molybdenum and Titanium-Aluminium-Vanadium alloys on cytokine gene expression and protein secretion in J774A.1 macrophages

    DEFF Research Database (Denmark)

    Jakobsen, Stig Storgaard; Larsen, Agnete; Stoltenberg, Meredin

    2007-01-01

    to the metal implant and wear-products. The aim of the present study was to compare surfaces of as-cast and wrought Cobalt-Chrome-Molybdenum (CoCrMo) alloys and Titanium-Aluminium-Vanadium (TiAlV) alloy when incubated with mouse macrophage J774A.1 cell cultures. Changes in pro- and anti-inflammatory cytokines...

  12. Comparison of modification with strontium and the refining with antimony in A 356 aluminium alloys; Comparacao entre a modificacao com estroncio e o refino com antimonio em ligas de aluminio a 356

    Energy Technology Data Exchange (ETDEWEB)

    Fuoco, Ricardo; Correa, Edison Roberto; Correa, Alzira V.O.; Bocalini Junior, Mario

    1992-12-31

    Strontium and Antimony treated A356 aluminium alloy samples were metallographically characterized in the as cast and solution and aged conditions. Antimony treated alloy has shown slower spheroidizing kinetics of the Silicon particles during solution treatment, lower porosity level and higher tensile strength and elongation than Strontium treated one. (author) 26 refs., 13 figs., 2 tabs.

  13. ZL101泡沫铝合金制备技术研究%Study on Preparation Technology of ZL101 Foamed Aluminium Alloy

    Institute of Scientific and Technical Information of China (English)

    李敬民; 周丹晨; 刘建辉; 黄姝珂

    2011-01-01

    以ZL101为基体材料,利用熔体发泡法制备泡沫铝合金,通过控制增粘温度、增粘物质和发泡物质的加入方式、发泡温度等关键参数获得稳定的制备工艺参数.实验结果表明,在660℃增粘效果要好于在700℃以上增粘;TiH2采用铝箔包裹方式加入可以有效减少加入过程的烧损量;加入发泡剂过程中使用带有下旋压力的双层折叶搅拌浆有利于将TiH2快速分散均匀和减小泡沫铝底部实心层;发泡温度为645℃时可以获得孔径较均匀的泡沫铝合金.%ZL101 foamed aluminium alloy was prepared by melt foaming method. The stabilized technological parameters was got by controlling the key factors such as the temperature of adding viscosity increaser, the way of adding viscosity increaser and blister, the temperature of foaming and so on. The results show that adding viscosity increaser at 660 ℃ is better than above 700 ℃. Packed TiH2 with aluminium foil is effective to reduce TiH2 burning loss. It is useful to break up powder of TiH2 quickly and decrease the solid thickness of foamed aluminium alloy using double-deck stirring paddle with downward stress. When the foaming temperature is 645 ℃, it could get uniform aperture aluminium alloy.

  14. Study of Pitting Corrosion Behavior of FSW weldments of AA6101- T6 Aluminium Alloy

    Directory of Open Access Journals (Sweden)

    L.V. Kamble

    2015-09-01

    Full Text Available Friction Stir Welding (FSW is a promising solid state joining process widely used generally for Al alloys, especially in aerospace, marine and automobile applications. In present work, the microstructure and corrosion behavior of friction stir welded AA6101 T6 Al alloy is studied. The friction stir welding was carried using vertical milling machine with different tool rotational speeds and welding speeds. The microstructure at weld nugget or stir zone (SN, thermo-mechanically affected zone (TMAZ, heat affected zone (HAZ and base metal were observed using optical microscopy. The corrosion tests of base alloy and welded joints were carried out in 3.5% NaCl solution at temperature of 30º C. Corrosion rate and emf were determined using cyclic polarization measurement.

  15. Fracture performance of high strength steels, aluminium and magnesium alloys during plastic deformation

    Directory of Open Access Journals (Sweden)

    Yu Haiyan

    2015-01-01

    Full Text Available A series of uniaxial tension tests were performed for 5052 and 6061 aluminum alloys, AZ31B magnesium alloy, TRIP600 and DP600 steels, to obtain a better understanding of their fracture performance. Scanning electron microscope (SEM observation of the microstructure evolution was conducted. The dimple structure, orientation relationship between the fracture surface and tensile direction, necking behavior were analyzed. The fracture mechanism and fracture mode of each material was discussed in detail. The results show that TRIP600 steel is subject to a typical inter-granular ductile fracture combined by shear fracture. DP600 steel belongs to mainly ductility mixed with normal fracture. Both 5052 and 6061 aluminum alloys are subject to a mixed ductility fracture and brittle fracture. AA5052 and AA6061 belong to a typical shear fracture and a normal fracture, respectively. Magnesium AZ31B is typical of a brittle fracture combined with normal fracture.

  16. Structure and properties of sintered titanium alloyed with aluminium, molybdenum and oxygen

    Energy Technology Data Exchange (ETDEWEB)

    Anokhin, V.M.; Petrunko, A.N. [State Research and Design Titanium Institute, Zaporozhye (Ukraine); Ivasishin, O.M. [Institute for Metal Physics, National Academy of Sciences of Ukraine, 36 Vernadsky St, 142 Kiev (Ukraine)

    1998-03-15

    Titanium alloys of Ti-Al-Mo-O system were manufactured by blended elemental powder method using Ti, Al, Mo and TiO{sub 2} powders as starting materials. It was found that cold compaction pressure of 800 MPa followed by sintering at 1150-1200 C, for 4 h provided sufficient densification of titanium materials. Complete dissolution of alloying elements in the titanium matrix resulted in a good combination of mechanical properties. Examples of alloys chosen for possible application were Ti-(1.5-2.0)%Mo-0.7%TiO{sub 2} and Ti-2%Al-2%Mo. The latter has already been tried for manufacturing parts in automotive industry. (orig.) 3 refs.

  17. Galvanostatic response of AA2024 aluminium alloy in 3.5% NaCl solution

    Indian Academy of Sciences (India)

    U DONATUS; G E THOMPSON

    2016-10-01

    Galvanostatic responses of AA2024T3 alloy in de-aerated and naturally aerated 3.5% NaCl solution have been investigated. In the de-aerated condition, two distinct stages of polarization were revealed. From the first stage, the relationships between the pitting incubation time, pitting potential and applied current density for AA2024T3 alloy in the de-aerated condition were established. The curves in the aerated condition showed no particular incubation time-applied current density relationship.

  18. Behaviour and modelling of aluminium alloy AA6060 subjected to a wide range of strain rates and temperatures

    Directory of Open Access Journals (Sweden)

    Vilamosa Vincent

    2015-01-01

    Full Text Available The thermo-mechanical behaviour in tension of an as-cast and homogenized AA6060 alloy was investigated at a wide range of strains (the entire deformation process up to fracture, strain rates (0.01–750 s−1 and temperatures (20–350 ∘C. The tests at strain rates up to 1 s−1 were performed in a universal testing machine, while a split-Hopkinson tension bar (SHTB system was used for strain rates from 350 to 750 s−1. The samples were heated with an induction-based heating system. A typical feature of aluminium alloys at high temperatures is that necking occurs at a rather early stage of the deformation process. In order to determine the true stress-strain curve also after the onset of necking, all tests were instrumented with a digital camera. The experimental tests reveal that the AA6060 material has negligible strain-rate sensitivity (SRS for temperatures lower than 200 ∘C, while both yielding and work hardening exhibit a strong positive SRS at higher temperatures. The coupled strain-rate and temperature sensitivity is challenging to capture with most existing constitutive models. The paper presents an outline of a new semi-physical model that expresses the flow stress in terms of plastic strain, plastic strain rate and temperature. The parameters of the model were determined from the tests, and the stress-strain curves from the tests were compared with the predictions of the model. Good agreement was obtained over the entire strain rate and temperature range.

  19. Wear behavior of 2-1/4 Cr-1 Mo tubing against alloy 718 tube-support material in sodium-cooled steam generators

    Energy Technology Data Exchange (ETDEWEB)

    Wilson, W L

    1983-05-01

    A series of prototypic steam generator 2-{1/4} Cr-1 Mo tube/alloy 718 tube support plate wear tests were conducted in direct support of the Westinghouse Nuclear Components Division -- Breeder Reactor Components Project Large Scale steam Generator design. The initial objective was to verify the acceptable wear behavior of softer, over-aged'' alloy 718 support plate material. For all interfaces under all test conditions, resultant wear damage was adhesive in nature with varying amounts of 2-{1/4} Cr-1 Mo tube material being adhesively transferred to the alloy 718 tube supports. Maximum tube wear depths exceeded the initially established design allowable limit of 127 {mu}m (.005 in.) at 17 of the 18 interfaces tested. A decrease in contact stresses produced acceptable tube wear depths below a readjusted maximum design allowable value of 381 {mu}m (.015 in.). Additional conservatisms associated with the simulation of a 40-year lifetime of rubbing in a one-week laboratory test provided further confidence that the 381 {mu}m maximum tube wear allowance would not be exceeded in service. Softer, over-aged'' alloy 718 material was found to produce slightly less wear damage on 2-{1/4} Cr-1 Mo tubing than fully age hardened material. Also, air formed oxide films on the alloy 718 reduced initial tube wear and delayed the onset of adhesive surface damage. However, at high surface stress levels, these films were not sufficiently stable to provide adequate long term protection from adhesive wear. The results of the present work and those of previous test programs suggest that the successful in-sodium tribological performance of 2-{1/4} Cr-1 Mo/alloy 718 rubbing couples is dependent upon the presence of lubricative surface films, such as oxides and/or surface reaction or deposition products. 11 refs., 13 figs., 4 tabs.

  20. Estimating multivariate response surface model with data outliers, case study in enhancing surface layer properties of an aircraft aluminium alloy

    Science.gov (United States)

    Widodo, Edy; Kariyam

    2017-03-01

    To determine the input variable settings that create the optimal compromise in response variable used Response Surface Methodology (RSM). There are three primary steps in the RSM problem, namely data collection, modelling, and optimization. In this study focused on the establishment of response surface models, using the assumption that the data produced is correct. Usually the response surface model parameters are estimated by OLS. However, this method is highly sensitive to outliers. Outliers can generate substantial residual and often affect the estimator models. Estimator models produced can be biased and could lead to errors in the determination of the optimal point of fact, that the main purpose of RSM is not reached. Meanwhile, in real life, the collected data often contain some response variable and a set of independent variables. Treat each response separately and apply a single response procedures can result in the wrong interpretation. So we need a development model for the multi-response case. Therefore, it takes a multivariate model of the response surface that is resistant to outliers. As an alternative, in this study discussed on M-estimation as a parameter estimator in multivariate response surface models containing outliers. As an illustration presented a case study on the experimental results to the enhancement of the surface layer of aluminium alloy air by shot peening.

  1. Microstructure and mechanical properties of similar and dissimilar joints of aluminium alloy and pure copper by friction stir welding

    Directory of Open Access Journals (Sweden)

    V.C. Sinha

    2016-09-01

    Full Text Available In the present study, the microstructure and mechanical properties of similar and dissimilar friction stir welded joints of aluminium alloy (AlA and pure copper (Cu were evaluated at variable tool rotational speeds from 150 to 900 rpm in steps of 150 rpm at 60 mm/min travel speed and constant tilt angle 2°. The interfacial microstructures of the joints were characterised by optical and scanning electron microscopy. The Al4Cu9, AlCu, Al2Cu and Al2Cu3 intermetallic compounds have been observed at the interface and stir zone region of dissimilar Al/Cu FSWed joints. Variation in the grain size was observed in the stir zone depending upon the heat input value. Axial force, traverse force and torque value were analysed with variation in tool rotational speed. Residual stresses were measured at the stir zone by X-ray diffraction technique. Maximum ultimate tensile strength of ∼75% of AlA strength for AlA–AlA joints has been obtained at 750 rpm and for Cu–Cu joint tensile strength of ∼100% of tensile strength of Cu was obtained at 300 rpm. However, for Cu–AlA joint when processed at 600 rpm tool rotational speed achieved maximum ultimate tensile strength of ∼77% of AlA.

  2. Impact resistance and hardness modelling of Aluminium alloy welds using square-headed friction-stir welding tool

    Science.gov (United States)

    Sudhakar, U.; Srinivas, J., Dr.

    2016-02-01

    This paper proposes modelling and optimization issues relating to friction-stir welding process of aluminium alloys. A specially prepared SS tool of square headed pin profile with cylindrical shoulder is used with a vertical milling machine. Effects of process variables including tool rotation and tool velocity on the weld performance are studied in terms of impact strength and hardness. Three different rotational motions and three welding speeds (feeds) of tool are considered at constant axial load (depth of cut) condition and altogether nine experiments are conducted on a vertical milling machine with specially prepared fixture. Each weld sample is then tested for its impact strength (IS) and hardness independently. A model is developed to correlate the relations between the hardness/impact strength with tool rotation and weld speed using neural networks. The optimized process conditions are predicted to improvise the impact strength and hardness of the weld. Further, the morphology of the weld is studied using SEM to know the material flow characteristics.

  3. Effect of Processing Parameters on the Protective Quality of Electroless Nickel-Phosphorus on Cast Aluminium Alloy

    Directory of Open Access Journals (Sweden)

    Olawale Olarewaju Ajibola

    2015-01-01

    Full Text Available The effects of temperature, pH, and time variations on the protective amount and quality of electroless nickel (EN deposition on cast aluminium alloy (CAA substrates were studied. The temperature, pH, and plating time were varied while the surface condition of the substrate was kept constant in acid or alkaline bath. Within solution pH of 5.0–5.5 range, the best quality is obtained in acid solution pH of 5.2. At lower pH (5.0–5.1, good adhesion characterised the EN deposition. Within the range of plating solution pH of 7.0 to 11.5, the highest quantity and quality of EN deposition are obtained on CAA substrate in solution pH of 10.5. It is characterised with few pores and discontinuous metallic EN film. The quantity of EN deposition is time dependent, whereas the adhesion and brightness are not time controlled. The best fit models were developed from the trends of result data obtained from the experiments. The surface morphologies and the chemical composition of the coating were studied using the Jeol JSM-7600F field emission scanning electron microscope.

  4. Experimental investigation on the effects of cooling system on surface quality in high speed milling of an aluminium alloy

    Science.gov (United States)

    Chirita, B.; Tampu, N. C.; Brabie, G.; Radu, M. C.

    2016-08-01

    Surface quality is often an important feature of industrial products, not only from the impact it has on the aesthetic aspect but also for the functional role of the parts. High quality surface increases corrosion resistance, assures a longer life cycle for the product and lowers the wear. For a machined part, surface quality is influenced by a series of factors such as the material of the part, the process type, tool geometry, cutting parameters or the cooling system. The choice of the cooling system is especially important, taking into account that the proper conditions will not only assure a superior surface quality, but will also lower the costs and reduce the environmental impact and health risks. The present study aims to investigate the performance of the cooling system and the effect of the cutting parameters on the characteristics of the surfaces resulted from high speed face milling of some parts made of Al 7050-T7451 aluminium alloy. Dry cutting conditions and minimum quantity lubrication (MQL) where used. The results were analysed using analysis of variance (ANOVA).

  5. Effects of cathodic voltages on structure and wear resistance of plasma electrolytic oxidation coatings formed on aluminium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Li, Qingbiao [State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000 (China); School of Science, Lanzhou University of Technology, Lanzhou 730050 (China); Liang, Jun, E-mail: jliang@licp.cas.cn [State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000 (China); Liu, Baixing; Peng, Zhenjun [State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000 (China); Wang, Qing [School of Science, Lanzhou University of Technology, Lanzhou 730050 (China)

    2014-04-01

    Highlights: • The PEO coating growth rate increased with the cathodic voltage increasing. • Higher cathodic voltage resulted in more compact coating structure. • The compact structure led to low surface roughness and high wear resistance. - Abstract: Plasma electrolytic oxidation (PEO) coatings were prepared on aluminium alloy using pulsed bipolar power supply at constant anodic voltage and different cathodic voltages. The samples were prepared to attain the same coating thickness by adjusting the processing time. The scanning electron microscope (SEM), energy dispersive spectrometer (EDS), X-ray diffraction (XRD) and tribometer were employed to investigate the microstructure, element content, phase composition and wear resistance of the coatings respectively. It was found that the coating growth rate enhanced obviously and the coatings exhibited a more compact structure with thicker inner layer and lower surface roughness when the cathodic voltage increased. The coatings were mainly composed of crystalline γ-Al{sub 2}O{sub 3} and amorphous silicate oxides and their relative content changed with the cathodic voltage. The wear resistance of the coatings improved significantly with the increase of cathodic voltage.

  6. Effect of the homogenisation conditions on the extrudability and high temperature fracture resistance of AA6063 aluminium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Lassance, D.; Pardoen, T.; Ryelandt, L.; Delannay, F. [Univ. catholique de Louvain, Dept. des Sciences des Materiaux et des Procedes, PCIM, Louvain-La-Neuve (Belgium); Dille, J.; Delplancke, J.L. [Univ. Libre de Bruxelles, Service Science des Materiaux et Electrochimie, Bruxelles (Belgium); Ryckeboer, M. [Remi Claeys International Services, Lichtervelde (Belgium)

    2003-07-01

    Homogenisation is an essential step in the preparation of aluminium billets for extrusion. It is designed to produce an homogeneous solid solution and to transform the {beta}-Al{sub 5}FeSi particles to the more equiaxed and thus more acceptable cubic {alpha}-Al{sub 12}(Fe{sub x},Mn{sub 1-x}){sub 3}Si variety. The effect of the homogenisation conditions on high temperature surface damage and fracture is investigated through full scale industrial extrusion experiments on AlMgSi alloy. The transformation of AlFeSi intermetallic particles from the {beta}-Al{sub 5}FeSi thin plate like shape to the more rounded {alpha}-Al{sub 12}(Fe,Mn){sub 3}Si form, quantified by EDS measurements, is shown to postpone the formation of surface defects. Transmission electron microscopy (TEM) analysis of extruded samples close to the location of extrusion defects, reveals that damage initiates by microcracks within the brittle {beta}-Al{sub 5}FeSi particles or due to incipient melting caused by the eutectic transformation Al+{beta}-Al{sub 5}FeSi+Si{yields}Liquid at 578 C. These microcracks open by plastic deformation around the cracked brittle phase and, after sufficient growth, coalesce into a large crack. (orig.)

  7. Effect of temperature and frequency of dynamic loading in the viscoelastic properties of aluminium alloy 7075-T6

    Energy Technology Data Exchange (ETDEWEB)

    Rojas, Jose I.; Aguiar, Albert; Crespo, Daniel [Escola d' Enginyeria de Telecomunicacio i Aeroespacial de Castelldefels (EPSC), Universitat Politecnica de Catalunya (UPC Barcelona Tech), Castelldefels, Barcelona (Spain)

    2011-11-15

    The viscoelastic response of a material offers an alternative method for analyzing its microstructure, phase transformations and fatigue behaviour. In this work, the viscoelastic properties of commercial aluminium alloy (AA) 7075-T6 are studied with a Dynamic-Mechanical Analyzer (DMA), and results are combined with Transmission Electron Microscopy (TEM) and Differential Scanning Calorimetry (DSC) data. In accordance with this analysis, we propose an analytical model for the storage modulus E' as a function of temperature, frequency of the dynamic loading and the concentration of Guinier-Preston Zones (GPZ). The latter parameter is obtained as a function of temperature after integration and fitting of the model. It is shown that the proposed model fits the experimental data for the storage modulus reasonably well in the prescribed region, and that this fact supports the hypothesis that the change in the storage modulus slope at about 130-160 C is due to GPZ decomposition. (copyright 2011 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

  8. Study of Simulated Temperature of Butt Joint during Friction Stir Welding Of Aluminium Alloy by Using Hyperworks

    Directory of Open Access Journals (Sweden)

    Mohd Anees Siddiqui

    2015-01-01

    Full Text Available Friction stir welding (FSW is one of the latest welding technology that utilizes a special tool for generation of frictional heat in the work piece by its rotation due to which joining occurs without melting of metal. For this reason friction stir welding lies under the category of solid state joining. A part from experimental work, there is large space to work on simulation of FSW by using simulation tools. In the present paper, simulation of friction stir welding of aluminium alloy AA-6061 is done by using HyperWeld module of Altair HyperWorks. The virtual experiment of friction stir welding is conducted for variable tool rotational speeds with constant travelling speed and study of simulation results of variation in temperature distribution along the weld line of butt joint is done. The results of simulation shows that the temperature is symmetrically distributed along the weld line. It is observed that the maximum temperature along the weld line increases with the increase in rotational speed. It is also observed that the temperature at advancing side is greater that retreating side.

  9. Influence of process parameters on physical dimensions of AA6063 aluminium alloy coating on mild steel in friction surfacing

    Directory of Open Access Journals (Sweden)

    B. Vijaya Kumar

    2015-09-01

    Full Text Available An attempt is made in the present study to obtain the relationships among process parameters and physical dimensions of AA6063 aluminium alloy coating on IS2062 mild steel obtained through friction surfacing and their impact on strength and ductility of the coating. Factorial experimental design technique was used to investigate and select the parameter combination to achieve a coating with adequate strength and ductility. Spindle speed, axial force and table traverse speed were observed to be the most significant factors on physical dimensions. It was observed that the thickness of the coating decreased as the coating width increased. In addition, the width and thickness of the coatings are higher at low and high torques. At intermediate torque values, when the force is high, the width of the coating is high, and its thickness is thin; and when the force is low, the width and thickness are low. The interaction effect between axial force (F – table traverse speed (Vx and spindle speed (N – table traverse speed (Vx produced an increasing effect on coating width and thickness, but other interactions exhibited decreasing influence. It has also been observed that sound coatings could be obtained in a narrow set of parameter range as the substrate-coating materials are metallurgically incompatible and have a propensity to form brittle intermetallics.

  10. Steam assisted oxide growth on aluminium alloys using oxidative chemistries: Part II corrosion performance

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Jellesen, Morten Stendahl; Ambat, Rajan

    2015-01-01

    and standard industrial test methods such as acetic acid salt spray (AASS) and filiform corrosion on commercial AA6060 alloy. Barrier properties of the film including adhesion were evaluated using tape test under wet and dry conditions. Electrochemical results showed reduced cathodic and anodic activity, while...

  11. Effect of united refining and modification on mechanical properties of A356 aluminium alloys

    Institute of Scientific and Technical Information of China (English)

    ZUO Xiu-rong; ZHONG Zhi-guo

    2006-01-01

    The refining and modification effect of Ti (from GRAI), B, Sr and RE (cerium-riched mixtures of rare earth) on the mechanical properties of A356 aluminum alloys under T5 and T6 treatment condition were studied by OM, SEM, EDAX, etc. It is found that the addition of RE to A356 alloys containing Ti and/or B and Sr makes strength and elongation increase in T6 treatment,but make elongation decrease in T5 treatment, at the same time, the long axis of α(Al) grain structure decreases and the mean diameters of silicon particles increase with RE additions increasing. Grain refining with 0.01%Ti plus 0.03% B makes the dendrite α(Al) grain structure transform into equiaxed structure, resulting in obvious increase of elongation percentage. The mean diameters of silicon particles in T5 treatment are smaller than that in T6 treatrnent. Roundness of silicon particles in T5 treatment is higher than that in T6 treatment. A356 alloys modified and refined with Ti, B and Sr obtain the best mechanical properties in T5 treatment,however, the alloys with Ti, B, RE and Sr additions obtain the best mechanical properties in T6 treatment.

  12. Application of Kaplan-Meier analysis in reliability evaluation of products cast from aluminium alloys

    Directory of Open Access Journals (Sweden)

    J. Szymszal

    2010-04-01

    Full Text Available The article evaluates the reliability of AlSi17CuNiMg alloys using Kaplan-Meier-based technique, very popular as a survival estimation tool in medical science. The main object of survival analysis is a group (or groups of units for which the time of occurrence of an event (failure taking place after some time of waiting is estimated. For example, in medicine, the failure can be patient’s death. In this study, the failure was the specimen fracture during a periodical fatigue test, while the survival time was either the test duration to specimen failure (complete observations, or the test end time (censored observations. The parameters of theoretical survival function were estimated with procedures based on the method of least squares, while typical survival time distribution followed either an exponential or two-parameter Weibull distribution. The goodness of fit of a model survival function was estimated with an incremental chi-square test, based on the values of the log likelihood ratio. The effect of alloy processing history on the run of a survival function was examined. The factors shaping the alloy processing history included: mould type (sand or metal mould, alloy modification process, and heat treatment type (solution heat treatment and ageing.

  13. Structure and tensile/wear properties of microarc oxidation ceramic coatings on aluminium alloy

    Institute of Scientific and Technical Information of China (English)

    魏同波; 阎逢元; 刘维民; 田军

    2004-01-01

    Thick and hard ceramic coatings were prepared on the Al-Cu-Mg alloy by microarc oxidation in alkali-silicate electrolytic solution. The thickness and microhardness of the oxide coatings were measured. The influence of current density on the growth rate of the coating was examined. The microstructure and phase composition of the coatings were investigated by means of scanning electron microscopy, energy dispersive spectroscopy, and X-ray diffraction. Moreover, the tensile strength of the Al alloy before and after microarc oxidation treatment were tested,and the fractography and morphology of the oxide coatings were observed using scanning electron microscope. It is found that the current density considerably influences the growth rate of the microarc oxidation coatings. The oxide coating is mainly composed of α-Al2 O3 and γ-Al2 O3, while high content of Si is observed in the superficial layer of the coating. The cross-section microhardness of 120 μm thick coating reaches the maximum at distance of 35 μm from the substrate/coating interface. The tensile strength and elongation of the coated Al alloy significantly decrease with increasing coating thickness. The microarc oxidation coatings greatly improve the wear resistance of Al alloy,but have high friction coefficient which changes in the range of 0.7 - 0.8. Under grease lubricating, friction coefficient is only 0.15 and wear loss is less than 1/10 of the loss under dry friction.

  14. Finite element modeling and analysis of electro-magnetic pulse welding of aluminium tubes to steel bars

    Science.gov (United States)

    Kumar, Ramesh; Doley, Jyoti; Kore, Sachine

    2016-10-01

    Magnetic pulse welding is a high-speed, solid-state welding process that is applicable to sheets or tube-to-tube or tube-to-bar configurations. In this article we discuss about the MPW process modeling and simulation for welding Al tubes to steel bars. Finite element simulation was done to weld 6061 Al tubes of 1.65 mm wall thickness to 1010 steel bars of a 47.6 mm nominal diameter. Simulation results indicate that Al tubes can be successfully welded to steel bars using MPW. It is found that the standoff distance between the Al tube and the steel bar i.e. gap between inner diameter of Al tube and diameter of steel bar is a dominant factor for achieving a sound weld. The addition of receding angles to the bars can promote MPW weldability window.

  15. Effects of process parameters on numerical control bending process for large diameter thin-walled aluminum alloy tubes

    Institute of Scientific and Technical Information of China (English)

    LI Cheng; YANG He; ZHAN Mei; XU Xu-dong; LI Guang-jun

    2009-01-01

    Numerical control(NC) bending experiments with different process parameters were carried out for 5052O aluminum alloy tubes with outer diameter of 70 mm, wall thickness of 1.5 mm, and centerline bending radius of 105 mm. And the effects of process parameters on tube wall thinning and cross section distortion were investigated. Meanwhile, acceptable bending of the 5052O aluminum tubes was accomplished based on the above experiments. The results show that the effects of process parameters on bending process for large diameter thin-walled aluminum alloy tubes are similar to those for small diameter thin-walled tubes, but the forming quality of the large diameter thin-walled aluminum alloy tubes is much more sensitive to the process parameters and thus it is more difficult to form.

  16. The Effect of Dynamic Compression on the Evolution of Microstructure in Aluminium and its Alloys

    Directory of Open Access Journals (Sweden)

    Leszczyńska-Madet B.

    2013-12-01

    Full Text Available W pracy przedstawiono wyniki badań mikrostruktury i wybranych właściwości polikrystalicznego aluminium i jego stopów: AlMg5, AlCu4Zr0.5, AlZn6Mg2.5CuZr ściskanych dynamicznie za pomocą młota spadowego. Próbki odkształcano w zakresie odkształceń rzeczywistych = 0-0.62 z prędkością odkształcenia z zakresu 1.77-6.06x102 s-1. Na tak odkształconych materiałach przeprowadzono pomiar mikrotwardości oraz badania mikrostruktury przy zastosowaniu transmisyjnego mikrosko- pu elektronowego (TEM i mikroskopu świetlnego (LM, dodatkowo przeprowadzono pomiar dezorientacji w mikroobszarach metodą linii Kikuchiego przy zastosowaniu oprogramowania KILIN. Cechą charakterystyczną mikrostruktury badanych materiałów były licznie obserwowane pasma i pasma ścinania. Wyniki uzyskane przy zastosowaniu transmisyjnego mikroskopu elektronowego dowiodły występowania licznych mikropasm i mikro- pasm ścinania, które w zależności od materiału przebiegały na tle różnych układów dyslokacyjnych. Obserwowane mikropasma wykazywały dużą dezorientację względem osnowy. Stwierdzono wzajemnie przecinanie się mikropasm. W zakresie wyższych wartości odkształcenia, mikropasma wypełniały niemal całą objętość próbek. Zaobserwowano zależność zmniejszania się średniej szerokości i mikropasm wraz ze wzrostem wielkości odkształcenia i prędkości odkształcenia. Praca miała na celu określenie wpływu prędkości odkształcenia (1.77x10' - 6.06xl02s_1 na możliwość rozdrobnienia mikrostruktury polikrystalicznego aluminium A199.5 i jego stopów (AlMg5, AlCu4Zr0.5, AlZn6Mg2.5CuZr odkształcanych w procesie dynamicznego ściskania za pomocą młota spadowego.

  17. Corrosion behaviour of ion implanted aluminium alloy in 0.1 M NaCl electrolyte

    Energy Technology Data Exchange (ETDEWEB)

    Chu, J.W.; Evans, P.J. [Australian Nuclear Science and Technology Organisation, Lucas Heights, NSW (Australia); Sood, D.K. [Royal Melbourne Inst. of Tech., VIC (Australia)

    1993-12-31

    Aluminum and its alloys are widely used in industry because of their light weight, high strength and good corrosion resistance which is due to the formation of a protective oxide layer. However, under saline conditions such as those encountered in marine environments, this group of metals are vulnerable to localised degradation in the form of pitting corrosion. This type of corrosion involves the adsorption of an anion, such as chlorine, at the oxide solution interface. Ion implantation of metal ions has been shown to improve the corrosion resistance of a variety of materials. This effect occurs : when the implanted species reduces anion adsorption thereby decreasing the corrosion rate. In this paper we report on the pitting behavior of Ti implanted 2011 Al alloy in dilute sodium chloride solution. The Ti implanted surfaces exhibited an increased pitting potential and a reduced oxygen uptake. 5 refs., 3 figs.

  18. Continuous sodium modification of nearly-eutectic aluminium alloys. Part II. Experimental studiem

    Directory of Open Access Journals (Sweden)

    Białobrzeski A.

    2007-01-01

    Full Text Available One of the possible means of continuous sodium modification of nearly-eutectic alloys may be continuous electrolysis of sodium compounds (salts, taking place directly in metal bath (in the crucible. For this process it is necessary to use a solid electrolyte conducting sodium ions. Under the effect of the applied direct current voltage, sodium salt placed in a retort made from the solid electrolyte undergoes dissociation, and next - electrolysis. The retort is immersed in liquid metal. The anode is sodium salt, at that temperature occurring in liquid state, connected to the direct current source through, e.g. a graphite electrode, while cathode is the liquid metal. Sodium ions formed during the sodium salt dissociation and electrolysis are transported through the wall of the solid electrolyte (the material of the retort and in contact with liquid alloy acting as a cathode, they are passing into atomic state, modifying the metal bath.

  19. Researches and studies regarding brazed aluminium alloys microstructure used in aeronautic industry

    Directory of Open Access Journals (Sweden)

    A. Dimitrescu

    2015-04-01

    Full Text Available Brazing is applied to the merge of the pieces which are most required, tensile strength of the solder can reach high values. By brazing there can be assembled pieces of most metals and ferrous and nonferrous alloys, with high melting temperature. This paper presents an analysis of the microstructure of materials from a brazed merge of aluminum alloy L103 which is often used to produce pieces of aeronautical industry. Brazing material was performed using several technologies, and after examination of the microstructure of materials from the merge area it was established as optimal technology the technology which consist of pickling in Aloclene 100 solution with the deposition of filler material on both sides of the base material and the use of spectral acetylene and neutral flame.

  20. EVOLUTION OF AS-CAST MICROSTRUCTURES OF 356 ALUMINIUM ALLOY CAST BY LIQUIDUS CASTING

    Institute of Scientific and Technical Information of China (English)

    J. Dong; G.M. Lu; J.Z. Cui; Z.H. Zhao

    2003-01-01

    A new method (liquidus casting) was used for 356 Al alloy semi-solid slurry mak-ing. The structures of 356 Al alloy cast by a Fe mould and semi-continuous castingmachine at different temperatures were investigated. How the globular grains formwas also discussed. The results show that either being cast by single Fe mould orsemi-continuous machine, the microstructures are not conventional dendrites but fineand net-globular grains. The average grain size is smaller than 30μm and suitableenough for thixoforming, meanwhile it can improve the mechanical properties of fol-lowing products. Under the suitable casting velocity and cooling intensity, most ofglobal grains prolong their global growth and collide with each other before dendriticgrowth because of the large amount of the nucleation sites.

