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Sample records for a356 aluminium alloy

  1. Comparison of modification with strontium and the refining with antimony in A 356 aluminium alloys

    International Nuclear Information System (INIS)

    Fuoco, Ricardo; Correa, Edison Roberto; Correa, Alzira V.O.; Bocalini Junior, Mario

    1992-01-01

    Strontium and Antimony treated A356 aluminium alloy samples were metallographically characterized in the as cast and solution and aged conditions. Antimony treated alloy has shown slower spheroidizing kinetics of the Silicon particles during solution treatment, lower porosity level and higher tensile strength and elongation than Strontium treated one. (author)

  2. Laser welding of SSM Cast A356 aluminium alloy processed with CSIR-Rheo technology

    CSIR Research Space (South Africa)

    Akhter, R

    2006-01-01

    Full Text Available Samples of aluminium alloy A356 were manufactured by Semi Solid Metals HPDC technology, developed recently in CSIR, Pretoria. They were butt welded in as cast conditions using as Nd: YAG laser. The best metal and weld microstructure were presented...

  3. Precipitation hardening of cast Zr-containing A356 aluminium alloy

    International Nuclear Information System (INIS)

    Baradarani, B.; Raiszadeh, R.

    2011-01-01

    The effect of small additions of zirconium on the hardness, grain size, precipitate type and size of cast A356 aluminium alloy was investigated. The cast alloys were solution treated and then artificially aged for different periods of time. Hardness tests and scanning electron microscope (SEM), energy dispersive X-ray (EDX) and X-ray diffraction (XRD) studies were carried out on the as-cast, as-solutionised and age-hardened specimens. Incoherent, coarse Al 3 Zr particles formed in the microstructure during the solidification of the alloy and caused grain refinement in the as-cast structure. These particles dissolved and reprecipitated as smaller-size particles during the solution treatment, causing the hardness of the alloy to remain constant at high temperatures for long periods of time due to the slow diffusion of Zr in the α-Al.

  4. Effect of process parameters on tensile strength of friction stir welding A356/C355 aluminium alloys joint

    Energy Technology Data Exchange (ETDEWEB)

    Dwivedi, Shashi Prakash [Noida Institute of Engineering and Technology, Greater Noida (Korea, Republic of)

    2014-01-15

    In the present investigation, A356/C355 aluminium alloys are welded by friction stir welding by controlling various welding parameters. A356 and C355 aluminium alloys materials have a set of mechanical and physical properties that are ideally suited for application in aerospace and automobile industries and not widely used because of its poor weldebility. To overcome this barrier, weldebility analysis of A356 and C355 aluminium alloys with high speed steel (Wc-Co) tool has been investigated. An attempt has been made to investigate the influence of the rotational speed of the tools, the axial force and welding speed on tensile strength of A356/C355 aluminium alloys joint. The experiments were conducted on a milling machine. The main focus of investigation is to determine good tensile strength. Response surface methodology (box Behnken design) is chosen to design the optimum welding parameters leading to maximum tensile strength. The result shows that axial force increases, tensile strength decreases. Whereas tool rotational speed and welding speed increase, tensile strength increases. Optimum values of axial force (3 /KN), tool rotational speed (900 RPM) and welding speed (75 mm/min.) during welding of A356/C355 aluminium alloys joint to maximize the tensile strength (Predicted 223.2 MPa) have been find out.

  5. Effect of process parameters on tensile strength of friction stir welding A356/C355 aluminium alloys joint

    International Nuclear Information System (INIS)

    Dwivedi, Shashi Prakash

    2014-01-01

    In the present investigation, A356/C355 aluminium alloys are welded by friction stir welding by controlling various welding parameters. A356 and C355 aluminium alloys materials have a set of mechanical and physical properties that are ideally suited for application in aerospace and automobile industries and not widely used because of its poor weldebility. To overcome this barrier, weldebility analysis of A356 and C355 aluminium alloys with high speed steel (Wc-Co) tool has been investigated. An attempt has been made to investigate the influence of the rotational speed of the tools, the axial force and welding speed on tensile strength of A356/C355 aluminium alloys joint. The experiments were conducted on a milling machine. The main focus of investigation is to determine good tensile strength. Response surface methodology (box Behnken design) is chosen to design the optimum welding parameters leading to maximum tensile strength. The result shows that axial force increases, tensile strength decreases. Whereas tool rotational speed and welding speed increase, tensile strength increases. Optimum values of axial force (3 /KN), tool rotational speed (900 RPM) and welding speed (75 mm/min.) during welding of A356/C355 aluminium alloys joint to maximize the tensile strength (Predicted 223.2 MPa) have been find out.

  6. Comparison of modification with strontium and the refining with antimony in A 356 aluminium alloys; Comparacao entre a modificacao com estroncio e o refino com antimonio em ligas de aluminio a 356

    Energy Technology Data Exchange (ETDEWEB)

    Fuoco, Ricardo; Correa, Edison Roberto; Correa, Alzira V.O.; Bocalini Junior, Mario

    1992-12-31

    Strontium and Antimony treated A356 aluminium alloy samples were metallographically characterized in the as cast and solution and aged conditions. Antimony treated alloy has shown slower spheroidizing kinetics of the Silicon particles during solution treatment, lower porosity level and higher tensile strength and elongation than Strontium treated one. (author) 26 refs., 13 figs., 2 tabs.

  7. Relationship between casting modulus and grain size in cast A356 aluminium alloys

    International Nuclear Information System (INIS)

    Niklas, A; Abaunza, U; Fernández-Calvo, A I; Lacaze, J

    2012-01-01

    Microstructure of Al-Si alloy castings depends most generally on melt preparation and on the cooling rate imposed by the thermal modulus of the component. In the case of Al-Si alloys, emphasis is put during melt preparation on refinement of pro-eutectic (Al) grains and on modification of the Al-Si eutectic. Thermal analysis has been used since long to check melt preparation before casting, i.e. by analysis of the cooling curve during solidification of a sample cast in an instrumented cup. The conclusions drawn from such analysis are however valid for the particular cooling conditions of the cups. It thus appeared of interest to investigate how these conclusions could extrapolate to predict microstructure in complicated cast parts showing local changes in the solidification conditions. For that purpose, thermal analysis cups and instrumented sand and die castings with different thermal moduli and thus cooling rates have been made, and the whole set of cooling curves thus recorded has been analysed. A statistical analysis of the characteristic features of the cooling curves related to grain refinement in sand and die castings allowed determining the most significant parameters and expressing the cube of grain size as a polynomial of these parameters. After introduction of a further parameter quantifying melt refining an excellent correlation, with a R 2 factor of 0.99 was obtained.

  8. Wear behaviour of A356 aluminium alloy reinforced with micron and nano size SiC particles

    CSIR Research Space (South Africa)

    Camagu, ST

    2013-07-01

    Full Text Available A method for producing metal matrix composites MMC was successfully implemented for mixing nano and low micron (“Hybrid”) sized SiC reinforcing particles in an aluminium alloy matrix. Due to the improved specific modulus and strength, MMC...

  9. Influence of prior natural aging on the subsequent artificial aging response of aluminium alloy A356 with respective globular and dendritic microstructures

    CSIR Research Space (South Africa)

    Moller, H

    2011-01-01

    Full Text Available Alloy A356 is one of the most popular alloys used for semisolid metal forming. The heat treatment cycles that are currently applied to semisolid processed components are mostly those that are in use for dendritic casting alloys. The assumption has...

  10. Evaluation of microstructure of A356 aluminum alloy casting ...

    Indian Academy of Sciences (India)

    The objective of this investigation was to evaluate the effect of vibrations (during solidification) on the metallurgical properties of A356 aluminum casting. Mechanical vibrations were applied to A356 aluminum alloy through set up. A356 melt has been subjected to mechanical vibration with the frequency range from 0 to 400 ...

  11. Effect of Rare Earth Erbium on Microstructure and Mechanical Properties of A356 Aluminum Alloy

    Directory of Open Access Journals (Sweden)

    LI Xiao-yan

    2018-01-01

    Full Text Available For conventional A356 aluminum alloy, the addition of rare earth elements is an effective way to modify its microstructures and improve its mechanical properties. The effect of rare earth Er on microstructures and properties of as-cast A356 aluminum alloy was studied by differential scanning calorimetry (DSC, X-ray diffraction (XRD and scanning electron microscopy (SEM. The results indicate that rare earth element Er is a good modifier for A356 aluminum alloy, which is able to improve obviously the microstructure of as-cast alloy. The addition of Er refines the primary α-Al phase, decreases the secondary dendrite arm spacing and the dendrite arm diameter, and modifies the eutectic Si in as-cast structure simultaneously. When the amount of Er reaches 0.4% (mass fraction, the same below, the refinement effect is the most significant, secondary dendrite arm spacing decreases from 53.6μm to 17.5μm and the morphology of eutectic Si transforms from thick lath-shaped to short rod-like or round granular. Compared with A356 alloy, the tensile strength and elongation of A356 aluminum alloy with the addition of 0.4%Er increase by 15.1% and 29.8% respectively.

  12. Comparison of heat treatment response of semisolid metal processed alloys A356 and F357

    CSIR Research Space (South Africa)

    Moller, H

    2010-01-01

    Full Text Available The heat treatment response of semisolid metal high pressure die cast Al-7Si-Mg alloys A356 and F357 was studied and compared. It was found that the heat treatment behaviour of alloy F357 is influenced markedly by the stability of the Mg containing...

  13. Effect of Dynamic Composite Refinement and Modification on Microstructure of A356 Aluminum Alloy

    Directory of Open Access Journals (Sweden)

    WANG Zheng-jun

    2017-01-01

    Full Text Available To make up for the inadequacy of Sr modification,Al-5Ti-1B-1RE master alloy refiner was prepared,then were used together with Al-10Sr master alloy for dynamic composite refinement and modification of A356 alloy.The A356 alloy microstructure of modification was studied and compared with the theoretical calculating results.The results show that the melt is fiercely stirred and vibrated by the JJ-1 laboratory electric stirrer;the refining effect of α-Al phase is excellent;the coarse and needle-like eutectic Si phase transforms into tiny,widely dispersed spherical particles and well-distributed at the grain boundaries.And mechanical property of the A356 alloy increases obviously.The grain size control study results are consistent with Johnson-Mehl equation theory.At the same time,the contents of gases of the A356 alloy are significantly reduced,which can not be achieved by Sr alone.Quantitative calculating results of degassing mechanism are consistent with the approximate calculating equations of thermodynamics and Stokes Law.

  14. Effect of Eu addition on the microstructures and mechanical properties of A356 aluminum alloys

    Energy Technology Data Exchange (ETDEWEB)

    Mao, Feng; Yan, Guangyuan; Xuan, Zhenjing [Key Laboratory of Materials Modification by Laser, Ion, and Electron Beams (Ministry of Education), School of Materials Science and Engineering, Dalian University of Technology, Dalian 116024 (China); Cao, Zhiqiang, E-mail: caozq@dlut.edu.cn [Laboratory of Special Processing of Raw Materials, Dalian University of Technology, Dalian 116024 (China); Wang, Tongmin, E-mail: tmwang@dlut.edu.cn [Key Laboratory of Materials Modification by Laser, Ion, and Electron Beams (Ministry of Education), School of Materials Science and Engineering, Dalian University of Technology, Dalian 116024 (China)

    2015-11-25

    The effect of Eu additions (0, 0.02, 0.04, 0.06, 0.08 and 0.1 wt.%) and T6 heat treatment on the microstructures and mechanical properties of A356 alloy have been investigated in the present work. Microstructures of the as-cast and T6 heat treated samples were examined by optical microscopy (OM) and scanning electron microscopy (SEM). It was found that 0.1%Eu modified the eutectic Si from a coarse plate-like form to a fully modified and fine fibrous one with a better uniform distribution. T6 treatment encouraged the spheroidization of eutectic Si particles. Correlating with the as-cast samples, the 0.1%Eu modified A356 alloy achieved likewise full modification of eutectic Si particles with lowest mean area and aspect ratio. In addition, the coarse and small Eu-rich intermetallics were both found in the 0.1%Eu modified A356 alloy. The cooling curves of A356 alloys showed that increasing Eu addition resulted in increasing nucleation undercooling and increasing growth undercooling. However, the recalescence (T{sub G} − T{sub Min}) increased by the initial addition of Eu, while it remained relatively stable for increasing additions (above 0.06%). The quenching experiment indicated that a large number of eutectic grains were located at or close to the tips of the aluminum dendrites with a jagged solid–liquid interface in unmodified alloy, while very few eutectic grains were formed in the interdendritic region with a smooth solid–liquid interface in 0.1%Eu modified alloy. An optimal combination of UTS (265 MPa) and EI (14.7%) of A356 alloy was achieved by the 0.1%Eu addition combined with T6 heat treatment. - Highlights: • The rare earth Eu is firstly used to improve the mechanical property of A356 alloy. • A fully modified and fine fibrous eutectic Si is observed by addition of 0.1 wt% Eu. • A complete spheroidization of 0.1wt%Eu modified eutectic Si is observed after T6. • Three kinds of Eu-rich intermetallics are found in the 0.1%Eu modified A356 alloy

  15. Influence of temper condition on microstructure and mechanical properties of semisolid metal processed Al–Si–Mg alloy A356

    CSIR Research Space (South Africa)

    Moller, H

    2009-01-01

    Full Text Available The microstructures and mechanical properties of strontium modified semisolid metal high pressure die cast A356 alloy are presented. The alloy A356-F (as cast) has a globular primary grain structure containing a fine eutectic. Solution treatment...

  16. Recent developments in advanced aircraft aluminium alloys

    International Nuclear Information System (INIS)

    Dursun, Tolga; Soutis, Costas

    2014-01-01

    Highlights: • To compete with composites, performance of aluminium alloys should be increased. • Al–Li alloys have higher strength, fracture and fatigue/corrosion resistance. • Improvements of aerospace Al alloys are due to optimised solute content and ratios. • In selecting new materials, there should be no reduction in the level of safety. • The use of hybrid materials could provide additional opportunities for Al alloys. - Abstract: Aluminium alloys have been the primary material for the structural parts of aircraft for more than 80 years because of their well known performance, well established design methods, manufacturing and reliable inspection techniques. Nearly for a decade composites have started to be used more widely in large commercial jet airliners for the fuselage, wing as well as other structural components in place of aluminium alloys due their high specific properties, reduced weight, fatigue performance and corrosion resistance. Although the increased use of composite materials reduced the role of aluminium up to some extent, high strength aluminium alloys remain important in airframe construction. Aluminium is a relatively low cost, light weight metal that can be heat treated and loaded to relatively high level of stresses, and it is one of the most easily produced of the high performance materials, which results in lower manufacturing and maintenance costs. There have been important recent advances in aluminium aircraft alloys that can effectively compete with modern composite materials. This study covers latest developments in enhanced mechanical properties of aluminium alloys, and high performance joining techniques. The mechanical properties on newly developed 2000, 7000 series aluminium alloys and new generation Al–Li alloys are compared with the traditional aluminium alloys. The advantages and disadvantages of the joining methods, laser beam welding and friction stir welding, are also discussed

  17. Natural and artificial aging response of semisolid metal processed Al–Si–Mg alloy A356

    CSIR Research Space (South Africa)

    Moller, H

    2007-12-01

    Full Text Available useful tool to gauge the effect of changes to the heat treatment cycles of SSM HPDC A356. The best QI in this study was obtained using a short solution heat treatment of only 1 h at 540uC, no natural aging and artificial aging at 180uC for 1 h. 5.... Sahoo, J. H. Sokolowski, P. Burke and M. Hart: Proc. 132th TMS Annual Conf., San Diego, CA, USA, March 2003, TMS, 983–989. 15. M. Badiali, C. J. Davidson, J. R. Griffiths and A. Zanada: Proc. 6th Int. Conf. on ‘Semi-solid processing of alloys...

  18. Irradiation effects in magnesium and aluminium alloys

    International Nuclear Information System (INIS)

    Sturcken, E.F.

    1979-01-01

    Effects of neutron irradiation on microstructure, mechanical properties and swelling of several magnesium and aluminium alloys were studied. The neutron fluences of 2-3 X 10 22 n/cm 2 , >0.2 MeV produced displacement doses of 20 to 45 displacements per atom (dpa). Ductility of the magnesium alloys was severely reduced by irradiation induced recrystallization and precipitation of various forms. Precipitation of transmuted silicon occurred in the aluminium alloys. However, the effect on ductility was much less than for the magnesium alloys. The magnesium and aluminium alloys had excellent resistance to swelling: The best magnesium alloy was Mg/3.0 wt% Al/0.19 wt% Ca; its density decreased by only 0.13%. The best aluminium alloy was 6063, with a density decrease of 0.22%. (Auth.)

  19. Dynamic and Thermal Properties of Aluminum Alloy A356/Silicon Carbide Hollow Particle Syntactic Foams

    Directory of Open Access Journals (Sweden)

    James Cox

    2014-12-01

    Full Text Available Aluminum alloy A356 matrix syntactic foams filled with SiC hollow particles (SiCHP are studied in the present work. Two compositions of syntactic foams are studied for quasi-static and high strain rate compression. In addition, dynamic mechanical analysis is conducted to study the temperature dependent energy dissipation and damping capabilities of these materials. The thermal characterization includes study of the coefficient of thermal expansion (CTE. A356/SiCHP syntactic foams are not strain rate sensitive as the compressive strength displayed little variation between the tested strain rates of 0.001–2100 s−1. Microscopic analysis of the high strain rate compression tested specimens showed that the fracture is initiated by the failure of hollow particles at the onset of the plastic deformation region. This is followed by plastic deformation of the matrix material and further crushing of particles. The syntactic foams showed decrease in storage modulus with increasing temperature and the trend was nearly linear up to 500 °C. The alloy shows a similar behavior at low temperature but the decrease in storage modulus increases sharply over 375 °C. The loss modulus is very small for the tested materials because of lack of viscoelasticity in metallic materials. The trend in the loss modulus is opposite, where the matrix alloy has lower loss modulus than syntactic foams at low temperature. However, over 250 °C the matrix loss modulus starts to increase rapidly and attains a peak around 460 °C. Syntactic foams have higher damping parameter at low temperatures than the matrix alloy. Incorporation of SiCHP helps in decreasing CTE. Compared to the CTE of the matrix alloy, 23.4 × 10−6 °C−1, syntactic foams showed CTE values as low as 11.67 × 10−6 °C−1.

  20. Surface treatments for aluminium alloys

    Science.gov (United States)

    Ardelean, M.; Lascău, S.; Ardelean, E.; Josan, A.

    2018-01-01

    Typically, in contact with the atmosphere, the aluminium surface is covered with an aluminium oxide layer, with a thickness of less than 1-2μm. Due to its low thickness, high porosity and low mechanical strength, this layer does not protect the metal from corrosion. Anodizing for protective and decorative purposes is the most common method of superficial oxidation processes and is carried out through anodic oxidation. The oxide films, resulted from anodizing, are porous, have a thickness of 20-50μm, and are heat-resistant, stable to water vapour and other corrosion agents. Hard anodizing complies with the same obtains principles as well as decorative and protective anodization. The difference is in that hard anodizing is achieved at low temperatures and high intensity of electric current. In the paper are presented the results of decorative and hard anodization for specimens made from several aluminium alloys in terms of the appearance of the specimens and of the thickness of the anodized.

  1. Secondary Solidification Behavior of A356 Aluminum Alloy Prepared by the Self-Inoculation Method

    Directory of Open Access Journals (Sweden)

    Ming Li

    2017-06-01

    Full Text Available Semisolid slurry of A356 aluminum alloy was prepared by Self-Inoculation Method, and the secondary solidification behavior during rheo-diecasting forming process was researched. The results indicate that the component with non-dendritic and uniformly distributed microstructures can be produced by Rheo-Diecasting (RDC process (combining Self-inoculation Method (SIM with High Pressure Die Casting (HPDC. The isothermal holding time of the slurry has large effect on primary particles, but has little effect on secondary particles. Growth rate of the primary particles in the isothermal holding process conforms to the dynamic equation of Dt3 − D03 = Kt. The suitable holding time for rheo-diecasting of A356 aluminum alloy is 3 min. During filling process, the nucleation occurs throughout the entire remaining liquid, and nuclei grow stably into globular particles with the limited grain size of 6.5μm firstly, then both α1 and α2 particles appear unstable growth phenomenon due to the existence of constitutional undercooling. The average particle sizes and shape factors of both α1 and α2 are decreasing with the increase of filling distance due to different cooling rate in different positions. The growth rate of the eutectic in RDC is 4 times faster than HPDC, which is mainly due to the limitation of α2 particles in RDC process. The average eutectic spacings are decreasing with the increase of filling distance.

  2. Shot peening of aluminium alloys

    International Nuclear Information System (INIS)

    Le Guernic, Y.

    1998-01-01

    Shot peening is a process of cold-hammering where a metallic surface is pelted with spherical grains. Each grain bumping into the surface acts as a hammer head and creates a small crater. The overlapping of these craters produces a residual compression layer just underneath the surface. It is well known that cracks cannot spread in a compression zone. In most cases of fatigue rupture and stress corrosion cracks propagate from the surface towards the inside so shot peening allows a longer lifetime of castings. Moreover most materials present a better resistance due to the cold-hammering effect of shot peening. Metallic surfaces can be treated in workshops or directly on site. Typical pieces that undergo shot peening on site are storing tanks, gas and steam turbines, tubes of steam generators and piping in oil or nuclear or chemical industries. This article describes shot peening from a theoretical and general point of view and presents the application to aluminium-lithium alloys. In the case of aluminium alloys shot peening can be used to shape the piece (peen-forming). (A.C.)

  3. Characterization of aluminium alloys rapidly solidified

    International Nuclear Information System (INIS)

    Monteiro, W.A.

    1988-01-01

    This paper discussed the investigation of the microstructural and mechanical properties of the aluminium alloys (3003; 7050; Al-9% Mg) rapidly solidified by melt spinning process (cooling rate 10 4 - 10 6 K/s). The rapidly solidification process of the studied aluminium alloys brought a microcrystallinity, a minimum presence of coarse precipitation and, also, better mechanical properties of them comparing to the same alloys using ingot process. (author) [pt

  4. Effect of hydrogen on aluminium and aluminium alloys: A review

    DEFF Research Database (Denmark)

    Ambat, Rajan; Dwarakadasa, E.S.

    1996-01-01

    Susceptibility of aluminium and its alloys towards hydrogen embrittlement has been well established. Still a lot of confusion exists on the question of transport of hydrogen and its possible role in stress corrosion cracking. This paper reviews some of the fundamental properties of hydrogen...... in aluminium and its alloys and its effect on mechanical properties. The importance of hydrogen embrittlement over anodic dissolution to explain the stress corrosion cracking mechanism of these alloys is also examined in considerable detail. The various experimental findings concerning the link between...... hydrogen embrittlement and stress corrosion cracking are also discussed....

  5. Machinability of magnesium and aluminium alloys. Part I: cutting resistance

    International Nuclear Information System (INIS)

    Balout, B.; Songmene, V.; Masounave, J.

    2002-01-01

    Aluminium (2.7 g/cm 3 ) and magnesium (1.7 g/cm 3 ) are two competing light metals with similar mechanical properties and excellent possibilities for recycling. The forming of magnesium is often seen as an impediment to its use. New forming techniques using magnesium shavings are being developed, particularly in Japan. The machining of magnesium alloys by removal of metal raises safety concerns (risk of fire), which limits many potential applications of magnesium. The purpose of this work is to clarify and compare the machining properties of these two types of metal and better understand the mechanisms that may explain the differences in behaviour. Such a comparison could eventually provide an estimate of the cost of producing shavings for the manufacture of aluminium and magnesium parts through forging and extrusion, which would limit environmental pollution. Based on an analysis of cutting resistance during machining, it was demonstrated that magnesium alloys are easier to machine than similar aluminium alloys. Magnesium shavings are shorter than those of 6061-T6, but are especially more regular than those of A356, and their size is independent of cutting speed. It was also demonstrated that the fragility of materials can be characterized based on the results of cutting resistance produced during drilling

  6. Impact toughness of laser surface alloyed Aluminium

    CSIR Research Space (South Africa)

    Mabhali, Luyolo AB

    2012-03-01

    Full Text Available Laser surface alloying of aluminium AA1200 was performed with a 4kW Nd:YAG laser and the impact resistance of the alloys was investigated. The alloying powders were a mixture of Ni, Ti and SiC in different proportions. Surfaces reinforced...

  7. Rheologic behaviors of A356 aluminum alloy billet produced by semisolid continuous casting process

    Directory of Open Access Journals (Sweden)

    Shuming XING

    2004-08-01

    Full Text Available The experiments for rheologic behaviors of semisolid continous casting billets of A356 alloy in semisolid state has been carried out with a multifunctional rheometer. The results show that the deformation rate increases with loading time, the maximum strain reaches 120% (which is one time larger than that of traditional casting billet and the strain can be rapidly eliminated to 10% after unloading. Moreover, there is a critic stress for billet deformation even in semisolid state, which is named as critic shear stress. This stress increases with the decreasing of heating time. The rheologic behaviors can be expressed by five elements mechanical model and can be modified with the increasing of heating time.

  8. Alloys of uranium and aluminium with low aluminium content

    International Nuclear Information System (INIS)

    Cabane, G.; Englander, M.; Lehmann, J.

    1955-01-01

    Uranium, as obtained after spinning in phase γ, presents an heterogeneous structure with large size grains. The anisotropic structure of the metal leads to an important buckling and surface distortion of the fuel slug which is incompatible with its tubular cladding for nuclear fuel uses. Different treatments have been made to obtain an isotropic structure presenting high thermal stability (laminating, hammering and spinning in phase α) without success. Alloys of uranium and aluminium with low aluminium content present important advantage in respect of non allied uranium. The introduction of aluminium in the form of intermetallic compound (UAl 2 ) gives a better resistance to thermal fatigue. Alloys obtained from raw casting present an improved buckling and surface distortion in respect of pure uranium. This improvement is obtained with uranium containing between 0,15 and 0,5 % of aluminium. An even more improvement in thermal stability is obtained by thermal treatments of these alloys. These new characteristics are explained by the fine dispersion of the UAl 2 particles in uranium. The results after treatments obtained from an alloy slug containing 0,4 % of aluminium show no buckling or surface distortion and no elongation. (M.P.)

  9. Semi-solid A356 alloy slurry for rheocasting prepared by a new process

    Directory of Open Access Journals (Sweden)

    Liu Zheng

    2013-05-01

    Full Text Available To obtain the semi-solid slurry with uniform and fine structure morphology that satisfies the requirement of rheocasting process, a new process for preparing semi-solid Al alloy slurry was developed, in which local chilling was combined with low superheat pouring and slight electromagnetic stirring (LSPSEMS. The morphology and the size of primary α-Al in the A356 alloy slurry prepared with the new process, i.e., LSPSEMS with local chilling, were investigated using MIAPS image analyzing software, and the grain refinement mechanism was discussed. The results indicate that the semi-solid primary phase consists of particle-like or globular-like α-Al, and the morphology and grain size of primary α-Al in the slurry can be markedly improved by the new process. The fine primary α-Al distributes uniformly in the slurry, which satisfies the requirement of rheocasting. Compared with the alloy prepared by LSPSEMS, the average equal-area-circle grain diameter of primary α-Al in semi-solid A356 alloy ingot prepared by the new process is decreased from 85.6 μm to 68.8 μm at the central area, 112.6 μm to 77.6 μm at the transition area and is 84.7 μm in the edge area, respectively. The corresponding shape factor of primary α-Al is increased from 0.78 to 0.83, 0.54 to 0.77 and 0.28 to 0.59, respectively. In addition, the pouring temperature could be suitably raised from 620-630 ℃ of the traditional process to 650 ℃ using this technique, which is convenient for practical operation. The mechanism of grain refinement, in the new process, is that the local chilling quickens up the temperature decrease in the center of the melt. The nuclei could not grow up in a short time so the finer grains are formed in the melt.

  10. Comparison of the heat treatment response of SSM-HPDC 6082 and 6004 wrought alloys with A356 and F357 casting alloys

    CSIR Research Space (South Africa)

    Müller, H

    2011-06-01

    Full Text Available Semi-solid metal high pressure die casting was used to produce plates from traditional wrought Al-Mg-Si alloys 6082 and 6004, as well as from traditional casting Al-Si-Mg alloys A356 and F357. The high Si-content of the casting alloys offer several...

  11. X-Ray Microtomographic Characterization of Porosity in Aluminum Alloy A356

    Science.gov (United States)

    Lashkari, Omid; Yao, Lu; Cockcroft, Steve; Maijer, Daan

    2009-04-01

    The presence of microporosity can, in certain circumstances, lead to a significant reduction in the mechanical properties of cast aluminum alloys. The size of the microporosity is especially crucial to the performance of castings in fatigue applications. The aim of this study is to investigate the effect of cooling rate and degassing time on the formation and evolution of microporosity in aluminum alloy A356 (Al-7Si-0.3Mg) castings using traditional metallography and X-ray microtomography (XMT) methods. The final results clearly confirm that increasing the cooling rate and degassing time yield lower microporosity within the microstructure. The XMT analysis enabled the calculation of the volume fraction and size distribution of microporosity. The XMT analysis revealed a bimodel distribution of pores with one population of small pores and a second population of large pores. The large population has been attributed to hydrogen gas solubility, whereas the smaller population is proposed to be linked to the localized entrapment of liquid metal occurring at the end of mass feeding.

  12. Interdiffusion between U(Mo,Pt) or U(Mo,Zr) and Al or Al A356 alloy

    International Nuclear Information System (INIS)

    Komar Varela, C.; Mirandou, M.; Arico, S.; Balart, S.; Gribaudo, L.

    2009-01-01

    Solid state reactions in chemical diffusion couples U-7 wt.%Mo-0.9 wt.%Pt/Al at 580 deg. C and U-7 wt.%Mo-0.9 wt.%Pt/Al A356 alloy, U-7 wt.%Mo-1 wt.%Zr/Al and U-7 wt.%Mo-1 wt.%Zr/Al A356 alloy at 550 deg. C were characterized. Results were obtained from optical and scanning electron microscopy, electron probe microanalysis and X-ray diffraction. The UAl 3, UAl 4 and Al 20 Mo 2 U phases were identified in the interaction layers of γU(Mo,Pt)/Al and γU(Mo,Zr)/Al diffusion couples. Al 43 Mo 4 U 6 ternary compound was also identified in γU(Mo,Zr)/Al due to the decomposition of γU(Mo,Zr) phase. The U(Al,Si) 3 and U 3 Si 5 phases were identified in the interaction layers of γU(Mo,Pt)/Al A356 and γU(Mo,Zr)/Al A356 diffusion couples. These phases are formed due to the migration of Si to the interaction layer. In the diffusion couple U(Mo,Zr)/Al A356, Zr 5 Al 3 phase was also identified in the interaction layer. The use of synchrotron radiation at Brazilian Synchrotron Light Laboratory (LNLS, CNPq, Campinas, Brazil) was necessary to achieve a complete crystallographic characterization.

  13. Comparison of Lost Foam Casting of AM60B Alloy and A356 Alloy

    Energy Technology Data Exchange (ETDEWEB)

    Han, Qingyou [ORNL; Dinwiddie, Ralph Barton [ORNL; Sklad, Philip S [ORNL; Currie, Kenneth [Tennessee Technological University; Vondra, Fred [Tennessee Technological University; Abdelrahman, Mohamed [Tennessee Technological University; Walford, Graham [Walford Technologies; Nolan, Dennis J [Foseco-Morval; Nedkova, Teodora [Kaiser Aluminum

    2007-01-01

    The article describes the research activities at Oak Ridge National Laboratory and Tennessee Technological University on lost foam casting of magnesium alloys. The work was focused on castings of simple geometries such as plate castings and window castings in order to compare the difference in castability between magnesium alloys and aluminum alloy using the lost foam casting process. Significant differences between lost foam aluminum casting and lost foam magnesium casting have been observed.

  14. Improving mechanical properties of aluminium alloy through ...

    African Journals Online (AJOL)

    This paper investigates the microstructure and mechanical properties of aluminum alloy (Al-Si-Fe) reinforced with coconut shell-ash particulate. The aluminium (Al-Si-Fe) alloy composite was produced by a double-stir casting process at a speed of 700 rpm for 10 and 5 minutes at first and second stirring respectively.

  15. Steam Initiated Surface Modification of Aluminium Alloys

    DEFF Research Database (Denmark)

    Din, Rameez Ud

    The extensive demand of aluminium alloys in various industries such as in transportationis mainly due to the high strength to weight ratio, which could be translated into fuel economy and efficiency. Corrosion protection of aluminium alloys is an important aspect for all applications which includes...... to 12 present various experimental results in the form of appended papers. The chapters consist of the experimental results obtained by the use of steam-based process and its effect on microstructureand corrosion resistance of the alloy as a function of steam pressure, use of various chemicals...... the use of aluminium alloys in the painted form requiring a conversion coating to improve the adhesion. Chromate based conversion coating processes are extremely good for these purposes, however the carcinogenic and toxic nature of hexavalent chromium led to the search for more benign and eco...

  16. Impact toughness of laser alloyed aluminium AA1200 alloys

    CSIR Research Space (South Africa)

    Mabhali, Luyolo AB

    2013-08-01

    Full Text Available Laser surface alloying of aluminium AA1200 was performed with a 4kW Nd:YAG laser and impact resistance of the alloys was investigated. The alloying powders were a mixture of Ni, Ti and SiC in different proportions. Surfaces reinforced...

