Acoustic emission monitoring of the bending under tension test

DEFF Research Database (Denmark)

Moghadam, Marcel; Sulaiman, Mohd Hafis Bin; Christiansen, Peter

2017-01-01

Preliminary investigations have shown that acoustic emission has promising aspects as an online monitoring technique for assessment of tribological conditions during metal forming as regards to determination of the onset of galling. In the present study the acoustic emission measuring technique h...... in BUT testing has been found to describe the frictional conditions during forming well and to allow for accurate assessment of the limits of lubrication....... been applied for online monitoring of the frictional conditions experienced during Bending Under Tension (BUT) testing. The BUT test emulates the forming conditions experienced when drawing sheet material over a die curvature as in deep drawing processes. Monitoring of the developed acoustic emission...

Potential of acoustic monitoring for safety assessment of primary system

International Nuclear Information System (INIS)

Olma, B.J.

1997-01-01

Safety assessment of the primary system and its components with respect to their mechanical integrity is increasingly supported by acoustic signature analysis during power operation of the plants. Acoustic signals of Loose Parts Monitoring System sensors are continuously monitored by dedicated digital systems for signal bursts associated with metallic impacts. Several years of ISTec/GRS experience and the practical use of its digital systems MEDEA and RAMSES have shown that acoustic monitoring is very successful for detecting component failures at an early stage. Advanced powerful tools for classification and acoustic evaluation of burst signals have recently been realized. The paper presents diagnosis experiences of BWR's and PWR's safety assessment. (author). 7 refs, 8 figs

Acoustic Techniques for Structural Health Monitoring

Science.gov (United States)

Frankenstein, B.; Augustin, J.; Hentschel, D.; Schubert, F.; Köhler, B.; Meyendorf, N.

2008-02-01

Future safety and maintenance strategies for industrial components and vehicles are based on combinations of monitoring systems that are permanently attached to or embedded in the structure, and periodic inspections. The latter belongs to conventional nondestructive evaluation (NDE) and can be enhanced or partially replaced by structural health monitoring systems. However, the main benefit of this technology for the future will consist of systems that can be differently designed based on improved safety philosophies, including continuous monitoring. This approach will increase the efficiency of inspection procedures at reduced inspection times. The Fraunhofer IZFP Dresden Branch has developed network nodes, miniaturized transmitter and receiver systems for active and passive acoustical techniques and sensor systems that can be attached to or embedded into components or structures. These systems have been used to demonstrate intelligent sensor networks for the monitoring of aerospace structures, railway systems, wind energy generators, piping system and other components. Material discontinuities and flaws have been detected and monitored during full scale fatigue testing. This paper will discuss opportunities and future trends in nondestructive evaluation and health monitoring based on new sensor principles and advanced microelectronics. It will outline various application examples of monitoring systems based on acoustic techniques and will indicate further needs for research and development.

Acoustic emission monitoring of HFIR vessel during hydrostatic testing

International Nuclear Information System (INIS)

Friesel, M.A.; Dawson, J.F.

1992-08-01

This report discusses the results and conclusions reached from applying acoustic emission monitoring to surveillance of the High Flux Isotope Reactor vessel during pressure testing. The objective of the monitoring was to detect crack growth and/or fluid leakage should it occur during the pressure test. The report addresses the approach, acoustic emission instrumentation, installation, calibration, and test results

Experience with digital acoustic monitoring systems for PWRs and BWRs

International Nuclear Information System (INIS)

Olma, B.J.

1998-01-01

Substantial progress could be reached both in system technics and in application of digital acoustic monitoring systems for assessing mechanical integrity of reactor primary systems. For the surveillance of PWRs and BWRs during power operation of the plants, acoustic signals of Loose Parts Monitoring System sensors are continuously monitored for signal bursts associated with metallic impacts. ISTec/GRS experience with its digital systems MEDEA and RAMSES has shown that acoustic signature analysis is very successful for detecting component failures at an early stage. Methods for trending and classification of digital burst signals are shown, experience with their practical use will be presented. (author)

Acoustic Signature Monitoring and Management of Naval Platforms

NARCIS (Netherlands)

Basten, T.G.H.; Jong, C.A.F. de; Graafland, F.; Hof, J. van 't

2015-01-01

Acoustic signatures make naval platforms susceptible to detection by threat sensors. The variable operational conditions and lifespan of a platform cause variations in the acoustic signature. To deal with these variations, a real time signature monitoring capability is being developed, with advisory

Chemometrics review for chemical sensor development, task 7 report

International Nuclear Information System (INIS)

1994-05-01

This report, the seventh in a series on the evaluation of several chemical sensors for use in the U.S. Department of Energy's (DOE's) site characterization and monitoring programs, concentrates on the potential use of chemometrics techniques in analysis of sensor data. Chemometrics is the chemical discipline that uses mathematical, statistical, and other methods that employ formal logic to: design or select optimal measurement procedures and experiments and provide maximum relevant chemical information by analyzing chemical data. The report emphasizes the latter aspect. In a formal sense, two distinct phases are in chemometrics applications to analytical chemistry problems: (1) the exploratory data analysis phase and (2) the calibration and prediction phase. For use in real-world problems, it is wise to add a third aspect - the independent validation and verification phase. In practical applications, such as the ERWM work, and in order of decreasing difficulties, the most difficult tasks in chemometrics are: establishing the necessary infrastructure (to manage sampling records, data handling, and data storage and related aspects), exploring data analysis, and solving calibration problems, especially for nonlinear models. Chemometrics techniques are different for what are called zeroth-, first-, and second-order systems, and the details depend on the form of the assumed functional relationship between the measured response and the concentrations of components in mixtures. In general, linear relationships can be handled relatively easily, but nonlinear relationships can be difficult

Chemometrics review for chemical sensor development, task 7 report

Energy Technology Data Exchange (ETDEWEB)

NONE

1994-05-01

This report, the seventh in a series on the evaluation of several chemical sensors for use in the U.S. Department of Energy`s (DOE`s) site characterization and monitoring programs, concentrates on the potential use of chemometrics techniques in analysis of sensor data. Chemometrics is the chemical discipline that uses mathematical, statistical, and other methods that employ formal logic to: design or select optimal measurement procedures and experiments and provide maximum relevant chemical information by analyzing chemical data. The report emphasizes the latter aspect. In a formal sense, two distinct phases are in chemometrics applications to analytical chemistry problems: (1) the exploratory data analysis phase and (2) the calibration and prediction phase. For use in real-world problems, it is wise to add a third aspect - the independent validation and verification phase. In practical applications, such as the ERWM work, and in order of decreasing difficulties, the most difficult tasks in chemometrics are: establishing the necessary infrastructure (to manage sampling records, data handling, and data storage and related aspects), exploring data analysis, and solving calibration problems, especially for nonlinear models. Chemometrics techniques are different for what are called zeroth-, first-, and second-order systems, and the details depend on the form of the assumed functional relationship between the measured response and the concentrations of components in mixtures. In general, linear relationships can be handled relatively easily, but nonlinear relationships can be difficult.

Acoustic monitoring techniques for corrosion degradation in cemented waste canisters

International Nuclear Information System (INIS)

Naish, C.C.; Buttle, D.; Wallace-Sims, R.; O'Brien, T.M.

1991-01-01

This report describes work to investigate acoustic emission as a non-intrusive monitor of corrosion and degradation of cemented wasteforms where the waste is a potentially reactive metal. The acoustic data collected shows good correlation with the corrosion rate as measured by hydrogen gas evolution rates and the electrochemically measured corrosion rates post cement hardening. The technique has been shown to be sensitive in detecting stress caused by expansive corrosion product within the cemented wasteform. The attenuation of the acoustic signal by the wasteform reduced the signal received by the monitoring equipment by a factor of 10 over a distance of approximately 150-400 mm, dependent on the water level in the cement. Full size packages were successfully monitored. It is concluded that the technique offers good potential for monitoring cemented containers of the more reactive metals, for example Magnox and aluminium. (author)

A review of near infrared spectroscopy and chemometrics in pharmaceutical technologies.

Science.gov (United States)

Roggo, Yves; Chalus, Pascal; Maurer, Lene; Lema-Martinez, Carmen; Edmond, Aurélie; Jent, Nadine

2007-07-27

Near-infrared spectroscopy (NIRS) is a fast and non-destructive analytical method. Associated with chemometrics, it becomes a powerful tool for the pharmaceutical industry. Indeed, NIRS is suitable for analysis of solid, liquid and biotechnological pharmaceutical forms. Moreover, NIRS can be implemented during pharmaceutical development, in production for process monitoring or in quality control laboratories. This review focuses on chemometric techniques and pharmaceutical NIRS applications. The following topics are covered: qualitative analyses, quantitative methods and on-line applications. Theoretical and practical aspects are described with pharmaceutical examples of NIRS applications.

Design of acoustic emission monitoring system based on VC++

Science.gov (United States)

Yu, Yang; He, Wei

2015-12-01

At present, a lot of companies at home and abroad have researched and produced a batch of specialized monitoring instruments for acoustic emission (AE). Most of them cost highly and the system function exists in less stable and less portability for the testing environment and transmission distance and other aspects. Depending on the research background and the status quo, a dual channel intelligent acoustic emission monitoring system was designed based on Microsoft Foundation Classes in Visual Studio C++ to solve some of the problems in the acoustic emission research and meet the needs of actual monitoring task. It contains several modules such as main module, acquisition module, signal parameters setting module and so on. It could give out corrosion AE waveform and signal parameters results according to the main menu selected parameters. So the needed information could be extracted from the experiments datum to solve the problem deeply. This soft system is the important part of AE detection g system.

Chemometrics in spectroscopy

International Nuclear Information System (INIS)

Geladi, Paul; Sethson, Britta; Nystroem, Josefina; Lillhonga, Tom; Lestander, Torbjoern; Burger, Jim

2004-01-01

Some of the principles and main methods of chemometrics are illustrated by examples. The examples are from electrochemistry, process analytical chemistry and multivariate imaging. Principal component analysis, partial least squares regression and multivariate image analysis are used to illustrate the power of chemometrical thinking. The emphasis is on plotting and visualization for showing the salient features of a model or data set

Spectroscopic and chemometric exploration of food quality

DEFF Research Database (Denmark)

Pedersen, Dorthe Kjær

2002-01-01

and multi-way chemometrics demonstrated the potential for screening of environmental contamination in complex food samples. Significant prediction models were established with correlation coefficients in the range from r = 0.69 to r = 0.97 for dioxin. Further development of the fluorescence measurements......The desire to develop non-invasive rapid measurements of essential quality parameters in foods is the motivation of this thesis. Due to the speed and noninvasive properties of spectroscopic techniques, they have potential as on-line or atline methods and can be employed in the food industry...... in order to control the quality of the end product and to continuously monitor the production. In this thesis, the possibilities and limitations of the application of spectroscopy and chemometrics in rapid control of food quality are discussed and demonstrated by the examples in the eight included...

Mechanical Seal Opening Condition Monitoring Based on Acoustic Emission Technology

Directory of Open Access Journals (Sweden)

Erqing Zhang

2014-06-01

Full Text Available Since the measurement of mechanical sealing film thickness and just-lift-off time is very difficult, the sealing film condition monitoring method based on acoustic emission signal is proposed. The mechanical seal acoustic emission signal present obvious characteristics of time-varying nonlinear and pulsating. In this paper, the acoustic emission signal is used to monitor the seal end faces just-lift-off time and friction condition. The acoustic emission signal is decomposed by empirical mode decomposition into a series of intrinsic mode function with independent characteristics of different time scales and different frequency band. The acoustic emission signal only generated by end faces friction is obtained by eliminating the false intrinsic mode function components. The correlation coefficient of acoustic emission signal and Multi-scale Laplace Wavelet is calculated. It is proved that the maximum frequency (8000 Hz of the correlation coefficient is appeared at the spindle speed of 300 rpm. And at this time (300 rpm the end faces have just lifted off. By a set of mechanical oil seal running test, it is demonstrated that this method could accurately identify mechanical seal end faces just-lift-off time and friction condition.

A guide to processing bat acoustic data for the North American Bat Monitoring Program (NABat)

Science.gov (United States)

Reichert, Brian; Lausen, Cori; Loeb, Susan; Weller, Ted; Allen, Ryan; Britzke, Eric; Hohoff, Tara; Siemers, Jeremy; Burkholder, Braden; Herzog, Carl; Verant, Michelle

2018-06-14

The North American Bat Monitoring Program (NABat) aims to improve the state of conservation science for all species of bats shared by the United States, Canada, and Mexico. To accomplish this goal, NABat offers guidance and standardized protocols for acoustic monitoring of bats. In this document, “A Guide to Processing Bat Acoustic Data for the North American Bat Monitoring Program (NABat),” we provide general recommendations and specific workflows for the process of identifying bat species from acoustic files recorded using the NABat stationary point and mobile transect acoustic monitoring protocols.

Tools for automated acoustic monitoring within the R package monitoR

DEFF Research Database (Denmark)

Katz, Jonathan; Hafner, Sasha D.; Donovan, Therese

2016-01-01

The R package monitoR contains tools for managing an acoustic-monitoring program including survey metadata, template creation and manipulation, automated detection and results management. These tools are scalable for use with small projects as well as larger long-term projects and those...... with expansive spatial extents. Here, we describe typical workflow when using the tools in monitoR. Typical workflow utilizes a generic sequence of functions, with the option for either binary point matching or spectrogram cross-correlation detectors....

Tools for automated acoustic monitoring within the R package monitoR

Science.gov (United States)

Katz, Jonathan; Hafner, Sasha D.; Donovan, Therese

2016-01-01

The R package monitoR contains tools for managing an acoustic-monitoring program including survey metadata, template creation and manipulation, automated detection and results management. These tools are scalable for use with small projects as well as larger long-term projects and those with expansive spatial extents. Here, we describe typical workflow when using the tools in monitoR. Typical workflow utilizes a generic sequence of functions, with the option for either binary point matching or spectrogram cross-correlation detectors.

Acoustic emission monitoring during hydrotest of a thin wall pressure vessel

International Nuclear Information System (INIS)

Fontana, E.; Grugni, G.; Panzani, C.; Pirovano, B.; Possa, G.; Tonolini, F.

1976-01-01

Results are presented of the acoustic emission monitoring during hydrotests of a thin wall steel pressure vessel. Location of acoustic sources was based on longitudinal wave front detection. The careful calibration of the three sensors used for acoustic source location was found to be very useful, and allowed an accurate location error analysis. Acoustic emission in the hydrotests was found to be due mainly to stress release in weld seams

Analysis of acoustic data from the PFR SGU condition monitor

International Nuclear Information System (INIS)

Rowley, R.; Airey, J.

1990-01-01

This paper gives an outline description of an acoustic monitoring system which has been installed on the SGU of the Prototype Fast Reactor (PFR) at Dounreay with the objective of giving early warning of any change in noise output which could be related to potentially damaging vibrations within the units. Data obtained from this PFR monitoring system is playing an important part in the development of acoustic instrumentation for leak detection although this had not been the primary objective of this particular installation. The PFR has three secondary circuits each containing an evaporator, a superheater and a reheater giving a total of nine SGUs. Although the design of the units is different from that intended for EFR, the measurements provide a valuable source of information on the character and amplitude of acoustic background noise in operational steam generator units. The vibration monitoring system uses the waveguides originally installed during reactor commissioning for leak detection studies. Twelve acoustic waveguides are fitted to the shell of each of the units. The superheaters and reheaters have three waveguides at each of four axial levels, while the evaporators have four waveguides at each of three axial levels. In addition the evaporators have a small number of waveguides attached to the top flange of the unit. Each waveguide is fitted with an accelerometer to record the acoustic signal from the SGU. Tape recordings of the acoustic noise from each unit are made on a regular basis and the tapes analysed on an automated analysis system which has been developed to extract and store in a database about 20 characteristic features from the data. The paper gives examples of the background noise from the SGU. The data demonstrates the use of location techniques to identify prominent acoustic source. 8 figs

Passive acoustic monitoring of bed load for fluvial applications

Science.gov (United States)

The sediment transported as bed load in streams and rivers is notoriously difficult to monitor cheaply and accurately. Passive acoustic methods are relatively simple, inexpensive, and provide spatial integration along with high temporal resolution. In 1963 work began on monitoring emissions from par...

Acoustic monitoring to support plant life extension at Sellafield

International Nuclear Information System (INIS)

Wit, M. de; Hovhanessian, G.

2015-01-01

Tensioned steel wires are widely used in civil engineering structures. They can, however, be vulnerable to corrosion. To reduce the probability of corrosion, sophisticated protection systems are used. Extensive inspection and maintenance regimes are also able to be implemented to confirm that the design strength is available over the lifetime of the wires. These regimes include tests to confirm the condition of post-tensioning cables or stay cables, which can verify the overall performance of the structure. This paper presents a technology to detect and locate wire failures in tensioned cables for use on a wide variety of pre-stressed or post tensioned structures, where they have increased confidence in the structures and reduced maintenance costs. This methodology is the continuous acoustic monitoring technology which uses distinctive acoustic characteristics of wire breaks to separate them from other acoustic activity on the structure. With a combination of instrumentation, data acquisition and data management, it is possible to identify a wire break event, as well as to locate the position and time of the failure. Over 10 years' experience of acoustic monitoring for this application with several independent and blind tests, shows that even in noisy environments the acoustic monitoring method is able to identify and locate wire breaks in fully grouted and partially grouted tendons, stay cables and suspension cables. The design (number of sensors and location) is very important to be sure to cover all wires in the structure. This paper explains the principles of the systems and shows them in practice on a case study of a project in a pre-stressed roof structure of an active tank farm at Sellafield site

Acoustic Emission Behavior of Early Age Concrete Monitored by Embedded Sensors.

Science.gov (United States)

Qin, Lei; Ren, Hong-Wei; Dong, Bi-Qin; Xing, Feng

2014-10-02

Acoustic emission (AE) is capable of monitoring the cracking activities inside materials. In this study, embedded sensors were employed to monitor the AE behavior of early age concrete. Type 1-3 cement-based piezoelectric composites, which had lower mechanical quality factor and acoustic impedance, were fabricated and used to make sensors. Sensors made of the composites illustrated broadband frequency response. In a laboratory, the cracking of early age concrete was monitored to recognize different hydration stages. The sensors were also embedded in a mass concrete foundation to localize the temperature gradient cracks.

Non-Invasive Acoustic-Based Monitoring of Heavy Water and Uranium Process Solutions

Energy Technology Data Exchange (ETDEWEB)

Pantea, Cristian [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Sinha, Dipen N. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Lakis, Rollin Evan [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Beedle, Christopher Craig [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Davis, Eric Sean [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

2017-10-20

This presentation includes slides on Project Goals; Heavy Water Production Monitoring: A New Challenge for the IAEA; Noninvasive Measurements in SFAI Cell; Large Scatter in Literature Values; Large Scatter in Literature Values; Highest Precision Sound Speed Data Available: New Standard in H/D; ~400 pts of data; Noninvasive Measurements in SFAI Cell; New funding from NA241 SGTech; Uranium Solution Monitoring: Inspired by IAEA Challenge in Kazakhstan; Non-Invasive Acoustic-Based Monitoring of Uranium in Solutions; Non-Invasive Acoustic-Based Monitoring of Uranium in Solutions; and finally a summary.

Progress for on-line acoustic emission monitoring of cracks in reactor systems

International Nuclear Information System (INIS)

Hutton, P.H.; Friesel, M.A.; Kurtz, R.J.

1985-10-01

This paper reviews FY1985 accomplishments and FY1986 plans for the NRC sponsored research program concerned with ''Acoustic Emission/Flaw Relationships for Inservice Monitoring of Nuclear Reactor Pressure Boundaries''. The objective of the acoustic emission (AE) monitoring program is to develop and validate the use of AE methods for continuous surveillance of reactor pressure boundaries to detect flaw growth. Topics discussed include testing AE monitoring on reactors, refinement of an AE signal identification relationship, study of slow crack growth rate effects on AE generation, and activity to produce an ASTM standard for AE monitoring and to gain ASME code acceptance of AE monitoring

Chemometrics: A new scenario in herbal drug standardization

Directory of Open Access Journals (Sweden)

Ankit Bansal

2014-08-01

Full Text Available Chromatography and spectroscopy techniques are the most commonly used methods in standardization of herbal medicines but the herbal system is not easy to analyze because of their complexity of chemical composition. Many cutting-edge analytical technologies have been introduced to evaluate the quality of medicinal plants and significant amount of measurement data has been produced. Chemometric techniques provide a good opportunity for mining more useful chemical information from the original data. Then, the application of chemometrics in the field of medicinal plants is spontaneous and necessary. Comprehensive methods and hyphenated techniques associated with chemometrics used for extracting useful information and supplying various methods of data processing are now more and more widely used in medicinal plants, among which chemometrics resolution methods and principal component analysis (PCA are most commonly used techniques. This review focuses on the recent various important analytical techniques, important chemometrics tools and interpretation of results by PCA, and applications of chemometrics in quality evaluation of medicinal plants in the authenticity, efficacy and consistency. Key words: Chemometrics, HELP, Herbal drugs, PCA, OPA

Acoustic emission monitoring during hydrotests of a thin wall pressure vessel

International Nuclear Information System (INIS)

Fontana, E.; Grugni, G.; Panzani, C.; Pirovano, B.; Possa, G.; Tonolini, F.

1975-01-01

The results are presented of an acoustic emission monitoring performed during hydrotests of a thin wall steel pressure vessel. The location of acoustic sources was based on longitudinal wave front detection. The careful calibration of the three sensors instrumentation system used for acoustic source location was found to be useful, and alllowed an accurate location error analysis. Acoustic emission in the hydrotests was found to be mainly due to stress release in weld seams. (Fontana, E.; Grugni, G.; Panzani, C.; Pirovano, B.; Possa, G.; Tonolini, F.)

Acoustic monitoring system to quantify ingestive behavior of free-grazing cattle

Science.gov (United States)

Methods to estimate intake in grazing livestock include using markers, visual observation, mechanical sensors that respond to jaw movement and acoustic recording. In most of the acoustic monitoring studies, the microphone is inverted on the forehead of the grazing livestock and the skull is utilize...

Flaw evolution monitoring by acoustic emission technique

International Nuclear Information System (INIS)

Ghia, S.; Sala, A.; Lucia, A.

1986-01-01

Flaw evolution monitoring during mechanical fatigue test has been performed by acoustic emission (AE) technique. Testing on 1:5 reduced scale vessel containing fabrication defects was carried out in the frame of an European program for pressure component residual life evaluation. Characteristics of AE signals associated to flaw evolution are discussed

Surface Acoustic Wave Monitor for Deposition and Analysis of Ultra-Thin Films

Science.gov (United States)

Hines, Jacqueline H. (Inventor)

2015-01-01

A surface acoustic wave (SAW) based thin film deposition monitor device and system for monitoring the deposition of ultra-thin films and nanomaterials and the analysis thereof is characterized by acoustic wave device embodiments that include differential delay line device designs, and which can optionally have integral reference devices fabricated on the same substrate as the sensing device, or on a separate device in thermal contact with the film monitoring/analysis device, in order to provide inherently temperature compensated measurements. These deposition monitor and analysis devices can include inherent temperature compensation, higher sensitivity to surface interactions than quartz crystal microbalance (QCM) devices, and the ability to operate at extreme temperatures.

Acoustic emission/flaw relationships for inservice monitoring of LWRs

International Nuclear Information System (INIS)

Hutton, P.H.; Kurtz, R.J.; Friesel, M.A.; Skorpik, J.R.; Dawson, J.F.

1991-10-01

The program concerning Acoustic Emission/Flaw Relationships for Inservice Monitoring of LWRs was initiated in FY76 with the objective of validating the application of acoustic emission (AE) to monitor nuclear reactor pressure-containing components during operation to detect cracking. The program has been supported by the US Nuclear Regulatory Commission, Office of Nuclear Regulatory Research. Research and development has been performed by Pacific Northwest Laboratory, operated for the Department of Energy by Battelle Memorial Institute. The program has shown the feasibility of continuous, on-line AE monitoring to detect crack growth and produced validated methods for applying the technology. Included are relationships for estimating flaw severity from AE data and field applications at Watts Bar Unit 1 Reactor, Limerick Unit 1 Reactor, and the High Flux Isotope Reactor. This report discusses the program scope and organization, the three program phases and the results obtained, standard and code activities, and instrumentation and software developed under this program

Acoustic-wave sensor for ambient monitoring of a photoresist-stripping agent

Science.gov (United States)

Pfeifer, K.B.; Hoyt, A.E.; Frye, G.C.

1998-08-18

The acoustic-wave sensor is disclosed. The acoustic-wave sensor is designed for ambient or vapor-phase monitoring of a photoresist-stripping agent such as N-methylpyrrolidinone (NMP), ethoxyethylpropionate (EEP) or the like. The acoustic-wave sensor comprises an acoustic-wave device such as a surface-acoustic-wave (SAW) device, a flexural-plate-wave (FPW) device, an acoustic-plate-mode (APM) device, or a thickness-shear-mode (TSM) device (also termed a quartz crystal microbalance or QCM) having a sensing region on a surface thereof. The sensing region includes a sensing film for sorbing a quantity of the photoresist-stripping agent, thereby altering or shifting a frequency of oscillation of an acoustic wave propagating through the sensing region for indicating an ambient concentration of the agent. According to preferred embodiments of the invention, the acoustic-wave device is a SAW device; and the sensing film comprises poly(vinylacetate), poly(N-vinylpyrrolidinone), or poly(vinylphenol). 3 figs.

Acoustic monitoring of a fluidized bed coating process

DEFF Research Database (Denmark)

Naelapaa, Kaisa; Veski, Peep; Pedersen, Joan G.

2007-01-01

  The aim of the study was to investigate the potential of acoustic monitoring of a production scale fluidized bed coating process. The correlation between sensor signals and the estimated amount of film applied and percentage release, respectively, were investigated in coating potassium chloride...

Acoustical monitoring of diesel engines in reverberant environment

International Nuclear Information System (INIS)

Mein, M.

1995-10-01

The feed-back knowledge of emergency diesel generators in nuclear power plants shows that some malfunctions, mainly affecting fuel-injection or distribution system of the engine can be heard and detected by experienced maintenance agents. This study consists in the feasibility,v of acoustical monitoring of those diesel engines, taking into account the reverberant environment of the machine. The operating cycle of the diesel is composed of transient events (injection, combustion, valve closure...) which generate highly non stationary acoustical signals. The detection of a malfunction appearing on such transients requires the use of adapted signal processing techniques. Visual analysis of the phenomena is first proceeded using time-frequency and time-scale representations. The second step will be parametric modeling of acoustical signatures for the extraction of characteristic parameters, in order to characterize the fault and to use an automatic classification system. The lest part of the study will concern the evaluation of the robustness of the detection methods in regard to acoustical reverberation. (author). 10 refs., 6 figs

Monitoring of drilling process with the application of acoustic signal

Directory of Open Access Journals (Sweden)

Labaš Milan

2000-09-01

Full Text Available Monitoring of rock disintegration process at drilling, scanning of input quantities: thrust F, revolution n and the course of some output quantities: the drilling rate v and the power input P are needed for the control of this process. We can calculate the specific volume work of rock disintegration w and ϕ - quotient of drilling rate v and the specific volume work of disintegration w from the presented quantities.Works on an expertimental stand showed that the correlation relationships between the input and output quantities can be found by scanning the accompanying sound of the drilling proces.Research of the rock disintegration with small-diameter diamond drill tools and different rock types is done at the Institute of Geotechnics. The aim of this research is the possibility of monitoring and controlling the rock disintegration process with the application of acoustic signal. The acoustic vibrations accompanying the drilling process are recorded by a microphone placed in a defined position in the acoustic space. The drilling device (drilling stand, the drilling tool and the rock are the source of sound. Two basic sound states exist in the drilling stand research : the noise at no-load running and the noise at the rotary drilling of rock. Suitable quantities for optimizing the rock disintegration process are searched by the study of the acoustic signal. The dominant frequencies that characterize the disintegration process for the given rock and tool are searched by the analysis of the acoustic signal. The analysis of dominant frequencies indicates the possibility of determining an optimal regime for the maximal drilling rate. Extreme of the specific disintegration energy is determinated by the dispersion of the dominant frequency.The scanned acoustic signal is processed by the Fourier transformation. The Fourier transformation facilitates the distribution of the general non-harmonic periodic process into harmonic components. The harmonic

Real Time Monitoring of Containerless Microreactions in Acoustically Levitated Droplets via Ambient Ionization Mass Spectrometry.

Science.gov (United States)

Crawford, Elizabeth A; Esen, Cemal; Volmer, Dietrich A

2016-09-06

Direct in-droplet (in stillo) microreaction monitoring using acoustically levitated micro droplets has been achieved by combining acoustic (ultrasonic) levitation for the first time with real time ambient tandem mass spectrometry (MS/MS). The acoustic levitation and inherent mixing of microliter volumes of reactants (3 μL droplets), yielding total reaction volumes of 6 μL, supported monitoring the acid-catalyzed degradation reaction of erythromycin A. This reaction was chosen to demonstrate the proof-of-principle of directly monitoring in stillo microreactions via hyphenated acoustic levitation and ambient ionization mass spectrometry. The microreactions took place completely in stillo over 30, 60, and 120 s within the containerless stable central pressure node of an acoustic levitator, thus readily promoting reaction miniaturization. For the evaluation of the miniaturized in stillo reactions, the degradation reactions were also carried out in vials (in vitro) with a total reaction volume of 400 μL. The reacted in vitro mixtures (6 μL total) were similarly introduced into the acoustic levitator prior to ambient ionization MS/MS analysis. The in stillo miniaturized reactions provided immediate real-time snap-shots of the degradation process for more accurate reaction monitoring and used a fraction of the reactants, while the larger scale in vitro reactions only yielded general reaction information.

Efficacy of extracting indices from large-scale acoustic recordings to monitor biodiversity.

Science.gov (United States)

Buxton, Rachel; McKenna, Megan F; Clapp, Mary; Meyer, Erik; Stabenau, Erik; Angeloni, Lisa M; Crooks, Kevin; Wittemyer, George

2018-04-20

Passive acoustic monitoring has the potential to be a powerful approach for assessing biodiversity across large spatial and temporal scales. However, extracting meaningful information from recordings can be prohibitively time consuming. Acoustic indices offer a relatively rapid method for processing acoustic data and are increasingly used to characterize biological communities. We examine the ability of acoustic indices to predict the diversity and abundance of biological sounds within recordings. First we reviewed the acoustic index literature and found that over 60 indices have been applied to a range of objectives with varying success. We then implemented a subset of the most successful indices on acoustic data collected at 43 sites in temperate terrestrial and tropical marine habitats across the continental U.S., developing a predictive model of the diversity of animal sounds observed in recordings. For terrestrial recordings, random forest models using a suite of acoustic indices as covariates predicted Shannon diversity, richness, and total number of biological sounds with high accuracy (R 2 > = 0.94, mean squared error MSE indices assessed, roughness, acoustic activity, and acoustic richness contributed most to the predictive ability of models. Performance of index models was negatively impacted by insect, weather, and anthropogenic sounds. For marine recordings, random forest models predicted Shannon diversity, richness, and total number of biological sounds with low accuracy (R 2 = 195), indicating that alternative methods are necessary in marine habitats. Our results suggest that using a combination of relevant indices in a flexible model can accurately predict the diversity of biological sounds in temperate terrestrial acoustic recordings. Thus, acoustic approaches could be an important contribution to biodiversity monitoring in some habitats in the face of accelerating human-caused ecological change. This article is protected by copyright. All rights

Between-hole acoustic surveying and monitoring of a granitic rock mass

International Nuclear Information System (INIS)

Paulsson, B.N.P.; King, M.S.

1980-02-01

The purpose of this technical note is to present preliminary results of an acoustic monitoring study performed as part of a comprehensive rock mechanic and geophysics research program (Ref.20) associated with large-scale heater tests in an abandoned iron-ore mine in central Sweden. The investigation was performed in a fractured granitic rock mass at a sub-surface depth of 340 m, in a drift adjacent to the original iron-ore mine workings. Acoustic monitoring took place between four empty, dry, vertical boreholes of 10 m depth spaced in the vicinity of a vertical heater borehole in the floor of a drift

Report on Non-invasive acoustic monitoring of D2O concentration Oct 31 2017

Energy Technology Data Exchange (ETDEWEB)

Pantea, Cristian [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Sinha, Dipen N. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Lakis, Rollin Evan [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Beedle, Christopher Craig [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Davis, Eric Sean [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

2017-11-06

There is an urgent need for real-time monitoring of the hydrogen /deuterium ratio (H/D) for heavy water production monitoring. Based upon published literature, sound speed is sensitive to the deuterium content of heavy water and can be measured using existing acoustic methods to determine the deuterium concentration in heavy water solutions. We plan to adapt existing non-invasive acoustic techniques (Swept-Frequency Acoustic Interferometry and Gaussian-pulse acoustic technique) for the purpose of quantifying H/D ratios in solution. A successful demonstration will provide an easily implemented, low cost, and non-invasive method for remote and unattended H/D ratio measurements with a resolution of less than 0.2% vol.

Acoustic impedance rhinometry (AIR): a technique for monitoring dynamic changes in nasal congestion

International Nuclear Information System (INIS)

Patuzzi, Robert; Cook, Alison

2014-01-01

We describe a simple and inexpensive method for monitoring nasal air flow resistance using measurement of the small-signal acoustic input impedance of the nasal passage, similar to the audiological measurement of ear drum compliance with acoustic tympanometry. The method requires generation of a fixed sinusoidal volume–velocity stimulus using ear-bud speakers, and an electret microphone to monitor the resultant pressure fluctuation in the nasal passage. Both are coupled to the nose via high impedance silastic tubing and a small plastic nose insert. The acoustic impedance is monitored in real-time using a laptop soundcard and custom-written software developed in LabView 7.0 (National Instruments). The compact, lightweight equipment and fast time resolution lends the technique to research into the small and rapid reflexive changes in nasal resistance caused by environmental and local neurological influences. The acoustic impedance rhinometry technique has the potential to be developed for use in a clinical setting, where the need exists for a simple and inexpensive objective nasal resistance measurement technique. (paper)

Spatial assessment and source identification of heavy metals pollution in surface water using several chemometric techniques.

Science.gov (United States)

Ismail, Azimah; Toriman, Mohd Ekhwan; Juahir, Hafizan; Zain, Sharifuddin Md; Habir, Nur Liyana Abdul; Retnam, Ananthy; Kamaruddin, Mohd Khairul Amri; Umar, Roslan; Azid, Azman

2016-05-15

This study presents the determination of the spatial variation and source identification of heavy metal pollution in surface water along the Straits of Malacca using several chemometric techniques. Clustering and discrimination of heavy metal compounds in surface water into two groups (northern and southern regions) are observed according to level of concentrations via the application of chemometric techniques. Principal component analysis (PCA) demonstrates that Cu and Cr dominate the source apportionment in northern region with a total variance of 57.62% and is identified with mining and shipping activities. These are the major contamination contributors in the Straits. Land-based pollution originating from vehicular emission with a total variance of 59.43% is attributed to the high level of Pb concentration in the southern region. The results revealed that one state representing each cluster (northern and southern regions) is significant as the main location for investigating heavy metal concentration in the Straits of Malacca which would save monitoring cost and time. The monitoring of spatial variation and source of heavy metals pollution at the northern and southern regions of the Straits of Malacca, Malaysia, using chemometric analysis. Copyright © 2015 Elsevier Ltd. All rights reserved.

Monitoring of diesel engine combustions based on the acoustic source characterisation of the exhaust system

Science.gov (United States)

Jiang, J.; Gu, F.; Gennish, R.; Moore, D. J.; Harris, G.; Ball, A. D.

2008-08-01

Acoustic methods are among the most useful techniques for monitoring the condition of machines. However, the influence of background noise is a major issue in implementing this method. This paper introduces an effective monitoring approach to diesel engine combustion based on acoustic one-port source theory and exhaust acoustic measurements. It has been found that the strength, in terms of pressure, of the engine acoustic source is able to provide a more accurate representation of the engine combustion because it is obtained by minimising the reflection effects in the exhaust system. A multi-load acoustic method was then developed to determine the pressure signal when a four-cylinder diesel engine was tested with faults in the fuel injector and exhaust valve. From the experimental results, it is shown that a two-load acoustic method is sufficient to permit the detection and diagnosis of abnormalities in the pressure signal, caused by the faults. This then provides a novel and yet reliable method to achieve condition monitoring of diesel engines even if they operate in high noise environments such as standby power stations and vessel chambers.

Listening to the Deep: Live monitoring of ocean noise and cetacean acoustic signals

OpenAIRE

André, Michel; Van der Schaar, Mike Connor Roger Malcolm; Zaugg, Serge Alain; Houégnigan, Ludwig; Sánchez, A.M.; Castell, Joan

2011-01-01

The development and broad use of passive acoustic monitoring techniques have the potential to help assessing the large-scale influence of artificial noise on marine organisms and ecosystems. Deep-sea observatories have the potential to play a key role in understanding these recent acoustic changes. LIDO(Listening to the Deep Ocean Environment) is an international project that is allowing the real-time longterm monitoring of marine ambient noise as well as marine mammal sounds at cabled and...

Automatic acoustic and vibration monitoring system for nuclear power plants

International Nuclear Information System (INIS)

Tothmatyas, Istvan; Illenyi, Andras; Kiss, Jozsef; Komaromi, Tibor; Nagy, Istvan; Olchvary, Geza

1990-01-01

A diagnostic system for nuclear power plant monitoring is described. Acoustic and vibration diagnostics can be applied to monitor various reactor components and auxiliary equipment including primary circuit machinery, leak detection, integrity of reactor vessel, loose parts monitoring. A noise diagnostic system has been developed for the Paks Nuclear Power Plant, to supervise the vibration state of primary circuit machinery. An automatic data acquisition and processing system is described for digitalizing and analysing diagnostic signals. (R.P.) 3 figs

Acoustic wave simulation using an overset grid for the global monitoring system

Science.gov (United States)

Kushida, N.; Le Bras, R.

2017-12-01

The International Monitoring System of the Comprehensive Nuclear-Test-Ban Treaty Organization (CTBTO) has been monitoring hydro-acoustic and infrasound waves over the globe. Because of the complex natures of the oceans and the atmosphere, computer simulation can play an important role in understanding the observed signals. In this regard, methods which depend on partial differential equations and require minimum modelling, are preferable. So far, to our best knowledge, acoustic wave propagation simulations based on partial differential equations on such a large scale have not been performed (pp 147 - 161 of ref [1], [2]). The main difficulties in building such simulation codes are: (1) considering the inhomogeneity of medium including background flows, (2) high aspect ratio of computational domain, (3) stability during long time integration. To overcome these difficulties, we employ a two-dimensional finite different (FDM) scheme on spherical coordinates with the Yin-Yang overset grid[3] solving the governing equation of acoustic waves introduces by Ostashev et. al.[4]. The comparison with real recording examples in hydro-acoustic will be presented at the conference. [1] Paul C. Etter: Underwater Acoustic Modeling and Simulation, Fourth Edition, CRC Press, 2013. [2] LIAN WANG et. al.: REVIEW OF UNDERWATER ACOUSTIC PROPAGATION MODELS, NPL Report AC 12, 2014. [3] A. Kageyama and T. Sato: "Yin-Yang grid": An overset grid in spherical geometry, Geochem. Geophys. Geosyst., 5, Q09005, 2004. [4] Vladimir E. Ostashev et. al: Equations for finite-difference, time-domain simulation of sound propagation in moving inhomogeneous media and numerical implementation, Acoustical Society of America. DOI: 10.1121/1.1841531, 2005.

Listening to the Deep: live monitoring of ocean noise and cetacean acoustic signals.

Science.gov (United States)

André, M; van der Schaar, M; Zaugg, S; Houégnigan, L; Sánchez, A M; Castell, J V

2011-01-01

The development and broad use of passive acoustic monitoring techniques have the potential to help assessing the large-scale influence of artificial noise on marine organisms and ecosystems. Deep-sea observatories have the potential to play a key role in understanding these recent acoustic changes. LIDO (Listening to the Deep Ocean Environment) is an international project that is allowing the real-time long-term monitoring of marine ambient noise as well as marine mammal sounds at cabled and standalone observatories. Here, we present the overall development of the project and the use of passive acoustic monitoring (PAM) techniques to provide the scientific community with real-time data at large spatial and temporal scales. Special attention is given to the extraction and identification of high frequency cetacean echolocation signals given the relevance of detecting target species, e.g. beaked whales, in mitigation processes, e.g. during military exercises. Copyright © 2011. Published by Elsevier Ltd.

Large hoisting machinery local damage acoustic emission monitoring of optical information acquisition research

Directory of Open Access Journals (Sweden)

Wan Shuai

2016-01-01

Full Text Available AE technology, an advanced fault diagnosis technique,is impacted by environmental noise during monitoring equipment. The occurrence of interfere noise,the fashion of interfere and the effect to the system in the AE automatic online monitoring system is analyzed. At present, most of the acoustic emission signal transmission by cable, this way of transmission has a limited transmission distance, shortcomings and so on signal easily disturbed. Is proposed in this paper based on the optical fiber transmission technology, designed and developed a information collection system based on optical fiber acoustic emission monitoring.This way has the advantages of long distance transmission, strong anti-jamming capability.

Online monitoring of the two-dimensional temperature field in a boiler furnace based on acoustic computed tomography

International Nuclear Information System (INIS)

Zhang, Shiping; Shen, Guoqing; An, Liansuo; Niu, Yuguang

2015-01-01

Online monitoring of the temperature field is crucial to optimally adjust combustion within a boiler. In this paper, acoustic computed tomography (CT) technology was used to obtain the temperature profile of a furnace cross-section. The physical principles behind acoustic CT, acoustic signals and time delay estimation were studied. Then, the technique was applied to a domestic 600-MW coal-fired boiler. Acoustic CT technology was used to monitor the temperature field of the cross-section in the boiler furnace, and the temperature profile was reconstructed through ART iteration. The linear sweeping frequency signal was adopted as the sound source signal, whose sweeping frequency ranged from 500 to 3000 Hz with a sweeping cycle of 0.1 s. The generalized cross-correlation techniques with PHAT and ML were used as the time delay estimation method when the boiler was in different states. Its actual operation indicated that the monitored images accurately represented the combustion state of the boiler, and the acoustic CT system was determined to be accurate and reliable. - Highlights: • An online monitoring approach to monitor temperature field in a boiler furnace. • The paper provides acoustic CT technology to obtain the temperature profile of a furnace cross-section. • The temperature profile was reconstructed through ART iteration. • The technique is applied to a domestic 600-MW coal-fired boiler. • The monitored images accurately represent the combustion state of the boiler

A Flexible Acoustic Sensor Network for Various Monitoring Applications

NARCIS (Netherlands)

Basten, T.G.H.; Wessels, P.W.

2013-01-01

Acoustic monitoring using a sensor network is a powerful instrument to assess and manage complex noise situations. It can provide a basis to identify appropriate and cost effective measures, and to assess their effect by comparing before and after implementation. It can also be an instrument for

Inspection of nuclear power plant piping welds by in-process acoustic emission monitoring

International Nuclear Information System (INIS)

Prine, D.W.

1976-01-01

The results of using in-process acoustic emission monitoring on nuclear power plant piping welds are discussed. The technique was applied to good and intentionally flawed test welds as well as production welds, and the acoustic emission results are compared to standard NDT methods and selected metallographic cross-sections

Use of information system data of jet crushing acoustic monitoring for the process management

Directory of Open Access Journals (Sweden)

T.M. Bulanaya

2012-12-01

Full Text Available The graphic interpretation of amplitude and frequency of acoustic signals of loose material jet grinding process are resulted. Criteria of process management is determined on the basis of the acoustic monitoring data of jet mill acting.

Comparison of PAM Systems for Acoustic Monitoring and Further Risk Mitigation Application.

Science.gov (United States)

Ludwig, Stefan; Kreimeyer, Roman; Knoll, Michaela

2016-01-01

We present results of the SIRENA 2011 research cruises conducted by the NATO Undersea Research Centre (NURC) and joined by the Research Department for Underwater Acoustics and Geophysics (FWG), Bundeswehr Technical Centre (WTD 71) and the Universities of Kiel and Pavia. The cruises were carried out in the Ligurian Sea. The main aim of the FWG was to test and evaluate the newly developed towed hydrophone array as a passive acoustic monitoring (PAM) tool for risk mitigation applications. The system was compared with the PAM equipment used by the other participating institutions. Recorded sounds were used to improve an automatic acoustic classifier for marine mammals, and validated acoustic detections by observers were compared with the results of the classifier.

Thermometric- and Acoustic-Based Beam Power Monitor for Ultra-Bright X-Rays

International Nuclear Information System (INIS)

2010-01-01

A design for an average beam power monitor for ultra-bright X-ray sources is proposed that makes simultaneous use of calorimetry and radiation acoustics. Radiation incident on a solid target will induce heating and ultrasonic vibrations, both of which may be measured to give a fairly precise value of the beam power. The monitor is intended for measuring ultra-bright Free-Electron Laser (FEL) X-ray beams, for which traditional monitoring technologies such as photo-diodes or scintillators are unsuitable. The monitor consists of a Boron Carbide (B 4 C) target designed to absorb most of the incident beam's energy. Resistance temperature detectors (RTD) and piezoelectric actuators are mounted on the outward faces of the target to measure the temperature changes and ultrasonic vibrations induced by the incident beam. The design was tested using an optical pulsed beam (780 nm, 120 and 360 Hz) from a Ti:sapphire oscillator at several energies between 0.8 and 2.6 mJ. The RTDs measured an increase in temperature of about 10 K over a period of several minutes. The piezoelectric sensors recorded ringing acoustic oscillations at 580 ± 40 kHz. Most importantly, the amplitude of the acoustic signals was observed to scale linearly with beam power up to 2 mJ of pulse energy. Above this pulse energy, the vibrational signals became nonlinear. Several causes for this nonlinearity are discussed, including amplifier saturation and piezoelectric saturation. Despite this nonlinearity, these measurements demonstrate the feasibility of such a beam power measurement device. The advantage of two distinct measurements (acoustic and thermometric) provides a useful method of calibration that is unavailable to current LCLS diagnostics tools.

Chemometric applications to assess quality and critical parameters of virgin and extra-virgin olive oil. A review.

Science.gov (United States)

Gómez-Caravaca, Ana M; Maggio, Rubén M; Cerretani, Lorenzo

2016-03-24

Today virgin and extra-virgin olive oil (VOO and EVOO) are food with a large number of analytical tests planned to ensure its quality and genuineness. Almost all official methods demand high use of reagents and manpower. Because of that, analytical development in this area is continuously evolving. Therefore, this review focuses on analytical methods for EVOO/VOO which use fast and smart approaches based on chemometric techniques in order to reduce time of analysis, reagent consumption, high cost equipment and manpower. Experimental approaches of chemometrics coupled with fast analytical techniques such as UV-Vis spectroscopy, fluorescence, vibrational spectroscopies (NIR, MIR and Raman fluorescence), NMR spectroscopy, and other more complex techniques like chromatography, calorimetry and electrochemical techniques applied to EVOO/VOO production and analysis have been discussed throughout this work. The advantages and drawbacks of this association have also been highlighted. Chemometrics has been evidenced as a powerful tool for the oil industry. In fact, it has been shown how chemometrics can be implemented all along the different steps of EVOO/VOO production: raw material input control, monitoring during process and quality control of final product. Copyright © 2016 Elsevier B.V. All rights reserved.

Progress toward acoustic emission characterization for continuous monitoring of reactor pressure vessels

International Nuclear Information System (INIS)

Hutton, P.H.; Schwenk, E.B.; Kurtz, R.J.

1980-01-01

The purpose of this work is to evaluate the feasibility of detecting and analyzing flaw growth in an operating reactor vessel using acoustic emission (AE) data. A preliminary AE-flaw growth relationship has been developed encompassing six variables. This model relates AE count and energy to fatigue crack driving force ΔK. Pattern recognition has been examined as a means of distinguishing crack growth AE from other acoustic signals with encouraging results. The program is moving into hardware implementation of relationships for testing and refinement by monitoring tests in heavy section specimens and subscale structures. The hardware system will become a reactor monitor prototype. (orig.) [de

Process monitored spectrophotometric titration coupled with chemometrics for simultaneous determination of mixtures of weak acids.

Science.gov (United States)

Liao, Lifu; Yang, Jing; Yuan, Jintao

2007-05-15

A new spectrophotometric titration method coupled with chemometrics for the simultaneous determination of mixtures of weak acids has been developed. In this method, the titrant is a mixture of sodium hydroxide and an acid-base indicator, and the indicator is used to monitor the titration process. In a process of titration, both the added volume of titrant and the solution acidity at each titration point can be obtained simultaneously from an absorption spectrum by least square algorithm, and then the concentration of each component in the mixture can be obtained from the titration curves by principal component regression. The method only needs the information of absorbance spectra to obtain the analytical results, and is free of volumetric measurements. The analyses are independent of titration end point and do not need the accurate values of dissociation constants of the indicator and the acids. The method has been applied to the simultaneous determination of the mixtures of benzoic acid and salicylic acid, and the mixtures of phenol, o-chlorophenol and p-chlorophenol with satisfactory results.

Operational monitoring of acoustic sensor networks

Directory of Open Access Journals (Sweden)

Boltenkov V.A.

2015-06-01

Full Text Available Acoustic sensor networks (ASN are widely used to monitor water leaks in the power generating systems. Since the ASN are used in harsh climatic conditions the failures of microphone elements of ASN are inevitable. That's why the failure detection of ASN elements is a problem of current interest. Two techniques of operational monitoring ASN are developed. Both of them are based on the placement of the test sound source within a network. The signal processing for ASN sensors had to detect the failed element. Techniques are based time difference of arrival (TDOA estimating at the each pair of ASN elements. TDOA estimates as argmaximum of cross-correlation function (CCF for signals on each microphone sensors pair. The M-sequence phase-shift keyed signal is applied as a test acoustic signal to ensure high accuracy of the CCF maximum estimation at low signal/noise ratio (SNR. The first technique is based on the isolation principle for TDOA sum at three points. It require to locate the test sound source in the far field. This is not always possible due to technological reasons. For the second proposed technique test sound source can be located near the ASN. It is based on a system of hyperbolic equations solving for each of the four elements of the ASN. Both techniques has been tested in the computer imitation experiment. It was found that for the SNR to –5 dB both techniques show unmistakable indicators of control quality. The second method requires significantly more time control.

A passive acoustic monitor of treatment effectiveness during extracorporeal lithotripsy

Science.gov (United States)

Fedele, F.; Thomas, K.; Leighton, T. G.; Ryves, S.; Phillips, D.; Coleman, A. J.

2011-02-01

Although extracorporeal shockwave lithotripsy (ESWL) has now been in the clinic for at least three decades, there has been little advance in efforts (i) to estimate the efficacy of the treatment whilst it is in progress, or (ii) to determine the end-point of a treatment session in terms of the degree of stone fragmentation achieved. Previous in vitro experimentation and clinical trials have shown that a passive acoustic monitor has the potential to provide evidence of the effectiveness and end-point of lithotripsy. The system exploits secondary emissions generated during shock-tissue interaction, whose features depend on the quality of tissue at the beam focus. This prototype was developed into the first commercially available clinical ESWL treatment monitor (Precision Acoustic Ltd, Dorchester, UK), and a unit has been acquired and tested in the clinical routine by urologists at Guy's and St Thomas NHS Trust in March 2009. This paper critically assesses the performance of the new system for the first 25 treatments monitored. The ESWL monitor correctly predicted the treatment outcome of 15 of the 18 treatments that were followed-up clinically. In addition, it was noted that the measure of treatment effectiveness provided by the monitor after 500 shocks was predictive of the final treatment outcome (p ESWL or if the patient should be sent for surgery.

Vibro-acoustic condition monitoring of Internal Combustion Engines: A critical review of existing techniques

Science.gov (United States)

Delvecchio, S.; Bonfiglio, P.; Pompoli, F.

2018-01-01

This paper deals with the state-of-the-art strategies and techniques based on vibro-acoustic signals that can monitor and diagnose malfunctions in Internal Combustion Engines (ICEs) under both test bench and vehicle operating conditions. Over recent years, several authors have summarized what is known in critical reviews mainly focused on reciprocating machines in general or on specific signal processing techniques: no attempts to deal with IC engine condition monitoring have been made. This paper first gives a brief summary of the generation of sound and vibration in ICEs in order to place further discussion on fault vibro-acoustic diagnosis in context. An overview of the monitoring and diagnostic techniques described in literature using both vibration and acoustic signals is also provided. Different faulty conditions are described which affect combustion, mechanics and the aerodynamics of ICEs. The importance of measuring acoustic signals, as opposed to vibration signals, is due since the former seem to be more suitable for implementation on on-board monitoring systems in view of their non-intrusive behaviour, capability in simultaneously capturing signatures from several mechanical components and because of the possibility of detecting faults affecting airborne transmission paths. In view of the recent needs of the industry to (-) optimize component structural durability adopting long-life cycles, (-) verify the engine final status at the end of the assembly line and (-) reduce the maintenance costs monitoring the ICE life during vehicle operations, monitoring and diagnosing system requests are continuously growing up. The present review can be considered a useful guideline for test engineers in understanding which types of fault can be diagnosed by using vibro-acoustic signals in sufficient time in both test bench and operating conditions and which transducer and signal processing technique (of which the essential background theory is here reported) could be

On-line Monitoring System Based on Principle of Electro-acoustic Monitoring for Transformer Partial Discharge

Directory of Open Access Journals (Sweden)

Guang Ya LIU

2014-02-01

Full Text Available Partial discharge inside a transformer is mainly responsible for the insulation aging and damage of the transformer. However, partial discharge is usually accompanied by external signals like sound, light and electrical signals and detectable physical phenomena such as characteristical gas and dielectric loss. Therefore, it is of great significance to monitor online the external signals and phenomena formed during partial discharge of the transformer when the transformer diagnoses faults. This paper gives a comprehensive overview of the electro-acoustic joint monitoring principles and its monitoring systems and the judgment skills concerned, on the basis of which the monitoring system is designed.

A Real-Time Audio Tele-Presence Device for Remote Acoustic Monitoring

National Research Council Canada - National Science Library

Vaudrey, Michael

2003-01-01

.... At the end of the Phase I effort, ATI delivered to ARL a fully functional wired binaural hearing device capable of accurately monitoring remote acoustic environments as far as 50 feet from the listener/operator...

Non-Imaging Acoustical Properties in Monitoring Arteriovenous Hemodialysis Access. A Review

Directory of Open Access Journals (Sweden)

Anas Mohd Noor

2015-12-01

Full Text Available The limitations of the gold standard angiography technique in arteriovenous access surveillance have opened a gap for researchers to find the best way to monitor this condition with low-cost, non-invasive and continuous bedside monitoring. The phonoangiography technique has been developed prior to these limits. This measurement and monitoring technique, associated with intelligence signal processing, promises better analysis for early detection of hemodialysis access problems, such as stenosis and thrombosis. Some research groups have shown that the phonoangiography technique could identify as many as 20% of vascular diameter changes and also its frequency characteristics due to hemodialysis access problems. The frequency characteristics of these acoustical signals are presented and discussed in detail to understand the association with the stenosis level, blood flows, sensor locations, fundamental frequency bands of normal and abnormal conditions, and also the spectral energy produced. This promising technique could be used in the near future as a tool for pre-diagnosis of arteriovenous access before any further access correction by surgical techniques is required. This paper provides an extensive review of various arteriovenous access monitoring techniques based on non-imaging acoustical properties.

Experimental study of advanced continuous acoustic-emission monitoring of BWR components. Final report

International Nuclear Information System (INIS)

McElroy, J.W.

1982-01-01

This report presents the results of a four year research program on the utilization of acoustic emission techniques on light water reactor component applications. Two techniques of the acoustic emission technology were applied to specific problems occurring within the light water reactor system. Crack detection AE monitoring was applied to thermal cycle fatigue cracking problems and stress corrosion cracking problems. Leak detection AE monitoring was applied to valve leakage in the main steam safety relief valves and incontainment packing gland valves. The report provides AE data showing how AE crack detection can be used as an on-line diagnostic monitoring tool. By having an active monitor on light water reactor components, the inservice inspection of the components is being performed during operation rather than refueling periods, thereby reducing critical path time during outages. The resultant benefit is increased plant availability and a reduction in accumulated radiation exposure

A passive acoustic monitor of treatment effectiveness during extracorporeal lithotripsy

International Nuclear Information System (INIS)

Fedele, F; Coleman, A J; Thomas, K; Ryves, S; Phillips, D; Leighton, T G

2011-01-01

Although extracorporeal shockwave lithotripsy (ESWL) has now been in the clinic for at least three decades, there has been little advance in efforts (i) to estimate the efficacy of the treatment whilst it is in progress, or (ii) to determine the end-point of a treatment session in terms of the degree of stone fragmentation achieved. Previous in vitro experimentation and clinical trials have shown that a passive acoustic monitor has the potential to provide evidence of the effectiveness and end-point of lithotripsy. The system exploits secondary emissions generated during shock-tissue interaction, whose features depend on the quality of tissue at the beam focus. This prototype was developed into the first commercially available clinical ESWL treatment monitor (Precision Acoustic Ltd, Dorchester, UK), and a unit has been acquired and tested in the clinical routine by urologists at Guy's and St Thomas NHS Trust in March 2009. This paper critically assesses the performance of the new system for the first 25 treatments monitored. The ESWL monitor correctly predicted the treatment outcome of 15 of the 18 treatments that were followed-up clinically. In addition, it was noted that the measure of treatment effectiveness provided by the monitor after 500 shocks was predictive of the final treatment outcome (p < 0.001). This suggests that the system could be used in pre-assessment; indicating if the stone is susceptible to ESWL or if the patient should be sent for surgery.

A passive acoustic monitor of treatment effectiveness during extracorporeal lithotripsy

Energy Technology Data Exchange (ETDEWEB)

Fedele, F; Coleman, A J [Medical Physics Department, Guy' s and St Thomas NHS Foundation Trust, Westminster Bridge Road, SE1 7EH, London (United Kingdom); Thomas, K; Ryves, S; Phillips, D [Urology Department, Guy' s and St Thomas NHS Foundation Trust, Great Maze Pond, SE1 9RT, London (United Kingdom); Leighton, T G, E-mail: fiammetta.fedele@gstt.nhs.uk [Institute of Sound and Vibration Research, University of Southampton, Highfield, S017 1BJ, Southampton (United Kingdom)

2011-02-01

Although extracorporeal shockwave lithotripsy (ESWL) has now been in the clinic for at least three decades, there has been little advance in efforts (i) to estimate the efficacy of the treatment whilst it is in progress, or (ii) to determine the end-point of a treatment session in terms of the degree of stone fragmentation achieved. Previous in vitro experimentation and clinical trials have shown that a passive acoustic monitor has the potential to provide evidence of the effectiveness and end-point of lithotripsy. The system exploits secondary emissions generated during shock-tissue interaction, whose features depend on the quality of tissue at the beam focus. This prototype was developed into the first commercially available clinical ESWL treatment monitor (Precision Acoustic Ltd, Dorchester, UK), and a unit has been acquired and tested in the clinical routine by urologists at Guy's and St Thomas NHS Trust in March 2009. This paper critically assesses the performance of the new system for the first 25 treatments monitored. The ESWL monitor correctly predicted the treatment outcome of 15 of the 18 treatments that were followed-up clinically. In addition, it was noted that the measure of treatment effectiveness provided by the monitor after 500 shocks was predictive of the final treatment outcome (p < 0.001). This suggests that the system could be used in pre-assessment; indicating if the stone is susceptible to ESWL or if the patient should be sent for surgery.