  1. EVOLUTION OF AS—CAST MICROSTRUCTURES OF 356 ALUMINIUM ALLOY CAST BY LIQUIDUS CASTING

    Institute of Scientific and Technical Information of China (English)

    J.Dong; G.M.Lu; 等

    2003-01-01

    A new method (liquidus casting)was used for 356 Al alloy semi-solid slurry mak-ing.The structures of 356 Al alloy cast by a fe mould and semi-continuous casting machine at different temperatures were inves tigated.How the globular grains form was qlso discussed.The results show that either being cast by single Fe mould or semi-continuous machine,the microstructures are not conventional dendrites but fine and net-globular grains.The average grain size is smaller than 30μm and suitable enough for thixoforming,meanwhile it can improve the mechanical properties of fol-lowing products.Under the suitable casting velocity and cooling intensity,most of global grains prolong their global browth and collide with each other before dendritic growth because of the large amount of the nucleation sites.

  2. Study of corrosion of aluminium alloys of nuclear purity in ordinary water, пart one

    Directory of Open Access Journals (Sweden)

    Pešić Milan P.

    2004-01-01

    Full Text Available Effects of corrosion of aluminum alloys of nuclear purity in ordinary water of the spent fuel storage pool of the RA research reactor at VINČA Institute of Nuclear Sciences has been examined in the frame work of the International Atomic Energy Agency Coordinated Research Project "Corrosion of Research Reactor Aluminum-Clad Spent Fuel in Water" since 2002. The study presented in this paper comprises activities on determination and monitoring of chemical parameters and radio activity of water and sludge in the RA spent fuel storage pool and results of the initial study of corrosion effects obtained by visual examinations of surfaces of various coupons made of aluminum alloys of nuclear purity of the test racks exposed to the pool water for a period from six months to six years.

  3. Emission of nanoparticles during friction stir welding (FSW) of aluminium alloys.

    Science.gov (United States)

    Gomes, J F; Miranda, R M; Santos, T J; Carvalho, P A

    2014-01-01

    Friction stir welding (FSW) is now well established as a welding process capable of joining some different types of metallic materials, as it was (1) found to be a reliable and economical way of producing high quality welds, and (2) considered a "clean" welding process that does not involve fusion of metal, as is the case with other traditional welding processes. The aim of this study was to determine whether the emission of particles during FSW in the nanorange of the most commonly used aluminum (Al) alloys, AA 5083 and AA 6082, originated from the Al alloy itself due to friction of the welding tool against the item that was being welded. Another goal was to measure Al alloys in the alveolar deposited surface area during FSW. Nanoparticles dimensions were predominantly in the 40- and 70-nm range. This study demonstrated that microparticles were also emitted during FSW but due to tool wear. However, the biological relevance and toxic manifestations of these microparticles remain to be determined.

  4. Computational prediction of the refinement of oxide agglomerates in a physical conditioning process for molten aluminium alloy

    Science.gov (United States)

    Tong, M.; Jagarlapudi, S. C.; Patel, J. B.; Stone, I. C.; Fan, Z.; Browne, D. J.

    2015-06-01

    Physically conditioning molten scrap aluminium alloys using high shear processing (HSP) was recently found to be a promising technology for purification of contaminated alloys. HSP refines the solid oxide agglomerates in molten alloys, so that they can act as sites for the nucleation of Fe-rich intermetallic phases which can subsequently be removed by the downstream de-drossing process. In this paper, a computational modelling for predicting the evolution of size of oxide clusters during HSP is presented. We used CFD to predict the macroscopic flow features of the melt, and the resultant field predictions of temperature and melt shear rate were transferred to a population balance model (PBM) as its key inputs. The PBM is a macroscopic model that formulates the microscopic agglomeration and breakage of a population of a dispersed phase. Although it has been widely used to study conventional deoxidation of liquid metal, this is the first time that PBM has been used to simulate the melt conditioning process within a rotor/stator HSP device. We employed a method which discretizes the continuous profile of size of the dispersed phase into a collection of discrete bins of size, to solve the governing population balance equation for the size of agglomerates. A finite volume method was used to solve the continuity equation, the energy equation and the momentum equation. The overall computation was implemented mainly using the FLUENT module of ANSYS. The simulations showed that there is a relatively high melt shear rate between the stator and sweeping tips of the rotor blades. This high shear rate leads directly to significant fragmentation of the initially large oxide aggregates. Because the process of agglomeration is significantly slower than the breakage processes at the beginning of HSP, the mean size of oxide clusters decreases very rapidly. As the process of agglomeration gradually balances the process of breakage, the mean size of oxide clusters converges to a

  5. Optimization of friction welding by taguchi and ANOVA method on commercial aluminium tube to Al 2025 tube plate with backing block using an external tool

    Energy Technology Data Exchange (ETDEWEB)

    Kanna, S.; Kumaraswamidhs, L. A. [Indian Institute of Technology, Dhanbad (India); Kumaran, S. Senthil [RVS School of Engineering and Technology, Dindigul (India)

    2016-05-15

    The aim of the present work is to optimize the Friction welding of tube to tube plate using an external tool (FWTPET) with clearance fit of commercial aluminum tube to Al 2025 tube plate using an external tool. Conventional frictional welding is suitable to weld only symmetrical joints either tube to tube or rod to rod but in this research with the help of external tool, the welding has been done by unsymmetrical shape of tube to tube plate also. In this investigation, the various welding parameters such as tool rotating speed (rpm), projection of tube (mm) and depth of cut (mm) are determined according to the Taguchi L9 orthogonal array. The two conditions were considered in this process to examine this experiment; where condition 1 is flat plate with plain tube Without holes [WOH] on the circumference of the surface and condition 2 is flat plate with plane tube has holes on its circumference of the surface With holes [WH]. Taguchi L9 orthogonal array was utilized to find the most significant control factors which will yield better joint strength. Besides, the most influential process parameter has been determined using statistical Analysis of variance (ANOVA). Finally, the comparison of each result has been done for conditions by means percentage of contribution and regression analysis. The general regression equation is formulated and better strength is obtained and it is validated by means of confirmation test. It was observed that value of optimal welded joint strength for both tube without holes and tube with holes are to be 319.485 MPa and 264.825 MPa, respectively.

  6. Cross-Roll Flow Forming of ODS Alloy Heat Exchanger Tubes For Hoop Creep Enhancement

    Energy Technology Data Exchange (ETDEWEB)

    Bimal K. Kad

    2005-11-23

    Mechanically alloyed oxide dispersion strengthened (ODS) Fe-Cr-Al alloy thin walled tubes and sheets, produced via powder processing and consolidation methodologies, are promising materials for eventual use at temperatures up to 1200 C in the power generation industry, far above the temperature capabilities of conventional alloys. Target end-uses range from gas turbine combustor liners to high aspect ratio (L/D) heat exchanger tubes. Grain boundary creep processes at service temperatures, particularly those acting in the hoop direction, are the dominant failure mechanisms for such components. The processed microstructure of ODS alloys consists of high aspect ratio grains aligned parallel to the tube axis, a result of dominant axial metal flow which aligns the dispersoid particles and other impurities in the longitudinal direction. The dispersion distribution is unaltered on a micro scale by recrystallization thermal treatments, but the high aspect ratio grain shape typically obtained limits transverse grain spacing and consequently the hoop creep response. Improving hoop creep in ODS-alloy components will require understanding and manipulating the factors that control the recrystallization behavior, and represents a critical materials design and development challenge that must be overcome in order to fully exploit the potential of ODS alloys. The objectives of this program are to (1) increase creep-strength at temperature in ODS-alloy tube and liner components by 100% via, (2) preferential cross-roll flow forming and grain/particle fibering in the critical hoop direction. Recent studies in crossrolled ODS-alloy sheets (produced from flattened tubes) indicate that transverse creep is significantly enhanced via controlled transverse grain fibering, and similar improvements are expected for cross-rolled tubes. The research program outlined here is iterative in nature and is intended to systematically (1) examine and identify post-extrusion forming methodologies to

  7. Investigation of welding and brazing of molybdenum and TZM alloy tubes

    Science.gov (United States)

    Lundblad, Wayne E.

    1991-01-01

    This effort involved investigating the welding and brazing techniques of molybdenum tubes to be used as cartridges in the crystal growth cartridge. Information is given in the form of charts and photomicrographs. It was found that the recrystallization temperature of molybdenum can be increased by alloying it with 0.5 percent titanium and 0.1 percent zirconium. Recrystallization temperatures for this alloy, known as TZM, become significant around 2500 F. A series of microhardness tests were run on samples of virgin and heat soaked TZM. The test results are given in tabular form. It was concluded that powder metallurgy TZM may be an acceptable cartridge material.

  8. Cross-Roll Flow Forming of ODS Alloy Heat Exchanger Tubes For Hoop Creep Enhancement

    Energy Technology Data Exchange (ETDEWEB)

    Bimal K. Kad

    2006-09-30

    Mechanically alloyed oxide dispersion strengthened (ODS) Fe-Cr-Al alloy thin walled tubes and sheets, produced via powder processing and consolidation methodologies, are promising materials for eventual use at temperatures up to 1200 C in the power generation industry, far above the temperature capabilities of conventional alloys. Target end-uses range from gas turbine combustor liners to high aspect ratio (L/D) heat exchanger tubes. Grain boundary creep processes at service temperatures, particularly those acting in the hoop direction, are the dominant failure mechanisms for such components. The processed microstructure of ODS alloys consists of high aspect ratio grains aligned parallel to the tube axis, a result of dominant axial metal flow which aligns the dispersoid particles and other impurities in the longitudinal direction. The dispersion distribution is unaltered on a micro scale by recrystallization thermal treatments, but the high aspect ratio grain shape typically obtained limits transverse grain spacing and consequently the hoop creep response. Improving hoop creep in ODS-alloy components will require understanding and manipulating the factors that control the recrystallization behavior, and represents a critical materials design and development challenge that must be overcome in order to fully exploit the potential of ODS alloys. The objectives of this program are to (1) increase creep-strength at temperature in ODS-alloy tube and liner components by 100% via, (2) preferential cross-roll flow forming and grain/particle fibering in the critical hoop direction. The research program outlined here is iterative in nature and is intended to systematically (a) examine and identify post-extrusion forming methodologies to create hoop strengthened tubes, which will be (b) evaluated at ''in-service'' loads at service temperatures and environments. In this 12th quarter of performance, program activities are concluded for Task 2 and continuing

  9. Microstructure and composition of rare earth-transition metal-aluminium-magnesium alloys

    Directory of Open Access Journals (Sweden)

    Lia Maria Carlotti Zarpelon

    2008-03-01

    Full Text Available The determination of the microstructure and chemical composition of La0.7-xPr xMg0.3Al 0.3Mn0.4Co0.5 Ni3.8 (0 < x < 0.7 metal hydride alloys has been carried out using scanning electron microscopy (SEM, energy dispersive X ray analysis (EDX and X ray diffraction analysis (XRD. The substitution of La with Pr changed the grain structure from equiaxial to columnar. The relative atomic ratio of rare earth to (Al, Mn, Co, Ni in the matrix phase was 1:5 (LaNi5-type structure. Magnesium was detected only in two other phases present. A grey phase revealed 11 at.% Mg and the concentration ratios of other elements indicated the composition to be close to PrMgNi4. A dark phase was very heterogeneous in composition, attributed to the as-cast state of these alloys. The phases identified by XRD analysis in the La0.7Mg0.3Al0.3Mn0.4Co 0.5Ni3.8 alloy were: La(Ni,Co5, LaAl(Ni,Co4, La2(Ni,Co7 and AlMn(Ni,Co2. Praseodymium favors the formation of a phase with a PuNi3-type structure. Cobalt substituted Ni in the structures and yielded phases of the type: Pr(Ni,Co5 and Pr(Ni,Co3.

  10. Observations on infiltration of silicon carbide compacts with an aluminium alloy

    Science.gov (United States)

    Asthana, R.; Rohatgi, P. K.

    1992-01-01

    The melt infiltration of ceramic particulates permits an opportunity to observe such fundamental materials phenomena as nucleation, dynamic wetting and growth in constrained environments. Experimental observations are presented on the infiltration behavior and matrix microstructures that form when porous compacts of platelet-shaped single crystals of alpha- (hexagonal) silicon carbide are infiltrated with a liquid 2014 Al alloy. The infiltration process involved counter gravity infiltration of suitably tamped and preheated compacts of silicon carbide platelets under an external pressure in a special pressure chamber for a set period, then by solidification of the infiltrant metal in the interstices of the bed at atmospheric pressure.

  11. [Comporison Sduty of Microstructure by Metallographicalk on the Polarized Light and Texture by XRD of CC 5083 and CC 5182 Aluminium Alloy after Cold Rolling and Recrystallization].

    Science.gov (United States)

    Chen, Ming-biao; Li, Yong-wei; Tan, Yuan-biao; Ma, Min; Wang, Xue-min; Liu, Wen-chang

    2015-03-01

    At present the study of relation between microstructure, texture and performance of CC 5083 aluminium alloy after cold tolling and recrystallization processes is still finitude. So that the use of the CC 5083 aluminium alloy be influenced. Be cased into electrical furnace, hot up with unlimited speed followed the furnace hot up to different temperature and annealed 2h respectively, and be cased into salt-beth furnace, hot up quickly to different temperature and annealed 30 min respectively for CC 5083 and CC 5182 aluminum alloy after cold roling with 91.5% reduction. The microstructure be watched use metallographic microscope, the texture be inspected by XRD. The start temperature of recrystallization and grain grow up temperature within annealing in the electric furnace of CC 5083 aluminum alloy board is 343 degrees C, and the shap of grain after grow up with long strip (the innovation point ); The start temperature of recrystallization within annealling in the salt bath furnace of CC 5083 is 343 degrees C. The start temperature and end temperature of recrystallization within annealling of CC 5083 and CC 5182 aluminum alloy is 371 degrees C. The grain grow up outstanding of cold rooled CC 5152 aluminum alloy after annealed with 454 degrees C in the electric furnace and salt bath furnace. The start temperature of grain grow up of CC 5083 alluminurn alloy annealed in the electric furnace and salt bath furnace respectively is higher than the start temperature of grain grow up of CC 5182 alluminum alloy annealed in the electric furnace and salt bath furnace respectively. The strat temperature of recrystallization grain grow up is higher than which annealled with other three manner annealing process. The recrystallization temperature of CC 5182 annealed in the salt bath furnace is higher than which annealed in the electric furnace. The recrystallization temperature of the surface layer of CC 5083 and CC 5182 aluminum alloy is higher than the inner layer (the innovation

  12. Effect of tool pin profile on microstructure and tensile properties of friction stir welded dissimilar AA 6061–AA 5086 aluminium alloy joints

    Directory of Open Access Journals (Sweden)

    M. Ilangovan

    2015-06-01

    Full Text Available Joints between two different grades of aluminium alloys are need of the hour in many light weight military structures. In this investigation, an attempt has been made to join the heat treatable (AA 6061 and non-heat treatable (AA 5086 aluminium alloys by friction stir welding (FSW process using three different tool pin profiles like straight cylindrical, taper cylindrical and threaded cylindrical. The microstructures of various regions were observed and analyzed by means of optical and scanning electron microscope. The tensile properties and microhardness were evaluated for the welded joint. From this investigation it is founded that the use of threaded pin profile of tool contributes to better flow of materials between two alloys and the generation of defect free stir zone. It also resulted in higher hardness values of 83 HV in the stir zone and higher tensile strength of 169 MPa compared to other two profiles. The increase in hardness is attributed to the formation of fine grains and intermetallics in the stir zone, and in addition, the reduced size of weaker regions, such as TMAZ and HAZ regions, results in higher tensile properties.

  13. Corrosion behavior of Cu-Ni-Ag-Al alloy anodes in aluminium electrolysis

    Institute of Scientific and Technical Information of China (English)

    徐君莉; 石忠宁; 邱竹贤

    2004-01-01

    The behavior of Cu-Ni-Ag-Al alloy used as anode for aluminum electrolysis was directly visualized in a two-compartment see-through cell during electrolysis, and its performances were tested at 850℃ in acidic electrolyte molten salts consisting of 39.3 % NaF-43.7 % AlF3-8 % NaCl-5 % CAF2-4 % Al2 O3 for 40 h in a laboratory cell. The results show that nascent oxygen oxidizes the anodic surface to form oxide film at the beginning of electrolysis. X-ray diffraction analysis of alloy surface show that the oxide film on the anodic surface consists of CuO, NiO, Al2O3,CuAl2 O4 and NiAl2 O4. However, SEM image shows the oxide film is porous, loose and easy to fall into electrolyte and to contaminate aluminum. The corrosion mechanism of metal anodes was analyzed.

  14. Corrosion of aluminium, stainless steels and AISI 680 nickel alloy in nitrogen-based fuels

    Energy Technology Data Exchange (ETDEWEB)

    Kap, I.; Starostin, M.; Shter, G.E.; Grader, G.S. [Department of Chemical Engineering, Technion-Israel Institute of Technology, Haifa (Israel)

    2012-07-15

    Nitrogen-based compounds can potentially be used as alternative non-carbon or low-carbon fuels. Nevertheless, the corrosion of construction materials at high temperatures and pressures in the presence of such fuel has not been reported yet. This work is focused on the corrosion of AISI Al 6061, 1005 carbon steel (CS), 304, 316L, 310 austenitic stainless steels (SS) and 680 nickel alloy in highly concentrated water solution of ammonium nitrate and urea (ANU). The corrosion at 50 C and ambient pressure and at 350 C and 20 bar was investigated to simulate storage and working conditions. Sodium chloride was added to the fuel (0-5 wt%) to simulate industrial fertilizers and accelerated corrosion environment. Heavy corrosion of CS was observed in ANU solution at 50 C, while Al 6061, 304 and 316L SS showed high resistance both to uniform and pitting corrosion in ANU containing 1% of sodium chloride. Addition of 5% sodium chloride caused pitting of Al 6061 but had no influence on the corrosion of SS. Tests in ANU at 350 C and 20 bar showed pitting on SS 304 and 316L and 680 nickel alloy. The highest corrosion resistance was found for SS 310 due to formation of stable oxide film on its surface. (Copyright copyright 2012 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

  15. Finite element analysis of free expansion of aluminum alloy tube under magnetic pressure

    Institute of Scientific and Technical Information of China (English)

    YU Hai-ping; LI Chun-feng

    2005-01-01

    A link between the electromagnetic code, ANSYS/Emag and the structural code, Ls-dyna was developed, and the numerical modeling of electromagnetic forming for aluminum alloy tube expansion was performed by means of them (discharge energy 0.75 kJ). A realistic distribution of magnetic pressure was calculated. The calculated values of displacement along the tube axis and versus time are in very good agreement with the measured ones.The maximum strain rate is 1 122 s-1, which is not large enough to change the constitutive equations of aluminum alloy. With the augment of discharge energy (0. 5 - 1.0 kJ), the relative errors of the maximum deformation increase from 2.93% to 11.4%. Therefore, coupled numerical modeling of the electromagnetic field and the structural field should be performed to investigate the electromagnetic forming with larger deformation.

  16. Evaluation of High Temperature Corrosion Resistance of Finned Tubes Made of Austenitic Steel And Nickel Alloys

    Directory of Open Access Journals (Sweden)

    Turowska A.

    2016-06-01

    Full Text Available The purpose of the paper was to evaluate the resistance to high temperature corrosion of laser welded joints of finned tubes made of austenitic steel (304,304H and nickel alloys (Inconel 600, Inconel 625. The scope of the paper covered the performance of corrosion resistance tests in the atmosphere of simulated exhaust gases of the following chemical composition: 0.2% HCl, 0.08% SO2, 9.0% O2 and N2 in the temperature of 800°C for 1000 hours. One found out that both tubes made of austenitic steel and those made of nickel alloy displayed good resistance to corrosion and could be applied in the energy industry.

  17. Containerless processing of hypermonotectic and glass forming alloys using the Marshall Space Flight Center 100 meter drop tube facility

    Science.gov (United States)

    Andrews, J. B.

    1986-01-01

    Two separate projects were carried out to study alloys whose solidification structures can be strongly influenced by the presence of a container during melting and solidifications. One project involved containerless solidification of hypermonotectic Au35Rh65 alloys. This alloy exhibits liquid immiscibility over a temperature range. It has been suggested that containerless melting might be one solution to the problem of sedimentation in the dispersions of immiscible liquid phases. However, surface tension driven flows could also lead to accumulation of the minority liquid phase at the external surface of a containerlessly melted alloy. The research underway is a first step in determining the influence of containerless, microgravity processing on immiscible alloys. Nickel-niobium alloys were studied using the drop tube facility. One alloy in this system, a Ni60Nb40 alloy, is a good candidate for the formation of a bulk metallic glass. Amorphous alloys of this composition were produced using thin film and mechanical alloying techniques. However, theory indicates that if heterogeneous nucleation can be avoided, it should be possible to produce an amorphous structure in this system using a moderate cooling rate from the melt. The containerless melting and solidification capabilities of the drop tube faciltiy provide ideal conditions for a study of this type. To date, several Ni60Nb40 samples have been levitated, melted and cooled during 4.6 seconds of free fall in the 100 meter drop tube. Structures obtained are discussed.

  18. Phase composition, microstructure and microhardness of electroless nickel composite coating co-deposited with SiC on cast aluminium LM24 alloy substrate

    OpenAIRE

    2013-01-01

    Electroless Ni–P (EN) and composite Ni–P–SiC (ENC) coatings were developed on cast aluminium alloy substrate, LM24. The coating phase composition, microstructure and microhardness were investigated using X-ray diffraction (XRD), scanning electron microscopy (SEM) and microhardness tester, respectively, on as-plated and heat-treated specimens. The original microstructure of the Ni–P matrix is not affected by the inclusion of the hard particles SiC. No formation of Ni–Si phase was observed up t...

  19. Characterisation of phase composition, microstructure and microhardness of electroless nickel composite coating co-deposited with SiC on casting aluminium LM24 alloy substrate

    OpenAIRE

    2013-01-01

    Electroless Ni-P (EN) and composite Ni-P-SiC (ENC) coatings were developed on cast aluminium alloy, LM24. The coating phase composition, microstructure and microhardness were investigated using X-ray diffraction (XRD), scanning electron microscopy (SEM) and microhardness tester, respectively, on as-plated and heat-treated specimens. The original microstructure of the Ni-P matrix is not affected by the inclusion of the hard particles SiC. No formation of Ni-Si phase was observed upto 500°C of ...

  20. Porosity evolution in additively manufactured aluminium alloy during high temperature exposure

    Science.gov (United States)

    Bai, J.; Ding, H. L.; Gu, J. L.; Wang, X. S.; Qiu, H.

    2017-01-01

    A 2319 aluminum alloy is deposited by the Wire+Arc Additive Manufacturing technology with Cold Metal Transfer process. Porosity that are both existing in the as-deposited and as-heat treated state metal are revealed by optical microscopy and quantitatively analyzed. It explains the reason why the newly initiated pores are easily tend to gather between each layer around the fusion line zone for the WAAM metal after heat treatment. The inner morphology of the pores are demonstrated by Scanning Electron Microscopy. Porosity evolution and distribution during high temperature exposure are demonstrated. Thus two porosity growth and number increase mechanisms are proposed eventually, providing theoretical basis for related material design and process optimization.

  1. Effect of partition coefficient on microsegregation during solidification of aluminium alloys

    Institute of Scientific and Technical Information of China (English)

    MH Avazkonandeh-Gharavol; M Haddad-Sabzevar; H Fredriksson

    2014-01-01

    In the modeling of microsegregation, the partition coefficient is usually calculated using data from the equilibrium phase diagrams. The aim of this study was to experimentally and theoretically analyze the partition coefficient in binary aluminum-copper alloys. The sam-ples were analyzed by differential thermal analysis (DTA), which were melted and quenched from different temperatures during solidifica-tion. The mass fraction and composition of phases were measured by image processing and scanning electron microscopy (SEM) equipped with an energy-dispersive X-ray spectroscopy (EDS) unit. These data were used to calculate as the experimental partition coefficients with four different methods. The experimental and equilibrium partition coefficients were used to model the concentration profile in the primary phase. The modeling results show that the profiles calculated by the experimental partition coefficients are more consistent with the experi-mental profiles, compared to those calculated using the equilibrium partition coefficients.

  2. On the melt infiltration of copper coated silicon carbide with an aluminium alloy

    Science.gov (United States)

    Asthana, R.; Rohatgi, P. K.

    1992-01-01

    Pressure-assisted infiltration of porous compacts of Cu coated and uncoated single crystals of platelet shaped alpha (hexagonal) SiC was used to study infiltration dynamics and particulate wettability with a 2014 Al alloy. The infiltration lengths were measured for a range of experimental variables which included infiltration pressure, infiltration time, and SiC size. A threshold pressure (P(th)) for flow initiation through compacts was identified from an analysis of infiltration data; P(th) decreased while penetration lengths increased with increasing SiC size (more fundamentally, due to changes in interparticle pore size) and with increasing infiltration times. Cu coated SiC led to lower P(th) and 60-80 percent larger penetration lengths compared to uncoated SiC under identical processing conditions.

  3. Effect of welding techniques on microstructure and mechanical properties of aluminium-lithium alloy welds

    Energy Technology Data Exchange (ETDEWEB)

    Madhusudhan Reddy, G.; Gokhale, A.A.; Saxena, V.K. [Defence Metallurgical Research Lab., Hyderabad (India); Prasad Rao, K.

    2000-07-01

    The tensile properties and fatigue crack growth behaviour of sheets of an Al-1.9Li-1.8Cu-1.0 Mg-0.1Zr alloy welded under different conditions were evaluated. The basic welding technique was constant current (CC) gas tungsten arc (GTA) welding. Two modifications viz. pulsed current (PC) and magnetic arc oscillation (AO) were introduced to study effects on microstructure and properties. Both PC and AO resulted in microstructural refinement in the fusion zone. The tensile residual stresses present in CC welds reduced when either PC or AO welding was used. The tensile strength and ductility increased, and fatigue crack growth rates lowered when PC or AO conditions replaced CC welding. (orig.)

  4. Spectroscopic study of plasma during electrolytic oxidation of magnesium- and aluminium-alloy

    Science.gov (United States)

    Jovović, J.; Stojadinović, S.; Šišović, N. M.; Konjević, N.

    2012-10-01

    We present the results of an optical emission spectroscopy study of Plasma during Electrolytic Oxidation (PEO) of magnesium- and aluminum-alloy. Plasma electron number density Ne diagnostics is performed either from the Hβ line shape or from the width or shift of non-hydrogenic ion lines of aluminum and magnesium. The line profile analysis of the Hβ suggests presence of two PEO processes characterized by relatively low electron number densities Ne≈1.2×1015 cm-3 and Ne≈2.3×1016 cm-3. Apart from these two low Ne processes, there is the third one related to the ejection of evaporated anode material through micro-discharge channels. This process is characterized by larger electron density Ne=(1.2-1.6)1017 cm-3, which is detected from the shape and shift of aluminum and magnesium singly charged ion lines. Two low Ne values detected from the Hβ and large Ne measured from the widths and shift of ion lines suggest presence of three types of discharges during PEO with aluminum- and magnesium-alloy anode. On the basis of present and earlier results one can conclude that low Ne processes do not depend upon anode material or electrolyte composition.The electron temperature of 4000 K and 33,000 K are determined from relative intensities of Mg I and O II lines, respectively. The attention is drawn to the possibility of Ne application for Te evaluation using Saha equation what is of importance for PEO metal plasma characterization. During the course of this study, difficulties in the analysis of spectral line shapes are encountered and the ways to overcome some of the obstacles are demonstrated.

  5. Tensile properties and fracture toughness of Zr–2.5Nb alloy pressure tubes of IPHWR220

    Energy Technology Data Exchange (ETDEWEB)

    Khandelwal, H.K. [Mechanical Metallurgy Division, Bhabha Atomic Research Centre, Trombay, Mumbai 400085 (India); Homi Bhabha National Institute, Anushaktinagar, Mumbai 400094 (India); Singh, R.N., E-mail: rnsingh@barc.gov.in [Mechanical Metallurgy Division, Bhabha Atomic Research Centre, Trombay, Mumbai 400085 (India); Homi Bhabha National Institute, Anushaktinagar, Mumbai 400094 (India); Bind, A.K.; Sunil, S.; Chakravartty, J.K. [Mechanical Metallurgy Division, Bhabha Atomic Research Centre, Trombay, Mumbai 400085 (India); Ghosh, A.; Dhandharia, P.; Bhachawat, D. [Engineering Directorate, Nuclear Power Corporation of India Ltd., NUB, Anushaktinagar, Mumbai 400094 (India); Shekhar, R.; Kumar, Sunil Jai [National Centre for Compositional Characterisation of Materials, Bhabha Atomic Research Centre, ECIL (PO), Hyderabad 500 062 (India)

    2015-11-15

    Highlights: • Evaluated tensile properties & fracture toughness of Zr–2.5Nb pressure tube alloy. • Studied the effect of test temperature, sample location and ingot melting. • Quadruple melting improves fracture toughness despite variation in fabrication route. • Fracture toughness of IPHWR220 pressure tubes compared with CANDU material. - Abstract: The pressure tubes of Indian Pressurized Heavy Water Reactor (IPHWR) of 220 MWe are made of Zr–2.5Nb alloy manufactured either from Double Melted (DM) or from Quadruple Melted (QM) ingots. These pressure tubes are manufactured by hot extrusion, two stages of cold pilgering with intermediate annealing and autoclaving. To achieve good in-reactor performance, it is required to have minimum variability in the mechanical properties of the pressure tube across its length and between tube to tube. In this work, tensile properties and fracture toughness parameters (J{sub max}, dJ/da and CCL determined as per ASTM E1820-11 standard) of unirradiated Zr–2.5Nb alloy pressure tubes manufactured from DM and QM ingots using samples obtained from front and back end of the tubes is presented. The mechanical properties were evaluated in temperature range of 25–450 °C and compared with the corresponding data reported in literature for CANDU pressure tubes.

  6. CROSS-ROLL FLOW FORMING OF ODS ALLOY HEAT EXCHANGER TUBES FOR HOOP CREEP ENHANCEMENT

    Energy Technology Data Exchange (ETDEWEB)

    Bimal K. Kad

    2005-06-27

    Mechanically alloyed oxide dispersion strengthened (ODS) Fe-Cr-Al alloy thin walled tubes and sheets, produced via powder processing and consolidation methodologies, are promising materials for eventual use at temperatures up to 1200 C in the power generation industry, far above the temperature capabilities of conventional alloys. Target end-uses range from gas turbine combustor liners to high aspect ratio (L/D) heat exchanger tubes. Grain boundary creep processes at service temperatures, particularly those acting in the hoop direction, are the dominant failure mechanisms for such components. The processed microstructure of ODS alloys consists of high aspect ratio grains aligned parallel to the tube axis, a result of dominant axial metal flow which aligns the dispersoid particles and other impurities in the longitudinal direction. The dispersion distribution is unaltered on a micro scale by recrystallization thermal treatments, but the high aspect ratio grain shape typically obtained limits transverse grain spacing and consequently the hoop creep response. Improving hoop creep in ODS-alloy components will require understanding and manipulating the factors that control the recrystallization behavior, and represents a critical materials design and development challenge that must be overcome in order to fully exploit the potential of ODS alloys. The objectives of this program are to (1) increase creep-strength at temperature in ODS-alloy tube and liner components by 100% via, (2) preferential cross-roll flow forming and grain/particle fibering in the critical hoop direction. Recent studies in cross-rolled ODS-alloy sheets (produced from flattened tubes) indicate that transverse creep is significantly enhanced via controlled transverse grain fibering, and similar improvements are expected for cross-rolled tubes. The research program outlined here is iterative in nature and is intended to systematically (i) prescribe extrusion consolidation methodologies via detailed

  7. Cross-Roll Flow Forming of ODS Alloy Heat Exchanger Tubes For Hoop Creep Enhancement

    Energy Technology Data Exchange (ETDEWEB)

    Bimal Kad

    2007-09-30

    Mechanically alloyed oxide dispersion strengthened (ODS) Fe-Cr-Al alloy thin walled tubes and sheets, produced via powder processing and consolidation methodologies are promising materials for eventual use at temperatures up to 1200 C in the power generation industry, far above the temperature capabilities of conventional alloys. Target end-uses range from gas turbine combustor liners to high aspect ratio (L/D) heat exchanger tubes. Grain boundary creep processes at service temperatures, particularly those acting in the hoop direction, are the dominant failure mechanisms for such components. The processed microstructure of ODS alloys consists of high aspect ratio grains aligned parallel to the tube axis, a result of dominant axial metal flow which aligns the dispersoid particles and other impurities in the longitudinal direction. The dispersion distribution is unaltered on a micro scale by recrystallization thermal treatments, but the high aspect ratio grain shape typically obtained limits transverse grain spacing and consequently the hoop creep response. Improving hoop creep in ODS-alloy components will require understanding and manipulating the factors that control the recrystallization behavior, and represents a critical materials design and development challenge that must be overcome in order to fully exploit the potential of ODS alloys. The objectives of this program were to (1) increase creep-strength at temperature in ODS-alloy tube and liner components by 100% via, (2) preferential cross-roll flow forming and grain/particle fibering in the critical hoop direction. The research program outlined was iterative and intended to systematically (i) examine and identify post-extrusion forming methodologies to create hoop strengthened tubes, to be (ii) evaluated at 'in-service' loads at service temperatures and environments. Our report outlines the significant hoop creep enhancements possible via secondary cross-rolling and/or flow-forming operations. Each

  8. Characterization of Tubing from Advanced ODS alloy (FCRD-NFA1)

    Energy Technology Data Exchange (ETDEWEB)

    Maloy, Stuart Andrew [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Aydogan, Eda [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Anderoglu, Osman [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Lavender, Curt [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Anderson, Iver [Ames Lab., Ames, IA (United States); Rieken, Joel [Ames Lab., Ames, IA (United States); Lewandowski, John [Case Western Reserve Univ., Cleveland, OH (United States); Hoelzer, Dave [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Odette, George R. [Univ. of California, Santa Barbara, CA (United States)

    2016-09-20

    Fabrication methods are being developed and tested for producing fuel clad tubing of the advanced ODS 14YWT and FCRD-NFA1 ferritic alloys. Three fabrication methods were based on plastically deforming a machined thick-wall tube sample of the ODS alloys by pilgering, hydrostatic extrusion or drawing to decrease the outer diameter and wall thickness and increase the length of the final tube. The fourth fabrication method consisted of the additive manufacturing approach involving solid-state spray deposition (SSSD) of ball milled and annealed powder of 14YWT for producing thin-wall tubes. Of the four fabrication methods, two methods were successful at producing tubing for further characterization: production of tubing by high-velocity oxy-fuel spray forming and production of tubing using high-temperature hydrostatic extrusion. The characterization described shows through neutron diffraction the texture produced during extrusion while maintaining the beneficial oxide dispersion. In this research, the parameters for innovative thermal spray deposition and hot extrusion processing methods have been developed to produce the final nanostructured ferritic alloy (NFA) tubes having approximately 0.5 mm wall thickness. Effect of different processing routes on texture and grain boundary characteristics has been investigated. It was found that hydrostatic extrusion results in combination of plane strain and shear deformations which generate rolling textures of α- and γ-fibers on {001}<110> and {111}<110> together with a shear texture of ζ-fiber on {011}<211> and {011}<011>. On the other hand, multi-step plane strain deformation in cross directions leads to a strong rolling textures of θ- and ε-fiber on {001}<110> together with weak γ-fiber on {111}<112>. Even though the amount of the equivalent strain is similar, shear deformation leads to much lower texture indexes compared to the plane strain deformations. Moreover, while 50% of hot rolling brings about a large number of

  9. Distribution of Si particles in hypereutectic aluminum alloy tubes prepared under electromagnetic field

    Institute of Scientific and Technical Information of China (English)

    ZHANG Zhi-qing; LI Qiu-lin; LIU Wei; LIU Qing

    2006-01-01

    Hypereutectic Al-Si alloy tubes were produced by centrifugal casting process using an electromagnetic field (EMF). A gradient distribution of the primary Si particles was formed along the tube thickness direction. In the absence of EMF the primary Si moves to inner periphery with increasing rotation speed. The distribution of primary Si can be controlled by the EMF. With increasing electromagnetic field intensity, the primary Si moves from the inner periphery to the outer periphery of the tubes. Most of the primary Si can be driven to the outer if the electromagnetic field intensity is increased to a certain value. It is found that the particle distribution and local volume fraction vary with both the rotation speed and the electromagnetic field intensity.

