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Sample records for advanced-gas-cooled-nuclear-reactor materials evaluation

  1. Advanced Gas Cooled Nuclear Reactor Materials Evaluation and Development Program. Progress report, January 1, 1980-March 31, 1980

    Energy Technology Data Exchange (ETDEWEB)

    1980-06-25

    Results are presented of work performed on the Advanced Gas-Cooled Nuclear Reactor Materials Evaluation and Development Program. The objectives of this program are to evaluate candidate alloys for Very High Temperature Reactor (VHTR) Nuclear Process Heat (NPH) and Direct Cycle Helium Turbine (DCHT) applications, in terms of the effect of simulated reactor primary coolant (helium containing small amounts of various other gases), high temperatures, and long time exposures, on the mechanical properties and structural and surface stability of selected candidate alloys. A second objective is to select and recommend materials for future test facilities and more extensive qualification programs. Included are the activities associated with the status of the simulated reactor helium supply system, testing equipment and gas chemistry analysis instrumentation and equipment. The progress in the screening test program is described, including screening creep results and metallographic analysis for materials thermally exposed or tested at 750, 850, and 950/sup 0/C.

  2. Advanced Gas Cooled Nuclear Reactor Materials Evaluation and Development Program. Progress report, July 1, 1980-September 30, 1980

    Energy Technology Data Exchange (ETDEWEB)

    1980-12-12

    Objectives of this program are to evaluate candidate alloys for Very High Temperature Reactor (VHTR) Nuclear Process Heat (NPH) and Direct Cycle Helium Turbine (DCHT) applications, in terms of the effect of simulated reactor primary coolant (helium containing small amounts of various other gases), high temperatures, and long time exposures, on the mechanical properties and structural and surface stability of selected candidate alloys. A second objective is to select and recommend materials for future test facilities and more extensive qualification programs. Work covered in this report includes the activities associated with the status of the simulated reactor helium supply system, testing equipment and gas chemistry analysis instrumentation and equipment. The progress in the screening test program is described: screening creep results and metallographic analysis for materials thermally exposed or tested at 750, 850, 950 and 1050/sup 0/C. Initiation of controlled purity helium creep-rupture testing in the intensive screening test program is discussed. In addition, the results of 1000-hour exposures at 750 and 850/sup 0/C on several experimental alloys are discussed.

  3. Advanced Gas Cooled Nuclear Reactor Materials Evaluation and Development Program. Progress report, April 1, 1980-June 30, 1980

    Energy Technology Data Exchange (ETDEWEB)

    1980-11-14

    Objectives of this program are to evaluate candidate alloys for Very High Temperature Reactor (VHTR) Nuclear Process Heat (NPH) and Direct Cycle Helium Turbine (DCHT) applications, in terms of the effect of simulated reactor primary coolant (helium containing small amounts of various other gases), high temperatures, and long time exposures, on the mechanical properties and structural and surface stability of selected candidate alloys. A second objective is to select and recommend materials for future test facilities and more extensive qualification programs. Work covered in this report includes the activities associated with the status of the simulated reactor helium supply system, testing equipment and gas chemistry analysis instrumentation and equipment. The progress in the screening test program is described; this includes: screening creep results and metallographic analysis for materials thermally exposed or tested at 750, 850 and 950/sup 0/C. The initiation of air creep-rupture testing in the intensive screening test program is discussed. In addition, the status of the data management system is described.

  4. Advanced Gas Cooled Nuclear Reactor Materials Evaluation and Development Program. Progress report, July 1, 1981-September 30, 1981

    International Nuclear Information System (INIS)

    Work covered in this report includes the activities associated with the status of the simulated reactor helium supply systems and testing equipment. The progress in the screening test program is described; this includes: screening creep results and metallographic analysis for materials thermally exposed or tested at 7500, 8500, 9500, and 10500C (13820, 15620, 17420, and 19220F). The status of controlled purity helium and air creep-rupture testing in the intensive screening test program is discussed. The results of metallographic studies of screening alloys exposed in controlled purity helium for 3000 hours at 7500C and 6000 hours at 8500C and for weldments exposed in controlled purity helium for 6000 hours at 8500 and 9500C are presented and discussed

  5. Advanced-gas-cooled-nuclear-reactor materials evaluation and development program. Volume 1.Final report, September 23, 1976-September 30, 1982

    International Nuclear Information System (INIS)

    Included in this report is a discussion of the materials selected for the screening phase and more intensive screening phase test programs and the systems and components for which they are candidate materials. Thirty-one (31) commercially available alloy and alloy/coating materials and ten (10) experimental alloys were evaluated in the program. The experimental test facilities developed as part of this program are discussed and experimental testing procedures are summarized. The results of the initial screening test programs are presented. This includes creep testing results and metallographic analyses of candidate materials exposed to simulated HTGR helium and air under stress at temperatures of 7500, 8500, 9500, or 10500C (13820, 15620, 17420, or 19220F) for exposure times to 10,000 hours. Metallographic analyses, weight change and carbon analyses results, and post exposure room temperature tensile and Charpy V-notch impact test results are presented for candidate materials exposed unstressed under the conditions stated above

  6. Advanced gas cooled nuclear reactor materials evaluation and development program. Selection of candidate alloys. Vol. 1. Advanced gas cooled reactor systems definition

    Energy Technology Data Exchange (ETDEWEB)

    Marvin, M.D.

    1978-10-31

    Candidate alloys for a Very High Temperature Reactor (VHTR) Nuclear Process Heal (NPH) and Direct Cycle Helium Turbine (DCHT) applications in terms of the effect of the primary coolant exposure and thermal exposure were evaluated. (FS)

  7. Advanced Gas Cooled Nuclear Reactor Materials Evaluation and Development program. Progress report, October 1, 1981-December 31, 1981. [Alloy-MA-956; alloy-MA-754

    Energy Technology Data Exchange (ETDEWEB)

    Kimball, O.F.

    1982-06-15

    Work covered in this report includes the activities associated with the status of the simulated reactor helium supply systems and testing equipment. The progress in the screening test program is descibed; this includes: screening creep results and metallographic analysis for materials thermally exposed or tested at 750/sup 0/, 850/sup 0/, 950/sup 0/ and 1050/sup 0/C (1382/sup 0/, 1562/sup 0/, 1742/sup 0/, and 1922/sup 0/F) in controlled-purity helium. The status of creep-rupture in controlled-purity helium and air and fatigue testing in the controlled-purity helium in the intensive screening test program is discussed. The results of metallographic studies of screening alloys exposed in controlled-purity helium for 3000 hours at 750/sup 0/C and 5500 hours at 950/sup 0/C, 3000 hours at 1050/sup 0/C and 6000 hours at 1050/sup 0/C and for weldments exposed in controlled-purity helium for 6000 hours at 750/sup 0/C and 6000 hours at 1050/sup 0/C are presented and discussed.

  8. Development of a CVD silica coating for UK advanced gas-cooled nuclear reactor fuel pins

    International Nuclear Information System (INIS)

    Vapour deposited silica coatings could extend the life of the 20% Cr/25% Ni niobium stabilised (20/25/Nb) stainless steel fuel cladding of the UK advanced gas cooled reactors. A CVD coating process developed originally to be undertaken at atmospheric pressure has now been adapted for operation at reduced pressure. Trials on the LP CVD process have been pursued to the production scale using commercial equipment. The effectiveness of the LP CVD silica coatings in providing protection to 20/25/Nb steel surfaces against oxidation and carbonaceous deposition has been evaluated. (author)

  9. Advanced gas-cooled nuclear reactor materials evaluation and development program: corrosion behavior of experimental alloys in controlled-purity helium at temperatures in the 750 to 10500C range

    International Nuclear Information System (INIS)

    A series of 10 experimental alloys (basically Ni-20Cr with addition of one or more of the elements Al, Ti, Si, Nb and Y) has been examined after exposure to controlled purity helium for periods of 1000 to 6000 hours at temperatures of 750 to 10500C. Alloys containing aluminum were particularly susceptible to internal oxidation at the lower temperatures, but at 9500C and above carburization became the dominant corrosive mechanism. The most corrosive resistant alloys were Ni-Cr20 and Ni-Cr containing Si, Ti and Nb. The presence of small amounts of yttrium dramatically promoted the occurrence of carburization, even at temperatures as low as 8500C. 69 figures, 7 tables

  10. Evaluation of learning materials

    DEFF Research Database (Denmark)

    Bundsgaard, Jeppe; Hansen, Thomas Illum

    2011-01-01

    This paper presents a holistic framework for evaluating learning materials and designs for learning. A holistic evaluation comprises investigations of the potential learning potential, the actualized learning potential, and the actual learning. Each aspect is explained and exemplified through...

  11. Holistic evaluations of learning materials

    DEFF Research Database (Denmark)

    Bundsgaard, Jeppe; Hansen, Thomas Illum

    2011-01-01

    , and the competences supposedly supported when working with the material - the actualized learning potential, i.e. the potential for learning when the design for learning is enacted by integrating the learning material in a situation in a given context, and - the actual learning, i.e. how the participants actually......The aim of this paper is to present a holistic framework for evaluating learning materials and designs for learning. A holistic evaluation of learning material comprises investigations of - the potential learning potential, i.e. the affordances and challenges of the learning material...... develop their competences through working with a learning material or enacting a design for learning....

  12. Evaluation of learning materials

    DEFF Research Database (Denmark)

    Hansen, Thomas Illum; Bundsgaard, Jeppe

    2011-01-01

    Artiklen præsenterer en teoretisk rammesætning af evlauering af læremidler, der både omfatter semiotisk og didaktisk analyse af læremidlets design, analyse og evaluering af kontekstspecifik brug og evaluering af læringsudbytte....

  13. Cyclic reheat materials evaluation

    International Nuclear Information System (INIS)

    A cyclic reheat system for a wet flue gas desulfurization system extracts heat from the inlet flue gas and transfers this heat to the outlet flue gas. One method of achieving this uses tube-type heat exchangers in the inlet and outlet gas streams with a fluid (e.g., water) circulated between them. For high sulfur coal, questions of material selection and cleaning methods for the inlet heat exchanger exist because of the potential for acid condensation. An inlet gas heat exchanger test apparatus was built and installed on a slipstream from a high sulfur coal fired power plant. Results obtained from the first 3061 hours of exposure indicate low corrosion rates for several stainless steels, and that a water wash prevented tube solids buildup

  14. Evaluative Review in Materials Development

    Science.gov (United States)

    Stoller, Fredricka L.; Horn, Bradley; Grabe, William; Robinson, Marin S.

    2006-01-01

    English for Academic Purposes (EAP) professionals know that initial efforts to produce or adapt materials generally require evaluative review and revision. A review process that solicits feedback from teacher and student users is critical because materials writers often find it difficult to envision the problems others may have with their…

  15. DWPF MATERIALS EVALUATION SUMMARY REPORT

    Energy Technology Data Exchange (ETDEWEB)

    Gee, T.; Chandler, G.; Daugherty, W.; Imrich, K.; Jankins, C.

    1996-09-12

    To better ensure the reliability of the Defense Waste Processing Facility (DWPF) remote canyon process equipment, a materials evaluation program was performed as part of the overall startup test program. Specific test programs included FA-04 ('Process Vessels Erosion/Corrosion Studies') and FA-05 (melter inspection). At the conclusion of field testing, Test Results Reports were issued to cover the various test phases. While these reports completed the startup test requirements, DWPF-Engineering agreed to compile a more detailed report which would include essentially all of the materials testing programs performed at DWPF. The scope of the materials evaouation programs included selected equipment from the Salt Process Cell (SPC), Chemical Process Cell (CPC), Melt Cell, Canister Decon Cell (CDC), and supporting facilities. The program consisted of performing pre-service baseline inspections (work completed in 1992) and follow-up inspections after completion of the DWPF cold chemical runs. Process equipment inspected included: process vessels, pumps, agitators, coils, jumpers, and melter top head components. Various NDE (non-destructive examination) techniques were used during the inspection program, including: ultrasonic testing (UT), visual (direct or video probe), radiography, penetrant testing (PT), and dimensional analyses. Finally, coupon racks were placed in selected tanks in 1992 for subsequent removal and corrosion evaluation after chemical runs.

  16. The Empirical Evaluation of Language Teaching Materials.

    Science.gov (United States)

    Ellis, Rod

    1997-01-01

    Distinguishes two types of materials evaluation: a predictive evaluation designed to make a decision regarding what materials to use, and a retrospective evaluation to examine materials already used. Describes a procedure for conducting task evaluations, suggesting that they constitute a kind of action research that can contribute to reflective…

  17. Material sampling for rotor evaluation

    International Nuclear Information System (INIS)

    Decisions regarding continued operation of aging rotating machinery must often be made without adequate knowledge of rotor material conditions. Physical specimens of the material are not generally available due to lack of an appropriate sampling technique or the high cost and inconvenience of obtaining such samples. This is despite the fact that examination of such samples may be critical to effectively assess the degradation of mechanical properties of the components in service or to permit detailed examination of microstructure and surface flaws. Such information permits a reduction in the uncertainty of remaining life estimates for turbine rotors to avoid unnecessarily premature and costly rotor retirement decisions. This paper describes the operation and use of a recently developed material sampling device which machines and recovers an undeformed specimen from the surface of rotor bores or other components for metallurgical analysis. The removal of the thin, wafer-like sample has a negligible effect on the structural integrity of these components, due to the geometry and smooth surface finish of the resulting shallow depression. Samples measuring approximately 0.03 to 0.1 inches (0.76 to 2.5 mm) thick by 0.5 to 1.0 inch (1.3 to 2.5 cm) in diameter can be removed without mechanical deformation or thermal degradation of the sample or the remaining component material. The device is operated remotely from a control console and can be used externally or internally on any surface for which there is at least a three inch (7.6 cm) working clearance. Application of the device in two case studies of turbine-generator evaluations are presented

  18. Heliostat materials development and evaluation

    Science.gov (United States)

    1980-05-01

    Both UV stabilized poly (ethylene terephthalate) (PET) polyvinylidiene fluoride films were produced, characterized, and tested to establish a data base of predicting life cycles and upgrading the cost/performance ratio of heliostat enclosures. Laminated aluminized PET, protected and unprotected by a thin layer of resin was studied as suitable reflector material. Procedures and results of weathering tests are presented. Methods for bonding plastic films, specularly optimized film reflectors, and the mechanism of a weathering degradation are discussed. Data on the flammability of plastic films are included.

  19. Evaluation of Terminated Nuclear Material Licenses

    International Nuclear Information System (INIS)

    This report presents the results of a six-year project that reviewed material licenses that had been terminated during the period from inception of licensing until approximately late-1994. The material licenses covered in the review project were Part 30, byproduct material licenses; Part 40, source material licenses; and Part 70, special nuclear material licenses. This report describes the methodology developed for the project, summarizes the findings of the license file inventory process, and describes the findings of the reviews or evaluations of the license files. The evaluation identified nuclear material use sites that need review of the licensing material or more direct follow-up of some type. The review process also identified licenses authorized to possess sealed sources for which there was incomplete or missing documentation of the fate of the sources

  20. Canister filling materials -- Design requirements and evaluation of candidate materials

    International Nuclear Information System (INIS)

    SKB has been evaluating a copper/steel canister for use in the disposal of spent nuclear reactor fuel. Once the canister is breached by corrosion, it is possible that the void volume inside the canister might fill with water. Water inside the canister would moderate the energy of the neutrons emitted by spontaneous fission in the fuel. It the space in the canister between and around the fuel pins is occupied by canister filling materials, the potential for criticality is avoided. The authors have developed a set of design requirements for canister filling material for the case where it is to be used alone, with no credit for burnup of the fuel or other measures, such as the use of neutron absorbers. Requirements were divided into three classes: essential requirements, desirable features, and undesirable features. The essential requirements are that the material fill at least 60% of the original void space, that the solubility of the filling material be less than 100 mg/l in pure water or expected repository waters at 50 C, and that the material not compact under its own weight by more than 10%. In this paper they review the reasons for these requirements, the desirable and undesirable features, and evaluate 11 candidate materials with respect to the design requirements and features. The candidate materials are glass beads, lead shot, copper spheres, sand, olivine, hematite, magnetite, crushed rock, bentonite, other clays, and concrete. Emphasis is placed on the determination of whether further work is needed to eliminate uncertainties in the evaluation of the ability of a particular filling material to be successfully used under actual conditions, and on the ability to predict the long-term performance of the material under the repository conditions

  1. A Critical Look at EFL Material Evaluation

    Institute of Scientific and Technical Information of China (English)

    刘艳

    2008-01-01

    As teachers,most of the time,we are involved in the selection of teaching materials for our students for various purposes and in various ways.But in most of the situations,we have to make decisions ourselves by looking at the materials.Hence.it is of great importance to choose proper criteria to see whether they are appropriate for our students.Based on what mentioned above,we will first come to the reasons for evaluating EFL materials and then evaluation criteria.

  2. Analytical nondestructive evaluation for materials characterization

    International Nuclear Information System (INIS)

    Science and technology of nondestructive testing and evaluation has contributed immensely to the safety and productivity of industrial plants. In recent years, nondestructive evaluation (NDE) has emerged as a frontline research area of equal if not greater technological relevance, for materials characterization as well. A comprehensive range of techniques from qualitative nondestructive testing for quality control of engineering products and materials to quantitative NDE for materials characterization is being used by the engineering industry and materials researchers, for better understanding of the manufacturing practices and materials behaviour. Quantitative NDE is considered essential for ensuring fitness for purpose at the start of the life in case the component has been designed using fracture mechanics parameters. Quantitative NDE is also vital for assessing degradation of material during service. Moreover, quantitative NDE enables characterization of dynamics of certain phenomenon (not achievable by destructive test methodologies) leading to better understanding of the performance of materials in relation to unavoidable defects in the materials. As the next logical step, the need for an analytical approach to NDE is felt. The need and motivation for such an approach is addressed and the means to achieve this objective are identified. It is argued that analytical NDE is essential to meet the challenges of characterization, intelligent processing of materials and life prediction of components and plants. These requirements are of significant importance in the context of recent developments in materials engineering, and for enhancing the competitive advantage of Indian engineering industry in the international market. (author). 9 refs., 3 figs

  3. Thermoelectric materials evaluation program. Technical summary report

    Energy Technology Data Exchange (ETDEWEB)

    Hinderman, J.D.

    1979-04-01

    Research progress on the thermoelectric materials evaluation program is reported covering the period January 1, 1976 to September 30, 1978. Topical reports are presented on (1) hot and cold end ..delta..T's, (2) hardware mobility, (3) p-leg sublimation suppression, (4) thermodynamic stability of p-legs, (5) n-leg material process improvements to reduce extraneous resistance, (6) n-leg cracking, (7) dynamic evaluation of converter, and (8) data base and degradation modes. Twenty attachments are included which present supporting drawings, specifications, procedures, and data. (WHK)

  4. An evaluation of candidate oxidation resistant materials

    Science.gov (United States)

    Rutledge, Sharon; Banks, Bruce; Mirtich, Michael; Difilippo, Frank; Hotes, Deborah; Labed, Richard; Dever, Terese; Kussmaul, Michael

    1987-01-01

    Ground based testing of materials considered for Kapton solar array blanket protection, graphite epoxy structural member protection, and high temperature radiators was performed in an RF plasma asher. Ashing rates for Kapton were correlated with rates measured on STS-8 to determine the exposure time equivalent to one year in low Earth orbit (LEO) at a constant density space station orbital flux. Protective coatings on Kapton from Tekmat, Andus Corporation, and LeRC were evaluated in the plasma asher and mass loss rates per unit area were measured for each sample. All samples evaluated provided some protection to the underlying surface but ion beam sputter deposited samples of SiO2 and SiO2 with 8% polytetrafluoroethylene (PTFE) showed no evidence of degradation after 47 hours of exposure. Mica paint was evaluated as a protective coating for graphite epoxy structural members. Mica appears to be resistant to attack by atomic oxygen but only offers some limited protection as a paint because the paint vehicles evaluated to date were not resistant to atomic oxygen. Four materials were selected for evaluation as candidate radiator materials: stainless steel, copper, niobium-1% zirconium, and titanium-6% aluminum-4% vanadium. These materials were surface textured by various means to improve their emittance. Emittances as high as 0.93 at 2.5 microns for stainless steel and 0.89 at 2.5 microns for Nb-1 Zr were obtained from surface texturing. There were no significant changes in emittance after asher exposure.

  5. Evaluation of nonaqueous processes for nuclear materials

    International Nuclear Information System (INIS)

    A working group was assigned the task of evaluating the status of nonaqueous processes for nuclear materials and the prospects for successful deployment of these technologies in the future. In the initial evaluation, the study was narrowed to the pyrochemical/pyrometallurgical processes closely related to the processes used for purification of plutonium and its conversion to metal. The status of the chemistry and process hardware were reviewed and the development needs in both chemistry and process equipment technology were evaluated. Finally, the requirements were established for successful deployment of this technology. The status of the technology was evaluated along three lines: (1) first the current applications were examined for completeness, (2) an attempt was made to construct closed-cycle flow sheets for several proposed applications, (3) and finally the status of technical development and future development needs for general applications were reviewed. By using these three evaluations, three different perspectives were constructed that together present a clear picture of how complete the technical development of these processes are

  6. Sodium fast reactor evaluation: Core materials

    Science.gov (United States)

    Cheon, Jin Sik; Lee, Chan Bock; Lee, Byoung Oon; Raison, J. P.; Mizuno, T.; Delage, F.; Carmack, J.

    2009-07-01

    In the framework of the Generation IV Sodium Fast Reactor (SFR) Program the Advanced Fuel Project has conducted an evaluation of the available fuel systems supporting future sodium cooled fast reactors. In this paper the status of available and developmental materials for SFR core cladding and duct applications is reviewed. To satisfy the Generation IV SFR fuel requirements, an advanced cladding needs to be developed. The candidate cladding materials are austenitic steels, ferritic/martensitic (F/M) steels, and oxide dispersion strengthened (ODS) steels. A large amount of irradiation testing is required, and the compatibility of cladding with TRU-loaded fuel at high temperatures and high burnup must be investigated. The more promising F/M steels (compared to HT9) might be able to meet the dose requirements of over 200 dpa for ducts in the GEN-IV SFR systems.

  7. Evaluation of Energy Value of Waste Material

    International Nuclear Information System (INIS)

    The evaluation of energy value of waste material is an unavoidable element of a complete national economic development strategy, and also of nature conservation strategy. The exploitation of energy from waste can be realized through direct and indirect measures, which, in every case, demand additional investment and operating costs. Only the complete evaluation of natural resources exploitation can show economic advantages of waste energy valuation. There are additional specific expenses, in relation to the Alternative option of land filling, dependent on the approach accepted and the conditions of the energy valuation of waste. These expenses range from 80 DM per tonne of waste (incineration without co-generation) to more then 300 DM per tonne of waste (for example, complex anaerobic-aerobic biological treatment with the production of bio-gas). (author). 11 refs., 2 tabs

  8. Evaluation of powder metallurgy superalloy disk materials

    Science.gov (United States)

    Evans, D. J.

    1975-01-01

    A program was conducted to develop nickel-base superalloy disk material using prealloyed powder metallurgy techniques. The program included fabrication of test specimens and subscale turbine disks from four different prealloyed powders (NASA-TRW-VIA, AF2-1DA, Mar-M-432 and MERL 80). Based on evaluation of these specimens and disks, two alloys (AF2-1DA and Mar-M-432) were selected for scale-up evaluation. Using fabricating experience gained in the subscale turbine disk effort, test specimens and full scale turbine disks were formed from the selected alloys. These specimens and disks were then subjected to a rigorous test program to evaluate their physical properties and determine their suitability for use in advanced performance turbine engines. A major objective of the program was to develop processes which would yield alloy properties that would be repeatable in producing jet engine disks from the same powder metallurgy alloys. The feasibility of manufacturing full scale gas turbine engine disks by thermomechanical processing of pre-alloyed metal powders was demonstrated. AF2-1DA was shown to possess tensile and creep-rupture properties in excess of those of Astroloy, one of the highest temperature capability disk alloys now in production. It was determined that metallographic evaluation after post-HIP elevated temperature exposure should be used to verify the effectiveness of consolidation of hot isostatically pressed billets.

  9. Synthesis and evaluation of energetic materials

    Science.gov (United States)

    Santhosh, G.

    Over the years new generations of propellants and explosives are being developed. High performance and pollution prevention issues have become the subject of interest in recent years. Desired properties of these materials are a halogen-free, nitrogen and oxygen rich molecular composition with high density and a positive heat of formation. The dinitramide anion is a new oxy anion of nitrogen and forms salts with variety of metal, organic and inorganic cations. Particular interest is in ammonium dinitramide (ADN, NH4N(NO 2)2) which is a potentially useful energetic oxidizer. ADN is considered as one of the most promising substitutes for ammonium perchlorate (AP, NH4ClO4) in currently used composite propellants. It is unique among energetic materials in that it has no carbon or chlorine; its combustion products are not detrimental to the atmosphere. Unquestionable advantage of ADN over AP is the significant improvement in the performance of solid rocket motors by 5-15%. The present thesis is centered on the experimental results along with discussion of some of the most pertinent aspects related to the synthesis and characterization of few dinitramide salts. The chemistry, mechanism and kinetics of the formation of dinitramide salts by nitration of deactivated amines are investigated. The evaluation of the thermal and spectral properties along with the adsorption and thermal decomposition characteristics of the dinitramide salts are also explored in this thesis.

  10. 46 CFR 30.30-3 - Evaluation materials.

    Science.gov (United States)

    2010-10-01

    ... 46 Shipping 1 2010-10-01 2010-10-01 false Evaluation materials. 30.30-3 Section 30.30-3 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY TANK VESSELS GENERAL PROVISIONS Interim Procedures for... materials. The materials to be submitted for evaluation must include the English text of the following:...

  11. Material performance evaluation -Development of the advanced nuclear materials-

    International Nuclear Information System (INIS)

    A multifrequency ACPD system was assembled. A SSRT equipment for stress corrosion cracking test was installed. A 25-ton capacity fatigue test machine was purchased as a first step to assemble a corrosion fatigue test facility. A test loop was designed to simulate the primary water chemistry condition. An Ag/AgCl external reference electrode which can be used at a temperature as high as 280 deg C was fabricated. A high temperature pH electrode was designed for fabrication. A creep test machine was designed conceptually for testing creep behaviors of Zr alloys. Preliminary design requirements were made for the instrumented capsule and a plan was made for using the uninstrumented capsule, as parts of activities to complete an integrated plan of in-reactor materials irradiation test. CHEC computer code which helped improving maintenance program against erosion/corrosion of secondary pipings of nuclear power plants was purchased. Erosion/corrosion of feedwater heater drain line of Kori Unit One was analyzed using the CHEC code as a sample calculation. (Author)

  12. CT Performance Evaluation Using Multi Material Assemblies

    DEFF Research Database (Denmark)

    Stolfi, Alessandro; De Chiffre, Leonardo

    2015-01-01

    This paper concerns an investigation of the accuracy of Computed Tomography measurements using multi-material assemblies. In this study, assemblies involving similar densities for elementary parts were considered. The investigation includes dimensional and geometrical measurements of two 10 mm high...

  13. Tribological evaluation and analysis of coating materials

    Science.gov (United States)

    Miyoshi, Kazuhisa

    1992-01-01

    A physical characterization of coating materials by analytical techniques such as XPS, AES, ellipsometry, and nuclear reaction analysis can contribute to the understanding of adhesion and friction of the coatings and can partially predict the tribological properties of the coatings. This two-part paper describes the tribological properties and physical characteristics of (1) diamondlike carbon (DLC) films and (2) silicon nitride (SiN(x)) films. Emphasis is to relate plasma deposition conditions to the film chemistry and composition and to the adhesion and friction of the films. With the DLC films, the higher the plasma deposition power, the less the hydrogen concentration and the greater the film density and the hardness. The friction behavior of DLC films deposited at higher deposition powers (200 to 300 W) is similar to that of bulk diamond. Even in a vacuum, the DLC films effectively lubricate ceramic surfaces (Si3N4) at temperatures to 500 C. With SiN(x) films, the silicon to nitrogen ratios and the amount of amorphous silicon depend on deposition frequency. The presence of rich amorphous silicon in the high-frequency plasma-deposited SiN(x) films increases their adhesion and friction above 500 C in vacuum.

  14. Evaluation of Eco-Efficiency and Performance of Retrofit Materials

    Science.gov (United States)

    Gopinath, Smitha; Rama Chandra Murthy, A.; Iyer, Nagesh R.; Kokila, S.

    2015-12-01

    In this work three materials namely Fiber Reinforced Polymer (FRP), ferrocement and Textile Reinforced Concrete (TRC) have been evaluated towards their performance efficiency and eco-effectiveness for sustainable retrofitting applications. Investigations have been carried out for flexural strengthening of RC beams with FRP, ferrocement and TRC. It is observed that in the case of FRP, it is not possible to tailor the material according to design requirements and most of the time strengthened structure becomes over stiff. Eco-effectiveness of these retrofitting materials has been evaluated by computing the embodied energy. It is observed that the amount of CO2 emitted by TRC is less compared to other retrofit materials. Further, the performance point of retrofitted RC frames has been evaluated and damage index has been calculated to find out the effective retrofit material. It is concluded that, if RC frame is retrofitted with FRP and TRC, it undergoes less damage compared to ferrocement.

  15. Test and evaluation of pressure vessel materials

    International Nuclear Information System (INIS)

    We have prepared a method for analyzing the Charpy impact test data, which is deduced from ''the standard anelastic solid equation''. The theoretical expression for the absorbed energy is in a form of W=Wsub(U)+(Wsub(R)-Wsub(U))/ [1+(ωtau)2] showing the Debye characteristics and where tau is given by the Arrhenius equation; tau=tau0 exp(ΔH/ksub(B)T). Four measurable parameters, at the present stage, can characterize the dynamic hehavior of cracking (Charpy impact result). They are the upper shelf energy(Wsub(R), the lower shelf energy (Wsub(U)), the activation energy of crack (ΔH, and wtau(0) where w tau(0) are the resonance frequency of the specimen and the jumping pre-exponential factor of propagating crack respectively. However the states of R (relaxed) and U (un-relaxed) should be defined from reasonable physical conditions in the future and it is possible that Wsub(U) is small enough to be taken as zero. The effects of irradiation, alloying elements, and heat treatment on the impact results should be interpreted as changes in the above characteristic parameters. The present method has been applied for weld metal of SA 508-2 irradiated up to a fluence of 4x1018n/cm2, E>1.0Mev, resulting in about 29% decrease in Wsub(R), negligible change in Wsub(U), 5.6 times increase in ωtau0, and no change in ΔH. This seems to indicate that irradiation degrades an average value of YOUNG's modulus so that cracks propagate more easily and it does not effect on breaking the lattice bond. However much more systematic analyses should be necessary for correct judgment. It is concluded that the present method is quite adequate for analyzing the Charpy impact data even though plastic deformation in the specimen was not considered separately so that the method should be applied for various cases in order to evaluate the proper trend of effects of irradiation, alloying elements, and heat treatment on the Charpy impact results. (Author)

  16. Evaluation of corrosion characteristics of SMART materials (III)

    Energy Technology Data Exchange (ETDEWEB)

    Jeong, Y. H.; Park, S. Y.; Baek, J. H.; Choi, B. K.; Park, J. Y.; Lee, M. H.; Kim, J. H.; Bang, J. G

    2006-02-15

    The corrosion characteristics of materials (Low-Sn Zircaloy-4, Zr-1.0Nb, PT-7M, ASTM Gr. 2 Ti, Inconel-690 alloys) for cladding and heat-exchanger tubes of SMART were evaluated in ammonia aqueous solution contained recirculating loop of pH 9.98 at 360 .deg. C 300 .deg. C. And CEDM materials (ball bearing, ball screw, magnetic material) were evaluated in ammonia aqueous solution contained static autoclave of pH 9.98 at 120 .deg. C.

  17. Standards for Evaluations of Educational Programs, Projects, and Materials.

    Science.gov (United States)

    Stufflebeam, Daniel L.

    Thirty specific standards developed as guiding principles to maintain the utility, feasibility, propriety and accuracy of evaluations in educational programs, projects and materials are presented. Utility Standards include Audience Identification, Evaluator Credibility, Information Scope and Selection, Valuational Interpretation, Report Clarity,…

  18. Evaluation for Applied Materials of Eco-technology

    Institute of Scientific and Technical Information of China (English)

    张俊斌; 梁大庆; 陈洁音; 翁韶良

    2005-01-01

    The eco-materials (include natural and artificial material) applied in the eco-technology in internal currently,usually lack of evaluation for applicative conditions.Hence,this study carry on the whole research and identifications to draft the eco-materials of eco-technology.The evaluation models of applied materials for eco-technology were proposed.The quantitative score were obtained by expert's person evaluation.Three models were proposed to quantify the effects of applied materials on the ecological environment.The statistical procedures were adopted to compare the performance of these materials for eco-technology.The results indicated that the comparison of applied materials can be treated by quantitative analysis.For the further analysis,more evaluated data from expert's experience need to be collected then the bias of person subject can be reduced.In addition to reach the benefits in the respects of ecosystem,society,economy and function,also practice the comprehensive effects in eco-technology.

  19. Economic evaluation of closure cap barrier materials study

    International Nuclear Information System (INIS)

    Volume II of the Economic Evaluation of the Closure Cap Barrier Materials, Revision I contains detailed cost estimates for closure cap barrier materials. The cost estimates incorporate the life cycle costs for a generic hazardous waste seepage basin closure cap under the RCRA Post Closure Period of thirty years. The economic evaluation assessed six barrier material categories. Each of these categories consists of several composite cover system configurations, which were used to develop individual cost estimates. The information contained in this report is not intended to be used as a cost estimating manual. This information provides the decision makers with the ability to screen barrier materials, cover system configurations, and identify cost-effective materials for further consideration

  20. Economic evaluation of closure cap barrier materials study

    Energy Technology Data Exchange (ETDEWEB)

    Serrato, M.G.; Bhutani, J.S.; Mead, S.M.

    1993-09-01

    Volume II of the Economic Evaluation of the Closure Cap Barrier Materials, Revision I contains detailed cost estimates for closure cap barrier materials. The cost estimates incorporate the life cycle costs for a generic hazardous waste seepage basin closure cap under the RCRA Post Closure Period of thirty years. The economic evaluation assessed six barrier material categories. Each of these categories consists of several composite cover system configurations, which were used to develop individual cost estimates. The information contained in this report is not intended to be used as a cost estimating manual. This information provides the decision makers with the ability to screen barrier materials, cover system configurations, and identify cost-effective materials for further consideration.

  1. Materials and Nondestructive Evaluation Laboratoriers: User Test Planning Guide

    Science.gov (United States)

    Schaschl, Leslie

    2011-01-01

    The Materials and Nondestructive Evaluation Laboratory process, milestones and inputs are unknowns to first-time users. The Materials and Nondestructive Evaluation Laboratory Planning Guide aids in establishing expectations for both NASA and non- NASA facility customers. The potential audience for this guide includes both internal and commercial spaceflight hardware developers. It is intended to assist their project engineering personnel in materials analysis planning and execution. Material covered includes a roadmap of the analysis process, roles and responsibilities of facility and user, major milestones, facility capabilities, and inputs required by the facility. Samples of deliverables, products, and inputs necessary to define scope of analysis, cost, and schedule are included as an appendix to the guide.

  2. Polymer materials and component evaluation in acidic-radiation environments

    Science.gov (United States)

    Celina, M.; Gillen, K. T.; Malone, G. M.; Clough, R. L.; Nelson, W. H.

    2001-07-01

    Polymeric materials used for cable/wire insulation, electrical connectors, O-rings, seals, and in critical components such as motors, level switches and resistive thermo-devices were evaluated under accelerated degradation conditions in combined radiation-oxidative elevated-temperature acidic-vapor (nitric/oxalic) environments relevant to conditions in isotope processing facilities. Experiments included the assessment of individual materials such as PEEK, polyimides, polyolefin based cable insulation, EPDM rubbers, various epoxy systems, commercial caulking materials as well as some functional testing of components. We discuss how to conduct laboratory experiments to simulate such complex hostile environments, describe some degradation effects encountered, and evaluate the impact on appropriate material and component selection.

  3. Evaluation of Water Resistance and Diffusion Properties of Paint Materials

    Directory of Open Access Journals (Sweden)

    J. Drchalová

    2001-01-01

    Full Text Available A simple method is presented for evaluating the water-proofness quality of paints on lining materials. The method is based on measuring the integral capillarity in dependence on time, and then comparing this value to the value determined for the basic lining material. Measurements of the effective water vapor permeability then provide information on the risk of condensation which may increase after applying the paint. A practical application of the method is performed with four Karlocolor paints on glass concrete substrates. All the Karlocolor paints are found to be very effective materials for driven rain protection. The diffusion properties of all the paints are found to be excellent.

  4. Environmental Evaluation of Building Materials of 5 Slovak Buildings

    Science.gov (United States)

    Porhincak, Milan; Estokova, Adriana

    2013-11-01

    Building activity has recently led to the deterioration of environment and has become unsustainable. Several strategies have been introduced in order to minimize consumption of energy and resulting CO2 emissions having their origin in the operational phase. But also other stages of Life Cycle should are important to identify the overall environmental impact of construction sector. In this paper 5 similar Slovak buildings (family houses) were analyzed in terms of environmental performance of building materials used for their structures. Evaluation included the weight of used materials, embodied energy and embodied CO2 and SO2 emissions. Analysis has proven that the selection of building materials is an important factor which influences the environmental profile. Findings of the case study indicated that materials like concrete, ceramic or thermal insulation materials based on polystyrene and mineral wool are ones with the most negative environmental impact.

  5. The development and evaluation of reference materials for food microbiology.

    NARCIS (Netherlands)

    in 't Veld, P.H.

    1998-01-01

    Since 1986 the National Institute of Public Health and the Environment (RIVM) has worked on the development and evaluation of microbiological reference materials (RMs) with support from the European Communities Bureau of Reference (BCR), now called Standards Measurement and Testing (SM&T). The RMs a

  6. Standard Practice for Evaluating Solar Absorptive Materials for Thermal Applications

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2007-01-01

    1.1 This practice covers a testing methodology for evaluating absorptive materials used in flat plate or concentrating collectors, with concentrating ratios not to exceed five, for solar thermal applications. This practice is not intended to be used for the evaluation of absorptive surfaces that are (1) used in direct contact with, or suspended in, a heat-transfer liquid, (that is, trickle collectors, direct absorption fluids, etc.); (2) used in evacuated collectors; or (3) used in collectors without cover plate(s). 1.2 Test methods included in this practice are property measurement tests and aging tests. Property measurement tests provide for the determination of various properties of absorptive materials, for example, absorptance, emittance, and appearance. Aging tests provide for exposure of absorptive materials to environments that may induce changes in the properties of test specimens. Measuring properties before and after an aging test provides a means of determining the effect of the exposure. 1.3 Th...

  7. Separator Materials Used in Secondary Alkaline Batteries Characterized and Evaluated

    Science.gov (United States)

    1996-01-01

    Nickel-cadmium (Ni/Cd) and nickel-hydrogen (Ni/H2) secondary alkaline batteries are vital to aerospace applications. Battery performance and cycle life are significantly affected by the type of separators used in those batteries. A team from NASA Lewis Research Center's Electrochemical Technology Branch developed standardized testing procedures to characterize and evaluate new and existing separator materials to improve performance and cycle life of secondary alkaline batteries. Battery separators must function as good electronic insulators and as efficient electrolyte reservoirs. At present, new types of organic and inorganic separator materials are being developed for Ni/Cd and Ni/H2 batteries. The separator material previously used in the NASA standard Ni/Cd was Pellon 2505, a 100-percent nylon-6 polymer that must be treated with zinc chloride (ZnCl2) to bond the fibers. Because of stricter Environmental Protection Agency regulation of ZnCl2 emissions, the battery community has been searching for new separators to replace Pellon 2505. As of today, two candidate separator materials have been identified; however, neither of the two materials have performed as well as Pellon 2505. The separator test procedures that were devised at Lewis are being implemented to expedite the search for new battery separators. The new test procedures, which are being carried out in the Separator Laboratory at Lewis, have been designed to guarantee accurate evaluations of the properties that are critical for sustaining proper battery operation. These properties include physical and chemical stability, chemical purity, gas permeability, electrolyte retention and distribution, uniformity, porosity, and area resistivity. A manual containing a detailed description of 12 separator test procedures has been drafted and will be used by the battery community to evaluate candidate separator materials for specific applications. These standardized procedures will allow for consistent, uniform

  8. APPROXIMATE MEANS FOR EVALUATING TENSILE STRENGTH OF HIGH POROSITY MATERIALS

    Institute of Scientific and Technical Information of China (English)

    1999-01-01

    Based on the simplified structure model of high porosity materials, the formulas for approximately evaluating the tensile strength of these materials have been derived from the corresponding deductions taken by means of the relative theories about geometry and mechanics. The results show that, the tensile strength of these materials not only associates with the material sort and production method, but do further have a direct value relationship with the porosity, θ. This value relationship can be specifically expressed by the power of the item (1-θ), and it makes the tensile strength variation display a complicated nonlinear law with the porosity. In addition, the application of those formulas has been investigated with the corresponding experiment on a nickel foam.

  9. Corrosion evaluation of alternate nuclear steam generator tubing materials

    International Nuclear Information System (INIS)

    Several materials were evaluated for use in nuclear steam generators (NSG). These materials were exposed to corrosive conditions representative of those found in nuclear steam generators. The materials evaluated were gold, titanium, tantalum, niobium, Hastelloy C-276, Hastelloy G. Nickel 200, nickel-base Alloy 625, and heat-tracked nickel-base Alloy 600. The test environments simulated acid pitting attack, caustic stress corrosion cracking and reduced sulfur attack. In the pitting environment, the monolithic materials did well, however Nickel 200, nickel-base Alloy 600 and Hastelloy G3 did poorly. The remaining alloys, nickel-base Alloy 625 and Hastelloy C-276 were relatively unaffected in the pitting environment. Tantalum, titanium, niobium, nickel-base Alloy 625 performed poorly in the environment designed to evaluate resistance to caustic cracking. Nickel-base Alloy 600 (stress-relieved), Hastelloy C-276, Hasteloy G-3 and Nickel 200 compared fair to good in the caustic sodium. The gold was unaffected in the hot caustic solution. In the environment selected to represent a reduced sulfur environment, nickel-base Alloy 625 and Hastelloy C-276 exhibited considerable resistance. The nickel-base Alloy 600 was attacked within a relatively short period of time

  10. Systematic Evaluation of Uncertainty in Material Flow Analysis

    DEFF Research Database (Denmark)

    Laner, David; Rechberger, Helmut; Astrup, Thomas Fruergaard

    2014-01-01

    Material flow analysis (MFA) is a tool to investigate material flows and stocks in defined systems as a basis for resource management or environmental pollution control. Because of the diverse nature of sources and the varying quality and availability of data, MFA results are inherently uncertain......) and exploratory MFA (identification of critical parameters and system behavior). Whereas mathematically simpler concepts focusing on data uncertainty characterization are appropriate for descriptive MFAs, statistical approaches enabling more-rigorous evaluation of uncertainty and model sensitivity are needed...

  11. Software for MUF evaluating in item nuclear material accounting

    International Nuclear Information System (INIS)

    Nuclear material accounting is a key measure for nuclear safeguard. Software for MUF evaluation in item nuclear material accounting was worked out in this paper. It is composed of several models, including input model, data processing model, data inquiring model, data print model, system setting model etc. It could be used to check the variance of the measurement and estimate the confidence interval according to the MUF value. To insure security of the data multi-user management function was applied in the software. (authors)

  12. Nondestructive evaluation of critical composite material structural elements

    Science.gov (United States)

    Duke, John C., Jr.; Lesko, John J.; Weyers, R.

    1996-11-01

    A small span bridge that has suffered corrosive deterioration of a number of the steel structural members is in the process of being rehabilitated with glass and carbon fiber reinforced, pultruded polymer structural beams. As part of a comprehensive research program to develop methods for modeling long term durability of the composite material, nondestructive evaluation if being used to provide a preliminary assessment of the initial condition of the beams as well as to monitor the deterioration of the beams during service.

  13. NON DESTRUCTIVE EVALUATION OF COMPOSITE MATERIALS USING ULTRASONIC SPECTROSCOPY

    OpenAIRE

    Ourak, M.; Nongaillard, B.; Rouvaen, J.; Imouloudene, N.

    1990-01-01

    The non destructive evaluation of the carbon epoxy composite materials (often used in aeronautics) is a difficult matter. The classical control methods prove unsatisfactory for the detection of distributed defects (like delaminations and porosities), which affect severely the mechanical properties of composite parts. Ultrasonic echography (A scan mode) allows for the detection of some kinds of delaminations, but the interpretation of the echographic signal remains difficult in the case of por...

  14. Evaluation of radiation-shielding properties of the composite material

    International Nuclear Information System (INIS)

    The paper presents the evaluation of radiation-shielding properties of composite materials with respect to gamma-radiation. As a binder for the synthesis of radiation-shielding composites we used lead boronsilicate glass matrix. As filler we used nanotubular chrysotile filled with lead tungstate PbWO4. It is shown that all the developed composites have good physical-mechanical characteristics, such as compressive strength, thermal stability and can be used as structural materials. On the basis of theoretical calculation we described the graphs of the gamma-quanta linear attenuation coefficient depending on the emitted energy for all investigated composites. We founded high radiation-shielding properties of all the composites on the basis of theoretical and experimental data compared to materials conventionally used in the nuclear industry - iron, concrete, etc

  15. Evaluation of different graft material in type 1 tympanoplasty

    Directory of Open Access Journals (Sweden)

    Kshitij Patil

    2014-01-01

    Full Text Available Aims and Objective: The present study was undertaken to compare the results of various autogeneous tissues temporalis fascia, tragal perichondrium, and fascia lata as graft materials for the type 1 tympanoplasty. Materials and Methods: A total of 120 cases with large, subtotal and total perforation were considered in the study. Of the 120 cases, temporalis fascia graft was used in 60 cases (Group-I, tragal perichondrium graft in 40 cases (Group-II, and fascia lata graft in 20 cases (Group-III. The results were evaluated in the form of rate of graft success, hearing gain, and mean residual air-bone gap with respect to the graft materials. Results and Observation: A nonsignificant association was observed between the groups, that is, temporalis fascia (Group-I, tragal perichondrium (Group-II, and fascia lata (Group-III and the graft uptake. (P = 0.96 > 0.05 and air bone closure (χ2 = 2.908, P = 0.059 > 0.05. Conclusion: The graft take-up rate and Hearing improvement are similar for the different graft materials used. Size of the perforation doesn′t significantly influence the success rate of tympanoplasty as per our study. Normal translucent appearance of neotympanum in the postoperative period was seen only with temporalis fascia, while in tragal perichondrial and fascia lata grafts the neotympanum was whitish, thicker, and translucent to opaque.

  16. Preparation and evaluation of biocomposites as wound dressing material.

    Science.gov (United States)

    Ramnath, V; Sekar, S; Sankar, S; Sankaranarayanan, C; Sastry, T P

    2012-12-01

    Collagen was isolated from the chrome containing leather waste (CCLW) which is a major solid waste in leather industry. Composite films were made using sago starch (SG), soya protein (SY), and collagen (C) and were cross linked with glutaraldehyde (G).The films prepared were characterized for their physico chemical properties like tensile strength, infrared spectra, thermogravimetric analysis, surface morphology, and water absorption studies. Better mechanical properties and surface morphology were observed for SG-SY-G-C films compared to other films prepared using collagen. The composite films prepared were used as wound dressing material on the experimental wounds of rats and healing pattern was evaluated using planimetric, biochemical, and histopathological studies. These studies have revealed better wound healing capacity of SG-SY-G-C film and utilization of CCLW in the preparation of value added product like wound dressing material.

  17. Evaluation Of Shielding Efficacy Of A Ferrite Containing Ceramic Material

    Energy Technology Data Exchange (ETDEWEB)

    Verst, C. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL)

    2015-10-12

    The shielding evaluation of the ferrite based Mitsuishi ceramic material has produced for several radiation sources and possible shielding sizes comparative dose attenuation measurements and simulated projections. High resolution gamma spectroscopy provided uncollided and scattered photon spectra at three energies, confirming theoretical estimates of the ceramic’s mass attenuation coefficient, μ/ρ. High level irradiation experiments were performed using Co-60, Cs-137, and Cf-252 sources to measure penetrating dose rates through steel, lead, concrete, and the provided ceramic slabs. The results were used to validate the radiation transport code MCNP6 which was then used to generate dose rate attenuation curves as a function of shielding material, thickness, and mass for photons and neutrons ranging in energy from 200 keV to 2 MeV.

  18. Quantitative Ultrasonic Evaluation of Mechanical Properties of Engineering Materials

    Science.gov (United States)

    Vary, A.

    1978-01-01

    Progress in the application of ultrasonic techniques to nondestructive measurement of mechanical strength of engineering materials is reviewed. A dormant concept in nondestructive evaluation (NDE) is invoked. The availability of ultrasonic methods that can be applied to actual parts to assess their potential susceptibility to failure under design conditions is discussed. It was shown that ultrasonic methods yield measurements of elastic moduli, microstructure, hardness, fracture toughness, tensile strength, yield strength, and shear strength for a wide range of materials (including many types of metals, ceramics, and fiber composites). It was also indicated that although most of these methods were shown feasible in laboratory studies, more work is needed before they can be used on actual parts in processing, assembly, inspection, and maintenance lines.

  19. Using ABAQUS Scripting Interface for Materials Evaluation and Life Prediction

    Science.gov (United States)

    Powers, Lynn M.; Arnold, Steven M.; Baranski, Andrzej

    2006-01-01

    An ABAQUS script has been written to aid in the evaluation of the mechanical behavior of viscoplastic materials. The purposes of the script are to: handle complex load histories; control load/displacement with alternate stopping criteria; predict failure and life; and verify constitutive models. Material models from the ABAQUS library may be used or the UMAT routine may specify mechanical behavior. User subroutines implemented include: UMAT for the constitutive model; UEXTERNALDB for file manipulation; DISP for boundary conditions; and URDFIL for results processing. Examples presented include load, strain and displacement control tests on a single element model. The tests are creep with a life limiting strain criterion, strain control with a stress limiting cycle and a complex interrupted cyclic relaxation test. The techniques implemented in this paper enable complex load conditions to be solved efficiently with ABAQUS.

  20. Transien elastic wave propagation and nodestructive evaluation of materials

    International Nuclear Information System (INIS)

    This paper summarizes the recent results on the application of transient elastic waves to the nondestructive evaluation of materials. The first part presents the numerical simulation of transient elastic waves propagating in plate structures that contain cracks and/or flaws. In the second part, a newly developed method for the determination of concrete elastic constants is described. The method is based on the measurements of the Rayleigh wave and the skimming longitudinal wave velocities. Also included in this part are the recent developed methods for the detection of surface breaking cracks in concrete using transient elastic waves. Finally, the application of laser generated ultrasonic waves to the nondestructive evaluation of anisotropic elastic constants and the bonding properties of layered specimens are addressed.

  1. Evaluation of microelectrode materials for direct-current electrocorticography

    Science.gov (United States)

    Li, Chunyan; Narayan, Raj K.; Wu, Pei-Ming; Rajan, Neena; Wu, Zhizhen; Mehan, Neal; Golanov, Eugene V.; Ahn, Chong H.; Hartings, Jed A.

    2016-02-01

    Objective. Direct-current electrocorticography (DC-ECoG) allows a more complete characterization of brain states and pathologies than traditional alternating-current recordings (AC-ECoG). However, reliable recording of DC signals is challenging because of electrode polarization-induced potential drift, particularly at low frequencies and for more conducting materials. Further challenges arise as electrode size decreases, since impedance is increased and the potential drift is augmented. While microelectrodes have been investigated for AC-ECoG recordings, little work has addressed microelectrode properties for DC-signal recording. In this paper, we investigated several common microelectrode materials used in biomedical application for DC-ECoG. Approach. Five of the most common materials including gold (Au), silver/silver chloride (Ag/AgCl), platinum (Pt), Iridium oxide (IrOx), and platinum-iridium oxide (Pt/IrOx) were investigated for electrode diameters of 300 μm. The critical characteristics such as polarization impedance, AC current-induced polarization, long-term stability and low-frequency noise were studied in vitro (0.9% saline). The two most promising materials, Pt and Pt/lrOx were further investigated in vivo by recording waves of spreading depolarization, one of the most important applications for DC-ECoG in clinical and basic science research. Main results. Our experimental results indicate that IrOx-based microelectrodes, particularly with composite layers of nanostructures, are excellent in all of the common evaluation characteristics both in vitro and in vivo and are most suitable for multimodal monitoring applications. Pt electrodes suffer high current-induced polarization, but have acceptable long-term stability suitable for DC-ECoG. Major significance. The results of this study provide quantitative data on the electrical properties of microelectrodes with commonly-used materials and will be valuable for development of neural recordings inclusive of

  2. Quality framework proposal for Component Material Evaluation (CME) projects.

    Energy Technology Data Exchange (ETDEWEB)

    Christensen, Naomi G.; Arfman, John F.; Limary, Siviengxay

    2008-09-01

    This report proposes the first stage of a Quality Framework approach that can be used to evaluate and document Component Material Evaluation (CME) projects. The first stage of the Quality Framework defines two tools that will be used to evaluate a CME project. The first tool is used to decompose a CME project into its essential elements. These elements can then be evaluated for inherent quality by looking at the subelements that impact their level of quality maturity or rigor. Quality Readiness Levels (QRLs) are used to valuate project elements for inherent quality. The Framework provides guidance for the Principal Investigator (PI) and stakeholders for CME project prerequisites that help to ensure the proper level of confidence in the deliverable given its intended use. The Framework also Provides a roadmap that defined when and how the Framework tools should be applied. Use of these tools allow the Principal Investigator (PI) and stakeholders to understand what elements the project will use to execute the project, the inherent quality of the elements, which of those are critical to the project and why, and the risks associated to the project's elements.

  3. Corrosive wear. Evaluation of wear and corrosive resistant materials; Noetningskorrosion. Utvaerdering av noetnings- och korrosionsbestaendiga material

    Energy Technology Data Exchange (ETDEWEB)

    Persson, H.; Hjertsen, D.; Waara, P.; Prakash, B.; Hardell, J.

    2007-12-15

    With a new purchase of a waste conveyer screw at hand, for the 'A-warehouse' at the combined power and heating plant at E.ON Norrkoeping, the request for improved construction materials was raised. The previous screw required maintenance with very short intervals due to the difficult operation conditions. With the new screw the expectation is to manage 6 months of operation without interruption. The environment for the screw has two main components that sets the demand on the materials, on one hand the corrosive products that comes along and which forms at digestion of the waste and on the other hand the abrasive content in the waste. The term of the mechanism is wear-corrosion and can give considerably higher material loss than the two mechanisms wear and corrosion separately. Combination of a strong corrosive environment together with extensive wear is something that we today have limited knowledge about. The overall objective of the project has been to establish better wear and corrosive resistant construction materials for a waste conveyer screw that will lead to reduced operational disturbance costs. The evaluation has been performed in both controlled laboratory environments and in field tests, which has given us a better understanding of what materials are more suitable in this tough environment and has given us a tool for future predictions of the wear rate of the different material. The new conveyer screw, installed in February 2007 and with which the field test have been performed, has considerably reduced the wear of the construction and the target of 6 month maintenance-free operation is met with this screw for all the evaluated materials. The wear along the screw varies very much and with a clear trend for all the materials to increase towards the feeding direction of the screw. As an example, the wear plate SS2377 (stainless duplex steel) has a useful life at the most affected areas that is calculated to be 1077 days of operation with the

  4. Production of Working Reference Materials for the Capability Evaluation Project

    Energy Technology Data Exchange (ETDEWEB)

    Phillip D. Noll, Jr.; Robert S. Marshall

    1999-03-01

    Nondestructive waste assay (NDA) methods are employed to determine the mass and activity of waste-entrained radionuclides as part of the National TRU (Trans-Uranic) Waste Characterization Program. In support of this program the Idaho National Engineering and Environmental Laboratory Mixed Waste Focus Area developed a plan to acquire capability/performance data on systems proposed for NDA purposes. The Capability Evaluation Project (CEP) was designed to evaluate the NDA systems of commercial contractors by subjecting all participants to identical tests involving 55 gallon drum surrogates containing known quantities and distributions of radioactive materials in the form of sealed-source standards, referred to as working reference materials (WRMs). Although numerous Pu WRMs already exist, the CEP WRM set allows for the evaluation of the capability and performance of systems with respect to waste types/configurations which contain increased amounts of {sup 241}Am relative to weapons grade Pu, waste that is dominantly {sup 241}Am, as well as wastes containing various proportions of depleted uranium. The CEP WRMs consist of a special mixture of PuO{sub 2}/AmO{sub 2} (IAP) and diatomaceous earth (DE) or depleted uranium (DU) oxide and DE and were fabricated at Los Alamos National Laboratory. The IAP WRMS are contained inside a pair of welded inner and outer stainless steel containers. The DU WRMs are singly contained within a stainless steel container equivalent to the outer container of the IAP standards. This report gives a general overview and discussion relating to the production and certification of the CEP WRMs.

  5. Materials Evaluation Test Series (METS) 04, 05, and 06

    Energy Technology Data Exchange (ETDEWEB)

    Zalk, D; Ingram, C; Simmons, L; Arganbright, R; Lyle, J; Wong, K

    2006-03-23

    The purpose of this work is to examine the environmental, safety, health and operational aspects of detonating a confined explosive test apparatus that has been designed to maximize the dynamics of impact on beryllium metal components for Contained Firing Facility (CFF) applications. A combination of experimental collection and evaluation methods were designed and implemented to provide an evaluation of immediately postdetonation by-products reflecting a potential worst-case scenario beryllium aerosolization explosive event. The collective Material Evaluation Test Series (METS) 04 - 06 provided explosive devices designed to scale for the dedicated METS firing tank that would provide a post-detonation internal environment comparable to the CFF. The experimental results provided appropriate information to develop operational parameters to be considered for conducting full-scale beryllium-containing experimental tests with similar designs within CFF and B801A. These operational procedures include the inclusion of chelating agents in pre-shot CFF cardboard containers with a minimum of 600 gallons content, an extended time period post-test before purging the CFF chamber, and an adaptation of approaches toward applications of the scrubber and HEPA systems during the post-shot sequence for an integrated environmental, safety, and health approach. In addition, re-entry and film retrieval procedures will be adapted, in line with abatement techniques for cleaning the chamber, that will be required for work inside a CFF that will contain an elevated concentration of spherical and highly aerosolizable beryllium particulate.

  6. Proficiency Testing for Evaluating Aerospace Materials Test Anomalies

    Science.gov (United States)

    Hirsch, D.; Motto, S.; Peyton, S.; Beeson, H.

    2006-01-01

    ASTM G 86 and ASTM G 74 are commonly used to evaluate materials susceptibility to ignition in liquid and gaseous oxygen systems. However, the methods have been known for their lack of repeatability. The inherent problems identified with the test logic would either not allow precise identification or the magnitude of problems related to running the tests, such as lack of consistency of systems performance, lack of adherence to procedures, etc. Excessive variability leads to increasing instances of accepting the null hypothesis erroneously, and so to the false logical deduction that problems are nonexistent when they really do exist. This paper attempts to develop and recommend an approach that could lead to increased accuracy in problem diagnostics by using the 50% reactivity point, which has been shown to be more repeatable. The initial tests conducted indicate that PTFE and Viton A (for pneumatic impact) and Buna S (for mechanical impact) would be good choices for additional testing and consideration for inter-laboratory evaluations. The approach presented could also be used to evaluate variable effects with increased confidence and tolerance optimization.

  7. Proposal of risk evaluation methodology for hazardous materials transportation

    International Nuclear Information System (INIS)

    The increasing concern with the level of risk associated with the transportation of hazardous materials took some international institutions to pledge efforts in the evaluation of risk in regional level. Following this trend, the objective of this work was to analyze the most recent processes of analysis of risks from road transportation of hazardous materials. In the present work 21 methodologies of analysis of risks, developed by some authors and for diverse localities have been evaluated. Two of them, in special, have been reviewed and discussed: a method recently developed by the Swiss Federal Institute of Technology (Nicolet-Monnier and Gheorghe, 1996) and the strategy delineated by the Center for Chemical Process Safety CCPS (1995), taking into consideration the estimate of the individual and social risk. Also, the models of Harwood et al. (1990) and of Ramos (1997), adapted by Hartman (2003) have been applied to the reality of the roads of the state of Sao Paulo. The extension of these methodologies was explored, in order to find its advantages and disadvantages. As a study case the present work considered the ammonia transportation throughout two routes evaluating the reality of the roads of the state of Sao Paulo, including a significant parcel of evaluation in a densely populated area, getting the results using risk, at least, one of the methodologies mentioned above. The innovation proposed by this work was the research, the development and the introduction of two variables to the model considered by Harwood et al. (1990). These variables that influence in the value of the risk are: the age of the driver of truck and the zone of impact that is function type of product, period of the day where the transport was carried and the volume that has been transported. The aim of the proposed modifications is to let the value of the risk more sensible in relation to the type of the product carried and the age of the truck driver. The main related procedural stages

  8. Evaluation of an electric field sensor for nondestructive material inspection

    Science.gov (United States)

    Kalyanasundaram, Kayatri; Arunachalam, Kavitha

    2013-01-01

    An electric field sensor is fabricated on a 125 micron thick flexible dielectric substrate for electromagnetic (EM) nondestructive material inspection at 915 MHz. The sensor consists of an electrically short dipole antenna and a radio frequency (RF) diode detector connected to a pair of high impedance screen printed carbon lines. The DC component of the rectified diode voltage conveyed across the high impedance lines is measured using a data acquisition circuit. Sensor measurements are validated with simulated data for a conformal patch antenna operating at 915 MHz. Sensor performance for EM nondestructive testing (NDT) is evaluated using phantom defects in low loss dielectric slabs. Preliminary results indicate sensor utility for EM NDT and support further testing on realistic defects.

  9. Microwave Nondestructive Evaluation of Dielectric Materials with a Metamaterial Lens

    Science.gov (United States)

    Shreiber, Daniel; Gupta, Mool; Cravey, Robin L.

    2008-01-01

    A novel microwave Nondestructive Evaluation (NDE) sensor was developed in an attempt to increase the sensitivity of the microwave NDE method for detection of defects small relative to a wavelength. The sensor was designed on the basis of a negative index material (NIM) lens. Characterization of the lens was performed to determine its resonant frequency, index of refraction, focus spot size, and optimal focusing length (for proper sample location). A sub-wavelength spot size (3 dB) of 0.48 lambda was obtained. The proof of concept for the sensor was achieved when a fiberglass sample with a 3 mm diameter through hole (perpendicular to the propagation direction of the wave) was tested. The hole was successfully detected with an 8.2 cm wavelength electromagnetic wave. This method is able to detect a defect that is 0.037 lambda. This method has certain advantages over other far field and near field microwave NDE methods currently in use.

  10. Material Model Evaluation of a Composite Honeycomb Energy Absorber

    Science.gov (United States)

    Jackson, Karen E.; Annett, Martin S.; Fasanella, Edwin L.; Polanco, Michael A.

    2012-01-01

    A study was conducted to evaluate four different material models in predicting the dynamic crushing response of solid-element-based models of a composite honeycomb energy absorber, designated the Deployable Energy Absorber (DEA). Dynamic crush tests of three DEA components were simulated using the nonlinear, explicit transient dynamic code, LS-DYNA . In addition, a full-scale crash test of an MD-500 helicopter, retrofitted with DEA blocks, was simulated. The four material models used to represent the DEA included: *MAT_CRUSHABLE_FOAM (Mat 63), *MAT_HONEYCOMB (Mat 26), *MAT_SIMPLIFIED_RUBBER/FOAM (Mat 181), and *MAT_TRANSVERSELY_ANISOTROPIC_CRUSHABLE_FOAM (Mat 142). Test-analysis calibration metrics included simple percentage error comparisons of initial peak acceleration, sustained crush stress, and peak compaction acceleration of the DEA components. In addition, the Roadside Safety Verification and Validation Program (RSVVP) was used to assess similarities and differences between the experimental and analytical curves for the full-scale crash test.

  11. Experimental evaluation of cement materials for solidifying sodium nitrate

    International Nuclear Information System (INIS)

    Low-level liquid waste containing sodium nitrate is planned to be transformed to salt block by evaporation with sodium borate in the Low-level Waste Treatment Facility (LWTF), then salt block will be stored temporally. It should be important to investigate the method how to treat these liquid waste suitable to final disposal criteria that will be settled in future. Cement solidification is one of promising candidates because it has been achieved as the solidification material for the shallow land disposal. The research was conducted to evaluate applicability of various cement materials to solidification of sodium nitrate. The following cements were tested. Ordinary Portland Cement (OPC). Portland Blast-furnace Slag Cement; C type (PBFSC). Alkali Activated Slag Cement (AASC, supplied by JGC). The test results are as follows; (1) AASC is characterized by a high sodium nitrate loading (-70 wt%) compared with other types of cement material. High fluidity of the cement paste, high strength after solidification, and minimization of free water on the cement paste are achieved under all test conditions. (2) OOPC and PBFSC produced free water on the cement paste in the early days and delayed the hardening period. 3 or more days are required to harden evan with 30 wt% content of sodium nitrate. (3) Though PBFSC contains blast furnace slag similar to AASC, there is no advantage prior to OPC. To design an ideal cement conditioning system for sodium nitrate liquid waste in the LWTF, the further studies are necessary such as the simulated waste test, Kd test, pilot test, and layout design. (author)

  12. Analyze of histopathelogical for medical devices and biological material on biocompatibility evaluation

    Institute of Scientific and Technical Information of China (English)

    NIE Wei; JIANG Hua; WANG Li; GUAN Jing-fang; SHI Hong-dao

    2001-01-01

    @@ The toxicity and biocompatibility of medical devices and biological material areprominent facts in evaluation of the material. There are two major methods to evaluate the biocompatibility of biological materials . one kind is to do vivo. The materialor extracts are used to study the effect of the material on the growth, metabolismand proliferation of the histocyte.

  13. An Experimental Evaluation of the Application of Smart Damping Materials for Reducing Structural Noise and Vibrations

    OpenAIRE

    Jeric, Kristina Marie

    1999-01-01

    An Experimental Evaluation of the Application of Smart Damping Materials for Reducing Structural Noise and Vibrations Kristina M. Jeric (ABSTRACT) This study evaluates the application of smart damping materials for reducing structural noise and vibrations. The primary purposes of this study are to: 1. Explore the feasibility of smart damping materials, such as piezoelectric materials, for augmenting and improving the noise and v...