A passive acoustic monitor of treatment effectiveness during extracorporeal lithotripsy

Energy Technology Data Exchange (ETDEWEB)

Fedele, F; Coleman, A J [Medical Physics Department, Guy' s and St Thomas NHS Foundation Trust, Westminster Bridge Road, SE1 7EH, London (United Kingdom); Thomas, K; Ryves, S; Phillips, D [Urology Department, Guy' s and St Thomas NHS Foundation Trust, Great Maze Pond, SE1 9RT, London (United Kingdom); Leighton, T G, E-mail: fiammetta.fedele@gstt.nhs.uk [Institute of Sound and Vibration Research, University of Southampton, Highfield, S017 1BJ, Southampton (United Kingdom)

2011-02-01

Although extracorporeal shockwave lithotripsy (ESWL) has now been in the clinic for at least three decades, there has been little advance in efforts (i) to estimate the efficacy of the treatment whilst it is in progress, or (ii) to determine the end-point of a treatment session in terms of the degree of stone fragmentation achieved. Previous in vitro experimentation and clinical trials have shown that a passive acoustic monitor has the potential to provide evidence of the effectiveness and end-point of lithotripsy. The system exploits secondary emissions generated during shock-tissue interaction, whose features depend on the quality of tissue at the beam focus. This prototype was developed into the first commercially available clinical ESWL treatment monitor (Precision Acoustic Ltd, Dorchester, UK), and a unit has been acquired and tested in the clinical routine by urologists at Guy's and St Thomas NHS Trust in March 2009. This paper critically assesses the performance of the new system for the first 25 treatments monitored. The ESWL monitor correctly predicted the treatment outcome of 15 of the 18 treatments that were followed-up clinically. In addition, it was noted that the measure of treatment effectiveness provided by the monitor after 500 shocks was predictive of the final treatment outcome (p < 0.001). This suggests that the system could be used in pre-assessment; indicating if the stone is susceptible to ESWL or if the patient should be sent for surgery.

Remote erosion and corrosion monitoring of subsea pipelines using acoustic telemetry and wet-mate connector technology

Energy Technology Data Exchange (ETDEWEB)

Painter, Howard; Barlow, Stewart [Teledyne ODI, Thousand Oaks, CA (United States); Clarke, Daniel [Teledyne Cormon, Thousand Oaks, CA (United States); Green, Dale [Teledyne Benthos, North Falmouth, MA (United States)

2009-07-01

This paper will present a novel approach for monitoring erosion and corrosion using proven sub sea technologies: intrusive erosion and corrosion monitoring, acoustic telemetry and wet-mateable connector technology. Intrusive metal loss based monitoring systems on sub sea pipelines are increasingly being used because of their ability to directly measure erosion and corrosion. These systems are integrated with the sub sea production control system or located close to the platform and hard-wired. However, locations remote from a sub sea control system or platform requires a dedicated communication system and long lengths of cable that can be cost prohibitive to procure and install. The system presented consists of an intrusive erosion or corrosion monitor with pressure and temperature transmitters, a retrievable electronics module with an acoustic modem, a data storage module, and a replaceable power module. Time-stamped erosion and corrosion data can be transmitted via an acoustic link to a surface platform, a vessel of opportunity or to a relaying modem. Acoustic signals can be transmitted up to 6 km from the monitoring location. The power module along with data module and acoustic modem are mounted on the erosion and corrosion module using wet-mateable connectors, allowing retrieval by remotely operated vehicles. The collected data can be used to assess the cumulative erosion and corrosion as well as use the real-time metal loss rate data to correlate with operational parameters. Benefits include optimization of corrosion inhibitor dosage rates, mitigation of damage caused by solids production, and increased flow assurance. (author)

A monitoring of superconducting magnets by acoustic emission

International Nuclear Information System (INIS)

Nomura, Harehiko; Tateishi, Hiroshi; Onishi, Toshitada

1990-01-01

Since superconducting magnets (SCM) are going to be indispensable to magnetic levitated train, nuclear fusion, magnetic resonating imaging, rotational machines, etc., they must be placed great reliance on its repetitional operations. But without appropriate evaluating methods, these promising techniques must remain still in science levels and hard to be transferable to real human technologies. SCM, being used under dynamical operation with linking other electro-magnetic systems as said above, induce high voltage from which monitoring superconducting to normal transitional voltage is difficult to distinguish. To solve this problem, monitoring SCM by Acoustic Emission (AE) from themselves, have been found effective, in particular, during the dynamical energizing of them. As for a demonstration, this paper will report mainly how to monitor 3 MJ-SCM and a few results of the experiments aquired both by counting and locational mode of AE in pulsed and repeated operations of the magnet. Some discussions on the AE monitorings are also made along the main issues to be solved in future. (author)

Condition Monitoring and Management from Acoustic Emissions

DEFF Research Database (Denmark)

Pontoppidan, Niels Henrik Bohl

2005-01-01

In the following, I will use technical terms without explanation as it gives the freedom to describe the project in a shorter form for those who already know. The thesis is about condition monitoring of large diesel engines from acoustic emission signals. The experiments have been focused...... is the analysis of the angular position changes of the engine related events such as fuel injection and valve openings, caused by operational load changes. With inspiration from speech recognition and voice effects the angular timing changes have been inverted with the event alignment framework. With the event...

HYDROBS: a long-term autonomous mooring for passive acoustic monitoring

Science.gov (United States)

Hello, Y.; Royer, J. Y.; Yegikyan, M.

2017-12-01

Passive acoustics proves an effective way for monitoring the low-level seismic activity of the ocean floor and low-frequency sounds from the ocean (baleen whales, sea-state, icebergs). Networks of synchronized autonomous hydrophones have thus been commonly deployed in the world ocean to monitor large sections of mid-oceanic ridges. HYDROBS is an improved system that meet two requirements: an easy access to the data collected by the instruments together with long-term deployments - up to 4 consecutive years - reducing the need of large vessels capable of yearly mooring operations in open seas. The system has two components: a data logger, up-to-date but similar to previous systems, and three messengers, releasable on demand to collect the data. The mooring line itself is classical, with an expandable weight at the sea-bottom to maintain the mooring, an acoustic release to free the mooring line for recovery, a line adjustable to the seafloor depth, and an immerged buoy, holding the acquisition system, to maintain the sensors at a constant depth and to bring the mooring line to the surface for its recovery. The data logger is based on a low-power microprocessor, an A/D-32bit convertor sampling at 250Hz, a 10-8 real time clock and SD card storage. Lithium batteries provide 3-4 years of autonomy. Acoustic communications with the surface-ship provide control over all functionalities at deployment and a health bulletin on demand. The 3 shuttles, encapsulated in 13" glass spheres, use the same CPU board and clock as the main station. Data transfer from the data logger to the shuttles is wireless (1Mbit/s digital inductive through water). Data are duplicated once per day on shuttles N and N+1 for redundancy. Prior to their release by acoustic command, the shuttles are synchronized with the master clock. At sea-surface, shuttles (as the main unit) look for GPS time and calculate their clock drift. So, the master clock drift can be monitored over time at every shuttle release

Utilisation of acoustic emission technique to monitor lubrication condition in a low speed bearing

International Nuclear Information System (INIS)

Nordin Jamaludin; Mohd Jailani Mohd Nor

2003-01-01

Monitoring of lubrication condition in rolling element bearings through the use of vibration analysis is an established technique. However, this success has not mirrored at low rotational speeds. At low speeds the energy generated from the poor lubricated bearing lubrication might not show as an obvious change in signature and thus become undetectable using conventional vibration measuring equipment. This paper presents an investigation into the applicability of acoustic emission technique and analysis for detecting poorly lubricated bearing rotating at a speed of 1.12 rpm. Investigations were centered on a test-rig designed to simulate the real bearing used in the field. The variation of lubricant amount in the low-speed bearing was successfully monitored using a new developed method known as pulse injection technique (PIT). The PIT technique was based on acoustic emission method. The technique involved transmitting a Dirac pulse to the test bearing via a transmitting acoustic emission sensor while the bearing was in operation. Analysing the captured acoustic emission signatures using established statistical method could differentiate between properly and poorly lubricated bearing. (Author)

An acoustic sensor for monitoring airflow in pediatric tracheostomy patients.

Science.gov (United States)

Ruscher, Thomas; Wicks Phd, Alexandrina; Muelenaer Md, Andre

2012-01-01

Without proper monitoring, patients with artificial airways in the trachea are at high risk for complications or death. Despite routine maintenance of the tube, dislodged or copious mucus can obstruct the airway. Young children ( 3yrs) have difficulty tending to their own tubes and are particularly vulnerable to blockages. They require external respiratory sensors. In a hospital environment, ventilators, end-tidal CO2 monitors, thermistors, and other auxiliary equipment provide sufficient monitoring of respiration. However, outpatient monitoring methods, such as thoracic impedance and pulse oximetry, are indirect and prone to false positives. Desensitization of caregivers to frequent false alarms has been cited in medical literature as a contributing factor in cases of child death. Ultrasonic time-of-flight (TOF) is a technique used in specialized industrial applications to non-invasively measure liquid and gas flow. Two transducers are oriented at a diagonal across a flow channel. Velocity measurement is accomplished by detecting slight variations in transit time of contra-propagating acoustic signals with a directional component parallel to air flow. Due to the symmetry of acoustic pathway between sensors, velocity measurements are immune to partial fouling in the tube from mucus, saliva, and condensation. A first generation proof of concept prototype was constructed to evaluate the ultrasonic TOF technique for medical tracheostomy monitoring. After successful performance, a second generation prototype was designed with a smaller form factor and more advanced electronics. This prototype was tested and found to measure inspired volume with a root-mean-square error < 2% during initial trials.

An assessment of acoustic emission for nuclear pressure vessel monitoring

International Nuclear Information System (INIS)

Scruby, C.B.

1983-01-01

Recent research has greatly improved our understanding of the basic mechanisms of deformation and fracture that generate detectable acoustic emission signals in structural steels. A critical review of the application of acoustic emission (AE) to the fabrication, proof testing and in-service monitoring of nuclear pressure vessels is presented in the light of this improved understanding. The detectability of deformation and fracture processes in pressure vessel steels is discussed, and recommendations made for improving source location accuracy and the development of quantitative source assessment techniques. Published data suggest that AE can make an important contribution to fabrication monitoring, and to the detection of defects in lower toughness materials during vessel proof testing. In high toughness materials, however, the signals generated during ductile crack growth may frequently be too weak for reliable detection. The feasibility of AE for continuous monitoring has not yet been adequately demonstrated because of high background noise levels and uncertainty about AE signal strengths from the defect growth processes that occur in service. In-service leak detection by AE shows considerable promise. It is recommended that further tests are carried out with realistic defects, and under realistic conditions of loading (including thermal shock and fatigue) and of environment. (author)

The use of acoustic monitoring to manage concrete structures in the nuclear industry

International Nuclear Information System (INIS)

Paulson, P.O.; Tozser, O.; Wit, M. de

2003-01-01

Concrete and steel are widely used in containment vessels within the nuclear industry. Both are excellent acoustic transmitters. In many structures tensioned wire elements are used within containment structures. However, tensioned wire can be vulnerable to corrosion. To reduce the probability of corrosion sophisticated protection systems are used. To confirm that the design strength is available through time, extensive inspection and maintenance regimes are implemented. These regimes include tests to confirm the condition of the post-tensioning, and pressure tests (leak tests) to verify the performance of vessel. This paper presents an acoustic monitoring technology which uses widely distributed sensors to detect and locate wire failures using the energy released at failure. The technology has been used on a range of structures including post-tensioned concrete bridges, suspension bridges, buildings, pre-cast concrete cylinder pipelines (PCCP) and prestressed concrete containment vessels (PCCV), where it has increased confidence in structures and reduced maintenance costs. Where the level of ambient noise is low then SoundPrint acoustic monitoring can detect concrete cracking. This has been shown in PCCP pipelines, on laboratory test structures and also in nuclear structures. The programme has shown that distributed sensors can locate internal cracking well before there is any external evidence. Several projects have been completed on nuclear vessels. The first has been completed on an Electricite de France (EDF) concrete test pressure vessel at Civaux in France. The second at the Sandia PCCV Test Vessel in Albuquerque, New Mexico, USA, which involved the testing of a steel lined concrete vessel. The third was on a PCCV in Maryland, USA. Acoustic monitoring is also able to monitor the deterioration of post-tensioned concrete structures as a result of seismic activity. Summary details of a case history are presented. (author)

Symbiosis of chemometrics and metabolomics: past, present, and future

NARCIS (Netherlands)

van der Greef, J.; Smilde, A. K.

2005-01-01

Metabolomics is a growing area in the field of systems biology. Metabolomics has already a long history and also the connection of metabolomics with chemometrics goes back some time. This review discusses the symbiosis of metabolomics and chemometrics with emphasis on the medical domain, puts the

Current application of chemometrics in traditional Chinese herbal medicine research.

Science.gov (United States)

Huang, Yipeng; Wu, Zhenwei; Su, Rihui; Ruan, Guihua; Du, Fuyou; Li, Gongke

2016-07-15

Traditional Chinese herbal medicines (TCHMs) are promising approach for the treatment of various diseases which have attracted increasing attention all over the world. Chemometrics in quality control of TCHMs are great useful tools that harnessing mathematics, statistics and other methods to acquire information maximally from the data obtained from various analytical approaches. This feature article focuses on the recent studies which evaluating the pharmacological efficacy and quality of TCHMs by determining, identifying and discriminating the bioactive or marker components in different samples with the help of chemometric techniques. In this work, the application of chemometric techniques in the classification of TCHMs based on their efficacy and usage was introduced. The recent advances of chemometrics applied in the chemical analysis of TCHMs were reviewed in detail. Copyright © 2015 Elsevier B.V. All rights reserved.

Research Based on the Acoustic Emission of Wind Power Tower Drum Dynamic Monitoring Technology

Science.gov (United States)

Zhang, Penglin; Sang, Yuan; Xu, Yaxing; Zhao, Zhiqiang

Wind power tower drum is one of the key components of the wind power equipment. Whether the wind tower drum performs safety directly affects the efficiency, life, and performance of wind power equipment. Wind power tower drum in the process of manufacture, installation, and operation may lead to injury, and the wind load and gravity load and long-term factors such as poor working environment under the action of crack initiation or distortion, which eventually result in the instability or crack of the wind power tower drum and cause huge economic losses. Thus detecting the wind power tower drum crack damage and instability is especially important. In this chapter, acoustic emission is used to monitor the whole process of wind power tower drum material Q345E steel tensile test at first, and processing and analysis tensile failure signal of the material. And then based on the acoustic emission testing technology to the dynamic monitoring of wind power tower drum, the overall detection and evaluation of the existence of active defects in the whole structure, and the acoustic emission signals collected for processing and analysis, we could preliminarily master the wind tower drum mechanism of acoustic emission source. The acoustic emission is a kind of online, efficient, and economic method, which has very broad prospects for work. The editorial committee of nondestructive testing qualification and certification of personnel teaching material of science and technology industry of national defense, "Acoustic emission testing" (China Machine Press, 2005.1).

GC/MS analysis of pesticides in the Ferrara area (Italy) surface water: a chemometric study.

Science.gov (United States)

Pasti, Luisa; Nava, Elisabetta; Morelli, Marco; Bignami, Silvia; Dondi, Francesco

2007-01-01

The development of a network to monitor surface waters is a critical element in the assessment, restoration and protection of water quality. In this study, concentrations of 42 pesticides--determined by GC-MS on samples from 11 points along the Ferrara area rivers--have been analyzed by chemometric tools. The data were collected over a three-year period (2002-2004). Principal component analysis of the detected pesticides was carried out in order to define the best spatial locations for the sampling points. The results obtained have been interpreted in view of agricultural land use. Time series data regarding pesticide contents in surface waters has been analyzed using the Autocorrelation function. This chemometric tool allows for seasonal trends and makes it possible to optimize sampling frequency in order to detect the effective maximum pesticide content.

GC/MS Analysis of Pesticides in the Ferrara Area (Italy) Surface Water: A Chemometric Study

International Nuclear Information System (INIS)

Pasti, L.; Dondi, F.; Nava, E.; Morelli, M.; Bignami, S.

2007-01-01

The development of a network to monitor surface waters is a critical element in the assessment, restoration and protection of water quality. In this study, concentrations of 42 pesticides - determined by GC-MS on samples from 11 points along the Ferrara area rivers - have been analyzed by chemometric tools. The data were collected over a three-year period (2002-2004). Principal component analysis of the detected pesticides was carried out in order to define the best spatial locations for the sampling points. The results obtained have been interpreted in view of agricultural land use. Time series data regarding pesticide contents in surface waters has been analyzed using the Autocorrelation function. This chemometric tool allows for seasonal trends and makes it possible to optimize sampling frequency in order to detect the effective maximum pesticide content

In Situ Monitoring of Chemical Reactions at a Solid-Water Interface by Femtosecond Acoustics.

Science.gov (United States)

Shen, Chih-Chiang; Weng, Meng-Yu; Sheu, Jinn-Kong; Yao, Yi-Ting; Sun, Chi-Kuang

2017-11-02

Chemical reactions at a solid-liquid interface are of fundamental importance. Interfacial chemical reactions occur not only at the very interface but also in the subsurface area, while existing monitoring techniques either provide limited spatial resolution or are applicable only for the outmost atomic layer. Here, with the aid of the time-domain analysis with femtosecond acoustics, we demonstrate a subatomic-level-resolution technique to longitudinally monitor chemical reactions at solid-water interfaces, capable of in situ monitoring even the subsurface area under atmospheric conditions. Our work was proven by monitoring the already-known anode oxidation process occurring during photoelectrochemical water splitting. Furthermore, whenever the oxide layer thickness equals an integer  number of the effective atomic layer thickness, the measured acoustic echo will show higher signal-to-noise ratios with reduced speckle noise, indicating the quantum-like behavior of this coherent-phonon-based technique.

On the use of horizontal acoustic doppler profilers for continuous bed shear stress monitoring

NARCIS (Netherlands)

Vermeulen, B.; Hoitink, A.J.F.; Sassi, M.G.

2013-01-01

Continuous monitoring of bed shear stress in large river systems may serve to better estimate alluvial sediment transport to the coastal ocean. Here we explore the possibility of using a horizontally deployed acoustic Doppler current profiler (ADCP) to monitor bed shear stress, applying a prescribed

Chemometric methods and near-infrared spectroscopy applied to bioenergy production

International Nuclear Information System (INIS)

Liebmann, B.

2010-01-01

The present work examines bioenergy production from different viewpoints. The three main objectives are: (1) to reveal the relation of technology, sustainability and economy in bioenergy processes; (2) to investigate spectroscopic methods as a tool for analytical monitoring of bioenergy processes; and (3) to develop new chemometric methods for advanced analysis of spectroscopic data. At the first stage, this thesis investigates the technological, ecological, and economic features of renewable-resource-based and de-centralized bioenergy production systems. In different scenarios, small-scale bioethanol production is combined with other technologies that provide renewable energy from residuals of the bioethanol process. The general aim is to substitute fossil energy conventionally used within the bioethanol process. The investigated technologies are biogas production and straw incineration. Agricultural aspects are introduced by sustainable crop rotation concepts that reconcile food, feed, and biofuel production. The sustainability of small-scale bioethanol production in the different scenarios is quantified by an ecological footprint method, the sustainable process index, SPI, and compared to conventional fuels. The main findings are: (i) small-scaled bioethanol production can be operated with 100 % renewable energy supply, (ii) the SPI of bioethanol can be reduced up to 92 % compared to conventional fuels, (iii) a complex trade-off between ecology-of-scale and economy-of-scale is necessary. At the second stage, this thesis approaches bioenergy production processes from an analytical perspective, and presents near-infrared spectroscopy (NIR) as promising method for fast process monitoring of bioethanol production and biomass characterization. In addition, new analytical methods are presented for a fast determination of the heating value of solid biomass fuel, based on IR and NIR spectroscopy. The main findings are that NIR spectroscopy and appropriate chemometric

Simultaneous acoustic and dielectric real time curing monitoring of epoxy systems

Science.gov (United States)

Gkikas, G.; Saganas, Ch.; Grammatikos, S. A.; Aggelis, D. G.; Paipetis, A. S.

2012-04-01

The attainment of structural integrity of the reinforcing matrix in composite materials is of primary importance for the final properties of the composite structure. The detailed monitoring of the curing process on the other hand is paramount (i) in defining the optimal conditions for the impregnation of the reinforcement by the matrix (ii) in limiting the effects of the exotherm produced by the polymerization reaction which create unwanted thermal stresses and (iii) in securing optimal behavior in matrix controlled properties, such as off axis or shear properties and in general the durability of the composite. Dielectric curing monitoring is a well known technique for distinguishing between the different stages of the polymerization of a typical epoxy system. The technique successfully predicts the gelation and the vitrification of the epoxy and has been extended for the monitoring of prepregs. Recent work has shown that distinct changes in the properties of the propagated sound in the epoxy which undergoes polymerization is as well directly related to the gelation and vitrification of the resin, as well as to the attainment of the final properties of the resin system. In this work, a typical epoxy is simultaneously monitored using acoustic and dielectric methods. The system is isothermally cured in an oven to avoid effects from the polymerization exotherm. Typical broadband sensors are employed for the acoustic monitoring, while flat interdigital sensors are employed for the dielectric scans. All stages of the polymerization process were successfully monitored and the validity of both methods was cross checked and verified.

Acoustic displacement sensor for harsh environment: application to SFR core support plate monitoring

International Nuclear Information System (INIS)

PeRISSE, J.; MACe, J.R.; VOUAGNER, P.

2013-06-01

The need for instrumentation able to monitor internal parameters inside reactor vessels during plant operation is getting stronger. Internal mechanical structures important for safety are concerned: for example core support plate, fuel assemblies or primary pumps. Because of very harsh environmental conditions (high temperature, pressure and radiation) and maintenance requirements, sensors are generally located on the outer shell of the vessel with, for example, strain gages, accelerometers, eddy current or US sensors. Then, some complex signal processing calculations must be performed to address internal structure behavior or health analysis but with bias effects (transfer path analysis method for example). This study will show an original displacement sensor based on an acoustic wave guide that can measure small displacement of mechanical structures inside reactor vessels. The application selected in this case is the monitoring of the core support plate for a sodium fast reactor (SFR). The wave guide - a thin tube sealed with pressurized argon gas inside - is installed inside the liquid sodium vessel (temperature between 400 deg. C to 550 deg. C). One extremity is connected to the mechanical structure for control. It includes two acoustic reflectors; such reflectors are dedicated to a calibration procedure to estimate the acoustic wave velocity whatever the temperature profile along the wave guide (velocity is temperature dependent). The opposite extremity of the wave guide is located outside the vessel and includes an emission/reception acoustic transducer. Using acoustic pulse reflectometry method, a plane wave pressure signal propagates inside the tube and reflects from the extremity and acoustic reflectors. The pulse-echo signals are recorded and processed in the frequency domain. Signal processing is performed to estimate the time of flight of pulse reflections patterns along the acoustic path. Then, monitored structure displacement - i.e. movement of the

Time Reversal Acoustic Structural Health Monitoring Using Array of Embedded Sensors, Phase I

Data.gov (United States)

National Aeronautics and Space Administration — Time Reversal Acoustic (TRA) structural health monitoring with an embedded sensor array represents a new approach to in-situ nondestructive evaluation of air-space...

Chemometrics applied to quality control and metabolomics for traditional Chinese medicines.

Science.gov (United States)

Liu, Shao; Liang, Yi-Zeng; Liu, Hai-Tao

2016-03-15

Traditional Chinese medicines (TCMs) bring a great challenge in quality control and evaluating the efficacy because of their complexity of chemical composition. Chemometric techniques provide a good opportunity for mining more useful chemical information from TCMs. Then, the application of chemometrics in the field of TCMs is spontaneous and necessary. This review focuses on the recent various important chemometrics tools for chromatographic fingerprinting, including peak alignment information features, baseline correction and applications of chemometrics in metabolomics and modernization of TCMs, including authentication and evaluation of the quality of TCMs, evaluating the efficacy of TCMs and essence of TCM syndrome. In the conclusions, the general trends and some recommendations for improving chromatographic metabolomics data analysis are provided. Copyright © 2016 Elsevier B.V. All rights reserved.

Monitoring and Analysis of In-Pile Phenomena in Advanced Test Reactor using Acoustic Telemetry

International Nuclear Information System (INIS)

Agarwal, Vivek; Smith, James A.; Jewell, James Keith

2015-01-01

The interior of a nuclear reactor presents a particularly harsh and challenging environment for both sensors and telemetry due to high temperatures and high fluxes of energetic and ionizing particles among the radioactive decay products. A number of research programs are developing acoustic-based sensing approach to take advantage of the acoustic transmission properties of reactor cores. Idaho National Laboratory has installed vibroacoustic receivers on and around the Advanced Test Reactor (ATR) containment vessel to take advantage of acoustically telemetered sensors such as thermoacoustic (TAC) transducers. The installation represents the first step in developing an acoustic telemetry infrastructure. This paper presents the theory of TAC, application of installed vibroacoustic receivers in monitoring the in-pile phenomena inside the ATR, and preliminary data processing results.

Monitoring and Analysis of In-Pile Phenomena in Advanced Test Reactor using Acoustic Telemetry

Energy Technology Data Exchange (ETDEWEB)

Agarwal, Vivek [Idaho National Lab. (INL), Idaho Falls, ID (United States). Dept. of Human Factors, Controls, and Statistics; Smith, James A. [Idaho National Lab. (INL), Idaho Falls, ID (United States). Dept. of Fuel Performance and Design; Jewell, James Keith [Idaho National Lab. (INL), Idaho Falls, ID (United States). Dept. of Fuel Performance and Design

2015-02-01

The interior of a nuclear reactor presents a particularly harsh and challenging environment for both sensors and telemetry due to high temperatures and high fluxes of energetic and ionizing particles among the radioactive decay products. A number of research programs are developing acoustic-based sensing approach to take advantage of the acoustic transmission properties of reactor cores. Idaho National Laboratory has installed vibroacoustic receivers on and around the Advanced Test Reactor (ATR) containment vessel to take advantage of acoustically telemetered sensors such as thermoacoustic (TAC) transducers. The installation represents the first step in developing an acoustic telemetry infrastructure. This paper presents the theory of TAC, application of installed vibroacoustic receivers in monitoring the in-pile phenomena inside the ATR, and preliminary data processing results.

Improvements to Passive Acoustic Tracking Methods for Marine Mammal Monitoring

Science.gov (United States)

2016-05-02

separate and associate calls from individual animals . Marine mammal; Passive acoustic monitoring; Localization; Tracking; Multiple source; Sparse array...position and hydrophone timing offset in addition to animal position Almost all marine mammal tracking methods treat animal position as the only unknown...Workshop on Detection, Classification and Localization (DCL) of Marine Mammals). The animals were expected to be relatively close to the surface

Chemometric methods in capillary electrophoresis

National Research Council Canada - National Science Library

Hanrahan, Grady; Gomez, Frank A

2010-01-01

... 113 6 CHEMOMETRIC METHODS FOR THE OPTIMIZATION OF CE AND CE- MS IN PHARMACEUTICAL, ENVIRONMENTAL, AND FOOD ANALYSIS Javier Hernández-Borges, Miguel Ángel Rodríguez-Delgado, and Alejandro Cifuent...

Chemometrics Methods for Specificity, Authenticity and Traceability Analysis of Olive Oils: Principles, Classifications and Applications

Directory of Open Access Journals (Sweden)

Habib Messai

2016-11-01

Full Text Available Background. Olive oils (OOs show high chemical variability due to several factors of genetic, environmental and anthropic types. Genetic and environmental factors are responsible for natural compositions and polymorphic diversification resulting in different varietal patterns and phenotypes. Anthropic factors, however, are at the origin of different blends’ preparation leading to normative, labelled or adulterated commercial products. Control of complex OO samples requires their (i characterization by specific markers; (ii authentication by fingerprint patterns; and (iii monitoring by traceability analysis. Methods. These quality control and management aims require the use of several multivariate statistical tools: specificity highlighting requires ordination methods; authentication checking calls for classification and pattern recognition methods; traceability analysis implies the use of network-based approaches able to separate or extract mixed information and memorized signals from complex matrices. Results. This chapter presents a review of different chemometrics methods applied for the control of OO variability from metabolic and physical-chemical measured characteristics. The different chemometrics methods are illustrated by different study cases on monovarietal and blended OO originated from different countries. Conclusion. Chemometrics tools offer multiple ways for quantitative evaluations and qualitative control of complex chemical variability of OO in relation to several intrinsic and extrinsic factors.

Chemometrics Methods for Specificity, Authenticity and Traceability Analysis of Olive Oils: Principles, Classifications and Applications

Science.gov (United States)

Messai, Habib; Farman, Muhammad; Sarraj-Laabidi, Abir; Hammami-Semmar, Asma; Semmar, Nabil

2016-01-01

Background. Olive oils (OOs) show high chemical variability due to several factors of genetic, environmental and anthropic types. Genetic and environmental factors are responsible for natural compositions and polymorphic diversification resulting in different varietal patterns and phenotypes. Anthropic factors, however, are at the origin of different blends’ preparation leading to normative, labelled or adulterated commercial products. Control of complex OO samples requires their (i) characterization by specific markers; (ii) authentication by fingerprint patterns; and (iii) monitoring by traceability analysis. Methods. These quality control and management aims require the use of several multivariate statistical tools: specificity highlighting requires ordination methods; authentication checking calls for classification and pattern recognition methods; traceability analysis implies the use of network-based approaches able to separate or extract mixed information and memorized signals from complex matrices. Results. This chapter presents a review of different chemometrics methods applied for the control of OO variability from metabolic and physical-chemical measured characteristics. The different chemometrics methods are illustrated by different study cases on monovarietal and blended OO originated from different countries. Conclusion. Chemometrics tools offer multiple ways for quantitative evaluations and qualitative control of complex chemical variability of OO in relation to several intrinsic and extrinsic factors. PMID:28231172

Proportional monitoring of the acoustic emission in crypto-conditions

Directory of Open Access Journals (Sweden)

Petr Dostál

2011-01-01

Full Text Available The work is aimed at studying corrosion and fatigue properties of aluminum alloys by means of acoustic emission (AE. During material degradation are acoustic events scanned and evaluated. The main objective of the article is a description of behavior of aluminum alloys degraded in specific conditions and critical degradation stages determination. The first part of the article describes controlled degradation of the material in the crypto–conditions. The acoustic emission method is used for process analyzing. This part contains the AE signals assessment and comparing aluminium alloy to steel. Then the specimens are loaded on high-cyclic loading apparatus for fatigue life monitoring. Also, the synergy of fatigue and corrosion processes is taken into account.The aim is the description of fatigue properties for aluminum alloys that have already been corrosion-degraded. Attention is also focused on the structure of fatigue cracks. The main part of the article is aimed at corrosion degradation of aluminium alloys researched in real time by means of AE. The most important benefit of AE detection/recording is that it provides information about the process in real time. Using this measurement system is possible to observe the current status of the machines/devices and to prevent serious accidents.

Monitoring the viscosity of diesel engine lubricating oil by using acoustic emission technique, the selection of measurement parameters

International Nuclear Information System (INIS)

Othman Inayatullah; Nordin Jamaludin; Fauziah Mat

2009-04-01

Acoustic emission technique has been developed through years of monitoring and diagnosis of bearing, but it is still new in the diagnosis and monitoring of lubrication oil to bearings drive. The propagation of acoustic emission signal is generated when the signal piston on the cylinder liner lubricating oil which is a par. The signal is analyzed in time domain to obtain the parameters of root mean squared, amplitude, energy and courtesy. Lubricant viscosity will undergo changes due to temperature, pressure and useful. This study focuses on the appropriate parameters for the diagnosis and monitoring of lubricating oil viscosity. Studies were conducted at a constant rotational speed and temperature, but use a different age. The results showed that the energy parameter is the best parameter used in this monitoring. However, this parameter cannot be used directly and it should be analyzed using mathematical formulas. This mathematical formula is a relationship between acoustic emission energy with the viscosity of lubricating oil. (author)

Acoustic Emission Monitoring of Cementitious Wasteforms

International Nuclear Information System (INIS)

Spasova, L.M.; Ojovan, M.I.

2013-01-01

A summary is presented of the potential of non-destructive acoustic emission (AE) method to be applied for structures immobilising nuclear wastes. The use and limitations of the method are discussed with given examples of experimental configurations and results obtained from AE monitoring and data analysis of two different processes addressing particular issues related to the nuclear waste immobilisation. These are (a) corrosion of aluminium, classified as intermediate level waste (ILW) in the UK, encapsulated in cementitious structures and (b) partial melting and solidification during cooling of granite at a pressure of 0.15 GPa which simulates the conditions in a deep borehole disposal of canisters of vitrified high level waste (HLW). Methodology for analysis of the collected data and characterisation of the potential AE sources is performed at different steps including simple signals count and more complex signal parameter-based approach and advanced signal processing. The AE method has been shown as a potential tool for monitoring and inspection of structures immobilising nuclear wastes in relation to the time progress of different interactions of the waste with the encapsulating matrix or the wasteform with the hosting environment for permanent disposal. (author)

Using acoustic emission technique to monitor fractures on the analogous pressure pipes

International Nuclear Information System (INIS)

Zhang Lichen

1989-01-01

By using the acoustic emission technique to monitor the fractures on analogous pressure pipes of the primary circuit which has had cracks and loading with pressure was investigated. The dynamical process, from cracking to fracturing, was recorded by the acoustic emission technique. Comparing with the conventional method, this method gives more informations, such as pre-cracking, cracking growing, fast fracturing and the pressure values at different phases. During testing time a microcomputer was used for real-time data processing and locating the fracturing position. These data are useful for the mechanical analysis of the reactor components

Acoustic emission for on-line reactor monitoring: results from field tests

International Nuclear Information System (INIS)

Hutton, P.H.; Kurtz, R.J.

1984-09-01

The objective of the acoustic emission (AE)/flaw characterization program is to develop use of the AE method on a continuous basis (during operation and during hydrotest) to detect and analyze flaw growth in reactor pressure vessels and primary piping. AE has the unique capability for continuous monitoring, high sensitivity, and remote flaw location

Activated sludge characterization through microscopy: A review on quantitative image analysis and chemometric techniques

Energy Technology Data Exchange (ETDEWEB)

Mesquita, Daniela P. [IBB-Institute for Biotechnology and Bioengineering, Centre of Biological Engineering, Universidade do Minho, Campus de Gualtar, 4710-057 Braga (Portugal); Amaral, A. Luís [IBB-Institute for Biotechnology and Bioengineering, Centre of Biological Engineering, Universidade do Minho, Campus de Gualtar, 4710-057 Braga (Portugal); Instituto Politécnico de Coimbra, ISEC, DEQB, Rua Pedro Nunes, Quinta da Nora, 3030-199 Coimbra (Portugal); Ferreira, Eugénio C., E-mail: ecferreira@deb.uminho.pt [IBB-Institute for Biotechnology and Bioengineering, Centre of Biological Engineering, Universidade do Minho, Campus de Gualtar, 4710-057 Braga (Portugal)

2013-11-13

Graphical abstract: -- Highlights: •Quantitative image analysis shows potential to monitor activated sludge systems. •Staining techniques increase the potential for detection of operational problems. •Chemometrics combined with quantitative image analysis is valuable for process monitoring. -- Abstract: In wastewater treatment processes, and particularly in activated sludge systems, efficiency is quite dependent on the operating conditions, and a number of problems may arise due to sludge structure and proliferation of specific microorganisms. In fact, bacterial communities and protozoa identification by microscopy inspection is already routinely employed in a considerable number of cases. Furthermore, quantitative image analysis techniques have been increasingly used throughout the years for the assessment of aggregates and filamentous bacteria properties. These procedures are able to provide an ever growing amount of data for wastewater treatment processes in which chemometric techniques can be a valuable tool. However, the determination of microbial communities’ properties remains a current challenge in spite of the great diversity of microscopy techniques applied. In this review, activated sludge characterization is discussed highlighting the aggregates structure and filamentous bacteria determination by image analysis on bright-field, phase-contrast, and fluorescence microscopy. An in-depth analysis is performed to summarize the many new findings that have been obtained, and future developments for these biological processes are further discussed.

Chilean flour and wheat grain: tracing their origin using near infrared spectroscopy and chemometrics.

Science.gov (United States)

González-Martín, Ma Inmaculada; Wells Moncada, Guillermo; González-Pérez, Claudio; Zapata San Martín, Nelson; López-González, Fernando; Lobos Ortega, Iris; Hernández-Hierro, Jose-Miguel

2014-02-15

Instrumental techniques such a near-infrared spectroscopy (NIRS) are used in industry to monitor and establish product composition and quality. As occurs with other food industries, the Chilean flour industry needs simple, rapid techniques to objectively assess the origin of different products, which is often related to their quality. In this sense, NIRS has been used in combination with chemometric methods to predict the geographic origin of wheat grain and flour samples produced in different regions of Chile. Here, the spectral data obtained with NIRS were analysed using a supervised pattern recognition method, Discriminat Partial Least Squares (DPLS). The method correctly classified 76% of the wheat grain samples and between 90% and 96% of the flour samples according to their geographic origin. The results show that NIRS, together with chemometric methods, provides a rapid tool for the classification of wheat grain and flour samples according to their geographic origin. Copyright © 2013 Elsevier Ltd. All rights reserved.

Chemometric strategy for automatic chromatographic peak detection and background drift correction in chromatographic data.

Science.gov (United States)

Yu, Yong-Jie; Xia, Qiao-Ling; Wang, Sheng; Wang, Bing; Xie, Fu-Wei; Zhang, Xiao-Bing; Ma, Yun-Ming; Wu, Hai-Long

2014-09-12

Peak detection and background drift correction (BDC) are the key stages in using chemometric methods to analyze chromatographic fingerprints of complex samples. This study developed a novel chemometric strategy for simultaneous automatic chromatographic peak detection and BDC. A robust statistical method was used for intelligent estimation of instrumental noise level coupled with first-order derivative of chromatographic signal to automatically extract chromatographic peaks in the data. A local curve-fitting strategy was then employed for BDC. Simulated and real liquid chromatographic data were designed with various kinds of background drift and degree of overlapped chromatographic peaks to verify the performance of the proposed strategy. The underlying chromatographic peaks can be automatically detected and reasonably integrated by this strategy. Meanwhile, chromatograms with BDC can be precisely obtained. The proposed method was used to analyze a complex gas chromatography dataset that monitored quality changes in plant extracts during storage procedure. Copyright © 2014 Elsevier B.V. All rights reserved.

Prototype acoustic resonance spectroscopy monitor

International Nuclear Information System (INIS)

Sinha, D.N.; Olinger, C.T.

1996-03-01

This report reports on work performed for the International Atomic Energy Agency (IAEA) through the Program Office for Technical Assistance (POTAS). In this work, we investigate possible applications of nondestructive acoustics measurements to facilitate IAEA safeguards at bulk processing facilities. Two different acoustic techniques for verifying the internal structure of a processing tank were investigated. During this effort we also examined two acoustic techniques for assessing the fill level within a processing tank. The fill-level measurements could be made highly portable and have an added safeguards advantage that they can also detect stratification of fill material. This later application may be particularly useful in confirming the absence of stratification in plutonium processing tanks before accountability samples are withdrawn

Monitoring power breakers using vibro acoustic techniques

Directory of Open Access Journals (Sweden)

Horia Balan

2017-09-01

Full Text Available Speaking about the commutation’s equipment, it can be said that the best solution in increasing reliability and lowering the maintenance costs is a continuous monitoring of the equipment. However, if the price/quality ratio is considered, it is obvious that, for the moment, the diagnosis can be also an acceptable solution. Nowadays the predictive maintenance for equipment’s diagnosis is currently replacing the preventive diagnosis. An efficient modality of lowering the maintenance costs is to online monitoring the power breakers, during their operation in the power systems. Consequently any connecting/disconnecting operations may be used in diagnosing a power breaker. Thus any supplementary and superfluous tests and/or maintenance maneuvers are avoided. The paper presents the operational maintenance in a power station with three high voltage active breakers, Areva type. The method of establishing the state of a breaker consists in the comparison between the signature of the acoustic signal provided by the manufacturer and the signal issued from the testing operation of the breaker’s state. The software processing procedure and the methodology of determining the faults of the monitored equipment are also developed. All the tests on the circuit breaker are made according the prescriptions of normative.

Acoustic emission

International Nuclear Information System (INIS)

Nichols, R.W.

1976-01-01

The volume contains six papers which together provide an overall review of the inspection technique known as acoustic emission or stress wave emission. The titles are: a welder's introduction to acoustic emission technology; use of acoustic emission for detection of defects as they arise during fabrication; examples of laboratory application and assessment of acoustic emission in the United Kingdom; (Part I: acoustic emission behaviour of low alloy steels; Part II: fatigue crack assessment from proof testing and continuous monitoring); inspection of selected areas of engineering structures by acoustic emission; Japanese experience in laboratory and practical applications of acoustic emission to welded structures; and ASME acoustic emission code status. (U.K.)

Non-Invasive Acoustic-Based Monitoring of Heavy Water and Uranium Process Solutions

Energy Technology Data Exchange (ETDEWEB)

Pantea, Cristian [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Sinha, Dipen N. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Lakis, Rollin Evan [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Beedle, Christopher Craig [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Davis, Eric Sean [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

2017-11-02

The goals of the project are to leverage laboratory scientific strength in physical acoustics for critical international safeguards applications; create hardware demonstration capability for noninvasive, near real time, and low cost process monitor to capture future technology development programs; and measure physical property data to support method applicability.

Acoustic emission monitoring from a lab scale high shear granulator--a novel approach.

Science.gov (United States)

Watson, N J; Povey, M J W; Reynolds, G K; Xu, B H; Ding, Y

2014-04-25

A new approach to the monitoring of granulation processes using passive acoustics together with precise control over the granulation process has highlighted the importance of particle-particle and particle-bowl collisions in acoustic emission. The results have shown that repeatable acoustic results could be obtained but only when a spray nozzle water addition system was used. Acoustic emissions were recorded from a transducer attached to the bowl and an airborne transducer. It was found that the airborne transducer detected very little from the granulation and only experienced small changes throughout the process. The results from the bowl transducer showed that during granulation the frequency content of the acoustic emission shifted towards the lower frequencies. Results from the discrete element model indicate that when larger particles are used the number of collisions the particles experience reduces. This is a result of the volume conservation methodology used in this study, therefore larger particles results in less particles. These simulation results coupled with previous theoretical work on the frequency content of an impacting sphere explain why the frequency content of the acoustic emissions reduces during granule growth. The acoustic system used was also clearly able to identify when large over-wetted granules were present in the system, highlighting its benefit for detecting undesirable operational conditions. High-speed photography was used to study if visual changes in the granule properties could be linked with the changing acoustic emissions. The high speed photography was only possible towards the latter stages of the granulation process and it was found that larger granules produced a higher magnitude of acoustic emission across a broader frequency range. Copyright © 2014 Elsevier B.V. All rights reserved.

Mechanical seal monitoring technique by acoustic emission measurements

Energy Technology Data Exchange (ETDEWEB)

Kataoka, Tadashi; Fujita, Yoshihiro; Kawaguchi, Kazunori; Saito, Kazuhiro; Yokota, Setsuo; Hisada, Yasuhide; Masahiro, Komatsu

1987-09-20

This report describes a technique for mechanical seal monitoring through acoustic emission (AE) measurement. The equipment consists of an AE sensor, preamplifier, multiplexer, main amplifier, effective value transducer and computer system. When the sealed liquid pressure undergoes a large change, the seal surface configuration is monitored and evaluated accurately through AE measurement. If the mechanical seal surface id damaged or worn, the AE level is kept high or continues to fluctuate largely for a rather long period. When leak occurs, the AE value shows great fluctuations either at extremely low levels or at high levels. The former trend is considered to result from a decrease in solid contact due to an excessive amount of liquid film being formed at the seal surface during leak. In the latter case, the leak is attributed to severe damage to the seal surface. (18 figs, 1 tab, 5 photos, 3 refs)

Helium gas purity monitor based on low frequency acoustic resonance

Science.gov (United States)

Kasthurirengan, S.; Jacob, S.; Karunanithi, R.; Karthikeyan, A.

1996-05-01

Monitoring gas purity is an important aspect of gas recovery stations where air is usually one of the major impurities. Purity monitors of Katherometric type are commercially available for this purpose. Alternatively, we discuss here a helium gas purity monitor based on acoustic resonance of a cavity at audio frequencies. It measures the purity by monitoring the resonant frequency of a cylindrical cavity filled with the gas under test and excited by conventional telephone transducers fixed at the ends. The use of the latter simplifies the design considerably. The paper discusses the details of the resonant cavity and the electronic circuit along with temperature compensation. The unit has been calibrated with helium gas of known purities. The unit has a response time of the order of 10 minutes and measures the gas purity to an accuracy of 0.02%. The unit has been installed in our helium recovery system and is found to perform satisfactorily.

Acoustic emission monitoring of preservice testing at Watts Bar Unit 1 Nuclear Reactor

International Nuclear Information System (INIS)

Hutton, P.H.; Pappas, R.A.; Friesel, M.A.

1985-02-01

Acoustic emission (AE) monitoring of selected pressure boundary areas at TVA's Watts Bar, Unit 1 Nuclear Plant in the US during hot functional preservice testing is described. Background, methodology, and results are included. The work discussed here is a major milestone in a program supported by the US NRC to develop and demonstrate application of AE monitoring for continuous surveillance of reactor pressure boundaries to detect and evaluate growing flaws. The subject work demonstrated that anticipated problem areas can be overcome. Work is continuing to AE monitoring during reactor operation. 3 refs., 6 figs

Chemometrics in analytical chemistry-part I: history, experimental design and data analysis tools.

Science.gov (United States)

Brereton, Richard G; Jansen, Jeroen; Lopes, João; Marini, Federico; Pomerantsev, Alexey; Rodionova, Oxana; Roger, Jean Michel; Walczak, Beata; Tauler, Romà

2017-10-01

Chemometrics has achieved major recognition and progress in the analytical chemistry field. In the first part of this tutorial, major achievements and contributions of chemometrics to some of the more important stages of the analytical process, like experimental design, sampling, and data analysis (including data pretreatment and fusion), are summarised. The tutorial is intended to give a general updated overview of the chemometrics field to further contribute to its dissemination and promotion in analytical chemistry.

Head Injury and Intracranial Pressure Monitor Using Ultrasonic and Low-Frequency Acoustic (ULFA) Detection

National Research Council Canada - National Science Library

Vo-Dinh, Tuan

2001-01-01

The main objective of this research project is the development of a non-invasive method and instrument for head injury detection and monitoring using a new approach based on ultrasonic and low-frequency acoustic (ULFA...

Monitoring of martensite formation during welding by means of acoustic emission

International Nuclear Information System (INIS)

Bohemen, S.M.C. van; Hermans, M.J.M.; Ouden, G. den

2001-01-01

The martensitic transformation during gas tungsten arc (GTA) welding of steel 42CrMo4 has been studied using the acoustic emission (AE) monitoring technique. Welds were produced under static conditions (spot welding) and under stationary conditions (travelling arc welding). After spot welding, the root mean square (RMS) value of the continuous acoustic emission was measured, revealing a peak that reflects the evolution of martensite formation during cooling of the spot weld. The RMS value was also measured during travelling arc welding at different heat inputs and corrected for the noise of the welding process to obtain the RMS value due to martensite formation. After welding, optical metallography was carried out to quantify the amount of martensite formed during cooling of the weld. An analysis of the results shows that the squared RMS value is proportional to the volume rate of martensite formation during welding, which is consistent with theory and in good agreement with the results obtained in the case of spot welding. The obtained results suggest that AE can be applied as a real time monitoring technique for the detection of martensite formation during steel welding. (author)

Fundamental and assessment of concrete structure monitoring by using acoustic emission technique testing: A review

Science.gov (United States)

Desa, M. S. M.; Ibrahim, M. H. W.; Shahidan, S.; Ghadzali, N. S.; Misri, Z.

2018-04-01

Acoustic emission (AE) technique is one of the non-destructive (NDT) testing, where it can be used to determine the damage of concrete structures such as crack, corrosion, stability, sensitivity, as structure monitoring and energy formed within cracking opening growth in the concrete structure. This article gives a comprehensive review of the acoustic emission (AE) technique testing due to its application in concrete structure for structural health monitoring (SHM). Assessment of AE technique used for structural are reviewed to give the perception of its structural engineering such as dam, bridge and building, where the previous research has been reviewed based on AE application. The assessment of AE technique focusing on basic fundamental of parametric and signal waveform analysis during analysis process and its capability in structural monitoring. Moreover, the assessment and application of AE due to its function have been summarized and highlighted for future references

Chemometric Strategies for Peak Detection and Profiling from Multidimensional Chromatography.

Science.gov (United States)

Navarro-Reig, Meritxell; Bedia, Carmen; Tauler, Romà; Jaumot, Joaquim

2018-04-03

The increasing complexity of omics research has encouraged the development of new instrumental technologies able to deal with these challenging samples. In this way, the rise of multidimensional separations should be highlighted due to the massive amounts of information that provide with an enhanced analyte determination. Both proteomics and metabolomics benefit from this higher separation capacity achieved when different chromatographic dimensions are combined, either in LC or GC. However, this vast quantity of experimental information requires the application of chemometric data analysis strategies to retrieve this hidden knowledge, especially in the case of nontargeted studies. In this work, the most common chemometric tools and approaches for the analysis of this multidimensional chromatographic data are reviewed. First, different options for data preprocessing and enhancement of the instrumental signal are introduced. Next, the most used chemometric methods for the detection of chromatographic peaks and the resolution of chromatographic and spectral contributions (profiling) are presented. The description of these data analysis approaches is complemented with enlightening examples from omics fields that demonstrate the exceptional potential of the combination of multidimensional separation techniques and chemometric tools of data analysis. © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Acoustic Emission Technology and Application

International Nuclear Information System (INIS)

Joo, Y. S.; Lim, S. H.; Eom, H. S.; Kim, J. H.; Jung, H. K.

2003-10-01

Acoustic emission is the elastic wave that is generated by the rapid release of energy from the localized sources within a material. After the observation of acoustic emission phenomenon in 1950, the research and further investigation had been performed. Acoustic emission examination becomes a rapidly matured nondestructive testing method with demonstrated capabilities for characterizing material behavior and for detecting the defect. It is of interest as a possible passive monitoring technique for detecting, locating and characterizing the defects in component and structure. Acoustic emission technology has recently strengthened the on-line monitoring application for the detection of incipient failures and the assurance of structural integrity. The field of acoustic emission testing is still growing vigorously and presents many challenges. Especially, acoustic emission has been successfully applied in the leak detection of primary pressure boundary of nuclear power plants. In this state-of-art report, the principle, measurement and field applications of acoustic emission technique is reviewed and summarized. Acoustic emission technology will contribute to the assurance of nuclear safety as the on-line monitoring technique of structural integrity of NSSS components and structures

Acoustic engineering and technology '90. Acoustic monitoring methods in maintenance and quality assurance and their effects on noise reduction. Schalltechnik '90. Akustische Ueberwachungsmethoden bei der Instandhaltung und Qualitaetssicherung und ihre Auswirkungen auf die Laermminderung

Energy Technology Data Exchange (ETDEWEB)

1990-01-01

Acoustic monitoring, testing and diagnosis in machines, production processes and products enhance the uptimes and profitability of machinery and plants. 18 papers discuss the current state of the art of acoustic monitoring systems including integrated factory planning as well as industrial health, and noise protection. (DG).

Application of the pattern recognition technique to fast reactor acoustic monitoring

International Nuclear Information System (INIS)

Brunet, M.; Val, M.

1981-10-01

The early detection of operating anomalies is an aim involving the safety of fast reactors. The most likely accident is the complete or partial blocking up of an assembly, one of the signs of which is the boiling of the sodium contained in it. This boiling is accompanied by the production of acoustic waves, the detection of which by appropriate sensors appears to be an efficient way of monitoring the core. For a number of years the CEA has been conducting an experimental programme for studying the detection of boiling by acoustic means. The text presents the various different experiments undertaken and then draws a parallel between the results obtained by conventional processing procedures and those obtained by applying the shape recognition method to the same basic data [fr

In Situ Acoustic Monitoring of Thermal Spray Process Using High-Frequency Impulse Measurements

Science.gov (United States)

Tillmann, Wolfgang; Walther, Frank; Luo, Weifeng; Haack, Matthias; Nellesen, Jens; Knyazeva, Marina

2018-01-01

In order to guarantee their protective function, thermal spray coatings must be free from cracks, which expose the substrate surface to, e.g., corrosive media. Cracks in thermal spray coatings are usually formed because of tensile residual stresses. Most commonly, the crack occurrence is determined after the thermal spraying process by examination of metallographic cross sections of the coating. Recent efforts focus on in situ monitoring of crack formation by means of acoustic emission analysis. However, the acoustic signals related to crack propagation can be absorbed by the noise of the thermal spraying process. In this work, a high-frequency impulse measurement technique was applied to separate different acoustic sources by visualizing the characteristic signal of crack formation via quasi-real-time Fourier analysis. The investigations were carried out on a twin wire arc spraying process, utilizing FeCrBSi as a coating material. The impact of the process parameters on the acoustic emission spectrum was studied. Acoustic emission analysis enables to obtain global and integral information on the formed cracks. The coating morphology and coating defects were inspected using light microscopy on metallographic cross sections. Additionally, the resulting crack patterns were imaged in 3D by means of x-ray microtomography.

Monitoring of Carbon Fiber-Reinforced Old Timber Beams via Strain and Multiresonant Acoustic Emission Sensors

Directory of Open Access Journals (Sweden)

Francisco J. Rescalvo

2018-04-01

Full Text Available This paper proposes the monitoring of old timber beams with natural defects (knots, grain deviations, fissures and wanes, reinforced using carbon composite materials (CFRP. Reinforcement consisted of the combination of a CFRP laminate strip and a carbon fabric discontinuously wrapping the timber element. Monitoring considered the use and comparison of two types of sensors: strain gauges and multi-resonant acoustic emission (AE sensors. Results demonstrate that: (1 the mechanical behavior of the beams can be considerably improved by means of the use of CFRP (160% in bending load capacity and 90% in stiffness; (2 Acoustic emission sensors provide comparable information to strain gauges. This fact points to the great potential of AE techniques for in-service damage assessment in real wood structures.

Monitoring of Carbon Fiber-Reinforced Old Timber Beams via Strain and Multiresonant Acoustic Emission Sensors.

Science.gov (United States)

Rescalvo, Francisco J; Valverde-Palacios, Ignacio; Suarez, Elisabet; Roldán, Andrés; Gallego, Antolino

2018-04-17

This paper proposes the monitoring of old timber beams with natural defects (knots, grain deviations, fissures and wanes), reinforced using carbon composite materials (CFRP). Reinforcement consisted of the combination of a CFRP laminate strip and a carbon fabric discontinuously wrapping the timber element. Monitoring considered the use and comparison of two types of sensors: strain gauges and multi-resonant acoustic emission (AE) sensors. Results demonstrate that: (1) the mechanical behavior of the beams can be considerably improved by means of the use of CFRP (160% in bending load capacity and 90% in stiffness); (2) Acoustic emission sensors provide comparable information to strain gauges. This fact points to the great potential of AE techniques for in-service damage assessment in real wood structures.

Acoustic Monitoring of the Arctic Ice Cap

Science.gov (United States)

Porter, D. L.; Goemmer, S. A.; Chayes, D. N.

2012-12-01

Introduction The monitoring of the Arctic Ice Cap is important economically, tactically, and strategically. In the scenario of ice cap retreat, new paths of commerce open, e.g. waterways from Northern Europe to the Far East. Where ship-going commerce is conducted, the U.S. Navy and U.S. Coast Guard have always stood guard and been prepared to assist from acts of nature and of man. It is imperative that in addition to measuring the ice from satellites, e.g. Icesat, that we have an ability to measure the ice extent, its thickness, and roughness. These parameters play an important part in the modeling of the ice and the processes that control its growth or shrinking and its thickness. The proposed system consists of three subsystems. The first subsystem is an acoustic source, the second is an array of geophones and the third is a system to supply energy and transmit the results back to the analysis laboratory. The subsystems are described below. We conclude with a plan on how to tackle this project and the payoff to the ice cap modeler and hence the users, i.e. commerce and defense. System Two historically tested methods to generate a large amplitude multi-frequency sound source include explosives and air guns. A new method developed and tested by the University of Texas, ARL is a combustive Sound Source [Wilson, et al., 1995]. The combustive sound source is a submerged combustion chamber that is filled with the byproducts of the electrolysis of sea water, i.e. Hydrogen and Oxygen, an explosive mixture which is ignited via a spark. Thus, no additional compressors, gases, or explosives need to be transported to the Arctic to generate an acoustic pulse capable of the sediment and the ice. The second subsystem would be geophones capable of listening in the O(10 Hz) range and transmitting that data back to the laboratory. Thus two single arrays of geophones arranged orthogonal to each other with a range of 1000's of kilometers and a combustive sound source where the two

Crack Propagation Analysis Using Acoustic Emission Sensors for Structural Health Monitoring Systems

Science.gov (United States)

Horn, Walter; Steck, James

2013-01-01

Aerospace systems are expected to remain in service well beyond their designed life. Consequently, maintenance is an important issue. A novel method of implementing artificial neural networks and acoustic emission sensors to form a structural health monitoring (SHM) system for aerospace inspection routines was the focus of this research. Simple structural elements, consisting of flat aluminum plates of AL 2024-T3, were subjected to increasing static tensile loading. As the loading increased, designed cracks extended in length, releasing strain waves in the process. Strain wave signals, measured by acoustic emission sensors, were further analyzed in post-processing by artificial neural networks (ANN). Several experiments were performed to determine the severity and location of the crack extensions in the structure. ANNs were trained on a portion of the data acquired by the sensors and the ANNs were then validated with the remaining data. The combination of a system of acoustic emission sensors, and an ANN could determine crack extension accurately. The difference between predicted and actual crack extensions was determined to be between 0.004 in. and 0.015 in. with 95% confidence. These ANNs, coupled with acoustic emission sensors, showed promise for the creation of an SHM system for aerospace systems. PMID:24023536

Passive acoustic monitoring of toothed whales with implications for mitigation, management and biology

DEFF Research Database (Denmark)

Kyhn, Line Anker

these differences to successfully differentiate the species in Monte Carlo simulations, which means that it may also be possible to separate sympatric NBHF species with acoustic monitoring. Secondly, I was interested in examining the species differences in an evolutionary light to see if there were differences...... that describes the probability of detecting an acoustic cue at a given distance from the datalogger? In chapter II I describe one such possibility where we tracked harbour porpoises visually around dataloggers by means of a theodolite and following compared the visual and acoustic detections in a mark...... is in accordance with new molecular phylogenies. In chapter I use the information I have gathered on spectral source properties as well as on source levels and directionality and use this information to challenge the theories for the evolution of the NBHF click type. I conclude that the NBHF signals likely evolved...