  10. The effects of nickel-pigmented aluminium oxide selective coating over aluminium alloy on the optical properties and thermal efficiency of the selective absorber prepared by alternate and reverse periodic plating technique

    Energy Technology Data Exchange (ETDEWEB)

    Wazwaz, A. [Chemical Engineering Department, College of Engineering, Dhofar University, P.O. Box 2509, Postal Code 211, Salalah (Oman); Salmi, J. [Marion Technologies Nanomaterials, Nanostructured Materials and Ceramic Powders, Cap Delta - Parc Technologique, Delta Sud, F-09340 Verniolle (France); Bes, R. [CIRIMAT/LCMIE, Universite Paul Sabatier, 31062 Toulouse Cedex 4 (France)

    2010-08-15

    Diffused reflectance measurements and Kubelka-Munk values were studied. The effects of the alumina layer and the nickel content on the optical properties of the selective absorber were discussed. In general and with respect to aluminium alloy substrate, the diffused reflectance decreased by 85.25-91.42% ({+-}0.01%). The emissivity increased by a factor of 252.50-624.50 ({+-}0.01). The average absorptivity increased by a factor of 4.99-5.35 ({+-}0.01). The average thermal efficiency is increased by a factor of 4.51-4.80 ({+-}0.01). The sample of nickel content 60 {mu}g/cm{sup 2} was found to have the optimum optical properties as a good selective absorber. It has the highest solar selectivity by the two measurements. The range of hemispherical solar selectivity is 4.22-8.36 ({+-}0.01); while for average solar selectivity is 7.410-17.456 ({+-}0.001). We found that the thermal efficiency is increased by increasing the nickel content to a certain limit (60 {mu}g/cm{sup 2}) then it decreased after this limit due to the increase in the emissivity. Also, the total hemispherical optical properties are accordance with the averaged optical properties obtained from diffused reflectance measurements over the solar range. The nickel-pigmented aluminium oxide is one of the best selective absorbers for the photo thermal conversion and it is of high durability. (author)

  11. Behaviour and fatigue damage study of cast aluminium alloys; Etude du comportement et de l'endommagement en fatigue d'alliages d'aluminium de fonderie

    Energy Technology Data Exchange (ETDEWEB)

    Barlas, B.

    2004-02-15

    This study is aimed at determining the influence of chemical composition and heat treatment of cast aluminium alloys Al-Si-Cu-Mg on mechanical behaviour and fatigue life of structures. The industrial frame of this study concerns cylinder-heads of high efficiency diesel engines, for Renault and Montupet companies. The experimental means involved in this work are as well microscopic (TEM, microhardness, image analysis), mechanical (LCF and aniso-thermal tests, macro-hardness) and numerical (simulation of the stability of the hardening phases, behaviour and damage model identification, cylinder-head life time calculation). The link between micro and macro approaches is provided by the means of an internal microscopic variable representing thermal aging through coarsening of the precipitates and implemented into the macroscopic model. (author)

  12. Investigation of surface finishing of carbon based coated tools for dry deep drawing of aluminium alloys

    Science.gov (United States)

    Steiner, J.; Andreas, K.; Merklein, M.

    2016-11-01

    Global trends like growing environmental awareness and demand for resource efficiency motivate an abandonment of lubricants in metal forming. However, dry forming evokes increased friction and wear. Especially, dry deep drawing of aluminum alloys leads to intensive interaction between tool and workpiece due to its high adhesion tendency. One approach to improve the tribological behavior is the application of carbon based coatings. These coatings are characterized by high wear resistance. In order to investigate the potential of carbon based coatings for dry deep drawing, friction and wear behavior of different coating compositions are evaluated in strip drawing tests. This setup is used to model the tribological conditions in the flange area of deep drawing operations. The tribological behavior of tetrahedral amorphous (ta-C) and hydrogenated amorphous carbon coatings with and without tungsten modification (a-C:H:W, a-C:H) is investigated. The influence of tool topography is analyzed by applying different surface finishing. The results show reduced friction with decreased roughness for coated tools. Besides tool topography the coating type determines the tribological conditions. Smooth tools with ta-C and a-C:H coatings reveal low friction and prevent adhesive wear. In contrast, smooth a-C:H:W coated tools only lead to slight improvement compared to rough, uncoated specimen.

  13. Market Opportunity of Some Aluminium Silicon Alloys Materials through Changing the Casting Process

    Directory of Open Access Journals (Sweden)

    Delfim SOARES

    2012-08-01

    Full Text Available Fatigue is considered to be the most common mechanism by which engineering components fail, and it accounts for at least 90% of all service failures attributed to mechanical causes. Mechanical properties (tensile strength, tensile strain, Young modulus, etc as well as fatigue properties (fatigue life are very dependent on casting method. The most direct effects of casting techniques are on the metallurgical microstructure that bounds the mechanical properties. One of the important variables affected by the casting technique is the cooling rate which is well known to strongly restrict the microstructure. In the present research has been done a comparison of fatigue properties of two aluminum silicon alloys obtained by two casting techniques. It was observed that the fatigue life is increasing with 24% for Al12Si and 31% for AL18Si by using centrifugal casting process instead of gravity casting. This increasing in fatigue life means that a component tailored from materials obtained by centrifugal casting will stay longer in service. It was made an estimation of the time required to recover the costs of technology in order to use the centrifuge process that will allow to obtain materials with improved properties. The amortization can be achieved by using two different marketing techniques: through the release of the product at the old price and with much longer life of the component which means "same price - longer life", or increasing price, by highlighting new product performance which means "higher price - higher properties".

  14. Investigation of Corrosion Behaviour of Aluminium Alloy Subjected to Laser Shock Peening without a Protective Coating

    Directory of Open Access Journals (Sweden)

    U. Trdan

    2015-01-01

    Full Text Available The effect of shock waves and strain hardening of laser shock peening without protective coating (LSPwC on alloy AA 6082-T651 was investigated. Analysis of residual stresses confirmed high compression in the near surface layer due to the ultrahigh plastic strains and strain rates induced by multiple laser shock waves. Corrosion tests in a chloride environment were carried out to determine resistance to localised attack, which was also verified on SEM/EDS. OCP transients confirmed an improved condition, that is, a more positive and stable potential after LSPwC treatment. Moreover, polarisation resistance of the LSPwC treated specimen was by a factor of 25 higher compared to the untreated specimen. Analysis of voltammograms confirmed an improved enhanced region of passivity and significantly smaller anodic current density of the LSPwC specimen compared to the untreated one. Through SEM, reduction of pitting attack at the LSPwC specimen surface was confirmed, despite its increased roughness.

  15. The effect of welding parameters on surface quality of AA6351 aluminium alloy

    Science.gov (United States)

    Yacob, S.; MAli, M. A.; Ahsan, Q.; Ariffin, N.; Ali, R.; Arshad, A.; Wahab, M. I. A.; Ismail, S. A.; Roji, NS M.; Din, W. B. W.; Zakaria, M. H.; Abdullah, A.; Yusof, M. I.; Kamarulzaman, K. Z.; Mahyuddin, A.; Hamzah, M. N.; Roslan, R.

    2015-12-01

    In the present work, the effects of gas metal arc welding-cold metal transfer (GMAW-CMT) parameters on surface roughness are experimentally assessed. The purpose of this study is to develop a better understanding of the effects of welding speed, material thickness and contact tip to work distance on the surface roughness. Experiments are conducted using single pass gas metal arc welding-cold metal transfer (GMAW-CMT) welding technique to join the material. The material used in this experiment was AA6351 aluminum alloy with the thickness of 5mm and 6mm. A Mahr Marsuft XR 20 machine was used to measure the average roughness (Ra) of AA6351 joints. The main and interaction effect analysis was carried out to identify process parameters that affect the surface roughness. The results show that all the input process parameters affect the surface roughness of AA6351 joints. Additionally, the average roughness (Ra) results also show a decreasing trend with increased of welding speed. It is proven that gas metal arc welding-cold metal transfer (GMAW-CMT)welding process has been successful in term of providing weld joint of good surface quality for AA6351 based on the low value surface roughness condition obtained in this setup. The outcome of this experimental shall be valuable for future fabrication process in order to obtained high good quality weld.

  16. Friction Stir Welds (FSW of aluminium alloy AW6082-T6

    Directory of Open Access Journals (Sweden)

    J. Adamowski

    2007-01-01

    Full Text Available Purpose: Purpose of this paper is the investigation on the properties and microstructural changes in Friction StirWelds in the aluminum alloy 6082-T6 in function of varying process parameters.Design/methodology/approach: Tensile strength of the produced joints was tested and the correlation withprocess parameter was assessed. Microstructures of various zones of FSW welds are presented and analyzed bymeans of optical microscopy and microhardness measurements.Findings: Mechanical resistance of test welds increased with the increase of travel (welding speed withconstant rotational speed. Softening of the material in weld nugget and heat affected zone was observed, ofentity inferior that that of fusion welds. Origin of tunnel (worm hole defects were found and analyzed.Research limitations/implications: The test welds were produced with various combinations of processparameters without the possibility of controlling the downward force. Further extension of applicable parameterscombinations could be examined.Practical implications: The increase of mechanical resistance with increasing welding speed offers animmediate economic return, as the process efficiency is increased.Originality/value: Information contained herein can be useful to further investigate on the possibility ofimproving the properties of FSW welds, as well as the efficiency of the process.

  17. Cross-Roll Flow Forming of ODS Alloy Heat Exchanger Tubes for Hoop Creep Enhancement

    Energy Technology Data Exchange (ETDEWEB)

    Bimal K. Kad

    2006-04-10

    Mechanically alloyed oxide dispersion strengthened (ODS) Fe-Cr-Al alloy thin walled tubes and sheets, produced via powder processing and consolidation methodologies, are promising materials for eventual use at temperatures up to 1200 C in the power generation industry, far above the temperature capabilities of conventional alloys. Target end-uses range from gas turbine combustor liners to high aspect ratio (L/D) heat exchanger tubes. Grain boundary creep processes at service temperatures, particularly those acting in the hoop direction, are the dominant failure mechanisms for such components. The processed microstructure of ODS alloys consists of high aspect ratio grains aligned parallel to the tube axis, a result of dominant axial metal flow which aligns the dispersoid particles and other impurities in the longitudinal direction. The dispersion distribution is unaltered on a micro scale by recrystallization thermal treatments, but the high aspect ratio grain shape typically obtained limits transverse grain spacing and consequently the hoop creep response. Improving hoop creep in ODS-alloy components will require understanding and manipulating the factors that control the recrystallization behavior, and represents a critical materials design and development challenge that must be overcome in order to fully exploit the potential of ODS alloys. The objectives of this program are to (1) increase creep-strength at temperature in ODS-alloy tube and liner components by 100% via, (2) preferential cross-roll flow forming and grain/particle fibering in the critical hoop direction. The research program outlined here is iterative in nature and is intended to systematically (1) examine and identify post-extrusion forming methodologies to create hoop strengthened tubes, which will be (2) evaluated at ''in-service'' loads at service temperatures and environments. This research program is being conducted in collaboration with the DOE's Oak Ridge National

  18. The influence of Mg content and impurities in AA5083 alloy on the properties of flow formed tubes

    Directory of Open Access Journals (Sweden)

    Milutin Nikačević

    2013-12-01

    Full Text Available Microstructure and mechanical properties of flow formed thin-walled tubes of AA5083 alloy from two metallurgical heats are presented. The influence of the chemical composition and applied reduction on the surface features and residual macro stresses were also studied. The residual macro stresses were estimated by ring method. The heat with higher content of alloying elements and impurities (Mg, Mn, Fe, Si had higher strength of preforms as well as flow formed tubes. These tubes exhibit three times higher residual stresses, lower spinnability, and the large amount of the surface defects (microcracks. This behaviour is attributed to the inhomogeneous material flow during deformation and presence of impurities.

  19. The influence of manufacturing processes on the microstructure, grain boundary characteristics and SCC behavior of Alloy 690 steam generator tubing

    Energy Technology Data Exchange (ETDEWEB)

    Sarver, J.M. [Babcock and Wilcox, Alliance, OH (United States). Research and Development Division; Doherty, P.E.; Doyle, D.M. [Babcock and Wilcox International Division, Cambridge, Ontario (Canada); Palumbo, G. [Ontario Hydro Technologies, Toronto, Ontario (Canada)

    1995-12-31

    Thermally treated Alloy 690 is the tubing material of choice for replacement steam generators in the United States. Throughout the world, it is manufactured using different melting and thermomechanical processing methods. The influence of different processing steps on the intergranular stress corrosion cracking (IGSCC) behavior of Alloy 690 has not been thoroughly evaluated. Evaluations were performed on Alloy 690 steam generator tubing produced using several different melting practices and thermomechanical processing procedures. The evaluations included extensive microstructural examinations as well as constant extension rate (CERT) tests. The CERT test results indicated that the thermally treated Alloy 690 tubing which was subjected to higher annealing temperatures displayed the highest degree of resistance to stress corrosion cracking (SCC). Examination of the microstructures indicated that the microstructural changes which are produced by increased annealing temperatures are subtle. In an attempt to further elucidate and quantify the effect of manufacturing processes on corrosion behavior, grain boundary character distribution (GBCD) measurements were performed on the same materials which were CERT tested. Analysis of GBCDs of the samples used in this study indicate that Alloy 690 exhibits a significantly larger fraction of special boundaries as compared to Alloy 600 and Alloy 800, regardless of the processing history of the tubing. Preliminary results indicate that a correlation may exist between processing method, GBCD`s and degree of IGSCC exhibited by the thermally treated samples examined in this study.

  20. Pengaruh Variasi Komposisi Serbuk Kayu Dengan Pengikat Semen Pada Pasir Cetak Terhadap Cacat Porositas Dan Kekasaran Permukaan Hasil Pengecoran Aluminium Alloy 6061

    Directory of Open Access Journals (Sweden)

    Fatkhur M Rohman

    2014-09-01

    Full Text Available Proses pengecoran dilakukan dengan cara mencairkan logam dalam dapur pelebur, kemudian dituangkan ke dalam cetakan dan dibiarkan membeku hingga dapat dikeluarkan dari dalam cetakan. Faktor yang berpengaruh terhadap kualitas hasil pengecoran cetakan pasir, diantaranya adalah komposisi cetakan pasir dan perancangan sistem saluran (gatting system. Pada penelitian ini bertujuan untuk menganalisa pengaruh variasi komposisi serbuk kayu dengan pengikat semen pada pasir cetak terhadap cacat porositas dan kekasaran permukaan hasil pengecoran aluminium alloy 6061. Bahan yang digunakan pada penelitian ini adalah aluminium Alloy 6061 dan komposisi semen dan air sebesar 6%, komposisi serbuk kayu sebesar 1%, 2%, 3%, 4%, 5% dan 6%  komposisi pasir silika sebesar 87%, 86%, 85%, 84%, 83% dan 82%. Dari hasil penelitian ini didapatkan nilai uji permeabilitas pasir cetak cenderung bertambah seiring dengan bertambahnya serbuk kayu. Nilai uji kompresi pasir cetak cenderung berkurang seiring dengan bertambahnya serbuk kayu.. Nilai pengujian porositas benda hasil coran didapatkan nilai terkecil terletak pada komposisi serbuk kayu 6% dan nilainya sebesar 0,25%, sedangkan nilai pengujian porositas benda hasil coran terbesar terletak pada komposisi serbuk kayu 1% dengan nilai sebesar 4,96%. Nilai pengujian kekasaran permukaan benda hasil coran didapatkan nilai terkecil terletak pada komposisi serbuk kayu 6% dan nilainya sebesar 0,06µm, sedangkan nilai pengujian kekasaran permukaan benda hasil coran terbesar terletak pada komposisi serbuk kayu 1% dengan nilai sebesar 2,00µm.

  1. Effect of Welding Speed and Tool Pin Geometry on Impact Strength in Friction Stir Welding of Aluminium 6101 T6 Alloy

    Directory of Open Access Journals (Sweden)

    Singh Rajbir

    2016-01-01

    Full Text Available Friction stir welding (FSW process is a solid state joining method in which the material that is being welded does not melt and recast. This process uses a non-consumable tool to generate frictional heat in the abutting surfaces. The welding parameters play a major role in deciding the joint characteristics. In this investigation the effect of welding speed and tool pin geometry in friction stir welds of Aluminium alloy was studied. The welded joints were made of Aluminium alloy AA 6101 T6 strips of 6mm thickness with different tool pin profile (Cylindrical, Taper cylindrical, Square and Taper Square. All the welding operations were done at the room temperature. Charpy tests were carried out to find the impact strength. From this investigation it is found that strength is superior with taper square tool pin profile than cylindrical, taper cylindrical and square tool pin profile. The pieces weld at rotational speed of 1200 r.p.m and welding speed of 70mm/min using taper square tool have higher strength.

  2. Deformation Mechanism of Hot Spinning of NiTi Shape Memory Alloy Tube Based on FEM

    Institute of Scientific and Technical Information of China (English)

    JIANG Shuyong; ZHANG Yanqiu; ZHENG Yufeng; LI Chunfeng

    2012-01-01

    As a successively and locally plastic deformation process,ball spinning is applied to manufacturing thin-walled Nickel-Titanium shape memory alloy (NiTi SMA) tube at high temperature.NiTi SMA tube blank belongs to the as-cast state which consists of a lot of dendritic grains and a few equiaxed grains.The compression tests of NiTi SMA were carried out at various strain rates at high temperature in order to obtain the constitutive model of NiTi SMA.Because NiTi SMA is sensitive to the strain rates at high temperature,rigid-viscoplastic finite element method (FEM) is used to simulate ball spinning of thin-walled NiTi SMA tube in order to analyze the deformation behavior of ball spinning of NiTi SMA tube.Stress fields,strain fields as well as velocity fields is obtained by means of rigid-viscoplastic FEM,which lays the profound foundations for studying the metal flow rule in ball spinning and forming perfect spun NiTi SMA tube.

  3. The Effect of Thermal Treatment on Mechanical Property of Alloy 690 Tubes

    Energy Technology Data Exchange (ETDEWEB)

    Jang, Ki-Nam; Cha, Hyun-Jin; An, Ji-Hyeong; Kim, Kyu-Tae [Dongguk University, Gyeongju (Korea, Republic of)

    2015-10-15

    The effect of thermal treatment on mechanical property of alloy 690 was investigated using tube specimens thermal treated in vacuum chamber at 705 .deg. C, 716 .deg. C, 727 .deg. C, 738 .deg. C, 749 .deg. C for 12 hours. The ultimate tensile strength and elongation was the highest at 727 .deg. C. Both the UTS and EL increased, it may be caused by dislocation and Cr carbides. Three types of alloy 690 were used in this paper. Fig.1 shows the configuration of ring specimen. The chemical composition is given in Table I. P55 and N55 are manufactured using mother pipe with outer diameter of 55mm, and N63 are manufactured using mother pipe with outer diameter of 63mm. N63 and N55 have the same chemical composition. During the long- term operation, the steam generator tubes were degraded under this condition. Stress corrosion crack(SCC) is one of the most serious problems of alloy 690. It is closely related to the amount of Cr in the grain boundary. This paper describes the effect of heat-treatment conditions on mechanical properties and microstructure.

  4. Compact-immersed-tube bath heating for anodizing aluminum sections; Le chauffage de bains par tubes immerges compacts pour l`anodisation de profiles aluminium

    Energy Technology Data Exchange (ETDEWEB)

    Bouillet, B. [Societe Alusuisse (France); Lhomme, P.J. [Gaz de France (GDF), 75 - Paris (France)

    1996-12-31

    The compact-immersed-tube system is composed of a burner, a combustor (where natural gas is burned) and a heat exchanger tube (where combustion heat is released to the surrounding bath); its compact configuration is designed for a direct implementation in an industrial process vessel. Natural gas is thus directly used at the utilization location, without any vapour stage and distribution heat losses. Temperature regulation, efficiency, corrosion issues and power requirements are discussed. An application example with the bath heating for aluminum anodization, is presented: energy savings and payback periods are discussed

  5. 铝热法制备高钒铝合金的研究%Study on high grade vanadium-aluminium alloy prepared by aluminothermic reaction

    Institute of Scientific and Technical Information of China (English)

    喇培清; 卢学峰; 申达; 魏玉鹏; 王鸿鼎; 郭鑫

    2012-01-01

    用V2O5粉和Al粉为原料,通过铝热还原法制备了高钒铝合金,研究了反应物配比中Al含量对制备的高钒铝合金纯度和钒回收率的影响.结果表明:当反应物配比中Al欠量5%时,高钒铝合金的纯度最高为98.45%;随着反应物配比中Al含量的增加,高钒铝合金的纯度降低,钒的回收率增加,在Al过量15%时回收率最高为92.4%(质量分数).高钒铝合金的布氏硬度在Al欠量5%时最低,为213.6 HB;在Al过量15%时布氏硬度最大,为250 HB.可以通过调节原料中Al含量来制备不同纯度的高钒铝合金.%High grade vanadium - aluminium alloy was prepared by aluminothermic reaction using V2O5 and Al powders as raw materials. The effects of Al content in raw materials on purity of alloy and recovery of vanadium were investigated in this study. The results show that the purity of vanadium decreases with the addition of aluminum element in raw materials and there exists a maximum value of 98. 45% when aluminum element is 5% shortfall in raw materials. The recovery rate of vanadium increases with increasing aluminum element in raw materials and there exists a maximum value of 92. 4% when aluminum element is 15% excess in raw materials. Brinell hardness of alloy comes to the minimum value of 213. 6 HB when aluminum element is 5% shortfall, and comes to the maximum value of 250 HB when aluminum element is 15% excess. The high grade vanadium - aluminium alloy with different purities can be prepared by varying the content of aluminium in raw materials.

  6. Brazing open cell reticulated copper foam to stainless steel tubing with vacuum furnace brazed gold/indium alloy plating

    Science.gov (United States)

    Howard, Stanley R.; Korinko, Paul S.

    2008-05-27

    A method of fabricating a heat exchanger includes brush electroplating plated layers for a brazing alloy onto a stainless steel tube in thin layers, over a nickel strike having a 1.3 .mu.m thickness. The resultant Au-18 In composition may be applied as a first layer of indium, 1.47 .mu.m thick, and a second layer of gold, 2.54 .mu.m thick. The order of plating helps control brazing erosion. Excessive amounts of brazing material are avoided by controlling the electroplating process. The reticulated copper foam rings are interference fit to the stainless steel tube, and in contact with the plated layers. The copper foam rings, the plated layers for brazing alloy, and the stainless steel tube are heated and cooled in a vacuum furnace at controlled rates, forming a bond of the copper foam rings to the stainless steel tube that improves heat transfer between the tube and the copper foam.

  7. Fireside corrosion testing of candidate superheater tube alloys, coatings, and claddings - phase II

    Energy Technology Data Exchange (ETDEWEB)

    Blough, J.L.; Stanko, G.J. [Foster Wheeler Development Corp., Livingston, NJ (United States)

    1996-08-01

    In Phase I a variety of developmental and commercial tubing alloys and claddings were exposed to laboratory fireside corrosion testing simulating a superheater or reheater in a coal-fired boiler. Phase II (in situ testing) has exposed samples of 347, RA-8511, HR3C, 253MA, Fe{sub 3}Al + 5Cr, 310 modified, 800HT, NF 709, 690 clad, and 671 clad for over 10,000 hours to the actual operating conditions of a 250-MW coal-fired boiler. The samples were installed on an air-cooled, retractable corrosion probe, installed in the reheater cavity, and controlled to the operating metal temperatures of an existing and advanced-cycle coal-fired boiler. Samples of each alloy will be exposed for 4000, 12,000, and 16,000 hours of operation. The results will be presented for the metallurgical examination of the corrosion probe samples after 4000 hours of exposure.

  8. Specific Energy Absorbed Study Of Aluminum (2024-351T Tubes Alloy Under Lateral Crush

    Directory of Open Access Journals (Sweden)

    Ayad Arab Ghaidan

    2013-04-01

    Full Text Available This paper aims to find SEA (Specific Energy Absorber for lateral crushing (statically behavior for Aluminum (2024-T351 alloy with difference lengths (10, 20, and 30 mm. An experimental, finite element simulation, and theoretical models present to find force-deformation curves and then find SEA for difference lengths. Experimental results more agreements with finite elements simulation and theoretical when length of tubes is increase for load deformation curve, because when the length increases the plastic region increase with initial plastic collapse load (Pc. The experimental, ANSYS simulation and theoretical results have plotted and it has seen that the theory also underestimates the ANSYS results because in theoretical model, is customary to assume that the material is perfectly plastic, therefore, the finite element simulation might predict the experimental results better than the theoretical one. The results show that light density Aluminum alloy is suitable for SEA.

  9. Mn对6061合金组织和硬度的影响%The effects of Mn addition on microstructure and hardness in 6061 aluminium alloy

    Institute of Scientific and Technical Information of China (English)

    文忠; 建塬; 王彬; 曾建民

    2013-01-01

    The effects of Mn addition on the microstructure and hardness of 6061 aluminum alloy were studied by means of scanning electron microscope (SEM) , energy dispersive X-Ray analysis (EDX), X-ray diffraction (XRD) and hardness tester in this work. The results show that rod and fishbone AlSiFeMn phase will be formed in the alloy with Mn addition in 6061 aluminium alloy, by the mean of XRD, the Mn12Si7Al5 phase is found in the 6061 aluminium alloy with 0.7%Mn. The hardness increases with the increasing of Mn contents both for as-cast and for T6 heat treatment. However, the hardness growth rate for as-cast is much more than that for T6 heat treatment at the same Mn addition in the 6061 alloy. Mn has a little effect on the hardness for T6 heat treatment in 6061 alloy.%通过扫描电镜/能谱仪、X射线衍射仪以及硬度计,研究了在6061合金中添加少量的 Mn,对6061合金的微观组织和硬度的影响。研究表明:在6061合金中添加微量的Mn,合金的微观组织中出现白色的鱼骨状和条块状的AlSiFeMn结晶相。在对含Mn量为0.7%的6061合金进行XRD分析时发现有Mn12Si7Al5相的衍射峰。对比6061合金的铸态硬度和时效硬度随Mn含量的变化趋势,发现添加微量的Mn对合金的铸态硬度的提高较明显,而对合金的时效硬度的提高所起的所用较小。

  10. Microchemistry in aluminium sheet production

    NARCIS (Netherlands)

    Lok, Z.J.

    2005-01-01

    The production of aluminium sheet alloys from as-cast ingots is a complex process, involving several rolling operations in combination with various thermal heat treatments. Through their influence on the alloy microchemistry and microstructure, these thermomechanical treatments are all aimed at cont

  11. Effects of Ca addition on tensile properties and microstructures of hot-extruded AZ91 alloy tube

    Institute of Scientific and Technical Information of China (English)

    WANG Feng; LIU Zheng; YU Bao-yi; ZHANG Kui

    2006-01-01

    As-cast AZ91+XCa (X=0, 0.5%, 1.0%, 1.5%, mass fraction) magnesium alloys were extruded into tube at 380℃ with an extrusion ratio of 6:1. The tensile properties and microstructures of extruded AZ91+XCa alloy tubes were investigated. The microstructural observation indicates that Ca can obviously refine both α-Mg grains and Mg17Al12 phase of AZ91 magnesium alloy. XRD analysis shows that the microstructure of AZ91+0.5Ca alloy consists of α-Mg solid solution and Mg17Al12 phase, while AZ91+1.5Ca alloy contains additionally Al2Ca phase. The tensile experimental results show that for the AZ91 alloy, the addition of Ca has little influence on the ambient temperature tensile properties but can improve the elevated temperature tensile properties. For the extruded AZ91+XCa alloys, the elevated temperature tensile strength decreases, and elongation increases with increasing the Ca content. The improvement in elevated temperature tensile strength of the alloy can be attributed to the presence of a Ca-containing phase, which can increase the microstructural stability of the alloy at elevated temperature.

  12. In situ monitoring of corrosion mechanisms and phosphate inhibitor surface deposition during corrosion of zinc-magnesium-aluminium (ZMA) alloys using novel time-lapse microscopy.

    Science.gov (United States)

    Sullivan, James; Cooze, Nathan; Gallagher, Callum; Lewis, Tom; Prosek, Tomas; Thierry, Dominique

    2015-01-01

    In situ time-lapse optical microscopy was used to examine the microstructural corrosion mechanisms in three zinc-magnesium-aluminium (ZMA) alloy coated steels immersed in 1% NaCl pH 7. Preferential corrosion of MgZn(2) lamellae within the eutectic phases was observed in all the ZMA alloys followed by subsequent dissolution of Zn rich phases. The total extent and rate of corrosion, measured using time-lapse image analysis and scanning vibrating electrode technique (SVET) estimated mass loss, decreased as Mg and Al alloying additions were increased up to a level of 3 wt% Mg and 3.7 wt% Al. This was probably due to the increased presence of MgO and Al(2)O(3) at the alloy surface retarding the kinetics of cathodic oxygen reduction. The addition of 1 × 10(-2) mol dm(-3) Na(3)PO(4) to 1% NaCl pH 7 had a dramatic influence on the corrosion mechanism for a ZMA with passivation of anodic sites through phosphate precipitation observed using time-lapse image analysis. Intriguing rapid precipitation of filamentous phosphate was also observed and it is postulated that these filaments nucleate and grow due to super saturation effects. Polarisation experiments showed that the addition of 1 × 10(-2) mol dm(-3) Na(3)PO(4) to the 1% NaCl electrolyte promoted an anodic shift of 50 mV in open circuit potential for the ZMA alloy with a reduction in anodic current of 2.5 orders of magnitude suggesting that it was acting primarily as an anodic inhibitor supporting the inferences from the time-lapse investigations. These phosphate additions resulted in a 98% reduction in estimated mass loss as measured by SVET demonstrating the effectiveness of phosphate inhibitors for this alloy system.

  13. Corner forming of AZ61A magnesium alloy tube within warm hydroforming

    Institute of Scientific and Technical Information of China (English)

    HU Lan; HAN Cong; HE Zhu-bin; TANG Ze-jun; LIU Gang; YUAN Shi-jian

    2009-01-01

    The corners with small radii on cross sections are crucial for forming hydroformed components with polygonal sections. In this paper, warm hydroforming experiments of AZ61 A magnesium alloy tubes were carried out to study the forming regularity of round corners by using a demonstration part with square sections.Effects of temperature on radius forming, thinning ratio distribution and microstructure were revealed and a component with relative outer corner radius of 3.0 was obtained by warm hydroforming at 240℃. The minimum thickness of the formed square section was located in the transition position between the corner and the straight wall. The thinning ratio of the round corner increased with the increase of forming temperature. Formability of the magnesium tube was improved by raising temperature under the effect of dynamic recrystallization at 240℃.

  14. Rapid dendritic growth of Al-Ge hypoeutectic alloy in a drop tube

    Institute of Scientific and Technical Information of China (English)

    2003-01-01

    Dendritic growth in Al-45% Ge hypoeutectic alloy has been investigated during free fall in a 3 m drop tube. Calculations indicate that the undercooling obtained for the falling Al-45% Ge droplets ranges from 13 K to 201 K. The maximum undercooling attains 0.27TL. With the increase of undercooling, the primary (Al) phase undergoes a "columnar dendrite to equiaxed dendrite" structural transition. According to the current rapid dendritic growth theory, the growth of primary (Al) phase is always controlled by solute diffusion.