  14. Design and evaluation of materials for space reactors

    International Nuclear Information System (INIS)

    The French programme envisages a 20 kWe reactor, project ERATO, with three technological options. The first option is a sodium cooled reactor, derived from the fast breeder reactor technology, (upper core outlet temperature of 7000C). The second option is based on the High Temperature Gas-cooled Reactor technology (outlet temperature range 7000C-9000C). The third option is the reference solution, lithium cooled and UN fuelled fast spectrum reactor, (outlet temperature as high as 12000C). The choice is essentially dominated by material considerations, and more specifically by the problems related to the compatibility with the cooling medium and to the high temperature creep resistance. For the first system limited work will be needed as the technology used is well experimented and there is a wealth of information on the austenitic stainless steel Type 316L-SPH. For the second system, most of the work has been concentrated on characterization of existing commercial alloys. This has included the preselection and the testing of a number of superalloys irradiated or not. The results obtained from high temperature tensile and creep tests have allowed selection of Haynes 230 as the primary candidate material and have also permitted calculation of allowable design stresses for this alloy. For the very high temperature system the French R and D programme has focused on Mo-Re alloys. The results obtained to this date from microstructural examinations and mechanical tests performed on different alloy compositions have allowed selection of Mo-25%Re for future optimization work. They have also shown the need for evaluation of creep properties at low stresses where microstructural instabilities are likely to occur as a result of long exposure to high temperature

  15. Non-destructive evaluation of mechanical properties of magnetic materials

    Energy Technology Data Exchange (ETDEWEB)

    Kankolenski, K.P.; Hua, S.Z.; Yang, D.X.; Hicho, G.E.; Swartzendruber, L.J.; Zang, Z.; Chopra, H.D.

    2000-07-01

    A magnetic-based non-destructive evaluation (NDE) method, which employs Barkhausen effect and measurement of the hysteresis loops, is used to correlate the magnetic and mechanical properties of ultra low carbon (ULC) steel. In particular, the NDE method was used to detect small deviations from linearity that occur in the stress-strain curve well below the 0.2% offset strain, and which generally defines the yield point in materials. Results show that three parameters: jumpsum and jumpsum rate (derived from the Barkhausen spectrum), and the relative permeability (derived from the B-H loops) varies sensitively with small permanent strains, and can be related to the plastic deformation in ULC steels. Investigation of micromagnetic structure revealed that plastic deformation leaves a residual stress state in the samples; the associated magneto-elastic energy makes the favorable easy axis of magnetization in a given grain to be the one that lies closest to the tensile axis. The consequence of this realignment of domains is that wall motion becomes intergranular in nature (as opposed to intragranular in unstrained samples). As a result, the more complex grain boundaries instead of dislocations, become the dominant pinning sites for domain walls. These observations provide a microscopic interpretation of the observed changes in the measured magnetic properties.

  16. Teaching Materials Evaluation and Adaptation of a Unit

    Institute of Scientific and Technical Information of China (English)

    沈化

    2014-01-01

    Teaching materials are quite important for teachers and students. Students only pay attention to interesting materials which can be counted good. Teachers should adapt the materials if they want to make the learning really take place and make their teaching more effective. The teaching materials in Unit 7 Weather in 21st Century Practical College English Viewing, Listen-ing&Speaking I can be counted good. But it is not good enough and needs adapting to make it better.

  17. Evaluation of advanced materials through experimental mechanics and modelling

    Science.gov (United States)

    Yang, Yii-Ching

    1993-01-01

    Composite materials have been frequently used in aerospace vehicles. Very often defects are inherited during the manufacture and damages are inherited during the construction and services. It becomes critical to understand the mechanical behavior of such composite structure before it can be further used. One good example of these composite structures is the cylindrical bottle of solid rocket motor case with accidental impact damages. Since the replacement of this cylindrical bottle is expensive, it is valuable to know how the damages affects the material, and how it can be repaired. To reach this goal, the damage must be characterized and the stress/strain field must be carefully analyzed. First the damage area, due to impact, is surveyed and identified with a shearography technique which uses the principle of speckle shearing interferometry to measure displacement gradient. Within the damage area of a composite laminate, such as the bottle of solid rocket motor case, all layers are considered to be degraded. Once a lamina being degraded the stiffness as well as strength will be drastically decreased. It becomes a critical area of failure to the whole bottle. And hence the stress/strain field within and around a damage should be accurately evaluated for failure prediction. To investigate the stress/strain field around damages a Hybrid-Numerical method which combines experimental measurement and finite element analysis is used. It is known the stress or strain at the singular point can not be accurately measured by an experimental technique. Nevertheless, if the location is far away from the singular spot, the displacement can be found accurately. Since it reflects the true displacement field locally regardless of the boundary conditions, it is an excellent input data for a finite element analysis to replace the usually assumed boundary conditions. Therefore, the Hybrid-Numerical method is chosen to avoid the difficulty and to take advantage of both experimental

  18. Method and Apparatus for Non-Destructive Evaluation of Materials

    Science.gov (United States)

    Goldfine, Neil J. (Inventor); Washabaugh, Andrew P. (Inventor); Lyons, Robert (Inventor); Thomas, Zachary (Inventor); Jablonski, David A. (Inventor); Martin, Christopher (Inventor)

    2015-01-01

    Methods and apparatus for characterizing composite materials for manufacturing quality assurance (QA), periodic inspection during the useful life, or for forensic analysis/material testing. System are provided that relate eddy-current sensor responses to the fiber layup of a composite structure, the presence of impact damage on a composite structure with or without a metal liner, volumetric stress within the composite, fiber tow density, and other NDE inspection requirements. Also provided are systems that determine electromagnetic material properties and material dimensions of composite materials from capacitive sensor inspection measurements. These properties are related to the presence of buried defects in non-conductive composite materials, moisture ingress, aging of the material due to service or environmental/thermal exposure, or changes in manufacturing quality.

  19. Evaluation of waste as a comparative criterion for building materials

    OpenAIRE

    Gómez Soberón, José Manuel Vicente; Gómez Soberón, M. Consolació; Cabrera Covarrubias, Francisca Guadalupe; Corral Higuera, Ramón; Gámez García, Diana C.; Guerrero Díaz, Antonio; Gómez Soberón, Luis Alberto

    2012-01-01

    In this paper, it analyzes and compares the use of three different materials (Reinforced Concrete -R. C.-, Steel and Wood) usable for the building, and construction processes that this entails. The analysis aimed to investigate which of the three materials is the most appropriate from the perspective of sustainability in order to propose alternatives that minimize the impact they have on the environment. Today, concrete is the material most commonly used in construction, and th...

  20. Proactive evaluation of potential and latent materials degradation phenomena

    International Nuclear Information System (INIS)

    A Proactive Materials Degradation Management (PMDM) project has been carried out at the Frontier Research Initiative (FRI), New Industry Creation Hatchery Center, Tohoku University for 5 years, as a part of a Nuclear Industries Safety Agency (NISA, now the Secretariat of the Nuclear Regulation Authority) project that was originally formed in 2007 to define an Aging Management Program that addresses unexpected structural material failures in Light Water Reactors (LWRs). Such a program required, therefore, the development of a life prediction capability for specific combinations of degradation modes, structural materials, and reactor components. In this paper, PIRT results for the aging degradation phenomena in LWR structural materials are introduced. (author)

  1. Evaluation of the radiation resistance of electrical insulation materials

    Science.gov (United States)

    Perrin, Sh.; Schönbacher, H.; Tavlet, M.; Widler, R.

    2002-12-01

    The qualification of insulating materials for electrical cables is often accomplished according to the IEC 60544 standard of the International Electrotechnical Commission. The mechanical properties of the polymeric insulators are tested prior and after irradiation at relatively high dose rates. To assess the ageing of selected materials under realistic service conditions, usually at lower dose rate, an IEC Working Group has proposed extrapolation methods (IEC 61244-2), one of which is applied here for a cable sheathing material from Huber+Suhner. The method is found to be suitable to compare radiation resistance data of different materials irradiated under different conditions.

  2. Development and evaluation of thermoplastic street maintenance material

    Science.gov (United States)

    Siemens, W. D.

    1973-01-01

    An all-weather permanent street patching material was investigated for flexible and rigid pavements. The economic, operational, and material requirements are discussed along with the results of field tests with various mixtures of EVA resins and asphalt. Cost analyses for thermoplastic patching methods are included.

  3. Evaluation of Dielectric-Barrier-Discharge Actuator Substrate Materials

    Science.gov (United States)

    Wilkinson, Stephen P.; Siochi, Emilie J.; Sauti, Godfrey; Xu, Tian-Bing; Meador, Mary Ann; Guo, Haiquan

    2014-01-01

    A key, enabling element of a dielectric barrier discharge (DBD) actuator is the dielectric substrate material. While various investigators have studied the performance of different homogeneous materials, most often in the context of related DBD experiments, fundamental studies focused solely on the dielectric materials have received less attention. The purpose of this study was to conduct an experimental assessment of the body-force-generating performance of a wide range of dielectric materials in search of opportunities to improve DBD actuator performance. Materials studied included commonly available plastics and glasses as well as a custom-fabricated polyimide aerogel. Diagnostics included static induced thrust, electrical circuit parameters for 2D surface discharges and 1D volume discharges, and dielectric material properties. Lumped-parameter circuit simulations for the 1D case were conducted showing good correspondence to experimental data provided that stray capacitances are included. The effect of atmospheric humidity on DBD performance was studied showing a large influence on thrust. The main conclusion is that for homogeneous, dielectric materials at forcing voltages less than that required for streamer formation, the material chemical composition appears to have no effect on body force generation when actuator impedance is properly accounted for.

  4. Comprehensive evaluation and study on material consumption of coal machinery

    Institute of Scientific and Technical Information of China (English)

    ZHENG Jin-fang

    2005-01-01

    Based on fuzzy mathematics, comprehensive comparisons among four kinds of materials for manufacturing shearer bits were made in six aspects which are respectively hardness, tensile strength, impact toughness, relative wearability, relative lifespan and relative cost. Material 4 is preferred to be the targeted choice for manufacturing bits with superior comprehensive and economic performances.

  5. Evaluation of a reference material for glycated haemoglobin

    NARCIS (Netherlands)

    Weykamp, CW; Penders, TJ; Muskiet, FAJ; vanderSlik, W

    1996-01-01

    The use of lyophilized blood as a reference material for glycated haemoglobin was investigated with respect to IFCC criteria for calibrators and control materials. Ninety-two laboratories, using 11 methods, detected no changes in glycated haemoglobin content when the lyophilizate was stored for one

  6. Evaluation of Mutagenicity of Three Eugenol-Containing Materials

    Directory of Open Access Journals (Sweden)

    Narlan Sumawinata

    2015-10-01

    Full Text Available Eugenol containing materials are still widely used, both by the lay people or by the dentist. Professionally it is used to relieve dental pain by placing it in the cavity, or as a mixture for temporary filling, temporary cementation, and root canal sealer. Eugenol, however, is also known to be toxic to the tissue, and aflatoxin, a substance known to be mutagenic, has been found in material labeled as clove oil. The purpose of this study was to investigate the safety of these materials, in particular the mutagenicity. The materials tested were imported eugenol material (95.8% eugenol and local eugenol material (99.5%, both used by dentists and clove-oil material (6.8% eugenol used by the lay people. These materials were assayed in Ames test using Salmonella typhimarium TA 1535 and TA 1537 strain without S-9 mixture. It was shown that all revertants were below the negative control of the test. It was concluded that neither the eugenol used by the dentist nor the clove oil used for suppressing the dental pain by the lay people showed mutagenicity to Salmonella typhimurium TA 1535 and TA 1537 strain.

  7. Evaluation of Student Outcomes in Materials Science and Technology

    Science.gov (United States)

    Piippo, Steven

    1996-01-01

    This paper specifies 14 benchmarks and exit standards for the introduction of Materials Science and Technology in a secondary school education. Included is the standard that students should be able to name an example of each category of technological materials including metals, glass/ceramics, polymers (plastics) and composites. Students should know that each type of solid material has specific properties that can be measured. Students will learn that all solid materials have either a long range crystalline structure or a short range amorphous structure (i.e., glassy). They should learn the choice of materials for a particular application depends on the properties of the material, and the properties of the material depends on its crystal structure and microstructure. The microstructure may be modified by the methods by which the material is processed; students should explain this by the example of sintering a ceramic body to reduce its porosity and increase its densification and strength. Students will receive exposure to the world of work, post secondary educational opportunities, and in general a learning that will lead to a technologically literate intelligent citizen.

  8. Preparation and biological evaluations of PLA/chitosan composite materials

    Institute of Scientific and Technical Information of China (English)

    ZHOU Chang-ren; LI Lihua; DING Shan

    2001-01-01

    @@ INTRODUCTION Polylactic acid (PLA) is a biodegradable material that is hontoxic and biocompatible. However, as scaffold materials, PLA has several obvious weaknesses:biodegrading too fast, acidic degradation product, and hydrophobic. When PLA isplanted in the body, the degradation takes place synchronously.

  9. Use of AWCC in evaluation of unknown fissile materials

    International Nuclear Information System (INIS)

    An important technological problem in the sphere of non-proliferation and safeguards is nondestructive analysis (NDA) methodology for qualitative and quantitative characterization of nuclear materials. Additionally, NDA tends to be labor and time intensive. Two NDA techniques used at KIPT included Gamma Spectroscopy (for qualitative analysis) and Neutron activation (for quantitative analysis). Gamma Spectroscopy was used to confirm the presence of radionuclides within the samples, whereas an Active Well Coincidence Counter (AWCC) in the active mode was used to quantitatively determine the 235U content in particular types of fissile materials at KIPT. This paper describes the usage of the AWCC at NSG KIPT for characterizing nuclear materials for IAEA safeguards. It was also an opportunity to estimate fissile materials of unknown composition. The equipment used was a model JCC-51 AWCC using a shift register model JSR-12 from Canberra and two neutron sources [AN-HP (241ArnLi)]. A Compaq Presario computer using Windows version of NCC (Los Alamos software) was used to operate the AWCC. Materials studied in this project included highly enriched nuclear material in the form of powder, compacts (tablets, microspheres, rods), salt and scrap. The chemical composition of nuclear material included uranium metal, uranium dioxide, uranium nitride, uranium carbonitride, thorium dioxide, and mixtures of these compounds. Scrap consisted of uranium and impurities of hydrocarbons, carbon, silicon, tungsten, etc

  10. Evaluation of Mutagenicity of Three Eugenol-Containing Materials

    OpenAIRE

    Narlan Sumawinata

    2015-01-01

    Eugenol containing materials are still widely used, both by the lay people or by the dentist. Professionally it is used to relieve dental pain by placing it in the cavity, or as a mixture for temporary filling, temporary cementation, and root canal sealer. Eugenol, however, is also known to be toxic to the tissue, and aflatoxin, a substance known to be mutagenic, has been found in material labeled as clove oil. The purpose of this study was to investigate the safety of these materials, in par...

  11. Nondestructive evaluation of a ceramic matrix composite material

    Science.gov (United States)

    Grosskopf, Paul P.; Duke, John C., Jr.

    1992-01-01

    Monolithic ceramic materials have proven their usefulness in many applications, yet, their potential for critical structural applications is limited because of their sensitivity to small imperfections. To overcome this extreme sensitivity to small imperfections, ceramic matrix composite materials have been developed that have the ability to withstand some distributed damage. A borosilicate glass reinforced with several layers of silicon-carbide fiber mat has been studied. Four-point flexure and tension tests were performed not only to determine some of the material properties, but also to initiate a controlled amount of damage within each specimen. Acousto-ultrasonic (AU) measurements were performed periodically during mechanical testing. This paper will compare the AU results to the mechanical test results and data from other nondestructive methods including acoustic emission monitoring and X-ray radiography. It was found that the AU measurements were sensitive to the damage that had developed within the material.

  12. Thermoelectric materials evaluation program spring design to minimize load relaxation

    Energy Technology Data Exchange (ETDEWEB)

    Grimm, F.R.

    1980-03-31

    The recommended spring material for use in thermoelectric modules is either Inconel x or Elgiloy based on their excellent performance and availability. The stress level for generator applications is 75,000 psi. (FS)

  13. Evaluation and development of advanced nuclear materials: IAEA activities

    International Nuclear Information System (INIS)

    Economical, environmental and non-proliferation issues associated with sustainable development of nuclear power bring about a need for optimization of fuel cycles and implementation of advanced nuclear systems. While a number of physical and design concepts are available for innovative reactors, the absence of reliable materials able to sustain new challenging irradiation conditions represents the real bottle-neck for practical implementation of these promising ideas. Materials performance and integrity are key issues for the safety and competitiveness of future nuclear installations being developed for sustainable nuclear energy production incorporating fuel recycling and waste transmutation systems. These systems will feature high thermal operational efficiency, improved utilization of resources (both fissile and fertile materials) and reduced production of nuclear waste. They will require development, qualification and deployment of new and advanced fuel and structural materials with improved mechanical and chemical properties combined with high radiation and corrosion resistance. The extensive, diverse, and expensive efforts toward the development of these materials can be more effectively organized within international collaborative programmes with wide participation of research, design and engineering communities. IAEA carries out a number of international projects supporting interested Member States with the use of available IAEA program implementation tools (Coordinated Research Projects, Technical Meetings, Expert Reviews, etc). The presentation summarizes the activities targeting material developments for advanced nuclear systems, with particular emphasis on fast reactors, which are the focal topics of IAEA Coordinated Research Projects 'Accelerator Simulation and Theoretical Modelling of Radiation Effects' (on-going), 'Benchmarking of Structural Materials Pre-Selected for Advanced Nuclear Reactors', 'Examination of advanced fast reactor fuel and core

  14. Evaluation of nanoparticles in the performance of energetic materials

    OpenAIRE

    José Atílio Fritz Fidel Rocco; Rene Francisco Boschi Gonçalves; Koshun Iha; Gilson da Silva

    2010-01-01

    The addition of nanosized metal particles in propulsion systems such as solid and liquid propellants, hybrid propellant and ramjet motors has recently became a major focus of research. Significant increases in the burning velocity and in the specific impulse are some of the advantages of using nano-scale energetic materials in many different types of propulsion systems. Aluminum has been largely employed as a metallic additive in energetic materials, also in a recently new propulsion system (...

  15. Evaluation of new active packaging materials and analytical approaches

    OpenAIRE

    Lantano, Claudia

    2014-01-01

    This PhD thesis deals with the study of different aspects of food contact materials, including active packaging and food safety controls. In the first part of the present work the development and optimization of a simple and reproducible procedure for the realization of new antimicrobial active packaging materials is presented. The sol-gel technique was employed in order to obtain hybrid organic-inorganic films aimed at incorporating lysozyme and natamycin as active agents. The sols were ...

  16. Bioreceptivity evaluation of cementitious materials designed to stimulate biological growth.

    Science.gov (United States)

    Manso, Sandra; De Muynck, Willem; Segura, Ignacio; Aguado, Antonio; Steppe, Kathy; Boon, Nico; De Belie, Nele

    2014-05-15

    Ordinary Portland cement (OPC), the most used binder in construction, presents some disadvantages in terms of pollution (CO2 emissions) and visual impact. For this reason, green roofs and façades have gain considerable attention in the last decade as a way to integrate nature in cities. These systems, however, suffer from high initial and maintenance costs. An alternative strategy to obtain green facades is the direct natural colonisation of the cementitious construction materials constituting the wall, a phenomenon governed by the bioreceptivity of such material. This work aims at assessing the suitability of magnesium phosphate cement (MPC) materials to allow a rapid natural colonisation taking carbonated OPC samples as a reference material. For that, the aggregate size, the w/c ratio and the amount of cement paste of mortars made of both binders were modified. The assessment of the different bioreceptivities was conducted by means of an accelerated algal fouling test. MPC samples exhibited a faster fouling compared to OPC samples, which could be mainly attributed to the lower pH of the MPC binder. In addition to the binder, the fouling rate was governed by the roughness and the porosity of the material. MPC mortar with moderate porosity and roughness appears to be the most feasible material to be used for the development of green concrete walls.

  17. Bioreceptivity evaluation of cementitious materials designed to stimulate biological growth.

    Science.gov (United States)

    Manso, Sandra; De Muynck, Willem; Segura, Ignacio; Aguado, Antonio; Steppe, Kathy; Boon, Nico; De Belie, Nele

    2014-05-15

    Ordinary Portland cement (OPC), the most used binder in construction, presents some disadvantages in terms of pollution (CO2 emissions) and visual impact. For this reason, green roofs and façades have gain considerable attention in the last decade as a way to integrate nature in cities. These systems, however, suffer from high initial and maintenance costs. An alternative strategy to obtain green facades is the direct natural colonisation of the cementitious construction materials constituting the wall, a phenomenon governed by the bioreceptivity of such material. This work aims at assessing the suitability of magnesium phosphate cement (MPC) materials to allow a rapid natural colonisation taking carbonated OPC samples as a reference material. For that, the aggregate size, the w/c ratio and the amount of cement paste of mortars made of both binders were modified. The assessment of the different bioreceptivities was conducted by means of an accelerated algal fouling test. MPC samples exhibited a faster fouling compared to OPC samples, which could be mainly attributed to the lower pH of the MPC binder. In addition to the binder, the fouling rate was governed by the roughness and the porosity of the material. MPC mortar with moderate porosity and roughness appears to be the most feasible material to be used for the development of green concrete walls. PMID:24602907

  18. ENVIRONMENTAL, ECONOMIC AND ENERGY IMPACTS OF MATERIAL RECOVERY FACILITIES - A MITE PROGRAM EVALUATION

    Science.gov (United States)

    This report documents an evaluation of the environmental, economic, and energy impacts of material recovery facilities (MRFS) conducted under the Municipal Solid Waste Innovative Technology Evaluation (MITE) Program. he MITE Program is sponsored by the U.S. Environmental Protecti...

  19. Use of AWCC in evaluation of unknown fissile materials

    International Nuclear Information System (INIS)

    An important technological problem in the sphere of non-proliferation and safeguards is nondestructive analysis (NDA) methodology for qualitative and quantitative characterization of nuclear materials. Additionally, NDA tends to be labor and time intensive. Two NDA techniques used at KIPT included Gamma Spectroscopy (for qualitative analysis) and Neutron activation (for quantitative analysis). Gamma Spectroscopy was used to confirm the presence of radionuclides within the samples, whereas an Active Well Coincidence Counter (AWCC) in the active mode was used to quantitatively determine the 235U content in particular types of fissile materials at KIPT. This paper describes the usage of the AWCC at NSC KIPT for characterizing nuclear materials for IAEA safeguards. It was also an opportunity to estimate fissile materials of unknown composition. The equipment used was a model JCC-51 AWCC using a shift register model JSR-12 from Canberra and two neutron sources [AN-HP (241AmLi)]. A Compaq Presario computer using Windows version of NCC (Los Alamos software) was used to operate the AWCC. Materials studied in this project included highly enriched nuclear material in the form of powder, compacts (tablets, microspheres, rods), salt and scrap. The chemical composition of nuclear material included uranium metal, uranium dioxide, uranium nitride, uranium carbonitride, thorium dioxide, and mixtures of these compounds. New standards were used to recalibrate the AWCC using material obtained at KIPT with documented compositional values more similar to the materials to be measured, and in similar containers as well. During this study, the AWCC calibration curves were obtained for uranium metal and uranium dioxide with different enrichments up to 90 % for 235U. A broad spectrum of other fissile materials of unknown composition with differing enrichments has also been studied, and the items' isotopic and quantitative compositions have also been determined. Using the new calibration

  20. A Step Forward: Investigating Expertise in Materials Evaluation

    Science.gov (United States)

    Johnson, Keith; Kim, Mija; Ya-Fang, Liu; Nava, Andrea; Perkins, Dawn; Smith, Anne Margaret; Soler-Canela, Oscar; Lu, Wang

    2008-01-01

    This article reports on a study investigating the textbook evaluation techniques of novice and experienced teachers, which was conducted by the Language Teaching Expertise Research Group (or LATEX) within Lancaster University's Department of Linguistics and English Language. Three ELT teachers were chosen to evaluate the student and teacher…

  1. Numerical Evaluation of Mode 1 Stress Intensity Factor as a Function of Material Orientation For BX-265 Foam Insulation Material

    Science.gov (United States)

    Knudsen, Erik; Arakere, Nagaraj K.

    2006-01-01

    Foam; a cellular material, is found all around us. Bone and cork are examples of biological cell materials. Many forms of man-made foam have found practical applications as insulating materials. NASA uses the BX-265 foam insulation material on the external tank (ET) for the Space Shuttle. This is a type of Spray-on Foam Insulation (SOFI), similar to the material used to insulate attics in residential construction. This foam material is a good insulator and is very lightweight, making it suitable for space applications. Breakup of segments of this foam insulation on the shuttle ET impacting the shuttle thermal protection tiles during liftoff is believed to have caused the space shuttle Columbia failure during re-entry. NASA engineers are very interested in understanding the processes that govern the breakup/fracture of this complex material from the shuttle ET. The foam is anisotropic in nature and the required stress and fracture mechanics analysis must include the effects of the direction dependence on material properties. Material testing at NASA MSFC has indicated that the foam can be modeled as a transversely isotropic material. As a first step toward understanding the fracture mechanics of this material, we present a general theoretical and numerical framework for computing stress intensity factors (SIFs), under mixed-mode loading conditions, taking into account the material anisotropy. We present mode I SIFs for middle tension - M(T) - test specimens, using 3D finite element stress analysis (ANSYS) and FRANC3D fracture analysis software, developed by the Cornel1 Fracture Group. Mode I SIF values are presented for a range of foam material orientations. Also, NASA has recorded the failure load for various M(T) specimens. For a linear analysis, the mode I SIF will scale with the far-field load. This allows us to numerically estimate the mode I fracture toughness for this material. The results represent a quantitative basis for evaluating the strength and

  2. Bonding to dentin: evaluation of three adhesive materials.

    Science.gov (United States)

    Sedighi, H; Davila, J M; Gwinnett, A J

    1992-01-01

    Dye penetration was observed in all specimens. SEM demonstrated isolated areas with no gap formation, suggesting a partial bond with dentin. A correlation is evident from the results of both techniques. Since dye-penetration was found to be similar in all the specimens, it was difficult to assess the effect of thermocycling on the amount of dye penetration. The use of posterior composites should be considered as a short-term tested procedure. It should be utilized carefully, following the manufacturer's instructions, and monitored routinely. Undoubtedly, the utilization of posterior composite materials is a very technique-sensitive procedure. Comparing the results of this in vitro study with those previously reported suggests that little improvement has been made in the bonding of the materials tested. Development of new materials and improved techniques are necessary.

  3. Evaluation of refractory materials for a nuclear waste incinerator

    International Nuclear Information System (INIS)

    An experiment to find a suitable refractory lining for a nuclear waste incinerator has been completed. Eleven brick and six castable products were analyzed by optical and scanning microscopy. All the materials were fashioned into cup shapes and subjected to temperatures ranging from 800 to 12000C for as long as six weeks. Some of the cups were charged weekly with pellets made from ash materials that would contact an incinerator liner. Refractory products containing a high percentage of aluminum oxide had the greatest resistance to cracking and slag buildup. 35 figures

  4. Evaluation of different graft material in type 1 tympanoplasty

    OpenAIRE

    Kshitij Patil; Nitish Baisakhiya; Deshmukh, P. T.

    2014-01-01

    Aims and Objective: The present study was undertaken to compare the results of various autogeneous tissues temporalis fascia, tragal perichondrium, and fascia lata as graft materials for the type 1 tympanoplasty. Materials and Methods: A total of 120 cases with large, subtotal and total perforation were considered in the study. Of the 120 cases, temporalis fascia graft was used in 60 cases (Group-I), tragal perichondrium graft in 40 cases (Group-II), and fascia lata graft in 20 cases (Group-I...

  5. Evaluation of diffusing properties of greenhouse covering materials

    NARCIS (Netherlands)

    Hemming, S.; Swinkels, G.L.A.M.; Breugel, van A.J.; Mohammadkhani, V.

    2016-01-01

    Modern greenhouse covering and screen materials are able to transform direct sunlight into diffuse light. After entering the greenhouse the sunlight is scattered and penetrates the crop where it is absorbed and used for photosynthesis. Diffuse light has been shown to increase light interception o

  6. Functional Nanostructured Materials: Synthetic Aspects and Properties Evaluation

    OpenAIRE

    Chen, Fei

    2011-01-01

    In this dissertation, the synthesis of functional nanostructured materials including stimuli responsive nanomat composites, nanoparticles and biodegradable polyester nanofibers are presented. Further the novel properties such as controlled water absorption/desorption, fast thermo responsive properties and potential applications in biomedical and microelectronic fields were investigated. In chapter 4.1, photoresponsive sup...

  7. EFL Learners' Perspectives on ELT Materials Evaluation Relative to Learning Styles

    Science.gov (United States)

    Lee, Bokyung

    2015-01-01

    This paper presents the relationship between Korean EFL learners' self-reporting learning style preferences and their perspectives on ELT materials evaluation. Quantitative data was acquired from 521 subjects' responses to a learning style survey and a questionnaire of materials evaluation checklist. The findings show that Korean EFL learners'…

  8. Survey and evaluation of available thermal insulation materials for use on solar heating and cooling systems

    Energy Technology Data Exchange (ETDEWEB)

    1980-03-01

    This is the final report of a survey and evaluation of insulation materials for use with components of solar heating and cooling systems. The survey was performed by mailing questionnaires to manufacturers of insulation materials and by conducting an extensive literature search to obtain data on relevant properties of various types of insulation materials. The study evaluated insulation materials for active and passive solar heating and cooling systems and for multifunction applications. Primary and secondary considerations for selecting insulation materials for various components of solar heating and cooling systems are presented.

  9. Rare earth boride electron emitter materials fabrication and evaluation

    Science.gov (United States)

    Swanson, L. W.; Davis, P. R.; Gesley, M. A.

    1982-03-01

    Techniques were developed for routine preparation of single crystal rods of LaB6, CeB6 and PrB6 by arc float zone refining. Single crystal, oriented samples were prepared from these rods and mounted as cathodes for testing. Several mounting systems were used, and flat, pointed cone and truncated cone thermionic cathodes were studied. Pointed field emitters of LaB6(100) were also investigated. Variation of thermionic emitted current density and thermal stability of materials were studied as functions of rare earth element, bulk stoichiometry and crystal orientation. Life tests were performed on several different LaB6(100) cathodes. One such cathode operated for over 3000 hours at approximately 10 A/sq cm emitted current density with no serious physical degradation. Surface properties of the materials were investigated by various surface analysis techniques.

  10. Evaluation of electromagnetic absorbing capacity of materials in foundry industry

    Directory of Open Access Journals (Sweden)

    D. Nowak

    2010-01-01

    Full Text Available In the paper, a research on determining the standing wave ratio as a measure of electromagnetic absorbing capacity of moulding materials is presented. Preliminary tests performed using a microwave strip line showed that high-silica, chromite and magnesite moulding sands are characterised by low absorbing capacity of microwaves. It was demonstrated that microwave absorbing capacity is significantly affected by chemical compounds included in the examined substrates. It was found that use of a microwave strip line permits precise determining characteristic microwave absorbing capacities of various moulding materials and thus their suitability for microwave drying/hardening of moulds and cores or for other foundry processes. Such a microwave drier can be applied for identifying mass components and for determining e.g. base granularity by means of precisely determined reflection ratios |Γ| and positions of minimum signal values.

  11. Biological evaluation of dental materials, in vitro and in vivo

    International Nuclear Information System (INIS)

    In this paper, the correlation between the user of tissue culture for in vitro tests and the tissue irritability and pupal response observed in in vitro tests, will be discussed. It would produce confusion if dental materials were standardised with the unreliable parameter of the living system in dynamic balance. Biological tests, both in vitro and in vivo, should be used for pre-standards testing, without any political control to establish physicochemical standards. As a first step, corrosion tests and the dissolution dosje of toxic components from the material in the tissue culture medium and/or artificial salvia should be standardised under conditions simulating the oral environment. The CNC method and photo-pattern analysis are used for the interpretation of cytotoxicity. The need for biological testing, both in vitro and in vivo, definitely exists in order to obtain physicochemical standards, with a biological simulation depending upon the feedback obtained from the results of in vitro and in vivo tests

  12. Evaluation of nanoparticles in the performance of energetic materials

    Directory of Open Access Journals (Sweden)

    José Atílio Fritz Fidel Rocco

    2010-04-01

    Full Text Available The addition of nanosized metal particles in propulsion systems such as solid and liquid propellants, hybrid propellant and ramjet motors has recently became a major focus of research. Significant increases in the burning velocity and in the specific impulse are some of the advantages of using nano-scale energetic materials in many different types of propulsion systems. Aluminum has been largely employed as a metallic additive in energetic materials, also in a recently new propulsion system (aluminum/ice propulsion, “Alice”, and some studies show that the advantages of using nanosized aluminum instead of microsized aluminum are facilitating the ignition of the systems and allowing better incorporation of the components in the formulations and improving its homogeneity. Some of the combustion processes that require high pressures and even higher temperatures can occur in moderate conditions due to the increase of the surface area of the reactants, in this case, the metallic additive.

  13. Quantitative ultrasonic evaluation of mechanical properties of engineering materials

    Science.gov (United States)

    Vary, A.

    1978-01-01

    Current progress in the application of ultrasonic techniques to nondestructive measurement of mechanical strength properties of engineering materials is reviewed. Even where conventional NDE techniques have shown that a part is free of overt defects, advanced NDE techniques should be available to confirm the material properties assumed in the part's design. There are many instances where metallic, composite, or ceramic parts may be free of critical defects while still being susceptible to failure under design loads due to inadequate or degraded mechanical strength. This must be considered in any failure prevention scheme that relies on fracture analysis. This review will discuss the availability of ultrasonic methods that can be applied to actual parts to assess their potential susceptibility to failure under design conditions.

  14. Innovative application of mathematical methods in evaluation of ore raw materials for production of iron

    Directory of Open Access Journals (Sweden)

    P. Besta

    2014-01-01

    Full Text Available Current principles of evaluation of ore raw materials are usually based on a comparison of selected isolated criteria. Today‘s sophisticated technological level of blast furnace process requires the introduction of raw material indicators that provide global characteristics of their quality. This can´t be realized with isolated parameters only. The evaluation should incorporate the key characteristics of iron ore and convert them into a uniform evaluation parameter. This article analyzes the use of mathematical methods in the evaluation of the quality of ore raw materials.

  15. Evaluation of the material assignment method used by a Monte Carlo treatment planning system.

    Science.gov (United States)

    Isambert, A; Brualla, L; Lefkopoulos, D

    2009-12-01

    An evaluation of the conversion process from Hounsfield units (HU) to material composition in computerised tomography (CT) images, employed by the Monte Carlo based treatment planning system ISOgray (DOSIsoft), is presented. A boundary in the HU for the material conversion between "air" and "lung" materials was determined based on a study using 22 patients. The dosimetric consequence of the new boundary was quantitatively evaluated for a lung patient plan.

  16. Evaluation of dimensional stability of autoclavable elastomeric impression material.

    Science.gov (United States)

    Surendra, G P; Anjum, Ayesha; Satish Babu, C L; Shetty, Shilpa

    2011-03-01

    Impressions are important sources of cross contamination between patients and dental laboratories. As a part of infection control impressions contaminated with variety of micro-organisms via blood and oral secretions should be cleaned and disinfected or sterilized before being handled in dental laboratory. The purpose of this study was to determine the effect of autoclaving on dimensional stability of elastomeric impression material (polyvinyl siloxane-Affinis). In this in vitro study standardized stainless steel die as per ADA specification number 19 was fabricated. Polyvinyl siloxane (Affinis) light body and putty viscosity elastomeric impression materials were used. A total of 40 impressions of the stainless steel die were made and numeric coding system was used to identify the samples. Measurements were made using a measuring microscope. Distance between the cross lines CD and C'D' reproduced in the impression were measured before autoclaving, immediately after autoclaving and 24 hours after autoclaving and dimensional change was calculated. The data obtained was subjected to statistical analysis. The mean difference in dimensional change between the three groups was not statistically significant (P > 0.05). However the results revealed that there was higher mean dimensional change immediately after autoclaving when compared to the other 2 time intervals. It is desirable to delay the casting of an autoclavable elastomeric impression material by about 24 hours. Though disinfection of impression is routinely followed autoclaving of impression is an effective method of sterilization.

  17. Evaluation of Cadmium-Free Thick Film Materials on Alumina Substrates

    Energy Technology Data Exchange (ETDEWEB)

    L. H. Perdieu

    2009-09-01

    A new cadmium-free material system was successfully evaluated for the fabrication of thick film hybrid microcircuits at Honeywell Federal Manufacturing & Technologies (FM&T). The characterization involved screen printing, drying and firing two groups of resistor networks which were made using the current material system and the cadmium-free material system. Electrical, environmental and adhesion tests were performed on both groups to determine the more suitable material system. Additionally, untrimmed test coupons were evaluated to further characterize the new materials. The cadmiumfree material system did as well or better than the current material system. Therefore, the new cadmium-free material system was approved for use on production thick film product.

  18. Performance Evaluation of Neutron Absorption Materials with Temperature Change

    Energy Technology Data Exchange (ETDEWEB)

    Jeong, Hae Sun; Jeong, Hyo Joon; Kim, Eun Han; Han, Moon Hee; Hwang, Won Tae [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2015-10-15

    Some of these facilities are operated at higher than room temperature, thus the neutron absorption material can be directly affected by the surrounding environment where the temperature is not maintained in a constant condition. Meanwhile, a nucleus in an atom is continuously vibrated with the thermal energy, after which there arises a range of relative speeds between a neutron and the nucleus, even for a fixed neutron speed. At higher temperature, the random motion of the nucleus reproduces new resonance with a lower and broader peak, i.e., Doppler broadening of a resonance, and the capture cross section of neutron is revised. Therefore, the performance of neutron absorption materials may vary with a change of temperature. In this study, the absorption abilities of three kinds of neutron absorbers generally used in the reactor core were analyzed at a range of temperatures from 293.6K to 584K. As a result, the neutron absorption abilities for B{sup 4}C and Ag-In-Cd do not vary with the change of temperature, while that for Gd{sup 2}O{sup 3} absorbers was shown to be decreased approximately 3% with reference to that at 293.6K in the temperature range between the 293.6K and 584K. This phenomenon of the Gd{sup 2}O{sup 3} absorber seems to be caused by the Doppler broadening of the neutron absorption cross-section. Therefore, it is expected that the effect of material temperature on the neutron absorption performance is needed to be considered in the design of nuclear reactor and the analysis of radiation shielding.

  19. State Education Department: Security over Pupil Evaluation Program and Program Evaluation Test Materials Needs Improvement. Report 91-S-2.

    Science.gov (United States)

    New York State Office of the Comptroller, Albany.

    Findings of an audit of the New York State Education Department's procedures to maintain security over Pupil Evaluation Program (PEP) and Program Evaluation Test (PET) examination materials are presented in this report. The audit sought to determine whether the department's security procedures adequately prevented unauthorized access to exam…

  20. Inverse Approach to Evaluate the Tubular Material Parameters Using the Bulging Test

    OpenAIRE

    Yulong Ge; Xiaoxing Li; Lihui Lang

    2015-01-01

    Tubular material parameters are required for both part manufactory process planning and finite element simulations. The bulging test is one of the most credible ways to detect the property parameters for tubular material. The inverse approach provides more effective access to the accurate material evaluation than with direct identifications. In this paper, a newly designed set of bulging test tools is introduced. An inverse procedure is adopted to determine the tubular material properties in ...

  1. Evaluation of aluminum drill-pipe material and design

    Energy Technology Data Exchange (ETDEWEB)

    Placido, Joao C. [PETROBRAS, Rio de Janeiro, RJ (Brazil); Lourenco, Marcelo I.; Netto, Theodoro Antoun [Universidade Federal do Rio de Janeiro (UFRJ), RJ (Brazil). Coordenacao dos Programas de Pos-graduacao de Engenharia (COPPE)

    2008-07-01

    Experimental program and numerical analyses were carried out to investigate the fatigue mechanisms of aluminum drill pipes designed and manufactured in compliance with ISO 15546. The main objective is to improve the fatigue performance of these components by selecting the appropriate aluminum alloy and by enhancing the mechanical design of the threaded steel connector. This paper presents the experimental test program and numerical analyses conducted on a drill-pipe of different materials (Al-Cu-Mg and Al-Zn-Mg system aluminum alloys) and geometry. Material mechanical properties, including S-N curve, were determined through small-scale tests on specimens cut from actual drill pipes. Full-scale experiments were also performed in laboratory. A finite element model of the drill pipe, including the tool-joint region, was developed. The model simulates, through different load steps, the tool-joint hot assembly, and then reproduces the physical experiments numerically in order to obtain the actual stress distribution. Good correlation between full-scale and small-scale fatigue tests was obtained by adjusting the strain/stress levels monitored in the full-scale tests in light of the numerical simulations and performing fatigue life calculations via multiaxial fatigue models. The weak points of the current practice design are highlighted for further development. (author)

  2. Electrostatic Evaluation of the ARES I FTS Antenna Materials

    Science.gov (United States)

    Hogue, Michael D.; Calle, Carlos I.

    2010-01-01

    Surface resistivity and volume resistivity data show all the tested non-metallic materials of the Ares I FTS antenna assembly to be insulative. The external materials (White foam, phenolic) should be able to develop a large surface charge density upon tribocharging with ice crystal impingement. Dielectric breakdown tests on the FTS antenna housing materials show that each of the insulative materials are very resistive to electrical breakdown. The thicknesses of these materials in a nominal housing should protect the antenna from direct breakdown from external triboelectric charging potentials. Per data from the Air Force study, a maximum external electric potential in the range of 100kV can be developed on surfaces tribocharged by ice crystal impingement. Testing showed that under operational pressure ranges, this level of exterior voltage can result in a potential of about 6 kV induced on the electrically floating interior antenna vanes. Testing the vanes up to this voltage level showed that electrostatic discharges can occur between the electrically floating vanes and the center, grounded screw heads. Repeated tests with multiple invisible and visible discharges caused only superficial physical damage to the vanes. Fourier analysis of the discharge signals showed that the frequency range of credible discharges would not interfere with the nominal operation of the FTS antenna. However, due to the limited scope, short timetable, and limited funding of this study, a direct measurement of the triboelectric charge that could be generated on the Ares I antenna housing when the rocket traverses an ice cloud at supersonic speeds was not performed. Instead, data for the limited Air Force study [3] was used as input for our experiments. The Air Force data used was not collected with a sensor located to provide us with the best approximation at the geometry of the Ares I rocket, namely that of the windshield electrometer, because brush discharges to the metal frame of the

  3. Artificial intelligence to maximise contributions of nondestructive evaluation to materials science and technology

    International Nuclear Information System (INIS)

    The paper reviews the current status of Nondestructive Testing and Evaluation (NDT and E), in relation to materials science and technology. It suggests a path of growth for Nondestructive Testing and Evaluation, taking into account the increase in data and knowledge. We recommend Artificial Intelligence (AI) concepts for maximising the contributions of and benefits from, Nondestructive Testing and Evaluation. (author)

  4. Toward sustainable material usage: evaluating the importance of market motivated agency in modeling material flows.

    Science.gov (United States)

    Gaustad, Gabrielle; Olivetti, Elsa; Kirchain, Randolph

    2011-05-01

    Increasing recycling will be a key strategy for moving toward sustainable materials usage. There are many barriers to increasing recycling, including quality issues in the scrap stream. Repeated recycling can compound this problem through the accumulation of tramp elements over time. This paper explores the importance of capturing recycler decision-making in accurately modeling accumulation and the value of technologies intended to mitigate it. A method was developed combining dynamic material flow analysis with allocation of those materials into production portfolios using blending models. Using this methodology, three scrap allocation methods were explored in the context of a case study of aluminum use: scrap pooling, pseudoclosed loop, and market-based. Results from this case analysis suggest that market-driven decisions and upgrading technologies can partially mitigate the negative impact of accumulation on scrap utilization, thereby increasing scrap use and reducing greenhouse gas emissions. A market-based allocation method for modeling material flows suggests a higher value for upgrading strategies compared to a pseudoclosed loop or pooling allocation method for the scenarios explored. PMID:21438601

  5. Usage of analytical diagnostics when evaluating functional surface material defects

    Directory of Open Access Journals (Sweden)

    R. Frischer

    2015-10-01

    Full Text Available There are occurring defects due to defects mechanisms on parts of production devices surfaces. Outer defects pronouncement is changing throw the time with unequal speed. This variability of defect’s mechanism development cause that is impossible to evaluate technical state of the device in any moment, without the necessary underlying information. Proposed model is based on analytical diagnostics basis. Stochastic model with usage of Weibull probability distribution can assign probability of function surface defect occurrence on the operational information in any moment basis. The knowledge of defect range limiting moment, then enable when and in what range will be necessary to make renewal.

  6. Evaluation of the Performance of Grouting Materials for Saturated Riprap

    OpenAIRE

    Daehyeon Kim; Sinkyu Jung; Kyungsub Cha

    2013-01-01

    In this study, four types of grout were developed to evaluate the effect of grouting of saturated riprap layers on ground water flow. The developed types of grout are divided into a quick-setting type and a general-type, and also into high and low viscosities. A number of grout tests were performed in a model acrylic chamber, 0.4 m in diameter and 2.0 m in length, for visual observation of injection. To reproduce the field flow condition of the saturated riprap layers (approach flow), the gro...

  7. Materials evaluation programs at the Defense Waste Processing Facility

    International Nuclear Information System (INIS)

    The Savannah River Site (SRS) has been operating a nuclear fuel cycle since the 1950s to produce nuclear materials in support of the national defense effort. About 83 million gallons of high-level waste produced since operations began has been consolidated by evaporation into 33 million gallons at the waste tank farm. The Department of Energy authorized the construction of the Defense Waste Processing Facility (DWPF), the function of which is to immobilize the waste as a durable borosilicate glass contained in stainless steel canisters prior to the placement of the canisters in a federal repository. The DWPF is now mechanically complete and is undergoing commissioning and run-in activities. A brief description of the DWPF process is provided

  8. Laser/EMAT measurement systems for materials evaluation

    Energy Technology Data Exchange (ETDEWEB)

    Dewhurst, R J; Dutton, B [Centre for Instrumentation and Analytical Science, School of Chemical Engineering and Analytical Science, Faraday Building, University of Manchester, PO Box 88, Manchester, M60 1QD (United Kingdom)

    2007-07-15

    This paper describes two applications of laser/ electromagnetic acoustic transducer (EMAT) systems. The first application uses laser-generated ultrasound for the characterisation of rear surface artificial defects (vertical slots) in metal samples. An EMAT sensitive to in-plane motion was used to detect these ultrasonic waves. B-scan images were used to visualise any changes of interrogating waves due to defects. These images were generated as the sensor head was moved along the material's surface, forming a 2D intensity profile that revealed changes in the presence of a defect. The defects produced distinctive parabolic features in the images from the time-of-flight diffraction by shear waves. The paper presents a new method based on a generalized Radon transform (GRT) to automatically determine the depth and location of back-surface artificial defects from B-scan images. Experimental evidence validated predicted results for the case of 1.5-3.5 mm-deep defects. The second application uses Rayleigh waves to quantify inhomogeneities in metal alloys using a transient Rayleigh pulse detected with an eight-element EMAT-array. The array spacing established sensor separation, so that velocity measurements were performed independent of the source-to-detector separation. Eliminating this distance, which would normally lead to systematic errors, has produced a measurement system capable of measuring velocities in metal with a precision of 99.9 %. As an example, variations in the Rayleigh wave velocity have characterised the inhomogeneities in rolled bars of aluminium.

  9. An evaluation of epoxy resin phantom materials for electron dosimetry

    Science.gov (United States)

    Nisbet, A.; Thwaites, D. I.

    1998-06-01

    The use of epoxy resin `solid water' (water substitute) phantoms is becoming increasingly common in radiotherapy dosimetry, and depth ionization curves and conversion factors from ionization to dose identical to water have often been assumed. Fluence ratios of water to solid water for WTe (produced by Radiation Physics, St Bartholomew's Hospital, London) and RMI 457 (produced by Radiation Measurements Inc., Middleton, Wisconsin) have therefore been determined and have been found to decrease with energy, which, within measurement uncertainty, can be described with a linear function dependent on mean electron beam energy at the depth of measurement, . The fluence ratios for WTe are very close to unity (i.e. within the measuring uncertainty) for most of the energies examined, the exception being a nominal 20 MeV beam. The results also show that an assumption of unity for the fluence ratios of RMI 457 may introduce a systematic error of the order of 1% in electron beam dosimetry at lower energies. As regards the depth ionization curves measured in the respective solid water materials, these are shown to be in agreement with those measured in water within the limits of the measuring uncertainty.

  10. Archaeometry of ceramic materials: an evaluation of the andalusian experience

    Directory of Open Access Journals (Sweden)

    Cordero Ruiz, Tomás

    2006-06-01

    Full Text Available This paper assesses the impact that the introduction of scientific methods for materials characterisation (conventionally grouped under the label of Archaeometry has had in the methodological configuration of Spanish archaeology over the last two decades. This is achieved through a bibliometric study of publications dealing with characterisation of archaeological ceramics from Andalucía (southern Spain. The variables handled in this study include aspects such as the number of sampled sites and items, their geographical provenance, the chronological and functional dimensions of the archaeological contexts they were taken from as well as the analytical techniques employed in their study.

    Este artículo intenta valorar el impacto que la introducción de métodos de caracterización de materiales procedentes de la física y la química (y agrupados habitualmente bajo la denominación genérica de Arqueometría ha tenido en la configuración metodológica de la investigación arqueológica de nuestro país durante las últimas dos décadas. Para ello se realiza un análisis bibliométrico de un ámbito específico de la aplicación de las técnicas arqueométricas, cual es el de la caracterización de materiales cerámicos dentro de la Arqueología andaluza. Las variables tenidas en cuenta incluyen aspectos tales como la cantidad de sitios arqueológicos muestreados y de muestras analizadas, su procedencia geográfica, los contextos cronológicos y funcionales de los que las muestras fueron tomadas y las técnicas analíticas empleadas.

  11. Evaluation of desiccated and deformed diaspores from natural building materials

    Directory of Open Access Journals (Sweden)

    Tamás Henn

    2015-03-01

    Full Text Available With the increasing sophistication of paleoethnobotanical methods, it is now possible to reconstruct new aspects of the day-to-day life of past peoples, and, ultimately, gain information about their cultivated plants, land-use practices, architecture, diet, and trade. Reliable identification of plant remains, however, remains essential to the study of paleoethnobotany, and there is still much to learn about precise identification. This paper describes and evaluates the most frequent types of deformed desiccated diaspores revealed from adobe bricks used in buildings in Southwestern Hungary that were built primarily between 1850 and 1950. A total of 24,634 diaspores were recovered from 333.05 kg adobe samples. These seeds and fruits belong to 303 taxa, and the majority were arable and ruderal weed species. A total of 98.97% of the diaspores were identified to species. In other cases, identification was possible only to genus or family (0.93% and 0.10% of diaspores, respectively. Difficulties in identification were caused mainly by morphological changes in the size, shape, color, and surface features of diaspores. Most diaspores were darker in color and significantly smaller than fresh or recently desiccated seeds and fruits. Surface features were often absent or fragmented. The most problematic seeds to identify were those of Centaurea cyanus, Consolida regalis, Scleranthus annuus and Daucus carota ssp. carota, which are discussed in detail. Our research aids archaeobotanists in the identification of desiccated and deformed diaspores.

  12. Evaluation of the Performance of Grouting Materials for Saturated Riprap

    Directory of Open Access Journals (Sweden)

    Daehyeon Kim

    2013-12-01

    Full Text Available In this study, four types of grout were developed to evaluate the effect of grouting of saturated riprap layers on ground water flow. The developed types of grout are divided into a quick-setting type and a general-type, and also into high and low viscosities. A number of grout tests were performed in a model acrylic chamber, 0.4 m in diameter and 2.0 m in length, for visual observation of injection. To reproduce the field flow condition of the saturated riprap layers (approach flow, the grout tests were carried out at 0 cm/s and 100 cm/s for the flow speed and 10 L/min for the grout injection speed after installing a flow injection opening on the lower part of the chamber. Based on the results of the grout tests, the injection of each grout in the saturated riprap layers was examined to find out the most effective grout.

  13. Property Evaluation Method Using Spherical Indentation for High-Yield Strength Materials

    Energy Technology Data Exchange (ETDEWEB)

    Choi, Youngsick; Marimuthu, Karuppasamy Pandian; Lee, Hyungyil [Sogang Univ., Seoul (Korea, Republic of); Lee, Jin Haeng [KAERI, Daejeon (Korea, Republic of)

    2015-11-15

    In this paper, we propose a method to evaluate the material properties of high-yield strength materials exceeding 10GPa from spherical indentation. Using a regression equation considering four indentation variables, we map the load displacement relation into a stress-strain relation. To calculate the properties of high-strength materials, we then write a program that produces material properties using the loading / unloading data from the indentation test. The errors in material properties computed by the program are within 0.3, 0.8, and 6.4 for the elastic modulus, yield strength, and hardening coefficient, respectively.

  14. Property evaluation method using spherical indentation for high-yield strength materials

    Energy Technology Data Exchange (ETDEWEB)

    Choi, Young Sick; Marimuthu, Karuppasamy Pandian; Lee, Hyung Yil [Dept. of Mechanical Engineering, Sogang University, Seoul (Korea, Republic of); Lee, Jin Haeng [Reactor Mechanical Engineering Division, Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2015-11-15

    In this paper, we propose a method to evaluate the material properties of high-yield strength materials exceeding 10 GPa from spherical indentation. Using a regression equation considering four indentation variables, we map the load displacement relation into a stress-strain relation. To calculate the properties of high-strength materials, we then write a program that produces material properties using the loading / unloading data from the indentation test. The errors in material properties computed by the program are within 0.3, 0.8, and 6.4 for the elastic modulus, yield strength, and hardening coefficient, respectively.

  15. Evaluation and Modeling of Edge-Seal Materials for Photovoltaic Applications

    Energy Technology Data Exchange (ETDEWEB)

    Kempe, M. D.; Dameron, A. A.; Moricone, T. J.; Reese, M. O.

    2011-02-01

    Because of the sensitivity of some photovoltaic devices to moisture-induced corrosion, they are packaged using impermeable front- and back-sheets along with an edge seal to prevent moisture ingress. Evaluation of edge seal materials can be difficult because of the low permeation rates involved and/or non-Fickian behavior. Here, using a Ca film deposited on a glass substrate, we demonstrate the evaluation of edge seal materials in a manner that effectively duplicates their use in a photovoltaic application and compare the results with standard methods for measuring water vapor transport. We demonstrate how moisture permeation data from polymer films can be used to estimate moisture ingress rates and compare the results of these two methods. Encapsulant materials were also evaluated for comparison and to highlight the need for edge seals. Of the materials studied, desiccant filled polyisobutylene materials demonstrate by far the best potential to keep moisture out for a 20 to 30 year lifetime.

  16. The Cyogenic Evaluation of Irradiated Composite Materials for Use in Composite Pressure Vessels Project

    Data.gov (United States)

    National Aeronautics and Space Administration — HyPerComp Engineering, Inc. (HEI) proposes to continue the characterization of the cryogenic evaluation of irradiated composite materials for use in composite...

  17. To Kit or Not to Kit? Evaluating and Implementing Science Materials and Resources

    Science.gov (United States)

    Schiller, Ellen; Melin, Jacque; Bair, Mary

    2016-01-01

    With the release of the "Next Generation Science Standards," many schools are reexamining the science materials they are using. Textbook companies and kit developers are eager to meet the demand for "NGSS"-aligned teaching materials. Teacher may have been asked to serve on a science curriculum committee, or to evaluate current…

  18. Evaluation of Structure Influence on Thermal Conductivity of Thermal Insulating Materials from Renewable Resources

    Directory of Open Access Journals (Sweden)

    Jolanta VĖJELIENĖ

    2011-07-01

    Full Text Available The development of new thermal insulation materials needs to evaluate properties and structure of raw material, technological factors that make influence on the thermal conductivity of material. One of the most promising raw materials for production of insulation material is straw. The use of natural fibres in insulation is closely linked to the ecological building sector, where selection of materials is based on factors including recyclable, renewable raw materials and low resource production techniques In current work results of research on structure and thermal conductivity of renewable resources for production thermal insulating materials are presented. Due to the high abundance of renewable resources and a good its structure as raw material for thermal insulation materials barley straw, reeds, cattails and bent grass stalks are used. Macro- and micro structure analysis of these substances is performed. Straw bales of these materials are used for determining thermal conductivity. It was found that the macrostructure has the greatest effect on thermal conductivity of materials. Thermal conductivity of material is determined by the formation of a bale due to the large amount of pores among the stalks of the plant, inside the stalk and inside the stalk wall.http://dx.doi.org/10.5755/j01.ms.17.2.494

  19. Toolkit for Evaluating Alignment of Instructional and Assessment Materials to the Common Core State Standards

    Science.gov (United States)

    Achieve, Inc., 2014

    2014-01-01

    In joint partnership, Achieve, The Council of Chief State School Officers, and Student Achievement Partners have developed a Toolkit for Evaluating the Alignment of Instructional and Assessment Materials to the Common Core State Standards (CCSS). The Toolkit is a set of interrelated, freely available instruments for evaluating alignment to the…

  20. IN VITRO TESTING – AN ESENTIAL METHOD FOR EVALUATING THE PERFORMANCE OF DENTAL MATERIALS AND DEVICES

    Directory of Open Access Journals (Sweden)

    Anca VIŢALARIU

    2015-06-01

    Full Text Available Dentistry is unique among biomaterials specialties as to the large variety of materials used, and nature of the challenges they must resist. Intra-oral service demands materials adapted to a warm and moist environment, resisting the attack of digestive acids and enzymes. The materials subjected to mechanical forces should preserve their strength, fatigue and wear characteristics, for accomplishing their function. The wide range of materials available for restorative dentistry demands knowledge of their relative strengths and trade-offs, and offers the opportunity for many interesting lines of research. The spectrum extensively ranges from elastic impression materials to extremely stiff metal and ceramic appliances, so that familiarity with a variety of mechanical testing situations is required from a well-rounded dental materials laboratory. Evaluating the mechanical and wear characteristics of dental restorative materials and analyzing the durability of adhesives is critical to the development of improved dental devices

  1. Evaluation of flexural strength and color stability of different denture base materials including flexible material after using different denture cleansers

    Science.gov (United States)

    Shah, Vrinda R.; Shah, Darshana Nilesh; Chauhan, Chirag J.; Doshi, Paras J.; Kumar, Ashish

    2015-01-01

    Aims: Present study aimed at evaluating the colour stability and flexural strength of flexible denture base materials (Valplast) and Polymethyl methacrylate (PMMA) denture base material (Meliodent) processed by two different methods (Injection moulding and compression moulding) after immersing them in three different denture cleansers with acidic, basic and neutral PH. Methods and Materials: Total 120 specimens (65 × 10 × 3 mm3), 40 specimens of each material (Valplast, Meliodent compression moulding and injection moulding) were immersed in denture cleansers having different PH; Valclean (Acidic), Clinsodent (Basic) and Polident (Neutral) as well as Distilled Water. Color changes were measured with a spectrophotometer after 1 month, 3 months and 6 months of immersion cycle. A flexural 3-point bending test was carried out by using an Instron universal testing machine after 6 months of soaking. Data were analyzed using SPSS software Results: Maximum effect on colour stability was noted with Clinsodent followed by Valclean. Least color changes were observed after immersion in Polident. Colour difference was increased significantly as the immersion time increased. For both Meliodent and Nylon resins, statistically significant change in flexural strength occurred with immersion in all denture cleansers. Clinsodent has greater effect as compared to Valclean and Polident. Conclusions: Polident and Valclean can be safely used as denture cleanser for both nylon and acrylic resin denture base materials as far as colour stability and flexural strength both are concerned. PMID:26929541

  2. Evaluation of written patient educational materials in the field of diagnostic imaging

    Energy Technology Data Exchange (ETDEWEB)

    Ryhaenen, A.M. [Department of Oncology and Radiotherapy, Turku University Hospital, FIN-20521 Turku (Finland)], E-mail: anne.m.ryhanen@tyks.fi; Johansson, K. [Department of Nursing Science, University of Turku, FIN-20014 Turku (Finland)], E-mail: kimajo@utu.fi; Virtanen, H. [Department of Nursing Science, University of Turku, FIN-20014 Turku (Finland)], E-mail: heli.virtanen@utu.fi; Salo, S. [Department of Radiology, Turku University Hospital, FIN-20521 Turku (Finland)], E-mail: sakari.salo@tyks.fi; Salanterae, S. [Department of Nursing Science, University of Turku, FIN-20014 Turku (Finland)], E-mail: sanna.salantera@utu.fi; Leino-Kilpi, H. [Department of Nursing Science, University of Turku, FIN-20014 Turku (Finland)], E-mail: helena.leino-kilpi@utu.fi

    2009-05-15

    Aim: To evaluate the quality of written educational materials for diagnostic imaging (radiological and nuclear medicine) patients. Materials and methods: Written educational materials (n = 70) for diagnostic imaging patients were analysed. The materials were evaluated based on their external appearance (9 criteria), instructiveness (7), content (7), language and structure (8) and readability (1). Deductive content analysis was used. Quantified parts of the analyses were analysed by SAS for Windows. Dependence between criteria (32) was tested by Pearson correlation coefficients. Results: The external appearance fulfilled almost completely the criteria of good written education materials. The instructiveness was addressed clearly, except for the purpose of the material. The contents of materials dealt with bio-physiological, functional and cognitive dimensions of knowledge, while financial dimensions of knowledge were hardly dealt with at all. The language and the structure were reasonably good, but the language was partly in passive voice and the text contained strange words. Most of the education material was moderately easy to read. Conclusions: The results show that the quality of material was quite good in all dimensions. Only a small number of criteria were unsatisfactory. The results can be used to further improve written patient education materials and patient education in the imaging unit.

  3. Application of Systematics in Evaluation of Complete Neutron Data of Structural Material Nuclei

    Institute of Scientific and Technical Information of China (English)

    WANG; Ji-min; TAO; Xi

    2012-01-01

    <正>The evaluation of nuclear data is necessary for practical applications. Usually, there are three ways of obtaining the data for evaluation. They are measurement, calculation and systematics respectively. A complete set neutron data of structural material nuclei are evaluated based on experimental data, and the results of systematics are used for some nuclei or energy regions that the measured data are scarce and

  4. A study of the stress wave factor technique for evaluation of composite materials

    Science.gov (United States)

    Duke, J. C., Jr.; Henneke, E. G., II; Kiernan, M. T.; Grosskopf, P. P.

    1989-01-01

    The acousto-ultrasonic approach for nondestructive evaluation provides a measurement procedure for quantifying the integrated effect of globally distributed damage characteristic of fiber reinforced composite materials. The evaluation procedure provides a stress wave factor that correlates closely with several material performance parameters. The procedure was investigated for a variety of materials including advanced composites, hybrid structure bonds, adhesive bonds, wood products, and wire rope. The research program focused primarily on development of fundamental understanding and applications advancements of acousto-ultrasonics for materials characterization. This involves characterization of materials for which detection, location, and identification of imperfections cannot at present be analyzed satisfactorily with mechanical performance prediction models. In addition to presenting definitive studies on application potentials, the understanding of the acousto-ultrasonic method as applied to advanced composites is reviewed.

  5. Evaluation of Botanical Reference Materials for the Determination of Vanadium in Biological Samples

    DEFF Research Database (Denmark)

    Heydorn, Kaj; Damsgaard, Else

    1982-01-01

    Three botanical reference materials prepared by the National Bureau of Standards have been studied by neutron activation analysis to evaluate their suitability with respect to the determination of vanadium in biological samples. Various decomposition methods were applied in connection with chemic....... A reference value of 1.15 mg/kg of this material is recommended, based on results from 3 different methods. All three materials are preferable to SRM 1571 Orchard Leaves, while Bowen's Kale remains the material of choice because of its lower concentration....

  6. Evaluation of high energy intense neutron source concepts for fusion materials testing

    International Nuclear Information System (INIS)

    Fusion materials testing and development cannot be achieved without a high energy intense neutron source which simulates the fusion reactor neutron environment. Criteria of suitability for a fusion materials irradiation test facility fulfilling the world-wide demand, so-called 'International Fusion Material Irradiation Facility' (IFMIF), were defined in an IEA activity on fusion materials research and development (R and D). Several concepts of IFMIF candidates were proposed. Furthermore, a concept of high energy neutron irradiation facility named 'Energy Selective Neutron Irradiation Test Facility' (ESNIT) was conceived at Japan Atomic Energy Research Institute (JAERI) as a facility for materials researches in generic nuclear applications of which major potential research incentives were originated from nuclear fusion application. In this paper, current evaluation of suitability of various IFMIF and ESNIT concepts for fusion material irradiation testing and their technological feasibility and so on is described. (author)

  7. Groundwater flow evaluation through backfilling materials of a surface coal mining site of Northeast Mexico

    Science.gov (United States)

    Gutierrez-Ojeda, C.; Martínez-Morales, M.; Ortíz-Flores, G.

    2013-05-01

    Surface coal mining at the Allende-Piedras Negras aquifer system requires the complete dewatering and removal of the aquifer. The aquifer contains several geologic layers of variable hydraulic conductivity. Backfilling material is composed of a mixture of permeable and impermeable layers and it was initially considered as impermeable. Exploratory drillings, pumping tests and a geophysical survey were performed in the backfilling materials and the surrounding unaltered materials in order to evaluate the natural groundwater flow modification due to the mining activities. Results of geophysical survey evidenced a saturated water table within the back filling material which was verified by exploratory drilling. Pumping tests showed that unaltered materials have a mean hydraulic conductivity of 34.5 m/day while the backfilling of 5.3 m/day. Although the mining activities reduce the hydraulic conductivity by almost an order of magnitude, it was corroborated the existence of a groundwater flow through the backfilling materials.

  8. EVALUATION AND RECOMMENDATION OF SALTSTONE MIXER AUGER/PADDLES MATERIALS OF CONSTRUCTION FOR IMPROVED WEAR RESISTANCE

    Energy Technology Data Exchange (ETDEWEB)

    Mickalonis, J.; Torres, R.

    2012-08-15

    Wear and corrosion testing were conducted to evaluate alternate materials of construction for the Saltstone mixer auger and paddles. These components have been degraded by wear from the slurry processed in the mixer. Material test options included PVD coatings (TiN, TiCN, and ZrN), weld overlays (Stellite 12 and Ultimet) and higher hardness steels and carbides (D2 and tungsten carbide). The corrosion testing demonstrated that the slurry is not detrimental to the current materials of construction or the new candidates. The ASTM G75 Miller wear test showed that the high hardness materials and the Stellite 12 weld overlay provide superior wear relative to the Astralloy and CF8M stainless steel, which are the current materials of construction, as well as the PVD coatings and Ultimet. The following recommendations are made for selecting new material options and improving the overall wear resistance of the Saltstone mixer components: A Stellite 12 weld overlay or higher hardness steel (with toughness equivalent to Astralloy) be used to improve the wear resistance of the Saltstone mixer paddles; other manufacturing specifications for the mixer need to be considered in this selection. The current use of the Stellite 12 weld overlay be evaluated so that coverage of the 316 auger can be optimized for improved wear resistance of the auger. The wear surfaces of the Saltstone mixer auger and paddles be evaluated so that laboratory data can be better correlated to actual service. The 2-inch Saltstone mixer prototype be used to verify material performance.

  9. Comparative Evaluation of Dimensional Accuracy of Elastomeric Impression Materials when Treated with Autoclave, Microwave, and Chemical Disinfection

    OpenAIRE

    Kamble, Suresh S.; Khandeparker, Rakshit Vijay; Somasundaram, P; Raghav, Shweta; Babaji, Rashmi P; Varghese, T Joju

    2015-01-01

    Background: Impression materials during impression procedure often get infected with various infectious diseases. Hence, disinfection of impression materials with various disinfectants is advised to protect the dental team. Disinfection can alter the dimensional accuracy of impression materials. The present study was aimed to evaluate the dimensional accuracy of elastomeric impression materials when treated with different disinfectants; autoclave, chemical, and microwave method. Materials and...