  17. Steam generated conversion coating on aluminium alloys

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Jellesen, Morten Stendahl; Ambat, Rajan

    Aluminium and its alloys are widely used in aerospace industry owing to their high strength to weight ratio. The surface of aluminium under normal conditions has a thin oxide film (2.5-10 nm) responsible for its inherent corrosion resistance. This oxide film can further be converted or transformed...... into functional conversion coatings in order to enhance corrosion resistance and adhesion to paint systems. Chromium based conversion coatings have been extensively used on aluminium alloys to improve adhesion of subsequent paint layers and corrosion resistance. However, the use of hexavalent chromium is strictly...... and growth of oxide film on different intermetallic particles and corrosion behaviour of such alloys.Surface morphology was observed by using FEG-SEM, EDX and FIB-SEM. Metal oxide surface characterization and compositional depth profiling were investigated by using XPS and GD-OES respectively...

  18. Effect of holding pressure on microstructure and fracture behavior of low-pressure die cast A356-T6 alloy

    Science.gov (United States)

    Wu, Xiaoyan; Yun, Ying; Zhang, Huarui; Ma, Zhen; Jia, Lina; Tao, Tongxiang; Zhang, Hu

    2017-12-01

    The effect of different holding pressures on microstructure, tensile properties and fracture behavior of A356-T6 aluminum alloy was investigated. It was observed that the ultimate strength, yield strength and elongation of A356-T6 aluminum alloy increased with the increasing of holding pressure from 85 kPa to 300 kPa. This was attributed to the finer microstructure and the elimination of porosity defects caused by high holding pressure. The fractographs of specimens obtained under lower holding pressure displayed mixed quasi-cleavage and dimple type morphology with flat dimples and large amount of porosities. However, the fractographs of specimens obtained under high holding pressure of 300 kPa clearly exhibited a dimple morphology with small and deep dimples. The differences in the tensile fracture were attributed to the different shape of eutectic Si particle and different amount of porosity defects.

  19. Friction Welding of Aluminium and Aluminium Alloys with Steel

    Directory of Open Access Journals (Sweden)

    Andrzej Ambroziak

    2014-01-01

    Full Text Available The paper presents our actual knowledge and experience in joining dissimilar materials with the use of friction welding method. The joints of aluminium and aluminium alloys with the different types of steel were studied. The structural effects occurring during the welding process were described. The mechanical properties using, for example, (i microhardness measurements, (ii tensile tests, (iii bending tests, and (iv shearing tests were determined. In order to obtain high-quality joints the influence of different configurations of the process such as (i changing the geometry of bonding surface, (ii using the interlayer, or (iii heat treatment was analyzed. Finally, the issues related to the selection of optimal parameters of friction welding process were also investigated.

  20. Fabrication and Performance Test of Aluminium Alloy-Rice Husk Ash Hybrid Metal Matrix Composite as Industrial and Construction Material

    Directory of Open Access Journals (Sweden)

    Md. Rahat Hossain

    2017-12-01

    Full Text Available Aluminium matrix composites (AMCs used extensively in various engineering fields due to their exceptional mechanical properties. In this present study, aluminium matrix composites (AMCs such as aluminium alloy (A356 reinforced with rice husk ash particles (RHA are made to explore the possibilities of reinforcing aluminium alloy. The stir casting method was applied to produce aluminium alloy (A356 reinforced with various amounts of (2%, 4%, and 6% rice husk ash (RHA particles. Physical treatment was carried out before the rice husk ash manufacturing process. The effect of mechanical strength of the fabricated hybrid composite was investigated. Therefore, impact test, tensile stress, compressive stress, and some other tests were carried out to analyse the mechanical properties. From the experimental results, it was found that maximum tensile, and compressive stress were found at 6% rice husk ash (RHA and aluminium matrix composites (AMCs. In future, the optimum percentages of rice husk ash (RHA to fabricate the hybrid composites will be determined. Also, simulation by finite element method (FEM will be applied for further investigation.

  1. Numerical predicting of recycling friendly wrought aluminium alloy compositions

    Directory of Open Access Journals (Sweden)

    Varužan Kevorkijan

    2013-09-01

    Full Text Available The model presented in this work enables the design of optimal (standard and non-standard “recycling-friendly” compositions and properties of wrought aluminium alloys with significantly increased amounts of post-consumed scrap. The following two routes were modelled in detail: (i the blending of standard and non-standard compositions of wrought aluminium alloys starting from post-consumed aluminium scrap sorted to various degrees simulated by the model; and (ii changing the initial standard composition of wrought aluminium alloys to non-standard “recycling friendly” ones - with broader concentration tolerance limits of alloying elements, without influencing the selected alloy properties, specified in advance.

  2. Steam Assisted Accelerated Growth of Oxide Layer on Aluminium Alloys

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Yuksel, Serkan; Jellesen, Morten Stendahl

    2013-01-01

    Corrosion resistance of aluminium alloys is related to the composition and morphology of the oxide film on the surface of aluminium. In this paper we investigated the use of steam on the surface modification of aluminium to produce boehmite films. The study reveals a detailed investigation...... of the effect of vapour pressure, structure of intermetallic particles and thickness of boehmite films on the corrosion behaviour of aluminium alloys....

  3. Effects and mechanisms of grain refinement in aluminium alloys

    Indian Academy of Sciences (India)

    Unknown

    Abstract. Grain refinement plays a crucial role in improving characteristics and properties of cast and wrought aluminium alloys. Generally Al–Ti and Al–Ti–B master alloys are added to the aluminium alloys to grain refine the solidified product. The mechanism of grain refinement is of considerable controversy in the scientific ...

  4. Effects and mechanisms of grain refinement in aluminium alloys

    Indian Academy of Sciences (India)

    2016-08-26

    Aug 26, 2016 ... Grain refinement plays a crucial role in improving characteristics and properties of cast and wrought aluminium alloys. Generally Al–Ti and Al–Ti–B master alloys are added to the aluminium alloys to grain refine the solidified product. The mechanism of grain refinement is of considerable controversy in the ...

  5. Rotary bending fatigue behavior of A356 –T6 aluminum alloys by vacuum pressurizing casting

    Directory of Open Access Journals (Sweden)

    Yong-qin Liu

    2015-09-01

    Full Text Available Vacuum pressurizing casting technique, providing better mould filling and inter-dendritic feeding, can reduce the porosity greatly in cast aluminum alloys, and improve the fatigue properties. The rotary bending fatigue properties of A356-T6 alloys prepared by vacuum pressurizing casting were investigated. The S-N curve and limit strength 90 MPa under fatigue life of 107 cycles were obtained. The analyses on the fatigue fractography and microstructure of specimens showed that the fatigue fracture mainly occurs at the positions with casting defects in the subsurface, especially at porosities regions, which attributed to the crack propagation during the fatigue fracture process. Using the empirical crack propagation law of Pairs-Erdogon, the quantitative relationship among the initial crack size, fatigue life and applied stress was established. The fatigue life decreases with an increase in initial crack size. Two constants in the Pairs-Erdogon equation of aluminum alloy A356-T6 were calculated using the experimental data.

  6. Influence of heat treatments for laser welded semi solid metal cast A356 alloy on the fracture mode of tensile specimens

    CSIR Research Space (South Africa)

    Kunene, G

    2008-09-01

    Full Text Available The CSIR rheo-process was used to prepare the aluminium A356 SSM slurries and thereafter plates (4x80x100 mm3) were cast using a 50 Ton Edgewick HPDC machine. Plates in the as cast, T4 and T6 heat treatment conditions which had passed radiography...

  7. The effect of trace amounts of antimony on the structure and properties of aluminum alloy A356. 2

    Energy Technology Data Exchange (ETDEWEB)

    Tuttle, B.L. (Tuttle (B.L.) (USA)); Keslinke, A. (Cast Metals Inst., Des Plaines, IL (USA)); Twarog, D.L. (American Foundrymens' Society, Des Plaines, IL (USA)); Daniels, E.J. (Argonne National Lab., IL (USA))

    1989-01-01

    This investigation was performed to determine the effect of trace amounts of antimony (Sb) on the microstructure, mechanical properties, and casting properties of strontium-modified A356.2 aluminum alloy that was cast in chemically bonded sand molds. The aluminum-silicon alloys were prepared in a high-frequency induction furnace from primary A356.2 ingot of commercial purity. Each melt was grain-refined with aluminum-titanium rod, modified with aluminum-strontium-silicon rod, and degassed with dry nitrogen. Five heats were prepared at each target level of Sb: 0.00, 0.05, 0.10, 0.15 and 0.20 wt %. Significant changes in mechanical and foundry properties resulted from changes in the morphology of the aluminum-silicon eutectic microstructure at the different Sb concentrations. The principle mechanical property affected was elongation (ductility). At an Sb concentration of 0.00%, elongation was 5.3%. At a concentration of 0.06%, elongation decreased to 2.9%. The fluidity of the alloy was also affected. At all three temperatures investigated, fluidity declined approximately 17% at 0.14% Sb relative to alloy containing no Sb. At an Sb content of 0.26%, the fluidity increased approximately 22% (relative to that at 0.14% Sb) to a value slightly higher than that of the Sr-modified alloy containing no Sb. None of the thermal analysis curves for the five levels of Sb addition indicated a cooling curve inflection that could be attributed to the presence of Sb alone. 14 refs., 9 figs., 10 tabs.

  8. Characteristics of mold filling and entrainment of oxide film in low pressure casting of A356 alloy

    Energy Technology Data Exchange (ETDEWEB)

    Liu, Shan-Guang; Cao, Fu-Yang; Zhao, Xin-Yi; Jia, Yan-Dong; Ning, Zhi-Liang; Sun, Jian-Fei, E-mail: jfsun_hit@263.net

    2015-02-25

    The effect of pressurizing speed of low pressure casting on mold filling and mechanical properties of A356 alloy was studied. The mold filling behavior was calculated by two phase flow model using VOF (Volume of Fluid) method. In order to evaluate the accuracy of simulated results, the real mold filling process observed by X-ray radiography was compared. The results show that during mold filling the gate velocity first increased dramatically, then kept unchanged under relatively low pressurizing speed, or increased slowly under relatively high pressurizing speed. High gate velocity causes melt falling back under gravity with high speed. The falling velocity and the resultant relative rotating vortex are the main causes of oxide film entrainment in low pressure casting. The mechanical properties of the as-cast A356 alloy were measured by four-point bend test. Weibull probability plots were used to assess the fracture mechanisms under different pressurizing speeds. The results obtained in this paper illuminate on designing suitable pressurizing speed for mold filling in low pressure casting.

  9. Gating system optimization of low pressure casting A356 aluminum alloy intake manifold based on numerical simulation

    Directory of Open Access Journals (Sweden)

    Jiang Wenming

    2014-03-01

    Full Text Available To eliminate the shrinkage porosity in low pressure casting of an A356 aluminum alloy intake manifold casting, numerical simulation on filling and solidification processes of the casting was carried out using the ProCAST software. The gating system of the casting is optimized according to the simulation results. Results show that when the gating system consists of only one sprue, the filling of the molten metal is not stable; and the casting does not follow the sequence solidification, and many shrinkage porosities are observed through the casting. After the gating system is improved by adding one runner and two in-gates, the filling time is prolonged from 4.0 s to 4.5 s, the filling of molten metal becomes stable, but this casting does not follow the sequence solidification either. Some shrinkage porosity is also observed in the hot spots of the casting. When the gating system was further improved by adding risers and chill to the hot spots of the casting, the shrinkage porosity defects were eliminated completely. Finally, by using the optimized gating system the A356 aluminum alloy intake manifold casting with integrated shape and smooth surface as well as dense microstructure was successfully produced.

  10. Melt spun aluminium alloys for moulding optics

    Science.gov (United States)

    Gubbels, G.; Tegelaers, L.; Senden, R.

    2013-09-01

    Melt spinning is a rapid quenching process that makes it possible to create materials with a very fine microstructure. Due to this very fine microstructure the melt spinning process is an enabler for diamond turning optics and moulds without the need of post-polishing. Using diamond turning of melt spun aluminium one can achieve coating concept RSA-905 can be upgraded to a competitive alternative to steel in terms of price, performance and logistics. This paper presents some recent developments for improved mould performance of such concept. Hardness, wear resistance and adhesion are topics of interest and they can be applied by special coatings such as diamond-like carbon (DLC) and chromium nitride (CrN). These coatings make the aluminium alloy suitable for moulding mass production of small as well as larger optics, such as spectacle lenses.

  11. Combined Corrosion and Wear of Aluminium Alloy 7075-T6

    NARCIS (Netherlands)

    Liu, Y.; Mol, J.M.C.; Janssen, G.C.A.M.

    2016-01-01

    The aluminium alloy 7075-T6 is widely used in engineering. In some applications, like slurry transport, corrosion and abrasion occur simultaneously, resulting in early material failure. In the present work, we investigated the combined effect of corrosion and wear on the aluminium alloy 7075-T6. We

  12. Effect of Solidification Rate and Rare Earth Metal Addition on the Microstructural Characteristics and Porosity Formation in A356 Alloy

    Directory of Open Access Journals (Sweden)

    M. G. Mahmoud

    2017-01-01

    Full Text Available The present study was performed on A356 alloy with the main aim of investigating the effects of La and Ce additions to 356 alloys (with and without 100 ppm Sr on the microstructure and porosity formation in these alloys. Measured amounts of La, Ce, and Sr were added to the molten alloy. The results showed that, in the absence of Sr, addition of La and Ce leads to an increase in the nucleation temperature of the α-Al dendritic network with a decrease in the temperature of the eutectic Si precipitation, resulting in increasing the freezing range. Addition of 100 ppm Sr results in neutralizing these effects. The presence of La or Ce in the casting has a minor effect on eutectic Si modification, in spite of the observed depression in the eutectic temperature. It should be noted that Ce is more effective than La as an alternate modifying agent. According to the atomic radius ratio, rLa/rSi is 1.604 and rCe/rSi is 1.559, theoretically, which shows that Ce is relatively more effective than La. The present findings confirm that Sr is the most dominating modification agent. Interaction between rare earth (RE metals and Sr would reduce the effectiveness of Sr. Although modification with Sr causes the formation of shrinkage porosity, it also reacts with RE-rich intermetallics, resulting in their fragmentation.

  13. Friction stir surfacing of cast A356 aluminium–silicon alloy with boron carbide and molybdenum disulphide powders

    Directory of Open Access Journals (Sweden)

    R. Srinivasu

    2015-06-01

    Full Text Available Good castability and high strength properties of Al–Si alloys are useful in defence applications like torpedoes, manufacture of Missile bodies, and parts of automobile such as engine cylinders and pistons. Poor wear resistance of the alloys is major limitation for their use. Friction stir processing (FSP is a recognized surfacing technique as it overcomes the problems of fusion route surface modification methods. Keeping in view of the requirement of improving wear resistance of cast aluminium–silicon alloy, friction stir processing was attempted for surface modification with boron carbide (B4C and molybdenum disulfide (MoS2 powders. Metallography, micro compositional analysis, hardness and pin-on-disc wear testing were used for characterizing the surface composite coating. Microscopic study revealed breaking of coarse silicon needles and uniformly distributed carbides in the A356 alloy matrix after FSP. Improvement and uniformity in hardness was obtained in surface composite layer. Higher wear resistance was achieved in friction stir processed coating with carbide powders. Addition of solid lubricant MoS2 powder was found to improve wear resistance of the base metal significantly.

  14. Deviatoric response of the aluminium alloy, 5083

    Science.gov (United States)

    Appleby-Thomas, Gareth; Hazell, Paul; Millett, Jeremy; Bourne, Neil

    2009-06-01

    Aluminium alloys such as 5083 are established light weight armour materials. As such, the shock response of these materials is of great importance. The shear strength of a material under shock loading provides an insight into its ballistic performance. In this investigation embedded manganin stress gauges have been employed to measure both the longitudinal and lateral components of stress during plate impact experiments over a range of impact stresses. In turn, these results were used to determine the shear strength and to investigate the time dependence of lateral stress behind the shock front to give an indication of material response.

  15. 3D study of intermetallics and their effect on the corrosion morphology of rheocast aluminium alloy

    International Nuclear Information System (INIS)

    Mingo, B.; Arrabal, R.; Pardo, A.; Matykina, E.; Skeldon, P.

    2016-01-01

    In the present study, the effect of heat treatment T6.1 on the microstructure and corrosion behaviour of rheocast aluminium alloy A356 is investigated on the basis of 2D/3D characterization techniques and electrochemical and SKPFM measurements. Heat treatment strengthens the α-Al matrix, modifies the intermetallic particles and spheroidizes eutectic Si. These changes do not modify significantly the corrosion behaviour of the alloy. 3D SEM-Tomography clearly shows that the corrosion advances in the shape of narrow paths between closely spaced intermetallics without a major influence of eutectic Si. - Highlights: • T6.1 spheroidizes Si, strengthens the matrix and modifies the intermetallics. • Electrochemical behaviour of untreated and heat-treated alloys is similar. • 3D SEM-Tomography provides additional information on the corrosion morphology. • Corrosion advances as paths between intermetallics with little influence of Si.

  16. Solidification behavior and rheo-diecasting microstructure of A356 aluminum alloy prepared by self-inoculation method

    Directory of Open Access Journals (Sweden)

    Ming Li

    2017-01-01

    Full Text Available Semisolid slurry of A356 aluminum alloy was prepared by self-inoculation method, and the microstructure and solidification behavior during rheo-diecasting process were investigated. The results indicate that the semisolid slurry of A356 aluminum alloy can be prepared by self-inoculation method at 600 °C. Primary α-Al particles with fine and spherical morphologies are uniformly distributed when the isothermal holding time of slurry is 3 min. Liquid phase segregation occurs during rheo-diecasting process of semisolid slurry and the primary particles (α1 show obvious plastic deformation in the area of high stress and low cooling rate. A small amount of dendrites resulting from the relatively low temperature of the shot chamber at the initial stage of secondary solidification are fragmented as they pass through the in-gate during the mould filling process. The amount of dendrite fragments decreases with the increase of filling distance. During the solidification process of the remaining liquid, the nucleation rate of secondary particles (α2 increases with the increase of cooling rate, and the content of Si in secondary particles (α2 are larger than primary particles (α1. With the increase of cooling rate, the content of Si in secondary particles (α2 gradually increases. The morphologies of eutectic Si in different parts of die casting are noticeably different. The low cooling rate in the first filling positions leads to coarse eutectic structures, while the high cooling rate in the post filling positions promotes small and compact eutectic structures.

  17. Optimisation of the T6 heat treatment of rheocast alloy A356

    CSIR Research Space (South Africa)

    Moller, H

    2007-11-01

    Full Text Available The heat treatment cycles that are currently applied to processed components are mostly those that are in use for traditional dendritic alloys. These heat treatments are not necessarily the optimum heat treatments for SSM processing. The T6 heat...

  18. Natural and artificial aging response of semi-solid metal processed alloy A356

    CSIR Research Space (South Africa)

    Möller, H

    2008-09-01

    Full Text Available The heat treatment cycles that are currently applied to semi-solid processed components are mostly those that are in use for dendritic casting alloys. These heat treatments are not necessarily the optimum treatments for non-dendritic microstructures...

  19. TITANIUM CARBON ALUMINIUM : A NOVEL GRAIN REFINER FOR ALUMINIUM-LITHIUM ALLOYS

    OpenAIRE

    Birch , M.; Cowell , A.

    1987-01-01

    This work explores the possibility of achieving grain size control in aluminium-lithium alloys with the titanium carbon aluminium (TiCAl) master alloys invented at the Technical University of Berlin and developed by London and Scandinavian Metallurgical Co Ltd (LSM). Grain refining tests were conducted on a single batch of 8090 alloy using addition rates of 0.2wt% and 0.4wt% of TiCAl and 3/1 titanium boron aluminium (TiBAl). Other tests using 0.4wt% of binary TiAl gave poor results, showing t...

  20. Aluminium alloys in municipal solid waste incineration bottom ash.

    Science.gov (United States)

    Hu, Yanjun; Rem, Peter

    2009-05-01

    With the increasing growth of incineration of household waste, more and more aluminium is retained in municipal solid waste incinerator bottom ash. Therefore recycling of aluminium from bottom ash becomes increasingly important. Previous research suggests that aluminium from different sources is found in different size fractions resulting in different recycling rates. The purpose of this study was to develop analytical and sampling techniques to measure the particle size distribution of individual alloys in bottom ash. In particular, cast aluminium alloys were investigated. Based on the particle size distribution it was computed how well these alloys were recovered in a typical state-of-the-art treatment plant. Assessment of the cast alloy distribution was carried out by wet physical separation processes, as well as chemical methods, X-ray fluorescence analysis and electron microprobe analysis. The results from laboratory analyses showed that cast alloys tend to concentrate in the coarser fractions and therefore are better recovered in bottom ash treatment plants.

  1. Friction factor of CP aluminium and aluminium–zinc alloys

    Indian Academy of Sciences (India)

    zinc alloys using ring compression test at different temperatures from 303 K to 773 K. It is found that CP aluminium exhibits stick- ing whereas Al–Zn alloys do not exhibit sticking at elevated temperatures. Hot working of Al–Zn alloy is easier.

  2. Thin-film cryogenic resistors from aluminium alloys

    Science.gov (United States)

    Tadros, N. N.; Holdeman, L. B.

    The temperature dependence of the resistances of thin films sputtered from three commercially available aluminium alloys (5052, 5086, 5456) has been measured in the temperature range 1.5-4.2 K. The 5052-alloy films had a positive temperature coefficient of resistance (TCR) throughout this temperature range, whereas films of the other two alloys had a negative TCR.

  3. Corrosion of Metal-Matrix Composites with Aluminium Alloy Substrate

    Directory of Open Access Journals (Sweden)

    B. Bobic

    2010-03-01

    Full Text Available The corrosion behaviour of MMCs with aluminium alloy matrix was presented. The corrosion characteristics of boron-, graphite-, silicon carbide-, alumina- and mica- reinforced aluminium MMCs were reviewed. The reinforcing phase influence on MMCs corrosion rate as well as on various corrosion forms (galvanic, pitting, stress corrosion cracking, corrosion fatique, tribocorrosion was discussed. Some corrosion protection methods of aluminium based MMCs were described

  4. Brazing of Titanium with Aluminium Alloys

    Directory of Open Access Journals (Sweden)

    Winiowski A.

    2017-06-01

    Full Text Available This study presents results of vacuum diffusion brazing of Grade 2 titanium with 6082 (AlMg1Si0.6Cu0.3 aluminium alloy using B-Ag72Cu-780 (Ag72Cu28 grade silver brazing metal as an interlayer. Brazed joints underwent shear tests, light-microscopy-based metallographic examinations and structural examinations using scanning electron microscopy (SEM and X-ray energy dispersive spectrometry (EDS. The highest quality and shear strength of 20 MPa was characteristic of joints brazed at 530°C with a 30-minute hold. The structural examinations revealed that in diffusion zone near the boundary with titanium the braze contained solid solutions based on hard and brittle Ti-Al type intermetallic phases determining the strength of the joints.

  5. Optimization design of a gating system for sand casting aluminium A356 using a Taguchi method and multi-objective culture-based QPSO algorithm

    Directory of Open Access Journals (Sweden)

    Wen-Jong Chen

    2016-04-01

    Full Text Available This article combined Taguchi method and analysis of variance with the culture-based quantum-behaved particle swarm optimization to determine the optimal models of gating system for aluminium (Al A356 sand casting part. First, the Taguchi method and analysis of variance were, respectively, applied to establish an L27(38 orthogonal array and determine significant process parameters, including riser diameter, pouring temperature, pouring speed, riser position and gating diameter. Subsequently, a response surface methodology was used to construct a second-order regression model, including filling time, solidification time and oxide ratio. Finally, the culture-based quantum-behaved particle swarm optimization was used to determine the multi-objective Pareto optimal solutions and identify corresponding process conditions. The results showed that the proposed method, compared with initial casting model, enabled reducing the filling time, solidification time and oxide ratio by 68.14%, 50.56% and 20.20%, respectively. A confirmation experiment was verified to be able to effectively reduce the defect of casting and improve the casting quality.

  6. Three body abrasion of laser surface alloyed aluminium AA1200

    CSIR Research Space (South Africa)

    Mabhali, Luyolo AB

    2012-06-01

    Full Text Available Laser surface alloying of aluminium AA1200 was performed with a 4 kW Nd:YAG laser to improve the abrasion wear resistance. Aluminium surfaces reinforced with metal matrix composites and intermetallic phases were achieved. The phases present depended...

  7. Gas accumulation at grain boundaries during 800 MeV proton irradiation of aluminium and aluminium-alloys

    DEFF Research Database (Denmark)

    Singh, Bachu Narain; Horsewell, Andy; Sommer, W. F.

    1986-01-01

    ) showed a complete absence of voids or bubbles in the grain interiors of the aluminium and the aluminium-alloys. Bubbles were clearly visible by TEM at grain boundaries in pure Al and the AlMg3 alloy; but bubbles were not visible in the Al6061 alloy. The bubble density in the AlMg3 alloy was considerably...

  8. Evaluation of surface chemical segregation of semi-solid cast aluminium alloy A356

    CSIR Research Space (South Africa)

    Govender, G

    2008-01-01

    Full Text Available In order for SSM forming to produce homogeneous properties in a casting, it is important that there is a uniform distribution of the primary grains. Besides producing a sound casting free of porosity, the amount of liquid segregation must...

  9. Adhesive Bonding of Aluminium Alloy A5754 by Epoxy Resins

    Directory of Open Access Journals (Sweden)

    Ivan Michalec

    2013-01-01

    Full Text Available Joining thin sheets of aluminium and its alloys is a promising area in the field of joining materials. Nowadays, joining methods that do not melt the material itself are increasingly being utilised. This paper deals with adhesive bonding of aluminium alloy A5754 by two-component epoxy resins. Theresults show that joints bonded by Hysol 9466 have appropriate mechanical properties, but that joints bonded by Hysol 9492 have better thermal stability.

  10. Influence of Chemical Composition on Porosity in Aluminium Alloys

    OpenAIRE

    Kucharčík L.; Brůna M.; Sládek A.

    2014-01-01

    Porosity is one of the major defects in aluminum castings, which results is a decrease of a mechanical properties. Porosity in aluminum alloys is caused by solidification shrinkage and gas segregation. The final amount of porosity in aluminium castings is mostly influenced by several factors, as amount of hydrogen in molten aluminium alloy, cooling rate, melt temperature, mold material, or solidification interval. This article deals with effect of chemical composition on porosity in Al-Si alu...

  11. Internal friction in iron-aluminium alloys having a high aluminium content

    International Nuclear Information System (INIS)

    Hillairet, J.; Delaplace, J.; Silvent, A.

    1966-01-01

    By using a torsion pendulum to measure the internal friction of iron-aluminium alloys containing between 25 and 50 atom per cent of aluminium, it has been possible to show the existence of three damping peaks due to interstitial carbon. Their evolution is followed as a function of the carbon content, of the thermal treatment and of the aluminium content. A model based on the preferential occupation of tetrahedral sites is proposed as an interpretation of the results. A study of the Zener peak in these substitution alloys shows also that a part of the short distance disorder existing at high temperatures can be preserved by quenching. (author) [fr

  12. Effect of iron and silicon in aluminium and its alloys

    International Nuclear Information System (INIS)

    Kovacs, I.

    1990-01-01

    The iron and silicon are the main impurities in aluminium, they are always present in alloys made from commercially pure base material. The solid solubility of iron in aluminium is very low, therefore its largest amount forms intermetallic compounds the kind of which depends strongly on the other impurities of alloying elements. Although the solid solubility of silicon is much larger than that of the iron, it is the constituent of both the primary and the secondary particles, the structure of which depends in general on the iron-silicon concentration ratio. These Fe and Si containing particles can cause various and basic changes in the macroscopic properties of the alloy. Since commercially pure aluminium has extensive consumer and industrial use, it is very important to know, not only from scientific but also from practical point of view, the effect of iron and silicon on the physical and mechanical properties of aluminium and its alloys. The aim of the ''International Workshop on the Effect of Iron and Silicon in Aluminium and its Alloys'' was to clarify the present knowledge on this subject. The thirty papers presented at the Workshop and collected in this Proceedings cover many important fields of the subject. I hope that they will contribute to both the deeper understanding of the related phenomena and the improvement of technologies for producing better aluminium alloys

  13. SUPERPLASTIC BEHAVIOUR IN DYNAMICALLY RECRYSTALLISING ALUMINIUM ALLOYS

    Directory of Open Access Journals (Sweden)

    R AMICHI

    1999-12-01

    Full Text Available Aluminium alloys can be thermomechanically processed to develop the grain fine microstructures required for superplasticity by either static recrystallisation prior to superplastic forming (SPF or by dynamic recrystallisation during the early stages of deformation. The present work has examined and compared the superplastic behaviour and the microstructural evolution in Al-Li alloys (8090 sheet material processed by the second route for a wide range of temperatures and strain-rates.  It was observed that the material showed a high potential for superplastic flow. Although significant superplasticity was observed at temperature of 400°C and below. The reasons for the high resistance of the material to strain localisation are discussed.  It was noted that ductility enhancement could also be achieved by the control of the strain-rate path. A rapid pre-strain improved significantly the subsequent superplastic elongation to failure at optimum strain rate.  Further enhancement has been obtained by pre-straining at constant velocity following by deformation to failure at lower constant velocity. The microstructure changes prior or during deformation were also examined.

  14. Modeling the effects of cooling rate, hydrogen content, grain refiner and modifier on microporosity formation in Al A356 alloys

    Energy Technology Data Exchange (ETDEWEB)

    Conley, J.G.; Huang, J.; Asada, J.; Akiba, K. [Northwestern Univ., Evanston, IL (United States). Dept. of Mechanical Engineering

    2000-06-15

    Cast Aluminum-Silicon alloys are used in numerous automotive and industrial weight sensitive applications because of their low density and excellent castability. The presence of trapped gas and or shrinkage pores in certain locations within castings has been shown to influence fatigue life. These micromechanical defects can be found most anywhere in a casting depending on processing conditions. A large amount of porosity located in the center of the cast material thickness may have no effect on mechanical properties or fatigue performance. A smaller, isolated pore near a surface may have a significant impact on mechanical properties. Hence, it is important to develop a comprehensive model to predict the size, location and distribution of microporosity in castings. In this work, we model the effect of various casting process parameters on microporosity formation for aluminum A356 alloy castings. The process parameters include cooling rate, hydrogen content, grain refiner and modifier. The proposed two-dimensional model predicts the size, morphology and distribution of microporosity at a given location in the casting. The method couples a mathematical model of porosity evolution with a probabilistic grain structure prediction model. The porosity evolution model is based on the simultaneous solution of the continuity and momentum equations for the metal and the mass conservation equation for the dissolved gas. The nucleation and growth of grains are simulated with a probabilistic method that uses the information from a heat transfer simulation, i.e. temperature and solid fraction, to determine the transition rules for grain evolution. The simulation results correlate well with experimental observation of porosity in cast structures. (orig.)

  15. Local electrochemical behaviour of 7xxx aluminium alloys

    NARCIS (Netherlands)

    Andreatta, F.

    2004-01-01

    Aluminium alloys of the 7xxx series (Al-Zn-Mg-Cu) are susceptible to localized types of corrosion like pitting, intergranular corrosion and exfoliation corrosion. This represents a limitation for the application of these alloys in the aerospace components because localized corrosion might have a

  16. Numerical Modelling of Drawbeads for Forming of Aluminium Alloys

    OpenAIRE

    Joshi, Y; Christiansen, Peter; Masters, I; Bay, Niels Oluf; Dashwood, R

    2016-01-01

    The drawbeads in stamping tools are usually designed based on experience from the forming of steel. However, aluminium alloys display different forming behaviour to steels, which is not reflected in the drawbead design for tools used for stamping aluminium. This paper presents experimental results from different semi-circular drawbead geometries commonly encountered in automotive dies and compares them to those obtained from Stoughton’s analytical drawbead model and the 2D plane strain drawbe...