  15. Preparation, microstructure and properties of Al-Zn-Mg-Sc alloy tubes

    Institute of Scientific and Technical Information of China (English)

    何振波; 尹志民; 林森; 邓英; 商宝川; 周向

    2010-01-01

    The Al-6.0Zn-2.0Mg-0.2Sc-0.10Zr hollow tube ingots, prepared by semi-continuous casting technology, were subjected to ho- mogenization treatment, hot extrusion, intermediate annealing, tension, solution and aging treatment. The microstructures and properties of as-cast Al-Zn-Mg-Sc alloy at different homogenization treatment conditions were studied using hardness measurement, X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) analysis. The results showed th...

  16. Regularities of crystallographic texture formation in cladding tubes from Zr-based alloys during their production

    Science.gov (United States)

    Isaenkova, M.; Perlovich, Yu; Fesenko, V.

    2016-04-01

    This paper summarizes researches of the authors, which are directed on the development of the methodological basis of X-ray studies in the materials science of zirconium and on the systematization of new experimental results obtained using developed methods. The paper describes regularities of the formation of the crystallographic texture and the substructure inhomogeneity of cladding tubes from zirconium alloys at various stages of their manufacturing, i.e. during hot and cold deformation, recrystallization, phase transformations and interactions of the above processes.

  17. Minimum Safety Factor for Evaluation of Critical Buckling Pressure of Zirconium Alloy Tube

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Hyung Kyu; Kim, Jae Yong; Yoon, Kyung Ho; Lee, Young Ho; Lee, Kang Hee; Kang, Heung Seok [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2011-03-15

    We consider the uncertainty in the elastic buckling formula for a thin tube. We take into account the measurement uncertainty of Young's modulus and Poisson's ratio and the tolerance of the tube thickness and diameter. Elastic buckling must be prohibited for a thin tube such as a nuclear fuel rod that must satisfy a self-stand criterion. Since the predicted critical buckling pressure overestimated that found in the experiment, the determination of the minimum safety factor is crucial. The uncertainty in each parameter (i.e., Young's modulus, Poisson's ratio, thickness, and diameter) is mutually independent, so the safety factor is evaluated as the sum of the inverse of each uncertainty. We found that the thickness variation greatly affects the uncertainty. The minimum safety factor of a thin tube of Zirconium alloy is evaluated as 1.547 for a thickness of 0.87 mm and 3.487 for a thickness of 0.254 mm.

  18. Fracture Behavior of TiNi Based Shape Memory Alloy Cold-rolled Tube

    Institute of Scientific and Technical Information of China (English)

    LI Yan-wu; LIU Fu-shun

    2006-01-01

    The microstructures and interfacial characteristics of matrices at the inwalls and the out-walls of the cold-rolled tube with different amounts of deformation were investigated by the scanning electronic microscope (SEM), the optical microscope (OM), and the transmission electronic microscope (TEM) techniques. It was observed that as the amount of deformation increases, the flaws nucleate at the out-walls of the cold rolled tube, the stress-induced martensites change from (11) type Ⅰ twins to (011) type Ⅱ twins and then to (100) compound twins, nanocrystals and bulk amorphisation happen, the high density dislocation causes stress concentration at the out-walls of the Ti50Ni50 cold-rolled tube, and then precipitates its fracture, and the Ti2Ni particles strengthen the grain boundaries and curb the dislocation movements during plastic deformation. The inhomogeneity level of the grains in the Ti50Ni50 alloy plays an important role on the fracture of the Ti50Ni50 cold rolled tube.

  19. Rolling process and bonding mechanism of micro-arc oxidation 6061 aluminium alloy clad plate%微弧氧化6061铝合金复合板轧制工艺及结合机理

    Institute of Scientific and Technical Information of China (English)

    郑艺; 吴国瑞; 张胜超; 张学术; 杨猛

    2014-01-01

    Micro-arc oxidation 6061 aluminium alloy clad plate was prepared by rolling which confirm the rolling composite feasibility of aluminum alloy plate .Bonding strength of the plate was tested by tear method and stripped surface was analyzed by SEM and EDS .The results show that aluminum alloy plate and micro-arc oxidation 6061 aluminium alloy plate can be bonded by rolling at the condition of rolling tempreture above 400 ℃and rolling reduction above 40%.During rolling, hardened layer on the aluminium alloy plate surface and ceramic layer on the micro-arc oxidation aluminium alloy plate surface ruptures , and ceramic particles involving in the interface bonding position , thus let the fresh aluminum alloy of the two plates extrude and the metallurgical bonding is obtained .%用轧制法制备了内含微弧氧化陶瓷颗粒的6061铝合金复合板,证实了微弧氧化铝合金板轧制复合可行性。用撕裂法测试了复合板的结合强度,对复合板剥离面进行了SEM和EDS分析。结果表明,在热轧温度不低于400℃,同时压下率不低于40%的轧制条件下,铝合金板/微弧氧化铝合金板通过轧制可以实现结合。在轧制时铝合金表面硬化层、微弧氧化铝合金表面陶瓷层破裂,陶瓷颗粒卷入界面结合处,复合板两侧铝合金新鲜金属挤出实现冶金结合。

  20. Hot-press Sintering and Properties of Al-Zn-Mg-Cu-Zr Aluminium Alloy%铝锌镁铜锆系铝合金的热压烧结及其性能

    Institute of Scientific and Technical Information of China (English)

    方攀; 李成章; 吴传栋; 罗国强; 沈强; 张联盟

    2013-01-01

    Using metal powder as raw material,Al-Zn-Mg-Cu-Zr aluminium alloys were prepared by hotpress sintering technology at different sintering temperatures.The density,phase,microstructure and mechanical properties of Al-Zn-Mg-Cu-Zr aluminium alloy specimens were measured.The results show that with the increase of sintering temperature,the porosity of the aluminium alloy decreased,but density increased,and the alloy had more homogeneous microstructure and better properties.When the sintering temperature was 600 ℃,the porosity was 0.01%,the aluminium alloy was close to completely dense and had a good degree of alloying.The maximum value of the average micro-hardness and tensile strength of the A1-Zn-Mg-Cu-Zr aluminium alloy specimen hit 174 HV and 502 MPa,respectively.The aluminium alloy with a high density,uniform structure and good mechanical property can be prepared by the hot-press sintering technology.%以金属粉体为原料,采用热压烧结技术在不同温度下烧结制备了铝锌镁铜锆系铝合金,并测试和分析了其密度、物相、显微组织以及力学性能.结果表明:随着烧结温度的升高,铝合金的气孔率降低,致密度上升,组织更均匀,性能更优异;当烧结温度为600℃时,气孔率低至0.01%,接近全致密,铝合金的合金化良好,显微硬度达到174 HV,抗拉强度达到502 MPa;采用热压烧结技术可以获得高致密度、组织均匀、力学性能良好的铝合金.

  1. A prediction method for the general corrosion behavior of Alloy 690 steam generator tube using eddy current testing

    Energy Technology Data Exchange (ETDEWEB)

    Shim, Hee-Sang; Choi, Myung Sik; Lee, Deok Hyun; Hur, Do Haeng, E-mail: dhhur@kaeri.re.kr

    2016-02-15

    Highlights: • A corrosion test for the tubes with different levels of eddy current noise was conducted. • A relationship between the corrosion rate and the eddy current noise of tubes was explored. • Corrosion rate was closely correlated to the tube noise of a rotating pancake probe. • Corrosion rate was not related to the tube noise measured using a bobbin probe. - Abstract: The purpose of this work is to develop an eddy current testing method to predict the general corrosion behavior of Alloy 690 steam generator tubes. A corrosion test was conducted for tubes with different levels of eddy current noise in simulated primary water at 330 °C, and their corrosion behavior was correlated with the tube noise measured using bobbin and rotating probes. The corrosion behavior was closely correlated with the tube noise measured using a rotating probe. However, there was no correlation between the corrosion behavior and the tube noise measured using a bobbin probe. The tube noise value measured using a rotating pancake coil probe is suggested to be a significant parameter in estimating the general corrosion behavior of tubes.

  2. Magnesium tube hydroforming

    Energy Technology Data Exchange (ETDEWEB)

    Liewald, M.; Pop, R. [Institute for Metal Forming Technology (IFU), Stuttgart (Germany)

    2008-04-15

    Magnesium alloys reveal a good strength-to-weight ratio in the family of lightweight metals and gains potential to provide up to 30% mass savings compared to aluminium and up to 75 % compared to steel. The use of sheet magnesium alloys for auto body applications is however limited due to the relatively low formability at room temperature. Within the scope of this paper, extruded magnesium tubes, which are suitable for hydroforming applications, have been investigated. Results obtained at room temperature using magnesium AZ31 tubes show that circumferential strains are limited to a maximal value of 4%. In order to examine the influence of the forming temperature on tube formability, investigations have been carried out with a new die set for hot internal high pressure (IHP) forming at temperatures up to 400 C. Earlier investigations with magnesium AZ31 tubes have shown that fractures occur along the welding line at tubes extruded over a spider die, whereby a non-uniform expansion at bursting with an elongation value of 24% can be observed. A maximum circumferential strain of approx. 60% could be attained when seamless, mechanically pre-expanded and annealed tubes of the same alloy have been used. The effect of annealing time on materials forming properties shows a fine grained structure for sufficient annealing times as well as deterioration with a large increase at same time. Hence, seamless ZM21 tubes have been used in the current investigations. With these tubes, an increased tensile fracture strain of 116% at 350 C is observed as against 19% at 20 C, obtained by tensile testing of milled specimens from the extruded tubes. This behaviour is also seen under the condition of tool contact during the IHP forming process. To determine the maximum circumferential strain at different forming temperatures and strain rates, the tubes are initially bulged in a die with square cross-section under plane stress conditions. Thereafter, the tubes are calibrated by using an

  3. Crack growth of throughwall flaw in Alloy 600 tube during leak testing

    Energy Technology Data Exchange (ETDEWEB)

    Bahn, Chi Bum, E-mail: bahn@pusan.ac.kr [Pusan National University, 2 Busandaehak-ro 63beon-gil, Geumjeong-gu, Busan 609-735 (Korea, Republic of); Majumdar, Saurin [Argonne National Laboratory, Lemont, IL 60439 (United States)

    2015-04-01

    Graphical abstract: - Highlights: • A series of leak testing was conducted at a constant pressure and room temperature. • The time-dependent increase in the leak rate was observed. • The fractography revealed slip offsets and crystallographic facets. • Time-dependent plasticity at the crack tip caused the slip offsets. • Fatigue by jet/structure interaction caused the crystallographic facets. - Abstract: We examined the issue of whether crack growth in a full thickness material can occur in a leaking crack. A series of leak tests was conducted at a room temperature and constant pressure (17.3 MPa) with Alloy 600 tube specimens containing a tight rectangular throughwall axial fatigue crack. To exclude a potential pulsation effect by a high pressure pump, the test water was pressurized by using high pressure nitrogen gas. Fractography showed that crack growth in the full thickness material can occur in the leaking crack by two mechanisms: time-dependent plasticity at the crack tip and fatigue induced by jet/structure interaction. The threshold leak rate at which the jet/structure interaction was triggered was between 1.3 and 3.3 L/min for the specific heat of the Alloy 600 tube tested.

  4. Fiber laser micromachining of magnesium alloy tubes for biocompatible and biodegradable cardiovascular stents

    Science.gov (United States)

    Demir, Ali Gökhan; Previtali, Barbara; Colombo, Daniele; Ge, Qiang; Vedani, Maurizio; Petrini, Lorenza; Wu, Wei; Biffi, Carlo Alberto

    2012-02-01

    Magnesium alloys constitute an attractive solution for cardiovascular stent applications due to their intrinsic properties of biocompatibility and relatively low corrosion resistance in human-body fluids, which results in as a less intrusive treatment. Laser micromachining is the conventional process used to cut the stent mesh, which plays the key role for the accurate reproduction of the mesh design and the surface quality of the produced stent that are important factors in ensuring the mechanical and corrosion resistance properties of such a kind of devices. Traditionally continuous or pulsed laser systems working in microsecond pulse regime are employed for stent manufacturing. Pulsed fiber lasers on the other hand, are a relatively new solution which could balance productivity and quality aspects with shorter ns pulse durations and pulse energies in the order of mJ. This work reports the study of laser micromachining and of AZ31 magnesium alloy for the manufacturing of cardiovascular stents with a novel mesh design. A pulsed active fiber laser system operating in nanosecond pulse regime was employed for the micromachining. Laser parameters were studied for tubular cutting on a common stent material, AISI 316L tubes with 2 mm in diameter and 0.2 mm in thickness and on AZ31 tubes with 2.5 mm in diameter and 0.2 in thickness. In both cases process parameters conditions were examined for reactive and inert gas cutting solutions and the final stent quality is compared.

  5. Some preliminary evaluations of black coating on aluminium AA2219 alloy produced by plasma electrolytic oxidation (PEO) process for space applications

    Science.gov (United States)

    Shrestha, S.; Merstallinger, A.; Sickert, D.; Dunn, B. D.

    2003-09-01

    This paper describes the results of a study of a black coating produced on aluminium AA2219 alloy using a process that involves creation of a hard ceramic oxide layer on the surface of the alloy by plasma electrolytic oxidation (PEO) known as the 'KERONITE®' process. Coating microstructure has been examined and the coating characteristics such as porosity, hardness, adhesion and phase composition were measured. The thermo-optical properties such as solar absorptance 'as' and normal infrared emittance 'en-IR' of the coating were measured in the 'as-prepared' condition and after environmental exposures to humidity, thermal cycling and UV-radiation in vacuum and to thermal shock. Comparison was made with alternative coatings produced using standard black anodising processes. The study also looked at the cold welding and friction behaviours of the coated alloy in vacuum and in an ambient laboratory environment. Standard spacecraft materials tests were conducted on the coated disc against an AISI 52100 steel ball and also against a coated pin using a pin-on-disc apparatus. Parameters such as friction coefficient and wear depth were measured and the cold welding behaviours were investigated. Test results were compared with the data generated for NiCr plated and anodised coatings. Corrosion performance was assessed using a salt spray exposure test and using an accelerated electrochemical test method. In addition, the study looked at the effect of post coating sealing with a sol-gel solution.

  6. Effect of Al–5Ti–1B grain refiner on the microstructure, mechanical properties and acoustic emission characteristics of Al5052 aluminium alloy

    Directory of Open Access Journals (Sweden)

    Amulya Bihari Pattnaik

    2015-04-01

    Full Text Available In the present investigation, the effect of Al–5Ti–1B grain refiner on the microstructure, mechanical properties and acoustic emission characteristics of Al 5052 aluminium alloy have been studied. Microstructural analysis showed the presence of primary α solid solution. No Al–Mg phase was found to be formed due to the presence of magnesium in the solid solution. The results indicated that the addition of Al–5Ti–1B grain refiner into the alloy caused a significant improvement in ultimate tensile strength (UTS and elongation values from 114 MPa and 7.8% to 185 MPa and 18% respectively. The main mechanisms behind this improvement were found to be due to the grain refinement during solidification and segregation of Ti at primary α grain boundaries. Acoustic emission (AE results indicated that intensity of AE signals increased with increase in Al–5Ti–1B master alloy content, which had been attributed to the combined effect of dislocation motion and grain refinement. The field emission scanning electron microscopy (FESEM and energy dispersive X-ray (EDX analysis were used to study the microstructure and fracture surfaces of the samples.

  7. Finite element modelling of shot peening and peen forming processes and characterisation of peened AA2024-T351 aluminium alloy

    Science.gov (United States)

    Gariepy, Alexandre

    The main purpose of this thesis was to develop and validate finite element (FE) simulation tools for shot peening and peen forming. The specific aim was to achieve quantitatively accurate predictions for both processes and demonstrate the potential of reliable FE modelling for scientific investigation and industrial applications. First, an improved dynamic impact model that takes into account the stochastic nature of shot peening was proposed by carefully studying its dimensions, introducing a dispersion of shot sizes and significantly reducing its computational cost. In addition, cyclic mechanical testing was conducted to define a suitable material constitutive theory for aluminium alloy (AA) 2024-T3/T351 subjected to shot peening. By combining a realistic shot peening model with an appropriate material law, fairly good residual stress predictions were achieved for three different sets of shot peening parameters. Second, an experimental and numerical characterization of AA2024-T351 shot peened with parameters representative of fatigue life improvement applications was conducted. Multiple techniques, such as micro-indentation, residual stress determination and electron backscatter diffraction, were combined to gain a better understanding of the influence of shot peening on the material. The potential uses of finite element simulation to complement experimental data were also studied. The material heterogeneity arising from the random impact sequence was investigated and it was found that the impact modelling methodology could provide useful information on such heterogeneities. Third, a novel peen forming simulation methodology was introduced. The impact model provided the necessary input data as part of a multiscale approach. Numerically calculated unbalanced induced stress profiles were input into shell elements and the deformed shape after peen forming was computed as a springback analysis. In addition, a simple interpolation method was proposed to model the

  8. 6061铝合金的电火花加工%Electrical discharge machining of 6061 aluminium alloy

    Institute of Scientific and Technical Information of China (English)

    A. PRAMANIK; A. K. BASAK; M. N. ISLAM; G. LITTLEFAIR

    2015-01-01

    在不同脉冲时间和导线张力下,研究6061铝合金电火花线切割加工过程中材料的去除率、切口/狭缝宽度、表面光洁度和线电极磨损,通过改变脉冲时间和导线张力,在电火花线切割加工机床上进行了8次实验.结果表明,随着脉冲时间的延长,材料的去除率增加,但导线张力不影响材料的去除率.较高的导线张力有利于促进加工工艺的稳定性,产生较低的线电极磨损和更好的表面光洁度.随着脉冲时间的变化,表面粗糙度没有明显变化.在所有加工条件下,表面外观非常相似.加工后表面包含凝固熔融材料、飞溅材料和气泡.由于热量输入的增加,脉冲时间的延长增大了线电极的磨损.线电极的磨损产生了斜槽,该斜槽正面的切口宽度比底部的宽.较高的电极损耗会产生较高的锥度.%The wire electrical discharge machining (EDM) of 6061 aluminium alloy in terms of material removal rate, kerf/slit width, surface finish and wear of electrode wire for different pulse on time and wire tension was studied. Eight experiments were carried out in a wire EDM machine by varying pulse on time and wire tension. It is found that the material removal rate increases with the increase of pulse on time though the wire tension does not affect the material removal rate. It seems that the higher wire tension facilitates steady machining process, which generates low wear in wire electrode and better surface finish. The surface roughness does not change notably with the variation of pulse on time. The appearance of the machined surfaces is very similar under all the machining conditions. The machined surface contains solidified molten material, splash of materials and blisters. The increase of the pulse on time increases the wear of wire electrode due to the increase of heat input. The wear of wire electrode generates tapered slot which has higher kerf width at top side than that at bottom side. The higher

  9. Observation of Built-up Edge Formation on a Carbide Cutting Tool with Machining Aluminium Alloy under Dry and Wet Conditions

    Directory of Open Access Journals (Sweden)

    Azlan U.A.A.

    2017-01-01

    Full Text Available This paper presents the morphology of built-up edge (BUE formation under wet and dry conditions with low and high cutting speeds. The workpiece materials and cutting tools selected for this work were aluminium alloy and canela carbide inserts graded PM25. The cutting tools underwent turning operation machining tests and their performance was evaluated by the flank wear and observation of the tool wear area. The machining tests were conducted at different spindle speeds and feed rates while the cut depth was kept constant. The analysis showed that formation of the BUE was dominant at low cutting speeds in dry conditions, but in wet conditions at high cutting speeds, a better performance was exhibited in terms of wear analysis.

  10. EDTA容量法测定锌合金中的铝量%Determination of Aluminium in Zinc Alloy by EDTA Titrimelry

    Institute of Scientific and Technical Information of China (English)

    涂小红

    2009-01-01

    the abundant sample and nitric acid sample dissolving were adopted in the paper,then excess EDTA was added and titrated by zinc acetate acid in pH≈5.8, Aluminum EDTA complex was released after adding of ammonium fluoride.,then released EDTA was titrated by zinc acetic acid. The method was simple,rapid and accurate,it can be used to determine the aluminium in zinc alloy.%本文采用称大样和用硝酸溶样,然后加入过量的EDTA,在PH≈5.8时用乙酸锌滴定过量的EDTA,加入氟化铵,释放出与铝络合的EDTA,再用乙酸锌滴定被释放出的EDTA.该方法简单、快速、准确,适用于锌合金中铝量的测定.

  11. Fireside corrosion testing of candidate superheater tube alloys, coatings, and claddings - Phase II

    Energy Technology Data Exchange (ETDEWEB)

    Blough, J.L.; Krawchuk, M.T.; Van Weele, S.F. [Foster Wheeler Development Corp., Livingston, NJ (United States)

    1995-08-01

    A number of developmental and commercial tubing alloys and claddings have previously been exposed in Phase I to laboratory fireside corrosion testing simulating a superheater or reheater in a coal-fired boiler. This program is exposing samples of TP 347, RA-85H, HR-3C, 253MA, Fe{sub 3}Al + 5Cr, 310 modified, NF-709, 690 clad, and 671 clad, which showed good corrosion resistance from Phase 1, to the actual operating conditions of a 250-MW, coal-fired boiler. The samples were installed on air-cooled, retractable corrosion probes, installed in the reheater cavity, and are being controlled to the operating metal temperatures of an existing and advanced-cycle coal-fired boiler. The exposure will continue for 4000, 12,000, and 16,000 hours of operation. After the three exposure times, the samples will be metallurgically examined to determine the wastage rates and mode of attack. The probes were commissioned November 16, 1994. The temperatures are being recorded every 15 minutes, and the weighted average temperature calculated for each sample. Each of the alloys is being exposed to a temperature in each of two temperature bands-1150 to 1260{degrees}F and 1260 to 1325{degrees}F. After 2000 hours of exposure, one of the corrosion probes was cleaned and the wall thicknesses were ultrasonically measured. The alloy performance from the field probes will be discussed.

  12. SeZnSb alloy and its nano tubes, graphene composites properties

    Directory of Open Access Journals (Sweden)

    Abhay Kumar Singh

    2013-04-01

    Full Text Available Composite can alter the individual element physical property, could be useful to define the specific use of the material. Therefore, work demonstrates the synthesis of a new composition Se96-Zn2-Sb2 and its composites with 0.05% multi-walled carbon nano tubes and 0.05% bilayer graphene, in the glassy form. The diffused amorphous structure of the multi walled carbon nano tubes and bilayer gaphene in the Se96-Zn2-Sb2 alloy have been analyzed by using the Raman, X-ray photoluminescence spectroscopy, Furrier transmission infrared spectra, photoluminescence, UV/visible absorption spectroscopic measurements. The diffused prime Raman bands (G and D have been appeared for the multi walled carbon nano tubes and graphene composites, while the X-ray photoluminescence core energy levels peak shifts have been observed for the composite materials. Subsequently the photoluminescence property at room temperature and a drastic enhancement (upto 80% in infrared transmission percentage has been obtained for the bilayer graphene composite, along with optical energy band gaps for these materials have been evaluated 1.37, 1.39 and 1.41 eV.

  13. Simulation calculations for the positron annihilation in aluminium alloys for the study of the segregate formation; Simulationsrechnungen zur Positronenannihilation in Aluminiumlegierungen zur Untersuchung der Ausscheidungsbildung

    Energy Technology Data Exchange (ETDEWEB)

    Korff, Bjoern

    2010-11-29

    Highly solid aluminium alloys owe their properties to small, finely distributed segregations of alloy atoms. For the better understanding of the temperature treatment, which is required in order to control the segregate formation, it is important, to determine informations on the first early stages from few atoms. In the positron-annihilation spectroscopy (PAS) positrons are trapped in the vacancies of a solid and yield at their annihilation with surrounding electrons informations from their direct environment. because the formation of segregates requires a diffusion of the extraneous atoms by means of the vacancies, the PAS represents one of the few examination methods, by which already the formation of smallest segregations can be observed. By the comparison of measurement quantities of the PAS with simulations for different possible arrangements of extraneous atoms around the vacancy the atomic environment of the vacancy can be identified. In order to make this possible also in aluminium alloys, in which the number of the possible defect types is relatively large, a good description of the measurement values by the simulation is especially important. In the framework of this thesis the program AB2D was developed, by which the Doppler shift of the annihilation radiation can be determined. Contrarily to already existing approaches here valence-electron wave functions are used, which were calculated with the program ABINIT. By this way the main uncertainty by the description of the valence electrons in atomic superposition is cancelled. Because ABINIT is based on pseudopotentials, the projector augmented-wave method is used in order to describe the higher momenta of the electrons near the nuclei more realistically. With AB2D simulations for vacancy-extraneous-atom complexes and segregation phases in the alloy systems Al-Cu, Al-Mg-Cu, and Al-Mg-Si were performed. A comparison with measurements on samples, which were only few minutes stored at room temperature

  14. Influence of aluminium content on the physical, mechanical and sliding wear properties of zinc-based alloys

    Energy Technology Data Exchange (ETDEWEB)

    Prasad, B.K. [CSIR, Bhopal (India). Regional Res. Lab.; Patwardhan, A.K. [Roorkee Univ. (India). Dept. of Metallurgical Engineering; Yegneswaran, A.H. [CSIR, Bhopal (India). Regional Res. Lab.

    1997-04-01

    Attention has been focussed on the influence of Al content on the physical, mechanical and sliding wear properties of Zn-based alloys. Aspects studied include microstructure, density, electrical conductivity, hardness, tensile strength and elongation as well as sliding wear response of the alloys. Microstructural features of the alloys showed the presence of primary {alpha}, eutectic/eutectoid {alpha} + {eta} (depending on whether the alloy was hypereutectic/hypereutectoid with regard to the concentration of Al) along with the meta stable {epsilon} phase. The study suggests that it is possible to design and develop Zn-based alloys with a wide range of concentration of Al. The alloys in turn attain different combinations of physical, mechanical and wear properties which could suit a variety of engineering applications. Increasing the Al content in the alloy system proves beneficial within limits. In other words, there exists an optimum quantity of Al which could reap its advantage to the maximum extent. This of course varies with reference to a specific property of the alloy(s). The changing response of the alloys has been explained in terms of their microstructural features and the effects produced as a result of the test conditions maintained while characterizing the specimens. (orig.)

  15. Investigation of microgravity effect on solidification of medium-low-melting-point alloy by drop tube experiment

    Institute of Scientific and Technical Information of China (English)

    2008-01-01

    The solidification microstructure of Al-Ni, Al-Cu, Ag-Cu, Al-Pb and Cu-Co alloys quenched in silicone oil before and after free fall in evacuated 50 m drop tube were investigated contrastively. The effect of microgravity on the solidification process of medium-low-melting-point eutectic, monotectic and peritectic alloys were ana-lyzed and discussed. The results indicated that the effects of microgravity on the eutectic cell shape, the pattern in eutectic cell and the inter-eutectic spacing were different for different types of eutectic systems; the size distribution of Pb particles in Al-5wt% Pb monotectic alloy was significantly changed by microgravity; and the shape of retained primary α-Co phase in Cu-10wt%Co peritectic alloy was also changed by microgravity. These results are beneficial for people to further identify and analyze the solidification behavior of multiphase alloys under microgravity.

  16. The Progress and Prospect of Research on Aluminium Alloys for Auto Body Sheets%汽车铝合金车身板材的研究现状及发展趋势

    Institute of Scientific and Technical Information of China (English)

    关绍康; 姚波; 王迎新

    2001-01-01

    In recent years, with the development of society and advancement of technology, aluminium and aluminium alloys are used more and more widely. It becomes a trend that traditional steel sheets are replaced by aluminium sheets for auto body. The research progress, application status and development prospect of aluminium alloys for auto body sheets are summarized in this paper. Among the 2000, 5000 and 6000 series aluminium alloys now studied, the new style 6000 series Al-Mg-Si based alloy is specially introduced as a emphasis in future research.There are many advantages about it: proper strength and plasticity, good corrosion-resistance performance, easycoloring and effect of painting strengthening. Besides, some problems such as high cost and poor formation performance, which hold up the application of aluminium alloys for auto body sheets, are listed. At last, several advices are presented to develop characteristic alurninium alloys of high properties for auto body sheets in China. For instance, the stamping property should be improved by designing the compostition and technology and the relationship of stamping property, mechanical properties, composition and technology should be made clear, the material composition and technology can be designed by using computer techniques such as artificial neural network and genetic algo rithrn.%综述了国内外汽车铝合金2000、5000和6000系车身板的研究进程、应用现状及发展前景,指出了新型Al-Mg-Si基合金是今后汽车车身板研究应用的一个重点,它具有强度和塑性的良好组合,耐蚀性优良,易着色等优点;此外,还列出了汽车铝合金车身板研究应用中存在的成本高和成型性差等问题,提出了我国开发高性能且具有特色的汽车铝合金车身板材的研究方向。

  17. 化学镀Ni-P合金在铝合金表面强化上的应用%Application of Electroless Plating Ni-P Alloy on Aluminium Alloy

    Institute of Scientific and Technical Information of China (English)

    朱晓云; 郭忠诚; 翟大成

    2001-01-01

    研究了化学镀镍-磷合金的性能,结果表明,热处理温度对镍-磷合金镀层硬度和耐磨性有较大的影响,二者经400℃×1 h热处理后达到峰值;镍-磷合金在酸、碱、盐介质中的耐蚀性优于1Cr18Ni9Ti不锈钢。应用结果证明,化学镀Ni-P合金在铝合金零部件上具有广泛的应用前景。%Properties of electroless plating Ni-Palloy have been studied, the results show that heattreatment temperature has a considerable effect onthe hardness and wear resistance of Ni-P alloy, andthey reach peak value after heat treatment at 400 ℃X 1h. Corrosion resistance of Ni-P alloy in acid,alkaline and salt media is superior to that of1Cr18Ni9Ti stainless steel. The electroless platingNi-P alloy has a wide application for the componentof aluminium alloy.

  18. Influence of the composition and heat treatments in the mechanical properties of aluminium bronze alloys; Influencia de la composicion y el tratamiento termico en las propiedades mecanicas de aleaciones de bronce al aluminio

    Energy Technology Data Exchange (ETDEWEB)

    Cenoz-Echeverria, I.; Fernandez-Carrasquilla, J.

    2007-07-01

    Aluminium bronzes are copper-base alloys containing aluminium within the limits between 5-12%. Additions of Fe, Ni and Mn are used as alloying elements forming a family of complex alloys noted for their exceptional strength and corrosion resistance. In present paper sd the Ni:Fe ratio and heat treatments have been analyzed by determining the mechanical properties for three different aluminium bronze alloys containing Cu-Al10-Fe3, Cu-Al10-Fe5-Ni5 and Cu-Al10-Fe4-Ni8. The effect of as cast, quenched and quenched and tempered structures has been investigated regarding hardness, proof and ultimate tensile strength, elongation, modules of elasticity, Poisson ratio, fracture toughness, fatigue strength, crack propagation and Charpy impact properties. The influence of temperature has been studied by testing the elastic modules, Poisson ratio, the proof stress, tensile strength and the Charpy impact properties at -20 degree centigree, 24 degree centigree and 100 degree centigree. (Author)

  19. The role of solidification rate in the corrosion resistance of a directionally solidified novel aluminium-lanthanum alloy

    Energy Technology Data Exchange (ETDEWEB)

    Dzib-Perez, L. [Programa de Corrosion del Golfo de Mexico, Universidad Autonoma de Campeche, Av. Agustin Melgar s/n, Col. Buenavista, CP 24030 Campeche, Campeche (Mexico); Gonzalez-Sanchez, J. [Programa de Corrosion del Golfo de Mexico, Universidad Autonoma de Campeche, Av. Agustin Melgar s/n, Col. Buenavista, CP 24030 Campeche, Campeche (Mexico)]. E-mail: jagonzal@uacam.mx; Perez, T. [Programa de Corrosion del Golfo de Mexico, Universidad Autonoma de Campeche, Av. Agustin Melgar s/n, Col. Buenavista, CP 24030 Campeche, Campeche (Mexico); Bartolo-Perez, P. [Programa de Corrosion del Golfo de Mexico, Universidad Autonoma de Campeche, Av. Agustin Melgar s/n, Col. Buenavista, CP 24030 Campeche, Campeche (Mexico); CINVESTAV-Merida, Applied Physics Department, Carr. antigua a Progreso, km 6, CP 97310 Merida, Yucatan (Mexico); Juarez, A. [CIATEQ. Calzada del Retablo 150, CP 76150 Queretaro, Queretaro (Mexico)

    2006-08-15

    The corrosion resistance of a novel Al-12.6 wt.%La alloy manufactured using unidirectional solidification was studied by sensitive electrochemical techniques. It was found that the electrochemical behaviour of the alloy depends upon the formation of non-passive corrosion product layers. Different solidification rates produced dissimilar microstructures which promoted selective dissolution when the alloy was anodically polarized in distilled water. A model for the electrochemical behaviour of this alloy was proposed based on an equivalent circuit that simulated the impedance results.

  20. A Study On Critical Thinning In Thin-walled Tube Bending Of Al-Alloy 5052O Via Coupled Ductile Fracture Criteria

    Science.gov (United States)

    Li, Heng; Yang, He; Zhan, Mei

    2010-06-01

    Thin-walled tube bending(TWTB) method of Al-alloy tube has attracted wide applications in aerospace, aviation and automobile,etc. While, under in-plane double tensile stress states at the extrados of bending tube, the over-thinning induced ductile fracture is one dominant defect in Al-alloy tube bending. The main objective of this study is to predict the critical wall-thinning of Al-alloy tube bending by coupling two ductile fracture criteria(DFCs) into FE simulation. The DFCs include Continuum Damage Mechanics(CDM)-based model and GTN porous model. Through the uniaxial tensile test of the curved specimen, the basic material properties of the Al-alloy 5052O tube is obtained; via the inverse problem solution, the damage parameters of both the two fracture criteria are interatively determined. Thus the application study of the above DFCs in the TWTB is performed, and the more reasonable one is selected to obtain the critical thinning of Al-alloy tube in bending. The virtual damage initiation and evolution (when and where the ductile fracture occurs) in TWTB are investigated, and the fracture mechanisms of the voided Al-alloy tube in tube bending are consequently discussed.