  10. Test Procedures for Characterizing, Evaluating, and Managing Separator Materials used in Secondary Alkaline Batteries

    Science.gov (United States)

    Guasp, Edwin; Manzo, Michelle A.

    1997-01-01

    Secondary alkaline batteries, such as nickel-cadmium and silver-zinc, are commonly used for aerospace applications. The uniform evaluation and comparison of separator properties for these systems is dependent upon the measurement techniques. This manual presents a series of standard test procedures that can be used to evaluate, compare, and select separator materials for use in alkaline batteries. Detailed test procedures evaluating the following characteristics are included in this manual: physical measurements of thickness and area weight, dimensional stability measurements, electrolyte retention, resistivity, permeability as measured via bubble pressure, surface evaluation via SEM, chemical stability, and tensile strength.

  11. Standard Practice for Evaluating Thermal Insulation Materials for Use in Solar Collectors

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    1994-01-01

    1.1 This practice sets forth a testing methodology for evaluating the properties of thermal insulation materials to be used in solar collectors with concentration ratios of less than 10. Tests are given herein to evaluate the pH, surface burning characteristics, moisture adsorption, water absorption, thermal resistance, linear shrinkage (or expansion), hot surface performance, and accelerated aging. This practice provides a test for surface burning characteristics but does not provide a methodology for determining combustibility performance of thermal insulation materials. 1.2 The tests shall apply to blanket, rigid board, loose-fill, and foam thermal insulation materials used in solar collectors. Other thermal insulation materials shall be tested in accordance with the provisions set forth herein and should not be excluded from consideration. 1.3 The assumption is made that elevated temperature, moisture, and applied stresses are the primary factors contributing to the degradation of thermal insulation mat...

  12. Test Methodology to Evaluate the Safety of Materials Using Spark Incendivity

    Science.gov (United States)

    Buhler, Charles; Calle, Carlos; Clements, Sid; Ritz, Mindy; Starnes, Jeff

    2007-01-01

    For many years scientists and engineers have been searching for the proper test method to evaluate an electrostatic risk for materials used in hazardous environments. A new test standard created by the International Electrotechnical Commission is a promising addition to conventional test methods used throughout industry. The purpose of this paper is to incorporate this test into a proposed new methodology for the evaluation of materials exposed to flammable environments. However, initial testing using this new standard has uncovered some unconventional behavior in materials that conventional test methods were thought to have reconciled. For example some materials tested at higher humidities were more susceptible to incendive discharges than at lower humidity even though the surface resistivity was lower.

  13. The Use of Digital Radiography in the Evaluation of Radioactive Materials. Packaging Performance Testing

    International Nuclear Information System (INIS)

    New designs of radioactive material shipping packages are required to be evaluated in accordance with 10 CFR Part 71, ''Packaging and Transportation of Radioactive Material''. This paper will discuss the use of digital radiography to evaluate the effects of the tests required by 10 CFR 71.71, Normal Conditions of Transport (NCT), and 10 CFR 71.73, Hypothetical Accident Conditions (HAC). One acceptable means of evaluating packaging performance is to subject packagings to the series of NCT and HAC tests. The evaluation includes a determination of the effect on the packaging by the conditions and tests. That determination has required that packagings be cut and sectioned to learn the actual effects on internal components. Digital radiography permits the examination of internal packaging components without sectioning a package. This allows a single package to be subjected to a series of tests. After each test, the package is digitally radiographed and the effects of particular tests evaluated. Radiography reduces the number of packages required for testing and also reduces labor and materials required to section and evaluate numerous packages. This paper will include a description of the digital radiography equipment used in the testing and evaluation of the 9977 and 9978 packages at SRNL. The equipment is capable of making a single radiograph of a full-sized package in one exposure. Radiographs will be compared to sectioned packages that show actual conditions compared to radiographic images

  14. A 3D Osteoblast In Vitro Model for the Evaluation of Biomedical Materials

    OpenAIRE

    Luciana Restle; Daniela Costa-Silva; Emanuelle Stellet Lourenço; Rober Freitas Bachinski; Ana Carolina Batista; Adriana Brandão Ribeiro Linhares; Gutemberg Gomes Alves

    2015-01-01

    Biomedical materials for bone therapy are usually assessed for their biocompatibility and safety employing animal models or in vitro monolayer cell culture assays. However, alternative in vitro models may offer controlled conditions closer to physiological responses and reduce animal testing. In this work, we developed a 3D spheroidal cell culture with potential to evaluate simultaneously material-cell and cell-cell interactions. Different cell densities of murine MC3T3-E1 preosteoblasts or h...

  15. SEM evaluation of pulp reaction to different pulp capping materials in dog’s teeth

    OpenAIRE

    Asgary, Saeed; Parirokh, Masoud; Eghbal, Mohammad Jafar; Ghoddusi, Jamileh

    2007-01-01

    Introduction: This investigation evaluates the effects of mineral trioxide aggregate (MTA), calcium hydroxide (CH) and calcium enriched mixture (CEM) as pulp capping materials on dental pulp tissues. Materials and Methods: The experimental procedures were performed on eighteen intact dog canine teeth. The pulps were exposed. Cavities were randomly filled with CEM, MTA, or CH followed by glass ionomer filling. After 2 months, animals were sacrificed, each tooth was sectioned into halves, and t...

  16. Analysis of difficulties accounting and evaluating nuclear material of PWR fuel plant

    International Nuclear Information System (INIS)

    Background: Nuclear materials accountancy must be developed for nuclear facilities, which is required by regulatory in China. Currently, there are some unresolved problems for nuclear materials accountancy of bulk nuclear facilities. Purpose: The retention values and measurement errors are analyzed in nuclear materials accountancy of Power Water Reactor (PWR) fuel plant to meet the regulatory requirements. Methods: On the basis of nuclear material accounting and evaluation data of PWR fuel plant, a deep analysis research including ratio among random error variance, long-term systematic error variance, short-term systematic error variance and total error involving Material Unaccounted For (MUF) evaluation is developed by the retention value measure in equipment and pipeline. Results: In the equipment pipeline, the holdup estimation error and its total proportion are not more than 5% and 1.5%, respectively. And the holdup estimation can be regraded as a constant in the PWR nuclear material accountancy. Random error variance, long-term systematic error variance, short-term systematic error variance of overall measurement, and analytical and sampling methods are also obtained. A valuable reference is provided for nuclear material accountancy. Conclusion: In nuclear material accountancy, the retention value can be considered as a constant. The long-term systematic error is a main factor in all errors, especially in overall measurement error and sampling error: The long-term systematic errors of overall measurement and sampling are considered important in the PWR nuclear material accountancy. The proposals and measures are applied to the nuclear materials accountancy of PWR fuel plant, and the capacity of nuclear materials accountancy is improved. (authors)

  17. A structure state evaluation method based on electric-thermo-acoustic effect for tension materials

    Science.gov (United States)

    Yin, Aijun; Zhang, Panpan; Ouyang, Qi

    2016-10-01

    The material properties of a structure will change over the course of its service life. Monitoring for material properties can be used to evaluate equipment state. Characterising and tracking variations in properties have promising potential for the detection and evaluation of material state caused by fatigue or residual stress. Theoretical analysis for the formation of a thermo-acoustic effect is carried out and it reveals a kind of interaction between the resonance of gas heat and that of solid heat. This paper introduces an electric-thermo-acoustic model with a multi-layered structure and analyses the effects of the material properties on sound pressure. Based on this effect, a method for evaluating the performance of a multi-layered structure material is proposed that can be used to assess a greater number of physical properties than the existing approaches. The simulations and experiments with variations in material property are generated and processed with the proposed model, and the results verify the method’s efficiency.

  18. TITLE III EVALUATION REPORT FOR THE MATERIAL AND PERSONNEL HANDLING SYSTEM

    Energy Technology Data Exchange (ETDEWEB)

    T. A. Misiak

    1998-05-21

    This Title III Evaluation Report (TER) provides the results of an evaluation that was conducted on the Material and Personnel Handling System. This TER has been written in accordance with the ''Technical Document Preparation Plan for the Mined Geologic Disposal System Title III Evaluation Reports'' (BA0000000-01717-4600-00005 REV 03). The objective of this evaluation is to provide recommendations to ensure consistency between the technical baseline requirements, baseline design, and the as-constructed Material and Personnel Handling System. Recommendations for resolving discrepancies between the as-constructed system, the technical baseline requirements, and the baseline design are included in this report. Cost and Schedule estimates are provided for all recommended modifications.

  19. Inverse Approach to Evaluate the Tubular Material Parameters Using the Bulging Test

    Directory of Open Access Journals (Sweden)

    Yulong Ge

    2015-01-01

    Full Text Available Tubular material parameters are required for both part manufactory process planning and finite element simulations. The bulging test is one of the most credible ways to detect the property parameters for tubular material. The inverse approach provides more effective access to the accurate material evaluation than with direct identifications. In this paper, a newly designed set of bulging test tools is introduced. An inverse procedure is adopted to determine the tubular material properties in Krupkowski-Swift constitutive model of material deformation using a hybrid algorithm that combines the differential evolution and Levenberg-Marquardt algorithms. The constitutive model’s parameters obtained from the conventional and inverse methods are compared, and this comparison shows that the inverse approach is able to offer more information with higher reliability and can simplify the test equipment.

  20. A sparse digital signal model for ultrasonic nondestructive evaluation of layered materials.

    Science.gov (United States)

    Bochud, N; Gomez, A M; Rus, G; Peinado, A M

    2015-09-01

    Signal modeling has been proven to be an useful tool to characterize damaged materials under ultrasonic nondestructive evaluation (NDE). In this paper, we introduce a novel digital signal model for ultrasonic NDE of multilayered materials. This model borrows concepts from lattice filter theory, and bridges them to the physics involved in the wave-material interactions. In particular, the proposed theoretical framework shows that any multilayered material can be characterized by a transfer function with sparse coefficients. The filter coefficients are linked to the physical properties of the material and are analytically obtained from them, whereas a sparse distribution naturally arises and does not rely on heuristic approaches. The developed model is first validated with experimental measurements obtained from multilayered media consisting of homogeneous solids. Then, the sparse structure of the obtained digital filter is exploited through a model-based inverse problem for damage identification in a carbon fiber-reinforced polymer (CFRP) plate. PMID:26092090

  1. Application of GRA for Sustainable Material Selection and Evaluation Using LCA

    Science.gov (United States)

    Jayakrishna, Kandasamy; Vinodh, Sekar; Sakthi Sanghvi, Vijayaselvan; Deepika, Chinadurai

    2016-07-01

    Material selection is identified as a successful key parameter in establishing any product to be sustainable, considering its end of life (EoL) characteristics. An accurate understanding of expected service conditions and environmental considerations are crucial in the selection of material plays a vital role with overwhelming customer expectations and stringent laws. Therefore, this article presents an integrated approach for sustainable material selection using grey relational analysis (GRA) considering the EoL disposal strategies with respect to an automotive product. GRA, an impact evaluation model measures the degree of similarity between the comparability (choice of material) sequence and reference (EoL strategies) sequence based on the relational grade. The ranking result shows that the outranking relationships in the order, ABS-REC > PP-INC > AL-REM > PP-LND > ABS-LND > ABS-INC > PU-LND > AL-REC > AL-LND > PU-INC > AL-INC. The best sustainable material selected was ABS and recycling was selected as the best EoL strategy with the grey relational value of 2.43856. The best material selected by this approach, ABS was evaluated for its viability using life cycle assessment and the estimated impacts also proved the practicability of the selected material highlighting the focus on dehumidification step in the manufacturing of the case product using this developed multi-criteria approach.

  2. Evaluation of Horizon Multimedia Learning Materials for Students with Learning Difficulties and Disabilities.

    Science.gov (United States)

    Barker, Trevor; Jones, Sara; Britton, Carol; Messer, David

    This paper describes the different methods used to evaluate individually configurable multimedia materials developed for the Horizon project, a program designed to increase employment opportunities for students with disabilities or learning difficulties. The project established a working cafe/restaurant in East London staffed by the students. Part…

  3. Optical/Dielectric Properties of Inhomogeneous Optical Material: A New Method of Evaluation

    Science.gov (United States)

    Nagendra, C. L.; Lamb, J. L.

    1993-01-01

    A new method, based on Effective mean Field Theory, is proposed for the evaluation of the optical/dielectric properties of inhomogeneous materials, in which the real and imaginary parts of the dielectric function are determined by solving a simultaneous non-linear equation.

  4. Reading with New Tools: An Evaluation of Personal Digital Assistants as Tools for Reading Course Materials.

    Science.gov (United States)

    Waycott, Jenny

    2002-01-01

    Discussion of using Personal Digital Assistants (PDAs) to read electronic text focuses on a study that evaluated the use of PDAs for reading course materials in an Open University (United Kingdom) master's course. Considers activity theory and how the PDA changed reading, including portability, screen display, navigation difficulties, and…

  5. Evaluation and selection of sensing materials for carbon dioxide (CO 2) sensor by molecular modeling

    NARCIS (Netherlands)

    Chen, X.P.; Wong, C.K.Y.; Yuan, C.A.; Zhang, G.Q.

    2011-01-01

    We report a molecular modeling study to evaluate and select conducting polymers (CPs) as the sensing materials of carbon dioxide (CO2) sensor. The interaction between polymer and gas and the adsorption of the gas molecules in the polymer matrix are investigated. Polymers considered for this work inc

  6. Evaluation and selection of sensing materials for carbon dioxide (CO2) sensor by molecular modeling

    NARCIS (Netherlands)

    Chen, X.P.; Wong, C.K.Y.; Yuan, C.A.; Zhang, G.Q.

    2011-01-01

    We report a molecular modeling study to evaluate and select conducting polymers (CPs) as the sensing materials of carbon dioxide (CO2) sensor. The interaction between polymer and gas and the adsorption of the gas molecules in the polymer matrix are investigated. Polymers considered for this work inc

  7. Focus Group Evaluation of Customized Family Health History Education Materials in a North Carolina Community

    Science.gov (United States)

    Powell, Karen; Edelson, Vaughn; O'Leary, James; Christianson, Carol; Henrich, Vincent

    2011-01-01

    The "Does It Run In The Family?" booklets provide educational materials about family health history (FHH) and basic genetics to readers of all levels and are customizable for local communities. Purpose: The booklets were customized and provided to focus groups to evaluate their usefulness in conveying health information at a low reading level.…

  8. In Vitro Cytotoxicity Evaluation of Three Root-End Filling Materials in Human Periodontal Ligament Fibroblasts.

    Science.gov (United States)

    Coaguila-Llerena, Hernán; Vaisberg, Abraham; Velásquez-Huamán, Zulema

    2016-01-01

    The aim of this study was to evaluate in vitro the cytotoxicity on human periodontal ligament fibroblasts of three root-end filling materials: MTA Angelus®, EndoSequence Root Repair Material Putty® and Super EBA®. A primary culture of human periodontal ligament fibroblasts was previously obtained in order to evaluate the cytotoxicity of the three extracts from the root-end filling materials after 2 and 7 days of setting. Serial dilutions of these extracts (1:1, 1:2, 1:4 and 1:8) were evaluated at 1, 3 and 7 days using the methyl-thiazol-tetrazolium (MTT) colorimetric assay. Cell viability was evaluated as percentage of the negative control group, which represented 100% cell viability. Statistical analyses were done with t-test, ANOVA and Kruskal-Wallis test at a significance level of 5%. It was found that the main difference among root-end filling materials was in the higher dilutions (p0.05). Cell viability of MTA Angelus® was superior for 2-day setting (pEBA® showed the lowest percentage of cell viability at higher dilutions (pEBA®. PMID:27058382

  9. Evaluation of the high-temperature materials programme of the Joint Research Centre (1980-85)

    International Nuclear Information System (INIS)

    This report covers the findings of the external panel of experts set up to evaluate the results of the Community's programme in the field of high-temperature materials (1980-85), carried out at the Petten establishment of the Joint Research Centre. The evaluation covers the quality and relevance of the research, the usefulness of the results and the role played by the JRC in this field at the European level. The report describes and gives comments on the content, structure and management of the five projects constituting the current programme, outlines the methods and procedures used during the evaluation and gives a number of recommendations pertinent to future activities

  10. A new method to evaluate the hydraulic activity of Al-Si materials

    Institute of Scientific and Technical Information of China (English)

    2008-01-01

    Slag,fly ash,gangue and 500℃ calcined gangue are analyzed by using identical coupled plasma optical emission spectroscopy (ICP),X-ray photoelectron spec-troscopy (XPS),infrared spectroscopy (IR) and magnetic angle spinning nuclear magnetic resonance (MAS NMR). Research results show that there is a negative linear relationship between the Si 2p and Al 2p binding energies of Al-Si materials and the compressive strength of aluminosilicate based cementitious materials prepared with these Al-Si materials,i.e. the lower the binding energies,the higher the compressive strength. Indeed,the Si 2p and Al 2p binding energies of Al-Si materials can be used to indicate their hydraulic activity. The binding energies of the four examined materials increase in the order of slag,fly ash,500℃ calcined gangue and untreated gangue. Moreover,the binding energies of Si 2p,Al 2p and O 1s of every Al-Si material have excellent correlation. By using the Al 2p binding energy and 27Al MAS NMR spectra,the coordination number of aluminum in slag is determined to be four,while that in gangue,is six. Based on the aforementioned discoveries,this paper presents a new effective method to evaluate the hydraulic activity of Al-Si materials by using the surface binding energies of silicon and alu-minum of Al-Si materials.

  11. A new method to evaluate the hydraulic activity of Al-Si materials

    Institute of Scientific and Technical Information of China (English)

    LI HuaJian; SUN HengHu; TIE XuChu; XIAO XueJun

    2008-01-01

    Slag, fly ash, gangue and 500℃ calcined gangue are analyzed by using identical coupled plasma optical emission spectroscopy (ICP), X-ray photoelectron spectroscopy (XPS), infrared spectroscopy (IR) and magnetic angle spinning nuclear magnetic resonance (MAS NMR). Research results show that there is a negative linear relationship between the Si 2p and Al 2p binding energies of Al-Si materials and the compressive strength of aluminosilicate based cementitious materials prepared with these Al-Si materials, i.e. the lower the binding energies, the higher the compressive strength. Indeed, the Si 2p and Al 2p binding energies of Al-Si materials can be used to indicate their hydraulic activity. The binding energies of the four examined materials increase in the order of slag, fly ash, 500℃ calcined gangue and untreated gangue. Moreover, the binding energies of Si 2p, Al 2p and O 1s of every Al-Si material have excellent correlation. By using the Al 2p binding energy and 27AI MAS NMR spectra, the coordination number of aluminum in slag is determined to be four, while that in gangue, is six. Based on the aforementioned discoveries, this paper presents a new effective method to evaluate the hydraulic activity of Al-Si materials by using the surface binding energies of silicon and aluminum of Al-Si materials.

  12. Cytotoxicity evaluation of root repair materials in human-cultured periodontal ligament fibroblasts

    Directory of Open Access Journals (Sweden)

    Voruganti Samyuktha

    2014-01-01

    Full Text Available Aim: To evaluate the cytotoxicity of three root repair materials, mineral trioxide aggregate (MTA, Endosequence Root Repair Material and Biodentine in human periodontal ligament fibroblasts. Materials and Methods: Periodontal ligament fibroblasts were cultured from healthy premolar extracted for orthodontic purpose. Cells in the third passage were used in the study. The cultured fibroblast cells were placed in contact with root repair materials: (a Biodentine, (b MTA, (c Endosequence, (d control. The effects of these three materials on the viability of Periodontal ligament (PDL fibroblasts were determined by trypan blue dye assay after 24 hours and 48-hour time period. Cell viability was determined using inverted phase contrast microscope. Statistical Analysis: Cell viability was compared for all the experimental groups with Wilcoxons matched pair test. Results: At the 24-hour examination period, all the materials showed increased cell viability. At 48-hour time period, there is slight decrease in cell viability. Mineral trioxide aggregate showed statistically significant increase in the cell viability when compared to other root repair materials. Conclusion: Mineral trioxide aggregate was shown to be less toxic to periodontal ligament fibroblasts than Endosequence Root Repair Material and Biodentine.

  13. An in vitro comparative evaluation of physical properties of four different types of core materials

    Directory of Open Access Journals (Sweden)

    Antara Agrawal

    2014-01-01

    Full Text Available Introduction: Compressive and tensile stresses of core materials are important properties because cores usually replace a large bulk of tooth structure and must resist multidirectional masticatory forces for many years. Material and Methods: The present study was undertaken to find out the best core build up material with respect to their physical properties among resin-based composites. Individual compressive, tensile, and flexural strength of fiber-reinforced dual cure resin core build up material, silorane-based composite resin, and dual curing composite for core build up with silver amalgam core was used as control were evaluated and compared using universal testing machine. Data were statistical analysed using Kruskal-Wallis test to determine whether statistically significant differences (P < 0.05 existed among core materials. Both dual cure composite materials with nanofillers were found superior to amalgam core. The silorane-based material showed the highest flexural strength, but other mechanical properties were inferior to dual cure composite materials with nanofillers.

  14. Environmental, economic, and energy impacts of material recovery facilities. A MITE Program evaluation

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1995-10-01

    This report documents an evaluation of the environmental, economic, and energy impacts of material recovery facilities (MRFs) conducted under the Municipal Solid Waste Innovative Technology Evaluation (MITE) Program. The MITE Program is sponsored by the US Environmental Protection Agency to foster the demonstration and development of innovative technologies for the management of municipal solid waste (MSW). This project was also funded by the National Renewable Energy Laboratory (NREL). Material recovery facilities are increasingly being used as one option for managing a significant portion of municipal solid waste (MSW). The owners and operators of these facilities employ a combination of manual and mechanical techniques to separate and sort the recyclable fraction of MSW and to transport the separated materials to recycling facilities.

  15. Evaluating simulant materials for understanding cranial backspatter from a ballistic projectile.

    Science.gov (United States)

    Das, Raj; Collins, Alistair; Verma, Anurag; Fernandez, Justin; Taylor, Michael

    2015-05-01

    In cranial wounds resulting from a gunshot, the study of backspatter patterns can provide information about the actual incidents by linking material to surrounding objects. This study investigates the physics of backspatter from a high-speed projectile impact and evaluates a range of simulant materials using impact tests. Next, we evaluate a mesh-free method called smoothed particle hydrodynamics (SPH) to model the splashing mechanism during backspatter. The study has shown that a projectile impact causes fragmentation at the impact site, while transferring momentum to fragmented particles. The particles travel along the path of least resistance, leading to partial material movement in the reverse direction of the projectile motion causing backspatter. Medium-density fiberboard is a better simulant for a human skull than polycarbonate, and lorica leather is a better simulant for a human skin than natural rubber. SPH is an effective numerical method for modeling the high-speed impact fracture and fragmentations. PMID:25739515

  16. Designing and Evaluating a Scientific Training Program and Virtual Learning Materials.

    Science.gov (United States)

    van Raalte, Lisa; Boulay, Rachel

    2013-01-01

    The University of Hawaii's John A. Burns School of Medicine developed a professional development program and virtual learning materials to assist high school science teachers become familiar with laboratory techniques prior to engaging in authentic molecular biology research. The purpose of this paper is to provide an evaluative overview of the program with emphasis on the virtual materials that were designed to employ a blended learning approach to augment offline classroom learning. The virtual learning materials provide a unique sphere for scientific learning in which skills can be reproduced in an offline environment. Twelve high school science teachers participated in the training program and were given full access to the online materials. After participation in the program, teachers filled out a final survey and completed a final written reflective statement as a form of evaluating the program and online materials. Thematic analysis was used to code participants' responses. Results showed that teachers recounted meeting the scientists as a valuable experience, teachers were grateful to learn real-world application of current research, and teachers described the importance of learning skills to prepare students to succeed in higher education. Additionally, results showed teacher's intent to use the virtual learning materials as homework tools and in classroom lessons. PMID:24524091

  17. Flow Chamber System for the Statistical Evaluation of Bacterial Colonization on Materials

    Directory of Open Access Journals (Sweden)

    Friederike Menzel

    2016-09-01

    Full Text Available Biofilm formation on materials leads to high costs in industrial processes, as well as in medical applications. This fact has stimulated interest in the development of new materials with improved surfaces to reduce bacterial colonization. Standardized tests relying on statistical evidence are indispensable to evaluate the quality and safety of these new materials. We describe here a flow chamber system for biofilm cultivation under controlled conditions with a total capacity for testing up to 32 samples in parallel. In order to quantify the surface colonization, bacterial cells were DAPI (4`,6-diamidino-2-phenylindole-stained and examined with epifluorescence microscopy. More than 100 images of each sample were automatically taken and the surface coverage was estimated using the free open source software g’mic, followed by a precise statistical evaluation. Overview images of all gathered pictures were generated to dissect the colonization characteristics of the selected model organism Escherichia coli W3310 on different materials (glass and implant steel. With our approach, differences in bacterial colonization on different materials can be quantified in a statistically validated manner. This reliable test procedure will support the design of improved materials for medical, industrial, and environmental (subaquatic or subaerial applications.

  18. Health evaluation of volatile organic compound (VOC) emissions from wood and wood-based materials.

    Science.gov (United States)

    Jensen, L K; Larsen, A; Mølhave, L; Hansen, M K; Knudsen, B

    2001-01-01

    In this study, the authors describe a method for evaluation of material emissions. The study was based on chemical analysis of emissions from 23 materials representing solid wood and wood-based materials commonly used in furniture, interior furnishings, and building products in Denmark in the 1990s. The authors used the emission chamber testing method to examine the selected materials with a qualitative screening and quantitative determination of volatile organic compounds. The authors evaluated the toxicological effects of all substances identified with chamber testing. Lowest concentration of interest and standard room concentrations were assessed, and the authors calculated an S-value for each wood and wood-based material. The authors identified 144 different chemical substances with the screening analyses, and a total of 84 individual substances were quantified with chamber measurements. The irritative effects dominated at low exposure levels; therefore, the lowest concentration of interest and the S-value were based predominantly on these effects. The S-values were very low for solid ash, oak, and beech. For solid spruce and pine, the determining substances for size of the S-value were delta3-carene, alpha-pinene, and limonene. For the surface-treated wood materials, the S-value reflected the emitted substances from the surface treatment. PMID:11777023

  19. Evaluation of Survival Time of Tooth Color Dental Materials in Primary Anterior Teeth

    Directory of Open Access Journals (Sweden)

    Behjat-Al-Molook Ajami

    2013-01-01

    Full Text Available Introduction: In restorative dentistry, selecting the proper material is an important factor for clinical success. The objective of this study was clinical evaluation of survival time of three tooth color materials in primary anterior teeth. Methods: In this interventional clinical trial study, 94 deciduous anterior teeth (36 teeth in boys, 58 teeth in girls belonging to 3-5 year old children in Pediatric Department of Mashhad Faculty of Dentistry, Iran were selected. Selective dental materials included compoglass, glass-ionomer Fuji II LC, and composite resin. The data were analyzed with Kaplan–Meyer and Log rank test. Results: compoglass had the highest survival time in comparison with composite and glass-ionomer. Nine months retention rate for teeth restored with compoglass, composite resin and glass-ionomer were estimated: 95%, 21%, and 12.5%, respectively. Conclusion: Compoglass can be a suitable material for anterior primary teeth restoration

  20. Evaluation of Survival Time of Tooth Color Dental Materials in Primary Anterior Teeth

    Directory of Open Access Journals (Sweden)

    Taraneh Movahhed

    2012-09-01

    Full Text Available Introduction: In restorative dentistry, selecting the proper material is an important factor for clinical success. The objective of this study was clinical evaluation of survival time of three tooth color materials in primary anterior teeth. Methods: In this interventional clinical trial study, 94 deciduous anterior teeth (36 teeth in boys, 58 teeth in girls belonging to 3-5 year old children in Pediatric Department of Mashhad Faculty of Dentistry, Iran were selected. Selective dental materials included compoglass, glass-ionomer Fuji II LC, and composite resin. The data were analyzed with Kaplan–Meyer and Log rank test. Results: compoglass had the highest survival time in comparison with composite and glass-ionomer. Nine months retention rate for teeth restored with compoglass, composite resin and glass-ionomer were estimated: 95%, 21%, and 12.5%, respectively. Conclusion: Compoglass can be a suitable material for anterior primary teeth restoration.

  1. Nondestructive Evaluation Approaches Developed for Material Characterization in Aeronautics and Space Applications

    Science.gov (United States)

    Baaklini, George Y.; Kautz, Harold E.; Gyekenyesi, Andrew L.; Abdul-Aziz, Ali; Martin, Richard E.

    2001-01-01

    At the NASA Glenn Research Center, nondestructive evaluation (NDE) approaches were developed or tailored for characterizing advanced material systems. The emphasis was on high-temperature aerospace propulsion applications. The material systems included monolithic ceramics, superalloys, and high-temperature composites. In the aeronautics area, the major applications were cooled ceramic plate structures for turbine applications, gamma-TiAl blade materials for low-pressure turbines, thermoelastic stress analysis for residual stress measurements in titanium-based and nickel-based engine materials, and acousto-ultrasonics for creep damage assessment in nickel-based alloys. In the space area, applications consisted of cooled carbon-carbon composites for gas generator combustors and flywheel rotors composed of carbon-fiber-reinforced polymer matrix composites for energy storage on the International Space Station.

  2. Evaluation of workload weighed transmission curves of commercial shielding materials used in diagnostic rooms

    International Nuclear Information System (INIS)

    Evaluation of beam attenuation properties of shielding materials used in diagnostic rooms was obtained following the method proposed by Archer et. Al (Med. Phys. 21 (9), 1994). These attenuation properties were measured by using a constant potential X-ray machine operated in voltages from 60 to 150 kV. Moreover, workload distributions (Simpkin, Med. Phys. 23(4) 1996) of typical diagnostic rooms were obtained. The workload weighed transmission curves were obtained considering the different shielding material manufacturer and workload spectrum. This method published in NCRP 147 presents a strong dependence on quantities workload distribution and transmission through the shielding materials. The correct consideration of this combination allows the optimized determination of the shielding material thickness needed for protecting the environment. (author)

  3. An evaluation of epoxy resin phantom materials for megavoltage photon dosimetry

    Science.gov (United States)

    Allahverdi, M.; Nisbet, A.; Thwaites, D. I.

    1999-05-01

    Epoxy resin phantom materials have been available for some time and are widely used for dosimetry purposes, not least in audit phantoms. Information on their behaviour is partly available in the literature, but there are different mixes and formulations often given similar names and it may not be appropriate to transfer information from one material to another. Five commercially available water-substitute materials have been evaluated for use in megavoltage photon beams: WT1, WTe, RMI 451, RMI 457 and `plastic water'. Four independent experiments were carried out to compare these materials with water in megavoltage photon beams ranging in energy from cobalt-60 to nominal 16 MV x-rays, and some general conclusions are drawn from the results as to their use. All are suitable for relative dosimetry in megavoltage photon beams. However, differences of up to 1% are observed for absolute measurements. The newer formulations, developed for electron beam use, are also closer to water for megavoltage photon beams.

  4. Evaluation of Activity Concentration Values and Doses due to the Transport of Low Level Radioactive Material

    Energy Technology Data Exchange (ETDEWEB)

    Rawl, Richard R [ORNL; Scofield, Patricia A [ORNL; Leggett, Richard Wayne [ORNL; Eckerman, Keith F [ORNL

    2010-04-01

    The International Atomic Energy Agency (IAEA) initiated an international Coordinated Research Project (CRP) to evaluate the safety of transport of naturally occurring radioactive material (NORM). This report presents the United States contribution to that IAEA research program. The focus of this report is on the analysis of the potential doses resulting from the transport of low level radioactive material. Specific areas of research included: (1) an examination of the technical approach used in the derivation of exempt activity concentration values and a comparison of the doses associated with the transport of materials included or not included in the provisions of Paragraph 107(e) of the IAEA Safety Standards, Regulations for the Safe Transport of Radioactive Material, Safety Requirements No. TS-R-1; (2) determination of the doses resulting from different treatment of progeny for exempt values versus the A{sub 1}/A{sub 2} values; and (3) evaluation of the dose justifications for the provisions applicable to exempt materials and low specific activity materials (LSA-I). It was found that the 'previous or intended use' (PIU) provision in Paragraph 107(e) is not risk informed since doses to the most highly exposed persons (e.g., truck drivers) are comparable regardless of intended use of the transported material. The PIU clause can also have important economic implications for co-mined ores and products that are not intended for the fuel cycle but that have uranium extracted as part of their industrial processing. In examination of the footnotes in Table 2 of TS-R-1, which identifies the progeny included in the exempt or A1/A2 values, there is no explanation of how the progeny were selected. It is recommended that the progeny for both the exemption and A{sub 1}/A{sub 2} values should be similar regardless of application, and that the same physical information should be used in deriving the limits. Based on the evaluation of doses due to the transport of low

  5. A quick and efficient measurement technique for performance evaluation of thermoelectric materials

    Science.gov (United States)

    Rao, Ashwin; Banjade, Pawan; Bosak, Gregg; Joshi, Binay; Keane, Jennifer; Nally, Luke; Peng, Adam; Perera, Susanthri; Waring, Alfred; Joshi, Giri; Poudel, Bed

    2016-10-01

    Evaluating the performance of thermoelectric (TE) materials is critical for developing an efficient long lasting thermoelectric generator. Various parameters like resistance, TE power, TE efficiency as a function of temperature and time play an important role in developing and optimizing TE materials and legs. If one needs to evaluate the TE legs for performance or contact metallization optimization, study of a brazed or packaged device everytime could prove to be an expensive, time consuming process especially as a quick intermediate qualification. In this work, a simple approach that uses eutectic Gallium Indium (Ga-In) paste as a metallizing substitute with good electrical/thermal contact is employed which also avoids the need for brazing/welding (or any permanent joining) and provides a reliable platform for a quick leg qualification. Using open circuit voltage (V oc) and device voltage (V d), one can evaluate important TE quantities like peak power, material resistance changes, peak current and power versus current characteristics to understand the leg performance. The proposed approach is successfully demonstrated with three different TE material systems namely Bismuth Telluride, Skutterudite and Half Heusler systems.

  6. Ecological evaluation of proposed dredged material from the Point Frazer Bend Reach, Winyah Bay, South Carolina

    Energy Technology Data Exchange (ETDEWEB)

    Gardiner, W.W.; Ward, J.A.; Word, J.Q.

    1995-02-01

    The port of Georgetown, South Carolina, is served by navigational channels within Winyah Bay and the lower Sampit River. Dredging is required to maintain these waterways and to facilitate normal shipping traffic. Prior to dredging, ecological evaluations must be conducted to determine the suitability of the proposed dredged material for open-ocean disposal. These evaluations are to be performed under Section 103 of the Marine Protection, Research, and, Sanctuaries Act of 1972 (MPRSA), following the testing protocols presented in Evaluation of Dredged Material Proposed for Ocean Disposal Testing Manual, hereafter referred to as the 1991 Implementation Manual. The Charleston Intensive Project is a reevaluation of sediments collected from two stations (IH-2 and IH-3) in the Frazier Point Bend reach of the Winyah Bay channel. Reference sediment was also collected from site IH-R2, just south of Hare Island. The results of physical/chemical analyses indicated that some contaminants of concern were present in test treatments representing dredged material when compared with the reference treatment IH-R2. The results of this study indicate that, based on the acute toxicity and chemical analyses, dredged material represented by these test treatments is suitable for open-ocean disposal.

  7. Designing and Evaluating a Web Supported Instructional Material based on Brain Based Learning

    Directory of Open Access Journals (Sweden)

    Günay PALİÇ

    2012-06-01

    Full Text Available In this study, it is aimed to evaluate a web supported instructional material based on Brain Based Learning concerning “Energy” unit for the 9th grades in secondary education. The Case Study Method was used in the study. The sample of the study consists of a total of three physics education experts and one computer and instructional education expert working at the Fatih Faculty of Education in KTU and 10 physics teachers working in secondary schools in the city of Rize. In order to evaluate the educational material published on www.isgucenerji.com, semi-structured interviews were conducted with the experts. Also, an evaluation scale for the website consisting of 21 items was used to be applied to the teachers. The findings indicated that teachers have positive views about designed material’s convenience to curriculum and Brain Based Teaching. It was also deduced that the prepared material can be used for both classroom practice and individual studies. The study was finished with suggestions aimed at using and developing web supported teaching materials.

  8. An interdisciplinary methodology for the comparative evaluation of splinting materials (orthotics, thermoplastics, clinical research).

    Science.gov (United States)

    Shimeld, A; Campbell, G; Ernest, M

    1982-06-01

    The methodology developed includes both the use of laboratory evaluation and clinical assessment in an area where there are no standard requirements, no specifications, nor any continuity of data available on the various thermoplastic splinting materials now on the market. A series of laboratory tests and clinical trials were devised such that these could be interpreted with regard to clinical considerations, cost analyses and serviceability factors relating to the materials. Laboratory testing covered possible effects on the chemical and mechanical properties of material likely to be caused by various environmental, sterilization and working factors. The complementary clinical evaluation to highlight the behaviour of materials during the fabrication and wearing of splints consisted of specific information generated with the assistance of experienced occupational therapists, occupational therapy students and patients. Biocompatibility studies were also carried out. The data to be published will provide needed information to physicians, occupational therapists, physical therapists, orthotists, prosthetists, and administrators with regard to their making informed decisions on the selection, purchase and use of thermoplastic materials.

  9. Advanced Small Rocket Chambers. Basic Program and Option 2: Fundamental Processes and Material Evaluation

    Science.gov (United States)

    Jassowski, Donald M.

    1993-01-01

    Propellants, chamber materials, and processes for fabrication of small high performance radiation cooled liquid rocket engines were evaluated to determine candidates for eventual demonstration in flight-type thrusters. Both storable and cryogenic propellant systems were considered. The storable propellant systems chosen for further study were nitrogen tetroxide oxidizer with either hydrazine or monomethylhydrazine as fuel. The cryogenic propellants chosen were oxygen with either hydrogen or methane as fuel. Chamber material candidates were chemical vapor deposition (CVD) rhenium protected from oxidation by CVD iridium for the chamber hot section, and film cooled wrought platinum-rhodium or regeneratively cooled stainless steel for the front end section exposed to partially reacted propellants. Laser diagnostics of the combustion products near the hot chamber surface and measurements at the surface layer were performed in a collaborative program at Sandia National Laboratories, Livermore, CA. The Material Sample Test Apparatus, a laboratory system to simulate the combustion environment in terms of gas and material temperature, composition, and pressure up to 6 Atm, was developed for these studies. Rocket engine simulator studies were conducted to evaluate the materials under simulated combustor flow conditions, in the diagnostic test chamber. These tests used the exhaust species measurement system, a device developed to monitor optically species composition and concentration in the chamber and exhaust by emission and absorption measurements.

  10. Isothermal Microcalorimetric Evaluation of Compatibility of Proposed Injector Materials with High-Test Hydrogen Peroxide Propellant

    Science.gov (United States)

    Gostowski, Rudy

    2003-01-01

    High-test hydrogen peroxide (HTP) is receiving renewed interest as a monopropellant and as the oxidizer for bipropellant systems. HTP is hydrogen peroxide in concentrations ranging from 70 to 98%. All surfaces wetted by HTP must be evaluated for compatibility with the fluid. In the case of tanks, lines and valves compatibility is required to preserve the HTP oxygen and energy content and to avoid overpressurization due to decomposition. With injectors and regenerative cooling passages shorter exposure time reduces these concerns. However, phase changes from fluid to gas impact heat transfer and become the dominant compatibility concern. Isothermal microcalorimetry (IMC) provides a convenient and reproducible means to observe the decomposition of HTP when exposed to structural materials and therefore the compatibility of those materials'. The instrument provides heat flow values in terms of watts that may be converted to a reaction rate given the heat of reaction for the decomposition of hydrogen peroxide. These values are then converted to percent active oxygen loss per week (%AOL/wk) to preserve an earlier convention for quantifying HTP compatibility. Additionally, qualitative designations of compatibility have been assigned to these values. This scheme consists of four classes with Class 1 being the most compatible. While historical compatibility data is available its current applicability is in question due to subtle changes in the compositions of both HTP and structural materials. Trace levels of molecules can have significant influence on compatibility. Therefore representative samples of materials must be evaluated with current HTP formulations. In this work seven materials were selected for their strength characteristics at high temperature as expected in a HTP injector. The materials were then evaluated by IMC for HTP compatibility.

  11. Quantitative evaluation of susceptibility effects caused by dental materials in head magnetic resonance imaging

    Science.gov (United States)

    Strocchi, S.; Ghielmi, M.; Basilico, F.; Macchi, A.; Novario, R.; Ferretti, R.; Binaghi, E.

    2016-03-01

    This work quantitatively evaluates the effects induced by susceptibility characteristics of materials commonly used in dental practice on the quality of head MR images in a clinical 1.5T device. The proposed evaluation procedure measures the image artifacts induced by susceptibility in MR images by providing an index consistent with the global degradation as perceived by the experts. Susceptibility artifacts were evaluated in a near-clinical setup, using a phantom with susceptibility and geometric characteristics similar to that of a human head. We tested different dentist materials, called PAL Keramit, Ti6Al4V-ELI, Keramit NP, ILOR F, Zirconia and used different clinical MR acquisition sequences, such as "classical" SE and fast, gradient, and diffusion sequences. The evaluation is designed as a matching process between reference and artifacts affected images recording the same scene. The extent of the degradation induced by susceptibility is then measured in terms of similarity with the corresponding reference image. The matching process involves a multimodal registration task and the use an adequate similarity index psychophysically validated, based on correlation coefficient. The proposed analyses are integrated within a computer-supported procedure that interactively guides the users in the different phases of the evaluation method. 2-Dimensional and 3-dimensional indexes are used for each material and each acquisition sequence. From these, we drew a ranking of the materials, averaging the results obtained. Zirconia and ILOR F appear to be the best choice from the susceptibility artefacts point of view, followed, in order, by PAL Keramit, Ti6Al4V-ELI and Keramit NP.

  12. On evaluated nuclear data for beta-delayed gamma rays following of special nuclear materials

    Energy Technology Data Exchange (ETDEWEB)

    Mencarini, Leonardo de H.; Caldeira, Alexandre D., E-mail: mencarini@ieav.cta.b, E-mail: alexdc@ieav.cta.b [Instituto de Estudos Avancados (IEAv/CTA), Sao Jose dos Campos, SP (Brazil)

    2011-07-01

    In this paper, a new type of information available in ENDF is discussed. During a consistency check of the evaluated nuclear data library ENDF/B-VII.0 performed at the Nuclear Data Subdivision of the Institute for Advanced Studies, the size of the files for some materials drew the attention of one of the authors. Almost 94 % of all available information for these special nuclear materials is used to represent the beta-delayed gamma rays following fission. This is the first time this information is included in an ENDF version. (author)

  13. On evaluated nuclear data for beta-delayed gamma rays following of special nuclear materials

    International Nuclear Information System (INIS)

    In this paper, a new type of information available in ENDF is discussed. During a consistency check of the evaluated nuclear data library ENDF/B-VII.0 performed at the Nuclear Data Subdivision of the Institute for Advanced Studies, the size of the files for some materials drew the attention of one of the authors. Almost 94 % of all available information for these special nuclear materials is used to represent the beta-delayed gamma rays following fission. This is the first time this information is included in an ENDF version. (author)

  14. Polymeric Materials Review on Oxidation, Stabilization and Evaluation using CL and DSC Methods

    CERN Document Server

    Ilie, Sorin; CERN. Geneva. TE Department

    2009-01-01

    Within TE - VSC Group, the Chemistry Laboratory actually works on the project entitled “Studies of Radiation Induced Aging Effects in Polymeric Cable Insulators”. The aim of the project is the characterization and the evaluation of the aging effects mainly induced by ionizing radiations on the various polymeric materials in cables structure. It is expected, using the accumulated data, to foresee the life-time of these materials in the specific CERN accelerator systems and, also, to assure an acceptance quality control of the supplied cables in CERN.

  15. Evaluation of Bi-Material Crack Using The Finite Block Method

    Science.gov (United States)

    Hinneh, P.; Wen, P. H.

    2016-08-01

    The Finite Block Method has been employed in this paper to evaluate the stress intensity factor of a bi-material plate. The complex stress intensity factor components K1 and K2 determined by the Finite Block Method is compared with an equivalent Finite Element Method (ABAQUS) analysis. The paper demonstrates the accuracy of the Meshfree approach by the Finite Block Method without the arduous demand of meshing around the crack surface as seen on standard FEM crack analysis. This paper also describes the application of the polygonal singular core and the collocations points around the interface crack. A computational example for various E1/E2 material combinations is presented.

  16. Evaluating Opportunities to Improve Material and Energy Impacts in Commodity Supply Chains.

    Energy Technology Data Exchange (ETDEWEB)

    Hanes, Rebecca J.; Carpenter, Alberta

    2016-06-28

    When evaluated at the process level, next-generation technologies may be more energy and emissions intensive than current technology. However, many advanced technologies have the potential to reduce material and energy consumption in upstream or downstream processing stages. In order to fully understand the benefits and consequences of technology deployment, next-generation technologies should be evaluated in context, as part of a supply chain. This work presents the Material Flows through Industry (MFI) scenario modeling tool. The MFI tool is a cradle-to-gate linear network model of the U.S. industrial sector that can model a wide range of manufacturing scenarios, including changes in production technology, increases in industrial energy efficiency, and substitution between functionally equivalent materials. The MFI tool was developed to perform supply chain scale analyses in order to quantify the impacts and benefits of next-generation technologies and materials at that scale. For the analysis presented in this paper, the MFI tool is utilized to explore a case study comparing a steel supply chain to the supply chains of several functionally equivalent materials. Several of the alternatives to the baseline steel supply chain include next-generation production technologies and materials. Results of the case study show that aluminum production scenarios can out-perform the steel supply chain by using either an advanced smelting technology or an increased aluminum recycling rate. The next-generation material supply chains do not perform as well as either aluminum or steel, but may offer additional use phase reductions in energy and emissions that are outside the scope of the MFI tool. Future work will combine results from the MFI tool with a use phase analysis.

  17. The design, fabrication and safety evaluation of a novel spent fuel storage basket material

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Peng, E-mail: wp739130046@nuaa.edu.cn [Department of Nuclear Science and Engineering, Nanjing University of Aeronautics and Astronautics, Nanjing 210016 (China); Jiangsu Key Laboratory of Nuclear Energy Equipment Materials Engineering (China); Tang, Xiaobin, E-mail: tangxiaobin@nuaa.edu.cn [Department of Nuclear Science and Engineering, Nanjing University of Aeronautics and Astronautics, Nanjing 210016 (China); Jiangsu Key Laboratory of Nuclear Energy Equipment Materials Engineering (China); Chen, Feida, E-mail: fdchen@nuaa.edu.cn [Department of Nuclear Science and Engineering, Nanjing University of Aeronautics and Astronautics, Nanjing 210016 (China); Jiangsu Key Laboratory of Nuclear Energy Equipment Materials Engineering (China); Chen, Da, E-mail: chenda@nuaa.edu.cn [Department of Nuclear Science and Engineering, Nanjing University of Aeronautics and Astronautics, Nanjing 210016 (China); Jiangsu Key Laboratory of Nuclear Energy Equipment Materials Engineering (China)

    2015-04-01

    Highlights: • Neutron absorption performance of the novel neutron absorbing material was improved by adding three different kinds of neutron absorbers (LiF, Sm{sub 2}O{sub 3}, and Gd{sub 2}O{sub 3}). • The percentage of the three kinds of neutron absorbers was optimised by Monte Carlo method. • Carbon fibre and polyimide were used to enhance its mechanical behaviour and thermal behaviour. • The radiation effect of the neutron absorbing material had been studied under Co-60 irradiation, and its irradiation-resistance performance was evaluated. - Abstract: A novel LiF, Sm{sub 2}O{sub 3}, Gd{sub 2}O{sub 3}/carbon fibre/polyimide material was designed in order to improve the neutron absorbing performance of the spent fuel storage basket in this paper. The volume fraction of three kinds of neutron absorbers (LiF, Sm{sub 2}O{sub 3}and Gd{sub 2}O{sub 3}) in polyimide was optimised by Monte Carlo method. Calculation results showed that the novel neutron-absorbing material, in which the volume ratio of LiF, Sm{sub 2}O{sub 3}and Gd{sub 2}O{sub 3} was 1:2:13, can achieve the best absorption capacity. Based on the calculated results, the basket material was fabricated by compression moulding, and its mechanical behaviour, thermal behaviour, and irradiation resistant behaviour were evaluated, respectively. The experimental results proved that the tensile strength of the novel neutron-absorbing material was between 195 and 346 MPa and the maximum service temperature was up to 300 °C. Gamma irradiation dose was limited to 160 kGy, the bending strength of the material kept increasing from 10 to 19 MPa.

  18. Evaluation of potential emission spectra for the reliable classification of fluorescently coded materials

    Science.gov (United States)

    Brunner, Siegfried; Kargel, Christian

    2011-06-01

    The conservation and efficient use of natural and especially strategic resources like oil and water have become global issues, which increasingly initiate environmental and political activities for comprehensive recycling programs. To effectively reutilize oil-based materials necessary in many industrial fields (e.g. chemical and pharmaceutical industry, automotive, packaging), appropriate methods for a fast and highly reliable automated material identification are required. One non-contacting, color- and shape-independent new technique that eliminates the shortcomings of existing methods is to label materials like plastics with certain combinations of fluorescent markers ("optical codes", "optical fingerprints") incorporated during manufacture. Since time-resolved measurements are complex (and expensive), fluorescent markers must be designed that possess unique spectral signatures. The number of identifiable materials increases with the number of fluorescent markers that can be reliably distinguished within the limited wavelength band available. In this article we shall investigate the reliable detection and classification of fluorescent markers with specific fluorescence emission spectra. These simulated spectra are modeled based on realistic fluorescence spectra acquired from material samples using a modern VNIR spectral imaging system. In order to maximize the number of materials that can be reliably identified, we evaluate the performance of 8 classification algorithms based on different spectral similarity measures. The results help guide the design of appropriate fluorescent markers, optical sensors and the overall measurement system.

  19. A Preliminary Evaluation of Using Fill Materials to Stabilize Used Nuclear Fuel During Storage and Transportation

    Energy Technology Data Exchange (ETDEWEB)

    Maheras, Steven J.; Best, Ralph; Ross, Steven B.; Lahti, Erik A.; Richmond, David J.

    2012-08-01

    This report contains a preliminary evaluation of potential fill materials that could be used to fill void spaces in and around used nuclear fuel contained in dry storage canisters in order to stabilize the geometry and mechanical structure of the used nuclear fuel during extended storage and transportation after extended storage. Previous work is summarized, conceptual descriptions of how canisters might be filled were developed, and requirements for potential fill materials were developed. Elements of the requirements included criticality avoidance, heat transfer or thermodynamic properties, homogeneity and rheological properties, retrievability, material availability and cost, weight and radiation shielding, and operational considerations. Potential fill materials were grouped into 5 categories and their properties, advantages, disadvantages, and requirements for future testing were discussed. The categories were molten materials, which included molten metals and paraffin; particulates and beads; resins; foams; and grout. Based on this analysis, further development of fill materials to stabilize used nuclear fuel during storage and transportation is not recommended unless options such as showing that the fuel remains intact or canning of used nuclear fuel do not prove to be feasible.

  20. Evaluation of dredged material proposed for ocean disposal from Buttermilk Channel, New York

    Energy Technology Data Exchange (ETDEWEB)

    Gardiner, W.W.; Barrows, E.S.; Antrim, L.D; Gruendell, B.D.; Word, J.Q.; Tokos, J.J.S. [Battelle/Marine Sciences Lab., Sequim, WA (United States)

    1996-08-01

    Buttermilk Channel was one of seven waterways that was sampled and evaluated for dredging and sediment disposal. Sediment samples were collected and analyses were conducted on sediment core samples. The evaluation of proposed dredged material from the channel included bulk sediment chemical analyses, chemical analyses of site water and elutriate, water column and benthic acute toxicity tests, and bioaccumulation studies. Individual sediment core samples were analyzed for grain size, moisture content, and total organic carbon. A composite sediment samples, representing the entire area proposed for dredging, was analyzed for bulk density, polynuclear aromatic hydrocarbons, and 1,4-dichlorobenzene. Site water and elutriate were analyzed for metals, pesticides, and PCBs.

  1. Material property evaluations of bimetallic welds, stainless steel saw fusion lines, and materials affected by dynamic strain aging

    Energy Technology Data Exchange (ETDEWEB)

    Rudland, D.; Scott, P.; Marschall, C.; Wilkowski, G. [Battelle Memorial Institute, Columbus, OH (United States)

    1997-04-01

    Pipe fracture analyses can often reasonably predict the behavior of flawed piping. However, there are material applications with uncertainties in fracture behavior. This paper summarizes work on three such cases. First, the fracture behavior of bimetallic welds are discussed. The purpose of the study was to determine if current fracture analyses can predict the response of pipe with flaws in bimetallic welds. The weld joined sections of A516 Grade 70 carbon steel to F316 stainless steel. The crack was along the carbon steel base metal to Inconel 182 weld metal fusion line. Material properties from tensile and C(T) specimens were used to predict large pipe response. The major conclusion from the work is that fracture behavior of the weld could be evaluated with reasonable accuracy using properties of the carbon steel pipe and conventional J-estimation analyses. However, results may not be generally true for all bimetallic welds. Second, the toughness of austenitic steel submerged-arc weld (SAW) fusion lines is discussed. During large-scale pipe tests with flaws in the center of the SAW, the crack tended to grow into the fusion line. The fracture toughness of the base metal, the SAW, and the fusion line were determined and compared. The major conclusion reached is that although the fusion line had a higher initiation toughness than the weld metal, the fusion-line J-R curve reached a steady-state value while the SAW J-R curve increased. Last, carbon steel fracture experiments containing circumferential flaws with periods of unstable crack jumps during steady ductile tearing are discussed. These instabilities are believed to be due to dynamic strain aging (DSA). The paper discusses DSA, a screening criteria developed to predict DSA, and the ability of the current J-based methodologies to assess the effect of these crack instabilities. The effect of loading rate on the strength and toughness of several different carbon steel pipes at LWR temperatures is also discussed.

  2. Evaluation of Dredged Material Proposed for Ocean Disposal from Port Chester, New York

    Energy Technology Data Exchange (ETDEWEB)

    Barrows, E.S.; Mayhew, H.L.; Word, J.Q.; Tokos, J.J.S. [Battelle Marine Sciences Laboratory, Sequim, WA (United States)

    1996-08-01

    Port Chester was one of seven waterways that the US Army Corps of Engineers-New York District requested the Battelle Marine Sciences Laboratory to sample and evaluate for dredging and disposal in March 1994. Tests and analyses were conducted on Port Chester sediment core samples. Because the Port Chester area is located on the border between New York and southeast Connecticut, its dredged material may also be considered for disposal at the Central Long Island Sound Disposal Site. The sediment evaluation consisted of bulk sediment chemical analyses, chemical analyses of site water and dredged material elutriate preparations, water-column and benthic acute toxicity tests, and bioaccumulation studies. Individual sediment core samples collected from Port Chester were analyzed for grain size, moisture content, and total organic carbon. In addition, sediment was analyzed for bulk density, specific gravity, metals, chlorinated pesticides, polychlorinated biphenyl congers, polynuclear aromatic hydrocarbons and 1,4-dichlorobenzene.

  3. Evaluation of dredged material proposed for ocean disposal from Shark River Project area

    Energy Technology Data Exchange (ETDEWEB)

    Antrim, L.D.; Gardiner, W.W.; Barrows, E.S.; Borde, A.B. [Battelle/Marine Sciences Lab., Sequim, WA (United States)

    1996-09-01

    The objective of the Shark River Project was to evaluate proposed dredged material to determine its suitability for unconfined ocean disposal at the Mud Dump Site. Tests and analyses were conducted on the Shark River sediments. The evaluation of proposed dredged material consisted of bulk sediment chemical and physical analysis, chemical analyses of dredging site water and elutriate, water-column and benthic acute toxicity tests, and bioaccumulation tests. Individual sediment core samples collected from the Shark River were analyzed for grain size, moisture content, and total organic carbon (TOC). One sediment composite was analyzed for bulk density, specific gravity, metals, chlorinated pesticides, polychlorinated biphenyl (PCB) congeners, polynuclear aromatic hydrocarbons (PAHs), and 1,4- dichlorobenzene. Dredging site water and elutriate, prepared from suspended-particulate phase (SPP) of the Shark River sediment composite, were analyzed for metals, pesticides, and PCBs. Benthic acute toxicity tests and bioaccumulation tests were performed.

  4. An in vitro comparative evaluation of fracture resistance of endodontically treated teeth obturated with different materials

    Directory of Open Access Journals (Sweden)

    Rupali Chadha

    2010-01-01

    Full Text Available The aim of this study was to evaluate the in vitro effect of various obturating materials on fracture resistance of root canal treated teeth. Sixty freshly extracted human mandibular premolars were used. After standardizing the length to 13 mm, the teeth were biomechanically prepared and divided into four groups based on type of obturating materials used. Teeth were embedded in acrylic resin and fracture strength was measured using a universal testing machine. Data obtained was evaluated statistically using one-way ANOVA and the unpaired t-test. Teeth obturated with AH Plus and gutta percha showed higher fracture resistance than those obturated with Resilon-Epiphany. The results suggested that the group obturated with gutta percha and zinc oxide-eugenol sealer had the lowest fracture resistance. No statistically significant difference was found between the unobturated (control group and the zinc oxide-eugenol group.

  5. Evaluation of using synthetic zeolite as a backfill material in radioactive waste disposal facility

    International Nuclear Information System (INIS)

    .e. the structure of backfill material, concentration of sorbed ions, sorption time, temperature, and ph.3- Use of thermodynamic sorption models, whose parameters express the surface properties and affinity of the sorbent backfill material at fixed temperature and ph, to represent the sorption behavior of radionuclides on zeolite Na A-X blend and determine the thermodynamic values of sorption such as equilibrium constant, activation energy, free energy, enthalpy, and entropy.4- Experimental column investigations to simulate the transport processes in the backfill material. Breakthrough curves measured in such experiments are useful to determine the hydrodynamic dispersion coefficient.5- The long -term behavior of the prepared zeolite has been evaluated using computer model. This model consists of two modules that have been developed to study the migration of Cs and Sr radionuclides from bare cementatoius waste form through the backfill material.

  6. Design and evaluation of physical protection systems for nuclear facilities and materials

    International Nuclear Information System (INIS)

    The spread of nuclear industry around the world has increased the risks and hazards of various possible forms of attack on nuclear facilities, operations and material. This work deals with the physical protection of nuclear facilities, operations and materials. It is intended to present detailed information on the physical protection aspects and the basic methodology to be used in the design and analysis of a facility's security system. Physical protection measures are directed against theft or unauthorized removal of nuclear materials and sabotage of nuclear facilities and operations individuals or groups of individuals. The design of an effective physical protection system includes the determination of the physical protection system objectives, the initial design of a physical protection system, and, probably, a redesign or refinement of the system. To develop the objectives, the designer mst begin by gathering information about facility operations and conditions, such as comprehensive description of the facility, operating states, and the physical protection requirements. The designer then needs to define the threat. This involves considering factors about potential adversaries: Class of adversary, adversary's capabilities, and range of adversary's tactics. Next, the designer should identify targets. Determination of whether or not nuclear materials are attractive targets is based mainly on the case or difficulty of acquisition and desirability of the material. The designer now knows the objectives of the physical protection system, that is, what to protect against whom. The next step is to design the system by determining how best to combine such elements as fences, vaults, sensors procedures, communication devices, and protective force personnel to meet the objectives of the system. Once a physical protection system is designed, it must be analyzed and evaluated to ensure it meets the physical protection objectives. Evaluation must allow for features working

  7. Tier 1 ecological evaluation of proposed discharge of dredged material from Oakland Harbor into ocean waters

    Energy Technology Data Exchange (ETDEWEB)

    Shreffler, D.K.; Thorn, R.M.; Walls, B.E.; Word, J.Q. [Battelle/Marine Sciences Lab., Sequim, WA (United States)

    1994-01-01

    The Water Resources Development Act of 1986 (Public Law 99--662) authorized the U.S. Army Corps of Engineers (USACE) -- San Francisco District, to accommodate larger, deeper draft vessels in Oakland inner and Outer Harbors by deepening and widening the existing navigation channel, and providing turning basins and maneuvering areas in Oakland inner Harbor. The suitability of the resulting dredged material for disposal into ocean waters was subject to the procedures of the 1991 Testing Manual, Evaluation of Dredged Material Proposed for Ocean Disposal, known as the ``Green Book``. The Green Book provides a tiered approach for testing the suitability of dredged materials through chemical, physical, and biological evaluations. The first level of investigation, or Tier 1 evaluation, is used to determine whether a decision on LPC compliance can be made on the basis of readily available information. The Tier 1 report primarily summarizes existing information on sediment contamination and toxicity potential, identifies contaminants of concern, and determines the need for further testing. To assist the USACE in determining the suitability of dredged material from Oakland inner and Outer Harbors for ocean disposal, Battelle/Marine Sciences Laboratory prepared this Tier 1 report based upon information and data provided by USACE. Because this Tier 1 report originated well after an LPC determination was made to require testing of project sediments in Tier 3, the primary purpose of this report was to identify contaminants of concern (if any) in that particular dredged material. In addition, this Tier 1 report summarizes available information on chemical, physical, and biological characterization of the sediments in Oakland inner and Outer Harbors.

  8. Technical committee meeting on evaluation of radioactive materials release and sodium fires in fast reactors

    International Nuclear Information System (INIS)

    The objectives of the Technical Committee Meeting was to review the activities of research on radioactive materials release and sodium fires in fast reactors in each of the participating countries. It covered: out-of-pile experiments and analysis codes on source term; in-pile experiments on source term; core disruptive accidents; sodium leak experience in liquid metal fast reactors; evaluation of sodium fire; and aerosol behaviour

  9. Histological and molecular evaluation of iron as degradable medical implant material in a murine animal model.

    OpenAIRE

    Mueller, Peter P; Arnold, Sylvia; Badar, Muhammad; Bormann, Dirk; Bach, Friedrich-Wilhelm; Drynda, Andreas; Meyer-Lindenberg, Andrea; Hauser, Hansjörg; Peuster, Matthias

    2012-01-01

    A small animal model was established to evaluate the potential of iron as a degradable implant material. After insertion into the tail of mice, the implants gradually degraded over a clinically relevant time period of several months. Histological analysis and gene expression data from whole-genome microarray analyses indicated a limited inflammatory reaction. No evidence of cellular responses to excess iron ions was detected, suggesting that the iron degradation products were metabolically in...

  10. One-year clinical evaluation of tooth-coloured materials in non-carious cervical lesions

    Directory of Open Access Journals (Sweden)

    Stojanac Igor

    2011-01-01

    Full Text Available Introduction. The restoration of non-carious cervical lesions is specific, mostly because of the location of their margins, especially the cervical margin, which is determined in cement and/or dentine. This feature makes the cervical margin more susceptible to micro-leak­age, causing marginal discoloration, postoperative sensitivity, development of the secondary caries and loss of the restoration. Material and methods. One of the criteria for inclusion of a patient in this study was the presence of at least two non-carious cervical lesions to be restored with the minimum depth of 1mm, independently of their location in the dental arch. A total of 60 restorations were placed in 30 patients, and every patient received both tested materials (composite resins and compomer on their non-carious cervical lesions. The clinical evaluation of the therapeutic success was performed six months and then one year after the day of the placement of restorations using the modified-United States Public Health Service criteria. The following was evaluated: retention, marginal integrity, marginal discoloration, wear, postoperative sensitivity and secondary caries. Results. A statistically significant high percent of restorations/teeth with postoperative sensitivity was found in the group of resin composite restorations after six months. At the end of the evaluation period, that is after one year, there were no statistically significant differences between materials for all evaluated criteria. Conclusion. The results of this study show the identical quality of both examined materials one year after the readjustment of non-carious cervical lesions.

  11. Evaluation of geologic materials to limit biological intrusion into low-level radioactive waste disposal sites

    Energy Technology Data Exchange (ETDEWEB)

    Hakonson, T.E.

    1986-02-01

    This report describes the results of a three-year research program to evaluate the performance of selected soil and rock trench cap designs in limiting biological intrusion into simulated waste. The report is divided into three sections including a discussion of background material on biological interactions with waste site trench caps, a presentation of experimental data from field studies conducted at several scales, and a final section on the interpretation and limitations of the data including implications for the user.

  12. Evaluation of geologic materials to limit biological intrusion into low-level radioactive waste disposal sites

    International Nuclear Information System (INIS)

    This report describes the results of a three-year research program to evaluate the performance of selected soil and rock trench cap designs in limiting biological intrusion into simulated waste. The report is divided into three sections including a discussion of background material on biological interactions with waste site trench caps, a presentation of experimental data from field studies conducted at several scales, and a final section on the interpretation and limitations of the data including implications for the user

  13. Calculation of resonant sound absorption parameters for performance evaluation of metal rubber material

    Institute of Scientific and Technical Information of China (English)

    E.A.IZZHEUROV

    2009-01-01

    The first resonant(anti-resonant)frequency and sound absorption coefficient of metal rubber(MR) material are theoretically studied with hard backed samples and with air layer.The equations of the first resonant and anti-resonant frequencies of MR are deduced from the undamped propagation characteristics of porous material.The first resonant and anti-resonance sound absorption coefficients are induced according to the theoretical formula for the acoustic characteristic parameters of MR,and the former is modified while the energy consumption at resonance is taken into consideration.The good agreement between the calculation results of these resonant sound absorption parameters and the experimental results verifies the effectiveness of this calculation method for the performance evaluation of MR as a sound absorption material.

  14. Steam oxidation and the evaluation of coatings and material performance through collaborative research

    Energy Technology Data Exchange (ETDEWEB)

    Fry, A.T. [National Physical Lab., Teddington (United Kingdom); Aguero, A. [INTA, Madrid (Spain)

    2010-07-01

    Over the last five years through the COST 536 Programme researchers across Europe have been collaborating to better understand the phenomena of steam oxidation and to characterise coated and uncoated materials for use in power plants. During this period fundamental study of the oxidation mechanisms and changes in the oxidation kinetics caused by the presence of steam have been undertaken. Materials covering a range of high temperature plant applications have been studied, from low alloy martensitic alloys through to Ni-based superalloy materials, with investigations into the effect of increasing temperatures and pressures on the oxidation kinetics, oxide morphology and spallation characteristics. In addition conventional and novel coatings have been evaluated to assess their potential use in new USC plant. This paper will present an overview of these activities demonstrating the effect that steam has on the oxidation of alloys and coatings. (orig.)

  15. Evaluation of food, nutrition and functional substances, in the selected food materials for space agriculture

    Science.gov (United States)

    Tomita-Yokotani, Kaori; Kimura, Yasuko; Yamashita, Masamichi; Kimura, Shunta; Sato, Seigo; Katoh, Hiroshi

    2016-07-01

    We have been studying the evaluation of food, nutrition and functional substances, in the selected organic materials for useful life-support systems in closed bio-ecosystems for space agriculture on Mars in the future. We have already proposed several species as food materials; cyanobacterium, Nostoc sp. HK-01 and the Japanese cherry tree. Nostoc sp. HK-01 is a terrestrial cyanobacterium which has high tolerances to several space environments. In addition to its high tolerances to serious environments, HK-01 has a high protein content. Total protein per 100 g of the dried colony of Nostoc sp. HK-01 was approximately 50 g. Woody plant materials also have several properties which can be utilized in our habitation environment and as food. We have already found abilities to produce important functional substances for humans in the selected trees. Here, we show the extended results of our experiments.