  17. PENGARUH VARIASI PUTARAN CETAKAN, INOKULAN TI-B PADA CENTRIFUGAL CASTING TERHADAP SIFAT MEKANIK DAN STRUKTUR MIKRO PADUAN ALUMINIUM A356.0

    Directory of Open Access Journals (Sweden)

    Eko Nugroho

    2015-06-01

    Full Text Available Paduan alumunium  A-356.0 merupakan  salah satu bahan material yang cocok untuk bahan baku pembuatan velg racing (cast wheel mobil maupun sepeda motor. Karena memiliki beberapa kelebihan seperti: ringan, tahan korosi dan warnanya menarik, namun memiliki kekurangnan yaitu sifat mekanisnya belum memenuhi syarat. proses pembuatannya  menggunakan proses Vertical Centrifugal Casting (VCC dengan penambahan inokulan Al-Ti-B sebagai unsur penghalus butir, inokulan Al-Ti-B akan dicampurkan kedalam 8 kg cairan aluminium dengan komposisi variasi campuran 0, 6, 9, dan 12 gram untuk selanjutnya dituangkan ke dalam cetakan dengan 2 variasi putaran yaitu 450 dan 850 rpm. Selanjutnya hasil dari pengecoran centrifugal casting diuji secara mekanis menggunakan pengujian standar yaitu; uji kekerasan, uji tarik dan struktur mikro nya mengunakan standar ASTM. Hasil pengujian di peroleh nilai kekerasan dan kekuatan tarik  yang paling tinggi pada spesimen A3 dan B3 yaitu 64.73 BHN dan 67.81 BHN, 182.18 Mpa  dan 188.28 Mpa. Titanium  yang  dikombinasikan  dengan  Boron  atau  Carbon  merupakan  unsur  paduan Al-Si  yang  berfungsi  untuk  menghaluskan butiran  (grain  refiner Hal  inilah  yang mempengaruhi  adanya  perubahan  sifat mekanik  dan  struktur  mikro  tersebut.  Dengan semakin  halus  butiran,  maka  penjalaran dislokasinya  akan  semakin  sulit,  sehingga mempunyai ketahanan yang lebih besar, karena diperlukan  energi  yang  lebih  besar  untuk merusak  butiran  yang  halus  tersebut. adanya gaya sentrifugal (CF selama proses penuangan kedalam cetakan. Logam cair akan dilempar oleh gaya sentrifugal sehingga menimbulkan tekanan pada setiap layer, hal ini juga menjelaskan bahwa .produk yang dibuat dengan menggunakan metode ini bebas cacat porosity, sisi terluar dari produk sentrifugal akan memiliki nilai kekerasan yang tinggi dibandingkan dengan sisi tengah produk, sifat mekanisnya juga akan memiliki nilai yang

  18. PENGARUH VARIASI PUTARAN CETAKAN DAN PENAMBAHAN INOKULAN Ti-B PADA CENTRIFUGAL CASTING TERHADAP SIFAT MEKANIK DAN STRUKTUR MIKRO PADUAN ALUMINIUM A356.0

    Directory of Open Access Journals (Sweden)

    Eko Nugroho

    2016-08-01

    Full Text Available Perkembangan industri pengecoran global hingga lokal sampai saat ini tumbuh dengan sangat pesat. Salah satu produk yang banyak dicari konsumen adalah velg, part pada roda sepeda motor. Tetapi sayangnya velg lokal sering dikeluhkan memiliki kualitas lebih rendah dari pabrikan. Paduan alumunium  A-356.0 merupakan  salah satu bahan material yang cocok untuk bahan baku pembuatan velg racing (cast wheel mobil maupun sepeda motor. Karena memiliki beberapa kelebihan seperti: ringan, tahan korosi dan warnanya menarik, namun memiliki kekurangnan yaitu sifat mekanisnya belum memenuhi syarat. proses pembuatannya  menggunakan proses Vertical Centrifugal Casting (VCC dengan penambahan inokulan Al-Ti-B sebagai unsur penghalus butir, inokulan Al-Ti-B akan dicampurkan kedalam 8 kg cairan aluminium dengan komposisi variasi campuran 0, 6, 9, dan 12 gram untuk selanjutnya dituangkan ke dalam cetakan dengan 2 variasi putaran yaitu 450 dan 850 rpm. Selanjutnya hasil dari pengecoran centrifugal casting diuji secara mekanis menggunakan pengujian standar yaitu; uji kekerasan, uji tarik dan struktur mikro nya mengunakan standar ASTM. Hasil pengujian di proleh nilai kekerasan dan kekuatan tarik  yang paling tinggi pada spesimen A3 dan B3 yaitu 64.73 BHN dan 67.81 BHN, 182.18 Mpa  dan 188.28 Mpa. Titanium  yang  dikombinasikan  dengan  Boron  atau  Carbon  merupakan  unsur  paduan Al-Si  yang  berfungsi  untuk  menghaluskan butiran  (grain  refiner Hal  inilah  yang mempengaruhi  adanya  perubahan  sifat mekanik  dan  struktur  mikro  tersebut.  Dengan semakin  halus  butiran,  maka  penjalaran dislokasinya  akan  semakin  sulit,  sehingga mempunyai ketahanan yang lebih besar, karena diperlukan  energi  yang  lebih  besar  untuk merusak  butiran  yang  halus  tersebut. adanya gaya sentrifugal (CF selama proses penuangan kedalam cetakan. Logam cair akan dilempar oleh gaya sentrifugal sehingga menimbulkan tekanan pada setiap

  19. Fatigue behaviour of GMAW welded aluminium alloy AA7020

    OpenAIRE

    Bloem, Carlos; Salvador Moya, Mª Dolores; Amigó, Vicente; Vicente-Escuder, Ángel

    2009-01-01

    [EN] The aim of this investigation is to evaluate the influence on fatigue behaviour of the finishing of the bulge in a welded aluminium zinc magnesium alloy AA7020. It was determined that total or partial elimination of the bulge has very little influence on its behaviour, giving a very similar result on both cases, where one is better than the other by only 3%. Bloem, C.; Salvador Moya, MD.; Amigó, V.; Vicente-Escuder, Á. (2009). Fatigue behaviour of GMAW welded aluminium alloy AA7020. W...

  20. Influence of Chemical Composition on Porosity in Aluminium Alloys

    Directory of Open Access Journals (Sweden)

    Kucharčík L.

    2014-06-01

    Full Text Available Porosity is one of the major defects in aluminum castings, which results is a decrease of a mechanical properties. Porosity in aluminum alloys is caused by solidification shrinkage and gas segregation. The final amount of porosity in aluminium castings is mostly influenced by several factors, as amount of hydrogen in molten aluminium alloy, cooling rate, melt temperature, mold material, or solidification interval. This article deals with effect of chemical composition on porosity in Al-Si aluminum alloys. For experiment was used Pure aluminum and four alloys: AlSi6Cu4, AlSi7Mg0, 3, AlSi9Cu1, AlSi10MgCu1.

  1. Mechanical properties of plasma-sprayed layers of aluminium and aluminium alloy on AZ 91

    Czech Academy of Sciences Publication Activity Database

    Kubatík, Tomáš František; Ctibor, Pavel; Mušálek, Radek; Janata, Marek

    2017-01-01

    Roč. 51, č. 2 (2017), s. 323-327 ISSN 1580-2949 R&D Projects: GA ČR(CZ) GP14-31538P Institutional support: RVO:61389021 Keywords : plasma spraying of aluminium * adhesion of coating * wear * magnesium alloy AZ91 Subject RIV: JG - Metallurgy OBOR OECD: Materials engineering Impact factor: 0.436, year: 2016

  2. Development of Niobium Boron grain retainer for aluminium silicon alloys

    OpenAIRE

    Nowak, Magdalena

    2011-01-01

    This thesis was submitted for the degree of Doctor of Philosophy and awarded by Brunel University Aluminium castings with a large grain structure have poor mechanical properties which are primarily due to casting defects as opposed to fine grain structure. The grain refinement practice using chemical addition is well established for wrought alloys, however in the case of casting alloys, the practice of adding grain refiners and the impact on castability is not well established. The additio...

  3. Laser alloying of aluminium to improve surface properties - MSSA 2010

    CSIR Research Space (South Africa)

    Mabhali, Luyolo AB

    2010-07-01

    Full Text Available Aluminium is vastly used in industry due to its low cost, light weight and excellent workability, but lacks in wear resistance and hardness. Laser alloying is used to improve the surface properties such as hardness by modifying the composition...

  4. Contribution to comprehensive study of aluminium alloy Aa 5083 ...

    African Journals Online (AJOL)

    Corrosion induced by elemental mercury in aqueous media of industrial Aluminium alloys AA5083 used in heat exchanger industries of natural gas liquefaction has been studied by linear sweep voltammétry on rotating amalgamated disk electrode. Corrosion process depends on: • Chemical processes of amalgamation of ...

  5. Structure analysis of 3104 aluminium alloy applied to deep drawing

    Energy Technology Data Exchange (ETDEWEB)

    Klyszewski, A.; Lech-Grega, M.; Zelechowski, J.; Szymanski, W. [Light Metals Div., Skawina (Poland). Inst. of Non-Ferrous Metals

    2000-07-01

    Optical and electron microscopy observations and X-ray investigations of 3104 aluminium alloy ingots and bands after experimental heat treatment were carried out. The influence of ingots homogenisation temperature and parameters of material heat treatment after hot rolling on structure, texture and earing of band 0.3 mm thick was analysed. (orig.)

  6. Crystallographic orientation-spray formed hypereutectic aluminium-silicon alloys

    Directory of Open Access Journals (Sweden)

    Hamilta de Oliveira Santos

    2005-06-01

    Full Text Available Aluminium-silicon alloys have been wide accepted in the automotive, electric and aerospace industries. Preferred orientation is a very common condition for metals and alloys. Particularly, aluminium induces texture during the forming process. The preparation of an aggregate with completely random crystal orientation is a difficult task. The present work was undertaken to analyse the texture by X-ray diffraction techniques, of three spray formed hypereutectic Al-Si alloys. Samples were taken from a billet of an experimental alloy (alloy 1 and were subsequently hot-rolled and cold-rolled (height reduction, 72% and 70%, respectively. The other used samples, alloys 2 and 3, were taken from cylinders liners. The results from the Laue camera showed texture just in the axial direction of alloy 3. The pole figures also indicated the presence of a typical low intensity deformation texture, especially for alloy 3. The spray formed microstructure, which is very fine, hinders the Al-Si texture formation during mechanical work.

  7. Fatigue in a heat treatable high silicon containing aluminium alloy

    Science.gov (United States)

    González, J. A.; Talamantes-Silva, J.; Valtierra, S.; Colás, Rafael

    2017-05-01

    The use of cast aluminium alloys in automobiles contributes to reductions in weight and fuel consumption without impairing the safety for the occupants or the performance of the car. Most of the alloys used are heat treatable hypoeutectic Al-Si alloys, which have the drawback of exhibiting low wear resistance. So industry relies in wear resistant alloys, such as grey iron, for the liners of the combustion chambers in engine blocks, which increase the weight of the engine. Therefore, it is of interest to cast high silicon containing alloys into engine components that are able to resist wear while maintaining the mechanical properties required by the components. This work presents the result of the work carried out in a high silicon containing heat treatable aluminium alloy as it is subjected to high cycle fatigue. The alloy was prepared and cast in ingots designed to promote one dimensional solidification gradient to obtain samples to study the high cycle fatigue. The material was machined into hour-glass specimens that were tested at room temperature in a servohydraulic machine under load control following the stair case method. The results show that the resistance to fatigue depends on the microstructure of the sample, as the fatigue cracks originate in pores close to the surface of the sample and propagate through the eutectic aggregate. The results from this work are compared with those from previously obtained with hypoeutectic alloys.

  8. The effects of radiation on aluminium alloys in the core of energy nuclear reactors

    International Nuclear Information System (INIS)

    Petrossian, V.G.

    1995-01-01

    One of the attractive directions in the worldwide practice of nuclear installations is the replacement of expensive zirconium alloy with more cheap materials, particularly aluminium allo. For Heat Supply Nuclear Plants (HSNP) with approximately 473 K core temperatures, the use of heat-resistant aluminium alloys seems to be reasonable. The present work is concerned with the studies on radiation effects on aluminium alloy, and interaction between the alloy and coolant in the reactor core. (author). 2 refs., 3 figs., 1 tab

  9. Fatigue behaviour of 6061 aluminium alloy and its composite

    OpenAIRE

    Hwa, Ping

    2001-01-01

    Fatigue behaviour of an artificial aged powder metallurgy 6061 aluminium alloy, and a composite made of this alloy with 15% volume fraction of SiCp was investigated. The alloy was subjected to T6 heat treatment, as was the composite material chosen (which incorporated SiC particles of average size 30pm). An extensive experimental programme was carried out in which fatigue lives were determined using load-controlled axial loading of unnotched cylindrical samples, at stress ratios of-1 and 0.1....

  10. Recycling of aluminium scrap for secondary Al-Si alloys.

    Science.gov (United States)

    Velasco, Eulogio; Nino, Jose

    2011-07-01

    An increasing amount of recycled aluminium is going into the production of aluminium alloy used for automotive applications. In these applications, it is necessary to control and remove alloy impurities and inclusions. Cleaning and fluxing processes are widely used during processing of the alloys for removal of inclusions, hydrogen and excess of magnesium. These processes use salt fluxes based in the system NaCl-KCl, injection of chlorine or mixture of chlorine with an inert gas. The new systems include a graphite wand and a circulation device to force convection in the melt and permit the bubbling and dispersion of reactive and cleaning agents. This paper discusses the recycling of aluminium alloys in rotary and reverberatory industrial furnaces. It focuses on the removal of magnesium during the melting process. In rotary furnaces, the magnesium lost is mainly due to the oxidation process at high temperatures. The magnesium removal is carried out by the reaction between chlorine and magnesium, with its efficiency associated to kinetic factors such as concentration of magnesium, mixing, and temperature. These factors are also related to emissions generated during the demagging process. Improvements in the metallic yield can be reached in rotary furnaces if the process starts with a proper salt, with limits of addition, and avoiding long holding times. To improve throughput in reverberatories, start the charging with high magnesium content material and inject chlorine gas if the molten metal is at the right temperature. Removal of magnesium through modern technologies can be efficiently performed to prevent environmental problems.

  11. Grain refinement of zinc-aluminium alloys

    International Nuclear Information System (INIS)

    Zaid, A.I.O.

    2006-01-01

    It is now well-established that the structure of the zinc-aluminum die casting alloys can be modified by the binary Al-Ti or the ternary Al-Ti-B master alloys. in this paper, grain refinement of zinc-aluminum alloys by rare earth materials is reviewed and discussed. The importance of grain refining of these alloys and parameters affecting it are presented and discussed. These include parameters related to the Zn-Al alloys cast, parameters related to the grain refining elements or alloys and parameters related to the process. The effect of addition of other alloying elements e.g. Zr either alone or in the presence of the main grain refiners Ti or Ti + B on the grain refining efficiency is also reviewed and discussed. Furthermore, based on the grain refinement and the parameters affecting it, a criterion for selection of the optimum grain refiner is suggested. Finally, the recent research work on the effect of grain refiners on the mechanical behaviour, impact strength, wear resistance, and fatigue life of these alloys are presented and discussed. (author)

  12. Laser surface alloying of aluminium-transition metal alloys

    International Nuclear Information System (INIS)

    Almeida, A.; Vilar, R.

    1998-01-01

    Laser surface alloying has been used as a tool to produce hard and corrosion resistant Al-transition metal (TM) alloys. Cr and Mo are particularly interesting alloying elements to produce stable high-strength alloys because they present low diffusion coefficients and solid solubility in Al. To produce Al-TM surface alloys a two-step laser process was developed: firstly, the material is alloyed using low scanning speed and secondly, the microstructure is modified by a refinement step. This process was used in the production of Al-Cr, Al-Mo and Al-Mo and Al-Nb surface alloys by alloying Cr, Mo or Nb powder into an Al and 7175 Al alloy substrate using a CO 2 laser . This paper presents a review of the work that has been developed at Instituto Superior Tecnico on laser alloying of Al-TM alloy, over the last years. (Author) 16 refs

  13. TORSIONAL DEFORMATION AND FATIGUE BEHAVIOUR OF 6061 ALUMINIUM ALLOY

    Directory of Open Access Journals (Sweden)

    marini marno

    2012-02-01

    Full Text Available Torsional deformation and fatigue behaviour of both solid and thin-walled tubular specimens were made from as-received and heat treated 6061 aluminium alloy were studied. 6061 aluminium alloy have been widely used as a candidate material in automobile, aerospace, aircraft and structural application because of their superior mechanical properties such as high strength to weight ratio, good ductility and others. The differences in cyclic deformation and fatigue behaviours between round and solid specimens where a stress gradient exist, and thin-walled tubular specimens where a uniform stress state is commonly assumed, are also discussed. Von Mises and Tresca criteria has been used to predict the monotonic and cyclic deformation curve and compared to the torsional data obtained from the experiment. The S-N curve was used to present and evaluate the fatigue life of the specimens. Through fractographic analysis, failure criteria of fracture surfaces were observed and discussed. 

  14. Distribution of trace elements in a modified and grain refined aluminium-silicon hypoeutectic alloy.

    Science.gov (United States)

    Faraji, M; Katgerman, L

    2010-08-01

    The influence of modifier and grain refiner on the nucleation process of a commercial hypoeutectic Al-Si foundry alloy (A356) was investigated using optical microscopy, scanning electron microscopy (SEM) and electron probe microanalysis technique (EPMA). Filtering was used to improve the casting quality; however, it compromised the modification of silicon. Effect of filtering on strontium loss was also studied using the afore-mentioned techniques. EPMA was used to trace the modifying and grain refining agents inside matrix and eutectic Si. This was to help understanding mechanisms of nucleation and modification in this alloy. Using EPMA, the negative interaction of Sr and Al3TiB was closely examined. In modified structure, it was found that the maximum point of Sr concentration was in line with peak of silicon; however, in case of just 0.1wt% added Ti, the peak of Ti concentration was not in line with aluminium, (but it was close to Si peak). Furthermore, EPMA results showed that using filter during casting process lowered the strontium content, although produced a cleaner melt. (c) 2010 Elsevier Ltd. All rights reserved.

  15. Corrosion behaviour of laser-cleaned AA7024 aluminium alloy

    Science.gov (United States)

    Zhang, F. D.; Liu, H.; Suebka, C.; Liu, Y. X.; Liu, Z.; Guo, W.; Cheng, Y. M.; Zhang, S. L.; Li, L.

    2018-03-01

    Laser cleaning has been considered as a promising technique for the preparation of aluminium alloy surfaces prior to joining and welding and has been practically used in the automotive industry. The process is based on laser ablation to remove surface contaminations and aluminium oxides. However the change of surface chemistry and oxide status may affect corrosion behaviour of aluminium alloys. Until now, no work has been reported on the corrosion characteristics of laser cleaned metallic surfaces. In this study, we investigated the corrosion behaviour of laser-cleaned AA7024-T4 aluminium alloy using potentiodynamic polarisation, electrochemical impedance spectroscopy (EIS) and scanning vibrating electrode technique (SVET). The results showed that the laser-cleaned surface exhibited higher corrosion resistance in 3.5 wt.% NaCl solution than as-received hot-rolled alloy, with significant increase in impedance and decrease in capacitance, while SVET revealed that the active anodic points appeared on the as-received surface were not presented on the laser-cleaned surfaces. Such corrosion behaviours were correlated to the change of surface oxide status measured by glow discharge optical emission spectrometry (GDOES) and X-ray photoelectron spectroscopy (XPS). It was suggested that the removal of the original less protective oxide layer consisting of MgO and MgAl2O4 on the as-received surfaces and the newly formed more protective oxide layer containing mainly Al2O3 and MgO by laser cleaning were responsible for the improvement of the corrosion performance.

  16. Aluminium base amorphous and crystalline alloys with Fe impurity

    International Nuclear Information System (INIS)

    Sitek, J.; Degmova, J.

    2006-01-01

    Aluminium base alloys show remarkable mechanical properties, however their low thermal stability still limits the technological applications. Further improvement of mechanical properties can be reached by partial crystallization of amorphous alloys, which gives rise to nanostructured composites. Our work was focused on aluminium based alloys with Fe, Nb and V additions. Samples of nominal composition Al 90 Fe 7 Nb 3 and Al 94 Fe 2 V 4 were studied in amorphous state and after annealing up to 873 K. From Moessbauer spectra taken on the samples in amorphous state the value of f-factor was determined as well as corresponding Debye temperatures were calculated. Annealing at higher temperatures induced nano and microcrystalline crystallization. Moessbauer spectra of samples annealed up to 573 K are fitted only by distribution of quadrupole doublets corresponding to the amorphous state. An increase of annealing temperature leads to the structural transformation, which consists in growth of nanometer sized aluminium nuclei. This is partly reflected in Moessbauer parameters. After annealing at 673 K intermetallic phase Al 3 Fe and other Al-Fe phases are created. In this case Moessbauer spectra are fitted by quadrupole doublets. During annealing up to 873 K large grains of Fe-Al phases are created. (authors)

  17. Fatigue crack paths and properties in A356-T6 aluminum alloy microstructurally modified by friction stir processing under different conditions

    Directory of Open Access Journals (Sweden)

    A. Tajiri

    2015-10-01

    Full Text Available A356-T6 cast aluminum alloy is a light weight structural material, but fatigue crack initiates and propagates from a casting defect leading to final fracture. Thus it is important to eliminate casting defects. In this study, friction stir processing (FSP was applied to A356-T6, in which rotating tool with probe and shoulder was plunged into the material and travels along the longitudinal direction to induce severe plastic deformation, resulting in the modification of microstructure. Two different processing conditions with low and high tool rotational speeds were tried and subsequently fully reversed fatigue tests were performed to investigate the effect of processing conditions on the crack initiation and propagation behavior. The fatigue strengths were successfully improved by both conditions due to the elimination of casting defects. But the lower tool rotational speed could further improve fatigue strength than the higher speed. EBSD analyses revealed that the higher tool rotational speed resulted in the severer texture having detrimental effects on fatigue crack initiation and propagation resistances.

  18. Mechanical behaviour of aluminium-lithium alloys

    Indian Academy of Sciences (India)

    Considerable worldwide research has gone into developing a range of these alloys over the last three decades. ... Defence Metallurgical Research Laboratory, P.O. Kanchanbagh, Hyderabad 500 058, India; Jawaharlal Nehru Centre for Advanced Scientific Research, Jakkur, Bangalore 560 064, India; International ...

  19. Evolution of morphology in solidifying aluminium alloys

    NARCIS (Netherlands)

    Dijkstra, W.O.

    2007-01-01

    In the thesis two different models of solidification of aluminum alloys are presented and analyzed. The first 1--D solidification model is derived from the conservation of solute, heat and mass. With numerical experiments it is shown that simulations with the Finite Difference discretization must

  20. Friction stir spot welding of dissimilar aluminium alloys

    International Nuclear Information System (INIS)

    Bozkurt, Yahya

    2016-01-01

    Friction stir spot welding (FSSW) has been proposed as an effective technology to spot weld the so-called “difficult to be welded” metal alloys such as thin sheets aluminum alloys and dissimilar materials. FSSW is derived from friction stir welding technology, its principle benefit being low cost joining, lower welding temperature and shorter welding time than conventional welding methods. In this study, dissimilar AlMg 3 and AlCu 4 Mg 1 aluminium alloy plates were FSSWed by offsetting the low strength sheet on upper side of the weld. The effects of tool rotation speed on the microstructure, lap shear fracture load (LSFL), microhardness and fracture features of the weld are investigated by constant welding parameters. The maximum LSFL was obtained by increasing the tool rotational speed. However, the joints exhibited pull-out nugget fracture mode under lap shear tensile testing conditions. The largest completely bonded zone was observed as 5.86 mm which was narrower at the opposite position of the joint. Key words: friction stir spot welding, aluminium alloys, mechanical properties, dissimilar joint, welding parameters

  1. Design of Grain Refiners for Aluminium Alloys

    Science.gov (United States)

    Tronche, A.; Greer, A. L.

    The efficiency of a grain refiner can be quantified as the number of grains per nucleant particle in the solidified product. Even for effective refiners in aluminium, such as Al-5Ti-1B, it is known from experiments that efficiencies are very low, at best 10-3 to 102. It is of interest to explore the reasons for such low values, and to assess the prospects for increased efficiency though design of refiners. Recently it has been shown [1] that a simple recalescence-based model can make quantitative predictions of grain size as a function of refiner addition level, cooling rate and solute content. In the model, the initiation of grains is limited by the free growth from nucleant particles, the size distribution of which is very important. The present work uses this model as the basis for discussing the effect of particle size distribution on grain refiner performance. Larger particles (of TiB2 in the case of present interest) promote greater efficiency, as do narrower size distributions. It is shown that even if the size distribution could be exactly specified, compromises would have to be made to balance efficiency (defined as above) with other desirable characteristics of a refiner.

  2. 3D printing of high-strength aluminium alloys

    Science.gov (United States)

    Martin, John H.; Yahata, Brennan D.; Hundley, Jacob M.; Mayer, Justin A.; Schaedler, Tobias A.; Pollock, Tresa M.

    2017-09-01

    Metal-based additive manufacturing, or three-dimensional (3D) printing, is a potentially disruptive technology across multiple industries, including the aerospace, biomedical and automotive industries. Building up metal components layer by layer increases design freedom and manufacturing flexibility, thereby enabling complex geometries, increased product customization and shorter time to market, while eliminating traditional economy-of-scale constraints. However, currently only a few alloys, the most relevant being AlSi10Mg, TiAl6V4, CoCr and Inconel 718, can be reliably printed; the vast majority of the more than 5,500 alloys in use today cannot be additively manufactured because the melting and solidification dynamics during the printing process lead to intolerable microstructures with large columnar grains and periodic cracks. Here we demonstrate that these issues can be resolved by introducing nanoparticles of nucleants that control solidification during additive manufacturing. We selected the nucleants on the basis of crystallographic information and assembled them onto 7075 and 6061 series aluminium alloy powders. After functionalization with the nucleants, we found that these high-strength aluminium alloys, which were previously incompatible with additive manufacturing, could be processed successfully using selective laser melting. Crack-free, equiaxed (that is, with grains roughly equal in length, width and height), fine-grained microstructures were achieved, resulting in material strengths comparable to that of wrought material. Our approach to metal-based additive manufacturing is applicable to a wide range of alloys and can be implemented using a range of additive machines. It thus provides a foundation for broad industrial applicability, including where electron-beam melting or directed-energy-deposition techniques are used instead of selective laser melting, and will enable additive manufacturing of other alloy systems, such as non-weldable nickel

  3. Improving the wettability of 2024 aluminium alloy by means of cold plasma treatment

    Science.gov (United States)

    Polini, W.; Sorrentino, L.

    2003-05-01

    Aluminium alloys are heavily used to manufacture structural parts in the aeronautic industry because of its lightness and its corrosion resistance. These alloys are successfully used in other industrial fields too, such as railway, automotive and naval industries. The need to contrast the severe use conditions and the heavy stresses developing in aeronautic field implies to protect the surfaces of the structures in aluminium alloy by any deterioration. To preserve by deterioration, it is necessary to make aluminium more suitable to be coated by protective paint. In the aeronautic industry, a complex and critical process is used in order to enhance both wettability and adhesive properties of aluminium alloy surfaces. Cold plasma treatment represents an efficient, clean and economic alternative to activate aluminium surfaces. The present work deals with air cold plasma treatment of 2024 aluminium alloy surfaces. The influence of dc electrical discharge cold plasma parameters on wettability of 2024 aluminium alloy surfaces has been studied. A set of process variables (voltage, time and air flow rate) has been identified and used to conduct some experimental tests on the basis of design of experiment (DOE) techniques. The experimental results show that the proposed plasma process may considerably increase aluminium alloy wettability. These results represent the first step in trying to optimise the aluminium adhesion by means of this non-conventional manufacturing process.

  4. Numerical Modelling of Drawbeads for Forming of Aluminium Alloys

    Science.gov (United States)

    Joshi, Y.; Christiansen, P.; Masters, I.; Bay, N.; Dashwood, R.

    2016-08-01

    The drawbeads in stamping tools are usually designed based on experience from the forming of steel. However, aluminium alloys display different forming behaviour to steels, which is not reflected in the drawbead design for tools used for stamping aluminium. This paper presents experimental results from different semi-circular drawbead geometries commonly encountered in automotive dies and compares them to those obtained from Stoughton's analytical drawbead model and the 2D plane strain drawbead model set up using LS-DYNA. The study was conducted on lubricated NG5754 strips. The results presented are in terms of drawbead restraining force versus strip displacement, as a function of drawbead depth. The FE drawbead model agrees well with the experiments whereas the analytical model overpredicted the drawbead forces.

  5. Neutron small angle scattering of irradiated aluminium-silicon alloys

    International Nuclear Information System (INIS)

    Kostorz, G.

    1976-01-01

    Technically pure aluminium and aluminium-silicon alloys (0.43, 0.83 and 1.2% Si, also containing 0.11 to 0.14 at. % Fe) were investigated by slow neutron small angle scattering after irradiation with fast neutrons at low temperatures. Different irradiation levels, ageing at room temperature and at 60/70 0 C had no measurable effect upon small angle scattering cross-sections. From the experimental precision upper limit for the amount of Si involved in clustering after irradiation can be given. The observed small angle scattering shows a strong dependence on scattering angles and is attributed to large precipitates of Al 12 Fe 3 Si. A surface layer on the as-received samples is identified as another source of low-intensity small angle scattering. (orig.) [de

  6. Mechanical Behaviour and Morphology of A356/SiC Nanocomposites Using Stir Casting

    Science.gov (United States)

    Tanwir Alam, Md.; Arif, Sajjad; Husain Ansari, Akhter

    2017-08-01

    In this research an attempt has been made to explore the experimental investigation of A356/SiC nanocomposites using two step stir casting process. A356 alloy ingot was selected for the matrix and the reinforcement (aluminium fine powder (99.9%) plus nano size SiC mechanically forged by using ball mill at 100 rpm for duration of 10 hours). Ball milling process enhances the wettability of the particles. Reinforcement was varied from 1% to 5% with a step of 1% by weight. The stirring process was carried out at 500±50 rpm with stirring duration 10 minutes in two steps. The melt composites were poured at 680±20° C into the die to fabricate the composites. In this process of fabrication, less oxides/segregations were depicted. Tensile strengths of fabricated composites were evaluated by using UTM and toughness was calculated from area under stress-strain curve. To identify the involvement and presence of the nanoreinforcement into the matrix alloy (A356), fractured surfaces of the fabricated nanocomposites were examined using SEM and EDX. Tensile test results have shown the fracture mechanism and enhanced mechanical properties with the addition of forged nanoreinforcements. Yield tensile strength (YTS) and ultimate tensile strength (UTS) of A356 parent alloy found as 212.76 MPa and 219.90 MPa respectively. The improvement of 41% in YTS and 45% in UTS in case of A356/SiC nanocomposites were investigated. Decrease in % elongation and toughness with increase in forged nanoreinforcement were predicted. Proper distribution of reinforcement was attributed by SEM micrographs. EDX spectrum disclosed the presence of the constituents in the parent alloy (A356) and stir cast nanocomposites.

  7. Microstructures of alloyed and dispersed hard particles in the aluminium surface

    CSIR Research Space (South Africa)

    Pityana, S

    2010-03-01

    Full Text Available Laser surface alloying of A1200 aluminium alloy was carried out using a 4.4 kW Nd:YAG laser. Powder mixtures of SiC and TiC hard particles were injected into the laser generated melt pool on the aluminium substrate using a commercial powder feeder...

  8. Grain Refinement of Commercial EC Grade 1070 Aluminium Alloy for Electrical Application

    OpenAIRE

    Hassanabadi, Massoud

    2015-01-01

    The aluminium alloys for electrical conductivity applications are generally not grain refinedsince the addition of grain refiners drops the electrical conductivity by introducing impuritiesinto the melt. Non-grain refined aluminium may lead to bar fracture and cracks during themetalworking process. The present study focuses to find an optimum balance between the grain refiner addition andthe electrical conductivity of commercial EC grade 1070 aluminium alloy for electricalapplication. In orde...

  9. Aluminium. II - A review of deformation properties of high purity aluminium and dilute aluminium alloys.

    Science.gov (United States)

    Reed, R. P.

    1972-01-01

    The elastic and plastic deformation behavior of high-purity aluminum and of dilute aluminum alloys is reviewed. Reliable property data, including elastic moduli, elastic coefficients, tensile, creep, fatigue, hardness, and impact are presented. Single crystal tensile results are discussed. Rather comprehensive reference lists, containing publications of the past 20 years, are included for each of the above categories. Defect structures and mechanisms responsible for mechanical behavior are presented. Strengthening techniques (alloys, cold work, irradiation, quenching, composites) and recovery are briefly reviewed.

  10. Role of acidic chemistries in steam treatment of aluminium alloys

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Jellesen, Morten Stendahl; Ambat, Rajan

    2015-01-01

    The effect of acidic chemistry on the accelerated growth of oxide on aluminium alloys Peraluman 706TM and AA6060 under exposure to high temperature steam was investigated. Studied chemistries were based on citrates and phosphates. Results showed that the presence of citrate and phosphate anions...... initiate doxide growth at the intermetallic particles while growth and corrosion performance of oxide was found tobe a function of anions type and their concentration. Further, steam treatment with phosphates exhibited better performance under acetic acid salt spray and filiform corrosion test whereas...

  11. Deviatoric Response of AN Armour-Grade Aluminium Alloy

    Science.gov (United States)

    Appleby-Thomas, G. J.; Hazell, P. J.; Millett, J.; Bourne, N. K.

    2009-12-01

    Aluminium alloys such as 5083 H32 are established light-weight armour materials. As such, the shock response of these materials is of great importance. The shear strength of a material under shock loading provides an insight into its ballistic performance. In this investigation embedded manganin stress gauges have been employed to measure both the longitudinal and lateral components of stress during plate-impact experiments over a range of impact stresses. In turn, these results were used to determine the shear strength and to investigate the time dependence of lateral stress behind the shock front to give an indication of material response.

  12. The fracture of boron fibre-reinforced 6061 aluminium alloy

    Science.gov (United States)

    Wright, M. A.; Welch, D.; Jollay, J.

    1979-01-01

    The fracture of 6061 aluminium alloy reinforced with unidirectional and cross-plied 0/90 deg, 0/90/+ or - 45 deg boron fibres has been investigated. The results have been described in terms of a critical stress intensity, K(Q). Critical stress intensity factors were obtained by substituting the failure stress and the initial crack length into the appropriate expression for K(Q). Values were obtained that depended on the dimensions of the specimens. It was therefore concluded that, for the size of specimen tested, the values of K(Q) did not reflect any basic materials property.