  1. Review on Plating Technology of Aluminium and Aluminium Alloy%铝及铝合金电镀研究进展

    Institute of Scientific and Technical Information of China (English)

    蔡婷婷; 王兆文

    2013-01-01

    铝及铝合金电镀层具有优良的防腐性能及装饰性能,广泛应用金属防护和表面装饰等领域。本文针对铝和铝合金电镀研究及发展状况,在电镀基体、电镀层成分、电镀体系、电镀添加剂等几个方面进行文献综述,其中主要对熔盐电镀金属铝及合金的发展作重点论述,并对近年来发展的一些新的电镀技术进行了介绍。本文在文献综述的基础上,结合我们在熔盐电镀领域的研究经验,对熔盐电镀铝的方法及研究成果进行分析总结,旨在推动铝与铝合金电镀技术的发展。%The aluminum and its alloy are widely used in the field of metal surface protection and surface decoration for their excellent corrosion resistance ability and fine appearance . The current research and development are reviewed in this paper , meanwhile the related literature are summarized into the following parts:the electrodeposition substrate , the content of electrodeposites , the reaction systems and the addictives . New techniques introduced into this area are mentioned and the molten salt system was emphasized especially . With the notion and experience aquired from years of study on molten salts , we proposed the analysis on the research techniques and achievements , in aim to impulse the progress in the aluminum electrodeposition area .

  2. Rapidly solidified aluminium for optical applications

    NARCIS (Netherlands)

    Gubbels, G.P.H.; Venrooy, B.W.H. van; Bosch, A.J.; Senden, R.

    2008-01-01

    This paper present the results of a diamond turning study of a rapidly solidified aluminium 6061 alloy grade, known as RSA6061. It is shown that this small grain material can be diamond turned to smaller roughness values than standard AA6061 aluminium grades. Also, the results are nearly as good as

  3. High undercooling and rapid dendritic growth of Cu-Sb alloy in drop tube

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    Droplets of Cu-20%Sb hypoeutectic alloy has been rapidly solidified in drop tube within the containerless condition. With the decrease of droplet diameter, undercooling increases and the microstructures of primary copper dendrite refines. Undercooling up to 207 K (0.17 TL) is obtained in experiment. Theoretic analysis indicated that, because of the broad temperature range of solidification, the rapid growth of primary copper dendrite is controlled by the solutal diffusion. Judging from the calculation of T0 curve in the phase diagram, it is shown that the critical undercooling of segregationless solidification is (T0 = 474 K. At the maximum undercooling of 207 K, the growth velocity of primary copper phase exceeds to 37 mm/s, and the distinct solute trapping occurs.

  4. Effect of Tool Geometry and Welding Speed on Mechanical Properties and Microstructure of Friction Stir Welded Joints of Aluminium Alloys AA6082-T6

    Directory of Open Access Journals (Sweden)

    Patil Hiralal Subhash

    2014-12-01

    Full Text Available Friction stir welding is a solid state innovative joining technique, widely being used for joining aluminium alloys in aerospace, marine automotive and many other applications of commercial importance. The welding parameters and tool pin profile play a major role in deciding the weld quality. In this paper, an attempt has been made to understand the influences of welding speed and pin profile of the tool on friction stir welded joints of AA6082-T6 alloy. Three different tool pin profiles (tapered cylindrical four flutes, triangular and hexagonal have been used to fabricate the joints at different welding speeds in the range of 30 to 74 mm/min. Microhardness (HV and tensile tests performed at room temperature were used to evaluate the mechanical properties of the joints. In order to analyse the microstructural evolution of the material, the weld’s cross-sections were observed optically and SEM observations were made of the fracture surfaces. From this investigation it is found that the hexagonal tool pin profile produces mechanically sound and metallurgically defect free welds compared to other tool pin profiles.

  5. An improved billet on billet extrusion process of continuous aluminium alloy shapes for cryogenic applications in the Compact Muon Solenoid experiment

    CERN Document Server

    Tavares, S S

    2003-01-01

    The Compact Muon Solenoid (CMS) is one of the experiments being designed in the framework of the Large Hadron Collider accelerator at CERN. CMS will contain the largest and the most powerful superconducting solenoid magnet ever built in terms of stored energy. It will work at 4.2 K, will have a magnetic length of 12.5 m, with a free bore of 6m and will be manufactured as a layered and modular structure of NbTi cables embedded in a high purity (99.998%) Al- stabiliser. Each layer consists of a wound continuous length of 2.55 km. In order to withstand the high electromagnetic forces, two external aluminium alloy reinforcing sections are foreseen. These reinforcements, of 24 mm multiplied by 18 mm cross-section, will be continuously electron beam (EB) welded to the pure Al-stabiliser. The alloy EN AW-6082 has been selected for the reinforcements due to its excellent extrudability, high strength in the precipitation hardened state, high toughness and strength at cryogenic temperatures and ready EB weldability. Ea...

  6. Inhibition Behaviour of 2-butine1, 4diol and Tartrate Salt, and Their Synergistic Effects on Corrosion of AA3003 Aluminium Alloy in 0.5% NaCl Solution

    Institute of Scientific and Technical Information of China (English)

    Taghi Shahrabi; Alireza Yazdzad; Mirghasem Hosseini

    2008-01-01

    This work intends to investigate the inhibition behaviour of 2-butine 1, 4diol and potassium sodium tartrate and their synergistic effects on 3003 aluminium alloy corrosion in 0.5% NaCl solution. Experiments were carried out by electrochemical impedance spectroscopy (EIS) and Tafel polarization method in a three-electrode cell. It was concluded that the inhibition efficiencies increased with an increase in the concentrations of inhibitors. For 2-butinel, 4diol and tartrate salt, the optimum in the inhibition efficiency, at room temperature and neutral pH, was observed for concentrations close to 10-3 mol/L and 1.5×10-3mol/L, respectively. The electrochemical results illustrated that 2-butine1, 4diol and tartrate salt, have significant synergistic inhibition effects on corrosion of 3003 aluminium alloy in 0.5% NaCl solution. The optimum ratio of concentrations for tartrate to alcohol was 2:1.

  7. Composite Nickel Coatings Produced on 6XXX Series Aluminium Alloys with the Addition of Vanadium / Kompozytowe Powłoki Niklowe Wytwarzane Na Stopach Aluminum Serii 6XXX Z Dodatkiem Wanadu

    Directory of Open Access Journals (Sweden)

    Nowak M.

    2015-12-01

    Full Text Available Studies of composite nickel coatings electrolytically deposited on aluminium alloys with different content of vanadium were described. Composite coatings were deposited from a Watts bath containing fine-dispersed SiC powder particles in an amount of 20 g/l and organic matters such as saccharin and sodium laurate. The morphology, structure and thickness of the obtained composite coatings were presented. The corrosion resistance of produced coatings was examined by electrochemical method. Basing on the results of studies it was found that coatings obtained with the sole addition of saccharin were characterized by numerous surface defects. The addition of sodium laurate eliminated the occurrence of defects caused by hydrogen evolution and the resulting coatings were continuous with good adhesion to the substrate. The distribution of the ceramic SiC phase in coatings was fairly uniform for all the examined variants of aluminium alloys. SEM examinations did not reveal the phenomenon of the ceramic particles agglomeration.

  8. Study of the uniform corrosion of an aluminium alloy used for the fuel cladding of the Jules Horowitz experimental reactor; Etude de la corrosion uniforme d'un alliage d'aluminium utilise comme gainage du combustible nucleaire du reacteur experimental Jules Horowitz

    Energy Technology Data Exchange (ETDEWEB)

    Wintergerst, M. [CEA Saclay, Dept. des Materiaux pour le Nucleaire (DEN/DANS/DMN/SEMI), 91 - Gif-sur-Yvette (France)

    2008-07-01

    For the Jules Horowitz new material testing reactor, an aluminium base alloy, AlFeNi, will be used for the cladding of the fuel plates. Taking into account the thermal properties of the alloy and of its oxide, the corrosion of the fuel cans presents many problems. The aim of this thesis is to provide a growing kinetic of the oxide layer at the surface of the AlFeNi fuel can in order to predict the life time of fuel element. Thus the mechanism of degradation of the cladding will be describe in order to integrate the different parameters of the operating reactor. (A.L.B.)

  9. Fireside corrosion testing of candidate superheater tube alloys, coatings, and claddings -- Phase 2 field testing

    Energy Technology Data Exchange (ETDEWEB)

    Blough, J.L.; Seitz, W.W.; Girshik, A. [Foster Wheeler Development Corp., Livingston, NJ (United States)

    1998-06-01

    In Phase 1 of this project, laboratory experiments were performed on a variety of developmental and commercial tubing alloys and claddings by exposing them to fireside corrosion tests which simulated a superheater or reheater in a coal-fired boiler. Phase 2 (in situ testing) has exposed samples of 347, RA85H, HR3C, RA253MA, Fe{sub 3}Al + 5Cr, Ta-modified 310, NF 709, 690 clad, 671 clad, and 800HT for up to approximately 16,000 hours to the actual operating conditions of a 250-MW, coal-fired boiler. The samples were installed on air-cooled, retractable corrosion probes, installed in the reheater cavity, and controlled to the operating metal temperatures of an existing and advanced-cycle, coal-fired boiler. Samples of each alloy were exposed for 4,483, 11,348, and 15,883 hours of operation. The present results are for the metallurgical examination of the corrosion probe samples after the full 15,883 hours of exposure. A previous topical report has been issued for the 4,483 hours of exposure.

  10. Aluminium bridges, aluminium bridge decks

    NARCIS (Netherlands)

    Soetens, F.; Straalen, IJ.J. van

    2003-01-01

    Applications of aluminium have grown considerably in building and civil engineering the last decade. In building and civil engineering the increase of aluminium applications is due to various aspects like light weight, durability and maintenance, use of extrusions, and esthetics. The paper starts wi

  11. A pulsed eddy current probe for inspection of support plates from within Alloy-800 steam generator tubes

    Energy Technology Data Exchange (ETDEWEB)

    Krause, T. W.; Babbar, V. K.; Underhill, P. R. [Department of Physics, Royal Military College of Canada, Kingston, ON (Canada)

    2014-02-18

    Support plate degradation and fouling in nuclear steam generators (SGs) can lead to SG tube corrosion and loss of efficiency. Inspection and monitoring of these conditions can be integrated with preventive maintenance programs, thereby advancing station-life management processes. A prototype pulsed eddy current (PEC) probe, targeting inspection issues associated with SG tubes in SS410 tube support plate structures, has been developed using commercial finite element (FE) software. FE modeling was used to identify appropriate driver and pickup coil configurations for optimum sensitivity to changes in gap and offset for Alloy-800 SG tubes passing through 25 mm thick SS410 support plates. Experimental measurements using a probe that was manufactured based on the modeled configuration, were used to confirm the sensitivity of differential PEC signals to changes in relative position of the tube within the tube support plate holes. Models investigated the effect of shift and tilt of tube with respect to hole centers. Near hole centers and for small shifts, modeled signal amplitudes from the differentially connected coil pairs were observed to change linearly with tube shift. This was in agreement with experimentally measured TEC coil response. The work paves the way for development of a system targeting the inspection and evaluation of support plate structures in steam generators.

  12. A pulsed eddy current probe for inspection of support plates from within Alloy-800 steam generator tubes

    Science.gov (United States)

    Krause, T. W.; Babbar, V. K.; Underhill, P. R.

    2014-02-01

    Support plate degradation and fouling in nuclear steam generators (SGs) can lead to SG tube corrosion and loss of efficiency. Inspection and monitoring of these conditions can be integrated with preventive maintenance programs, thereby advancing station-life management processes. A prototype pulsed eddy current (PEC) probe, targeting inspection issues associated with SG tubes in SS410 tube support plate structures, has been developed using commercial finite element (FE) software. FE modeling was used to identify appropriate driver and pickup coil configurations for optimum sensitivity to changes in gap and offset for Alloy-800 SG tubes passing through 25 mm thick SS410 support plates. Experimental measurements using a probe that was manufactured based on the modeled configuration, were used to confirm the sensitivity of differential PEC signals to changes in relative position of the tube within the tube support plate holes. Models investigated the effect of shift and tilt of tube with respect to hole centers. Near hole centers and for small shifts, modeled signal amplitudes from the differentially connected coil pairs were observed to change linearly with tube shift. This was in agreement with experimentally measured TEC coil response. The work paves the way for development of a system targeting the inspection and evaluation of support plate structures in steam generators.

  13. A quantitative evaluation of the deformation texture predictions for aluminium alloys from crystal plasticity finite element method

    Science.gov (United States)

    Li, Saiyi; Van Houtte, Paul; Kalidindi, Surya R.

    2004-09-01

    Crystal plasticity finite element (CPFE) models are useful tools in modelling the anisotropic stress-strain responses in large deformation of polycrystalline metals. In this study, a CPFE model is applied to simulate the evolution of crystallographic textures during cold rolling of hot-rolled aluminium plates and during uniaxial tensile, uniaxial compression and simple shear tests of annealed aluminium sheets. The performance of the model is critically evaluated through quantitative comparisons of the simulated textures with those predicted by the full constraints (FC) Taylor model and the experimentally measured textures. It is shown that the CPFE model performs better than the FC Taylor model in all the cases. However, the quality of the texture predictions deteriorates with increasing strain values. The CPFE model gives better texture predictions in the moderately deformed tensile and compression samples (~20% strain), compared to the more heavily deformed simple shear (0.85-0.95 shear strain) and cold-rolled (40-98% thickness reduction) samples. It is also shown that the CPFE predictions for cold rolling can be improved with finer discretization, i.e. by assigning multiple elements per grain instead of one element per grain in the finite element model. The improvement is mainly reflected in an improved prediction of the copper component and, in some cases, an improved prediction of the brass component. Inspection of the local deformation gradients reveals that these texture changes can be attributed to the increase of shear relaxations in the RD-ND and RD-TD planes.

  14. Tailored Aluminium based Coatings for Optical Appearance and Corrosion Resistance

    DEFF Research Database (Denmark)

    Aggerbeck, Martin

    of these applications, but the use of recycled aluminium compromises this due to the presence of increased levels of impurity and alloying elements. Knowledge on how different alloying elements affect the optical appearance might therefore increase the applicability of recycled aluminium. It was investigated how...

  15. Light-weight aluminium bridges and bridge decks. An overview of recent applications

    NARCIS (Netherlands)

    Maljaars, J.; Soetens, F.; Kluyver, D. de

    2008-01-01

    The last decades have shown a large increase in the application of aluminium alloys for light-weight bridges. For bridge construction, aluminium alloys have some specific advantages, but also some points of attention. This paper deals with some recent projects of aluminium bridges, and for these pro

  16. Oxide Dispersion Strengthened Fe(sub 3)Al-Based Alloy Tubes: Application Specific Development for the Power Generation Industry

    Energy Technology Data Exchange (ETDEWEB)

    Kad, B.K.

    1999-07-01

    A detailed and comprehensive research and development methodology is being prescribed to produce Oxide Dispersion Strengthened (ODS)-Fe3Al thin walled tubes, using powder extrusion methodologies, for eventual use at operating temperatures of up to 1100C in the power generation industry. A particular 'in service application' anomaly of Fe3Al-based alloys is that the environmental resistance is maintained up to 1200C, well beyond where such alloys retain sufficient mechanical strength. Grain boundary creep processes at such high temperatures are anticipated to be the dominant failure mechanism.

  17. Forming limits under multi-index constraints in NC bending of aluminum alloy thin-walled tubes with large diameters

    Institute of Scientific and Technical Information of China (English)

    2010-01-01

    With increasing diameters of aluminum alloy thin-walled tubes (AATTs), the tube forming limits, i.e. the minimum bending factors, and their predictions under multi-index constraints including wrinkling, thinning and flattening have been being a key problem to be urgently solved for improving tube forming potential in numerical control (NC) bending processes of AATTs with large diameters. Thus in this paper, a search algorithm of the forming limits is put forward based on a 3D elastic-plastic finite element (FE) model and a wrinkling energy prediction model for the bending processes under axial compression loading (ACL) or not. This algorithm enables to be considered the effects of process parameter combinations including die, friction parameters on the multi-indices. Based on this algorithm, the forming limits of the different size tubes are obtained, and the roles of the process parameter combinations in enabling the limit bending processes are also revealed. The followings are found: the first, within the appropriate ranges of friction and clearances between the different dies and the tubes enabling the bending processes with smaller bending factors, the ACL enables the tube limit bending processes after a decrease of the mandrel ball thickness and diameters; then, without considering the effects of the tube geometry sizes on the tube constitutive equations, the forming limits will be decided by the limit thinning values for the tubes with diameters smaller than 80 mm, while the wrinkling for the tubes with diameters no less than 80 mm. The forming limits obtained from this algorithm are smaller than the analytical results, and reduced by 57.39%; the last, the roles of the process parameter combinations in enabling the limit bending processes are verified by experimental results.

  18. Effect of stress ratio and frequency on fatigue crack growth rate of 2618 aluminium alloy silicon carbide metal matrix composite

    Indian Academy of Sciences (India)

    Nirbhay Singh; Ram Khelawan; G N Mathur

    2001-04-01

    Effect of stress ratio and frequency on the fatigue crack propagation of 2618 aluminium alloy–silicon carbide composite were investigated at ambient temperature. With the first set of specimens, the fatigue crack growth rates were studied at three frequencies of 1 Hz, 5 Hz and 10 Hz at a stress ratio of 0.1 whereas the effects of stress ratios of 0.1, 0.25 and 0.50 were studied with the second set of specimens. The study showed that the fatigue crack propagation behaviour of this metal matrix composite was influenced to an appreciable extent by the stress ratio, but not by the fatigue frequencies used in this investigation.

  19. Investigation of the Wear and Hardness Behaviour of Aluminium Alloy Coated Using the Powder Flame Spraying Method

    Directory of Open Access Journals (Sweden)

    Nurullah KIRATLI

    2009-03-01

    Full Text Available In this study, the wear behavior of aluminum alloy AL 5754 ( Etial 53 coated with powders of 10Al-Cu alloy (RotoTec® 19850 and 15Cr7Fe-Ni alloy (RotoTec® 19985 using powder flame spraying method has been investigated. To avoid thermal expansions between substrate and coating materials, Ni-Al RotoTec® 51000 was used as binding material. The wear test was performed on a pin-on-disc test apparatus. As an abrasive material, a SiC, 800 sandpaper was used. The wear tests of coated materials were carried out at room temperature and at 1.0m/s sliding speed with 0.35 and 0.70MPa pressures. To characterize coated specimens, they have been examined with optical microscope. As a result, it is found that the both coating materials have improved wear resistance.

  20. Welding Stress and Welding Distortion of 6061 Aluminium Alloy Thin Plate%6061铝合金薄板焊接应力与焊接变形

    Institute of Scientific and Technical Information of China (English)

    陈丽华; 封艳

    2013-01-01

    the relationship between the plate size, welding current, welding voltage and welding stress, the welding distortion for 6061 aluminum alloy sheet TIG welding is studied. With the increase of welding current, welding voltage,aluminium alloy of the longitudinal and lateral contraction deformation increase; With the increase of the length of the plate, due to the much more constraint, the plate of the longitudinal residual deformation decrease,for the bending stress in thickness direction increases,the transverse deformation increases. Residual stress of welding is tensile, and the parent metal close to weld is compressive stress, and the rest of the parent metal is tensile stress, the more the welding energy is, the greater the residual stress.%研究了6061铝合金薄板TIG焊焊接应力、焊接变形与焊接电流、焊接电压和板材尺寸的关系.随着焊接线能量的增加,铝合金的纵向和横向收缩变形增加;随着板的长度的增加,由于约束增加,板的纵向残余变形减少,厚度方向的抗弯增大,横向变形增大.板焊后,焊缝处受拉应力,而紧靠焊缝的母材处却受压应力,其余部分受拉应力且焊接线能量越大,残余应力越大.

  1. 6061铝合金板材锯齿形屈服行为的研究%Study of Serrated Yielding in 6063 Aluminium Alloy Board

    Institute of Scientific and Technical Information of China (English)

    孙萍; 刘程; 王辉

    2012-01-01

    The stress drop amplitude and the duration of the serration, etc. of serrated yielding effect in 6063 aluminium alloy are analyzed systematically, and the influence of serrated yielding effect on mechanical properties is discussed. The results show that the stress drop amplitude number, drop duration and its number, reloading time and its number decrease when the strain rate increases. The serrated yielding effect is weakest and the mechanical properties are best when the strain rate is 1.4×10^-3s^-1%对6061铝合金板材锯齿形屈服行为中应力跌幅、跌落时间等多个特征物理量随应变率的变化规律进行了系统的研究,探讨了锯齿形行为对材料力学性能的影响。结果表明,应力跌幅个数,跌落时间及其个数,再加载时间及其个数均随着应变率的增大而逐渐减少;当应变率为1.4×10^-3s^-1时,6061铝合金板材的锯齿形屈服行为最弱,板材的力学性能最好。

  2. Evaluation of interfacial bonding in dissimilar materials of YSZ-alumina composites to 6061 aluminium alloy using friction welding

    Energy Technology Data Exchange (ETDEWEB)

    Uday, M.B., E-mail: ummb2008@gmail.com [School of Materials and Mineral Resources Engineering, Engineering Campus, Universiti Sains Malaysia, 14300 Nibong Tebal, Penang (Malaysia); Ahmad Fauzi, M.N., E-mail: afauzi@eng.usm.my [School of Materials and Mineral Resources Engineering, Engineering Campus, Universiti Sains Malaysia, 14300 Nibong Tebal, Penang (Malaysia); Zuhailawati, H.; Ismail, A.B. [School of Materials and Mineral Resources Engineering, Engineering Campus, Universiti Sains Malaysia, 14300 Nibong Tebal, Penang (Malaysia)

    2011-01-25

    Research highlights: {yields} Friction-welding process. {yields} Joining between ceramic composite and metal alloy. {yields} Slip casting of the yttria stabilized zirconia/alumina composite samples. - Abstract: The interfacial microstructures characteristics of alumina ceramic body reinforced with yttria stabilized zirconia (YSZ) was evaluated after friction welding to 6061 aluminum alloy using optical and electron microscopy. Alumina rods containing 25 and 50 wt% yttria stabilized zirconia were fabricated by slip casting in plaster of Paris (POP) molds and subsequently sintered at 1600 deg. C. On the other hand, aluminum rods were machine down to the required dimension using a lathe machine. The diameter of the ceramic and the metal rods was 16 mm. Rotational speeds for the friction welding were varied between 900 and 1800 rpm. The friction pressure was maintained at 7 MPa for a friction time of 30 s. Optical and scanning electron microscopy was used to analyze the microstructure of the resultant joints, particularly at the interface. The joints were also examined with EDX line (energy dispersive X-ray) in order to determine the phases formed during the welding. The mechanical properties of the friction welded YSZ-Al{sub 2}O{sub 3} composite to 6061 alloy were determined with a four-point bend test and Vickers microhardness. The experimental results showed the degree of deformation varied significantly for the 6061 Al alloy than the ceramic composite part. The mechanical strength of friction-welded ceramic composite/6061 Al alloy components were obviously affected by joining rotational speed selected which decreases in strength with increasing rotational speed.

  3. Fireside corrosion testing of candidate superheater tube alloys, coatings, and claddings -- Phase 2

    Energy Technology Data Exchange (ETDEWEB)

    Blough, J.L.; Seitz, W.W. [Foster Wheeler Development Corp., Livingston, NJ (United States)

    1997-12-01

    In Phase 1 a variety of developmental and commercial tubing alloys and claddings were exposed to laboratory fireside corrosion testing simulating a superheater or reheater in a coal-fired boiler. Phase 2 (in situ testing) has exposed samples of 347 RA-85H, HR3C, 253MA, Fe{sub 3}Al + 5Cr, 310 Ta modified, NF 709, 690 clad, and 671 clad for approximately 4,000, 12,000, and 16,000 hours to the actual operating conditions of a 250-MW coal-fired boiler. The samples were assembled on an air-cooled, retractable corrosion probe, the probe was installed in the reheater activity of the boiler and controlled to the operating metal temperatures of an existing and advanced-cycle coal-fired boiler. The results will be presented for the preliminary metallurgical examination of the corrosion probe samples after 16,000 hours of exposure. Continued metallurgical and interpretive analysis is still on going.

  4. Morphologies of Fe-66.7 at.%Si alloy solidified in a drop tube

    Institute of Scientific and Technical Information of China (English)

    WANG; Haiyan; LIU; Riping; MA; Mingzhen; JING; Qin; LI; Gon

    2005-01-01

    Solidification of 0.1―1.0 mm diameter droplets of Fe-66.7 at.%Si alloy was achieved in a 3 m drop tube. The XRD, EDS, and SEM measurements reveal that all the droplets are composed of the primary phase α and the α+ε eutectic. With decreasing droplet diameter, the growth mode of the primary phase α changes from faceted to nonfaceted growth and the eutectic changes from needle-like to anomalous eutectic. In addition, the width of the primary phase α decreases with decreasing droplet size. The different cooling rates and undercooling levels corresponding to the samples with different sizes are responsible for the morphology changes. The cooling rates of the samples with different diameters during free fall were calculated and their effects on the microstructure formation were discussed. This kind of transition is also found inside the same sample, which is due to the larger cooling rate on the surface than at the center.

  5. Impact properties of the aircraft cast aluminium alloy Al-7Si0.6Mg (A357

    Directory of Open Access Journals (Sweden)

    Alexopoulos N.D.

    2010-06-01

    Full Text Available The impact mechanical properties of the widely used in the aeronautics A357 cast aluminum alloy were investigated by exploiting experiments on an instrumented Charpy impact testing machine. The evaluated impact properties for 25 different artificial aging heat treatment conditions were analyzed and discussed in conjunction with the respective tensile properties. Correlations are proposed to establish useful relationships between impact resistance and tensile strain energy density properties. The established correlations, which are well supported by the performed experiments, can be used to estimate the tensile ductility and toughness of the A357 cast aluminum alloy from the Charpy impact test. Performed fractographic analyses were supporting the physically arbitrary correlation between tensile strain energy density and impact resistance.

  6. Impact properties of the aircraft cast aluminium alloy Al-7Si0.6Mg (A357)

    Science.gov (United States)

    Alexopoulos, N. D.

    2010-06-01

    The impact mechanical properties of the widely used in the aeronautics A357 cast aluminum alloy were investigated by exploiting experiments on an instrumented Charpy impact testing machine. The evaluated impact properties for 25 different artificial aging heat treatment conditions were analyzed and discussed in conjunction with the respective tensile properties. Correlations are proposed to establish useful relationships between impact resistance and tensile strain energy density properties. The established correlations, which are well supported by the performed experiments, can be used to estimate the tensile ductility and toughness of the A357 cast aluminum alloy from the Charpy impact test. Performed fractographic analyses were supporting the physically arbitrary correlation between tensile strain energy density and impact resistance.

  7. Investigation impact of stressed state conditions and thermomechanical parameters on the texture and structure evolution in 1565ph aluminium alloy

    Science.gov (United States)

    Yashin, V. V.; Aryshensky, E. V.; Kawalla, R. F.; Serebryany, V. N.; Rushchits, S. V.

    2016-11-01

    The paper is devoted to study of the impact stress condition and thermomechanical treatment parameters on the structure and texture evolution of new 1565 ph aluminum alloy. For that purposes, we use test on Gleeble equipment, FM calculation, optical microscopy and x ray diffraction texture analysis. The dependency between the deformation texture components development and strain rate value was established. Differences in the texture evolution at uniaxial compression stress and plain strain mode were revealed.

  8. Fatigue FEM analysis in the case of brazed aluminium alloy 3L59 used in aeronautical industry

    Science.gov (United States)

    Dimitrescu, A.; Amza, Gh; Niţoi, D. F.; Amza, C. Gh; Apostolescu, Z.

    2016-08-01

    The use, on a larger scale, of brazed aluminum alloys in the aerospace industry led to the need for a detailed study of the assemblies behavior. These are built from 6061 aluminum aloy (3L59) brazed with aluminum aloy A103. Therefore, a finit element simulation (FEM) of durability is necessary, that consists in the observation of gradual deterioration until failure. These studies are required and are previous to the stage of the producing the assembly and test it by traditional methods.

  9. Biochemical analysis of the Hormoconis resinae fungal mycelium in the corrosion of aeronautical aluminium alloys

    Directory of Open Access Journals (Sweden)

    Araya, R.

    2007-06-01

    Full Text Available Biochemical analyses of the Hormoconis resinae fungal mycelium would explain behaviour differences of corrosive and non-corrosive strains on Al and its aeronautical alloys. In previous works its aggressiveness had been studied through SEM-EDX surface analysis, electrochemical techniques and immersion testing. In this paper separation of the proteins of the mycelium produced by a non-corrosive strain and its culture along three generations was performed. Cultures were prepared in batch in the presence and absence of pure Al and AA 2024, AA 7005 and AA 7075 alloys. The mycelia grown throughout the three generations increasingly
    recovered usual characteristics at the third replication, included their corrosiveness on Al and its alloys previously shown by all our strains. Amongst the bio-molecule fractions isolated and analysed during this preliminary study only the proteins revealed changes with the generation grown. When this fungal strain was cultured in the presence of alloy metal sheets electrophoresis of the protean fraction was correlative with the distinct mycelia behaviour observed, including corrosiveness on Al and its alloys.

    Las diferencias entre el comportamiento corrosivo y no corrosivo de una cepa del hongo Hormoconis resinae sobre aluminio y sus aleaciones aeronáuticas se explicarían a través de análisis bioquímicos del micelio. En trabajos previos, el comportamiento corrosivo se estudió mediante análisis de superficie SEM-EDX, técnicas electroquímicas y ensayos de inmersión. En este trabajo, se llevó a cabo la separación de proteínas del micelio producido por una cepa que perdió su corrosividad y su cultivo a través de tres generaciones. Cultivos en batch, en presencia y ausencia de aluminio y sus aleaciones AA 2024, AA 7005 y AA 7075, a través de tres generaciones del micelio crecido, fueron recuperando sus características, incluida su habitual corrosividad, en la tercera replicaci

  10. Application of glass ellipsoid aluminium alloy structure in building engineering%玻璃椭球体铝合金结构在建筑工程中的应用

    Institute of Scientific and Technical Information of China (English)

    吴志平; 朱伟信; 赵华; 蒋乃杰; 魏国华

    2001-01-01

    The aluminium and titanium are used as mesh shell construction of ellipsoid glass building with major axis length of 66.8 m, minor axis length of 57.0 m, above ground 34.3 m, under ground 7.25 m. The weight of glass as building covering outside is 400 t. The aluminium alloy H beam, aluminium round gusset and stainless steel lock bolts are used for construction to form single layer aluminium mesh shell system. This engineering structure stressing is complicated. The requirements for component fabrication are very strict with bigger difficulty during construction and installation. This is a first large aluminium structure ellipsoid engineering in China. The plan selection, structure design, material selection and ellipsoid engineering construction and installation for this building were presented in the paper.%以铝钛合金为网壳结构的玻璃椭球体建筑,长轴为 66.8 m,短轴为 57.0 m,地面以上 34.3 m,地下 7.25 m高。该建筑外覆玻璃盖层重达 400 t,结构采用铝合金工字梁、铝质圆形节点板与不锈钢锁紧螺栓,构成单层铝网壳体系。工程结构受力复杂,构件制作要求严格,施工安装难度较大,是我国首例铝结构大型椭球形工程。文中对该建筑工程从方案选定、结构设计、材料选用及球体工程施工安装等作了较详细介绍。

  11. The Study of Heat Treatment Effects on Chromium Carbide Precipitation of 35Cr-45Ni-Nb Alloy for Repairing Furnace Tubes

    Directory of Open Access Journals (Sweden)

    Nakarin Srisuwan

    2016-01-01

    Full Text Available This paper presents a specific kind of failure in ethylene pyrolysis furnace tubes. It considers the case in which the tubes made of 35Cr-45Ni-Nb high temperature alloy failed to carburization, causing creep damage. The investigation found that used tubes became difficult to weld repair due to internal carburized layers of the tube. The microstructure and geochemical component of crystallized carbide at grain boundary of tube specimens were characterized by X-ray diffractometer (XRD, scanning electron microscopy (SEM with back-scattered electrons mode (BSE, and energy dispersive X-ray spectroscopy (EDS. Micro-hardness tests was performed to determine the hardness of the matrix and the compounds of new and used tube material. The testing result indicated that used tubes exhibited a higher hardness and higher degree of carburization compared to those of new tubes. The microstructure of used tubes also revealed coarse chromium carbide precipitation and a continuous carbide lattice at austenite grain boundaries. However, thermal heat treatment applied for developing tube weld repair could result in dissolving or breaking up chromium carbide with a decrease in hardness value. This procedure is recommended to improve the weldability of the 35Cr-45Ni-Nb used tubes alloy.

  12. A Study Into Effects of Different Parameters on Mechanical Properties in Friction Stir Welding of AA 2024 Aluminium Alloy

    Directory of Open Access Journals (Sweden)

    Aydın ŞIK

    2010-02-01

    Full Text Available In this study AA2024 alloy, which is used especially in aircraft body, wings and automotive industry due to its lightness, workable aspect, high corrosion resistance and durability, was welded with stir friction method, and fatigue, hardness, bending and tension experiments of the joints obtained were conducted. Welding progress speed of the 4 mm thick sheets and stir tool rotation were determined to be the variable parameters. These parameters were taken as 20 mm shoulder width, 1000 rpm traverse speed, 1500 rpm, 2500 rpm and the progress speed was taken as 120 mm/min and 200 mm/min.