Monitoring of lubrication conditions in journal bearing by acoustic emission

International Nuclear Information System (INIS)

Yoon, Dong Jin; Kwon, Oh Yang; Jung, Min Hwa

1993-01-01

Systems with journal bearings generally operate in large scale and under severe loading conditions such as steam generator turbines and internal combustion engines, in contrast to the machinery using rolling element bearings. Failure of the bearings in these machinery can result in the system breakdown. To avoid the time consuming repair and considerable economic loss, the detection of incipient failure in journal bearings becomes very important. In this experimental approach, acoustic emission monitoring is employed to the detection of incipient failure caused by intervention of foreign particles most probable in the journal bearing systems. It has been known that the intervention of foreign materials, insufficient lubrication and misassembly etc. are principal factors to cause bearing failure and distress. The experiment was conducted under such designed conditions as inserting alumina particles to the lubrication layer in the simulated journal bearing system. The results showed that acoustic emission could be an effective tool to detect the incipient failure in journal bearings.

Application of acoustic emission monitoring to pressure tests of a steam receiver vessel with flawed nozzle welds

International Nuclear Information System (INIS)

Woodward, B.; McDonald, N.R.; Hincksman, M.J.

1976-01-01

As part of the first stage of an Australian Welding Research Association co-operative research project, acoustic emission monitoring has been applied to a steam receiver vessel withdrawn from service owing to severe weld cracking. This technique is used to check acceptance standards for defects in nozzle welds and to apply modern methods of assessing the integrity of pressurised plant. Acoustic emission monitoring has been used, together with strain gauge measurements and ultrasonic scanning, to detect the occurrence of any significant defect growth during cyclic pressurisation of the vessel. During this first stage, no significant defect growth has been produced by 1000 cycles of pressure up to 24.1 MPa (3500 psi), subsequent pressurisation up to 35.8 MPa (5200 psi), or 97 per cent of the expected yield stress of the vessel shell. The small amount of acoustic emission detected was consistent with this result. (author)

On the Application of the Raspberry Pi as an Advanced Acoustic Sensor Network for Noise Monitoring

Directory of Open Access Journals (Sweden)

Juan Emilio Noriega-Linares

2016-10-01

Full Text Available The concept of Smart Cities and the monitoring of environmental parameters is an area of research that has attracted scientific attention during the last decade. These environmental parameters are well-known as important factors in their affection towards people. Massive monitoring of this kind of parameters in cities is an expensive and complex task. Recent technologies of low-cost computing and low-power devices have opened researchers to a wide and more accessible research field, developing monitoring devices for deploying Wireless Sensor Networks. Gathering information from them, improved urban plans could be carried out and the information could help citizens. In this work, the prototyping of a low-cost acoustic sensor based on the Raspberry Pi platform for its use in the analysis of the sound field is described. The device is also connected to the cloud to share results in real time. The computation resources of the Raspberry Pi allow treating high quality audio for calculating acoustic parameters. A pilot test was carried out with the installation of two acoustic devices in the refurbishment works of a neighbourhood. In this deployment, the evaluation of these devices through long-term measurements was carried out, obtaining several acoustic parameters in real time for its broadcasting and study. This test has shown the Raspberry Pi as a powerful and affordable computing core of a low-cost device, but also the pilot test has served as a query tool for the inhabitants of the neighbourhood to be more aware about the noise in their own place of residence.

Acoustic monitoring of rotating machine by advanced signal processing technology

International Nuclear Information System (INIS)

Kanemoto, Shigeru

2010-01-01

The acoustic data remotely measured by hand held type microphones are investigated for monitoring and diagnosing the rotational machine integrity in nuclear power plants. The plant operator's patrol monitoring is one of the important activities for condition monitoring. However, remotely measured sound has some difficulties to be considered for precise diagnosis or quantitative judgment of rotating machine anomaly, since the measurement sensitivity is different in each measurement, and also, the sensitivity deteriorates in comparison with an attached type sensor. Hence, in the present study, several advanced signal processing methods are examined and compared in order to find optimum anomaly monitoring technology from the viewpoints of both sensitivity and robustness of performance. The dimension of pre-processed signal feature patterns are reduced into two-dimensional space for the visualization by using the standard principal component analysis (PCA) or the kernel based PCA. Then, the normal state is classified by using probabilistic neural network (PNN) or support vector data description (SVDD). By using the mockup test facility of rotating machine, it is shown that the appropriate combination of the above algorithms gives sensitive and robust anomaly monitoring performance. (author)

Evolving chemometric models for predicting dynamic process parameters in viscose production

Energy Technology Data Exchange (ETDEWEB)

Cernuda, Carlos [Department of Knowledge-Based Mathematical Systems, Johannes Kepler University Linz (Austria); Lughofer, Edwin, E-mail: edwin.lughofer@jku.at [Department of Knowledge-Based Mathematical Systems, Johannes Kepler University Linz (Austria); Suppan, Lisbeth [Kompetenzzentrum Holz GmbH, St. Peter-Str. 25, 4021 Linz (Austria); Roeder, Thomas; Schmuck, Roman [Lenzing AG, 4860 Lenzing (Austria); Hintenaus, Peter [Software Research Center, Paris Lodron University Salzburg (Austria); Maerzinger, Wolfgang [i-RED Infrarot Systeme GmbH, Linz (Austria); Kasberger, Juergen [Recendt GmbH, Linz (Austria)

2012-05-06

Highlights: Black-Right-Pointing-Pointer Quality assurance of process parameters in viscose production. Black-Right-Pointing-Pointer Automatic prediction of spin-bath concentrations based on FTNIR spectra. Black-Right-Pointing-Pointer Evolving chemometric models for efficiently handling changing system dynamics over time (no time-intensive re-calibration needed). Black-Right-Pointing-Pointer Significant reduction of huge errors produced by statistical state-of-the-art calibration methods. Black-Right-Pointing-Pointer Sufficient flexibility achieved by gradual forgetting mechanisms. - Abstract: In viscose production, it is important to monitor three process parameters in order to assure a high quality of the final product: the concentrations of H{sub 2}SO{sub 4}, Na{sub 2}SO{sub 4} and Z{sub n}SO{sub 4}. During on-line production these process parameters usually show a quite high dynamics depending on the fiber type that is produced. Thus, conventional chemometric models, which are trained based on collected calibration spectra from Fourier transform near infrared (FT-NIR) measurements and kept fixed during the whole life-time of the on-line process, show a quite imprecise and unreliable behavior when predicting the concentrations of new on-line data. In this paper, we are demonstrating evolving chemometric models which are able to adapt automatically to varying process dynamics by updating their inner structures and parameters in a single-pass incremental manner. These models exploit the Takagi-Sugeno fuzzy model architecture, being able to model flexibly different degrees of non-linearities implicitly contained in the mapping between near infrared spectra (NIR) and reference values. Updating the inner structures is achieved by moving the position of already existing local regions and by evolving (increasing non-linearity) or merging (decreasing non-linearity) new local linear predictors on demand, which are guided by distance-based and similarity criteria. Gradual

Acoustic system for pipe rupture monitoring and leak detection

International Nuclear Information System (INIS)

Herzog, W.; Jonas, H.

1982-06-01

As a safety aspect pipe rupture and leakage effects are of particular interest in nuclear power plants where severe consequences for the reactor may result. Counter measures against postulated pipe breaks and leakages in nuclear power plants are necessary whenever the main safety goals: safe shut-down, safe afterheat removal and retention of radioactivity, are endangered. The requirements to be met by a leak detection system depend on the time available for counter actions. If this time is short so that automatic actions are necessary the German safety criteria for nuclear power plants (Criterion 6.1) require two physically diverse signals to be monitored. One fairly obvious possibility of leak detection is to monitor process parameters (pressure, flow). As a diverse signal physical parameters outside the process may be employed: pressure transients temperature, humidity are principally suitable. In practical application, however, it is difficult to predict these parameters by way of calculation in order to establish the required set-point of the monitoring system. Experimental determination is possible only in special cases. A study of several ways of diverse leak detection methods leads to the very promising acoustic method. We investigated experimentally the feasibility of monitoring the sound created by a leakage. Air borne sound as well as body borne sound was analyzed

Acoustic remote monitoring of rock and concrete structures for nuclear waste repositories

International Nuclear Information System (INIS)

Young, R.P.

2000-01-01

Excavation and thermally induced damage is of significance for many types of engineering structures but no more so than in the case of nuclear waste repository design. My research and that of my group, formally at Queen's University Canada and Keele University UK and now at the University of Liverpool UK, has focused on the development of acoustic techniques for the in situ detection and quantification of induced damage and fracturing. The application of earthquake seismology to this problem has provided the opportunity to study the micro mechanics of damage mechanisms in situ and provide validation data for predictive geomechanical models used for engineering design. Since 1987 I have been a principal investigator at Atomic Energy of Canada's Underground Research Laboratory (URL), responsible for the development of acoustic emission techniques (AE). In the last twelve years, the application of acoustic techniques to rock damage assessment has been pioneered by my group at the URL and successfully applied in several other major international projects including the ZEDEX, Retrieval and Prototype repository experiments at the Aspo Hard Rock Laboratory (HRL) of SKB Sweden. In this paper I describe what information is available by remote acoustic monitoring of rock and concrete structures and demonstrate this with reference to two international scientific experiments carried out at the URL Canada and the HRL Sweden. (author)

Accuracy of acoustic respiration rate monitoring in pediatric patients.

Science.gov (United States)

Patino, Mario; Redford, Daniel T; Quigley, Thomas W; Mahmoud, Mohamed; Kurth, C Dean; Szmuk, Peter

2013-12-01

Rainbow acoustic monitoring (RRa) utilizes acoustic technology to continuously and noninvasively determine respiratory rate from an adhesive sensor located on the neck. We sought to validate the accuracy of RRa, by comparing it to capnography, impedance pneumography, and to a reference method of counting breaths in postsurgical children. Continuous respiration rate data were recorded from RRa and capnography. In a subset of patients, intermittent respiration rate from thoracic impedance pneumography was also recorded. The reference method, counted respiratory rate by the retrospective analysis of the RRa, and capnographic waveforms while listening to recorded breath sounds were used to compare respiration rate of both capnography and RRa. Bias, precision, and limits of agreement of RRa compared with capnography and RRa and capnography compared with the reference method were calculated. Tolerance and reliability to the acoustic sensor and nasal cannula were also assessed. Thirty-nine of 40 patients (97.5%) demonstrated good tolerance of the acoustic sensor, whereas 25 of 40 patients (62.5%) demonstrated good tolerance of the nasal cannula. Intermittent thoracic impedance produced erroneous respiratory rates (>50 b·min(-1) from the other methods) on 47% of occasions. The bias ± SD and limits of agreement were -0.30 ± 3.5 b·min(-1) and -7.3 to 6.6 b·min(-1) for RRa compared with capnography; -0.1 ± 2.5 b·min(-1) and -5.0 to 5.0 b·min(-1) for RRa compared with the reference method; and 0.2 ± 3.4 b·min(-1) and -6.8 to 6.7 b·min(-1) for capnography compared with the reference method. When compared to nasal capnography, RRa showed good agreement and similar accuracy and precision but was better tolerated in postsurgical pediatric patients. © 2013 John Wiley & Sons Ltd.

Laser tattoo removal as an ablation process monitored by acoustical and optical methods

Science.gov (United States)

Cencič, Boris; Gregorčič, Peter; Možina, Janez; Jezeršek, Matija

2013-07-01

Strength of the laser-tissue interaction varies even within a single tattoo because of the inhomogeneous distribution of the tattoo pigment embedded in the skin. A monitoring system is therefore developed for simultaneous monitoring of the laser tattoo removal process based on acoustical and optical techniques. A laser-beam-deflection probe is used for measuring the acoustical signals accompanying the breakdown, and a CCD camera captures the level and the spatial distribution of the plasma radiation. Using these methods we examine the degree of excitation-pulse absorption within the pigment and the degree of the structural changes of the skin. A Nd:YAG laser with a top-hat beam profile, designed for tattoo removal, is used as the excitation source in our experiments. Special attention is given to structural changes in the skin, which depend on the applied fluence. Tattoo removal with multiple pulses is also analyzed. Experiments are made in vitro (skin phantoms) and ex vivo (marking tattoos on the pig skin). The presented results are important for the understanding and optimization of the process used in medical therapies.

Evaluation of the sensitivity of electro-acoustic measurements for process monitoring and control of an atmospheric pressure plasma jet system

Energy Technology Data Exchange (ETDEWEB)

Law, V J [Dublin City University, National Centre of Plasma Science and Technology, Collins Avenue, Glasnevin, Dublin 9, Dublin (Ireland); O' Neill, F T; Dowling, D P, E-mail: vic.law@dcu.ie [School Mechanical and Materials Engineering, University College Dublin, Belfield, Dublin 4 (Ireland)

2011-06-15

The development of non-invasive process diagnostic techniques for the control of atmospheric plasmas is a critical issue for the wider adoption of this technology. This paper evaluates the use of a frequency-domain deconvolution of an electro-acoustic emission as a means to monitor and control the plasma formed using an atmospheric pressure plasma jet (APPJ) system. The air plasma system investigated was formed using a PlasmaTreat(TM) OpenAir applicator. Change was observed in the electro-acoustic signal with changes in substrate type (ceramic, steel, polymer). APPJ nozzle to substrate distance and substrate feature size were monitored. The decoding of the electro-acoustic emission yields three subdatasets that are described by three separate emission mechanisms. The three emissions are associated with the power supply fundamental drive frequency and its harmonics, the APPJ nozzle longitudinal mode acoustic emission and its odd overtones, and the acoustic surface reflection that is produced by the impedance mismatch between the discharge and the surface. Incorporating this knowledge into a LabVIEW program facilitated the continuous deconvolution of the electro-acoustic data. This enabled the use of specific frequency band test limits to control the APPJ treatment process which is sensitive to both plasma processing conditions and substrate type and features.

Online monitoring of pipe wall thinning by electromagnetic acoustic resonance method

International Nuclear Information System (INIS)

Urayama, Ryoichi; Takagi, Toshiyuki; Uchimoto, Tetsuya; Kanemoto, Shigeru

2013-01-01

The electromagnetic acoustic resonance (EMAR) method provides accurate and stable evaluation in high temperature environment, and it is an effective tool for online monitoring. In this study, the EMAR method and the superposition of the n-th compression (SNC) for data processing are applied to online monitoring of pipe wall thinning, and the accuracy and reliability of the measurements are demonstrated through field tests using a large-scale corrosion test loop at high temperature. To measure the thickness of pipes with complicated wall thinning, the SNC extracts thickness information from the spectral responses of the EMAR. Results from monitoring test show that EMAR with SNC can evaluate pipe wall thinning with an accuracy of 10 μm at 165degC. In addition, time evaluation of evaluated thickness decreases monotonically all over the test duration, which indicates high stability of this measurement technique. (author)

Acoustic engineering and technology '90

International Nuclear Information System (INIS)

1990-01-01

Acoustic monitoring, testing and diagnosis in machines, production processes and products enhance the uptimes and profitability of machinery and plants. 18 papers discuss the current state of the art of acoustic monitoring systems including integrated factory planning as well as industrial health, and noise protection. (DG) [de

Analysis of Precursors Prior to Rock Burst in Granite Tunnel Using Acoustic Emission and Far Infrared Monitoring

OpenAIRE

Liang, Zhengzhao; Liu, Xiangxin; Zhang, Yanbo; Tang, Chunan

2013-01-01

To understand the physical mechanism of the anomalous behaviors observed prior to rock burst, the acoustic emission (AE) and far infrared (FIR) techniques were applied to monitor the progressive failure of a rock tunnel model subjected to biaxial stresses. Images of fracturing process, temperature changes of the tunnel, and spatiotemporal serials of acoustic emission were simultaneously recorded during deformation of the model. The b-value derived from the amplitude distribution data of AE wa...

Acoustic surveillance techniques for SGU leak monitoring

International Nuclear Information System (INIS)

McKnight, J.A.; Rowley, R.; Beesley, M.J.

1990-01-01

The paper presents a brief review of the acoustic techniques applicable to the detection of steam generator unit leaks that have been studied in the UK. Before discussion of the acoustic detection methods a reference representation of the required performance as developed in the UK is given. The conclusion is made that preliminary specification for the acoustic leak detection of sodium/water leaks in steam generating units suggests that it will be necessary to detect better than a leak rate of 3 g/s within a few seconds. 10 refs, 12 figs

[Identification of two varieties of Citri Fructus by fingerprint and chemometrics].

Science.gov (United States)

Su, Jing-hua; Zhang, Chao; Sun, Lei; Gu, Bing-ren; Ma, Shuang-cheng

2015-06-01

Citri Fructus identification by fingerprint and chemometrics was investigated in this paper. Twenty-three Citri Fructus samples were collected which referred to two varieties as Cirtus wilsonii and C. medica recorded in Chinese Pharmacopoeia. HPLC chromatograms were obtained. The components were partly identified by reference substances, and then common pattern was established for chemometrics analysis. Similarity analysis, principal component analysis (PCA) , partial least squares-discriminant analysis (PLS-DA) and hierarchical cluster analysis heatmap were applied. The results indicated that C. wilsonii and C. medica could be ideally classified with common pattern contained twenty-five characteristic peaks. Besides, preliminary pattern recognition had verified the chemometrics analytical results. Absolute peak area (APA) was used for relevant quantitative analysis, results showed the differences between two varieties and it was valuable for further quality control as selection of characteristic components.

{sup 1}H qNMR and chemometric analyses of urban wastewater

Energy Technology Data Exchange (ETDEWEB)

Alves Filho, Elenilson G.; Silva, Lorena M. A.; Venâncio, Tiago; Carneiro, Renato L.; Ferreira, Antonio G., E-mail: elenilson.godoy@yahoo.com.br [Universidade Federal de São Carlos (UFSCar), São Carlos, SP (Brazil). Departamento de Química; Sartori, Luci [Serviço Autônomo de Água e Esgoto de São Carlos (SAAE), São Carlos, SP (Brazil)

2015-07-01

The industrial development, urbanization and agriculture play a major role in the degradation of the global environmental. Thus, the wastewater treatments need to be monitored continuously to ensure efficient operation. This manuscript presents an application of {sup 1}H nuclear magnetic resonance (NMR) associated with chemometric and quantitative analyses to study the wastewater before and after the sewage treatment plant (STP). The concentration of compounds related to organic matter degradation ranged with treatment and seasonality. Anomalous discharges and the influence of storm water on the sewage composition were further identified. All the variations indicated that the employed procedure might be useful to enhance the effectiveness of STPs, plan prevention actions for equipment protection and preserve the environment. (author)

ONKALO POSE experiment. Phase 3: acoustic and ultrasonic monitoring

International Nuclear Information System (INIS)

Reyes-Montes, J.; Flynn, W.; Huang, J.

2014-01-01

The objectives of the third phase of the POSE experiment are to determine the in situ state of stress at Olkiluoto and the spalling strength of Olkiluoto rock, by internal heating of the experimental hole (ONK-EH3) using 8 vertically installed heaters. This report presents the results from the Acoustic and ultrasonic monitoring carried out around the third experimental hole of the POSE niche between November 2012 and May 2013. The experiment was monitored using an array of 24 transducers installed along 4 monitoring drillholes and data was automatically acquired and processed using the system installed at the niche by Applied Seismology Consultants in May 2012. Daily ultrasonic surveys were carried out between 14 th November 2012 and 21 st May 2013, monitoring the changes in transmission velocities of P and S-waves with an estimated error of ±2 m x s -1 (ASC, 2013). Changes in transmission velocities closely follow the evolution of the temperature profile in the hole wall. An increase in both P-and S-wave transmission velocities is observed at all depth levels and surveyed raypaths during the heating phase, with the highest changes observed in raypaths skimming the hole surface and depths between 2.33 m and 3.7 m. This observation indicates the closure of in situ and excavation-induced microcracks due to thermal stress. After the heaters were switched off, P-wave velocities show a marked decrease, in all raypaths reaching values below those measured at the start of the monitoring approximately 4 weeks after the heaters were switched off. The highest decrease was observed along raypaths surveying the region skimming the hole wall. This decrease below original background values indicates the induction of rock degradation as microcracking induced through the heating-cooling cycle. Changes in P- and S-wave transmission velocity were used to calculate changes in Young's modulus and Poisson's ratio along the different raypaths and depth levels. An overall

Experimental study of advanced continuous acoustic emission monitoring of BWR components. Final report

International Nuclear Information System (INIS)

McElroy, J.W.; Hartman, W.F.

1980-09-01

The program consisted of installing, maintaining, and monitoring AE sensors located on primary piping, nozzles, and valves in the BWR system. Analysis of the AE data was correlated to the results of supplementary nondestructive testing techniques used during the in-service inspection, performed at refueling outages. Purpose of the program was to develop the on-line surveillance acoustic emission technique in order to identify areas of possible structural degradation. Result of reducing inspection time was to reduce accumulated radiation exposure to inspecting personnel and to reduce the amount of critical plant outage time by identifying the critical inspection areas during operation. The program demonstrated the capability of acoustic emission instrumentation to endure the nuclear reactor environment. The acoustic emission sensors withstood 12 months of reactor operation at temperatures of 400 0 F and greater in high radiation fields. The preamplifiers, also mounted in the reactor environment, operated for the 12-month period in 100% humidity, 250 0 F conditions. The remaining cable and AE instrumentation were operated in controlled environments

Health monitoring of Ceramic Matrix Composites from waveform-based analysis of Acoustic Emission

Directory of Open Access Journals (Sweden)

Maillet Emmanuel

2015-01-01

Full Text Available Ceramic Matrix Composites (CMCs are anticipated for use in the hot section of aircraft engines. Their implementation requires the understanding of the various damage modes that are involved and their relation to life expectancy. Acoustic Emission (AE has been shown to be an efficient technique for monitoring damage evolution in CMCs. However, only a waveform-based analysis of AE can offer the possibility to validate and precisely examine the recorded AE data with a view to damage localization and identification. The present work fully integrates wave initiation, propagation and acquisition in the analysis of Acoustic Emission waveforms recorded at various sensors, therefore providing more reliable information to assess the relation between Acoustic Emission and damage modes. The procedure allows selecting AE events originating from damage, accurate determination of their location as well as the characterization of effects of propagation on the recorded waveforms. This approach was developed using AE data recorded during tensile tests on carbon/carbon composites. It was then applied to melt-infiltrated SiC/SiC composites.

Processing of acoustic signal in rock desintegration

Directory of Open Access Journals (Sweden)

Futó Jozef

2002-12-01

Full Text Available For the determination of an effective rock disintegration for a given tool and rock type it is needed to define an optimal disintegration regime. Optimisation of the disintegration process by drilling denotes the finding out an appropriate couple of input parameters of disintegration, i.e. the thrust and revolutions for a quasi-equal rock environment. The disintegration process can be optimised to reach the maximum immediate drilling rate, to reach the minimum specific disintegration energy or to reach the maximum ratio of immediate drilling rate and specific disintegration energy. For the determination of the optimal thrust and revolutions it is needed to monitor the disintegration process. Monitoring of the disintegration process in real conditions is complicated by unfavourable factors, such as the presence of water, dust, vibrations etc. Following our present experience in the monitoring of drilling or full-profile driving, we try to replace the monitoring of input values by monitoring of the scanned acoustic signal. This method of monitoring can extend the optimisation of disintegration process in the technical practice. Its advantage consists in the registration of one acoustic signal by an appropriate microphone. Monitoring of acoustic signal is used also in monitoring of metal machining by milling and turning jobs. The research results of scanning of the acoustic signal in machining of metals are encouraging. Acoustic signal can be processed by different statistical parameters. The paper decribes some results of monitoring of the acoustic signal in rock disintegration on the drilling stand of the Institute of Geotechnics SAS in Košice. The acoustic signal has been registered and processed in no-load run of electric motor, in no-load run of electric motor with a drilling fluid, and in the Ruskov andesite drilling. Registration and processing of the acoustic signal is solved as a part of the research grant task within the basic research

Acoustic communication for Maya Autonomous Underwater Vehicle - performance evaluation of acoustic modem

Digital Repository Service at National Institute of Oceanography (India)

Afzulpurkar, S.; Maurya, P.; Navelkar, G.S.; Desa, E.S.; Mascarenhas, A.A.M.Q.; Dabholkar, N.A.; Madhan, R.; Prabhudesai, S.P.

traffic. This necessitates monitoring the AUV status and data quality through an acoustic link which needs to perform reliably under such conditions, at long range. To address these situations partially, acoustic communication capability is planned...

New liquid chromatographic-chemometric approach for the determination of sunset yellow and tartrazine in commercial preparation.

Science.gov (United States)

Dinç, Erdal; Aktaş, A Hakan; Ustündağ, Ozgür

2005-01-01

A new liquid chromatographic (LC)-chemometric approach was developed for the determination of sunset yellow (SUN) and tartrazine (TAR) in commercial preparations. This approach uses LC and chemometric calibration methods, i.e., classical least-squares (CLS), principal component regression (PCR), and partial-least squares (PLS), simultaneously. The combined LC-chemometric approaches, denoted as LC-CLS, LC-PCR, and LC-PLS, are based on photodiode array (PDA) detection at multiple wavelengths. Optimum chromatographic separation of SUN and TAR with allura red as the internal standard (IS) was obtained by using a Waters Symmetry C18 column, 5 microm, 4.6 x 250 mm, and 0.2 M acetate buffer (pH 5)-acetonitrile-methano-bidistilled water (55 + 20 + 15 + 10, v/v) as the mobile phase at a flow rate of 1.9 mL/min. The LC data sets consisting of the ratios of analyte peak areas to the IS peak area were obtained by using PDA detection at 5 wavelengths (465, 470, 475, 480, and 485 nm). LC-chemometric calibrations for SUN and TAR were separately constructed by using the relationship between the peak-area ratio and the training sets for each colorant. LC-chemometric approaches were tested for different synthetic mixtures containing SUN and TAR in the presence of the IS. These LC-chemometric calibrations were applied to a commercial preparation of the 2 colorants. The experimental results of the LC-chemometric approaches were compared with those obtained by a developed classical LC method using single-wavelength detection.

Flexible surface acoustic wave respiration sensor for monitoring obstructive sleep apnea syndrome

Science.gov (United States)

Jin, Hao; Tao, Xiang; Dong, Shurong; Qin, Yiheng; Yu, Liyang; Luo, Jikui; Deen, M. Jamal

2017-11-01

Obstructive sleep apnea syndrome (OSAS) has received much attention in recent years due to its significant harm to human health and high morbidity rate. A respiration monitoring system is needed to detect OSAS, so that the patient can receive treatment in a timely manner. Wired and wireless OSAS monitoring systems have been developed, but they require a wire connection and batteries to operate, and they are bulky, heavy and not user-friendly. In this paper, we propose the use of a flexible surface acoustic wave (SAW) microsensor to detect and monitor OSAS by measuring the humidity change associated with the respiration of a person. SAW sensors on rigid 128° YX LiNbO3 substrate are also characterized for this application. Results show both types of SAW sensors are suitable for OSAS monitoring with good sensitivity, repeatability and reliability, and the response time and recovery time for the flexible SAW sensors are 1.125 and 0.75 s, respectively. Our work demonstrates the potential for an innovative flexible microsensor for the detection and monitoring of OSAS.

An explorative chemometric approach applied to hyperspectral images for the study of illuminated manuscripts

Science.gov (United States)

Catelli, Emilio; Randeberg, Lise Lyngsnes; Alsberg, Bjørn Kåre; Gebremariam, Kidane Fanta; Bracci, Silvano

2017-04-01

Hyperspectral imaging (HSI) is a fast non-invasive imaging technology recently applied in the field of art conservation. With the help of chemometrics, important information about the spectral properties and spatial distribution of pigments can be extracted from HSI data. With the intent of expanding the applications of chemometrics to the interpretation of hyperspectral images of historical documents, and, at the same time, to study the colorants and their spatial distribution on ancient illuminated manuscripts, an explorative chemometric approach is here presented. The method makes use of chemometric tools for spectral de-noising (minimum noise fraction (MNF)) and image analysis (multivariate image analysis (MIA) and iterative key set factor analysis (IKSFA)/spectral angle mapper (SAM)) which have given an efficient separation, classification and mapping of colorants from visible-near-infrared (VNIR) hyperspectral images of an ancient illuminated fragment. The identification of colorants was achieved by extracting and interpreting the VNIR spectra as well as by using a portable X-ray fluorescence (XRF) spectrometer.

Monitoring of the threshing process quality by using advanced vibro-acoustic indicators

OpenAIRE

Fiorati, Stefano

2011-01-01

This PhD thesis concerns the vibro-acoustic monitoring of the threshing process in an axial flow harvesting machine. This research is a step towards the development of online control systems finalized to maximize the process efficiency and the product quality. By using different signal processing tools it is possible to analyse the link between sound/vibration and material distribution in the threshing unit. In more details, the threshing process is mainly given by two principa...

Chemometrics-based process analytical technology (PAT) tools: applications and adaptation in pharmaceutical and biopharmaceutical industries.

Science.gov (United States)

Challa, Shruthi; Potumarthi, Ravichandra

2013-01-01

Process analytical technology (PAT) is used to monitor and control critical process parameters in raw materials and in-process products to maintain the critical quality attributes and build quality into the product. Process analytical technology can be successfully implemented in pharmaceutical and biopharmaceutical industries not only to impart quality into the products but also to prevent out-of-specifications and improve the productivity. PAT implementation eliminates the drawbacks of traditional methods which involves excessive sampling and facilitates rapid testing through direct sampling without any destruction of sample. However, to successfully adapt PAT tools into pharmaceutical and biopharmaceutical environment, thorough understanding of the process is needed along with mathematical and statistical tools to analyze large multidimensional spectral data generated by PAT tools. Chemometrics is a chemical discipline which incorporates both statistical and mathematical methods to obtain and analyze relevant information from PAT spectral tools. Applications of commonly used PAT tools in combination with appropriate chemometric method along with their advantages and working principle are discussed. Finally, systematic application of PAT tools in biopharmaceutical environment to control critical process parameters for achieving product quality is diagrammatically represented.

[Application of chemometrics in composition-activity relationship research of traditional Chinese medicine].

Science.gov (United States)

Han, Sheng-Nan

2014-07-01

Chemometrics is a new branch of chemistry which is widely applied to various fields of analytical chemistry. Chemometrics can use theories and methods of mathematics, statistics, computer science and other related disciplines to optimize the chemical measurement process and maximize access to acquire chemical information and other information on material systems by analyzing chemical measurement data. In recent years, traditional Chinese medicine has attracted widespread attention. In the research of traditional Chinese medicine, it has been a key problem that how to interpret the relationship between various chemical components and its efficacy, which seriously restricts the modernization of Chinese medicine. As chemometrics brings the multivariate analysis methods into the chemical research, it has been applied as an effective research tool in the composition-activity relationship research of Chinese medicine. This article reviews the applications of chemometrics methods in the composition-activity relationship research in recent years. The applications of multivariate statistical analysis methods (such as regression analysis, correlation analysis, principal component analysis, etc. ) and artificial neural network (such as back propagation artificial neural network, radical basis function neural network, support vector machine, etc. ) are summarized, including the brief fundamental principles, the research contents and the advantages and disadvantages. Finally, the existing main problems and prospects of its future researches are proposed.

Big (Bio)Chemical Data Mining Using Chemometric Methods: A Need for Chemists.

Science.gov (United States)

Tauler, Roma; Parastar, Hadi

2018-03-23

This review aims to demonstrate abilities to analyze Big (Bio)Chemical Data (BBCD) with multivariate chemometric methods and to show some of the more important challenges of modern analytical researches. In this review, the capabilities and versatility of chemometric methods will be discussed in light of the BBCD challenges that are being encountered in chromatographic, spectroscopic and hyperspectral imaging measurements, with an emphasis on their application to omics sciences. In addition, insights and perspectives on how to address the analysis of BBCD are provided along with a discussion of the procedures necessary to obtain more reliable qualitative and quantitative results. In this review, the importance of Big Data and of their relevance to (bio)chemistry are first discussed. Then, analytical tools which can produce BBCD are presented as well as some basics needed to understand prospects and limitations of chemometric techniques when they are applied to BBCD are given. Finally, the significance of the combination of chemometric approaches with BBCD analysis in different chemical disciplines is highlighted with some examples. In this paper, we have tried to cover some of the applications of big data analysis in the (bio)chemistry field. However, this coverage is not extensive covering everything done in the field. © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Acoustic techniques in nuclear safeguards

International Nuclear Information System (INIS)

Olinger, C.T.; Sinha, D.N.

1995-01-01

Acoustic techniques can be employed to address many questions relevant to current nuclear technology needs. These include establishing and monitoring intrinsic tags and seals, locating holdup in areas where conventional radiation-based measurements have limited capability, process monitoring, monitoring containers for corrosion or changes in pressure, and facility design verification. These acoustics applications are in their infancy with respect to safeguards and nuclear material management, but proof-of-principle has been demonstrated in many of the areas listed

Acoustic emission-based in-process monitoring of surface generation in robot-assisted polishing

DEFF Research Database (Denmark)

Pilny, Lukas; Bissacco, Giuliano; De Chiffre, Leonardo

2016-01-01

The applicability of acoustic emission (AE) measurements for in-process monitoring of surface generation in the robot-assisted polishing (RAP) was investigated. Surface roughness measurements require interruption of the process, proper surface cleaning and measurements that sometimes necessitate...... automatic detection of optimal process endpoint allow intelligent process control, creating fundamental elements in development of robust fully automated RAP process for its widespread industrial application....... removal of the part from the machine tool. In this study, stabilisation of surface roughness during polishing rotational symmetric surfaces by the RAP process was monitored by AE measurements. An AE sensor was placed on a polishing arm in direct contact with a bonded abrasive polishing tool...

Combined passive acoustic mapping and magnetic resonance thermometry for monitoring phase-shift nanoemulsion enhanced focused ultrasound therapy

Science.gov (United States)

Crake, Calum; Meral, F. Can; Burgess, Mark T.; Papademetriou, Iason T.; McDannold, Nathan J.; Porter, Tyrone M.

2017-08-01

Focused ultrasound (FUS) has the potential to enable precise, image-guided noninvasive surgery for the treatment of cancer in which tumors are identified and destroyed in a single integrated procedure. However, success of the method in highly vascular organs has been limited due to heat losses to perfusion, requiring development of techniques to locally enhance energy absorption and heating. In addition, FUS procedures are conventionally monitored using MRI, which provides excellent anatomical images and can map temperature, but is not capable of capturing the full gamut of available data such as the acoustic emissions generated during this inherently acoustically-driven procedure. Here, we employed phase-shift nanoemulsions (PSNE) embedded in tissue phantoms to promote cavitation and hence temperature rise induced by FUS. In addition, we incorporated passive acoustic mapping (PAM) alongside simultaneous MR thermometry in order to visualize both acoustic emissions and temperature rise, within the bore of a full scale clinical MRI scanner. Focal cavitation of PSNE could be resolved using PAM and resulted in accelerated heating and increased the maximum elevated temperature measured via MR thermometry compared to experiments without nanoemulsions. Over time, the simultaneously acquired acoustic and temperature maps show translation of the focus of activity towards the FUS transducer, and the magnitude of the increase in cavitation and focal shift both increased with nanoemulsion concentration. PAM results were well correlated with MRI thermometry and demonstrated greater sensitivity, with the ability to detect cavitation before enhanced heating was observed. The results suggest that PSNE could be beneficial for enhancement of thermal focused ultrasound therapies and that PAM could be a critical tool for monitoring this process.

A novel exploratory chemometric approach to environmental monitorring by combining block clustering with Partial Least Square (PLS) analysis

Science.gov (United States)

2013-01-01

Background Given the serious threats posed to terrestrial ecosystems by industrial contamination, environmental monitoring is a standard procedure used for assessing the current status of an environment or trends in environmental parameters. Measurement of metal concentrations at different trophic levels followed by their statistical analysis using exploratory multivariate methods can provide meaningful information on the status of environmental quality. In this context, the present paper proposes a novel chemometric approach to standard statistical methods by combining the Block clustering with Partial least square (PLS) analysis to investigate the accumulation patterns of metals in anthropized terrestrial ecosystems. The present study focused on copper, zinc, manganese, iron, cobalt, cadmium, nickel, and lead transfer along a soil-plant-snai food chain, and the hepatopancreas of the Roman snail (Helix pomatia) was used as a biological end-point of metal accumulation. Results Block clustering deliniates between the areas exposed to industrial and vehicular contamination. The toxic metals have similar distributions in the nettle leaves and snail hepatopancreas. PLS analysis showed that (1) zinc and copper concentrations at the lower trophic levels are the most important latent factors that contribute to metal accumulation in land snails; (2) cadmium and lead are the main determinants of pollution pattern in areas exposed to industrial contamination; (3) at the sites located near roads lead is the most threatfull metal for terrestrial ecosystems. Conclusion There were three major benefits by applying block clustering with PLS for processing the obtained data: firstly, it helped in grouping sites depending on the type of contamination. Secondly, it was valuable for identifying the latent factors that contribute the most to metal accumulation in land snails. Finally, it optimized the number and type of data that are best for monitoring the status of metallic

A novel exploratory chemometric approach to environmental monitorring by combining block clustering with Partial Least Square (PLS) analysis.

Science.gov (United States)

Nica, Dragos V; Bordean, Despina Maria; Pet, Ioan; Pet, Elena; Alda, Simion; Gergen, Iosif

2013-08-30

Given the serious threats posed to terrestrial ecosystems by industrial contamination, environmental monitoring is a standard procedure used for assessing the current status of an environment or trends in environmental parameters. Measurement of metal concentrations at different trophic levels followed by their statistical analysis using exploratory multivariate methods can provide meaningful information on the status of environmental quality. In this context, the present paper proposes a novel chemometric approach to standard statistical methods by combining the Block clustering with Partial least square (PLS) analysis to investigate the accumulation patterns of metals in anthropized terrestrial ecosystems. The present study focused on copper, zinc, manganese, iron, cobalt, cadmium, nickel, and lead transfer along a soil-plant-snai food chain, and the hepatopancreas of the Roman snail (Helix pomatia) was used as a biological end-point of metal accumulation. Block clustering deliniates between the areas exposed to industrial and vehicular contamination. The toxic metals have similar distributions in the nettle leaves and snail hepatopancreas. PLS analysis showed that (1) zinc and copper concentrations at the lower trophic levels are the most important latent factors that contribute to metal accumulation in land snails; (2) cadmium and lead are the main determinants of pollution pattern in areas exposed to industrial contamination; (3) at the sites located near roads lead is the most threatfull metal for terrestrial ecosystems. There were three major benefits by applying block clustering with PLS for processing the obtained data: firstly, it helped in grouping sites depending on the type of contamination. Secondly, it was valuable for identifying the latent factors that contribute the most to metal accumulation in land snails. Finally, it optimized the number and type of data that are best for monitoring the status of metallic contamination in terrestrial ecosystems

Rapid monitoring of the spoilage of minced beef stored under conventionally and active packaging conditions using Fourier transform infrared spectroscopy in tandem with chemometrics.

Science.gov (United States)

Ammor, Mohammed Salim; Argyri, Anthoula; Nychas, George-John E

2009-03-01

Fourier transform infrared (FTIR) spectroscopy was exploited to measure biochemical changes within fresh minced beef in an attempt to rapidly monitor beef spoilage. Minced beef packaged either aerobically, under modified atmosphere and using an active packaging were held from freshness to spoilage at 0, 5, 10, and 15°C. Frequent FTIR measurements were collected directly from the sample surface using attenuated total reflectance, in parallel the total viable counts of bacteria, the sensory quality and the pH were also determined. Principal components analysis allowed illuminating the wavenumbers potentially correlated with the spoilage process. Qualitative interpretation of spectral data was carried out using discriminant factorial analysis and used to corroborate sensory data and to accurately determine samples freshness and packaging. Partial least-squares regressions permitted estimates of bacterial loads and pH values from the spectral data with a fit of R(2)=0.80 for total viable counts and fit of R(2)=0.92 for the pH. Obtained results demonstrated that a FTIR spectrum may be considered as a metabolic fingerprint and that the method in tandem with chemometrics represents a powerful, rapid, economical and non-invasive method for monitoring minced beef freshness regardless the storage conditions (e.g. packaging and temperature).

Development of an acoustic measurement protocol to monitor acetabular implant fixation in cementless total hip Arthroplasty: A preliminary study.

Science.gov (United States)

Goossens, Quentin; Leuridan, Steven; Henyš, Petr; Roosen, Jorg; Pastrav, Leonard; Mulier, Michiel; Desmet, Wim; Denis, Kathleen; Vander Sloten, Jos

2017-11-01

In cementless total hip arthroplasty (THA), the initial stability is obtained by press-fitting the implant in the bone to allow osseointegration for a long term secondary stability. However, finding the insertion endpoint that corresponds to a proper initial stability is currently based on the tactile and auditory experiences of the orthopedic surgeon, which can be challenging. This study presents a novel real-time method based on acoustic signals to monitor the acetabular implant fixation in cementless total hip arthroplasty. Twelve acoustic in vitro experiments were performed on three types of bone models; a simple bone block model, an artificial pelvic model and a cadaveric model. A custom made beam was screwed onto the implant which functioned as a sound enhancer and insertor. At each insertion step an acoustic measurement was performed. A significant acoustic resonance frequency shift was observed during the insertion process for the different bone models; 250 Hz (35%, second bending mode) to 180 Hz (13%, fourth bending mode) for the artificial bone block models and 120 Hz (11%, eighth bending mode) for the artificial pelvis model. No significant frequency shift was observed during the cadaveric experiment due to a lack of implant fixation in this model. This novel diagnostic method shows the potential of using acoustic signals to monitor the implant seating during insertion. Copyright © 2017 IPEM. Published by Elsevier Ltd. All rights reserved.

Structural Health Monitoring of Wind Turbine Blades: Acoustic Source Localization Using Wireless Sensor Networks

Directory of Open Access Journals (Sweden)

Omar Mabrok Bouzid

2015-01-01

Full Text Available Structural health monitoring (SHM is important for reducing the maintenance and operation cost of safety-critical components and systems in offshore wind turbines. This paper proposes an in situ wireless SHM system based on an acoustic emission (AE technique. By using this technique a number of challenges are introduced due to high sampling rate requirements, limitations in the communication bandwidth, memory space, and power resources. To overcome these challenges, this paper focused on two elements: (1 the use of an in situ wireless SHM technique in conjunction with the utilization of low sampling rates; (2 localization of acoustic sources which could emulate impact damage or audible cracks caused by different objects, such as tools, bird strikes, or strong hail, all of which represent abrupt AE events and could affect the structural health of a monitored wind turbine blade. The localization process is performed using features extracted from aliased AE signals based on a developed constraint localization model. To validate the performance of these elements, the proposed system was tested by testing the localization of the emulated AE sources acquired in the field.

Use of large-scale acoustic monitoring to assess anthropogenic pressures on Orthoptera communities.

Science.gov (United States)

Penone, Caterina; Le Viol, Isabelle; Pellissier, Vincent; Julien, Jean-François; Bas, Yves; Kerbiriou, Christian

2013-10-01

Biodiversity monitoring at large spatial and temporal scales is greatly needed in the context of global changes. Although insects are a species-rich group and are important for ecosystem functioning, they have been largely neglected in conservation studies and policies, mainly due to technical and methodological constraints. Sound detection, a nondestructive method, is easily applied within a citizen-science framework and could be an interesting solution for insect monitoring. However, it has not yet been tested at a large scale. We assessed the value of a citizen-science program in which Orthoptera species (Tettigoniidae) were monitored acoustically along roads. We used Bayesian model-averaging analyses to test whether we could detect widely known patterns of anthropogenic effects on insects, such as the negative effects of urbanization or intensive agriculture on Orthoptera populations and communities. We also examined site-abundance correlations between years and estimated the biases in species detection to evaluate and improve the protocol. Urbanization and intensive agricultural landscapes negatively affected Orthoptera species richness, diversity, and abundance. This finding is consistent with results of previous studies of Orthoptera, vertebrates, carabids, and butterflies. The average mass of communities decreased as urbanization increased. The dispersal ability of communities increased as the percentage of agricultural land and, to a lesser extent, urban area increased. Despite changes in abundances over time, we found significant correlations between yearly abundances. We identified biases linked to the protocol (e.g., car speed or temperature) that can be accounted for ease in analyses. We argue that acoustic monitoring of Orthoptera along roads offers several advantages for assessing Orthoptera biodiversity at large spatial and temporal extents, particularly in a citizen science framework. © 2013 Society for Conservation Biology.

Application of chemometric techniques to classify the quality of surface water in the watershed of the river Bermudez in Heredia, Costa Rica

International Nuclear Information System (INIS)

Herrera Murillo, Jorge; Rodriguez Roman, Susana; Solis Torres, Ligia Dina; Castro Delgado, Francisco

2009-01-01

The application of selected chemometric techniques have been investigated: cluster analysis, principal component analysis and factor analysis, to classify the quality of rivers water and evaluate pollution data. Fourteen physicochemical parameters were monitored at 10 stations located in the watershed of the river Bermudez, from August 2005 to February 2007. The results have identified the existence of two natural clusters of monitoring sites with similar characteristics of contamination and identify the DQO, DBO, NO 3 - , SO 4 -2 and SST, as the main variables that discriminate between sampling sites. (author) [es

Acoustic monitoring indicates a correlation between calling and spawning in captive spotted seatrout (Cynoscion nebulosus

Directory of Open Access Journals (Sweden)

Eric W. Montie

2017-02-01

Full Text Available Background Fish sound production is widespread throughout many families. Territorial displays and courtship are the most common reasons for fish sound production. Yet, there is still some questions on how acoustic signaling and reproduction are correlated in many sound-producing species. In the present study, our aim was to determine if a quantitative relationship exists between calling and egg deposition in captive spotted seatrout (Cynoscion nebulosus. This type of data is essential if passive acoustics is to be used to identify spawning aggregations over large spatial scales and monitor reproductive activity over annual and decadal timeframes. Methods Acoustic recorders (i.e., DSG-Oceans were placed in three laboratory tanks to record underwater sound over an entire, simulated reproductive season. We enumerated the number of calls, calculated the received sound pressure level, and counted the number of eggs every morning in each tank. Results Spotted seatrout produced three distinct call types characterized as “drums,” “grunts,” and “staccatos.” Spotted seatrout calling increased as the light cycle shifted from 13.5 to 14.5 h of light, and the temperature increased to 27.7 °C. Calling decreased once the temperature fell below 27.7 °C, and the light cycle shifted to 12 h of light. These temperature and light patterns followed the natural reproductive season observed in wild spotted seatrout in the Southeast United States. Spotted seatrout exhibited daily rhythms in calling. Acoustic signaling began once the lights turned off, and calling reached maximum activity approximately 3 h later. Eggs were released only on evenings in which spotted seatrout were calling. In all tanks, spotted seatrout were more likely to spawn when male fish called more frequently. A positive relationship between SPL and the number of eggs collected was found in Tanks 1 and 3. Discussion Our findings indicate that acoustic metrics can predict spawning

Principal Component Analysis: Most Favourite Tool in Chemometrics

Indian Academy of Sciences (India)

Abstract. Principal component analysis (PCA) is the most commonlyused chemometric technique. It is an unsupervised patternrecognition technique. PCA has found applications in chemistry,biology, medicine and economics. The present work attemptsto understand how PCA work and how can we interpretits results.

Acoustic Emission Based In-process Monitoring in Robot Assisted Polishing

DEFF Research Database (Denmark)

Pilny, Lukas; Bissacco, Giuliano; De Chiffre, Leonardo

The applicability of acoustic emission (AE) measurements for in-process monitoring in the Robot Assisted Polishing (RAP) process was investigated. Surface roughness measurements require interruption of the process, proper surface cleaning and measurements that sometimes necessitate removal...... improving the efficiency of the process. It also allows for intelligent process control and generally enhances the robustness and reliability of the automated RAP system in industrial applications....... of the part from the machine tool. In this study, development of surface roughness during polishing rotational symmetric surfaces by the RAP process was inferred from AE measurements. An AE sensor was placed on a polishing tool, and a cylindrical rod of Vanadis 4E steel having an initial turned surface...

Preliminary studies for monitoring erosion in pipelines by the acoustic emission technique

Energy Technology Data Exchange (ETDEWEB)

Tiboni, G.B. [Universidade Tecnologica Federal do Parana (UTFPR), Curitiba, PR (Brazil). Programa de Pos-graduacao em Engenharia Mecanica e de Materiais; Marquardt, T.A.S; SantaMaria, V.A.R.; Silva, C.H. [Universidade Tecnologica Federal do Parana (UTFPR), Curitiba, PR (Brazil)

2009-07-01

The aim of this work is to present some applications of Acoustic Emission (AE), which is a powerful technique for nondestructive testing in Tribology, treated here as tests of friction, wear by contact fatigue, wear by slip and wear by erosion. In this work a special attention is given to solid particle erosion and hydro-abrasive erosion, problems found in almost every pipeline that lead to local loss of material and eventually rupture of the line. The technique of AE can be used as an efficient online tool when, primarily, to monitor tribological aspects such as the rate of wear of materials, as well as detect the spread of flaws in them. In wear by erosion, specifically, the parameters of RMS and acoustic energy are capable of correlation with the type of mechanism for removal of material. As a preliminary goal, erosive tests were performed with gas (air) without erosive particles, monitored by AE, varying the surface of the samples and the internal diameter the nozzle, taking the differences in signs of AE. Correlation between parameters of RMS and amplitude were noticed with the variables of the tests, such as roughness and fluid velocity. The RMS parameter showed a exponential correction with the fluid velocity, however the amplitude signals had a linear behavior. The knowledge of these parameters is essential for the development of a system that is able to quantify the wear rate of a pipeline without taking it out of operation. (author)

Surface Acoustic Wave (SAW Resonators for Monitoring Conditioning Film Formation

Directory of Open Access Journals (Sweden)

Siegfried Hohmann

2015-05-01

Full Text Available We propose surface acoustic wave (SAW resonators as a complementary tool for conditioning film monitoring. Conditioning films are formed by adsorption of inorganic and organic substances on a substrate the moment this substrate comes into contact with a liquid phase. In the case of implant insertion, for instance, initial protein adsorption is required to start wound healing, but it will also trigger immune reactions leading to inflammatory responses. The control of the initial protein adsorption would allow to promote the healing process and to suppress adverse immune reactions. Methods to investigate these adsorption processes are available, but it remains difficult to translate measurement results into actual protein binding events. Biosensor transducers allow user-friendly investigation of protein adsorption on different surfaces. The combination of several transduction principles leads to complementary results, allowing a more comprehensive characterization of the adsorbing layer. We introduce SAW resonators as a novel complementary tool for time-resolved conditioning film monitoring. SAW resonators were coated with polymers. The adsorption of the plasma proteins human serum albumin (HSA and fibrinogen onto the polymer-coated surfaces were monitored. Frequency results were compared with quartz crystal microbalance (QCM sensor measurements, which confirmed the suitability of the SAW resonators for this application.

Acoustic Emission Weld Monitoring in the 2195 Aluminum-Lithium Alloy

Science.gov (United States)

Walker, James L.

2005-01-01

Due to its low density, the 2195 aluminum-lithium alloy was developed as a replacement for alloy 2219 in the Space Shuttle External Tank (ET). The external tank is the single largest component of the space shuttle system. It is 154 feet long and 27.6 feet in diameter, and serves as the structural backbone for the shuttle during launch, absorbing most of the 7 million plus pounds of thrust produced. The almost 4% decrease in density between the two materials provides an extra 7500 pounds of payload capacity necessary to put the International Space Station components into orbit. The ET is an all-welded structure; hence, the requirement is for up to five rewelds without hot cracking. Unfortunately, hot cracking during re-welding or repair operations was occurring and had to be dealt with before the new super lightweight tank could be used. Weld metal porosity formation was also of concern because it leads to hot cracking during weld repairs. Accordingly, acoustic emission (AE) nondestructive testing was employed to monitor the formation of porosity and hot cracks in order to select the best filler metal and optimize the weld schedule. The purpose of this work is to determine the feasibility of detecting hot cracking in welded aluminum-lithium (Al-Li) structures through the analysis of acoustic emission data. By acoustically characterizing the effects of reheating during a repair operation, the potential for hidden flaws coalescing and becoming "unstable" as the panel is repaired could be reduced. Identification of regions where microcrack growth is likely to occur and the location of active flaw growth in the repair weld will provide the welder with direct feedback as to the current weld quality enabling adjustments to the repair process be made in the field. An acoustic emission analysis of the source mechanisms present during welding has been conducted with the goals of locating regions in the weld line that are susceptible to damage from a repair operation

Detection of Genetically Modified Sugarcane by Using Terahertz Spectroscopy and Chemometrics

Science.gov (United States)

Liu, J.; Xie, H.; Zha, B.; Ding, W.; Luo, J.; Hu, C.

2018-03-01

A methodology is proposed to identify genetically modified sugarcane from non-genetically modified sugarcane by using terahertz spectroscopy and chemometrics techniques, including linear discriminant analysis (LDA), support vector machine-discriminant analysis (SVM-DA), and partial least squares-discriminant analysis (PLS-DA). The classification rate of the above mentioned methods is compared, and different types of preprocessing are considered. According to the experimental results, the best option is PLS-DA, with an identification rate of 98%. The results indicated that THz spectroscopy and chemometrics techniques are a powerful tool to identify genetically modified and non-genetically modified sugarcane.

Registration and processing of acoustic signal in rock drilling

Directory of Open Access Journals (Sweden)

Futó Jozef

2002-03-01

Full Text Available For the determination of an effective rock disintegration for a given tool and rock type it is needed to define an optimal disintegration regime. Optimisation of the disintegration process by drilling denotes the finding out an appropriate couple of input parameters of disintegration, i.e. the thrust and revolutions for a quasi-equal rock environment. The disintegration process can be optimised to reach the maximum immediate drilling rate, to reach the minimum specific disintegration energy or to reach the maximum ratio of immediate drilling rate and specific disintegration energy. For the determination of the optimal thrust and revolutions it is needed to monitor the disintegration process. Monitoring of the disintegration process in real conditions is complicated by unfavourable factors, such as the presence of water, dust, vibrations etc. Following our present experience in the monitoring of drilling or full-profile driving, we try to replace the monitoring of input values by monitoring of the scanned acoustic signal. This method of monitoring can extend the optimisation of disintegration process in the technical practice. Its advantage consists in the registration of one acoustic signal by an appropriate microphone. Monitoring of acoustic signal is used also in monitoring of metal machining by milling and turning jobs. The research results of scanning of the acoustic signal in machining of metals are encouraging. Acoustic signal can be processed by different statistical parameters. The paper decribes some results of monitoring of the acoustic signal in rock disintegration on the drilling stand of the Institute of Geotechnics SAS in Košice. The acoustic signal has been registered and processed in no-load run of electric motor, in no-load run of electric motor with a drilling fluid, and in the Ruskov andesite drilling. Registration and processing of the acoustic signal is solved as a part of the research grant task within the basic research

Attempt to separate the fluorescence spectra of adrenaline and noradrenaline using chemometrics

DEFF Research Database (Denmark)

Nikolajsen, Rikke P; Hansen, Åse Marie; Bro, R

2000-01-01

An investigation was conducted on whether the fluorescence spectra of the very similar catecholamines adrenaline and noradrenaline could be separated using chemometric methods. The fluorescence landscapes (several excitation and emission spectra were measured) of two data sets with respectively 16...... regression (Unfold-PLSR) on the larger data set and parallel factor analysis (PARAFAC) of the six samples of the smaller set showed that there was no difference between the fluorescence landscapes of adrenaline and noradrenaline. It can be concluded that chemometric separation of adrenaline and noradrenaline...

Cardiorespiratory system monitoring using a developed acoustic sensor.

Science.gov (United States)

Abbasi-Kesbi, Reza; Valipour, Atefeh; Imani, Khadije

2018-02-01

This Letter proposes a wireless acoustic sensor for monitoring heartbeat and respiration rate based on phonocardiogram (PCG). The developed sensor comprises a processor, a transceiver which operates at industrial, scientific and medical band and the frequency of 2.54 GHz as well as two capacitor microphones which one for recording the heartbeat and another one for respiration rate. To evaluate the precision of the presented sensor in estimating heartbeat and respiration rate, the sensor is tested on the different volunteers and the obtained results are compared with a gold standard as a reference. The results reveal that root-mean-square error are determined sensor estimate sounds of [Formula: see text] to [Formula: see text] obtained PCG signal with sensitivity and specificity 98.1% and 98.3% in turn that make 3% improvement than previous works. The results prove that the sensor can be appropriate candidate for recognising abnormal condition in the cardiorespiratory system.

Distributed acoustic fibre optic sensors for condition monitoring of pipelines

Science.gov (United States)

Hussels, Maria-Teresa; Chruscicki, Sebastian; Habib, Abdelkarim; Krebber, Katerina

2016-05-01

Industrial piping systems are particularly relevant to public safety and the continuous availability of infrastructure. However, condition monitoring systems based on many discrete sensors are generally not well-suited for widespread piping systems due to considerable installation effort, while use of distributed fibre-optic sensors would reduce this effort to a minimum. Specifically distributed acoustic sensing (DAS) is employed for detection of third-party threats and leaks in oil and gas pipelines in recent years and can in principle also be applied to industrial plants. Further possible detection routes amenable by DAS that could identify damage prior to emission of medium are subject of a current project at BAM, which aims at qualifying distributed fibre optic methods such as DAS as a means for spatially continuous monitoring of industrial piping systems. Here, first tests on a short pipe are presented, where optical fibres were applied directly to the surface. An artificial signal was used to define suitable parameters of the measurement system and compare different ways of applying the sensor.

Acoustical monitoring of diesel engines in reverberant environment; Methodes de surveillance acoustique des diesels en milieu reverberant

Energy Technology Data Exchange (ETDEWEB)

Mein, M.

1995-10-01

The feed-back knowledge of emergency diesel generators in nuclear power plants shows that some malfunctions, mainly affecting fuel-injection or distribution system of the engine can be heard and detected by experienced maintenance agents. This study consists in the feasibility,v of acoustical monitoring of those diesel engines, taking into account the reverberant environment of the machine. The operating cycle of the diesel is composed of transient events (injection, combustion, valve closure...) which generate highly non stationary acoustical signals. The detection of a malfunction appearing on such transients requires the use of adapted signal processing techniques. Visual analysis of the phenomena is first proceeded using time-frequency and time-scale representations. The second step will be parametric modeling of acoustical signatures for the extraction of characteristic parameters, in order to characterize the fault and to use an automatic classification system. The lest part of the study will concern the evaluation of the robustness of the detection methods in regard to acoustical reverberation. (author). 10 refs., 6 figs.