  16. Calculation of resonant sound absorption parameters for performance evaluation of metal rubber material

    Institute of Scientific and Technical Information of China (English)

    WU GuoQi; AO HongRui; JIANG HongYuan; E.A.IZZHEUROV

    2009-01-01

    The first resonant(anti-resonant)frequency and sound absorption coefficient of metal rubber(MR)material are theoretically studied with hard backed samples and with air layer.The equations of the first resonant and anti-resonant frequencies of MR are deduced from the undamped propagation characteristics of porous material.The first resonant and anti-resonance sound absorption coefficients are induced according to the theoretical formula for the acoustic characteristic parameters of MR,and the former is modified while the energy consumption at resonance is taken into consideration.The good agreement between the calculation results of these resonant sound absorption parameters and the experimental results verifies the effectiveness of this calculation method for the performance evaluation of MR as a sound absorption material.

  17. Thermoelectric Materials Evaluation Program. Annual technical report for fiscal year 1979

    International Nuclear Information System (INIS)

    Optimization was initiated with respect to performance, operating temperatures, and thermoelectric properties of an N-type material based on rare earth (neodymium and gadolinium) selenide technology. Effort was expanded to experimentally describe the chemical, electrical and physical behavior of P-type thermoelectric material over a range of temperatures. Emphasis was changed in P-type material research from basic properties to sublimation suppression by wrapping, and to the understanding of contact resistance problems at the hot end. Analytical performance calculations were made as an aid in couple development. In the area of module development an evaluation of the reduction of bypass-heat loss was made and module M-22R was placed on test. Parts were fabricated for M23R. Data on long term operating characteristics, ingradient compatibility, and reliability of elements and couples was obtained

  18. Evaluating emission levels of polycyclic aromatic hydrocarbons from organic materials by analytical pyrolysis

    Energy Technology Data Exchange (ETDEWEB)

    Fabbri, Daniele; Vassura, Ivano [Laboratory of Chemistry, C.I.R.S.A., University of Bologna, via S. Alberto 163, I-48100 Ravenna (Italy)

    2006-03-01

    A procedure in off-line analytical pyrolysis was investigated for the rapid determination of polycyclic aromatic hydrocarbons (PAHs) evolved from thermal degradation of organic materials. Samples spiked with perdeuterated PAHs were pyrolysed at 1000{sup o}C for 60s by means of a resistively heated filament pyrolyser inserted into a glass chamber connected to a cartridge with a sorbent (XAD-2 resin). PAHs trapped onto the resin were extracted with dichloromethane and analysed by gas chromatography-mass spectrometry (GC-MS). The analytical performance of the overall procedure (precision, recovery, effect of experimental parameters) was evaluated by pyrolysing a bituminous coal certified reference material (CRM). Emission levels of naphthalene, 1-methylnaphthalene, 2-methylnaphthalene, acenaphtylene, acenaphthene, fluorene, phenanthrene, anthracene, fluoranthene, pyrene were determined for bituminous and anthracite coals, tyre, and cellulose. Despite some limitations, the method was adequate to the purpose of quantitatively measuring the tendency of various materials to release volatile PAHs upon heating. (author)

  19. Sensory evaluation based fuzzy AHP approach for material selection in customized garment design and development process

    Science.gov (United States)

    Hong, Y.; Curteza, A.; Zeng, X.; Bruniaux, P.; Chen, Y.

    2016-06-01

    Material selection is the most difficult section in the customized garment product design and development process. This study aims to create a hierarchical framework for material selection. The analytic hierarchy process and fuzzy sets theories have been applied to mindshare the diverse requirements from the customer and inherent interaction/interdependencies among these requirements. Sensory evaluation ensures a quick and effective selection without complex laboratory test such as KES and FAST, using the professional knowledge of the designers. A real empirical application for the physically disabled people is carried out to demonstrate the proposed method. Both the theoretical and practical background of this paper have indicated the fuzzy analytical network process can capture expert's knowledge existing in the form of incomplete, ambiguous and vague information for the mutual influence on attribute and criteria of the material selection.

  20. Evaluation of Parameters Influencing the Moisture Buffering Potential of Hygroscopic Materials with BSim Simulations

    Directory of Open Access Journals (Sweden)

    Xiangjin Yang

    2014-07-01

    Full Text Available Validated by a large-scale experimental investigation on moisture buffering (MB effect, a whole building Heat, Air and Moisture (HAM simulation tool, BSim, is applied to evaluate the impact of a number of parameters on the moisture buffering potential of a full-scale test room finished with hygroscopic materials. The Maximum Accumulated Moisture Buffering Value (MAMBV, developed from the moisture balance analyses in the experimental study, is used in the BSim simulation result analyses to evaluate the impact of various parameters. The parameters investigated include ventilation rates (0.5–5 ACH, types of materials (uncoated gypsum board, wood paneling, orientated strand board, aerated cellular concrete, and telephone book paper, humidity conditions of supply air, volume rates, and steady-state outdoor conditions. It is found that all these parameters have a significant impact on the moisture buffering potential except for the steady-state outdoor conditions. Two material properties, the moisture capacity and vapor permeability, determine the moisture buffering capacities of materials under different moisture generation regimes.

  1. A 3D Osteoblast In Vitro Model for the Evaluation of Biomedical Materials

    Directory of Open Access Journals (Sweden)

    Luciana Restle

    2015-01-01

    Full Text Available Biomedical materials for bone therapy are usually assessed for their biocompatibility and safety employing animal models or in vitro monolayer cell culture assays. However, alternative in vitro models may offer controlled conditions closer to physiological responses and reduce animal testing. In this work, we developed a 3D spheroidal cell culture with potential to evaluate simultaneously material-cell and cell-cell interactions. Different cell densities of murine MC3T3-E1 preosteoblasts or human primary osteoblasts (HOb were used to determine the ideal procedure of spheroidal cultures and their adequacy to material testing. Cells were seeded on 96-well plates coated with agar and incubated in agitation from 1 to 7 days. Aggregate morphology was qualitatively evaluated considering the shape, size, repeatability, handling, and stability of spheroids. Higher cell densities induced more stable spheroids, and handling was considered appropriate starting from 2 × 104 cells. Confocal microscopy and Scanning Electron Microscopy indicate that most cells within the aggregate core are viable. Exposure to positive controls has shown a dose dependent cell death as measured by XTT assay. Aggregates were stable and presented good viability when employed on standardized testing of metallic and polymer-based biomaterials. Therefore, osteoblast spheroids may provide a promising tool for material screening and biocompatibility testing.

  2. Evaluation of a fungal collection as certified reference material producer and as a biological resource center.

    Science.gov (United States)

    Forti, Tatiana; Souto, Aline da S S; do Nascimento, Carlos Roberto S; Nishikawa, Marilia M; Hubner, Marise T W; Sabagh, Fernanda P; Temporal, Rosane Maria; Rodrigues, Janaína M; da Silva, Manuela

    2016-01-01

    Considering the absence of standards for culture collections and more specifically for biological resource centers in the world, in addition to the absence of certified biological material in Brazil, this study aimed to evaluate a Fungal Collection from Fiocruz, as a producer of certified reference material and as Biological Resource Center (BRC). For this evaluation, a checklist based on the requirements of ABNT ISO GUIA34:2012 correlated with the ABNT NBR ISO/IEC17025:2005, was designed and applied. Complementing the implementation of the checklist, an internal audit was performed. An evaluation of this Collection as a BRC was also conducted following the requirements of the NIT-DICLA-061, the Brazilian internal standard from Inmetro, based on ABNT NBR ISO/IEC 17025:2005, ABNT ISO GUIA 34:2012 and OECD Best Practice Guidelines for BRCs. This was the first time that the NIT DICLA-061 was applied in a culture collection during an internal audit. The assessments enabled the proposal for the adequacy of this Collection to assure the implementation of the management system for their future accreditation by Inmetro as a certified reference material producer as well as its future accreditation as a Biological Resource Center according to the NIT-DICLA-061. PMID:26991280

  3. Evaluation of a fungal collection as certified reference material producer and as a biological resource center

    Directory of Open Access Journals (Sweden)

    Tatiana Forti

    2016-06-01

    Full Text Available Abstract Considering the absence of standards for culture collections and more specifically for biological resource centers in the world, in addition to the absence of certified biological material in Brazil, this study aimed to evaluate a Fungal Collection from Fiocruz, as a producer of certified reference material and as Biological Resource Center (BRC. For this evaluation, a checklist based on the requirements of ABNT ISO GUIA34:2012 correlated with the ABNT NBR ISO/IEC17025:2005, was designed and applied. Complementing the implementation of the checklist, an internal audit was performed. An evaluation of this Collection as a BRC was also conducted following the requirements of the NIT-DICLA-061, the Brazilian internal standard from Inmetro, based on ABNT NBR ISO/IEC 17025:2005, ABNT ISO GUIA 34:2012 and OECD Best Practice Guidelines for BRCs. This was the first time that the NIT DICLA-061 was applied in a culture collection during an internal audit. The assessments enabled the proposal for the adequacy of this Collection to assure the implementation of the management system for their future accreditation by Inmetro as a certified reference material producer as well as its future accreditation as a Biological Resource Center according to the NIT-DICLA-061.

  4. Energy Absorption and Dynamic Deformation of Backing Material for Ballistic Evaluation of Body Armour

    Directory of Open Access Journals (Sweden)

    Debarati Bhattacharjee

    2013-09-01

    Full Text Available The measurement of back face signature (BFS or behind armour blunt trauma (BABT is a critical aspect of ballistic evaluation of body armour. BFS is the impact experienced by the armour wearing body, when subjected to a non-penetrating projectile. Mineral or polymeric clay is used to measure the BFS. In addition to stopping the projectile, the body armour can be used only when the BFS also falls within permissible limits. The extent of the BFS depends upon the behavior of the backing material in different loading conditions and prior history. This paper explains some of the studies carried out on the backing material used for ballistic evaluation in Terminal Ballistics Research Laboratory, Chandigarh. It has been observed that the backing material is highly non-linear viscoelastic in nature. The depth of deformation is also linearly proportional to the impact energy and temperature. The effect of time on the depth of deformation is gradual and does not influence the BFS values during a standard ballistic evaluation comprising of 6-8 shots.Defence Science Journal, 2013, 63(5, pp.462-466, DOI:http://dx.doi.org/10.14429/dsj.63.3821

  5. Design of a high-temperature experiment for evaluating advanced structural materials

    Science.gov (United States)

    Mockler, Theodore T.; Castro-Cedeno, Mario; Gladden, Herbert J.; Kaufman, Albert

    1992-08-01

    This report describes the design of an experiment for evaluating monolithic and composite material specimens in a high-temperature environment and subject to big thermal gradients. The material specimens will be exposed to aerothermal loads that correspond to thermally similar engine operating conditions. Materials evaluated in this study were monolithic nickel alloys and silicon carbide. In addition, composites such as tungsten/copper were evaluated. A facility to provide the test environment has been assembled in the Engine Research Building at the Lewis Research Center. The test section of the facility will permit both regular and Schlieren photography, thermal imaging, and laser Doppler anemometry. The test environment will be products of hydrogen-air combustion at temperatures from about 1200 F to as high as 4000 F. The test chamber pressure will vary up to 60 psia, and the free-stream flow velocity can reach Mach 0.9. The data collected will be used to validate thermal and stress analysis models of the specimen. This process of modeling, testing, and validation is expected to yield enhancements to existing analysis tools and techniques.

  6. An inset CT specimen for evaluating fracture in small samples of material.

    Science.gov (United States)

    Yahyazadehfar, M; Nazari, A; Kruzic, J J; Quinn, G D; Arola, D

    2014-02-01

    In evaluations on the fracture behavior of hard tissues and many biomaterials, the volume of material available to study is not always sufficient to apply a standard method of practice. In the present study an inset Compact Tension (inset CT) specimen is described, which uses a small cube of material (approximately 2×2×2mm(3)) that is molded within a secondary material to form the compact tension geometry. A generalized equation describing the Mode I stress intensity was developed for the specimen using the solutions from a finite element model that was defined over permissible crack lengths, variations in specimen geometry, and a range in elastic properties of the inset and mold materials. A validation of the generalized equation was performed using estimates for the fracture toughness of a commercial dental composite via the "inset CT" specimen and the standard geometry defined by ASTM E399 (2006). Results showed that the average fracture toughness obtained from the new specimen (1.23±0.02MPam(0.5)) was within 2% of that from the standard. Applications of the inset CT specimen are presented for experimental evaluations on the crack growth resistance of dental enamel and root dentin, including their fracture resistance curves. Potential errors in adopting this specimen are then discussed, including the effects of debonding between the inset and molding material on the estimated stress intensity distribution. Results of the investigation show that the inset CT specimen offers a viable approach for studying the fracture behavior of small volumes of structural materials. PMID:24268892

  7. Microbes on building materialsEvaluation of DNA extraction protocols as common basis for molecular analysis

    International Nuclear Information System (INIS)

    The study of microbial life in building materials is an emerging topic concerning biodeterioration of materials as well as health risks in houses and at working places. Biodegradation and potential health implications associated with microbial growth in our residues claim for more precise methods for quantification and identification. To date, cultivation experiments are commonly used to gain insight into the microbial diversity. Nowadays, molecular techniques for the identification of microorganisms provide efficient methods that can be applied in this field. The efficiency of DNA extraction is decisive in order to perform a reliable and reproducible quantification of the microorganisms by qPCR or to characterize the structure of the microbial community. In this study we tested thirteen DNA extraction methods and evaluated their efficiency for identifying (1) the quantity of DNA, (2) the quality and purity of DNA and (3) the ability of the DNA to be amplified in a PCR reaction using three universal primer sets for the ITS region of fungi as well as one primer pair targeting the 16S rRNA of bacteria with three typical building materials — common plaster, red brick and gypsum cardboard. DNA concentration measurements showed strong variations among the tested methods and materials. Measurement of the DNA yield showed up to three orders of magnitude variation from the same samples, whereas A260/A280 ratios often prognosticated biases in the PCR amplifications. Visualization of the crude DNA extracts and the comparison of DGGE fingerprints showed additional drawbacks of some methods. The FastDNA Spin kit for soil showed to be the best DNA extraction method and could provide positive results for all tests with the three building materials. Therefore, we suggest this method as a gold standard for quantification of indoor fungi and bacteria in building materials. -- Highlights: ► Up to thirteen extraction methods were evaluated with three building materials.

  8. Evaluation of dredged material proposed for ocean Disposal from Shoal Harbor/Compton Creek Project Area

    Energy Technology Data Exchange (ETDEWEB)

    Gardiner, W.W.; Borde, A.B.; Nieukirk, S.L.; Barrows, E.S.; Gruendell, B.D.; Word, J.Q.

    1996-10-01

    The objective of the Shoal Harbor/Compton Creek Project was to evaluate proposed dredged material from the Shoal harbor/Compton Creek Project Area in Belford and Monmouth, New Jersey to determine its suitability for unconfined ocean disposal at the Mud Dump Site. This was one of five waterways that the US Army Corps of Engineers- New York District requested the Battelle Marine Sciences Laboratory (MSL) to sample and evaluate for dredging and disposal in May 1995. The evaluation of proposed dredged material from the Shoal Harbor/Compton Creek Project area consisted of bulk chemical analyses, chemical analyses of dredging site water and elutriate, benthic and water-column acute toxicity tests and bioaccumulation studies. Eleven core samples were analyzed or grain size, moisture content, and total organic carbon. Other sediments were evaluated for bulk density, specific gravity, metals, chlorinated pesticides, polychlorinated biphenyl (PCB) congers, polynuclear aromatic hydrocarbons, and 1,4- dichlorobenzene. Dredging site water and elutriate water were analyzed for metals, pesticides, and PCBs.

  9. Evaluation of the ion implantation process for production of solar cells from silicon sheet materials

    Science.gov (United States)

    Spitzer, M. B.

    1983-01-01

    The objective of this program is the investigation and evaluation of the capabilities of the ion implantation process for the production of photovoltaic cells from a variety of present-day, state-of-the-art, low-cost silicon sheet materials. Task 1 of the program concerns application of ion implantation and furnace annealing to fabrication of cells made from dendritic web silicon. Task 2 comprises the application of ion implantation and pulsed electron beam annealing (PEBA) to cells made from SEMIX, SILSO, heat-exchanger-method (HEM), edge-defined film-fed growth (EFG) and Czochralski (CZ) silicon. The goals of Task 1 comprise an investigation of implantation and anneal processes applied to dendritic web. A further goal is the evaluation of surface passivation and back surface reflector formation. In this way, processes yielding the very highest efficiency can be evaluated. Task 2 seeks to evaluate the use of PEBA for various sheet materials. A comparison of PEBA to thermal annealing will be made for a variety of ion implantation processes.

  10. AN EVALUATION OF POTENTIAL LINER MATERIALS FOR ELIMINATING FCCI IN IRRADIATED METALLIC NUCLEAR FUEL ELEMENTS

    International Nuclear Information System (INIS)

    Metallic nuclear fuels are being looked at as part of the Global Nuclear Energy Program for transmuting longlive transuranic actinide isotopes contained in spent nuclear fuel into shorter-lived fission products. In order to optimize the performance of these fuels, the concept of using liners to eliminate the fuel/cladding chemical interactions that can occur during irradiation of a fuel element has been investigated. The potential liner materials Zr and V have been tested using solid-solid diffusion couples, consisting of liner materials butted against fuel alloys and against cladding materials. The couples were annealed at the relatively high temperature of 700 C. This temperature would be the absolute maximum temperature present at the fuel/cladding interface for a fuel element in-reactor. Analysis was performed using a scanning electron microscope equipped with energy-dispersive and wavelength dispersive spectrometers (SEM/EDS/WDS) to evaluate any developed diffusion structures. At 700 C, minimal interaction was observed between the metallic fuels and either Zr or V. Similarly, limited interaction was observed between the Zr and V and the cladding materials. The best performing liner material appeared to be the V, based on amounts of interaction

  11. An Evaluation of Potential Liner Materials for Eliminating FCCI in Irradiated Metallic Nuclear Fuel Elements

    International Nuclear Information System (INIS)

    Metallic nuclear fuels are being looked at as part of the Global Nuclear Energy Program for transmuting long live transuranic actinide isotopes contained in spent nuclear fuel into shorter-lived fission products. In order to optimize the performance of these fuels, the concept of using liners to eliminate the fuel/cladding chemical interactions that can occur during irradiation of a fuel element has been investigated. The potential liner materials Zr and V have been tested using solid-solid diffusion couples, consisting of liner materials butted against fuel alloys and against cladding materials. The couples were annealed at the relatively high temperature of 700 deg. C. This temperature would be the absolute maximum temperature present at the fuel/cladding interface for a fuel element in-reactor. Analysis was performed using a scanning electron microscope equipped with energy-dispersive and wavelength dispersive spectrometers (SEM/EDS/WDS) to evaluate any developed diffusion structures. At 700 deg. C, minimal interaction was observed between the metallic fuels and either Zr or V. Similarly, limited interaction was observed between the Zr and V and the cladding materials. The best performing liner material appeared to be the V, based on amounts of interaction. (authors)

  12. Evaluation of simulation learning materials use to fill the gap in Japanese dental English education.

    Science.gov (United States)

    Seki, Naoko; Moross, Janelle; Sunaga, Masayo; Hobo, Koki; Miyoshi, Tomoe; Nitta, Hiroshi; Kinoshita, Atsuhiro; Morio, Ikuko

    2016-01-01

    Even though English is most frequently the common language when the patient's native language differs from that of a dentist, the opportunities for Japanese undergraduate dental students to learn dental English are now quite limited. The purposes of our study were to investigate: the effectiveness and feasibility of the computer-assisted simulation materials as one solution strategy for dental English education in Japan, and the needs and demands for dental English from the learners' side. Interactive simulation materials for medical interviews in English and clinical cases which were translated to English, were delivered via Learning Management System (LMS) to nineteen trainee residents of dentistry (residents). Evaluation for the materials, learners' knowledge and interests in the contents, and ease of operation were obtained by post-questionnaire (response rates were 100% and 95%, respectively). Both questionnaire-surveys received positive feedback toward the materials, yet 47% answered that they lacked the level of knowledge about contents of the medical interview in English. Results were sufficient to suggest that the residents would like to have the opportunity to study or practice medical interview in English, or English related to dentistry, and that the simulation materials could be one of the solution strategies for opportunity provision.

  13. Evaluation of simulation learning materials use to fill the gap in Japanese dental English education.

    Science.gov (United States)

    Seki, Naoko; Moross, Janelle; Sunaga, Masayo; Hobo, Koki; Miyoshi, Tomoe; Nitta, Hiroshi; Kinoshita, Atsuhiro; Morio, Ikuko

    2016-01-01

    Even though English is most frequently the common language when the patient's native language differs from that of a dentist, the opportunities for Japanese undergraduate dental students to learn dental English are now quite limited. The purposes of our study were to investigate: the effectiveness and feasibility of the computer-assisted simulation materials as one solution strategy for dental English education in Japan, and the needs and demands for dental English from the learners' side. Interactive simulation materials for medical interviews in English and clinical cases which were translated to English, were delivered via Learning Management System (LMS) to nineteen trainee residents of dentistry (residents). Evaluation for the materials, learners' knowledge and interests in the contents, and ease of operation were obtained by post-questionnaire (response rates were 100% and 95%, respectively). Both questionnaire-surveys received positive feedback toward the materials, yet 47% answered that they lacked the level of knowledge about contents of the medical interview in English. Results were sufficient to suggest that the residents would like to have the opportunity to study or practice medical interview in English, or English related to dentistry, and that the simulation materials could be one of the solution strategies for opportunity provision. PMID:27181485

  14. An Approach to Acoustic Emission Technique Applications to Evaluate Damage Mechanisms in Composite Materials

    Directory of Open Access Journals (Sweden)

    Rios-Soberanis C.R.

    2015-01-01

    Full Text Available Acoustic Emission technique is a versatile method for characterization in materials science. It is considered to be a “passive” non-destructive method since damage can be only evaluated when de defects are being developed during the test which, at the end of the day, it is considered an advantage because failure mechanisms and damage process can be monitored and identified during the load history. When a failure mechanism is activated due to a discontinuity in the material such as crack propagation, part of the total strain energy is dissipated as an elastic waves that propagate from the damage source through the medium. Therefore, this released energy can be detected by piezoelectric sensors that perceive the emitted signal from the damage notation site by the surface dynamic movement and convert it in an electrical response. Acoustic emission signals can be correlated with the onset of damage process occurring in the tested materials and also to de diverse failure mechanisms such as matrix cracking, interface damage, fiber fracture, etc. This paper proposes to discuss our information and results on acoustic emission materials characterization undertaken on different types of materials.

  15. Radiopacity evaluation of root-end filling materials by digitization of images

    Directory of Open Access Journals (Sweden)

    Mario Tanomaru-Filho

    2008-12-01

    Full Text Available The purpose of this study was to evaluate the radiopacity of 5 root-end filling materials (white MTA-Angelus, grey MTA-Angelus, IRM, Super EBA and Sealer 26. Five specimens (10 mm diameter X 1 mm thickness were made from each material and radiographed next to an aluminum stepwedge varying in thickness from 2 to 16 mm. Radiographs were digitized and the radiopacity of the materials was compared to that of the aluminum stepwedge using VIXWIN 2000 software in millimeters of aluminum (mm Al. Data were analyzed statistically by ANOVA and Tukey's test at 5% significance level. Radiopacity values varied from 3 mm Al to 5.9 mm Al. Sealer 26 and IRM presented the highest radiopacity values (p<0.05, while white/grey MTA and Super EBA presented the lowest radiopacity values (p<0.05. The tested root-end filling materials presented different radiopacities, white/grey MTA and Super EBA being the least radiopaque materials.

  16. Analytical Method to Evaluate Hugoniot of Metallic Materials with Different Initial Temperatures

    Institute of Scientific and Technical Information of China (English)

    WANG Qing-Song; LAN Qiang; HU Jian-Bo; WU Jing; DAI Cheng-Da

    2008-01-01

    @@ An analytical method is proposed to evaluate the Hugoniot parameters of preheated metallic materials by relating to its principal Hugoniot.Modelling calculations for 1100 AI, Cu and Ta show that the preheating lowers to a certain extent the shock impedance and the degree of lowering the shock impedance increases with increasing pre-heating temperature.The Hugoniots of 6061-T6 AI and TC4 preheated flyers at known preheating temperatures are evaluated, and are utilized to calculate the particle velocity and shock pressure using the impedance-match method based on the measured shock wave velocity and impact velocity reported in Z pinch-driven and threestage gun-driven Hugoniot experiments.The presented method allows a reasonable evaluation for Hugoniot of the preheated metallic flyers.

  17. The Oil Point Method - A tool for indicative environmental evaluation in material and process selection

    DEFF Research Database (Denmark)

    Bey, Niki

    2000-01-01

    , transport, use to final disposal. Therefore, efforts focus on attempts to integrate environmental aspects into the whole process of product development and design. They often involve established tools and methods for environmental evaluation, such as formal Life Cycle Assessment (LCA). These tools...... of environmental evaluation and only approximate information about the product and its life cycle. This dissertation addresses this challenge in presenting a method, which is tailored to these requirements of designers - the Oil Point Method (OPM). In providing environmental key information and confining itself...... methods for environmental evaluation: A formal LCA method and another indicator-based method. A set of data for applying the method is presented including over 70 materials in pure or semi-finished form, over 20 manufacturing processes and some 20 other life cycle processes. Other contributions...

  18. SEM evaluation of the interface between filling and root-end filling materials.

    Science.gov (United States)

    Rosa, R A; Santini, M F; Heiden, K; Só, B B; Kuga, M C; Pereira, J R; Só, M V R

    2014-01-01

    The aim of this ex vivo study was to evaluate, by scanning electron microscopy (SEM), the presence of gaps at the interface between filling material and three root-end filling materials. Thirty human upper molars disto-buccal roots were instrumented and filled with gutta-percha and eugenol-based sealer. The apicoectomy was performed 2 mm from the apex and retrograde cavities were prepared with ultrasonic points (3 mm in deep). The samples were divided into three experimental groups (n = 10): Group I-white mineral trioxide aggregate (MTA); Group II-Super EBA; and Group III-Portland cement. The root-end filling materials were inserted into the retocavities using a MTA carrier. After 48 h, the roots were transversally sectioned in order to obtain the apical 5 mm. Next, each specimen was prepared longitudinally with crescent granulation of abrasives water-wet sandpapers in order to expose the filling and root-end filling materials. Then, the specimens were subjected to slow dehydration with silica gel, mounted onto specific stubs and coated with paladium coverage for SEM analysis of the interface between filling and root-end filling materials. The percentage of gaps at the interfacial area was calculated by using Image Tool 3.0 software. Super EBA presented the higher percentage of gaps (1.5 ± 0.67%), whereas MTA presented the lowest values (0.33 ± 0.20%; p = 0.0004). Despite the statistical differences observed between Super EBA and MTA, all the root-end filling materials presented great adaptation to the filling material, presenting small amount of gaps. PMID:23733414

  19. Evaluation of Alternate Materials and Methods for Strontium and Alpha Removal from Savannah River Site High-Level Waste Solutions

    Energy Technology Data Exchange (ETDEWEB)

    Hobbs, D.T.

    2000-11-07

    A literature survey indicated a number of alternate materials and methods for the removal of strontium and alpha-emitting radionuclides (actinides). We evaluated the use of alternate materials versus proposed flowsheets for salt processing at the Savannah River Site (SRS). From this evaluation we recommend the following materials for further testing to determine the rate and extent of removal. We do not recommend testing of liquid/liquid extraction and polymer filtration methods at this time.

  20. Living in a material world: Development and evaluation of a new materials science course for non-science majors

    Science.gov (United States)

    Brust, Gregory John

    This study was designed to discover if there is a difference in the scientific attitudes and process skills between a group of students who were instructed with Living in a Material World and groups of students in non-science majors sections of introductory biology, chemistry, and geology courses at the University of Southern Mississippi (USM). Each of the four courses utilized different instructional techniques. Students' scientific attitudes were measured with the Scientific Attitudes Inventory (SAI II) and their knowledge of science process skills were measured with the Test of Integrated Process Skills (TIPS II). The Group Assessment of Logical Thinking (GALT) was also administered to determine if the cognitive levels of students are comparable. A series of four questionnaires called Qualitative Course Assessments (QCA) were also administered to students in the experimental course to evaluate subtle changes in their understanding of the nature and processes of science and attitudes towards science. Student responses to the QCA questionnaires were triangulated with results of the qualitative instruments, and students' work on the final project. Results of the GALT found a significant difference in the cognitive levels of students in the experimental course (PSC 190) and in one of the control group, the introductory biology (BSC 107). Results of the SAI II and the TIPS II found no significant difference between the experimental group and the control groups. Qualitative analyses of students' responses to selected questions from the TIPS II, selected items on the SAI II, QCA questionnaires, and Materials that Fly project reports demonstrate an improvement in the understanding of the nature and processes of science and a change to positive attitude toward science of students in the experimental group. Students indicated that hands-on, inquiry-based labs and performance assessment were the most effective methods for their learning. These results indicate that science

  1. Progress Report {number_sign}1 on the materials identification, characterization and evaluation activity: Acquisition of materials data from the Exploratory Studies Facility

    Energy Technology Data Exchange (ETDEWEB)

    Meike, A., LLNL

    1998-02-01

    This paper reports on the initial work within the Materials Identification, Characterization and Evaluation Sub-activity Integration Activity within the Introduced Materials Task (IMT) (WBS 1.2.3.12.5). The goals of this activity are twofold.: (1) to identify and characterize types and usage of materials that are most likely to be introduced into a potential High Level Radioactive Waste (HLW) repository at Yucca Mountain, Nevada, as a result of its construction and operation and (2) to provide tools for the Integration Activity to evaluate the chemical impact on the repository based on information gathered from sources external and internal to the Introduced Materials Task-by the Literature Survey Sub-activity (Integration Activity, IMT). Based on this information and assessment, the Integration Activity activates relevant activities within the Introduced Materials Task and provides information to other Tasks within the Yucca Mountain Project.

  2. Evaluation of dimensional stability and accuracy of autoclavable polyvinyl siloxane impression material.

    Science.gov (United States)

    Reddy, Subash M; Vijitha, D; Karthikeyan, S; Balasubramanian, R; Satish, A

    2013-12-01

    Dimensionally stable autoclavable impressions will be effective in controlling the cross-infection and contamination caused by patient's saliva and other oral secretions. The accuracy of newly introduced autoclavable polyvinyl siloxane impression material was assessed for its dimensional stability and accuracy. A standard metal model (Dentoform, U-501, Columbia) was customised for impression making. The impressions were made using the newly introduced polyvinyl siloxane impression materials (AFFINIS, Coltene/Whaledent AG, 9450 Alstalten, Switzerland). Fifty impressions were made and were divided into two groups A and B of 25 each. Group A was the control sample (non-autoclaved impressions) and group B was the test sample (autoclaved impressions), which was subjected to the steam autoclave procedure at 134 °C for 18 min, casts were poured in type IV gypsum products. The customised metal model, casts obtained from control and test group were subjected to laboratory evaluation with help of a travelling microscope (×10 magnification), and digital vernier calliper (0.01 mm/10 μm accuracy). Data analysis was done using one-way ANOVA and One-Sample t test to evaluate the overall accuracy (P polyvinyl siloxane impression material is accurate and dimensional stable for clinical use when steam autoclaved at 134 °C for 18 min.

  3. Improvement and evaluation of thermal, electrical, sealing and mechanical contacts, and their interface materials

    Science.gov (United States)

    Luo, Xiangcheng

    Material contacts, including thermal, electrical, seating (fluid sealing and electromagnetic sealing) and mechanical (pressure) contacts, together with their interface materials, were, evaluated, and in some cases, improved beyond the state of the art. The evaluation involved the use of thermal, electrical and mechanical methods. For thermal contacts, this work evaluated and improved the heat transfer efficiency between two contacting components by developing various thermal interface pastes. Sodium silicate based thermal pastes (with boron nitride particles as the thermally conductive filler) as well as polyethylene glycol (PEG) based thermal pastes were developed and evaluated. The optimum volume fractions of BN in sodium silicate based pastes and PEG based pastes were 16% and 18% respectively. The contribution of Li+ ions to the thermal contact conductance in the PEG-based paste was confirmed. For electrical contacts, the relationship between the mechanical reliability and electrical reliability of solder/copper and silver-epoxy/copper joints was addressed. Mechanical pull-out testing was conducted on solder/copper and silver-epoxy/copper joints, while the contact electrical resistivity was measured. Cleansing of the copper surface was more effective for the reliability of silver-epoxy/copper joint than that of solder/copper joint. For sealing contacts, this work evaluated flexible graphite as an electromagnetic shielding gasket material. Flexible graphite was found to be at least comparable to conductive filled silicone (the state of the art) in terms of the shielding effectiveness. The conformability of flexible graphite with its mating metal surface under repeated compression was characterized by monitoring the contact electrical resistance, as the conformability is important to both electromagnetic scaling and fluid waling using flexible graphite. For mechanical contacts, this work focused on the correlation of the interface structure (such as elastic

  4. Comparative Evaluation of Flexural Strength of Provisional Crown and Bridge Materials-An Invitro Study

    Science.gov (United States)

    Garg, Sandeep

    2016-01-01

    Introduction Provisional restorations serve a key role as a functional and esthetic try-in for the design of the final prosthesis. During selection of materials for this restoration, clinicians must consider physical properties, ease of handling, cost and patient satisfaction and approval. Aim To evaluate and compare the flexural strength of provisional crown and bridge materials available commercially. Materials and Methods This in-vitro study was done to compare the flexural strength of six temporary crown and bridge materials available commercially at 24 hours, 8 days and after repair. Three poly methyl methacrylate based materials (DPI, SC10 and Trulon) and three bis-acrylic based composite resins (Protemp, Cooltemp and Luxatemp) were selected. A total of 72 specimens of dimensions 64mm×10mm×2.5mm were prepared from these materials (12 from each material) and divided into two groups (n=36). Specimens were stored in artificial saliva and were fractured after 24 hours and 8 days using Universal Testing Machine. The fractured samples from the 8 days study were then subjected to repair. A uniform space of 2mm and a 450 bevel was maintained for all the repaired samples for better distribution of forces. Flexural strength of these repaired samples was recorded using the same machine. Results were recorded and statistically analysed by one-way Anova and Post hoc tests. Result: Results revealed that there was decrease in flexural strength for all the materials tested from 24 hours to 8 days, though flexural strength between poly methyl methacrylate and bis-acrylic resins was similar at 24 hours and 8 days time interval. A substantial decrease was noticed in the strength of bis-acrylic composite resins after repair. Conclusion From the current study it can be suggested that though there is decrease in flexural strength for all the materials from 24 hours to 8 days, both can be used to fabricate the provisional restorations. However, in the event of a fracture of a bis

  5. Evaluation of municipal solid waste management performance by material flow analysis: Theoretical approach and case study.

    Science.gov (United States)

    Zaccariello, Lucio; Cremiato, Raffaele; Mastellone, Maria Laura

    2015-10-01

    The main role of a waste management plan is to define which is the combination of waste management strategies and method needed to collect and manage the waste in such a way to ensure a given set of targets is reached. Objectives have to be sustainable and realistic, consistent with the environmental policies and regulations and monitored to verify the progressive achievement of the given targets. To get the aim, the setting up and quantification of indicators can allow the measurement of efficiency of a waste management system. The quantification of efficiency indicators requires the developing of a material flow analysis over the system boundary, from waste collection to secondary materials selling, processing and disposal. The material flow analysis has been carried out with reference to a case study for which a reliable, time- and site-specific database was available. The material flow analysis allowed the evaluation of the amount of materials sent to recycling, to landfilling and to waste-to-energy, by highlighting that the sorting of residual waste can further increase the secondary materials amount. The utilisation of energy recovery to treat the low-grade waste allows the maximisation of waste diversion from landfill with a low production of hazardous ash. A preliminary economic balance has been carried out to define the gate fee of the waste management system that was in the range of 84-145 € t(-1) without including the separate collection cost. The cost of door-by-door separate collection, designed to ensure the collection of five separate streams, resulted in 250 € t(-1) ±30%. PMID:26253498

  6. Evaluation of dredged material proposed for ocean disposal from Westchester Creek project area, New York

    Energy Technology Data Exchange (ETDEWEB)

    Pinza, M.R.; Gardiner, W.W.; Barrows, E.S.; Borde, A.B.

    1996-11-01

    The objective of the Westchester Creek project was to evaluate proposed dredged material from this area to determine its suitability for unconfined ocean disposal at the Mud Dump Site. Westchester Creek was one of five waterways that the US Army Corps of Engineers- New York District (USACE-NYD) requested the Battelle/Marine Sciences Laboratory (MSL) to sample and evaluate for dredging and disposal in May 1995. The evaluation of proposed dredged material from the Westchester Creek project area consisted of bulk sediment chemical analyses, chemical analyses of dredging site water and elutriate, benthic acute and water-column toxicity tests, and bioaccumulation studies. Thirteen individual sediment core samples were collected from this area and analyzed for grain size, moisture content, and total organic carbon (TOC). One composite sediment sample representing the Westchester Creek area to be dredged, was analyzed for bulk density, specific gravity, metals, chlorinated pesticides, polychlorinated biphenyl (PCB) congeners, polynuclear aromatic hydrocarbons (PAHs), and 1,4-dichlorobenzene. Dredging site water and elutriate water, which is prepared from the suspended- particulate phase (SPP) of the Westchester Creek sediment composite, was analyzed for metals, pesticides, and PCBS.

  7. Energy Absorption and Dynamic Deformation of Backing Material for Ballistic Evaluation of Body Armour

    Directory of Open Access Journals (Sweden)

    Debarati\tBhattacharjee

    2014-09-01

    Full Text Available The\tmeasurement\tof back face signature\t(BFS or\tbehind armour\tblunt trauma (BABT is\ta critical\taspect of ballistic evaluation of body\tarmour. BFS is the impact experienced by the\tarmour wearing body,\twhen subjected to\ta non-penetrating\tprojectile. Mineral\tor polymeric\tclay\tis used to measure the\tBFS. In addition to stopping the\tprojectile,\tthe body armour can be used only when the BFS also falls within\tpermissible limits.\tThe\textent of\tthe BFS depends upon the\tbehavior\tof the backing material\tin different loading conditions and prior history.\tThis\tpaper explains some of the\tstudies carried out on the backing\tmaterial used for ballistic evaluation\tin Terminal Ballistics Research\tLaboratory, Chandigarh. It has been observed\tthat\tthe backing material is highly non-linear\tviscoelastic in nature. The depth\tof\tdeformation is also linearly\tproportional to the\timpact\tenergy\tand\ttemperature. The\teffect of time\ton the depth of deformation\tis gradual and does\tnot influence the BFS values during a\tstandard\tballistic evaluation comprising of 6-8\tshots.

  8. Evaluation of hardness and color stability in the soft lining materials after thermocycling and chemical polishing.

    Science.gov (United States)

    Goiato, Marcelo Coelho; Falcón-Antenucci, Rosse Mary; Santos, Daniela Micheline dos; Pellizzer, Eduardo Piza

    2009-01-01

    The aim of this study was to evaluate the Shore A hardness and color stability of two soft lining materials after thermocycling and when chemical polishing was used or omitted. Two acrylic-based soft lining materials were tested: Coe-Soft and Soft Confort, 14 specimens were made for each material. They were distributed in four groups according to the treatment performed. The specimens were thermocycled (1000 cycles) and half of the group submitted to chemical polishing (methyl methacrylate). Shore A hardness was determined and color stability was calculated by means of Commission International de l'Eclairage Lab uniform color scale using a spectrophotometer, the measurements were made immediately after deflasked, chemical polishing and thermocycling. Analysis of variance (ANOVA) and Tukey's tests were performed at p Confort (10.60) showed significantly higher values than Coe-Soft (4.57). Coe-Soft (26.42) showed higher Shore A hardness values than Soft Confort (19.42). Chemical polishing did not influence in the color stability of both materials; however, influenced in the hardness values of Coe-Soft. PMID:19601498

  9. Nevada Nuclear Waste Storage Investigations: Exploratory Shaft Facility fluids and materials evaluation

    Energy Technology Data Exchange (ETDEWEB)

    West, K.A.

    1988-11-01

    The objective of this study was to determine if any fluids or materials used in the Exploratory Shaft Facility (ESF) of Yucca Mountain will make the mountain unsuitable for future construction of a nuclear waste repository. Yucca Mountain, an area on and adjacent to the Nevada Test Site in southern Nevada, USA, is a candidate site for permanent disposal of high-level radioactive waste from commercial nuclear power and defense nuclear activities. To properly characterize Yucca Mountain, it will be necessary to construct an underground test facility, in which in situ site characterization tests can be conducted. The candidate repository horizon at Yucca Mountain, however, could potentially be compromised by fluids and materials used in the site characterization tests. To minimize this possibility, Los Alamos National Laboratory was directed to evaluate the kinds of fluids and materials that will be used and their potential impacts on the site. A secondary objective was to identify fluids and materials, if any, that should be prohibited from, or controlled in, the underground. 56 refs., 19 figs., 11 tabs.

  10. Ecological evaluation of proposed dredged material from St. Andrew Bay, Florida

    Energy Technology Data Exchange (ETDEWEB)

    Mayhew, H.L.; Word, J.Q.; Kohn, N.P.; Pinza, M.R.; Karle, L.M.; Ward, J.A. [Battelle/Marine Sciences Lab., Sequim, WA (United States)

    1993-10-01

    The US Army Corps of Engineers (USACE), Mobile District, requested that the Battelle/Marine Sciences Laboratory (MSL) conduct field sampling and chemical and biological testing to determine the suitability of potential dredged material for open ocean disposal. Sediment from St. Andrew Bay was chemically characterized and evaluated for biological toxicity and bioaccumulation of contaminants. The Tier III guidance for ocean disposal testing requires tests of water column effects (following dredged material disposal), deposited sediment toxicity, and bioaccumulation of contaminants from deposited sediment (dredged material). To meet these requirements, the MSL conducted suspended-particulate-phase (SPP) toxicity tests, solid-phase toxicity tests, and bioaccumulation testing on sediment representing potential dredged material from Panama City Harbor. Physical and chemical characterization of sediment to support toxicity and bioaccumulation results was also conducted on both the test and reference sediments. The MSL collected sediment samples from five sites in St. Andrew Bay and one reference site near Lands End Peninsula. The five test sediments and the reference sediment were analyzed for physical and chemical sediment characteristics, SPP chemical contaminants, solid-phase toxicity, SPP toxicity, and bioaccumulation of contaminants.

  11. Nevada Nuclear Waste Storage Investigations: Exploratory Shaft Facility fluids and materials evaluation

    International Nuclear Information System (INIS)

    The objective of this study was to determine if any fluids or materials used in the Exploratory Shaft Facility (ESF) of Yucca Mountain will make the mountain unsuitable for future construction of a nuclear waste repository. Yucca Mountain, an area on and adjacent to the Nevada Test Site in southern Nevada, USA, is a candidate site for permanent disposal of high-level radioactive waste from commercial nuclear power and defense nuclear activities. To properly characterize Yucca Mountain, it will be necessary to construct an underground test facility, in which in situ site characterization tests can be conducted. The candidate repository horizon at Yucca Mountain, however, could potentially be compromised by fluids and materials used in the site characterization tests. To minimize this possibility, Los Alamos National Laboratory was directed to evaluate the kinds of fluids and materials that will be used and their potential impacts on the site. A secondary objective was to identify fluids and materials, if any, that should be prohibited from, or controlled in, the underground. 56 refs., 19 figs., 11 tabs

  12. Evaluation of laser induced breakdown spectroscopy for the determination of micronutrients in plant materials

    Energy Technology Data Exchange (ETDEWEB)

    Trevizan, Lilian Cristina [Centro de Energia Nuclear na Agricultura-Universidade de Sao Paulo, Av. Centenario 303, 13416-000, Piracicaba-SP (Brazil); Santos, Dario [Universidade Federal de Sao Paulo - UNIFESP, Rua Prof. Artur Riedel 275, 09972-270, Diadema-SP (Brazil); Elgul Samad, Ricardo; Dias Vieira, Nilson [Centro de Lasers e Aplicacoes, IPEN/CNEN-SP, Av. Prof. Lineu Prestes 2242, 05508-000, Sao Paulo-SP (Brazil); Nunes, Lidiane Cristina [Centro de Energia Nuclear na Agricultura-Universidade de Sao Paulo, Av. Centenario 303, 13416-000, Piracicaba-SP (Brazil); Departamento de Quimica, Universidade Federal de Sao Carlos, Rodovia Washington Luis (SP-310), km 235, 13565-905, Sao Carlos-SP (Brazil); Aparecida Rufini, Iolanda [Centro de Energia Nuclear na Agricultura-Universidade de Sao Paulo, Av. Centenario 303, 13416-000, Piracicaba-SP (Brazil); Krug, Francisco Jose [Centro de Energia Nuclear na Agricultura-Universidade de Sao Paulo, Av. Centenario 303, 13416-000, Piracicaba-SP (Brazil)], E-mail: fjkrug@cena.usp.br

    2009-05-15

    Laser induced breakdown spectroscopy (LIBS) has been evaluated for the determination of micronutrients (B, Cu, Fe, Mn and Zn) in pellets of plant materials, using NIST, BCR and GBW biological certified reference materials for analytical calibration. Pellets of approximately 2 mm thick and 15 mm diameter were prepared by transferring 0.5 g of powdered material to a 15 mm die set and applying 8.0 tons cm{sup -2}. An experimental setup was designed by using a Nd:YAG laser operating at 1064 nm (200 mJ per pulse, 10 Hz) and an Echelle spectrometer with ICCD detector. Repeatability precision varied from 4 to 30% from measurements obtained in 10 different positions (8 laser shots per test portion) in the same sample pellet. Limits of detection were appropriate for routine analysis of plant materials and were 2.2 mg kg{sup -1} B, 3.0 mg kg{sup -1} Cu, 3.6 mg kg{sup -1} Fe, 1.8 mg kg{sup -1} Mn and 1.2 mg kg{sup -1} Zn. Analysis of different plant samples were carried out by LIBS and results were compared with those obtained by ICP OES after wet acid decomposition.

  13. Physical evaluation of a new pulp capping material developed from portland cement

    Science.gov (United States)

    Negm, Ahmed; Hassanien, Ehab; Abu-Seida, Ashraf

    2016-01-01

    Background This study examined the effects of addition of 10% and 25% by weight calcium hydroxide on the physicochemical properties of Portland cement associated with 20% bismuth oxide in order to develop a new pulp capping material. Material and Methods The solubility, pH value, setting time, compressive strength, and push out bond strength of modified Portland were evaluated and compared to those of mineral trioxide aggregate (MTA) and Portland cement containing 20% bismuth oxide. Results The statistical analysis was performed with ANOVA and Duncan’s post-hoc test. The results show that the strength properties and push out bond strength of Portland cement were adversely affected by addition of calcium hydroxide especially with a ratio of 25 wt%, however, the setting time and pH were not affected. MTA showed a statistically significant lower setting time than other cements (P≤0.001). Portland cement with bismuth oxide and Port Cal I showed a statistically significant higher Push out Bond strength than MTA and Port Cal II (P=0.001). Conclusions Taking the setting time, push out bond strength and pH value into account, addition of 10 wt% calcium hydroxide to Portland cement associated with 20% bismuth oxide produces a new pulp capping material with acceptable physical and adhesive properties. Further studies are recommended to test this cement biologically as a new pulp capping material. Key words:Calcium hydroxide, MTA, Portland cement, setting time, solubility, strength. PMID:27398178

  14. DAMAGE AND FRACTURE EVALUATION OF GRANULAR COMPOSITE MATERIALS BY DIGITAL IMAGE CORRELATION METHOD

    Institute of Scientific and Technical Information of China (English)

    ZHANG Jue; XIONG Chunyang; LI Hongju; LI Ming; WANG Jianxiang; FANG Jing

    2004-01-01

    This paper presents the applications of digital image correlation technique to the mesoscopic damage and fracture study of some granular based composite materials including steelfiber reinforced concrete, sandstone and crystal-polymer composite. The deformation fields of the composite materials resulted from stress localization were obtained by the correlation computation of the surface images with loading steps and thus the related damage prediction and fracture parameters were evaluated. The correlation searching could be performed either directly based on the gray levels of the digital images or from the wavelet transform (WT) coefficients of the transform spectrum. The latter was developed by the authors and showed higher resolution and sensitivity to the singularity detection.Because the displacement components came from the rough surfaces of the composite materials without any coats of gratings or fringes of optical interferometry, both surface profiles and the deformation fields of the composites were visualized which was helpful to compare each other to analyze the damage of those heterogeneous materials.

  15. Evaluation of hardness and color stability in the soft lining materials after thermocycling and chemical polishing.

    Science.gov (United States)

    Goiato, Marcelo Coelho; Falcón-Antenucci, Rosse Mary; Santos, Daniela Micheline dos; Pellizzer, Eduardo Piza

    2009-01-01

    The aim of this study was to evaluate the Shore A hardness and color stability of two soft lining materials after thermocycling and when chemical polishing was used or omitted. Two acrylic-based soft lining materials were tested: Coe-Soft and Soft Confort, 14 specimens were made for each material. They were distributed in four groups according to the treatment performed. The specimens were thermocycled (1000 cycles) and half of the group submitted to chemical polishing (methyl methacrylate). Shore A hardness was determined and color stability was calculated by means of Commission International de l'Eclairage Lab uniform color scale using a spectrophotometer, the measurements were made immediately after deflasked, chemical polishing and thermocycling. Analysis of variance (ANOVA) and Tukey's tests were performed at p Confort (10.60) showed significantly higher values than Coe-Soft (4.57). Coe-Soft (26.42) showed higher Shore A hardness values than Soft Confort (19.42). Chemical polishing did not influence in the color stability of both materials; however, influenced in the hardness values of Coe-Soft.

  16. Evaluation on mechanical and corrosion properties of steam generator tubing materials

    Energy Technology Data Exchange (ETDEWEB)

    Kim, In Sup; Lee, Byong Whi; Lee, Sang Kyu; Lee, Young Ho; Kim, Jun Whan; Lee, Ju Seok; Kwon, Hyuk Sang; Kim, Su Jung [Korea Advanced Institute of Science and Technology, Taejon (Korea, Republic of)

    1998-06-15

    Steam generator is one of the major components of nuclear reactor pressure boundary. It's main function os transferring heat which generated in the reactor to turbine generator through steam generator tube. In these days, steam generator tubing materials of operating plant are used Inconel 600 alloys. But according to the operation time, there are many degradation phenomena which included mechanical damage due to flow induced vibration and corrosion damage due to PWSCC, IGA/SCC and pitting etc. Recently Inconel 690 alloys are selected as new and replacement steam generator tubes for domestic nuclear power plant. But there are few study about mechanical and corrosion properties of Inconel 600 and 690. The objectives of this study is to evaluate and compare mechanical and corrosion propertied of steam generator tube materials.

  17. Impact and Friction Sensitivity of Energetic Materials:Methodical Evaluation of Technological Safety Features

    Institute of Scientific and Technical Information of China (English)

    Aleksandr Smirnov; Oleg Voronko; Boris Korsunsky; Tatyana Pivina

    2015-01-01

    Key methods developed and used in the USSR and in the Russian Federation to determine the impact and friction sensitivity of energetic materials and explosives have been discussed.Experimental methodologies and instruments that underlie the assessment of their production and handling safety have been described.Studies of a large number of compounds have revealed relationships between their sensitivity parameters and structure of individual compounds and compositions.The range of change of physical and chemical characteristics for the compounds we examined covers the entire region of their existence.Theoretical methodology and equations have been formulated to estimate the impact and friction sensitivity parameters of energetic materials and to evaluate the technological safety in use.The developed methodology is characterized by high-accuracy calculations and prediction of sensitivity parameters.

  18. Evaluation on mechanical and corrosion properties of steam generator tubing materials

    International Nuclear Information System (INIS)

    Steam generator is one of the major components of nuclear reactor pressure boundary. It's main function os transferring heat which generated in the reactor to turbine generator through steam generator tube. In these days, steam generator tubing materials of operating plant are used Inconel 600 alloys. But according to the operation time, there are many degradation phenomena which included mechanical damage due to flow induced vibration and corrosion damage due to PWSCC, IGA/SCC and pitting etc. Recently Inconel 690 alloys are selected as new and replacement steam generator tubes for domestic nuclear power plant. But there are few study about mechanical and corrosion properties of Inconel 600 and 690. The objectives of this study is to evaluate and compare mechanical and corrosion propertied of steam generator tube materials

  19. Evaluation of the Community's research programme ''Nuclear measurements and reference materials'' (1980-1985)

    International Nuclear Information System (INIS)

    A panel has evaluated the research programme ''Nuclear measurements and reference materials'' performed by JRC-Geel, CBNM (Central Bureau for Nuclear Measurements) during the period 1980-85. Furthermore the panel has considered more general topics such as major facilities, staff and collaboration between JRC-Geel, CBNM and other organizations. Finally, the panel has discussed the future direction of the programme. The panel expressed its satisfaction with the scientific and technical quality of the work and recommended that JRC-Geel, CBNM should continue to play an important role in Europe in the fields of nuclear measurements and nuclear reference materials. The panel also recommended that the underlying research be strengthened and that the nuclear experience and expertise of JRC-Geel, CBNM be utilized for non-nuclear applications

  20. Evaluation of Sulfur 'Concrete' for Use as a Construction Material on the Lunar Surface

    Science.gov (United States)

    Grugel, R. N.

    2008-01-01

    Combining molten sulfur with any number of aggregate materials forms, when solid, a mixture having attributes similar, if not better, to conventional water-based concrete. As a result the use of sulfur "concrete" on Earth is well established, particularly in corrosive environments. Consequently, discovery of troilite (FeS) on the lunar surface prompted numerous scenarios about its reduction to elemental sulfur for use, in combination with lunar regolith, as a potential construction material; not requiring water, a precious resource, for its manufacture is an obvious advantage. However, little is known about the viability of sulfur concrete in an environment typified by extreme temperatures and essentially no atmosphere. The experimental work presented here evaluates the response of pure sulfur and sulfur concrete subjected to laboratory conditions that approach those expected on the lunar surface, the results suggesting a narrow window of application.

  1. Evaluating knowledge benefits of automotive lightweighting materials R&D projects.

    Science.gov (United States)

    Peretz, Jean H; Das, Sujit; Tonn, Bruce E

    2009-08-01

    This paper presents a set of metrics used to evaluate short-run knowledge benefits that accrued from research and development (R&D) projects funded in fiscal years 2000-2004 by automotive lightweighting materials (ALM) of the U.S. Department of Energy (DOE). Although DOE presents to Congress energy, environmental, and security benefits and costs of its R&D efforts under the Government Performance and Results Act, DOE has yet to include knowledge benefits in that report [U.S. Department of Energy. (2007). Projected benefits of federal energy efficiency and renewable energy programs: FY2008 budget request. NREL/TP-640-41347 (March). Washington, DC: National Renewable Energy Laboratory for DOE Energy Efficiency and Renewable Energy. Retrieved February 12, 2007 from http://www1.eere.energy.gov/ba/pba/2008_benefits.html]. ALM focuses on development and validation of advanced technologies that significantly reduce automotive vehicle body and chassis weight without compromising other attributes such as safety, performance, recyclability, and cost [U.S. Department of Energy. (2005a). Automotive lightweighting materials 2004 annual progress report. Washington, DC: DOE Energy Efficiency and Renewable Energy. Retrieved March 30, 2005 from http://www.eere.energy.gov/vehiclesandfuels/resources/fcvt_alm_fy04.shtml]. The ultimate goal of ALM to have lightweighter materials in vehicles hinges on many issues, including the (1) collaborative nature of ALMs R&D with the automobile industry and (2) manufacturing knowledge gained through the R&D effort. The ALM projects evaluated in this paper yielded numerous knowledge benefits in the short run. While these knowledge benefits are impressive, there remains uncertainty about whether the research will lead to incorporation of lightweight materials by the Big Three automakers into their manufacturing process and introduction of lightweight vehicles into the marketplace. The uncertainty illustrates a difference between (1) knowledge

  2. Evaluating Safeguards Benefits of Process Monitoring as compared with Nuclear Material Accountancy

    Energy Technology Data Exchange (ETDEWEB)

    Humberto Garcia; Wen-Chiao Lin; Reed Carlson

    2014-07-01

    This paper illustrates potential safeguards benefits that process monitoring (PM) may have as a diversion deterrent and as a complementary safeguards measure to nuclear material accountancy (NMA). This benefit is illustrated by quantifying the standard deviation associated with detecting a considered material diversion scenario using either an NMA-based method or a PM-based approach. To illustrate the benefits of PM for effective safeguards, we consider a reprocessing facility. We assume that the diversion of interest for detection manifests itself as a loss of Pu caused by abnormally operating a dissolver for an extended period to accomplish protracted diversion (or misdirection) of Pu to a retained (unconditioned) waste stream. For detecting the occurrence of this diversion (which involves anomalous operation of the dissolver), we consider two different data evaluation and integration (DEI) approaches, one based on NMA and the other based on PM. The approach based on PM does not directly do mass balance calculations, but rather monitors for the possible occurrence of anomaly patterns related to potential loss of nuclear material. It is thus assumed that the loss of a given mass amount of nuclear material can be directly associated with the execution of proliferation-driven activities that trigger the occurrence of an anomaly pattern consisting of series of events or signatures occurring at different unit operations and time instances. By effectively assessing these events over time and space, the PM-based DEI approach tries to infer whether this specific pattern of events has occurred and how many times within a given time period. To evaluate the goodness of PM, the 3 Sigma of the estimated mass loss is computed under both DEI approaches as function of the number of input batches processed. Simulation results are discussed.

  3. Evaluation of dredged material proposed for ocean disposal from Arthur Kill Project Area, New York

    Energy Technology Data Exchange (ETDEWEB)

    Gruendell, B.D.; Barrows, E.S.; Borde, A.B. [Battelle Marine Sciences Lab., Sequim, WA (United States)

    1997-01-01

    The objective of the bioassay reevaluation of Arthur Kill Federal Project was to reperform toxicity testing on proposed dredged material following current ammonia reduction protocols. Arthur Kill was one of four waterways sampled and evaluated for dredging and disposal in April 1993. Sediment samples were recollected from the Arthur Kill Project areas in August 1995. Tests and analyses were conducted according to the manual developed by the USACE and the U.S. Environmental Protection Agency (EPA), Evaluation of Dredged Material Proposed for Ocean Disposal (Testing Manual), commonly referred to as the {open_quotes}Green Book,{close_quotes} and the regional manual developed by the USACE-NYD and EPA Region II, Guidance for Performing Tests on Dredged Material to be Disposed of in Ocean Waters. The reevaluation of proposed dredged material from the Arthur Kill project areas consisted of benthic acute toxicity tests. Thirty-three individual sediment core samples were collected from the Arthur Kill project area. Three composite sediments, representing each reach of the area proposed for dredging, was used in benthic acute toxicity testing. Benthic acute toxicity tests were performed with the amphipod Ampelisca abdita and the mysid Mysidopsis bahia. The amphipod and mysid benthic toxicity test procedures followed EPA guidance for reduction of total ammonia concentrations in test systems prior to test initiation. Statistically significant acute toxicity was found in all Arthur Kill composites in the static renewal tests with A. abdita, but not in the static tests with M. bahia. Statistically significant acute toxicity and a greater than 20% increase in mortality over the reference sediment was found in the static renewal tests with A. abdita. M. bahia did not show statistically significant acute toxicity or a greater than 10% increase in mortality over reference sediment in static tests. 5 refs., 2 figs., 2 tabs.

  4. Evaluation of dredged material proposed for ocean disposal from Hackensack River Project Area, New York

    Energy Technology Data Exchange (ETDEWEB)

    Gruendell, B.D.; Barrows, E.S.; Borde, A.B. [Battelle Marine Sciences Lab., Sequim, WA (United States)

    1997-01-01

    The objective of the bioassay reevaluation of the Hackensack River Federal Project was to reperform toxicity testing on proposed dredged material with current ammonia reduction protocols. Hackensack River was one of four waterways sampled and evaluated for dredging and disposal in April 1993. Sediment samples were re-collected from the Hackensack River Project area in August 1995. Tests and analyses were conducted according to the manual developed by the USACE and the U.S. Environmental Protection Agency (EPA), Evaluation of Dredged Material Proposed for Ocean Disposal (Testing Manual), commonly referred to as the {open_quotes}Green Book,{close_quotes} and the regional manual developed by the USACE-NYD and EPA Region II, Guidance for Performing Tests on Dredged Material to be Disposed of in Ocean Waters. The reevaluation of proposed dredged material from the Hackensack River project area consisted of benthic acute toxicity tests. Thirty-three individual sediment core samples were collected from the Hackensack River project area. Three composite sediments, representing each reach of the area proposed for dredging, were used in benthic acute toxicity testing. Benthic acute toxicity tests were performed with the amphipod Ampelisca abdita and the mysid Mysidopsis bahia. The amphipod and mysid benthic toxicity test procedures followed EPA guidance for reduction of total ammonia concentrations in test systems prior to test initiation. Statistically significant acute toxicity was found in all three Hackensack River composites in the static renewal tests with A. abdita, but not in the static tests with M. bahia. Statistically significant acute toxicity and a greater than 20% increase in mortality over the reference sediment was found in the static renewal tests with A. abdita. Statistically significant mortality 10% over reference sediment was observed in the M. bahia static tests. 5 refs., 2 figs., 2 tabs.

  5. Iranian Junior High school English Book Series (Right Path to English Weighted against Material Evaluation Checklists

    Directory of Open Access Journals (Sweden)

    Farhad Golpour

    2012-11-01

    Full Text Available Choosing a course textbook is an overwhelming task for both teachers and administrators. The aim of this study was to evaluate Iranian junior high school textbook series base on validated criteria. For this purpose a careful analyzing textbook evaluation checklists suggested by Sheldon (1984 skierso (1991 and Tucker (1992 was picked out. Among proposed criteria, eighteen critical features were selected to analyze Iranian junior high school series written by Birjandi in (1991. The Criteria were applied to the series analytically by researcher to examine the materials. The criteria in a form of questionnaire given to 15 experienced teachers who were teaching mentioned series for more than ten years. The gathered data revealed that it lacks appropriate layout and physical characteristics, materials have not be recycled, not all skills have been considered equally, emphasis is on grammatical points which practiced through speaking and listening. Moreover; recordings are artificial, no attention is paid to students needs and topics are out of date and boring .Also audio-visual materials, teachers’ guide and communicative tasks seems to be forgotten by writer. Therefore; all eighteen features except vocabulary lists, availability of glossary and lots of grammatical points have not been considered a lot. That is, students' interests have been ignored totally and little communicative issues have been regarded in these series. In fact, at end of this determined time students would be proficient at structural points with no efficiency at communication. These findings can be helpful for curriculum designers, textbook writers to design some valuable textbooks that are useful for teachers to teach language communicatively. Keywords: Junior High school, Evaluation, book series, criteria

  6. MATERIAL COMPATIBILITY EVALUATION FOR DWPF NITRIC-GLYCOLIC ACID - LITERATURE REVIEW

    Energy Technology Data Exchange (ETDEWEB)

    Mickalonis, J.; Skidmore, E.

    2013-06-05

    Glycolic acid is being evaluated as an alternative for formic and nitric acid in the DWPF flowsheet. Demonstration testing and modeling for this new flowsheet has shown that glycolic acid and glycolate has a potential to remain in certain streams generated during the production of the nuclear waste glass. A literature review was conducted to assess the impact of glycolic acid on the corrosion of the materials of construction for the DWPF facility as well as facilities downstream which may have residual glycolic acid and glycolates present. The literature data was limited to solutions containing principally glycolic acid. The reported corrosion rates and degradation characteristics have shown the following for the materials of construction.  For C276 alloy, the primary material of construction for the CPC vessels, corrosion rates of either 2 or 20 mpy were reported up to a temperature of 93 C.  For the austenitic stainless steels, 304L and 316L, variable rates were reported over a range of temperatures, varying from 2 mpy up to 200 mpy (at 100 C).  For 690, G30, Allcorr, Ultimet and Stellite alloys no data were available.  For relevant polymers where data are available, the data suggests that exposure to glycolic acid is not detrimental. The literature data had limited application to the DWPF process since only the storage and feed vessels, pumps and piping used to handle the glycolic acid are directly covered by the available data. These components are either 304L or 316L alloys for which the literature data is inconsistent (See Bullet 2 above). Corrosion rates in pure glycolic acid solutions also are not representative of the DWPF process streams. This stream is complex and contains aggressive species, i.e. chlorides, sulfates, mercury, as well as antifoaming agents which cumulatively have an unknown effect on the corrosion rates of the materials of construction. Therefore, testing is recommended to investigate any synergistic effects of the

  7. Testing and performance evaluation of T1000G/RS-14 graphite/polycyanate composite materials

    Energy Technology Data Exchange (ETDEWEB)

    Starbuck, J.M.

    1997-01-01

    The performance of a graphite fiber/polycyanate matrix composite material system, T1000G/RS-14, was evaluated by performing an extensive mechanical property test program. The test program included both static strength and long-term tests for creep, fatigue, and stress rupture. The system was evaluated at both ambient temperature and elevated temperatures. The specimens were machined from composite cylinders that had a unidirectional layup with all the fibers oriented in the hoop direction. The cylinders were fabricated using the wet-filament winding process. In general, the T1000G/RS-14 system demonstrated adequate static strengths for possible aerospace structural applications. The results from the static tests indicated that very high composite hoop tensile strengths can be achieved with this system at both ambient and elevated temperatures as high as 350{degree}F. However, in the long-term testing for compressive creep and tension-tension fatigue the results indicated a lower elevated temperature was required to minimize the risk of using this material system. Additional testing and analysis activities led to the selection of 275{degree}F as the desired temperature for future performance evaluation. Subsequent testing efforts for determining the resin and composite transverse compressive creep responses at 275{degrees}F indicated that excessive creep strain rates may still be a weakness of this system. In the long-term tests, sufficient data was generated from impregnated strand and composite ring stress-life testing, and composite ring tension-tension fatigue to determine failure probabilities for a given set of design requirements. The statistical analyses of the test data, in terms of determining failure probability curves, will be reported on in a separate report. However, it is expected that this material system will have a very low failure probability for stress rupture based on the collected stress-life data. Material responses that will require further

  8. Applicability of miniature specimen techniques for evaluating the mechanical properties of pressure tube and cladding material

    International Nuclear Information System (INIS)

    The Miniature Specimen Test Techniques (MSTT) namely Small Punch Test (SPT) and Ball Indentation Test (BIT) are commonly employed for evaluating the tensile properties of metallic materials. While discs of 3mm diameter with 0.25mm thickness are utilized for SPT method, the samples for BIT are of any shape with parallel polished top and bottom surfaces having thickness of at least 1mm. The SPT technique is based on driving a ball through clamped miniature disc specimens for deforming till it fractures whereas BIT involves multiple indentations, load and unload cycles at a single indentation point on a polished metallic surface by a spherical indenter. The specimens were fabricated from Zr-2.5%Nb pressure tube (PT) material that is used in pressurised heavy water reactor (PHWR). A suitable die-punch assembly was designed and developed in house to clamp the specimen to carry out the small punch test with the help of a screw-driven universal testing machine. In this work we have utilized miniature tensile specimens for evaluating and comparing the mechanical properties of PT material with that obtained from SPT and BIT. The tensile specimens were prepared using wire cut Electrical Discharge Machining (EDM) as per general guideline of ASTM standard E-8. Tests were carried out at ambient and higher temperatures. The tensile properties obtained from tension test and two MSTTs show that the tensile properties vary with orientation and temperature. In order to evaluate mechanical properties of cladding tube two techniques namely SPT and Ring Tension Test (RTT) have been used. The RTT is another technique, already established for estimation of the mechanical properties of cladding tube material in the transverse direction. Experimental results were generated at ambient and higher temperatures by preparing specimens from the same cladding tube in the form of 3mm discs and rings. The basic fixture that was used for carrying out ring tension test of the cladding tube consists

  9. [Diagnosis and integrative evaluation on soil fertility of three Chinese medicinal materials in GAP plots].