  13. Evolution of the microstructure, texture and creep properties of the 7075 aluminium alloy during hot accumulative roll bonding

    OpenAIRE

    Hidalgo-Manrique, P.; Cepeda-Jiménez, C.M.; Orozco-Caballero, Alberto; Ruano, Oscar Antonio; Carreño, Fernando

    2014-01-01

    The 7075 Al alloy was severely deformed at 350 °C by a 3:1 thickness reduction per pass accumulative roll bonding (ARB) process up to six passes. It was found that discontinuous recrystallisation occurs during the inter-pass annealing stages from the third pass on, attributable to the increment of the mean particle size during processing. As a consequence, the mean crystallite size did not decrease, but remained approximately constant at 440 nm along the present ARB process and the mean bound...

  14. Experimental Study of the Micro-Arc Oxide Coating Effect on Thermal Properties of an Aluminium Alloy Piston Head

    Directory of Open Access Journals (Sweden)

    N.Yu. Dudareva

    2015-09-01

    Full Text Available The purpose of the present study is to investigate the influence of differently sized microarc oxidation coatings, applied to the bottom of pistons made with an Al-12Si-Mg-Cu-Ni alloy, on its thermal properties by simulating the operation of a real engine. This study is based on the premise that the alumina coating thickness affects the heat transfer and temperature distribution in the piston. The analysis of thermal properties of pistons and suggestions for the optimal thermal barrier coating thickness are presented.

  15. Challenges in LCA modelling of multiple loops for aluminium cans

    DEFF Research Database (Denmark)

    Niero, Monia; Olsen, Stig Irving

    packaging scrap sources (i.e. used beverage can and mixed aluminium packaging) to understand the limiting factors for multiple loop aluminium can recycling. Secondly, we performed a comparative LCA of aluminium can production and recycling in multiple loops considering the two aluminium packaging scrap...... this information to perform an LCA of 30 recycling loops based on the actual alloy composition. From the comparative LCA the closed product loop option (i.e. using used beverage can scraps) turned out to have lower environmental impact than the open loop option (i.e. using mixed aluminium packaging scraps...

  16. Circular economy: To be or not to be in a closed product loop? A Life Cycle Assessment of aluminium cans with inclusion of alloying elements

    DEFF Research Database (Denmark)

    Niero, Monia; Olsen, Stig Irving

    2016-01-01

    to a temporal interval of five years. Different aluminium packaging scrap sources were considered: mixed packaging aluminium scrap and used beverage can scrap. The outcomes of the mass balance were used to quantify the amount of Mn and primary Al that needs to be reintegrated in each scenario according...

  17. Investigation of the aluminium-aluminium oxide reversible transformation as observed by hot stage electron microscopy.

    Science.gov (United States)

    Grove, C. A.; Judd, G.; Ansell, G. S.

    1972-01-01

    Thin foils of high purity aluminium and an Al-Al2O3 SAP type of alloy were oxidised in a specially designed hot stage specimen chamber in an electron microscope. Below 450 C, amorphous aluminium oxide formed on the foil surface and was first detectable at foil edges, holes, and pits. Islands of aluminium then nucleated in this amorphous oxide. The aluminium islands displayed either a lateral growth with eventual coalescence with other islands, or a reoxidation process which caused the islands to disappear. The aluminium island formation was determined to be related to the presence of the electron beam. A mechanism based upon electron charging due to the electron beam was proposed to explain the nucleation, growth, coalescence, disappearance, and geometry of the aluminium islands.

  18. Microstructure, elastic deformation behavior and mechanical properties of biomedical β-type titanium alloy thin-tube used for stents.

    Science.gov (United States)

    Tian, Yuxing; Yu, Zhentao; Ong, Chun Yee Aaron; Kent, Damon; Wang, Gui

    2015-05-01

    Cold-deformability and mechanical compatibility of the biomedical β-type titanium alloy are the foremost considerations for their application in stents, because the lower ductility restricts the cold-forming of thin-tube and unsatisfactory mechanical performance causes a failed tissue repair. In this paper, β-type titanium alloy (Ti-25Nb-3Zr-3Mo-2Sn, wt%) thin-tube fabricated by routine cold rolling is reported for the first time, and its elastic behavior and mechanical properties are discussed for the various microstructures. The as cold-rolled tube exhibits nonlinear elastic behavior with large recoverable strain of 2.3%. After annealing and aging, a nonlinear elasticity, considered as the intermediate stage between "double yielding" and normal linear elasticity, is attributable to a moderate precipitation of α phase. Quantitive relationships are established between volume fraction of α phase (Vα) and elastic modulus, strength as well as maximal recoverable strain (εmax-R), where the εmax-R of above 2.0% corresponds to the Vα range of 3-10%. It is considered that the "mechanical" stabilization of the (α+β) microstructure is a possible elastic mechanism for explaining the nonlinear elastic behavior.

  19. The ‘full sleeve’ application in the horizontal cold-chamber machine for pressure die casting of aluminium alloys

    Directory of Open Access Journals (Sweden)

    Z. Konopka

    2008-04-01

    Full Text Available The ‘full sleeve’ construction has been designed and accomplished in the horizontal cold-chamber pressure die casting machine. Main part of this solution is a counter plunger placed in a movable die half which allows for full filling of the shot sleeve and precisely fixes the metal quantity needed for casting. The purpose of this new construction solution is mainly the reduction of the casting porosity caused by air entrapment and the improvement of both castability and accuracy of the die cavity reproduction. For such a redesigned machine there have been performed examinations consisting in pressure casting of AlSi9Cu alloy (EN AC-46000 at varying plunger velocity in the second stage of injection and varying intensification pressure. The alloy castability (the die filling ability has been measured for each parameter setting. For the purpose of comparison, similar measurements have been performed also for the conventional system without a counter plunger. The castability examination has been done by means of a specially designed die with an impression of a trial casting of variable wall thickness. The experiments have been held according to the assumed factor design 22, what allowed for determining the mathematical models describing the influence of die filling parameters on the castability and the die cavity reproduction level. Both alternatives of the experiment confirmed the positive influence of plunger velocity and intensification pressure increase on the improvement of castability, the measure of the latter being the filled length of the impression. Applying of the new ‘full sleeve’ solution has improved castability for each experiment by about 20% as compared with conventional alternative. Castability in the ‘full sleeve’ system has been increased even for low values of plunger velocity and intensification pressure. For both alternative systems the influence of plunger velocity has been found, as an average, by four times

  20. Fatigue Property of Friction Stir Welded Extruded Aluminium Alloy 6005A%6005A铝合金型材搅拌摩擦焊接头疲劳性能研究

    Institute of Scientific and Technical Information of China (English)

    陈荣康; 孙春方; 戴瑛

    2012-01-01

    A friction stir welded(FSW) butted aluminium alloy 6005A plate, which is used for train wall sides, was tested under static tensile and fatigue tensile loads. Due to effect of FSW, its static and fatigue strength are lower as compare that with parent material. Full-scale static tensile, fatigue tensile and 3-points bending fatigue test were completed on friction stir welded extruded aluminium alloy 6005A. The fatigue behaviors of tensile and bending characterised by S-N curve with a stress ratio of 0.1 were obtained by least square method. The fatigue limits of friction stir welded extruded aluminium alloy 6005A subjected to tensile and bending loading were experimentally established. Furthermore, failure location of such structure under fatigue loading proofs the strength of FSW butt joint. The presented test data provides solid base for design and practical application of the friction stir welded extruded aluminium alloy 6005A.%对车身用6005A铝合金FSW对接板材进行了拉伸性能、拉伸疲劳性能试验研究,并与母材进行了对比;对6005A铝合金FSW对接型材进行了拉伸性能、拉伸疲劳性能和三点弯曲疲劳性能试验研究;根据疲劳试验结果,拟合出6005A铝合金FSW对接板材、型材的拉伸、三点弯曲的S-N曲线(R=0.1),并由此得出该结构的疲劳强度;由6005A铝合金FSW对接型材的静拉伸、疲劳拉伸和三点弯曲疲劳载荷作用下的失效位置,证实了FSW接头的可靠性,为结构的设计和使用提供了可靠的试验数据支持.

  1. Modeling and Simulation of Laser Welding for Aluminium Alloy%激光焊接铝合金材料过程的建模与仿真

    Institute of Scientific and Technical Information of China (English)

    卢艳; 张静; 胡敬佩; 项俊锋

    2012-01-01

    The distribution of the temperature field during laser welding based on aluminium alloy 3A21 was dynamically simulated by FEA software-ANSYS. In view of the highly non-linear characters of laser welding, a travel heat source combining with the body loads was built by analyzing the thermal physical parameters of material, such as latent heat of fusion, thermal conduction,convection and radiation. The results show that the temperature gradient of laser welding is larger, and HAZ is smaller than others. The temperature curves in the temperature fields rise and decline exponential], and the temperature in weld and near weld changes rapidly. The simulation results of width in the weld is in line with the experimental results, which verify the applicability of the model established by moving heat source during the laser welding based on aluminum alloy sheet applying to the temperature field simulation, and to a certain extent, the forming mechanism of the laser welding is revealed.%在试验基础上,利用有限元软件ANSYS对3A21铝合金材料激光焊接温度场进行了动态模拟.通过对激光焊接非线性瞬态过程的分析,分析与温度场有关的潜热、热传导、对流、辐射等材料热物理属性,建立了激光焊接的移动热源模型.仿真结果表明:激光焊接薄板铝合金的温度场梯度大,热影响区小;温度场中各点温度呈指数式升高和衰减;焊缝和近焊缝区温度升降急剧,焊缝宽度的仿真结果与试验结果相一致,从而验证了所建立的移动热源模型在激光焊接铝合金薄板温度场模拟中的适用性,在一定程度上揭示了激光焊接的成型机理.

  2. Microstructure and Properties of Welded Joint of Extruded 6005A Aluminium Alloy%6005A铝合金型材焊接接头组织与性能

    Institute of Scientific and Technical Information of China (English)

    尹志民; 张爱琼; 王炎金

    2001-01-01

    采用国产6005A铝合金进行焊接试验,并对焊接接头进行了力学性能检测及金相显微组织观察。结果表明,6005A铝合金的焊接接头焊缝两侧离焊缝中心约10~15mm的地方存在一对对称分布的软化区,其原因是由于焊接热的影响使该部位发生了过时效.对进口的6005A大型多孔铝型材焊接接头进行分析,发现焊接接头上软化区硬度降低的程度明显较小,这是由于实际的多孔型材在该部位设置有加强筋,加强筋有显著的散热作用,降低了焊接过程中该部位的温升.另一方面,加强筋增大了软化区的承载面积,有机械补强作用。%Welding test of extruded 6005A Aluminium alloy was performed and mechanical properties and optical microstructures were studied. The results show that there is a pair of symmetric soft zone which was located on both sides of the weld about 10~15 mm apart from the weld center. The occurrence of soft zone is due to overaging caused by heat input during welding. In the condition of big practical extruded 6005A alloy welded joint, the softing degree of mentioned above soft zone obviously decreases, attributed to that there is a reinforce rib which have obvious heat scatting action, and then decreases the temperature increasing during welding. On another hand, this reinforce rib increase the loading area and have a strength compensating.

  3. Effect of tool shape and welding parameters on mechanical properties and microstructure of dissimilar friction stir welded aluminium alloys

    Directory of Open Access Journals (Sweden)

    Chetan Aneja

    2016-07-01

    Full Text Available In the present experimental study, dissimilar aluminum alloy AA5083 and AA6082 were friction stir welded by varying tool shape, welding speed and rotary speed of the tool in order to investigate the effect of varying tool shape and welding parameters on the mechanical properties as well as microstructure. The friction stir welding (FSW process parameters have great influence on heat input per unit length of weld. The outcomes of experimental study prove that mechanical properties increases with decreasing welding speed. Furthermore mechanical properties were also found to improve as the rotary speed increases and the same phenomenon was found to happen while using straight cylindrical threaded pin profile tool. The microstructure of the dissimilar joints revealed that at low welding speeds, the improved material mixing was observed. The similar phenomenon was found to happen at higher rotational speeds using straight cylindrical threaded tool.

  4. Influence of annealing and deformation on optical properties of ultra precision diamond turned and anodized 6060 aluminium alloy

    DEFF Research Database (Denmark)

    Tabrizian-Ghalehno, Naja; Hansen, Hans Nørgaard; Hansen, P.E.;

    2010-01-01

    function (BRDF), an optical instrument. Results indicated that the post-forging heat treatment had a great influence on the appearance of the anodized layer, which was also a function of the deformation introduced prior to heat treatment. The effect was assumed to be attributed to the change...... in microstructure, especially the distribution and the amount of the intermetallic particles such as elemental Si and Mg2Si. Roughness of the oxide film was also found to be a function of the heat treatment and deformation condition.......Influence of cold forging, and subsequent heat treatment and diamond turning on optical quality of anodized film on 6060 (AlMgSi) alloy was investigated and compared with microstructural changes. Heat treatment of the samples was carried out either prior to forging, post-forging, or both...

  5. Comparison between diffraction contrast tomography and high-energy diffraction microscopy on a slightly deformed aluminium alloy.

    Science.gov (United States)

    Renversade, Loïc; Quey, Romain; Ludwig, Wolfgang; Menasche, David; Maddali, Siddharth; Suter, Robert M; Borbély, András

    2016-01-01

    The grain structure of an Al-0.3 wt%Mn alloy deformed to 1% strain was reconstructed using diffraction contrast tomography (DCT) and high-energy diffraction microscopy (HEDM). 14 equally spaced HEDM layers were acquired and their exact location within the DCT volume was determined using a generic algorithm minimizing a function of the local disorientations between the two data sets. The microstructures were then compared in terms of the mean crystal orientations and shapes of the grains. The comparison shows that DCT can detect subgrain boundaries with disorientations as low as 1° and that HEDM and DCT grain boundaries are on average 4 µm apart from each other. The results are important for studies targeting the determination of grain volume. For the case of a polycrystal with an average grain size of about 100 µm, a relative deviation of about ≤10% was found between the two techniques.

  6. Comparison between diffraction contrast tomography and high-energy diffraction microscopy on a slightly deformed aluminium alloy

    Directory of Open Access Journals (Sweden)

    Loïc Renversade

    2016-01-01

    Full Text Available The grain structure of an Al–0.3 wt%Mn alloy deformed to 1% strain was reconstructed using diffraction contrast tomography (DCT and high-energy diffraction microscopy (HEDM. 14 equally spaced HEDM layers were acquired and their exact location within the DCT volume was determined using a generic algorithm minimizing a function of the local disorientations between the two data sets. The microstructures were then compared in terms of the mean crystal orientations and shapes of the grains. The comparison shows that DCT can detect subgrain boundaries with disorientations as low as 1° and that HEDM and DCT grain boundaries are on average 4 µm apart from each other. The results are important for studies targeting the determination of grain volume. For the case of a polycrystal with an average grain size of about 100 µm, a relative deviation of about ≤10% was found between the two techniques.

  7. Standard specification for Nickel-Chromium-Iron alloys (UNS N06600, N06601, N06603, N06690, N06693, N06025, N06045, and N06696), Nikel-Chromium-Cobalt-Molybdenum alloy (UNS N06617), and Nickel-Iron-Chromium-Tungsten alloy (UNS N06674) seamless pipe and tube

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2011-01-01

    Standard specification for Nickel-Chromium-Iron alloys (UNS N06600, N06601, N06603, N06690, N06693, N06025, N06045, and N06696), Nikel-Chromium-Cobalt-Molybdenum alloy (UNS N06617), and Nickel-Iron-Chromium-Tungsten alloy (UNS N06674) seamless pipe and tube

  8. Effect of Rotational Speeds on the Cast Tube During Vertical Centrifugal Casting Process on Appearance, Microstructure, and Hardness Behavior for Al-2Si Alloy

    Science.gov (United States)

    Shailesh Rao, A.; Tattimani, Mahantesh S.; Rao, Shrikantha S.

    2015-04-01

    The flow of molten metal plays a crucial role in determining casting quality. During rotation of the mold, melt flow around its inner circumference determines the final configurations and properties of the cast tube. In this paper, Al-2Si alloy is cast in the vertical mold at the various rotational speeds of the mold. The uniform cylinder tube is formed at a rotational speed of 1000 rpm, while before and beyond this speed, irregular-shaped cast tube is formed. Finally, fine structured grain size with high hardness value is found in uniform cast tube compared with others.

  9. Synthesis and characterization of Ni-Mo filler brazing alloy for Mo-W joining for microwave tube technology

    Directory of Open Access Journals (Sweden)

    Frank Ferrer Sene

    2013-04-01

    Full Text Available A brazing process based on Ni-Mo alloy was developed to join porous tungsten cathode bottom and dense molybdenum cathode body for microwave tubes manufacture. The Ni-Mo alloy was obtained by mixing and milling powders in the eutectic composition, and applied on the surface of the components. The brazing was made at 1400 °C by using induction heating in hydrogen for 5 minutes. Alumina surfaces were coated with the binder and analyzed by Energy Dispersive X-rays Fluorescence. The brazed samples were analyzed by Scanning Electron Microscopy coupled to Energy Dispersive Spectroscopy. Stress-strain tests were performed to determine the mechanical behavior of the joining. The quality of the brazing was evaluated by assuring the presence of a "meniscus" formed by the Ni-Mo alloy on the border of the tungsten and molybdenum joint, the absence of microstructural defects in the interface between the tungsten and molybdenum alloys, and the adhesion of the brazed components.

  10. Cold forming of aluminium - State of the art

    DEFF Research Database (Denmark)

    Bay, Niels

    1997-01-01

    to that of unalloyed steel. After description of the different types of alloys and their individual properties and applications, the special requirements for tool design by cold forging in aluminium is discussed. Finally, a large number of industrial examples on cold forged aluminium components are presented. (C) 1997......The ongoing development of cold forging technology has been manifested lately by the increasing application of components in cold forged aluminium alloys. Applying precipitation hardening alloys components with great strength/weight ratio can be produced with a strength comparable...

  11. Accuracy of Ceramic Mould Filling with Liquid AlSi9 Aluminium Alloy in the Process Using Back-pressure

    Directory of Open Access Journals (Sweden)

    A. Karwiński

    2013-01-01

    Full Text Available The paper presents the effect of suction pressure exerted on the liquid AlSi alloy when it is introduced into a ceramic mould made in the investment process and the results compared with data obtained on gravity poured castings.The study used special pattern sets and ceramic moulds made with the alternately applied soluble silicate binder and ethyl silicate.Additionally, self-supported moulds based entirely on the Ekosil binder were used. In the analysis of castings, the following parameters were examined: a linear dimensional accuracy, the state of surface microgeometry and the possibility of metal penetration into a complex ceramic mould, allowing also for the presence of capillary phenomena. In the process of casting with back-pressure, the pressure values of 500 hPa, 600 hPa and 700 hPa were applied in the chamber where the ceramic mould was located, with the temperature of the said mould kept at a level of 150  10C.

  12. Aluminium alloyed iron-silicide/silicon solar cells: A simple approach for low cost environmental-friendly photovoltaic technology

    Science.gov (United States)

    Kumar Dalapati, Goutam; Masudy-Panah, Saeid; Kumar, Avishek; Cheh Tan, Cheng; Ru Tan, Hui; Chi, Dongzhi

    2015-12-01

    This work demonstrates the fabrication of silicide/silicon based solar cell towards the development of low cost and environmental friendly photovoltaic technology. A heterostructure solar cells using metallic alpha phase (α-phase) aluminum alloyed iron silicide (FeSi(Al)) on n-type silicon is fabricated with an efficiency of 0.8%. The fabricated device has an open circuit voltage and fill-factor of 240 mV and 60%, respectively. Performance of the device was improved by about 7 fold to 5.1% through the interface engineering. The α-phase FeSi(Al)/silicon solar cell devices have promising photovoltaic characteristic with an open circuit voltage, short-circuit current and a fill factor (FF) of 425 mV, 18.5 mA/cm2, and 64%, respectively. The significant improvement of α-phase FeSi(Al)/n-Si solar cells is due to the formation p+-n homojunction through the formation of re-grown crystalline silicon layer (~5-10 nm) at the silicide/silicon interface. Thickness of the regrown silicon layer is crucial for the silicide/silicon based photovoltaic devices. Performance of the α-FeSi(Al)/n-Si solar cells significantly depends on the thickness of α-FeSi(Al) layer and process temperature during the device fabrication. This study will open up new opportunities for the Si based photovoltaic technology using a simple, sustainable, and los cost method.

  13. Aluminium alloyed iron-silicide/silicon solar cells: A simple approach for low cost environmental-friendly photovoltaic technology.

    Science.gov (United States)

    Kumar Dalapati, Goutam; Masudy-Panah, Saeid; Kumar, Avishek; Cheh Tan, Cheng; Ru Tan, Hui; Chi, Dongzhi

    2015-12-03

    This work demonstrates the fabrication of silicide/silicon based solar cell towards the development of low cost and environmental friendly photovoltaic technology. A heterostructure solar cells using metallic alpha phase (α-phase) aluminum alloyed iron silicide (FeSi(Al)) on n-type silicon is fabricated with an efficiency of 0.8%. The fabricated device has an open circuit voltage and fill-factor of 240 mV and 60%, respectively. Performance of the device was improved by about 7 fold to 5.1% through the interface engineering. The α-phase FeSi(Al)/silicon solar cell devices have promising photovoltaic characteristic with an open circuit voltage, short-circuit current and a fill factor (FF) of 425 mV, 18.5 mA/cm(2), and 64%, respectively. The significant improvement of α-phase FeSi(Al)/n-Si solar cells is due to the formation p(+-)n homojunction through the formation of re-grown crystalline silicon layer (~5-10 nm) at the silicide/silicon interface. Thickness of the regrown silicon layer is crucial for the silicide/silicon based photovoltaic devices. Performance of the α-FeSi(Al)/n-Si solar cells significantly depends on the thickness of α-FeSi(Al) layer and process temperature during the device fabrication. This study will open up new opportunities for the Si based photovoltaic technology using a simple, sustainable, and los cost method.

  14. Experiment on high speed machining parametres for sport shoe sole mold making using aluminium alloy 5083, 6163 and 7075

    Directory of Open Access Journals (Sweden)

    S. Chartakom

    2008-12-01

    Full Text Available Purpose: The objective of this experiment is to obtain the fine surface roughness that is required less final polishing process as well as shortest manufacturing lead time.Design/methodology/approach: the aluminum Alloy 5058, 6163 and 7075 are selected for the experiment on a high speed machine. The machine used for testing is namely Mold Maker 200&2500 which is the high precision machining center. Secondly, the study is emphasizes on the suitable cutting tool and cutting parameters. Accurate surface roughness measured level is an important factor for injection mold making. This section explains the process of surface roughness measurement on the machine, namely MarSurf XCR 20 V1.20-4.Findings: The investigations are shown that the Aluminum graded Al 6163 and Al 7075 can be suitably used for the sport sole mold making in or to obtain the acceptable surface roughness without polishingPractical implications: The method can be adapted for all global shapes of tools, even in the case of complex geometriesOriginality/value: The investigations are shown that the Aluminum Al 6163 and Al 7075 can extremely save machining and polishing time.

  15. The corrosion protection of AA2024-T3 aluminium alloy by leaching of lithium-containing salts from organic coatings.

    Science.gov (United States)

    Visser, Peter; Liu, Yanwen; Zhou, Xiaorong; Hashimoto, Teruo; Thompson, George E; Lyon, Stuart B; van der Ven, Leendert G J; Mol, Arjan J M C; Terryn, Herman A

    2015-01-01

    Lithium carbonate and lithium oxalate were incorporated as leachable corrosion inhibitors in model organic coatings for the protection of AA2024-T3. The coated samples were artificially damaged with a scribe. It was found that the lithium-salts are able to leach from the organic coating and form a protective layer in the scribe on AA2024-T3 under neutral salt spray conditions. The present paper shows the first observation and analysis of these corrosion protective layers, generated from lithium-salt loaded organic coatings. The scribed areas were examined by scanning and transmission electron microscopy before and after neutral salt spray exposure (ASTM-B117). The protective layers typically consist of three different layered regions, including a relatively dense layer near the alloy substrate, a porous middle layer and a flake-shaped outer layer, with lithium uniformly distributed throughout all three layers. Scanning electron microscopy and white light interferometry surface roughness measurements demonstrate that the formation of the layer occurs rapidly and, therefore provides an effective inhibition mechanism. Based on the observation of this work, a mechanism is proposed for the formation of these protective layers.

  16. EFFECT OF TOOL PIN PROFILES AND HEAT TREATMENT PROCESS IN THE FRICTION STIR WELDING OF AA 6061 ALUMINIUM ALLOY

    Directory of Open Access Journals (Sweden)

    P.Prasanna

    2013-01-01

    Full Text Available Friction stir linear welding (FSLW uses a non consumable tool to generate frictional heat in the abutting surfaces. The welding parameters such as rotational speed, welding speed, axial force, tool tilt angle, etc., and tool pin profiles play a major role in deciding the joint properties. In this paper, an attempt has been made to study the effect of four different tool pin profiles on mechanical properties of AA 6061 aluminum alloy. Four different profiles have been used to fabricate the butt joints by keeping constant process parameters of tool rotational speed 1200RPM, welding speed 14mm/min and an axial force 7kN. Different heat treatment methods like annealing, normalizing and quenching have been applied on the joints and evaluation of the mechanical properties like tensile strength, percentage of elongation, hardness and microstructure in the friction stirring formation zone are evaluated. From this investigation, it is found that the hexagonal tool profile produces good tensile strength, percent of elongation in annealing and hardness in quenching process.

  17. Relation between feeding mechanisms and solidification mode in 380 aluminium alloy with different iron contents; Relacion entre los mecanismos de alimentacion y el modo de solidificacion en una aleacion de aluminio 380 con distintos contenidos de hierro

    Energy Technology Data Exchange (ETDEWEB)

    Tovio, D. O.; Gonzalez, A.C.; Mugica, G. W.; Cuyas, J. C.

    2003-07-01

    In the present work the effect of iron (0.15, 0.42 and 0.86%) content in feeding mechanisms for 380 aluminium alloy has been studied. The feeding capacity has been evaluated by a device that produces a barrier removable to allowing the movement of the inter dendritic liquid. The results show the flow of different quantity of liquid, it depends of the temperature of operating the device and of the iron content. For minimum and maximum iron content, the inter dendritic and bursts feeding mechanisms are fundamentally involved, for 0.42% of iron the feeding mechanisms was the inter dendritic. The authors establish this behavior by the solidification mode of alloy, which promotes the presence of particles of Si or plates of b-Al{sub 3}FeDi phase, in the inter dendritic channels and produce the different feeding mechanisms. (Author) 15 refs.

  18. Experimental study to analyse the workpiece surface temperature in deep hole drilling of aluminium alloy engine blocks using MQL technology

    Directory of Open Access Journals (Sweden)

    A.J. Filipovic

    2008-12-01

    Full Text Available Purpose: The objective of this applied research is to investigate the MQL deep hole drilling method, in orderto increase productivity and replace the current method of drilling main oil gallery holes in aluminum alloycylinder blocks that uses MWFs.Design/methodology/approach: The experimentation was performed at the Guhring, Inc. (a tool manufacturingcompany in Germany. The MQL drilling machine, machine operators, CNC programming, hole drilling, andtool layouts were be provided by Guhring. The main components of this experiment were the MQL machinewith dual channel system, machine tool fixture, special carbide drills, data acquisition system, thermal opticalcamera to measure surface temperature, and computers. The surface along the axis of the of the oil gallery holewas milled to produce uniform thickness of 2.5 mm. The drill was spinning but not moving into the engineblock, the engine block was moving into the drill. All experiments were performed in random order with noreplications. The other output variables, surface finish, true position, roundness, straightness, diameter andmisalignment, were measured by a surface analyzer and coordinate measuring machine (CMM.Findings: Based on this research it can be concluded that MQL is a viable production solution for DHDin automotive cast aluminum alloy. Good part quality characteristics were achieved using this method withproduction feeds and speeds.Practical implications: The MQL method has shown potential to be even more productive as compared totraditional deep hole drilling which would result in less capital investment.Originality/value: Good part quality characteristics were achieved using this method with production feeds and speeds.

  19. Evaluating the Applicability of GTN Damage Model in Forward Tube Spinning of Aluminum Alloy

    OpenAIRE

    Xianxian Wang; Mei Zhan; Jing Guo; Bin Zhao

    2016-01-01

    Tube spinning is an effective plastic-forming technology for forming light-weight, high-precision and high-reliability components in high-tech fields, such as aviation and aerospace. However, cracks commonly occur in tube spinning due to the complexity of stress state, which severely restricts the improvement of the forming quality and forming limit of components. In this study, a finite element (FE) model coupled with Gurson-Tvergaard-Needleman (GTN) damage model for forward tube spinning of...

  20. Hydrogen diffusion into fatigue cracks of aluminium alloy 6013 in a corrosive environment; Wasserstoffeinlagerung an Ermuedungsrissen der Aluminiumlegierung 6013 unter korrosiver Umgebung

    Energy Technology Data Exchange (ETDEWEB)

    Lenk, Christian Alexander

    2009-08-13

    The author attempted a time-resolved detection of raised hydrogen concentrations in the plastic deformation region of fatigue cracks in an aluminium test piece deformed by cyclic stress in a corrosive environment. Mechanical material parameters like the crack propagation velocity under cyclic stress change dramatically in a corrosive environment. This is assumed to be caused by hydrogen diffusion, but so far there is no method that reliably measures additional hydrogen from the corrosive environment. For this reason, a special analytical configuration was set up which makes use of the thermal desorption method. First, chips with a thickness of about 20 micrometers are sawed out of the test specimen in high-vacuum conditions. The chips fall into a hot melting vessel in a UHV chamber, where the hydrogen contained in the chips is released. The resulting pressure increase is recorded by a mass spectrometer. A hydrogen profile of the test specimen is obtained by assigning the chip position to the signal. For the corrosive medium in which the test specimen is immersed during crack initiation, i.e. NaCl solution, heavy water was used. This makes it possible to distinguish between the hydrogen contained in a piece of technical aluminium alloy (AA6013) and the deuterium diffusing in from the corrosive fluid. The deuterium is found exclusively in the test piece volume in the strongly plastically deformed region surrounding the fatigue crack. (orig.) [German] Das Ziel der vorliegenden Arbeit besteht im ortsaufgeloesten Nachweis einer erhoehten Wasserstoffkonzentration im plastisch deformierten Bereich von Ermuedungsrissen einer unter korrosiver Umgebung zyklisch verformten Aluminiumprobe. Mechanische Materialparameter wie z.B. die Rissausbreitungsgeschwindigkeit unter zyklischer Belastung aendern sich drastisch in korrosiver Umgebung. Als Ursache fuer dieses Verhalten wird eine Eindiffusion von Wasserstoff vermutet, jedoch gibt es bisher keine Messung die den zusaetzlichen

  1. Preparation of Wax-Emulsion Releasing Agent for Aluminium Alloy Die Casting%一种铝合金压铸蜡乳液脱模剂的研制

    Institute of Scientific and Technical Information of China (English)

    吴国江; 曹桂芝; 江敏

    2014-01-01

    研究了用氧化聚乙烯蜡、58#全炼蜡制备铝合金压铸蜡乳液脱模剂的方法。考查了乳化剂类型、乳化剂用量、乳化工艺对乳液稳定性的影响。实验结果表明,当复合乳化剂用量为复合蜡的30%,乳化温度为95℃,搅拌速度为500~700 r/min时,乳化时间为40~45 min,可以制取一种稳定的用于铝合金压铸蜡乳液脱模剂。%A preparation method of wax-emulsion releasing agent for aluminium alloy die casting from oxidized polyethylene wax and 58# fully refined paraffin wax was studied. Effects of emulsifier type, emulsifier dosage and emulsifying process on the emulsion stability were studied. The results show that, when the compounded emulsifier dosage is 30%of the mixed wax mass, the emulsifying-temperature is 95℃, the stirring speed is between 500~700 r/min, the emulsifying time is between 40~45min, stable wax-emulsion releasing agent for aluminium alloy die casting can be prepared.

  2. Fatigue of thin walled tubes in copper alloy CuNi10

    DEFF Research Database (Denmark)

    Lambertsen, Søren Heide; Damkilde, Lars; Jepsen, Michael S.

    2016-01-01

    The current work concerns the investigation of the fatigue resistance of CuNi10 tubes, which are frequently used in heat exchangers of large ship engines. The lifetime performances of the exchanger tubes are greatly affected by the environmental conditions, where especially the temperature fluctu...

  3. Enhanced corrosion protection by microstructural control of aluminium brazing sheet

    NARCIS (Netherlands)

    Norouzi Afshar, F.

    2013-01-01

    Aluminium brazing sheet is a sandwich material made out of two aluminium alloys (AA4xxx/AA3xxx) and is widely used in automotive heat exchangers. One of the main performance criteria for heat exchanger units is the lifetime of the product. The lifetime of the heat exchanger units is determined by th

  4. Replacement of alloy 600 by alloy 690 for steam generator tubes and closure heads in PWR; Gains apportes par le changement de materiau dans les generateurs de vapeur et les couvercles de cuve des REP: passage de l'alliage 600 a l'alliage 690

    Energy Technology Data Exchange (ETDEWEB)

    Bioulac, M.; Cipiere, M.F.; Poudroux, G. [FRAMATOME ANP, 92 - Paris-La-Defence (France); Champigny, F.; Mercier, L.; Rouillon, Y.; Vaillant, F. [Electricite de France (EDF), 75 - Paris (France)

    2004-07-01

    The replacement of alloy 600 by alloy 690 for steam generator tubes, tube plugs and closure head penetrations has well fulfilled its expectation concerning resistance to stress corrosion. The first steam generators fitted with tubes in alloy 690 have been operating for 14 years, the first plugs were set more than 20 years ago and the first closure head equipped with adapters in alloy 690 was installed in 1993. The feedback experience on non-destructive testing for these 3 components have shown no cracks. As a consequence the maintenance program has been reduced. A majority of nuclear power plant operators throughout the world have also selected the alloy 690. (A.C.)