  13. Friction stir welding of 6061 aluminium alloy

    International Nuclear Information System (INIS)

    Abdel Rahman, M.A.M.S.

    2009-01-01

    6061 AA (Al-Mg-Si alloy) has gathered wide acceptance in the fabrication of light weight structures requiring a high strength-to-weight ratio and good corrosion resistance such as marine frames, pipelines, storage tanks, and aircraft components [1]. It is also used for the manufacturing of fuel elements in the nuclear research reactors. Compared to many of the fusion welding processes that are routinely used for joining structural alloys, friction stir welding (FSW) is a solid state joining process in which the material that is being welded is not melted and recast [2]. The welding parameters such as tool rotational speed, welding traverse speed, and tool profile play a major role in deciding the weld quality. Several FSW tools (differ from each other in pin angle, shoulder diameter, and shoulder concavity) have been used to fabricate a number of joints in order to obtain a tool with which a sound weld can be produced. It was found that the FSW tool with tapered cone pin, concave shoulder, and shoulder diameter equal to four times the welded plate thickness is suitable to produce a sound weld. The effect of the traverse speed on the global and local tensile properties of friction stir welded joints has been investigated in the 6061-T6 AA. The global tensile properties of the FSW joints were improved with increasing the traverse speed at constant rotation rate. It is found that the global tensile strength of the FSW joint is limited by the local tensile strength of the nearest region to the weld center at which the cross section is composed mainly of the HAZ. The effect of the initial butt surface on the formation of the zigzag line on the tensile properties of the welds was examined by using three types of welding samples differ in the preparation of the initial butt surface. The first type of samples welded without removing the oxide layer from the initial butt surface (uncleaned butt surfaces joint). In the second type of samples the oxide layer was removed from

  14. Fractographic analysis of fatigue damage in 7000 aluminium alloys.

    Science.gov (United States)

    Cvijović, Z; Vratnica, M; Gerić, K

    2008-12-01

    In this paper, an attempt is made to correlate the fatigue damage in 7000 aluminium alloys with different impurity contents to the microstructural features and to explain their interdependence through fractographic observations. The Paris constants of these alloys in the form of hot-forged plates subjected to the overaged T73 temper are evaluated and differences in the fatigue crack growth rate described by striation spacing measurements. Scanning electron microscopy analysis of fatigue fracture surfaces revealed that the type and morphological parameters of coarse intermetallic particles play a critical role in fatigue crack growth behaviour. The elemental distribution determined by means of energy-dispersive spectroscopy analysis showed that the fractured particles accelerating the crack advances are larger particles of Fe-rich phases. The fatigue crack growth rate increases considerably with increasing amounts of these particles. The smaller eta, S and Mg(2)Si particles contribute beneficially to fatigue life.

  15. Contradictory effect of chromate inhibitor on corrosive wear of aluminium alloy

    International Nuclear Information System (INIS)

    Pokhmurskii, V.I.; Zin, I.M.; Vynar, V.A.; Bily, L.M.

    2011-01-01

    Research highlights: → Corrosive wear of aluminium alloy in inhibited artificial acid rain was studied. → Tribometer with linear reciprocating ball-on-flat geometry was used.→ Corrosion potential, polarization current and friction coefficient were measured. → Chromate decreases corrosion of aluminium alloy under wear conditions. → Chromate in general accelerates corrosive wear of the alloy in acid rain. - Abstract: The corrosive wear of D16T aluminium alloy in artificial acid rain was studied. A special tribometer with the linear reciprocating ball-on-flat geometry was used. The setup allows to measure simultaneously an open circuit potential, to carry out potentiostatic and potentiodynamic polarization studies of the alloy corrosion and to record the friction coefficient. It was established that the addition of strontium chromate inhibitor to the working environment decreases an electrochemical corrosion of the aluminium alloy under wear conditions, but in general accelerates its destruction due to insufficient wear resistance of a formed surface film.

  16. Overheating influence on solidification - thermal variables and microstructure formation of aluminium alloy

    OpenAIRE

    Rodrigues, JRP; Sousa, TXD; de Andrade, RB; dos Santos, RG; Mello, MDNM

    2009-01-01

    A comparative analysis of the 5052 aluminum alloy solidification process involving different overheating ranges is presented herein. Experimentally determined, the main parameters of the solidification process were affected in the overheating range and influenced the microstructure arrangement. The 5052 aluminium alloy was selected. It contains about. 3% magnesium and is used for commercial purposes. The aluminium alloy was poured into a device that allows unidirectional solidification and wa...

  17. Comparative study on laser welding and TIG welding of semi-solid high pressure die cast A356 aluminium alloy

    CSIR Research Space (South Africa)

    Govender, G

    2007-07-01

    Full Text Available . The microstructures were observed using optical microscopy. The hardness profiles were measured using a Future-Tech FM-700 hardness tester. A 300g load was selected for the microhardness testing. This was selected in order to reduce the noise in the hardness...) was composed of globular primary  & a fine eutectic structure composed primarily of Al and Si. The base metal microstructures of the T4 HT, and T6 HT samples were found to be very similar (figure 5), consisting of primary globular α and fine spheroidal Si...

  18. Investigation of the T4 and T6 heat treatment cycles of semi-solid processed aluminium alloy A356

    CSIR Research Space (South Africa)

    Moller, H

    2008-01-01

    Full Text Available savings. Natural aging prior to artificial aging causes the time-to-peak-hardness to be longer compared to the time when only artificial aging is used. Quenching after solution treatment in water at 70 C results in slightly lower tensile properties than...

  19. Multiphase Model of Semisolid Slurry Generation and Isothermal Holding During Cooling Slope Rheoprocessing of A356 Al Alloy

    Science.gov (United States)

    Das, Prosenjit; Samanta, Sudip K.; Mondal, Biswanath; Dutta, Pradip

    2018-04-01

    In the present paper, we present an experimentally validated 3D multiphase and multiscale solidification model to understand the transport processes involved during slurry generation with a cooling slope. In this process, superheated liquid alloy is poured at the top of the cooling slope and allowed to flow along the slope under the influence of gravity. As the melt flows down the slope, it progressively loses its superheat, starts solidifying at the melt/slope interface with formation of solid crystals, and eventually exits the slope as semisolid slurry. In the present simulation, the three phases considered are the parent melt as the primary phase, and the solid grains and air as secondary phases. The air phase forms a definable air/liquid melt interface as the free surface. After exiting the slope, the slurry fills an isothermal holding bath maintained at the slope exit temperature, which promotes further globularization of microstructure. The outcomes of the present model include prediction of volume fractions of the three different phases considered, grain evolution, grain growth, size, sphericity and distribution of solid grains, temperature field, velocity field, macrosegregation and microsegregation. In addition, the model is found to be capable of making predictions of morphological evolution of primary grains at the onset of isothermal coarsening. The results obtained from the present simulations are validated by performing quantitative image analysis of micrographs of the rapidly oil-quenched semisolid slurry samples, collected from strategic locations along the slope and from the isothermal slurry holding bath.

  20. Microstructure and mechanical properties of thixoformed A319 aluminium alloy

    International Nuclear Information System (INIS)

    Salleh, M.S.; Omar, M.Z.; Syarif, J.; Alhawari, K.S.; Mohammed, M.N.

    2014-01-01

    Highlights: • A319 was successfully thixoformed at 50% liquid, i.e. at 571 °C. • T6 heat treatment has increased the strength and hardness of the thixoformed alloy. • The elongation after T6 heat treatment is even significantly improved. • The iron-rich intermetallic phase reduces the strength of the thixoformed alloy. - Abstract: Thixoforming is a viable technology for forming alloys in a semisolid state into near net-shaped products. In the present study, the effect of a thixoforming process on the microstructure and mechanical properties of A319 aluminium alloy was investigated. The ingots obtained from the cooling slope were thixoformed in a press after they remained at 571 °C for 5 min, yielding a microstructure predominantly composed of α-Al globules and inter-globular Si particles. Some of the thixoformed samples were treated with an ageing process (T6) and then, hardness and tensile samples were prepared from the as-cast, as-thixoformed and thixoformed T6. All the thixoformed samples were characterised using optical microscopy, scanning electron microscopy (SEM), energy dispersive X-ray (EDX) and X-ray diffraction (XRD) as well as hardness measurements and tensile tests. The results indicate that the mechanical properties of the thixoformed A319 alloy increased after the T6 heat treatment (hardness of 124.2 ± 3.2 HV, tensile strength of 298 ± 3.0 MPa, yield strength of 201 ± 2.6 MPa and elongation to fracture of 4.5 ± 0.3%). The fracture samples from the tensile test were analysed, revealing that the iron-rich intermetallic observed in the samples reduced the tensile strength and ductility of the thixoformed A319 alloys

  1. The influence of alloy composition on residual stresses in heat treated aluminium alloys

    Energy Technology Data Exchange (ETDEWEB)

    Robinson, J.S., E-mail: jeremy.robinson@ul.ie [Department of Mechanical, Aeronautical and Biomedical Engineering, University of Limerick (Ireland); Redington, W. [Materials and Surface Science Institute, University of Limerick (Ireland)

    2015-07-15

    The as quenched properties of eight different heat treatable aluminium alloys are related to residual stress magnitudes with the objective being to establish if there is a relationship between the residual stress and the as quenched alloy hardness and strength. Near surface residual stresses were assessed with X-ray diffraction using both the established sin{sup 2}ψ method and the more recent cos α technique. Through thickness residual stresses were also characterised using neutron diffraction. The alloys were chosen to encompass a wide range of strengths. The low to medium strength alloys were 6060 and 6082, medium to high strength 2618A, 2014A, 7075, 7010 and two variants of 7449, while the very high strength alloy was the powder metallurgy alloy N707. To assess the as quenched strength, dynamic hardness and tensile properties were determined from samples tested immediately after quenching to minimise the influence of precipitation hardening by natural aging. In addition, hot hardness measurements were made in situ on samples cooled to simulate quench paths. Within the experimental constraints of the investigation, the distribution of residual stress through the thickness was found to follow the same pattern for all the alloys investigated, varying from tensile in the interior to surface compression. The influence of alloy strength was manifested as a change in the observed residual stress magnitudes, and surface residual stresses were found to vary linearly with as quenched hardness and strength. - Highlights: • As quenched aluminium alloys contain high magnitude residual stresses. • Surface is compressive balance by a tensile core. • As quenched surface residual stress is linear function of alloy strength. • In situ hot hardness demonstrates rapid change in intrinsic hardness during rapid cooling.

  2. Comparison of microstructure and mechanical properties of A356 aluminum alloy/Al2O3 composites fabricated by stir and compo-casting processes

    International Nuclear Information System (INIS)

    Sajjadi, S.A.; Ezatpour, H.R.; Torabi Parizi, M.

    2012-01-01

    Highlights: → Nano and micro-composites (A356/Al 2 O 3 ) were fabricated by stir-casting and compo-casting. → Uniform distribution, grain refinement and low porosity in the composites were attained. → Addition of alumina led to the improvement in yield, ultimate tensile and compression strength. → Nano-alumina particles and compo-casting process obtained the best mechanical properties. -- Abstract: Metal-matrix composites (MMCs), as light and strong materials, are very attractive for application in different industries. In the present work, nano and micro-composites (A356/Al 2 O 3 ) with different weight percent of particles were fabricated by two melt techniques such as stir-casting and compo-casting. Microstructural characterization was investigated by optical (OP) and scanning electron microscopy (SEM). Tensile, hardness and compression tests were carried out in order to identify mechanical properties of the composites. The results of microstructural study revealed uniform distribution, grain refinement and low porosity in micro and nano-composite specimens. The mechanical results showed that the addition of alumina (micro and nano) led to the improvement in yield strength, ultimate tensile strength, compression strength and hardness. It was indicated that type of fabrication process and particle size were the effective factors influencing on the mechanical properties. Decreasing alumina particle size and using compo-casting process obtained the best mechanical properties.

  3. The role of magnesium in the electrochemical behaviour of 5XXX aluminium-magnesium alloys

    NARCIS (Netherlands)

    Flores Ramirez, J.R.

    2006-01-01

    An investigation concerning the effects of magnesium on the intergranular corrosion susceptibility of AA5XXX aluminium alloys was carried out. In the present work, magnesium is found to be highly mobile in the bulk metal as well as in the aluminium oxide. This mobility is also found to be dependent

  4. GAS-CREATION OF SEPARATING COVERINGS FOR MOULDS FOR DIE CASTING OF ALUMINIUM ALLOYS

    Directory of Open Access Journals (Sweden)

    A. M. Mihaltsov

    2010-01-01

    Full Text Available The methods of experiments on determination of gascreating ability of different separating coverings for the moulds of aluminium alloys die casting are given and described in the article, and the results of investigation are given as well.

  5. In-situ electron microscopy studies on the tensile deformation mechanisms in aluminium 5083 alloy

    CSIR Research Space (South Africa)

    Motsi, G

    2014-10-01

    Full Text Available In this study tensile deformation mechanisms of aluminium alloy 5083 were investigated under observations made from SEM equipped with a tensile stage. Observations during tensile testing revealed a sequence of surface deformation events...

  6. Mackay icosahedron explaining orientation relationship of dispersoids in aluminium alloys.

    Science.gov (United States)

    Muggerud, Astrid Marie F; Li, Yanjun; Holmestad, Randi; Andersen, Sigmund J

    2014-10-01

    The orientation relations (ORs) of the cubic icosahedral quasicrystal approximant phase α-Al(Fe,Mn)Si have been studied after low temperature annealing of a 3xxx wrought aluminium alloy by transmission electron microscopy. From diffraction studies it was verified that the most commonly observed OR for the α-Al(Fe,Mn)Si dispersoids is [1\\bar 11]α // [1\\bar 11]Al, (5\\bar 2\\bar 7)α // (011)Al. This orientation could be explained by assuming that the internal Mackay icosahedron (MI) in the α-phase has a fixed orientation in relation to Al, similar to that of the icosahedral quasi-crystals existing in this alloy system. It is shown that mirroring of the normal-to-high-symmetry icosahedral directions of the MI explains the alternative orientations, which are therefore likely to be caused by twinning of the fixed MI. Only one exception was found, which was related to the Bergman icosahedron internal to the T-phase of the Al-Mg-Zn system.

  7. Mechanical and Fatigue Properties of Functionally Graded Aluminium Silicon Alloys =

    Science.gov (United States)

    Maricel, Chirita Georgel

    by both centrifugal casting technique and gravity casting technique were tested. To isolate the vibration effect, experimental equipment was designed and constructed in order to be able to cast within a certain level of vibration equivalent with the vibration level of the centrifugal casting equipment. The results are confirming that there is a correlation of improving mechanical properties with the vibration of the melt during solidification. The difference of the mechanical properties of castings obtained by gravity casting technique and by centrifugal casting technique could be explained by the fact that, the vibration due to the inherently vibration of the equipment, the fluid dynamics and the centrifugal pressure make the melt, during solidification, to initiate more nuclei of solidification. Then, the centrifugal pressure moves the nuclei of solidification to the furthest point of the mould (where the pressure is higher) fact that explains the obtained results which are higher on one side of the ingots which corresponds with the side of the mould where the pressure is higher and smaller on the other side where the pressure is smaller. This causes several differences in microstructures in both sides of the ingot. The mechanical and fatigue properties are largely influenced by microstructure and the presence of material inhomogeneities. Pores, inclusions or secondary phase particles are common sites for fatigue crack nucleation in aluminium alloys. The constituent particle’s size and shape are also important characteristics that influence crack nucleation. This study intends to assess also the problem of fatigue life prediction by establishing a relation within some of the characteristics of the micro structural features of studied aluminium silicon alloys such as: micropores, secondary dendrites arm spacing (SDAS), volume fractions of phases (α-Al phase, eutectic and intermetallic phases), the size of silicon lamellas in interdendritic eutectic regions and

  8. Microscopic observation of pattern attack by aggressive ions on finished surface of aluminium alloy sacrificial anode

    International Nuclear Information System (INIS)

    Zaifol Samsu; Muhammad Daud; Siti Radiah Mohd Kamarudin; Nur Ubaidah Saidin; Azali Muhammad; Mohd Shaari Ripin; Rusni Rejab; Mohd Shariff Sattar

    2010-01-01

    This paper presents the results of a microscopic observation on submerged finished surface of aluminium alloy sacrificial anode. Experimental tests were carried out on polished surface aluminium anode exposed to seawater containing aggressive ions in order to observe of pattern corrosion attack on corroding surface of anode. Results have shown, at least under the present testing condition, that surface of sacrificial anode were attack by an aggressive ion such as chloride along grain boundaries. In addition, results of microanalysis showed that the corrosion products on surface of aluminium alloy have Al, Zn and O element for all sample and within the pit was consists of Al, Zn, O and Cl element. (author)

  9. A Fundamental Approach to Developing Aluminium based Bulk Amorphous Alloys based on Stable Liquid Metal Structures and Electronic Equilibrium - 154041

    Science.gov (United States)

    2017-03-28

    AFRL-AFOSR-JP-TR-2017-0027 A Fundamental Approach to Developing Aluminium -based Bulk Amorphous Alloys based on Stable Liquid-Metal Structures and...to 16 Dec 2016 4.  TITLE AND SUBTITLE A Fundamental Approach to Developing Aluminium -based Bulk Amorphous Alloys based on Stable Liquid-Metal...Air Force Research Laboratory for accurately predicting compositions of new amorphous alloys specifically based on aluminium with properties superior

  10. Physicochemical properties of aluminium alloys with elements of II and III groups of periodic table

    International Nuclear Information System (INIS)

    Eshov, B.B.

    2016-01-01

    The purpose of the present work is to establish the mechanism and regularities of changes of physicochemical properties of binary and multicomponent aluminium alloys with elements of II and III groups of periodic table as well as optimization and elaboration of new alloys.

  11. An efficient method of spot welding Aluminium alloys with induction preheating

    Directory of Open Access Journals (Sweden)

    Jawad Saleem

    2016-12-01

    Full Text Available Steel has been the material of choice for automobile manufacturers. In the recent years material such as aluminium and its alloys are taking over the market because of their light weight. The use of aluminium, in automobile manufacturing can result in overall fuel efficiency. Spot welding aluminium alloys require higher electric power and less welding time as compared to steel. Welding guns that can produce an electric current which is approximately 2 to 3 times higher, as compared to steel are required for spot welding aluminium. An efficient method of spot welding Aluminium alloys with the preheating process has been proposed in this paper. Preheating Aluminium sheet before spot welding reduces the thermal and electrical resistance which brings down the electric current requirement to spot weld Aluminium structures. Both spot welding and induction preheating process have been modelled in this paper. The test results of the preheating process have also been verified with practical heating trials. The preheating is performed on-the-fly in advance to spot welding process. The results show that spot welding Al 6082 after preheating up to 200 oC, the output current requirements to make the spot weld are reduced by 22%.

  12. Nanostructure of aluminium alloy 2024: Segregation, clustering and precipitation processes

    International Nuclear Information System (INIS)

    Sha, G.; Marceau, R.K.W.; Gao, X.; Muddle, B.C.; Ringer, S.P.

    2011-01-01

    Variations in solute element distribution occurring in a commercial 2024 aluminium alloy during isothermal ageing treatments at 170 deg. C for up to 120 h have been characterized using atom probe tomography. An early (0.5 h at 170 deg. C) rapid increase in hardness was correlated with the formation of fine scale (average 24 atom) solute clusters, comprising principally Mg and Cu, but with minor concentrations of Si and Zn. There was, in addition, evidence of significant segregation of Mg, Cu and Si to at least some fraction of grain boundaries and existing matrix dislocations. At peak hardness (80 h at 170 deg. C) the microstructure comprised coarse precipitates of S phase, with a composition approaching stoichiometric Al 2 CuMg, a dense distribution of Guinier-Preston-Bagaryatsky zones elongated parallel to in a matrix of α-Al and a residual distribution of smaller equiaxed solute clusters. Both the clusters and zones contained predominantly Mg and Cu, with minor concentrations of Si and Zn. The S phase contained small but significant (0.5-1.8 at.%) concentrations of Si, which was non-uniformly distributed in elongated domains within the laths of the S phase. In overaged samples (114 h at 170 deg. C) the microstructure comprised almost exclusively coarse S phase, Al 2 Mg(Cu,Si), in assemblies suggestive of a combination of precipitate coarsening and coalescence.

  13. Ductility of aluminium alloy AA7075 at high strain rates

    Energy Technology Data Exchange (ETDEWEB)

    El-Magd, E.; Brodmann, M. [Technische Hochschule Aachen (Germany). Dept. of Mater. Sci.

    2000-09-01

    Under dynamic loading the stabilising effect of increased strain rate sensitivity of the material restrains neck formation in tension tests and leads to an increase in ductility. On the other hand the adiabatic character of the deformation process reduces the flow stress and promotes instability, localisation and adiabatic shear band initiation. Furthermore, the notch sensitivity of the material increases with increasing strain rate. Dynamic and quasi-static tension and compression tests were carried out on the age hardenable aluminium wrought alloy AA7075. There, dispers distributed precipitations are often the starting point for ductile fracture caused by impact due to the nucleation, growth and coalescence of voids and micro-cracks in case of tension. Neck formation under tensile loading and instabilities like shear bands in case of compression are discussed on the basis of the theory of imperfection under consideration of the increased strain rate sensitivity of the material and the adiabatic character of the deformation process at high strain rates. In case of tensile loading, tests with various notched geometries allowed the study of the influence of degree of multiaxiality. Through combination of experiment and simulation, the influence of strain rate on the local fracture strain could be determined for tensile and compression loading. (orig.)

  14. Researches focused on structure of aluminium alloys processed by rapid solidification, used in automotive industry

    International Nuclear Information System (INIS)

    Sfat, C.; Vasile, T.; Vasilescu, M.

    2001-01-01

    The paper present some new results focused on an aluminium high temperature alloy, obtained by 'melt spinning method'. alloy composition, processing conditions, resulted structures and the influence between them are presented. There are studied the two zone structures of the alloy and the relation between processing conditions and the characteristics of the zones, with implications on mechanical behavior in real conditions. The final conclusion show that is possible to control the structure in order to improve material behavior. (author)

  15. Characterization of steam generated anti-corrosive oxide films on Aluminium alloys

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Jellesen, Morten Stendahl; Ambat, Rajan

    2014-01-01

    Aluminium and its alloys are widely used in structural and transportation industry owing to their high strength to weight ratio. The surface of aluminium under normal conditions has a thin oxide film (2.5-10 nm) responsible for its inherent corrosion resistance. This oxide film can further...... be converted or transformed into functional conversion coatings in order to enhance corrosion resistance and adhesion to paint systems. Chromium based conversion coatings have been extensively used on aluminium alloys to improve adhesion of subsequent paint layers and corrosion resistance. However, the use...... chemical additives on surface morphology and growth of oxide film on different intermetallic particles and corrosion behaviour of such alloys.Surface morphology was observed by using FEG-SEM, EDX and FIB-SEM. Metal oxide surface characterization and compositional depth profiling were investigated by using...

  16. Self-Pierce Riveting of Three Aluminium Alloy and Mild Steel Sheets

    Science.gov (United States)

    Mori, K.; Abe, Y.; Kato, T.; Sakai, S.

    2010-06-01

    Three aluminium alloy and steel sheets were joined with a self-piercing rivet. Self-pierce riveting has the function of joining steel and aluminium alloys having very different melting points due to plastic joining. The requisites for joining the three sheets are the driving of the rivet leg through the middle sheet, the flaring of the rivet leg in the lower sheet and the prevention of the fracture of the lower sheet. The joinability for various combinations of the three sheets was determined. When the rivet leg is small, no driving through the middle sheet occurs, the lower sheet ruptures for a large rivet leg. In addition, 980 MPa high strength steel, mild steel and aluminium alloy sheets were joined by the self-pierce riveting.

  17. Effect of aluminium on formation of metastable phases in titanium-niobium alloys

    International Nuclear Information System (INIS)

    Trenogina, T.L.; Derevyanko, V.N.; Vozilkin, V.A.

    2001-01-01

    Specific features of phase transformations in the alloy of Ti-20Nb-29Al (at.%) are investigated in comparison with those in the aluminium-free Ti-21Nb alloy. It is states that in the alloy Ti-20Nb-29Al on quenching the ordering of β-solid solution takes place with B2-structure formation. The B2-matrix experiences decomposition with the formation of ordered Ω 0 -phase which field ranges up to 700 deg C. The investigation results show that the sequence of phase formation in Ti-Nb-Al and aluminium-free alloys is much the same. The only difference between them is the formation of ordered phases in the alloy Ti-20Nb-29Al [ru

  18. Aluminium alloys welding with high-power Nd:YAG lasers

    International Nuclear Information System (INIS)

    Garcia Orza, J.A.

    1998-01-01

    Aluminium alloys have good mechanical properties (high strength-to-weight ratio, corrosion resistance) and good workability. their applications are growing up, specially in the transportation industry. Weldability is however poorer than in other materials; recent advances in high power YAG laser are the key to obtain good appearance welds and higher penetration, at industrial production rates. Results of the combination of high power YAG beams with small fiber diameters and specific filler wires are presented. It is also characterized the air bone particulate material, by-product of the laser process: emission rates, size distribution and chemical composition are given for several aluminium alloys. (Author) 6 refs

  19. An indirect method for determining phosphorus in aluminium alloys by atomic-absorption spectrometry.

    Science.gov (United States)

    Bernal, J L; Del Nozal, M A; Deban, L; Aller, A J

    1981-07-01

    An indirect method is described for the determination of phosphorus in aluminium alloys. Ammonium molybdate is added to a solution of the aluminium alloy and the molybdophosphoric acid formed is selectively extracted into n-butyl acetate. The twelve molybdenum atoms associated with each phosphate ion are determined by direct atomic-absorption spectrometry with the n-butyl acetate phase in a nitrous oxide-acetylene flame, with measurement at 313.2 nm. The most suitable conditions have been established and the effect of other ions has been studied.

  20. Predicting the thermal conductivity of aluminium alloys in the cryogenic to room temperature range

    Science.gov (United States)

    Woodcraft, Adam L.

    2005-06-01

    Aluminium alloys are being used increasingly in cryogenic systems. However, cryogenic thermal conductivity measurements have been made on only a few of the many types in general use. This paper describes a method of predicting the thermal conductivity of any aluminium alloy between the superconducting transition temperature (approximately 1 K) and room temperature, based on a measurement of the thermal conductivity or electrical resistivity at a single temperature. Where predictions are based on low temperature measurements (approximately 4 K and below), the accuracy is generally better than 10%. Useful predictions can also be made from room temperature measurements for most alloys, but with reduced accuracy. This method permits aluminium alloys to be used in situations where the thermal conductivity is important without having to make (or find) direct measurements over the entire temperature range of interest. There is therefore greater scope to choose alloys based on mechanical properties and availability, rather than on whether cryogenic thermal conductivity measurements have been made. Recommended thermal conductivity values are presented for aluminium 6082 (based on a new measurement), and for 1000 series, and types 2014, 2024, 2219, 3003, 5052, 5083, 5086, 5154, 6061, 6063, 6082, 7039 and 7075 (based on low temperature measurements in the literature).

  1. Study of fatigue behaviour of 7475 aluminium alloy

    Indian Academy of Sciences (India)

    Unknown

    controlled toughness alloy developed for applications that require a combination of high strength, superior fracture toughness and resistance to fatigue crack propagation both in air and aggressive environment. The 7475 alu- minium alloy is basically a modified version of 7075 alloy. Properties in 7075 alloy are improved by ...

  2. Evaluation of the mechanical properties of microarc oxidation coatings and 2024 aluminium alloy substrate

    CERN Document Server

    Xue Wen Bin; Deng Zhi Wei; Chen Ru Yi; Li Yong Liang; Zhang Ton Ghe

    2002-01-01

    A determination of the phase constituents of ceramic coatings produced on Al-Cu-Mg alloy by microarc discharge in alkaline solution was performed using x-ray diffraction. The profiles of the hardness, H, and elastic modulus, E, across the ceramic coating were determined by means of nanoindentation. In addition, a study of the influence of microarc oxidation coatings on the tensile properties of the aluminium alloy was also carried out. The results show that the H-and E-profiles are similar, and both of them exhibit a maximum value at the same depth of coating. The distribution of the alpha-Al sub 2 O sub 3 phase content determines the H- and E-profiles of the coatings. The tensile properties of 2024 aluminium alloy show less change after the alloy has undergone microarc discharge surface treatment.

  3. Recovery of actinides from actinide–aluminium alloys by chlorination: Part II

    Energy Technology Data Exchange (ETDEWEB)

    Souček, P., E-mail: pavel.soucek@ec.europa.eu [European Commission, JRC, Institute for Transuranium Elements, Postfach 2340, 76125 Karlsruhe (Germany); Cassayre, L. [Laboratoire de Génie Chimique (LGC), Département Procédés Electrochimiques, CNRS-UMR 5503, Université de Toulouse III – Paul Sabatier, 31062 Toulouse Cedex 9 (France); Eloirdi, R.; Malmbeck, R.; Meier, R.; Nourry, C.; Claux, B.; Glatz, J.-P. [European Commission, JRC, Institute for Transuranium Elements, Postfach 2340, 76125 Karlsruhe (Germany)

    2014-04-01

    A chlorination route is being investigated for recovery of actinides from actinide–aluminium alloys, which originate from pyrochemical recovery of actinides from spent metallic nuclear fuel by electrochemical methods in molten LiCl–KCl. In the present work, the most important steps of this route were experimentally tested using U–Pu–Al alloy prepared by electrodeposition of U and Pu on solid aluminium plate electrodes. The investigated processes were vacuum distillation for removal of the salt adhered on the electrode, chlorination of the alloy by chlorine gas and sublimation of the AlCl{sub 3} formed. The processes parameters were set on the base of a previous thermochemical study and an experimental work using pure UAl{sub 3} alloy. The present experimental results indicated high efficiency of salt distillation and chlorination steps, while the sublimation step should be further optimised.

  4. Study of localized corrosion in AA2024 aluminium alloy using electron tomography

    International Nuclear Information System (INIS)

    Zhou, X.; Luo, C.; Hashimoto, T.; Hughes, A.E.; Thompson, G.E.

    2012-01-01

    Highlights: ► SEM tomography of localized corrosion has been achieved. ► Nanotomography provides evidence that links microstructure and corrosion propagation path. ► IGC stemmed from localized corrosion associated with buried clusters of intermetallics. ► IGC started beneath the alloy surface and may emerge on the alloy surface. - Abstract: SEM based tomography of localized corrosion has been achieved using selective detection of backscattered electrons. The high resolution tomography provides direct evidence that links the surface appearance of corroded alloy, the alloy microstructure and the corrosion propagation path. Stable localized corrosion of AA2024-T351 aluminium alloy was initiated at locations where large clusters of S phase particles were buried beneath the surface. Propagating away from the initiation sites, corrosion developed preferentially along the grain boundary network. The grain boundary attack started beneath the alloy surface, proceeded along preferred grain boundaries and may emerge at the alloy surface.

  5. Anti-corrosive Conversion Coating on Aluminium Alloys Using High Temperature Steam

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Jellesen, Morten Stendahl; Ambat, Rajan

    Aluminium is extensively used as a structural material due to its excellent strength to weight ratio and corrosion resistance properties. The surface of aluminium under normal conditions has a thin oxide film (1-10nm) which provides corrosion resistance. However due to lower thickness, flaws...... and heterogeneity of native oxide layer does not provide long time corrosion resistance and adhesion of organic coating for a particular function in different environments. In order to enhance the corrosion resistance and adhesion of organic coating, the aluminium native oxide layer is treated to transform...... or convert to a functional conversion coating. In the last several decades chromate conversion coating (CrCCs) have been the most common conversion coatings used for aluminium alloys. Due to the toxicity of the hexavalent chrome, however, environmental friendly alternatives to CrCCs have been investigated...

  6. Experimental Analysis of the Behaviour of Aluminium Alloy EN 6082AW T6 at High Temperature

    Directory of Open Access Journals (Sweden)

    Neno Torić

    2017-04-01

    Full Text Available The paper presents test results for the mechanical and creep properties of European aluminium alloy EN 6082AW T6 at high temperatures. Mechanical properties of the aluminium alloy were determined by means of two types of test: constant stress-rate and stationary creep tests. Mechanical properties were determined up to a temperature of 350 °C, while the creep tests were conducted within the temperature interval 150–300 °C. The creep tests conducted identified the critical temperature interval for creep development, which represents an important factor when analysing creep behaviour of aluminium structures. This temperature interval was found to be within the range 200–300 °C. Test results for stress at 0.2% strain and modulus of elasticity at different temperatures showed good agreement with the codified values from Eurocode 9 and with other comparable studies.

  7. Emeraldine base as corrosion protective layer on aluminium alloy AA5182, effect of the surface microstructure

    DEFF Research Database (Denmark)

    Cecchetto, L; Ambat, Rajan; Davenport, A.J.

    2007-01-01

    AA5182 aluminium alloy cold rolled samples were coated by thin Wlms of emeraldine base (EB) obtained from a 5% solution in N-methylpyrrolidinone. Accelerated corrosion tests prove this coating very eVective for corrosion protection of aluminium alloys in neutral environment. This study underlines...... the prominent role of surface cathodic intermetallic particles in pit initiation and coating break down in enhanced corrosion conditions and suggest that, beside the EB barrier properties, the enhanced corrosion resistance observed on the EB coated samples could partly arise from two other mains factors......: • a weak redox activity of the polymer which passivate the metal, • a proton involving self-healing process taking place at the polymer–metal interface, which contributes to delay local acidiWcation in Wrst steps of corrosion on EB coated aluminium surfaces....