    Science.gov (United States)

    Pan, Chaomei; Huang, Haibo; Zhan, Ruoting; Xu, Honghua; Liao, Guanrong

    2002-03-01

    The fertility of soil was diagnosed and integratively evaluated by modified Nemoro Index with eight indexes, i.e. pH, organic matter, total N, P, K and available N, P, K on three national Chinese medicinal materials GAP (Good Agricultural Practice) experimental plots of Pogostemon cablin, Citrus medica and Morinda officinalis in Guangdong. The results showed that the pH, organic matter and other major nutrient contents were low and imbalance. There are lots of nutritive disturbance factors. The level of soil integrative fertility in any of the plots was poor. PMID:12583155

  10. Evaluating the progress of the UK’s material recycling facilities:a mini review

    OpenAIRE

    Ali, Muhammad; Courtenay, Peter

    2014-01-01

    Over the last 15 years, the UK has made great strides in reducing the amount of waste being sent to landfill while also increasing the amount of waste being recycled. The key drivers for this change are the European Union Landfill Directive (1999/31/EC) and the UK Landfill Tax. However, also playing their part are the growing numbers of Material Recycling Facilities (MRFs), which process recyclables. This mini review evaluates the current state of MRFs in the UK, through extensive secondary r...

  11. Material compatibility evaluation for DWPF nitric-glycolic acid-literature review

    Energy Technology Data Exchange (ETDEWEB)

    Mickalonis, J. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL); Skidmore, E. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL)

    2013-06-01

    Glycolic acid is being evaluated as an alternative for formic and nitric acid in the DWPF flowsheet. Demonstration testing and modeling for this new flowsheet has shown that glycolic acid and glycolate has a potential to remain in certain streams generated during the production of the nuclear waste glass. A literature review was conducted to assess the impact of glycolic acid on the corrosion of the materials of construction for the DWPF facility as well as facilities downstream which may have residual glycolic acid and glycolates present. The literature data was limited to solutions containing principally glycolic acid.

  12. Material Evaluation and Process Optimization of CNT-Coated Polymer Powders for Selective Laser Sintering

    Directory of Open Access Journals (Sweden)

    Shangqin Yuan

    2016-10-01

    Full Text Available Multi-walled carbon nanotubes (CNTs as nano-reinforcements were introduced to facilitate the laser sintering process and enhance the thermal and mechanical properties of polymeric composites. A dual experimental-theoretical method was proposed to evaluate the processability and predict the process parameters of newly developed CNT-coated polyamide 12 (CNTs/PA12 powders. The thermal conductivity, melt viscosity, phase transition and temperature-dependent density and heat capacity of PA12 and CNTs/PA12 powders were characterized for material evaluation. The composite powders exhibited improved heat conduction and heat absorption compared with virgin polymer powders, and the stable sintering range of composite powders was extended and found to be favourable for the sintering process. The microstructures of sintered composites revealed that the CNTs remained at the powder boundaries and formed network architectures, which instantaneously induced the significant enhancements in tensile strength, elongation at break and toughness without sacrificing tensile modulus.

  13. EVALUATION OF SORPTIVE PROPERTIES OF VARIOUS CARRIERS AND COATING MATERIALS FOR LIQUISOLID SYSTEMS.

    Science.gov (United States)

    Vraníková, Barbora; Gajdziok, Jan

    2015-01-01

    The basic principle of liquisolid systems formulation lies in the conversion of the drug in a liquid state into an apparently dry, free-flowing and readily compressible powder by its blending (or spraying) with specific carriers and coating materials. The selection of the most suitable carrier and coating material depends especially on their values of flowable liquid retention potential (Φ), which is defined as the maximum mass of liquid that can be retained per unit mass of powder material, while maintaining an acceptable flowability. The presented work focused on the determination of the maximum amount of propylene glycol (PG), which can be retained by several selected carriers and coating materials while maintaining acceptable flow properties of the liquisolid powder blend. Granulated forms of magnesium aluminometasilicates (Neusilin® US2 and Neusilin® NS2N), dibasic calcium phosphate (Fujicalin®) and microcrystalline cellulose (Avicel® PH 101) were tested due to their frequent use. Powdered forms of magnesium aluminometasilicate (Neusilin® UFL2) and colloidal silica (Aerosil® 200) were used as common coating materials. From the evaluation of liquisolid mixtures with different amounts of liquid, it could be observed that 1 g of Neusilin® US2, Neusilin® UFL2, Neusilin® NS2N, Aerosil® 200, Fujicalin® and Avicel® PH 101 can retain 1.00, 0.97, 0.54, 0.04, 0.25 and 0.12 g of propylene glycol, respectively, while maintaining acceptable flowing properties for further processing. PMID:26642662

  14. Evaluation of two water-equivalent phantom materials for output calibration of photon and electron beams

    International Nuclear Information System (INIS)

    Two commercially available water-equivalent solid phantom materials were evaluated for output calibration in both photon (6-15 MV) and electron (6-20 MeV) beams. The solid water 457 and virtual water materials have the same chemical composition but differ in manufacturing process and density. A Farmer-type ionization chamber was used for measuring the output of the photon beams at 5- and 10-cm depth and electron beams at maximum buildup depth in the solid phantoms and in natural water. The water-equivalency correction factor for the solid materials is defined as the ratio of the chamber reading in natural water to that in the solid at the same linear depth. For photon beams, the correction factor was found to be independent of depth and was 0.987 and 0.993 for 6- and 15-MV beams, respectively, for solid water. For virtual water, the corresponding correction factors were 0.993 and 0.998 for 6- and 15-MV beams, respectively. For electron beams, the correction factors ranged from 1.013 to 1.007 for energies of 6 to 20 MeV for both solid materials. This indicated that the water-equivalency of these materials is within ± 1.3%, making them suitable substitutes for natural water in both photon and electron beam output measurements over a wide energy range. These correction factors are slightly larger than the manufacturers' advertised values (± 1.0% for solid water and ± 0.5% for virtual water). We suggest that these corrections are large enough in most cases and should be applied in the calculation of beam outputs

  15. New methodology to evaluate bond strength of root-end filling materials.

    Science.gov (United States)

    Marques, Jorge Henrique Stefaneli; Silva-Sousa, Yara Teresinha Corrêa; Rached-Júnior, Fuad Jacob Abi; Mazzi-Chaves, Jardel Francisco; Miranda, Carlos Eduardo Saraiva; da Silva, Silvio Rocha Correa; Steier, Liviu; Sousa-Neto, Manoel Damião

    2015-01-01

    This study evaluated the bond strength of root-end filling materials to root-end cavities using a new methodology. Twenty maxillary central incisors were subjected to biomechanical preparation (#80 hand file) and sectioned transversally 2 mm short of the apex and 4 mm coronally to this point. The root cylinders were embedded in acrylic resin and positioned at 45° to the horizontal plane for preparation of root-end cavities with a diamond ultrasonic retrotip. Two groups (n=10) were formed according to the root-end filling material: MTA and Super EBA. A gutta-percha cone (#80) was tug-backed at the limit between the canal and the root-end cavity. The cavity was filled and the gutta-percha cone was removed after complete setting of the sealer. The specimens were placed in an Instron machine with the root-end filling turned downwards. The push-out shaft was inserted in the space previously occupied by the gutta-percha cone and run at a crosshead speed of 1.0 mm/min for pushing out the root-end filling material. Data were analyzed by ANOVA (α=5%). Super EBA (6.03±1.31) presented higher bond strength (MPa) than MTA (1.81±0.45) (p>0.05). There was a predominance of cohesive failures for Super EBA and mixed for MTA. The protocol of specimen preparation is effective and introduces a specific methodology for assessing bond strength of root-end filling materials to dentin. Among the materials, Super EBA presented the highest bond strength. PMID:26200155

  16. Electrical characterization of conductive textile materials and its evaluation as electrodes for venous occlusion plethysmography.

    Science.gov (United States)

    Goy, C B; Dominguez, J M; Gómez López, M A; Madrid, R E; Herrera, M C

    2013-08-01

    The ambulatory monitoring of biosignals involves the use of sensors, electrodes, actuators, processing tools and wireless communication modules. When a garment includes these elements with the purpose of recording vital signs and responding to specific situations it is call a 'Smart Wearable System'. Over the last years several authors have suggested that conductive textile material (e-textiles) could perform as electrode for these systems. This work aims at implementing an electrical characterization of e-textiles and an evaluation of their ability to act as textile electrodes for lower extremity venous occlusion plethysmography (LEVOP). The e-textile electrical characterization is carried out using two experimental set-ups (in vitro evaluation). Besides, LEVOP records are obtained from healthy volunteers (in vivo evaluation). Standard Ag/AgCl electrodes are used for comparison in all tests. Results shown that the proposed e-textiles are suitable for LEVOP recording and a good agreement between evaluations (in vivo and in vitro) is found. PMID:23875930

  17. Fifty years of Brazilian Dental Materials Group: scientific contributions of dental materials field evaluated by systematic review

    Science.gov (United States)

    ROSA, Wellington Luiz de Oliveira; SILVA, Tiago Machado; LIMA, Giana da Silveira; SILVA, Adriana Fernandes; PIVA, Evandro

    2016-01-01

    ABSTRACT Objective A systematic review was conducted to analyze Brazilian scientific and technological production related to the dental materials field over the past 50 years. Material and Methods This study followed the Preferred Reporting Items for Systematic Reviews and Meta-Analysis (Prisma) statement. Searches were performed until December 2014 in six databases: MedLine (PubMed), Scopus, LILACS, IBECS, BBO, and the Cochrane Library. Additionally, the Brazilian patent database (INPI - Instituto Nacional de Propriedade Industrial) was screened in order to get an overview of Brazilian technological development in the dental materials field. Two reviewers independently analyzed the documents. Only studies and patents related to dental materials were included in this review. Data regarding the material category, dental specialty, number of documents and patents, filiation countries, and the number of citations were tabulated and analyzed in Microsoft Office Excel (Microsoft Corporation, Redmond, Washington, United States). Results A total of 115,806 studies and 53 patents were related to dental materials and were included in this review. Brazil had 8% affiliation in studies related to dental materials, and the majority of the papers published were related to dental implants (1,137 papers), synthetic resins (681 papers), dental cements (440 papers), dental alloys (392 papers) and dental adhesives (361 papers). The Brazilian technological development with patented dental materials was smaller than the scientific production. The most patented type of material was dental alloys (11 patents), followed by dental implants (8 patents) and composite resins (7 patents). Conclusions Dental materials science has had a substantial number of records, demonstrating an important presence in scientific and technological development of dentistry. In addition, it is important to approximate the relationship between academia and industry to expand the technological development in

  18. Report of the evaluation by the Ad Hoc Review Committee on Materials Science Research. In-advance evaluation in fiscal year 2002

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2002-11-01

    The Research Evaluation Committee, which consisted of 13 members from outside of the Japan Atomic Energy Research Institute (JAERI), set up an Ad Hoc Review Committee on Materials Science Research in accordance with the Fundamental Guideline for the Evaluation of Research and Development (R and D) at JAERI' and its subsidiary regulations in order to evaluate the adequacy of the R and D programs to be implemented for five years starting in Fiscal Year 2003 at Department of Materials Science in Tokai Research Establishment of JAERI. The Ad Hoc Review Committee consisted of eight specialists from outside of JAERI. The Ad Hoc Review Committee conducted its activities from April 2002 to August 2002. The evaluation was performed on the basis of the materials submitted in advance and of the oral presentations made at the Ad Hoc Review Committee meeting which was held on June 5th, 2002, in line with the items, viewpoints, and criteria for the evaluation specified by the Research Evaluation Committee. The result of the evaluation by the Ad Hoc Review Committee was submitted to the Research Evaluation Committee, and was judged to be appropriate at its meeting held on August 5th, 2002. This report describes the result of the evaluation by the Ad Hoc Review Committee on Materials Science Research. (author)

  19. Vacuum Ultraviolet Radiation and Atomic Oxygen Durability Evaluation of HST Bi-Stem Thermal Shield Materials

    Science.gov (United States)

    Dever, Joyce; deGroh, Kim K.

    2002-01-01

    Bellows-type thermal shields were used on the bi-stems of replacement solar arrays installed on the Hubble Space Telescope (HST) during the first HST servicing mission (SMI) in December 1993. These thermal shields helped reduce the problem of thermal gradient- induced jitter observed with the original HST solar arrays during orbital thermal cycling and have been in use on HST for eight years. This paper describes ground testing of the candidate solar array bi-stem thermal shield materials including backside aluminized Teflon(R)FEP (fluorinated ethylene propylene) with and without atomic oxygen (AO) and ultraviolet radiation protective surface coatings for durability to AO and combined AO and vacuum ultraviolet (VOV) radiation. NASA Glenn Research Center (GRC) conducted VUV and AO exposures of samples of candidate thermal shield materials at HST operational temperatures and pre- and post-exposure analyses as part of an overall program coordinated by NASA Goddard Space Flight Center (GSFC) to determine the on-orbit durability of these materials. Coating adhesion problems were observed for samples having the AO- and combined AO/UV-protective coatings. Coating lamination occurred with rapid thermal cycling testing which simulated orbital thermal cycling. This lack of adhesion caused production of coating flakes from the material that would have posed a serious risk to HST optics if the coated materials were used for the bi-stem thermal shields. No serious degradation was observed for the uncoated aluminized Teflon(R) as evaluated by optical microscopy, although atomic force microscopy (AFM) microhardness testing revealed that an embrittled surface layer formed on the uncoated Teflon(R) surface due to vacuum ultraviolet radiation exposure. This embrittled layer was not completely removed by AO erosion, No cracks or particle flakes were produced for the embrittled uncoated material upon exposure to VUV and AO at operational temperatures to an equivalent exposure of

  20. Evaluation of frost damage in cement-based materials by a nonlinear elastic wave technique

    Science.gov (United States)

    Eiras, J. N.; Kundu, T.; Popovics, J. S.; Monzó, J.; Soriano, L.; Payá, J.

    2014-03-01

    Frost resistance of concrete is a major concern in cold regions. RILEM (International union of laboratories and experts in construction materials, systems and structures) recommendations provide two alternatives for evaluating frost damage by nondestructive evaluation methods for concrete like materials. The first method is based on the ultrasonic pulse velocity measurement, while the second alternative technique is based on the resonant vibration test. In this study, we monitor the frost damage in Portland cement mortar samples with water to cement ratio of 0.5 and aggregate to cement ratio of 3. The samples are completely saturated by water and are frozen for 24 hours at -25°C. The frost damage is monitored after 0, 5, 10, 15 and 20 freezing-thawing cycles by nonlinear impact resonance acoustic spectroscopy (NIRAS). The results obtained are compared with those obtained by resonant vibration tests, the second alternative technique recommended by RILEM. The obtained results show that NIRAS is more sensitive to early stages of damage than the standard resonant vibration tests.

  1. Modified application of HS-SPME for quality evaluation of essential oil plant materials.

    Science.gov (United States)

    Dawidowicz, Andrzej L; Szewczyk, Joanna; Dybowski, Michal P

    2016-01-01

    The main limitation in the standard application of head space analysis employing solid phase microextraction (HS-SPME) for the evaluation of plants as sources of essential oils (EOs) are different quantitative relations of EO components from those obtained by direct analysis of EO which was got in the steam distillation (SD) process from the same plant (EO/SD). The results presented in the paper for thyme, mint, sage, basil, savory, and marjoram prove that the quantitative relations of EO components established by HS-SPME procedure and direct analysis of EO/SD are similar when the plant material in the HS-SPME process is replaced by its suspension in oil of the same physicochemical character as that of SPME fiber coating. The observed differences in the thyme EO composition estimated by both procedures are insignificant (F(exp)evaluation time of plant material quality and thus may improve the efficiency of analytical laboratories. PMID:26695252

  2. Fluorescence-Based Bioassays for the Detection and Evaluation of Food Materials

    Directory of Open Access Journals (Sweden)

    Kentaro Nishi

    2015-10-01

    Full Text Available We summarize here the recent progress in fluorescence-based bioassays for the detection and evaluation of food materials by focusing on fluorescent dyes used in bioassays and applications of these assays for food safety, quality and efficacy. Fluorescent dyes have been used in various bioassays, such as biosensing, cell assay, energy transfer-based assay, probing, protein/immunological assay and microarray/biochip assay. Among the arrays used in microarray/biochip assay, fluorescence-based microarrays/biochips, such as antibody/protein microarrays, bead/suspension arrays, capillary/sensor arrays, DNA microarrays/polymerase chain reaction (PCR-based arrays, glycan/lectin arrays, immunoassay/enzyme-linked immunosorbent assay (ELISA-based arrays, microfluidic chips and tissue arrays, have been developed and used for the assessment of allergy/poisoning/toxicity, contamination and efficacy/mechanism, and quality control/safety. DNA microarray assays have been used widely for food safety and quality as well as searches for active components. DNA microarray-based gene expression profiling may be useful for such purposes due to its advantages in the evaluation of pathway-based intracellular signaling in response to food materials.

  3. Evaluation of resilient modulus of subgrade and base materials in Indiana and its implementation in MEPDG.

    Science.gov (United States)

    Ji, Richard; Siddiki, Nayyarzia; Nantung, Tommy; Kim, Daehyeon

    2014-01-01

    In order to implement MEPDG hierarchical inputs for unbound and subgrade soil, a database containing subgrade M R , index properties, standard proctor, and laboratory M R for 140 undisturbed roadbed soil samples from six different districts in Indiana was created. The M R data were categorized in accordance with the AASHTO soil classifications and divided into several groups. Based on each group, this study develops statistical analysis and evaluation datasets to validate these models. Stress-based regression models were evaluated using a statistical tool (analysis of variance (ANOVA)) and Z-test, and pertinent material constants (k 1, k 2 and k 3) were determined for different soil types. The reasonably good correlations of material constants along with M R with routine soil properties were established. Furthermore, FWD tests were conducted on several Indiana highways in different seasons, and laboratory resilient modulus tests were performed on the subgrade soils that were collected from the falling weight deflectometer (FWD) test sites. A comparison was made of the resilient moduli obtained from the laboratory resilient modulus tests with those from the FWD tests. Correlations between the laboratory resilient modulus and the FWD modulus were developed and are discussed in this paper. PMID:24701162

  4. Evaluation of Resilient Modulus of Subgrade and Base Materials in Indiana and Its Implementation in MEPDG

    Directory of Open Access Journals (Sweden)

    Richard Ji

    2014-01-01

    Full Text Available In order to implement MEPDG hierarchical inputs for unbound and subgrade soil, a database containing subgrade MR, index properties, standard proctor, and laboratory MR for 140 undisturbed roadbed soil samples from six different districts in Indiana was created. The MR data were categorized in accordance with the AASHTO soil classifications and divided into several groups. Based on each group, this study develops statistical analysis and evaluation datasets to validate these models. Stress-based regression models were evaluated using a statistical tool (analysis of variance (ANOVA and Z-test, and pertinent material constants (k1, k2 and k3 were determined for different soil types. The reasonably good correlations of material constants along with MR with routine soil properties were established. Furthermore, FWD tests were conducted on several Indiana highways in different seasons, and laboratory resilient modulus tests were performed on the subgrade soils that were collected from the falling weight deflectometer (FWD test sites. A comparison was made of the resilient moduli obtained from the laboratory resilient modulus tests with those from the FWD tests. Correlations between the laboratory resilient modulus and the FWD modulus were developed and are discussed in this paper.

  5. A modified method for evaluation of materials containing volatile corrosion inhibitor

    Institute of Scientific and Technical Information of China (English)

    WAN Hong-jing; HUANG Hong-jun; ZHANG Min; LI Zhi-guang

    2005-01-01

    A systematic research on a modified method that was developed to evaluate the effectiveness of volatile corrosion inhibitor(VCI) materials was carried out. The metal specimen in size of 50 mm×25 mm×2 mm was level mounted on the top of a beaker by transparent adhesive tape and the assembly was placed in a constant temperature water bath and kept at approximately 40 ℃ to accelerate the vaporization of VCI and distilled water, which was placed at the bottom of the beaker at the same time. The experimental results show that the reproducibility of rust appearance and corrosion rate calculated by specimen's mass loss is perfect. The outstanding characteristic of the rust appearance based on different VCI formula is discovered that is very important in studying the mechanism of VCI and the synergism of chemical reagent. The accelerated ratio is increased greatly as compared with the traditional method and the value is approximately 15 as compared with Shijiazhuang atmospheric environment corrosion test. The modified method is suitable for formula screening test and quick effectiveness evaluation of VCI materials.

  6. Evaluation of the Benefits Attributable to Automotive Lightweight Materials Program Research and Development Projects; TOPICAL

    International Nuclear Information System (INIS)

    The purpose of this project is to identify and test methods appropriate for estimating the benefits attributable to research and development (R and D) projects funded by the Automotive Lightweight Materials (ALM) Program of the Office of Advanced Automotive Technologies (OAAT) of the U.S. Department of Energy (DOE). Funded projects range from basic materials science research to applied research in production environments. Collaborators on these projects include national laboratories, universities, and private sector firms, such as leading automobile manufacturers and their suppliers. Three ALM R and D projects were chosen for this pilot evaluation: Low-Cost, Continuous Cast Aluminum Sheet; Advanced Forming Technologies for Aluminum; and Manufacturing of Composite Automotive Structures. These projects were chosen because they represent a range of benefits evaluation situations. The first project resulted in an improved process that may be commercialized. The second project is on going and has two distinct components. The third project has yielded an improved technology that has been commercialized. This completed project also benefited from numerous complementary projects

  7. Spectrophotometric Evaluation of Polyetheretherketone (PEEK as a Core Material and a Comparison with Gold Standard Core Materials

    Directory of Open Access Journals (Sweden)

    Bogna Stawarczyk

    2016-06-01

    Full Text Available This study investigated the colorimetric properties of different veneering materials on core materials. Standardized specimens (10 mm × 10 mm × 1.5 mm reflecting four core (polyetheretherketone (PEEK, zirconia (ZrO2, cobalt–chromium–molybdenum alloy (CoCrMo, and titanium oxide (TiO2; thickness: 1.5 mm and veneering materials (VITA Mark II, IPS e.max CAD, LAVA Ultimate and VITA Enamic, all in shade A3; thickness: 0.5, 1.0, 1.5 and 2 mm, respectively were fabricated. Specimens were superimposed to assemblies, and the color was determined with a spectrophotometer (CieLab-System or a chair-side color measurement device (VITA EasyShade, respectively. Data were analyzed using three-, two-, and one-way ANOVA, a Chi2-test, and a Wilson approach (p < 0.05. The measurements with EasyShade showed A2 for VITA Mark II, A3.5 for VITA Enamic, B2 for LAVA Ultimate, and B3 for IPS e.max CAD. LabE-values showed significant differences between the tested veneering materials (p < 0.001. CieLab-System and VITA EasyShade parameters of the different assemblies showed a significant impact of core (p < 0.001, veneering material (p < 0.001, and thickness of the veneering material (p < 0.001. PEEK as core material showed comparable outcomes as compared to ZrO2 and CoCrMo, with respect to CieLab-System parameters for each veneering material. The relative frequency of the measured VITA EasyShade parameters regarding PEEK cores also showed comparable results as compared to the gold standard CoCrMo, regardless of the veneering material used.

  8. An evaluation on the adherence of Candida albicans to different denture- base materials

    Directory of Open Access Journals (Sweden)

    Savabi O

    2004-02-01

    Full Text Available The surface topography of denture base material is an important factor for the"nadhesion of Candida albicans and other microorganisms."nPurpose: The aim of this study was to evaluate the adherence of Candida albicans to four types of denture"nbase materials (Acropars acrylic resin, Meliodent acrylic resin, rough and smooth surfaces of Molloplast B."nMaterials and Methods: Seven blocks of two types of acrylic resins and ten blocks of silicone with one"nrough and one smooth surface were made and incubated in a suspension of Candida albicans. After washing,"nthe blocks were stained with acridine orange and examined under fluorescent microscope. For statistical"nanalysis ANOVA and Duncan tests were used."nResults: It was observed that Candida adhesion to rough surfaces of acrylic resins and silicone was"nsignificantly more than polished surfaces of acrylic resins and smooth silicone (PO.0001. However, no"nstatistical significant difference was found between polished acrylic resins surfaces and smooth silicone."nConclusion: Significant differences in the adherence of Candida to the surfaces of different denture base"nmaterials are due to differences in surface topography, chemical, physical and hydrophobic properties so it is"nrecommended to minimize the roughness and irregularities of denture base.

  9. Evaluating the progress of the UK's Material Recycling Facilities: a mini review.

    Science.gov (United States)

    Ali, Muhammad; Courtenay, Peter

    2014-12-01

    Over the last 15 years, the UK has made great strides in reducing the amount of waste being sent to landfill while also increasing the amount of waste being recycled. The key drivers for this change are the European Union Landfill Directive (1999/31/EC) and the UK Landfill Tax. However, also playing their part are the growing numbers of Material Recycling Facilities (MRFs), which process recyclables. This mini review evaluates the current state of MRFs in the UK, through extensive secondary research, and detailed primary data analysis focussing on MRFs located in South-East England, UK. This study also explores technologies that aim to generate energy from waste, including Waste-to-Energy (WtE) and Refuse-derived Fuel (RDF) facilities. These facilities can have a huge appetite for waste, which can be detrimental to recycling efforts as some of the waste being sent there should be recycled. It was found that the waste sent to a typical UK MRF would recycle around 92% of materials while 6% was sent to energy recovery and the remaining 2% ended up in landfill. Therefore, the total estimated rejected or non-compliance materials from MRFs are around 8%. A key recommendation from this study is to adopt a strategy to combine MRFs with a form of energy generation, such as WtE or RDF. This integrated approach would ensure any residual waste arising from the recycling process can be used as a sustainable fuel, while also increasing the recycling rates.

  10. Evaluating the progress of the UK's Material Recycling Facilities: a mini review.

    Science.gov (United States)

    Ali, Muhammad; Courtenay, Peter

    2014-12-01

    Over the last 15 years, the UK has made great strides in reducing the amount of waste being sent to landfill while also increasing the amount of waste being recycled. The key drivers for this change are the European Union Landfill Directive (1999/31/EC) and the UK Landfill Tax. However, also playing their part are the growing numbers of Material Recycling Facilities (MRFs), which process recyclables. This mini review evaluates the current state of MRFs in the UK, through extensive secondary research, and detailed primary data analysis focussing on MRFs located in South-East England, UK. This study also explores technologies that aim to generate energy from waste, including Waste-to-Energy (WtE) and Refuse-derived Fuel (RDF) facilities. These facilities can have a huge appetite for waste, which can be detrimental to recycling efforts as some of the waste being sent there should be recycled. It was found that the waste sent to a typical UK MRF would recycle around 92% of materials while 6% was sent to energy recovery and the remaining 2% ended up in landfill. Therefore, the total estimated rejected or non-compliance materials from MRFs are around 8%. A key recommendation from this study is to adopt a strategy to combine MRFs with a form of energy generation, such as WtE or RDF. This integrated approach would ensure any residual waste arising from the recycling process can be used as a sustainable fuel, while also increasing the recycling rates. PMID:25391552

  11. Preparation and Evaluation of New Nanoporous Silica Materials for Molecular Filtration and for Core Materials in Vacuum Insulation Panels

    OpenAIRE

    Twumasi Afriyie, Ebenezer

    2013-01-01

    Nanoporous materials for gas purification and thermal insulation have been studied and developed for application in many areas. It is known that a single adsorbent may not adequately control multiple contaminants. Further the utilization of nanoporous material as thermal insulator in building applications is limited due to high cost. Moreover, in view of the global environmental movement for clean air and reduction of heating energy consumption in built environment, the development of new and...

  12. Grain size evaluation of structural materials in nuclear power plant using a thickness independent ultrasonic method

    Energy Technology Data Exchange (ETDEWEB)

    Li, Xiongbing, E-mail: lixb_ex@163.com [CAD/CAM Institute, Central South University, Changsha 410075 (China); State Key Laboratory of Powder Metallurgy, Central South University, Changsha 410083 (China); Song, Yongfeng [CAD/CAM Institute, Central South University, Changsha 410075 (China); Ni, Peijun [The Ningbo Branch of Ordnance Science Institute of China, Ningbo 315103 (China); Wang, Zi; Liu, Feng [State Key Laboratory of Powder Metallurgy, Central South University, Changsha 410083 (China); Du, Hualong [Mechanical and Aerospace Engineering Department, North Carolina State University, Raleigh, NC 27606 (United States)

    2015-05-15

    Highlights: •We derive a coefficient of ultrasonic attenuation rate related to the grain size. •The mean grain size of the pipe can be evaluated without measuring its thickness. •Experiments show this method is better suited to square pipe than other methods. -- Abstract: It is important to accurately and nondestructively evaluate the grain size of structural materials used in nuclear power plants. The current ultrasonic non-destructive methods are so dependent on the thickness measurement of a square pipe that it reduces their practicality and reliability. In this paper, a novel method using the coefficient of ultrasonic attenuation rate is developed by using the transmission and reflection coefficients. As a result, the mean grain size of the pipe can be nondestructively evaluated without measuring its thickness. Moreover, the signal preprocessing is studied to improve the stability and accuracy of evaluation results. The experimental results show that the dependence of the attenuation rate on grain sizes is much higher than that of the ultrasonic velocity. The relative error of the attenuation rate method is lower than that of the backscatter method if the thickness of the sample is less than 5 mm. When evaluating a TP304 stainless steel square pipe whose thickness is not convenient to measure, the mean grain sizes are measured 103.5 ± 2.6 μm, 96.9 ± 3.5 μm and 94.0 ± 1.7 μm by the attenuation method, the attenuation rate method and the electron backscattering diffraction method, respectively. The result verifies that the presented method works better than the attenuation method due to the fact that the error of the thickness measurement has no effect on the ultrasonic attenuation rate.

  13. Grain size evaluation of structural materials in nuclear power plant using a thickness independent ultrasonic method

    International Nuclear Information System (INIS)

    Highlights: •We derive a coefficient of ultrasonic attenuation rate related to the grain size. •The mean grain size of the pipe can be evaluated without measuring its thickness. •Experiments show this method is better suited to square pipe than other methods. -- Abstract: It is important to accurately and nondestructively evaluate the grain size of structural materials used in nuclear power plants. The current ultrasonic non-destructive methods are so dependent on the thickness measurement of a square pipe that it reduces their practicality and reliability. In this paper, a novel method using the coefficient of ultrasonic attenuation rate is developed by using the transmission and reflection coefficients. As a result, the mean grain size of the pipe can be nondestructively evaluated without measuring its thickness. Moreover, the signal preprocessing is studied to improve the stability and accuracy of evaluation results. The experimental results show that the dependence of the attenuation rate on grain sizes is much higher than that of the ultrasonic velocity. The relative error of the attenuation rate method is lower than that of the backscatter method if the thickness of the sample is less than 5 mm. When evaluating a TP304 stainless steel square pipe whose thickness is not convenient to measure, the mean grain sizes are measured 103.5 ± 2.6 μm, 96.9 ± 3.5 μm and 94.0 ± 1.7 μm by the attenuation method, the attenuation rate method and the electron backscattering diffraction method, respectively. The result verifies that the presented method works better than the attenuation method due to the fact that the error of the thickness measurement has no effect on the ultrasonic attenuation rate

  14. Evaluation of simulation techniques for radiation damage in the bulk of fusion first wall materials

    International Nuclear Information System (INIS)

    An international workshop on 'Evaluation of Simulation Techniques for Radiation Damage in the Bulk of Fusion First Wall Materials' was held at Interlaken, Switzerland, June 27-30 1983. The idea was to gather a small group of people (∼20) actively engaged in experimental simulation of bulk radiation damage in the first wall material (e.g. damage by fusion neutrons). Because of the very positive response the number of participants ended up at 36 (from Belgium, Denmark, Federal Republic of Germany, France, Italy (ISPRA), Japan, Switzerland, U.K. and U.S.A.). The workshop was initially rather restrictive in the definition of experimental facilities for simulation of the first wall material, as it included only those facilities which simultaneously introduce helium (at high rate) and displacement damage . At the workshop a few simulation techniques that do not fulfill this requirement were discussed together with those that do. The basic programme of the workshop was composed of a series of invited presentations intended to cover the whole spectrum of simulation techniques and some of the underlying physics and basic technology. Time was also reserved for short presentations on any subject that the participants found relevant. Throughout the workshop ample time was allocated for discussions. As it turned out, the discussions tended to focus on the evaluation of the general situation for simulation of radiation damage in the first wall. The workshop covered the following topics: the concept of simulation; the important parameters (He generation to damage rate ratio; displacement damage rate; He generation rate; total doses; H generation; solid transmutation products; cascade effects; effect of beam pulsation; specimen dimension); and the irradiation effects (mechanical properties and swelling; microstructure). There was general agreement among the participants that ideal simulation, providing unambiguous information about the behaviour of the first wall material, is at

  15. Evaluation of dredged material proposed for ocean disposal from Eastchester Project Area, New York

    Energy Technology Data Exchange (ETDEWEB)

    Antrim, L.D.; Pinza, M.R.; Barrows, E.S.; Gardiner, W.W.; Tokos, J.J.S.; Gruendell, B.D.; Word, J.Q. [Battelle Marine Research Lab., Sequim, WA (United States)

    1996-07-01

    The objective of the Eastchester project (Federal Project [FP] No. 6) was to evaluate proposed dredged material from the Eastchester project area in the Hutchinson River to determine its suitability for unconfined ocean disposal at the Mud Dump Site. Eastchester was one of seven waterways that the U. S. Army Corps of Engineers-New York District (USACE-NYD) requested the Battelle/Marine Sciences Laboratory (MSL) to sample and evaluate for dredging and disposal in March 1994. The evaluation of proposed dredged material from the Eastchester project area consisted of bulk sediment chemical analyses, chemical analyses of dredging site water and elutriate, water- column and benthic acute toxicity tests, and bioaccumulation studies. Eighteen individual sediment core samples collected from the Eastchester project area were analyzed for grain size, moisture content, and total organic carbon (TOC). Two composite sediment samples, representing the upstream and lower reaches of the area proposed for dredging, were analyzed for bulk density, specific gravity, metals, chlorinated pesticides, polychlorinated biphenyl (PCB) congeners, polynuclear aromatic hydrocarbons (PAHs), and 1,4- dichlorobenzene. Dredging site water and elutriate water, which is prepared from the suspended-particulate phase (SPP) of the two Eastchester sediment composites, were analyzed for metals, pesticides, and PCBS. An additional 1 1 composite samples were created for the USACE-New England Division (USACE-NED) using the same 18 Eastchester core samples but combined into different composites. These composites were analyzed for metals, chlorinated pesticides, PCB congeners, PAHS, and 1,4-dichlorobenzene. Water-column or SPP toxicity tests were performed along with bioaccumulation tests.

  16. ASR mitigation by the use of supplementary cementing materials : evaluation of the available alkali content

    Energy Technology Data Exchange (ETDEWEB)

    Duchesne, J. [Laval Univ., Quebec City, PQ (Canada). Dept. of Geology and Geological Engineering

    2006-07-01

    Cement companies in Canada are involved in the global initiative to voluntarily implement strategies to address global warming, enhance occupational health and safety, reduce emissions, and use fuels and raw materials in a sustainable manner. This paper reported on a study in which the behaviour of common supplementary cementing materials (SCMs) were compared with an industrial by-product from the aluminium industry (ABP). The alkali content in SCMs is particularly critical in terms of its ability to prevent excessive expansion due to alkali-silica reactivity (ASR). The 6 common SCMs with various total alkali contents were: 2 condensed silica fumes, 3 pulverized fly ashes and 1 ground granulated blast furnace slag. The ABP was also investigated as a suitable candidate to replace Portland cement. The testing program involved measuring the expansion and alkali content. The methods used to evaluate the amount of available alkalies were ASTM C114; ASTM C311; modified ASTM C311; pore fluid expression; and, the accelerated mortar bar method. The main objectives of this study were to determine the best procedure for evaluating the amount of available alkalies from SCMs and to discuss the relationship between concrete expansion and alkali content. The recommended methods to evaluate the performance of non usual SCM as suitable candidates to replace Portland cement in the presence of potentially reactive aggregates were accelerated mortar bar method CSA A23.2-25A as well as the available alkalies from cement-SCM paste samples measured by the pore solution expression method. 10 refs., 2 tabs., 2 figs.

  17. Biological evaluation of zirconia/PEG hybrid materials synthesized via sol–gel technique

    Energy Technology Data Exchange (ETDEWEB)

    Catauro, M., E-mail: michelina.catauro@unina2.it [Department of Industrial and Information Engineering, Second University of Naples, Via Roma 29, 81031 Aversa (Italy); Papale, F.; Bollino, F. [Department of Industrial and Information Engineering, Second University of Naples, Via Roma 29, 81031 Aversa (Italy); Gallicchio, M.; Pacifico, S. [Department Environmental, Biological and Pharmaceutical Sciences and Technologies, Second University of Naples, Via Vivaldi 43, 81100 Caserta (Italy)

    2014-07-01

    The objective of the following study has been the synthesis via sol–gel and the characterization of novel organic–inorganic hybrid materials to be used in biomedical field. The prepared materials consist of an inorganic zirconia matrix containing as organic component the polyethylene glycol (PEG), a water-soluble polymer used in medical and pharmaceutical fields. Various hybrids have been synthesized changing the molar ratio between the organic and inorganic parts. Fourier transform spectroscopy suggests that the structure of the interpenetrating network is realized by hydrogen bonds between the Zr-OH group in the sol–gel intermediate species and both the terminal alcoholic group and ethereal oxygen atoms in the repeating units of polymer The amorphous nature of the gels has been ascertained by X-ray diffraction analysis. The morphology observation has been carried out by using the Scanning Electron Microscope and has confirmed that the obtained materials are nanostructurated hybrids. The bioactivity of the synthesized system has been shown by the formation of a hydroxyapatite layer on the surface of samples soaked in a fluid simulating the human blood plasma. The potential biocompatibility of hybrids has been assessed as performing indirect MTT cytotoxicity assay towards 3T3 cell line at 24, 48, and 72 h exposure times. - Highlights: • ZrO{sub 2}/PEG amorphous class I organic–inorganic hybrid synthesis via sol–gel • Bioactivity evaluation of materials by the formation of apatite on surface in SBF • Biocompatibility test with indirect MTT cytotoxicity assay on NHI 3T3 cell line.

  18. Evaluation of dredged material proposed for ocean disposal from South Brother Island Channel, New York

    Energy Technology Data Exchange (ETDEWEB)

    Barrows, E.S.; Gardiner, W.W.; Antrim, L.D.; Gruendell, B.D.; Word, J.Q.; Tokos, J.J.S. [Battelle Marine Sciences Laboratory, Sequim, Washington (United States)

    1996-09-01

    South Brother Island Channel was one of seven waterways that the US Army Crops of Engineers-New York District requested the Battelle/Marine Sciences Laboratory to sample and evaluate for dredging and disposal. Tests and analyses were conducted on South Brother Island Channel sediment core samples and evaluations were performed. The evaluation of proposed dredged material from South Brother Island Channel included bulk sediment chemical analyses, chemical analyses of site water and elutriate, water-column and benthic acute toxicity tests, and bioaccumulation studies. Individual sediment core samples collected from Souther Brother Island Channel were analyzed for grain size, moisture content, and total organic carbon. a composite sediment sample, representing the entire area proposed for dredging, was analyzed for bulk density, specific gravity, metals, chlorinated pesticides, polychlorinated biphenyl congers, polynuclear aromatic hydrocarbons, and 1,4- dichlorobenzene. Site water and elutriate water, prepared from the suspended-particle phase of South Brother Island Channel sediment, were analyzed for metals, pesticides, and PCBs.

  19. Study on Ultrasonic Transducer for Non-Destructive Evaluation of Highly Attenuative Material Using PMN-PT Single Crystal

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Ki Bok; Ahn, Bong Young; Kim, Young Gil [Korea Research Institute of Standards and Science, Daejeon (Korea, Republic of); Park, Sang Ki; Ha, Jeong Soo [KEPRI, Daejeon (Korea, Republic of)

    2007-08-15

    Recently, a new class of single-crystal piezoelectric materials such as lead metaniobate doped with lead titanate (PMN-PT) has been synthesized and were found to further enhance the electro-mechanical coupling factor compared to piezo-ceramic materials. This paper describes fabrication and evaluation of PMN-PT single crystal ultrasonic transducers for contact measurement of stainless steel that is one of the highly attenuative materials. The design conditions for ultrasonic transducer such as front matching layer between test materials and piezo-material and backing materials were investigated based on the simulation results by KLM model. The PMN-PT single crystal ultrasonic transducers with centre frequencies at 1 and 2.25 MHz were fabricated and their performances were evaluated

  20. Photometric Evaluation of Photo-luminescent Materials for Multi-Egress Guidance Placards: Lighting Environment Test Facility

    Science.gov (United States)

    Maida, James C.

    2005-01-01

    The purpose of this investigation was to evaluate several photo luminescent (PL) materials being considered for construction of emergency egress placards in the International Space Station (ISS). The use of PL material is intended to allow the placards to be read by ISS crew members in the event of an extensive power failure resulting in the loss of interior illumination.

  1. Restoration of endodontically treated anterior teeth: an evaluation of coronal microleakage of glass ionomer and composite resin materials.

    Science.gov (United States)

    Diaz-Arnold, A M; Wilcox, L R

    1990-12-01

    A glass ionomer material was evaluated for coronal microleakage in permanent lingual access restorations of endodontically treated anterior teeth. The material was tested as a restoration, placed over a zinc oxide-eugenol base, and as a base with an acid-etched composite resin veneer and a dentinal bonding agent. Restored teeth were thermocycled, immersed in silver nitrate, developed, and sectioned to assess microleakage. Significant coronal leakage was observed with all materials used.

  2. Evaluation of Different Disinfactants on Dimensional Accuracy and Surface Quality of Type IV Gypsum Casts Retrieved from Elastomeric Impression Materials

    OpenAIRE

    Pal, P K; Kamble, Suresh S.; Chaurasia, Ranjitkumar Rampratap; Chaurasia, Vishwajit Rampratap; Tiwari, Samarth; Bansal, Deepak

    2014-01-01

    Background: The present study was done to evaluate the dimensional stability and surface quality of Type IV gypsum casts retrieved from disinfected elastomeric impression materials. Materials and Methods: In an in vitro study contaminated impression material with known bacterial species was disinfected with disinfectants followed by culturing the swab sample to assess reduction in level of bacterial colony. Changes in surface detail reproduction of impression were a...

  3. Qualitative evaluation of the accuracy of maps for release of hazardous materials.

    Energy Technology Data Exchange (ETDEWEB)

    Darby, John L.; Marianno, Craig [National Security Technologies, Las Vegas, NV

    2008-08-01

    The LinguisticBelief%C2%A9 software tool developed by Sandia National Laboratories was applied to provide a qualitative evaluation of the accuracy of various maps that provide information on releases of hazardous material, especially radionuclides. The methodology, %E2%80%9CUncertainty for Qualitative Assessments,%E2%80%9D includes uncertainty in the evaluation. The software tool uses the mathematics of fuzzy sets, approximate reasoning, and the belief/ plausibility measure of uncertainty. SNL worked cooperatively with the Remote Sensing Laboratory (RSL) and the National Atmospheric Release Advisory Center (NARAC) at Lawrence Livermore National Laboratory (LLNL) to develop models for three types of maps for use in this study. SNL and RSL developed the maps for %E2%80%9CAccuracy Plot for Area%E2%80%9D and %E2%80%9CAerial Monitoring System (AMS) Product Confidence%E2%80%9D. SNL and LLNL developed the %E2%80%9CLLNL Model%E2%80%9D. For each of the three maps, experts from RSL and LLNL created a model in the LinguisticBelief software. This report documents the three models and provides evaluations of maps associated with the models, using example data. Future applications will involve applying the models to actual graphs to provide a qualitative evaluation of the accuracy of the maps, including uncertainty, for use by decision makers. A %E2%80%9CQuality Thermometer%E2%80%9D technique was developed to rank-order the quality of a set of maps of a given type. A technique for pooling expert option from different experts was provided using the PoolEvidence%C2%A9 software.

  4. Evaluation of piezoelectric material properties for a higher power output from energy harvesters with insight into material selection using a coupled piezoelectric-circuit-finite element method.

    Science.gov (United States)

    Daniels, Alice; Zhu, Meiling; Tiwari, Ashutosh

    2013-12-01

    Piezoelectric material properties have substantial influence on electrical power output from piezoelectric energy harvesters (PEHs). Understanding their influences is the first step in designing effective PEHs to generate higher power outputs. This paper uses a coupled piezoelectric-circuit-finite element method to study the power outputs of different types of piezoelectric materials, including single crystal, polyvinylidene fluoride (PVDF), and soft and hard lead zirconate titanate (PZT) materials. The purpose of this study is to try to gain an understanding of which piezoelectric material property--the elastic compliance s11, the piezoelectric strain constant d31, the piezoelectric stress constant g31, and the relative dielectric constant ϵ(T)r33, and the associated material properties of the d31 × g31, called the figure of merit (FOM), and the coupling coefficient k31--dominates the power output. A rectangular piezoelectric plate under a low-frequency excitation is used to evaluate piezoelectric material properties for a higher power output. It was found that 1) d31 is a more dominant material property over other material properties for higher power output; 2) FOM was more linearly related to the power output than either the k31 or the d31; and 3) ϵ(T)r33 had some role; when the materials have an identical d31; a lower ϵ(T)r33 was preferred. Because of unexplained outliers, no single material parameter was able to be recommended as selection criteria, but combined FOM with d31 parameters is recommended for selection of piezoelectric material for a higher power output from PEHs.

  5. Evaluation of the high-voltage high-frequency transformer insulating materials for satellites

    International Nuclear Information System (INIS)

    Environment resistance evaluation was made of the insulating materials of impregnated injection type for high-voltage high-frequency transformers mounted in satellites. (1) The stress occurring in the impregnated injection type resin is small in silicon resin and urethane resin and large in epoxy resin. (2) The dielectric characteristic at high frequency is good in silicone resin. In epoxy resin, when the transformer is operated at high temperature, its thermal runaway may take place. (3) The radiation deterioration at 1 Mrad - 10 Mrad is slight in urethane resin. (4) The degassing is not good in silicone resin. (5) The adhesive power is good in urethane resin. (6) From the above results, in silicone resin there is problem in degassing and adhesive power. In epoxy resin there is problem in stress and dielectric characteristic. (Mori, K.)

  6. Comparative evaluation of photon cross section libraries for materials of interest in PET Monte Carlo simulations

    CERN Document Server

    Zaidi, H

    1999-01-01

    the many applications of Monte Carlo modelling in nuclear medicine imaging make it desirable to increase the accuracy and computational speed of Monte Carlo codes. The accuracy of Monte Carlo simulations strongly depends on the accuracy in the probability functions and thus on the cross section libraries used for photon transport calculations. A comparison between different photon cross section libraries and parametrizations implemented in Monte Carlo simulation packages developed for positron emission tomography and the most recent Evaluated Photon Data Library (EPDL97) developed by the Lawrence Livermore National Laboratory was performed for several human tissues and common detector materials for energies from 1 keV to 1 MeV. Different photon cross section libraries and parametrizations show quite large variations as compared to the EPDL97 coefficients. This latter library is more accurate and was carefully designed in the form of look-up tables providing efficient data storage, access, and management. Toge...

  7. Fracture Toughness Evaluation of Space Shuttle External Tank Thermal Protection System Polyurethane Foam Insulation Materials

    Science.gov (United States)

    McGill, Preston; Wells, Doug; Morgan, Kristin

    2006-01-01

    Experimental evaluation of the basic fracture properties of Thermal Protection System (TPS) polyurethane foam insulation materials was conducted to validate the methodology used in estimating critical defect sizes in TPS applications on the Space Shuttle External Fuel Tank. The polyurethane foam found on the External Tank (ET) is manufactured by mixing liquid constituents and allowing them to react and expand upwards - a process which creates component cells that are generally elongated in the foam rise direction and gives rise to mechanical anisotropy. Similarly, the application of successive foam layers to the ET produces cohesive foam interfaces (knitlines) which may lead to local variations in mechanical properties. This study reports the fracture toughness of BX-265, NCFI 24-124, and PDL-1034 closed-cell polyurethane foam as a function of ambient and cryogenic temperatures and knitline/cellular orientation at ambient pressure.

  8. Forecasting volcanic eruptions and other material failure phenomena: An evaluation of the failure forecast method

    Science.gov (United States)

    Bell, Andrew F.; Naylor, Mark; Heap, Michael J.; Main, Ian G.

    2011-08-01

    Power-law accelerations in the mean rate of strain, earthquakes and other precursors have been widely reported prior to material failure phenomena, including volcanic eruptions, landslides and laboratory deformation experiments, as predicted by several theoretical models. The Failure Forecast Method (FFM), which linearizes the power-law trend, has been routinely used to forecast the failure time in retrospective analyses; however, its performance has never been formally evaluated. Here we use synthetic and real data, recorded in laboratory brittle creep experiments and at volcanoes, to show that the assumptions of the FFM are inconsistent with the error structure of the data, leading to biased and imprecise forecasts. We show that a Generalized Linear Model method provides higher-quality forecasts that converge more accurately to the eventual failure time, accounting for the appropriate error distributions. This approach should be employed in place of the FFM to provide reliable quantitative forecasts and estimate their associated uncertainties.

  9. Evaluation of residual stresses in composite materials by using neutron diffraction; study of elasto-plasticity

    International Nuclear Information System (INIS)

    This work deals with the study of Metal Matrix Composites (MMC) using neutrons diffraction method and the analysis of the elastoplastic behavior in such materials. First, we evaluated macro-stresses in aluminium MMC reinforced with 17%vol. of SiC particles. One of the analyzed sample has been 4 point bending deformed, measurements have been performed after relaxation. The difference between the coefficients of thermal expansion constrains the matrix to be in tensile state and the particles in compressive state in the sample which has not be deformed. In the sample deformed, the MMC response is predicted by the science of Resistance Materials applied to a bent bar. We assume that macro-stresses are the sum of stresses with different origins (elastic, plastic, thermal mismatch): elastic mismatch is evaluated by Eshelby model and we determined micro-stresses in the unbent bar: they are equivalent and constant along width direction. For the bent bar, we observe relaxation of thermal stresses in the surface region. Theses results are confirmed by measurements of tensile/compressive sample using neutrons diffraction method. We also observed the influence of mechanical and thermal treatment on such MMC: the shear stress (established by the auto-coherent model) depends only on the way of cooling. Finally, a study was performed on titanium MMC for SNECMA on rotor beings used in the gas turbine engine industry. Evolution of stresses between felloe and boring is confirmed by a finite elements modeling and they are the first experimental results in this application. (author)

  10. Evaluation of Zirconium Silico phosphate Material for the Removal of Copper Ions from Waste Water

    International Nuclear Information System (INIS)

    Zirconium silico phosphate/polyacrylamide (ZrSP/PAA) nano composite was synthesized. Synthesis process was based on the intercalation polymerization technique. The obtained nano product was characterized using XRF, XRD, FTIR, TG-DTA, SEM and TEM techniques. The physicochemical properties indicated that the synthesized material was semicrystalline in nature with a particle size in the nan orange (45 nm). FTIR analysis suggested that the intercalation polymerization was achieved via hydrogen bonding. The kinetics of copper retention at different temperatures were analyzed using pseudo first-order, pseudo second-order and Helfferich kinetic models. Kinetic modeling of the experimentally obtained data indicated that the intra-particle diffusion was the controlled mechanism of the sorption process. Various parameters such as effective diffusion coefficient and activation energy were evaluated. The mean free energy was in the range corresponding to the ion exchange type of sorption. Results indicated that synthetic ZrSP/PAA nano composite can be used as an efficient ion exchange material for the removal of cupper ions from waste water

  11. Evaluation of exposure pathways to man from disposal of radioactive materials into sanitary sewer systems

    Energy Technology Data Exchange (ETDEWEB)

    Kennedy, W.E. Jr.; Parkhurst, M.A.; Aaberg, R.L.; Rhoads, K.C.; Hill, R.L.; Martin, J.B. [Pacific Northwest Lab., Richland, WA (United States)

    1992-05-01

    In accordance with 10 CFR 20, the US Nuclear Regulatory Commission (NRC) regulates licensees` discharges of small quantities of radioactive materials into sanitary sewer systems. This generic study was initiated to examine the potential radiological hazard to the public resulting from exposure to radionuclides in sewage sludge during its treatment and disposal. Eleven scenarios were developed to characterize potential exposures to radioactive materials during sewer system operations and sewage sludge treatment and disposal activities and during the extended time frame following sewage sludge disposal. Two sets of deterministic dose calculations were performed; one to evaluate potential doses based on the radionuclides and quantities associated with documented case histories of sewer system contamination and a second, somewhat more conservative set, based on theoretical discharges at the maximum allowable levels for a more comprehensive list of 63 radionuclides. The results of the stochastic uncertainty and sensitivity analysis were also used to develop a collective dose estimate. The collective doses for the various radionuclides and scenarios range from 0.4 person-rem for {sup 137}Cs in Scenario No. 5 (sludge incinerator effluent) to 420 person-rem for {sup 137}Cs in Scenario No. 3 (sewage treatment plant liquid effluent). None of the 22 scenario/radionuclide combinations considered have collective doses greater than 1000 person-rem/yr. However, the total collective dose from these 22 combinations was found to be about 2100 person-rem.

  12. Self-assembled peptide nanotubes as electronic materials: An evaluation from first-principles calculations

    Energy Technology Data Exchange (ETDEWEB)

    Akdim, Brahim, E-mail: brahim.akdim.ctr@us.af.mil, E-mail: ruth.pachter@us.af.mil [Air Force Research Laboratory, Materials and Manufacturing Directorate, Wright-Patterson Air Force Base, Ohio 45433 (United States); General Dynamics Information Technology, Inc., 500 Springfield Pike, Dayton, Ohio 454331 (United States); Pachter, Ruth, E-mail: brahim.akdim.ctr@us.af.mil, E-mail: ruth.pachter@us.af.mil; Naik, Rajesh R. [Air Force Research Laboratory, Materials and Manufacturing Directorate, Wright-Patterson Air Force Base, Ohio 45433 (United States)

    2015-05-04

    In this letter, we report on the evaluation of diphenylalanine (FF), dityrosine (YY), and phenylalanine-tryptophan (FW) self-assembled peptide nanotube structures for electronics and photonics applications. Realistic bulk peptide nanotube material models were used in density functional theory calculations to mimic the well-ordered tubular nanostructures. Importantly, validated functionals were applied, specifically by using a London dispersion correction to model intertube interactions and a range-separated hybrid functional for accurate bandgap calculations. Bandgaps were found consistent with available experimental data for FF, and also corroborate the higher conductance reported for FW in comparison to FF peptide nanotubes. Interestingly, the predicted bandgap for the YY tubular nanostructure was found to be slightly higher than that of FW, suggesting higher conductance as well. In addition, the band structure calculations along the high symmetry line of nanotube axis revealed a direct bandgap for FF. The results enhance our understanding of the electronic properties of these material systems and will pave the way into their application in devices.

  13. Evaluation of exposure pathways to man from disposal of radioactive materials into sanitary sewer systems

    International Nuclear Information System (INIS)

    In accordance with 10 CFR 20, the US Nuclear Regulatory Commission (NRC) regulates licensees' discharges of small quantities of radioactive materials into sanitary sewer systems. This generic study was initiated to examine the potential radiological hazard to the public resulting from exposure to radionuclides in sewage sludge during its treatment and disposal. Eleven scenarios were developed to characterize potential exposures to radioactive materials during sewer system operations and sewage sludge treatment and disposal activities and during the extended time frame following sewage sludge disposal. Two sets of deterministic dose calculations were performed; one to evaluate potential doses based on the radionuclides and quantities associated with documented case histories of sewer system contamination and a second, somewhat more conservative set, based on theoretical discharges at the maximum allowable levels for a more comprehensive list of 63 radionuclides. The results of the stochastic uncertainty and sensitivity analysis were also used to develop a collective dose estimate. The collective doses for the various radionuclides and scenarios range from 0.4 person-rem for 137Cs in Scenario No. 5 (sludge incinerator effluent) to 420 person-rem for 137Cs in Scenario No. 3 (sewage treatment plant liquid effluent). None of the 22 scenario/radionuclide combinations considered have collective doses greater than 1000 person-rem/yr. However, the total collective dose from these 22 combinations was found to be about 2100 person-rem

  14. Superconducting Gamma/Neutron Spectrometer Task 1 Completion Report Evaluation of Candidate Neutron-Sensitive Materials

    CERN Document Server

    Bell, Z W

    2002-01-01

    A review of the scientific literature regarding boron- and lithium-containing compounds was completed. Information such as Debye temperature, heat capacity, superconductivity properties, physical and chemical characteristics, commercial availability, and recipes for synthesis was accumulated and evaluated to develop a list of neutron-sensitive materials likely to perform properly in the spectrometer. The best candidate borides appear to be MgB sub 2 (a superconductor with T sub c = 39 K), B sub 6 Si, B sub 4 C, and elemental boron; all are commercially available. Among the lithium compounds are LiH, LiAl, Li sub 1 sub 2 Si sub 7 , and Li sub 7 Sn sub 2. These materials have or are expected to have high Debye temperatures and sufficiently low heat capacities at 100 mK to produce a useful signal. The responses of sup 1 sup 0 B and sup 6 Li to a fission neutron spectrum were also estimated. These demonstrated that the contribution of scattering events is no more than 3% in a boron-based system and 1.5% in a lith...

  15. Evaluation of support materials for the surface immobilization and decoloration of amaranth by Trametes versicolor.

    Science.gov (United States)

    Shin, M; Nguyen, T; Ramsay, J

    2002-10-01

    The ability of Trametes versicolor ATCC 20869 to colonize several natural and synthetic materials (wheat straw, jute, hemp, maple woodchips, and nylon and polyethylene teraphthalate fibers) and to subsequently decolorize amaranth was evaluated. Jute was found to be the best support material as T. versicolor grew well on it without color leaching from the support and without loss of the jute's integrity over a 4 week period. The fungus immobilized on jute, straw and hemp decolorized amaranth (50 mg l(-1)) at a rate of about 5 mg l(-1) h(-1) without glucose being added. When 1 g l(-1) glucose was added, the dye was degraded more quickly (about 8 mg l(-1) h(-1)). Decoloration did not occur in a suspension culture without glucose. As the number of decoloration cycles increased, the rate of decoloration decreased. This rate was restored to its original level after the biomass was incubated in fresh growth medium for 5 days. With all immobilization supports, the toxicity of the medium before and after decoloration was the same or lower.

  16. Criteria for the Research Institute for Fragrance Materials, Inc. (RIFM) safety evaluation process for fragrance ingredients.

    Science.gov (United States)

    Api, A M; Belsito, D; Bruze, M; Cadby, P; Calow, P; Dagli, M L; Dekant, W; Ellis, G; Fryer, A D; Fukayama, M; Griem, P; Hickey, C; Kromidas, L; Lalko, J F; Liebler, D C; Miyachi, Y; Politano, V T; Renskers, K; Ritacco, G; Salvito, D; Schultz, T W; Sipes, I G; Smith, B; Vitale, D; Wilcox, D K

    2015-08-01

    The Research Institute for Fragrance Materials, Inc. (RIFM) has been engaged in the generation and evaluation of safety data for fragrance materials since its inception over 45 years ago. Over time, RIFM's approach to gathering data, estimating exposure and assessing safety has evolved as the tools for risk assessment evolved. This publication is designed to update the RIFM safety assessment process, which follows a series of decision trees, reflecting advances in approaches in risk assessment and new and classical toxicological methodologies employed by RIFM over the past ten years. These changes include incorporating 1) new scientific information including a framework for choosing structural analogs, 2) consideration of the Threshold of Toxicological Concern (TTC), 3) the Quantitative Risk Assessment (QRA) for dermal sensitization, 4) the respiratory route of exposure, 5) aggregate exposure assessment methodology, 6) the latest methodology and approaches to risk assessments, 7) the latest alternatives to animal testing methodology and 8) environmental risk assessment. The assessment begins with a thorough analysis of existing data followed by in silico analysis, identification of 'read across' analogs, generation of additional data through in vitro testing as well as consideration of the TTC approach. If necessary, risk management may be considered.

  17. Self-assembled peptide nanotubes as electronic materials: An evaluation from first-principles calculations

    International Nuclear Information System (INIS)

    In this letter, we report on the evaluation of diphenylalanine (FF), dityrosine (YY), and phenylalanine-tryptophan (FW) self-assembled peptide nanotube structures for electronics and photonics applications. Realistic bulk peptide nanotube material models were used in density functional theory calculations to mimic the well-ordered tubular nanostructures. Importantly, validated functionals were applied, specifically by using a London dispersion correction to model intertube interactions and a range-separated hybrid functional for accurate bandgap calculations. Bandgaps were found consistent with available experimental data for FF, and also corroborate the higher conductance reported for FW in comparison to FF peptide nanotubes. Interestingly, the predicted bandgap for the YY tubular nanostructure was found to be slightly higher than that of FW, suggesting higher conductance as well. In addition, the band structure calculations along the high symmetry line of nanotube axis revealed a direct bandgap for FF. The results enhance our understanding of the electronic properties of these material systems and will pave the way into their application in devices

  18. Evaluation of the biodiesel production using three sources of raw material and ethanol

    Energy Technology Data Exchange (ETDEWEB)

    Radecki, Angela Patricia; Fracaro, Cristiane; Gnoatto, Estor; Kavanagh, Edward; Anami, Marcelo Hidemassa; Fischborn, Marcos; Lobo, Viviane da Silva [Universidade Tecnologica Federal do Parana (UTFPR), Medianeira, PR (Brazil)], E-mail: mhanami@utfpr.edu.br; Zara, Ricardo Fiori [Prati Donaduzzi e Cia. Ltda., Toledo, PR (Brazil)

    2008-07-01

    The conversion of different oils in ethyl ester (biodiesel) through the transesterification with anhydrous ethanol, together with its quality and its consumption in mixture with diesel of petroleum in different ratios, they were evaluated using a stationary diesel engine connected to an electric energy generator. The raw materials used in this transformation were oil of refined soybean, oil of refined sunflower and animal fat (swine). In the transesterification reaction it was used an alkaline catalyst (sodium hydroxide), because of its proven effectiveness and the high speed facing other catalyst, beyond being less corrosive and demands less molar' reasons between the alcohol and the vegetal oil. The tests in stationary diesel engine were carried through the dilutions of 0%, 5%, 10%, 15% and 20% of biodiesel produced in mixture with diesel of petroleum. The results showed that the yield of biodiesel gotten by different sources is satisfactory. It was also observed that the basic catalysis is adjusted to the production of biodiesel from raw materials with low acidity. The tests in diesel engine appeared to be sufficiently satisfactory once it was not observed any alteration in the functioning of the engine. The consumption was also not modified by the studied dilutions, demonstrating that the biodiesel can be added to the pure diesel reducing the use of the fuel derived from petroleum. (author)

  19. Measurement of standing wave ratio for evaluation of microwave absorption efficiency by molding materials

    Directory of Open Access Journals (Sweden)

    K. Granat

    2008-08-01

    Full Text Available The presented work includes results of standing wave measurement for evaluation of microwave absorption efficiency by molding materials. Initial research has been conducted using microwave gap line. It has been demonstrated that foundry quartz sands have minimal microwave absorption capability. The following binders used for research: bentonite „Geco” and bentonite „Specjal”, demonstrated the highest absorption of Pabs microwave power output of over 60% Pin. It has also been demonstrated that water content, constituting component of synthetic molding sands, significantly influences change of microwave absorption. We have established that application of this kind of measuring device may allow for precise determination of characteristic features, such as microwave absorption factor k, of various foundry materials as well as determination of their suitability in foundry processes, e.g. microwave formation of foundry molds and cores. Microwave gap line may also serve as a device for precise determination of water content as well as other molding sand components and for their identification with the use of characteristic parameters, e.g. reflection factor |Γk|.

  20. Self-assembled peptide nanotubes as electronic materials: An evaluation from first-principles calculations

    Science.gov (United States)

    Akdim, Brahim; Pachter, Ruth; Naik, Rajesh R.

    2015-05-01

    In this letter, we report on the evaluation of diphenylalanine (FF), dityrosine (YY), and phenylalanine-tryptophan (FW) self-assembled peptide nanotube structures for electronics and photonics applications. Realistic bulk peptide nanotube material models were used in density functional theory calculations to mimic the well-ordered tubular nanostructures. Importantly, validated functionals were applied, specifically by using a London dispersion correction to model intertube interactions and a range-separated hybrid functional for accurate bandgap calculations. Bandgaps were found consistent with available experimental data for FF, and also corroborate the higher conductance reported for FW in comparison to FF peptide nanotubes. Interestingly, the predicted bandgap for the YY tubular nanostructure was found to be slightly higher than that of FW, suggesting higher conductance as well. In addition, the band structure calculations along the high symmetry line of nanotube axis revealed a direct bandgap for FF. The results enhance our understanding of the electronic properties of these material systems and will pave the way into their application in devices.

  1. Selection and evaluation of blood- and tribologically compatible journal bearing materials.

    Science.gov (United States)

    Murray, S F; Calabrese, S J; Malanoski, S B; Golding, L R; Smith, W A; Hamby, M

    1997-01-01

    A critical issue in the Cleveland Clinic Foundation (CCF) Innovative Ventricular Assist System (IVAS) blood pump is the selection of materials for the blood-lubricated journal bearing. Under normal operating conditions, the journal bearing geometry creates a thick blood film that separates the rotating and stationary surfaces. However, since start-up and certain transients could cause temporary contact, the material pair selected for these surfaces must be both tribologically and blood compatible. Combinations of two biocompatible alloys were tested: a titanium-zirconium-niobium alloy (Ti-13Zr-13Nb) and a zirconium-niobium alloy (Zr-2.5Nb). A standard pin-on-disk tester was used, with the contact surfaces lubricated by glycerol/saline mixtures simulating the viscosity range of blood. One test series evaluated start-up conditions; the other modeled a high-speed rub that might occur if the fluid film broke down. Results showed that the preoxidized Zr-2.5Nb pin/Ti-13Zr-13Nb disk combination was superior at all sliding velocities; a self-mated Zr-2.5Nb pair also showed promise. The oxide film on a self-mated Ti-13Zr-13Nb pair, and a Ti-13Zr-13Nb pin and Zr-2.5Nb disk combination did not show adequate wear life. More work remains to explain distinct performance differences of certain combinations, with more data needed on mechanical properties of thin, hard coatings on softer metal substrates. PMID:9360116

  2. Evaluation of the Total Cost of Ownership of Fuel Cell-Powered Material Handling Equipment

    Energy Technology Data Exchange (ETDEWEB)

    Ramsden, T.