Monitoring Industrial Food Processes Using Spectroscopy & Chemometrics

DEFF Research Database (Denmark)

Pedersen, Dorthe Kjær; Engelsen, Søren Balling

2001-01-01

In the last decade rapid spectroscopic measurements have revolutionized quality control in practically all areas of primary food and feed production. Near-infrared spectroscopy (NIR & NIT) has been implemented for monitoring the quality of millions of samples of cereals, milk and meat with unprec......In the last decade rapid spectroscopic measurements have revolutionized quality control in practically all areas of primary food and feed production. Near-infrared spectroscopy (NIR & NIT) has been implemented for monitoring the quality of millions of samples of cereals, milk and meat...

Acoustic emission monitoring of damage in ceramic matrix composites: Effects of weaves and feature

Science.gov (United States)

Ojard, Greg; Mordasky, Matt; Kumar, Rajesh

2018-04-01

Ceramic matrix composites (CMCs) are a class of high temperature materials with better damage tolerance properties compared to monolithic ceramics. The improved toughness is attributed to weak interface coating between the fiber and the matrix that allows for crack deflection and fiber pull-out. Thus, CMCs have gained consideration over monolithic materials for high temperature applications such as in gas turbines. The current standard fiber architecture for CMCs is a harness satin (HS) balanced weave (5HS and 8HS); however, other architectures such as uni-weave materials (tape layup) are now being considered due to fiber placement control and higher fiber volume fraction in the tensile loading direction. Engineering components require additional features in the CMC laminates, such as holes for attachments. Past work has shown that acoustic emission could differentiate the effect of changing interface conditions due to heat treatment effects. The focus of the present work is to investigate the effects of different weaves and the presence of a feature on damage behavior of CMCs as observed via acoustic emission technique. The results of the tensile testing with acoustic emission monitoring will be presented and discussed.

Analysis of acoustic emission signals of fatigue crack growth and corrosion processes. Investigation of the possibilities for continuous condition monitoring of transport containers by acoustic emission testing

International Nuclear Information System (INIS)

Wachsmuth, Janne

2016-01-01

Fatigue crack growth and active corrosion processes are the main causes of structural failures of transport products like road tankers, railway tank cars and ships. To prevent those failures, preventive, time-based maintenance is performed. However, preventive inspections are costly and include the risk of not detecting a defect, which could lead to a failure within the next service period. An alternative is the idea of continuous monitoring of the whole structure by means of acoustic emission testing (AT). With AT, defects within the material shall be detected and repaired directly after their appearance. Acoustic emission testing is an online non-destructive testing method. Acoustic emission (AE) arises from changes within the material and is transported by elastic waves through the material. If the AE event generates enough energy, the elastic wave propagates to the boundaries of the component, produces a displacement in the picometre scale and can be detected by a piezoelectric sensor. The sensor produces an electrical signal. From this AE signal, AE features such as the maximum amplitude or the frequency can be extracted. Methods of signal analysis are used to investigate the time and frequency dependency of signal groups. The purpose of the signal analysis is to connect the AE signal with the originating AE source. If predefined damage mechanisms are identified, referencing the damage condition of the structure is possible. Acoustic emission from events of the actual crack propagation process can for example lead to the crack growth rate or the stress intensity factor, both specific values from fracture mechanics. A new development in the domain of acoustic emission testing is the pattern recognition of AE signals. Specific features are extracted from the AE signals to assign them to their damage mechanisms. In this thesis the AE signals from the damage mechanisms corrosion and fatigue crack growth are compared and analysed. The damage mechanisms were

Real-time temperature estimation and monitoring of HIFU ablation through a combined modeling and passive acoustic mapping approach

International Nuclear Information System (INIS)

Jensen, C R; Cleveland, R O; Coussios, C C

2013-01-01

Passive acoustic mapping (PAM) has been recently demonstrated as a method of monitoring focused ultrasound therapy by reconstructing the emissions created by inertially cavitating bubbles (Jensen et al 2012 Radiology 262 252–61). The published method sums energy emitted by cavitation from the focal region within the tissue and uses a threshold to determine when sufficient energy has been delivered for ablation. The present work builds on this approach to provide a high-intensity focused ultrasound (HIFU) treatment monitoring software that displays both real-time temperature maps and a prediction of the ablated tissue region. This is achieved by determining heat deposition from two sources: (i) acoustic absorption of the primary HIFU beam which is calculated via a nonlinear model, and (ii) absorption of energy from bubble acoustic emissions which is estimated from measurements. The two sources of heat are used as inputs to the bioheat equation that gives an estimate of the temperature of the tissue as well as estimates of tissue ablation. The method has been applied to ex vivo ox liver samples and the estimated temperature is compared to the measured temperature and shows good agreement, capturing the effect of cavitation-enhanced heating on temperature evolution. In conclusion, it is demonstrated that by using PAM and predictions of heating it is possible to produce an evolving estimate of cell death during exposure in order to guide treatment for monitoring ablative HIFU therapy. (paper)

Semi-automatic long-term acoustic surveying

DEFF Research Database (Denmark)

Andreassen, Tórur; Surlykke, Annemarie; Hallam, John

2014-01-01

Increasing concern about decline in biodiversity has created a demand for population surveys. Acoustic monitoring is an efficient non-invasive method, which may be deployed for surveys of animals as diverse as insects, birds, and bats. Long-term unmanned automatic monitoring may provide unique...... to determine bat behavior and correct for the bias toward loud bats inherent in acoustic surveying....

Study of ultrasonic propagation through vortices for acoustic monitoring of high-temperature and turbulent fluid

International Nuclear Information System (INIS)

Massacret, Nicolas; Moysan, Joseph; Ploix, Marie-Aude; Chaouch, Naim; Jeannot, Jean-Philippe

2016-01-01

Ultrasonic monitoring in high temperature fluids with turbulences requires the knowledge of wave propagation in such media and the development of simulation tools. Applications could be the monitoring of sodium-cooled fast reactors. The objectives are mainly acoustic telemetry and thermometry, which involve the propagation of ultrasounds in turbulent and heated sodium flows. We developed a ray-tracing model to simulate the wave propagation and to determine wave deviations and delays due to an inhomogeneous medium. In previous work we demonstrated the sensitivity of ultrasounds to temperature gradients in liquid sodium. To complete that study, we need to investigate the sensitivity of ultrasounds to vortices created in a moving fluid. We designed a specific experimental setup called IKHAR (Instabilities of Kelvin-Helmholtz for Acoustic Research) in order to assess the validity of the ray-tracing model and the potential of ultrasounds for monitoring such fluid. In this experiment, Von Karman instabilities were created in a flow of water. Fluid temperature was homogeneous in our experimental setup. Through a careful choice of the parameters, periodic vortices were generated. The experiment was also simulated using Comsol registered to allow discussion about repeatability. The throughtransmission method was used to measure wave delays due to the vortices. Arrays of transducers were used to measure time of flight variations of several nanoseconds with a high spatial resolution. Results were similar to simulation results. They demonstrate that beam delays due to vortices can be measured and confirm the potential of ultrasounds in monitoring very inhomogeneous fluid media such as liquid sodium used as coolant fluid in nuclear fast reactors.

Use of Acoustic Emission to Monitor Progressive Damage Accumulation in KEVLAR® 49 Composites

Science.gov (United States)

Waller, J. M.; Andrade, E.; Saulsberry, R. L.

2010-02-01

Acoustic emission (AE) data acquired during intermittent load hold tensile testing of epoxy impregnated Kevlar® 49 (K/Ep) composite strands were analyzed to monitor progressive damage during the approach to tensile failure. Insight into the progressive damage of K/Ep strands was gained by monitoring AE event rate and energy. Source location based on energy attenuation and arrival time data was used to discern between significant AE attributable to microstructural damage and spurious AE attributable to noise. One of the significant findings was the observation of increasing violation of the Kaiser effect (Felicity ratio <1.0) with damage accumulation. The efficacy of three different intermittent load hold stress schedules that allowed the Felicity ratio to be determined analytically is discussed.

Rapid detection of Listeria monocytogenes in milk using confocal micro-Raman spectroscopy and chemometric analysis.

Science.gov (United States)

Wang, Junping; Xie, Xinfang; Feng, Jinsong; Chen, Jessica C; Du, Xin-jun; Luo, Jiangzhao; Lu, Xiaonan; Wang, Shuo

2015-07-02

Listeria monocytogenes is a facultatively anaerobic, Gram-positive, rod-shape foodborne bacterium causing invasive infection, listeriosis, in susceptible populations. Rapid and high-throughput detection of this pathogen in dairy products is critical as milk and other dairy products have been implicated as food vehicles in several outbreaks. Here we evaluated confocal micro-Raman spectroscopy (785 nm laser) coupled with chemometric analysis to distinguish six closely related Listeria species, including L. monocytogenes, in both liquid media and milk. Raman spectra of different Listeria species and other bacteria (i.e., Staphylococcus aureus, Salmonella enterica and Escherichia coli) were collected to create two independent databases for detection in media and milk, respectively. Unsupervised chemometric models including principal component analysis and hierarchical cluster analysis were applied to differentiate L. monocytogenes from Listeria and other bacteria. To further evaluate the performance and reliability of unsupervised chemometric analyses, supervised chemometrics were performed, including two discriminant analyses (DA) and soft independent modeling of class analogies (SIMCA). By analyzing Raman spectra via two DA-based chemometric models, average identification accuracies of 97.78% and 98.33% for L. monocytogenes in media, and 95.28% and 96.11% in milk were obtained, respectively. SIMCA analysis also resulted in satisfied average classification accuracies (over 93% in both media and milk). This Raman spectroscopic-based detection of L. monocytogenes in media and milk can be finished within a few hours and requires no extensive sample preparation. Copyright © 2015 Elsevier B.V. All rights reserved.

Acoustic emission monitoring of leakage through seal-plug in PHWR systems

Energy Technology Data Exchange (ETDEWEB)

Jha, S K; Badgujar, B P; Goswami, G L [Bhabha Atomic Research Centre, Bombay (India). Atomic Fuels Div.; Patel, R J; Bhattacharya, S; Agrawal, R G [Bhabha Atomic Research Centre, Mumbai (India). Refuelling Technology Division

1994-12-31

Acoustic Emission (AE) technique is being developed as an in-service inspection tool for monitoring the leakage through seal-plugs in Pressurised Heavy Water Reactors (PHWRs). Time as well as frequency domain analysis have been utilised during the experiment carried out at Bhabha Atomic Research Centre (BARC) using test set up simulating the pressure and temperature conditions. The work involved were to determine the temperature profile on end-fitting, effect of pressure and temperature on leakage etc. This paper discusses various relationships like signal-level vs. pressure, frequency spectrum of signal, signal-level vs. leakage based on the above experimental work. (author). 4 refs., 6 figs.

Controlling Sample Rotation in Acoustic Levitation

Science.gov (United States)

Barmatz, M. B.; Stoneburner, J. D.

1985-01-01

Rotation of acoustically levitated object stopped or controlled according to phase-shift monitoring and control concept. Principle applies to square-cross-section levitation chamber with two perpendicular acoustic drivers operating at same frequency. Phase difference between X and Y acoustic excitation measured at one corner by measuring variation of acoustic amplitude sensed by microphone. Phase of driver adjusted to value that produces no rotation or controlled rotation of levitated object.

A portable Raman acoustic levitation spectroscopic system for the identification and environmental monitoring of algal cells.

Science.gov (United States)

Wood, Bayden R; Heraud, Philip; Stojkovic, Slobodanka; Morrison, Danielle; Beardall, John; McNaughton, Don

2005-08-01

We report the coupling of a portable Raman spectrometer to an acoustic levitation device to enable environmental monitoring and the potential taxonomic identification of microalgae. Spectra of living cells were recorded at 785 nm using a fiber-optic probe coupled to a portable Raman spectrometer. The spectra exhibit an excellent signal-to-noise ratio and clearly show bands from chlorophyll a and beta-carotene. Spectra of levitated photobleached microalgae clearly show a reduction in chlorophyll a concentration relative to beta-carotene after 10 min of exposure to a quartz halogen lamp. Spectra recorded from levitated nitrogen-limited cells also show a significant reduction in bands associated with chlorophyll a, as compared to nitrogen-replete cells. To investigate the diagnostic capability of the technique, four species of microalgae were analyzed. Good quality spectra of all four species were obtained showing varying ratios of beta-carotene to chlorophyll. The combination of an acoustic levitation device and a portable Raman spectrometer shows potential as a taxonomic and environmental monitoring tool with direct application to field studies in remote environments.

Wireless microwave acoustic sensor system for condition monitoring in power plant environments

Energy Technology Data Exchange (ETDEWEB)

Pereira da Cunha, Mauricio [Univ. of Maine, Orno, ME (United States)

2017-03-30

This project successfully demonstrated novel wireless microwave acoustic temperature and pressure sensors that can be embedded into equipment and structures located in fossil fuel power plant environments to monitor the condition of components such as steam headers, re-heat lines, water walls, burner tubes, and power turbines. The wireless microwave acoustic sensor technology researched and developed through a collaborative partnership between the University of Maine and Environetix Technologies Corporation can provide a revolutionary impact in the power industry since it is anticipated that the wireless sensors will deliver reliable real-time sensing information in harsh power plant conditions that involve temperatures up to 1100oC and pressures up to 750 psi. The work involved the research and development of novel high temperature harsh environment thin film electrodes, piezoelectric smart microwave acoustic sensing elements, sensor encapsulation materials that were engineered to function over long times up to 1100oC, and a radio-frequency (RF) wireless interrogation electronics unit that are located both inside and outside the high temperature harsh environment. The UMaine / Environetix team have interacted with diverse power plant facilities, and identified as a testbed a local power generation facility, which burns municipal solid waste (MSW), the Penobscot Energy Recovery Company (PERC), Orrington, Maine. In this facility Environetix / UMaine successfully implemented and tested multiple wireless temperature sensor systems within the harsh-environment of the economizer chamber and at the boiler tubes, transferring the developed technology to the power plant environment to perform real-time sensor monitoring experiments under typical operating conditions, as initially targeted in the project. The wireless microwave acoustic sensor technology developed under this project for power plant applications offers several significant advantages including wireless

Acoustic Ecology and Remote Acoustic Monitoring of a Minke Whale Population

National Research Council Canada - National Science Library

Gedamke, Jason

2000-01-01

Sound is the most effective means of communication in the ocean. A uniquely inquisitive minke whale population on the northern Great Barrier Reef presents an unprecedented research opportunity to study minke acoustics...

Classification of java tea ( Orthosiphon aristatus ) quality using FTIR spectroscopy and chemometrics

International Nuclear Information System (INIS)

Heryanto, R; Pradono, D I; Darusman, L K; Marlina, E

2017-01-01

Java tea ( Orthosiphon aristatus ) is a plant that widely used as a medicinal herb in Indonesia. Its quality is varying depends on various factors, such as cultivating area, climate and harvesting time. This study aimed to investigate the effectiveness of FTIR spectroscopy coupled with chemometrics for discriminating the quality of java tea from different cultivating area. FTIR spectra of ethanolic extracts were collected from five different regions of origin of java tea. Prior to chemometrics evaluation, spectra were pre-processed by using baselining, normalization and derivatization. Principal Components Analysis (PCA) was used to reduce the spectra to two PCs, which explained 73% of the total variance. Score plot of two PCs showed groupings of the samples according to their regions of origin. Furthermore, Partial Least Squares-Discriminant Analysis (PLSDA) was applied to the pre-processed data. The approach produced an external validation success rate of 100%. This study shows that FTIR analysis and chemometrics has discriminatory power to classify java tea based on its quality related to the region of origin. (paper)

Monitoring Anthropogenic Ocean Sound from Shipping Using an Acoustic Sensor Network and a Compressive Sensing Approach †

Science.gov (United States)

Harris, Peter; Philip, Rachel; Robinson, Stephen; Wang, Lian

2016-01-01

Monitoring ocean acoustic noise has been the subject of considerable recent study, motivated by the desire to assess the impact of anthropogenic noise on marine life. A combination of measuring ocean sound using an acoustic sensor network and modelling sources of sound and sound propagation has been proposed as an approach to estimating the acoustic noise map within a region of interest. However, strategies for developing a monitoring network are not well established. In this paper, considerations for designing a network are investigated using a simulated scenario based on the measurement of sound from ships in a shipping lane. Using models for the sources of the sound and for sound propagation, a noise map is calculated and measurements of the noise map by a sensor network within the region of interest are simulated. A compressive sensing algorithm, which exploits the sparsity of the representation of the noise map in terms of the sources, is used to estimate the locations and levels of the sources and thence the entire noise map within the region of interest. It is shown that although the spatial resolution to which the sound sources can be identified is generally limited, estimates of aggregated measures of the noise map can be obtained that are more reliable compared with those provided by other approaches. PMID:27011187

Discrimination of sugarcane according to cultivar by 1H NMR and chemometric analyses

Energy Technology Data Exchange (ETDEWEB)

Alves Filho, Elenilson G.; Silva, Lorena M.A.; Choze, Rafael; Liao, Luciano M. [Laboratorio de Ressonancia Magnetica Nuclear, Instituto de Quimica, Universidade Federal de Goias (UFG), Goiania, GO (Brazil); Honda, Neli K.; Alcantara, Glaucia B. [Departamento de Quimica, Universidade Federal de Mato Grosso do Sul (UFMS), Campo Grande, MS (Brazil)

2012-07-01

Several technologies for the development of new sugarcane cultivars have mainly focused on the increase in productivity and greater disease resistance. Sugarcane cultivars are usually identified by the organography of the leaves and stems, the analysis of peroxidase and esterase isoenzyme activities and the total soluble protein as well as soluble solid content. Nuclear magnetic resonance (NMR) associated with chemometric analysis has proven to be a valuable tool for cultivar assessment. Thus, this article describes the potential of chemometric analysis applied to 1H high resolution magic angle spinning (HRMAS) and NMR in solution for the investigation of sugarcane cultivars. For this purpose, leaves from eight different cultivars of sugarcane were investigated by {sup 1}H NMR spectroscopy in combination with chemometric analysis. The approach shows to be a useful tool for the distinction and classification of different sugarcane cultivars as well as to access the differences on its chemical composition. (author)

Application of an Integrated and Self-contained Electromagnetic Acoustic Recorder for Monitoring the Rock Mass Structure and Development of Geodynamic Processes in Ore Mines

Directory of Open Access Journals (Sweden)

Bespal’ko Anatoly

2016-01-01

Full Text Available The paper presents a block diagram of the recorder of electromagnetic and acoustic signals. The recorder provides monitoring of electromagnetic and acoustic signals under changing stress-strain state of heterogeneous materials and rocks. The analog amplifier input sensitivity of electromagnetic signals in 4 channels is 10 μV, that of the electromagnetic signal intensity is 10 μ and that of acoustic signals is 50 μV. The operating frequency range of recording is (1÷100 kHz. The averaging of electromagnetic and acoustic signal amplitudes is performed within 1 or 5 seconds. The data on electromagnetic and acoustic emission materials is recorded in digital format in the internal memory of the recorder. The recorder operates off-line within 7 days. Repeated testing of the recorder in natural conditions of the Tashtagol mine showed that the changes in the amplitude and frequency parameters of electromagnetic signals (EMC indicate the structural damage in mines made of rocks which differ in their electrical properties. Measurements of the intensity of electromagnetic signals enable monitoring the changes in the stress-strain state of rocks during and after blasting and other geodynamic phenomena.

Transition section for acoustic waveguides

International Nuclear Information System (INIS)

Karplus, H.H.B.

1975-01-01

A means of facilitating the transmission of acoustic waves with minimal reflection between two regions having different specific acoustic impedances is described comprising a region exhibiting a constant product of cross-sectional area and specific acoustic impedance at each cross-sectional plane along the axis of the transition region. A variety of structures that exhibit this feature is disclosed, the preferred embodiment comprising a nested structure of doubly reentrant cones. This structure is useful for monitoring the operation of nuclear reactors in which random acoustic signals are generated in the course of operation

Monitoring of temperature fatigue failure mechanism for polyvinyl alcohol fiber concrete using acoustic emission sensors.

Science.gov (United States)

Li, Dongsheng; Cao, Hai

2012-01-01

The applicability of acoustic emission (AE) techniques to monitor the mechanism of evolution of polyvinyl alcohol (PVA) fiber concrete damage under temperature fatigue loading is investigated. Using the temperature fatigue test, real-time AE monitoring data of PVA fiber concrete is achieved. Based on the AE signal characteristics of the whole test process and comparison of AE signals of PVA fiber concretes with different fiber contents, the damage evolution process of PVA fiber concrete is analyzed. Finally, a qualitative evaluation of the damage degree is obtained using the kurtosis index and b-value of AE characteristic parameters. The results obtained using both methods are discussed.

An Efficient Audio Coding Scheme for Quantitative and Qualitative Large Scale Acoustic Monitoring Using the Sensor Grid Approach

Directory of Open Access Journals (Sweden)

Félix Gontier

2017-11-01

Full Text Available The spreading of urban areas and the growth of human population worldwide raise societal and environmental concerns. To better address these concerns, the monitoring of the acoustic environment in urban as well as rural or wilderness areas is an important matter. Building on the recent development of low cost hardware acoustic sensors, we propose in this paper to consider a sensor grid approach to tackle this issue. In this kind of approach, the crucial question is the nature of the data that are transmitted from the sensors to the processing and archival servers. To this end, we propose an efficient audio coding scheme based on third octave band spectral representation that allows: (1 the estimation of standard acoustic indicators; and (2 the recognition of acoustic events at state-of-the-art performance rate. The former is useful to provide quantitative information about the acoustic environment, while the latter is useful to gather qualitative information and build perceptually motivated indicators using for example the emergence of a given sound source. The coding scheme is also demonstrated to transmit spectrally encoded data that, reverted to the time domain using state-of-the-art techniques, are not intelligible, thus protecting the privacy of citizens.

Evaluating Acoustic Emission Signals as an in situ process monitoring technique for Selective Laser Melting (SLM)

Energy Technology Data Exchange (ETDEWEB)

Fisher, Karl A. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Candy, Jim V. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Guss, Gabe [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Mathews, M. J. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

2016-10-14

In situ real-time monitoring of the Selective Laser Melting (SLM) process has significant implications for the AM community. The ability to adjust the SLM process parameters during a build (in real-time) can save time, money and eliminate expensive material waste. Having a feedback loop in the process would allow the system to potentially ‘fix’ problem regions before a next powder layer is added. In this study we have investigated acoustic emission (AE) phenomena generated during the SLM process, and evaluated the results in terms of a single process parameter, of an in situ process monitoring technique.

Method and apparatus for generating acoustic waves

International Nuclear Information System (INIS)

Rao, G.V.; Gopal, R.

1982-01-01

A portable source of acoustic waves comprises a sample of iron-nickel alloy including an austenite phase cooled to become martensite, and a wave guide to transmit the acoustic waves. The source is applied to the pressure boundary region of a pressurized water reactor to simulate an actual metal flaw and test the calibration of the monitoring and surveillance system. With at most 29.7% nickel in the sample, the source provides acoustic emission due to ductile deformation, and with at least 30% nickel the acoustic emission is characteristic of a brittle deformation. Thus, the monitoring and surveillance system can be tested in either or both situations. In the prior art, synthetic waveform signals were used for such calibration but found not suitable for on-line simulation of the surveillance system. This invention provides an improved system in that it generates true acoustic signals. (author)

Acoustic emission monitoring of medieval towers considered as sensitive earthquake receptors

Directory of Open Access Journals (Sweden)

A. Carpinteri

2007-01-01

Full Text Available Many ancient masonry towers are present in Italian territory. In some cases these structures are at risk on account of the intensity of the stresses they are subjected to due to the high level of regional seismicity. In order to preserve this inestimable cultural heritage, a sound safety assessment should take into account the evolution of damage phenomena. In this connection, acoustic emission (AE monitoring can be highly effective. This study concerns the structural stability of three medieval towers rising in the centre of Alba, a characteristic town in Piedmont (Italy. During the monitoring period a correlation between peaks of AE activity in the masonry of these towers and regional seismicity was found. Earthquakes always affect structural stability. Besides that, the towers behaved as sensitive earthquake receptors. Here a method to correlate bursts of AE activity in a masonry building and regional seismicity is proposed. In particular, this method permits to identify the premonitory signals that precede a catastrophic event on a structure, since, in most cases, these warning signs can be captured well in advance.

Acoustic emission from thermal-gradient cracks in UO2

International Nuclear Information System (INIS)

Kennedy, C.R.; Kupperman, D.S.; Wrona, B.J.

1975-01-01

A feasibility study has been conducted to evaluate the potential use of acoustic emission to monitor thermal-shock damage in direct electrical heating of UO 2 pellets. In the apparatus used for the present tests, two acoustic-emission sensors were placed on extensions of the upper and lower electrical feedthroughs. Commercially available equipment was used to accumulate acoustic-emission data. The accumulation of events displayed on a cathode-ray-tube screen indicates the total number of acoustic-emission events at a particular location within the pellet stack. These tests have indicated that acoustic emission can be used to monitor thermal-shock damage in UO 2 pellets subjected to direct-electrical heating. 8 references

Use of Acoustic Emission to Monitor Progressive Damage Accumulation in Kevlar (R) 49 Composites

Science.gov (United States)

Waller, Jess M.; Saulsberry, Regor L.; Andrade, Eduardo

2009-01-01

Acoustic emission (AE) data acquired during intermittent load hold tensile testing of epoxy impregnated Kevlar(Registeres TradeMark) 49 (K/Ep) composite strands were analyzed to monitor progressive damage during the approach to tensile failure. Insight into the progressive damage of K/Ep strands was gained by monitoring AE event rate and energy. Source location based on energy attenuation and arrival time data was used to discern between significant AE attributable to microstructural damage and spurious AE attributable to noise. One of the significant findings was the observation of increasing violation of the Kaiser effect (Felicity ratio < 1.0) with damage accumulation. The efficacy of three different intermittent load hold stress schedules that allowed the Felicity ratio to be determined analytically is discussed.

Department of Cybernetic Acoustics

Science.gov (United States)

The development of the theory, instrumentation and applications of methods and systems for the measurement, analysis, processing and synthesis of acoustic signals within the audio frequency range, particularly of the speech signal and the vibro-acoustic signal emitted by technical and industrial equipments treated as noise and vibration sources was discussed. The research work, both theoretical and experimental, aims at applications in various branches of science, and medicine, such as: acoustical diagnostics and phoniatric rehabilitation of pathological and postoperative states of the speech organ; bilateral ""man-machine'' speech communication based on the analysis, recognition and synthesis of the speech signal; vibro-acoustical diagnostics and continuous monitoring of the state of machines, technical equipments and technological processes.

Thermal Cracking in Westerly Granite Monitored Using Direct Wave Velocity, Coda Wave Interferometry, and Acoustic Emissions

Science.gov (United States)

Griffiths, L.; Lengliné, O.; Heap, M. J.; Baud, P.; Schmittbuhl, J.

2018-03-01

To monitor both the permanent (thermal microcracking) and the nonpermanent (thermo-elastic) effects of temperature on Westerly Granite, we combine acoustic emission monitoring and ultrasonic velocity measurements at ambient pressure during three heating and cooling cycles to a maximum temperature of 450°C. For the velocity measurements we use both P wave direct traveltime and coda wave interferometry techniques, the latter being more sensitive to changes in S wave velocity. During the first cycle, we observe a high acoustic emission rate and large—and mostly permanent—apparent reductions in velocity with temperature (P wave velocity is reduced by 50% of the initial value at 450°C, and 40% upon cooling). Our measurements are indicative of extensive thermal microcracking during the first cycle, predominantly during the heating phase. During the second cycle we observe further—but reduced—microcracking, and less still during the third cycle, where the apparent decrease in velocity with temperature is near reversible (at 450°C, the P wave velocity is decreased by roughly 10% of the initial velocity). Our results, relevant for thermally dynamic environments such as geothermal reservoirs, highlight the value of performing measurements of rock properties under in situ temperature conditions.

Passive acoustic monitoring of beaked whale densities in the Gulf of Mexico.

Science.gov (United States)

Hildebrand, John A; Baumann-Pickering, Simone; Frasier, Kaitlin E; Trickey, Jennifer S; Merkens, Karlina P; Wiggins, Sean M; McDonald, Mark A; Garrison, Lance P; Harris, Danielle; Marques, Tiago A; Thomas, Len

2015-11-12

Beaked whales are deep diving elusive animals, difficult to census with conventional visual surveys. Methods are presented for the density estimation of beaked whales, using passive acoustic monitoring data collected at sites in the Gulf of Mexico (GOM) from the period during and following the Deepwater Horizon oil spill (2010-2013). Beaked whale species detected include: Gervais' (Mesoplodon europaeus), Cuvier's (Ziphius cavirostris), Blainville's (Mesoplodon densirostris) and an unknown species of Mesoplodon sp. (designated as Beaked Whale Gulf - BWG). For Gervais' and Cuvier's beaked whales, we estimated weekly animal density using two methods, one based on the number of echolocation clicks, and another based on the detection of animal groups during 5 min time-bins. Density estimates derived from these two methods were in good general agreement. At two sites in the western GOM, Gervais' beaked whales were present throughout the monitoring period, but Cuvier's beaked whales were present only seasonally, with periods of low density during the summer and higher density in the winter. At an eastern GOM site, both Gervais' and Cuvier's beaked whales had a high density throughout the monitoring period.

Application of mass spectrometry based electronic nose and chemometrics for fingerprinting radiation treatment

International Nuclear Information System (INIS)

Gupta, Sumit; Variyar, Prasad S.; Sharma, Arun

2015-01-01

Volatile compounds were isolated from apples and grapes employing solid phase micro extraction (SPME) and subsequently analyzed by GC/MS equipped with a transfer line without stationary phase. Single peak obtained was integrated to obtain total mass spectrum of the volatile fraction of samples. A data matrix having relative abundance of all mass-to-charge ratios was subjected to principal component analysis (PCA) and linear discriminant analysis (LDA) to identify radiation treatment. PCA results suggested that there is sufficient variability between control and irradiated samples to build classification models based on supervised techniques. LDA successfully aided in segregating control from irradiated samples at all doses (0.1, 0.25, 0.5, 1.0, 1.5, 2.0 kGy). SPME-MS with chemometrics was successfully demonstrated as simple screening method for radiation treatment. - Highlights: • Total mass spectra obtained from HS-MS for control and irradiated fruits. • Grapes and apples are chosen for present study. • Total mass spectrum was analyzed by two chemometric techniques (PCA and LDA). • Successful segregation of control and irradiated samples achieved using chemometrics

Developments in acoustic emission for application to nuclear reactor systems

International Nuclear Information System (INIS)

Bentley, P.G.

1982-01-01

Developments in acoustic emission are summarised as they relate to the principal applications to nuclear reactors, and light water reactor pressure vessels in particular. Improvement in the understanding of acoustic emission has come from materials tests and these confirm the problems in applying the technique for in-service or periodic proof test monitoring of growing fatique cracks. Applications in LMFBR have confirmed that acoustic emission can be applied in the nuclear environment and the detection of stress corrosion cracking in both BWR and LMFBR seems possible. Some information is included on the developing interest in applying the techniques of acoustic emission for leak detection during shop hydro and in-service monitoring. Acoustic emission is also being developed for weld fabrication monitoring and recently introduced pattern recognition techniques are having a significant impact in this application. (author)

Effect of emodin on Candida albicans growth investigated by microcalorimetry combined with chemometric analysis.

Science.gov (United States)

Kong, W J; Wang, J B; Jin, C; Zhao, Y L; Dai, C M; Xiao, X H; Li, Z L

2009-07-01

Using the 3114/3115 thermal activity monitor (TAM) air isothermal microcalorimeter, ampoule mode, the heat output of Candida albicans growth at 37 degrees C was measured, and the effect of emodin on C. albicans growth was evaluated by microcalorimetry coupled with chemometric methods. The similarities between the heat flow power (HFP)-time curves of C. albicans growth affected by different concentrations of emodin were calculated by similarity analysis (SA). In the correspondence analysis (CA) diagram of eight quantitative parameters taken from the HFP-time curves, it could be deduced that emodin had definite dose-effect relationship as the distance between different concentrations of it increased along with the dosage and the effect. From the principal component analysis (PCA) on eight quantitative parameters, the action of emodin on C. albicans growth could be easily evaluated by analyzing the change of values of the main two parameters, growth rate constant k (2) and maximum power output P(2)(m). The coherent results of SA, CA, and PCA showed that emodin at different concentrations had different effects on C. albicans growth metabolism: A low concentration (0-10 microg ml(-1)) poorly inhibited the growth of C. albicans, and a high concentration (15-35 microg ml(-1)) could notably inhibit growth of this fungus. This work provided a useful idea of the combination of microcalorimetry and chemometric analysis for investigating the effect of drug and other compounds on microbes.

Acoustic emission monitoring of recycled aggregate concrete under bending

Science.gov (United States)

Tsoumani, A. A.; Barkoula, N.-M.; Matikas, T. E.

2015-03-01

The amount of construction and demolition waste has increased considerably over the last few years, making desirable the reuse of this waste in the concrete industry. In the present study concrete specimens are subjected at the age of 28 days to four-point bending with concurrent monitoring of their acoustic emission (AE) activity. Several concrete mixtures prepared using recycled aggregates at various percentages of the total coarse aggregate and also a reference mix using natural aggregates, were included to investigate their influence of the recycled aggregates on the load bearing capacity, as well as on the fracture mechanisms. The results reveal that for low levels of substitution the influence of using recycled aggregates on the flexural strength is negligible while higher levels of substitution lead into its deterioration. The total AE activity, as well as the AE signals emitted during failure, was related to flexural strength. The results obtained during test processing were found to be in agreement with visual observation.

Application of chemometric methods for assessment and modelling of microbiological quality data concerning coastal bathing water in Greece

Directory of Open Access Journals (Sweden)

Agelos Papaioannou

2014-12-01

Full Text Available Background. Worldwide, the aim of managing water is to safeguard human health whilst maintaining sustainable aquatic and associated terrestrial, ecosystems. Because human enteric viruses are the most likely pathogens responsible for waterborne diseases from recreational water use, but detection methods are complex and costly for routine monitoring, it is of great interest to determine the quality of coastal bathing water with a minimum cost and maximum safety. Design and methods. This study handles the assessment and modelling of the microbiological quality data of 2149 seawater bathing areas in Greece over 10-year period (1997-2006 by chemometric methods. Results. Cluster analysis results indicated that the studied bathing beaches are classified in accordance with the seasonality in three groups. Factor analysis was applied to investigate possible determining factors in the groups resulted from the cluster analysis, and also two new parameters were created in each group; VF1 includes E. coli, faecal coliforms and total coliforms and VF2 includes faecal streptococci/enterococci. By applying the cluster analysis in each seasonal group, three new groups of coasts were generated, group A (ultraclean, group B (clean and group C (contaminated. Conclusions. The above analysis is confirmed by the application of discriminant analysis, and proves that chemometric methods are useful tools for assessment and modeling microbiological quality data of coastal bathing water on a large scale, and thus could attribute to effective and economical monitoring of the quality of coastal bathing water in a country with a big number of bathing coasts, like Greece.

Acoustical experiment of yogurt fermentation process.

Science.gov (United States)

Ogasawara, H; Mizutani, K; Ohbuchi, T; Nakamura, T

2006-12-22

One of the important factors through food manufacturing is hygienic management. Thus, food manufactures prove their hygienic activities by taking certifications like a Hazard Analysis and Critical Control Point (HACCP). This concept also applies to food monitoring. Acoustical measurements have advantage for other measurement in food monitoring because they make it possible to measure with noncontact and nondestructive. We tried to monitor lactic fermentation of yogurt by a probing sensor using a pair of acoustic transducers. Temperature of the solution changes by the reaction heat of fermentation. Consequently the sound velocity propagated through the solution also changes depending on the temperature. At the same time, the solution change its phase from liquid to gel. The transducers usage in the solution indicates the change of the temperature as the change of the phase difference between two transducers. The acoustic method has advantages of nondestructive measurement that reduces contamination of food product by measuring instrument. The sensor was inserted into milk with lactic acid bacterial stain of 19 degrees C and monitored phase retardation of propagated acoustic wave and its temperature with thermocouples in the mild. The monitoring result of fermentation from milk to Caspian Sea yogurt by the acoustic transducers with the frequency of 3.7 MHz started to show gradient change in temperature caused by reaction heat of fermentation but stop the gradient change at the end although the temperature still change. The gradient change stopped its change because of phase change from liquid to gel. The present method will be able to measure indirectly by setting transducers outside of the measuring object. This noncontact sensing method will have great advantage of reduces risk of food contamination from measuring instrument because the measurement probes are set out of fermentation reactor or food containers. Our proposed method will contribute to the

Acoustic signal emission monitoring as a novel method to predict steam pops during radiofrequency ablation: preliminary observations.

Science.gov (United States)

Chik, William W B; Kosobrodov, Roman; Bhaskaran, Abhishek; Barry, Michael Anthony Tony; Nguyen, Doan Trang; Pouliopoulos, Jim; Byth, Karen; Sivagangabalan, Gopal; Thomas, Stuart P; Ross, David L; McEwan, Alistair; Kovoor, Pramesh; Thiagalingam, Aravinda

2015-04-01

predictably occur before imminent steam popping during RF ablations. Such acoustic emissions can be carefully monitored during an ablation and may be useful to prevent serious complications during RF delivery. © 2014 Wiley Periodicals, Inc.

Circum-Arctic petroleum systems identified using decision-tree chemometrics

Science.gov (United States)

Peters, K.E.; Ramos, L.S.; Zumberge, J.E.; Valin, Z.C.; Scotese, C.R.; Gautier, D.L.

2007-01-01

Source- and age-related biomarker and isotopic data were measured for more than 1000 crude oil samples from wells and seeps collected above approximately 55??N latitude. A unique, multitiered chemometric (multivariate statistical) decision tree was created that allowed automated classification of 31 genetically distinct circumArctic oil families based on a training set of 622 oil samples. The method, which we call decision-tree chemometrics, uses principal components analysis and multiple tiers of K-nearest neighbor and SIMCA (soft independent modeling of class analogy) models to classify and assign confidence limits for newly acquired oil samples and source rock extracts. Geochemical data for each oil sample were also used to infer the age, lithology, organic matter input, depositional environment, and identity of its source rock. These results demonstrate the value of large petroleum databases where all samples were analyzed using the same procedures and instrumentation. Copyright ?? 2007. The American Association of Petroleum Geologists. All rights reserved.

Chemometric classification of casework arson samples based on gasoline content.

Science.gov (United States)

Sinkov, Nikolai A; Sandercock, P Mark L; Harynuk, James J

2014-02-01

Detection and identification of ignitable liquids (ILs) in arson debris is a critical part of arson investigations. The challenge of this task is due to the complex and unpredictable chemical nature of arson debris, which also contains pyrolysis products from the fire. ILs, most commonly gasoline, are complex chemical mixtures containing hundreds of compounds that will be consumed or otherwise weathered by the fire to varying extents depending on factors such as temperature, air flow, the surface on which IL was placed, etc. While methods such as ASTM E-1618 are effective, data interpretation can be a costly bottleneck in the analytical process for some laboratories. In this study, we address this issue through the application of chemometric tools. Prior to the application of chemometric tools such as PLS-DA and SIMCA, issues of chromatographic alignment and variable selection need to be addressed. Here we use an alignment strategy based on a ladder consisting of perdeuterated n-alkanes. Variable selection and model optimization was automated using a hybrid backward elimination (BE) and forward selection (FS) approach guided by the cluster resolution (CR) metric. In this work, we demonstrate the automated construction, optimization, and application of chemometric tools to casework arson data. The resulting PLS-DA and SIMCA classification models, trained with 165 training set samples, have provided classification of 55 validation set samples based on gasoline content with 100% specificity and sensitivity. Copyright © 2013 Elsevier Ireland Ltd. All rights reserved.

Preliminary Development of Online Monitoring Acoustic Emission System for the Integrity of Research Reactor Components

Science.gov (United States)

Bakhri, S.; Sumarno, E.; Himawan, R.; Akbar, T. Y.; Subekti, M.; Sunaryo, G. R.

2018-02-01

Three research reactors owned by BATAN have been more than 25 years. Aging of (Structure, System and Component) SSC which is mainly related to mechanical causes become the most important issue for the sustainability and safety operation. Acoustic Emission (AE) is one of the appropriate and recommended methods by the IAEA for inspection as well as at the same time for the monitoring of mechanical SSC related. However, the advantages of AE method in detecting the acoustic emission both for the inspection and the online monitoring require a relatively complex measurement system including hardware software system for the signal detection and analysis purposes. Therefore, aim of this work was to develop an AE system based on an embedded system which capable for doing both the online monitoring and inspection of the research reactor’s integrity structure. An embedded system was selected due to the possibility to install the equipment on the field in extreme environmental condition with capability to store, analyses, and send the required information for further maintenance and operation. The research was done by designing the embedded system based on the Field Programmable Gate Array (FPGA) platform, because of their execution speed and system reconfigurable opportunities. The AE embedded system is then tested to identify the AE source location and AE characteristic under tensile material testing. The developed system successfully acquire the AE elastic waveform and determine the parameter-based analysis such as the amplitude, peak, duration, rise time, counts and the average frequency both for the source location test and the tensile test.

Chemometric modeling of thermogravimetric data for the compositional analysis of forest biomass.

Science.gov (United States)

Acquah, Gifty E; Via, Brian K; Fasina, Oladiran O; Adhikari, Sushil; Billor, Nedret; Eckhardt, Lori G

2017-01-01

The objective of this study was to investigated the use of chemometric modeling of thermogravimetric (TG) data as an alternative approach to estimate the chemical and proximate (i.e. volatile matter, fixed carbon and ash contents) composition of lignocellulosic biomass. Since these properties affect the conversion pathway, processing costs, yield and / or quality of products, a capability to rapidly determine these for biomass feedstock entering the process stream will be useful in the success and efficiency of bioconversion technologies. The 38-minute long methodology developed in this study enabled the simultaneous prediction of both the chemical and proximate properties of forest-derived biomass from the same TG data. Conventionally, two separate experiments had to be conducted to obtain such information. In addition, the chemometric models constructed with normalized TG data outperformed models developed via the traditional deconvolution of TG data. PLS and PCR models were especially robust in predicting the volatile matter (R2-0.92; RPD- 3.58) and lignin (R2-0.82; RPD- 2.40) contents of the biomass. The application of chemometrics to TG data also made it possible to predict some monomeric sugars in this study. Elucidation of PC loadings obtained from chemometric models also provided some insights into the thermal decomposition behavior of the chemical constituents of lignocellulosic biomass. For instance, similar loadings were noted for volatile matter and cellulose, and for fixed carbon and lignin. The findings indicate that common latent variables are shared between these chemical and thermal reactivity properties. Results from this study buttresses literature that have reported that the less thermally stable polysaccharides are responsible for the yield of volatiles whereas the more recalcitrant lignin with its higher percentage of elementary carbon contributes to the yield of fixed carbon.

Chemometric modeling of thermogravimetric data for the compositional analysis of forest biomass.

Directory of Open Access Journals (Sweden)

Gifty E Acquah

Full Text Available The objective of this study was to investigated the use of chemometric modeling of thermogravimetric (TG data as an alternative approach to estimate the chemical and proximate (i.e. volatile matter, fixed carbon and ash contents composition of lignocellulosic biomass. Since these properties affect the conversion pathway, processing costs, yield and / or quality of products, a capability to rapidly determine these for biomass feedstock entering the process stream will be useful in the success and efficiency of bioconversion technologies. The 38-minute long methodology developed in this study enabled the simultaneous prediction of both the chemical and proximate properties of forest-derived biomass from the same TG data. Conventionally, two separate experiments had to be conducted to obtain such information. In addition, the chemometric models constructed with normalized TG data outperformed models developed via the traditional deconvolution of TG data. PLS and PCR models were especially robust in predicting the volatile matter (R2-0.92; RPD- 3.58 and lignin (R2-0.82; RPD- 2.40 contents of the biomass. The application of chemometrics to TG data also made it possible to predict some monomeric sugars in this study. Elucidation of PC loadings obtained from chemometric models also provided some insights into the thermal decomposition behavior of the chemical constituents of lignocellulosic biomass. For instance, similar loadings were noted for volatile matter and cellulose, and for fixed carbon and lignin. The findings indicate that common latent variables are shared between these chemical and thermal reactivity properties. Results from this study buttresses literature that have reported that the less thermally stable polysaccharides are responsible for the yield of volatiles whereas the more recalcitrant lignin with its higher percentage of elementary carbon contributes to the yield of fixed carbon.

Acoustical method of whole-body hydration status monitoring

Science.gov (United States)

Sarvazyan, A. P.; Tsyuryupa, S. N.; Calhoun, M.; Utter, A.

2016-07-01

An acoustical handheld hydration monitor (HM) for assessing the water balance of the human body was developed. Dehydration is a critical public health problem. Many elderly over age of 65 are particularly vulnerable as are infants and young children. Given that dehydration is both preventable and reversible, the need for an easy-to-perform method for the detection of water imbalance is of the utmost clinical importance. The HM is based on an experimental fact that ultrasound velocity in muscle is a linear function of water content and can be referenced to the hydration status of the body. Studies on the validity of HM for the assessment of whole-body hydration status were conducted in the Appalachian State University, USA, on healthy young adults and on elderly subjects residing at an assisted living facility. The HM was able to track changes in total body water during periods of acute dehydration and rehydration in athletes and day-to-day and diurnal variability of hydration in elderly. Results of human studies indicate that HM has a potential to become an efficient tool for detecting abnormal changes in the body hydration status.

Effects of subsampling of passive acoustic recordings on acoustic metrics.

Science.gov (United States)

Thomisch, Karolin; Boebel, Olaf; Zitterbart, Daniel P; Samaran, Flore; Van Parijs, Sofie; Van Opzeeland, Ilse

2015-07-01

Passive acoustic monitoring is an important tool in marine mammal studies. However, logistics and finances frequently constrain the number and servicing schedules of acoustic recorders, requiring a trade-off between deployment periods and sampling continuity, i.e., the implementation of a subsampling scheme. Optimizing such schemes to each project's specific research questions is desirable. This study investigates the impact of subsampling on the accuracy of two common metrics, acoustic presence and call rate, for different vocalization patterns (regimes) of baleen whales: (1) variable vocal activity, (2) vocalizations organized in song bouts, and (3) vocal activity with diel patterns. To this end, above metrics are compared for continuous and subsampled data subject to different sampling strategies, covering duty cycles between 50% and 2%. The results show that a reduction of the duty cycle impacts negatively on the accuracy of both acoustic presence and call rate estimates. For a given duty cycle, frequent short listening periods improve accuracy of daily acoustic presence estimates over few long listening periods. Overall, subsampling effects are most pronounced for low and/or temporally clustered vocal activity. These findings illustrate the importance of informed decisions when applying subsampling strategies to passive acoustic recordings or analyses for a given target species.

Continuous wavelet transform analysis and modal location analysis acoustic emission source location for nuclear piping crack growth monitoring

Energy Technology Data Exchange (ETDEWEB)

Mohd, Shukri [Nondestructive Testing Group, Industrial Technology Division, Malaysian Nuclear Agency, 43000, Bangi, Selangor (Malaysia); Holford, Karen M.; Pullin, Rhys [Cardiff School of Engineering, Cardiff University, Queen' s Buildings, The Parade, CARDIFF CF24 3AA (United Kingdom)

2014-02-12

Source location is an important feature of acoustic emission (AE) damage monitoring in nuclear piping. The ability to accurately locate sources can assist in source characterisation and early warning of failure. This paper describe the development of a novelAE source location technique termed 'Wavelet Transform analysis and Modal Location (WTML)' based on Lamb wave theory and time-frequency analysis that can be used for global monitoring of plate like steel structures. Source location was performed on a steel pipe of 1500 mm long and 220 mm outer diameter with nominal thickness of 5 mm under a planar location test setup using H-N sources. The accuracy of the new technique was compared with other AE source location methods such as the time of arrival (TOA) techniqueand DeltaTlocation. Theresults of the study show that the WTML method produces more accurate location resultscompared with TOA and triple point filtering location methods. The accuracy of the WTML approach is comparable with the deltaT location method but requires no initial acoustic calibration of the structure.

Continuous wavelet transform analysis and modal location analysis acoustic emission source location for nuclear piping crack growth monitoring

International Nuclear Information System (INIS)

Shukri Mohd

2013-01-01

Full-text: Source location is an important feature of acoustic emission (AE) damage monitoring in nuclear piping. The ability to accurately locate sources can assist in source characterisation and early warning of failure. This paper describe the development of a novelAE source location technique termed Wavelet Transform analysis and Modal Location (WTML) based on Lamb wave theory and time-frequency analysis that can be used for global monitoring of plate like steel structures. Source location was performed on a steel pipe of 1500 mm long and 220 mm outer diameter with nominal thickness of 5 mm under a planar location test setup using H-N sources. The accuracy of the new technique was compared with other AE source location methods such as the time of arrival (TOA) technique and DeltaTlocation. The results of the study show that the WTML method produces more accurate location results compared with TOA and triple point filtering location methods. The accuracy of the WTML approach is comparable with the deltaT location method but requires no initial acoustic calibration of the structure. (author)

Continuous wavelet transform analysis and modal location analysis acoustic emission source location for nuclear piping crack growth monitoring

International Nuclear Information System (INIS)

Mohd, Shukri; Holford, Karen M.; Pullin, Rhys

2014-01-01

Source location is an important feature of acoustic emission (AE) damage monitoring in nuclear piping. The ability to accurately locate sources can assist in source characterisation and early warning of failure. This paper describe the development of a novelAE source location technique termed 'Wavelet Transform analysis and Modal Location (WTML)' based on Lamb wave theory and time-frequency analysis that can be used for global monitoring of plate like steel structures. Source location was performed on a steel pipe of 1500 mm long and 220 mm outer diameter with nominal thickness of 5 mm under a planar location test setup using H-N sources. The accuracy of the new technique was compared with other AE source location methods such as the time of arrival (TOA) techniqueand DeltaTlocation. Theresults of the study show that the WTML method produces more accurate location resultscompared with TOA and triple point filtering location methods. The accuracy of the WTML approach is comparable with the deltaT location method but requires no initial acoustic calibration of the structure

Near-Real-Time Acoustic Monitoring of Beaked Whales and Other Cetaceans Using a Seaglider™

Science.gov (United States)

Klinck, Holger; Mellinger, David K.; Klinck, Karolin; Bogue, Neil M.; Luby, James C.; Jump, William A.; Shilling, Geoffrey B.; Litchendorf, Trina; Wood, Angela S.; Schorr, Gregory S.; Baird, Robin W.

2012-01-01

In most areas, estimating the presence and distribution of cryptic marine mammal species, such as beaked whales, is extremely difficult using traditional observational techniques such as ship-based visual line transect surveys. Because acoustic methods permit detection of animals underwater, at night, and in poor weather conditions, passive acoustic observation has been used increasingly often over the last decade to study marine mammal distribution, abundance, and movements, as well as for mitigation of potentially harmful anthropogenic effects. However, there is demand for new, cost-effective tools that allow scientists to monitor areas of interest autonomously with high temporal and spatial resolution in near-real time. Here we describe an autonomous underwater vehicle – a glider – equipped with an acoustic sensor and onboard data processing capabilities to passively scan an area for marine mammals in near-real time. The glider was tested extensively off the west coast of the Island of Hawai'i, USA. The instrument covered approximately 390 km during three weeks at sea and collected a total of 194 h of acoustic data. Detections of beaked whales were successfully reported to shore in near-real time. Manual analysis of the recorded data revealed a high number of vocalizations of delphinids and sperm whales. Furthermore, the glider collected vocalizations of unknown origin very similar to those made by known species of beaked whales. The instrument developed here can be used to cost-effectively screen areas of interest for marine mammals for several months at a time. The near-real-time detection and reporting capabilities of the glider can help to protect marine mammals during potentially harmful anthropogenic activities such as seismic exploration for sub-sea fossil fuels or naval sonar exercises. Furthermore, the glider is capable of under-ice operation, allowing investigation of otherwise inaccessible polar environments that are critical habitats for many

Near-real-time acoustic monitoring of beaked whales and other cetaceans using a Seaglider™.

Directory of Open Access Journals (Sweden)

Holger Klinck

Full Text Available In most areas, estimating the presence and distribution of cryptic marine mammal species, such as beaked whales, is extremely difficult using traditional observational techniques such as ship-based visual line transect surveys. Because acoustic methods permit detection of animals underwater, at night, and in poor weather conditions, passive acoustic observation has been used increasingly often over the last decade to study marine mammal distribution, abundance, and movements, as well as for mitigation of potentially harmful anthropogenic effects. However, there is demand for new, cost-effective tools that allow scientists to monitor areas of interest autonomously with high temporal and spatial resolution in near-real time. Here we describe an autonomous underwater vehicle--a glider--equipped with an acoustic sensor and onboard data processing capabilities to passively scan an area for marine mammals in near-real time. The glider was tested extensively off the west coast of the Island of Hawai'i, USA. The instrument covered approximately 390 km during three weeks at sea and collected a total of 194 h of acoustic data. Detections of beaked whales were successfully reported to shore in near-real time. Manual analysis of the recorded data revealed a high number of vocalizations of delphinids and sperm whales. Furthermore, the glider collected vocalizations of unknown origin very similar to those made by known species of beaked whales. The instrument developed here can be used to cost-effectively screen areas of interest for marine mammals for several months at a time. The near-real-time detection and reporting capabilities of the glider can help to protect marine mammals during potentially harmful anthropogenic activities such as seismic exploration for sub-sea fossil fuels or naval sonar exercises. Furthermore, the glider is capable of under-ice operation, allowing investigation of otherwise inaccessible polar environments that are critical

Holographic and acoustic emission evaluation of pressure vessels

International Nuclear Information System (INIS)

Boyd, D.M.

1980-01-01

Optical holographic interfereometry and acoustic emission monitoring were simultaneously used to evaluate two small, high pressure vessels during pressurization. The techniques provide pressure vessel designers with both quantitative information such as displacement/strain measurements and qualitative information such as flaw detection. The data from the holographic interferograms were analyzed for strain profiles. The acoustic emission signals were monitored for crack growth and vessel quality

Swept frequency acoustic interferometry technique for chemical weapons verification and monitoring

Energy Technology Data Exchange (ETDEWEB)

Sinha, D.N.; Anthony, B.W.; Lizon, D.C.

1995-03-01

Nondestructive evaluation (NDE) techniques are important for rapid on-site verification and monitoring of chemical munitions, such as artillery shells and bulk containers. Present NDE techniques provide only limited characterizations of such munitions. This paper describes the development of a novel noninvasive technique, swept-frequency acoustic interferometry (SFAI), that significantly enhances the capability of munitions characterizations. The SFAI technique allows very accurate and simultaneous determination of sound velocity and attenuation of chemical agents over a large frequency range inside artillery shells, in addition to determining agent density. The frequency-dependent sound velocity and attenuation can, in principle, provide molecular relaxation properties of the chemical agent. The same instrument also enables a direct fill-level measurement in bulk containers. Industrial and other applications of this general-purpose technique are also discussed.

Controlled ultrasound-induced blood-brain barrier disruption using passive acoustic emissions monitoring.

Directory of Open Access Journals (Sweden)

Costas D Arvanitis

Full Text Available The ability of ultrasonically-induced oscillations of circulating microbubbles to permeabilize vascular barriers such as the blood-brain barrier (BBB holds great promise for noninvasive targeted drug delivery. A major issue has been a lack of control over the procedure to ensure both safe and effective treatment. Here, we evaluated the use of passively-recorded acoustic emissions as a means to achieve this control. An acoustic emissions monitoring system was constructed and integrated into a clinical transcranial MRI-guided focused ultrasound system. Recordings were analyzed using a spectroscopic method that isolates the acoustic emissions caused by the microbubbles during sonication. This analysis characterized and quantified harmonic oscillations that occur when the BBB is disrupted, and broadband emissions that occur when tissue damage occurs. After validating the system's performance in pilot studies that explored a wide range of exposure levels, the measurements were used to control the ultrasound exposure level during transcranial sonications at 104 volumes over 22 weekly sessions in four macaques. We found that increasing the exposure level until a large harmonic emissions signal was observed was an effective means to ensure BBB disruption without broadband emissions. We had a success rate of 96% in inducing BBB disruption as measured by in contrast-enhanced MRI, and we detected broadband emissions in less than 0.2% of the applied bursts. The magnitude of the harmonic emissions signals was significantly (P<0.001 larger for sonications where BBB disruption was detected, and it correlated with BBB permeabilization as indicated by the magnitude of the MRI signal enhancement after MRI contrast administration (R(2 = 0.78. Overall, the results indicate that harmonic emissions can be a used to control focused ultrasound-induced BBB disruption. These results are promising for clinical translation of this technology.

Electrical Resistance and Acoustic Emission Measurements for Monitoring the Structural Behavior of CFRP Laminate

KAUST Repository

Zhou, Wei

2015-07-12

Electrical resistance and acoustic emission (AE) measurement are jointly used to monitor the degradation in CFRP laminates subjected to tensile tests. The objective of this thesis is to perform a synergertic analysis between a passive and an active methods to better access how these perform when used for Structural Health Moni- toring (SHM). Laminates with three different stacking sequences: [0]4, [02/902]s and [+45/ − 45]2s are subjected to monotonic and cyclic tensile tests. In each laminate, we carefully investigate which mechanisms of degradation can or cannot be detect- ed by each technique. It is shown that most often, that acoustic emission signals start before any electrical detection is possible. This is is explained based on the redundance of the electrical network that makes it less sensitive to localized damages. Based on in depth study of AE signals clustering, a new classification is proposed to recognize the different damage mechanims based on only two parameters: the RA (rise time/amplitude) and the duration of the signal.

Relationships between acoustic emissions and microstructures

International Nuclear Information System (INIS)

Rao, G.V.; Gopal, R.

1979-01-01

Results of a systematic study of 'microstructure-deformation-acoustic emission' relationships on two widely used pressure retaining component materials, namely A533-B nuclear pressure vessel steel and a 7075 aluminum alloy, are presented. The study consists of conducting acoustic monitored tensile tests on a variety of quenched and aged microstructures in the two alloy systems and extensive microstructural characterization of test specimens by light optic and electron microscopy techniques. The results suggest a consistent relationship between acoustic emissions and microdeformation mechanisms. The role of specific microstructural constituents in generating acoustic emissions in the two alloys is discussed. (author)

Acoustic emission measurement on large scale coils at JAERI

International Nuclear Information System (INIS)

Yoshida, K.; Hattori, Y.; Nishi, M.F.; Shimamoto, S.; Tsuji, H.