  8. Emeraldine base as corrosion protective layer on aluminium alloy AA5182, effect of the surface microstructure

    Energy Technology Data Exchange (ETDEWEB)

    Cecchetto, L. [Laboratoire d' Electrochimie et de Physicochimie des Materiaux et des Interfaces, CNRS-UJF-INP-Grenoble (UMR 5631), ENSEEG, BP 75, 38402 St. Martin d' Heres (France); Ambat, R. [School of Engineering Metallurgy and Materials, University of Birmingham, Edgbaston, Birmingham B15 2TT (United Kingdom); Davenport, A.J. [School of Engineering Metallurgy and Materials, University of Birmingham, Edgbaston, Birmingham B15 2TT (United Kingdom); Delabouglise, D. [Laboratoire d' Electrochimie et de Physicochimie des Materiaux et des Interfaces, CNRS-UJF-INP-Grenoble (UMR 5631), ENSEEG, BP 75, 38402 St. Martin d' Heres (France)]. E-mail: Didier.Delabouglise@lepmi.inpg.fr; Petit, J.-P. [Laboratoire d' Electrochimie et de Physicochimie des Materiaux et des Interfaces, CNRS-UJF-INP-Grenoble (UMR 5631), ENSEEG, BP 75, 38402 St. Martin d' Heres (France); Neel, O. [Centre de Recherche de Voreppe, Pechiney, Parc economique Centr' Alp, 38340 Voreppe (France)

    2007-02-15

    AA5182 aluminium alloy cold rolled samples were coated by thin films of emeraldine base (EB) obtained from a 5% solution in N-methylpyrrolidinone. Accelerated corrosion tests prove this coating very effective for corrosion protection of aluminium alloys in neutral environment. This study underlines the prominent role of surface cathodic intermetallic particles in pit initiation and coating break down in enhanced corrosion conditions and suggest that, beside the EB barrier properties, the enhanced corrosion resistance observed on the EB coated samples could partly arise from two other mains factors:- a weak redox activity of the polymer which passivate the metal, - a proton involving self-healing process taking place at the polymer-metal interface, which contributes to delay local acidification in first steps of corrosion on EB coated aluminium surfaces.

  9. Aluminium Alloy AA6060 surface treatment with high temperature steam containing chemical additives

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Tabrizian, Naja; Jellesen, Morten S.

    2015-01-01

    The steam treatment process was employed to produce a conversion coating on aluminium alloy AA6060. The changes in microstructure and its effect on corrosion resistance properties were investigated. Various concentrations of KMnO4 containing Ce(NO3)3 was injected into the steam and its effect on ...

  10. Corrosion behaviour of 6063 aluminium alloy in acidic and in alkaline media

    Directory of Open Access Journals (Sweden)

    Prabhu Deepa

    2017-05-01

    Full Text Available The corrosion behaviour of 6063 aluminium alloy was investigated in different concentrations of phosphoric acid medium and sodium hydroxide medium at different temperatures. The study was done by electrochemical method, using Tafel polarization technique and electrochemical impedance spectroscopy (EIS technique. The surface morphology was investigated using scanning electron microscope (SEM with Energy-dispersive X-ray spectroscopy (EDX. The results showed that the 6063 aluminium alloy undergoes severe corrosion in sodium hydroxide medium than in phosphoric acid medium. The corrosion rate of 6063 aluminium alloy increased with an increase in the concentration of acid as well as with alkali. The corrosion rate was increased with an increase in temperature. The kinetic parameters and thermodynamic parameters were calculated using Arrhenius theory and transition state theory. Suitable mechanism was proposed for the corrosion of 6063 aluminium alloy in phosphoric acid medium and sodium hydroxide medium. The results obtained by Tafel polarization and electrochemical impedance spectroscopy (EIS techniques were in good agreement with each other.

  11. Galvanostatic response of AA2024 aluminium alloy in 3.5% NaCl ...

    Indian Academy of Sciences (India)

    s12034-016-1301-0. Galvanostatic response of AA2024 aluminium alloy in 3.5% NaCl solution. U DONATUS. ∗ and G E THOMPSON. Corrosion and Protection Centre, School of Materials, The University of Manchester, Manchester M13 9PL, UK.

  12. Intermetallic particles-induced pitting corrosion in 6061-T651 aluminium alloy

    CSIR Research Space (South Africa)

    Mutombo, K

    2011-07-01

    Full Text Available The polished 6061-T651 aluminium alloy was immersed in 3.5% NaCl solution with about 7 ppm dissolved oxygen. Scanning Electron Microscopy equipped with Energy dispersive Xray Spectroscopy revealed the presence of Al-Si-Fe-containing particles...

  13. Investigation of photocatalytic activity of titanium dioxide coating deposited on aluminium alloy substrate by plasma technique

    DEFF Research Database (Denmark)

    Daviðsdóttir, Svava; Soyama, Juliano; Dirscherl, Kai

    2011-01-01

    . Literature consists of large number of publications on titanium dioxide coating for self-cleaning applications, with glass as the main substrate. Only little work is available on TiO2 coating of metallic alloys used for engineering applications. Engineering materials, such as light-weight aluminium and steel...

  14. Improvement of hardness of aluminium AA1200 by laser surface alloying

    CSIR Research Space (South Africa)

    Mabhali, Luyolo AB

    2010-07-01

    Full Text Available Aluminium is vastly used in industry due to its low cost, light weight and excellent workability, but lacks in wear resistance and hardness. Laser alloying is used to improve the surface properties such as hardness by modifying the composition...

  15. Laser surface alloying of aluminium with WC+Co+NiCr for improved wear resistance

    CSIR Research Space (South Africa)

    Nath, S

    2012-03-01

    Full Text Available In the present study, laser surface alloying of aluminium with WC + Co + NiCr (in the ratio of 70:15:15) has been conducted using a 5 kW continuous wave (CW) Nd:YAG laser (at a beam diameter of 0.003 m), with the output power ranging from 3 to 3.5 k...

  16. A morphological study of filiform corrosive attack on cerated AA2024-T351 aluminium alloy

    NARCIS (Netherlands)

    Hughes, A.E.; Mol, J.M.C.; Hinton, B.R.W.; Zwaag, S. van der

    2005-01-01

    SEM and EDS studies were carried out to characterise filiform attack on a cerated AA2024- T351 aluminium alloy with a polyurethane topcoat. The filiforms developed on AA2024-T351 were sectioned, stripped of corrosion product and etched to reveal the grain structure. Examination of sections through

  17. A Comparative Study on Wear Properties of As Cast, Cast Aged and Forge Aged A356 Alloy with Addition of Grain Refiner and/or Modifier

    Directory of Open Access Journals (Sweden)

    D.G. Mallapur

    2015-03-01

    Full Text Available In the present work, a comparative wear behavior study of three categories of materials viz, as cast, cast aged (casting followed by T6 and forge aged (forging followed by T6 has been investigated. Neither melt treatment nor solid state processing (like aging and forging seems to be altering the wear behavior of the materials drastically. Cast aged A356 materials exhibit higher wear resistance compared to as cast and forge aged A356 materials. Further, it was observed that cast aged samples register lower coefficient of friction compared to other samples. It is also noted that the difference in wear behavior is revealed only at conditions of higher load, higher speed and longer sliding distance of testing. At lower regimes the difference is marginal. Among cast aged samples, ones treated with combined addition exhibit better wear resistance compared to other materials. Samples treated with combined addition register lowest coefficient of friction followed by samples treated with Sr, those with B, those with Ti and untreated ones. Abrasive wear mechanism is found to be operative in the regime of higher loading and higher velocity of sliding. Adhesive wear mechanism seems to be dominating the wear process at the lower regime of load and velocity of sliding.

  18. Property enhancement by grain refinement of zinc-aluminium foundry alloys

    International Nuclear Information System (INIS)

    Krajewski, W K; Piwowarski, G; Krajewski, P K; Greer, A L

    2016-01-01

    Development of cast alloys with good mechanical properties and involving less energy consumption during their melting is one of the key demands of today's industry. Zinc foundry alloys of high and medium Al content, i.e. Zn-(15-30) wt.% Al and Zn-(8-12) wt.% Al, can satisfy these requirements. The present paper summarizes the work [1-9] on improving properties of sand-cast ZnAl10 (Zn-10 wt.% Al) and ZnAl25 (Zn-25 wt. % Al) alloys by melt inoculation. Special attention was devoted to improving ductility, whilst preserving high damping properties at the same time. The composition and structural modification of medium- and high-aluminium zinc alloys influence their strength, tribological properties and structural stability. In a series of studies, Zn - (10-12) wt. % Al and Zn - (25-26) wt.% Al - (1-2.5) wt.% Cu alloys have been doped with different levels of added Ti. The melted alloys were inoculated with ZnTi-based refiners and it was observed that the dendritic structure is significantly finer already after addition of 50 - 100 ppm Ti to the melted alloys. The alloy's structure and mechanical properties have been studied using: SEM (scanning electron microscopy), LM (light microscopy), dilatometry, pin-on-disc wear, and tensile strength measurements. Grain refinement leads to significant improvement of ductility in the binary high-aluminium Zn-(25-27) Al alloys while in the medium-aluminium alloys the effect is rather weak. In the ternary alloys Zn-26Al-Cu, replacing a part of Cu with Ti allows dimensional changes to be reduced while preserving good tribological properties. Furthermore, the high initial damping properties were nearly entirely preserved after inoculation. The results obtained allow us to characterize grain refinement of the examined high-aluminium zinc alloys as a promising process leading to the improvement of their properties. At the same time, using low melting ZnTi-based master alloys makes it possible to avoid the excessive melt

  19. Structure and selected properties of high-aluminium Zn alloy with silicon addition

    Directory of Open Access Journals (Sweden)

    A. Zyska

    2011-07-01

    Full Text Available The results of examinations concerning the abrasive wear resistance, hardness, and thermal expansion of high-aluminium zinc alloys are presented. The examinations were carried out for five synthetic ZnAl28 alloys with variable silicon content ranging from 0.5% to 3.5%, and – for the purpose of comparison – for the standardised ZnAl28Cu4 alloy. It was found that silicon efficiently increases the tribological properties and decreases the coefficient of thermal expansion of zinc alloys. The most advantageous set of the examined properties is exhibited by the alloys containing over 2.5% Si. They are characterised by higher parameters as compared with the standardised alloy. Observations of microstructures reveal that silicon precipitates as a separate compact phase, and its morphology depends on t he Si content in the alloy. The performed examinations show that silicon can satisfactorily replace copper in high aluminium Zn alloys, thus eliminating the problem of dimensional instability of castings.

  20. Recovery of aluminium, nickel-copper alloys and salts from spent fluorescent lamps.

    Science.gov (United States)

    Rabah, Mahmoud A

    2004-01-01

    This study explores a combined pyro-hydrometallurgical method to recover pure aluminium, nickel-copper alloy(s), and some valuable salts from spent fluorescent lamps (SFLs). It also examines the safe recycling of clean glass tubes for the fluorescent lamp industry. Spent lamps were decapped under water containing 35% acetone to achieve safe capture of mercury vapour. Cleaned glass tubes, if broken, were cut using a rotating diamond disc to a standard shorter length. Aluminium and copper-nickel alloys in the separated metallic parts were recovered using suitable flux to decrease metal losses going to slag. Operation variables affecting the quality of the products and the extent of recovery with the suggested method were investigated. Results revealed that total loss in the glass tube recycling operation was 2% of the SFLs. Pure aluminium meeting standard specification DIN 1712 was recovered by melting at 800 degrees C under sodium chloride/carbon flux for 20 min. Standard nickel-copper alloys with less than 0.1% tin were prepared by melting at 1250 degrees C using a sodium borate/carbon flux. De-tinning of the molten nickel-copper alloy was carried out using oxygen gas. Tin in the slag as oxide was recovered by reduction using carbon or hydrogen gas at 650-700 degrees C. Different valuable chloride salts were also obtained in good quality. Further research is recommended on the thermodynamics of nickel-copper recovery, yttrium and europium recovery, and process economics.

  1. Recovery of actinides from actinide-aluminium alloys by chlorination: Part I

    International Nuclear Information System (INIS)

    Cassayre, L.; Soucek, P.; Mendes, E.; Malmbeck, R.; Nourry, C.; Eloirdi, R.; Glatz, J.-P.

    2011-01-01

    Pyrochemical processes in molten LiCl-KCl are being developed in ITU for recovery of actinides from spent nuclear fuel. The fuel is anodically dissolved to the molten salt electrolyte and actinides are electrochemically reduced on solid aluminium cathodes forming solid actinide-aluminium alloys. A chlorination route is being investigated for recovery of actinides from the alloys. This route consists in three steps: Vacuum distillation for removal of the salt adhered on the electrode, chlorination of the actinide-aluminium alloys by chlorine gas and sublimation of the formed AlCl 3 . A thermochemical study showed thermodynamic feasibility of all three steps. On the basis of the conditions identified by the calculations, experiments using pure UAl 3 alloy were carried out to evaluate and optimise the chlorination step. The work was focused on determination of the optimal temperature and Cl 2 /UAl 3 molar ratio, providing complete chlorination of the alloy without formation of volatile UCl 5 and UCl 6 . The results showed high efficient chlorination at a temperature of 150 deg. C.

  2. Steam assisted oxide growth on aluminium alloys using oxidative chemistries: Part II corrosion performance

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Jellesen, Morten Stendahl; Ambat, Rajan

    2015-01-01

    Surface treatment of aluminium alloys using steam with oxidative chemistries, namely KMnO4 and HNO3 resulted in accelerated growth of oxide on aluminium alloys. Detailed investigation of the corrosion performance of the treated surfaces was carried out using potentiodynamic polarisation...... and standard industrial test methods such as acetic acid salt spray (AASS) and filiform corrosion on commercial AA6060 alloy. Barrier properties of the film including adhesion were evaluated using tape test under wet and dry conditions. Electrochemical results showed reduced cathodic and anodic activity, while...... the protection provided by steam treatment with HNO3was a function of the concentration of NO3−ions. The coating generated by inclusion of KMnO4showed highest resistance to filiform corrosion. Overall, the performance of the steam treated surfaces under filiform corrosion and AASS test was a result of the local...

  3. The influence of alloying elements in aluminium on the grain refinement with ALTI5B1

    Directory of Open Access Journals (Sweden)

    Naglič I.

    2009-07-01

    Full Text Available This work deals with the influence of alloying elements in aluminium on the grain refinement with various additions of AlTi5B1. Grain-refinement tests were made at a cooling rate of 15 °C/s. The results revealed that in both aluminium and an Al-Fe alloy the grain size decreases with increasing additions of the AlTi5B1 grain refiner. We found that for the same boron content the grain size was smaller in the case of the Al-Fe alloy. The difference in the grain sizes for the same content of boron was approximately 15 μm; this is considerably smaller than the difference between the grain sizes in samples with the same difference of growth-restricting factor made at slower cooling rates.

  4. Abrasive wear response of aluminium alloy-sillimanite particle reinforced composite under low stress condition

    International Nuclear Information System (INIS)

    Singh, M.; Mondal, D.P.; Das, S.

    2006-01-01

    The abrasive wear behaviour of aluminium alloy-sillimanite particle reinforced composite under low stress condition has been reported and the results have been compared with the corresponding matrix alloy which was produced and cast under similar conditions. The study showed that wear resistance (inverse of wear rate) of the composite was higher than the matrix alloy. The wear rate decreased with sliding distance and increased with applied load irrespective of materials. The worn surfaces and subsurfaces of the tested samples were examined in the scanning electron microscope in order to understand the material removal mechanism during low stress abrasive wear process

  5. High frequency ohmic loss of beryllium and its alloy with aluminium

    International Nuclear Information System (INIS)

    Prentslau, N.N.

    1999-01-01

    The surface resistance of Be of different purity and its alloy with Al (50%Be-50%Al) is investigated at temperatures ranged from 4,2 to 300 K in the 0-10 10 Hz frequency region. It is shown that within the temperature range (in the vicinity of 77 K) where beryllium is a de hyper conductor. Its surface resistance and the surface resistance of the alloy are minimum compared to that of other metals, in particular, of aluminium. The temperature dependence of the surface resistance of Be and its alloys is well described by the classical formulae of electrodynamics

  6. Summary of structural refinement in hi-silicon aluminium piston alloy with phosphorous as grain refiner

    International Nuclear Information System (INIS)

    Malik, F.A.; Sheikh, S.T.; Choudhry, A.A.

    2003-01-01

    Aluminium Silicon Alloys are extensively used in a wide variety of applications. There are numerous variables in composition, production control, final structure which can influence the mechanical properties of Hi - Silicon Piston alloys. Hypereutectic AlSi alloys develop coarse grain primary silicon crystals, which have a strong negative effect on the tensile strength, the ductility, and the hardness. These crystals slow machining and reduce the tool life considerably. Phosphorous addition produce a fine, evenly spread crystal structure, lamellar structure of the silicon changes into a granular structure. (author)

  7. Diamond turning and polishing tests on new RSP aluminium alloys

    NARCIS (Netherlands)

    Horst, R. ter; Haan, M. de; Gubbels, G.P.H.; Senden, R.; Venrooy, B.W.H. van; Hoogstrate, A.M.

    2012-01-01

    For years now conventional aluminium 6061 T6 has widely been used for mirrors in astronomical instruments, being diamond turned or since a few years also being optically polished. This allows the development of optical systems that can be tested and operated at any temperature, without being

  8. Cavitation-aided grain refinement in aluminium alloys

    NARCIS (Netherlands)

    Atamanenko, T.V.

    2010-01-01

    This thesis deals with grain refinement under the influence of ultrasonic-driven cavitation in aluminium casting processes. Three major goals of this research were: (1) to identify the mechanism of the cavitation-aided grain refinement at different stages of solidification; (2) to reveal the

  9. Elaboration in the area of aluminium containing alloys

    International Nuclear Information System (INIS)

    Mirsaidov, U.M.

    2002-01-01

    In the Institute of Chemistry was elaborated the experimental-industrial installation and technology of deep aluminium purification by the methods of zone melting and recrystallization. The developed technology let receive the metal of model A5 N A6 N dependence from number of induction zone passage

  10. A multiple buckling curve formulation for design of aluminium alloy ...

    African Journals Online (AJOL)

    The paper refers to the overall stability design of aluminium structural elements. Buckling curves for members subjected to compression and members subjected to bending are dealt with. The formulation is based on probabilistic considerations of two random events, namely the elastic buckling of a perfect member and the ...

  11. Development of multilayer coatings for forming dies and tools of aluminium alloy from liquid state

    International Nuclear Information System (INIS)

    Torres, E; Ugues, D; Brytan, Z; Perucca, M

    2009-01-01

    In this work, a nanocomposite (Cr,Al) x N 1-x /Si 3 N 4 coating system was deposited on H11 hot work tool steel, using the Lateral Arc Rotating Cathodes (LARC (registered) ) deposition system and modulating the chemical composition of the chromium and aluminium-silicon content. Structural characterizations were performed using scanning electron microscopy, equipped with energy dispersive spectroscopy probe, and applying x-ray diffraction, for the evaluation of phase constitution and crystallite size. In addition to the structural features, the coatings' resistance to cyclic immersions in molten aluminium alloy was evaluated. The deposited CrAlSiN coatings exhibited an fcc-Cr 1-x Al x N type structure with different aluminium contents, which directly influence hardness and wear and fatigue resistance in cyclic immersion tests. The main failure modes that occurred on the coatings' surface were soldering and thermal fatigue cracks mainly in the form of heat checks. The aluminium rich coatings were able to withstand about 15 000 cycles, whereas the decrease in the aluminium content in the coatings results in a decrease in the resistance to the immersion in molten aluminium bath. It is worthwhile to note that uncoated H11, subjected to similar testing conditions, withstood at maximum 5000 cycles.

  12. Steam assisted oxide growth on aluminium alloys using oxidative chemistries: Part I Microstructural investigation

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Piotrowska, Kamila; Gudla, Visweswara Chakravarthy

    2015-01-01

    The surface treatment of aluminium alloys under steam containing KMnO4 and HNO3resulted in the formation of an oxide layer having a thickness of up to 825 nm. The use of KMnO4 and HNO3 in the steam resulted in incorporation of the respective chemical species into the oxide layer. Steam treatment...... resulting in poor coverage by the steam generated oxide layer compared to the coating formed using MnO4−ions. Further, increase in the concentration of NO3−ions in the solution retards precipitation of the steam generated aluminium hydroxide layer....

  13. Predicting tensile strength of friction stir welded AA6061 aluminium alloy joints by a mathematical model

    International Nuclear Information System (INIS)

    Elangovan, K.; Balasubramanian, V.; Babu, S.

    2009-01-01

    AA6061 aluminium alloy (Al-Mg-Si alloy) has gathered wide acceptance in the fabrication of light weight structures requiring a high strength-to weight ratio and good corrosion resistance. Compared to the fusion welding processes that are routinely used for joining structural aluminium alloys, friction stir welding (FSW) process is an emerging solid state joining process in which the material that is being welded does not melt and recast. This process uses a non-consumable tool to generate frictional heat in the abutting surfaces. The welding parameters such as tool rotational speed, welding speed, axial force etc., and tool pin profile play a major role in deciding the joint strength. An attempt has been made to develop a mathematical model to predict tensile strength of the friction stir welded AA6061 aluminium alloy by incorporating FSW process parameters. Four factors, five levels central composite design has been used to minimize number of experimental conditions. Response surface method (RSM) has been used to develop the model. Statistical tools such as analysis of variance (ANOVA), student's t-test, correlation co-efficient etc. have been used to validate the developed model. The developed mathematical model can be effectively used to predict the tensile strength of FSW joints at 95% confidence level

  14. Friction factor of CP aluminium and aluminium–zinc alloys

    Indian Academy of Sciences (India)

    The Rock- well hardness of all the samples were also measured. 3. Results and discussion. Friction factor, m, of CP aluminium is given in table 1 for various test temperatures. The friction factor, m, was low. (0⋅09–0⋅34) up to 673 K but it reached 0⋅90 at 773 K ex- hibiting sticking behaviour. Figure 5 shows the plot of.

  15. Study of fatigue behaviour of 7475 aluminium alloy

    Indian Academy of Sciences (India)

    Unknown

    highly stressed region. The greatest potential of commer- cial exploitation is offered by the medium strength. Al–Zn–Mg alloys such as 7075, 7050, etc. The applica- tions of these alloys remained restricted due to their low toughness and environmental sensitive fracture in service, particularly under cyclic loading condition ...

  16. Corrosion of alloys of the niobium--titanium--aluminium system

    International Nuclear Information System (INIS)

    Andreeva, V.V.; Alekseeva, E.L.; Dontsov, S.N.; Moiseeva, I.S.

    The mechanical properties and corrosion resistance of niobium--titanium--aluminum alloys in 20 percent HCl and 40--75 percent H 2 SO 4 at 40 and 100 0 C are considered. Current density vs potential and corrosion rate vs potential potentiostatic curves plotted in 75 percent H 2 SO 4 at 140 0 C for the alloys with different titanium contents at a constant content of aluminum and also for alloys with a constant titanium content at different contents of aluminum are given. It was shown that the corrosion resistance of the alloys in 75 percent H 2 SO 4 at 140 0 C is an exponential function of the atomic content of the alloying components (Ti, Al) in them; aluminum vitiates the corrosion resistance very strongly

  17. Phase composition and properties of rapidly cooled aluminium-zirconium-chromium alloys

    International Nuclear Information System (INIS)

    Sokolovskaya, E.M.; Badalova, L.M.; Podd''yakova, E.I.; Kazakova, E.F.; Loboda, T.P.; Gribanov, A.V.

    1989-01-01

    Using the methods of physicochemical analysis the interaction of aluminium with zirconium and chromium is studied. Polythermal cross sections between Al 3 -Zr-Al 7 Cr and radial polythermal cross section from aluminium-rich corner with the ratio of components Zr:Cr=5:7 by mass are constructed. The effect of zirconium and chromium content on electrochemical characteristics of aluminium-base rapidly quenching alloys in systems Al-Cr, Al-Zr, Al-Cr-Zr. An increase in chromium concentration in oversaturated solid solution of Al-Cr system expands considerably the range of passive state. When Al 7 Cr phase appears the range of passive stae vanishes

  18. Joining of Aluminium Alloy and Steel by Laser Assisted Reactive Wetting

    Science.gov (United States)

    Liedl, Gerhard; Vázquez, Rodrigo Gómez; Murzin, Serguei P.

    2017-12-01

    Compounds of dissimilar materials, like aluminium and steel offer an interesting opportunity for the automotive industry to reduce the weight of a car body. Thermal joining of aluminium and steel leads to the formation of brittle intermetallic compounds, which negatively affects the properties of the welded joint. Amongst others, growth of such intermetallic compounds depends on maximum temperature and on the time at certain temperatures. Laser welding with its narrow well seam and its fast heating and cooling cycles provides an excellent opportunity to obtain an ultrathin diffusion zone. Joining of sheet metal DC01 with aluminium alloy AW6016 has been chosen for research. The performed experimental studies showed that by a variation of the beam power and scanning speed it is possible to obtain an ultrathin diffusion zone with narrow intermetallic interlayers. With the aim of supporting further investigation of laser welding of the respective and other dissimilar pairings a multi-physical simulation model has been developed.

  19. A new tribological system test for integrated hot forming and die quenching of aluminium alloy sheets

    Science.gov (United States)

    Snilsberg, Knut Erik; Welo, Torgeir; Moen, Knut Erling; Holmedal, Bjørn; Jensrud, Ola; Koroschetz, Christian

    2017-10-01

    The automotive industry is searching for alternative powertrain and lightweight solutions to meet steadily stricter emission standards and regulations. To leverage the use of high-strength age-hardening aluminium alloys, new processes such as hot forming and in-die quenching are under development in a number of different groups. 0ne of the challenges with in-die quenching is controlling the friction regime stability due to rapidly changing temperatures at both the tool and the blank surfaces under complex deformation modes. In this paper, a cup-based test method is developed and tested for combinations of draw ring materials and lubricants on AA6070 aluminium sheets. Qualitative investigations of formed cups indicate reduced adhesion of aluminium at the tool surface can be obtained by choosing the right combination of tool and lubrication parameters. A correlation between maximum punch force, formed cup height and average Coulomb friction coefficient is observed in both physical experiments and forming simulation.

  20. Mechanical properties of aluminium-uranium alloy and aluminium commercially pure at several temperatures

    International Nuclear Information System (INIS)

    Quadros, N.F. de.

    1976-01-01

    The mechanical properties of Ai-U (18,4 wt %) alloy with and without heat treatment were determined, and they were compared with the mechanical properties of aluminum alloy of commercial purity, AI-1100, at tempiratures of 25, 500, 550 and 600 0 C, the changes of both the yield point stress and the ultimate tensile strength as a function of temperature may be described through two emperical relationships. A fractography study was also made [pt

  1. Determination of initial stages of recrystallization in aluminium alloys by X-ray diffraction

    International Nuclear Information System (INIS)

    Loew, Marjorie

    2000-01-01

    Aluminium is a metal with a wide variety of application, such as beer cans, pans, door and window borders, and others more advanced, such as airplane structure, car engines, nuclear reactors components, rocket propulsion components and so on. Most of aluminium application is in alloy form. Such alloys must present suitable mechanical and chemical properties that are obtained, not entirely, by microstructure development. In this work, the beginning of recrystallization processes of AA1050 and AA3003 aluminium alloys were studied using X-ray diffraction techniques, transmission electron microscopy and hardness test. For such a sample, an initial heat treatment was done in order to homogenize the samples microstructure, followed by cold rolling and submitted again to a heat treatment in different temperatures in a hot furnace. After that samples were analyzed to verify the beginning of the recrystallization. Vickers hardness test revealed that the beginning of recrystallization is between 150 and 300 deg C for 1050 aluminium alloy and 200 and 300 deg C for 3003 aluminium alloy. X-ray diffraction using transmission chamber showed that the beginning of recrystallization is 240 and 260 deg C for AA1050 and AA3003, respectively. These temperatures were determined as the diffraction patterns recorded in the photographic plates changes when the recrystallization takes place. In this way, the deformed sample shows continuous concentric lines and the beginning of recrystallization is characterized by the occurrence of defined spots in this pattern. The Pole Figures goniometric method revealed that the beginning of recrystallization takes place between 250 and 300 deg C for both alloys. In the same way, orientation distribution functions showed the same temperature range for the recrystallization. However, the analysis by α and β fiber figures, the recrystallization temperatures are 240 and 260 deg C for AA1050 and AA3003, respectively. Finally, after the analysis of all

  2. Analysing the strength of friction stir welded dissimilar aluminium alloys using Sugeno Fuzzy model

    Science.gov (United States)

    Barath, V. R.; Vaira Vignesh, R.; Padmanaban, R.

    2018-02-01

    Friction stir welding (FSW) is a promising solid state joining technique for aluminium alloys. In this study, FSW trials were conducted on two dissimilar plates of aluminium alloy AA2024 and AA7075 by varying the tool rotation speed (TRS) and welding speed (WS). Tensile strength (TS) of the joints were measured and a Sugeno - Fuzzy model was developed to interconnect the FSW process parameters with the tensile strength. From the developed model, it was observed that the optimum heat generation at WS of 15 mm.min-1 and TRS of 1050 rpm resulted in dynamic recovery and dynamic recrystallization of the material. This refined the grains in the FSW zone and resulted in peak tensile strength among the tested specimens. Crest parabolic trend was observed in tensile strength with variation of TRS from 900 rpm to 1200 rpm and TTS from 10 mm.min-1 to 20 mm.min-1.

  3. RESEARCH OF FATIGUE AND MECHANICAL PROPERTIES AlMg1SiCu ALUMINIUM ALLOYS

    Directory of Open Access Journals (Sweden)

    Mária Mihaliková

    2015-11-01

    Full Text Available The paper is concerned with an analysis of utility and fatigue properties of industrially produced aluminium alloy, specifically EN AW 6061 (AlMg1SiCu, reinforced with the particles of SiC. The following properties were subject to evaluation: microstructure and sub-structure, mechanical characteristics. All of these mechanical properties in pre- and post- equal channel angular pressed (ECAP state have been studied. The hardness was evaluated by Vickers hardness test at the load of HV10. The significant part the thesis was devoted to the fatigue properties at cyclic load in torsion. The presented results demonstrate well that the combination of fractography and microscopy can give a significant contribution to the knowledge of initiation and propagation crack in the aluminium alloy.

  4. Electrochemical Estimation of the Corrosion Rate of Magnesium/Aluminium Alloys

    Directory of Open Access Journals (Sweden)

    A. Pardo

    2010-01-01

    Full Text Available The corrosion rate of AZ31, AZ80, and AZ91D magnesium/aluminium alloys immersed in 3.5 wt.% NaCl was determined comparing gravimetric and electrochemical measurements. The findings revealed that, for all investigated materials, a fraction of the metallic surface exposed to the corrosive medium did not reveal a normal electrochemical response to the applied signal. This may be associated with phenomena such as partial disintegration of specimens into fine metallic particles, electrochemical formation of Mg+ ions, and/or anomalous chemical attack occurring simultaneously with the normal electrochemical corrosion attack. The abnormal electrochemical behaviour was more evident for lower amounts of aluminium in the bulk composition of the investigated materials. Thus, the electrochemical estimates of pure Mg and the AZ31 alloy were not reliable and tended to underestimate corrosion losses.

  5. Braze Welding TIG of Titanium and Aluminium Alloy Type Al – Mg

    Directory of Open Access Journals (Sweden)

    Winiowski A.

    2016-03-01

    Full Text Available The article presents the course and the results of technological tests related to TIG-based arc braze welding of titanium and AW-5754 (AlMg3 aluminium alloy. The tests involved the use of an aluminium filler metal (Al99.5 and two filler metals based on Al-Si alloys (AlSi5 and AlSi12. Braze welded joints underwent tensile tests, metallographic examinations using a light microscope as well as structural examinations involving the use of a scanning electron microscope and an X-ray energy dispersive spectrometer (EDS. The highest strength and quality of welds was obtained when the Al99.5 filler metal was used in a braze welding process. The tests enabled the development of the most convenient braze welding conditions and parameters.

  6. A crystallographic texture perspective formability investigation of aluminium 5052 alloy sheets at various annealing temperatures

    Energy Technology Data Exchange (ETDEWEB)

    Narayanasamy, R. [Department of Production Engineering, National Institute of Technology, Tiruchirappalli - 620015, Tamilnadu (India); Ravindran, R. [Department of Mechanical Engineering, VLB Janakiammal College of Engineering and Technology, Coimbatore - 641042, Tamilnadu (India)], E-mail: mceravindran@yahoo.co.in; Manonmani, K. [Department of Mechanical Engineering, Government College of Technology, Coimbatore - 641013, Tamilnadu (India)], E-mail: manokmani@yahoo.co.in; Satheesh, J. [Department of Production Engineering, National Institute of Technology, Tiruchirappalli - 620015, Tamilnadu (India)

    2009-05-15

    Formability, an important mechanical property of the sheet metal is strongly reliant on the crystallographic texture. Consequently deep drawability is also influenced. This paper deals with the perspective of crystallographic texture and its relevance with the formability of AA 5052 aluminium alloy sheet of 2 mm thickness annealed at four different temperatures namely 200 deg. C, 250 deg. C, 300 deg. C and 350 deg. C. Forming limit diagrams determined and plotted experimentally, their crystallographic textures obtained and their ODF plots prepared by X-ray diffraction were analyzed. The Forming limit diagrams (FLDs) of AA 5052 sheets annealed under different temperatures were examined with respect to the crystallographic texture point of view. The FLDs and crystallographic textures were then correlated with normal anisotropy of the sheet metal. It was found that the formability of aluminium alloy AA 5052 annealed at 350 deg. C possessed good formability, optimal texture and high normal anisotropy value.