    2013-04-01

    This report discusses an analysis of the total cost of ownership of fuel cell-powered and traditional battery-powered material handling equipment (MHE, or more typically 'forklifts'). A number of fuel cell MHE deployments have received funding support from the federal government. Using data from these government co-funded deployments, DOE's National Renewable Energy Laboratory (NREL) has been evaluating the performance of fuel cells in material handling applications. NREL has assessed the total cost of ownership of fuel cell MHE and compared it to the cost of ownership of traditional battery-powered MHE. As part of its cost of ownership assessment, NREL looked at a range of costs associated with MHE operation, including the capital costs of battery and fuel cell systems, the cost of supporting infrastructure, maintenance costs, warehouse space costs, and labor costs. Considering all these costs, NREL found that fuel cell MHE can have a lower overall cost of ownership than comparable battery-powered MHE.

  3. Evaluation of the Characteristics of the Aluminum Alloy Casting Material by Heat Treatment

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Syung Yul; Park, Dong Hyun; Won, Jong Pil; Kim, Yun Hae; Lee, Myung Hoon; Moon, Kyung Man; Jeong, Jae Hyun [Korea Maritime Univ., Busan (Korea, Republic of)

    2012-06-15

    Aluminum is on active metal, but it is well known that its oxide film plays a role as protective barrier which is comparatively stable in air and neutral aqueous solution. Thus, aluminum alloys have been widely applied in architectural trim, cold and hot-water storage vessels and piping etc., furthermore, the aluminum alloy of AC8A have been widely used in mold casting material of engine piston because of its properties of temperature and wear resistance. In recent years, the oil price is getting higher and higher, thus the using of low quality oil has been significantly increased in engines of ship and vehicle. Therefore it is considered that evaluation of corrosion resistance as well as wear resistance of AC8A material is also important to improve its property and prolong its lifetime. In this study, the effect of solution and tempering heat treatment to corrosion and wear resistance is investigated with electrochemical method and measurement of hardness. The hardness decreased with solution heat treatment compared to mold casting condition, but its value increased with tempering heat treatment and exhibited the highest value of hardness with tempering heat treatment temperature at 190 .deg. C for 24hrs. Furthermore, corrosion resistance increased with decreasing of the hardness, and decreased with increasing of the hardness reversely. As a result, it is suggested that the optimum heat treatment to improve both corrosion and wear resistance is tempering heat treatment temperature at 190 .deg. C for 16hrs.

  4. Criteria for the Research Institute for Fragrance Materials, Inc. (RIFM) safety evaluation process for fragrance ingredients.

    Science.gov (United States)

    Api, A M; Belsito, D; Bruze, M; Cadby, P; Calow, P; Dagli, M L; Dekant, W; Ellis, G; Fryer, A D; Fukayama, M; Griem, P; Hickey, C; Kromidas, L; Lalko, J F; Liebler, D C; Miyachi, Y; Politano, V T; Renskers, K; Ritacco, G; Salvito, D; Schultz, T W; Sipes, I G; Smith, B; Vitale, D; Wilcox, D K

    2015-08-01

    The Research Institute for Fragrance Materials, Inc. (RIFM) has been engaged in the generation and evaluation of safety data for fragrance materials since its inception over 45 years ago. Over time, RIFM's approach to gathering data, estimating exposure and assessing safety has evolved as the tools for risk assessment evolved. This publication is designed to update the RIFM safety assessment process, which follows a series of decision trees, reflecting advances in approaches in risk assessment and new and classical toxicological methodologies employed by RIFM over the past ten years. These changes include incorporating 1) new scientific information including a framework for choosing structural analogs, 2) consideration of the Threshold of Toxicological Concern (TTC), 3) the Quantitative Risk Assessment (QRA) for dermal sensitization, 4) the respiratory route of exposure, 5) aggregate exposure assessment methodology, 6) the latest methodology and approaches to risk assessments, 7) the latest alternatives to animal testing methodology and 8) environmental risk assessment. The assessment begins with a thorough analysis of existing data followed by in silico analysis, identification of 'read across' analogs, generation of additional data through in vitro testing as well as consideration of the TTC approach. If necessary, risk management may be considered. PMID:25510979

  5. Field evaluations of residual pesticide applications and misting system on militarily relevant materials against medically important mosquitoes in Thailand

    Science.gov (United States)

    A key strategy to reduce insect-borne disease is to reduce contact between disease vectors and hosts. In the current study, residual pesticide application and misting system were applied on militarily relevant materials and evaluated against medically important mosquitoes. Field evaluations were car...

  6. The evaluation of carrier material for increasing qualities of gel inoculum for nata de coco

    Directory of Open Access Journals (Sweden)

    RUTH MELLIAWATI

    2008-10-01

    Full Text Available Producion of nata de coco is growing fast, in line with increasing product of biocellulose demand. It is requrire a pure inoculum to reach the best biocellulose product. The aim of this reseach is to evaluate the most appropriate carrier material of gel inoculum for nata de coco. The four carrier material are Carboxy Methyl Cellulose (CMC, Agar, Sagu starch and biocellulose pap and its inoculated by Acetobacter sp. RMG-2 and A. xylinum. After inoculation, then put in the plastic bag (50 g/bag and stored in 4° C. The texture of gel, population of cell and biocellulose production were observer in 7 days. The result shown that all matterial were suitable to used as carrier for gel inoculum. Both CMC and biocellulose pap have good texture as standard qualities. Population of A. xylinum was 1.28x109 cfu/mL (in CMC carrier, 1.6x106 cfu/mL (in biocellulose pap carrier after 15 weeks. The weight of biocellulose production was 500 g/L and 740 g/L medium respectively. While the population of Acetobacter sp. RMG-2 on CMC carrier was 1.79x108 cfu/mL and 7.75x107 cfu/mL on cellulose carrier with the weight of biocellulose production 630 g/L and 775 g/L medium respectively. Thus, the carrier material (CMC and Biocellulose pap are able to keep bacteria without loss their capability to produce cellulose.

  7. An electrochemical evaluation of new materials and methods for corrosion protection

    Science.gov (United States)

    Kus, Esra

    An electrochemical evaluation of various electrode/electrolyte systems was performed by means of electrochemical impedance spectroscopy (EIS) and other techniques. Each chapter in this thesis presents an individual project with a specific objective which serves an ultimate goal of finding better materials and methods of corrosion protection. An overview of new environmentally friendly and cost effective materials and corrosion protection methods is given in Chapter 1. The protective properties of non-toxic, environmentally friendly polymer coatings, which were developed in the purpose of minimizing biofouling and providing corrosion protection on steel, were investigated and discussed in Chapter 2. The corrosion resistance of steel panels coated with crosslinked siloxanes was evaluated using EIS. Differences in protective properties of the coatings were observed due to differences in the degree of fluorination, the way the films were cured and also the degree of crosslinking. In Chapter 3, a comparison of the corrosion behavior of nanocrystalline (NC) Al 5083 with that of the conventional alloy was made in order to determine what differences if any could be attributed to the NC microstructure. Pit growth rates decreased with time for both materials based on the analysis of the impedance spectra as a function of time. NC samples were resistant to intergranular corrosion whereas conventional Al 5083 was not. The concept of the bacterial battery is presented in Chapter 4. A galvanic cell with Cu and Al 2024 and an electrolyte containing Shewanella oneidensis MR-1 in a growth medium was prepared. A control cell, which did not contain the bacteria, was also tested. For the cell with MR-1 the maximum power values increased continuously with time, whereas in the control cell the maximum power output was obtained in the first day of exposure. The objective of the study presented in Chapter 5 was to examine the interaction of MR-1 with different metal surfaces in order to

  8. Evaluation of anode (electro)catalytic materials for the direct borohydride fuel cell: Methods and benchmarks

    Science.gov (United States)

    Olu, Pierre-Yves; Job, Nathalie; Chatenet, Marian

    2016-09-01

    In this paper, different methods are discussed for the evaluation of the potential of a given catalyst, in view of an application as a direct borohydride fuel cell DBFC anode material. Characterizations results in DBFC configuration are notably analyzed at the light of important experimental variables which influence the performances of the DBFC. However, in many practical DBFC-oriented studies, these various experimental variables prevent one to isolate the influence of the anode catalyst on the cell performances. Thus, the electrochemical three-electrode cell is a widely-employed and useful tool to isolate the DBFC anode catalyst and to investigate its electrocatalytic activity towards the borohydride oxidation reaction (BOR) in the absence of other limitations. This article reviews selected results for different types of catalysts in electrochemical cell containing a sodium borohydride alkaline electrolyte. In particular, propositions of common experimental conditions and benchmarks are given for practical evaluation of the electrocatalytic activity towards the BOR in three-electrode cell configuration. The major issue of gaseous hydrogen generation and escape upon DBFC operation is also addressed through a comprehensive review of various results depending on the anode composition. At last, preliminary concerns are raised about the stability of potential anode catalysts upon DBFC operation.

  9. Evaluation of dredged material proposed for ocean disposal from Bronx River Project Area, New York

    Energy Technology Data Exchange (ETDEWEB)

    Gruendell, B.D.; Gardiner, W.W.; Antrim, L.D.; Pinza, M.R.; Barrows, E.S.; Borde, A.B. [Battelle Marine Research Lab., Sequim, WA (United States)

    1996-12-01

    The objective of the Bronx River project was to evaluate proposed dredged material from the Bronx River project area in Bronx, New York, to determine its suitability for unconfined ocean disposal at the Mud Dump Site. Bronx River was one of five waterways that the US Army Corps of Engineers-New York District (USAGE-NYD) requested the Battelle Marine Sciences Laboratory (MSL) to sample and to evaluate for dredging and disposal. Sediment samples were submitted for physical and chemical analyses, chemical analyses of dredging site water and elutriate, benthic and water-column acute toxicity tests, and bioaccumulation studies. Fifteen individual sediment core samples collected from the Bronx River project area were analyzed for grain size, moisture content, and total organic carbon (TOC). One composite sediment sample, representing the entire reach of the area proposed for dredging, was analyzed for bulk density, specific gravity, metals, chlorinated pesticides, polychlorinated biphenyl (PCB) congeners, polynuclear aromatic hydrocarbons (PAH), and 1,4- dichlorobenzene. Dredging site water and elutriate water, which was prepared from the suspended-particulate phase (SPP) of the Bronx River sediment composite, were analyzed for metals, pesticides, and PCBS.

  10. Evaluation of dredged material proposed for ocean disposal from Hudson River, New York

    Energy Technology Data Exchange (ETDEWEB)

    Gardiner, W.W.; Barrows, E.S.; Antrim, L.D.; Gruendell, B.D.; Word, J.Q.; Tokos, J.J.S. [Battelle/Marine Sciences Lab., Sequim, WA (United States)

    1996-09-01

    The Hudson River (Federal Project No. 41) was one of seven waterways that the U.S. Army Corps of Engineers-New York District (USACE-NYD) requested the Battelle Marine Sciences Laboratory (MSL) to sample and evaluate for dredging and disposal in March 1994. Sediment samples were collected from the Hudson River. Tests and analyses were conducted on Hudson River sediment core samples. The evaluation of proposed dredged material from the Hudson River included bulk sediment chemical analyses, chemical analyses of site water and elutriate, water-column and benthic acute toxicity tests, and bioaccumulation studies. Individual sediment core samples collected from Hudson River were analyzed for grain size, moisture content, and total organic carbon (TOC). A composite sediment sample, representing the entire area proposed for dredging, was analyzed for bulk density, specific gravity, metals, chlorinated pesticides, polychlorinated biphenyl (PCB) congeners, polynuclear aromatic hydrocarbons (PAH), and 1,4-dichlorobenzene. Site water and elutriate water, prepared from the suspended-particulate phase (SPP) of Hudson River sediment, were analyzed for metals, pesticides, and PCBS. Water-column or SPP toxicity tests were performed with three species. Benthic acute toxicity tests were performed. Bioaccumulation tests were also conducted.

  11. Evaluation of ductility of zircaloy-2 materials using a small ellipsoidal-shaped punch

    International Nuclear Information System (INIS)

    Seam-welded Zircaloy-2 calandria tubes are used in the fuel channel of CANDU reactors, to isolate the hot pressure tube from the cool heavy-water moderator. The mechanical properties of irradiated welds are required to assess whether they will be satisfactory to the end-of-life of the reactor. It is impractical to irradiate short sections of calandria tube for burst testing. Therefore, we have developed a small ellipsoidal-shaped punch to evaluate the mechanical properties of anisotropic Zircaloy-2 material having various microstructures such as those present in a welded calandria tube. Small punch tests were performed on four different types of calandria tubes, two welded and two seamless, and the results show that the mechanical anisotropy of the tubes could be differentiated. The fracture produced in unirradiated small specimens showed a straight-line crack, similar to a straight-line rupture on a tube during burst testing. A re-constitution of the properties from small specimens was used for correlation with the burst properties of the tubes. A consistent correlation was obtained for the punch load and displacement with the burst strength and ductility of the tubes. Based on this correlation, mechanical properties of irradiated welds using the small ellipsoidal punch method are being evaluated. (author)

  12. Fabrication and performance evaluation of oil –fired crucible furnace using locally sourced materials

    Directory of Open Access Journals (Sweden)

    J.O Osarenmwinda

    2015-03-01

    Full Text Available The technological advancement of any nation have been influenced and uplifted by the extent to which it can usefully harness and convert its mineral resources.The production of metal in foundries and in all human lives have become a general practice.This paper deals with the design, fabrication and performance evaluation of an oil-fired crucible furnace using locally sourced materials . The components of oil fired crucible furnace were furnace casing, crucible,furnace cover,burner housing,furnace cover stand,base stand and burner, Design drawings were produced and mild steel sheet was used for the fabrication of the furnace, while the other components needed for the design were selected based on functionality, durability, cost and local availability.. Experimental tests were performed to evaluate the performance of the furnace. The results showed that the furnace has a heating rate of 43.9°C/min and attained a temperature as high as 1386 °C . The furnace also had a melting rate of 333.3g/min for Aluminum and 115.8 g/min for Copper. The efficiency of the furnace was determined to be 10.34%.The low value was as result of the large energy wastage due to the open nature of the furnace.

  13. Formation of ultra slow position beam and upgrading of material evaluation using it

    Energy Technology Data Exchange (ETDEWEB)

    Mikado, Tomohisa; Suzuki, Ryoichi; Odaira, Toshiyuki; Ohgaki, Hideaki; Yamada, Kawakatsu; Yamazaki, Tetsuo; Kobayashi, Yoshinori; Hirata, Koichi [Electrotechnical Lab., Tsukuba, Ibaraki (Japan)

    2000-02-01

    The Electrotechnical Laboratory has carried out development on a technique to form and control high intensity and slow positron beam by using high energy electron beam of electron accelerator, success in generation of ultra short pulse beam of incident energy variable positron with the highest intensity in the world, development on testing techniques of positron life, spectroscopic flight time of positron annihilation excited Auger electron and so on, and their applications. The 1998 fiscal year was the last fiscal year of this researching project, and together with conducting reform of forming method of high intensity positron beam, energy analysis of ultra slow positron beam and upgrading of incident energy variable positron lifetime testing the testing technique of the positron annihilation excited Auger electron spectroscopy and positron lifetime developed by this study was applied to various samples and effectiveness of analysis and evaluation methods using the ultra slow positron beam was investigated. As a result, it was succeeded in to make high intensity of 1 eV plus/minus 0.5 eV in energy And, on the positron annihilation excited Auger electron spectroscopy, at lifetime measurement of about 40 eV short pulse beam and incident energy variable positron beam, 0.2 to 0.3 keV short pulse positron beam could be formed to realize a material evaluation method with high counting rate, low background and high resolution. (G.K.)

  14. Formation of ultra slow position beam and upgrading of material evaluation using it

    International Nuclear Information System (INIS)

    The Electrotechnical Laboratory has carried out development on a technique to form and control high intensity and slow positron beam by using high energy electron beam of electron accelerator, success in generation of ultra short pulse beam of incident energy variable positron with the highest intensity in the world, development on testing techniques of positron life, spectroscopic flight time of positron annihilation excited Auger electron and so on, and their applications. The 1998 fiscal year was the last fiscal year of this researching project, and together with conducting reform of forming method of high intensity positron beam, energy analysis of ultra slow positron beam and upgrading of incident energy variable positron lifetime testing the testing technique of the positron annihilation excited Auger electron spectroscopy and positron lifetime developed by this study was applied to various samples and effectiveness of analysis and evaluation methods using the ultra slow positron beam was investigated. As a result, it was succeeded in to make high intensity of 1 eV plus/minus 0.5 eV in energy And, on the positron annihilation excited Auger electron spectroscopy, at lifetime measurement of about 40 eV short pulse beam and incident energy variable positron beam, 0.2 to 0.3 keV short pulse positron beam could be formed to realize a material evaluation method with high counting rate, low background and high resolution. (G.K.)

  15. Summative Evaluation of Polymers, Composites & Sports Materials: An Introduction to Chemistry and Physics.

    Science.gov (United States)

    Hagedorn, Eric

    2008-03-01

    During Fall 2007, 70 pre-science freshman completed a one-credit science course with three goals: 1) enhance and maintain student interest in science majors while completing necessary prerequisite mathematics courses, 2) provide students with a solid content & mathematical foundation for introductory physics and chemistry, and 3) pilot hands-on activities developed for the Materials World Modules program. Eight pre/post quizzes, along with a midterm and final were used to assess student learning. Traditional course evaluations were supplemented with completed SALG (Student Assessment of Learning Gains) instruments. Analysis of these data indicated the following: 1) on 6 out of 7 pre-post quizzes, students showed statistically significant gains with medium or large effect sizes, 2) while students who completed the SALG instrument found all aspects of the course helpful, the hands-on activities were not as helpful as intended, and 3) logistical issues had the most detrimental impact on this course. The evaluation results have led to a number of changes for the Fall 2008 offering of this course.

  16. Evaluation of a standard test method and material for low-activity waste product acceptance

    International Nuclear Information System (INIS)

    The dissolution behavior of a candidate reference glass has been measured under a range of test conditions. The data base from these tests can be used to evaluate the credibility and validity of test results reported by Private Contractors as part of the acceptance process for immobilized low-activity waste (ILAW) products for DOE wastes. The LRM-1 glass that was used in the tests was formulated to be compositionally representative of anticipated ILAW products for Hanford and other Department of Energy sites. Replicate tests with this glass were used to measure the variability in the response (i.e., the solution concentrations of B, Na, and Si) under different test conditions. The glass was further evaluated for possible use as a standard material by analysis of its composition, microstructure, density, and compressive strength. In addition, the Na leachability index was measured with the ANS 16.1 test, and the Toxicity Characteristic Leach Procedure was run. The results of those tests and analyses are summarized

  17. Report of a technical evaluation panel on the use of beryllium for ITER plasma facing material and blanket breeder material

    International Nuclear Information System (INIS)

    Beryllium because of its low atomic number and high thermal conductivity, is a candidate for both ITER first wall and divertor surfaces. This study addresses the following: why beryllium; design requirements for the ITER divertor; beryllium supply and unirradiated physical/mechanical property database; effects of irradiation on beryllium properties; tritium issues; beryllium health and safety; beryllium-coolant interactions and safety; thermal and mechanical tests; plasma erosion of beryllium; recommended beryllium grades for ITER plasma facing components; proposed manufacturing methods to produce beryllium parts for ITER; emerging beryllium materials; proposed inspection and maintenance techniques for beryllium components and coatings; time table and costs; and the importance of integrating materials and manufacturing personnel with designers

  18. Report of a technical evaluation panel on the use of beryllium for ITER plasma facing material and blanket breeder material

    Energy Technology Data Exchange (ETDEWEB)

    Ulrickson, M.A. [ed.] [Sandia National Labs., Albuquerque, NM (United States); Manly, W.D. [Oak Ridge National Lab., TN (United States); Dombrowski, D.E. [Brush Wellman, Inc., Cleveland, OH (United States)] [and others

    1995-08-01

    Beryllium because of its low atomic number and high thermal conductivity, is a candidate for both ITER first wall and divertor surfaces. This study addresses the following: why beryllium; design requirements for the ITER divertor; beryllium supply and unirradiated physical/mechanical property database; effects of irradiation on beryllium properties; tritium issues; beryllium health and safety; beryllium-coolant interactions and safety; thermal and mechanical tests; plasma erosion of beryllium; recommended beryllium grades for ITER plasma facing components; proposed manufacturing methods to produce beryllium parts for ITER; emerging beryllium materials; proposed inspection and maintenance techniques for beryllium components and coatings; time table and costs; and the importance of integrating materials and manufacturing personnel with designers.

  19. Calculational Models for Quantitative Evaluation of Proliferation Protection for Fissionable Materials

    International Nuclear Information System (INIS)

    This work is devoted to the development of calculational models, on the basis of which it is possible to evaluate proliferation protection for various fissionable materials. The main physical, kinematic and thermal processes that take place in a hypothetical nuclear explosive device (HNED) are simulated. Consideration is referred both to gun-type and implosion-type HNED. The objective of the gun-type HNED model is to estimate the maximum speed at which subcritical masses can be assembled. At the basis of the model it is laid the assumption that the movement of the projectile in the barrel is uniformly accelerated. To estimate maximum allowable explosive gas pressure the model of A. V. Gadolin (proposed in 1852 year) is used (1). The addition of spontaneous neutron source (for example, 232U with beryllium admixture) into nuclear material (U) in order to provide a premature initiation of chain reaction (pre-detonation) was analyzed. Required neutron source strength and fraction of 232U with beryllium admixture for a pre-detonation were evaluated. The principle design of implosion-type HNED is based on the model which was proposed by Doctor G. Kessler (2). The implosion-type HNED consists of a central plutonium charge surrounded by spherical layers of natural uranium, aluminum and chemical high explosive (HE). To protect nuclear material (Pu) it is suggested (2) to add some amount of radioactive isotope (238Pu), the alpha decay heat of which could overheat HNED and render it non-functional. When heated up, HNED loses its effectiveness mainly due to the high-temperature instability of HE (meltdown, pyrolysis and self-ignition). A calculational model of non-stationary warm-up of implosive-type HNED has been developed in order to evaluate the rate of loss of its effectiveness for different isotopic compositions of plutonium and for different methods of heat removal. The paper presents the obtained results in numerical studies of the transient behavior of temperature

  20. Calculational Models for Quantitative Evaluation of Proliferation Protection for Fissionable Materials

    Energy Technology Data Exchange (ETDEWEB)

    Shmelev, A.N.; Kulikov, E.G.; Apse, V.A.; Kulikov, G.G. [Moscow Engineering Physics Institute (State University), Kashirskoe shosse 31, Moscow, 115409 (Russian Federation)

    2009-06-15

    This work is devoted to the development of calculational models, on the basis of which it is possible to evaluate proliferation protection for various fissionable materials. The main physical, kinematic and thermal processes that take place in a hypothetical nuclear explosive device (HNED) are simulated. Consideration is referred both to gun-type and implosion-type HNED. The objective of the gun-type HNED model is to estimate the maximum speed at which subcritical masses can be assembled. At the basis of the model it is laid the assumption that the movement of the projectile in the barrel is uniformly accelerated. To estimate maximum allowable explosive gas pressure the model of A. V. Gadolin (proposed in 1852 year) is used (1). The addition of spontaneous neutron source (for example, {sup 232}U with beryllium admixture) into nuclear material (U) in order to provide a premature initiation of chain reaction (pre-detonation) was analyzed. Required neutron source strength and fraction of {sup 232}U with beryllium admixture for a pre-detonation were evaluated. The principle design of implosion-type HNED is based on the model which was proposed by Doctor G. Kessler (2). The implosion-type HNED consists of a central plutonium charge surrounded by spherical layers of natural uranium, aluminum and chemical high explosive (HE). To protect nuclear material (Pu) it is suggested (2) to add some amount of radioactive isotope ({sup 238}Pu), the alpha decay heat of which could overheat HNED and render it non-functional. When heated up, HNED loses its effectiveness mainly due to the high-temperature instability of HE (meltdown, pyrolysis and self-ignition). A calculational model of non-stationary warm-up of implosive-type HNED has been developed in order to evaluate the rate of loss of its effectiveness for different isotopic compositions of plutonium and for different methods of heat removal. The paper presents the obtained results in numerical studies of the transient behavior

  1. Technical evaluation panel summary report. Ceramic and glass immobilization options fissile materials disposition program

    Energy Technology Data Exchange (ETDEWEB)

    Myers, B. R. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Brummond, W. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Armantrout, G. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Shaw, H. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Jantzen, C. M. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Jostons, A. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); McKibben, M. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Strachan, D. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Vienna, J. D. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

    1997-12-23

    This report documents the results of a technical evaluation of the merits of ceramic and glass immobilization forms for the disposition of surplus weapons-useable plutonium. The evaluation was conducted by a Technical Evaluation Panel (TEP), whose members were selected to cover a relevant range of scientific and technical expertise and represented each of the technical organizations involved in the Plutonium Immobilization Program. The TEP held a formal review at Lawrence Liver-more National Laboratory (LLNL) from July 2%August 1, 1997. Following this review, the TEP documented the review and its evaluation of the two immobilization technologies in this report to provide a technical basis for a recommendation by LLNL to the Department of Energy (DOE) for the preferred immobilization form. The comparison of the glass and ceramic forms and manufacturing processes was a tremendous challenge to the TEP. The two forms and their processes are similar in many ways. The TEP went to great effort to accurately assess what were, in many cases, fine details of the processes, unit operations, and the glass and ceramic forms themselves. The set of criteria used by the Fissile Materials Disposition Program (FMDP) in past screenings and down-selections was used to measure-the two options. One exception is that the TEP did not consider criteria that were largely nontechnical (namely international impact, public acceptance, and effects on other : DOE programs). The TEP' s measures and assessments are documented in detail. Care was taken to ensure that the data used were well documented and traceable to their source. Although no final conclusion regarding the preferred form was reached or explicitly stated in this report (this was not within the TEP' s charter), no "show stoppers" were identified for either form. Both forms appear capable of satisfying all the criteria, as interpreted by the TEP. The TEP identified a number of distinct and quantifiable differences between

  2. Evaluation of thermal aging effect on primary pipe material in nuclear power plant by micro hardness test method

    International Nuclear Information System (INIS)

    The investigation was carried out on the changes in mechanical properties of the primary pipe material Z3CN20.09M after 10000 h aging at 400℃ by using micro- Vickers and impact testing machine. The results show that the impact energy of testing material decreases. However, the micro-Vickers hardness of ferrite phase and austenite phase which constitute the testing material increase and keep constant, respectively. The intrinsic relations were analyzed between the micro-Vickers hardness and the impact energy to make an attempt to present the micro-Vickers hardness measurement as a method applicable to evaluating the thermal aging of the primary pipe material. (authors)

  3. Multi-material laser densification (MMLD) of dental restorations: Process optimization and properties evaluation

    Science.gov (United States)

    Li, Xiaoxuan

    This Ph.D. thesis proposes to investigate the feasibility of laser-assisted dental restoration and to develop a fundamental understanding of the interaction between laser beam and dental materials. Traditional dental restorations are produced by the porcelain-fused-to-metal (PFM) process, in which a dental restoration is cast from a metallic alloy and then coated with dental porcelains by multiple furnace-firing processes. PFM method is labor-intensive and hence very expensive. In order to fabricate dental restoration units faster and more cost-effectively, the Solid Freeform Fabrication (SFF) technique has been employed in this study. In particular, a Multi-Material Laser Densification (MMLD) process has been investigated for its potential to fabricate artificial teeth automatically from 3-D computer dental tooth files. Based on the principle of SFF, the MMLD process utilizes a micro-extruder system to deliver commercial dental alloy and porcelain slurry in a computer-controlled pattern line by line and layer by layer. Instead of firing the artificial tooth/teeth in a furnace, the extruded dental materials are laser scanned to convert the loose powder to a fully dense body. Different laser densification parameters including the densification temperature, laser output power, laser beam size, line dimension, ratio of the beam size to line width, beam scanning rate, processing atmosphere and pressure, dental powder state (powder bed or slurry), powder particle size, etc. have been used to evaluate their effects on the microstructures and properties of the laser densified dental body, and hence to optimize MMLD conditions. Furthermore, laser-scanning induced phase transformations in dental porcelains have been studied because the transformations have great impact on coefficient of thermal expansion (CTE) of dental porcelains, which should match that of dental alloy substrate. Since a single dental material line delivered by the MMLD system functions as a "construction

  4. Evaluation of the effect of various beverages and food material on the color stability of provisional materials – An in vitro study

    OpenAIRE

    Gupta, Gaurav; Gupta, Tina

    2011-01-01

    Aim: This study evaluated the color stability of four provisional materials: 1) Poly-methyl methacrylates (DPI); 2) Bis-acryl composite (ProtempTM II – 3M ESPE); 3) Bis-acryl composite (Systemp® c and b – Ivoclar Vivadent) and 4) Light polymerized composite resin (Revotek LC- GC). Materials and Methods: The color and color difference of each specimen after immersion in different staining solutions i.e. 1) tea and artificial saliva, 2) coffee and artificial saliva, 3) Pepsi and artificial sali...

  5. Evaluation of the effect of various beverages and food material on the color stability of provisional materials - An in vitro study

    OpenAIRE

    Gaurav Gupta; Tina Gupta

    2011-01-01

    Aim: This study evaluated the color stability of four provisional materials: 1) Poly-methyl methacrylates (DPI); 2) Bis-acryl composite (ProtempTM II - 3M ESPE); 3) Bis-acryl composite (Systemp; c and b - Ivoclar Vivadent) and 4) Light polymerized composite resin (Revotek LC- GC). Materials and Methods: The color and color difference of each specimen after immersion in different staining solutions i.e. 1) tea and artificial saliva, 2) coffee and artificial saliva, 3) Pepsi and artificial...

  6. Moisture evaluation of wood material using GPR with WARR method - COST Action TU1208

    Science.gov (United States)

    Reci, Hamza; Sbart'i, Zoubir Mehdi; Pajewski, Lara; Marciniak, Marian

    2016-04-01

    This work deals with the study of the sensitivity of GPR electromagnetic waves to moisture variation in wood material in relation with the direction of fibers and polarization of Electromagnetic field. The relations between relative permittivity and moisture content and the amplitude attenuation with distance was a target study using the direct waves in Wide Angle Radar Reflection (WARR) configuration. Comparison of results measured with reflected waves and direct waves was of main importance since they have different behavior in relation with moisture variation, due to different path of propagation. This research activity has been carried out during one Short-Term Scientific Missions (STSM) funded by the COST (European Cooperation in Science and Technology) Action TU1208 "Civil Engineering Applications of Ground Penetrating Radar" in November-December 2015. In context of durability evaluation of construction materials, several studies have been carried out by the I2M team, University of Bordeaux, using direct and reflected waves for the evaluation of water content on concrete and wood materials [1-3]. As related to the wood material there is one study carried out using the reflected waves on wood for different humidity and different wood samples, in all the direction of polarization using GPR technique ground coupled antenna at 1.5 GHz [3]. This work continued with different moisture content in order to study the behavior of direct waves as function of moisture. Results taken from those measurements are compared with them from Fixed Offset (reflected method) with one antenna (1.5GHz or 2.6GHz), realized from the previous studies from the I2M and already published [1-3]. The results taken from this work from the reflected waves, show that the effect of wood anisotropy is significant on the variation of relative permittivity with moisture content on wood sample and that is in good agreement with the previous results [3-6]. As related to the direct waves, a small

  7. Moisture evaluation of wood material using GPR with WARR method - COST Action TU1208

    Science.gov (United States)

    Reci, Hamza; Sbart'i, Zoubir Mehdi; Pajewski, Lara; Marciniak, Marian

    2016-04-01

    This work deals with the study of the sensitivity of GPR electromagnetic waves to moisture variation in wood material in relation with the direction of fibers and polarization of Electromagnetic field. The relations between relative permittivity and moisture content and the amplitude attenuation with distance was a target study using the direct waves in Wide Angle Radar Reflection (WARR) configuration. Comparison of results measured with reflected waves and direct waves was of main importance since they have different behavior in relation with moisture variation, due to different path of propagation. This research activity has been carried out during one Short-Term Scientific Missions (STSM) funded by the COST (European Cooperation in Science and Technology) Action TU1208 "Civil Engineering Applications of Ground Penetrating Radar" in November-December 2015. In context of durability evaluation of construction materials, several studies have been carried out by the I2M team, University of Bordeaux, using direct and reflected waves for the evaluation of water content on concrete and wood materials [1-3]. As related to the wood material there is one study carried out using the reflected waves on wood for different humidity and different wood samples, in all the direction of polarization using GPR technique ground coupled antenna at 1.5 GHz [3]. This work continued with different moisture content in order to study the behavior of direct waves as function of moisture. Results taken from those measurements are compared with them from Fixed Offset (reflected method) with one antenna (1.5GHz or 2.6GHz), realized from the previous studies from the I2M and already published [1-3]. The results taken from this work from the reflected waves, show that the effect of wood anisotropy is significant on the variation of relative permittivity with moisture content on wood sample and that is in good agreement with the previous results [3-6]. As related to the direct waves, a small

  8. Evaluation of Radiation Processed Polymers as Materials for Agricultural Purposes. Chapter 8

    International Nuclear Information System (INIS)

    inhibitory activity against Tobacco Mosaic Virus (TMV). The highest inhibition degree was noticed when the Mw of irradiated alginate was around 5 × 104. The degree of inhibition increased with alginate concentration. On the other hand, it was noticed that degraded chitosan could control the growth of gray mold fungus that infected tomato fruits. High concentrations of degraded chitosan with an Mw range of 2–6 × 104 controlled the increase of gray mold infections and enhanced fungal decay in tomato fruit. Cross-linked fast swelling super porous hydrogels were prepared by irradiating acrylamide-based copolymers in solid and solution states using electron beam irradiation. As the Polyacrylamide/potassium polyacrylate (PAAm/PAAcK) water swellability increased, the PAAm in the copolymer and/or irradiation dose required for the cross-linking process decreased. A field evaluation of PAAm/PAAcK as super water absorbent materials for Zea maze plants revealed that PAAm/PAAcK does not cause salt buildup in the soil, possesses a high ability to absorb water, improves germination of seeds planted in sandy soil, prevents plant losses due to drought and water stress in non-irrigated areas, and increases the Zea maze plant growth and performance. Thus, such a hydrogel could be used for soil amendment to improve the growth of plants and increase their production yield. Field evaluation using polyacrylamide/Na-alginate, copolymer was performed in a range of garden plants using Faba bean and Zea maize. The growth of bean plant cultivated in a polyacrylamide/Na-alginate treated soil was higher than that of polyacrylamide treated soil or in a gel-free soil (control). (author)

  9. Accelerated method for high temperature degradation of materials for power plant and application of fracture mechanics approach for its evaluation

    International Nuclear Information System (INIS)

    A new procedure for express-ageing of structural materials in gaseous hydrogen is developed. It is based on the facilitating effect of hydrogen on the diffusion processes, which causes metal structure degradation. Two methods for in-laboratory-ageing of materials are proposed. The first one consists in the exposure of the specimen to the simultaneous action of the tensile load, high temperature and the gaseous hydrogen. The second method is based on the thermo-cycling of materials in the hydrogen environment. The range of thermo-cycle is based on the information about the service of a specific power plant steam pipeline. The structural changes in the material after the in-laboratory-ageing during the 40 hours are similar to the ones, which have taken place in the material after 140-190 thousands service hours. To evaluate the damage of material qualitatively, the parameters of fatigue crack growth were used. The achieved test results have shown, that the application of the above parameters to the evaluation of the material damage level can be useful. These methods can be applied as the express-technique for the residual life time evaluation. (orig.)

  10. Electrolyte optimization and electrode material evaluation for the vanadium redox battery

    Science.gov (United States)

    Kazacos, Michael

    1990-05-01

    The preparation of the electrolyte for the all vanadium redox flow battery was investigated using both chemical and electrolytic reduction of V2O5 powder. Oxalic acid and SO2 reduction were found to be unsuitable as only the V(IV) state could be produced directly. With suspended powder hydrolysis, however, vanadium sulphate of any oxidation state, in this case 50 percent V(IV) plus 50 percent V(III) in sulphuric acid can readily be prepared from V2O5 powder, thus allowing a significant reduction in the cost of the vanadium battery electrolyte. Results from conductivity and electrolyte stability tests at elevated temperature have led to modification of the electrolyte composition for the vanadium redox cell, from the 2 M V plus 2 M H2SO4, originally employed, to the use of 3 M H2SO4, much higher energy efficiencies and greater electrolyte stability was demonstrated with the 3 M H2SO4 supporting electrolyte. Spectroscopy and electrolyte conductivity were demonstrated as suitable techniques for state-of-charge monitoring. A number of electrode materials were also evaluated and a Toray graphite bonded to a carbon plastic electrode was selected for further prototype development. Energy efficiencies of between 83 and 86 percent obtained for a current density of 30 mA/sq cm for a temperature range of 5 to 45 C, and between 0 and 100 percent state-of-charge. A wide range of construction materials was tested for long term stability in the vanadium redox electrolyte.

  11. The Evaluation of Material Properties of Low-pH Cement Grout for the Application of Cementitious Materials to Deep Radioactive Waste Repository Tunnels

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Jin Seop; Kwon, S. K.; Cho, W. J.; Kim, G. W

    2009-12-15

    Considering the current construction technology and research status of deep repository tunnels for radioactive waste disposal, it is inevitable to use cementitious materials in spite of serious concern about their long-term environmental stability. Thus, it is an emerging task to develop low pH cementitious materials. This study reviews the state of the technology on low pH cements developed in Sweden, Switzerland, France, and Japan as well as in Finland which is constructing a real deep repository site for high-level radioactive waste disposal. Considering the physical and chemical stability of bentonite which acts as a buffer material, a low pH cement limits to pH {<=}11 and pozzolan-type admixtures are used to lower the pH of cement. To attain this pH requirement, silica fume, which is one of the most promising admixtures, should occupy at least 40 wt% of total dry materials in cement and the Ca/Si ratio should be maintained below 0.8 in cement. Additionally, selective super-plasticizer needs to be used because a high amount of water is demanded from the use of a large amount of silica fume. In this report, the state of the technology on application of cementitious materials to deep repository tunnels for radioactive waste disposal was analysed. And the material properties of low-pH and high-pH cement grouts were evaluated base on the grout recipes of ONKALO in Finlan.

  12. Development and evaluation of novel sensing materials for detecting food contamination

    Science.gov (United States)

    Sankaran, Sindhuja

    Rapid detection of food-borne volatile organic compounds (VOCs) such as organic acids and alcohols released by bacterial pathogens is being used as an indicator for detecting bacterial contamination in food by our research group. One of our current research thrusts is to develop novel sensors that will be sensitive to specific compounds (at low operating temperature) associated with food safety. This study evaluates two approaches employed to develop sensors for detecting acid and alcohols at low concentrations. Chemoresistive and piezoelectric sensors were developed based on metal oxides and olfactory system based biomaterials, respectively to detect acetic acid, butanol, 3-methyl-1-butanol, 1-pentanol, and 1-hexanol. The metal oxide based sensors were developed by the sol-gel method. A zinc oxide (ZnO) sensor was found to be sensitive to acetic acid with lower detection limit ranging from 13-40 ppm. The three-layered dip-coated gold electrode based ZnO sensors had a LDL of 18 ppm for acetic acid detection. The ZnO-iron oxide (Fe2O3) based nanocomposite sensors were developed to detect butanol operating at 100°C. The 5% Fe/Zn mole ratio based ZnO-Fe2O3 nanocomposite sensors had high correlation coefficients (>0.90) of calibration curves, low butanol LDLs (26 +/- 7 ppm), and lower variation among the sensor responses. The ZnO and ZnO-Fe2O3 nanocomposite sensors showed potential to detect acetic acid and butanol at low concentrations, respectively at 100°C. QCM based olfactory sensors were developed from olfactory receptor and odorant binding protein based sequences to detect low concentrations of acetic acid and alcohols (3-methyl-1-butanol and 1-hexanol), respectively. The average LDLs for acetic acid as well as alcohols detection of the QCM sensors were 0.80. Finally, a computational simulation based peptide sequences was designed from olfactory receptors and evaluated as sensor material for the detection of alcohols at low concentrations. The results indicated

  13. Evaluation of the local temperature of conductive filaments in resistive switching materials.

    Science.gov (United States)

    Yalon, E; Cohen, S; Gavrilov, A; Ritter, D

    2012-11-23

    The resistive switching effect in metal oxides and other dielectric materials is among the leading future non-volatile memory technologies. Resistive switching is widely ascribed to the formation and rupture of conductive filaments in the oxide, which are generated by temperature-enhanced nano-scale ion migration or other thermal effects. In spite of the central role of the local filament temperature on the switching effect, as well as on the conduction and reliability physics, no measurement methods of the filament temperature are yet available. In this work, we report on a method for evaluating the conducting filament temperature, using a metal-insulator-semiconductor bipolar transistor structure. The filament temperature is obtained by analyzing the thermal excitation rate of electrons from the filament Fermi level into the conduction band of a p-type semiconductor electrode. Measurements were carried out to obtain the conductive filament temperature in hafnia at varying ambient temperatures in the range of 3-300 K. Significant Joule heating of the filament was observed across the entire measured ambient temperature range. The extracted temperatures provide physical insight into the resistive switching effect. PMID:23093285

  14. Evaluation of bionanocomposites as packaging material on properties of soft white cheese during storage period.

    Science.gov (United States)

    Youssef, Ahmed M; El-Sayed, Samah M; Salama, Heba H; El-Sayed, Hoda S; Dufresne, A

    2015-11-01

    Novel bionanocomposites based on chitosan/poly(vinyl alcohol)/titanium nanoparticles (CS/PVA/TiO2 nanocomposite) were prepared and used as packaging materials for soft white cheese. The prepared bionanocomposites were characterized using XRD, SEM, TEM and FT-IR. The CS/PVA/TiO2 bionanocomposites exhibited good mechanical properties. Furthermore, the obtained bionanocomposites exhibited superior antibacterial activity against gram positive (Staphylococcus aureus), gram negative (Pseudomonas aeruginosa, Escherichia coli) bacteria and fungi (Candidia albicans). The soft white cheese was manufactured and packaged within the CS/PVA/TiO2 nanocomposite films and stored at 7 °C for 30 days. The color, rheological and chemical properties of cheese were evaluated, also the influence of CS/PVA/TiO2 bionanocomposites on microbiological analysis of soft white cheese was assessed, the results indicated that the total bacterial counts, mold & yeast and coliform decreased with the increasing storage period and disappeared at the end of storage period compared with control. Consequently, CS/PVA/TiO2 bionanocomposite can be used in food packaging applications. PMID:26256350

  15. Evaluation of gum damar as a novel microencapsulating material for ibuprofen and diltiazem hydrochloride

    Directory of Open Access Journals (Sweden)

    Morkhade D

    2007-01-01

    Full Text Available A natural gum, damar was investigated as a novel microencapsulating material for sustained drug delivery. Microparticles were prepared by oil-in-oil emulsion solvent evaporation method. Ibuprofen and diltiazem hydrochloride were used as model drugs. Microparticles were evaluated for particle size, encapsulation efficiency and in vitro drug release kinetics. Images of the microparticles were obtained by bright field microscopy. The effect of different gum:drug ratios and solubility of drug on microparticle properties was principally investigated. Gum damar could produce discrete and spherical microparticles with both drugs. With a freely water soluble drug (diltiazem hydrochloride, gum damar produced bigger (45-50 µm and fast drug releasing microparticles with low encapsulation efficiencies (44-57%. Contrary, with a slightly water soluble drug (ibuprofen, gum damar produced small (24-33 µm microparticles with better drug encapsulation (85-91% and sustained drug delivery. The increase in gum:drug ratio showed an increase in particle size, encapsulation efficiency and decrease in drug release rate in all cases. Drug release profiles of all microparticles followed zero order kinetics. In conclusion, gum damar can be used successfully to produce discrete and spherical microparticles of ibuprofen and diltiazem hydrochloride.

  16. Evaluation of chemical properties of super stainless steel for nuclear internal materials

    Energy Technology Data Exchange (ETDEWEB)

    Park, Yong Soo [Yonsei University, Seoul (Korea); Kim, Young Sik [Andong National University, Andong (Korea)

    2002-03-01

    This work dealt with the evaluation of super stainless steels for heat exchanger tubing of internal of NPP. Experimental alloys were designed on the base of UNS S32050. SCC resistance of UNS S32050 was affected by nitrogen content of alloys and grain size. Increasing nitrogen content facilitates the formation of the planar dislocation. TT(thermal treatment at 550oC 15hrs) facilitates cross slip of dislocation and reduces the residual stress of materials and increases the grain size and enhances SCC-resistance than that of mill annealed specimen. Increasing cold rolling percent improves yield strength and ultimate tensile strength but greatly reduces the elongation. Thus, SCC resistance of cold rolled alloys is largely reduced with increasing rolling percent. Increasing Mn and N improves the SCC resistance but cold rolling over 50% reduces the resistance mainly due to the loss of mechanical properties. In 1500 psi, 315oC 10% NaOH solution, increased Ni-content of alloys improves passivation behavior in anodic polarization test and U-bend test shows cold rolling increases the mean crack propagation rate, but TT decreases the mean crack propagation rate. In ambient environment, 110oC 40% NaOH solution, SCC is a little observed in only outside of cross section and fracture mode is intergranular cracking. 73 refs., 92 figs., 4 tabs. (Author)

  17. The evaluation of hydroxyapatite (HA) coated and uncoated porous tantalum for biomedical material applications

    International Nuclear Information System (INIS)

    Porous tantalum has been used as an orthopedic implant for bone defects as it has a good corrosion resistance and fatigue behaviour properties. However, there are some reports on the rejection of porous Ta after the implantation. Those clinical cases refer to the less bioactivity of metallic-based materials. This study aims to evaluate hydroxyapatite coated and uncoated porous Tantalum in order to improve the biocompatibility of porous tantalum implant and osseointegration. Porous tantalum was used as metallic-base substrate and hydroxyapatite coating has been done using plasma-spraying technique. Scanning Electron Microscopy (SEM) and Field Emission Scanning Electron Microscopy (FESEM) techniques were utilizes to investigate the coating characteristics while Confocal Raman Microscopy to investigate the interface and image. The effect of coating to the corrosion behaviour was assessed by employing potentiodynamic polarization tests in simulated body fluid at 37±1 °C. Based on SEM and FESEM results, the morphologies as well the weight element consists in the uncoated and hydroxyapatite coated porous tantalum were revealed. The results indicated that the decrease in corrosion current density for HA coated porous Ta compared to the uncoated porous Ta. This study concluded that by coating porous tantalum with HA supports to decrease the corrosion rate of pure porous.

  18. Evaluation and redesign of manual material handling in a vaccine production centre's warehouse.

    Science.gov (United States)

    Torres, Yaniel; Viña, Silvio

    2012-01-01

    This study was conducted in a warehouse at a vaccine production centre where improvement to existing storage and working conditions were sought through the construction of a new refrigerated store section (2-8C°). Warehousing tasks were videotaped and ergonomics analysis tools were used to assess the risk of developing MSDs. Specifically, these tools were the Rapid Entire Body Assessment (REBA) and the NIOSH equation. The current plant layout was sketched and analyzed to find possible targets for improvement trough the application of general work space design and ergonomics principles. Seven of the eight postures evaluated with REBA had a total score between 8 and 10, meaning a high risk, and only one was at a medium risk level. Nine of the eleven manual material handling tasks analyzed with the NIOSH equation had a Lifting Index between 1.14 and 1.80 and two had a recommended weight limit of 0 kg, indicating a need for job redesign. Solutions included the redesign of shelves, the design of a two-step stair and a trolley with adjustable height; also, changes in work methods were proposed by introducing a two-workers lifting strategy and job rotation, and, finally, a restructuring of plant layout was completed. PMID:22317092

  19. Biodiesel feasibility study: An evaluation of material compatibility; performance; emission and engine durability

    Energy Technology Data Exchange (ETDEWEB)

    Fazal, M.A.; Haseeb, A.S.M.A.; Masjuki, H.H. [Department of Mechanical Engineering, University of Malaya, 50603 Kuala Lumpur (Malaysia)

    2011-02-15

    Biodiesel, derived from the transesterification of vegetable oils or animal fats, is composed of saturated and unsaturated long-chain fatty acid alkyl esters. In spite of having some application problems, recently it is being considered as one of the most promising alternative fuels in internal combustion engine. From scientific literatures, this paper has collected and analyzed the data on both advantages and disadvantages of biodiesel over conventional diesel. Since the aim of this study is to evaluate the biodiesel feasibility in automobiles, the first section is dedicated to materials compatibility in biodiesel as compared to that in diesel. The highest consensus is related to enhanced corrosion of automotive parts due to its compositional differences. In the subsequent sections, data on performance, emission and engine durability have been analyzed and compared. In this case, the highest consensus is found in reducing emissions as well as in increasing moving parts sticking, injector coking and filter plugging. This paper has also summarized the factors of biodiesel in contributing these technical performances. (author)

  20. Characteristic evaluation of Al2O3/CNTs hybrid materials for micro-electrical discharge machining

    Institute of Scientific and Technical Information of China (English)

    Hyun-Seok TAK; Chang-Seung HA; Ho-Jun LEE; Hyung-Woo LEE; Young-Keun JEONG; Myung-Chang KANG

    2011-01-01

    The characteristic evaluation of aluminum oxide (Al2O3)/carbon nanotubes (CNTs) hybrid composites for micro-electrical discharge machining (EDM) was described. Alumina matrix composites reinforced with CNTs were fabricated by a catalytic chemical vapor deposition method. Al2O3 composites with different CNT concentrations were synthesized. The electrical characteristic of Al2O3/CNTs composites was examined. These composites were machined by the EDM process according to the various EDM parameters, and the characteristics of machining were analyzed using field emission scanning electron microscope (FESEM). The electrical conductivity has a increasing tendency as the CNTs content is increased and has a critical point at 5% Al2O3 (volume fraction). In the machining accuracy, many tangles of CNT in Al2O3/CNTs composites cause violent spark. Thus, it causes the poor dimensional accuracy and circularity. The results show that conductivity of the materials and homogeneous distribution of CNTs in the matrix are important factors for micro-EDM of Al2O3/CNTs hybrid composites.

  1. SEQUESTRATION OF METALS IN ACTIVE CAP MATERIALS: A LABORATORY AND NUMERICAL EVALUATION

    Energy Technology Data Exchange (ETDEWEB)

    Dixon, K.; Knox, A.

    2012-02-13

    Active capping involves the use of capping materials that react with sediment contaminants to reduce their toxicity or bioavailability. Although several amendments have been proposed for use in active capping systems, little is known about their long-term ability to sequester metals. Recent research has shown that the active amendment apatite has potential application for metals contaminated sediments. The focus of this study was to evaluate the effectiveness of apatite in the sequestration of metal contaminants through the use of short-term laboratory column studies in conjunction with predictive, numerical modeling. A breakthrough column study was conducted using North Carolina apatite as the active amendment. Under saturated conditions, a spike solution containing elemental As, Cd, Co, Se, Pb, Zn, and a non-reactive tracer was injected into the column. A sand column was tested under similar conditions as a control. Effluent water samples were periodically collected from each column for chemical analysis. Relative to the non-reactive tracer, the breakthrough of each metal was substantially delayed by the apatite. Furthermore, breakthrough of each metal was substantially delayed by the apatite compared to the sand column. Finally, a simple 1-D, numerical model was created to qualitatively predict the long-term performance of apatite based on the findings from the column study. The results of the modeling showed that apatite could delay the breakthrough of some metals for hundreds of years under typical groundwater flow velocities.

  2. EVALUATION OF SAMAAR MORR (JUNCUS ACUTUS) PLANT AS RAW MATERIAL FOR PAPER MAKING

    Institute of Scientific and Technical Information of China (English)

    EssamS.A.EI-Sayed

    2004-01-01

    The potential use of Samaar Morr (JUNCUS ACUTUS) plant as fibrous material in papermaking was evaluated in this study. The chemical analysis and fibre charactersitcs of this plant were determinedfor better understanding its behaviour in papermaking. Samaar morr stalks were subjected to sulfur-free three-stage (peroxyformic acid, formic acid, peroxyformic acid) Milox process. Some conventional pulping experiments such as soda, soda-anthraquinon (S-AQ), kraft and kraft-AQ pulping in addition to two- and one-stage peroxyformic acid pulping were also carried out for comparison with the three-stage peroxyformic acid pulping method. It was found that the pulping with Milox process produces pulp with good properties compared to the pulp produced from the other methods. The physical and optical properties of different pulps were also examined. The behaviour of Milox samaar morr pulp towards bleaching withalkaline hydrogen peroxide has been investigated in presence and absence of formic acid. The results showed that the final brightness about 81.5% ISO could be achieved after 3% peroxide in two bleaching steps with formic acid treatment between the two steps.

  3. EVALUATION OF SAMAAR MORR (JUNCUS ACUTUS) PLANT AS RAW MATERIAL FOR PAPER MAKING

    Institute of Scientific and Technical Information of China (English)

    Essam S.A.El-Sayed

    2004-01-01

    The potential use of Samaar Morr (JUNCUS A CUTUS) plant as fibrous material in papermaking was evaluated in this study. The chemical analysis and fibre charactersitcs of this plant were determined for better understanding its behaviour in papermaking. Samaar morr stalks were subjected to sulfur-free three-stage (peroxyformic acid, formic acid, peroxyformic acid) Milox process. Some conventional pulping experiments such as soda,soda-anthraquinon (S-AQ), kraft and kraft-AQ pulping in addition to two- and one-stage peroxyformic acid pulping were also carried out for comparison with the three-stage peroxyformic acid pulping method. It was found that the pulping with Milox process produces pulp with good properties compared to the pulp produced from the other methods. The physical and optical properties of different pulps were also examined. The behaviour of Milox samaar morr pulp towards bleaching with alkaline hydrogen peroxide has been investigated in presence and absence of formic acid. The results showed that the final brightness about 81.5% ISO could be achieved after 3% peroxide in two bleaching steps with formic acid treatment between the two steps.

  4. Formulation and evaluation of fast dissolving tablets of cinnarizine using superdisintegrant blends and subliming material.

    Science.gov (United States)

    Basu, Biswajit; Bagadiya, Abhishek; Makwana, Sagar; Vipul, Vora; Batt, Devraj; Dharamsi, Abhay

    2011-10-01

    The aim of this investigation was to develop fast dissolving tablet of cinnarizine. A combination of super disintegrants, i.e., sodium starch glycolate (SSG) and crosscarmellose sodium (CCS) were used along with camphor as a subliming material. An optimized concentration of camphor was added to aid the porosity of the tablet. A 3(2) full factorial design was applied to investigate the combined effect of two formulation variables: Amount of SSG and CCS. Infrared (IR) spectroscopy was performed to identify the physicochemical interaction between drug and polymer. IR spectroscopy showed that there is no interaction of drug with polymer. In the present study, direct compression was used to prepare the tablets. The powder mixtures were compressed into tablet using flat face multi punch tablet machine. Camphor was sublimed from the tablet by exposing the tablet to vacuum drier at 60°C for 12 hours. All the formulations were evaluated for their characteristics such as average weight, hardness, wetting time, friability, content uniformity, dispersion time (DT), and dissolution rate. An optimized tablet formulation (F 9) was found to have good hardness of 3.30 ± 0.10 kg/cm(2), wetting time of 42.33 ± 4.04 seconds, DT of 34.67 ± 1.53 seconds, and cumulative drug release of not less than 99% in 16 minutes. PMID:22247895

  5. Seed germination bioassay using maize seeds for phytoxicity evaluation of different composted materials

    International Nuclear Information System (INIS)

    In this paper we evaluated the phytotoxicity of different composts obtained by two different composting methods using seed germination bioassay. Seeds of Zea mays were sown in 1:5 extract of composts and these were compared with the control (100% distilled water) for each type of material. Composting of herbal pharmaceutical solid waste (HPSW) was carried out using both conventional bin and pit method. HPSW was mixed separately with poultry manure, cow-manure and goat manure in three different ratios. Uncomposted and composted HPSW were tested to study the Phytotoxicity on Zea mays seed germination, after composting increase in percent germination as well as germination index (GI) values were observed in all combinations regardless, composted by pit or bin method. The results clearly showed that composting reduced Phytotoxicity. The results showed that use of completely composted organic waste reduces the phytotoxicity and is better than the use of uncomposted waste. It was found that pit method was more suitable than bin method. Herbal waste with goat manure in 1:1 ratio was found to be the most effective combination as compared to other combinations here. Germination was 100% and the germination index was 1.4 whereas uncomposted HPSW showed the lowest percent germination i.e., 77% and germination index 52.31 respectively. (author)

  6. Formulation and evaluation of fast dissolving tablets of cinnarizine using superdisintegrant blends and subliming material

    Directory of Open Access Journals (Sweden)

    Biswajit Basu

    2011-01-01

    Full Text Available The aim of this investigation was to develop fast dissolving tablet of cinnarizine. A combination of super disintegrants, i.e., sodium starch glycolate (SSG and crosscarmellose sodium (CCS were used along with camphor as a subliming material. An optimized concentration of camphor was added to aid the porosity of the tablet. A 3 2 full factorial design was applied to investigate the combined effect of two formulation variables: Amount of SSG and CCS. Infrared (IR spectroscopy was performed to identify the physicochemical interaction between drug and polymer. IR spectroscopy showed that there is no interaction of drug with polymer. In the present study, direct compression was used to prepare the tablets. The powder mixtures were compressed into tablet using flat face multi punch tablet machine. Camphor was sublimed from the tablet by exposing the tablet to vacuum drier at 60°C for 12 hours. All the formulations were evaluated for their characteristics such as average weight, hardness, wetting time, friability, content uniformity, dispersion time (DT, and dissolution rate. An optimized tablet formulation (F 9 was found to have good hardness of 3.30 ± 0.10 kg/cm 2 , wetting time of 42.33 ± 4.04 seconds, DT of 34.67 ± 1.53 seconds, and cumulative drug release of not less than 99% in 16 minutes.

  7. Development of evaluation methodology for effects of cementitious grouting materials on groundwater and rock in fractured media

    International Nuclear Information System (INIS)

    Leachates from cementitious grouting materials used for reducing water inflow are hyperalkaline and chemically reactive with the engineered barriers and host rock for geological disposal of high-level radioactive waste. Evaluation methods for long-term alteration of the fractured rock have been developed since the extent of chemical modification may influence the transport and retardation properties of radionuclides in the far field. The present study shows the current status of the development of the methodology (i.e., procedure, models, and simulation codes) for evaluating the effects of cementitious grouting materials on groundwater and rock. (author)

  8. Evaluation on materials performance of Hastelloy Alloy XR for HTTR uses-6. Tensile and creep properties of heat exchanger tube base materials and its welded-joints

    International Nuclear Information System (INIS)

    Tensile and creep properties of heat exchanger tube base materials and its welded-joints were investigated as a series of evaluation tests on Hastelloy Alloy XR heat exchanger tube and filler metal for the High Temperature Engineering Test Reactor (HTTR) components. As for tensile properties after thermal aging of base materials and welded joints, ductility was remarkably reduced at room temperature while it was raised at 950degC. On creep properties, the difference between base materials and welded joints in creep rupture strength was relatively small. Creep rupture elongation tended to decrease with increasing rupture time, and rupture elongation of welded joint had a tendency to be lower than that of base material. On the other hand, a comparison of plate with tube on high temperature tensile ductility after thermal aging was found to be higher in tube than in plate while its difference was slight at room temperature. As for creep properties, base materials and welded joints of tube had a tendency to be slightly shorter in rupture time at lower stress and long terms than those of plate. However, it is concluded that this is not problematic in practical uses from the fact that the rupture time in tube is comparable or greater than that of Hastelloy Alloy XR master curve and that it is much longer than that of design creep rupture strength =SR=. (author)

  9. Evaluation of the toxicity of radiosterilized implantable materials; Ocena wplywu sterylizacji radiacyjnej na toksycznosc wybranych materialow implantacyjnych

    Energy Technology Data Exchange (ETDEWEB)

    Lewandowska-Szumiel, M.; Kudelska, D.; Mazur, M. [Akademia Medyczna, Wroclaw (Poland); Zimek, Z. [Institute of Nuclear Chemistry and Technology, Warsaw (Poland)

    1997-12-01

    Autoclave and radiation sterilization modes of selected biomaterials and polymers were studied to evaluate the toxicity, if any, induced in the cells grown in vitro. The materials examined induced: crystalline and amorphous biocarbon, alumina, hydroxyapatite, powdered primary PP (radiation-sensitive), and PP modified with a polypropylene/ethylene or an ethylene/vinyl acetate copolymer to enhance its radiation resistance. Results showed no material to be toxic toward the cell examined. The viability of the cells cultivated in the presence of materials examined was found to remain unaffected regardless of the sterilization mode. (author). 12 refs, 3 figs.

  10. New improved method for evaluation of growth by food related fungi on biologically derived materials

    DEFF Research Database (Denmark)

    Bergenholtz, Karina P.; Nielsen, Per Væggemose

    2002-01-01

    Biologically derived materials, obtained as commercial and raw materials (Polylactate (PLA), Polyhydroxybutyrate (PHB), potato, wheat and corn starch) were tested for their ability to support fungal growth using a modified ASTM G21-96 (American Society for Testing and Materials) standard as well ...

  11. Ultrasonic non-destructive evaluation for characterisation, microdefects detection and imaging of industrial/medical based materials

    International Nuclear Information System (INIS)

    The ultrasonic non-destructive evaluation (NDE) has emerged as one of the powerful methods to characterise the materials. The recent adventure of electronics and computers lead to tremendous developments in the field of ultrasonics NDE. In the present paper an attempt has been made to characterise the industrial based materials such as semiconducting glasses, superconducting glass and glass ceramics and bio active glasses through ultrasonic NDE. The factors like surface defects, subsurface defects etc. can not be studied using the traditional ultrasonics NDT and other methods. However, microdefects detection and imaging of the above materials will give a better insight into the properties of the above materials. Therefore, the basic principle, operation and application of scanning acoustic microscopy has been discussed briefly for the NDE of microdefects detection and imaging of the materials. (author)

  12. 20th International Training Course (ITC-20) on the physical protection of nuclear facilities and materials evaluation report.

    Energy Technology Data Exchange (ETDEWEB)

    Ramirez, Amanda Ann

    2008-09-01

    The goal of this evaluation report is to provide the information necessary to improve the effectiveness of the ITC provided to the International Atomic Energy Agency Member States. This report examines ITC-20 training content, delivery methods, scheduling, and logistics. Ultimately, this report evaluates whether the course provides the knowledge and skills necessary to meet the participants needs in the protection of nuclear materials and facilities.

  13. Evaluation of conceptual flowsheets for incorporating Light Water Reactor (LWR) fuel materials in an advanced nuclear fuel cycle

    Energy Technology Data Exchange (ETDEWEB)

    Bell, J.T.; Burch, W.D.; Collins, E.D.; Forsberg, C.W.; Prince, B.E.; Bond, W.D.; Campbell, D.O.; Delene, J.G.; Mailen, J.C.

    1990-08-01

    A preliminary study by a group of experts at ORNL has generated and evaluated a number of aqueous and non-aqueous flowsheets for recovering transuranium actinides from LWR fuel for use as fuel in an LMR and, at the same time, for transmutation of the wastes to less hazardous materials. The need for proliferation resistance was a consideration in the flowsheets. The current state of development of the flowsheets was evaluated and recommendations for additional study were made. 3 refs., 6 figs.

  14. Evaluation of adsorption of uranium from aqueous solution using biochar materials

    Energy Technology Data Exchange (ETDEWEB)

    Correa, Wagner Clayton; Guilhen, Sabine Neusatz; Ortiz, Nilce; Fungaro, Denise Alves, E-mail: wcorrea@ipen.br, E-mail: snguilhen@ipen.br, E-mail: notriz@ipen.br, E-mail: dfungaro@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2015-07-01

    Uranium is present in the environment as a result of leaching from natural deposits and activities associated with nuclear fuel, copper mining, uranium mining, milling industry, etc. For the purpose of protecting ecosystem stability and public health, it is crucial to eliminate uranium from aqueous solutions before they are discharged into the environment. Various technologies have been used for removing U(VI) ions from aqueous systems. Among these methods, adsorption has been applied in wastewater because of simple operation procedure and high removal efficiency. Brazil is the largest producer of charcoal in the world, with nearly half of the woody biomass harvested for energy in Brazil being transformed into charcoal. Biochar exhibits a great potential as an adsorbent because of favorable physical/chemical surface characteristics. The objective of this work was to evaluate the adsorption potential of biochar materials prepared from pyrolysis of Bamboo (CBM), Eucalyptus (CEM) and Macauba (CMA) nuts for the removal of uranium from solutions. Adsorption experiments were carried out by a batch technique. Equilibrium adsorption experiments were performed by shaking a known amount of biochar material with 100 mL of U(VI) solution in Erlenmeyer flasks in a shaker at 120 rpm and room temperature (25 deg C) for 24 h. The adsorbent was separated by centrifugation from the solution. The U(VI) concentration remaining in the supernatant solution was determined using inductively coupled plasma optical emission spectrometry (ICP-OES). The influences of different experimental parameters such as solution pH and bioadsorbent dose on adsorption were investigated. The highest uranium adsorption capacity were obtained at pH 3.0 and 16 g/L biomass dosage for CMA, pH 3.0 and 12 g/L biomass dosage for CBM and pH 2.0 and 10 g/L biomass dosage for CEM. The results demonstrated that the biomass derived char can be used as a low-cost adsorbent for removal of uranium from wastewater. (author)

  15. Evaluation of iron phosphate (III) as reactive material for removal of uranium in water

    International Nuclear Information System (INIS)

    The levels of toxic metals in the atmosphere are topic of growing interest. This has provoked that the legislation is stricter, for that that the industry and centers of investigation has worried and busy of to look for and to develop more effective methods for the control of the contamination, with the purpose of being inside this levels. The phosphate compounds are being investigated for the removal of pollutants of the water and soil. In this work, it was synthesized to the ferric phosphate in a simple way in the laboratory, obtaining high grade of purity and yield. The characterization of this product was in a physicochemical way and of surface, through diverse analytical techniques. In the first place, the physicochemical characterization was carried out for Scanning Electron Microscopy of High Vacuum, X-ray diffraction, Infrared Spectroscopy with Fourier Transform, and Thermal gravimetric Analysis, the surface characterization was carried out for analysis of the surface area, determination of the isoelectric point by potentiometric and of mass titrations. The previous techniques allowed to identify the ferric phosphate synthesized as a compound amorphous beige color, with a relationship of atoms Fe:1, P:1, O:4, which showed connections P-O and went stable to changes of temperature. The surface area it was of 21 g / m2, the isoelectric point corresponded to a p H of 1.5, which coincided so much by potentiometric like by mass titration. The number of active sites was of 106 sites /nm2. After the characterization of the ferric phosphate the compound was evaluated as reactive material for the removal of uranyl ions through sorption tests. The kinetics of hydration showed that the product requires of 24 hours to saturate the sites capable of to be hydrated. The sorption kinetics required 22 hours of contact to reach the maximum sorption of uranyl ions for the ferric phosphate. The sorption isotherms showed that not significant difference exists when using 0.05, 0

  16. Evaluation of performance of materials used in the ceramic materials restoration of the Plaza de España (Sevilla

    Directory of Open Access Journals (Sweden)

    Alejandre Sánchez, F. J.