1986-01-01

The objective of acoustic emission measurement at Japan Atomic Energy Research Institute (JAERI) is an establishment of a general diagnostic method for superconducting magnet systems. Output of strain and displacement gages can not cover a whole system in monitoring premonitory phenomena of a magnet system s failure, because these sensors are mounted on points and therefore localized. Acoustic emissions can be transmitted to sensors through structural materials without electrical noise. Monitoring of acoustic emission will be one of the methods to predict a serious failure of magnet systems in a vacuum vessel. For this purpose, several sensors were installed on the Japanese LCT coil and the Test Module Coil (TMC). Some of acoustic activity was similar as seen in these coils. The correlation between voltage spikes and acoustic events is excellent during single coil charging mode, but poorer during out of plane force mode. There are no indicative acoustical phenomena before a magnet quench or during normal zone generation. The conditioning of acoustic events and voltage spikes can be seen after any cooling down. The localization of electrical insulation damage with the acoustic emission technique is one of its most useful applications

Damage Accumulation in Cyclically-Loaded Glass-Ceramic Matrix Composites Monitored by Acoustic Emission

Directory of Open Access Journals (Sweden)

D. G. Aggelis

2013-01-01

Full Text Available Barium osumilite (BMAS ceramic matrix composites reinforced with SiC-Tyranno fibers are tested in a cyclic loading protocol. Broadband acoustic emission (AE sensors are used for monitoring the occurrence of different possible damage mechanisms. Improved use of AE indices is proposed by excluding low-severity signals based on waveform parameters, rather than only threshold criteria. The application of such improvements enhances the accuracy of the indices as accumulated damage descriptors. RA-value, duration, and signal energy follow the extension cycles indicating moments of maximum or minimum strain, while the frequency content of the AE signals proves very sensitive to the pull-out mechanism.

Testing the effectiveness of automated acoustic sensors for monitoring vocal activity of Marbled Murrelets Brachyramphus marmoratus

Science.gov (United States)

Cragg, Jenna L.; Burger, Alan E.; Piatt, John F.

2015-01-01

Cryptic nest sites and secretive breeding behavior make population estimates and monitoring of Marbled Murrelets Brachyramphus marmoratus difficult and expensive. Standard audio-visual and radar protocols have been refined but require intensive field time by trained personnel. We examined the detection range of automated sound recorders (Song Meters; Wildlife Acoustics Inc.) and the reliability of automated recognition models (“recognizers”) for identifying and quantifying Marbled Murrelet vocalizations during the 2011 and 2012 breeding seasons at Kodiak Island, Alaska. The detection range of murrelet calls by Song Meters was estimated to be 60 m. Recognizers detected 20 632 murrelet calls (keer and keheer) from a sample of 268 h of recordings, yielding 5 870 call series, which compared favorably with human scanning of spectrograms (on average detecting 95% of the number of call series identified by a human observer, but not necessarily the same call series). The false-negative rate (percentage of murrelet call series that the recognizers failed to detect) was 32%, mainly involving weak calls and short call series. False-positives (other sounds included by recognizers as murrelet calls) were primarily due to complex songs of other bird species, wind and rain. False-positives were lower in forest nesting habitat (48%) and highest in shrubby vegetation where calls of other birds were common (97%–99%). Acoustic recorders tracked spatial and seasonal trends in vocal activity, with higher call detections in high-quality forested habitat and during late July/early August. Automated acoustic monitoring of Marbled Murrelet calls could provide cost-effective, valuable information for assessing habitat use and temporal and spatial trends in nesting activity; reliability is dependent on careful placement of sensors to minimize false-positives and on prudent application of digital recognizers with visual checking of spectrograms.

Chemometric Analysis of Selected Organic Contaminants in Surface Water of Langat River Basin

International Nuclear Information System (INIS)

Mohamad Rafaie Mohamed Zubir; Rozita Osman; Norashikin Saim

2016-01-01

Chemometric techniques namely hierarchical agglomerative cluster analysis (HACA), discriminant analysis (DA), principal component analysis (PCA) and factor analysis (FA) were applied to the distribution of selected organic contaminants (polycyclic aromatic hydrocarbons (PAHs), sterols, pesticides (chloropyrifos), and phenol) to assess the potential of using these organic contaminants as chemical markers in Langat River Basin. Water samples were collected from February 2012 to January 2013 on a monthly basis for nine monitoring sites along Langat River Basin. HACA was able to classify the sampling sites into three clusters which can be correlated to the level of contamination (low, moderate and high contamination sites). DA was used to discriminate the sources of contamination using the selected organic contaminants and relate to the existing DOE local activities groupings. Forward and backward stepwise DA was able to discriminate two and five organic contaminants variables, respectively, from the original 13 selected variables. The five significant variables identified using backward stepwise DA were fluorene, pyrene, stigmastanol, stigmasterol and phenol. PCA and FA (varimax functionality) were used to identify the possible sources of each organic contaminant based on the inventory of local activities. Five principal components were obtained with 66.5 % of the total variation. Result from FA indicated that PAHs (pyrene, fluorene, acenaphthene, benzo[a]anthracene) originated from industrial activity and socio-economic activities; while sterols (coprostanol, stigmastanol and stigmasterol) were associated to domestic sewage and local socio-economic activities. The occurrence of chloropyrifos was correlated to agricultural activities, urban and domestic discharges. This study showed that the application of chemometrics on the distribution of selected organic contaminants was able to trace the sources of contamination in surface water. (author)

Determination of Commercials Cooking Oils and Fats Using Chemometrics Methods

International Nuclear Information System (INIS)

Azwan Mat Lazim; Mohd Zuli Jaafar; Phang Wei Shong, P.W.; Suzereen Jamil

2013-01-01

In this study, chemometric method has been used in determining the oil quality. The samples used were olive oil, sunflower oil and butter from two different brands. Two different conditions were applied, either it was fresh or fried. Titratio, a conventional method was used to determine free fatty acids content (FFA), iodine value (IV), and peroxide value (PV). Twelve samples were then used for analysis and their FTIR spectra were measured at 4000-400 cm -1 . The computer stimulation was used to process the data based on their pattern recognition which optimized by principal component analysis (PCA) and partial least squares (PLS). PCA model was used to distinguish the properties between fresh and fried oil. The PLS model was used to predict the value for validation test in comparison with conventional results. Results showed the validation value for fresh oil was 0.90. This indicated the chemometric method was in agreement with conventional method. (author)

Fort Davis National Historic Site : acoustical monitoring

Science.gov (United States)

2013-06-01

During the summer of 2010 (September - October 2010), the Volpe Center collected baseline acoustical data at Fort Davis National Historic Site (FODA)at two sites deployed for approximately 30 days each. The baseline data collected during this period ...

Big Bend National Park: Acoustical Monitoring 2010

Science.gov (United States)

2013-06-01

During the summer of 2010 (September October 2010), the Volpe Center collected baseline acoustical data at Big Bend National Park (BIBE) at four sites deployed for approximately 30 days each. The baseline data collected during this period will he...

Chemometrics for ion mobility spectrometry data: recent advances and future prospects

NARCIS (Netherlands)

Szymanska, E.; Davies, Antony N.; Buydens, L.M.C.

2016-01-01

Historically, advances in the field of ion mobility spectrometry have been hindered by the variation in measured signals between instruments developed by different research laboratories or manufacturers. This has triggered the development and application of chemometric techniques able to reveal and

Practical acoustic emission testing

CERN Document Server

2016-01-01

This book is intended for non-destructive testing (NDT) technicians who want to learn practical acoustic emission testing based on level 1 of ISO 9712 (Non-destructive testing – Qualification and certification of personnel) criteria. The essential aspects of ISO/DIS 18436-6 (Condition monitoring and diagnostics of machines – Requirements for training and certification of personnel, Part 6: Acoustic Emission) are explained, and readers can deepen their understanding with the help of practice exercises. This work presents the guiding principles of acoustic emission measurement, signal processing, algorithms for source location, measurement devices, applicability of testing methods, and measurement cases to support not only researchers in this field but also and especially NDT technicians.

Chemometric analysis of frequency-domain photon migration data: quantitative measurements of optical properties and chromophore concentrations in multicomponent turbid media

International Nuclear Information System (INIS)

Berger, Andrew J.; Venugopalan, Vasan; Durkin, Anthony J.; Pham, Tuan; Tromberg, Bruce J.

2000-01-01

Frequency-domain photon migration (FDPM) is a widely used technique for measuring the optical properties (i.e., absorption, μ a , and reduced scattering, μ s ' , coefficients) of turbid samples. Typically, FDPM data analysis is performed with models based on a photon diffusion equation; however, analytical solutions are difficult to obtain for many realistic geometries. Here, we describe the use of models based instead on representative samples and multivariate calibration (chemometrics). FDPM data at seven wavelengths (ranging from 674 to 956 nm) and multiple modulation frequencies (ranging from 50 to 600 MHz) were gathered from turbid samples containing mixtures of three absorbing dyes. Values for μ a and μ s ' were extracted from the FDPM data in different ways, first with the diffusion theory and then with the chemometric technique of partial least squares. Dye concentrations were determined from the FDPM data by three methods, first by least-squares fits to the diffusion results and then by two chemometric approaches. The accuracy of the chemometric predictions was comparable or superior for all three dyes. Our results indicate that chemometrics can recover optical properties and dye concentrations from the frequency-dependent behavior of photon density waves, without the need for diffusion-based models. Future applications to more complicated geometries, lower-scattering samples, and simpler FDPM instrumentation are discussed. (c) 2000 Optical Society of America

Assessment on pattern of urban air quality by using chemometric ...

African Journals Online (AJOL)

The study evaluate the relationship between the main daily concentrations of criteria air pollutants in urban areas and their associations by using chemometric technique. Data were gathered from the Department of Environmental for three years observations (2011-2013) consisting of 5 major pollutants such as SO2, NO2, ...

Simultaneous determination of three herbicides by differential pulse voltammetry and chemometrics.

Science.gov (United States)

Ni, Yongnian; Wang, Lin; Kokot, Serge

2011-01-01

A novel differential pulse voltammetry method (DPV) was researched and developed for the simultaneous determination of Pendimethalin, Dinoseb and sodium 5-nitroguaiacolate (5NG) with the aid of chemometrics. The voltammograms of these three compounds overlapped significantly, and to facilitate the simultaneous determination of the three analytes, chemometrics methods were applied. These included classical least squares (CLS), principal component regression (PCR), partial least squares (PLS) and radial basis function-artificial neural networks (RBF-ANN). A separately prepared verification data set was used to confirm the calibrations, which were built from the original and first derivative data matrices of the voltammograms. On the basis relative prediction errors and recoveries of the analytes, the RBF-ANN and the DPLS (D - first derivative spectra) models performed best and are particularly recommended for application. The DPLS calibration model was applied satisfactorily for the prediction of the three analytes from market vegetables and lake water samples.

Development of an incipient rotor crack detection method by acoustic emission techniques

International Nuclear Information System (INIS)

Le Reverend, D.; Massouri, M.H.

1988-01-01

The objective of the program presented is to develop a method of detection and monitoring of crack growth in machine rotor by application of acoustic emission techniques. This program is performed by R and D Division of Electricite de France, jointly with INSA de Lyon. The first task of the program is relative to the characterization of acoustic emission during a progressive tensile test performed on a NCT specimen. The second task of the program deals with the experimentation of acoustic emission techniques for the monitoring of a specimen during cycling bending tests. The last task of the program is relative to evaluation of application of acoustic emission techniques for a small rotor integrity monitoring during fatigue rotation tests [fr

Acoustic Emission Monitoring of Incipient in Journal Bearings - Part I : Detectability and measurement for bearing damages

International Nuclear Information System (INIS)

Yoon, Dong Jin; Kwon, Oh Yang; Chung, Min Hwa; Kim, Kyung Woong

1994-01-01

In contrast to the machinery using rolling element bearings, systems with journal bearings generally operate in large scale and under severe loading condition such as steam generator turbines and internal combustion engines. Failure of the bearings in these machinery can result in the system breakdown. To avoid the time consuming repair and considerable economic loss, the detection of incipient failure in journal bearings becomes very important. In this experimental approach, acoustic emission monitoring is applied to the detection of incipient failure caused by several types of abnormal operating condition most probable in the journal bearing systems. It has been known that the intervention of foreign materials, insufficient lubrication and misassembly etc. are principal factors to cause bearing failure and distress. The experiment was conducted under such designed conditions as hard particles in the lubrication layer, insufficient lubrication, and metallic contact in the simulated journal bearing system. The results showed that acoustic emission could be an effective tool to detect the incipient failure in journal bearings

Diesel Engine Valve Clearance Detection Using Acoustic Emission

Directory of Open Access Journals (Sweden)

Fathi Elamin

2010-01-01

Full Text Available This paper investigated, using experimental method, the suitability of acoustic emission (AE technique for the condition monitoring of diesel engine valve faults. The clearance fault was adjusted experimentally in an exhaust valve and successfully detected and diagnosed in a Ford FSD 425 four-cylinder, four-stroke, in-line OHV, direct injection diesel engine. The effect of faulty exhaust valve clearance on engine performance was monitored and the difference between the healthy and faulty engine was observed from the recorded AE signals. The measured results from this technique show that using only time domain and frequency domain analysis of acoustic emission signals can give a superior measure of engine condition. This concludes that acoustic emission is a powerful and reliable method of detection and diagnosis of the faults in diesel engines and this is considered to be a unique approach to condition monitoring of valve performance.

Authenticity study of Phyllanthus species by NMR and FT-IR techniques coupled with chemometric methods

International Nuclear Information System (INIS)

Santos, Maiara S.; Pereira-Filho, Edenir R.; Ferreira, Antonio G.; Boffo, Elisangela F.; Figueira, Glyn M.

2012-01-01

The importance of medicinal plants and their use in industrial applications is increasing worldwide, especially in Brazil. Phyllanthus species, popularly known as 'quebra-pedras' in Brazil, are used in folk medicine for treating urinary infections and renal calculus. This paper reports an authenticity study, based on herbal drugs from Phyllanthus species, involving commercial and authentic samples using spectroscopic techniques: FT-IR, 1 H HR-MAS NMR and 1 H NMR in solution, combined with chemometric analysis. The spectroscopic techniques evaluated, coupled with chemometric methods, have great potential in the investigation of complex matrices. Furthermore, several metabolites were identified by the NMR techniques. (author)

Monitoring and Failure Analysis of Corroded Bridge Cables under Fatigue Loading Using Acoustic Emission Sensors

Directory of Open Access Journals (Sweden)

Hui Li

2012-03-01

Full Text Available Cables play an important role in cable-stayed systems, but are vulnerable to corrosion and fatigue damage. There is a dearth of studies on the fatigue damage evolution of corroded cable. In the present study, the acoustic emission (AE technology is adopted to monitor the fatigue damage evolution process. First, the relationship between stress and strain is determined through a tensile test for corroded and non-corroded steel wires. Results show that the mechanical performance of corroded cables is changed considerably. The AE characteristic parameters for fatigue damage are then established. AE energy cumulative parameters can accurately describe the fatigue damage evolution of corroded cables. The failure modes in each phase as well as the type of acoustic emission source are determined based on the results of scanning electron microscopy. The waveform characteristics, damage types, and frequency distribution of the corroded cable at different damage phases are collected. Finally, the number of broken wires and breakage time of the cables are determined according to the variation in the margin index.

Monitoring and Failure Analysis of Corroded Bridge Cables under Fatigue Loading Using Acoustic Emission Sensors

Science.gov (United States)

Li, Dongsheng; Ou, Jinping; Lan, Chengming; Li, Hui

2012-01-01

Cables play an important role in cable-stayed systems, but are vulnerable to corrosion and fatigue damage. There is a dearth of studies on the fatigue damage evolution of corroded cable. In the present study, the acoustic emission (AE) technology is adopted to monitor the fatigue damage evolution process. First, the relationship between stress and strain is determined through a tensile test for corroded and non-corroded steel wires. Results show that the mechanical performance of corroded cables is changed considerably. The AE characteristic parameters for fatigue damage are then established. AE energy cumulative parameters can accurately describe the fatigue damage evolution of corroded cables. The failure modes in each phase as well as the type of acoustic emission source are determined based on the results of scanning electron microscopy. The waveform characteristics, damage types, and frequency distribution of the corroded cable at different damage phases are collected. Finally, the number of broken wires and breakage time of the cables are determined according to the variation in the margin index. PMID:22666009

Multivariate data analysis as a tool in advanced quality monitoring in the food production chain

DEFF Research Database (Denmark)

Bro, R.; van den Berg, F.; Thybo, A.

2002-01-01

This paper summarizes some recent advances in mathematical modeling of relevance in advanced quality monitoring in the food production chain. Using chemometrics-multivariate data analysis - it is illustrated how to tackle problems in food science more efficiently and, moreover, solve problems...

Mobile acoustic transects miss rare bat species: implications of survey method and spatio-temporal sampling for monitoring bats

Directory of Open Access Journals (Sweden)

Elizabeth C. Braun de Torrez

2017-11-01

Full Text Available Due to increasing threats facing bats, long-term monitoring protocols are needed to inform conservation strategies. Effective monitoring should be easily repeatable while capturing spatio-temporal variation. Mobile acoustic driving transect surveys (‘mobile transects’ have been touted as a robust, cost-effective method to monitor bats; however, it is not clear how well mobile transects represent dynamic bat communities, especially when used as the sole survey approach. To assist biologists who must select a single survey method due to resource limitations, we assessed the effectiveness of three acoustic survey methods at detecting species richness in a vast protected area (Everglades National Park: (1 mobile transects, (2 stationary surveys that were strategically located by sources of open water and (3 stationary surveys that were replicated spatially across the landscape. We found that mobile transects underrepresented bat species richness compared to stationary surveys across all major vegetation communities and in two distinct seasons (dry/cool and wet/warm. Most critically, mobile transects failed to detect three rare bat species, one of which is federally endangered. Spatially replicated stationary surveys did not estimate higher species richness than strategically located stationary surveys, but increased the rate at which species were detected in one vegetation community. The survey strategy that detected maximum species richness and the highest mean nightly species richness with minimal effort was a strategically located stationary detector in each of two major vegetation communities during the wet/warm season.

Mobile acoustic transects miss rare bat species: implications of survey method and spatio-temporal sampling for monitoring bats.

Science.gov (United States)

Braun de Torrez, Elizabeth C; Wallrichs, Megan A; Ober, Holly K; McCleery, Robert A

2017-01-01

Due to increasing threats facing bats, long-term monitoring protocols are needed to inform conservation strategies. Effective monitoring should be easily repeatable while capturing spatio-temporal variation. Mobile acoustic driving transect surveys ('mobile transects') have been touted as a robust, cost-effective method to monitor bats; however, it is not clear how well mobile transects represent dynamic bat communities, especially when used as the sole survey approach. To assist biologists who must select a single survey method due to resource limitations, we assessed the effectiveness of three acoustic survey methods at detecting species richness in a vast protected area (Everglades National Park): (1) mobile transects, (2) stationary surveys that were strategically located by sources of open water and (3) stationary surveys that were replicated spatially across the landscape. We found that mobile transects underrepresented bat species richness compared to stationary surveys across all major vegetation communities and in two distinct seasons (dry/cool and wet/warm). Most critically, mobile transects failed to detect three rare bat species, one of which is federally endangered. Spatially replicated stationary surveys did not estimate higher species richness than strategically located stationary surveys, but increased the rate at which species were detected in one vegetation community. The survey strategy that detected maximum species richness and the highest mean nightly species richness with minimal effort was a strategically located stationary detector in each of two major vegetation communities during the wet/warm season.

Acoustically assisted diffusion through membranes and biomaterials

International Nuclear Information System (INIS)

Floros, J.D.; Liang, H.

1994-01-01

Part of a special section on the symposium ''Ultrasonic Applications in the Food Industry.'' The use of high-intensity ultrasound in food processing is reviewed. Acoustic radiation, or sound, can be used to monitor various operations or products or to alter a process or product; however, the direct use of sound to improve food processes is not very popular. High-intensity acoustic radiation induces various changes as it passes through a medium, largely as a result of heating, cavitation, agitation and shear stresses, compression and rarefaction, and turbulence. The diffusion of sound through a medium is influenced by factors such as the temperature, acoustic intensity, acoustic frequency, direction of the acoustic wave, pulsation of the acoustic wave, and properties of the medium. Some potential applications of acoustic energy in food processes are increased drying efficiency, acceleration of diffusion through polymeric and biological membranes, and enhanced diffusion through porous materials

Early corrosion monitoring of prestressed concrete piles using acoustic emission

Science.gov (United States)

Vélez, William; Matta, Fabio; Ziehl, Paul H.

2013-04-01

The depassivation and corrosion of bonded prestressing steel strands in concrete bridge members may lead to major damage or collapse before visual inspections uncover evident signs of damage, and well before the end of the design life. Recognizing corrosion in its early stage is desirable to plan and prioritize remediation strategies. The Acoustic Emission (AE) technique is a rational means to develop structural health monitoring and prognosis systems for the early detection and location of corrosion in concrete. Compelling features are the sensitivity to events related to micro- and macrodamage, non-intrusiveness, and suitability for remote and wireless applications. There is little understanding of the correlation between AE and the morphology and extent of early damage on the steel surface. In this paper, the evidence collected from prestressed concrete (PC) specimens that are exposed to salt water is discussed vis-à-vis AE data from continuous monitoring. The specimens consist of PC strips that are subjected to wet/dry salt water cycles, representing portions of bridge piles that are exposed to tidal action. Evidence collected from the specimens includes: (a) values of half-cell potential and linear polarization resistance to recognize active corrosion in its early stage; and (b) scanning electron microscopy micrographs of steel areas from two specimens that were decommissioned once the electrochemical measurements indicated a high probability of active corrosion. These results are used to evaluate the AE activity resulting from early corrosion.

HR-MAS NMR allied to chemometric on Hancornia speciosa varieties differentiation

Energy Technology Data Exchange (ETDEWEB)

Flores, Igor S. [Instituto Federal de Goiás (IFG), Luziânia, GO (Brazil); Silva, Andressa K.; Chaves, Lazaro J.; Collevatti, Rosane G.; Lião, Luciano M., E-mail: lucianoliao@ufg.br [Universidade Federal de Goiás (UFG), Goiânia, GO (Brazil); Furquim, Leonnardo C. [Faculdade Objetivo, GO (Brazil); Castro, Carlos F.S. [Instituto Federal de Educação, Ciência e Tecnologia Goiano (IFGoiano), GO (Brazil)

2018-05-01

This work describes the potential of chemometric analyses applied to {sup 1}H high-resolution magic angle spinning nuclear magnetic resonance ({sup 1}H HR-MAS NMR) data for the chemotaxonomic investigation of Hancornia speciosa (Apocynaceae) varieties. This plant, popularly known as mangaba, has a complex morphological differentiation and thus chemical analyses can be used for their taxonomic classification. In comparison to traditional techniques, {sup 1}H HR-MAS NMR allied with chemometrics provided a simple and low cost method for chemotaxonomy. Leaves of four varieties of H. speciosa from a common garden experiment was studied and demonstrated that H. speciosa var. speciosa differs from others due to its specific metabolic profile, and var. pubescens was discriminated based on its high phenolic compound content. The distinction between the latter variety and gardineri is important once it allows for the selection of samples with greater commercial value, once they produce the largest and heaviest fruits. (author)

Considerations for acoustic emission monitoring of spherical Kevlar/epoxy composite pressure vessels

Science.gov (United States)

Hamstad, M. A.; Patterson, R. G.

1977-01-01

We are continuing to research the applications of acoustic emission testing for predicting burst pressure of filament-wound Kevlar 49/epoxy pressure vessels. This study has focused on three specific areas. The first area involves development of an experimental technique and the proper instrumentation to measure the energy given off by the acoustic emission transducer per acoustic emission burst. The second area concerns the design of a test fixture in which to mount the composite vessel so that the acoustic emission transducers are held against the outer surface of the composite. Included in this study area is the calibration of the entire test setup including couplant, transducer, electronics, and the instrument measuring the energy per burst. In the third and final area of this study, we consider the number, location, and sensitivity of the acoustic emission transducers used for proof testing composite pressure vessels.

Assessment of genetically modified soybean crops and different cultivars by Fourier transform infrared spectroscopy and chemometric analysis

Directory of Open Access Journals (Sweden)

Glaucia Braz Alcantara

2010-06-01

Full Text Available This paper describes the potentiality of Fourier transform infrared (FT-IR spectroscopy associated to chemometric analysis for assessment of conventional and genetically modified soybean crops. Recently, genetically modified organisms have been queried about their influence on the environment and their safety as food/feed. In this regard, chemical investigations are ever more required. Thus three different soybean cultivars distributed in transgenic Roundup ReadyTM soybean and theirs conventional counterparts were directly investigated by FT-IR spectroscopy and chemometric analysis. The application of PCA and KNN methods permitted the discrimination and classification of the genetically modified samples from conventional ones when they were separately analysed. The analyses showed the chemical variation according to genetic modification. Furthermore, this methodology was efficient for cultivar grouping and highlights cultivar dependence for discrimination between transgenic and non-transgenic samples. According to this study, FT-IR and chemometrics could be used as a quick, easy and low cost tool to assess the chemical composition variation in genetically modified organisms.

A Permanent Automated Real-Time Passive Acoustic Monitoring System for Bottlenose Dolphin Conservation in the Mediterranean Sea.

Directory of Open Access Journals (Sweden)

Marco Brunoldi

Full Text Available Within the framework of the EU Life+ project named LIFE09 NAT/IT/000190 ARION, a permanent automated real-time passive acoustic monitoring system for the improvement of the conservation status of the transient and resident population of bottlenose dolphin (Tursiops truncatus has been implemented and installed in the Portofino Marine Protected Area (MPA, Ligurian Sea. The system is able to detect the simultaneous presence of dolphins and boats in the area and to give their position in real time. This information is used to prevent collisions by diffusing warning messages to all the categories involved (tourists, professional fishermen and so on. The system consists of two gps-synchronized acoustic units, based on a particular type of marine buoy (elastic beacon, deployed about 1 km off the Portofino headland. Each one is equipped with a four-hydrophone array and an onboard acquisition system which can record the typical social communication whistles emitted by the dolphins and the sound emitted by boat engines. Signals are pre-filtered, digitized and then broadcast to the ground station via wi-fi. The raw data are elaborated to get the direction of the acoustic target to each unit, and hence the position of dolphins and boats in real time by triangulation.

Detecting and identifying damage in sandwich polymer composite by using acoustic emission

Energy Technology Data Exchange (ETDEWEB)

McGugan, M.; Soerensen, Bent F.; Oestergaard, R.; Bech, T.

2006-12-15

Acoustic emission is a useful monitoring tool for extracting extra information during mechanical testing of polymer composite sandwich materials. The study of fracture mechanics within test specimens extracted from wind turbine blade material is presented. The contribution of the acoustic emission monitoring technique in defining different failure modes identified during the testing is discussed. The development of in-situ structural monitoring and control systems is considered. (au)

A case study of real-time monitoring of solid-state phase transformations in acoustically levitated particles using near infrared and Raman spectroscopy.

Science.gov (United States)

Rehder, Sönke; Wu, Jian X; Laackmann, Julian; Moritz, Hans-Ulrich; Rantanen, Jukka; Rades, Thomas; Leopold, Claudia S

2013-01-23

The objective of this study was to monitor the amorphous-to-crystalline solid-state phase transformation kinetics of the model drug ibuprofen with spectroscopic methods during acoustic levitation. Chemical and physical information was obtained by real-time near infrared (NIRS) and Raman spectroscopy measurements. The recrystallisation kinetic parameters (overall recrystallisation rate constant β and the time needed to reach 50% of the equilibrated level t(50)), were determined using a multivariate curve resolution approach. The acoustic levitation device coupled with non-invasive spectroscopy enabled monitoring of the recrystallisation process of the difficult-to-handle (adhesive) amorphous sample. The application of multivariate curve resolution enabled isolation of the underlying pure spectra, which corresponded well with the reference spectra of amorphous and crystalline ibuprofen. The recrystallisation kinetic parameters were estimated from the recrystallisation profiles. While the empirical recrystallisation rate constant determined by NIR and Raman spectroscopy were comparable, the lag time for recrystallisation was significantly lower with Raman spectroscopy as compared to NIRS. This observation was explained by the high energy density of the Raman laser beam, which might have led to local heating effects of the sample and thus reduced the recrystallisation onset time. It was concluded that acoustic levitation with NIR and Raman spectroscopy combined with multivariate curve resolution allowed direct determination of the recrystallisation kinetics of amorphous drugs and thus is a promising technique for monitoring solid-state phase transformations of adhesive small-sized samples during the early phase of drug development. Copyright © 2012 Elsevier B.V. All rights reserved.

The application of acoustic emission measurements on laboratory testpieces to large scale pressure vessel monitoring

International Nuclear Information System (INIS)

Ingham, T.; Dawson, D.G.

1975-01-01

A test pressure vessel containing 4 artificial defects was monitored for emission whilst pressure cycling to failure. Testpieces cut from both the failed vessel and from as-rolled plate material were tested in the laboratory. A marked difference in emission characteristics was observed between plate and vessel testpieces. Activity from vessel material was virtually constant after general yield and emission amplitudes were low. Plate testpieces showed maximum activity at general yield and more frequent high amplitude emissions. An attempt has been made to compare the system sensitivities between the pressure vessel test and laboratory tests. In the absence of an absolute calibration device, system sensitivities were estimated using dummy signals generated by the excitation of an emission sensor. The measurements have shown an overall difference in sensitivity between vessel and laboratory tests of approximately 25db. The reduced sensitivity in the vessel test is attributed to a combination of differences in sensors, acoustic couplant, attenuation, and dispersion relative to laboratory tests and the relative significance of these factors is discussed. Signal amplitude analysis of the emissions monitored from laboratory testpieces showed that, whith losses of the order of 25 to 30db, few emissions would be detected from the pressure vessel test. It is concluded that no reliable prediction of acoustic behaviour of a structure may be made from laboratory test unless testpieces of the actual structural material are used. A considerable improvement in detection sensitivity, is also required for reliable detection of defects in low strength ductile materials and an absolute method of system calibration is required between tests

The dimerization study of some cationic monomethine cyanine dyes by chemometrics method

Czech Academy of Sciences Publication Activity Database

Ahmadi, S.; Deligeorgiev, T.G.; Vasilev, A.; Kubista, Mikael

2012-01-01

Roč. 86, č. 13 (2012), s. 1974-1981 ISSN 0036-0244 Institutional research plan: CEZ:AV0Z50520701 Keywords : dimerization * chemometrics * UV-vis spectroscopy * monomethine cyanine dyes Subject RIV: CF - Physical ; Theoretical Chemistry Impact factor: 0.386, year: 2012

A Simple Photometer and Chemometrics Analysis for Quality Control of Sambiloto (Andrographis paniculata Raw Material

Directory of Open Access Journals (Sweden)

Rudi Heryanto

2017-09-01

Full Text Available In this paper, we described the use of a light emitting diode (LED-based photometer and chemometric analysis for quality control of king of bitter or sambiloto (Andrographis paniculata raw material. The quality of medicinal plants is determined by their chemical composition. The quantities of chemical components in medicinal plants can be assessed using spectroscopic technique. We used an “in house” photometer to generate spectra of sambiloto. The spectra were analyzed by chemometric methods, i.e. principal component analysis (PCA and partial least square discriminant analysis (PLS-DA, with the aim of herbal quality classification based on the harvesting time. From the results obtained, based on thin layer chromatography analysis, sambiloto with different collection times (1, 2, and 3 months contained different amounts of active compounds. Evaluation of sambiloto, using its spectra and chemometric analysis has successfully differentiated its quality based on harvesting time. PCA with the first two PC’s (PC-1 = 60% and PC-2 = 35% was able to differentiate according to the harvesting time of sambiloto. Three models were obtained by PLS-DA and could be used to predict unknown sample of sambiloto according to the harvesting time

An introduction to acoustic emission technology for in-process inspection of welds

International Nuclear Information System (INIS)

Goswami, G.L.

1983-01-01

Weld quality monitoring, as it stands today, is primarily done by X-ray radiography and ultrasonic testing which is applied after welding is complete. Acoustic Emission Technique (AET) also presents a possible substitute for weld quality monitoring which can be used during welding. Acoustic signals are generated during welding and the sound waves of weld defects are picked up by using AE sensors. With the introduction of sophisticated instrumentation in AET, it is possible to carry out the test even in noisy shop floor environments. Large number of reports on the subject of acoustic emission in recent years is a clear indication that it is gaining importance in welding industry. The present day status of the acoustic emission technology as an on-line weld quality monitoring technique has been reviewed. This report discusses the technique and system along with the acoustic emission parameters important for weld quality analysis. This also deals with the application of this technique in different welding processes like TIG, resistance, electro slag and submerged arc. It has been reported that monitoring of emission during welding can detect crack formation, crack growth and lack of fusion precisely. Static defects like porosity and inclusion do not generate very strong acoustic signals and are therefore difficult to intercept, but, however, lately they have detected successfully. (author)

Do they stay or do they go? Acoustic monitoring of whale sharks at Ningaloo Marine Park, Western Australia.

Science.gov (United States)

Norman, B M; Whitty, J M; Beatty, S J; Reynolds, S D; Morgan, D L

2017-12-01

Whale sharks Rhincodon typus were monitored via acoustic transmitters at the northern end of Western Australia's Ningaloo Marine Park to establish the extent to which the species inhabits the region beyond the whale-shark ecotourism industry season, which usually extends from March to August in each year. Despite the vast majority (c. 98%) of photographic submissions of R. typus from Ningaloo Reef being between March and August, acoustic detections from the tagged R. typus at Ningaloo were recorded in all months of the year, but do not preclude the occurrence of extended absences. It is concluded that as a species, R. typus occurs year round at Ningaloo, where it generally remains in close proximity to the reef edge, but that some individuals move outside of the detection range of the array for extended periods. © 2017 The Fisheries Society of the British Isles.

Authenticity study of Phyllanthus species by NMR and FT-IR techniques coupled with chemometric methods

Energy Technology Data Exchange (ETDEWEB)

Santos, Maiara S.; Pereira-Filho, Edenir R.; Ferreira, Antonio G. [Universidade Federal de Sao Carlos (UFSCAR), SP (Brazil). Dept. de Quimica; Boffo, Elisangela F. [Universidade Federal da Bahia (UFBA), Salvador, BA (Brazil). Inst. de Quimica; Figueira, Glyn M., E-mail: maiarassantos@yahoo.com.br [Universidade Estadual de Campinas (UNICAMP), Campinas, SP (Brazil). Centro Pluridisciplinar de Pesquisas Quimicas, Biologicas e Agricolas

2012-07-01

The importance of medicinal plants and their use in industrial applications is increasing worldwide, especially in Brazil. Phyllanthus species, popularly known as 'quebra-pedras' in Brazil, are used in folk medicine for treating urinary infections and renal calculus. This paper reports an authenticity study, based on herbal drugs from Phyllanthus species, involving commercial and authentic samples using spectroscopic techniques: FT-IR, {sup 1}H HR-MAS NMR and {sup 1}H NMR in solution, combined with chemometric analysis. The spectroscopic techniques evaluated, coupled with chemometric methods, have great potential in the investigation of complex matrices. Furthermore, several metabolites were identified by the NMR techniques. (author)

Grape juice quality control by means of {sup 1}H NMR spectroscopy and chemometric analyses

Energy Technology Data Exchange (ETDEWEB)

Grandizoli, Caroline Werner Pereira da Silva; Campos, Francinete Ramos; Simonelli, Fabio; Barison, Andersson [Universidade Federal do Paraná (UFPR), Curitiba (Brazil). Departamento de Química

2014-07-01

This work shows the application of {sup 1}H NMR spectroscopy and chemometrics for quality control of grape juice. A wide range of quality assurance parameters were assessed by single {sup 1}H NMR experiments acquired directly from juice. The investigation revealed that conditions and time of storage should be revised and indicated on all labels. The sterilization process of homemade grape juices was efficient, making it possible to store them for long periods without additives. Furthermore, chemometric analysis classified the best commercial grape juices to be similar to homemade grape juices, indicating that this approach can be used to determine the authenticity after adulteration. (author)

Authenticity study of Phyllanthus species by NMR and FT-IR Techniques coupled with chemometric methods

Directory of Open Access Journals (Sweden)

Maiara S. Santos

2012-01-01

Full Text Available The importance of medicinal plants and their use in industrial applications is increasing worldwide, especially in Brazil. Phyllanthus species, popularly known as "quebra-pedras" in Brazil, are used in folk medicine for treating urinary infections and renal calculus. This paper reports an authenticity study, based on herbal drugs from Phyllanthus species, involving commercial and authentic samples using spectroscopic techniques: FT-IR, ¹H HR-MAS NMR and ¹H NMR in solution, combined with chemometric analysis. The spectroscopic techniques evaluated, coupled with chemometric methods, have great potential in the investigation of complex matrices. Furthermore, several metabolites were identified by the NMR techniques.

Authenticity study of Phyllanthus species by NMR and FT-IR techniques coupled with chemometric methods

Energy Technology Data Exchange (ETDEWEB)

Santos, Maiara S.; Pereira-Filho, Edenir R.; Ferreira, Antonio G. [Universidade Federal de Sao Carlos (UFSCAR), SP (Brazil). Dept. de Quimica; Boffo, Elisangela F. [Universidade Federal da Bahia (UFBA), Salvador, BA (Brazil). Inst. de Quimica; Figueira, Glyn M., E-mail: maiarassantos@yahoo.com.br [Universidade Estadual de Campinas (UNICAMP), Campinas, SP (Brazil). Centro Pluridisciplinar de Pesquisas Quimicas, Biologicas e Agricolas

2012-07-01

The importance of medicinal plants and their use in industrial applications is increasing worldwide, especially in Brazil. Phyllanthus species, popularly known as 'quebra-pedras' in Brazil, are used in folk medicine for treating urinary infections and renal calculus. This paper reports an authenticity study, based on herbal drugs from Phyllanthus species, involving commercial and authentic samples using spectroscopic techniques: FT-IR, {sup 1}H HR-MAS NMR and {sup 1}H NMR in solution, combined with chemometric analysis. The spectroscopic techniques evaluated, coupled with chemometric methods, have great potential in the investigation of complex matrices. Furthermore, several metabolites were identified by the NMR techniques. (author)

Passive acoustic monitoring to detect spawning in large-bodied catostomids

Science.gov (United States)

Straight, Carrie A.; Freeman, Byron J.; Freeman, Mary C.

2014-01-01

Documenting timing, locations, and intensity of spawning can provide valuable information for conservation and management of imperiled fishes. However, deep, turbid or turbulent water, or occurrence of spawning at night, can severely limit direct observations. We have developed and tested the use of passive acoustics to detect distinctive acoustic signatures associated with spawning events of two large-bodied catostomid species (River Redhorse Moxostoma carinatum and Robust Redhorse Moxostoma robustum) in river systems in north Georgia. We deployed a hydrophone with a recording unit at four different locations on four different dates when we could both record and observe spawning activity. Recordings captured 494 spawning events that we acoustically characterized using dominant frequency, 95% frequency, relative power, and duration. We similarly characterized 46 randomly selected ambient river noises. Dominant frequency did not differ between redhorse species and ranged from 172.3 to 14,987.1 Hz. Duration of spawning events ranged from 0.65 to 11.07 s, River Redhorse having longer durations than Robust Redhorse. Observed spawning events had significantly higher dominant and 95% frequencies than ambient river noises. We additionally tested software designed to automate acoustic detection. The automated detection configurations correctly identified 80–82% of known spawning events, and falsely indentified spawns 6–7% of the time when none occurred. These rates were combined over all recordings; rates were more variable among individual recordings. Longer spawning events were more likely to be detected. Combined with sufficient visual observations to ascertain species identities and to estimate detection error rates, passive acoustic recording provides a useful tool to study spawning frequency of large-bodied fishes that displace gravel during egg deposition, including several species of imperiled catostomids.

Chemometrics applications in biotechnology processes: predicting column integrity and impurity clearance during reuse of chromatography resin.

Science.gov (United States)

Rathore, Anurag S; Mittal, Shachi; Lute, Scott; Brorson, Kurt

2012-01-01

Separation media, in particular chromatography media, is typically one of the major contributors to the cost of goods for production of a biotechnology therapeutic. To be cost-effective, it is industry practice that media be reused over several cycles before being discarded. The traditional approach for estimating the number of cycles a particular media can be reused for involves performing laboratory scale experiments that monitor column performance and carryover. This dataset is then used to predict the number of cycles the media can be used at manufacturing scale (concurrent validation). Although, well accepted and widely practiced, there are challenges associated with extrapolating the laboratory scale data to manufacturing scale due to differences that may exist across scales. Factors that may be different include: level of impurities in the feed material, lot to lot variability in feedstock impurities, design of the column housing unit with respect to cleanability, and homogeneity of the column packing. In view of these challenges, there is a need for approaches that may be able to predict column underperformance at the manufacturing scale over the product lifecycle. In case such an underperformance is predicted, the operators can unpack and repack the chromatography column beforehand and thus avoid batch loss. Chemometrics offers one such solution. In this article, we present an application of chemometrics toward the analysis of a set of chromatography profiles with the intention of predicting the various events of column underperformance including the backpressure buildup and inefficient deoxyribonucleic acid clearance. Copyright © 2012 American Institute of Chemical Engineers (AIChE).

Aespoe Pillar Stability Experiment. Acoustic emission and ultrasonic monitoring

Energy Technology Data Exchange (ETDEWEB)

Haycox, Jon; Pettitt, Will; Young, R. Paul [Applied Seismology Consultants Ltd., Shrewsbury (United Kingdom)

2005-12-15

This report describes the results from acoustic emission (AE) and ultrasonic monitoring of the Aespoe Pillar Stability Experiment (APSE) at SKB's Hard Rock Laboratory (HRL), Sweden. The APSE is being undertaken to demonstrate the current capability to predict spalling in a fractured rock mass using numerical modelling techniques, and to demonstrate the effect of backfill and confining pressure on the propagation of micro-cracks in rock adjacent to deposition holes within a repository. An ultrasonic acquisition system has provided acoustic emission and ultrasonic survey monitoring throughout the various phases of the experiment. Results from the entire data set are provided with this document so that they can be effectively compared to several numerical modelling studies, and to mechanical and thermal measurements conducted around the pillar volume, in an 'integrated analysis' performed by SKB staff. This document provides an in-depth summary of the AE and ultrasonic survey results for future reference. The pillar has been produced by excavating two 1.8 m diameter deposition holes 1 m apart. These were bored in 0.8 m steps using a Tunnel Boring Machine specially adapted for vertical drilling. The first deposition hole was drilled in December 2003. Preceding this a period of background monitoring was performed so as to obtain a datum for the results. The hole was then confined to 0.7 MPa internal over pressure using a specially designed water-filled bladder. The second deposition hole was excavated in March 2004. Heating of the pillar was performed over a two month period between ending in July 2004, when the confined deposition hole was slowly depressurised. Immediately after depressurisation the pillar was allowed to cool with cessation of monitoring occurring a month later. A total of 36,676 AE triggers were recorded over the reporting period between 13th October 2003 and 14th July 2004. Of these 15,198 have produced AE locations. The AE data set

Aespoe Pillar Stability Experiment. Acoustic emission and ultrasonic monitoring

International Nuclear Information System (INIS)

Haycox, Jon; Pettitt, Will; Young, R. Paul

2005-11-01

This report describes the results from acoustic emission (AE) and ultrasonic monitoring of the Aespoe Pillar Stability Experiment (APSE) at SKB's Hard Rock Laboratory (HRL), Sweden. The APSE is being undertaken to demonstrate the current capability to predict spalling in a fractured rock mass using numerical modelling techniques, and to demonstrate the effect of backfill and confining pressure on the propagation of micro-cracks in rock adjacent to deposition holes within a repository. An ultrasonic acquisition system has provided acoustic emission and ultrasonic survey monitoring throughout the various phases of the experiment. Results from the entire data set are provided with this document so that they can be effectively compared to several numerical modelling studies, and to mechanical and thermal measurements conducted around the pillar volume, in an 'integrated analysis' performed by SKB staff. This document provides an in-depth summary of the AE and ultrasonic survey results for future reference. The pillar has been produced by excavating two 1.8 m diameter deposition holes 1 m apart. These were bored in 0.8 m steps using a Tunnel Boring Machine specially adapted for vertical drilling. The first deposition hole was drilled in December 2003. Preceding this a period of background monitoring was performed so as to obtain a datum for the results. The hole was then confined to 0.7 MPa internal over pressure using a specially designed water-filled bladder. The second deposition hole was excavated in March 2004. Heating of the pillar was performed over a two month period between ending in July 2004, when the confined deposition hole was slowly depressurised. Immediately after depressurisation the pillar was allowed to cool with cessation of monitoring occurring a month later. A total of 36,676 AE triggers were recorded over the reporting period between 13th October 2003 and 14th July 2004. Of these 15,198 have produced AE locations. The AE data set shows an intense

Detection method of internal leakage from valve using acoustic method

International Nuclear Information System (INIS)

Kumagai, Hiromichi; Kitajima, Akira; Suzuki, Akio.

1990-01-01

The objective of this study is to estimate the feasibility of the acoustic method for the internal leakage from the valves in power plants. From the experimental results, it was suggested that the acoustic method for the monitoring of leakage was feasible. When the background levels are higher than the acoustic signals from leakage, we can detect the leakage analyzing the spectrum of the remainders which take the background noise from the acoustic signals. (author)

Acoustic telemetry validates a citizen science approach for monitoring sharks on coral reefs.

Science.gov (United States)

Vianna, Gabriel M S; Meekan, Mark G; Bornovski, Tova H; Meeuwig, Jessica J

2014-01-01

Citizen science is promoted as a simple and cost-effective alternative to traditional approaches for the monitoring of populations of marine megafauna. However, the reliability of datasets collected by these initiatives often remains poorly quantified. We compared datasets of shark counts collected by professional dive guides with acoustic telemetry data from tagged sharks collected at the same coral reef sites over a period of five years. There was a strong correlation between the number of grey reef sharks (Carcharhinus amblyrhynchos) observed by dive guides and the telemetry data at both daily and monthly intervals, suggesting that variation in relative abundance of sharks was detectable in datasets collected by dive guides in a similar manner to data derived from telemetry at these time scales. There was no correlation between the number or mean depth of sharks recorded by telemetry and the presence of tourist divers, suggesting that the behaviour of sharks was not affected by the presence of divers during our study. Data recorded by dive guides showed that current strength and temperature were important drivers of the relative abundance of sharks at monitored sites. Our study validates the use of datasets of shark abundance collected by professional dive guides in frequently-visited dive sites in Palau, and supports the participation of experienced recreational divers as contributors to long-term monitoring programs of shark populations.

Critical heat flux acoustic detection: Methods and application to ITER divertor vertical target monitoring

Energy Technology Data Exchange (ETDEWEB)

Courtois, X., E-mail: xavier.courtois@cea.fr [CEA, IRFM, F-13108 Saint-Paul-Lez-Durance (France); Escourbiac, F. [ITER Organization, Route de Vinon sur Verdon, F-13115 Saint-Paul-Lez-Durance (France); Richou, M.; Cantone, V. [CEA, IRFM, F-13108 Saint-Paul-Lez-Durance (France); Constans, S. [AREVA-NP, Le Creusot (France)

2013-10-15

Actively cooled plasma facing components (PFCs) have to exhaust high heat fluxes from plasma radiation and plasma–wall interaction. Critical heat flux (CHF) event may occur in the cooling channel due to unexpected heat loading or operational conditions, and has to be detected as soon as possible. Therefore it is essential to develop means of monitoring based on precursory signals providing an early detection of this destructive phenomenon, in order to be able to stop operation before irremediable damages appear. Capabilities of CHF early detection based on acoustic techniques on PFC mock-ups cooled by pressurised water were already demonstrated. This paper addresses the problem of the detection in case of flow rate reduction and of flow dilution resulting from multiple plasma facing units (PFU) which are hydraulically connected in parallel, which is the case of ITER divertor. An experimental study is launched on a dedicated mock-up submitted to heat loads up to the CHF. It shows that the measurement of the acoustic waves, generated by the cooling phenomena, allows the CHF detection in conditions similar to that of the ITER divertor, with a reasonable number of sensors. The paper describes the mock-ups and the tests sequences, and comments the results.

Stargate-based Acoustic Sensor Platform

OpenAIRE

Hanbiao Wang; Kung Yao; Deborah Estrin

2004-01-01

To facilitate the study of the wireless sensor network for demanding acoustic monitoring of long distance sources, we recently have also started working on the development of a new generation of wireless acoustic sensor network platform using the Stargate nodes. The 400 MHz PXA-255 XScale processor and the 64 MB SDRAM provide the Stargate platform a decent processing capability. The VX Pocket 440 sound card with four external microphones are attached to each Stargate node through the PCMCIA s...

Feasibility of evaluating the integrity of FTR duct to end fixture welds using acoustic emission monitoring

International Nuclear Information System (INIS)

Trantow, R.L.

1975-11-01

A method of applying real-time acoustic emission (AE) source location to evaluate the integrity of duct-to-end fixture welds was developed and evaluated using the HEDL R8-4 AE monitor coupled with a PDP-8e minicomputer. Operational software was developed to control the system's data acquisition, storage, and display functions. Performance was evaluated on the basis of comparisons between AE source location data and subsequent destructive examination of six duct-to-transition ring qualification welds. Ten separate discontinuities seen in the metallography performed at 35 locations along these welds correlated with the averaged acoustic emission activity revealed by the AE source location maps. This relationship is not presently considered to be usable as a system calibration method however, because of the limited range of discontinuity lengths (from 0.0003 to 0.004 in. long) that were correlated. The presence of six other discontinuities, found in regions showing low levels of emission activity, indicated that significant stress risers can go undetected under the conditions investigated

Casa Grande Ruins National Monument acoustical monitoring 2010

Science.gov (United States)

2014-11-01

During September 2010, The Volpe Center collected baseline acoustical data at Casa Grande National Monument (CAGR), at one site for 28 days. The baseline data collected during this period will help park managers and planners estimate the effects of f...

Chemometric techniques in distribution, characterisation and source apportionment of polycyclic aromatic hydrocarbons (PAHS) in aquaculture sediments in Malaysia.

Science.gov (United States)

Retnam, Ananthy; Zakaria, Mohamad Pauzi; Juahir, Hafizan; Aris, Ahmad Zaharin; Zali, Munirah Abdul; Kasim, Mohd Fadhil

2013-04-15

This study investigated polycyclic aromatic hydrocarbons (PAHs) pollution in surface sediments within aquaculture areas in Peninsular Malaysia using chemometric techniques, forensics and univariate methods. The samples were analysed using soxhlet extraction, silica gel column clean-up and gas chromatography mass spectrometry. The total PAH concentrations ranged from 20 to 1841 ng/g with a mean of 363 ng/g dw. The application of chemometric techniques enabled clustering and discrimination of the aquaculture sediments into four groups according to the contamination levels. A combination of chemometric and molecular indices was used to identify the sources of PAHs, which could be attributed to vehicle emissions, oil combustion and biomass combustion. Source apportionment using absolute principle component scores-multiple linear regression showed that the main sources of PAHs are vehicle emissions 54%, oil 37% and biomass combustion 9%. Land-based pollution from vehicle emissions is the predominant contributor of PAHs in the aquaculture sediments of Peninsular Malaysia. Copyright © 2013 Elsevier Ltd. All rights reserved.

Field application of a multi-frequency acoustic instrument to monitor sediment for silt erosion study in Pelton turbine in Himalayan region, India

Science.gov (United States)

Rai, A. K.; Kumar, A.; Hies, T.; Nguyen, H. H.

2016-11-01

High sediment load passing through hydropower components erodes the hydraulic components resulting in loss of efficiency, interruptions in power production and downtime for repair/maintenance, especially in Himalayan regions. The size and concentration of sediment play a major role in silt erosion. The traditional process of collecting samples manually to analyse in laboratory cannot suffice the need of monitoring temporal variation in sediment properties. In this study, a multi-frequency acoustic instrument was applied at desilting chamber to monitor sediment size and concentration entering the turbine. The sediment size and concentration entering the turbine were also measured with manual samples collected twice daily. The samples collected manually were analysed in laboratory with a laser diffraction instrument for size and concentration apart from analysis by drying and filtering methods for concentration. A conductivity probe was used to calculate total dissolved solids, which was further used in results from drying method to calculate suspended solid content of the samples. The acoustic instrument was found to provide sediment concentration values similar to drying and filtering methods. However, no good match was found between mean grain size from the acoustic method with the current status of development and laser diffraction method in the first field application presented here. The future versions of the software and significant sensitivity improvements of the ultrasonic transducers are expected to increase the accuracy in the obtained results. As the instrument is able to capture the concentration and in the future most likely more accurate mean grain size of the suspended sediments, its application for monitoring silt erosion in hydropower plant shall be highly useful.

EZG08 project: acoustic experiments to monitor the EDZ during the gallery excavation process in the Mont Terri Underground Research Laboratory (Switzerland)

International Nuclear Information System (INIS)

Le Gonidec, Y.; Kergosien, B.; Schubnel, A.; Gueguen, Y.; Wassermann, J.; Gibert, D.; Sarout, J.; Nussbaum, C.

2010-01-01

Document available in extended abstract form only. In the Underground Research Laboratory (URL) at Mont Terri, a new gallery G08 was planned to be excavated in 2008 following an original process: the excavation process allowed to monitor the Excavation Damaged Zone (EDZ) from geophysical measurements designed and installed at the end of face of the EZ-G04 gallery during the excavation from the other side, i.e. the end face of the EZ-G08 gallery. The objectives of the project concern spatio-temporal changes of the EDZ: among the methodological developments adapted for the EZG08 project to provide complementary information, acoustic experiments have been prepared in horizontal boreholes to perform the continuous acoustic monitoring of the Excavation Damaged Zone (EDZ). The acoustic measurements, performed on acoustic arrays of several receivers, have been recorded during one month, following two main steps: - Active acoustic surveys: a source is introduced in a central borehole (BEZG5) allowing tomography experiments in the far field and in the near field, i.e. close to and far from BEZG5, respectively. - Acoustic emissions: during the excavation process, numerous acoustic emissions can be detected and associated to micro-seismic events due to rapid crack propagation, generated by the rock relaxation, or simply associated to the excavation process. From the tomography measurements, the acoustic wave velocity field can be estimated, with P and S-wave velocities roughly equal to 2500 m/s-3500 m/s, and 1500 m/s, respectively. The acoustic setup does not show variations of P-wave velocity during the campaign, but spatial variations which could be associated to anisotropic elastic properties of the rock with the maximum P-wave velocities close to the bedding plane. An original method based on a multifrequency approach puts in evidence a frequency dependence of the velocity, with a striking phenomena since the wave velocity decreases with increasing frequency. This effect

Chemometrics-assisted spectrophotometry method for the determination of chemical oxygen demand in pulping effluent.

Science.gov (United States)

Chen, Honglei; Chen, Yuancai; Zhan, Huaiyu; Fu, Shiyu

2011-04-01

A new method has been developed for the determination of chemical oxygen demand (COD) in pulping effluent using chemometrics-assisted spectrophotometry. Two calibration models were established by inducing UV-visible spectroscopy (model 1) and derivative spectroscopy (model 2), combined with the chemometrics software Smica-P. Correlation coefficients of the two models are 0.9954 (model 1) and 0.9963 (model 2) when COD of samples is in the range of 0 to 405 mg/L. Sensitivities of the two models are 0.0061 (model 1) and 0.0056 (model 2) and method detection limits are 2.02-2.45 mg/L (model 1) and 2.13-2.51 mg/L (model 2). Validation experiment showed that the average standard deviation of model 2 was 1.11 and that of model 1 was 1.54. Similarly, average relative error of model 2 (4.25%) was lower than model 1 (5.00%), which indicated that the predictability of model 2 was better than that of model 1. Chemometrics-assisted spectrophotometry method did not need chemical reagents and digestion which were required in the conventional methods, and the testing time of the new method was significantly shorter than the conventional ones. The proposed method can be used to measure COD in pulping effluent as an environmentally friendly approach with satisfactory results.

A new qualitative acoustic emission parameter based on Shannon's entropy for damage monitoring

Science.gov (United States)

Chai, Mengyu; Zhang, Zaoxiao; Duan, Quan

2018-02-01

An important objective of acoustic emission (AE) non-destructive monitoring is to accurately identify approaching critical damage and to avoid premature failure by means of the evolutions of AE parameters. One major drawback of most parameters such as count and rise time is that they are strongly dependent on the threshold and other settings employed in AE data acquisition system. This may hinder the correct reflection of original waveform generated from AE sources and consequently bring difficulty for the accurate identification of the critical damage and early failure. In this investigation, a new qualitative AE parameter based on Shannon's entropy, i.e. AE entropy is proposed for damage monitoring. Since it derives from the uncertainty of amplitude distribution of each AE waveform, it is independent of the threshold and other time-driven parameters and can characterize the original micro-structural deformations. Fatigue crack growth test on CrMoV steel and three point bending test on a ductile material are conducted to validate the feasibility and effectiveness of the proposed parameter. The results show that the new parameter, compared to AE amplitude, is more effective in discriminating the different damage stages and identifying the critical damage.

Multi-component determination and chemometric analysis of Paris polyphylla by ultra high performance liquid chromatography with photodiode array detection.

Science.gov (United States)

Chen, Pei; Jin, Hong-Yu; Sun, Lei; Ma, Shuang-Cheng

2016-09-01

Multi-source analysis of traditional Chinese medicine is key to ensuring its safety and efficacy. Compared with traditional experimental differentiation, chemometric analysis is a simpler strategy to identify traditional Chinese medicines. Multi-component analysis plays an increasingly vital role in the quality control of traditional Chinese medicines. A novel strategy, based on chemometric analysis and quantitative analysis of multiple components, was proposed to easily and effectively control the quality of traditional Chinese medicines such as Chonglou. Ultra high performance liquid chromatography was more convenient and efficient. Five species of Chonglou were distinguished by chemometric analysis and nine saponins, including Chonglou saponins I, II, V, VI, VII, D, and H, as well as dioscin and gracillin, were determined in 18 min. The method is feasible and credible, and enables to improve quality control of traditional Chinese medicines and natural products. © 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Acoustic Measurement Of Periodic Motion Of Levitated Object

Science.gov (United States)

Watkins, John L.; Barmatz, Martin B.

1992-01-01

Some internal vibrations, oscillations in position, and rotations of acoustically levitated object measured by use of microphone already installed in typical levitation chamber for tuning chamber to resonance and monitoring operation. Levitating acoustic signal modulated by object motion of lower frequency. Amplitude modulation detected and analyzed spectrally to determine amplitudes and frequencies of motions.

Acoustic emission experiments for PHWR technology development

International Nuclear Information System (INIS)

Pellionisz, P.; Jha, S.K.; Goswami, G.L.

1992-06-01

An Indian-Hungarian joint research project has been started with the aim of applying acoustic emission testing to solve specific problems of nuclear power plants. Acoustic emission measurement and analyzing instrumentation and software have been provided by the Hungarian side, while the measurements have been performed at the Bhabha Atomic Research Centre (BARC), India. The first task of the project was to check the capability of the method for leakage detection and shuttle movement monitoring of Pressurized Heavy Water Reactors (PHWR), and for monitoring manufacturing processes as laser welding. The preliminary measurements and results are presented. (R.P.) 15 refs.; 11 figs.; 3 tabs

Acoustical Detection Of Leakage In A Combustor

Science.gov (United States)

Puster, Richard L.; Petty, Jeffrey L.

1993-01-01

Abnormal combustion excites characteristic standing wave. Acoustical leak-detection system gives early warning of failure, enabling operating personnel to stop combustion process and repair spray bar before leak grows large enough to cause damage. Applicable to engines, gas turbines, furnaces, and other machines in which acoustic emissions at known frequencies signify onset of damage. Bearings in rotating machines monitored for emergence of characteristic frequencies shown in previous tests associated with incipient failure. Also possible to monitor for signs of trouble at multiple frequencies by feeding output of transducer simultaneously to multiple band-pass filters and associated circuitry, including separate trigger circuit set to appropriate level for each frequency.