  7. Advances in aluminium alloy products for structural applications in transportation

    International Nuclear Information System (INIS)

    Staley, J.T.; Lege, D.J.

    1993-01-01

    This paper describes the needs of the aviation and automotive markets for structural materials and presents examples of developments of aluminum alloy products to fill these needs. Designers of aircraft desire materials which will allow them to design lightweight, cost-effective structures which have the performance characteristics of durability and damage tolerance. Their needs are being met by new and emerging materials varying from Al-Li alloys for thick structure, high-strength plate and extrusions for wings, and new monolithic and aluminum-fiber laminates for fuselages. Increase in fuel economy because of lighter weight structure is the driving force for aluminum alloys in the automotive market, and cost is extremely important. Mechanical properties for automotive use also depend on the application, and corrosion resistance must be adequate. For ''hang-on'' components such as fenders and hoods, formability is typically the limiting mechanical property. Strength must be adequate to resist denting at a thickness which offers cost-effective weight savings over steel. Because formability often decreases with increasing yield strength, alloys which are highly formable in the T4 temper and which age harden during the paint bake operation were developed. Alloys such as 6009 and 6010 are now being challenged by 2008, 6111 and 6016. Body structure components must be made from materials which absorb energy and fail gracefully during a crash. Such components for an automotive space frame are being die cast from an Al-Si-Mg alloy. These ductile die castings are joined to thin 6XXX extrusions which must combine formability, strength, ductility and the ability to deform plastically on impact. Bumpers must combine strength and adequate formability; in the event that current alloys are inadequate for future needs, a new 7XXX alloy offers an improved combination of properties. (orig.)

  8. Study of quality of nine aluminium alloys surfaces created using abrasiv waterjet

    Czech Academy of Sciences Publication Activity Database

    Klichová, Dagmar; Klich, Jiří; Gurková, Lucie

    2016-01-01

    Roč. 2016, March 2016 (2016), s. 892-895 ISSN 1805-0476 R&D Projects: GA MŠk(CZ) LO1406; GA MŠk ED2.1.00/03.0082 Institutional support: RVO:68145535 Keywords : abrasive waterjet * aluminium alloy * optical profilometer Subject RIV: JQ - Machines ; Tools http://www.mmscience.eu/content/file/archives/MM_Science_201608.pdf

  9. Heat input effect of friction stir welding on aluminium alloy AA 6061-T6 welded joint

    Directory of Open Access Journals (Sweden)

    Sedmak Aleksandar

    2016-01-01

    Full Text Available This paper deals with the heat input and maximum temperature developed during friction stir welding with different parameters. Aluminium alloy (AA 6061-T6 has been used for experimental and numerical analysis. Experimental analysis is based on temperature measurements by using infrared camera, whereas numerical analysis was based on empirical expressions and finite element method. Different types of defects have been observed in respect to different levels of heat input.

  10. Tensile behaviour of aluminium 7017 alloy at various temperatures and strain rates

    Directory of Open Access Journals (Sweden)

    Ravindranadh Bobbili

    2016-04-01

    Full Text Available The objective of the present study is to carry out high strain rate tensile tests on 7017 aluminium alloy under different strain rates ranging from 0.01, 500, 1000 and 1500 s−1 and at temperatures of 25, 100, 200 and 300 °C. Quasi-Static tensile stress–strain curves were generated using INSTRON 8500 machine. Johnson-Cook (J-C constitutive model was developed for 7017 aluminium alloy based on high strain rate tensile data generated from split Hopkinson tension bar (SHTB at various temperatures. This study evidently showed an improvement in dynamic strength as the strain rate increases. The predictions of J-C model are observed to be in consistence with the experimental data for all strain rates and temperatures. The fracture surfaces of specimens tested were studied under SEM. The change in fracture mode has been observed at different strain rates. The shear mode of fracture is dominant at lower strain rates (0.01 and 500 s−1; whereas cup- and cone-like surface representing dimple structure is found at the higher strain rates (1000 and 1500 s−1. The numbers of dimples at high strain rates are more than the quasi-static and intermediate strain rates. It is also observed that the flow stress decreases with increase in temperature. The 7017 aluminium alloy demonstrates thermal softening at higher temperatures. So when the temperature is more than 200 °C at these strain rates, thermal softening is predominant mode of deformation mechanism. It is found that when the temperature increases to 200 °C, the number of dimples rises and the dimple size of 7017 aluminium alloy is larger than at lower temperatures.

  11. Residual stress development and relief in high strength aluminium alloys using standard and retrogression thermal treatments

    OpenAIRE

    Robinson, J.S; Tanner, D.A

    2003-01-01

    peer-reviewed Residual stresses develop in the aluminium alloy 7010 when the material is quenched from the solution heat treatment temperature. Residual stress measurements have been made using the X-ray diffraction technique and a longitudinal split sawcut method to determine the magnitude of residual stress that develops in specimens sectioned from large open die forgings as a result of (a) quenching these specimens into water at different temperatures, and (b) cold water quenching from ...

  12. Effect of equal channel angular pressing (ECAP) on creep in aluminium alloys

    Czech Academy of Sciences Publication Activity Database

    Sklenička, Václav; Dvořák, Jiří; Král, Petr; Kvapilová, Marie; Svoboda, Milan; Saxl, Ivan; Horita, Z.

    2007-01-01

    Roč. 539-543, - (2007), s. 2904-2909 ISSN 0255-5476 R&D Projects: GA AV ČR(CZ) IAA2041301 Institutional research plan: CEZ:AV0Z20410507; CEZ:AV0Z10190503 Keywords : equal-channel angular pressing * aluminium alloys * ultrafine-grained microscructure Subject RIV: JG - Metallurgy Impact factor: 0.399, year: 2005

  13. Removal of chromium (VI) from water by micro-alloyed aluminium ...

    African Journals Online (AJOL)

    This paper deals with Cr(VI) ion removal from water, by micro-alloyed aluminium composite (MAlC), under flow conditions. In a water environment the MAlC acts as a strong reducing agent. Dissolving it in water is accompanied by the generation of Al(III) ions and reduction of water to H2, with OH- ions. The final product is ...

  14. Metallurgical bond between magnesium AZ91 alloy and aluminium plasma sprayed coatings

    Czech Academy of Sciences Publication Activity Database

    Kubatík, Tomáš František; Pala, Zdeněk; Neufuss, Karel; Vilémová, Monika; Mušálek, Radek; Stoulil, J.; Slepička, P.; Chráska, Tomáš

    2015-01-01

    Roč. 282, November (2015), s. 163-170 ISSN 0257-8972 R&D Projects: GA ČR(CZ) GP14-31538P Institutional support: RVO:61389021 Keywords : Plasma spraying * AZ91 magnesium alloy * Aluminium * Metallurgical bond * X-ray diffraction Subject RIV: JK - Corrosion ; Surface Treatment of Materials Impact factor: 2.139, year: 2015 http://www.sciencedirect.com/science/article/pii/S0257897215303297

  15. Experimental investigations on thermo mechanical behaviour of aluminium alloys subjected to tensile loading and laser irradiation

    Science.gov (United States)

    Jelani, Mohsan; Li, Zewen; Shen, Zhonghua; Sardar, Maryam; Tabassum, Aasma

    2017-05-01

    The present work reports the investigation of the thermal and mechanical behaviour of aluminium alloys under the combined action of tensile loading and laser irradiations. The two types of aluminium alloys (Al-1060 and Al-6061) are used for the experiments. The continuous wave Ytterbium fibre laser (wavelength 1080 nm) was employed as irradiation source, while tensile loading was provided by tensile testing machine. The effects of various pre-loading and laser power densities on the failure time, temperature distribution and on deformation behaviour of aluminium alloys are analysed. The experimental results represents the significant reduction in failure time and temperature for higher laser powers and for high load values, which implies that preloading may contribute a significant role in the failure of the material at elevated temperature. The reason and characterization of material failure by tensile and laser loading are explored in detail. A comparative behaviour of under tested materials is also investigated. This work suggests that, studies considering only combined loading are not enough to fully understand the mechanical behaviour of under tested materials. For complete characterization, one must consider the effect of heating as well as loading rate.

  16. Inhibitive Behaviour of Corrosion of Aluminium Alloy in NaCl by Mangrove Tannin

    International Nuclear Information System (INIS)

    Solhan Yahya; Afidah Abdul Rahim; Affaizza Mohd Shah; Rohana Adnan

    2011-01-01

    Anticorrosion potential of mangrove tannins on aluminium alloys AA6061 in NaCl solution has been studied using potentiodynamic polarisation method and scanning electron microscopy (SEM). The study was carried out in different pH of corrosive medium in the absence and presence of various concentrations of tannin. The corrosion inhibition behaviour of the mangrove tannin on AA6061 aluminium alloy corrosion was found to be dependant on the pH of NaCl solution. Our results showed that the inhibition efficiency increased with increasing tannins concentration in chloride solution at pH 6. Treatment of aluminium alloy 6061 with all concentrations of mangrove tannins reduced the current density, thus decreased the corrosion rate. Tannins behaved as mixed inhibitors at pH 6 and reduction in current density predominantly affected in cathodic reaction. Meanwhile, at pH 12, addition of tannins shifted the corrosion potential to more cathodic potentials and a passivating effect was observed in anodic potentials. SEM studies have shown that the addition of tannins in chloride solution at pH 12 reduced the surface degradation and the formation of pits. (author)

  17. Effect of Laser Feeding on Heat Treated Aluminium Alloy Surface Properties

    Directory of Open Access Journals (Sweden)

    Labisz K.

    2016-06-01

    Full Text Available In this paper are presented the investigation results concerning microstructure as well as mechanical properties of the surface layer of cast aluminium-silicon-copper alloy after heat treatment alloyed and/ or remelted with SiC ceramic powder using High Power Diode Laser (HPDL. For investigation of the achieved structure following methods were used: light and scanning electron microscopy with EDS microanalysis as well as mechanical properties using Rockwell hardness tester were measured. By mind of scanning electron microscopy, using secondary electron detection was it possible to determine the distribution of ceramic SiC powder phase occurred in the alloy after laser treatment. After the laser surface treatment carried out on the previously heat treated aluminium alloys, in the structure are observed changes concerning the distribution and morphology of the alloy phases as well as the added ceramic powder, these features influence the hardness of the obtained layers. In the structure, there were discovered three zones: the remelting zone (RZ the heat influence zone (HAZ and transition zone, with different structure and properties. In this paper also the laser treatment conditions: the laser power and ceramic powder feed rate were investigated. The surface laser structure changes in a manner, that there zones are revealed in the form of. This carried out investigations make it possible to develop, interesting technology, which could be very attractive for different branches of industry.

  18. Microstructural and electrochemical characterization of environmentally friendly conversion layers on aluminium alloys

    Directory of Open Access Journals (Sweden)

    Palomino Luis Enrique M.

    2003-01-01

    Full Text Available Cerium conversion layers (CeCL have been investigated as a replacement for chromium conversion layers to protect Al alloys against corrosion. In this work the microstructure and the electrochemical behaviour of aluminium alloy 2024 with and without CeCL were investigated using, respectively, SEM-EDX and EIS. EDX results have shown that the presence of dispersed plated Cu particles on the alloy surface enhances the formation of the CeCL increasing the intensity of Ce peaks in the EDX spectra. EIS measurements on conversion-coated samples have shown that the presence of the layer increases the impedance, and that its presence is detected by the presence of a high frequency time constant. Results of potentiodynamic experiments have shown that the corrosion protection afforded by the conversion layer is due to the hindrance of the oxygen reduction reaction and that the pitting potential of the alloy is not changed.

  19. Optimization of Drilling Parameters for Reducing the Burr Height in Machining the Silicon Carbide Particle (SiCp) Coated with Multi Wall Carbon Nano Tubes (MWCNT) Reinforced in Aluminum Alloy (A 356) Using Meta Modeling Approach

    Science.gov (United States)

    Sangeetha, M.; Prakash, S.

    2017-05-01

    This paper explains the optimization of drilling parameters using meta modeling approach to reduce the burr height while machining Silicon Carbide Particle (SiCp) coated with Multi Wall Carbon Nano Tubes (MWCNT) and reinforced in aluminum alloy (A 356). The specimen is prepared by the combination of sonication and stir casting processes. The volume fraction of MWCNT used is 1.5% and the volume fraction of SiCp is 10%. The combination of input parameters for drilling the holes is designed using Taguchi experimental design technique. The input parameters chosen for drilling operations are spindle speed, feed rate and drill diameter. The ranges of input parameters are listed in Table 1. The tools used for drilling operation are made up of solid carbide drill bit. Meta model is a mathematical and statistical model whose second-order model can be fitted by factorial design. The optimization model can be improved significantly by the second-order model compared to the first-order model. Twenty-seven holes are drilled using vertical machining center in the prepared specimen (A 356/MWCNT coated SiCp). Desirability function shows the optimized values of input parameters to obtain minimum burr height. Meta modeling approach is used to design a model using input parameters and output response burr height. The residuals plot shows the predicted values are closer to the measured values. This plot explains that the Meta model is adequately used to predict the burr height. The optimized values of input parameters for obtaining minimum burr height are the combination of high speed, low feed and low drill diameter. The minimum value of burr height observed in this experiment is 0.002mm and it is obtained in the optimized combination of N3, f1 and d1.

  20. Ballistic impact velocity response of carbon fibre reinforced aluminium alloy laminates for aero-engine

    Science.gov (United States)

    Mohammed, I.; Abu Talib, A. R.; Sultan, M. T. H.; Saadon, S.

    2017-12-01

    Aerospace and other industries use fibre metal laminate composites extensively due to their high specific strength, stiffness and fire resistance, in addition to their capability to be tailored into different forms for specific purposes. The behaviours of such composites under impact loading is another factor to be considered due to the impacts that occur in take-off, landing, during maintenance and operations. The aim of the study is to determine the specific perforation energy and impact strength of the fibre metal laminates of different layering pattern of carbon fibre reinforced aluminium alloy and hybrid laminate composites of carbon fibre and natural fibres (kenaf and flax). The composites are fabricated using the hand lay-up method in a mould with high bonding polymer matrix and compressed by a compression machine, cured at room temperature for one day and post cure in an oven for three hours. The impact tests are conducted using a gun tunnel system with a flat cylindrical bullet fired using a helium gas at a distance of 14 inches to the target. Impact and residual velocity of the projectile are recorded by high speed video camera. Specific perforation energy of carbon fibre reinforced aluminium alloy (CF+AA) for both before and after fire test are higher than the specific perforation energy of the other composites considered before and after fire test respectively. CF +AA before fire test is 55.18% greater than after. The same thing applies to impact strength of the composites where CF +AA before the fire test has the highest percentage of 11.7%, 50.0% and 32.98% as respectively compared to carbon fibre reinforced aluminium alloy (CARALL), carbon fibre reinforced flax aluminium alloy (CAFRALL) and carbon fibre reinforced kenaf aluminium alloy (CAKRALL), and likewise for the composites after fire test. The considered composites in this test can be used in the designated fire zone of an aircraft engine to protect external debris from penetrating the engine

  1. Effects and mechanisms of grain refinement in aluminium alloys

    Indian Academy of Sciences (India)

    Unknown

    grain refine the solidified product. The mechanism of grain refinement is of considerable ... The present paper attempts to review the literature on the nucleant effects and solute effects on grain refinement and ... cast alloys. Firstly, reduced mechanical properties have been noted in plate products for structural application.

  2. Effect of Refiner Addition Level on Zirconium-Containing Aluminium Alloys

    International Nuclear Information System (INIS)

    Jaradeh, M M R; Carlberg, T

    2012-01-01

    It is well known that in aluminium alloys containing Zr, grain refiner additions do not function as desired, producing an effect often referred to as nuclei poisoning. This paper investigates the structure of direct chill-cast ingots of commercial AA3003 aluminium alloys, with and without Zr, at various addition levels of Al5Ti1B master alloy. In Bridgman experiments simulating ingot solidification, Zr-containing alloys were studied after the addition of various amounts of Ti. It could be demonstrated, in both ingot casting and simulation experiments, that Zr poisoning can be compensated for by adding more Ti and/or Al5Ti1B. The results confirm better refinement behaviour with the addition of Ti + B than of only Ti. The various combinations of Zr and Ti also influenced the formation of AlFeMn phases, and the precipitation of large Al 6 (Mn,Fe) particles was revealed. AlZrTiSi intermetallic compounds were also detected.

  3. Effect of Refiner Addition Level on Zirconium-Containing Aluminium Alloys

    Science.gov (United States)

    Jaradeh, M. M. R.; Carlberg, T.

    2012-01-01

    It is well known that in aluminium alloys containing Zr, grain refiner additions do not function as desired, producing an effect often referred to as nuclei poisoning. This paper investigates the structure of direct chill-cast ingots of commercial AA3003 aluminium alloys, with and without Zr, at various addition levels of Al5Ti1B master alloy. In Bridgman experiments simulating ingot solidification, Zr-containing alloys were studied after the addition of various amounts of Ti. It could be demonstrated, in both ingot casting and simulation experiments, that Zr poisoning can be compensated for by adding more Ti and/or Al5Ti1B. The results confirm better refinement behaviour with the addition of Ti + B than of only Ti. The various combinations of Zr and Ti also influenced the formation of AlFeMn phases, and the precipitation of large Al6(Mn,Fe) particles was revealed. AlZrTiSi intermetallic compounds were also detected.

  4. A hybrid aluminium alloy and its zoo of interacting nano-precipitates

    Energy Technology Data Exchange (ETDEWEB)

    Wenner, Sigurd, E-mail: sigurd.wenner@ntnu.no [Department of Physics, NTNU, Høgskoleringen 5, NO-7491 Trondheim (Norway); Marioara, Calin Daniel; Andersen, Sigmund Jarle [Materials and Chemistry, SINTEF, Høgskoleringen 5, NO-7491 Trondheim (Norway); Ervik, Martin; Holmestad, Randi [Department of Physics, NTNU, Høgskoleringen 5, NO-7491 Trondheim (Norway)

    2015-08-15

    An alloy with aluminium as its base element is heat treated to form a multitude of precipitate phases known from different classes of industrial alloys: Al–Cu(–Mg), Al–Mg–Si–Cu, and Al–Zn–Mg. Nanometer-sized needle-shaped particles define the starting point of the phase nucleation, after which there is a split in the precipitation sequence into six phases of highly diverse compositions and morphologies. There are several unique effects of phases from different alloy systems being present in the same host lattice, of which we concentrate on two: the replacement of Ag by Zn on the Ω interface and the formation of combined plates of the θ′ and C phases. Using atomically resolved scanning transmission electron microscopy and energy-dispersive X-ray spectroscopy, we investigate the formation mechanisms, crystal structures and compositions of the precipitates. - Graphical abstract: Display Omitted - Highlights: • An aluminium alloy composition in-between the 2/6/7xxx systems was investigated. • Six different phases from the three systems coexist in an over-aged state. • All phases with 〈001〉{sub Al} coherencies can nucleate on 6xxx needle precipitates. • Modified theta′ and omega interfaces are observed.

  5. Microstructural characterization aluminium alloys from the addition of boron

    International Nuclear Information System (INIS)

    Nunes, A.G.P.; Pipano, T.F.; Mota, M.A.; Mariano, N.A.; Ramos, E.C.T.

    2014-01-01

    In the electrical industry, the aluminum becomes attractive because it has excellent characteristics for transmitting electricity. The liquid aluminum has in its composition transition elements (zirconium, titanium, vanadium and chromium) that interfere negatively on the quality of the product. The addition of aluminum-boron alloys have been used to remove transition metals through the formation of borides, enabling an increase in electrical conductivity. However, no detailed reports of reactions between boron, transition metals and primary aluminum engines. However, the objective is to determine the stoichiometric composition that enables an increase in electrical conductivity of an aluminum alloy. Samples with different concentrations of boron were characterized by optical emission spectrometry, electrical conductivity and X-ray diffraction. The addition of boron in excess reduces the time in the formation of borides, and enable an increase in electrical conductivity. (author)

  6. Microstructure and mechanical properties of aluminium-lithium alloys

    International Nuclear Information System (INIS)

    Hargarter, H.

    1995-01-01

    The following topis were dealt with: materials and heat treatments, microstructural and mechanical testing, fractography, mechanical properties of IN 905XL and Al 8090 under quasistatic load (tensile testing and fracture toughness), fatigue behaviour in air (Woehler test, microcrack and macrocrack propagation), the influence of environmental media on the crack propagation in the alloy Al 8090 in air, NaCl and NaCl with inhibitors

  7. The solidification behavior of dilute aluminium-scandium alloys

    International Nuclear Information System (INIS)

    Norman, A.F.; Prangnell, P.B.; McEwen, R.S.

    1998-01-01

    The solidification behavior of dilute Sc containing Al alloys has been investigated. In binary Al-Sc alloys, Sc additions greater than the eutectic composition (0.55 wt%) were found to produce a remarkable refinement in the grain size of aluminum castings, of two orders of magnitude, due to the formation of the primary Al 3 Sc intermetallic phase during solidification. The refinement in grain size only occurred in hypereutectic compositions and was shown to be far greater than can be achieved by conventional Al grain refiners. Grain refinement by the addition of Sc is accompanied by a change in growth morphology from dendritic, in the large unrefined grains, to fine spherical grains with a divorced eutectic appearing on the grain boundaries in the refined castings. Similar levels of refinement were observed in Al-Sc-Zr and Al-Cu-Sc alloys. In the latter, a change in the segregation behavior of Cu was observed, from a strongly interdendritic segregation pattern to a more homogeneous distribution. The supersaturated Al-Sc solid solution can decompose via a discontinuous precipitation reaction to form coherent rod-like precipitates of the L1 2 Al 3 Sc phase

  8. Gating System Design for Casting thin Aluminium Alloy (Al-Si Plates

    Directory of Open Access Journals (Sweden)

    Victor ANJO

    2013-11-01

    Full Text Available The main problems caused by improper gating are entrained aluminium oxide films, cuts and washes, low casting yield and entrapped gas. This study describes the design of a gating system to produce thin Aluminium cast alloy plates of different sizes and thicknesses of 4mm, 6mm, 8mm, and 10mm using the non-pressurized gating with ratio of 1:4:4 and green sand moulding technique. The gating design was based on the laws of fluid mechanics and empirical rules of gating for non ferrous metals. The equipments used for this experiment includes; a coal fired crucible furnace and an X-Ray machine. Materials used include; silica sand, clay, wood, glue and Aluminium alloy scraps. The experimental procedure involved: the gating design calculations, construction of wooden pattern and gating; using the wooden pattern and gating to produce the mould cavities and gating; melting, melt treatment and pouring of melt in the sand mould to produce the casting. The plate castings after removal from mould were visually examined for surface defects and after fettling and cleaning X-Ray radiography was used to find the internal soundness of the castings. From the results obtained in the experiment, it was found that there were no internal defects and quality castings were produced.

  9. Analysis of wear properties of aluminium based journal bearing alloys with and without lubrication.

    Science.gov (United States)

    Mathavan, J. Joy; Patnaik, Amar

    2016-09-01

    Apart from classical bearing materials, Aluminium alloys are used as bearing materials these days because of their superior quality. In this analysis, new Aluminium based bearing materials, with filler metals Si, Ni, and Cr are prepared by metal mould casting in burnout furnace machine, and tribological properties of these alloys with and without lubrication were tested. The experiments for wear with lubrication are conducted on multiple specimen tester and experiments without lubrication is conducted on Pin on disk tribometer. The disc material used was SAE 1050 steel. Wear tests were conducted at a sliding speed of 0.785 m/s and at a normal load of 20 N. Coefficient of friction values, temperature changes and wear of the specimens were plotted on graph according to the above mentioned working conditions. Hardness and weight losses of the specimens were calculated. The obtained results demonstrate how the friction and wear properties of these samples have changed with the % addition of Silicon, Chromium and Nickel to the base metal aluminium.

  10. Study on optimal surface property of WC-Co cutting tool for aluminium alloy cutting

    International Nuclear Information System (INIS)

    Nizar, Mohd; Arimatsu, Naoya; Kawamitsu, Hiroshi; Takai, Kazuteru; Fukumoto, Masahiro

    2016-01-01

    The light weight property as well as high corrosion resistance of aluminium alloy has increased their demand especially in automobile industries. Aluminium alloy as a matter of fact has a low melting point and high ductility that severely adhere to the cutting tool surface and cause deterioration of chip evacuation. This problem often resulting in tools breakage. In this paper, in order to impart functions of anti-adhesion, we propose a technique by controlling the grinding marks micro texture on the tool surface by using the blast polishing treatment without any coating technologies. The results show that the tool which underwent polishing treatment reduces the cutting force as well as the aluminium adherence during the initial cutting process, and become worst as the process cutting continues. These results indicate that grinding mark texture improves the anti-adhesion by reducing the contact area during cutting and provide storage for the lubricant. In addition, too much polishing on the tool surface may remove these textures and resultantly worsen the tool performance. (paper)

  11. Study on optimal surface property of WC-Co cutting tool for aluminium alloy cutting

    Science.gov (United States)

    Nizar, Mohd; Arimatsu, Naoya; Kawamitsu, Hiroshi; Takai, Kazuteru; Fukumoto, Masahiro

    2016-02-01

    The light weight property as well as high corrosion resistance of aluminium alloy has increased their demand especially in automobile industries. Aluminium alloy as a matter of fact has a low melting point and high ductility that severely adhere to the cutting tool surface and cause deterioration of chip evacuation. This problem often resulting in tools breakage. In this paper, in order to impart functions of anti-adhesion, we propose a technique by controlling the grinding marks micro texture on the tool surface by using the blast polishing treatment without any coating technologies. The results show that the tool which underwent polishing treatment reduces the cutting force as well as the aluminium adherence during the initial cutting process, and become worst as the process cutting continues. These results indicate that grinding mark texture improves the anti-adhesion by reducing the contact area during cutting and provide storage for the lubricant. In addition, too much polishing on the tool surface may remove these textures and resultantly worsen the tool performance.

  12. Effect of pulsed current welding on fatigue behaviour of high strength aluminium alloy joints

    International Nuclear Information System (INIS)

    Balasubramanian, V.; Ravisankar, V.; Madhusudhan Reddy, G.

    2008-01-01

    High strength aluminium alloys (Al-Zn-Mg-Cu alloys) have gathered wide acceptance in the fabrication of light weight structures requiring high strength-to weight ratio, such as transportable bridge girders, military vehicles, road tankers and railway transport systems. The preferred welding processes of high strength aluminium alloy are frequently gas tungsten arc welding (GTAW) process and gas metal arc welding (GMAW) process due to their comparatively easier applicability and better economy. Weld fusion zones typically exhibit coarse columnar grains because of the prevailing thermal conditions during weld metal solidification. This often results inferior weld mechanical properties and poor resistance to hot cracking. In this investigation, an attempt has been made to refine the fusion zone grains by applying pulsed current welding technique. Rolled plates of 6 mm thickness have been used as the base material for preparing single pass welded joints. Single V butt joint configuration has been prepared for joining the plates. The filler metal used for joining the plates is AA 5356 (Al-5Mg (wt%)) grade aluminium alloy. Four different welding techniques have been used to fabricate the joints and they are: (i) continuous current GTAW (CCGTAW), (ii) pulsed current GTAW (PCGTAW), (iii) continuous current GMAW (CCGMAW) and (iv) pulsed current GMAW (PCGMAW) processes. Argon (99.99% pure) has been used as the shielding gas. Fatigue properties of the welded joints have been evaluated by conducting fatigue test using rotary bending fatigue testing machine. Current pulsing leads to relatively finer and more equi-axed grain structure in gas tungsten arc (GTA) and gas metal arc (GMA) welds. In contrast, conventional continuous current welding resulted in predominantly columnar grain structures. Grain refinement is accompanied by an increase in fatigue life and endurance limit

  13. Investigation of Selective Laser Melting Surface Alloyed Aluminium Metal Matrix Dispersive Reinforced Layers

    Science.gov (United States)

    Kamburov, V. V.; Dimitrova, R. B.; Kandeva, M. K.; Sofronov, Y. P.

    2018-01-01

    The aim of the paper is to investigate the improvement of mechanical properties and in particular wear resistance of laser surface alloyed dispersive reinforced thin layers produced by selective laser melting (SLM) technology. The wear resistance investigation of aluminium matrix composite layers in the conditions of dry friction surface with abrasive particles and nanoindentation tests were carried out. The process parameters (as scan speed) and their impact on the wear resistant layers have been evaluated. The alloyed layers containing metalized SiC particles were studied by Optical and Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray microanalysis (EDX). The obtained experimental results of the laser alloyed thin layers show significant development of their wear resistance and nanohardness due to the incorporated reinforced phase of electroless nickel coated SiC particles.

  14. Premature Cracking of Dies for Aluminium Alloy Die-Casting

    Directory of Open Access Journals (Sweden)

    Pawłowski B.

    2013-12-01

    Full Text Available Dwie identyczne matryce do ciśnieniowego odlewania stopów aluminium zostały przedwcześnie wycofane z eksploatacji z powodu wystąpienia na ich powierzchniach roboczych szeregu równoległych pęknięć. Kierunek propagacji pęknięć pokry w ał się z kierunkiem pasmowości mikrostrukturalnej a samo tworzenie się pęknięć było skutkiem niewłaściwej obróbki cieplnej matryc. Stwierdzono nieprawidłową orientację geometryczną matrycy wrzględem kierunku włókien struktury pierwotnej. Badania przy użyciu skaningowego mikroskopu elektronowego z wykorzystaniem techniki EDS wykazały, że przyczyną powstawania pęknięć matryc była nieprawidłową przeprowadzona obróbki cieplna matryc.

  15. Properties of experimental copper-aluminium-nickel alloys for dental post-and-core applications.

    Science.gov (United States)

    Rittapai, Apiwat; Urapepon, Somchai; Kajornchaiyakul, Julathep; Harniratisai, Choltacha

    2014-06-01

    This study aimed to develop a copper-aluminium-nickel alloy which has properties comparable to that of dental alloys used for dental post and core applications with the reasonable cost. Sixteen groups of experimental copper alloys with variants of 3, 6, 9, 12 wt% Al and 0, 2, 4, 6 wt% Ni were prepared and casted. Their properties were tested and evaluated. The data of thermal, physical, and mechanical properties were analyzed using the two-way ANOVA and Tukey's test (α=0.05). The alloy toxicity was evaluated according to the ISO standard. The solidus and liquidus points of experimental alloys ranged from 1023℃ to 1113℃ and increased as the nickel content increased. The highest ultimate tensile strength (595.9 ± 14.2 MPa) was shown in the Cu-12Al-4Ni alloy. The tensile strength was increased as the both elements increased. Alloys with 3-6 wt% Al exhibited a small amount of 0.2% proof strength. Accordingly, the Cu-9Al-2Ni and Cu-9Al-4Ni alloys not only demonstrated an appropriate modulus of elasticity (113.9 ± 8.0 and 122.8 ± 11.3 GPa, respectively), but also had a value of 0.2% proof strength (190.8 ± 4.8 and 198.2 ± 3.4 MPa, respectively), which complied with the ISO standard requirement (>180 MPa). Alloys with the highest contents of nickel (6 wt% Ni) revealed a widespread decolourisation zone (5.0-5.9 mm), which correspondingly produced the largest cell response, equating positive control. The copper alloys fused with 9 wt% Al and 2-4 wt% Ni can be considered for a potential use as dental post and core applications.

  16. Properties of experimental copper-aluminium-nickel alloys for dental post-and-core applications

    Science.gov (United States)

    Rittapai, Apiwat; Kajornchaiyakul, Julathep; Harniratisai, Choltacha

    2014-01-01

    PURPOSE This study aimed to develop a copper-aluminium-nickel alloy which has properties comparable to that of dental alloys used for dental post and core applications with the reasonable cost. MATERIALS AND METHODS Sixteen groups of experimental copper alloys with variants of 3, 6, 9, 12 wt% Al and 0, 2, 4, 6 wt% Ni were prepared and casted. Their properties were tested and evaluated. The data of thermal, physical, and mechanical properties were analyzed using the two-way ANOVA and Tukey's test (α=0.05). The alloy toxicity was evaluated according to the ISO standard. RESULTS The solidus and liquidus points of experimental alloys ranged from 1023℃ to 1113℃ and increased as the nickel content increased. The highest ultimate tensile strength (595.9 ± 14.2 MPa) was shown in the Cu-12Al-4Ni alloy. The tensile strength was increased as the both elements increased. Alloys with 3-6 wt% Al exhibited a small amount of 0.2% proof strength. Accordingly, the Cu-9Al-2Ni and Cu-9Al-4Ni alloys not only demonstrated an appropriate modulus of elasticity (113.9 ± 8.0 and 122.8 ± 11.3 GPa, respectively), but also had a value of 0.2% proof strength (190.8 ± 4.8 and 198.2 ± 3.4 MPa, respectively), which complied with the ISO standard requirement (>180 MPa). Alloys with the highest contents of nickel (6 wt% Ni) revealed a widespread decolourisation zone (5.0-5.9 mm), which correspondingly produced the largest cell response, equating positive control. CONCLUSION The copper alloys fused with 9 wt% Al and 2-4 wt% Ni can be considered for a potential use as dental post and core applications. PMID:25006386

  17. Influence of heat treatment on fatigue performances for self-piercing riveting similar and dissimilar titanium, aluminium and copper alloys

    OpenAIRE

    Zhang, Xianlian; He, Xiaocong; Xing, Baoying; Zhao, Lun; Lu, Yi; Gu, Fengshou; Ball, Andrew

    2016-01-01

    The fatigue performances of self-piercing riveting (SPR) joints connecting similar and dissimilar sheets of TA1 titanium alloy (TA1), Al5052 aluminium alloy (Al5052) and H62 copper alloy (H62) were studied in this paper. The specimens of similar TA1 sheets treated with stress relief annealing were prepared to investigate the influence of relief annealing on the mechanical properties of SPR joints. Fatigue tests were conducted to characterize the fatigue lives and failure modes of the joints. ...