    2005-06-01

    Full Text Available Different commercial mortars and stuecos used to cold restore the glazing on deteriorated tile in Seville s Plaza de España were tested for performance and durability. Five types of samples were applied to ceramic bisques and subsequently coloured and protected with resins. The samples were subjected to accelerated weathering consisting in salt crystallization, temperature and relative humidity cycles and ultraviolet radiation. Durability was assessed by visually comparing the effect of salt crystallization, determining the colour parameters with colourimetry and measuring adherence and capillary water absorption. The results obtained were used to differentiate the materials tested in two respects: stucco and protective resin performance under the environmental conditions prevailing in the Plaza de España on the one hand and colour stability on the other.

    En el presente trabajo se estudia el comportamiento y la durabilidad de diferentes morteros y estucos comerciales que se han utilizado para restituir enfrío las pérdidas de vidriado en azulejos deteriorados de la Plaza de España (Sevilla. Para ello se han preparado 5 tipos de muestras que se han aplicado sobre bizcochos cerámicos y que posteriormente se han coloreado y protegido con resinas. Las muestras se han sometido a ensayos de alteración acelerada: cristalización de sales, ciclos de temperatura y humedad relativa, y radiación ultravioleta. La evaluación de la durabilidad se ha llevado a cabo mediante la comparación visual del efecto de cristalización de las sales, la determinación de los parámetros de color mediante colorimetría, de la adherencia y de la absorción de agua por capilaridad. Los resultados obtenidos, permiten realizar una diferenciación en dos aspectos, por un lado, el comportamiento del estuco y su protección para soportar las condiciones medioambientales de la Plaza de España, y, por otro, la estabilidad de los diferentes colores.

  17. Evaluation of the e-Learning material developed by EMERALD and EMIT for diagnostic imaging and radiotherapy.

    Science.gov (United States)

    Aitken, Victoria; Tabakov, Slavik

    2005-09-01

    Two Leonardo projects, EMERALD and EMIT, have developed in a partnershipof university and hospital departments (the consortia) e-Learning materials in X-ray diagnostic radiology, nuclear medicine, radiotherapy, ultrasound and magnetic resonance imaging for medical physics graduates and other healthcare professionals. These e-Learning materials are described in a separate paper in this issue. To assess the effectiveness and relevance of the e-Learning material, a series of evaluations by student users groups plus experts in medical physics education and training were undertaken. The students, with backgrounds in physics and clinical ultrasound, reviewed the e-Learning material using an evaluation form developed by the consortia. The student feedback was favourable with students commenting that their level of knowledge had increased having completed the tasks. Areas identified for development were a reduction in text volume and an increase in the time allowed for completion of some tasks. The feedback from the experts was positive with an overall appreciation of the value of the learning material as a resource for students in medical physics field across Europe and identified other disciplines in which the access to the learning material could be useful contribution to their learning. Suggestions made for improvements ranged from grading the tasks into basic and advanced topics to increasing the interactive nature of the material. These early evaluation of the e-Learning material look promising and provide a framework for further developments in the field. Insight into users and providers views is important if developers are to provide relevant and worthwhile educational learning opportunities. PMID:16087384

  18. Tanks 18 And 19-F Structural Flowable Grout Fill Material Evaluation And Recommendations

    International Nuclear Information System (INIS)

    Cementitious grout will be used to close Tanks 18-F and 19-F. The functions of the grout are to: 1) physically stabilize the final landfill by filling the empty volume in the tanks with a non-compressible material; 2) provide a barrier for inadvertent intrusion into the tank; 3) reduce contaminant mobility by a) limiting the hydraulic conductivity of the closed tank and b) reducing contact between the residual waste and infiltrating water; and 4) providing an alkaline, chemically reducing environment in the closed tank to control speciation and solubility of selected radionuclides. The objective of this work was to identify a single (all-in-one) grout to stabilize and isolate the residual radionuclides in the tank, provide structural stability of the closed tank and serve as an inadvertent intruder barrier. This work was requested by V. A. Chander, High Level Waste (HLW) Tank Engineering, in HLW-TTR-2011-008. The complete task scope is provided in the Task Technical and QA Plan, SRNL-RP-2011-00587 Revision 0. The specific objectives of this task were to: 1) Identify new admixtures and dosages for formulating a zero bleed flowable tank fill material selected by HLW Tank Closure Project personnel based on earlier tank fill studies performed in 2007. The chemical admixtures used for adjusting the flow properties needed to be updated because the original admixture products are no longer available. Also, the sources of cement and fly ash have changed, and Portland cements currently available contain up to 5 wt. % limestone (calcium carbonate). 2) Prepare and evaluate the placement, compressive strength, and thermal properties of the selected formulation with new admixture dosages. 3) Identify opportunities for improving the mix selected by HLW Closure Project personnel and prepare and evaluate two potentially improved zero bleed flowable fill design concepts; one based on the reactor fill grout and the other based on a shrinkage compensating flowable fill mix design. 4

  19. Tanks 18 And 19-F Structural Flowable Grout Fill Material Evaluation And Recommendations

    International Nuclear Information System (INIS)

    Cementitious grout will be used to close Tanks 18-F and 19-F. The functions of the grout are to: (1) physically stabilize the final landfill by filling the empty volume in the tanks with a non compressible material; (2) provide a barrier for inadvertent intrusion into the tank; (3) reduce contaminant mobility by (a) limiting the hydraulic conductivity of the closed tank and (b) reducing contact between the residual waste and infiltrating water; and (4) providing an alkaline, chemically reducing environment in the closed tank to control speciation and solubility of selected radionuclides. The objective of this work was to identify a single (all-in-one) grout to stabilize and isolate the residual radionuclides in the tank, provide structural stability of the closed tank and serve as an inadvertent intruder barrier. This work was requested by V. A. Chander, High Level Waste (HLW) Tank Engineering, in HLW-TTR-2011-008. The complete task scope is provided in the Task Technical and QA Plan, SRNL-RP-2011-00587 Revision 0. The specific objectives of this task were to: (1) Identify new admixtures and dosages for formulating a zero bleed flowable tank fill material selected by HLW Tank Closure Project personnel based on earlier tank fill studies performed in 2007. The chemical admixtures used for adjusting the flow properties needed to be updated because the original admixture products are no longer available. Also, the sources of cement and fly ash have changed, and Portland cements currently available contain up to 5 wt. % limestone (calcium carbonate). (2) Prepare and evaluate the placement, compressive strength, and thermal properties of the selected formulation with new admixture dosages. (3) Identify opportunities for improving the mix selected by HLW Closure Project personnel and prepare and evaluate two potentially improved zero bleed flowable fill design concepts; one based on the reactor fill grout and the other based on a shrinkage compensating flowable fill mix

  20. TANKS 18 AND 19-F STRUCTURAL FLOWABLE GROUT FILL MATERIAL EVALUATION AND RECOMMENDATIONS

    Energy Technology Data Exchange (ETDEWEB)

    Stefanko, D.; Langton, C.

    2011-11-01

    Cementitious grout will be used to close Tanks 18-F and 19-F. The functions of the grout are to: (1) physically stabilize the final landfill by filling the empty volume in the tanks with a non compressible material; (2) provide a barrier for inadvertent intrusion into the tank; (3) reduce contaminant mobility by (a) limiting the hydraulic conductivity of the closed tank and (b) reducing contact between the residual waste and infiltrating water; and (4) providing an alkaline, chemically reducing environment in the closed tank to control speciation and solubility of selected radionuclides. The objective of this work was to identify a single (all-in-one) grout to stabilize and isolate the residual radionuclides in the tank, provide structural stability of the closed tank and serve as an inadvertent intruder barrier. This work was requested by V. A. Chander, High Level Waste (HLW) Tank Engineering, in HLW-TTR-2011-008. The complete task scope is provided in the Task Technical and QA Plan, SRNL-RP-2011-00587 Revision 0. The specific objectives of this task were to: (1) Identify new admixtures and dosages for formulating a zero bleed flowable tank fill material selected by HLW Tank Closure Project personnel based on earlier tank fill studies performed in 2007. The chemical admixtures used for adjusting the flow properties needed to be updated because the original admixture products are no longer available. Also, the sources of cement and fly ash have changed, and Portland cements currently available contain up to 5 wt. % limestone (calcium carbonate). (2) Prepare and evaluate the placement, compressive strength, and thermal properties of the selected formulation with new admixture dosages. (3) Identify opportunities for improving the mix selected by HLW Closure Project personnel and prepare and evaluate two potentially improved zero bleed flowable fill design concepts; one based on the reactor fill grout and the other based on a shrinkage compensating flowable fill mix

  1. Tanks 18 And 19-F Structural Flowable Grout Fill Material Evaluation And Recommendations

    Energy Technology Data Exchange (ETDEWEB)

    Langton, C. A.; Stefanko, D. B.

    2013-04-23

    Cementitious grout will be used to close Tanks 18-F and 19-F. The functions of the grout are to: 1) physically stabilize the final landfill by filling the empty volume in the tanks with a non-compressible material; 2) provide a barrier for inadvertent intrusion into the tank; 3) reduce contaminant mobility by a) limiting the hydraulic conductivity of the closed tank and b) reducing contact between the residual waste and infiltrating water; and 4) providing an alkaline, chemically reducing environment in the closed tank to control speciation and solubility of selected radionuclides. The objective of this work was to identify a single (all-in-one) grout to stabilize and isolate the residual radionuclides in the tank, provide structural stability of the closed tank and serve as an inadvertent intruder barrier. This work was requested by V. A. Chander, High Level Waste (HLW) Tank Engineering, in HLW-TTR-2011-008. The complete task scope is provided in the Task Technical and QA Plan, SRNL-RP-2011-00587 Revision 0. The specific objectives of this task were to: 1) Identify new admixtures and dosages for formulating a zero bleed flowable tank fill material selected by HLW Tank Closure Project personnel based on earlier tank fill studies performed in 2007. The chemical admixtures used for adjusting the flow properties needed to be updated because the original admixture products are no longer available. Also, the sources of cement and fly ash have changed, and Portland cements currently available contain up to 5 wt. % limestone (calcium carbonate). 2) Prepare and evaluate the placement, compressive strength, and thermal properties of the selected formulation with new admixture dosages. 3) Identify opportunities for improving the mix selected by HLW Closure Project personnel and prepare and evaluate two potentially improved zero bleed flowable fill design concepts; one based on the reactor fill grout and the other based on a shrinkage compensating flowable fill mix design. 4

  2. Evaluation of mechanical properties of structural materials by small punch test

    International Nuclear Information System (INIS)

    Small punch(SP) test method was applied to evaluate the mechanical properties of structural steels for nuclear power plant components. The yield strength of several nuclear structural steels was estimated based on the detailed examination of initial deformation characteristics during the SP test. In addition, the ductile-brittle transition temperature(DBTT) of heat-treated SA508 Cl. 3 nuclear pressure vessel steel was correlated with the temperature dependence of the SP characteristics. Finally, the SP test was performed on duplex stainless steel to estimate the extent of thermal aging embrittlement. Initial deformation behavior during small punch test was investigated using two SP specimen sizes, 10x10x0.5 mm3 and 10x10x0.25 mm3 by finite element analysis and by experiments with heat-treated SA508 Cl. 3 and 12Cr steel. The increase of specimen thickness resulted in a deviation from the initial linearity of the load-displacement curve at higher load. The deviation was attributed to different causes, namely loss of the constraint by the surrounding material and radial propagation of plastic bending deformation for 0.5 and 0.25mm specimens, respectively. The causes for the transition of deformation mode were identical irrespective of material strength and work-hardening rate in the range of yield strength about 400 to 900 MPa. Based on the invariance of the deformation mode, a distinct linear relationship between the load at the deviation from the linearity and the yield stress was predicted by finite element analysis and compared with the experimental results. The validity of using the SP test for the DBTT evaluation of SA508 Cl. 3 steel was investigated. It was clearly observed that the variation of load-displacement curves with temperature was accompanied by the change of fracture mode and appearance. The temperature dependence of the SP characteristics well described the toughness degradation which was made by heat treatment. The SP energy was selected to

  3. A Market Model for Evaluating Technologies That Impact Critical-Material Intensity

    Science.gov (United States)

    Iyer, Ananth V.; Vedantam, Aditya

    2016-04-01

    A recent Critical Materials Strategy report highlighted the supply chain risk associated with neodymium and dysprosium, which are used in the manufacturing of neodymium-iron-boron permanent magnets (PM). In response, the Critical Materials Institute is developing innovative strategies to increase and diversify primary production, develop substitutes, reduce material intensity and recycle critical materials. Our goal in this paper is to propose an economic model to quantify the impact of one of these strategies, material intensity reduction. Technologies that reduce material intensity impact the economics of magnet manufacturing in multiple ways because of: (1) the lower quantity of critical material required per unit PM, (2) more efficient use of limited supply, and (3) the potential impact on manufacturing cost. However, the net benefit of these technologies to a magnet manufacturer is an outcome of an internal production decision subject to market demand characteristics, availability and resource constraints. Our contribution in this paper shows how a manufacturer's production economics moves from a region of being supply-constrained, to a region enabling the market optimal production quantity, to a region being constrained by resources other than critical materials, as the critical material intensity changes. Key insights for engineers and material scientists are: (1) material intensity reduction can have a significant market impact, (2) benefits to manufacturers are non-linear in the material intensity reduction, (3) there exists a threshold value for material intensity reduction that can be calculated for any target PM application, and (4) there is value for new intellectual property (IP) when existing manufacturing technology is IP-protected.

  4. A Market Model for Evaluating Technologies That Impact Critical-Material Intensity

    Science.gov (United States)

    Iyer, Ananth V.; Vedantam, Aditya

    2016-07-01

    A recent Critical Materials Strategy report highlighted the supply chain risk associated with neodymium and dysprosium, which are used in the manufacturing of neodymium-iron-boron permanent magnets (PM). In response, the Critical Materials Institute is developing innovative strategies to increase and diversify primary production, develop substitutes, reduce material intensity and recycle critical materials. Our goal in this paper is to propose an economic model to quantify the impact of one of these strategies, material intensity reduction. Technologies that reduce material intensity impact the economics of magnet manufacturing in multiple ways because of: (1) the lower quantity of critical material required per unit PM, (2) more efficient use of limited supply, and (3) the potential impact on manufacturing cost. However, the net benefit of these technologies to a magnet manufacturer is an outcome of an internal production decision subject to market demand characteristics, availability and resource constraints. Our contribution in this paper shows how a manufacturer's production economics moves from a region of being supply-constrained, to a region enabling the market optimal production quantity, to a region being constrained by resources other than critical materials, as the critical material intensity changes. Key insights for engineers and material scientists are: (1) material intensity reduction can have a significant market impact, (2) benefits to manufacturers are non-linear in the material intensity reduction, (3) there exists a threshold value for material intensity reduction that can be calculated for any target PM application, and (4) there is value for new intellectual property (IP) when existing manufacturing technology is IP-protected.

  5. Adaptation of adhesive post and cores to dentin after in vitro occlusal loading: evaluation of post material influence

    OpenAIRE

    Dietschi, Didier; Ardu, Stefano; Rossier-Gerber, Anne; Krejci, Ivo

    2006-01-01

    Fatigue resistance of post and cores is critical to the long term behavior of restored nonvital teeth. The purpose of this in vitro trial was to evaluate the influence of the post material's physical properties on the adaptation of adhesive post and core restorations after cyclic mechanical loading.

  6. Engineering evaluation/cost analysis: Waste Pit Area storm water runoff control, Feed Materials Production Center, Fernald, Ohio

    International Nuclear Information System (INIS)

    This report evaluates remedial action alternatives at the Feed Materials production Center in response to the need to contain contaminated storm water runoff. The storm water is being contaminated as it falls over a radioactive/chemical waste pit which contains uranium contaminated wastes. Alternatives considered include no action, surface capping, surface capping with lateral drainage, runoff collection and treatment, and source removal

  7. Preliminary Evaluation of Commercial Off the Shelf (COTS) Packing Materials for Flight Medication Dispenser (FMD) Technology Development

    Science.gov (United States)

    Du, B.; Daniels, V.; Crady, C.; Putcha, L.

    2011-01-01

    This slide presentation reviews preliminary results of the program to evaluate Commercial Off the Shelf (COTS) packaging materials for pharmaceutical stability. The need for improved packaging is due to possible changes in chemical and/or physical properties of the drugs, which cause reported reduced potency and/or altered bioavailability and decreased efficacy.

  8. SOC-DS computer code provides tool for design evaluation of homogeneous two-material nuclear shield

    Science.gov (United States)

    Disney, R. K.; Ricks, L. O.

    1967-01-01

    SOC-DS Code /Shield Optimization Code-Direc Search/, selects a nuclear shield material of optimum volume, weight, or cost to meet the requirments of a given radiation dose rate or energy transmission constraint. It is applicable to evaluating neutron and gamma ray shields for all nuclear reactors.

  9. Evaluation of Co-precipitation Processes for the Synthesis of Mixed-Oxide Fuel Feedstock Materials

    Energy Technology Data Exchange (ETDEWEB)

    Collins, Emory D [ORNL; Voit, Stewart L [ORNL; Vedder, Raymond James [ORNL

    2011-06-01

    The focus of this report is the evaluation of various co-precipitation processes for use in the synthesis of mixed oxide feedstock powders for the Ceramic Fuels Technology Area within the Fuels Cycle R&D (FCR&D) Program's Advanced Fuels Campaign. The evaluation will include a comparison with standard mechanical mixing of dry powders and as well as other co-conversion methods. The end result will be the down selection of a preferred sequence of co-precipitation process for the preparation of nuclear fuel feedstock materials to be used for comparison with other feedstock preparation methods. A review of the literature was done to identify potential nitrate-to-oxide co-conversion processes which have been applied to mixtures of uranium and plutonium to achieve recycle fuel homogeneity. Recent studies have begun to study the options for co-converting all of the plutonium and neptunium recovered from used nuclear fuels, together with appropriate portions of recovered uranium to produce the desired mixed oxide recycle fuel. The addition of recycled uranium will help reduce the safeguard attractiveness level and improve proliferation resistance of the recycled fuel. The inclusion of neptunium is primarily driven by its chemical similarity to plutonium, thus enabling a simple quick path to recycle. For recycle fuel to thermal-spectrum light water reactors (LWRs), the uranium concentration can be {approx}90% (wt.), and for fast spectrum reactors, the uranium concentration can typically exceed 70% (wt.). However, some of the co-conversion/recycle fuel fabrication processes being developed utilize a two-step process to reach the desired uranium concentration. In these processes, a 50-50 'master-mix' MOX powder is produced by the co-conversion process, and the uranium concentration is adjusted to the desired level for MOX fuel recycle by powder blending (milling) the 'master-mix' with depleted uranium oxide. In general, parameters that must be

  10. A model-based method for the characterisation of stress in magnetic materials using eddy current non-destructive evaluation

    International Nuclear Information System (INIS)

    A precise knowledge of the distribution of internal stresses in materials is key to the prediction of magnetic and mechanical performance and lifetime of many industrial devices. This is the reason why many efforts have been made to develop and enhance the techniques for the non-destructive evaluation of stress. In the case of magnetic materials, the use of eddy current (EC) techniques is a promising pathway to stress evaluation. The principle is based on the significant changes in magnetic permeability of magnetic materials subjected to mechanical stress. These modifications of magnetic permeability affect in turn the signal obtained from an EC probe inspecting the material. From this principle, a numerical tool is proposed in this paper to predict the EC signal obtained from a material subjected to stress. This numerical tool is a combination of a 3D finite element approach with a magneto-mechanical constitutive law describing the effect of stress on the magnetic permeability. The model provides the variations of impedance of an EC probe as a function of stress. An experimental setup in which a magnetic material subjected to a tension stress is inspected using EC techniques is tailored in order to validate the model. A very good agreement is found between experimental and modelling results. For the Iron-Cobalt alloy tested in this study, it is shown that a uniaxial tensile stress can be detected with an error lower than 3 MPa in the range from 0 to 100 MPa. (paper)

  11. Evaluating the Flow Processes in Ultrafine-Grained Materials at Elevated Temperatures

    OpenAIRE

    Megumi Kawasaki; Terence G. Langdon

    2013-01-01

    When polycrystalline materials are tested in tension at elevated temperatures, the flow mechanisms depend upon various parameters including the temperature of testing, the applied stress and the material grain size. The plotting of deformation mechanism maps is a procedure used widely in displaying and interpreting the creep properties of conventional coarse-grained metals but there have been few attempts to date to use this same procedure for ultrafine-grained and nanocrystalline materials p...

  12. Geomorphological approach to surficial material evaluation in the Serang River Basin Kulonprogo, Yogyakarta, Indonesia

    Directory of Open Access Journals (Sweden)

    Sutikno .

    2013-07-01

    Among landform units in the studied area which contains a large amount of the materials are: natural levees, river terraces, river bed and hill foot slopes. Generally, the river bed materials decrease in grain size downstreams and increase in sphericity and roundness coefficient. In some cross sections a reversal was found to the general tendency. This situation might be due to human activities for getting material for construction. Due to human activities some environmental impacts occur.

  13. In vitro evaluation of fracture strength of zirconia restoration veneered with various ceramic materials

    OpenAIRE

    Choi, Yu-Sung; Kim, Sung-Hun; Lee, Jai-Bong; Han, Jung-Suk; Yeo, In-Sung

    2012-01-01

    PURPOSE Fracture of the veneering material of zirconia restorations frequently occurs in clinical situations. The purpose of this in vitro study was to compare the fracture strengths of zirconia crowns veneered with various ceramic materials by various techniques. MATERIALS AND METHODS A 1.2 mm, 360° chamfer preparation and occlusal reduction of 2 mm were performed on a first mandibular molar, and 45 model dies were fabricated in a titanium alloy by CAD/CAM system. Forty-five zirconia copings...

  14. Evaluation for cell affinity of the composite material containing carbon nanotubes

    Institute of Scientific and Technical Information of China (English)

    KANG Shizhao; WAN Yuqing; YAN Huijuan; BEI Jianzhong; WANG Chen; WANG Shenguo; WANG Chunru; WAN Lijun; BAI Chunli

    2004-01-01

    The composite material of poly-(L-lactide) (PLLA) and carbon nanotubes (CNTs) were prepared. Its surface morphologies and property were worked out by using atomic force microscopy (AFM) and contact angle measurement. Moreover, the prime cytocompatibility was used to investigate the biocompatibility of the composite material containing CNTs and the effects of CNTs on one aspect of cell function, cell affinity. The results obtained indicate that the composite material of PLLA and CNTs possesses good biocompatibility for both the 3T3 fibroblasts and Oct-1 osteoblast-like cells. The addition of CNTs will greatly affect cell affinity of the material, which may be disadvantage for the cell adhesion.

  15. Evaluation of Proactive Management Issues Associated with Materials Aging in Light Water Reactors

    International Nuclear Information System (INIS)

    A Proactive Materials Degradation Management (PMDM) project has been carried out at the Fracture Research Institute (FRI), Tohoku University for 4 years, as a part of a Nuclear Industries Safety Agency (NISA) project that was formed in 2007 to define an Aging Management Program that addresses unexpected structural material failures in Light Water Reactors (LWRs). Such a program required, therefore, the development of a life prediction capability for specific combinations of degradation modes, structural materials, and reactor components. In this paper, the research subjects needed to predict quantitatively aging degradation phenomena in LWR structural materials are introduced. (author)

  16. Standard practice for slow strain rate testing to evaluate the susceptibility of metallic materials to environmentally assisted cracking

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2000-01-01

    1.1 This practice covers procedures for the design, preparation, and use of axially loaded, tension test specimens and fatigue pre-cracked (fracture mechanics) specimens for use in slow strain rate (SSR) tests to investigate the resistance of metallic materials to environmentally assisted cracking (EAC). While some investigators utilize SSR test techniques in combination with cyclic or fatigue loading, no attempt has been made to incorporate such techniques into this practice. 1.2 Slow strain rate testing is applicable to the evaluation of a wide variety of metallic materials in test environments which simulate aqueous, nonaqueous, and gaseous service environments over a wide range of temperatures and pressures that may cause EAC of susceptible materials. 1.3 The primary use of this practice is to furnish accepted procedures for the accelerated testing of the resistance of metallic materials to EAC under various environmental conditions. In many cases, the initiation of EAC is accelerated through the applic...

  17. Clinical and radiographic evaluation of pulpectomies using three root canal filling materials: An in-vivo study

    Directory of Open Access Journals (Sweden)

    Ramar K

    2010-03-01

    Full Text Available Various root canal filling materials are used to preserve a pulpally involved carious primary tooth. But there is no single material so far available to fulfill all the requirements of an ideal root canal filling material for a primary tooth. Hence this study was undertaken to evaluate clinically and radiographically the efficacy of three obturating materials - Calcium hydroxide with Iodoform (METAPEX, Zinc Oxide Eugenol with Iodoform (RC FILL and Zinc Oxide Eugenol and Calcium hydroxide with Iodoform (ENDOFLAS for a period of 9 months. Results show ENDOFLAS gave an overall success rate of 95.1%, METAPEX - 90.5% and RC FILL - 84.7%. In our study, we conclude that ENDOFLAS, a mixture of Zinc Oxide Eugenol and Calcium hydroxide with Iodoform fulfills most of the required properties of an ideal root canal filling for primary teeth.

  18. Evaluating woody material transport and deposition in alpine rivers and deducing risk mitigation approaches

    Science.gov (United States)

    Mazzorana, B.; Zischg, A.; Hübl, J.; Largiader, A.

    2009-04-01

    The impact levels of recent flashflood events in Switzerland and Western Austria in 2005 have significantly been accentuated by a considerable amount of transported woody material. As a consequence, either protection measures or bridges suffered considerable damage. Furthermore, cross-sectional obstructions due to woody material entrapment caused unexpected floodplain inundations resulting in severe damage to elements at risk. Until now, these woody material transport phenomena are neither sufficiently taken into account nor systematically considered, leading to a decrease in prediction accuracy during the procedure of hazard mapping. To close this gap, a procedure is proposed that (1) allows for the estimation of woody material recruitment from wood covered bankslopes and floodplains within the perimeter of the considered extreme flood event; and (2) permits the analysis of, the disposition for woody material entrainment and transport to selected critical configurations along the channel. The proposed procedure had been implemented into an ArcGIS-environment and provided indications for potential accentuation of flood hazards due to the transport of woody material. Results from a case study suggested the general applicability of the concept. The computational results can be used to devise effective risk mitigation strategies that comprise: (1) selective woody material volume reduction within the source areas, (2) thinning measures to increase the elasticity of the forest structure, (3) preventive interception of transported woody material and (4) redesign of the critical configurations.

  19. Development and Evaluation of Educational Materials for Embedded Systems to Increase the Learning Motivation

    Science.gov (United States)

    Koshino, Makoto; Kojima, Yuki; Kanedera, Noboru

    2013-01-01

    Educational materials of embedded systems are currently used in many educational institutions. However, they have difficulties in arousing the interest of students. One of the reasons is that a poor CPU (central processing unit), which has been loaded in the current materials, cannot execute the multimedia processing. In order to make the…

  20. Evaluating Multimedia Library Materials: Clues from Hand-Printed Books and Art History.

    Science.gov (United States)

    Nicholls, Paul; Ridley, Jacquline

    1997-01-01

    Apart from archival print collections, digital multimedia materials will be the primary form of library resources in the future. Argues that all published materials, print or electronic, are subject to analytical and critical examination. Describes art historian Erwin Panofsky's "Circulus Methodicus," a method of iconological analysis, that could…

  1. Evaluation of using ferrofluid as an interface material for a field-reversible thermal connector

    Science.gov (United States)

    Yousif, Ahmed S.

    conduction heat transfer path. Having started as a student design competition named RevCon Challenge, work was performed to evaluate the use of new field-reversible thermal connectors. The new design proposed by the University of Missouri utilized oil based iron nanoparticles, commonly known as a ferrofluid, as a thermal interface material. By using a liquid type of interface material the channel gap can be reduced to a few micrometers, within machining tolerances, and heat can be dissipated off both sides of the card. The addition of nanoparticles improves the effective thermal conductivity of base fluid. The use of iron nanoparticles allows magnets to be used to hold the fluid in place, so the electronic cards may be easily inserted and removed while keeping the ferrofluid in the cold block channel. The ferrofluid-based design which was investigated has shown lower thermal resistance than the current wedgelock design. These results open the door for further development of electronic cards by using higher heat emitting components without compromising the simplicity of attaching/detaching cards from cooling plates.

  2. Tanks 18 And 19-F Equipment Grout Fill Material Evaluation And Recommendations

    International Nuclear Information System (INIS)

    The United States Department of Energy (US DOE) intends to remove Tanks 18-F and 19-F at the Savannah River Site (SRS) from service. The high-level waste (HLW) tanks have been isolated from the F-area Tank Farm (FTF) facilities and will be filled with cementitious grout for the purpose of: (1) physically stabilizing the empty volumes in the tanks, (2) limiting/eliminating vertical pathways from the surface to residual waste on the bottom of the tanks, (3) providing an intruder barrier, and (4) providing an alkaline, chemical reducing environment within the closure boundary to limit solubility of residual radionuclides. Bulk waste and heel waste removal equipment will remain in Tanks 18-F and 19-F when the tanks are closed. This equipment includes: mixer pumps, transfer pumps, transfer jets, equipment support masts, sampling masts and dip tube assemblies. The current Tank 18-F and 19-F closure strategy is to grout the internal void spaces in this equipment to eliminate fast vertical pathways and slow water infiltration to the residual material on the tank floor. This report documents the results of laboratory testing performed to identify a grout formulation for filling the abandoned equipment in Tanks 18-F and 19-F. The objective of this work was to formulate a flowable grout for filling internal voids of equipment that will remain in Tanks 18-F and 19-F during the final closures. This work was requested by V. A. Chander, Tank Farm Closure Engineering, in HLW-TTR-2011-008. The scope for this task is provided in the Task Technical and Quality Assurance Plan (TTQAP), SRNL-RP-2011-00587. The specific objectives of this task were to: (1) Prepare and evaluate the SRR cooling coil grout identified in WSRC-STI-2008-00298 per the TTR for this work. The cooling coil grout is a mixture of BASF MasterFlow(regsign) 816 cable grout (67.67 wt. %), Grade 100 ground granulated blast furnace slag (7.52 wt. %) and water (24.81 wt. %); (2) Identify equipment grout placement and

  3. TANKS 18 AND 19-F EQUIPMENT GROUT FILL MATERIAL EVALUATION AND RECOMMENDATIONS

    Energy Technology Data Exchange (ETDEWEB)

    Stefanko, D.; Langton, C.

    2011-12-15

    The United States Department of Energy (US DOE) intends to remove Tanks 18-F and 19-F at the Savannah River Site (SRS) from service. The high-level waste (HLW) tanks have been isolated from the F-area Tank Farm (FTF) facilities and will be filled with cementitious grout for the purpose of: (1) physically stabilizing the empty volumes in the tanks, (2) limiting/eliminating vertical pathways from the surface to residual waste on the bottom of the tanks, (3) providing an intruder barrier, and (4) providing an alkaline, chemical reducing environment within the closure boundary to limit solubility of residual radionuclides. Bulk waste and heel waste removal equipment will remain in Tanks 18-F and 19-F when the tanks are closed. This equipment includes: mixer pumps, transfer pumps, transfer jets, equipment support masts, sampling masts and dip tube assemblies. The current Tank 18-F and 19-F closure strategy is to grout the internal void spaces in this equipment to eliminate fast vertical pathways and slow water infiltration to the residual material on the tank floor. This report documents the results of laboratory testing performed to identify a grout formulation for filling the abandoned equipment in Tanks 18-F and 19-F. The objective of this work was to formulate a flowable grout for filling internal voids of equipment that will remain in Tanks 18-F and 19-F during the final closures. This work was requested by V. A. Chander, Tank Farm Closure Engineering, in HLW-TTR-2011-008. The scope for this task is provided in the Task Technical and Quality Assurance Plan (TTQAP), SRNL-RP-2011-00587. The specific objectives of this task were to: (1) Prepare and evaluate the SRR cooling coil grout identified in WSRC-STI-2008-00298 per the TTR for this work. The cooling coil grout is a mixture of BASF MasterFlow{reg_sign} 816 cable grout (67.67 wt. %), Grade 100 ground granulated blast furnace slag (7.52 wt. %) and water (24.81 wt. %); (2) Identify equipment grout placement and

  4. Damage evaluation system for materials used in fossil thermal power plants

    Energy Technology Data Exchange (ETDEWEB)

    Okamura, Hiroyuki [Science Univ. of Tokyo (Japan); Sakai, Shinsuke [Tokyo Univ. (Japan); Tomita, Akira [Japan Power Engineering and Inspection Corp., Tokyo (Japan); Koyama, Teruo [Babcock Hitachi K.K., Tokyo (Japan); Sakurai, Shigeo; Kawasaki, Yoshiya [Hitachi Ltd., Ibaraki (Japan)

    1998-11-01

    The summary of this research paper is as follows: The fundamental design of the damage evaluation system is carried out based on the basic concept. Prototype systems for boilers and turbines have been constructed: (a) Boiler: (I) Evaluation part: Outer surface of the primary pendant superheater tube; (II) Damage mode: Creep; (III) Damage evaluation method: Hardness measurement method; (b) Turbine: (I) Evaluation part: Inner surface at the center bore of high pressure turbine rotor; (II) Damage mode: Creep; (III) Damage evaluation method: Electric potential method. (orig./MM)

  5. Evaluation of multidensity orthotic materials used in footwear for patients with diabetes.

    Science.gov (United States)

    Foto, J G; Birke, J A

    1998-12-01

    Selected combinations of multidensity orthotic materials were tested under simulated walking conditions found in the forefoot of diabetic patients. Materials were compared for therapeutic effectiveness by their stress/strain properties and dynamic compression set. Results showed that all of the multidensity materials experienced losses in performance throughout the testing period of 100,000 cycles, with the greatest losses occurring within the first 10,000 cycles. Of the materials tested, Poron + Plastazote #2 and Spenco + Microcel Puff Lite had the highest dynamic material strain and the lowest dynamic compression set over 100,000 cycles. In comparison, these are better multidensity combinations than the others tested to use as therapeutic orthoses in footwear for diabetic patients. PMID:9872471

  6. Evaluation of radiation effects on dental enamel hardness and dental restorative materials

    International Nuclear Information System (INIS)

    This research presents the results of the microhardness of human dental enamel and of the following dental restorative materials: three dental porcelains - Ceramco II, Finesse and Noritake, and two resin restorative materials - Artglass and Targis, for materials submitted to different times of irradiation at the IEA-R1m nuclear reactor under a thermal neutron flux of 1012n cm-2.s-1 . The results obtained indicated that there is a decrease of the surface microhardness when the enamel is irradiated for 1 h and when dental materials are irradiated for 3 h. However, enamels irradiated for 30 min. did not show significant change of their surface hardness. Therefore, the selection of irradiation time is an important factor to be considered when irradiated teeth or dental materials are used in the investigations of their properties. (author)

  7. Evaluating the flow processes in ultrafine-grained materials at elevated temperatures

    Directory of Open Access Journals (Sweden)

    Megumi Kawasaki

    2013-06-01

    Full Text Available When polycrystalline materials are tested in tension at elevated temperatures, the flow mechanisms depend upon various parameters including the temperature of testing, the applied stress and the material grain size. The plotting of deformation mechanism maps is a procedure used widely in displaying and interpreting the creep properties of conventional coarse-grained metals but there have been few attempts to date to use this same procedure for ultrafine-grained and nanocrystalline materials produced through the application of severe plastic deformation (SPD. This report examines the potential for using deformation mechanism mapping for materials processed by SPD and presents examples for materials processed using equal-channel angular pressing and high-pressure torsion.

  8. Evaluation of chitosan quaternary ammonium salt-modified resin denture base material.

    Science.gov (United States)

    Song, Rong; Zhong, Zhaohua; Lin, Lexun

    2016-04-01

    Chitosan quaternary ammonium salt displays good antioxidant and antibacterial characteristics and it shows appreciable solubility in water. When added to the traditional denture material to form a resin base, it could promote good oral health by improving the oral environment. In this study, chitosan quaternary ammonium salt was added to the denture material following two different methods. After three months of immersion in artificial saliva, the specimens were tested for tensile strength and were scanned by electron microscope. The murine fibroblast cytotoxicity and antibacterial properties were also tested. The result showed no significant differences in the tensile strength and in the proliferation of murine L929 fibroblast cells. The two structures of chitosan quaternary ammonium salt-modified denture material had different degrees of corrosion resistance and antimicrobial properties. These results indicate that chitosan quaternary ammonium salt-modified resin denture base material has the potential to become a new generation oral denture composite material.

  9. Evaluating Material Flammability in Microgravity and Martian Gravity Compared to the NASA Standard Normal Gravity Test

    Science.gov (United States)

    Oslon, Sandra. L.; Ferkul, Paul

    2012-01-01

    Drop tower tests are conducted at Martian gravity to determine the flammability of three materials compared to previous tests in other normal gravity and reduced gravity environments. The comparison is made with consideration of a modified NASA standard test protocol. Material flammability limits in the different gravity and flow environments are tabulated to determine the factor of safety associated with normal gravity flammability screening. Previous testing at microgravity and Lunar gravity indicated that some materials burned to lower oxygen concentrations in low gravity than in normal gravity, although the low g extinction limit criteria are not the same as 1g due to time constraints in drop testing. Similarly, the data presented in this paper for Martian gravity suggest that there is a gravity level below Earth s at which materials burn more readily than on Earth. If proven for more materials, this may indicate the need to include a factor of safety on 1g flammability limits.

  10. Ecological evaluation of proposed dredged material from the John F. Baldwin Ship Channel: Phase 3 -- biological testing

    Energy Technology Data Exchange (ETDEWEB)

    Kohn, N.P.; Karle, L.M.; Pinza, M.R.; Mayhew, H.L.; White, P.J.; Gruendell, B.D.; Word, J.Q. [Battelle/Marine Sciences Lab., Sequim, WA (United States)

    1993-10-01

    The John F. Baldwin Ship Channel is a 28-mile-long portion of the San Francisco Bay to Stockton Ship Channel, the primary shipping lane through San Francisco Bay and Delta. The San Francisco District of the US Army Corps of Engineers (USACE) is responsible for construction of the John F. Baldwin Ship Channel, which is authorized to be deepened to a project depth of {minus}45 ft relative to mean lower low water (MLLW). Approximately 8.5 million cubic yards (mcy) of sediment will be removed from the channel to reach this project depth. The USACE requested Battelle/Marine Sciences Laboratory (MSL) to conduct testing for ocean disposal under the guidelines in Evaluation of Dredged Material Proposed for Ocean Disposal-Testing Manual (EPA/USACE 1991). This testing manual contains a tiered evaluation approach developed specifically for ocean disposal of dredged material at a selected site. In this study, John F. Baldwin Ship Channel sediments were evaluated under the Tier III (biological) testing guidance, which is considered to be highly stringent and protective of the environment. The Tier III guidance for ocean disposal testing requires tests of water column effects, (following dredged material disposal), deposited sediment toxicity, and bioaccumulation of contaminants from deposited sediment (dredged material).

  11. Field Evaluation of the Potential for Creep in Thermoplastic Encapsulant Materials: Preprint

    Energy Technology Data Exchange (ETDEWEB)

    Kempe, M. D.; Miller, D. C.; Wohlgemuth, J.; Kurtz, S. R.; Moseley, J. M.; Shah, Q.; Tamizhmani, G.; Sakurai, K.; Inoue, M.; Doi, T.; Masuda, A.; Samuels, S. L.; Vanderpan, C. E.

    2012-06-01

    There has been recent interest in the use of thermoplastic encapsulant materials in photovoltaic modules to replace chemically crosslinked materials, e.g., ethylene-vinyl acetate. The related motivations include the desire to: reduce lamination time or temperature; use less moisture-permeable materials; use materials with better corrosion characteristics or with improved electrical resistance. However, the use of any thermoplastic material in a high-temperature environment raises safety and performance concerns, as the standardized tests currently do not expose the modules to temperatures in excess of 85 degrees C, though fielded modules may experience temperatures above 100 degrees C. Here we constructed eight pairs of crystalline-silicon modules and eight pairs of glass/encapsulation/glass thin-film mock modules using different encapsulant materials of which only two were designed to chemically crosslink. One module set was exposed outdoors with insulation on the back side in Arizona in the summer, and an identical set was exposed in environmental chambers. High precision creep measurements (+/- 20 um) and performance measurements indicate that despite many of these polymeric materials being in the melt state during outdoor deployment, very little creep was seen because of their high viscosity, temperature heterogeneity across the modules, and the formation of chemical crosslinks in many of the encapsulants as they aged. In the case of the crystalline silicon modules, the physical restraint of the backsheet reduced the creep further.

  12. Hardness to toughness relationship on WC-Co tool gradient materials evaluated by Palmqvist method

    Directory of Open Access Journals (Sweden)

    G. Matula

    2010-06-01

    Full Text Available Purpose: Development of a new generation tool materials on the basis of M2 high speed-steel reinforced with the carbides. Application of powder injection moulding as a manufacturing method gives the possibility to produce these materials in a mass scale with relative low cost of production.Design/methodology/approach: Powder Injection Moulding, solvent debinding, sintering, thermogravimetric analysis, microstructure examination, porosity examination,Findings: To manufacture the proposed new tool materials was used powder injection moulding processes.It was found out based on the investigations carried out that the powder injection moulding method is suitable for fabrication of M2 high speed-steel reinforced with the carbides. The main advantage of the presented experimental tool materials is the wide sintering window being only about 5°C oftentimes in case of the high-speed steels; whereas, it is about 40°C for the investigated material.Practical implications: Application of powder metallurgy and especially powder injection moulding to manufacturing of high speed-steel reinforced with the carbides gives the possibility to obtain tool materials with the relative high ductility characteristic of steel and high hardness and wear resistance typical for cemented carbides.Originality/value: The powder injection moulding gives the possibility to fabricate carbide alloyed composite which, with their structure and mechanical properties, fill the gap in tool materials between the high-speed steels and cemented carbides.

  13. Evaluation of the Elastic Properties of Thirteen Silicone Interocclusal Recording Materials

    Science.gov (United States)

    Zietek, Marek

    2016-01-01

    Background. Addition silicones are popular as dental impression materials and are used in bite registration procedures. Objective. This study aimed to compare the postsetting elasticities and other mechanical properties of thirteen addition silicone interocclusal recording materials. Materials and Methods. The following materials were investigated: Colorbite D, Futar D, Genie Bite, Jet Blue Bite fast, Memoreg 2, O-Bite, Occlufast Rock, Omni-Bite Plus, Regidur i, Registrado X-tra, Regofix transparent, StoneBite, and Variotime Bite. Thirty specimens of each material were tested. The elasticities and strengths of the materials were measured with a universal testing machine, and computer software was used to determine the E-moduli, ultimate tensile strengths, and ultimate elongations of the specimens. Results. The results were subjected to statistical analysis using the Kruskal-Wallis test (p ≤ 0.05). The statistics revealed that the mean E-modulus values varied significantly across the materials (p = 0.000) and were highest for the StoneBite and Registrado X-tra and lowest for the Regofix transparent. The ultimate tensile strengths were highest for the Regofix transparent and Registrado X-tra (p = 0.000) and lowest for the Jet Blue Bite fast and Memoreg 2 (p = 0.000). The elongation percentages at the point of breaking varied significantly across the materials (p = 0.000); the lowest value was observed for the StoneBite, whereas the Regofix transparent nearly doubled original length. Conclusions. The authors concluded that materials with the high E-moduli and great ultimate tensile strengths may be most useful clinically. Registrado X-tra and StoneBite best met these criteria. PMID:27747239

  14. Metrological aspects related to stable isotope reference materials: the traceability concept and uncertainty evaluation scheme supporting every day practice.

    Science.gov (United States)

    Assonov, Sergey; Groening, Manfred; Fajgelj, Ales

    2016-04-01

    The worldwide metrological comparability of stable isotope measurement results is presently achieved by linking them to the conventional delta scales. Delta scales are realized by scale defining reference materials, most of them being supplied by the IAEA (examples are VSMOW2 & SLAP2). In fact, these reference materials are artefacts, characterized by a network of laboratories using the current best measurement practice. In reality any measurement result is linked to the scale via reference materials (RMs) in use. Any RMs is traceable to the highest-level RMs which define the scale; this is valid not only for international RMs (mostly secondary RMs like IAEA-CH-7, NBS22) but for any lab standard calibrated by users. This is a basic of measurement traceability. The traceability scheme allows addressing both the comparability and long-term compatibility of measurement results. Correspondingly, the uncertainty of any measurement result has to be propagated up to the scale level. The uncertainty evaluation should include (i) the uncertainty of the RMs in use; (ii) the analytical uncertainty of the materials used in calibration runs performed at the user laboratory; (iii) the reproducibility on results obtained on sample material; (iv) the uncertainty of corrections applied (memory, drift, etc). Besides these, there may be other uncertainty components of to be considered. The presentation will illustrate the metrological concepts involved (comparability, traceability etc) and give a generic scheme for the uncertainty evaluation.

  15. A prospective clinical evaluation of electronically mixed polyvinyl siloxane impression materials: results from the prosthetic "SuperStudy"--a consumer evaluation.

    Science.gov (United States)

    Kugel, G; Swift, E J; Sorensen, J A; Tucker, J H; Dunne, J T

    1999-01-01

    Polyvinyl siloxane (PVS) impression materials incorporating a polyether carbosilane wetting agent and mixed with an electronic mixing system (Pentamix) were clinically compared with traditionally delivered (i.e., automixed) PVS impression materials during routine use by 1,505 general and specialized dental practitioners evaluating more than 30,000 impressions. Each study participant selected 20 patients and used standard tooth-preparation procedures appropriate to the therapy required, supplied specific data on each case, and ultimately evaluated the marginal detail, fit, and success of the final restorations. The areas requiring evaluation upon completion of the final restorations were ranked between "excellent," "good," "poor," and "remake needed," among users of the PVS materials with the electronic mixing system. About 80% of the respondents rated the Pentamix system as easier to mix and deliver than the gun or hand-mixed systems and two thirds said it was faster to mix. The system also received high scores for hygienic delivery, ease of mixing, and clean-up.

  16. Synthesis and processing of intelligent cost-effective structures phase II (SPICES II): smart materials aircraft applications evaluation

    Science.gov (United States)

    Dunne, James P.; Jacobs, Steven W.; Baumann, Erwin W.

    1998-06-01

    The second phase of the synthesis and processing of intelligent cost effective structures (SPICES II) program sought to identify high payoff areas for both naval and aerospace military systems and to evaluate military systems and to evaluate the benefits of smart materials incorporation based on their ability to redefine the mission scenario of the candidate platforms in their respective theaters of operation. The SPICES II consortium, consisting of The Boeing Company, Electric Boat Corporation, United Technologies Research Center, and Pennsylvania State University, surveyed the state-of-the-art in smart structures and evaluated potential applications to military aircraft, marine and propulsion systems components and missions. Eleven baseline platforms comprising a wide variety of missions were chosen for evaluation. Each platform was examined in its field of operation for areas which can be improved using smart materials insertion. Over 250 smart materials applications were proposed to enhance the platforms. The applications were examined and, when possible, quantitatively analyzed for their effect on mission performance. The applications were then ranked for payoff, risk, and time frame for development and demonstration. Details of the efforts made in the SPICES II program pertaining to smart structure applications on military and transport aircraft will be presented. A brief discussion of the core technologies will be followed by presentation of the criteria used in ranking each application. Thereafter, a selection of the higher ranking proposed concepts are presented in detail.

  17. A trans-well-based cellular model for the rapid pre-evaluation of tympanic membrane repair materials.

    Science.gov (United States)

    Hung, Shih-Han; Su, Chin-Hui; Tseng, How

    2016-08-01

    It is important to have a standardized tympanic membrane (TM) perforation platform to evaluate the various myringoplasty materials that have been studied and developed extensively during recent years. However, currently there are no cellular models specifically designed for this purpose, and animal models remain unsatisfactory. The purpose of this study is to propose an inexpensive, readily available, well-controlled, and easy-to-create cellular model as a substitute for use in the evaluation of TM repairing materials. A trans-well model was created using a cell culture insert with a round hole created at the center of the polycarbonate membrane. HaCaT cells were cultured on the fenestrated culture insert, and the desired myringoplasty graft was placed at the center of the window for one week and observed by fluorescent microscopy under vital staining. Under this cellular model, there was notable migration of HaCaT cells onto the positive control graft (rabbit fascia), while only a few cell clusters were observed on the negative control graft (paper). Model validation showed that the cell migration ratio for the PLLA + 1% hyaluronic acid (HA) graft is significantly higher than using myringoplasty paper, poly L-lactide (PLLA), or PLLA + 0.5% HA (p < 0.05). This trans-well-based cellular model might be a useful pre-evaluation platform for the evaluation of TM repairing materials. The model is inexpensive, readily available, easy to create, and standardized for use. PMID:26335291

  18. Uses and evaluation methods of potential hydrogen permeation barriers for nuclear reactor materials

    International Nuclear Information System (INIS)

    This report summarizes results on the use of coatings as hydrogen permeation barriers on nuclear reactor component materials. Two classes of base materials were considered, exothermic hydrogen absorbers and endothermic hydrogen absorbers. The results of the tests indicate that substantial reductions in the amount of hydrogen absorbed by a metal can be achieved through the use of hydrogen permeation barrier coatings. Gold was determined to provide an effective hydrogen permeation barrier on Zr-2-1/2 Nb pressure tube material. Tin was determined to be a suitable hydrogen permeation barrier when applied on AISI 410 stainless steel and iron. Both gas phase and electrochemical permeation techniques were used to determine hydrogen permeabilities through coatings and base materials

  19. The Cryogenic Impact Resistant Evaluation of Filament Wound Materials for Use in Composite Pressure Vessels Project

    Data.gov (United States)

    National Aeronautics and Space Administration — HyPerComp Engineering Inc. (HEI) and Utah State University (USU) propose to develop technology for lightweight composite materials for use in composite structures...

  20. Evaluation of the effect of various beverages and food material on the color stability of provisional materials - An in vitro study

    Directory of Open Access Journals (Sweden)

    Gaurav Gupta

    2011-01-01

    Full Text Available Aim: This study evaluated the color stability of four provisional materials: 1 Poly-methyl methacrylates (DPI; 2 Bis-acryl composite (ProtempTM II - 3M ESPE; 3 Bis-acryl composite (Systemp; c and b - Ivoclar Vivadent and 4 Light polymerized composite resin (Revotek LC- GC. Materials and Methods: The color and color difference of each specimen after immersion in different staining solutions i.e. 1 tea and artificial saliva, 2 coffee and artificial saliva, 3 Pepsi and artificial saliva, 4 turmeric solution and artificial saliva was measured using reflectance spectrophotometer with CIELAB system before immersion and after immersion at 2, 5 ,7 , 10 and 15 days. Results: Revotek LC- GC (light polymerized composite resin was found to be the most color stable provisional restorative material followed by Protemp II (Bis-acryl composite, Systemp (Bis-acryl composite and DPI (Methylmethacrylate resin. Turmeric solution had the maximum staining potential followed by coffee, tea and Pepsi.

  1. Evaluation of the effect of various beverages and food material on the color stability of provisional materials – An in vitro study

    Science.gov (United States)

    Gupta, Gaurav; Gupta, Tina

    2011-01-01

    Aim: This study evaluated the color stability of four provisional materials: 1) Poly-methyl methacrylates (DPI); 2) Bis-acryl composite (ProtempTM II – 3M ESPE); 3) Bis-acryl composite (Systemp® c and b – Ivoclar Vivadent) and 4) Light polymerized composite resin (Revotek LC- GC). Materials and Methods: The color and color difference of each specimen after immersion in different staining solutions i.e. 1) tea and artificial saliva, 2) coffee and artificial saliva, 3) Pepsi and artificial saliva, 4) turmeric solution and artificial saliva was measured using reflectance spectrophotometer with CIELAB system before immersion and after immersion at 2, 5 ,7 , 10 and 15 days. Results: Revotek LC- GC (light polymerized composite resin) was found to be the most color stable provisional restorative material followed by Protemp II (Bis-acryl composite), Systemp (Bis-acryl composite) and DPI (Methylmethacrylate resin). Turmeric solution had the maximum staining potential followed by coffee, tea and Pepsi. PMID:22025835

  2. Evaluation of natural colonisation of cementitious materials: Effect of bioreceptivity and environmental conditions

    OpenAIRE

    Manso Blanco, Sandra; Calvo-Torrás, María Angeles; De Belie, Nele; Segura Pérez, Ignacio; Aguado de Cea, Antonio

    2015-01-01

    Incorporation of living organisms, such as photosynthetic organisms, on the structure envelope has become a priority in the area of architecture and construction due to aesthetical, economic and ecological advantages. Important research efforts are made to achieve further improvements, such as for the development of cementitious materials with an enhanced bioreceptivity to stimulate biological growth. Previously, the study of the bioreceptivity of cementitious materials has been carried out m...

  3. Evaluating the chemical compatibility of potential substrate materials for Bi-Sr-Ca-Cu-O films

    International Nuclear Information System (INIS)

    Potential substrate and buffer layer materials for Bi2Sr2CaCu2Ox (BSCCO) were surveyed using bulk ceramic processing techniques. Of the materials tested, only Ag was inert with respect to BSCCO. MgO slightly degrades the superconducting onset temperature and volume fraction. LaGaO3 may be a feasible ceramic substrate for BSCCO, although some reaction appears to occur

  4. Pulmonary bone cement embolism: CT angiographic evaluation with material decomposition using gemstone special imaging

    Energy Technology Data Exchange (ETDEWEB)

    Huh, Sun; Lee, Heon [Dept. of Radiology, Soonchunhyang University Hospital Bucheon, Bucheon (Korea, Republic of)

    2014-08-15

    We report a case of pulmonary bone cement embolism in a female who presented with dyspnea following multiple sessions of vertebroplasty. She underwent spectral CT pulmonary angiography and the diagnosis was made based on enhanced visualization of radiopaque cement material in the pulmonary arteries and a corresponding decrease in the parenchymal iodine content. Here, we describe the CT angiography findings of bone cement embolism with special emphasis on the potential benefits of spectral imaging, providing additional information on the material composition.

  5. Evaluation method of multiaxial low cycle fatigue life for cubic single crystal material

    Institute of Scientific and Technical Information of China (English)

    CHEN Jiping; DING Zhiping

    2007-01-01

    The coupling effect of normal stress and shear stress on orthotropic materials happens when applied loading deflects from the directions of the principal axes of the material coordinate system.By taking account of the coupling effects,formulas of equivalent stress and strain for cubic single crystal materials are cited.Using the equivalent strain and equivalent stress for such material and a variable k,which is introduced to express the effect of asymmetrical cyclic loading on fatigue life,a low cycle fatigue (LCF) life prediction model for such material in multiaxial stress starts is proposed.On the basis of the yield criterion and constitutive model of cubic single crystal materials,a subroutine to calculate the thermo elastic-plastic stress-strain of the material on an ANSYS platform was developed.The cyclic stress-strain of DD3 notched specimens under asymmetrical loading at 680℃ was analyzed.Low cycle fatigue test data of the single crystal nickel-based superalloy are used to fit the different parameters of the power law with multiple linear regression analysis.The equivalent stress and strain for a cubic single crystal material as failure parameters have the largest correlation coefficient.A power law exists between k and the failure cycle.The model was validated with LCF test data of CMSX-2 and DD3 single crystal nickel-based superalloys.All the test data fall into the factor of 2.5 for CMSX-2 hollow cylinder specimens and 2.0 scatter band for DD3 notched specimens,respectively.

  6. Hardness to toughness relationship on WC-Co tool gradient materials evaluated by Palmqvist method

    OpenAIRE

    G. Matula

    2010-01-01

    Purpose: Development of a new generation tool materials on the basis of M2 high speed-steel reinforced with the carbides. Application of powder injection moulding as a manufacturing method gives the possibility to produce these materials in a mass scale with relative low cost of production.Design/methodology/approach: Powder Injection Moulding, solvent debinding, sintering, thermogravimetric analysis, microstructure examination, porosity examination,Findings: To manufacture the proposed new t...

  7. A NEW PORTABLE INSTRUMENT TO EVALUATE SOFT FLOORING MATERIALS IN DAIRY COW HOUSING

    OpenAIRE

    Paolo Liberati

    2012-01-01

    The improvement of flooring materials performance on animal health and welfare requires the support of reliable testing techniques. This is particularly relevant with the synthetic soft coverings used for walking areas since the friction coefficient is not only dependent on the surface characteristics, but also on the penetration of the animal hoof into the material. The paper presents the functioning of a new instrument capable of reproducing more closely the real interaction between the flo...

  8. Evaluation of Lead Equivalence Thickness Measurement for Radiation Shielding Materials Used in Diagnostic Radiology

    International Nuclear Information System (INIS)

    Verification of lead equivalence thickness of radiation room and shielding material such as personal protective clothing are crucial to ensure that they fulfill their task in protecting patient and personnel as well as the member of public from ionizing radiation. The radiation room or shielding materials need to be verified according to Ministry of Health (MOH) requirements comply with a current standard. The thickness of the shielding materials is determined using direct comparison between the attenuation of X-ray or gamma ray by the shielding materials and high purity lead sheets (99.99 %). Currently Americium-241 is used to measure the thickness of the shielding materials for diagnostic X-ray room due to the gamma energy of 59 keV which is adequate to measure the thickness of 2 mmPb. However, the uncertainties of thickness getting higher for a thicker shielding materials due to so called a build-up factor. Various sizes of collimator and stronger radiation source were used to reduce the build-up factor and improve the accuracy of the lead equivalence thickness. From the measurement the accuracy of the thickness were increased when using a narrow beam and a stronger radiation source. (author)

  9. Re-evaluation of the use of low activation materials in waste management strategies for fusion

    International Nuclear Information System (INIS)

    The world fusion programs have had a long goal that fusion power stations should produce only low level waste and thus not pose a burden for the future generations. However, the environmental impact of waste material is determined not only by the level of activation, but also the total volume of activated material. Since a tokamak power plant is large, the potential to generate a correspondingly large volume of activated material exists. The adoption of low activation materials, while important for reducing the radiotoxicity of the most active components, should be done as part of a strategy that also minimizes the volume of waste material that might be categorized as radioactive, even if lower in level. In this paper we examine different fusion blanket and shield designs in terms of their ability to limit the activation of the large vessel/ex-vessel components (e.g. vacuum vessel, magnets) and we identify the trends that allow improved in-vessel shielding to result in reduced vessel/ex-vessel activation. Recycling and clearance are options for reducing the volume of radioactive waste in a fusion power plant. Thus, the performance of typical fusion power plant designs with respect to recycling and clearance criteria are also assessed, to show the potential for improvement in waste volume reduction by careful selection of materials' combinations. We discuss the impact of these results on fusion waste strategies and on the development of fusion power in the future

  10. Evaluation of magnetostrictive composite coated fabric as a fragment barrier material

    Science.gov (United States)

    Son, Kwon Joong; Fahrenthold, Eric P.

    2012-10-01

    Over the last decade a surge in fragment barrier research has led to investigation of numerous materials and material augmentations in the attempt to improve the ballistic performance of systems designed to protect personnel, vehicles or infrastructure from impact and blast loads. One widely studied material augmentation approach is the use of coatings, often polymers, to enhance the performance of protection systems constructed from metal, concrete, composite and fabric materials. In recent research the authors have conducted the first experimental study of the ballistic performance of fabrics coated with a magnetically responsive polymer. Zero field impact experiments on coated fabric targets showed a 61% increase in impact energy dissipation, although the coated targets were not competitive with neat fabrics on a protection per unit mass basis. Under an applied field of 110 kA m-1, the ballistic performance of the coated fabric was reduced. The reduction in performance may be attributed to a reduction in material damping and an increase in material modulus for the magnetostrictive component of the coating. Analysis of the coated fabric response to magnetic preloads suggests that coating tensile stresses and coating-fabric interface stresses induced by the applied field may also adversely affect ballistic performance.

  11. Performance demonstration and evaluation of the synergetic application of vanadium dioxide glazing and phase change material in passive buildings

    International Nuclear Information System (INIS)

    Highlights: • VO2 and PCM were combined in passive building application for the first time. • Synergetic performance of them is demonstrated in a full size room. • Synergetic application has a better performance than the solo ones. • The materials interact with each other in synergetic application. • ESI can be used to evaluate the performance of the synergetic application. - Abstract: One of the key methods to improve the energy saving performance of a building is to apply advanced materials or components to the building envelope. However, the two parts of a building’s envelope, the transparent one and the non-transparent one, are usually investigated individually by existing literature. In this study, vanadium dioxide (VO2) glazing, an advanced energy-efficient element applied to the transparent parts of the building envelope, and phase change material (PCM), a typical thermal storage material used to improve the non-transparent parts of the building envelope, were adopted simultaneously for the first time. The synergetic performance of VO2 glazing and PCM, demonstrated in a full-scale, lightweight, passive room, resulted in a significant improvement in the thermal comfort degree. The Energy Saving Index (ESI) is a simple and effective indicator that can be used to evaluate the passive application performance of a single energy-efficient material or component on a common standpoint. In this work, the index was broadened to evaluate the performance of more than one material, showing that ESI is feasible and favorable to analyze the coefficient application of several building materials and/or components. Using the ESI, the performance of the synergetic application was also compared with those of the sole materials, indicating that the synergetic application has a better performance during the cooling period. Furthermore the synergetic application involves an interplay rather than a simple combination of the energy-efficient materials. The application to

  12. Development of evaluation and prevention techniques to the dynamic damage for extending lifetime of part materials in nuclear power plants

    International Nuclear Information System (INIS)

    The goals of this project are to develop the evaluation technique of dynamic damage including devising of tester and to establish the appropriate surface modification technique for improving the performance of part materials under dynamic damage in nuclear power plants. The surface modification techniques being feasible to the components include two methods, ceramic ion plating and flame hardening. The various characteristics including mechanical properties such as hardness, adhesion, sliding wear of the surface modified materials were studied to obtain the optimum processing condition. As a result of liquid impact erosion tests, the surface modified materials (TiN coating, flame hardened 12Cr steel) showed a great improvement in resistance to erosion. The origins of erosion resistance of surface modified materials were studied by theoretical stress wave analysis, which also allows us to select the appropriate coating materials. In order to simulate the fretting wear conditions in nuclear power plants, the fretting wear tester was designed and developed. Fretting wear properties of Zirlo as a current fuel rod material were studied

  13. Evaluation of the Flexural Strength of Interim Restorative Materials in Fixed Prosthodontics

    Science.gov (United States)

    Mehrpour, Hanieh; Farjood, Ehsan; Giti, Rashin; Barfi Ghasrdashti, Alireza; Heidari, Hossein

    2016-01-01

    Statement of the Problem Mechanical properties of interim restorations are considered as important factors specially when selecting materials for long-term application or for patients with para-functional habits. Flexural strength is one of the most important components of these restorations. Purpose The purpose of this study was to compare the flexural strength of five interim restorative materials. Materials and Method Fifty identical samples sized 25×2×2-mm were made from five interim materials (TempSpan; Protemp 4, Unifast III, Trim, and Revotek LC) according to ADA specification #27. The specimens were stored in artificial saliva for 2 weeks and then thermocycled for 2500 cycles (5-55˚C). A standard three-point bending test was conducted on the specimens with a universal testing machine at a crosshead speed of 0.75mm/min. Data were analyzed by using one-way ANOVA and Tamhane’s post-hoc tests to measure the flexural strength of temporary materials. Results One of the bis-acryl resins (TempSpan) showed the highest, and the light polymerized resin (Revotek LC) showed the lowest flexural strength. The mean values of flexural strength (MPa) for the examined materials were as follow: TempSpan=120.00, Protemp 4=113.00, Unifast III=64.20, Trim= 63.73 and Revotek LC=47.16. There were significant differences between all materials except Trim and Unifast III which did not show any statistical significant difference. Conclusion Bis-acryl resins were statistically superior to traditional methacrylate and light-cured resins. Therefore, application of bis-acryl resins should be deliberated in patients with heavy occlusion and in cases that need long-term use of interim restorations. PMID:27602395

  14. Design and evaluation of carbon nanofiber and silicon materials for neural implant applications

    Science.gov (United States)

    McKenzie, Janice L.

    Reduction of glial scar tissue around central nervous system implants is necessary for improved efficacy in chronic applications. Design of materials that possess tunable properties inspired by native biological tissue and elucidation of pertinent cellular interactions with these materials was the motivation for this study. Since nanoscale carbon fibers possess the fundamental dimensional similarities to biological tissue and have attractive material properties needed for neural biomaterial implants, this present study explored cytocompatibility of these materials as well as modifications to traditionally used silicon. On silicon materials, results indicated that nanoscale surface features reduced astrocyte functions, and could be used to guide neurite extension from PC12 cells. Similarly, it was determined that astrocyte functions (key cells in glial scar tissue formation) were reduced on smaller diameter carbon fibers (125 nm or less) while PC12 neurite extension was enhanced on smaller diameter carbon fibers (100 nm or less). Further studies implicated laminin adsorption as a key mechanism in enhancing astrocyte adhesion to larger diameter fibers and at the same time encouraging neurite extension on smaller diameter fibers. Polycarbonate urethane (PCU) was then used as a matrix material for the smaller diameter carbon fibers (100 and 60 nm). These composites proved very versatile since electrical and mechanical properties as well as cell functions and directionality could be influenced by changing bulk and surface composition and features of these matrices. When these composites were modified to be smooth at the micronscale and only rough at the nanoscale, P19 cells actually submerged philopodia, extensions, or whole cells bodies beneath the PCU in order to interact with the carbon nanofibers. These carbon nanofiber composites that have been formulated are a promising material to coat neural probes and thereby enhance functionality at the tissue interface. This

  15. Acousto-ultrasonic nondestructive evaluation of materials using laser beam generation and detection. M.S. Thesis

    Science.gov (United States)

    Huber, Robert D.; Green, Robert E., Jr.

    1990-01-01

    The acousto-ultrasonic method has proven to be a most interesting technique for nondestructive evaluation of the mechanical properties of a variety of materials. Use of the technique or a modification thereof, has led to correlation of the associated stress wave factor with mechanical properties of both metals and composite materials. The method is applied to the nondestructive evaluation of selected fiber reinforced structural composites. For the first time, conventional piezoelectric transducers were replaced with laser beam ultrasonic generators and detectors. This modification permitted true non-contact acousto-ultrasonic measurements to be made, which yielded new information about the basic mechanisms involved as well as proved the feasibility of making such non-contact measurements on terrestrial and space structures and heat engine components. A state-of-the-art laser based acousto-ultrasonic system, incorporating a compact pulsed laser and a fiber-optic heterodyne interferometer, was delivered to the NASA Lewis Research Center.