UV-Vis spectroscopy with chemometric data treatment. An option for on-line control in nuclear industry

International Nuclear Information System (INIS)

Kirsanov, Dmitry; Legin, Andrey

2017-01-01

Chemometrics can be very useful for the classical field of UV-Vis determination of metals in aqueous solutions. A conventional approach consisting of using selective bands in a univariate mode is often not applicable to the real-world samples from e.g. hydrometallurgical processes, because of overlapping signals, light scattering on foreign particles, gas bubble formation, etc. And this is where chemometrics can do a good job. This paper overviews certain contributions to the field of multivariate data processing of UV-Vis spectra for seemingly simple case of metal detection in aqueous solutions. Special attention is given to applications in nuclear technology field. (author)

Acoustic emission evolution during sliding friction of Hadfield steel single crystal

Science.gov (United States)

Lychagin, D. V.; Novitskaya, O. S.; Kolubaev, A. V.; Sizova, O. V.

2017-12-01

Friction is a complex dynamic process. Direct observation of processes occurring in the friction zone is impossible due to a small size of a real contact area and, as a consequence, requires various additional methods applicable to monitor a tribological contact state. One of such methods consists in the analysis of acoustic emission data of a tribological contact. The use of acoustic emission entails the problem of interpreting physical sources of signals. In this paper, we analyze the evolution of acoustic emission signal frames in friction of Hadfield steel single crystals. The chosen crystallographic orientation of single crystals enables to identify four stages related to friction development as well as acoustic emission signals inherent in these stages. Acoustic emission signal parameters are studied in more detail by the short-time Fourier transform used to determine the time variation of the median frequency and its power spectrum. The results obtained will facilitate the development of a more precise method to monitor the tribological contact based on the acoustic emission method.

Discriminatory components retracing strategy for monitoring the preparation procedure of Chinese patent medicines by fingerprint and chemometric analysis.

Directory of Open Access Journals (Sweden)

Shuai Yao

Full Text Available Chinese patent medicines (CPM, generally prepared from several traditional Chinese medicines (TCMs in accordance with specific process, are the typical delivery form of TCMs in Asia. To date, quality control of CPMs has typically focused on the evaluation of the final products using fingerprint technique and multi-components quantification, but rarely on monitoring the whole preparation process, which was considered to be more important to ensure the quality of CPMs. In this study, a novel and effective strategy labeling "retracing" way based on HPLC fingerprint and chemometric analysis was proposed with Shenkang injection (SKI serving as an example to achieve the quality control of the whole preparation process. The chemical fingerprints were established initially and then analyzed by similarity, principal component analysis (PCA and partial least squares-discriminant analysis (PLS-DA to evaluate the quality and to explore discriminatory components. As a result, the holistic inconsistencies of ninety-three batches of SKIs were identified and five discriminatory components including emodic acid, gallic acid, caffeic acid, chrysophanol-O-glucoside, and p-coumaroyl-O-galloyl-glucose were labeled as the representative targets to explain the retracing strategy. Through analysis of the targets variation in the corresponding semi-products (ninety-three batches, intermediates (thirty-three batches, and the raw materials, successively, the origins of the discriminatory components were determined and some crucial influencing factors were proposed including the raw materials, the coextraction temperature, the sterilizing conditions, and so on. Meanwhile, a reference fingerprint was established and subsequently applied to the guidance of manufacturing. It was suggested that the production process should be standardized by taking the concentration of the discriminatory components as the diagnostic marker to ensure the stable and consistent quality for multi

Non-invasive acoustic-based monitoring of uranium in solution and H/D ratio

Energy Technology Data Exchange (ETDEWEB)

Pantea, Cristian [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Beedle, Christopher Craig [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Sinha, Dipen N. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Lakis, Rollin Evan [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

2017-08-01

The primary objective of this project is to adapt existing non-invasive acoustic techniques (Swept-Frequency Acoustic Interferometry and Gaussian-pulse acoustic technique) for the purpose of demonstrating the ability to quantify U or H/D ratios in solution. Furthermore, a successful demonstration will provide an easily implemented, low cost, and non-invasive method for remote and unattended uranium mass measurements for International Atomic Energy Agency (IAEA).

Comparative Study of Bio-implantable Acoustic Generator Architectures

International Nuclear Information System (INIS)

Christensen, D; Roundy, S

2013-01-01

This paper is a comparative study of the design spaces of two bio-implantable acoustically excited generator architectures: the thickness-stretch-mode circular piezoelectric plate and the bending-mode unimorph piezoelectric diaphragm. The generators are part of an acoustic power transfer system for implanted sensors and medical devices such as glucose monitors, metabolic monitors, drug delivery systems, etc. Our studies indicate that at small sizes the diaphragm architecture outperforms the plate architecture. This paper will present the results of simulation studies and initial experiments that explore the characteristics of the two architectures and compare their performance

Acoustic leak detection in nuclear power plants

International Nuclear Information System (INIS)

McElroy, J.W.

1986-01-01

For several years now, utilities have been utilizing acoustic leak detection methods as an operating tool in their nuclear power stations. The purpose for using the leak detection system at the various stations vary from safety, ALARA, improved operations, preventive maintenance, or increased plant availability. This paper describes the various acoustic techniques and their application. The techniques are divided into three categories: specific component leakage, intersystem leakage, and pipe through-wall crack leakage. The paper addresses each category in terms of motivation to monitor, method of application and operation, and benefits to be gained. Current requirements are reviewed and analyzed with respect to the acoustic techniques. The paper shows how acoustic leak detection is one of the most effective leak detection tools available. 9 figures, 1 table

Persistent Monitoring of Urban Infrasound Phenomenology. Report 1: Modeling an Urban Environment for Acoustical Analyses using the 3-D Finite-Difference Time-Domain Program PSTOP3D

Science.gov (United States)

2015-08-01

ER D C TR -1 5- 5 Remote Assessment of Critical Infrastructure Persistent Monitoring of Urban Infrasound Phenomenology Report 1...ERDC TR-15-5 August 2015 Persistent Monitoring of Urban Infrasound Phenomenology Report 1: Modeling an Urban Environment for Acoustical Analyses...Figure 5.1. Main spreadsheet containing problem setup. ..................................................................... 74 Figure 5.2. Definition

Dark Fiber and Distributed Acoustic Sensing: Applications to Monitoring Seismicity and Near-Surface Properties

Science.gov (United States)

Ajo Franklin, J. B.; Lindsey, N.; Dou, S.; Freifeld, B. M.; Daley, T. M.; Tracy, C.; Monga, I.

2017-12-01

"Dark Fiber" refers to the large number of fiber-optic lines installed for telecommunication purposes but not currently utilized. With the advent of distributed acoustic sensing (DAS), these unused fibers have the potential to become a seismic sensing network with unparalleled spatial extent and density with applications to monitoring both natural seismicity as well as near-surface soil properties. While the utility of DAS for seismic monitoring has now been conclusively shown on built-for-purpose networks, dark fiber deployments have been challenged by the heterogeneity of fiber installation procedures in telecommunication as well as access limitations. However, the potential of telecom networks to augment existing broadband monitoring stations provides a strong incentive to explore their utilization. We present preliminary results demonstrating the application of DAS to seismic monitoring on a 20 km run of "dark" telecommunications fiber between West Sacramento, CA and Woodland CA, part of the Dark Fiber Testbed maintained by the DOE's ESnet user facility. We show a small catalog of local and regional earthquakes detected by the array and evaluate fiber coupling by using variations in recorded frequency content. Considering the low density of broadband stations across much of the Sacramento Basin, such DAS recordings could provide a crucial data source to constrain small-magnitude local events. We also demonstrate the application of ambient noise interferometry using DAS-recorded waveforms to estimate soil properties under selected sections of the dark fiber transect; the success of this test suggests that the network could be utilized for environmental monitoring at the basin scale. The combination of these two examples demonstrates the exciting potential for combining DAS with ubiquitous dark fiber to greatly extend the reach of existing seismic monitoring networks.

Passive Acoustic Monitoring of the Environmental Impact of Oil Exploration on Marine Mammals in the Gulf of Mexico.

Science.gov (United States)

Sidorovskaia, Natalia A; Ackleh, Azmy S; Tiemann, Christopher O; Ma, Baoling; Ioup, Juliette W; Ioup, George E

2016-01-01

The Gulf of Mexico is a region densely populated by marine mammals that must adapt to living in a highly active industrial environment. This paper presents a new approach to quantifying the anthropogenic impact on the marine mammal population. The results for sperm and beaked whales of a case study of regional population dynamics trends after the Deepwater Horizon oil spill, derived from passive acoustic-monitoring data gathered before and after the spill in the vicinity of the accident, are presented.

Modified Acoustic Emission for Prognostic Health Monitoring, Phase II

Data.gov (United States)

National Aeronautics and Space Administration — Prime Photonics proposes to team with Dr. Duke of Virginia Tech to develop a multi-mode, enhanced piezoelectric acoustic emission sensing system to couple large...

Chemometric techniques in oil classification from oil spill fingerprinting.

Science.gov (United States)

Ismail, Azimah; Toriman, Mohd Ekhwan; Juahir, Hafizan; Kassim, Azlina Md; Zain, Sharifuddin Md; Ahmad, Wan Kamaruzaman Wan; Wong, Kok Fah; Retnam, Ananthy; Zali, Munirah Abdul; Mokhtar, Mazlin; Yusri, Mohd Ayub

2016-10-15

Extended use of GC-FID and GC-MS in oil spill fingerprinting and matching is significantly important for oil classification from the oil spill sources collected from various areas of Peninsular Malaysia and Sabah (East Malaysia). Oil spill fingerprinting from GC-FID and GC-MS coupled with chemometric techniques (discriminant analysis and principal component analysis) is used as a diagnostic tool to classify the types of oil polluting the water. Clustering and discrimination of oil spill compounds in the water from the actual site of oil spill events are divided into four groups viz. diesel, Heavy Fuel Oil (HFO), Mixture Oil containing Light Fuel Oil (MOLFO) and Waste Oil (WO) according to the similarity of their intrinsic chemical properties. Principal component analysis (PCA) demonstrates that diesel, HFO, MOLFO and WO are types of oil or oil products from complex oil mixtures with a total variance of 85.34% and are identified with various anthropogenic activities related to either intentional releasing of oil or accidental discharge of oil into the environment. Our results show that the use of chemometric techniques is significant in providing independent validation for classifying the types of spilled oil in the investigation of oil spill pollution in Malaysia. This, in consequence would result in cost and time saving in identification of the oil spill sources. Copyright © 2016. Published by Elsevier Ltd.

Fatigue damage monitoring for basalt fiber reinforced polymer composites using acoustic emission technique

Science.gov (United States)

Wang, Wentao; Li, Hui; Qu, Zhi

2012-04-01

Basalt fiber reinforced polymer (BFRP) is a structural material with superior mechanical properties. In this study, unidirectional BFRP laminates with 14 layers are made with the hand lay-up method. Then, the acoustic emission technique (AE) combined with the scanning electronic microscope (SEM) technique is employed to monitor the fatigue damage evolution of the BFRP plates in the fatigue loading tests. Time-frequency analysis using the wavelet transform technique is proposed to analyze the received AE signal instead of the peak frequency method. A comparison between AE signals and SEM images indicates that the multi-frequency peaks picked from the time-frequency curves of AE signals reflect the accumulated fatigue damage evolution and fatigue damage patterns. Furthermore, seven damage patterns, that is, matrix cracking, delamination, fiber fracture and their combinations, are identified from the time-frequency curves of the AE signals.

Exploitation of process knowledge for the monitoring and closed loop control of fermentation processes; Erschliessen von Prozesswissen fuer das Monitoring und die Regelung von Fermentationsprozessen

Energy Technology Data Exchange (ETDEWEB)

Grote, Bianca; Hitzmann, Bernd [Hohenheim Univ., Stuttgart (Germany). FG Prozessanalytik und Getreidetechnologie; John, Jinu Mulamoottil

2011-07-01

The significance of process knowledge for the monitoring and closed loop control of biotechnical processes is demonstrated. An important problem of the development of chemometric models is the expense of calibration measurements required to calculate values of process variables from unselective measurements. To reduce this expense a method was developed which uses a dynamic process model instead of measurements. As an example the chemometric modeling will be discussed of a baker's yeast cultivation measuring fluorescence spectra and estimating biomass, glucose, and ethanol concentrations. We demonstrate the exploitation of process knowledge during an Escherichia colifermentation for the closed loop control of glucose concentration by using an extended Kalman filter. Here the effective dead time and the measurement noise will be compensated by this method. The glucose set point is 0.05g/L. The yield of the process exceeds by far that of batch fermentations. (orig.)

Undersea acoustic telemetry across the North Anatolian Fault, Marmara Sea: results from the first 6 months of monitoring of the fault displacement

Science.gov (United States)

Royer, J. Y.; Deschamps, A.; Piete, H.; Sakic, P.; Ballu, V.; Apprioual, R.; Kopp, H.; Lange, D.; Ruffine, L.; Géli, L.

2015-12-01

Located in the Marmara Sea, the Istanbul-Silivri segment of the North Anatolian Fault (NAF) is known to be a seismic gap since 1766, although, in the last century, the NAF has caused major devastating earthquakes over most of its extent. This fault segment, void of seismicity, may be either creeping aseismically or blocked and accumulating enough strain to produce an earthquake of magnitude 7 or greater. This section of the NAF may thus represent a major seismic and tsunamigenic hazard for the Istanbul megalopolis, located only 40 km away. The objective of the MARSITE project, funded by the European Union and coordinated by the Observatory of the University of Kandilli (KOERI), is to determine the blocking state of the Istanbul-Silivri fault segment. In this context, an array of 10 acoustic transponders has been deployed on either sides of the fault, in the eastern part of the Kumburgaz Basin, to measure the displacements of the fault over a period of 3 to 5 years. The telemetric beacons (4 from the University of Brest and 6 from the GEOMAR Institute in Kiel) form two arrays fitted in one another. The principle of the experiment is to repeatedly measure the distance (ie two-way-travel time of acoustic pings) between pairs of beacons and thus to monitor the deformation of an array of 9 baselines, 500m to 3000m long, of which 5 cross obliquely the assumed fault trace. The French and German arrays are independent but ensure a redundancy of rangings along common baselines. Each acoustic transponder also monitors the temperature, pressure, sound-velocity and attitude (tiltmeters), every one or two hours. Data are stored in each beacon and can be downloaded from the surface using an acoustic modem. We present here the first 6 months of recording by the French array, from November 1st, 2014 to April 25, 2015. All acoustic transponders worked nominally for 6 months and appear to have remained stable on the seafloor. Recorded sea-bottom temperatures provide evidence for

Sediment acoustic index method for computing continuous suspended-sediment concentrations

Science.gov (United States)

Landers, Mark N.; Straub, Timothy D.; Wood, Molly S.; Domanski, Marian M.

2016-07-11

Suspended-sediment characteristics can be computed using acoustic indices derived from acoustic Doppler velocity meter (ADVM) backscatter data. The sediment acoustic index method applied in these types of studies can be used to more accurately and cost-effectively provide time-series estimates of suspended-sediment concentration and load, which is essential for informed solutions to many sediment-related environmental, engineering, and agricultural concerns. Advantages of this approach over other sediment surrogate methods include: (1) better representation of cross-sectional conditions from large measurement volumes, compared to other surrogate instruments that measure data at a single point; (2) high temporal resolution of collected data; (3) data integrity when biofouling is present; and (4) less rating curve hysteresis compared to streamflow as a surrogate. An additional advantage of this technique is the potential expansion of monitoring suspended-sediment concentrations at sites with existing ADVMs used in streamflow velocity monitoring. This report provides much-needed standard techniques for sediment acoustic index methods to help ensure accurate and comparable documented results.

Acoustic emission from hydrogen saturated Type 304L stainless steel

International Nuclear Information System (INIS)

Caskey, G.R. Jr.

1978-01-01

Acoustic emission is attributed to energy release within a material body by localized plastic deformation or failure processes. The elastic stress waves may come from slip band formation, mechanical twinning, martensite transformation, or crack propagation. Each of these processes has slightly different acoustic characteristics allowing for easy identification. Acoustic emission was monitored during tensile tests of Type 304L austenitic stainless steel to explore the applicability of the technique to hydrogen-assisted fracture

Analysis of lard in meatball broth using Fourier transform infrared spectroscopy and chemometrics.

Science.gov (United States)

Kurniawati, Endah; Rohman, Abdul; Triyana, Kuwat

2014-01-01

Meatball is one of the favorite foods in Indonesia. For the economic reason (due to the price difference), the substitution of beef meat with pork can occur. In this study, FTIR spectroscopy in combination with chemometrics of partial least square (PLS) and principal component analysis (PCA) was used for analysis of pork fat (lard) in meatball broth. Lard in meatball broth was quantitatively determined at wavenumber region of 1018-1284 cm(-1). The coefficient of determination (R(2)) and root mean square error of calibration (RMSEC) values obtained were 0.9975 and 1.34% (v/v), respectively. Furthermore, the classification of lard and beef fat in meatball broth as well as in commercial samples was performed at wavenumber region of 1200-1000 cm(-1). The results showed that FTIR spectroscopy coupled with chemometrics can be used for quantitative analysis and classification of lard in meatball broth for Halal verification studies. The developed method is simple in operation, rapid and not involving extensive sample preparation. © 2013.

Acoustic emission detection with fiber optical sensors for dry cask storage health monitoring

Science.gov (United States)

Lin, Bin; Bao, Jingjing; Yu, Lingyu; Giurgiutiu, Victor

2016-04-01

The increasing number, size, and complexity of nuclear facilities deployed worldwide are increasing the need to maintain readiness and develop innovative sensing materials to monitor important to safety structures (ITS). In the past two decades, an extensive sensor technology development has been used for structural health monitoring (SHM). Technologies for the diagnosis and prognosis of a nuclear system, such as dry cask storage system (DCSS), can improve verification of the health of the structure that can eventually reduce the likelihood of inadvertently failure of a component. Fiber optical sensors have emerged as one of the major SHM technologies developed particularly for temperature and strain measurements. This paper presents the development of optical equipment that is suitable for ultrasonic guided wave detection for active SHM in the MHz range. An experimental study of using fiber Bragg grating (FBG) as acoustic emission (AE) sensors was performed on steel blocks. FBG have the advantage of being durable, lightweight, and easily embeddable into composite structures as well as being immune to electromagnetic interference and optically multiplexed. The temperature effect on the FBG sensors was also studied. A multi-channel FBG system was developed and compared with piezoelectric based AE system. The paper ends with conclusions and suggestions for further work.

Acoustic Emission Monitoring of Lightning-Damaged CFRP Laminates during Compression-after-Impact Test

Energy Technology Data Exchange (ETDEWEB)

Kwon, Oh Yang; Shin, Jae Ha [Department of Mechanical Engineering, Inha University, Incheon (Korea, Republic of)

2012-06-15

Carbon-fiber reinforced plastic(CFRP) laminates made of nano-particle-coated carbon fibers and damaged by a simulated lightning strike were tested under compression-after-impact(CAI) mode, during which the damage progress due to compressive loading has been monitored by acoustic emission(AE). The impact damage was induced not by mechanical loading but by a simulated lightning strike. Conductive nano-particles were coated directly on the fibers, from which CFRP coupons were made. The coupon were subjected to the strikes with a high voltage/current impulse of 10-40 kA within a few . The effects of nano-particle coating and the degree of damage induced by the simulated lightning strikes on AE activities were examined, and the relationship between the compressive residual strength and AE behavior has been evaluated in terms of AE event counts and the onset of AE activity with the compressive loading. The degree of impact damage was also measured in terms of damage area by using ultrasonic C-scan images. The assessment during the CAI tests of damaged CFRP showed that AE monitoring appeared to be useful to differentiate the degree of damage hence the mechanical integrity of composite structures damaged by lightning strikes.

Estimating population size of a nocturnal burrow-nesting seabird using acoustic monitoring and habitat mapping

Directory of Open Access Journals (Sweden)

Steffen Oppel

2014-04-01

Full Text Available Population size assessments for nocturnal burrow-nesting seabirds are logistically challenging because these species are active in colonies only during darkness and often nest on remote islands where manual inspections of breeding burrows are not feasible. Many seabird species are highly vocal, and recent technological innovations now make it possible to record and quantify vocal activity in seabird colonies. Here we test the hypothesis that remotely recorded vocal activity in Cory’s shearwater (Calonectris borealis breeding colonies in the North Atlantic increases with nest density, and combined this relationship with cliff habitat mapping to estimate the population size of Cory’s shearwaters on the island of Corvo (Azores. We deployed acoustic recording devices in 9 Cory’s shearwater colonies of known size to establish a relationship between vocal activity and local nest density (slope = 1.07, R2 = 0.86, p < 0.001. We used this relationship to predict the nest density in various cliff habitat types and produced a habitat map of breeding cliffs to extrapolate nest density around the island of Corvo. The mean predicted nest density on Corvo ranged from 6.6 (2.1–16.2 to 27.8 (19.5–36.4 nests/ha. Extrapolation of habitat-specific nest densities across the cliff area of Corvo resulted in an estimate of 6326 Cory’s shearwater nests (95% confidence interval: 3735–10,524. This population size estimate is similar to previous assessments, but is too imprecise to detect moderate changes in population size over time. While estimating absolute population size from acoustic recordings may not be sufficiently precise, the strong positive relationship that we found between local nest density and recorded calling rate indicates that passive acoustic monitoring may be useful to document relative changes in seabird populations over time.

Acoustic change detection algorithm using an FM radio

Science.gov (United States)

Goldman, Geoffrey H.; Wolfe, Owen

2012-06-01

The U.S. Army is interested in developing low-cost, low-power, non-line-of-sight sensors for monitoring human activity. One modality that is often overlooked is active acoustics using sources of opportunity such as speech or music. Active acoustics can be used to detect human activity by generating acoustic images of an area at different times, then testing for changes among the imagery. A change detection algorithm was developed to detect physical changes in a building, such as a door changing positions or a large box being moved using acoustics sources of opportunity. The algorithm is based on cross correlating the acoustic signal measured from two microphones. The performance of the algorithm was shown using data generated with a hand-held FM radio as a sound source and two microphones. The algorithm could detect a door being opened in a hallway.

Early detection of emerging street drugs by near infrared spectroscopy and chemometrics.

Science.gov (United States)

Risoluti, R; Materazzi, S; Gregori, A; Ripani, L

2016-06-01

Near-infrared spectroscopy (NIRs) is spreading as the tool of choice for fast and non-destructive analysis and detection of different compounds in complex matrices. This paper investigated the feasibility of using near infrared (NIR) spectroscopy coupled to chemometrics calibration to detect new psychoactive substances in street samples. The capabilities of this approach in forensic chemistry were assessed in the determination of new molecules appeared in the illicit market and often claimed to contain "non-illegal" compounds, although exhibiting important psychoactive effects. The study focused on synthetic molecules belonging to the classes of synthetic cannabinoids and phenethylamines. The approach was validated comparing results with officials methods and has been successfully applied for "in site" determination of illicit drugs in confiscated real samples, in cooperation with the Scientific Investigation Department (Carabinieri-RIS) of Rome. The achieved results allow to consider NIR spectroscopy analysis followed by chemometrics as a fast, cost-effective and useful tool for the preliminary determination of new psychoactive substances in forensic science. Copyright © 2016 Elsevier B.V. All rights reserved.

Condition monitoring of a check valve for nuclear power plants by means of acoustic emission technique

International Nuclear Information System (INIS)

Lee, Min Rae; Leee, Jun Hyun; Kim, Jung Tack; Kim, Jung Soo; Luk, V. K.

2003-01-01

This work performed in support of the International Nuclear Energy Research Initiative(INERI) program, which was to develop and demonstrate advanced sensor and computational technology for on-line monitoring of the condition of components, structures, and systems in advanced and next-generation nuclear power plants (NPPs). The primary object of this work is to investigate advanced condition monitoring systems based on acoustic emission detection that can provide timely detection of check valve degradation and service aging so that maintenance/replacement could be preformed prior to loss of safety function. The research is focused on the capability of AE technique to provide diagnostic information useful in determining check valve aging and degradation, check valve failures and undesirable operating modes. This work also includes the investigation and adaptation of several advanced sensor technologies such as accelerometer and advanced ultrasonic technique. In addition, this work will develop advanced sophisticated signal processing, noise reduction, and pattern recognition techniques and algorithms from check valve degradation.

Condition monitoring of a check valve for nuclear power plants by means of acoustic emission technique

International Nuclear Information System (INIS)

Lee, M. R.; Lee, J. H.; Kim, J. T.; Kim, J. S.; Luk, V. K.

2003-01-01

This work performed in support of the International Nuclear Energy Research Institute (INERI) program, which was to develop and demonstrate advanced sensor and computational technology for on-line monitoring of the condition of components, structures, and systems in advanced and next-generation nuclear power plants (NPPs). This primary object of this work is to investigate advanced condition monitoring systems based on acoustic emission detection that can provide timely detection of check valve degeneration and service aging so that maintenance/replacement could be preformed prior to loss safety function. The research is focused on the capability of AE technique to provide diagnostic information useful in determining check valve aging and degradation check valve failure and undesirable operating modes. This work also includes the investigation and adaptation of several advanced sensor technologies such as accelerometer and advanced ultrasonic technique. In addition, this work will develop advanced sophisticated signal processing, noise reduction, and pattern recognition techniques and algorithms from check valve degradation.

Acoustic monitoring of the BOR-60 reactor circulating pump state

International Nuclear Information System (INIS)

Efimov, V.N.; Myntsov, A.A.

1988-01-01

Diagnostics methods for circulation pumps of the experimental BOR-60 fast reactor are described. The results of signal processing during a microcompain, as well as detected anomalies in pump operation in the earth stage are presented. Analysis carried out for an acoustic signal envelope has shown high efficiency of the method. When oscillations of a mechanical shaft are present, the envelope level increases 1.5 times. More detailed investigation is carried out by the analysis of the spectrum of the pump acoustic signal envelope. During abnormal operation there are peaks, corresponding to the circulation frequency, and harmonics multiple of it, in the spectrum. 6 figs

Acoustic cloaking and transformation acoustics

International Nuclear Information System (INIS)

Chen Huanyang; Chan, C T

2010-01-01

In this review, we give a brief introduction to the application of the new technique of transformation acoustics, which draws on a correspondence between coordinate transformation and material properties. The technique is formulated for both acoustic waves and linear liquid surface waves. Some interesting conceptual devices can be designed for manipulating acoustic waves. For example, we can design acoustic cloaks that make an object invisible to acoustic waves, and the cloak can either encompass or lie outside the object to be concealed. Transformation acoustics, as an analog of transformation optics, can go beyond invisibility cloaking. As an illustration for manipulating linear liquid surface waves, we show that a liquid wave rotator can be designed and fabricated to rotate the wave front. The acoustic transformation media require acoustic materials which are anisotropic and inhomogeneous. Such materials are difficult to find in nature. However, composite materials with embedded sub-wavelength resonators can in principle be made and such 'acoustic metamaterials' can exhibit nearly arbitrary values of effective density and modulus tensors to satisfy the demanding material requirements in transformation acoustics. We introduce resonant sonic materials and Helmholtz resonators as examples of acoustic metamaterials that exhibit resonant behaviour in effective density and effective modulus. (topical review)

Flaw identification using acoustic emission

International Nuclear Information System (INIS)

Woodward, B.; McDonald, N.R.

1975-01-01

Acoustic emission 'signatures' contain information about the fine structure of metallurgical source events and their interpretation may provide a means of assessing the severity of internal flaws as well as surface flaws. The ultimate aim of this research on signature analysis is to develop a real time non-destructive testing technique having the capability of flaw recognition as well as flaw location in nuclear reactor components and structures under stress. Thus the requisite, unlike that in most acoustic emission work to date, is for a technique which affords discrimination between acoustic emission from different types of flaws propagating simultaneously. The approach described here requires detailed analysis of the emission signatures in terms of a specific statistical parameter, energy spectral density. In order to realise the full inspection potential of acoustic emission monitoring data obtained from zirconium and steel testpieces have been correlated with metallurgical condition and mechanical behaviour, since the nature of emission signatures is strongly affected by the physical characteristics and internal structure of the material. (Auth.)

Mechanical Weakening during Fluid Injection in Critically Stressed Sandstones with Acoustic Monitoring

Science.gov (United States)

David, C.; Dautriat, J. D.; Sarout, J.; Macault, R.; Bertauld, D.

2014-12-01

Water weakening is a well-known phenomenon which can lead to subsidence during the production of hydrocarbon reservoirs. The example of the Ekofisk oil field in the North Sea has been well documented for years. In order to assess water weakening effects in reservoir rocks, previous studies have focused on changes in the failure envelopes derived from mechanical tests conducted on rocks saturated either with water or with inert fluids. However, little attention has been paid so far on the mechanical behaviour during the fluid injection stage, like in enhanced oil recovery operations. We studied the effect of fluid injection on the mechanical behaviour of Sherwood sandstone, a weakly-consolidated sandstone sampled at Ladram Bay in UK. In order to highlight possible weakening effects, water and inert oil have been injected into critically-loaded samples to assess their effect on strength and elastic properties and to derive the acoustic signature of the saturation front for each fluid. The specimens were instrumented with 16 ultrasonic P-wave transducers for both passive and active acoustic monitoring during fluid injection and loading. After conducting standard triaxial tests on three samples saturated with air, water and oil respectively, mechanical creep tests were conducted on dry samples loaded at 80% of the compressive strength of the dry rock. While these conditions are kept constant, a fluid is injected at the bottom end of the sample with a low back pressure (0.5 MPa) to minimize effective stress variations during injection. Both water and oil were used as the injected pore fluid in two experiments. As soon as the fluids start to flow into the samples, creep is taking place with a much higher strain rate for water injection compared to oil injection. A transition from secondary creep to tertiary creep is observed in the water injection test whereas in the oil injection test no significant creep acceleration is observed after one pore volume of oil was

Acoustic control of sodium leakage in valve gates of NPP

International Nuclear Information System (INIS)

Trykov, E.L.; Kovtun, S.N.; Anan'ev, A.A.; Yugov, S.I.

2014-01-01

Short description of sodium bench and acoustic investigation results on leakage monitoring of valves DN10 and DN40 are given. It is shown that acoustic method can be used successfully to control the leakages of sodium valves. Leakages on both type of valves increase the acoustic signal dispersion by 2-3 orders. For each type of valve acoustic system of leakage determination allows to conduct the preliminary graduation of signal dispersion on the sodium discharge rate. It make possible not only to record the leakage presence but also to determine the sodium discharge rate through the valve during the leakage [ru

Nondestructive online testing method for friction stir welding using acoustic emission

Science.gov (United States)

Levikhina, Anastasiya

2017-12-01

The paper reviews the possibility of applying the method of acoustic emission for online monitoring of the friction stir welding process. It is shown that acoustic emission allows the detection of weld defects and their location in real time. The energy of an acoustic signal and the median frequency are suggested to be used as informative parameters. The method of calculating the median frequency with the use of a short time Fourier transform is applied for the identification of correlations between the defective weld structure and properties of the acoustic emission signals received during welding.

A Small Acoustic Goniometer for General Purpose Research.

Science.gov (United States)

Pook, Michael L; Loo, Sin Ming

2016-04-29

Understanding acoustic events and monitoring their occurrence is a useful aspect of many research projects. In particular, acoustic goniometry allows researchers to determine the source of an event based solely on the sound it produces. The vast majority of acoustic goniometry research projects used custom hardware targeted to the specific application under test. Unfortunately, due to the wide range of sensing applications, a flexible general purpose hardware/firmware system does not exist for this purpose. This article focuses on the development of such a system which encourages the continued exploration of general purpose hardware/firmware and lowers barriers to research in projects requiring the use of acoustic goniometry. Simulations have been employed to verify system feasibility, and a complete hardware implementation of the acoustic goniometer has been designed and field tested. The results are reported, and suggested areas for improvement and further exploration are discussed.

Chemical analysis of acoustically levitated drops by Raman spectroscopy.

Science.gov (United States)

Tuckermann, Rudolf; Puskar, Ljiljana; Zavabeti, Mahta; Sekine, Ryo; McNaughton, Don

2009-07-01

An experimental apparatus combining Raman spectroscopy with acoustic levitation, Raman acoustic levitation spectroscopy (RALS), is investigated in the field of physical and chemical analytics. Whereas acoustic levitation enables the contactless handling of microsized samples, Raman spectroscopy offers the advantage of a noninvasive method without complex sample preparation. After carrying out some systematic tests to probe the sensitivity of the technique to drop size, shape, and position, RALS has been successfully applied in monitoring sample dilution and preconcentration, evaporation, crystallization, an acid-base reaction, and analytes in a surface-enhanced Raman spectroscopy colloidal suspension.

Acoustic emission condition monitoring of a nuclear power plant check valve using artificial neural networks

International Nuclear Information System (INIS)

Lee, Joon Hyun; Lee, Min Rae; Kim, Jung Teak

2005-01-01

In this study, an advanced condition monitoring technique based on acoustic emission (AE) detection and artificial neural networks was applied to a check valve, one of the components being used extensively in a safety system of a nuclear power plant (Npp). AE testing for a check valve under controlled flow loop conditions was performed to detect and evaluate disk movement for valve degradation such as wear and leakage due to foreign object interference in a check valve. It is clearly demonstrated that the evaluation of different types of failure modes such as disk wear and check valve leakage were successful by systematically analyzing the characteristics of various AE parameters. It is also shown that the leak size can be determined with an artificial neural network

Acoustics aspects of technological process in the rock disintegration

Directory of Open Access Journals (Sweden)

Jozef Futó

2007-04-01

Full Text Available The paper describes some results of monitoring and aspects of the acoustic signal in the rock disintegration on the drillig stand of the Institute of Geotechnics, SAS in Košice. The registration and processing of the acoustic signal is solved as a part of the research grant task within the basic research of the rock disintegration by drilling.

Passive wireless surface acoustic wave sensors for monitoring sequestration sites CO₂ emission

Energy Technology Data Exchange (ETDEWEB)

Wang, Yizhong [Univ. of Pittsburgh, PA (United States); Chyu, Minking [Univ. of Pittsburgh, PA (United States); Wang, Qing-Ming [Univ. of Pittsburgh, PA (United States)

2013-02-14

University of Pittsburgh’s Transducer lab has teamed with the U.S. Department of Energy’s National Energy Technology Laboratory (DOE NETL) to conduct a comprehensive study to develop/evaluate low-cost, efficient CO₂ measuring technologies for geological sequestration sites leakage monitoring. A passive wireless CO₂ sensing system based on surface acoustic wave technology and carbon nanotube nanocomposite was developed. Surface acoustic wave device was studied to determine the optimum parameters. Delay line structure was adopted as basic sensor structure. CNT polymer nanocomposite was fabricated and tested under different temperature and strain condition for natural environment impact evaluation. Nanocomposite resistance increased for 5 times under pure strain, while the temperature dependence of resistance for CNT solely was -1375ppm/°C. The overall effect of temperature on nanocomposite resistance was -1000ppm/°C. The gas response of the nanocomposite was about 10% resistance increase under pure CO₂ . The sensor frequency change was around 300ppm for pure CO₂ . With paralyne packaging, the sensor frequency change from relative humidity of 0% to 100% at room temperature decreased from over 1000ppm to less than 100ppm. The lowest detection limit of the sensor is 1% gas concentration, with 36ppm frequency change. Wireless module was tested and showed over one foot transmission distance at preferred parallel orientation.

Acoustic observations of internal tides and tidal currents in shallow water.

Science.gov (United States)

Turgut, Altan; Mignerey, Peter C; Goldstein, David J; Schindall, Jeffrey A

2013-04-01

Significant acoustic travel-time variability and frequency shifts of acoustic intensity level curves in broadband signal spectrograms were measured in the East China Sea during the summer of 2008. The broadband pulses (270-330 Hz) were transmitted from a fixed source and received at a bottomed horizontal array, located at the 33 km range. The acoustic intensity level curves of the received signals indicate regular frequency shifts that are well correlated with the measured internal tides. Similarly, regular travel-time shifts of the acoustic mode arrivals correlate well with the barotropic tides and can be explained by tidal currents along the acoustic propagation track. These observations indicate the potential of monitoring internal tides and tidal currents using low-frequency acoustic signals propagating at long ranges.

An analysis of beam parameters on proton-acoustic waves through an analytic approach.

Science.gov (United States)

Kipergil, Esra Aytac; Erkol, Hakan; Kaya, Serhat; Gulsen, Gultekin; Unlu, Mehmet Burcin

2017-06-21

It has been reported that acoustic waves are generated when a high-energy pulsed proton beam is deposited in a small volume within tissue. One possible application of proton-induced acoustics is to get real-time feedback for intra-treatment adjustments by monitoring such acoustic waves. A high spatial resolution in ultrasound imaging may reduce proton range uncertainty. Thus, it is crucial to understand the dependence of the acoustic waves on the proton beam characteristics. In this manuscript, firstly, an analytic solution for the proton-induced acoustic wave is presented to reveal the dependence of the signal on the beam parameters; then it is combined with an analytic approximation of the Bragg curve. The influence of the beam energy, pulse duration and beam diameter variation on the acoustic waveform are investigated. Further analysis is performed regarding the Fourier decomposition of the proton-acoustic signals. Our results show that the smaller spill time of the proton beam upsurges the amplitude of the acoustic wave for a constant number of protons, which is hence beneficial for dose monitoring. The increase in the energy of each individual proton in the beam leads to the spatial broadening of the Bragg curve, which also yields acoustic waves of greater amplitude. The pulse duration and the beam width of the proton beam do not affect the central frequency of the acoustic wave, but they change the amplitude of the spectral components.

ACOUSTIC DETECTING AND LOCATING GAS PIPE LINE INFRINGEMENT

Energy Technology Data Exchange (ETDEWEB)

John L. Loth; Gary J. Morris; George M. Palmer; Richard Guiler; Patrick Browning

2004-10-31

The extensive network of high-pressure natural gas transmission pipelines covering the United States provides an important infrastructure for our energy independence. Early detection of pipeline leaks and infringements by construction equipment, resulting in corrosion fractures, presents an important aspect of our national security policy. The National Energy Technology Laboratory Strategic Center for Natural Gas (SCVG) is and has been funding research on various applicable techniques. The WVU research team has focused on monitoring pipeline background acoustic signals generated and transmitted by gas flowing through the gas inside the pipeline. In case of a pipeline infringement, any mechanical impact on the pipe wall, or escape of high-pressure gas, generates acoustic signals traveling both up and down stream through the gas. Sudden changes in flow noise are detectable with a Portable Acoustic Monitoring Package (PAMP), developed under this contract. It incorporates a pressure compensating microphone and a signal- recording device. Direct access to the gas inside the line is obtained by mounting such a PAMP, with a 1/2 inch NPT connection, to a pipeline pressure port found near most shut-off valves. An FFT of the recorded signal subtracted by that of the background noise recorded one-second earlier appears to sufficiently isolate the infringement signal to allow source interpretation. Using cell phones for data downloading might allow a network of such 1000-psi rated PAMP's to acoustically monitor a pipeline system and be trained by neural network software to positively identify and locate any pipeline infringement.

ACOUSTIC DETECTING AND LOCATING GAS PIPE LINE INFRINGEMENT

Energy Technology Data Exchange (ETDEWEB)

John L. Loth; Gary J. Morris; George M. Palmer; Richard Guiler; Patrick Browning

2004-12-01

The extensive network of high-pressure natural gas transmission pipelines covering the United States provides an important infrastructure for our energy independence. Early detection of pipeline leaks and infringements by construction equipment, resulting in corrosion fractures, presents an important aspect of our national security policy. The National Energy Technology Laboratory Strategic Center for Natural Gas (SCVG) is and has been funding research on various applicable techniques. The WVU research team has focused on monitoring pipeline background acoustic signals generated and transmitted by gas flowing through the gas inside the pipeline. In case of a pipeline infringement, any mechanical impact on the pipe wall, or escape of high-pressure gas, generates acoustic signals traveling both up and down stream through the gas. Sudden changes in flow noise are detectable with a Portable Acoustic Monitoring Package (PAMP), developed under this contract. It incorporates a pressure compensating microphone and a signal- recording device. Direct access to the gas inside the line is obtained by mounting such a PAMP, with a 1/2 inch NPT connection, to a pipeline pressure port found near most shut-off valves. An FFT of the recorded signal subtracted by that of the background noise recorded one-second earlier appears to sufficiently isolate the infringement signal to allow source interpretation. Using cell phones for data downloading might allow a network of such 1000-psi rated PAMP's to acoustically monitor a pipeline system and be trained by neural network software to positively identify and locate any pipeline infringement.

Acoustic Emission Beamforming for Detection and Localization of Damage

Science.gov (United States)

Rivey, Joshua Callen

The aerospace industry is a constantly evolving field with corporate manufacturers continually utilizing innovative processes and materials. These materials include advanced metallics and composite systems. The exploration and implementation of new materials and structures has prompted the development of numerous structural health monitoring and nondestructive evaluation techniques for quality assurance purposes and pre- and in-service damage detection. Exploitation of acoustic emission sensors coupled with a beamforming technique provides the potential for creating an effective non-contact and non-invasive monitoring capability for assessing structural integrity. This investigation used an acoustic emission detection device that employs helical arrays of MEMS-based microphones around a high-definition optical camera to provide real-time non-contact monitoring of inspection specimens during testing. The study assessed the feasibility of the sound camera for use in structural health monitoring of composite specimens during tensile testing for detecting onset of damage in addition to nondestructive evaluation of aluminum inspection plates for visualizing stress wave propagation in structures. During composite material monitoring, the sound camera was able to accurately identify the onset and location of damage resulting from large amplitude acoustic feedback mechanisms such as fiber breakage. Damage resulting from smaller acoustic feedback events such as matrix failure was detected but not localized to the degree of accuracy of larger feedback events. Findings suggest that beamforming technology can provide effective non-contact and non-invasive inspection of composite materials, characterizing the onset and the location of damage in an efficient manner. With regards to the nondestructive evaluation of metallic plates, this remote sensing system allows us to record wave propagation events in situ via a single-shot measurement. This is a significant improvement over

Energy scavenging system by acoustic wave and integrated wireless communication

Science.gov (United States)

Kim, Albert

The purpose of the project was developing an energy-scavenging device for other bio implantable devices. Researchers and scientist have studied energy scavenging method because of the limitation of traditional power source, especially for bio-implantable devices. In this research, piezoelectric power generator that activates by acoustic wave, or music was developed. Follow by power generator, a wireless communication also integrated with the device for monitoring the power generation. The Lead Zirconate Titanate (PZT) bimorph cantilever with a proof mass at the free end tip was studied to convert acoustic wave to power. The music or acoustic wave played through a speaker to vibrate piezoelectric power generator. The LC circuit integrated with the piezoelectric material for purpose of wireless monitoring power generation. However, wireless monitoring can be used as wireless power transmission, which means the signal received via wireless communication also can be used for power for other devices. Size of 74 by 7 by 7cm device could generate and transmit 100mVp from 70 mm distance away with electrical resonant frequency at 420.2 kHz..

Real-time measurement of electron beam weld penetration in uranium by acoustic emission monitoring

International Nuclear Information System (INIS)

Whittaker, J.W.; Murphy, J.L.

1991-07-01

High quality electron beam (EB) welds are required in uranium test articles. Acoustic emission (AE) techniques are under development with the goal of measuring weld penetration in real-time. One technique, based on Average Signal Level (ASL) measurement was used to record weld AE signatures. Characteristic AE signatures were recorded for bead-on-plate (BOP) and butt joint (BJ) welds made under varied welding conditions. AE waveforms were sampled to determine what microscopic AE behavior led to the observed macroscopic signature features. Deformation twinning and weld expulsion are two of the main sources of emission. AE behavior was correlated with weld penetration as measured by standard metallographic techniques. The ASL value was found to increase approximately linearly with weld penetration in BJ welds. These results form the basis for a real-time monitoring technique for weld penetration. 5 refs

Distributed acoustic sensing technique and its field trial in SAGD well

Science.gov (United States)

Han, Li; He, Xiangge; Pan, Yong; Liu, Fei; Yi, Duo; Hu, Chengjun; Zhang, Min; Gu, Lijuan

2017-10-01

Steam assisted gravity drainage (SAGD) is a very promising way for the development of heavy oil, extra heavy oil and tight oil reservoirs. Proper monitoring of the SAGD operations is essential to avoid operational issues and improve efficiency. Among all the monitoring techniques, micro-seismic monitoring and related interpretation method can give useful information about the steam chamber development and has been extensively studied. Distributed acoustic sensor (DAS) based on Rayleigh backscattering is a newly developed technique that can measure acoustic signal at all points along the sensing fiber. In this paper, we demonstrate a DAS system based on dual-pulse heterodyne demodulation technique and did field trial in SAGD well located in Xinjiang Oilfield, China. The field trail results validated the performance of the DAS system and indicated its applicability in steam-chamber monitoring and hydraulic monitoring.

Chromatographic fingerprinting through chemometric techniques for herbal slimming pills: A way of adulterant identification.

Science.gov (United States)

Shekari, Nafiseh; Vosough, Maryam; Tabar Heidar, Kourosh

2018-05-01

In the current study, gas chromatography-mass spectrometry (GC-MS) fingerprinting of herbal slimming pills assisted by chemometric methods has been presented. Deconvolution of two-way chromatographic signals of nine herbal slimming pills into pure chromatographic and spectral patterns was performed. The peak clusters were resolved using multivariate curve resolution-alternating least squares (MCR-ALS) by employing appropriate constraints. It was revealed that more useful chemical information about the composition of the slimming pills can be obtained by employing sophisticated GC-MS method coupled with proper chemometric tools yielding the extended number of identified constituents. The thorough fingerprinting of the complex mixtures proved the presence of some toxic or carcinogen components, such as toluene, furfural, furfuryl alcohol, styrene, itaconic anhydride, citraconic anhydride, trimethyl phosphate, phenol, pyrocatechol, p-propenylanisole and pyrogallol. In addition, some samples were shown to be adulterated with undeclared ingredients, including stimulants, anorexiant and laxatives such as phenolphthalein, amfepramone, caffeine and sibutramine. Copyright © 2018 Elsevier B.V. All rights reserved.

Quasi-static acoustic tweezing thromboelastometry.

Science.gov (United States)

Holt, R G; Luo, D; Gruver, N; Khismatullin, D B

2017-07-01

Essentials Blood coagulation measurement during contact with an artificial surface leads to unreliable data. Acoustic tweezing thromboelastometry is a novel non-contact method for coagulation monitoring. This method detects differences in the blood coagulation state within 10 min. Coagulation data were obtained using a much smaller sample volume (4 μL) than currently used. Background Thromboelastography is widely used as a tool to assess the coagulation status of critical care patients. It allows observation of changes in material properties of whole blood, beginning with early stages of clot formation and ending with clot lysis. However, the contact activation of the coagulation cascade at surfaces of thromboelastographic systems leads to inherent variability and unreliability in predicting bleeding or thrombosis risks. Objectives To develop acoustic tweezing thromboelastometry as a non-contact method for perioperative assessment of blood coagulation. Methods Acoustic tweezing is used to levitate microliter drops of biopolymer and human blood samples. By quasi-statically changing the acoustic pressure we control the sample drop location and deformation. Sample size, deformation and location are determined by digital imaging at each pressure. Results Simple Newtonian liquid solutions maintain a constant, reversible location vs. deformation curve. In contrast, the location/deformation curves for gelatin, alginate, whole blood and blood plasma uniquely change as the samples solidify. Increasing elasticity causes the sample to deform less, leading to steeper stress/strain curves. By extracting a linear regime slope, we show that whole blood or blood plasma exhibits a unique slope profile as it begins to clot. By exposing blood samples to pro- or antithrombotic agents, the slope profile changes, allowing detection of hyper- or hypocoagulable states. Conclusions We demonstrate that quasi-static acoustic tweezing can yield information about clotting onset, maturation

Application of Chemometric Techniques to Colorimetric Data in Classifying Automobile Paint

International Nuclear Information System (INIS)

Nur Awatif Rosli; Rozita Osman; Norashikin Saim; Mohd Zuli Jaafar

2015-01-01

The analysis of paint chips is of great interest to forensic investigators, particularly in the examination of hit-and run cases. This study proposes a direct and rapid method in classifying automobile paint samples based on colorimetric data sets; absorption value, reflectance value, luminosity value (L), degree of redness (a) and degree of yellowness (b) obtained from video spectral comparator (VSC) technique. A total of 42 automobile paint samples from 7 manufacturers were analysed. The colorimetric datasets obtained from VSC analysis were subjected to chemometric technique namely cluster analysis (CA) and principal component analysis (PCA). Based on CA, 5 clusters were generated; Cluster 1 consisted of silver color, cluster 2 consisted of white color, cluster 3 consisted of blue and black colors, cluster 4 consisted of red color and cluster 5 consisted of light blue color. PCA resulted in two latent factors explaining 95.58 % of the total variance, enabled to group the 42 automobile paints into five groups. Chemometric application on colorimetric datasets provide meaningful classification of automobile paints based on their tone colour (L, a, b) and light intensity These approaches have the potential to ease the interpretation of complex spectral data involving a large number of comparisons. (author)

Cider fermentation process monitoring by Vis-NIR sensor system and chemometrics.

Science.gov (United States)

Villar, Alberto; Vadillo, Julen; Santos, Jose I; Gorritxategi, Eneko; Mabe, Jon; Arnaiz, Aitor; Fernández, Luis A

2017-04-15

Optimization of a multivariate calibration process has been undertaken for a Visible-Near Infrared (400-1100nm) sensor system, applied in the monitoring of the fermentation process of the cider produced in the Basque Country (Spain). The main parameters that were monitored included alcoholic proof, l-lactic acid content, glucose+fructose and acetic acid content. The multivariate calibration was carried out using a combination of different variable selection techniques and the most suitable pre-processing strategies were selected based on the spectra characteristics obtained by the sensor system. The variable selection techniques studied in this work include Martens Uncertainty test, interval Partial Least Square Regression (iPLS) and Genetic Algorithm (GA). This procedure arises from the need to improve the calibration models prediction ability for cider monitoring. Copyright © 2016 Elsevier Ltd. All rights reserved.

The Contact State Monitoring for Seal End Faces Based on Acoustic Emission Detection

Directory of Open Access Journals (Sweden)

Xiaohui Li

2016-01-01

Full Text Available Monitoring the contact state of seal end faces would help the early warning of the seal failure. In the acoustic emission (AE detection for mechanical seal, the main difficulty is to reduce the background noise and to classify the dispersed features. To solve these problems and achieve higher detection rates, a new approach based on genetic particle filter with autoregression (AR-GPF and hypersphere support vector machine (HSSVM is presented. First, AR model is used to build the dynamic state space (DSS of the AE signal, and GPF is used for signal filtering. Then, multiple features are extracted, and a classification model based on HSSVM is constructed for state recognition. In this approach, AR-GPF is an excellent time-domain method for noise reduction, and HSSVM has advantage on those dispersed features. Finally experimental data shows that the proposed method can effectively detect the contact state of the seal end faces and has higher accuracy rates than some other existing methods.

Acoustic Monitoring of a Previously Unstudied Whale Shark Aggregation in the Red Sea

KAUST Repository

Cochran, Jesse

2012-01-01

The whale shark (Rhincodon, typus), is a large, pelagic, filter feeder for which the available information is limited. The Red Sea populations in particular are practically unstudied. An aggregation site was recently discovered off the western coast of Saudi Arabia. We report the use of passive acoustic monitoring to assess the spatial and temporal behavior patterns of whale sharks in this new site. The aggregation occurs in the spring and peaks in April/ May. Whale sharks showed a preference for a single near shore reef and even a specific area within it. There is no evidence of sexual segregation as the genders were present in roughly equal proportion and used the same habitat at similar times. This information can be used to guide future studies in the area and to inform local management. Continued study will add to the collective knowledge on Red Sea whale sharks, including the population dynamics within the region and how they interact with the global whale shark community.

Quality control of the paracetamol drug by chemometrics and imaging spectroscopy in the near infrared region

Science.gov (United States)

Baptistao, Mariana; Rocha, Werickson Fortunato de Carvalho; Poppi, Ronei Jesus

2011-09-01

In this work, it was used imaging spectroscopy and chemometric tools for the development and analysis of paracetamol and excipients in pharmaceutical formulations. It was also built concentration maps to study the distribution of the drug in the tablets surface. Multivariate models based on PLS regression were developed for paracetamol and excipients concentrations prediction. For the construction of the models it was used 31 samples in the tablet form containing the active principle in a concentration range of 30.0-90.0% (w/w) and errors below to 5% were obtained for validation samples. Finally, the study of the distribution in the drug was performed through the distribution maps of concentration of active principle and excipients. The analysis of maps showed the complementarity between the active principle and excipients in the tablets. The region with a high concentration of a constituent must have, necessarily, absence or low concentration of the other one. Thus, an alternative method for the paracetamol drug quality monitoring is presented.

Artificial Neural Network Model for Monitoring Oil Film Regime in Spur Gear Based on Acoustic Emission Data

Directory of Open Access Journals (Sweden)

Yasir Hassan Ali

2015-01-01

Full Text Available The thickness of an oil film lubricant can contribute to less gear tooth wear and surface failure. The purpose of this research is to use artificial neural network (ANN computational modelling to correlate spur gear data from acoustic emissions, lubricant temperature, and specific film thickness (λ. The approach is using an algorithm to monitor the oil film thickness and to detect which lubrication regime the gearbox is running either hydrodynamic, elastohydrodynamic, or boundary. This monitoring can aid identification of fault development. Feed-forward and recurrent Elman neural network algorithms were used to develop ANN models, which are subjected to training, testing, and validation process. The Levenberg-Marquardt back-propagation algorithm was applied to reduce errors. Log-sigmoid and Purelin were identified as suitable transfer functions for hidden and output nodes. The methods used in this paper shows accurate predictions from ANN and the feed-forward network performance is superior to the Elman neural network.

Acoustic emission from polycrystalline graphites

International Nuclear Information System (INIS)

Ioka, I.; Yoda, S.; Oku, T.; Miyamoto, Y.

1987-01-01

Acoustic emission was monitored from polycrystalline graphites with different microstructure (pore size and pore volume) subjected to compressive loading. The graphites used in this study comprised five brands, that is, PGX, ISEM-1, IG-11, IG-15, and ISO-88. A root mean square (RMS) voltage and event counts of acoustic emission for graphites were measured during compressive loading. The acoustic emission was measured using a computed-based data acquisition and analysis system. The graphites were first deformed up to 80 % of the average fracture stress, then unloaded and reloaded again until the fracture occured. During the first loading, the change in RMS voltage for acoustic emission was detected from the initial stage. During the unloading, the RMS voltage became zero level as soon as the applied stress was released and then gradually rose to a peak and declined. The behavior indicated that the reversed plastic deformation occured in graphites. During the second loading, the RMS voltage gently increased until the applied stress exceeded the maximum stress of the first loading; there is no Kaiser effect in the graphites. A bicrystal model could give a reasonable explanation of this results. The empirical equation between the ratio of σ AE to σ f and σ f was obtained. It is considered that the detection of microfracture by the acoustic emission technique is effective in macrofracture prediction of polycrystalline graphites. (author)

Chemometric brand differentiation of commercial spices using direct analysis in real time mass spectrometry.

Science.gov (United States)

Pavlovich, Matthew J; Dunn, Emily E; Hall, Adam B

2016-05-15

Commercial spices represent an emerging class of fuels for improvised explosives. Being able to classify such spices not only by type but also by brand would represent an important step in developing methods to analytically investigate these explosive compositions. Therefore, a combined ambient mass spectrometric/chemometric approach was developed to quickly and accurately classify commercial spices by brand. Direct analysis in real time mass spectrometry (DART-MS) was used to generate mass spectra for samples of black pepper, cayenne pepper, and turmeric, along with four different brands of cinnamon, all dissolved in methanol. Unsupervised learning techniques showed that the cinnamon samples clustered according to brand. Then, we used supervised machine learning algorithms to build chemometric models with a known training set and classified the brands of an unknown testing set of cinnamon samples. Ten independent runs of five-fold cross-validation showed that the training set error for the best-performing models (i.e., the linear discriminant and neural network models) was lower than 2%. The false-positive percentages for these models were 3% or lower, and the false-negative percentages were lower than 10%. In particular, the linear discriminant model perfectly classified the testing set with 0% error. Repeated iterations of training and testing gave similar results, demonstrating the reproducibility of these models. Chemometric models were able to classify the DART mass spectra of commercial cinnamon samples according to brand, with high specificity and low classification error. This method could easily be generalized to other classes of spices, and it could be applied to authenticating questioned commercial samples of spices or to examining evidence from improvised explosives. Copyright © 2016 John Wiley & Sons, Ltd.

Incore monitoring device

International Nuclear Information System (INIS)

Tai, Ichiro; Shirayama, Shin-pei; Nozaki, Shin-ichi.

1978-01-01

Purpose: To provide an incore monitoring device wherein both radiation monitoring and acoustic monitoring are carried out simultaneously by one detector, whereby installation of the device and signal pick-up are facilitated. Incore conditions are accurately grasped. Constitution: When a neutron is irradiated in a state where a DC voltage is applied between the electrode and the vessel in the device, an ionization current is occured by (n.γ) reaction of the transformed substance as in an ionization chamber, Accordingly, a voltage drop occurs at both ends of the resistor of the radiation signal processing system, as a result of which a neutron flux can be detected. Further, when a sound is generated in the reactor, the monitoring device bottom wall which formed by a piezoelectric element detects the sound-waves. This output signal is picked up by the acoustic signal processing system to judge the generation of sound. (Aizawa, K.)

Monitoring multiple components in vinegar fermentation using Raman spectroscopy.

Science.gov (United States)

Uysal, Reyhan Selin; Soykut, Esra Acar; Boyaci, Ismail Hakki; Topcu, Ali

2013-12-15

In this study, the utility of Raman spectroscopy (RS) with chemometric methods for quantification of multiple components in the fermentation process was investigated. Vinegar, the product of a two stage fermentation, was used as a model and glucose and fructose consumption, ethanol production and consumption and acetic acid production were followed using RS and the partial least squares (PLS) method. Calibration of the PLS method was performed using model solutions. The prediction capability of the method was then investigated with both model and real samples. HPLC was used as a reference method. The results from comparing RS-PLS and HPLC with each other showed good correlations were obtained between predicted and actual sample values for glucose (R(2)=0.973), fructose (R(2)=0.988), ethanol (R(2)=0.996) and acetic acid (R(2)=0.983). In conclusion, a combination of RS with chemometric methods can be applied to monitor multiple components of the fermentation process from start to finish with a single measurement in a short time. Copyright © 2013 Elsevier Ltd. All rights reserved.

Acoustic Levitator Power Device: Study of Ethylene-Glycol Water Mixtures

Science.gov (United States)

Caccamo, M. T.; Cannuli, A.; Calabrò, E.; Magazù, S.