  18. Fabrication of self-healing super-hydrophobic surfaces on aluminium alloy substrates

    Directory of Open Access Journals (Sweden)

    Yang Wang

    2015-04-01

    Full Text Available We present a method to fabricate a super-hydrophobic surface with a self-healing ability on an aluminium alloy substrate. The coatings are obtained by combining a two-step process (first, the substrate is immersed in a solution of HCl, HF and H2O, and then in boiling water and succeeding surface fluorination with a solution of poly(vinylidene-fluoride-co-hexafluoropropylene and a fluoroalkyl silane. The morphological features and chemical composition were studied by scanning electron micrometry and energy-dispersive X-ray spectroscopy. The prepared super-hydrophobic aluminium surfaces showed hierarchical structures forming pores, petals and particles with a contact angle of 161° and a sliding angle of 3°.

  19. Determination of lattice orientation in aluminium alloy grains by low energy gallium ion-channelling

    Energy Technology Data Exchange (ETDEWEB)

    Silk, Jonathan R. [Aerospace Metal Composites Ltd., RAE Road, Farnborough, GU14 6XE (United Kingdom); Dashwood, Richard J. [WMG, University of Warwick, Coventry, CV4 7AL (United Kingdom); Chater, Richard J., E-mail: r.chater@imperial.ac.u [Department of Materials, Imperial College, London SW7 2AZ (United Kingdom)

    2010-06-15

    Polished sections of a fine-grained aluminium, silicon carbide metal matrix composite (MMC) alloy were prepared by sputtering using a low energy gallium ion source and column (FIB). The MMC had been processed by high temperature extrusion. Images of the polished surface were recorded using the ion-induced secondary electron emission. The metal matrix grains were distinguished by gallium ion-channelling contrast from the silicon carbide component. The variation of the contrast from the aluminium grains with tilt angle can be recorded and used to determine lattice orientation with the contrast from the silicon carbide (SiC) component as a reference. This method is rapid and suits site-specific investigations where classical methods of sample preparation fail.

  20. Enhancement of wear and ballistic resistance of armour grade AA7075 aluminium alloy using friction stir processing

    Directory of Open Access Journals (Sweden)

    I. Sudhakar

    2015-03-01

    Full Text Available Industrial applications of aluminium and its alloys are restricted because of their poor tribological properties. Thermal spraying, laser surfacing, electron beam welding are the most widely used techniques to alter the surface morphology of base metal. Preliminary studies reveal that the coating and layering of aluminium alloys with ceramic particles enhance the ballistic resistance. Furthermore, among aluminium alloys, 7075 aluminium alloy exhibits high strength which can be compared to that of steels and has profound applications in the designing of lightweight fortification structures and integrated protection systems. Having limitations such as poor bond integrity, formation of detrimental phases and interfacial reaction between reinforcement and substrate using fusion route to deposit hard particles paves the way to adopt friction stir processing for fabricating surface composites using different sizes of boron carbide particles as reinforcement on armour grade 7075 aluminium alloy as matrix in the present investigation. Wear and ballistic tests were carried out to assess the performance of friction stir processed AA7075 alloy. Significant improvement in wear resistance of friction stir processed surface composites is attributed to the change in wear mechanism from abrasion to adhesion. It has also been observed that the surface metal matrix composites have shown better ballistic resistance compared to the substrate AA7075 alloy. Addition of solid lubricant MoS2 has reduced the depth of penetration of the projectile to half that of base metal AA7075 alloy. For the first time, the friction stir processing technique was successfully used to improve the wear and ballistic resistances of armour grade high strength AA7075 alloy.

  1. Microstructure and age-hardening effects of aluminium alloys with additions of scandium and zirconium

    Energy Technology Data Exchange (ETDEWEB)

    Galun, R.; Mordike, B.L. [Inst. fuer Werkstoffkunde und Werkstofftechnik, Technische Univ. Clausthal, Clausthal-Zellerfeld (Germany); Maiwald, T.; Smola, B. [Zentrum fuer Funktionswerkstoffe GmbH, Clausthal-Zellerfeld (Germany); Mergen, R.; Manner, M.; Uitz, W. [Miba Gleitlager GmbH, Laakirchen (Australia)

    2004-12-01

    The aim of the work presented in this report was to produce age-hardenable aluminium alloys containing scandium and zirconium by a casting process with similar cooling conditions like an industrial casting process. Microstructure, precipitation structure and age-hardening response of different alloys with up to 0.4 wt.% Sc and Zr were investigated. Age-hardening experiments from the as-cast condition without solution annealing showed a significant increase of hardness of about 100% for Sc-rich alloys and of 50% for Zr-rich alloys compared to the as-cast condition. TEM investigations revealed the formation of precipitates of ternary Al{sub 3}(Sc{sub x}Zr{sub 1-x}) phases with a cubic cP4 crystal structure. In addition to the strengthening effect, a high thermal stability especially of the precipitates in Zr-rich alloys up to 400 C let these alloys look very promising for high-temperature applications. (orig.)

  2. Effect of Pre/Post T6 Heat Treatment on the Mechanical Properties of Laser Welded SSM Cast A356 Aluminium Alloy

    CSIR Research Space (South Africa)

    Akhter, R

    2007-02-01

    Full Text Available HT) were butt welded, using an Nd: YAG laser. In another experiment, as cast welded samples were heat treated to T6 condition (post HT). The base metal and weld microstructures were presented. The effect of heat treatments on microstructure...

  3. Corrosion Characteristics and Kinetics of Zircaloys and Aluminium Alloys

    International Nuclear Information System (INIS)

    Sugondo; Chaidir, A

    1998-01-01

    Corrosion rate characterization of cladding materials has been done by dynamic method. The materials are zircaloy-2,zircaloy-4,AIMg2,and AIMgSi.The zircaloy alloys are characterized in the electrolytes of boric ion,iodide ion,lithium ion and cesium ion with a pH variation.The aluminum alloys are characterized in the cooling water of RSG-GAS reactor in different temperatures and Ph values .The results, show that corrosion product of iodine on zircaloy is not passivated, meanwhile the corrosion product of cesium undergoes passivation. However, the deposited substance in the surface of the specimens as indicated using WDX-SEM shows the same deposition rate.it is concluded therefore that iodine is diffused into the materials without getting resistance from the deposited substances on the surface. The effect of pH to corrosion rate of iodine on the zircaloy fluctuates meanwhile the cesium has the minimum corrosion rate at pH 7.5 At the concentration of 0.1 gram/1,cesium ion is more reactive than iodine but at higher concentration the reactivity becomes competitive . Furthermore , the interaction between zircaloy and boric ion at concentration of 300 ppm and lithium ion at 10 ppm shows an outstanding corrosion rate, i.e. 0.1 mpy. if both substances are mixed then the corrosion rate decreases drastically in the order of 10 -2 mpy.The reason of such a decrease may be due to the formation of complexes of boron lithium on the electrode surface. The arrhenius activation energies for such reaction have been found to be 37629.322 joule/mole 0 K for Al Mg 2 and 41609.822 joule /mole 0 K for AIMgSi ,respectively. This underlies the argument that AI Mg 2 is more reactive than AI Mg Si besides , AI Mg 2 is more reactive under acid condition meanwhile AI Mg Si more reactive under basic condition. Both alloys over come the minimum corrosion rate at the pH in between 4.7 to 7.5 and the level of the corrosion rate in the pH interval was outstanding

  4. Experimental and theoretical investigation on corrosion inhibition of AA5052 aluminium alloy by L-cysteine in alkaline solution

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Dapeng; Gao, Lixin [School of Environmental and Chemical Engineering, Shanghai University of Electric Power, Shanghai 200090 (China); Zhang, Daquan, E-mail: zhangdaquan@shiep.edu.cn [School of Environmental and Chemical Engineering, Shanghai University of Electric Power, Shanghai 200090 (China); Yang, Dong [School of Environmental and Chemical Engineering, Shanghai University of Electric Power, Shanghai 200090 (China); Wang, Hongxia; Lin, Tong [Institute for Frontier Materials, Deakin University, Geelong, VIC 3216 (Australia)

    2016-02-01

    The corrosion inhibition of L-cysteine on AA5052 aluminium alloy in 4 mol/L NaOH solution was investigated by hydrogen gas evolution experiment, polarisation curve, galvanostatic discharge, electrochemical impedance spectroscopy measurements and quantum chemical calculations. The adsorption of L-cysteine on aluminium alloy surface obeyed the amended Langmuir's adsorption isotherm. The polarisation curves indicated that L-cysteine acted as a cathodic inhibitor to inhibit cathodic reaction. The inhibition mechanism was dominated by the geometric covering effect. The galvanostatic discharge shows that the additives restrain the hydrogen evolution and increase the anodic utilization rate. Quantum chemical calculations indicated that L-cysteine molecules mainly interacted with on the carboxyl groups on the aluminium alloy surface. A strong hybridization occurred between the s-orbital and p-orbital of reactive sites in the L-cysteine molecule and the sp-orbital of Aluminium. - Highlights: • L-cysteine was used as corrosion inhibitor for Al alloy in alkaline solution. • Adsorption of L-cysteine on Al alloy surface obeyed the amended Langmuir's isotherm. • L-cysteine molecules interacted with the carboxyl groups on the Al alloy surface. • A strong orbital hybridization occurred between the reactive sites in L-cysteine and Al.

  5. Some of the properties of plutonium and the aluminium-plutonium alloy

    International Nuclear Information System (INIS)

    Abramson, R.; Boucher, R.; Fabre, R.; Monti, H.

    1959-01-01

    1- Study of the physical properties of plutonium. 1) Study of the allotropy of plutonium. a) Thermal analysis: the apparatus used and the measurement technique are briefly described. The transition point temperatures and the corresponding heats of transformation have been determined. Finally, the results of the particular study of certain transition points are given. b) Dilatometry. The dilatometric analysis of the phase changes of plutonium has been carried out by means of the Chevenard dilatometer with photographic recording. The testing conditions (heating and cooling speeds, isotherm plateaux) have been varied in order to determine accurately the characteristics of each transition, particularly the δ → γ transition on cooling. 2) Micrography of plutonium. For the accurate preparation of metallographic samples the electrolytic polishing must be rapid, which implies a mechanical polishing of excellent quality. Information is given on new attacking reagents which show the structure of the metal very clearly. 2- Study of aluminium-plutonium alloys. Comparative study of Al-Pu and Al-U alloys rich in aluminium. a) Thermal analysis. The liquids and fusion temperatures of the eutectic Al-XAl 4 , have been accurately determined. From the measurement of the heats of fusion the exact composition of the eutectic alloy has been determined. b) Thermal treatments. The eutectic coalescence kinetics have been studied by a micrographic method and by following the evolution of hardness. The results obtained show that the phenomenon is more rapid in Al-Pu alloys than in Al-U alloys. c) Micrographic study of the transition XAl 3 → XAl 4 . The peritectic reaction XAl 3 + liq. → XAl 4 has been suppressed by quenching. The transformation of the XAl 3 phase to the solid phase has been studied as well as the effect of small additions of silicon on the kinetics of this reaction. (author) [fr

  6. SOLIDIFICATION CHARACTERISTIC OF TITANIUM CARBIDE PARTICULATE REINFORCED ALUMINIUM ALLOY MATRIX COMPOSITES

    Directory of Open Access Journals (Sweden)

    N. FATCHURROHMAN

    2012-04-01

    Full Text Available In this research solidification characteristic of metal matrix composites consisted of titanium carbide particulate reinforced aluminium-11.8% silicon alloy matrix is performed. Vortex mixing and permanent casting method are used as the manufacturing method to produce the specimens. Temperature measurements during the casting process are captured and solidification graphs are plotted to represent the solidification characteristic. The results show, as volume fraction of particulate reinforcement is increased, solidification time is faster. Particulate reinforcement promotes rapid solidification which will support finer grain size of the casting specimen. Hardness test is performed and confirmed that hardness number increased as more particulate are added to the system.

  7. Investigation on local ductility of 6xxx-aluminium sheet alloys

    Science.gov (United States)

    Henn, P.; Liewald, M.; Sindel, M.

    2017-09-01

    Within the scope of this paper influence of localization of loading conditions on the ductility of two different 6xxx-aluminium sheet alloys is investigated. In order to improve the prediction of sheet material crash performance, material parameters based on uniaxial tensile and notched tensile tests are determined with varying consolidation areas. Especially evaluation methods based on the localized necking behaviour in tensile tests are investigated. The potential of local ductility characterisation is validated with results of Edge-Compression Tests (ECT) which applies load conditions that occur in actual crash events.

  8. Characterising ductility of 6xxx-series aluminium sheet alloys at combined loading conditions

    Science.gov (United States)

    Henn, Philipp; Liewald, Mathias; Sindel, Manfred

    2017-10-01

    This paper presents a new approach to characterise material ductility when combined, three dimensional loading conditions occurring during vehicle crash are applied. So called "axial crush test" of closed hat sections is simplified by reducing it down to a two-dimensional testing procedure. This newly developed edge-compression test (ECT) provides the opportunity to investigate a defined characteristic axial folding behaviour of a profile edge. The potential to quantify and to differentiate crashworthiness of material by use of new edge-compression test is investigated by carrying out experimental studies with two different 6xxx-aluminium sheet alloys.

  9. Laser assisted cold spraying of aluminium alloy powder on stainless steel substrate

    CSIR Research Space (South Africa)

    Tlotleng, Monnamme

    2012-12-01

    Full Text Available International Conference on Information Warfare and Security, Denver, USA 25-26 March 2013 LASER ASSISTED COLD SPRAYING OF ALUMINIUM ALLOY POWDER ON STAINLESS STEEL SUBSTRATE M. Tlotleng1, 2; E.O. Olakanmi2; C. Meacock; Sisa Pityana1, 3; E.T. Akinlabi2...; M. Shukla2; and M. Doyoyo2 1Department of Mechanical Engineering Science, University of Johannesburg, P.O.Box 524, Auckland Park, 2006, South Africa 2Department of Chemical and Metallurgical Engineering, Tshwane University of Technology...

  10. Bond strength of pressure sensitive adhesives for CFRP aluminium-alloy hybrid beams under impact loading

    Science.gov (United States)

    Sato, C.

    2003-09-01

    This paper discusses the impact absorbing capabilities of CFRP aluminium-alloy hybrid beams bonded with double-coated pressure sensitive adhesive tapes. Two sorts of double-coated adhesive tapes (VHB and SBT, 3M) were used in experiments. The strength and absorbed energy of the beams under impact loading were measured using an instrumented Charpy tester. Using the beams having the different adhesive tapes and the CFRP of different length, the variations of the strength and the absorbed energy were investigated. The beams bonded with VHB showed sufficient strength and absorbed energy. SBT showed also great capability of absorbing impact energy.

  11. Assessment of Fatigue Behavior and Effects of Crack Growth in Aluminium Alloys 6082 Under Various Stress Ratios

    OpenAIRE

    Roundi, Walid; Elgharad, Abdellah

    2016-01-01

    The purpose of this study is to investigate the fatigue behaviour of the aluminium alloy 6082 by a finite element analysis (FEA). The tests are released for various specimens subjected to cyclic tensile loading in order to characterize the damage evolution and the fatigue strength of the aluminium alloy 6082. The results show the Wöhler curves (S-N curves) for the tested specimens under various stress amplitude levels and for different stress ratios values (R=0, R=0.5, R=-1). The obtained dat...

  12. B2-ordered iron-aluminium alloys strengthening. Influence of additions (Ni and B) and microstructure

    International Nuclear Information System (INIS)

    Colas, David

    2004-01-01

    We study the effects of additions (Ni and B) and microstructure on the mechanical behaviour of 40 at. % Al iron-aluminium alloys. From a macroscopic point of view, we show that nickel reinforces FeAl alloys over the whole temperature range, but that it simultaneously leads to emphasize the room temperature brittleness of these alloys through a cleavage stress decrease. We confirm powder metallurgy grain refining interest to enhance yield stress as well as fracture resistance. We show that nickel-induced yield stress effect is additive to 'Hall-Petch' one. Also, we point out that the strengthening phenomena (nickel or grain size) cause the yield stress anomaly, which these alloys usually present, to be hidden. Through a dislocation structures analysis of deformed materials we precise that low temperature nickel-induced solid solution hardening (SSH) cannot be explained on the basis of classical SSH theories but more probably through nickel influence upon the Peierls stress. Moreover, we show that the APB tubes dragging model may be compatible with our microscopic and macroscopic results about the anomaly. Eventually, we put into relation a dynamic super-dislocations multiplication process observation (in situ transmission microscopy) with the nickel-containing alloys tendency to cleavage. (author) [fr

  13. Decomposition in aluminium alloys: diffuse scattering and crystal modelling

    International Nuclear Information System (INIS)

    Aslam-Malik, A.

    1995-01-01

    In the present study the microstructure of metastable precipitates in Al-Ag and Al-Cu, so called pre-precipitates or Guinier-Preston (GP) zones, was investigated. In both systems important aspects of the microstructure are still controversially discussed. In Al-Ag two forms of GP zones are suggested; depending on the aging temperatures above or below about 443 K, ε- or η-zones should evolve. Differences between these two types of zones may be due to differences in internal order and/or composition. In Al-Cu the characterization of GP I zones is difficult because of the strong atomic displacements around the zones. The proper separation of short-range order and displacement scattering within a diffuse scattering experiment is still under discussion. The technique used to determine the short-range order in both alloys was diffuse scattering with neutrons and X-rays. To separate short-range order and displacement scattering, the methods of Georgopoulos-Cohen (X-ray scattering) and Borie-Sparks (neutron scattering) were used. Of main importance is the optimization of the scattering contrast and thus the scattering contribution due to short-range order. Short-range order scattering is rationalized in terms of pair correlations. Crystals may subsequently be modelled to visualize the microstructure. The Al-Ag system was investigated by diffuse X-ray wide-angle scattering and small-angle neutron scattering. The small-angle neutron scattering measurement was necessary since the GP zones in Al-Ag are almost spherical and the main scattering contribution is found close to the origin of reciprocal space. The small-angle scattering is not that important in the case of Al-Cu because the main scattering extends along (100) owing to the planar character of the GP I zones on (100) lattice planes. (author) 24 figs., 10 tabs., refs

  14. Mechanical Behaviour Investigation Of Aluminium Alloy Tailor Welded Blank Developed By Using Friction Stir Welding Technique

    Science.gov (United States)

    Dwi Anggono, Agus; Sugito, Bibit; Hariyanto, Agus; Subroto; Sarjito

    2017-10-01

    The objective on the research was to investigate the mechanical properties and microstructure of tailor welded blank (TWB) made from AA6061-T6 and AA1100 using friction stir welding (FSW) process. Due to the dissimilar mechanical properties of the two aluminium alloys, microhardness test was conducted to measure the hardness distribution across the weld nugget. The mixing of two distinct materials was influenced by tool rotation speed. Therefore, microstructure analysis was carried out to investigate the grain size and shape. The grain size of AA6061-T6 has increased in the heat affected zone (HAZ) while for AA1100 has decreased. In the weld nugget, it has found a hook defects in the dissimilar aluminium joining. By using monotonic tensile load, the different weld line direction was observed with the expansion in tool rotation. The joints failure were consistently on the area of AA1100 series. Furthermore, two specimens were investigated, one through the dissimilar aluminium and the other through similiar material. Inspection of the weld nugget hardness was shown that nonhomogen material intermixing during the stiring process as confirmed by microhardness measurement.

  15. Effect of Lubrication on Sliding Wear of Red Mud Particulate Reinforced Aluminium Alloy 6061

    Directory of Open Access Journals (Sweden)

    N. Panwar

    2017-09-01

    Full Text Available In present study, Red mud, an industrial waste, has been utilized as a reinforcement material to fabricate Aluminium 6061 matrix based metal matrix composite. Taguchi L18 orthogonal array has been employed for fabrication of composite castings and for conducting the tribological experimentation. ANOVA analysis has been applied to examine the effect of individual parameters such as sliding condition: dry and wet, reinforcement weight fraction, load, speed, and sliding distance on specific wear rate obtained experimentally. It has been found that tensile strength and impact energy increases while elongation decreases, with increasing weight fraction and decrease in particle size of red mud. The percentage contribution of the effect of factors on SWR is Sliding condition (73.17, speed (7.84, percentage reinforcement (7.35, load (5.75, sliding distance (2.24, and particle size (1.25. It has also been observed that specific wear rate is very low in wet condition. However, it decreases with increase in weight fraction of reinforcement, decrease in load and sliding speed. Al6061/red mud metal matrix composites have shown reasonable strength and wear resistance. The use of red mud in Aluminium composite provides the solution for disposal of red mud and can possibly become an economic replacement of Aluminium and its alloys.

  16. Microstructure evolution in a 2618 aluminium alloy during creep-fatigue tests

    Energy Technology Data Exchange (ETDEWEB)

    Novy, Frantisek; Hadzima, Branislav [Zilina Univ. (Slovakia). Dept. of Materials Engineering; Janecek, Milos; Kral, Robert [Charles Univ., Prague (Czech Republic). Dept. of Physics of Materials

    2012-06-15

    Microstructure changes in the 2 618 aluminium alloy during creep-fatigue tests were studied. These tests simulate the conditions of the application of this alloy in devices for the exhaustion of hot gasses generated during fire in closed or difficultly accessible areas. Creep-fatigue tests result in high dislocation density in subgrains and narrow subgrain boundaries, in contrast to creep tests reported in our previous work where large subgrains were observed with relatively wide subgrain boundaries and relatively low dislocation density in grains. Extensive precipitation occurred with denuded (precipitate-free) zones along grain boundaries. The coherent S-phase (Al{sub 2}CuMg) transformed into partially coherent needle-shaped S' precipitates. Superior stress amplitude caused reduced lifetime and wider denuded zones. A model of the formation of denuded zones along (sub)-grain boundaries was proposed. (orig.)

  17. Microstructural characterization of fly ash particulate reinforced AA6063 aluminium alloy for aerospace applications

    Science.gov (United States)

    Razzaq, A. M.; Majid, D. L. Abang Abdul; Ishak, M. R.; Uday, M. B.

    2017-12-01

    Aluminium-fly ash (FA) particulate reinforced composites (AA6063-FA) have been used in automotive and aerospace industries because of their low density and good mechanical properties. Three different weight fraction of FA: 2%, 4% and 6% are added to AA6063 alloy using compocasting method. The effect of FA particulates on microstructure, density and compression strength of AA6063- FA composites are investigated. Field Emission Scanning Electron Microscope (FESEM) micrographs reveal that the FA particulates are uniformly distributed in AA6063 alloy. The results also show that density, compression strength and microstructure of the AA6063-FA composites are significantly influenced by the FA amount. The increase in the weight fraction of FA will improve the microstructure and enhance the compression strength. The density of AA6063-FA composites decreases as the incorporation of FA increases.

  18. Relation between feeding mechanisms and solidification mode in 380 aluminium alloy with different iron contents

    International Nuclear Information System (INIS)

    Tovio, D. O.; Gonzalez, A.C.; Mugica, G. W.; Cuyas, J. C.

    2003-01-01

    In the present work the effect of iron (0.15, 0.42 and 0.86%) content in feeding mechanisms for 380 aluminium alloy has been studied. The feeding capacity has been evaluated by a device that produces a barrier removable to allowing the movement of the inter dendritic liquid. The results show the flow of different quantity of liquid, it depends of the temperature of operating the device and of the iron content. For minimum and maximum iron content, the inter dendritic and bursts feeding mechanisms are fundamentally involved, for 0.42% of iron the feeding mechanisms was the inter dendritic. The authors establish this behavior by the solidification mode of alloy, which promotes the presence of particles of Si or plates of b-Al 3 FeDi phase, in the inter dendritic channels and produce the different feeding mechanisms. (Author) 15 refs

  19. Short Fatigue Crack Growth Micromechanisms in a Cast Aluminium Piston Alloy

    Science.gov (United States)

    Mbuya, T. O.; Crump, J.; Sinclair, I.; Soady, K. A.; Thomson, R. C.; Reed, P. A. S.

    The short fatigue crack growth behaviour of a model cast aluminium piston alloy has been investigated. This has been achieved using a combination of fatigue crack replication methods at various intervals during fatigue testing and post-mortem analysis of fracture surfaces and crack profiles. Crack-microstructure interactions have been clearly delineated using a combination of optical microscopy (OM), scanning electron microscopy (SEM) and three dimensional (3D) X-ray microtomography (SRCT). Results show that intermetallic particles play a significant role in determining the crack path and growth rate of short fatigue cracks. It is observed that the growth of short cracks is often retarded or even arrested at intermetallic particles and grain boundaries. Crack deflection at intermetallics and grain boundaries is also frequently observed. These results have been compared with the long crack growth behaviour of the alloy

  20. Evaluating stress corrosion cracking behaviour of high strength AA7075-T651 aluminium alloy

    Science.gov (United States)

    Prabhuraj, P.; Rajakumar, S.; Lakshminarayanan, A. K.; Balasubramanian, V.

    2017-12-01

    The objective of the present study is to determine the threshold stress level of stress corrosion cracking (SCC) in AA7075-T651 aluminium alloy by suitable experimentation. The test was carried out using a circumferential notch specimen in a horizontal-type constant load SCC setup in a 3.5 wt.% NaCl solution. The time to failure by SCC was determined at various loading conditions. The threshold stress of AA7075-T651 alloy was found to be 242 MPa in a 3.5 wt.% NaCl solution. The various regions of the fractured surface specimen such as machined notch, SCC region and final overload fracture area were examined using scanning electron microscopy (SEM) in order to identify the SCC mechanism.

  1. Influence of Process Parameters on the Quality of Aluminium Alloy EN AW 7075 Using Selective Laser Melting (SLM)

    Science.gov (United States)

    Kaufmann, N.; Imran, M.; Wischeropp, T. M.; Emmelmann, C.; Siddique, S.; Walther, F.

    Selective laser melting (SLM) is an additive manufacturing process, forming the desired geometry by selective layer fusion of powder material. Unlike conventional manufacturing processes, highly complex parts can be manufactured with high accuracy and little post processing. Currently, different steel, aluminium, titanium and nickel-based alloys have been successfully processed; however, high strength aluminium alloy EN AW 7075 has not been processed with satisfying quality. The main focus of the investigation is to develop the SLM process for the wide used aluminium alloy EN AW 7075. Before process development, the gas-atomized powder material was characterized in terms of statistical distribution: size and shape. A wide range of process parameters were selected to optimize the process in terms of optimum volume density. The investigations resulted in a relative density of over 99%. However, all laser-melted parts exhibit hot cracks which typically appear in aluminium alloy EN AW 7075 during the welding process. Furthermore the influence of processing parameters on the chemical composition of the selected alloy was determined.

  2. Isoelectronic substitutions and aluminium alloying in the Ta-Nb-Hf-Zr-Ti high-entropy alloy superconductor

    Science.gov (United States)

    von Rohr, Fabian O.; Cava, Robert J.

    2018-03-01

    High-entropy alloys (HEAs) are a new class of materials constructed from multiple principal elements statistically arranged on simple crystallographic lattices. Due to the large amount of disorder present, they are excellent model systems for investigating the properties of materials intermediate between crystalline and amorphous states. Here we report the effects of systematic isoelectronic replacements, using Mo-Y, Mo-Sc, and Cr-Sc mixtures, for the valence electron count 4 and 5 elements in the body-centered cubic (BCC) Ta-Nb-Zr-Hf-Ti high-entropy alloy (HEA) superconductor. We find that the superconducting transition temperature Tc strongly depends on the elemental makeup of the alloy, and not exclusively its electron count. The replacement of niobium or tantalum by an isoelectronic mixture lowers the transition temperature by more than 60%, while the isoelectronic replacement of hafnium, zirconium, or titanium has a limited impact on Tc. We further explore the alloying of aluminium into the nearly optimal electron count [TaNb] 0.67(ZrHfTi) 0.33 HEA superconductor. The electron count dependence of the superconducting Tc for (HEA)Al x is found to be more crystallinelike than for the [TaNb] 1 -x(ZrHfTi) x HEA solid solution. For an aluminum content of x =0.4 the high-entropy stabilization of the simple BCC lattice breaks down. This material crystallizes in the tetragonal β -uranium structure type and superconductivity is not observed above 1.8 K.

  3. Fatigue and heat transfer behaviour of shot penned aluminium alloy for automobile applications

    Energy Technology Data Exchange (ETDEWEB)

    Nadkarni, V.S.; Sharma, M.C. [M.A.C.T., Bhopal (India). Dept. of Mech. Eng.

    2000-07-01

    In the present investigation glass beads and zirconium oxide shots were used as media to shot peening aluminium alloy specimens. Fatigue and boiling heat transfer behaviour of this alloy after shot peening was studied. Out of 0.2N and 0.4N peening intensities, 0.4N gave higher improvement on fatigue strength and boiling heat transfer. Fatigue of butt welded aluminium joints were also studied. Shot peening with zirconium oxide shots at 0.4N intensity was found to be more advantageous than glass beads. Welding reduces 19.4% fatigue strength compared to virgin samples, but shot peening could improve fatigue strength by 12% compared to welded samples. Effect of corrosive (3N Nacl) environment on fatigue strength was also studied. Zir shots were found to be economical. The commercial application of shot peening in automobiles to enhance boiling heat transfer was also studied. The heat transfer media then used was the coolant commonly used in car radiators. That was 95% ethylene glycol with some inhibitor to prevent corrosion. This was a mixture of water and glycol in 3:1 ratio. The optimum surface roughness was 6.2 {mu}m which gave optimum heat transfer at 90% improvement in boiling heat transfer compared to unpeened samples. (orig.)

  4. Investigating the Acid Failure of Aluminium Alloy in 2 M Hydrochloric Acid Using Vernonia amygdalina

    Directory of Open Access Journals (Sweden)

    Olugbenga A. Omotosho

    2012-04-01

    Full Text Available The acid failure of aluminium alloy in 2 M hydrochloric acid solution in the presence of Vernonia amygdalina extract was investigated using gasometric technique. Aluminium alloy coupons of dimension 4 cm by 1 cm were immersed in test solutions of free acid and also those containing extract volumes of 2, 3, 4 and 5 cm3 at ambient temperature for 30 minutes. The volumes of hydrogen gas evolved as a result of the rate of reaction were recorded and analyzed. Analysis revealed that maximum inhibitor efficiency which corresponds to the lowest corrosion rate was obtained at optimum inhibitor volumes of 5 cm3, with reduction in the corrosion rate observed to follow in order of increasing extract volumes. Adsorption study revealed that Temkin isotherm best described the metal surface interaction with the extract phytochemicals, with 12 minutes becoming the best exposure time for the phytochemicals to adsorb to the metal surface at all volumes. Statistical modelling of the corrosion rate yielded an important relationship suitable for estimating corrosion rate values once volumes of the extract is known. Microstructural studies, showed an indirect relationship between crack growth rates and extract volumes, while consistency of the irregular intermetallic phases increases with increasing extract volumes.

  5. Effect of the temperature and the chlorine pressure, over the aluminium chlorides obtained by direct chlorination of the 6061 alloy

    International Nuclear Information System (INIS)

    Alvarez, Fabiola J.; Bohe, Ana E.; Pasquevich, Daniel M.

    2003-01-01

    The aluminium chloride is synthesized by direct chlorination of aluminium, in agreement with the following reaction: Al(s) + 3/2 Cl 2 AlCl 3 (s,g).The present work focuses on the preparation of aluminium chlorides by two methods: (a) Chlorination of 6061 aluminium alloy with gaseous chlorine in sealed containers, filled with different pressures of gas, from 0.8 to 74 Kpa and in the range of temperature between 200 0 and 500 0 C.(b) Chlorination of the same alloy in chlorine flow between 150 0 and 400 0 C.In the sealed systems, the hexahydrated aluminium trichloride predominated over the anhydrous form. For pressures lower than 14 Kpa and temperatures under 250 0 C, the chloride didn't appear.The residues were rich in aluminium, chlorine and magnesium.In the other systems, the anhydrous chloride was found in the areas of the reactor of temperatures above 100 0 C, for all the thermal treatments. The waste was composed by CrCl 3 and AlCl 3 .6H 2 O.The influence of the chlorine pressures and the heating temperature over the characteristics of the product, was studied.The characterization techniques were x-ray diffraction and energy dispersive spectroscopy, and the evolution of the structure was followed by scanning electron microscopy

  6. Effect of plasma electrolytic oxidation on joining of AA 5052 aluminium alloy to polypropylene using friction stir spot welding

    OpenAIRE

    Aliasghari, S.; Ghorbani, M.; Skeldon, P.; Karami, H.; Movahedi, M.