  16. Development of evaluation method with X-ray tomography for material property of IG-430 graphite for VHTR/HTGR

    Energy Technology Data Exchange (ETDEWEB)

    Sumita, Junya, E-mail: sumita.junya@jaea.go.jp [HTGR Design Group Nuclear Hydrogen and Heat Application Research Center, Japan Atomic Energy Agency, 4002 Oarai-machi, Higashiibaraki-gun, Ibaraki-ken 311-1393 (Japan); Shibata, Taiju [Graphite and Carbon Materials Characterization Special Group, Nuclear Engineering Research Collaboration Center, Japan Atomic Energy Agency, 4002 Oarai-machi, Higashiibaraki-gun, Ibaraki-ken, 311-1393 (Japan); Fujita, Ichiro; Kunimoto, Eiji; Yamaji, Masatoshi; Eto, Motokuni; Konishi, Takashi [Atomic Energy Section, Production Division, Toyo Tanso Co., Ltd., 2791 Matsuzaki, Takuma-cho, Mitoyoshi, Kagawa-ken, 769-1102 (Japan); Sawa, Kazuhiro [Department of HTTR, Japan Atomic Energy Agency, Higashiibaraki-gun, Ibaraki-ken 311-1393 (Japan)

    2014-05-01

    Graphite materials are used for the in-core components of High Temperature Gas-cooled Reactor (HTGR) which is a graphite-moderated and helium gas-cooled reactor. The HTGR is particularly attractive due to capability of producing high temperature helium gas, and its passive and inherent safety features. The Very High Temperature Reactor (VHTR) is one of the most promising candidates for the Generation-IV nuclear reactor systems. IG-110 graphite having high strength and resistance to oxidation is used in the HTTR of JAEA. IG-110 is a major candidate for the in-core graphite components of VHTR, too. From the standpoint of the safety at air ingress accident, it is important for graphite materials to have adequate resistance against oxidation damage. IG-430 graphite having higher strength and resistance to oxidation than IG-110 is an advanced candidate for the VHTR. Recently, X-ray tomography method is expected to apply the evaluation of neutron irradiation effects by measuring the irradiation-induced change of geometry of graphite grains and pores. This method is also applicable to evaluate the oxidation damage on graphite from the oxidation-induced change of grain/pore microstructures. In this study, in order to develop evaluation method for material properties and to evaluate the irradiation-induced property changes under higher neutron doses for IG-430, the oxidation and densification effects on elastic modulus of IG-430 were investigated. Moreover, the correlation of the microstructure based on the X-ray tomography images and the material properties was discussed. It was shown that the elastic modulus of the densified graphite depends on only the open pores and it is possible to evaluate the material properties of graphite by using X-ray tomography method. However, it is necessary to take into account of the change in the number and shape of closed pores in the grain to simulate the elastic modulus of the highly oxidized and irradiated materials by the

  17. Benchmark Evaluation of Fuel Effect and Material Worth Measurements for a Beryllium-Reflected Space Reactor Mockup

    Energy Technology Data Exchange (ETDEWEB)

    Marshall, Margaret A. [Idaho National Lab. (INL), Idaho Falls, ID (United States). Center for Space Nuclear Research; Bess, John D. [Idaho National Lab. (INL), Idaho Falls, ID (United States)

    2015-02-01

    The critical configuration of the small, compact critical assembly (SCCA) experiments performed at the Oak Ridge Critical Experiments Facility (ORCEF) in 1962-1965 have been evaluated as acceptable benchmark experiments for inclusion in the International Handbook of Evaluated Criticality Safety Benchmark Experiments. The initial intent of these experiments was to support the design of the Medium Power Reactor Experiment (MPRE) program, whose purpose was to study “power plants for the production of electrical power in space vehicles.” The third configuration in this series of experiments was a beryllium-reflected assembly of stainless-steel-clad, highly enriched uranium (HEU)-O2 fuel mockup of a potassium-cooled space power reactor. Reactivity measurements cadmium ratio spectral measurements and fission rate measurements were measured through the core and top reflector. Fuel effect worth measurements and neutron moderating and absorbing material worths were also measured in the assembly fuel region. The cadmium ratios, fission rate, and worth measurements were evaluated for inclusion in the International Handbook of Evaluated Criticality Safety Benchmark Experiments. The fuel tube effect and neutron moderating and absorbing material worth measurements are the focus of this paper. Additionally, a measurement of the worth of potassium filling the core region was performed but has not yet been evaluated Pellets of 93.15 wt.% enriched uranium dioxide (UO2) were stacked in 30.48 cm tall stainless steel fuel tubes (0.3 cm tall end caps). Each fuel tube had 26 pellets with a total mass of 295.8 g UO2 per tube. 253 tubes were arranged in 1.506-cm triangular lattice. An additional 7-tube cluster critical configuration was also measured but not used for any physics measurements. The core was surrounded on all side by a beryllium reflector. The fuel effect worths were measured by removing fuel tubes at various radius. An accident scenario

  18. Hardness to toughness relationship on WC-Co tool gradient materials evaluated by Palmqvist method

    Directory of Open Access Journals (Sweden)

    B. Dołżańska

    2010-06-01

    Full Text Available Purpose: Goal of this work was to describe the propagation characteristic of cracks produced at the corners of Vickers indent and the toughness change in functionally graded WC–Co cemented carbide with high disproportion of cobalt matrix portion between core and surface layer.Design/methodology/approach: Investigations of toughness methods were developed during the investigations for tungsten carbide and cobalt, making it possible to obtain four materials and then their structure was determined.Findings: A wide variation in hardness and toughness has been obtained in WC-Co composites. The propagation characteristic of cracks produced at the corners of Vickers indent and the toughness change in functionally graded WC–Co cemented carbide with dual phase structure were investigated. It is shown that cracks tend to propagate both around and across WC crystal grain. The changes of toughness with the microstructure and an integrated strengthening effect, as well as high toughness characteristic of the tool gradient material are revealed.Practical implications: Material presented in this paper are characterized by very high hardness of the surface and relative ductility of core. The cobalt phase in obtained TGM material will changing smoothly.Originality/value: The Palmqvist test provides a useful method of measuring fracture toughness of material characterized by very high hardness of the surface and relative ductility of core.

  19. Evaluation of in-plane shear test methods for composite material laminates

    Institute of Scientific and Technical Information of China (English)

    WANG Yan-lei; HAO Qing-duo; OU Jin-ping

    2007-01-01

    In-plane shear properties of composite material laminates are very important in structural design of composite material. Four commonly used in-plane shear test methods were introduced in this paper. In order to study the differences of various shear test methods, two ASTM standard in-plane shear test methods for composite material laminates were experimentally investigated. They are ±45℃ tensile shear test (ASTM D3518) and V-notched rail shear test (ASTM D7078). Five types of composite material laminates composed of E-glass fiber fabric and vinyl ester resin were utilized, whose stacking sequences are [0]3s, [0/90]3s, [CSM/0/90]2s, [±45]3s and [(0/90)2/(±45)2/(0/90)2]s, respectively. The test results indicate that the±45℃ tensile shear test can predict shear moduli of composite material laminates accurately. However, the predictions of shear strength using±45℃ tensile shear test are significantly lower than those of V-notched rail shear test.

  20. A comparative evaluation of four restorative materials to support undermined occlusal enamel of permanent teeth

    Directory of Open Access Journals (Sweden)

    Prabhakar A

    2006-09-01

    Full Text Available The purpose of this study was to test the support to undermined occlusal enamel provided by posterior restorative composite (FiltekTM P60, 3M Dental products USA, polyacid modified resin composite (F2000 compomer, 3M Dental products, USA., radiopaque silver alloy-glass ionomer cement (Miracle Mix. GC Corp, Tokyo, Japan and Glass Ionomer cement (Fuji IX GP. To test each material, 20 human permanent mandibular third molars were selected. The lingual cusps were removed and the dentin supporting the facial cusps was cut away, leaving a shell of enamel. Each group of prepared teeth was restored using the materials according to the manufacturer′s instructions. All the specimens were thermocycled (250 cycles, 6°C- 60°C, dwell time 30 seconds and then mounted on an acrylic base. Specimens were loaded evenly across the cusp tips at a crosshead speed of 5 mm /minute in Hounsfield universal testing machine until fracture occurred. Data obtained was analyzed using analysis of variance and Studentized- Newman- Keul′s range test. No significant differences were detected in the support provided by P-60, F 2000, Miracle Mix or Fuji IX GP groups. The support provided to undermined occlusal enamel by these materials was intermediate between no support and that provided by sound dentin. Without further development in dental material technology and evidence of its efficacy, restorative materials should not be relied upon to support undermined occlusal enamel to a level comparable to that provided by sound dentin.

  1. Laser-shocked energetic materials with metal additives: evaluation of detonation performance

    Science.gov (United States)

    Gottfried, Jennifer; Bukowski, Eric

    A focused, nanosecond-pulsed laser with sufficient energy to exceed the breakdown threshold of a material generates a laser-induced plasma with high peak temperatures, pressures, and shock velocities. Depending on the laser parameters and material properties, nanograms to micrograms of material is ablated, atomized, ionized and excited in the laser-induced plasma. The subsequent shock wave expansion into the air above the sample has been monitored using high-speed schlieren imaging in a recently developed technique, laser-induced air shock from energetic materials (LASEM). The estimated detonation velocities using LASEM agree well with published experimental values. A comparison of the measured shock velocities for various energetic materials including RDX, DNTF, and LLM-172 doped with Al or B to the detonation velocities predicted by CHEETAH for inert or active metal participation demonstrates that LASEM has potential for predicting the early time participation of metal additives in detonation events. The LASEM results show that reducing the amount of hydrogen present in B formulations increases the resulting detonation velocities

  2. Development and evaluation of elastomeric materials for geothermal applications. Annual report, October 1977-December 1978

    Energy Technology Data Exchange (ETDEWEB)

    Mueller, W.A.; Kalfayan, S.H.; Reilly, W.W.; Yavrouian, A.H.; Mosesman, I.D.; Ingham, J.D.

    1979-05-15

    The research involved formulation of commercially available materials and synthesis of new elastomers. Formulation studies at JPL and elsewhere produced a material having about 250-350 psi tensile strength and 30 to 80% elongation at 260/sup 0/C for at least 24 hours in simulated brine. The relationship between these laboratory test results and sealing performance in actual or simulated test conditions is not entirely clear; however, it is believed that no conventional formation or casing packer design is likely to perform well using these materials. The synthetic effort focused on high temperature block copolymers and development of curable polystyrene. Procedures were worked out for synthesizing these new materials. Initial results with heat-cured unfilled polystyrene gum at 260/sup 0/C indicated a tensile strength of about 50 psi. Cast films of the first sample of polyphenyl quinoxaline-polystyrene block copolymer, which has a graft-block structure consisting of a polystyrene chain with pendant polyphenyl quinoxaline groups, showed elastomeric behavior in the required temperature range. Its tensile strength and elongation at 260/sup 0/C were 220 to 350 psi and 18 to 36%, respectively. All of these materials also showed satisfactory hydrolytic stability. A procedure for the synthesis of a linear block copolymer of this type has been devised, and the required new intermediates have been synthesized and characterized. A description of the previous year's work is included in an appendix.

  3. A sequential extraction procedure to evaluate the mobilization behavior of rare earth elements in soils and tailings materials.

    Science.gov (United States)

    Mittermüller, Marc; Saatz, Jessica; Daus, Birgit

    2016-03-01

    A novel sequential extraction method for evaluation of the mobilization behavior of rare earth elements in soils and mine tailings materials is presented. The sequence consists of the following four steps: 0.05 mol L(-1) calcium nitrate (easily soluble and ion exchange fraction), 0.1 mol L(-1) citric acid (fraction mobilized by complexation and carbonate bound), 0.05 mol L(-1) hydroxylamine hydrochloride (pH = 2) (reducible fraction), 1.4 mol L(-1) nitric acid (acid soluble fraction). The procedure was optimized with a certified soil material and a mine tailings material and was applied to eight samples of a soil profile. The different results obtained by using either the developed method or the widespread used BCR-Method for comparison are discussed. There were clear advantages using the newly created sequential extraction procedure in getting more detailed information about the bioavailable fraction and a fraction addressing REE phosphates. PMID:26766351

  4. EVALUATION OF THE PROBABILITY DISTRIBUTION OF PITTING CORROSION FATIGUE LIFE IN AIRCRAFT MATERIALS

    Institute of Scientific and Technical Information of China (English)

    WANG Qingyuan (王清远); N.KAWAGOISHI; Q.CHEN; R.M.PIDAPARTI

    2003-01-01

    Corrosion and fatigue properties of aircraft materials are known to have a considerable scatter due to the random nature of materials,loading,and environmental conditions.A probabilistic approach for predicting the pitting corrosion fatigue life has been investigated which captures the effect of the interaction of the cyclic load and corrosive environment and all stages of the corrosion fatigue process (i.e.the pit nucleation and growth,pit-crack transition,short- and long-crack propagation).The probabilistic model investigated considers the uncertainties in the initial pit size,corrosion pitting current,and material properties due to the scatter found in the experimental data.Monte Carlo simulations were performed to define the failure probability distribution.Predicted cumulative distribution functions of fatigue life agreed reasonably well with the existing experimental data.

  5. EVALUATION OF THE PROBABILITY DISTRIBUTION OF PITTING CORROSION FATIGUE LIFE IN AIRCRAFT MATERIALS

    Institute of Scientific and Technical Information of China (English)

    王清远; N.KAWAGOISHI; Q.CHEN; R.M.PIDAPARTI

    2003-01-01

    Corrosion and fatigue properties of aircraft materials axe known to have a considerablescatter due to the random nature of materials, loading, and environmental conditions. A probabilisticapproach for predicting the pitting corrosion fatigue life has been investigated which captures the effectof the interaction of the cyclic load and corrosive environment and all stages of the corrosion fatigueprocess (i.e. the pit nucleation and growth, pit-crack transition, short- and long-crack propagation).The probabilistic model investigated considers the uncertainties in the initial pit size, corrosion pittingcurrent, and material properties due to the scatter found in the experimental data. Monte Carlo simu-lations were performed to define the failure probability distribution. Predicted cumulative distributionfunctions of fatigue life agreed reasonably well with the existing experimental data.

  6. Clay modified crushed salt for shaft sealing elements. Material optimization and evaluation in field tests

    Energy Technology Data Exchange (ETDEWEB)

    Glaubach, Uwe; Hofmann, Martin; Gruner, Matthias; Kudla, Wolfram [TU Bergakademie Freiberg (Germany). Inst. of Mining and Special Civil Engineering

    2015-07-01

    Salt-based materials are intended to use for backfill and sealing systems in geotechnical barriers in underground HLW-repositories. Due to the creep of the saliniferous host rock, the salt backfill will be compacted during several hundreds or thousands years of operation to a minimum of porosity resp. permeability. To raise the sealing potential of a salt-based backfill, the porosity after construction should be minimized by optimal material performance and compaction performance. A procedure to optimize the grain size distribution of crushed salt and its water and clay content is described. The optimized salt fraction gets a better compaction behavior than straight mine-run salt. The addition of a filler-like material (e.g. Friedland Clay Powder) reduces the total porosity and permeability. Backfill columns made from crushed salt and clay probably include an instant sealing function.

  7. Evaluation of Calcium Phosphate Cement As a Root Canal Sealer Filling Material

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    Calcium phosphate cement for root end sealing was obtained by mixing α-tricalcium phosphate and additives with an aqueous solution of citric. Powder and liquid were mixed at a ratio of 1.25g/mL. The biocompatibility of this material was investigated primarily by subcutaneous implantation tests. Then calcium phosphate cement was used to fill three adult dogs' root canal, both calcium hydroxide paste and hydroxyapatite paste as control. The animals were killed at 4,12,20 weeks postoperatively respectively. The effects of different materials on the apical closure, restoration of periapical tissues and adaptability to the dentinal surface were examined by optical and electronic microscope. The observation at 20 weeks shows that the calcium phosphate cement has the potentialities of being a root canal sealer filling material available for pulpless teeth with open-apex and destructive periapical tissue.

  8. A chemical activity evaluation of two dental calcium silicate-based materials

    Directory of Open Access Journals (Sweden)

    Chalas Renata

    2015-06-01

    Full Text Available Calcium silicate-based materials are interesting products widely used in dentistry. The study was designed to compare the chemical reaction between analyzed two preparates and dentin during cavity lining. In our work, dentinal discs were prepared from human extracted teeth filled with Biodentine and MTA+. The samples were then analyzed by way of SEM, EDS and Raman spectroscopy. The obtained results revealed differences in elemental composition between both materials. Biodentine showed higher activity in contact with dentine. Moreover, the interfacial layer in the tooth filled by Biodentine was wider than that in the tooth filled with MTA+. The applied methods of analysis confirmed that both materials have a bioactive potential which is a promising ability.

  9. Evaluation of plasma-wall interactions using material probes in the Large Helical Device

    International Nuclear Information System (INIS)

    Control of plasma-wall interactions (PWIs) and understanding their mechanism are essential issues for realization of fusion reactor. In this study, plasma-wall interactions during FY2010 and FY2011 experiments in the Large Helical Device (LHD) were analyzed by using material probes. We installed material probes at the positions expected to have different deposits of materials such as boron and titanium and investigated the correlation between this impurity deposition and gas retention. The desorption behavior of hydrogen and helium depended on the level of impurity deposition. We observed a new peak for hydrogen desorption at the probe with large boron deposits. The amount of retained hydrogen was large in that probe; however the amount of retained helium was small in the same probe, which is opposite what we observe in the probe with titanium deposits and the probe with a thin deposition layer. (author)

  10. Standard Practice for Evaluating Material Property Characteristic Values for Polymeric Composites for Civil Engineering Structural Applications

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2006-01-01

    1.1 This practice covers the procedures for computing characteristic values of material properties of polymeric composite materials intended for use in civil engineering structural applications. The characteristic value is a statistically-based material property representing the 80 % lower confidence bound on the 5th-percentile value of a specified population. Characteristic values determined using this standard practice can be used to calculate structural member resistance values in design codes for composite civil engineering structures and for establishing limits upon which qualification and acceptance criteria can be based. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

  11. Evaluation of proton scattering at an interface between two materials of different compositions

    Energy Technology Data Exchange (ETDEWEB)

    Roder, Ana Flavia Vidotti; Inocente, Guilherme Franco; Mesa, Joel, E-mail: afv.roder@yahoo.com.br, E-mail: gfinocente@gmail.com, E-mail: joel.mesa@gmail.com [Universidade Estadual Paulista Julio de Mesquita Filho (UNESP), Botucatu, SP (Brazil). Instituto de Biociencias. Departamento de Fisica e Biofisica

    2013-07-01

    Proton radiation therapy is a precise form of non-invasive image-guided cancer therapy. It is based on the well defined range of protons in material, with low entrance dose, a maximum dose and a rapid distal dose fall-off, providing better sparing of healthy tissue and allowing higher tumor doses than conventional radiation therapy with photons. In X-rays' studies is common to use PMMA (polymethyl-methacrylate) and water phantoms for calculation of absorbed dose. As the effective atomic numbers of these materials are practically the same, simulations are used often to provide similar results. In the case of beams of protons, is not so obvious that they have the same behavior due to differences in the composition of these materials. In this sense, it is necessary to know how the presence of materials with different densities and compositions interfere in the energy deposition by ionization and coulomb excitation, during its trajectory. Monte Carlo simulations were accomplished using MCNPX 2.5. In this study, we simulated the interaction of a beam of protons of 200 MeV with a target composed by PMMA and water, separated by a interface with the beam focusing on this interface region. These conditions were compared with those obtained for pure targets for each material (no interface). For all situations, the beam produced a higher peak in water than PMMA, indicating that there were more interactions with the first, probably. Thus, can conclude that the two materials are not fully equivalent for represent the same soft tissue to beams of protons. (author)

  12. CBCT fine preoperative evaluation of inflammatory radicular cysts and postoperative local integration appreciation of alloplastic grafts materials.

    Science.gov (United States)

    Nica, Diana; Ianes, Emilia; Brad, S

    2014-01-01

    The purpose of this paper is to point out the value of CBCT exam in pre and postoperative diagnosis assessment of inflammatory radicular cysts together with full appreciation of local integration of alloplastic graft materials used to repair the osseous defects. There were statistically retrospective evaluated the pre and postoperative results of CBCT and x-ray examinations of 34 patients with inflammatory radicular cysts clinically, biologically and histopathologically assessed at Oral and Maxilo-Facial Surgery Clinic from Timisoara. In all cases we proceeded to surgical radicular cysts removement, extraction of the associated non-vital tooth together with alloplastic graft materials repairement of the osseous defects. The CBCT preoperative scans clearly showed the extent, the morphological characteristics and the topoanatomic reports, in all 34 cases of inflammatory radicular cysts together with regional endodontic status. The CBCT postoperative scans revealed the very local integration of alloplastic graft materials used to repair the osseous defects and, in some cases, the dental rehabilitation by metallic implants. CBCT scan is the imaging method of choice in pre and postoperative diagnosis assessment of inflammatory radicular cysts together with alloplastic graft materials repairement of the osseous defects and dental rehabilitation by metallic implants, due to high specific abilities in bone tissue 3D evaluation. PMID:25341308

  13. Environmental Impact Evaluation of Packaging Materials%包装材料的环境影响评价

    Institute of Scientific and Technical Information of China (English)

    霍李江; 齐藤胜彦

    2008-01-01

    对有关环境影响评价技术和指标建立方法进行了比较,从而确定出能够适合可持续包装需要的包装材料环境影响评价方法.并就基于末端模型包装生命周期影响评价和单一可持续性指标的确立进行了讨论,以便能够为实践中优选包装材料提供指导.%The related environmental impact evaluation techniques and impact indicator establishing methods used in environmental impact evaluation of packaging materials were compared,and appropriate methods of environmental impact evaluation of packaging materials for sustainable packaging purpose were established.Life-cycle impact assessment method based on endpoint modeling and the establishment of single sustainability indicator was discussed.The purpose was to provide guidance for packaging material selection.

  14. Evaluation of the efficacy of a bioactive synthetic graft material in the treatment of intrabony periodontal defects

    Directory of Open Access Journals (Sweden)

    Vishakha Grover

    2013-01-01

    Full Text Available Background: Bioactive ceramic fillers are synthetic materials which have shown the potential to enhance bone formation. The purpose of this study was to evaluate the efficacy of a bioactive synthetic graft material in the treatment of intrabony periodontal defects. Materials and Methods: Fourteen intrabony defects in twelve systemically healthy subjects having moderate to severe chronic periodontitis were evaluated after bone grafting with bioactive ceramic filler for a period of 6 months. Clinical and radiographic evaluations were made at baseline, at 3 and 6 months following surgery. Results: Mean radiographic defect fill of 64.76% (2.49±0.5 mm was observed in 6 months, which was statistically significant. A statistically significant relative attachment level gain of 2.71±1.13 mm and probing pocket depth reduction of 4.21±1.18 mm was recorded at the end of the study. A significant decrease in mobility and gingival index was observed. Conclusions: Bioactive glass is an efficacious treatment option for the reconstruction of intrabony periodontal defects as it led to statistically significant improvements in the clinical and radiographic parameters.

  15. Evaluation of Core Loss in Magnetic Materials Employed in Utility Grid AC Filters

    DEFF Research Database (Denmark)

    Beres, Remus Narcis; Wang, Xiongfei; Blaabjerg, Frede;

    2016-01-01

    the core, depending on the magnetic material of choice and current ripple specifications. Additionally, shunt or series reactors that exists in LCL or trap filters and which are subjected to sinusoidal excitations have different specifications and requirements. Therefore, the core losses of different...... magnetic materials adopted in utility grid ac filters have been investigated and measured for both sinusoidal and rectangular excitation, with and without dc bias condition. The core loss information can ensure cost effective passive filter designs and may avoid trial-error design procedures of the passive...

  16. Evaluation of Blue Value in different plant materials as a tool for rapid starch determination

    OpenAIRE

    Bogusław Samotus; Joanna Tuz; Elżbieta Doerre

    2014-01-01

    In order to determine the concentration of starch in plant materials from the intensity of the blue iodine complex, it is necessary to know the Blue Value (B.V.), which is defined in this paper as the absorbancy of 100 mg of a starch-iodine complex in 100 ml of aqueous solution. An adequate amount of plant material is treated with a hot CaCl2 solution for 1/2 hour and the solute is diluted to 25 ml with CaCl2. This basic solution serves to measure absorbancy, as well as for starch determinati...

  17. Material and energy recovery in integrated waste management systems. An evaluation based on life cycle assessment.

    Science.gov (United States)

    Giugliano, Michele; Cernuschi, Stefano; Grosso, Mario; Rigamonti, Lucia

    2011-01-01

    This paper reports the environmental results, integrated with those arising from mass and energy balances, of a research project on the comparative analysis of strategies for material and energy recovery from waste, funded by the Italian Ministry of Education, University and Research. The project, involving the cooperation of five University research groups, was devoted to the optimisation of material and energy recovery activities within integrated municipal solid waste (MSW) management systems. Four scenarios of separate collection (overall value of 35%, 50% without the collection of food waste, 50% including the collection of food waste, 65%) were defined for the implementation of energetic, environmental and economic balances. Two sizes of integrated MSW management system (IWMS) were considered: a metropolitan area, with a gross MSW production of 750,000 t/year and an average province, with a gross MSW production of 150,000 t/year. The environmental analysis was conducted using Life Cycle Assessment methodology (LCA), for both material and energy recovery activities. In order to avoid allocation we have used the technique of the expansion of the system boundaries. This means taking into consideration the impact on the environment related to the waste management activities in comparison with the avoided impacts related to the saving of raw materials and primary energy. Under the hypotheses of the study, both for the large and for the small IWMS, the energetic and environmental benefits are higher than the energetic and environmental impacts for all the scenarios analysed in terms of all the indicators considered: the scenario with 50% separate collection in a drop-off scheme excluding food waste shows the most promising perspectives, mainly arising from the highest collection (and recycling) of all the packaging materials, which is the activity giving the biggest energetic and environmental benefits. Main conclusions of the study in the general field of the

  18. Quantitative evaluation of erosive cavitation pressure field from pits in material: fact or myth?

    Science.gov (United States)

    Choi, J.-K.; Chahine, G. L.

    2015-12-01

    Material pitting in a cavitating flow has been used for a long time as an indicator of the vague ‘cavitation intensity’ concept. Periodically, some researchers suggest pitting tests as a “simple” means to provide quantitative measurements of the amplitude of the impulsive pressures in the cavitation field, especially when combined with Tabor's formula or with simple finite element computations with static loads. This paper examines the viability of such a method using fully coupled bubble dynamics and material response, and strongly concludes that the commonly accepted idea is a myth, as different loading scenarios with the same amplitude of the cavitation impulsive pressure result in different pit aspect ratios.

  19. HEMA/MMA/EDMA packing material evaluation for size exclusion chromatography (SEC

    Directory of Open Access Journals (Sweden)

    Cristina Duarte Vianna-Soares

    2005-03-01

    Full Text Available HEMA/MMA/EDMA (2-hydroxyethyl methacrylate/methyl methacrylate/ethyleneglycol methacrylate copolymer beads have been synthesized for use in aqueous SEC. This porous chromatographic support consisted of a large average particle size (250 µm and contained macropores with a median pore size of approximately 880 Å. The material was packed in glass and stainless columns to assess their chromatographic performance. The packed columns were calibrated using narrow molecular weight (MW distribution standards (dextran and exhibited a range of molecular weight separation between 40,000 and 2,000,000 daltons. The packing material showed the ability to separate large molecules through the size exclusion mechanism.

  20. Evaluation of Corrosion of Aluminum Based Reactor Fuel Cladding Materials During Dry Storage

    Energy Technology Data Exchange (ETDEWEB)

    Peacock, H.B. Jr.

    1999-10-21

    This report provides an evaluation of the corrosion behavior of aluminum cladding alloys and aluminum-uranium alloys at conditions relevant to dry storage. The details of the corrosion program are described and the results to date are discussed.

  1. Recent European Food Safety Authority toxicological evaluations of major phthalates used in food contact materials.

    Science.gov (United States)

    Lhuguenot, Jean-Claude

    2009-08-01

    During the 1980s and 1990s, and at the EU level, the Scientific Committee for Food evaluated a number of phthalates that were being used, or were requested for use, as additives in plastics. At this time, peroxisome proliferation was considered as the pivotal effect on which toxicological evaluation of these chemicals was based. At the end of 1990s, a general consensus has been agreed that rodents are highly sensitive to the phenomenon of peroxisome proliferation and that this particular effect should not be used for human risk assessment. Consequently in 2004, it was requested from the newly created European Food Safety Authority to perform a new evaluation of the mainly used phthalates on the basis of existing data. This paper summarizes evaluations of butylbenzylphthalate, dibutylphthalate, diethylhexylphthalate.

  2. EVALUATION OF SOCIAL ENVIRONMENTAL EFFICIENCY ON RECYCLING OF CONSTRUCTION SLUDGES AS GROUND MATERIALS

    Science.gov (United States)

    Inazumi, Shinya; Ohtsu, Hiroyasu; Isoda, Takayuki; Shigematsu, Yuji

    Although waste recycling has been promoted in response to increasing environmental awareness in Japan, its marketability is being questioned due to the recycling cost. The ultimate goal of waste recycling is to reduce the environmental load. In this paper, we examined the evaluation method for social environmental efficiency to socially evaluate waste recycling, by incorporating environmental load as an environmental cost in addition to the direct cost. Specifically, by applying sensitivity analysis and Monte-Carlo Simulation, we conducted the social environmental efficiency evaluation including consideration of uncertainties, because waste recycling involves various uncertain elements. As a result, we were able to quantitatively evaluate the social environmental significance of construction sludge recycling while focusing on the particular construction sludge with a lower recycling rate.

  3. Evaluation of Corrosion of Aluminum Based Reactor Fuel Cladding Materials During Dry Storage

    International Nuclear Information System (INIS)

    This report provides an evaluation of the corrosion behavior of aluminum cladding alloys and aluminum-uranium alloys at conditions relevant to dry storage. The details of the corrosion program are described and the results to date are discussed

  4. Evaluation of ultra-low background materials for uranium and thorium using ICP-MS

    Energy Technology Data Exchange (ETDEWEB)

    Hoppe, E. W.; Overman, N. R.; LaFerriere, B. D. [Pacific Northwest National Laboratory, Richland, WA 99354 (United States)

    2013-08-08

    An increasing number of physics experiments require low background materials for their construction. The presence of Uranium and Thorium and their progeny in these materials present a variety of unwanted background sources for these experiments. The sensitivity of the experiments continues to drive the necessary levels of detection ever lower as well. This requirement for greater sensitivity has rendered direct radioassay impractical in many cases requiring large quantities of material, frequently many kilograms, and prolonged counting times, often months. Other assay techniques have been employed such as Neutron Activation Analysis but this requires access to expensive facilities and instrumentation and can be further complicated and delayed by the formation of unwanted radionuclides. Inductively Coupled Plasma Mass Spectrometry (ICP-MS) is a useful tool and recent advancements have increased the sensitivity particularly in the elemental high mass range of U and Th. Unlike direct radioassay, ICP-MS is a destructive technique since it requires the sample to be in liquid form which is aspirated into a high temperature plasma. But it benefits in that it usually requires a very small sample, typically about a gram. This paper discusses how a variety of low background materials such as copper, polymers, and fused silica are made amenable to ICP-MS assay and how the arduous task of maintaining low backgrounds of U and Th is achieved.

  5. Evaluation of Ultra-Low Background Materials for Uranium and Thorium Using ICP-MS

    Energy Technology Data Exchange (ETDEWEB)

    Hoppe, Eric W.; Overman, Nicole R.; LaFerriere, Brian D.

    2013-08-08

    An increasing number of physics experiments require low background materials for their construction. The presence of Uranium and Thorium and their progeny in these materials present a variety of unwanted background sources for these experiments. The sensitivity of the experiments continues to drive the necessary levels of detection ever lower as well. This requirement for greater sensitivity has rendered direct radioassay impractical in many cases requiring large quantities of material, frequently many kilograms, and prolonged counting times, often months. Other assay techniques have been employed such as Neutron Activation Analysis but this requires access to expensive facilities and instrumentation and can be further complicated and delayed by the formation of unwanted radionuclides. Inductively Coupled Plasma Mass Spectrometry (ICP-MS) is a useful tool and recent advancements have increased the sensitivity particularly in the elemental high mass range of U and Th. Unlike direct radioassay, ICP-MS is a destructive technique since it requires the sample to be in liquid form which is aspirated into a high temperature plasma. But it benefits in that it usually requires a very small sample, typically about a gram. Here we will discuss how a variety of low background materials such as copper, polymers, and fused silica are made amenable to ICP-MS assay and how the arduous task of maintaining low backgrounds of U and Th is achieved.

  6. Evaluation of ultra-low background materials for uranium and thorium using ICP-MS

    Science.gov (United States)

    Hoppe, E. W.; Overman, N. R.; LaFerriere, B. D.

    2013-08-01

    An increasing number of physics experiments require low background materials for their construction. The presence of Uranium and Thorium and their progeny in these materials present a variety of unwanted background sources for these experiments. The sensitivity of the experiments continues to drive the necessary levels of detection ever lower as well. This requirement for greater sensitivity has rendered direct radioassay impractical in many cases requiring large quantities of material, frequently many kilograms, and prolonged counting times, often months. Other assay techniques have been employed such as Neutron Activation Analysis but this requires access to expensive facilities and instrumentation and can be further complicated and delayed by the formation of unwanted radionuclides. Inductively Coupled Plasma Mass Spectrometry (ICP-MS) is a useful tool and recent advancements have increased the sensitivity particularly in the elemental high mass range of U and Th. Unlike direct radioassay, ICP-MS is a destructive technique since it requires the sample to be in liquid form which is aspirated into a high temperature plasma. But it benefits in that it usually requires a very small sample, typically about a gram. This paper discusses how a variety of low background materials such as copper, polymers, and fused silica are made amenable to ICP-MS assay and how the arduous task of maintaining low backgrounds of U and Th is achieved.

  7. Evaluation of ultra-low background materials for uranium and thorium using ICP-MS

    International Nuclear Information System (INIS)

    An increasing number of physics experiments require low background materials for their construction. The presence of Uranium and Thorium and their progeny in these materials present a variety of unwanted background sources for these experiments. The sensitivity of the experiments continues to drive the necessary levels of detection ever lower as well. This requirement for greater sensitivity has rendered direct radioassay impractical in many cases requiring large quantities of material, frequently many kilograms, and prolonged counting times, often months. Other assay techniques have been employed such as Neutron Activation Analysis but this requires access to expensive facilities and instrumentation and can be further complicated and delayed by the formation of unwanted radionuclides. Inductively Coupled Plasma Mass Spectrometry (ICP-MS) is a useful tool and recent advancements have increased the sensitivity particularly in the elemental high mass range of U and Th. Unlike direct radioassay, ICP-MS is a destructive technique since it requires the sample to be in liquid form which is aspirated into a high temperature plasma. But it benefits in that it usually requires a very small sample, typically about a gram. This paper discusses how a variety of low background materials such as copper, polymers, and fused silica are made amenable to ICP-MS assay and how the arduous task of maintaining low backgrounds of U and Th is achieved

  8. Evaluation of critical materials in five additional advance design photovoltaic cells

    Energy Technology Data Exchange (ETDEWEB)

    Smith, S.A.; Watts, R.L.; Martin, P.; Gurwell, W.E.

    1981-02-01

    The objective of this study is to identify potential material supply constraints due to the large-scale deployment of five advanced photovoltaic (PV) cell designs, and to suggest strategies to reduce the impacts of these production capacity limitations and potential future material shortages. The Critical Materials Assessment Program (CMAP) screens the designs and their supply chains and identifies potential shortages which might preclude large-scale use of the technologies. The results of the screening of five advanced PV cell designs are presented: (1) indium phosphide/cadmium sulfide, (2) zinc phosphide, (3) cadmium telluride/cadmium sulfide, (4) copper indium selenium, and (5) cadmium selenide photoelectrochemical. Each of these five cells is screened individually assuming that they first come online in 1991, and that 25 Gwe of peak capacity is online by the year 2000. A second computer screening assumes that each cell first comes online in 1991 and that each cell has a 5 GWe of peak capacity by the year 2000, so that the total online capacity for the five cells is 25 GWe. Based on a review of the preliminary baseline screening results, suggestions were made for varying such parameters as the layer thickness, cell production processes, etc. The resulting PV cell characterizations were then screened again by the CMAP computer code. The CMAP methodology used to identify critical materials is described; and detailed characterizations of the advanced photovoltaic cell designs under investigation, descriptions of additional cell production processes, and the results are presented. (WHK)

  9. Engineering spinal fusion: evaluating ceramic materials for cell based tissue engineered approaches

    NARCIS (Netherlands)

    Wilson, C.E.

    2011-01-01

    The principal aim of this thesis was to advance the development of tissue engineered posterolateral spinal fusion by investigating the potential of calcium phosphate ceramic materials to support cell based tissue engineered bone formation. This was accomplished by developing several novel model syst

  10. DEVELOPMENT AND EVALUATION OF SELF-INSTRUCTIONAL MATERIALS FOR UNDERACHIEVING AND OVERACHIEVING STUDENTS.

    Science.gov (United States)

    SILBERMAN, HARRY; AND OTHERS

    AN EXPLORATION OF THE INTERACTION BETWEEN PROGRAMED TEACHING DEVICES AND INDIVIDUAL CHARACTERISTICS OF HIGH SCHOOL STUDENTS WAS UNDERTAKEN. THERE WERE FOUR PARTS -- PREPARATION OF MATERIALS ON GEOMETRY, THE ESTABLISHMENT OF CRITERION MEASURES, PRELIMINARY PILOT EXPERIMENTS, AND THE MAIN EXPERIMENT. THE MAIN EXPERIMENT WAS PERFORMED IN 27 CLASSES…

  11. Importance of material evaluation prior to the construction of devices for in vitro techniques.

    Science.gov (United States)

    Rach, Jessica; Halter, Beat; Aufderheide, Michaela

    2013-11-01

    The development and validation of new in vitro methods in the field of toxicology have gained more importance in recent years due to stricter guidelines for animal testing, especially in the European Union. Consequently, advances in the construction of technical devices for the exposure of cell or tissue cultures to test substances are necessary. Here, to obtain reliable results, it is important to exclusively use materials that do not interfere with the cell viability. Thus, similar to the biomaterials testing of medical devices which is regulated in the Directive 93/42/EEC, the biocompatibility of the materials has to be verified prior to the construction of such devices. We present here a novel approach for biomaterials testing which allows the quantitative and qualitative assessment of cytotoxicity of material samples. Stainless steel and silicone are often used for laboratory equipment, due to their high chemical, thermal and mechanical resistance. However, our results highlight that some types of silicone may have adverse effects on cultured cells. Moreover, special methods for the surface treatment of metals may also be a critical factor for in vitro devices. Therefore, the testing of all materials coming in contact with cell cultures is highly recommended. PMID:23452617

  12. Evaluation of precision and accuracy of selenium measurements in biological materials using neutron activation analysis

    International Nuclear Information System (INIS)

    In recent years, the accurate determination of selenium in biological materials has become increasingly important in view of the essential nature of this element for human nutrition and its possible role as a protective agent against cancer. Unfortunately, the accurate determination of selenium in biological materials is often difficult for most analytical techniques for a variety of reasons, including interferences, complicated selenium chemistry due to the presence of this element in multiple oxidation states and in a variety of different organic species, stability and resistance to destruction of some of these organo-selenium species during acid dissolution, volatility of some selenium compounds, and potential for contamination. Neutron activation analysis (NAA) can be one of the best analytical techniques for selenium determinations in biological materials for a number of reasons. Currently, precision at the 1% level (1s) and overall accuracy at the 1 to 2% level (95% confidence interval) can be attained at the U.S. National Bureau of Standards (NBS) for selenium determinations in biological materials when counting statistics are not limiting (using the 75Se isotope). An example of this level of precision and accuracy is summarized. Achieving this level of accuracy, however, requires strict attention to all sources of systematic error. Precise and accurate results can also be obtained after radiochemical separations

  13. Development and evaluation of a biocide release system for prolonged antifungal activity in finishing materials

    NARCIS (Netherlands)

    Eversdijk, J.; Erich, S.J.F.; Hermanns, S.P.M.; Adan, O.C.G.; Bolle, M. de; Meyer, K. de; Bylemans, D.; Bekker, M.; Cate, A.T. ten

    2012-01-01

    This paper focuses on the use of modified nano-clay particles as a controlled release system for biocides from building materials. Different (model) biocides were incorporated in a biocide/nano-clay composite and subsequently the release of the biocides was monitored under different environmental co

  14. Evaluation of Varying Biochars as Carrier Materials for Bacterial Soil Inoculants

    Science.gov (United States)

    Hale, Lauren; Crowley, David

    2014-05-01

    The incorporation of biochar into agricultural soils for carbon sequestration and improved soil fertility creates an opportunity to simultaneously deliver plant-growth promoting rhizobacteria (PGPR). Many characteristics of biochar materials indicate that these particles could be conducive as inoculum carriers. This could provide a value-added component for biochar marketing and has an advantage over traditional carrier materials, which can be unsustainable or expensive to produce. Here, we assessed the suitability of 10 biochar types, made from 5 feedstocks at 2 pyrolysis temperatures (300°C and 600°C), to serve as carriers for 2 model PGPR strains, Enterobacter cloacae UW5 and Pseudomonas putida UW4. All biochars were characterized based on BET specific surface area, C-N content, pH, EC, and their abilities to adsorb bacterial cells from a liquid inoculum. Further studies incorporated qPCR to quantify the survival of inoculants after introduction into soils via biochar carriers. The biochars that performed well were further assayed for their influence on PGPR traits, 1-aminocyclopropane-1-carboxylate (ACC) deaminase and auxin production. Peat and vermiculite served as traditional carrier materials to which we compared the biochars. Our findings indicated that biochars varied in their interactions with our model PGPR strains. Based on our analysis several biochar types were able to serve as carriers which were as good, if not better than, the traditional carrier materials. Future work should seek to assess shelf life and varying inoculation methods for the biochar-inoculant complexes.

  15. Evaluation of Modular EFL Educational Program (Audio-Visual Materials Translation & Translation of Deeds & Documents)

    Science.gov (United States)

    Imani, Sahar Sadat Afshar

    2013-01-01

    Modular EFL Educational Program has managed to offer specialized language education in two specific fields: Audio-visual Materials Translation and Translation of Deeds and Documents. However, no explicit empirical studies can be traced on both internal and external validity measures as well as the extent of compatibility of both courses with the…

  16. Evaluation of select blends of cotton byproducts in the manufacture of biodegradable packaging material

    Science.gov (United States)

    Polystyrene is one of the most widely used plastics in the manufacture of packaging materials. Extruded polystyrene foam is commonly sold under the trademark name of StyrofoamTM. Polystyrene packaging is a multibillion dollar a year industry. Since polystyrene is non-biodegradable, a biodegradable m...

  17. Evaluation of the Benefits Attributable to Automotive Lighweight Materials Program Research and Development Projects

    Energy Technology Data Exchange (ETDEWEB)

    Das, S.

    2002-01-11

    The purpose of this project is to identify and test methods appropriate for estimating the benefits attributable to research and development (R and D) projects funded by the Automotive Lightweight Materials (ALM) Program of the Office of Advanced Automotive Technologies (OAAT) of the U.S. Department of Energy (DOE). The program focuses on the development and validation of advanced lightweight materials technologies to significantly reduce automotive vehicle body and chassis weight without compromising other attributes such as safety, performance, recyclability, and cost. The work supports the goals of the Partnership for a New Generation of Vehicles (PNGV). Up to thirty percent of the improvement required to meet the PNGV goal of tripling vehicle fuel economy and much of its cost, safety, and recyclability goal depend on the lightweight materials. Funded projects range from basic materials science research to applied research in production environments. Collaborators on these projects include national laboratories, universities, and private sector firms, such as leading automobile manufacturers and their suppliers.

  18. Pilot Randomized Evaluation of Publically Available Concussion Education Materials: Evidence of a Possible Negative Effect

    Science.gov (United States)

    Kroshus, Emily; Baugh, Christine M.; Hawrilenko, Matt; Daneshvar, Daniel H.

    2015-01-01

    Many states and sports leagues are instituting concussion policies aimed at reducing risk of morbidity and mortality; many include mandates about the provision of concussion education to youth athletes. However, there is limited evidence if educational materials provided under these typically vague mandates are in fact effective in changing…

  19. Dynamic materials evaluation by confined plasma ablation and laser-generated shocks

    Science.gov (United States)

    Paisley, Dennis L.; Swift, D. C.; Forsman, A. C.; Kyrala, George A.; Johnson, Randall P.; Kopp, Roger A.; Hauer, Allan A.; Wark, Justin S.; Loveridge, A.; Allen, A. M.; Kalantar, Daniel H.

    2000-08-01

    Laser-generated shocks can and have been used to study their effects on single crystal materials during shock compression. While a crystal undergoes shock compression and release, the transient x- ray diffraction (TXD) of the Bragg and Laue signals is indicative of the change in the crystal lattice spacing. The lattice spacing directly relates to the strain in the crystal. From the dynamic lattice data, strain, strain rate, and/or phase change in a material may be determined. Confined ablation plasmas can efficiently launch a flyer plate for direct impact on a target material imparting a well-characterized shock input and generate kilobar to megabar pressure pulses over a wide range of pulse duration (EQ 1 - >= 20 ns). The laser-launched flyer plates are analogous to those launched by gas guns, but the smaller size provides an experimental method not easily accessible by larger gas gun experiments. With lasers, diagnostic equipment can be easily synchronized to study dynamic material parameters, i.e., single crystal shock dynamics, interfacial bond strengths of thin coatings, grain-interfaces, texture, and high strain rates (106 - 109 sec-1).

  20. The Relation between Life Satisfaction and the Material Situation: A Re-Evaluation Using Alternative Measures

    Science.gov (United States)

    Christoph, Bernhard

    2010-01-01

    Among the surprising results of research on the relation between a person's material circumstances and his or her subjective well-being was the finding that this relationship appears to be rather weak (throughout this paper the terms "(general) life satisfaction", "(subjective) satisfaction", "happiness" and "subjective well-being" will be used…

  1. Experimental method for the evaluation of the susceptibility of materials to shear band formation

    Directory of Open Access Journals (Sweden)

    Tham R.

    2012-08-01

    Full Text Available In order to characterize materials with respect to their susceptibility to shear band formation at high strain rates, a modified Hopkinson pressure bar apparatus and hat-shaped steel specimens with a shear zone having a width significantly larger than the typical width of adiabatic bands are used. The sample is directly impacted by the striker. The force acting on the sample is measured with a PVDF-gauge between the sample and the output bar. The displacement is recorded with an electro-optical extensometer. The energy absorbed by the shearing process up to failure can be used as a reference for the susceptibility of materials to shear band formation. The method is demonstrated comparing the shear behavior of two high-strength steels with similar metallic structure and strength. Differences were found in the transition region between quasi-static and fully adiabatic shearing conditions where the energy up to rupture differs by 40 %. For fully adiabatic shear band formation, the deformation process of both materials equals. At extreme rates, shear processes are mainly governed by the thermodynamic properties of the materials. On the other hand, strength and structural properties play a role for low and intermediate rates where global and localized shear mechanisms occur in parallel.

  2. Evaluation of alternative phase change materials for energy storage in solar dynamic applications

    Science.gov (United States)

    Crane, R. A.; Dustin, M. O.

    1988-01-01

    The performance of fluoride salt and metallic thermal energy storage materials are compared in terms of basic performance as applied to solar dynamic power generation. Specific performance considerations include uniformity of cycle inlet temperature, peak cavity temperature, TES utilization, and system weights. Also investigated were means of enhancing the thermal conductivity of the salts and its effect on the system performance.

  3. Developing Guidelines for Evaluating the Adaptation of Accessible Web-Based Learning Materials

    Science.gov (United States)

    Radovan, Marko; Perdih, Mojca

    2016-01-01

    E-learning is a rapidly developing form of education. One of the key characteristics of e-learning is flexibility, which enables easier access to knowledge for everyone. Information and communications technology (ICT), which is e-learning's main component, enables alternative means of accessing the web-based learning materials that comprise the…

  4. Evaluation of silk-floss fiber and dog fur as sorbent materials for the petroleum sector

    Energy Technology Data Exchange (ETDEWEB)

    Santos, Lucas P. dos [Universidade Federal do Parana (PGMec/UFPR), Curitiba, PR (Brazil). Programa de Pos-Graduacao em Engenharia Mecanica; Dubiella, Juliana [Universidade Federal do Parana (DEMEC/UFPR), Curitiba, PR (Brazil). Dept. de Engenharia Mecanica. Programa Institucional de Bolsas de Iniciacao Cientifica; Perotta, Larissa [Universidade Federal do Parana (UFPR), Curitiba, PR (Brazil). Programa Interdisciplinar em Engenharia de Petroleo e Gas Natural; Satyanarayana, Kestur G. [Universidade Federal do Parana (UFPR), Curitiba, PR (Brazil). Dept. de Quimica; Flores-Sahagun, Thais Sydenstricker [Universidade Federal do Parana (DEMEC/UFPR), Curitiba, PR (Brazil). Dept. de Engenharia Mecanica

    2009-07-01

    In this study silk-floss and dog fur were tested as sorbent materials for oils and the results were compared with peat, a commercial sorbent. Sorption tests were carried out in dry and aqueous systems, with and without stirring for different periods of time (5-1440 min). Density, hydrophobicity, buoyancy and water uptake by the fibers of the impregnated sorbents have been determined. The use of silk-floss and dog fur was also tested in columns to purify water containing toluene, benzene, motor oil or sunflower oil. Breakthrough curves during 120 min were drawn for each material with the samples (oily water or water containing benzene or toluene) and were analyzed by ultraviolet spectroscopy. It was concluded that the silk-floss is the best sorbent material (65.3 g oil/g sorbent) followed by the dog fur (34.6 g oil/g sorbent) and peat (19.5 g oil/g sorbent), for sorption time of 1 h in dynamic condition. The efficiency of the pollutant removal from water with the use of adsorption columns was high for both materials although the use of dog fur was preferable because of the slight superiority in efficiency compared to silk-floss and also, due to the easier packing of the dog fur in the column. (author)

  5. Evaluating use stage exposure to food contact materials in a LCA framework

    DEFF Research Database (Denmark)

    Ernstoff, Alexi; Jolliet, Olivier; Fantke, Peter

    2015-01-01

    in a way compatible with intake fraction, iF, a metric traditionally used in LCIA. The model predicts PiF increases with temperature and for compounds with lower octanol-water partition coefficients within more permeable materials which are in contact with foods with high ethanol equivalencies (fatty foods)....

  6. Focus Framework: A New Guideline for Presenting and Evaluating Lexical Contents in ELT Materials

    Science.gov (United States)

    Zarifi, Abdolvahed

    2015-01-01

    Despite the not-so-distant negligence of lexicon in language instruction, it is currently taking on a core role in designing ELT materials. Selection of the lexical content is usually informed by a set of pedagogical and non-pedagogical factors like learnability, usefulness, the level of proficiency targeted, frequency, range, coverage, etc. With…

  7. Evaluation of Surlyn 8920 as PHE Visor Material and Evaluations of New Adhesives for Improving Bonding Between Teflon and Stainless Steel at Cryogenic Temperature

    Science.gov (United States)

    Ray, Asit K.

    1991-01-01

    Two studies are presented, and in the first study, Surlyn 8920 (an ionic and amorphous low density polyethylene made by Dupont) was evaluated as a possible replacement of Plexyglass G as PHE visor material. Four formulations of the polymer were made by adding different amounts of UV stabilizer, energy quencher, and antioxident in a Brabender Plasticorder. The formulated polymers were molded in the form of sheets in a compression molder. Cut samples from the molded sheets were exposed in a weatherometer and tested on Instron Tensile Tester for strength and elongation. Specially molded samples of the formulated polymers were subjected to Charpy Impact Tests. In the second study, preliminary evaluations of adhesives for improvement of bonding between Teflon and stainless steel (SS) were performed. Kapton, a high temperature polyimide made by Dupont, and a rubber based adhesive made by Potter Paint Co., were evaluated against industrial quality epoxy, the current material used to bond Teflon and SS. The degreased surfaces of the SS discs were etched mechanically, with a few of these etched chemically. The surfaces of the SS discs were etched mechanically, with a few of these etched chemically. Bonding strengths were evaluated using lap shear tests on the Instron Tensile Tester for the samples bonded by Kapton and industrial quality epoxy. Bond strengths were also evaluated using a pull test on the Instron for the samples bonded by Potter adhesive (CWL-152) and industrial quality epoxy. Based on limited lap shear data, Kapton gave bond strength favorable compared to that of industrial epoxy. Based on limited pull test data, Kapton bonded and CWL-152 bonded samples showed poor strength compared to epoxy bonded sample.

  8. Evaluation of natural colonisation of cementitious materials: effect of bioreceptivity and environmental conditions.

    Science.gov (United States)

    Manso, Sandra; Calvo-Torras, María Ángeles; De Belie, Nele; Segura, Ignacio; Aguado, Antonio

    2015-04-15

    Incorporation of living organisms, such as photosynthetic organisms, on the structure envelope has become a priority in the area of architecture and construction due to aesthetical, economic and ecological advantages. Important research efforts are made to achieve further improvements, such as for the development of cementitious materials with an enhanced bioreceptivity to stimulate biological growth. Previously, the study of the bioreceptivity of cementitious materials has been carried out mainly under laboratory conditions although field-scale experiments may present different results. This work aims at analysing the colonisation of cementitious materials with different levels of bioreceptivity by placing them in three different environmental conditions. Specimens did not present visual colonisation, which indicates that environmental conditions have a greater impact than intrinsic properties of the material at this stage. Therefore, it appears that in addition to an optimized bioreceptivity of the concrete (i.e., composition, porosity and roughness), extra measures are indispensable for a rapid development of biological growth on concrete surfaces. An analysis of the colonisation in terms of genus and quantity of the most representative microorganisms found on the specimens for each location was carried out and related to weather conditions, such as monthly average temperature and total precipitation, and air quality in terms of NOx, SO2, CO and O3. OPC-based specimens presented a higher colonisation regarding both biodiversity and quantity. However, results obtained in a previous experimental programme under laboratory conditions suggested a higher suitability of Magnesium Phosphate Cement-based (MPC-based) specimens for algal growth. Consequently, carefully considering the environment and the relationships between the different organisms present in an environment is vital for successfully using a cementitious material as a substrate for biological growth. PMID

  9. Evaluation of recriticality behavior in the material-relocation phase for Japan sodium-cooled fast reactor

    International Nuclear Information System (INIS)

    As the most promising concept of sodium-cooled fast reactors, the Japan Atomic Energy Agency has selected the advanced loop-type fast reactor, so-called Japan sodium-cooled fast reactor (JSFR). Through the evaluation of event progressions during hypothetical core-disruptive accident (CDA) under the design extension condition, a CDA scenario for JSFR has been evaluated. It has already been demonstrated that in-vessel retention (IVR) against CDA could be achieved by taking adequate design measures under best estimate conditions. The whole sequence of CDA scenario for JSFR was categorized into four phases according to the progress of core-disruption status. In the third phase, so-called material-relocation phase, the accident events would progress in the subcritical state. However, if the uncertainties about the molten state of core remnant and their discharge behavior outward from core are conservatively superposed, the disrupted core may lead up to recriticality. In the present study, the factors leading to recriticality in the material-relocation phase were investigated using the phenomenological diagrams, and the recriticality behaviors were evaluated through parametric analyses using SIMMER-III/IV codes. The results of parametric analyses suggested that a significant mechanical energy leading to the boundary failure of reactor vessel would not be released even assuming recriticality due to the uncertainties about molten state and discharge behavior. Through the present evaluation of the hypothetical recriticality event, the CDA scenario for JSFR could obtain further robustness from the viewpoint of achieving IVR. (author)

  10. Modular Sequence: English as a Second Language, Methods and Techniques. TTP 001.13 Evaluating and Adapting Materials. Teacher Corps Bilingual Project.

    Science.gov (United States)

    Hernandez, Alberto; Melnick, Susan L.

    The purpose of this unit of work is to provide the teacher participant with some useful guidelines for evaluating and adapting written materials for specific English as a second language (ESL) classes. There is pre- and post-assessment of specific learning tasks relevant to evaluating and adapting materials as well as learning activities, which…

  11. Developing and Evaluating Candidate Materials for Generation IV Supercritical Water Reactors

    Energy Technology Data Exchange (ETDEWEB)

    Jang, Jin Sung; Kim, Sung Ho; Hwang Sung Sik and others

    2006-03-15

    High temperature mechanical behavior High temperature behavior of two F-M steels were investigated, considering the transient temperature range of the SCWR (above 800 .deg. C). T91 and T122 specimens were five times cyclically heat treated to the temperature 810 .deg. C and 845 .deg. C respectively. And the heat treatments were found to have little effect on the creep rupture behavior at 550, 600, or 650 .deg. C. However, the microstructural change was detected by the rapid hardness change after the holding the specimens at 840 .deg. C even for 10 sec. (by INL, previously ANL-W) A 20Cr Fe-base ODS alloy (MA956) was isothermally heat treated at 475 .deg. C for various times and then impact tested. The material was found to become very brittle after the heat treatment even for 100 hrs by the drastic decrease of the impact absorption energy (from 300 J to about the nil) and by the typically brittle fracture surface. (by KAIST) Corrosion and SCC Behavior in SCW (1) The corrosion behaviors of the F-M steels (T91, T92, and T122) and high Ni alloys (alloy 625, Alloy 690, and alloy 800H) and an ODS alloy (MA 956) were studied in the aerated SCW (8 ppm of D.O; dissolved oxygen) under 25 MPa from 300 to 600 .deg. C with an interval of 50 .deg. C. The test durations were 100, 200, and 500 hrs respectively. In general high Ni alloys were definitely more resistant to corrosion in SCW than F-M steels. As the Cr content increases the resistance of F-M steels to corrosion becomes better. The resistance of F-M steels to corrosion at 350 .deg. C, a subcritical temperature, was revealed to be comparatively similar to those at 550 .deg. C, a 200 .deg. C higher temperature. (2) The SCC resistance of F-M steels, T91 and T92, was evaluated by CERT (constant extension rate test) method. T91 specimens were tested at 500, 550 and 600 .deg. C in a fully deaerated SCW (below 10 ppb D.O), and SCC did not happen in the T91 specimens. T92 specimens were tested at 500 .deg. C in SCW of different

  12. Developing and Evaluating Candidate Materials for Generation IV Supercritical Water Reactors

    Energy Technology Data Exchange (ETDEWEB)

    Jang, Jin Sung; Kim, Sung Ho; Hwang Sung Sik and others

    2006-03-15

    High temperature mechanical behavior High temperature behavior of two F-M steels were investigated, considering the transient temperature range of the SCWR (above 800 .deg. C). T91 and T122 specimens were five times cyclically heat treated to the temperature 810 .deg. C and 845 .deg. C respectively. And the heat treatments were found to have little effect on the creep rupture behavior at 550, 600, or 650 .deg. C. However, the microstructural change was detected by the rapid hardness change after the holding the specimens at 840 .deg. C even for 10 sec. (by INL, previously ANL-W) A 20Cr Fe-base ODS alloy (MA956) was isothermally heat treated at 475 .deg. C for various times and then impact tested. The material was found to become very brittle after the heat treatment even for 100 hrs by the drastic decrease of the impact absorption energy (from 300 J to about the nil) and by the typically brittle fracture surface. (by KAIST) Corrosion and SCC Behavior in SCW (1) The corrosion behaviors of the F-M steels (T91, T92, and T122) and high Ni alloys (alloy 625, Alloy 690, and alloy 800H) and an ODS alloy (MA 956) were studied in the aerated SCW (8 ppm of D.O; dissolved oxygen) under 25 MPa from 300 to 600 .deg. C with an interval of 50 .deg. C. The test durations were 100, 200, and 500 hrs respectively. In general high Ni alloys were definitely more resistant to corrosion in SCW than F-M steels. As the Cr content increases the resistance of F-M steels to corrosion becomes better. The resistance of F-M steels to corrosion at 350 .deg. C, a subcritical temperature, was revealed to be comparatively similar to those at 550 .deg. C, a 200 .deg. C higher temperature. (2) The SCC resistance of F-M steels, T91 and T92, was evaluated by CERT (constant extension rate test) method. T91 specimens were tested at 500, 550 and 600 .deg. C in a fully deaerated SCW (below 10 ppb D.O), and SCC did not happen in the T91 specimens. T92 specimens were tested at 500 .deg. C in SCW of different

  13. Quantifying nonhomogeneous colors in agricultural materials. Part II: comparison of machine vision and sensory panel evaluations.

    Science.gov (United States)

    Balaban, M O; Aparicio, J; Zotarelli, M; Sims, C

    2008-11-01

    The average colors of mangos and apples were measured using machine vision. A method to quantify the perception of nonhomogeneous colors by sensory panelists was developed. Three colors out of several reference colors and their perceived percentage of the total sample area were selected by untrained panelists. Differences between the average colors perceived by panelists and those from the machine vision were reported as DeltaE values (color difference error). Effects of nonhomogeneity of color, and using real samples or their images in the sensory panels on DeltaE were evaluated. In general, samples with more nonuniform colors had higher DeltaE values, suggesting that panelists had more difficulty in evaluating more nonhomogeneous colors. There was no significant difference in DeltaE values between the real fruits and their screen image, therefore images can be used to evaluate color instead of the real samples.

  14. Improvement of Nuclear Heating Evaluation Inside the Core of the OSIRIS Material Testing Reactor

    Science.gov (United States)

    Péron, Arthur; Malouch, Fadhel; Diop, Cheikh M.

    2016-02-01

    In this paper we present a nuclear heating from neutron and photon rays calculation scheme mainly based on the Monte-Carlo neutral particle transport code TRIPOLI-4® which takes into account the axial distributions of fuel element compositions. This calculation scheme is applied to the OSIRIS reactor in order to evaluate the effect of using realistic axially heterogeneous compositions instead of uniform ones. After a description of nuclear heating evaluation, the calculation scheme is described. Numerical simulations and related results are detailed and analysed to determine the impact of axially heterogeneous compositions on fluxes, power and nuclear heating.

  15. Evaluation of surgical implantation of electronic tags in European eel and effects of different suture materials

    DEFF Research Database (Denmark)

    Thorstad, Eva B.; Økland, Finn; Westerberg, Håkan;

    2013-01-01

    Effects of implanting data-storage tags in European eel, Anguilla anguilla, and the suitability of different suture materials (braided permanent silk, permanent monofilament, absorbable and absorbable antibacterial) were examined. The tags consisted of an electronic unit and three floats on a wire......, making them flexible and able to follow the swimming movements of the eel. No mortality occurred, and tagged fish did not differ from the control fish in growth. Sutures were shed or dissolved slowly. After 4 weeks, there was no difference among the groups in the proportion of sutures left. After 6....... Antibacterial treatment had no effect on inflammation or healing rates. After 6 months, the tag started to become expelled through the incision in five fish (12%). The internal reaction appeared stronger around the floats, suggesting that the coating material of the floats created a tissue reaction, which...

  16. Physical interpretation and application of principles of ultrasonic nondestructive evaluation of high-performance materials

    Science.gov (United States)

    Miller, James G.

    1990-01-01

    An ultrasonic measurement system employed in the experimental interrogation of the anisotropic properties (through the measurement of the elastic stiffness constants) of the uniaxial graphite-epoxy composites is presented. The continuing effort for the development of improved visualization techniques for physical parameters is discussed. The background is set for the understanding and visualization of the relationship between the phase and energy/group velocity for propagation in high-performance anisotropic materials by investigating the general requirements imposed by the classical wave equation. The consequences are considered when the physical parameters of the anisotropic material are inserted into the classical wave equation by a linear elastic model. The relationship is described between the phase velocity and the energy/group velocity three dimensional surfaces through graphical techniques.

  17. Complex evaluation of properties for some thermal insulating materials of NPP

    International Nuclear Information System (INIS)

    The effects of the main operational factors (temperature, ionizing radiation, increased humidity) on some most widely applied fibrous materials are investigated. The samples were irradiated by 60Co gamma photons at the PKhM-gamma-20 device in air at temperature of 40±1 deg C in order to analyze the radiation resistance of thermal insulating materials. The analysis and generalization of the results of laboratory tests give an opportunity to make the following conclusions. The thermal insulation articles and constructions made of superfine basalt fiber may be used in the zones of rigorous regime. The superfine glass fibers (GF) are recommended to be used for equipment and pipeline shielding in the zones of rigorous control only as a part of multilayer insulation as the second or next layers and only in places where leaks are impossible

  18. Electromagnetic Nondestructive Evaluation of Wire Insulation and Models of Insulation Material Properties

    Science.gov (United States)

    Bowler, Nicola; Kessler, Michael R.; Li, Li; Hondred, Peter R.; Chen, Tianming

    2012-01-01

    Polymers have been widely used as wiring electrical insulation materials in space/air-craft. The dielectric properties of insulation polymers can change over time, however, due to various aging processes such as exposure to heat, humidity and mechanical stress. Therefore, the study of polymers used in electrical insulation of wiring is important to the aerospace industry due to potential loss of life and aircraft in the event of an electrical fire caused by breakdown of wiring insulation. Part of this research is focused on studying the mechanisms of various environmental aging process of the polymers used in electrical wiring insulation and the ways in which their dielectric properties change as the material is subject to the aging processes. The other part of the project is to determine the feasibility of a new capacitive nondestructive testing method to indicate degradation in the wiring insulation, by measuring its permittivity.

  19. Long-term environmental effects and flight service evaluation of composite materials

    Science.gov (United States)

    Dexter, H. Benson

    1987-01-01

    Results of a NASA-Langley sponsored research program to establish the long term effects of realistic flight environments and ground based exposure on advanced composite materials are presented. The effects of moisture, ultraviolet radiation, aircraft fuels and fluids, sustained stress, and fatigue loading are reported. Residual strength and stiffness as a function of exposure time and exposure location are reported for seven different material systems after 10 years of worldwide outdoor exposure. Flight service results of over 300 composite components installed on rotorcraft and transport aircraft are included. Over 4 million total component flight hours were accumulated on various aircraft since initiation of flight service in 1973. Service performance, maintenance characteristics, and residual strength of numerous composite components installed on commercial and military aircraft are reported as a function of flight hours and years in service. Residual strength test results of graphite/epoxy spoilers with 10 years of worldwide service and over 28,000 flight hours are reported.

  20. Evaluation of pitches and cokes from solvent-extracted coal materials

    Energy Technology Data Exchange (ETDEWEB)

    McHenry, E.R.

    1996-12-01

    Three initial coal-extracted (C-E) samples were received from the West Virginia University (WVU) Chemical Engineering Department. Two samples had been hydrogenated to obtain pitches that satisfy Theological requirements. One of the hydrogenated (HC-E) samples had been extracted by toluene to remove ash and higher molecular weight aromatic compounds. We were unable to measure the softening point and viscosity of the non-hydro treated solid extract sample, Positive characteristics in the HC-E materials were softening points of 113-119{degrees}C, low sulfur and ash. The oxygen and nitrogen content of the HC-E samples may limit future usage in premium carbon and graphite products. Coking values were similar to petroleum pitches. Laboratory anode testing indicates that in combination with standard coal-tar pitch, the HC-E material can be used as a binder pitch.