  5. Effects of Process Conditions on the Mechanical Behavior of Aluminium Wrought Alloy EN AW-2219 (AlCu6Mn Additively Manufactured by Laser Beam Melting in Powder Bed

    Directory of Open Access Journals (Sweden)

    Michael Cornelius Hermann Karg

    2017-01-01

    Full Text Available Additive manufacturing is especially suitable for complex-shaped 3D parts with integrated and optimized functionality realized by filigree geometries. Such designs benefit from low safety factors in mechanical layout. This demands ductile materials that reduce stress peaks by predictable plastic deformation instead of failure. Al–Cu wrought alloys are established materials meeting this requirement. Additionally, they provide high specific strengths. As the designation “Wrought Alloys” implies, they are intended for manufacturing by hot or cold working. When cast or welded, they are prone to solidification cracks. Al–Si fillers can alleviate this, but impair ductility. Being closely related to welding, Laser Beam Melting in Powder Bed (LBM of Al–Cu wrought alloys like EN AW-2219 can be considered challenging. In LBM of aluminium alloys, only easily-weldable Al–Si casting alloys have succeeded commercially today. This article discusses the influences of boundary conditions during LBM of EN AW-2219 on sample porosity and tensile test results, supported by metallographic microsections and fractography. Load direction was varied relative to LBM build-up direction. T6 heat treatment was applied to half of the samples. Pronounced anisotropy was observed. Remarkably, elongation at break of T6 specimens loaded along the build-up direction exceeded the values from literature for conventionally manufactured EN AW-2219 by a factor of two.

  6. Experimental residual stress evaluation of hydraulic expansion transitions in Alloy 690 steam generator tubing

    Energy Technology Data Exchange (ETDEWEB)

    McGregor, R.; Doherty, P. [Babcock and Wilcox International, Cambridge, Ontario (Canada); Hornbach, D. [Lambda Research Inc., Cincinnati, OH (United States); Abdelsalam, U. [McMaster Univ., Hamilton, Ontario (Canada)

    1995-12-31

    Nuclear Steam Generator (SG) service reliability and longevity have been seriously affected worldwide by corrosion at the tube-to-tubesheet joint expansion. Current SG designs for new facilities and replacement projects enhance corrosion resistance through the use of advanced tubing materials and improved joint design and fabrication techniques. Here, transition zones of hydraulic expansions have undergone detailed experimental evaluation to define residual stress and cold-work distribution on and below the secondary-side surface. Using X-ray diffraction techniques, with supporting finite element analysis, variations are compared in tubing metallurgical condition, tube/pitch geometry, expansion pressure, and tube-to-hole clearance. Initial measurements to characterize the unexpanded tube reveal compressive stresses associated with a thin work-hardened layer on the outer surface of the tube. The gradient of cold-work was measured as 3% to 0% within .001 inch of the surface. The levels and character of residual stresses following hydraulic expansion are primarily dependent on this work-hardened surface layer and initial stress state that is unique to each tube fabrication process. Tensile stresses following expansion are less than 25% of the local yield stress and are found on the transition in a narrow circumferential band at the immediate tube surface (< .0002 inch/0.005 mm depth). The measurements otherwise indicate a predominance of compressive stresses on and below the secondary-side surface of the transition zone. Excellent resistance to SWSCC initiation is offered by the low levels of tensile stress and cold-work. Propagation of any possible cracking would be deterred by the compressive stress field that surrounds this small volume of tensile material.

  7. Aluminium in human sweat.

    Science.gov (United States)

    Minshall, Clare; Nadal, Jodie; Exley, Christopher

    2014-01-01

    It is of burgeoning importance that the human body burden of aluminium is understood and is measured. There are surprisingly few data to describe human excretion of systemic aluminium and almost no reliable data which relate to aluminium in sweat. We have measured the aluminium content of sweat in 20 healthy volunteers following mild exercise. The concentration of aluminium ranged from 329 to 5329μg/L. These data equate to a daily excretion of between 234 and 7192μg aluminium and they strongly suggest that perspiration is the major route of excretion of systemic aluminium in humans.

  8. Severity of the Bend and Its Effect on the Subsequent Hydroforming Process for Aluminum Alloy Tube

    Science.gov (United States)

    Gholipour, J.; Worswick, M. J.; Oliveira, D. A.; Khodayari, G.

    2004-06-01

    The interaction between pre-bending and subsequent hydroforming of AlMg3.5Mn aluminum tubes is examined in this paper. Pre-bending induces large strains and strain gradients in the tube, which reduce the available formability for the subsequent hydroforming process. Corner fill hydroforming operations were performed on straight tubes (R/D=∞) and pre-bent tubes with R/D=2.5, representing a transition from low severity to moderate severity bending conditions. An Eagle EPT-75 instrumented mandrel-rotary draw tube bender was used for the pre-bending stage, which records all process parameters. The experiments were modeled using an explicit dynamic finite element code, LS-DYNA. An in-house Gurson-Tvergaard-Needleman (GTN) constitutive softening model, incorporated within LS-DYNA, has been considered to predict damage and formability. Based on these results, the formability of a tube bent at an R/D=2.0 is predicted as a higher severity bend condition.

  9. Study on vibration fatigue damage due to the blow of OPGW aluminum tube; OPGW aluminium kan no kyofu ni yoru shindo hiro hason ni kansuru kenkyu

    Energy Technology Data Exchange (ETDEWEB)

    Aikawa, S.; Kohara, H. [Chugoku Electric Power Co. Inc., Hiroshima (Japan)

    2000-03-24

    The cause of damage in the cashing portion of an aluminum tube incorporating OPGW (OPAC 120mm{sup 2}) was investigated and proper measures for the prevention of recurrence were examined. The investigation result of the past accident of the same kind or the result of stress measurement showed that the cause of aluminum tube damage is the fatigue rupture based on the repeated stress occurring by the rolling of OPGW. Moreover, it was known that the attached wire in a jumper lead-in system is most effective and valid as preventative measures of damage. (translated by NEDO)

  10. Inspection of ferromagnetic support structures from within alloy 800 steam generator tubes using pulsed eddy current

    Science.gov (United States)

    Buck, Jeremy Andrew

    Nondestructive testing is a critical aspect of component lifetime management. Nuclear steam generator (SG) tubes are the thinnest barrier between irradiated primary heat transport system and the secondary heat transport system, whose components are not rated for large radiation fields. Conventional eddy current testing (ECT) and ultrasonic testing are currently employed for inspecting SG tubes, with the former doing most inspections due to speed and reliability based on an understanding of how flaws affect coil impedance parameters when conductors are subjected to harmonically induced currents. However, when multiple degradation modes are present simultaneously near ferromagnetic materials, such as tube fretting, support structure corrosion, and magnetite fouling, ECT reliability decreases. Pulsed eddy current (PEC), which induces transient eddy currents via square wave excitation, has been considered in this thesis to simultaneously examine SG tube and support structure conditions. An array probe consisting of a central driver, coaxial with the tube, and an array of 8 sensing coils, was used in this thesis to perform laboratory measurements. The probe was delivered from the inner diameter (ID) of the SG tube, where support hole diameter, tube frets, and 2D off-centering were varied. When considering two variables simultaneously, scores obtained from a modified principal components analysis (MPCA) were sufficient for parameter extraction. In the case of hole ID variation with two dimensional tube off-centering (three parameters), multiple linear regression (MLR) of the MPCA scores provided good estimates of parameters. However, once a fourth variable, outer diameter tube frets, was introduced, MLR proved insufficient. Artificial neural networks (ANNs) were investigated in order to perform pattern recognition on the MPCA scores to simultaneously extract the four measurement parameters from the data. All models throughout this thesis were created and validated using

  11. Circular economy: To be or not to be in a closed product loop? A Life Cycle Assessment of aluminium cans with inclusion of alloying elements

    DEFF Research Database (Denmark)

    Niero, Monia; Olsen, Stig Irving

    2016-01-01

    economy implementation the key actions are: to reduce the weight of the lid, to develop methods to separate the body and lid at the point of collection, and to investigate the potentials of a closed supply chain loop for aluminium cans in terms of combined environmental and economic value creation....... recycling scenario using mixed Al packaging scrap. The main recommendation from an LCA methodological point of view is to include the idea of multiple co-functions in the functional unit definition. To further improve the environmental performances of the aluminium beverage can sector towards circular...

  12. Study on Cold Metal Transfer(CMT)Welding of Aluminium Alloy Sheet with Space Curve Weld%薄板铝合金空间曲线焊缝CMT焊接试验研究

    Institute of Scientific and Technical Information of China (English)

    田志杰; 熊林玉; 李延民; 周庆; 杜岩峰; 李鸣钺

    2015-01-01

    针对薄板铝合金三维曲线焊缝较大的残余应力和焊接变形,进行了冷金属过渡(CMT)无垫板自动焊试验研究,分析了电流、焊接速度、弧长修正、保护气流量对焊接过程的影响,进行了接头拉伸性能试验及焊缝微观组织研究,并焊接了变形小的产品。结果表明,利用合理的焊接参数,可实现厚度1.5 mm的5 A06铝合金的无垫板CMT焊接,焊缝成形稳定均匀,焊接接头抗拉强度值达到347 MPa,接头断裂位置在热影响区。无垫板CMT焊接技术可用于薄板铝合金空间曲线焊缝的焊接。%For the higher residual stress and distortion of aluminium alloy sheet with three-dimensional curve weld,no-liner plate auto-welding was studied.The effect of current,speed,arc voltage,gas flux were investigated.The tensile performance and microstructure of joint were determined.The product with little weld distortion was manufactured.The results show that 1 .5 mm thick 5 A06 aluminium alloy three-dimen-sional curve weld can be achieved by reasonable no-liner plate CMT parameters.The weld shape is stable and uniform,tensile strength reached 347 MPa,fracture occurred in HAZ.No-liner plate CMT welding technology can be used in space curve welding for the aluminium alloy sheet.

  13. IEC 61267: Feasibility of type 1100 aluminium and a copper/aluminium combination for RQA beam qualities.

    Science.gov (United States)

    Leong, David L; Rainford, Louise; Zhao, Wei; Brennan, Patrick C

    2016-01-01

    In the course of performance acceptance testing, benchmarking or quality control of X-ray imaging systems, it is sometimes necessary to harden the X-ray beam spectrum. IEC 61267 specifies materials and methods to accomplish beam hardening and, unfortunately, requires the use of 99.9% pure aluminium (Alloy 1190) for the RQA beam quality, which is expensive and difficult to obtain. Less expensive and more readily available filters, such as Alloy 1100 (99.0% pure) aluminium and copper/aluminium combinations, have been used clinically to produce RQA series without rigorous scientific investigation to support their use. In this paper, simulation and experimental methods are developed to determine the differences in beam quality using Alloy 1190 and Alloy 1100. Additional simulation investigated copper/aluminium combinations to produce RQA5 and outputs from this simulation are verified with laboratory tests using different filter samples. The results of the study demonstrate that although Alloy 1100 produces a harder beam spectrum compared to Alloy 1190, it is a reasonable substitute. A combination filter of 0.5 mm copper and 2 mm aluminium produced a spectrum closer to that of Alloy 1190 than Alloy 1100 with the added benefits of lower exposures and lower batch variability.

  14. Influence of energy input in friction stir welding on structure evolution and mechanical behaviour of precipitation-hardening in aluminium alloys (AA2024-T351, AA6013-T6 and Al-Mg-Sc)

    Energy Technology Data Exchange (ETDEWEB)

    Weis Olea, Cesar Afonso [GKSS-Forschungszentrum Geesthacht GmbH (Germany). Inst. fuer Werkstofforschung

    2008-12-04

    Aluminium alloys AA2024 T351, AA6013 T6 and the recently developed Al-Mg-Sc for aircraft industry applications, which are usually considered difficult to weld by conventional fusion welding processes, demonstrate outstanding performance when joined by friction stir welding (FSW). The main feature of the process is to produce solid-state welds, where the maximum temperatures attained during the process are about 80 % that of the melting temperature of the base material. The process generates substantial plastic deformation, due to the solid-state stirring, and consequently creates a high dislocation density, which is a precursor to dynamic recrystallization, a metallurgical feature that characterizes the stir zone (weld centre). A relevant aspect considered, regarding precipitation-hardening aluminium alloys, is the deterioration of the mechanical properties in the weld zones, which are fundamentally attributed to changes in the characteristics of strengthening precipitates. Among the strengthening mechanisms acting in these aluminium alloys, the most important is basically dependent on the morphology, size and population of the precipitates. The thermal cycle and deformation generated during the FSW process alter the precipitation characteristics previously present in the base material. FSW input energy regulates the magnitude of the thermal cycle and the intensity of deformation taking place during the process, and it can be controlled by the welding parameters, affecting the precipitates evolution and consequently the mechanical properties of the joint. Nevertheless, there remains a lack of knowledge about the substructural evolution of these alloys during FSW, and its correlation with weld energy input and their respective mechanical properties, particularly for the Al-Mg-Sc alloy. The main objective of this work is to explain the micro and substructural evolution (emphasizing precipitates evolution) of AA2024- T351, AA6013-T6 and Al-Mg-Sc alloys in similar

  15. Influence of energy input in friction stir welding on structure evolution and mechanical behaviour of precipitation-hardening in aluminium alloys (AA2024-T351, AA6013-T6 and Al-Mg-Sc)

    Energy Technology Data Exchange (ETDEWEB)

    Weis Olea, Cesar Afonso [GKSS-Forschungszentrum Geesthacht GmbH (Germany). Inst. fuer Werkstofforschung

    2008-12-04

    Aluminium alloys AA2024 T351, AA6013 T6 and the recently developed Al-Mg-Sc for aircraft industry applications, which are usually considered difficult to weld by conventional fusion welding processes, demonstrate outstanding performance when joined by friction stir welding (FSW). The main feature of the process is to produce solid-state welds, where the maximum temperatures attained during the process are about 80 % that of the melting temperature of the base material. The process generates substantial plastic deformation, due to the solid-state stirring, and consequently creates a high dislocation density, which is a precursor to dynamic recrystallization, a metallurgical feature that characterizes the stir zone (weld centre). A relevant aspect considered, regarding precipitation-hardening aluminium alloys, is the deterioration of the mechanical properties in the weld zones, which are fundamentally attributed to changes in the characteristics of strengthening precipitates. Among the strengthening mechanisms acting in these aluminium alloys, the most important is basically dependent on the morphology, size and population of the precipitates. The thermal cycle and deformation generated during the FSW process alter the precipitation characteristics previously present in the base material. FSW input energy regulates the magnitude of the thermal cycle and the intensity of deformation taking place during the process, and it can be controlled by the welding parameters, affecting the precipitates evolution and consequently the mechanical properties of the joint. Nevertheless, there remains a lack of knowledge about the substructural evolution of these alloys during FSW, and its correlation with weld energy input and their respective mechanical properties, particularly for the Al-Mg-Sc alloy. The main objective of this work is to explain the micro and substructural evolution (emphasizing precipitates evolution) of AA2024- T351, AA6013-T6 and Al-Mg-Sc alloys in similar

  16. Corrosion issues of powder coated AA6060 aluminium profiles

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Valgarðsson, Smári; Jellesen, Morten Stendahl

    2015-01-01

    In this study detailed microstructural investigation of the reason for unexpected corrosion of powder coated aluminium alloy AA6060 windows profiles has been performed. The results from this study reveals that the failure of the window profiles was originated from the surface defects present...... on the extruded AA6060 aluminium profile after metallurgical process prior to powder coating. Surface defects are produced due to intermetallic particles in the alloy, which disturb the flow during the extrusion process. The corrosion mechanism leading to the failure of the powder coated AA6060 aluminium profiles...

  17. Earnings Increased 500 Million Yuan Thanks to the Rise of Export Tax Rebate for Aluminium and Copper Products

    Institute of Scientific and Technical Information of China (English)

    2009-01-01

    <正>In mid-November,the Ministry of Finance and the State Administration of Taxation issued a tax circular Notification on Raising Export Tax Rebate Rate of the Value-added Tax for Com- modities including Labor-intensive Products, raising the export tax rebate rate by 9% and 13% respectively for refined copper tubes with a outer diameter no more than 25mm and non- alloy aluminium products including rectangular plates,sheets and strips.This is the first time China has adjusted the export tax for nonfer- rous metal products.The adjustment will have a direct positive effect on improving the busi-

  18. Microstructurally Controlled Mechanical Properties of Al-Mg-Si Alloys for Warm Forming Applications

    NARCIS (Netherlands)

    Ghosh, M.

    2011-01-01

    Owing to their light weight and excellent corrosion resistance the use of aluminium alloys in automotive industries is increasing progressively. However, aluminium alloys remain mainly handicapped by poor room temperature formability compared to steel. Increasing temperature during forming, but stil

  19. Microstructure and corrosion performance of steam-based conversion coatings produced in the presence of TiO2 particles on aluminium alloys

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Gudla, Visweswara Chakravarthy; Jellesen, Morten Stendahl;

    2016-01-01

    The steam-based conversion coatings containing TiO2 particleswere prepared using a two-step process comprising of spin coating of particles onto an aluminiumsubstrate followed by a high-pressure steam treatment. Process has resulted in the formation of aluminium oxide layer (~1.3 μm thick) embedded...

  20. Effect of ageing on the mechanical behaviour of aluminium alloy AA2009 reinforced with SIC particles; Influencia del estado de envejecimiento en el comportamiento mecanico de una aleacion de aluminio AA2009 reforzada con particulas de SiC

    Energy Technology Data Exchange (ETDEWEB)

    Rodrigo, P.; Poza, P.; Utrilla, M. v.; Urena, A.

    2005-07-01

    A study of the mechanical behaviour of an aluminium matrix composite (AA2009) reinforced with 15 volume percent of SiC particles has been carried out. The ageing kinetic for this material has been evaluated at two different ageing temperatures (170 and 190 degree centigree). The hardness peaks for the two different precipitation sequences existing in the matrix alloy have been identified. The mechanical behaviour of the composite was also evaluated for the different thermal conditions (as-received and aged). This research has been completed with the identification of the fracture mechanisms by means of observation with scanning electron microscopy (SEM) both of the fracture surface and transversal sections of them. In addition, transmission electron microscopy (TEM) of the treated composites has been used to determine the influence of the SiC particles on the distribution of strengthening phases precipitated in the matrix. (Author) 14 refs.

  1. Human exposure to aluminium.

    Science.gov (United States)

    Exley, Christopher

    2013-10-01

    Human activities have circumvented the efficient geochemical cycling of aluminium within the lithosphere and therewith opened a door, which was previously only ajar, onto the biotic cycle to instigate and promote the accumulation of aluminium in biota and especially humans. Neither these relatively recent activities nor the entry of aluminium into the living cycle are showing any signs of abating and it is thus now imperative that we understand as fully as possible how humans are exposed to aluminium and the future consequences of a burgeoning exposure and body burden. The aluminium age is upon us and there is now an urgent need to understand how to live safely and effectively with aluminium.

  2. HEAT-UP AND COOL-DOWN TEMPERATURE-DEPENDENT HYDRIDE REORIENTATION BEHAVIORS IN ZIRCONIUM ALLOY CLADDING TUBES

    Directory of Open Access Journals (Sweden)

    JU-JIN WON

    2014-10-01

    Full Text Available Hydride reorientation behaviors of PWR cladding tubes under typical interim dry storage conditions were investigated with the use of as-received 250 and 485ppm hydrogen-charged Zr-Nb alloy cladding tubes. In order to evaluate the effect of typical cool-down processes on the radial hydride precipitation, two terminal heat-up temperatures of 300 and 400°C, as well as two terminal cool-down temperatures of 200 and 300°C, were considered. In addition, two cooling rates of 2.5 and 8.0°C/min during the cool-down processes were taken into account along with zero stress or a tensile hoop stress of 150MPa. It was found that the 250ppm hydrogen-charged specimen experiencing the higher terminal heat-up temperature and the lower terminal cool-down temperature generated the highest number of radial hydrides during the cool-down process under 150MPa hoop tensile stress, which may be explained by terminal solid hydrogen solubilities for precipitation, and dissolution and remaining circumferential hydrides at the terminal heat-up temperatures. In addition, the slower cool-down rate generates the larger number of radial hydrides due to a cooling rate-dependent, longer residence time at a relatively high temperature that can accelerate the radial hydride nucleation and growth.

  3. Effect of Aluminium Addition on Glass Forming Ability of Nd55-xAl10+xFe15Co20 (x=0, 5, 10) Alloys

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    Nd55-xAl10+xCo20Fe15 (x=0, 5, 10) bulk glass-forming alloys with distinct glass transition in differential scanning calorimetry (DSC) traces were obtained by suction casting. The glass forming ability (GFA) of the alloys was investigated. It was found that the reduced glass transition temperature (Trg) and the parameter γ of the alloys increased with the increasing concentration of Al. The glass formation enthalpy of the alloys was calculated based on Miedema′s model, and it was suggested that the GFA of the alloys could be enhanced by the decrease of the glass formation enthalpy with Al additions.

  4. 焊接修复汽轮发电机转子铝合金叶片接头强度校核%Strength Checking for Welded Joint of Aluminium Alloy Blade Used in Turbo Generator

    Institute of Scientific and Technical Information of China (English)

    张乔斌; 熊征

    2011-01-01

    为了评估焊接修复汽轮发电机转子铝合金叶片接头强度的可靠性,基于空气动力学理论,分析和计算了由离心力与空气升力在旋转运动叶片TIG焊接接头上产生的拉伸应力,并进行强度校核.强度校核表明,用SalSi-1铝合金焊丝形成的焊接接头安全许用应力大于接头受到的拉伸应力,焊接接头安全可靠.本分析方法为旋转体焊接接头强度校核提供了一定理论基础.%For assessing the safety of welded joint of aluminium alloy blade used in turbo generator, the tensile stress of welded joint caused by centrifugal force and air lift acting rotation blade was calculated according to the basic theories of the aerodynamicist. Based on the results, the tensile strength of the welded joint by TIG is conducted by strength checking. The permissible stress of TIG joint welded with SAISi-1 aluminium alloy wire is larger than the bearable stress in the welded zone. The repaired blade is safe. The analysis method provides some theories foundation for the safe assessment on welded joint strength in rotation blade.

  5. Surface Powder Technology of Aluminium Alloy Based of Communication Filter Module%通信滤波器铝基模块表面喷粉工艺研究

    Institute of Scientific and Technical Information of China (English)

    王小青; 吴道琴

    2013-01-01

    In order to improve the corrosion resistance of the wrought aluminium alloy (6061) and die casting aluminium alloy (YL102 ) for the base of communication filter module, powder was sprayed on its surface. The effect of coating type, module structure, treatment process (module pre-processing, baking) on the film-forming corrosion resistance was studied. The results show that: the reasonable choice of different coating, proper rounding, narrow groove depth to width ratio and hole depth and the aperture ratio not greater than 3, special function of surface transition processing, reasonable arrangements for powder processing technology can improve corrosion resistance of powder sprayed film-forming.%为了提高以变形铝合金(6061)和压铸铝合金(YL102)为基材的通信滤波器模块的防腐蚀能力,在其表面进行喷粉处理,研究了涂料类型、模块结构、处理工艺(模块前处理、喷涂烘烤)对成膜耐蚀性能的影响.结果表明:针对不同基材选择涂料,适当的圆角过渡,窄槽的深宽比和孔深/孔径比不大于3,特殊的功能表面进行过渡处理,合理地安排喷粉处理工艺,均有利于提高喷粉层的防腐蚀能力.

  6. Prediction of Burst Pressure in Multistage Tube Hydroforming of Aerospace Alloys.

    Science.gov (United States)

    Saboori, M; Gholipour, J; Champliaud, H; Wanjara, P; Gakwaya, A; Savoie, J

    2016-08-01

    Bursting, an irreversible failure in tube hydroforming (THF), results mainly from the local plastic instabilities that occur when the biaxial stresses imparted during the process exceed the forming limit strains of the material. To predict the burst pressure, Oyan's and Brozzo's decoupled ductile fracture criteria (DFC) were implemented as user material models in a dynamic nonlinear commercial 3D finite-element (FE) software, ls-dyna. THF of a round to V-shape was selected as a generic representative of an aerospace component for the FE simulations and experimental trials. To validate the simulation results, THF experiments up to bursting were carried out using Inconel 718 (IN 718) tubes with a thickness of 0.9 mm to measure the internal pressures during the process. When comparing the experimental and simulation results, the burst pressure predicated based on Oyane's decoupled damage criterion was found to agree better with the measured data for IN 718 than Brozzo's fracture criterion.

  7. Effects of geometrical parameters on wrinkling of thin-walled rectangular aluminum alloy wave-guide tubes in rotary-draw bending

    Institute of Scientific and Technical Information of China (English)

    Tian Shan; Liu Yuli; Yang He

    2013-01-01

    Inner flange and side wrinkling often occur in rotary-draw bending process of rectangular aluminum alloy wave-guide tubes,and the distribution and magnitude of wrinkling is related to geometrical parameters of the tubes.In order to study the effects of geometrical parameters on wrinkling of rectangular wave-guide tubes,a 3D-FE model for rotary-draw bending processes of thin-walled rectangular aluminum alloy wave-guide tubes was built based on the platform of ABAQUS/Explicit,and its reliability was validated by experiments.Simulation and analysis of the influence laws of geometrical parameters on the wave heights of inner flange and side wrinkling were then carried out.The results show that inner flange wrinkling is the main wrinkling way to rectangular wave-guide tubes in rotary-draw bending processes,but side wrinkling cannot be neglected because side wrinkling is 2/3 of inner flange wrinkling when b and h are smaller.Inner flange and side wrinkling increase with increasing b and h; the influence of b on side wrinkling is larger than that of h,while both b and h affect inner flange wrinkling greatly.Inner flange and side wrinkling decrease with increasing R/h; the influence of h on inner flange and side wrinkling is larger than that of R.

  8. Application of Anodization Process for Cast Aluminium Surface Properties Enhancement

    Directory of Open Access Journals (Sweden)

    Włodarczyk-Fligier A.

    2016-09-01

    Full Text Available An huge interest is observed in last years in metal matrix composite, mostly light metal based, which have found their applications in many industry branches, among others in the aircraft industry, automotive-, and armaments ones, as well as in electrical engineering and electronics, where one of the most important issue is related to the corrosion resistance, especially on the surface layer of the used aluminium alloys. This elaboration presents the influence of ceramic phase on the corrosion resistance, quality of the surface layer its thickness and structure of an anodic layer formed on aluminium alloys. As test materials it was applied the aluminium alloys Al-Si-Cu and Al-Cu-Mg, for which heat treatment processes and corrosion tests were carried out. It was presented herein grindability test results and metallographic examination, as well. Hardness of the treated alloys with those ones subjected to corrosion process were compared.

  9. 镍钛形状记忆合金管材的研究进展%Recent research of nickel-titanium shape memory alloy tube

    Institute of Scientific and Technical Information of China (English)

    陆鹏; 赵亚楠; 张艳秋; 江树勇

    2013-01-01

      Nickel-Titanium shape memory alloy tube is widely applied in the engineering fields because of excellent shape memory effect and perfect superelasticity. In this paper, according to the scientific achievements of domestic and overseas researchers, Nickel-Titanium shape memory alloy tube is systematically introduced in terms of mechanical behavior, plastic deformation and typical engineering application. Nickel-Titanium shape memory alloy tube exhibits different mechanical behaviors in the cases of uniaxial tension loading, uniaxial torsion loading as well as combined tension and torsion loading. Stress-induced martensitic bands are observed on austenitic Nickel-Titanium shape memory alloy tube which is subjected to uniaxial tension loading. Nickel-Titanium shape memory alloy tube is mainly manufactured by means of plastic deformation methods, such as drawing, extrusion and spinning. Drawing remains the main approach to producing Nickel-Titanium shape memory alloy tube. Nickel-Titanium shape memory alloy tube is typically applied to biomedical stent and pipe couplings in the engineering fields. Nickel-Titanium shape memory alloy tube remains a promising candidate for scientific research and engineering application.%  镍钛形状记忆合金管材因为具有良好的形状记忆效应和超弹性而在工程领域得到了广泛的应用。文章总结了国内外众多学者的研究成果,系统介绍了镍钛形状记忆合金管材的加载力学行为、塑性成形方法和典型工程应用。镍钛形状记忆合金管材在单向拉伸加载、单向扭转加载以及拉伸扭转复合加载方式下表现出了不同的力学行为。奥氏体镍钛形状记忆合金管材在单向拉伸加载下,可以观察到明显的应力诱发马氏体螺旋带。镍钛形状记忆合金管材的塑性成形方法主要有拉拔、挤压和旋压,拉拔工艺仍是目前生产镍钛形状记忆合金管材的主要手段。镍钛形状记忆合金

  10. PWSCC susceptibility evaluation of mill annealed Alloy 600 SG tubings using mock-up specimens in lithium enhanced 360 C water

    Energy Technology Data Exchange (ETDEWEB)

    Tsuruta, T.; Okamoto, S.; Kitera, T. [Mitsubishi Heavy Industries, Ltd., Takasago (Japan); Takamatsu, H.; Matsunaga, T. [Kansai Electric Power Co., Inc., Osaka (Japan)

    1995-12-31

    Intergranular stress corrosion cracking (IGSCC) behavior of Alloy 600 steam generator (SG) tubing in pressurized water reactor (PWR) primary water environments, or so called PWSCC, has been investigated since the first report by Coriou in 1959. The acceleration of PWSCC by elevating the test temperature up to 365 C, was first reported in 1980 by Bulischeck et al.. Since then, many results of PWSCC phenomena have been reported. It is important for preventive maintenance planning, to predict the life expectation at the operating temperature for a specific structural design. PWSCC susceptibility of mill annealed alloy 600 (MA 600) SG tubing was investigated using mock-up specimens, such as tube sheet expansion specimens and dent shape deformed specimens in lithium enhanced 360 C water (500ppm as B, 20ppm as Li, 45ccH{sub 2}/kgH{sub 2}O). Uniaxial constant load (UCL) tests were carried out for MA 600, thermally treated (TT) Alloy 600, and TT 690 to evaluate the effect of stress, and to evaluate the acceleration factor of the environment compared with the results in normal 360 C reactor coolant system (RCS) water (500ppm as B, 2ppm as Li, 30ccH{sub 2}/kgH{sub 2}O).

  11. Microstructure and corrosion performance of steam-based conversion coatings produced in the presence of TiO2 particles on aluminium alloys

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Gudla, Visweswara Chakravarthy; Jellesen, Morten Stendahl

    2016-01-01

    The steam-based conversion coatings containing TiO2 particleswere prepared using a two-step process comprising of spin coating of particles onto an aluminiumsubstrate followed by a high-pressure steam treatment. Process has resulted in the formation of aluminium oxide layer (~1.3 μm thick) embedded...... to the coatings without TiO2 particles, while the shift in thepitting potential was a function of the steam treatment time and degree of particle incorporation into the oxide....

  12. Durability of Lacquered Aluminium Profile Considering Tropical Weather Conditions

    Directory of Open Access Journals (Sweden)

    Rigoberto Marrero Águila

    2013-11-01

    Full Text Available Searching for solutions against the degradation of materials by corrosion effect, is a common practice to use alloys such as aluminium instead of steel due to the advantages obtained. The lacquered aluminium profiles can substitute other materials like wood, in the carpentry production, becoming an economic saving. There is an increasingly use of aluminium replacing other traditional materials in the constructions in process, but its quality has been reduced in a considerable amount of installations. In this research, aluminium profiles from five different sources were submitted to a trial in natural exposition conditions at the Tropical weather condition Testing Lab, in order to evaluate their behaviour and establish, for the first time in our country, standing rules for lacquered aluminium profiles to be strictly fulfilled by manufacturers and importers. The results will allow modifying thickness standards of this type of coating, to guaranty its durability and to eliminate the failures provoked by our high severe weather conditions.

  13. Experimental investigations on mechanical behavior of aluminium metal matrix composites

    Science.gov (United States)

    Rajesh, A. M.; Kaleemulla, Mohammed

    2016-09-01

    Today we are widely using aluminium based metal matrix composite for structural, aerospace, marine and automobile applications for its light weight, high strength and low production cost. The purpose of designing metal matrix composite is to add the desirable attributes of metals and ceramics to the base metal. In this study we developed aluminium metal matrix hybrid composite by reinforced Aluminium7075 alloy with silicon carbide (SiC) and aluminium oxide (alumina) by method of stir casting. This technique is less expensive and very effective. The Hardness test and Wear test were performed on the specimens which are prepared by stir casting techniques. The result reveals that the addition of silicon carbide and alumina particles in aluminium matrix improves the mechanical properties.

  14. Effects of Rolling Reduction and Strength of Composed Layers on Bond Strength of Pure Copper and Aluminium Alloy Clad Sheets Fabricated by Cold Roll Bonding

    Directory of Open Access Journals (Sweden)

    Yoji Miyajima

    2014-01-01

    Full Text Available Three types of clad sheets, Cu/Al, Cu/AA5052, and Cu/AA5083, were produced by cold roll bonding with the rolling reduction of 50% and 75%. Tensile shear tests which give tensile shear strength were performed in order to assess the bond strength. Scanning electron microscopy was performed on the fractured interface produced by the tensile shear tests, which suggests that the fracture occurs within the Al alloy layer. The tensile shear strengths considering the area fraction of deposit of Al alloy on Cu side were compared with the shear stress converting from the ultimate tensile strengths. As a result, the tensile shear strength of the clad sheets is attributed to the shear strength of Al alloy layer close to the well bonded interface. A simple model was proposed that explains the effects of the rolling reduction and area fraction of deposit of Al alloy.