2017-05-01

Acoustic levitator power device is formed by two vertically and opposed high output acoustic transducers working at 22 kHz frequency and produces sound pressure levels of 160 dB. The acoustic waves are monitored from an oscilloscope using a signal amplifier. The ability to perform contactless measurements, avoidance of undesired contamination from the container, are some of advantages of this apparatus. Acoustic levitation can be also used for sample preparation of high concentrated mixtures starting from solutions. In the present paper, an acoustic levitator power device is employed to collect data on levitated water mixtures of Ethylene Glycol (EG) which are then analysed by Infra-Red spectroscopy. The study allows to follow the drying process versus time and to obtain a gel-like compound characterized by an extended chemical crosslinking.

Acoustic Localization with Infrasonic Signals

Science.gov (United States)

Threatt, Arnesha; Elbing, Brian

2015-11-01

Numerous geophysical and anthropogenic events emit infrasonic frequencies (<20 Hz), including volcanoes, hurricanes, wind turbines and tornadoes. These sounds, which cannot be heard by the human ear, can be detected from large distances (in excess of 100 miles) due to low frequency acoustic signals having a very low decay rate in the atmosphere. Thus infrasound could be used for long-range, passive monitoring and detection of these events. An array of microphones separated by known distances can be used to locate a given source, which is known as acoustic localization. However, acoustic localization with infrasound is particularly challenging due to contamination from other signals, sensitivity to wind noise and producing a trusted source for system development. The objective of the current work is to create an infrasonic source using a propane torch wand or a subwoofer and locate the source using multiple infrasonic microphones. This presentation will present preliminary results from various microphone configurations used to locate the source.

Acoustic probe for solid-gas-liquid suspensions. 1998 annual progress report

International Nuclear Information System (INIS)

Greenwood, M.S.; Sangani, A.S.; Tavlarides, L.L.

1998-01-01

'The proposed research will develop an acoustic probe for monitoring particle size and volume fraction in slurries in the absence and presence of gas. The goals are to commission and verify the probe components and system operation, develop theory for the forward and inverse problems for acoustic wave propagation through a three phase medium, and experimentally verify the theoretical analysis. The acoustic probe will permit measurement of solid content in gas-liquid-solid waste slurries in tanks across the DOE complex.'

Passive Acoustic Studies of North Atlantic Right Whales

Data.gov (United States)

National Oceanic and Atmospheric Administration, Department of Commerce — Passive acoustic monitoring buoys have been deployed in shallow waters between North Carolina and Northern Florida since 2003. These units are bottom mounted...

Calibration of AN Acoustic Sensor (geophone) for Continuous Bedload Monitoring in Mountainous Streams

Science.gov (United States)

Tsakiris, A. G.; Papanicolaou, T.

2010-12-01

Measurement of bedload rates is a crucial component in the study of alluvial processes in mountainous streams. Stream restoration efforts, the validation of morphodynamic models and the calibration empirical transport formulae rely on accurate bedload transport measurements. Bedload measurements using traditional methods (e.g. samplers, traps) are time consuming, resource intensive and not always feasible, especially at higher flow conditions. These limitations could potentially be addressed by acoustic instruments, which may provide unattended, continuous bedload measurements even at higher flow conditions, provided that these instruments are properly calibrated. The objective of this study is to calibrate an acoustic instrument (geophone) for performing bedload measurements in a well-monitored laboratory environment at conditions corresponding to low flow regime in mountainous streams. The geophone was manufactured by ClampOn® and was attached to the bottom of a steel plate with dimensions 0.15x0.15 m. The geophone registers the energy of the acoustic signal produced by the movement of the bedload particles over the steel plate with time resolution of one second. The plate-sensor system was installed in an acrylic housing such that the steel plate top surface was at the same level with the surface of a flat porous bed consisting of unisize spheres with diameter 19.1 mm. Unisize spherical glass particles, 15.9 mm in diameter, were preplaced along a 2 m long section upstream of the sensor, and were entrained over the steel plate. In these experiments, the geophone records spanned the complete experiment duratio. Plan view video of the particle movement over the steel plate was recorded via an overhead camera, and was used to calculate the actual bedload rate over the steel plate. Synchronized analysis of this plan view video and the geophone time series revealed that the geophone detected 62% of the bedload particles passing over the steel plate, which triggered

A Methodological Review of Piezoelectric Based Acoustic Wave Generation and Detection Techniques for Structural Health Monitoring

Directory of Open Access Journals (Sweden)

Zhigang Sun

2013-01-01

Full Text Available Piezoelectric transducers have a long history of applications in nondestructive evaluation of material and structure integrity owing to their ability of transforming mechanical energy to electrical energy and vice versa. As condition based maintenance has emerged as a valuable approach to enhancing continued aircraft airworthiness while reducing the life cycle cost, its enabling structural health monitoring (SHM technologies capable of providing on-demand diagnosis of the structure without interrupting the aircraft operation are attracting increasing R&D efforts. Piezoelectric transducers play an essential role in these endeavors. This paper is set forth to review a variety of ingenious ways in which piezoelectric transducers are used in today’s SHM technologies as a means of generation and/or detection of diagnostic acoustic waves.

Indo-Pacific humpback dolphin occurrence north of Lantau Island, Hong Kong, based on year-round passive acoustic monitoring.

Science.gov (United States)

Munger, Lisa; Lammers, Marc O; Cifuentes, Mattie; Würsig, Bernd; Jefferson, Thomas A; Hung, Samuel K

2016-10-01

Long-term passive acoustic monitoring (PAM) was conducted to study Indo-Pacific humpback dolphins, Sousa chinensis, as part of environmental impact assessments for several major coastal development projects in Hong Kong waters north of Lantau Island. Ecological acoustic recorders obtained 2711 days of recording at 13 sites from December 2012 to December 2014. Humpback dolphin sounds were manually detected on more than half of days with recordings at 12 sites, 8 of which were within proposed reclamation areas. Dolphin detection rates were greatest at Lung Kwu Chau, with other high-occurrence locations northeast of the Hong Kong International Airport and within the Lung Kwu Tan and Siu Ho Wan regions. Dolphin detection rates were greatest in summer and autumn (June-November) and were significantly reduced in spring (March-May) compared to other times of year. Click detection rates were significantly higher at night than during daylight hours. These findings suggest high use of many of the proposed reclamation/development areas by humpback dolphins, particularly at night, and demonstrate the value of long-term PAM for documenting spatial and temporal patterns in dolphin occurrence to help inform management decisions.

Acoustic emission monitoring of crack formation during alkali silica\

Czech Academy of Sciences Publication Activity Database

Lokajíček, Tomáš; Přikryl, R.; Šachlová, Š.; Kuchařová, A.

2017-01-01

Roč. 220, MAR 30 (2017), s. 175-182 ISSN 0013-7952 R&D Projects: GA ČR(CZ) GAP104/12/0915 Institutional support: RVO:67985831 Keywords : Alkali-silica reaction * accelerated expansion test * ultrasonic sounding * acoustic emission * backscattered electron imaging Subject RIV: JJ - Other Materials OBOR OECD: Materials engineering Impact factor: 2.569, year: 2016

Analysis of Precursors Prior to Rock Burst in Granite Tunnel Using Acoustic Emission and Far Infrared Monitoring

Directory of Open Access Journals (Sweden)

Zhengzhao Liang

2013-01-01

Full Text Available To understand the physical mechanism of the anomalous behaviors observed prior to rock burst, the acoustic emission (AE and far infrared (FIR techniques were applied to monitor the progressive failure of a rock tunnel model subjected to biaxial stresses. Images of fracturing process, temperature changes of the tunnel, and spatiotemporal serials of acoustic emission were simultaneously recorded during deformation of the model. The b-value derived from the amplitude distribution data of AE was calculated to predict the tunnel rock burst. The results showed that the vertical stress enhanced the stability of the tunnel, and the tunnels with higher confining pressure demonstrated a more abrupt and strong rock burst. Abnormal temperature changes around the wall were observed prior to the rock burst of the tunnel. Analysis of the AE events showed that a sudden drop and then a quiet period could be considered as the precursors to forecast the rock burst hazard. Statistical analysis indicated that rock fragment spalling occurred earlier than the abnormal temperature changes, and the abnormal temperature occurred earlier than the descent of the AE b-value. The analysis indicated that the temperature changes were more sensitive than the AE b-value changes to predict the tunnel rock bursts.

Discriminating the Geographical Origins of Chinese White Lotus Seeds by Near-Infrared Spectroscopy and Chemometrics

Directory of Open Access Journals (Sweden)

Lu Xu

2015-01-01

Full Text Available The traceability of a Chinese white lotus seed (WLS with Protected Designation of Origin (PDO was investigated using near-infrared (NIR spectroscopy and chemometrics. Three chemometrics methods, discrimination analysis (DA, class modeling, and a newly proposed strategy, the fusion of DA and class modeling, were investigated to compare their capacity to trace the geographical origins of WLS. Least squares support vector machine (LS-SVM was developed to distinguish the PDO WLS from non-PDO WLS of four main producing areas. A class modeling technique, one-class partial least squares (OCPLS, was developed only using the data of PDO WLS. By the fusion of LS-SVM and OCPLS, the best prediction sensitivity and specificity were 0.900 and 0.973, respectively. The results indicate that fusion of DA and class modeling can enhance the specificity for detection of non-PDO products. The conclusion is that DA and class modeling should be combined for tracing food geographical origins.

Mesoscale variations in acoustic signals induced by atmospheric gravity waves.

Science.gov (United States)

Chunchuzov, Igor; Kulichkov, Sergey; Perepelkin, Vitaly; Ziemann, Astrid; Arnold, Klaus; Kniffka, Anke

2009-02-01

The results of acoustic tomographic monitoring of the coherent structures in the lower atmosphere and the effects of these structures on acoustic signal parameters are analyzed in the present study. From the measurements of acoustic travel time fluctuations (periods 1 min-1 h) with distant receivers, the temporal fluctuations of the effective sound speed and wind speed are retrieved along different ray paths connecting an acoustic pulse source and several receivers. By using a coherence analysis of the fluctuations near spatially distanced ray turning points, the internal wave-associated fluctuations are filtered and their spatial characteristics (coherences, horizontal phase velocities, and spatial scales) are estimated. The capability of acoustic tomography in estimating wind shear near ground is shown. A possible mechanism describing the temporal modulation of the near-ground wind field by ducted internal waves in the troposphere is proposed.

Acoustic monitoring of terrorist intrusion in a drinking water network

NARCIS (Netherlands)

Quesson, B.A.J.; Sheldon-Robert, M.K.; Vloerbergh, I.N.; Vreeburg, J.H.G.

2009-01-01

In collaboration with Kiwa Water Research, TNO (Netherlands Organisation for Applied Scientific Research) has investigated the possibilities to detect and classify aberrant sounds in water networks, using acoustic sensors. Amongst the sources of such sounds are pumps, drills, mechanical impacts,

Operational experiences with automated acoustic burst classification by neural networks

International Nuclear Information System (INIS)

Olma, B.; Ding, Y.; Enders, R.

1996-01-01

Monitoring of Loose Parts Monitoring System sensors for signal bursts associated with metallic impacts of loose parts has proved as an useful methodology for on-line assessing the mechanical integrity of components in the primary circuit of nuclear power plants. With the availability of neural networks new powerful possibilities for classification and diagnosis of burst signals can be realized for acoustic monitoring with the online system RAMSES. In order to look for relevant burst signals an automated classification is needed, that means acoustic signature analysis and assessment has to be performed automatically on-line. A back propagation neural network based on five pre-calculated signal parameter values has been set up for identification of different signal types. During a three-month monitoring program of medium-operated check valves burst signals have been measured and classified separately according to their cause. The successful results of the three measurement campaigns with an automated burst type classification are presented. (author)

Progress on acoustic techniques for LMFBR structural surveillance

Energy Technology Data Exchange (ETDEWEB)

Burton, E J; Bentley, P G; McKnight, J A [RNL, UKAEA, Risley, Warrington, Cheshire (United Kingdom)

1980-11-01

Acoustic techniques are being developed to monitor remotely the incipient events of various modes of failure. Topics have been selected from the development programme which are either of special importance or in which significant advances have been made recently. Ultrasonic inspection of stainless steel welds is difficult and one alternative approach which is being explored is to identify manufacturing defects during fabrication by monitoring the welding processes. Preliminary measurements are described of the acoustic events measured during deliberately defective welding tests in the laboratory and some initial analysis using pattern recognition techniques is described. The assessment of structural failures using probability analysis has emphasised the potential value of continuous monitoring during operation and this has led to the investigation into the use of vibrational analysis and acoustic emission as monitoring techniques. Mechanical failure from fatigue may be anticipated from measurement of vibrational modes and experience from PFR and from models have indicated the depth of detailed understanding required to achieve this. In the laboratory a vessel with an artificial defect has been pressurised to failure. Detection of the weak stress wave emissions was possible but difficult and the prospects for on-line monitoring are discussed. Ultrasonic technology for providing images of components immersed in the opaque sodium of LMFBRs is being developed. Images are cormed by the physical scanning of a target using transducers in a pulse-echo mode. Lead zirconate transducers have been developed which can be deployed during reactor shut-down. The first application will be to examine a limited area of the core of PFR. Handling the data from such an experiment involves developing methods for reading and storing the information from such ultrasonic echo. Such techniques have been tested in real time by simulation in a water model. Methods of enhancing the images to be

In-situ monitoring of pitting corrosion on vertically positioned 304 stainless steel by analyzing acoustic-emission energy parameter

International Nuclear Information System (INIS)

Wu, Kaige; Jung, Woo-Sang; Byeon, Jai-Won

2016-01-01

Highlights: • Pitting process in vertically positioned 304 SS is investigated by AE energy. • Gravity-influenced elongated pit, crack and rupture of pit cover were observed. • Hydrogen bubble evolution and pit covers rupturing were separately monitored by AE. • Four stages of AE energy were correlated with observed pitting mechanism. - Abstract: The acoustic emission (AE) energy was analyzed to monitor the pitting process on a vertically positioned 304-stainless steel. The gravity-dependent morphology of the elongated corrosion pits was observed. A scatter plot of the duration and energy indicated two AE clusters with different energy levels. There was a time delay after the detection of the low-energy hydrogen-bubble signals. Subsequently, high-energy signals were observed, whose AE source was attributed to large-scale cracks formed during the rupture of the elongated pit cover. An in-situ analysis of the AE energy evolution provided detailed insights into the corrosion process in relation to the specimen position.

Grading of Chinese Cantonese Sausage Using Hyperspectral Imaging Combined with Chemometric Methods

Science.gov (United States)

Gong, Aiping; Zhu, Susu; He, Yong; Zhang, Chu

2017-01-01

Fast and accurate grading of Chinese Cantonese sausage is an important concern for customers, organizations, and the industry. Hyperspectral imaging in the spectral range of 874–1734 nm, combined with chemometric methods, was applied to grade Chinese Cantonese sausage. Three grades of intact and sliced Cantonese sausages were studied, including the top, first, and second grades. Support vector machine (SVM) and random forests (RF) techniques were used to build two different models. Second derivative spectra and RF were applied to select optimal wavelengths. The optimal wavelengths were the same for intact and sliced sausages when selected from second derivative spectra, while the optimal wavelengths for intact and sliced sausages selected using RF were quite similar. The SVM and RF models, using full spectra and the optimal wavelengths, obtained acceptable results for intact and sliced sausages. Both models for intact sausages performed better than those for sliced sausages, with a classification accuracy of the calibration and prediction set of over 90%. The overall results indicated that hyperspectral imaging combined with chemometric methods could be used to grade Chinese Cantonese sausages, with intact sausages being better suited for grading. This study will help to develop fast and accurate online grading of Cantonese sausages, as well as other sausages. PMID:28757578

A Preliminary Study Application Clustering System in Acoustic Emission Monitoring

Directory of Open Access Journals (Sweden)

Saiful Bahari Nur Amira Afiza

2017-01-01

Full Text Available Acoustic Emission (AE is a non-destructive testing known as assessment on damage detection in structural engineering. It also can be used to discriminate the different types of damage occurring in a composite materials. The main problem associated with the data analysis is the discrimination between the different AE sources and analysis of the AE signal in order to identify the most critical damage mechanism. Clustering analysis is a technique in which the set of object are assigned to a group called cluster. The objective of the cluster analysis is to separate a set of data into several classes that reflect the internal structure of data. In this paper was used k-means algorithm for partitioned clustering method, numerous effort have been made to improve the performance of application k-means clustering algorithm. This paper presents a current review on application clustering system in Acoustic Emission.

Acoustic rhinometry (AR): An Alternative Method to Image Nasal Airway Geometry

DEFF Research Database (Denmark)

Straszek, Sune; Pedersen, O.F.

  ACOUSTIC RHINOMETRY (AR): AN ALTERNATIVE METHOD TO IMAGE NASAL AIRWAY GEOMETRY.  INTRODUCTION AND BACKGROUND:  In human studies the acoustic reflection technique was first applied to describe the area-distance relationship of the lower airways, but later the acoustic reflection technique appeared...... to be of more use in the description of nasal cavity geometry. Applied to human subjects AR has been applied to monitor the effect of corrective surgery and mucosal effects of pharmacological interventions. In recent years, however, AR has found use also in pharmacological studies in animals ranging in size...

Acoustic Emission from Elevator Wire Ropes During Tensile Testing

Science.gov (United States)

Bai, Wenjie; Chai, Mengyu; Li, Lichan; Li, Yongquan; Duan, Quan

The acoustic emission (AE) technique was used to monitor the tensile testing process for two kinds of elevator wire ropes in our work. The AE signals from wire breaks were obtained and analyzed by AE parameters and waveforms. The results showed that AE technique can be a useful tool to monitor wire break phenomenon of wire ropes and effectively capture information of wire break signal. The relationship between AE signal characteristics and wire breaks is investigated and it is found that the most effective acoustic signal discriminators are amplitude and absolute energy. Moreover, the wire break signal of two kinds of ropes is a type of burst signal and it is believed that the waveform and spectrum can be applied to analyze the AE wire break signals.

Acoustic calibration for the KM3NeT pre-production module

Energy Technology Data Exchange (ETDEWEB)

Enzenhöfer, A., E-mail: alexander.enzenhoefer@physik.uni-erlangen.de [Friedrich-Alexander-Universität Erlangen-Nürnberg, Erlangen Centre for Astroparticle Physics, Erwin-Rommel-Str. 1, D-91058 Erlangen (Germany)

2013-10-11

The proposed large scale Cherenkov neutrino telescope KM3NeT will carry photo-sensors on flexible structures, the detection units. The Mediterranean Sea, where KM3NeT will be installed, constitutes a highly dynamic environment in which the detection units are constantly in motion. Thus it is necessary to monitor the exact sensor positions continuously to achieve the desired resolution for the neutrino telescope. A common way to perform this monitoring is the use of acoustic positioning systems with emitters and receivers based on the piezoelectric effect. The acoustic receivers are attached to detection units whereas the emitters are located at known positions on the sea floor. There are complete commercial systems for this application with sufficient precision. But these systems are limited in the use of their data and inefficient as they were designed to perform only this single task. Several working groups in the KM3NeT consortium are cooperating to custom-design a positioning system for the specific requirements of KM3NeT. Most of the studied solutions hold the possibility to extend the application area from positioning to additional tasks like acoustic particle detection or monitoring of the deep-sea acoustic environment. The KM3NeT Pre-Production Module (PPM) is a test system to verify the correct operation and interoperability of the major involved hardware and software components developed for KM3NeT. In the context of the PPM, alternative designs of acoustic sensors including small piezoelectric elements equipped with preamplifiers inside the same housing as the optical sensors will be tested. These will be described in this article.

Numerical Models for the Assessment of Historical Masonry Structures and Materials, Monitored by Acoustic Emission

Directory of Open Access Journals (Sweden)

Stefano Invernizzi

2016-04-01

Full Text Available The paper reviews some recent numerical applications for the interpretation and exploitation of acoustic emission (AE monitoring results obtained from historical masonry structures and materials. Among possible numerical techniques, the finite element method and the distinct method are considered. The analyzed numerical models cover the entire scale range, from microstructure and meso-structure, up to full-size real structures. The micro-modeling includes heterogeneous concrete-like materials, but mainly focuses on the masonry texture meso-structure, where each brick and mortar joint is modeled singularly. The full-size models consider the different typology of historical structures such as masonry towers, cathedrals and chapels. The main difficulties and advantages of the different numerical approaches, depending on the problem typology and scale, are critically analyzed. The main insight we can achieve from micro and meso numerical modeling concerns the scaling of AE as a function of volume and time, since it is also able to simulate the b-value temporal evolution as the damage spread into the structure. The finite element modeling of the whole structure provides useful hints for the optimal placement of the AE sensors, while the combination of AE monitoring results is crucial for a reliable assessment of structural safety.

Monitoring of 3MJ palsed magnet by AE

International Nuclear Information System (INIS)

Nomura, Harehiko; Tateishi, Hiroshi; Komuro, Kazuo; Onishi, Toshitada

1987-01-01

According to a pulse operation of SCM, there appears high voltage which makes difficult to distinguish the resistive voltage from inductive and fluctant potential. We have monitored 3MJ SCM by acoustic emission with applying 44 sensors on the magnet. 4 sensors were located symmetrically between each double pancake. Counts and amplitude of acoustic bursts and also the acoustic epicenter were observed. The monitoring of burst counts continuously during the operation has been found effective for getting reliable pulsed SCM, by knowing fatigue properties of the magnet and the preferable duty cycle of the magnet chargings. (author)

Noncontacting acoustics-based temperature measurement techniques in rapid thermal processing

Science.gov (United States)

Lee, Yong J.; Chou, Ching-Hua; Khuri-Yakub, Butrus T.; Saraswat, Krishna C.

1991-04-01

Temperature measurement of silicon wafers based on the temperature dependence of acoustic waves is studied. The change in the temperature-dependent dispersion relations of the plate modes through the wafer can be exploited to provide a viable temperature monitoring scheme with advantages over both thermocouples and pyrometers. Velocity measurements of acoustic waves through a thin layer of ambient directly above the wafer provides the temperature of the wafer-ambient interface. 1.

Electrochemical monitoring of citric acid production by Aspergillus niger

International Nuclear Information System (INIS)

Kutyła-Olesiuk, Anna; Wawrzyniak, Urszula E.; Ciosek, Patrycja; Wróblewski, Wojciech

2014-01-01

Highlights: • Citric acid fermentation process (production) by Aspergillus niger. • Qualitative/quantitative monitoring of standard culture and culture infected with yeast. • Electronic tongue based on potentiometric and voltammetric sensors. • Evaluation of the progress and the correctness of the fermentation process. • The highest classification abilities of the hybrid electronic tongue. - Abstract: Hybrid electronic tongue was developed for the monitoring of citric acid production by Aspergillus niger. The system based on various potentiometric/voltammetric sensors and appropriate chemometric techniques provided correct qualitative and quantitative classification of the samples collected during standard Aspergillus niger culture and culture infected with yeast. The performance of the proposed approach was compared with the monitoring of the fermentation process carried out using classical methods. The results obtained proved, that the designed hybrid electronic tongue was able to evaluate the progress and correctness of the fermentation process

Electrochemical monitoring of citric acid production by Aspergillus niger

Energy Technology Data Exchange (ETDEWEB)

Kutyła-Olesiuk, Anna; Wawrzyniak, Urszula E.; Ciosek, Patrycja; Wróblewski, Wojciech, E-mail: wuwu@ch.pw.edu.pl

2014-05-01

Highlights: • Citric acid fermentation process (production) by Aspergillus niger. • Qualitative/quantitative monitoring of standard culture and culture infected with yeast. • Electronic tongue based on potentiometric and voltammetric sensors. • Evaluation of the progress and the correctness of the fermentation process. • The highest classification abilities of the hybrid electronic tongue. - Abstract: Hybrid electronic tongue was developed for the monitoring of citric acid production by Aspergillus niger. The system based on various potentiometric/voltammetric sensors and appropriate chemometric techniques provided correct qualitative and quantitative classification of the samples collected during standard Aspergillus niger culture and culture infected with yeast. The performance of the proposed approach was compared with the monitoring of the fermentation process carried out using classical methods. The results obtained proved, that the designed hybrid electronic tongue was able to evaluate the progress and correctness of the fermentation process.

Analysis of acoustic emission signals of fatigue crack growth and corrosion processes. Investigation of the possibilities for continuous condition monitoring of transport containers by acoustic emission testing; Analyse der Schallemissionssignale aus Ermuedungsrisswachstum und Korrosionsprozessen. Untersuchung der Moeglichkeiten fuer die kontinuierliche Zustandsueberwachung von Transportbehaeltern mittels Schallemissionspruefung

Energy Technology Data Exchange (ETDEWEB)

Wachsmuth, Janne

2016-05-01

Fatigue crack growth and active corrosion processes are the main causes of structural failures of transport products like road tankers, railway tank cars and ships. To prevent those failures, preventive, time-based maintenance is performed. However, preventive inspections are costly and include the risk of not detecting a defect, which could lead to a failure within the next service period. An alternative is the idea of continuous monitoring of the whole structure by means of acoustic emission testing (AT). With AT, defects within the material shall be detected and repaired directly after their appearance. Acoustic emission testing is an online non-destructive testing method. Acoustic emission (AE) arises from changes within the material and is transported by elastic waves through the material. If the AE event generates enough energy, the elastic wave propagates to the boundaries of the component, produces a displacement in the picometre scale and can be detected by a piezoelectric sensor. The sensor produces an electrical signal. From this AE signal, AE features such as the maximum amplitude or the frequency can be extracted. Methods of signal analysis are used to investigate the time and frequency dependency of signal groups. The purpose of the signal analysis is to connect the AE signal with the originating AE source. If predefined damage mechanisms are identified, referencing the damage condition of the structure is possible. Acoustic emission from events of the actual crack propagation process can for example lead to the crack growth rate or the stress intensity factor, both specific values from fracture mechanics. A new development in the domain of acoustic emission testing is the pattern recognition of AE signals. Specific features are extracted from the AE signals to assign them to their damage mechanisms. In this thesis the AE signals from the damage mechanisms corrosion and fatigue crack growth are compared and analysed. The damage mechanisms were

Acoustic Emission Stethoscope - Measurements with Acoustic Emission on Wind Turbines

Energy Technology Data Exchange (ETDEWEB)

Krystof Kryniski [AaF Infrastructure, Stockholm (Sweden)

2013-02-15

A remote ultrasonic stethoscope, designed on mobile devices to help a maintenance team in diagnosing drive train problems, has been demonstrated. By implementing an acoustic emission technology, the operating conditions of wind turbines have been assessed by trending techniques and ultrasonic acoustic emission converted into audible sound. The new approach has been developed and tested and compared to other monitoring techniques. Acoustic emission has generally been shown to provide a number of advantages over vibration and shock pulse methods because the system is operating in a substantially higher frequency range (100 kHz) and therefore it is more immune to operation of surrounding machines and components. Quick attenuation of ultrasonic propagation waves in the drive-train structure helps to pin-point the origin of any fault as the signals are sharper and more pronounced. Further, with the intensity measurements a direction of the source of ultrasonic energy can be identified. Using a high frequency thus makes the method suitable for measuring local effects and to determine local defects since the disturbing signals from other parts are damped. Recently developed programmable sensors capable of processing signals onboard, producing quality outputs with extremely low noise-to-signal ratio, have been used. It is discussed how the new approach can lower the cost of a wind-turbine monitoring system, while at the same time making it simple and more reliable, see Appendix A. The method has been tested on rotating parts of wind-turbines, including traditionally difficult areas such as low speed main bearings and planetary gearboxes. The method developed in the project was designed to see physical processes such as friction, impacts and metal removal, occurring when machinery degrades, can be detected and notified with the developed notification system. Apart from reporting the status and displaying the changes of the pre-defined parameters or symptoms, the system has

The role of chemometrics in single and sequential extraction assays: a review. Part II. Cluster analysis, multiple linear regression, mixture resolution, experimental design and other techniques.

Science.gov (United States)

Giacomino, Agnese; Abollino, Ornella; Malandrino, Mery; Mentasti, Edoardo

2011-03-04

Single and sequential extraction procedures are used for studying element mobility and availability in solid matrices, like soils, sediments, sludge, and airborne particulate matter. In the first part of this review we reported an overview on these procedures and described the applications of chemometric uni- and bivariate techniques and of multivariate pattern recognition techniques based on variable reduction to the experimental results obtained. The second part of the review deals with the use of chemometrics not only for the visualization and interpretation of data, but also for the investigation of the effects of experimental conditions on the response, the optimization of their values and the calculation of element fractionation. We will describe the principles of the multivariate chemometric techniques considered, the aims for which they were applied and the key findings obtained. The following topics will be critically addressed: pattern recognition by cluster analysis (CA), linear discriminant analysis (LDA) and other less common techniques; modelling by multiple linear regression (MLR); investigation of spatial distribution of variables by geostatistics; calculation of fractionation patterns by a mixture resolution method (Chemometric Identification of Substrates and Element Distributions, CISED); optimization and characterization of extraction procedures by experimental design; other multivariate techniques less commonly applied. Copyright © 2010 Elsevier B.V. All rights reserved.

Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between April 2009 and September 2009

Energy Technology Data Exchange (ETDEWEB)

Haycox, Jon; Pettitt, Will [ASC, Applied Seismology Consultants, Shrewsbury, Shropshire (United Kingdom)

2009-12-15

This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and changes in pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation (Pettitt et al. 1999), and during stages of canister heating and tunnel pressurisation (Haycox and Pettitt 2005a, b, 2006a, b, Zolezzi et al. 2007, 2008, Duckworth et al. 2008, 2009, Haycox and Duckworth 2009). Further information on the previous monitoring undertaken can be found in Appendix 1. This report covers the period between 1st April 2009 and 30th September 2009 and is the ninth 6-monthly processing and interpretation of the results from the experiment.

Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between October 2009 and March 2010

Energy Technology Data Exchange (ETDEWEB)

Haycox, Jon; Andrews, Jennifer [ASC, Applied Seismology Consultants, Shrewsbury, Shropshire (United Kingdom)

2010-09-15

This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and changes in pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation (Pettitt et al. 1999), and during stages of canister heating and tunnel pressurisation (Haycox and Pettitt 2005a, b, 2006a, b, 2009, Zolezzi et al. 2007, 2008, Duckworth et al. 2008, 2009, Haycox and Duckworth 2009). Further information on the previous monitoring periods can be found in Appendix 1. This report covers the period between 1st October 2009 and 31st March 2010 and is the tenth 6-monthly processing and interpretation of the results from the experiment.

Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between October 2008 and March 2009

Energy Technology Data Exchange (ETDEWEB)

Haycox, Jon; Duckworth, Damion [ASC, Applied Seismology Consultants, Shrewsbury, Shropshire (United Kingdom)

2009-06-15

This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and changes in pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation (Pettitt et al. 1999), and during stages of canister heating and tunnel pressurisation (Haycox and Pettitt 2005a, b, 2006a, b, Zolezzi et al. 2007, 2008, Duckworth et al. 2008, 2009). Further information on the previous monitoring undertaken can be found in Appendix 1. This report covers the period between 1st October 2008 and 31st March 2009 and is the eighth 6-monthly processing and interpretation of the results from the experiment.

Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between April 2010 and September 2010

Energy Technology Data Exchange (ETDEWEB)

Haycox, Jon (ASC Applied Seismology Consultants (United Kingdom))

2011-05-15

This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and changes in pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation (Pettitt et al. 1999), and during stages of canister heating and tunnel pressurisation (Haycox and Pettitt 2005a, b, 2006a, b, Zolezzi et al. 2007, 2008, Duckworth et al. 2008, 2009, Haycox et al. 2009a, b, 2010). Appendix I contains further information about previous monitoring periods. This report covers the period between 1st April 2010 and 30th September 2010 and is the eleventh 6-monthly processing and interpretation of the results from the experiment

Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between October 2008 and March 2009

International Nuclear Information System (INIS)

Haycox, Jon; Duckworth, Damion

2009-06-01

This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and changes in pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation (Pettitt et al. 1999), and during stages of canister heating and tunnel pressurisation (Haycox and Pettitt 2005a, b, 2006a, b, Zolezzi et al. 2007, 2008, Duckworth et al. 2008, 2009). Further information on the previous monitoring undertaken can be found in Appendix 1. This report covers the period between 1st October 2008 and 31st March 2009 and is the eighth 6-monthly processing and interpretation of the results from the experiment

Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between October 2009 and March 2010

International Nuclear Information System (INIS)

Haycox, Jon; Andrews, Jennifer

2010-09-01

This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and changes in pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation (Pettitt et al. 1999), and during stages of canister heating and tunnel pressurisation (Haycox and Pettitt 2005a, b, 2006a, b, 2009, Zolezzi et al. 2007, 2008, Duckworth et al. 2008, 2009, Haycox and Duckworth 2009). Further information on the previous monitoring periods can be found in Appendix 1. This report covers the period between 1st October 2009 and 31st March 2010 and is the tenth 6-monthly processing and interpretation of the results from the experiment

Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between April 2009 and September 2009

International Nuclear Information System (INIS)

Haycox, Jon; Pettitt, Will

2009-12-01

This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and changes in pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation (Pettitt et al. 1999), and during stages of canister heating and tunnel pressurisation (Haycox and Pettitt 2005a, b, 2006a, b, Zolezzi et al. 2007, 2008, Duckworth et al. 2008, 2009, Haycox and Duckworth 2009). Further information on the previous monitoring undertaken can be found in Appendix 1. This report covers the period between 1st April 2009 and 30th September 2009 and is the ninth 6-monthly processing and interpretation of the results from the experiment

Acoustic emission and ultrasonic monitoring results from deposition hole DA3545G01 in the Prototype Repository between April 2010 and September 2010

International Nuclear Information System (INIS)

Haycox, Jon

2011-05-01

This report describes results from acoustic emission (AE) and ultrasonic monitoring around a canister deposition hole (DA3545G01) in the Prototype Repository Experiment at SKB's Hard Rock Laboratory (HRL), Sweden. The monitoring aims to examine changes in the rock mass caused by an experimental repository environment, in particular due to thermal stresses induced from canister heating and changes in pore pressures induced from tunnel sealing. Monitoring of this volume has previously been performed during excavation (Pettitt et al. 1999), and during stages of canister heating and tunnel pressurisation (Haycox and Pettitt 2005a, b, 2006a, b, Zolezzi et al. 2007, 2008, Duckworth et al. 2008, 2009, Haycox et al. 2009a, b, 2010). Appendix I contains further information about previous monitoring periods. This report covers the period between 1st April 2010 and 30th September 2010 and is the eleventh 6-monthly processing and interpretation of the results from the experiment

Use of acoustic vortices in acoustic levitation

DEFF Research Database (Denmark)

Cutanda Henriquez, Vicente; Santillan, Arturo Orozco; Juhl, Peter Møller

2009-01-01

Acoustic fields are known to exert forces on the surfaces of objects. These forces are noticeable if the sound pressure is sufficiently high. Two phenomena where acoustic forces are relevant are: i) acoustic levitation, where strong standing waves can hold small objects at certain positions......, counterbalancing their weight, and ii) acoustic vortices, spinning sound fields that can impinge angular momentum and cause rotation of objects. In this contribution, both force-creating sound fields are studied by means of numerical simulations. The Boundary Element Method is employed to this end. The simulation...... of acoustical vortices uses an efficient numerical implementation based on the superposition of two orthogonal sound fields with a delay of 90° between them. It is shown that acoustic levitation and the use of acoustic vortices can be combined to manipulate objects in an efficient and controlled manner without...

Signal frequency distribution and natural-time analyses from acoustic emission monitoring of an arched structure in the Castle of Racconigi

Directory of Open Access Journals (Sweden)

G. Niccolini

2017-07-01

Full Text Available The stability of an arch as a structural element in the thermal bath of King Charles Albert (Carlo Alberto in the Royal Castle of Racconigi (on the UNESCO World Heritage List since 1997 was assessed by the acoustic emission (AE monitoring technique with application of classical inversion methods to recorded AE data. First, damage source location by means of triangulation techniques and signal frequency analysis were carried out. Then, the recently introduced method of natural-time analysis was preliminarily applied to the AE time series in order to reveal a possible entrance point to a critical state of the monitored structural element. Finally, possible influence of the local seismic and microseismic activity on the stability of the monitored structure was investigated. The criterion for selecting relevant earthquakes was based on the estimation of the size of earthquake preparation zones. The presented results suggest the use of the AE technique as a tool for detecting both ongoing structural damage processes and microseismic activity during preparation stages of seismic events.

Signal frequency distribution and natural-time analyses from acoustic emission monitoring of an arched structure in the Castle of Racconigi

Science.gov (United States)

Niccolini, Gianni; Manuello, Amedeo; Marchis, Elena; Carpinteri, Alberto

2017-07-01

The stability of an arch as a structural element in the thermal bath of King Charles Albert (Carlo Alberto) in the Royal Castle of Racconigi (on the UNESCO World Heritage List since 1997) was assessed by the acoustic emission (AE) monitoring technique with application of classical inversion methods to recorded AE data. First, damage source location by means of triangulation techniques and signal frequency analysis were carried out. Then, the recently introduced method of natural-time analysis was preliminarily applied to the AE time series in order to reveal a possible entrance point to a critical state of the monitored structural element. Finally, possible influence of the local seismic and microseismic activity on the stability of the monitored structure was investigated. The criterion for selecting relevant earthquakes was based on the estimation of the size of earthquake preparation zones. The presented results suggest the use of the AE technique as a tool for detecting both ongoing structural damage processes and microseismic activity during preparation stages of seismic events.

A plan for the North American Bat Monitoring Program (NABat)

Science.gov (United States)

Loeb, Susan C.; Rodhouse, Thomas J.; Ellison, Laura E.; Lausen, Cori L.; Reichard, Jonathan D.; Irvine, Kathryn M.; Ingersoll, Thomas E.; Coleman, Jeremy; Thogmartin, Wayne E.; Sauer, John R.; Francis, Charles M.; Bayless, Mylea L.; Stanley, Thomas R.; Johnson, Douglas H.

2015-01-01

The purpose of the North American Bat Monitoring Program (NABat) is to create a continent-wide program to monitor bats at local to rangewide scales that will provide reliable data to promote effective conservation decisionmaking and the long-term viability of bat populations across the continent. This is an international, multiagency program. Four approaches will be used to gather monitoring data to assess changes in bat distributions and abundances: winter hibernaculum counts, maternity colony counts, mobile acoustic surveys along road transects, and acoustic surveys at stationary points. These monitoring approaches are described along with methods for identifying species recorded by acoustic detectors. Other chapters describe the sampling design, the database management system (Bat Population Database), and statistical approaches that can be used to analyze data collected through this program.

Clinical Studies of Real-Time Monitoring of Lithotripter Performance Using Passive Acoustic Sensors

Science.gov (United States)

Leighton, T. G.; Fedele, F.; Coleman, A. J.; McCarthy, C.; Ryves, S.; Hurrell, A. M.; De Stefano, A.; White, P. R.

2008-09-01

This paper describes the development and clinical testing of a passive device which monitors the passive acoustic emissions generated within the patient's body during Extracorporeal Shock Wave Lithotripsy (ESWL). Designed and clinically tested so that it can be operated by a nurse, the device analyses the echoes generated in the body in response to each ESWL shock, and so gives real time shock-by-shock feedback on whether the stone was at the focus of the lithotripter, and if so whether the previous shock contributed to stone fragmentation when that shock reached the focus. A shock is defined as being `effective' if these two conditions are satisfied. Not only can the device provide real-time feedback to the operator, but the trends in shock `effectiveness' can inform treatment. In particular, at any time during the treatment (once a statistically significant number of shocks have been delivered), the percentage of shocks which were `effective' provides a treatment score TS(t) which reflects the effectiveness of the treatment up to that point. The TS(t) figure is automatically delivered by the device without user intervention. Two clinical studies of the device were conducted, the ethics guidelines permitting only use of the value of TS(t) obtained at the end of treatment (this value is termed the treatment score TS0). The acoustically-derived treatment score was compared with the treatment score CTS2 given by the consultant urologist at the three-week patient's follow-up appointment. In the first clinical study (phase 1), records could be compared for 30 out of the 118 patients originally recruited, and the results of phase 1 were used to refine the parameter values (the `rules') with which the acoustic device provides its treatment score. These rules were tested in phase 2, for which records were compared for 49 of the 85 patients recruited. Considering just the phase 2 results (since the phase 1 data were used to draw up the `rules' under which phase 2 operated

Chemometric characterization of the hydrogen bonding complexes of secondary amides and aromatic hydrocarbons

OpenAIRE

Jović, Branislav; Nikolić, Aleksandar; Petrović, Slobodan

2012-01-01

The paper reports the results of the study of hydrogen bonding complexes between secondary amides and various aromatic hydrocarbons. The possibility of using chemometric methods was investigated in order to characterize N-H•••π hydrogen bonded complexes. Hierarchical clustering and Principal Component Analysis (PCA) have been applied on infrared spectroscopic and Taft parameters of 43 N-substituted amide complexes with different aromatic hydrocarbons. Results obtained in this report are...

Acoustic emission from fuel pellets in a simulated reactor environment

International Nuclear Information System (INIS)

Kupperman, D.S.; Kennedy, C.R.; Reimann, K.J.

1977-01-01

Thermal-shock damage of nuclear reactor fuel pellets in a simulated reactor environment has been correlated with acoustic-emission data obtained from sensors placed on extensions of the electrical feedthroughs. Ringdown counts, rms output data, and event-location data has been acquired for experiments carried out with single pellets as well as multiple pellet stacks. These tests have shown that acoustic-emission monitoring can provide information indicating the onset and the extent of cracking

IMMAN: free software for information theory-based chemometric analysis.

Science.gov (United States)

Urias, Ricardo W Pino; Barigye, Stephen J; Marrero-Ponce, Yovani; García-Jacas, César R; Valdes-Martiní, José R; Perez-Gimenez, Facundo

2015-05-01

The features and theoretical background of a new and free computational program for chemometric analysis denominated IMMAN (acronym for Information theory-based CheMoMetrics ANalysis) are presented. This is multi-platform software developed in the Java programming language, designed with a remarkably user-friendly graphical interface for the computation of a collection of information-theoretic functions adapted for rank-based unsupervised and supervised feature selection tasks. A total of 20 feature selection parameters are presented, with the unsupervised and supervised frameworks represented by 10 approaches in each case. Several information-theoretic parameters traditionally used as molecular descriptors (MDs) are adapted for use as unsupervised rank-based feature selection methods. On the other hand, a generalization scheme for the previously defined differential Shannon's entropy is discussed, as well as the introduction of Jeffreys information measure for supervised feature selection. Moreover, well-known information-theoretic feature selection parameters, such as information gain, gain ratio, and symmetrical uncertainty are incorporated to the IMMAN software ( http://mobiosd-hub.com/imman-soft/ ), following an equal-interval discretization approach. IMMAN offers data pre-processing functionalities, such as missing values processing, dataset partitioning, and browsing. Moreover, single parameter or ensemble (multi-criteria) ranking options are provided. Consequently, this software is suitable for tasks like dimensionality reduction, feature ranking, as well as comparative diversity analysis of data matrices. Simple examples of applications performed with this program are presented. A comparative study between IMMAN and WEKA feature selection tools using the Arcene dataset was performed, demonstrating similar behavior. In addition, it is revealed that the use of IMMAN unsupervised feature selection methods improves the performance of both IMMAN and WEKA

Spatial Air Quality Modelling Using Chemometrics Techniques: A Case Study in Peninsular Malaysia

International Nuclear Information System (INIS)

Azman Azid; Hafizan Juahir; Mohammad Azizi Amran; Zarizal Suhaili; Mohamad Romizan Osman; Asyaari Muhamad; Asyaari Muhamad; Ismail Zainal Abidin; Nur Hishaam Sulaiman; Ahmad Shakir Mohd Saudi

2015-01-01

This study shows the effectiveness of hierarchical agglomerative cluster analysis (HACA), discriminant analysis (DA), principal component analysis (PCA), and multiple linear regressions (MLR) for assessment of air quality data and recognition of air pollution sources. 12 months data (January-December 2007) consisting of 14 stations in Peninsular Malaysia with 14 parameters were applied. Three significant clusters - low pollution source (LPS), moderate pollution source (MPS), and slightly high pollution source (SHPS) were generated via HACA. Forward stepwise of DA managed to discriminate eight variables, whereas backward stepwise of DA managed to discriminate nine variables out of fourteen variables. The PCA and FA results show the main contributor of air pollution in Peninsular Malaysia is the combustion of fossil fuel from industrial activities, transportation and agriculture systems. Four MLR models show that PM_1_0 account as the most and the highest pollution contributor to Malaysian air quality. From the study, it can be stipulated that the application of chemometrics techniques can disclose meaningful information on the spatial variability of a large and complex air quality data. A clearer review about the air quality and a novelty design of air quality monitoring network for better management of air pollution can be achieved via these methods. (author)

Application of Raman spectroscopy and chemometric techniques to assess sensory characteristics of young dairy bull beef.

Science.gov (United States)

Zhao, Ming; Nian, Yingqun; Allen, Paul; Downey, Gerard; Kerry, Joseph P; O'Donnell, Colm P

2018-05-01

This work aims to develop a rapid analytical technique to predict beef sensory attributes using Raman spectroscopy (RS) and to investigate correlations between sensory attributes using chemometric analysis. Beef samples (n = 72) were obtained from young dairy bulls (Holstein-Friesian and Jersey×Holstein-Friesian) slaughtered at 15 and 19 months old. Trained sensory panel evaluation and Raman spectral data acquisition were both carried out on the same longissimus thoracis muscles after ageing for 21 days. The best prediction results were obtained using a Raman frequency range of 1300-2800 cm -1 . Prediction performance of partial least squares regression (PLSR) models developed using all samples were moderate to high for all sensory attributes (R 2 CV values of 0.50-0.84 and RMSECV values of 1.31-9.07) and were particularly high for desirable flavour attributes (R 2 CVs of 0.80-0.84, RMSECVs of 4.21-4.65). For PLSR models developed on subsets of beef samples i.e. beef of an identical age or breed type, significant improvements on prediction performances were achieved for overall sensory attributes (R 2 CVs of 0.63-0.89 and RMSECVs of 0.38-6.88 for each breed type; R 2 CVs of 0.52-0.89 and RMSECVs of 0.96-6.36 for each age group). Chemometric analysis revealed strong correlations between sensory attributes. Raman spectroscopy combined with chemometric analysis was demonstrated to have high potential as a rapid and non-destructive technique to predict the sensory quality traits of young dairy bull beef. Copyright © 2018. Published by Elsevier Ltd.

A modern approach to the authentication and quality assessment of thyme using UV spectroscopy and chemometric analysis.

Science.gov (United States)

Gad, Haidy A; El-Ahmady, Sherweit H; Abou-Shoer, Mohamed I; Al-Azizi, Mohamed M

2013-01-01

Recently, the fields of chemometrics and multivariate analysis have been widely implemented in the quality control of herbal drugs to produce precise results, which is crucial in the field of medicine. Thyme represents an essential medicinal herb that is constantly adulterated due to its resemblance to many other plants with similar organoleptic properties. To establish a simple model for the quality assessment of Thymus species using UV spectroscopy together with known chemometric techniques. The success of this model may also serve as a technique for the quality control of other herbal drugs. The model was constructed using 30 samples of authenticated Thymus vulgaris and challenged with 20 samples of different botanical origins. The methanolic extracts of all samples were assessed using UV spectroscopy together with chemometric techniques: principal component analysis (PCA), soft independent modeling of class analogy (SIMCA) and hierarchical cluster analysis (HCA). The model was able to discriminate T. vulgaris from other Thymus, Satureja, Origanum, Plectranthus and Eriocephalus species, all traded in the Egyptian market as different types of thyme. The model was also able to classify closely related species in clusters using PCA and HCA. The model was finally used to classify 12 commercial thyme varieties into clusters of species incorporated in the model as thyme or non-thyme. The model constructed is highly recommended as a simple and efficient method for distinguishing T. vulgaris from other related species as well as the classification of marketed herbs as thyme or non-thyme. Copyright © 2013 John Wiley & Sons, Ltd.

Monitoring of Acoustic Emission During the Disintegration of Rock

Czech Academy of Sciences Publication Activity Database

Tripathi, R.; Srivastava, M.; Hloch, Sergej; Adamčík, P.; Chattopadhyaya, S.; Das, A. K.

2016-01-01

Roč. 149, č. 149 (2016), s. 481-488 E-ISSN 1877-7058. [International Conference on Manufacturing Engineering and Materials, ICMEM 2016. Nový Smokovec, 06.06.2016-10.06.2016] R&D Projects: GA MŠk ED2.1.00/03.0082; GA MŠk(CZ) LO1406 Institutional support: RVO:68145535 Keywords : acoustic emission * rock disintegration * waterjet Subject RIV: JQ - Machines ; Tools http://www.sciencedirect.com/science/article/pii/S1877705816312127

Translational illusion of acoustic sources by transformation acoustics.

Science.gov (United States)

Sun, Fei; Li, Shichao; He, Sailing

2017-09-01

An acoustic illusion of creating a translated acoustic source is designed by utilizing transformation acoustics. An acoustic source shifter (ASS) composed of layered acoustic metamaterials is designed to achieve such an illusion. A practical example where the ASS is made with naturally available materials is also given. Numerical simulations verify the performance of the proposed device. The designed ASS may have some applications in, e.g., anti-sonar detection.

Contrasting movements and connectivity of reef-associated sharks using acoustic telemetry: implications for management.

Science.gov (United States)

Espinoza, Mario; Lédée, Elodie J I; Simpfendorfer, Colin A; Tobin, Andrew J; Heupel, Michelle R

2015-12-01

Understanding the efficacy of marine protected areas (MPAs) for wide-ranging predators is essential to designing effective management and conservation approaches. The use of acoustic monitoring and network analysis can improve our understanding of the spatial ecology and functional connectivity of reef-associated species, providing a useful approach for reef-based conservation planning. This study compared and contrasted the movement and connectivity of sharks with different degrees of reef association. We examined the residency, dispersal, degree of reef connectivity, and MPA use of grey reef (Carcharhinus amblyrhynchos), silvertip (C. albimarginatus), and bull (C. leucas) sharks monitored in the central Great Barrier Reef (GBR). An array of 56 acoustic receivers was used to monitor shark movements on 17 semi-isolated reefs. Carcharhinus amblyrhynchos and C. albimarginatus were detected most days at or near their tagging reef. However, while C. amblyrhynchos spent 80% of monitoring days in the array, C. albimarginatus was only detected 50% of the time. Despite both species moving similar distances (sharks like C. leucas, a combination of spatial planning and other alternative measures is critical. Our findings demonstrate that acoustic monitoring can serve as a useful platform for designing more effective MPA networks for reef predators displaying a range of movement patterns.

Age group estimation in free-ranging African elephants based on acoustic cues of low-frequency rumbles

OpenAIRE

Stoeger, Angela S.; Zeppelzauer, Matthias; Baotic, Anton

2014-01-01

Animal vocal signals are increasingly used to monitor wildlife populations and to obtain estimates of species occurrence and abundance. In the future, acoustic monitoring should function not only to detect animals, but also to extract detailed information about populations by discriminating sexes, age groups, social or kin groups, and potentially individuals. Here we show that it is possible to estimate age groups of African elephants (Loxodonta africana) based on acoustic parameters extracte...

Experimental Design, Near-Infrared Spectroscopy, and Multivariate Calibration: An Advanced Project in a Chemometrics Course

Science.gov (United States)

de Oliveira, Rodrigo R.; das Neves, Luiz S.; de Lima, Kassio M. G.

2012-01-01

A chemometrics course is offered to students in their fifth semester of the chemistry undergraduate program that includes an in-depth project. Students carry out the project over five weeks (three 8-h sessions per week) and conduct it in parallel to other courses or other practical work. The students conduct a literature search, carry out…

Chemometrics approach to substrate development, case: semisyntetic cheese

DEFF Research Database (Denmark)

Nielsen, Per Væggemose; Hansen, Birgitte Vedel

1998-01-01

from food production facilities.The Chemometrics approach to substrate development is illustrated by the development of a semisyntetic cheese substrate. Growth, colour formation and mycotoxin production of 6 cheese related fungi were studied on 9 types of natural cheeses and 24 synthetic cheese......, the most frequently occurring contaminant on semi-hard cheese. Growth experiments on the substrate were repeatable and reproducible. The substrate was also suitable for the starter P. camemberti. Mineral elements in cheese were shown to have strong effect on growth, mycotoxin production and colour...... formation of fungi. For P. roqueforti, P. discolor, P. verrucosum and Aspergillus versicolor the substrate was less suitable as a model cheese substrate, which indicates great variation in nutritional demands of the fungi. Substrates suitable for studies of specific cheese types was found for P. roqueforti...

Structural Analysis of Multi-component Amyloid Systems by Chemometric SAXS Data Decomposition

DEFF Research Database (Denmark)

Trillo, Isabel Fatima Herranz; Jensen, Minna Grønning; van Maarschalkerweerd, Andreas

2017-01-01

Formation of amyloids is the hallmark of several neurodegenerative pathologies. Structural investigation of these complex transformation processes poses significant experimental challenges due to the co-existence of multiple species. The additive nature of small-angle X-ray scattering (SAXS) data...... least squares (MCR-ALS) chemometric method. The approach enables rigorous and robust decomposition of synchrotron SAXS data by simultaneously introducing these data in different representations that emphasize molecular changes at different time and structural resolution ranges. The approach has allowed...

Fourier transform infrared spectroscopy and chemometrics for the characterization and discrimination of writing/photocopier paper types: Application in forensic document examinations.

Science.gov (United States)

Kumar, Raj; Kumar, Vinay; Sharma, Vishal

2017-01-05

The aim of the present work is to explore the non-destructive application of ATR-FTIR technique for characterization and discrimination of paper samples which could be helpful to give forensic aid in resolving legal cases. Twenty-four types of paper brands were purchased from local market in and around Chandigarh, India. All the paper samples were subjected to ATR-FTIR analysis from 400 to 4000cm(-1) wavenumber range. The qualitative feature and Chemometrics of the obtained spectral data are used for characterization and discrimination. Characterization is achieved by matching the peaks with standards of cellulose and inorganic fillers, a usual constituents of paper. Three different regions of IR, i.e. 400-2000cm(-1), 2000-4000cm(-1) and 400-4000cm(-1) were selected for differentiation by Chemometrics analysis. The discrimination is achieved on the basis of three principal components, i.e. PC 1, PC 2 and PC 3. It is observed that maximum discrimination was procured in the wave number range of i.e. 2000-4000cm(-1). Discriminating power was calculated on the basis of qualitative features as well, and it is found that the discrimination of paper samples was better achieved by Chemometrics analysis rather than qualitative features. The discriminating power by Chemometrics is 99.64% and which is larger as ever achieved by any group for present number of samples. The present result confirms that this study will be highly useful in forensic document examination work in the legal cases, where the authenticity of the document is challenged. The results are completely analytical and, therefore, overcome the problem encounter in traditional routine light/radiation scanning methods which are still in practice by various questioned document laboratories. Copyright © 2016 Elsevier B.V. All rights reserved.

Fourier transform infrared spectroscopy and chemometrics for the characterization and discrimination of writing/photocopier paper types: Application in forensic document examinations

Science.gov (United States)

Kumar, Raj; Kumar, Vinay; Sharma, Vishal

2017-01-01

The aim of the present work is to explore the non-destructive application of ATR-FTIR technique for characterization and discrimination of paper samples which could be helpful to give forensic aid in resolving legal cases. Twenty-four types of paper brands were purchased from local market in and around Chandigarh, India. All the paper samples were subjected to ATR-FTIR analysis from 400 to 4000 cm- 1 wavenumber range. The qualitative feature and Chemometrics of the obtained spectral data are used for characterization and discrimination. Characterization is achieved by matching the peaks with standards of cellulose and inorganic fillers, a usual constituents of paper. Three different regions of IR, i.e. 400-2000 cm- 1, 2000-4000 cm- 1 and 400-4000 cm- 1 were selected for differentiation by Chemometrics analysis. The discrimination is achieved on the basis of three principal components, i.e. PC 1, PC 2 and PC 3. It is observed that maximum discrimination was procured in the wave number range of i.e. 2000-4000 cm- 1. Discriminating power was calculated on the basis of qualitative features as well, and it is found that the discrimination of paper samples was better achieved by Chemometrics analysis rather than qualitative features. The discriminating power by Chemometrics is 99.64% and which is larger as ever achieved by any group for present number of samples. The present result confirms that this study will be highly useful in forensic document examination work in the legal cases, where the authenticity of the document is challenged. The results are completely analytical and, therefore, overcome the problem encounter in traditional routine light/radiation scanning methods which are still in practice by various questioned document laboratories.

An experimental modeling and acoustic emission monitoring of abrasive wear in a steel/diabase pair

Science.gov (United States)

Korchuganov, M. A.; Filippov, A. V.; Tarasov, S. Yu.; Podgornyh, O. A.; Shamarin, N. N.; Filippova, E. O.

2016-11-01

The earthmoving of permafrost soil is a critical task for excavation of minerals and construction on new territories. Failure by abrasive wear is the main reason for excavation parts of earthmoving and soil cutting machines. Therefore investigation of this type of wear is a challenge for developing efficient and wear resistant working parts. This paper is focused on conducting tribological experiments with sliding the steel samples over the surface of diabase stone sample where abrasive wear conditions of soil cutting are modeled experimentally. The worn surfaces of all samples have been examined and transfer of metal and stone particles revealed. The acoustic emission (AE) signals have been recorded and related to the results of worn surface analysis. he acoustic emission (AE) signals have been recorded and related to the results of worn surface analysis. As shown the wear intensity correlates to that of acoustic emission. Both acoustic emission signal median frequency and energy are found to be sensitive to the wear mode.

Characterization and authentication of Spanish PDO wine vinegars using multidimensional fluorescence and chemometrics

DEFF Research Database (Denmark)

Ríos-Reina, Rocío; Elcoroaristizabal, Saioa; Ocaña-Gonzalez, Juan A.

2017-01-01

This work assesses the potential of multidimensional fluorescence spectroscopy combined with chemometrics for characterization and authentication of Spanish Protected Designation of Origin (PDO) wine vinegars. Seventy-nine vinegars of different categories (aged and sweet) belonging to the Spanish...... obtained better results (>92% of classification). In each category, SVM also allows the differentiation between PDOs. The proposed methodology could be used as an analysis method for the authentication of Spanish PDO wine vinegars....

Longitudinal acoustic properties of poly(lactic acid) and poly(lactic-co-glycolic acid)

International Nuclear Information System (INIS)

Parker, N G; Povey, M J W; Mather, M L; Morgan, S P

2010-01-01

Acoustics offers rich possibilities for characterizing and monitoring the biopolymer structures being employed in the field of biomedical engineering. Here we explore the rudimentary acoustic properties of two common biodegradable polymers: poly(lactic acid) and poly(lactic-co-glycolic acid). A pulse-echo technique is developed to reveal the bulk speed of sound, acoustic impedance and acoustic attenuation of small samples of the polymer across a pertinent temperature range of 0-70 0 C. The glass transition appears markedly as both a discontinuity in the first derivative of the speed of sound and a sharp increase in the acoustic attenuation. We further extend our analysis to consider the role of ethanol, whose presence is observed to dramatically modify the acoustic properties and reduce the glass transition temperature of the polymers. Our results highlight the sensitivity of acoustic properties to a range of bulk properties, including visco-elasticity, molecular weight, co-polymer ratio, crystallinity and the presence of plasticizers.