  15. New decorative applications of alloys at base of aluminium-molybdenum; Nuevas aplicaciones decorativas de aleaciones a base de aluminio-molibdeno

    Energy Technology Data Exchange (ETDEWEB)

    Mesa L, V.H.; Hernandez P, C.D.; Alvarez P, M.A.; Guzman, J.; Garcia H, M.; Juarez I, J.A.; Gonzalez, C.; Alvarez F, O. [IIM-UNAM, A.P. 70-360, 04510 Mexico D.F. (Mexico)]. e-mail: oaf@servidor.unam.mx

    2005-07-01

    Decorative properties of aluminum-molybdenum alloys have been analyzed as a function of chemical composition and applied heat treatment. These decorative application are due exclusively for their nano structure nature. The alloys were prepared at room temperature by DC magnetron sputtering technique in argon atmosphere at different deposition time to obtain several thickness and chemical compositions in the range 3 to 30 % of molybdenum metal. (Author)

  16. 缓蚀剂对LY12铝合金搭接件疲劳寿命的影响%Influence of Corrosion Inhibitors on Fatigue Life of LY12 Aluminium Alloy Lap Joints

    Institute of Scientific and Technical Information of China (English)

    张勇; 卞贵学; 陈跃良; 张泰峰

    2013-01-01

    模拟飞机服役环境,对未涂抹及涂抹缓蚀剂的航空LY12铝合金搭接试验件进行了腐蚀试验和疲劳试验.通过对试验件分解检查,分析了腐蚀环境对涂抹缓蚀剂航空LY12铝合金典型螺栓搭接件的影响.对缓蚀剂对搭接件的疲劳性能的影响进行了统计和分析.结果表明,相同腐蚀时间,未涂抹缓蚀剂试验件的螺栓孔附近和搭接面腐蚀程度较涂抹缓蚀剂试验件严重,缓蚀剂可有效减缓腐蚀,且不同的缓蚀剂类型对腐蚀的减缓程度不同.一般环境下,涂抹缓蚀剂的试验件比未涂抹缓蚀剂试验件的疲劳寿命有所减少,应力水平越小影响程度越明显;腐蚀40 d后,涂抹缓蚀剂的试验件较未涂抹缓蚀剂的试验件寿命育所增加,且不同应力水平和缓蚀剂类型对疲劳寿命的影响程度不同.%Corrosion test and fatigue test were carried out for LYl2 aluminium alloy lap joints with and without corrosion inhibitors.Influence of corrosion environment on LY12 aluminium alloy typical bolt lap joints daubed with corrosion inhibitors was analysed by overhauling specimens.Influence of corrosion inhibitors on fatigue property of lap joints was collected and analysed.The results show that faying surface of specimens without corrosion inhibitors corroded more severely during the same time,corrosion inhibitors can inhibite corrosion,and the effectiveness of various corrosion inhibitors is different In general environment,the fatigue life of specimens daubed with corrosion inhibitors reduced,influence extent is increasing obviously with the decrease of stess level.After 40 d corrosion,the fatigue life of specimens daubed with corrosion inhibitors increased,and influence extent is different with various stress level and corrosion inhibitors.

  17. Corrosion processing technology of high-silicon aluminium alloy cylinder sleeve material%高硅铝合金缸套材料腐蚀加工技术研究

    Institute of Scientific and Technical Information of China (English)

    孙廷富; 洪晓露; 杨亚琛; 崔崇亮; 翟景; 郭安振; 李胜杰

    2014-01-01

    The micro-structure,particle size and alkaline corrosion depth of high-silicon aluminium alloy cylinder sleeve material were tested by three-dimensional video micro-metallographical technique;The concave-convex of particles and surface texture on the alkaline corrosion interface were observed by laser confocal microscopy technique;The tribology property of alkaline corrosion samples was evaluated by reciprocating friction-wear tester. Results show that the micro-structure of high-silicon aluminium alloy was composed of Si particles with average size 4.00μm and hard second phase particles with average size 3.05μm. With the extension of corrosion time,the corrosion depth increases and corrosion interface enlarges. The surface concave-convex is more clearer as well. Through friction-wear test,it is also revealed that the tribology property reaches the best under the condition that alkaline concentration was 5Wt%,solution temperature is 40℃and alkaline corrosion time is 30~40 s.%采用三维视频显微金相技术对高硅铝合金缸套材料的组织构成、颗粒尺寸以及碱腐蚀深度进行测试与评价;用激光共聚焦显微镜技术对碱腐蚀界面颗粒凹凸以及表面纹理进行观察与描述;用往复式摩擦磨损实验机对碱腐蚀试样进行摩擦学性能评价。结果表明:高硅铝合金组织中主要由硅颗粒及第二相硬质点颗粒构成,平均硅颗粒尺寸为4.00μm,平均第二相颗粒尺寸为3.05μm;随腐蚀时间、深度的增加,腐蚀界面区域增大,表面凸凹及纹理更加清晰,当碱的质量分数为5%,溶液温度为40℃,腐蚀时间为30~40 s,摩擦学性能最优越。

  18. Effects of aluminium surface morphology and chemical modification on wettability

    DEFF Research Database (Denmark)

    Rahimi, Maral; Fojan, Peter; Gurevich, Leonid;

    2014-01-01

    Aluminium alloys are some of the predominant metals in industrial applications such as production of heat exchangers, heat pumps. They have high heat conductivity coupled with a low specific weight. In cold working conditions, there is a risk of frost formation on the surface of aluminium...... in the presence of water vapour, which can lead to the deterioration of equipment performance. This work addresses the methods of surface modification of aluminium and their effect of the underlying surface morphology and wettability, which are the important parameters for frost formation. Three groups of real...

  19. Sustainable Aluminium Systems

    Directory of Open Access Journals (Sweden)

    Sergio R. Ermolli

    2010-09-01

    Full Text Available In the present paper, an analytical presentation of some popular aluminium systems that contribute to sustainability of structures is presented. Special emphasis has been given to the properties of aluminium, while the influence of these systems in the overall performance of the structure regarding environment and economy is described. In particular, characteristics of aluminium elements such as high reflectivity and recyclability and their role in life cycle analysis (LCA are analyzed. The connections between energy efficiency and conservation of buildings and aluminium application are also discussed. Building applications such as curtain walls, window frames and facade sheets are presented and thoroughly investigated, considering their environmental and economic aspects. Furthermore, many innovative techniques that use aluminium elements in collaboration with other systems in order to produce renewable energy, such as solar panels and photovoltaics, are introduced. Finally, environmental innovations such as optimized ventilation mechanisms and light and shade management systems based on aluminium members are presented.

  20. Potentiostatic Electrochemical Preparation and Characterisation of Aluminium Containing Nickel Selenide

    Directory of Open Access Journals (Sweden)

    Sandeep Gohar

    2014-01-01

    Full Text Available The wide range of properties exhibited by Al based alloy makes them suitable for different applications. Aluminium containing nickel Selenide ternary alloy possess considerable corrosion resistance as compared to their pure metal counterparts. The objective of the present work has been focused on the preparation and characterisation of its thin film. Alloying with Aluminium improve the oxidation resistance and increases the heat conductivity of the alloy. There is always a high demand for plating Al and its alloys in automotive and aerospace products, house-hold goods, and artificial jewellery etc,. The morphological and the structural studies of the electrodeposited thin film were determined by Scanning Electron Microscope (SEM images and X-Ray Diffraction Pattern (XRD while elemental composition has been done by Energy Dispersive X-Ray Spectroscopy (EDAX analysis.

  1. Cold rolling simulation of 6061 aluminium alloy ring based on ABAQUS/Explicit code%基于ABAQUS/Explicit 6061铝合金环件冷轧仿真研究

    Institute of Scientific and Technical Information of China (English)

    罗晓东; 柳浩; 朱永祥

    2014-01-01

    基于ABAQUS/Explicit平台建立了6061铝合金环件冷轧模型,研究环件轧制过程中金属的变形规律,包括环件的咬入和锻透情况、应力-应变分布情况、轧制力与轧制力矩等。研究表明,环件的最终成型质量好,壁厚误差在0.1 mm以内,直径误差在1 mm左右。%Based on ABAQUS/Explicit code,a cold rolling model of 6061 aluminium alloy ring was proposed to study deformation law,such as bite condition,plastic penetration condition,stress and strain distribution,rolling force and rolling moment,and so on. The results show that the formed ring has good quality,the wall thickness error is less than 0.1 mm and the diameter error is about 1 mm.

  2. Rows of Dislocation Loops in Aluminium Irradiated by Aluminium Ions

    DEFF Research Database (Denmark)

    Henriksen, L.; Johansen, A.; Koch, J.

    1967-01-01

    Single-crystal aluminium specimens, irradiated with 50-keV aluminium ions, contain dislocation loops that are arranged in regular rows along <110 > directions. ©1967 The American Institute of Physics......Single-crystal aluminium specimens, irradiated with 50-keV aluminium ions, contain dislocation loops that are arranged in regular rows along directions. ©1967 The American Institute of Physics...

  3. An Investigation on Axial Deformation Behavior of Thin-Wall Unfilled and Filled Tube with Aluminum Alloy (Al-Si7Mg) Foam Reinforced with SiC Particles

    Science.gov (United States)

    Kumaraswamidhas, L. A.; Rajak, Dipen Kumar; Das, S.

    2016-08-01

    The objective of this research is to produce superior quality aluminum alloy foam with low relative density and higher resistance against compression deformation. This investigation has studied crash energy capacities of unfilled and filled aluminum alloy foams in mild steel tubes. The foam has been prepared by the melt route process with an addition of 5wt.% silicon carbide particles. The fabricated aluminum alloy foams were characterized by field emission scanning electron microscopy, x-ray diffraction, Fourier transform infrared spectroscopy, and Material Pro analyzer. It was observed that the foam-filled tubes could absorb more energy as compared to the unfilled tubes before reaching the complete densification point. Also, the aluminum alloy foams had better energy absorption capacity during the crash or impact loading. This article demonstrates the excellent ability of aluminum alloy foam application in the field where there is a need to absorb crash energy. It is to be noted that the amount of energy absorption will be greater for low-density foam filled in thin-wall rectangular section tubes. We have seen an increasing trend in the application of aluminum foams inside the thin-wall mild steel tubes for maximum energy absorption.

  4. Experimental comparison of the MIG, friction stir welding, cold metal transfer and hybrid laser-MIG processes for AA 6005-T6 aluminium alloy

    Science.gov (United States)

    Caruso, Serafino; Sgambitterra, Emanuele; Rinaldi, Sergio; Gallone, Antonello; Viscido, Lucio; Filice, Luigino; Umbrello, Domenico

    2016-10-01

    In this study, the mechanical properties of welded joints of AA 6005-T6 aluminum alloy obtained with hybrid laser-MIG and cold metal transfer (CMT) welding were analyzed. The performance of hybrid laser-MIG and CMT welded joints were identified using tensile, bending, shear and fatigue life tests. Taking into account the process conditions and requirements, hybrid laser-MIG and CMT welding processes were compared with friction stir welding (FSW) and conventional metal inert gas (MIG) welding processes, shown in a previous work, to understand the advantages and disadvantages of the processes for welding applications of studied Al alloy. Better tensile, bending and shear strength and fatigue life behavior were obtained with hybrid laser-MIG and FSW welded joints compared with conventional MIG processes.

  5. STRUCTURE, PHASE COMPOSITION AND PROPERTIES OF GAS-THERMAL COVERINGS OF MECHANICALLY ALLOYED THERMOREACTING COMPOSITE POWDERS OF NICKEL-ALUMINIUM SYSTEM

    Directory of Open Access Journals (Sweden)

    F. G. Lovshenko

    2015-01-01

    Full Text Available The presented results show that coverings from mechanically alloyed thermoreacting powders of system «nickel–aluminum» are nonequilibrium multiphase systems which basis represents solid solution of aluminum in nickel. It has the microcrystalline type of structure which is characterized by an advanced surface of borders of the grains and subgrains stabilized by nanodimensional inclusions of oxides and alyuminid. These coverings surpass by 1,2–1,6 times analogs in durability, hardness and wear resistance.

  6. The effect of MAO processing time on surface properties and low temperature infrared emissivity of ceramic coating on aluminium 6061 alloy

    Science.gov (United States)

    Al Bosta, Mohannad M. S.; Ma, Keng-Jeng; Chien, Hsi-Hsin

    2013-09-01

    MAO ceramic coatings were prepared on aluminium 6061 surfaces at different treating durations (10, 20, ... 60 min), using alkali silicate electrolyte and pulsed bipolar current mode. The surface microstructures and properties were studied using SEM, XRD, EDX and a surface roughness tester. Image-Pro Plus and MATCH! softwares were used to analyze SEM micrographs and XRD results, respectively. The infrared emissivities of the ceramic coatings were measured at the 70 °C using FTIR spectrometer. We found a linear correlation between the volcano-like area and the surface roughness. The compositions and phases were associated with the volcano-like population and area. The curve of IR spectral emissivity was influenced by surface roughness, γ-alumina, sillimanite and cristobalite phases. The emissivity was enhanced by the surface roughness in the ranges 4.0-9.6 μm and 10.5-14.8 μm. In the range 7.0-8.0 μm, α-alumina and sillimanite phases enhanced the emissivity, while the cristobalite has a negative impact to the emissivity. A negative contributions were found for α-alumina in the region 9.6-16.0 μm and for the surface thickness in the region 15.0-16.0 μm. Overall, the average of long wave infrared (LWIR) emissivity ranged from 87.05% to 91.65%.

  7. Thermo-kinetic prediction of metastable and stable phase precipitation in Al–Zn–Mg series aluminium alloys during non-isothermal DSC analysis

    Energy Technology Data Exchange (ETDEWEB)

    Lang, Peter, E-mail: pl404@cam.ac.uk [Department of Materials Science and Metallurgy, University of Cambridge, Charles Babbage Road 27, Cambridge CB3 0FS (United Kingdom); Wojcik, Tomasz [Institute of Materials Science and Technology, Vienna University of Technology, Favoritenstraße 9-11, Vienna 1040 (Austria); Povoden-Karadeniz, Erwin [Institute of Materials Science and Technology, Vienna University of Technology, Favoritenstraße 9-11, Vienna 1040 (Austria); Christian Doppler Laboratory “Early Stages of Precipitation”, Institute of Materials Science and Technology, Vienna University of Technology, Favoritenstraße 9-11, Vienna 1040 (Austria); Falahati, Ahmad [Institute of Materials Science and Technology, Vienna University of Technology, Favoritenstraße 9-11, Vienna 1040 (Austria); Kozeschnik, Ernst [Institute of Materials Science and Technology, Vienna University of Technology, Favoritenstraße 9-11, Vienna 1040 (Austria); Christian Doppler Laboratory “Early Stages of Precipitation”, Institute of Materials Science and Technology, Vienna University of Technology, Favoritenstraße 9-11, Vienna 1040 (Austria)

    2014-10-01

    Highlights: • Comparison of laboratory Al–Zn–Mg alloy to industrial Al 7xxx series. • Heat flow evolution during non-isothermal DSC analysis is calculated. • TEM investigations of laboratory Al–Zn–Mg alloy at three pronounced temperatures. • Simulation and modelling of precipitation sequence. • Calculation and prediction of heat flow curves of Al 7xxx series. - Abstract: The technological properties of heat treatable Al–Zn–Mg alloys originate in the morphology and distribution of metastable particles. Starting from the solution-annealed condition, this paper describes the precipitate evolution during non-isothermal temperature changes, namely continuous heating differential scanning calorimetry (DSC) analysis. The distribution and the morphology of the metastable and stable precipitates and the heat flow accompanying the precipitation process is investigated experimentally and calculated by numerical thermo-kinetic simulations. The computer simulation results of the sizes and distributions are confirmed by transmission electron microscopy (TEM). The theoretical background and the results of the investigations are discussed.

  8. Role of aluminium addition on structure of Fe substituted Fe73.5−Si13.5B9Nb3Cu1Al alloy ribbons

    Indian Academy of Sciences (India)

    Gautam Agarwal; Himanshu Agrawal; M Srinivas; B Majumdar; N K Mukhopadhyay

    2013-08-01

    The investigation has dealt with the structure and magnetic properties of rapidly solidified and annealed Fe73.5−Si13.5B9Nb3Cu1Al ( = 0, 2, 4, 6 at%) ribbons prepared by melt spinning. Complete amorphous structure was obtained in as-spun ribbons of = 0 and 2 at% compositions, whereas structure of ribbons containing higher Al was found to be partially crystalline. Detailed thermal analyses of the alloys and the melt spun ribbons revealed that the glass forming ability in the form of x/l (ratio between crystallization and liquidus temperature) is the highest for 2 at% Al alloys and decreases with further addition of Al. Annealing of all as spun ribbons resulted in the precipitation of nanocrystalline phase embedded in amorphous matrix in the form of either 3 phase or -Fe(Si/Al) solid solution depending on the initial composition of the alloy. Only -Fe(Si/Al) solid solution was formed in 2 at% Al ribbons whereas ordered DO3 structure was found to be stabilized in other ribbons including 0 at% Al. A detailed study on determination of precision lattice parameter of nanocrystalline phase revealed that the lattice parameter increases with the addition of Al indicating the partitioning behaviour of Al in nanocrystalline phase.

  9. Diamond grooving of rapidly solidified optical aluminium

    Science.gov (United States)

    Abou-El-Hossein, Khaled; Hsu, Wei-Yao; Ghobashy, Sameh; Cheng, Yuan-Chieh; Mkoko, Zwelinzima

    2015-10-01

    Traditional optical aluminium grades such as Al 6061 are intensively used for making optical components for applications ranging from mould insert fabrication to laser machine making. However, because of their irregular microstructure and relative inhomogeneity of material properties at micro scale, traditional optical aluminium may exhibit some difficulties when ultra-high precision diamond turned. Inhomogeneity and micro-variation in the material properties combined with uneven and coarse microstructure may cause unacceptable surface finish and accelerated tool wear, especially in grooving operation when the diamond tool edge is fully immersed in the material surface. Recently, new grades of optical aluminium that are featured by their ultra-fine microstructure and improved material properties have been developed to overcome the problem of high tool wear rates. The new aluminium grades have been developed using rapid solidification process which results in extremely small grain sizes combined with improved mechanical properties. The current study is concerned with investigating the performance of single-point diamond turning when grooving two grades of rapidly solidified aluminium (RSA) grades: RSA905 which is a high-alloyed aluminium grade and RSA443 which has a high silicon content. In this study, two series of experiments employed to create radial microgrooves on the two RSA grades. The surface roughness obtained on the groove surface is measured when different combinations of cutting parameters are used. Cutting speed is varied while feed rate and depth of cut were kept constant. The results show that groove surface roughness produced on RSA443 is higher than that obtained on RSA905. Also, the paper reports on the effect of cutting speed on surface roughness for each RSA grade.

  10. Characterization of mechanical properties of hydroxyapatite-silicon-multi walled carbon nano tubes composite coatings synthesized by EPD on NiTi alloys for biomedical application.

    Science.gov (United States)

    Khalili, Vida; Khalil-Allafi, Jafar; Sengstock, Christina; Motemani, Yahya; Paulsen, Alexander; Frenzel, Jan; Eggeler, Gunther; Köller, Manfred

    2016-06-01

    Release of Ni(1+) ions from NiTi alloy into tissue environment, biological response on the surface of NiTi and the allergic reaction of atopic people towards Ni are challengeable issues for biomedical application. In this study, composite coatings of hydroxyapatite-silicon multi walled carbon nano-tubes with 20wt% Silicon and 1wt% multi walled carbon nano-tubes of HA were deposited on a NiTi substrate using electrophoretic methods. The SEM images of coated samples exhibit a continuous and compact morphology for hydroxyapatite-silicon and hydroxyapatite-silicon-multi walled carbon nano-tubes coatings. Nano-indentation analysis on different locations of coatings represents the highest elastic modulus (45.8GPa) for HA-Si-MWCNTs which is between the elastic modulus of NiTi substrate (66.5GPa) and bone tissue (≈30GPa). This results in decrease of stress gradient on coating-substrate-bone interfaces during performance. The results of nano-scratch analysis show the highest critical distance of delamination (2.5mm) and normal load before failure (837mN) as well as highest critical contact pressure for hydroxyapatite-silicon-multi walled carbon nano-tubes coating. The cell culture results show that human mesenchymal stem cells are able to adhere and proliferate on the pure hydroxyapatite and composite coatings. The presence of both silicon and multi walled carbon nano-tubes (CS3) in the hydroxyapatite coating induce more adherence of viable human mesenchymal stem cells in contrast to the HA coated samples with only silicon (CS2). These results make hydroxyapatite-silicon-multi walled carbon nano-tubes a promising composite coating for future bone implant application.

  11. Volatilisation and oxidation of aluminium scraps fed into incineration furnaces

    Energy Technology Data Exchange (ETDEWEB)

    Biganzoli, Laura, E-mail: laura.biganzoli@mail.polimi.it [Politecnico di Milano, Piazza L. Da Vinci 32, 20133 Milano (Italy); Gorla, Leopoldo; Nessi, Simone; Grosso, Mario [Politecnico di Milano, Piazza L. Da Vinci 32, 20133 Milano (Italy)

    2012-12-15

    Highlights: Black-Right-Pointing-Pointer Aluminium packaging partitioning in MSW incineration residues is evaluated. Black-Right-Pointing-Pointer The amount of aluminium packaging recoverable from the bottom ashes is evaluated. Black-Right-Pointing-Pointer Aluminium packaging oxidation rate in the residues of MSW incineration is evaluated. Black-Right-Pointing-Pointer 80% of aluminium cans, 51% of trays and 27% of foils can be recovered from bottom ashes. - Abstract: Ferrous and non-ferrous metal scraps are increasingly recovered from municipal solid waste incineration bottom ash and used in the production of secondary steel and aluminium. However, during the incineration process, metal scraps contained in the waste undergo volatilisation and oxidation processes, which determine a loss of their recoverable mass. The present paper evaluates the behaviour of different types of aluminium packaging materials in a full-scale waste to energy plant during standard operation. Their partitioning and oxidation level in the residues of the incineration process are evaluated, together with the amount of potentially recoverable aluminium. About 80% of post-consumer cans, 51% of trays and 27% of foils can be recovered through an advanced treatment of bottom ash combined with a melting process in the saline furnace for the production of secondary aluminium. The residual amount of aluminium concentrates in the fly ash or in the fine fraction of the bottom ash and its recovery is virtually impossible using the current eddy current separation technology. The average oxidation levels of the aluminium in the residues of the incineration process is equal to 9.2% for cans, 17.4% for trays and 58.8% for foils. The differences between the tested packaging materials are related to their thickness, mechanical strength and to the alloy.

  12. On the effect of silicon and phosphorus during the precipitation of kappa-carbide in Iron-Manganese-Aluminium-Carbon alloys

    Science.gov (United States)

    Bartlett, Laura Nicole

    Implementation of lightweight high manganese and aluminum steels for use in high energy absorbing applications requires a detailed knowledge of how alloying additions and impurities affect age hardening and high strain rate fracture properties. Dynamic fracture toughness is an important design criterion but has not been reported previously in these alloys. In addition, previous studies have shown that silicon and phosphorus increased the strength and aged hardness; however, the mechanism was unknown. This research mainly focuses on the effect of silicon and phosphorus on the precipitation of kappa-carbide and alloy partitioning during aging. Short range ordering, SRO, of Fe-Al-C into relative atomic positions described by the E21 superlattice structure preceded and occurred concurrent to spinodal decomposition. Short range diffusion of phosphorus increased the kinetics of ordering resulting in a decrease in the time required for subsequent spinodal decomposition and an increase the amplitude of carbon concentration with time. Silicon increased the strength and hardness as a result of increased carbon partitioning into the kappa-carbide during aging. Dynamic fracture toughness was found to depend upon aluminum and carbon. Increasing the amount of solid solution carbon increased the dynamic fracture toughness in solution treated specimens. However, increasing carbon in aged specimens increased the amount of kappa-carbide and produced brittle fracture. Additions of aluminum from three to nine weight percent decreased toughness regardless of the heat treatment. Dynamic fracture toughness was a strong function of AlN content. A good combination of high strength and dynamic toughness with a corresponding density reduction of 10 to 12% is obtained with aluminum additions between 6 and 7% and carbon below 1.2%.

  13. Effect of silicon on recrystallization of wrought aluminium alloy%Si元素对变形铝合金再结晶影响

    Institute of Scientific and Technical Information of China (English)

    华琪; 邵光杰

    2012-01-01

    Effects of silicon contents, deformation and solution treatment on hardness of the recrystalled wrought aluminum alloy were investigated by means of optical microscopy and hardness tests. The results show that coarse grain size in the aluminumsilicon alloy solutiontreated at 500 ℃ for 30 rain and followed by rapidly compressive deformation is obtained after annealingdue to the rapid deformation. Less silicon contents of alu, in inumsilicon alloy can accelerate the recrystallization and get the coarse grain. The addition of silicon significantly causes a reduction in recrystallization grain size when silicon content is greater than 1%.%围绕不同的成分、变形温度和变形量同再结晶退火后的合金硬度之间的关系,通过偏光显微组织分析以及硬度测试对铝硅合金变形再结晶进行了研究。结果表明,铝硅合金在500℃进行0~h固溶处理后以较快的速度进行变形会使得退火后再结晶晶粒尺寸变大。硅含量较少的时候可以促进铝硅合金再结晶的发生,并使再结晶晶粒粗化,而当硅含量大于1%之后,随着硅含量的增加再结晶晶粒会显著减小。

  14. Effects of Rolling Reduction and Strength of Composed Layers on Bond Strength of Pure Copper and Aluminium Alloy Clad Sheets Fabricated by Cold Roll Bonding

    OpenAIRE

    Yoji Miyajima; Kotaro Iguchi; Susumu Onaka; Masaharu Kato

    2014-01-01

    Three types of clad sheets, Cu/Al, Cu/AA5052, and Cu/AA5083, were produced by cold roll bonding with the rolling reduction of 50% and 75%. Tensile shear tests which give tensile shear strength were performed in order to assess the bond strength. Scanning electron microscopy was performed on the fractured interface produced by the tensile shear tests, which suggests that the fracture occurs within the Al alloy layer. The tensile shear strengths considering the area fraction of deposit of Al al...

  15. The Process Improvement and Extruding Die Design of Aluminium-Alloy Parts%铝合金制件工艺改进与挤压模设计

    Institute of Scientific and Technical Information of China (English)

    罗国军

    2012-01-01

    通过分析梅花形铝合金制件工艺,采用合理的坯料、坯料加热与模具结构,证明可以完成一次挤压成形,简化工序流程和节省材料成本。%Through analyzing the process of plum-shape aluminum alloy parts, adopted reasonable raw material design, raw material heating and die structure, make sure that the extruded part can be done once, simplify the processes procedures and saving the cost of raw materials.

  16. Texture and EBSD of TA18 Titanium Alloys Tubes%TA18钛合金管材织构的测试与EBSD分析

    Institute of Scientific and Technical Information of China (English)

    杨磊; 惠松骁; 叶文君; 黄亮

    2011-01-01

    The texture of TA18 titanium alloys tubes was studied by means of X-ray diffraction and electron backscattered diffraction (EBSD), the CSR values were calculated too. The results of (0002) pole figures for different types of TA18 titanium alloys tubes showed that the c-axis of the grains distributed in the plane of RD-TD and deflected 30° from the ND direction, most of which scattered at the range of 0 ~ 60°. The Reams factors of different types of TA18 titanium alloys tubes showed that fr, was about 0. 6 while ft and fl was relatively small. The results of EBSD showed that the preferred orientation of the grains in the Φ6 mm ×0. 5 nun TA18 titanium alloys tube was observed, after passes of rolling, the grains were stretched along the rolling direction. The c-axis of the grains paralleled to the ND direction and formed basal (0002) texture. Besides, the method of calculating CSR values was an effective way to measure the texture of TA18 titanium alloys tubes, the results matched the EBSD value and tested value very well.%用X射线衍射和电子背散射衍射技术,测试了航空用不同规格TA18钛合金管材的织构,并利用织构测试的数据计算了管材的CSR值.由不同规格TA18钛合金管材的(0002)面极图可以得出,管材内部晶粒基面的c轴主要分布在试样RD-TD面内,且沿着ND方向偏转了约30°左右,大部分分布在0~60°的范围之内.利用极图数据所计算的管材的Kearns系数显示,各种规格管材的fr值约为0.6左右,而ft与f1相对较小.同时结合EBSD测试结果,阐述了晶粒形貌与织构产生的原因,对比分析了管材φ6 mm ×0.5 mm横截面与展开面晶粒取向分布特点,结果显示,管材经过多道次的轧制变形,晶粒沿着轧制方向被拉长,试样内部晶粒也出现了明显的择优取向,其中晶粒c轴主要沿ND方向分布,形成了较强的(0002)基面织构.通过EBSD测试方法得到的CSR值与极图计算值和实测值得到的结果相近,因

  17. Corrosion and Protection of Ni-based Alloy Heating Tube%镍基合金电加热管腐蚀与防护

    Institute of Scientific and Technical Information of China (English)

    魏刚; 白阿香; 乔宁

    2012-01-01

    通过草酸浸蚀试验、动电位扫描测试、自腐蚀电位测试、电偶腐蚀试验和扫描电镜(SEM)观察,研究镍基合金Incoloy800、Incoloy840以及用它们制成的加热管在试验条件下的腐蚀情况;分析加工工艺对两种镍基合金腐蚀性能的影响;比较两种镍基合金加热管抗腐蚀性能的差异。结果表明,加工工艺显著降低了Incoloy840镍基合金的点蚀电位,对Incoloy800镍基合金的点蚀电位影响较小;对两种镍基合金晶间腐蚀敏感性几乎都没有影响;Incoloy800加热管试样品间腐蚀敏感性小于Incoloy840加热管;Incoloy800加热管点蚀电位高于Incoloy840加热管;白腐蚀电位高低顺序为:Incoloy800加热管,Incoloy840加热管,Mg;Incoloy800加热管/镁电偶对电偶电流密度大于lncoloy840加热管/镁电偶对,lncoloy800加速电偶阳极镁腐蚀的作用更大。%The corrosion performance of Ni-based alloy Incoloy800 and Incoloy840 was studied by oxalic acid etch test, potentiodynamic polarization test, galvanic corrosion experiment and SEM. The influence of processing on the corrosion resistance of these two alloys was also discussed. The results showed that alloy Incoloy800 and the heating tube made of it had better intergranular corrosion resistance compared with Incoloy840 and the tube made of it. Pitting potential of Incoloy840 decreased significantly and Incoloy800 ahnost showed little change in pitting potential after processing. The galvanic current density of Incoloy800 heating tube/Mg was higher than that of Incoloy840 heating tube/Mg, indicating that Incoloy800 accelerated the corrosion rate of Mg anode more remarkably.

  18. 淬火速率对AA7108铝合金的微观结构和力学性能的影响%Effect of quenching rate on microstructure and mechanical properties of commercial AA7108 aluminium alloy

    Institute of Scientific and Technical Information of China (English)

    Ida WESTERMANN; Ann Leni HAUGSTAD; Yngve LANGSRUD; Knut MARTHINSEN

    2012-01-01

    A commercial AA7108 aluminium alloy subjected to different quenching procedures from the solid solution temperature of 480 ℃ was considered.Both continuously cooling and quenching to intermediate temperatures (400,300 and 200 ℃) followed by different holding times were applied.All the materials were subsequently subjected to the same industrial two-step artificial ageing procedure to obtain a maximum strength (T6).Tensile testing of the different quenched materials in the T6 temper reveals a large deviation in strength dependent on the cooling/holding time,compared with the reference sample.A collection of the different quenched materials was chosen for further investigation of the precipitate structure by transmission electron microscopy (TEM) to explain the differences in mechanical properties.%在480℃固溶温度对AA7108铝合金进行不同工艺的淬火.将合金连续冷却、淬火至中间温度(400,300和200℃)并保温不同时间,再进行工业两步人工时效处理,以获得最大强度(T6).T6态淬火材料的拉伸试验表明,材料的强度很大程度上取决于冷却/保温时间.通过透射电子显微镜(TEM)观察材料中沉淀物结构来解释材料的力学性能差异.

  19. Alloy

    Science.gov (United States)

    Cabeza, Sandra; Garcés, Gerardo; Pérez, Pablo; Adeva, Paloma

    2014-07-01

    The Mg98.5Gd1Zn0.5 alloy produced by a powder metallurgy route was studied and compared with the same alloy produced by extrusion of ingots. Atomized powders were cold compacted and extruded at 623 K and 673 K (350 °C and 400 °C). The microstructure of extruded materials was characterized by α-Mg grains, and Mg3Gd and 14H-LPSO particles located at grain boundaries. Grain size decreased from 6.8 μm in the extruded ingot, down to 1.6 μm for powders extruded at 623 K (350 °C). Grain refinement resulted in an increase in mechanical properties at room and high temperatures. Moreover, at high temperatures the PM alloy showed superplasticity at high strain rates, with elongations to failure up to 700 pct.

  20. The effect orientation of features in reconstructed atom probe data on the resolution and measured composition of T1 plates in an A2198 aluminium alloy.

    Science.gov (United States)

    Mullin, Maria A; Araullo-Peters, Vicente J; Gault, Baptiste; Cairney, Julie M

    2015-12-01

    Artefacts in atom probe tomography can impact the compositional analysis of microstructure in atom probe studies. To determine the integrity of information obtained, it is essential to understand how the positioning of features influences compositional analysis. By investigating the influence of feature orientation within atom probe data on measured composition in microstructural features within an AA2198 Al alloy, this study shows differences in the composition of T1 (Al2CuLi) plates that indicates imperfections in atom probe reconstructions. The data fits a model of an exponentially-modified Gaussian that scales with the difference in evaporation field between solutes and matrix. This information provides a guide for obtaining the most accurate information possible.