Real-time monitoring of focused ultrasound blood-brain barrier opening via subharmonic acoustic emission detection: implementation of confocal dual-frequency piezoelectric transducers

Science.gov (United States)

Tsai, Chih-Hung; Zhang, Jia-Wei; Liao, Yi-Yi; Liu, Hao-Li

2016-04-01

Burst-tone focused ultrasound exposure in the presence of microbubbles has been demonstrated to be effective at inducing temporal and local opening of the blood-brain barrier (BBB), which promises significant clinical potential to deliver therapeutic molecules into the central nervous system (CNS). Traditional contrast-enhanced imaging confirmation after focused ultrasound (FUS) exposure serves as a post-operative indicator of the effectiveness of FUS-BBB opening, however, an indicator that can concurrently report the BBB status and BBB-opening effectiveness is required to provide effective feedback to implement this treatment clinically. In this study, we demonstrate the use of subharmonic acoustic emission detection with implementation on a confocal dual-frequency piezoelectric ceramic structure to perform real-time monitoring of FUS-BBB opening. A confocal dual-frequency (0.55 MHz/1.1 MHz) focused ultrasound transducer was designed. The 1.1 MHz spherically-curved ceramic was employed to deliver FUS exposure to induce BBB-opening, whereas the outer-ring 0.55 MHz ceramic was employed to detect the subharmonic acoustic emissions originating from the target position. In stage-1 experiments, we employed spectral analysis and performed an energy spectrum density (ESD) calculation. An optimized 0.55 MHz ESD level change was shown to effectively discriminate the occurrence of BBB-opening. Wideband acoustic emissions received from 0.55 MHz ceramics were also analyzed to evaluate its correlations with erythrocyte extravasations. In stage-2 real-time monitoring experiments, we applied the predetermined ESD change as a detection threshold in PC-controlled algorithm to predict the FUS exposure intra-operatively. In stage-1 experiment, we showed that subharmonic ESD presents distinguishable dynamics between intact BBB and opened BBB, and therefore a threshold ESD change level (5.5 dB) can be identified for BBB-opening prediction. Using this ESD change threshold detection as a

Real-time monitoring of focused ultrasound blood-brain barrier opening via subharmonic acoustic emission detection: implementation of confocal dual-frequency piezoelectric transducers

International Nuclear Information System (INIS)

Tsai, Chih-Hung; Zhang, Jia-Wei; Liao, Yi-Yi; Liu, Hao-Li

2016-01-01

Burst-tone focused ultrasound exposure in the presence of microbubbles has been demonstrated to be effective at inducing temporal and local opening of the blood-brain barrier (BBB), which promises significant clinical potential to deliver therapeutic molecules into the central nervous system (CNS). Traditional contrast-enhanced imaging confirmation after focused ultrasound (FUS) exposure serves as a post-operative indicator of the effectiveness of FUS-BBB opening, however, an indicator that can concurrently report the BBB status and BBB-opening effectiveness is required to provide effective feedback to implement this treatment clinically. In this study, we demonstrate the use of subharmonic acoustic emission detection with implementation on a confocal dual-frequency piezoelectric ceramic structure to perform real-time monitoring of FUS-BBB opening. A confocal dual-frequency (0.55 MHz/1.1 MHz) focused ultrasound transducer was designed. The 1.1 MHz spherically-curved ceramic was employed to deliver FUS exposure to induce BBB-opening, whereas the outer-ring 0.55 MHz ceramic was employed to detect the subharmonic acoustic emissions originating from the target position. In stage-1 experiments, we employed spectral analysis and performed an energy spectrum density (ESD) calculation. An optimized 0.55 MHz ESD level change was shown to effectively discriminate the occurrence of BBB-opening. Wideband acoustic emissions received from 0.55 MHz ceramics were also analyzed to evaluate its correlations with erythrocyte extravasations. In stage-2 real-time monitoring experiments, we applied the predetermined ESD change as a detection threshold in PC-controlled algorithm to predict the FUS exposure intra-operatively. In stage-1 experiment, we showed that subharmonic ESD presents distinguishable dynamics between intact BBB and opened BBB, and therefore a threshold ESD change level (5.5 dB) can be identified for BBB-opening prediction. Using this ESD change threshold detection as a

Integration of acoustic emission systems within Integri-TechTM analysis system for structural health monitoring of pressurised engineering plant

International Nuclear Information System (INIS)

Ghouri, A A; Galbraith, Walter; Pierce, S Gareth; Gachagan, Anthony; Rafferty, Steven; Pickwell, Andy

2015-01-01

The aim of this Acoustic Emission (AE) based Structural Health Monitoring project is to enable accurate location of AE sources in pressurised engineering plant and to use AE source location data to establish defect locations for use within Integri-Tech TM ; a finite element based analysis, monitoring and fitness for service assessment system. Integri-Tech TM is a windows based system which carries out combined analysis and assessment providing fatigue life and remnant life calculations and inspection priorities presenting the results in an accessible web portal format. The software uses finite element stress models created in the companion software Model Wizard. The AE monitoring system that has been developed can be used with an array of up to four AE broad band sensor channels with associated signal processing. Using a flexible approach in MATLAB, the authors have developed algorithms which were used for analysing the received AE signals to extract information about the nature and location of the source. The ability to carry out source location and possibly perform real time monitoring (detecting cracking as it occurs) is attractive feature of the AE system developed for this project. The time of arrival (TOA) data was used by Integri-Tech TM software to calculate source location using its own built-in algorithm, and this was verified independently using a MATLAB approach. (paper)

Characterizing Focused-Ultrasound Mediated Drug Delivery to the Heterogeneous Primate Brain In Vivo with Acoustic Monitoring

Science.gov (United States)

Wu, Shih-Ying; Sanchez, Carlos Sierra; Samiotaki, Gesthimani; Buch, Amanda; Ferrera, Vincent P.; Konofagou, Elisa E.

2016-11-01

Focused ultrasound with microbubbles has been used to noninvasively and selectively deliver pharmacological agents across the blood-brain barrier (BBB) for treating brain diseases. Acoustic cavitation monitoring could serve as an on-line tool to assess and control the treatment. While it demonstrated a strong correlation in small animals, its translation to primates remains in question due to the anatomically different and highly heterogeneous brain structures with gray and white matteras well as dense vasculature. In addition, the drug delivery efficiency and the BBB opening volume have never been shown to be predictable through cavitation monitoring in primates. This study aimed at determining how cavitation activity is correlated with the amount and concentration of gadolinium delivered through the BBB and its associated delivery efficiency as well as the BBB opening volume in non-human primates. Another important finding entails the effect of heterogeneous brain anatomy and vasculature of a primate brain, i.e., presence of large cerebral vessels, gray and white matter that will also affect the cavitation activity associated with variation of BBB opening in different tissue types, which is not typically observed in small animals. Both these new findings are critical in the primate brain and provide essential information for clinical applications.

Acoustic Emission based on sentry function to monitor the initiation of delamination in composite materials

International Nuclear Information System (INIS)

Bakhtiary Davijani, A.A.; Hajikhani, M.; Ahmadi, M.

2011-01-01

Research highlights: → Constant load does not confirm constant damage in composite materials. → Different damages have different AE events. → Sentry function is a useful tool to monitor the initiation of damage in delamination. → The less sentry function number is the more damage the material has endured. -- Abstract: Delamination is the most common failure mode in composite materials, since it will result in the reduction of stiffness and can grow throughout other layers. Delamination is consisted of two main stages including initiation and propagation. Understanding the behavior of the material in these zones is very important, hence it has been thoroughly studied by different methods such as numerical methods, Acoustic Emission (AE), and modeling. Between these two regions initiation is a more vital stage in the delamination of the material. Once initiation occurs, which normally requires greater amount of force, cracks can easily propagate through the structure with little force and cause the failure of the structure. A better knowledge of initiation can lead to better design and production of stronger materials. Additionally, more knowledge about crack initiation and its internal microevents would help improve other parameters and result in higher strength against crack initiation. AE is a suitable method for in situ monitoring of damage in composite materials. In this study, AE was applied to test different glass/epoxy specimens which were loaded under mode I delamination. A function that combines AE and mechanical information is employed to investigate the initiation of delamination. Scanning electron microscope (SEM) was used to verify the results of this function. It is shown that this method is an appropriate technique to monitor the behavior of the initiation of delamination.

Acoustic measurements of soil-pipeflow and internal erosion

Science.gov (United States)

Internal erosion of soil pipes can lead to embankment failures, landslides, and gully erosion. Therefore, non-intrusive methods are needed to detect and monitor soil pipeflow and the resulting internal erosion. This paper presents a laboratory study using both active and passive acoustic techniques ...

Induced clustering of Escherichia coli by acoustic fields.

Science.gov (United States)

Gutiérrez-Ramos, Salomé; Hoyos, Mauricio; Ruiz-Suárez, J C

2018-03-16

Brownian or self-propelled particles in aqueous suspensions can be trapped by acoustic fields generated by piezoelectric transducers usually at frequencies in the megahertz. The obtained confinement allows the study of rich collective behaviours like clustering or spreading dynamics in microgravity-like conditions. The acoustic field induces the levitation of self-propelled particles and provides secondary lateral forces to capture them at nodal planes. Here, we give a step forward in the field of confined active matter, reporting levitation experiments of bacterial suspensions of Escherichia coli. Clustering of living bacteria is monitored as a function of time, where different behaviours are clearly distinguished. Upon the removal of the acoustic signal, bacteria rapidly spread, impelled by their own swimming. Nevertheless, long periods of confinement result in irreversible bacteria entanglements that could act as seeds for levitating bacterial aggregates.

Status reports on developments and applications of acoustic emission analysis. Lectures

International Nuclear Information System (INIS)

1994-01-01

The 25 lectures give a survey of the field of acoustic emission analysis. After a state-of-the-art report, the 4 new SE regulations of the DGZfP are presented which will standardize the applications of acoustic emission analysis. Acoustic emission sources and signal processing, including 3D detection, are discussed in 5 papers. After this, the practical applications of acoustic emission analysis are discussed in detail: Testing of gas tanks, inspection of storage container bottoms, reinforced concrete (3D analysis during extension testing), polymer-impregnated concrete, glass (testing up to 90 MHz), ceramics (thermoshock behaviour), fibre-reinforced plastics (4 contributions), PVD films, rock (analysis of workability and structure), glued joints between metals, monitoring of laser beam welding, metal cutting, and drying of cut wood. (orig.) [de

Acoustical User Identification Based on MFCC Analysis of Keystrokes

Directory of Open Access Journals (Sweden)

Matus Pleva

2015-01-01

Full Text Available This paper introduces a novel approach of person identification using acoustical monitoring of typing the required word on the monitored keyboard. This experiment was motivated by the idea of COST IC1106 (Integrating Biometrics and Forensics for the Digital Age partners to acoustically analyse the captured keystroke dynamics database using widely used time-invariant mathematical models tools. The MFCC (Mel-Frequency Cepstral Coefficients and HMM (Hidden Markov Models was introduced in this experiment, which gives promising results of 99.33% accuracy, when testing 25% of realizations (randomly selected from 100 identifying between 50 users/models. The experiment was repeated for different training/testing configurations and cross-validated, so this first approach could be a good starting point for next research including feature selection algorithms, biometric authentication score normalization, different audio & keyboard setup tests, etc.

Near infrared system coupled chemometric algorithms for enumeration of total fungi count in cocoa beans neat solution.

Science.gov (United States)

Kutsanedzie, Felix Y H; Chen, Quansheng; Hassan, Md Mehedi; Yang, Mingxiu; Sun, Hao; Rahman, Md Hafizur

2018-02-01

Total fungi count (TFC) is a quality indicator of cocoa beans when unmonitored leads to quality and safety problems. Fourier transform near infrared spectroscopy (FT-NIRS) combined with chemometric algorithms like partial least square (PLS); synergy interval-PLS (Si-PLS); synergy interval-genetic algorithm-PLS (Si-GAPLS); Ant colony optimization - PLS (ACO-PLS) and competitive-adaptive reweighted sampling-PLS (CARS-PLS) was employed to predict TFC in cocoa beans neat solution. Model results were evaluated using the correlation coefficients of the prediction (Rp) and calibration (Rc); root mean square error of prediction (RMSEP), and the ratio of sample standard deviation to RMSEP (RPD). The developed models performance yielded 0.951≤Rp≤0.975; and 3.15≤RPD≤4.32. The models' prediction stability improved in the order of PLSmonitoring. Copyright © 2017 Elsevier Ltd. All rights reserved.

Classification of Tempranillo wines according to geographic origin: Combination of mass spectrometry based electronic nose and chemometrics

Energy Technology Data Exchange (ETDEWEB)

Cynkar, Wies, E-mail: wies.cynkar@awri.com.au [Australian Wine Research Institute, PO Box 197, Glen Osmond, SA 5064 (Australia); Dambergs, Robert [Australian Wine Research Institute, Tasmanian Institute of Agricultural Research, University of Tasmania, Private Bag 98, Hobart Tasmania 7001 (Australia); Smith, Paul; Cozzolino, Daniel [Australian Wine Research Institute, PO Box 197, Glen Osmond, SA 5064 (Australia)

2010-02-15

Rapid methods employing instruments such as electronic noses (EN) or gas sensors are used in the food and beverage industries to monitor and assess the composition and quality of products. Similar to other food industries, the wine industry has a clear need for simple, rapid and cost effective techniques for objectively evaluating the quality of grapes, wine and spirits. In this study a mass spectrometry based electronic nose (MS-EN) instrument combined with chemometrics was used to predict the geographical origin of Tempranillo wines produced in Australia and Spain. The MS-EN data generated were analyzed using principal components analysis (PCA), partial least squares discriminant analysis (PLS-DA) and stepwise linear discriminant analysis (SLDA) with full cross validation (leave-one-out method). The SLDA classified correctly 86% of the samples while PLS-DA 85% of Tempranillo wines according to their geographical origin. The relative benefits of using MS-EN will provide capability for rapid screening of wines. However, this technique does not provide the identification and quantitative determination of individual compounds responsible for the different aroma notes in the wine.

Classification of Tempranillo wines according to geographic origin: Combination of mass spectrometry based electronic nose and chemometrics

International Nuclear Information System (INIS)

Cynkar, Wies; Dambergs, Robert; Smith, Paul; Cozzolino, Daniel

2010-01-01

Rapid methods employing instruments such as electronic noses (EN) or gas sensors are used in the food and beverage industries to monitor and assess the composition and quality of products. Similar to other food industries, the wine industry has a clear need for simple, rapid and cost effective techniques for objectively evaluating the quality of grapes, wine and spirits. In this study a mass spectrometry based electronic nose (MS-EN) instrument combined with chemometrics was used to predict the geographical origin of Tempranillo wines produced in Australia and Spain. The MS-EN data generated were analyzed using principal components analysis (PCA), partial least squares discriminant analysis (PLS-DA) and stepwise linear discriminant analysis (SLDA) with full cross validation (leave-one-out method). The SLDA classified correctly 86% of the samples while PLS-DA 85% of Tempranillo wines according to their geographical origin. The relative benefits of using MS-EN will provide capability for rapid screening of wines. However, this technique does not provide the identification and quantitative determination of individual compounds responsible for the different aroma notes in the wine.

Real-time nondestructive monitoring of the gas tungsten arc welding (GTAW) process by combined airborne acoustic emission and non-contact ultrasonics

Science.gov (United States)

Zhang, Lu; Basantes-Defaz, Alexandra-Del-Carmen; Abbasi, Zeynab; Yuhas, Donald; Ozevin, Didem; Indacochea, Ernesto

2018-03-01

Welding is a key manufacturing process for many industries and may introduce defects into the welded parts causing significant negative impacts, potentially ruining high-cost pieces. Therefore, a real-time process monitoring method is important to implement for avoiding producing a low-quality weld. Due to high surface temperature and possible contamination of surface by contact transducers, the welding process should be monitored via non-contact transducers. In this paper, airborne acoustic emission (AE) transducers tuned at 60 kHz and non-contact ultrasonic testing (UT) transducers tuned at 500 kHz are implemented for real time weld monitoring. AE is a passive nondestructive evaluation method that listens for the process noise, and provides information about the uniformity of manufacturing process. UT provides more quantitative information about weld defects. One of the most common weld defects as burn-through is investigated. The influences of weld defects on AE signatures (time-driven data) and UT signals (received signal energy, change in peak frequency) are presented. The level of burn-through damage is defined by using single method or combine AE/UT methods.

Monitoring microstructural evolution of alloy 617 with non-linear acoustics for remaining useful life prediction; multiaxial creep-fatigue and creep-ratcheting

International Nuclear Information System (INIS)

Lissenden, Cliff; Hassan, Tasnin; Rangari, Vijaya

2014-01-01

The research built upon a prior investigation to develop a unified constitutive model for design-@by-@analysis of the intermediate heat exchanger (IHX) for a very high temperature reactor (VHTR) design of next generation nuclear plants (NGNPs). Model development requires a set of failure data from complex mechanical experiments to characterize the material behavior. Therefore uniaxial and multiaxial creep-@fatigue and creep-@ratcheting tests were conducted on the nickel base Alloy 617 at 850 and 950°C. The time dependence of material behavior, and the interaction of time dependent behavior (e.g., creep) with ratcheting, which is an increase in the cyclic mean strain under load-@controlled cycling, are major concerns for NGNP design. This research project aimed at characterizing the microstructure evolution mechanisms activated in Alloy 617 by mechanical loading and dwell times at elevated temperature. The acoustic harmonic generation method was researched for microstructural characterization. It is a nonlinear acoustics method with excellent potential for nondestructive evaluation, and even online continuous monitoring once high temperature sensors become available. It is unique because it has the ability to quantitatively characterize microstructural features well before macroscale defects (e.g., cracks) form. The nonlinear acoustics beta parameter was shown to correlate with microstructural evolution using a systematic approach to handle the complexity of multiaxial creep-@fatigue and creep-@ratcheting deformation. Mechanical testing was conducted to provide a full spectrum of data for: thermal aging, tensile creep, uniaxial fatigue, uniaxial creep-@fatigue, uniaxial creep-ratcheting, multiaxial creep-fatigue, and multiaxial creep-@ratcheting. Transmission Electron Microscopy (TEM), Scanning Electron Microscopy (SEM), and Optical Microscopy were conducted to correlate the beta parameter with individual microstructure mechanisms. We researched application of the

Determination of the geographic origin of rice by chemometrics with strontium and lead isotope ratios and multielement concentrations.

Science.gov (United States)

Ariyama, Kaoru; Shinozaki, Miyuki; Kawasaki, Akira

2012-02-22

The objective of this study was to develop a technique for determining the country of origin of rice in the Japanese market. The rice samples included a total of 350 products grown in Japan (n = 200), the United States (n = 50), China (n = 50), and Thailand (n = 50). In this study, (87)Sr/(86)Sr and Pb isotope ((204)Pb, (206)Pb, (207)Pb, and (208)Pb) ratios and multielement concentrations (Al, Fe, Co, Ni, Cu, Rb, Sr, and Ba) were determined by high-resolution inductively coupled plasma mass spectrometry. By combining three chemometric techniques based on different principles and determination criteria, the countries of origin of rice were determined. The predictions made by 10-fold cross-validation were around 97% accurate. The presented method demonstrated the effectiveness of determining the geographic origin of an agricultural product by combining several chemometric techniques using heavy element isotope ratios and multielement concentrations.

Fundamentals of Acoustics. Psychoacoustics and Hearing. Acoustical Measurements

Science.gov (United States)

Begault, Durand R.; Ahumada, Al (Technical Monitor)

1997-01-01

These are 3 chapters that will appear in a book titled "Building Acoustical Design", edited by Charles Salter. They are designed to introduce the reader to fundamental concepts of acoustics, particularly as they relate to the built environment. "Fundamentals of Acoustics" reviews basic concepts of sound waveform frequency, pressure, and phase. "Psychoacoustics and Hearing" discusses the human interpretation sound pressure as loudness, particularly as a function of frequency. "Acoustic Measurements" gives a simple overview of the time and frequency weightings for sound pressure measurements that are used in acoustical work.

Communication Acoustics

DEFF Research Database (Denmark)

Blauert, Jens

Communication Acoustics deals with the fundamentals of those areas of acoustics which are related to modern communication technologies. Due to the advent of digital signal processing and recording in acoustics, these areas have enjoyed an enormous upswing during the last 4 decades. The book...... the book a source of valuable information for those who want to improve or refresh their knowledge in the field of communication acoustics - and to work their way deeper into it. Due to its interdisciplinary character Communication Acoustics is bound to attract readers from many different areas, such as......: acoustics, cognitive science, speech science, and communication technology....

Association and discrimination of diesel fuels using chemometric procedures.

Science.gov (United States)

Marshall, Lucas J; McIlroy, John W; McGuffin, Victoria L; Waddell Smith, Ruth

2009-08-01

Five neat diesel samples were analyzed by gas chromatography-mass spectrometry and total ion chromatograms as well as extracted ion profiles of the alkane and aromatic compound classes were generated. A retention time alignment algorithm was employed to align chromatograms prior to peak area normalization. Pearson product moment correlation coefficients and principal components analysis were then employed to investigate association and discrimination among the diesel samples. The same procedures were also used to investigate the association of a diesel residue to its neat counterpart. Current limitations in the retention time alignment algorithm and the subsequent effect on the association and discrimination of the diesel samples are discussed. An understanding of these issues is crucial to ensure the accuracy of data interpretation based on such chemometric procedures.

Non-destructive evaluation of nuclear material storage container integrity using an acoustic technique

International Nuclear Information System (INIS)

Miller, R.F.; Pechersky, M.J.; Raju, P.K.

1994-01-01

A non-intrusive method for determining the gas mixture in a sealed container using acoustics has been conceived. Analysis has shown that it is possible to both excite the acoustic resonance of the gas cavity, and detect when resonance occurs from the outside surface of the container. The resonant frequency of the acoustic cavity is dependent on the molecular weight of the gas that fills it. A change in the mixture of gases within the cavity alters the gas molecular weight and can produce a detectable change in the resonant frequency of the cavity. This concept provides a method of monitoring and/or analyzing the gas mixture in a sealed container without taking physical samples. An advantage of this technique is that it eliminates safety and contamination risks associated with breaching a pressure boundary and taking a sample of potentially hazardous gases in order to monitor or analyze the mixture

Chemometric comparison of polychlorinated biphenyl residues and toxicologically active polychlorinated biphenyl congeners in the eggs of Forster's Terns (Sterna fosteri)

Science.gov (United States)

Schwartz, Ted R.; Stalling, David L.

1991-01-01

The separation and characterization of complex mixtures of polychlorinated biphenyls (PCBs) is approached from the perspective of a problem in chemometrics. A technique for quantitative determination of PCB congeners is described as well as an enrichment technique designed to isolate only those congener residues which induce mixed aryl hydrocarbon hydroxylase enzyme activity. A congener-specific procedure is utilized for the determination of PCBs in whichn-alkyl trichloroacetates are used as retention index marker compounds. Retention indices are reproducible in the range of ±0.05 to ±0.7 depending on the specific congener. A laboratory data base system developed to aid in the editing and quantitation of data generated from capillary gas chromatography was employed to quantitate chromatographic data. Data base management was provided by computer programs written in VAX-DSM (Digital Standard MUMPS) for the VAX-DEC (Digital Equipment Corp.) family of computers.In the chemometric evaluation of these complex chromatographic profiles, data are viewed from a single analysis as a point in multi-dimensional space. Principal Components Analysis was used to obtain a representation of the data in a lower dimensional space. Two-and three-dimensional proections based on sample scores from the principal components models were used to visualize the behavior of Aroclor® mixtures. These models can be used to determine if new sample profiles may be represented by Aroclor profiles. Concentrations of individual congeners of a given chlorine substitution may be summed to form homologue concentration. However, the use of homologue concentrations in classification studies with environmental samples can lead to erroneous conclusions about sample similarity. Chemometric applications are discussed for evaluation of Aroclor mixture analysis and compositional description of environmental residues of PCBs in eggs of Forster's terns (Sterna fosteri) collected from colonies near Lake Poygan

Acoustic emission monitoring of activation behavior of LaNi5 hydrogen storage alloy

Directory of Open Access Journals (Sweden)

Igor Maria De Rosa, Alessandro Dell'Era, Mauro Pasquali, Carlo Santulli and Fabrizio Sarasini

2011-01-01

Full Text Available The acoustic emission technique is proposed for assessing the irreversible phenomena occurring during hydrogen absorption/desorption cycling in LaNi5. In particular, we have studied, through a parametric analysis of in situ detected signals, the correlation between acoustic emission (AE parameters and the processes occurring during the activation of an intermetallic compound. Decreases in the number and amplitude of AE signals suggest that pulverization due to hydrogen loading involves progressively smaller volumes of material as the number of cycles increases. This conclusion is confirmed by electron microscopy observations and particle size distribution measurements.

Acoustic source for generating an acoustic beam

Science.gov (United States)

Vu, Cung Khac; Sinha, Dipen N.; Pantea, Cristian

2016-05-31

An acoustic source for generating an acoustic beam includes a housing; a plurality of spaced apart piezo-electric layers disposed within the housing; and a non-linear medium filling between the plurality of layers. Each of the plurality of piezoelectric layers is configured to generate an acoustic wave. The non-linear medium and the plurality of piezo-electric material layers have a matching impedance so as to enhance a transmission of the acoustic wave generated by each of plurality of layers through the remaining plurality of layers.

Rapid quantification of casein in skim milk using Fourier transform infrared spectroscopy, enzymatic perturbation, and multiway partial least squares: Monitoring chymosin at work

DEFF Research Database (Denmark)

Baum, Andreas; Hansen, P. W.; Nørgaard, Lars

2016-01-01

In this study, we introduce enzymatic perturbation combined with Fourier transform infrared (FTIR) spectroscopy as a concept for quantifying casein in subcritical heated skim milk using chemometric multiway analysis. Chymosin is a protease that cleaves specifically caseins. As a result of hydroly......In this study, we introduce enzymatic perturbation combined with Fourier transform infrared (FTIR) spectroscopy as a concept for quantifying casein in subcritical heated skim milk using chemometric multiway analysis. Chymosin is a protease that cleaves specifically caseins. As a result...... of hydrolysis, all casein proteins clot to form a creamy precipitate, and whey proteins remain in the supernatant. We monitored the cheese-clotting reaction in real time using FTIR and analyzed the resulting evolution profiles to establish calibration models using parallel factor analysis and multiway partial...

Acoustic calibration apparatus for calibrating plethysmographic acoustic pressure sensors

Science.gov (United States)

Zuckerwar, Allan J. (Inventor); Davis, David C. (Inventor)

1995-01-01

An apparatus for calibrating an acoustic sensor is described. The apparatus includes a transmission material having an acoustic impedance approximately matching the acoustic impedance of the actual acoustic medium existing when the acoustic sensor is applied in actual in-service conditions. An elastic container holds the transmission material. A first sensor is coupled to the container at a first location on the container and a second sensor coupled to the container at a second location on the container, the second location being different from the first location. A sound producing device is coupled to the container and transmits acoustic signals inside the container.

Online monitoring of Accessories for Underground Electrical Installations through Acoustics Emissions

Directory of Open Access Journals (Sweden)

Casals-Torrens P.

2012-04-01

Full Text Available The acoustic waves caused by Partial Discharges inside the dielectric materials, can be detected by acoustic emission (AE sensors and analyzed in the time domain. The experimental results presented, show the online detection capability of these sensors in the environment near a cable accessory, such as a splice or terminal. The AE sensors are immune to electromagnetic interference and constitute a detection method non-intrusive and non-destructive, which ensures a galvanic decoupling with respect to electric networks, this technique of partial discharge detection can be applied as a test method for preventive or predictive maintenance (condition-based maintenance to equipments or facilities of medium and high voltage in service and represents an alternative method to electrical detection systems, conventional or not, that continue to rely on the detection of current pulses. This paper presents characterization tests of the sensors AE through comparative tests of partial discharge on accessories for underground power cables.

Results of investigations within the IWGFR benchmark test acoustic boiling noise detection

International Nuclear Information System (INIS)

Mauersberger, H.; Froehlich, K.J.

1989-01-01

The present paper deals with investigations of acoustic signals from a boiling experiment performed on the KNS I loop at KfK Karlsruhe. Signals have been analysed in frequency as well as in time domain. Signal characteristics successfully used to detect the boiling process have been found in time domain. A proposal for in-service boiling monitoring by acoustic means is briefly described. (author). 10 refs, 16 figs, 1 tab

Chemometric analysis for discrimination of extra virgin olive oils from whole and stoned olive pastes.

Science.gov (United States)

De Luca, Michele; Restuccia, Donatella; Clodoveo, Maria Lisa; Puoci, Francesco; Ragno, Gaetano

2016-07-01

Chemometric discrimination of extra virgin olive oils (EVOO) from whole and stoned olive pastes was carried out by using Fourier transform infrared (FTIR) data and partial least squares-discriminant analysis (PLS1-DA) approach. Four Italian commercial EVOO brands, all in both whole and stoned version, were considered in this study. The adopted chemometric methodologies were able to describe the different chemical features in phenolic and volatile compounds contained in the two types of oil by using unspecific IR spectral information. Principal component analysis (PCA) was employed in cluster analysis to capture data patterns and to highlight differences between technological processes and EVOO brands. The PLS1-DA algorithm was used as supervised discriminant analysis to identify the different oil extraction procedures. Discriminant analysis was extended to the evaluation of possible adulteration by addition of aliquots of oil from whole paste to the most valuable oil from stoned olives. The statistical parameters from external validation of all the PLS models were very satisfactory, with low root mean square error of prediction (RMSEP) and relative error (RE%). Copyright © 2016 Elsevier Ltd. All rights reserved.

A procedure of experimental data acquisition for an evaluation of the acoustic emission in the rock disintegration

Directory of Open Access Journals (Sweden)

František Krepelka

2007-04-01

Full Text Available The paper describes some results of the monitoring of acoustic signal in the rock disintegration on the drillig stand of the Institute of Geotechnics, SAS, in Košice. The acoustic signal has been registered. The registration and processing of the acoustic signal is solved as a part of the research grant task within the basic research of the rock disintegration by drilling.

Investigation of the Sintering Process Using Non-Contact Electromagnetic Acoustic Transducers

International Nuclear Information System (INIS)

James C. Foley; David K. Rehbein; Daniel J. Barnard

2001-01-01

In-situ characterizations of green state part density and sintering state have long been desired in the powder metal community. Recent advances in non-contact electromagnetic acoustic transducer (EMAT) technology have enabled in-situ monitoring of acoustic amplitude and velocity as sintering proceeds. Samples were made from elemental powders of Al (99.99%), Al (99.7%), Ag, (99.99%), Cu (99.99%) and Fe (99.9%). The powders were pressed in a uniaxial die and examined with acoustic waves for changes in velocity and amplitude during sintering for the samples containing Al, Ag, and Cu. The changes in acoustic properties were correlated with sample microstructures and mechanical properties. Evolution of a series of reverberating echoes during sintering is shown to provide information on the state of sintering, and changes in sintering kinetics as well as having the potential for detection of interior flaws

Simultaneous chemometric determination of pyridoxine hydrochloride and isoniazid in tablets by multivariate regression methods.

Science.gov (United States)

Dinç, Erdal; Ustündağ, Ozgür; Baleanu, Dumitru

2010-08-01

The sole use of pyridoxine hydrochloride during treatment of tuberculosis gives rise to pyridoxine deficiency. Therefore, a combination of pyridoxine hydrochloride and isoniazid is used in pharmaceutical dosage form in tuberculosis treatment to reduce this side effect. In this study, two chemometric methods, partial least squares (PLS) and principal component regression (PCR), were applied to the simultaneous determination of pyridoxine (PYR) and isoniazid (ISO) in their tablets. A concentration training set comprising binary mixtures of PYR and ISO consisting of 20 different combinations were randomly prepared in 0.1 M HCl. Both multivariate calibration models were constructed using the relationships between the concentration data set (concentration data matrix) and absorbance data matrix in the spectral region 200-330 nm. The accuracy and the precision of the proposed chemometric methods were validated by analyzing synthetic mixtures containing the investigated drugs. The recovery results obtained by applying PCR and PLS calibrations to the artificial mixtures were found between 100.0 and 100.7%. Satisfactory results obtained by applying the PLS and PCR methods to both artificial and commercial samples were obtained. The results obtained in this manuscript strongly encourage us to use them for the quality control and the routine analysis of the marketing tablets containing PYR and ISO drugs. Copyright © 2010 John Wiley & Sons, Ltd.

From echolocation clicks to animal density – acoustic sampling of harbour porpoises with static dataloggers

DEFF Research Database (Denmark)

Kyhn, Line Anker; Tougaard, Jakob; Thomas, L.

2012-01-01

Monitoring abundance and population trends of small odontocetes is notoriously difficult and labour intensive. There is a need to develop alternative methods to the traditional visual line transect surveys, especially for low density areas. Here, the prospect of obtaining robust density estimates....... This provides a method suitable for monitoring in areas with densities too low for visual surveys to be practically feasible, e.g. the endangered harbour porpoise population in the Baltic....... for porpoises by passive acoustic monitoring (PAM) is demonstrated by combining rigorous application of methods adapted from distance sampling to PAM. Acoustic dataloggers (T-PODs) were deployed in an area where harbour porpoises concurrently were tracked visually. Probability of detection was estimated...

Acoustic emission in a superconductor (Nb-Ti) during magnetic field and current sweep

International Nuclear Information System (INIS)

Nomura, Harehiko

1980-01-01

Though superconducting magnets are indispensable in the fields of nuclear fusion, MHD power generation, high energy technology, and the trains using magnetic levitation, the safety of the magnets used for those fields is required to be fully investigated because their accumulating energy reaches up to several GJ. For this purpose, the improvement of monitoring techniques is extremely important to grasp exactly the magnetization of such large energy magnets. Although the detection of the terminal voltage of the magnets has been mainly used so far, the purpose has not yet been fulfilled because various phenomena appear in the form of noises in the terminal voltage. The authors have found the monitoring method using acoustic emission in a system completely independent from voltage observation. From this viewpoint, the experiments have been performed aiming at the generation of acoustic emission in conjunction with magnetization out of the fine structure of super-conductors, taking notice of the emitted sound frequency ranging over several hundred kHz. The results and investigation revealed that the superconductor itself emitted ultrasonic sound. It was found that the observation of this acoustic power intensity was able to monitor not only the magnetization of superconductors but also its current sweep. Since the motion of the magnetic flux is converted into the signal of acoustic field, this measuring method is less affected by noise disturbance from electromagnetic systems, and is expected to be useful for the researches on analyzing superconductor characteristics. (Wakatsuki, Y.)

Acoustically Induced Vibration of Structures: Reverberant Vs. Direct Acoustic Testing

Science.gov (United States)

Kolaini, Ali R.; O'Connell, Michael R.; Tsoi, Wan B.

2009-01-01

Large reverberant chambers have been used for several decades in the aerospace industry to test larger structures such as solar arrays and reflectors to qualify and to detect faults in the design and fabrication of spacecraft and satellites. In the past decade some companies have begun using direct near field acoustic testing, employing speakers, for qualifying larger structures. A limited test data set obtained from recent acoustic tests of the same hardware exposed to both direct and reverberant acoustic field testing has indicated some differences in the resulting structural responses. In reverberant acoustic testing, higher vibration responses were observed at lower frequencies when compared with the direct acoustic testing. In the case of direct near field acoustic testing higher vibration responses appeared to occur at higher frequencies as well. In reverberant chamber testing and direct acoustic testing, standing acoustic modes of the reverberant chamber or the speakers and spacecraft parallel surfaces can strongly couple with the fundamental structural modes of the test hardware. In this paper data from recent acoustic testing of flight hardware, that yielded evidence of acoustic standing wave coupling with structural responses, are discussed in some detail. Convincing evidence of the acoustic standing wave/structural coupling phenomenon will be discussed, citing observations from acoustic testing of a simple aluminum plate. The implications of such acoustic coupling to testing of sensitive flight hardware will be discussed. The results discussed in this paper reveal issues with over or under testing of flight hardware that could pose unanticipated structural and flight qualification issues. Therefore, it is of paramount importance to understand the structural modal coupling with standing acoustic waves that has been observed in both methods of acoustic testing. This study will assist the community to choose an appropriate testing method and test setup in

Multi-functional surface acoustic wave sensor for monitoring enviromental and structural condition

Science.gov (United States)

Furuya, Y.; Kon, T.; Okazaki, T.; Saigusa, Y.; Nomura, T.

2006-03-01

As a first step to develop a health monitoring system with active and embedded nondestructive evaluation devices for the machineries and structures, multi-functional SAW (surface acoustic wave) device was developed. A piezoelectric LiNbO3(x-y cut) materials were used as a SAW substrate on which IDT(20μm pitch) was produced by lithography. On the surface of a path of SAW between IDTs, environmentally active material films of shape memory Ti50Ni41Cu(at%) with non-linear hysteresis and superelastic Ti48Ni43Cu(at%) with linear deformation behavior were formed by magnetron-sputtering technique. In this study, these two kinds of shape memory alloys SMA) system were used to measure 1) loading level, 2) phase transformation and 3)stress-strain hysteresis under cyclic loading by utilizing their linearity and non-linearity deformation behaviors. Temperature and stress dependencies of SAW signal were also investigated in the non-sputtered film state. Signal amplitude and phase change of SAW were chosen to measure as the sensing parameters. As a result, temperature, stress level, phase transformation in SMA depending on temperature and mechanical damage accumulation could be measured by the proposed multi-functional SAW sensor. Moreover, the wireless SAW sensing system which has a unique feature of no supplying electric battery was constructed, and the same characteristic evaluation is confirmed in comparison with wired case.

Multiharmonic Frequency-Chirped Transducers for Surface-Acoustic-Wave Optomechanics

Science.gov (United States)

Weiß, Matthias; Hörner, Andreas L.; Zallo, Eugenio; Atkinson, Paola; Rastelli, Armando; Schmidt, Oliver G.; Wixforth, Achim; Krenner, Hubert J.

2018-01-01

Wide-passband interdigital transducers are employed to establish a stable phase lock between a train of laser pulses emitted by a mode-locked laser and a surface acoustic wave generated electrically by the transducer. The transducer design is based on a multiharmonic split-finger architecture for the excitation of a fundamental surface acoustic wave and a discrete number of its overtones. Simply by introducing a variation of the transducer's periodicity p , a frequency chirp is added. This combination results in wide frequency bands for each harmonic. The transducer's conversion efficiency from the electrical to the acoustic domain is characterized optomechanically using single quantum dots acting as nanoscale pressure sensors. The ability to generate surface acoustic waves over a wide band of frequencies enables advanced acousto-optic spectroscopy using mode-locked lasers with fixed repetition rate. Stable phase locking between the electrically generated acoustic wave and the train of laser pulses is confirmed by performing stroboscopic spectroscopy on a single quantum dot at a frequency of 320 MHz. Finally, the dynamic spectral modulation of the quantum dot is directly monitored in the time domain combining stable phase-locked optical excitation and time-correlated single-photon counting. The demonstrated scheme will be particularly useful for the experimental implementation of surface-acoustic-wave-driven quantum gates of optically addressable qubits or collective quantum states or for multicomponent Fourier synthesis of tailored nanomechanical waveforms.

Acoustic emission: technical review for PWR applications

International Nuclear Information System (INIS)

Bentley, P.G.

1981-07-01

Acoustic emission has been studied since the early 1960's, particularly with a view to periodic or continuous monitoring of steel pressure vessels. In the years 1970-75 it was realised that ductile steels, used in nuclear vessels, give small amplitude signals which are barely detectable by available instruments. The technique for application in periodic or continuous monitoring and also as applied to leak detection and weld fabrication monitoring is reviewed. It is concluded that manufacturing defects may be detectable during pre-service hydrotest, but that there is insufficient evidence on which to base an estimate of detection probability. In-service hydrotest or continuous monitoring is unlikely to detect growing cracks because of the quiet nature of the material and the noisy reactor background. Both leak detection and fabrication weld monitoring show some promise of successful application in the future. (author)

Size Effect on Acoustic Emission Characteristics of Coal-Rock Damage Evolution

Directory of Open Access Journals (Sweden)

Zhijie Wen

2017-01-01

Full Text Available Coal-gas outburst, rock burst, and other mine dynamic disasters are closely related to the instability and failure of coal-rock. Coal-rock is the assemblies of mineral particles of varying sizes and shapes bonded together by cementing materials. The damage and rupture process of coal-rock is accompanied by acoustic emission (AE, which can be used as an effective means to monitor and predict the instability of coal-rock body. In this manuscript, considering the size effect of coal-rock, the influence of different height to diameter ratio on the acoustic emission characteristics of coal-rock damage evolution was discussed by microparticle flow PFC2D software platform. The results show that coal-rock size influences the uniaxial compressive strength, peak strain, and elastic modulus of itself; the size effect has little effect on the acoustic emission law of coal-rock damage and the effects of the size of coal-rock samples on acoustic emission characteristics are mainly reflected in three aspects: the triggering time of acoustic emission, the strain range of strong acoustic emission, and the intensity of acoustic emission; the damage evolution of coal-rock specimen can be divided into 4 stages: initial damage, stable development, accelerated development, and damage.

Interior acoustic cloak

Directory of Open Access Journals (Sweden)

Wael Akl

2014-12-01

Full Text Available Acoustic cloaks have traditionally been intended to externally surround critical objects to render these objects acoustically invisible. However, in this paper, the emphasis is placed on investigating the application of the acoustic cloaks to the interior walls of acoustic cavities in an attempt to minimize the noise levels inside these cavities. In this manner, the acoustic cloaks can serve as a viable and efficient alternative to the conventional passive noise attenuation treatments which are invariably heavy and bulky. The transformation acoustics relationships that govern the operation of this class of interior acoustic cloaks are presented. Physical insights are given to relate these relationships to the reasons behind the effectiveness of the proposed interior acoustic cloaks. Finite element models are presented to demonstrate the characteristics of interior acoustic cloaks used in treating the interior walls of circular and square cavities both in the time and frequency domains. The obtained results emphasize the effectiveness of the proposed interior cloaks in eliminating the reflections of the acoustic waves from the walls of the treated cavities and thereby rendering these cavities acoustically quiet. It is important to note here that the proposed interior acoustic cloaks can find applications in acoustic cavities such as aircraft cabins and auditoriums as well as many other critical applications.

Acoustic tomography in the atmospheric surface layer

Directory of Open Access Journals (Sweden)

A. Ziemann

Full Text Available Acoustic tomography is presented as a technique for remote monitoring of meteorological quantities. This method and a special algorithm of analysis can directly produce area-averaged values of meteorological parameters. As a result consistent data will be obtained for validation of numerical atmospheric micro-scale models. Such a measuring system can complement conventional point measurements over different surfaces. The procedure of acoustic tomography uses the horizontal propagation of sound waves in the atmospheric surface layer. Therefore, to provide a general overview of sound propagation under various atmospheric conditions a two-dimensional ray-tracing model according to a modified version of Snell's law is used. The state of the crossed atmosphere can be estimated from measurements of acoustic travel time between sources and receivers at different points. Derivation of area-averaged values of the sound speed and furthermore of air temperature results from the inversion of travel time values for all acoustic paths. Thereby, the applied straight ray two-dimensional tomographic model using SIRT (simultaneous iterative reconstruction technique is characterised as a method with small computational requirements, satisfactory convergence and stability properties as well as simple handling, especially, during online evaluation.

Key words. Meteorology and atmospheric dynamics (turbulence; instruments and techniques.

Analysis of acoustic data from UK sodium/water reaction test facilities

International Nuclear Information System (INIS)

Rowley, R.; Mcknight, J.A.; Airey, J.

1990-01-01

This paper describes acoustic measurements made during a number of sodium/water reaction experiments in the UK. The tests have included water and steam injections through both realistic (fatigue crack) defects and machined orifices and have covered a range of experimental conditions including those appropriate to the inlet and outlet regions of the EFR steam generators. Injection rates were typically in the range 0.1 to 30 g/s. Where possible, gas injections were also included in the test programme for comparison, since it is anticipated that a practical SGU acoustic leak detection system would include a facility for gas injections to allow system calibration, and to confirm transmission properties within the SGU. The test sections were instrumented with accelerometers on waveguides and in some cases included an under-sodium microphone situated about 300mm above the reaction zone. Tape recordings were made during the tests and used for detailed analysis off-line, although an audible output from one of the acoustic channels was used to monitor the progress of the injections and provide information for the rig operators. A comparison of the signal amplitudes measured during the experiments with typical reactor background noise was made and an estimate of the detection sensitivity of an acoustic monitoring system was deduced. 3 refs, 5 figs, 1 tab

Identification of heparin samples that contain impurities or contaminants by chemometric pattern recognition analysis of proton NMR spectral data

Energy Technology Data Exchange (ETDEWEB)

Zang, Qingda [University of Medicine and Dentistry of New Jersey, Department of Pharmacology, Robert Wood Johnson Medical School, Piscataway, NJ (United States); Snowdon, Inc., Monmouth Junction, NJ (United States); University of Medicine and Dentistry of New Jersey, Department of Health Informatics, School of Health Related Professions, Newark, NJ (United States); Keire, David A.; Buhse, Lucinda F.; Trehy, Michael L. [Food and Drug Administration, CDER, Division of Pharmaceutical Analysis, St. Louis, MO (United States); Wood, Richard D. [Snowdon, Inc., Monmouth Junction, NJ (United States); Mital, Dinesh P.; Haque, Syed; Srinivasan, Shankar [University of Medicine and Dentistry of New Jersey, Department of Health Informatics, School of Health Related Professions, Newark, NJ (United States); Moore, Christine M.V.; Nasr, Moheb; Al-Hakim, Ali [Food and Drug Administration, CDER, Office of New Drug Quality Assessment, Silver Spring, MD (United States); Welsh, William J. [University of Medicine and Dentistry of New Jersey, Department of Pharmacology, Robert Wood Johnson Medical School, Piscataway, NJ (United States)

2011-08-15

Chemometric analysis of a set of one-dimensional (1D) {sup 1}H nuclear magnetic resonance (NMR) spectral data for heparin sodium active pharmaceutical ingredient (API) samples was employed to distinguish USP-grade heparin samples from those containing oversulfated chondroitin sulfate (OSCS) contaminant and/or unacceptable levels of dermatan sulfate (DS) impurity. Three chemometric pattern recognition approaches were implemented: classification and regression tree (CART), artificial neural network (ANN), and support vector machine (SVM). Heparin sodium samples from various manufacturers were analyzed in 2008 and 2009 by 1D {sup 1}H NMR, strong anion-exchange high-performance liquid chromatography, and percent galactosamine in total hexosamine tests. Based on these data, the samples were divided into three groups: Heparin, DS {<=} 1.0% and OSCS = 0%; DS, DS > 1.0% and OSCS = 0%; and OSCS, OSCS > 0% with any content of DS. Three data sets corresponding to different chemical shift regions (1.95-2.20, 3.10-5.70, and 1.95-5.70 ppm) were evaluated. While all three chemometric approaches were able to effectively model the data in the 1.95-2.20 ppm region, SVM was found to substantially outperform CART and ANN for data in the 3.10-5.70 ppm region in terms of classification success rate. A 100% prediction rate was frequently achieved for discrimination between heparin and OSCS samples. The majority of classification errors between heparin and DS involved cases where the DS content was close to the 1.0% DS borderline between the two classes. When these borderline samples were removed, nearly perfect classification results were attained. Satisfactory results were achieved when the resulting models were challenged by test samples containing blends of heparin APIs spiked with non-, partially, or fully oversulfated chondroitin sulfate A, heparan sulfate, or DS at the 1.0%, 5.0%, and 10.0% (w/w) levels. This study demonstrated that the combination of 1D {sup 1}H NMR spectroscopy

On-line monitoring of fermentation processes using multi-wavelength fluorescence

DEFF Research Database (Denmark)

Odman, Peter; Petersen, Nanna; Johansen, Claus Lindvald

2007-01-01

. The model system considered in this work is the antibiotic production by Streptomyces coelicolor, a filamentous bacterium. In addition to predicting concentrations of biomass in the fermentation broth, the data allowed detection of different physiological states, i.e. growth phase and phosphate limitation......Fermentation processes often suffer from a lack of real-time methods for on-line determination of variables like the concentrations of nutrients and products. This work aims at investigating the possibilities of implementing an on-line fermentation monitoring system based on multi......-wavelength fluorescence (MWF). This type of sensor has previously showed promising accuracy and selectivity for in situ monitoring of cell mass and certain metabolites in bioreactors (Lantz et al., 2006). The sensor generates multivariate data outputs, which necessitate chemometric modeling for signal interpretation...

Responsive acoustic surfaces

DEFF Research Database (Denmark)

Peters, Brady; Tamke, Martin; Nielsen, Stig Anton

2011-01-01

Acoustic performance is defined by the parameter of reverberation time; however, this does not capture the acoustic experience in some types of open plan spaces. As many working and learning activities now take place in open plan spaces, it is important to be able to understand and design...... for the acoustic conditions of these spaces. This paper describes an experimental research project that studied the design processes necessary to design for sound. A responsive acoustic surface was designed, fabricated and tested. This acoustic surface was designed to create specific sonic effects. The design...... was simulated using custom integrated acoustic software and also using Odeon acoustic analysis software. The research demonstrates a method for designing space- and sound-defining surfaces, defines the concept of acoustic subspace, and suggests some new parameters for defining acoustic subspaces....

Flat acoustic lens by acoustic grating with curled slits

KAUST Repository

Peng, Pai

2014-10-01

We design a flat sub-wavelength lens that can focus acoustic wave. We analytically study the transmission through an acoustic grating with curled slits, which can serve as a material with tunable impedance and refractive index for acoustic waves. The effective parameters rely on the geometry of the slits and are independent of frequency. A flat acoustic focusing lens by such acoustic grating with gradient effective refractive index is designed. The focusing effect is clearly observed in simulations and well predicted by the theory. We demonstrate that despite the large impedance mismatch between the acoustic lens and the matrix, the intensity at the focal point is still high due to Fabry-Perot resonance.

On Mass Loading and Dissipation Measured with Acoustic Wave Sensors: A Review

Directory of Open Access Journals (Sweden)

Marina V. Voinova

2009-01-01

Full Text Available We summarize current trends in the analysis of physical properties (surface mass density, viscosity, elasticity, friction, and charge of various thin films measured with a solid-state sensor oscillating in a gaseous or liquid environment. We cover three different types of mechanically oscillating sensors: the quartz crystal microbalance with dissipation (QCM-D monitoring, surface acoustic wave (SAW, resonators and magnetoelastic sensors (MESs. The fourth class of novel acoustic wave (AW mass sensors, namely thin-film bulk acoustic resonators (TFBARs on vibrating membranes is discussed in brief. The paper contains a survey of theoretical results and practical applications of the sensors and includes a comprehensive bibliography.

Parametric Room Acoustic workflows with real-time acoustic simulation

DEFF Research Database (Denmark)

Parigi, Dario

2017-01-01

The paper investigates and assesses the opportunities that real-time acoustic simulation offer to engage in parametric acoustics workflow and to influence architectural designs from early design stages......The paper investigates and assesses the opportunities that real-time acoustic simulation offer to engage in parametric acoustics workflow and to influence architectural designs from early design stages...

Acoustics short-term passive monitoring using sonobuoys in the Bering, Chukchi, and Western Beaufort Seas conducted by Alaska Fisheries Scientific Center, National Marine Mammal Laboratory from 2007-08-01 to 2015-09-28 (NCEI Accession 0138863)

Data.gov (United States)

National Oceanic and Atmospheric Administration, Department of Commerce — The National Marine Mammal Laboratory (NMML) has conducted passive acoustic monitoring in the Bering, Chukchi, and Western Beaufort Seas to determine spatio-temporal...

New algorithm for controlling electric arc furnaces using their vibrational and acoustic characteristics

Science.gov (United States)

Cherednichenko, V. S.; Bikeev, R. A.; Serikov, V. A.; Rechkalov, A. V.; Cherednichenko, A. V.

2016-12-01

The processes occurring in arc discharges are analyzed as the sources of acoustic radiation in an electric arc furnace (EAF). Acoustic vibrations are shown to transform into mechanical vibrations in the furnace laboratory. The shielding of the acoustic energy fluxes onto water-cooled wall panels by a charge is experimentally studied. It is shown that the rate of charge melting and the depth of submergence of arc discharges in the slag and metal melt can be monitored by measuring the vibrational characteristics of furnaces and using them in a universal industrial process-control system, which was developed for EAFs.

Frequency Analysis of Acoustic Emission Signal to Monitor Damage Evolution in Masonry Structures

International Nuclear Information System (INIS)

Masera, D; Bocca, P; Grazzini, A

2011-01-01

A crucial aspect in damage evaluation of masonry structures is the analysis of long-term behaviour and for this reason fatigue analysis has a great influence on safety assessment of this structures. Acoustic Emission (AE) are very effective non-destructive techniques applied to identify micro and macro-defects and their temporal evolution in several materials. This technique permits to estimate the velocity of ultrasound waves propagation and the amount of energy released during fracture propagation to obtain information on the criticality of the ongoing process. By means of AE monitoring, an experimental analysis on a set of reinforced and unreinforced masonry walls under variable amplitude and static loading has been carried out. During these tests, the AE signals were recorded. The AE signals were analysed using Fast Fourier Transform (FFT) to examine the frequency distribution of the micro and macro cracking. It possible to evaluate the evolution of the wavelength of the AE signal through the two characteristic peak in the AE spectrum signals and the wave speed of the P or S waves. This wavelength evolution can be represent the microcrak and macrocrack evolution in masonry walls. This procedure permits to estimate the fracture dimension characteristic in several loading condition and for several masonry reinforced condition.

Acoustic Research on the Damage Mechanism of Carbon Fiber Composite Materials

Science.gov (United States)

Wang, Bing; Liu, Yanlei; Sheng, Shuiping

This thesis involves the study about different processes including the tensile fracture, inter-layer tear or avulsion, as well as the interlaminar shear or split regarding carbon fiber composite materials with the aid of acoustic emission technique. Also, various acoustic emission signals that are released by composite samples in the process of fracture are analyzed. As is indicated by the test results, different acoustic emissive signals that are released by carbon fiber layers in various stages of damage and fracture bear different characteristics. Acoustic detection can effectively monitor the whole stage of elastic deformation, the damage development, and even the accumulation process while figuring out in an efficient manner about the internal activities of the composites, plus the diverse types of damages. In addition, its fabulous application value lies in its relevant structural evaluation as well as the evaluation of integrity with regard to carbon fiber composite.

Simultaneous determination of trace-levels of alloying zinc and copper by semi-mercury-free potentiometric stripping analysis with chemometric data treatment

DEFF Research Database (Denmark)

Andersen, Jens Enevold Thaulov; Hansen, Elo Harald

1998-01-01

Assays of copper and zinc in brass samples were performed by Semi-Mercury Free Potentiometric Stripping Analysis (S-MF PSA) using a thin-film mercury covered glassy-carbon working electrode and dissolved oxygen as oxidizing agent during the stripping step. The stripping peak transients were...... resolved by chemometrics which enabled simultaneous determination of both the copper and the zinc concentrations, thereby eliminating the conventional necessary pretreatment of the sample solution, such as initial addition of Ga(III) or solvent extraction of copper. The brass samples were diluted...... by factors in the range 2.104 - 5.105 which resulted in quantification of the copper and of zinc contents comparable to the specified values within 10%. On the basis of the chemometric treatment, an empirical expression is deduced relating the stripping time to the recorded potential....

Chemometric expertise of the quality of groundwater sources for domestic use.

Science.gov (United States)

Spanos, Thomas; Ene, Antoaneta; Simeonova, Pavlina

2015-01-01

In the present study 49 representative sites have been selected for the collection of water samples from central water supplies with different geographical locations in the region of Kavala, Northern Greece. Ten physicochemical parameters (pH, electric conductivity, nitrate, chloride, sodium, potassium, total alkalinity, total hardness, bicarbonate and calcium) were analyzed monthly, in the period from January 2010 to December 2010. Chemometric methods were used for monitoring data mining and interpretation (cluster analysis, principal components analysis and source apportioning by principal components regression). The clustering of the chemical indicators delivers two major clusters related to the water hardness and the mineral components (impacted by sea, bedrock and acidity factors). The sampling locations are separated into three major clusters corresponding to the spatial distribution of the sites - coastal, lowland and semi-mountainous. The principal components analysis reveals two latent factors responsible for the data structures, which are also an indication for the sources determining the groundwater quality of the region (conditionally named "mineral" factor and "water hardness" factor). By the apportionment approach it is shown what the contribution is of each of the identified sources to the formation of the total concentration of each one of the chemical parameters. The mean values of the studied physicochemical parameters were found to be within the limits given in the 98/83/EC Directive. The water samples are appropriate for human consumption. The results of this study provide an overview of the hydrogeological profile of water supply system for the studied area.

Chemometric characterization of the hydrogen bonding complexes of secondary amides and aromatic hydrocarbons

Directory of Open Access Journals (Sweden)

Jović Branislav

2012-01-01

Full Text Available The paper reports the results of the study of hydrogen bonding complexes between secondary amides and various aromatic hydrocarbons. The possibility of using chemometric methods was investigated in order to characterize N-H•••π hydrogen bonded complexes. Hierarchical clustering and Principal Component Analysis (PCA have been applied on infrared spectroscopic and Taft parameters of 43 N-substituted amide complexes with different aromatic hydrocarbons. Results obtained in this report are in good agreement with conclusions of other spectroscopic and thermodynamic analysis.

Passive acoustic monitoring using a towed hydrophone array results in identification of a previously unknown beaked whale habitat.

Science.gov (United States)

Yack, Tina M; Barlow, Jay; Calambokidis, John; Southall, Brandon; Coates, Shannon

2013-09-01

Beaked whales are diverse and species rich taxa. They spend the vast majority of their time submerged, regularly diving to depths of hundreds to thousands of meters, typically occur in small groups, and behave inconspicuously at the surface. These factors make them extremely difficult to detect using standard visual survey methods. However, recent advancements in acoustic detection capabilities have made passive acoustic monitoring (PAM) a viable alternative. Beaked whales can be discriminated from other odontocetes by the unique characteristics of their echolocation clicks. In 2009 and 2010, PAM methods using towed hydrophone arrays were tested. These methods proved highly effective for real-time detection of beaked whales in the Southern California Bight (SCB) and were subsequently implemented in 2011 to successfully detect and track beaked whales during the ongoing Southern California Behavioral Response Study. The three year field effort has resulted in (1) the successful classification and tracking of Cuvier's (Ziphius cavirostris), Baird's (Berardius bairdii), and unidentified Mesoplodon beaked whale species and (2) the identification of areas of previously unknown beaked whale habitat use. Identification of habitat use areas will contribute to a better understanding of the complex relationship between beaked whale distribution, occurrence, and preferred habitat characteristics on a relatively small spatial scale. These findings will also provide information that can be used to promote more effective management and conservation of beaked whales in the SCB, a heavily used Naval operation and training region.

Towards Noise Tomography and Passive Monitoring Using Distributed Acoustic Sensing