    2017-01-01

    The effect of a plasma electrolytic oxidation (PEO) pre-treatment on joining of AA 5052 aluminium alloy and polypropylene by friction stir spot welding (FSSW) is investigated using lap tensile shear tests. Two surface conditions of the AA 5052 alloy are compared, one with a PEO pre-treatment in a silicate-based electrolyte, another without any pre-treatment. The resultant specimens are examined by high resolution scanning electron microscopy, thermogravimetric analysis and attenuated total re...

  7. Neutralization of the negative influence of iron and silicon on the mechanical properties of aluminium casting alloys

    International Nuclear Information System (INIS)

    Zolotorevsky, V.S.; Axenov, A.A.; Belov, N.A.

    1990-01-01

    In most of casting aluminium alloys iron is a harmful impurity due to the appearance of rough particles with needle, plate or sceleton shapes of intermetallic compounds during crystallization. As a result of it the plasticity, fracture toughness and sometimes the strength are decreased

  8. Experimental and numerical analysis of in- and out- of plane constraint effects on fracture parameters: Aluminium alloy 2024

    Czech Academy of Sciences Publication Activity Database

    Seitl, Stanislav; Hutař, Pavel; García, T.; Canteli, A.

    7 2013, č. 7 (2013), s. 53-64 ISSN 1802-680X Grant - others:Interní podpora AV ČR(CZ) M100411204 Keywords : LELM * stress intensity tensor * constraint * aluminium alloy * plane strain * plane stress Subject RIV: JL - Materials Fatigue, Friction Mechanics

  9. A silanol-based nanocomposite coating for protection of AA-2024 aluminium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Gonzalez, E.; Pavez, J.; Azocar, I.; Zagal, J.H. [Departamento de Quimica de los Materiales, Facultad de Quimica y Biologia, Universidad de Santiago de Chile, Avenida Bernardo O' Higgins 3363, Casilla 40, Correo 33, Santiago (Chile); Zhou, X. [Corrosion and Protection Centre, School of Materials, University of Manchester, Manchester M13 9PL (United Kingdom); Melo, F. [Departamento de Fisica, Facultad de Ciencias, Universidad de Santiago de Santiago de Chile, Avenida Bernardo O' Higgins 3363, Santiago (Chile); Thompson, G.E. [Corrosion and Protection Centre, School of Materials, University of Manchester, Manchester M13 9PL (United Kingdom); Paez, M.A., E-mail: maritza.paez@usach.cl [Departamento de Quimica de los Materiales, Facultad de Quimica y Biologia, Universidad de Santiago de Chile, Avenida Bernardo O' Higgins 3363, Casilla 40, Correo 33, Santiago (Chile)

    2011-09-01

    Highlights: {center_dot} A new silanol-based hybrid coating has been synthesized. {center_dot} The incorporation of CeO{sub 2} and ZrO{sub 2} nanoparticles into the coating greatly improves the corrosion resistance of the coated aluminium alloy. {center_dot} The effectiveness of the coating is increasingly evident for long term exposure to the sodium chloride solution. {center_dot} The silanol-based nanocomposite coatings have self-healing ability. - Abstract: A new hybrid sol-gel type film, composed of tetraethylorthosilicate (TEOS) and tetraocthylorthosilicate (TEOCS), and modified with different nanoparticle systems, has been investigated as a coating for protection of AA-2024-T3 aluminium alloy. The nanoparticle systems considered were either ZrO{sub 2} or CeO{sub 2} or their combination{sub .} The zirconia nanoparticles were prepared from a Zr (IV) propoxide sol (TPOZ), using an organic stabilizer, and the CeO{sub 2} nanoparticles were developed spontaneously after adding cerium nitrate solution to the hybrid sol. The chemical composition and the structure of the hybrid sol-gel films were examined by X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM) and atomic force microscopy (AFM). The corrosion resistance of the coated AA-2024 alloy was examined by potentiodynamic polarization. The results revealed that, for short exposure times in the electrolyte, incorporation of ZrO{sub 2} or CeO{sub 2} nanoparticles in the hybrid film does not provide an increase in the corrosion resistance of the coated AA-2024 alloy. Further, the resistance was significantly reduced by increasing the nanoparticle content. Conversely, by incorporating both nanoparticles (ZrO{sub 2} and CeO{sub 2}), the corrosion resistance of the resulting hybrid films increased slightly. The behavior changed significantly when the coated alloy was exposed to the electrolyte for 5 days. The corrosion resistance of the coatings, unmodified and modified with CeO{sub 2} or Zr

  10. Experimental Evaluation of Springback in Aluminium Alloys Using Optical Measurement and Numerical Analysis

    Science.gov (United States)

    Bhattacharya, R.; Stanton, M.; Dargue, I.; Aylmore, R.; Williams, G.

    2011-05-01

    The aim of this paper is to establish an efficient and effective means of understanding the springback behaviour of a 5xxx-O and a 6xxx-T61 series aluminium alloy. The tooling used for investigating the springback is a small U-channel stamping draw die using two die radii of 8 or 12 mm and a punch radius of 12 mm. The samples were drawn to depths of 50 or 75 mm with a minimum of 5 samples being drawn for each condition. The U-channel samples were then evaluated using an optical scanning technique and the springback values were calculated using a numerical analysis as developed by one of the authors. The comparison of the sidewall springback, sidewall curl and flange springback under different conditions is conducted and the effect of the draw depth and die radius on the final springback is shown. Statistical analyses of both the drawing condition and the scanning technique are conducted to understand the effect of process variation on the results obtained. The 6xxx series shows higher springback values when compared to 5xxx series alloy. An increase in drawing depth suggests higher springback for both the alloys.

  11. Characterization of semi-solid processing of aluminium alloy 7075 with Sc and Zr additions

    Energy Technology Data Exchange (ETDEWEB)

    Rogal, Ł., E-mail: l.rogal@imim.pl [Institute of Metallurgy and Materials Science of the Polish Academy of Sciences, 25 Reymonta St., 30-059 Krakow (Poland); Dutkiewicz, J. [Institute of Metallurgy and Materials Science of the Polish Academy of Sciences, 25 Reymonta St., 30-059 Krakow (Poland); Atkinson, H.V. [The University of Leicester, Department of Engineering University Road, Leicester, LE1 7RH (United Kingdom); Lityńska-Dobrzyńska, L.; Czeppe, T. [Institute of Metallurgy and Materials Science of the Polish Academy of Sciences, 25 Reymonta St., 30-059 Krakow (Poland); Modigell, M. [RWTH Aachen—Department of Mechanical Process Engineering, 55 Templergraben St., Aachen (Germany)

    2013-09-15

    For thixoforming (semi-solid processing) it is necessary to have a fine globular microstructure in a semi-solid range. Here this has been obtained for 7075 aluminium alloy by addition of modifying agents: 0.5 weight % of scandium and zirconium. The thixoforming process was carried out at 632 °C which gave about 23 volume % of liquid phase. The microstructure of the thixo-formed part (a rotor) consisted of globular grains surrounded by precipitates of secondary phase. The average hardness of thixo-formed parts was 105 HV{sub 5} and the tensile strength 300 MPa. T6 heat treatments were performed with solutionisation at 450 °C for 30 min and 10 h. In both cases the ageing time was set as 18 h at 120 °C. The heat treatments led to an increase in average tensile strength up to 495 MPa. Transmission Electron Microscopy (TEM) analysis enabled the identification of precipitates of the metastable dispersoids of L1{sub 2}–Al{sub 3} (Zr, Sc) and η′ (MgZn{sub 2}) phases in the alloy after the thixoforming and T6 treatment. The measurements of rheological properties of 7075Al alloy with Sc and Zr additions in the semi-solid range indicated an increase of particle size and spheroidization leading to an observable decrease of viscosity during isothermal shearing. A shear rate jump experiment showed that with increasing shear rate the viscosity rapidly falls.

  12. Influence of friction stir welding parameters on properties of 2024 T3 aluminium alloy joints

    Directory of Open Access Journals (Sweden)

    Eramah Abdsalam M.

    2014-01-01

    Full Text Available The aim of this work is to analyse the process of friction stir welding (FSW of 3mm thick aluminium plates made of high strength aluminium alloy - 2024 T3, as well as to assess the mechanical properties of the produced joints. FSW is a modern procedure which enables joining of similar and dissimilar materials in the solid state, by the combined action of heat and mechanical work. This paper presents an analysis of the experimental results obtained by testing the butt welded joints. Tensile strength of the produced joints is assessed, as well as the distribution of hardness, micro-and macrostructure through the joints (in the base material, nugget, heat affected zone and thermo-mechanically affected zone. Different combinations of the tool rotation speed and the welding speed are used, and the dependence of the properties of the joints on these parameters of welding technology is determined. [Projekat Ministarstva nauke Republike Srbije, br. TR 34018 i br. TR 35006

  13. Radiographic and ultrasonic testings of welded joints of 6063 aluminium alloy

    International Nuclear Information System (INIS)

    Oliveira e Silva Mury, A.G. de.

    1980-05-01

    A study on evaluation of weld defects in aluminium butt joints was made in a comparative way through the radiographic and ultrasonic testing. This work was conducted with pipes 5 IPS (6,35 mm thickness) of 6063 aluminium alloy, circumferential TIG welded, due to the difficulty on performing non-destructive testing with this schedule. It was concluded thta ultrasonic testing has adequate sensitivity when setting gain adjustment is made with aid of a reference curve constructed by using a Reference Block (among others studied) with 1,5 mm dia. Hole as reference reflector, and a 5 MHz angle beam search-unit. In this case the ultrasonic testing is more accurate than radiographic testing to detect planar defects like lack of fusion and lack of penetration. Defect sizing by ultrasonic methods employed were 6 and 20 dB drop methods. In spite of your observed limitations concerning the establishment of the real size of defects, the procedure applied was precise for locate and define the weld defects that where found in this study. (author) [pt

  14. Tribological Behaviour of W-DLC against an Aluminium Alloy Subjected to Lubricated Sliding

    Directory of Open Access Journals (Sweden)

    S. Bhowmick

    2015-09-01

    Full Text Available Diamond like carbon (DLC coatings mitigate aluminium adhesion and reduce friction under the ambient conditions but their tribological behaviour under lubricated sliding need to be further investigated. In this study, tribological tests were performed to evaluate the friction and wear characteristics of W-DLC and H-DLC coatings sliding against an aluminium alloy (319 Al under unlubricated (40 % RH and lubricated sliding conditions. For unlubricated sliding, coefficient of friction (COF values of H-DLC and W-DLC were 0.15 and 0.20. A lower COF value of 0.11 was observed when W-DLC was tested using lubricant oil incorporating sulphur while the H-DLC’s COF remained almost unchanged. The mechanisms responsible for the low friction of W-DLC observed during lubricated sliding were revealed by studying the compositions of the coating surfaces and the transfer layers formed on 319 Al. Micro-Raman spectroscopy indicated that the transfer layers formed during lubricated sliding of W-DLC incorporated tungsten disulphide (WS2.

  15. Circular economy: To be or not to be in a closed product loop? A Life Cycle Assessment of aluminium cans with inclusion of alloying elements

    OpenAIRE

    Niero, Monia; Olsen, Stig Irving

    2016-01-01

    Packaging, representing the second largest source of aluminium scrap at global level, deserves a key role in the transition towards the circular economy. Life Cycle Assessment (LCA) of aluminium products has been typically based on one life cycle considering pure aluminium flows and neglecting the presence of alloying elements and impurities. However, this simplification undermines the potentials of using LCA to quantify the environmental performances of products in multiple loops, as require...

  16. Analysis of the strain behaviour of a friction stir processed superplastic aluminium alloy

    Directory of Open Access Journals (Sweden)

    Sorgente Donato

    2015-01-01

    Full Text Available Superplastic forming is a well-established process by which very large, very complex shaped and also multi-sheets components can be manufactured in a single step. Combining this process with a suitable joining technique is of great industrial interest. In this work the strain behaviour of a friction stir processed aluminium alloy was investigated through free inflation tests. Principal parameters of the friction stir process were changed and free inflation tests were performed to assess the formability of the processed sheet. A strong influence of the friction stir process parameters was recorded on the formability of the processed material. Only a specified set of parameters assured a strain behaviour close to the one of the base material.

  17. Material Characterization of Dissimilar Friction Stir Spot Welded Aluminium and Copper Alloy

    Science.gov (United States)

    Sanusi, K. O.; Akinlabi, E. T.

    2017-08-01

    In this research study, material characterization of dissimilar friction stir spot welded Aluminium and Copper was evaluated. Rotational speeds of 800 rpm and transverse speeds of 50 mm/min, 150 mm/min and 250 mm/min were used. The total numbers of samples evaluated were nine altogether. The spot welds were characterised by microstructure characterization using optical microscope (OEM) and scanning electron microscopy technique (SEM) by observing the evolution of the microstructure across the weld’s cross-section. lap-shear test of the of the spot weld specimens were also done. From the results, it shows that welding of metals and alloys using Friction stir spot welding is appropriate and can be use in industrial applications.

  18. Microstructure of friction stir welded joints of 2017A aluminium alloy sheets.

    Science.gov (United States)

    Mroczka, K; Dutkiewicz, J; Pietras, A

    2010-03-01

    The present study examines a friction stir welded 2017A aluminium alloy. Transmission electron microscope investigations of the weld nugget revealed the average grain size of 5 microm, moderate density of dislocations as well as the presence of nanometric precipitates located mostly in grains interiors. Scanning electron microscope observations of fractures showed the presence of ductile fracture in the region of the weld nugget with brittle precipitates in the lower part. The microhardness analysis performed on the cross-section of the joints showed fairly small changes; however, after the artificial ageing process an increase in hardness was observed. The change of the joint hardness subject to the ageing process indicates partial supersaturation in the material during friction stir welding and higher precipitation hardening of the joint.

  19. Microstructural evolution and properties of friction stir welded aluminium alloy AA2219

    International Nuclear Information System (INIS)

    Gupta, R. K.; Biju, S.; Ghosh, B. R.; Sinha, P. P.

    2007-01-01

    Low weld strength of fusion welded joints of aluminium alloy AA2219 is a concern in fabrication of pressure vessels and is attributable to the presence of weld defects, as well as various metallurgical factors. Friction stir welding (FSW), being a solid state joining process has obvious advantages over fusion welding. Results of preliminary FSW experiments conducted on 10 mm thick plate using a particular tool configuration are presented here. Microscopic studies show the presence of very fine equiaxed recrystallised grain at the weld nugget and a flow pattern of grains due to heavy deformation in defect-free weld coupons. Mechanical properties are correlated with the microstructure and process variables. Fractographic analysis complements the observations of optical microscopy and mechanical properties

  20. Neutron-activation analysis of phosphorus in aluminium-silicon alloys

    International Nuclear Information System (INIS)

    Rajchev, Kh.

    1976-01-01

    Silicon-aluminium alloy samples weighing about 50 mg are irradiated in a nuclear reactor with a neutron flow of 5x10 12 neutrons, cm -2 .s -1 . After a period of one week for decay of the short-lived isotopes, the sample is dissolved in a mixture of nitric and hydrofluoric acid. It is neutralized up to pH 2,5 and the present radioactive two- and three-valent cations are sorbed on chelating ion exchange resin Dowex A1. An ammonium phosphate standard is irradiated in parallel with the sample for qualitative determinations. The quantity of phosphorus is measured in aliquots from the sample and the standard with a liquid counter. The method proposed for separating and determining the phosphorus in silumins ensures practically the full separation of phosphorus (98,5 +- 0,5 %) and a precise determination of microquantities of the element - up to 10 -10 g. (author)

  1. Microscopic Study of 5083-H321 Aluminium Alloy Under Fretting Fatigue Condition

    International Nuclear Information System (INIS)

    Eslamian, S; Sahari, B B; Ali, Aidy; Mahdi, El-Sadiq; Hamouda, A M

    2011-01-01

    Fretting occurs where there is small amplitude oscillating motion between solid surfaces in contact. With even small loads or prolonged operation, fretting may lead to crack initiation followed by fretting fatigue. Its effect on fatigue is to speed up the nucleation of fatigue surface cracks and it can be extremely damaging. Fretting fatigue is a critical concern in aircraft structures and a widespread problem in naval structural components and is often the root cause of fatigue crack nucleation in machine components. In this investigation, fretting fatigue study is carried out using 5083-H321 marine/ aerospace aluminium alloy. The test rig and the experiments were designed with an emphasis to study the crack initiation behaviour in the fretted region using scanning electron microscope (SEM). Fretting damage and its relationship to the fretting fatigue life are presented and discussed.

  2. Microscopic study of 5083-H321 Aluminium alloy under fretting fatigue condition

    International Nuclear Information System (INIS)

    Eslamian, S.; Sahari, B.B.; Aidy Ali; El-Sadiq, M.; Hamouda, A.M.

    2009-01-01

    Full text: Fretting occurs where there is small amplitude oscillating motion between solid surfaces in contact. With even small loads or prolonged operation, fretting may lead to crack initiation followed by fretting fatigue. Its effect on fatigue is to speed up the nucleation of fatigue surface cracks and it can be extremely damaging. Fretting fatigue is a critical concern in aircraft structures and a widespread problem in naval structural components and is often the root cause of fatigue crack nucleation in machine components. In this investigation, fretting fatigue study is carried out using 5083-H321 marine/ aerospace aluminium alloy. The test rig and the experiments were designed with an emphasis to study the crack initiation behaviour in the fretted region using scanning electron microscope (SEM). The damages produced by fretting and its relationship to the fretting fatigue life are discussed in the paper in some depth. (author)

  3. Fatigue behaviour of post weld heat treated electron beam welded AA2219 aluminium alloy joints

    International Nuclear Information System (INIS)

    Malarvizhi, S.; Raghukandan, K.; Viswanathan, N.

    2008-01-01

    This paper reports the effect of post weld heat treatment on fatigue behaviour of electron beam welded AA2219 aluminium alloy. An attempt has been made to enhance the fatigue strength of the electron beam welded joints through post weld heat treatment methods such as solution treatment, artificial aging, solution treatment and artificial aging. Electron beam welding machine with 100 kV capacity has been used to fabricate the square butt joints. Servo hydraulic controlled fatigue testing machine with a capacity of 100 kN has been used to evaluate the fatigue life of the welded joints. Of the three post weld heat treated joints, the solution treated and aged joints are enduring higher number of cycles under the action of cyclic loads

  4. Microscopic Study of 5083-H321 Aluminium Alloy Under Fretting Fatigue Condition

    Energy Technology Data Exchange (ETDEWEB)

    Eslamian, S; Sahari, B B [Institute Advanced Technology, Universiti Putra Malaysia 43400 Serdang, Selangor (Malaysia); Ali, Aidy [Department of Mechanical and Manufacturing Engineering Faculty of Engineering, Universiti Putra Malaysia 43400 Serdang, Selangor (Malaysia); Mahdi, El-Sadiq; Hamouda, A M, E-mail: saeed.eslamian@gmail.com [Mechanical and Industrial Engineering Department, College of Engineering, Qatar University 2713 Doha (Qatar)

    2011-02-15

    Fretting occurs where there is small amplitude oscillating motion between solid surfaces in contact. With even small loads or prolonged operation, fretting may lead to crack initiation followed by fretting fatigue. Its effect on fatigue is to speed up the nucleation of fatigue surface cracks and it can be extremely damaging. Fretting fatigue is a critical concern in aircraft structures and a widespread problem in naval structural components and is often the root cause of fatigue crack nucleation in machine components. In this investigation, fretting fatigue study is carried out using 5083-H321 marine/ aerospace aluminium alloy. The test rig and the experiments were designed with an emphasis to study the crack initiation behaviour in the fretted region using scanning electron microscope (SEM). Fretting damage and its relationship to the fretting fatigue life are presented and discussed.

  5. Mechanical spectroscopy of thermal stress relaxation in aluminium alloys reinforced with short alumina fibres

    Energy Technology Data Exchange (ETDEWEB)

    Carreno-Morelli, E.; Schaller, R. [Ecole Polytechnique Federale, Lausanne (Switzerland). Inst. de Genie Atomique; Urreta, S.E.

    1998-05-01

    The mechanical behaviour under low temperature thermal cycling of aluminium-based composites reinforced with short Al{sub 2}O{sub 3} SAFFIL fibres has been investigated by mechanical spectroscopy (mechanical loss and elastic shear modulus measurements). A mechanical loss maximum has been observed during cooling which originates in the relaxation of thermal stresses at the interfaces due to the differential thermal expansion between matrix and reinforcement. The maximum height increases with the volumetric fibre content. In addition, if the matrix strength is increased by the appropriated choice of alloy and thermal treatment, the maximum diminishes and shifts to lower temperatures. No damage accumulation at the interfaces has been detected during long period thermal cycling in the range 100 to 500 K. A description of the damping behaviour is made in terms of the development of microplastic zones which surround the fibres. (orig.) 9 refs.

  6. D.C. Casting of Aluminium Alloys — Past, Present and Future

    Science.gov (United States)

    Schneider, Wolfgang

    The principles of D.C. casting of aluminium alloys were invented in 1936. Due to the importance of this process to the industry for the fabrication of semi-finished products intensive development work has taken place over the last 30 years. Increasing demands on ingot quality necessitated the development of innovative casting technologies. This has led, for example, to the introduction of air-assisted hot top moulds for the casting of extrusion ingots and electro-magnetic moulds for the casting of rolling ingots. Further techniques and tools were also developed to optimize the use of modern mould techniques and to increase the safety and reliability of the D.C. casting process. A review will be given of the history of D.C, casting and the state of the art of the process concerning casting technologies and ingot quality. Finally, future development trends and challenges will be discussed.

  7. Strain rate effects on mechanical properties in tension of aluminium alloys used in armour applications

    Science.gov (United States)

    Cadoni, E.; Dotta, M.; Forni, D.; Bianchi, S.; Kaufmann, H.

    2012-08-01

    The mechanical properties in tension of two aluminium alloys (AA5059-H131 and AA7039-T651) used in armour applications were determined from tests carried out over a wide range of strain-rates on round specimens. The experimental research was developed in the DynaMat laboratory of the University of Applied Sciences of Southern Switzerland. The target strain rates were set at the following four levels: 10-3, 30, 300 and 1000s-1. The quasi-static tests were performed with a universal electromechanical machine, whereas a hydro-pneumatic machine and a Split Hopkinson Tensile Bar apparatus were used for medium and high strain-rates respectively. The required parameters by the Johnson-Cook constitutive law were also determined.

  8. Studies of the Action of Grain-Refining Particles in Aluminium Alloys

    Science.gov (United States)

    Schumacher, P.; Greer, A. L.

    Crystallization from a melt and from a metallic glass both occur in an undercooled liquid. In this way identical nucleation mechanisms can operate in the two cases. However, in metallic glasses, unlike conventional solidification at low undercooling, the low atomic mobility permits the resolution and microscopical study of nucleation processes on added particles. Conventional aluminium grain-refiner based on Al-Ti-B has been used to obtain nucleant particles embedded in a glassy matrix of Al85Y8Ni5Co2 (at%). During crystallization from the glassy state, nucleation and growth of α-Al can be observed on TiB2 particles coated with a layer of Al3Ti Empirical relations found in casting practice of Al-alloys, such as excess Ti necessary for grain refinement, can be related to the observed nucleation mechanism, which is found to be very sensitive to both crystallographic and chemical factors.

  9. Multi response optimization of wire-EDM process parameters of ballistic grade aluminium alloy

    Directory of Open Access Journals (Sweden)

    Ravindranadh Bobbili

    2015-12-01

    Full Text Available In the current investigation, a multi response optimization technique based on Taguchi method coupled with Grey relational analysis is planned for wire-EDM operations on ballistic grade aluminium alloy for armour applications. Experiments have been performed with four machining variables: pulse-on time, pulse-off time, peak current and spark voltage. Experimentation has been planned as per Taguchi technique. Three performance characteristics namely material removal rate (MRR, surface roughness (SR and gap current (GC have been chosen for this study. Results showed that pulse-on time, peak current and spark voltage were significant variables to Grey relational grade. Variation of performance measures with process variables was modelled by using response surface method. The confirmation tests have also been performed to validate the results obtained by Grey relational analysis and found that great improvement with 6% error is achieved.

  10. Finite element modelling of deformation behaviour in incremental sheet forming of aluminium alloy

    Directory of Open Access Journals (Sweden)

    Huang Tsung-Han

    2015-01-01

    Full Text Available In this paper, the finite element method (FEM is used to study the incremental sheet forming process of pyramidal shape. The material used is aluminium alloy 5052. The tool, a hemispherical ball-head with a diameter (d = 4 mm made of HSS tool steel, is used to press down on the sheet metal causing locally plastic deformation. The comparison between spiral tool path, spiral-step tool path and z-level tool path is carried out. Moreover, the final thickness distribution is investigated. The results indicate that the minimal thickness can be found on the corner of wall angle in SPIF process. Under the same step over, spiral-step tool path can obtain the deepest depth for pyramidal shape. The maximum formability for successful forming of the pyramidal shape with depth 60 mm is wall angles 65∘.

  11. Hybrid Ti-MoS2 Coatings for Dry Machining of Aluminium Alloys

    Directory of Open Access Journals (Sweden)

    Tomasz L. Brzezinka

    2017-09-01

    Full Text Available Combinatorial deposition, comprising filtered cathodic vacuum arc (FCVA and physical vapor deposition (PVD magnetron sputtering is employed to deposit molybdenum disulphide (MoS2 and titanium (Ti thin films onto TiB2-coated tool inserts specifically designed for the dry machining of aluminium alloys. Titanium is deposited by FCVA while MoS2 is magnetron sputtered. The deposition set up allows several compositions of Ti-MoS2 to be deposited simultaneously, with Ti content ranging between 5 and 96 at. %, and their machining performances to be evaluated. Milling took place using a CNC Vertical Machining Center at a 877 mm/min feed rate. The effect of different coating compositional ratios on the degree of aluminium sticking when a milling insert is used to face mill an Al alloy (SAE 6061 was investigated using a combination of energy-dispersive X-ray spectroscopy (EDX and X-ray photoelectron spectroscopy (XPS analysis. XPS studies suggest that the greater degree of Al sticking on the rake face of the inserts is due to the formation of greater amounts of non-protective Ti-O phases. EDX mapping of the milling inserts after machining reveal that a Ti:MoS2 ratio of around 0.39 prevents Al from sticking to the tool edges. Since we prevent Al from sticking to the tool surface, the resultant machined surface finish is improved thus validating the machining performance of TiB2-coated tools using optimum compositions of Ti:MoS2 thin film coatings.

  12. Fracture mechanisms of aluminium alloy AA7075-T651 under various loading conditions

    International Nuclear Information System (INIS)

    Pedersen, Ketill O.; Borvik, Tore; Hopperstad, Odd Sture

    2011-01-01

    The fracture behaviour of the aluminium alloy AA7075-T651 is investigated for quasi-static and dynamic loading conditions and different stress states. The fracture surfaces obtained in tensile tests on smooth and notched axisymmetric specimens and compression tests on cylindrical specimens are compared to the fracture surfaces that occur when a projectile, having either a blunt or an ogival nose shape, strikes a 20 mm thick plate of the aluminium alloy. The stress state in the impact tests is much more complex and the strain rate significantly higher than in the tensile and compression tests. Optical and scanning electron microscopes are used in the investigation. The fracture surface obtained in tests with smooth axisymmetric specimens indicates that the crack growth is partly intergranular along the grain boundaries or precipitation free zones and partly transgranular by void formation around fine and coarse intermetallic particles. When the stress triaxiality is increased through the introduction of a notch in the tensile specimen, delamination along the grain boundaries in the rolling plane is observed perpendicular to the primary crack. In through-thickness compression tests, the crack propagates within an intense shear band that has orientation about 45 o with respect to the load axis. The primary failure modes of the target plate during impact were adiabatic shear banding when struck by a blunt projectile and ductile hole-enlargement when struck by an ogival projectile. Delamination and fragmentation of the plates occurred for both loading cases, but was stronger for the ogival projectile. The delamination in the rolling plane was attributed to intergranular fracture caused by tensile stresses occurring during the penetration event.

  13. Microstructures in the 6060 aluminium alloy after various severe plastic deformation treatments

    International Nuclear Information System (INIS)

    Adamczyk-Cieslak, Boguslawa; Mizera, Jaroslaw; Kurzydlowski, Krzysztof Jan

    2011-01-01

    This paper presents the results concerning the microstructural refinement of the industrial 6060 aluminium alloy processed by severe plastic deformation (SPD). The high level of plastic deformation was achieved using the three methods: hydrostatic extrusion (HE), equal channel angular extrusion (ECAE) and extrusion torsion (ET), which differed in the dynamics of the loading, intensity and homogeneity of the plastic strain field. Microstructure analyses were performed before and after SPD deformation using a transmission (TEM) and a scanning electron microscope (SEM). The refined microstructures were examined qualitatively and quantitatively by the stereological methods and computer image analyses. The microstructure of the industrial 6060 aluminium alloy after deformation was characterized by an average grain size of about 0.4 μm. The results show that the precipitates strongly affect the degree of refinement and the mechanism of microstructural transformations. During the SPD, the second phase particles break apart and homogenize. The HE method generates the largest increase of the volume fraction of the small primary particles. Moreover, the HE process is most effective in reducing the primary particle size. During HE and ECAE processes the second phase precipitates dissolve partially and change their shape. - Research Highlights: → SPD results in a significant increase in the density of the small primary particles. → SPD homogenizes the particle size distribution. → HE and ECAE processes bring nano-grains in the vicinity of the primary particles. → HE and ECAE processing results in the β' precipitates partial dissolutions. → During HE and ECAE processes the β' particles change their shape.

  14. High temperature oxidation of copper and copper aluminium alloys: Impact on furnace side wall cooling systems

    Science.gov (United States)

    Plascencia Barrera, Gabriel

    The high temperature oxidation behaviours of copper and dilute Cu-Al alloys were investigated. Experiments were carried out by: (i) Oxidizing under various oxygen potentials at different temperatures using a combined TG-DTA apparatus. (ii) Oxidizing in a muffle furnace (in air) at different temperatures for extended periods of time. The oxidation mechanisms were evaluated based upon the kinetic data obtained as well as by X-ray diffraction and microscopical (SEM and optical) analyses. It was found that oxidation of copper strongly depends on the temperature. Two distinct mechanisms were encountered. Between 300 and 500°C, the oxidation rate is controlled by lateral growth of the oxide on the metal surface, whereas between 600 and 1000°C oxidation is controlled by lattice diffusion of copper ions through the oxide scale. On the other hand, the partial pressure of oxygen only has a small effect on the oxidation of copper. Alloy oxidation is also dependent on the temperature. As temperature increases, more aluminium is required to protect copper from being oxidized. It was shown that if the amount of oxygen that dissolves in the alloy exceeds the solubility limit of oxygen in copper, an internal oxidation layer will develop, leading to the formation of a tarnishing scale. On the other hand if the oxygen content in the alloy lies below the solubility limit of oxygen in copper, no oxidation products will form since a tight protective alumina layer will form on the alloy surface. Surface phenomena may affect the oxidation behaviour of dilute Cu-Al alloys. Immersion tests in molten copper matte and copper converting slag, using laboratory scale cooling elements with various copper based materials, were conducted. Results from these tests showed that alloying copper with 3 to 4 wt% Al decreases the oxidation rate of pure copper by 4 orders of magnitude; however due to a significant drop in thermal conductivity, the ability to extract heat is compromised, leading to

  15. Oxidation of an aluminium-magnesium alloy in liquid state. Methodology of determination of mechanisms from not necessarily repeatable experiments

    International Nuclear Information System (INIS)

    Surla, Karine

    1998-01-01

    This research thesis reports the study of the oxidation of an aluminium-5 pc magnesium alloy in its liquid state in an oxygen environment, using thermogravimetric analysis and that of magnesium in its solid state. In a first part, the author reports a thermodynamic and bibliographical study on magnesium transformation in its solid state (Mg/O 2 and Mg/H 2 O systems, transformation with dry and humid synthetic air, oxidation inhibitors) and on Al-Mg alloy transformation in presence of oxygen (thermodynamic properties of aluminium-rich Al-Mg alloys, Al-Mg/O 2 /N 2 and Al-Mg/O 2 /N 2 /H 2 O systems). The next parts address the selection of reaction systems for the different cases (oxidation of solid magnesium in oxygen, oxidation of the Al-Mg alloy in oxygen), the modelling of the formation of magnesia from solid magnesium and from the Al-Mg alloy, and the modelling of the liquid Al-Mg A5182 alloy oxidation in oxygen [fr

  16. Neutron and synchrotron measurements of residual strain in TIG welded aluminium alloy 2024

    International Nuclear Information System (INIS)

    Owen, R.A.; Preston, R.V.; Withers, P.J.; Shercliff, H.R.; Webster, P.J.

    2003-01-01

    Tungsten inert gas (TIG) welding is one method of joining aluminium alloys with potential application in the aerospace industry. However, for it to be seriously considered as an alternative to mechanical fasteners the interrelated problems of residual stress and distortion need to be addressed. In this paper neutron, laboratory and synchrotron X-ray diffraction methods are used to provide non-destructive information about the residual stress field in TIG-welded 2024 Al alloy. The results compare well despite the differing penetration and sampling volumes associated with each technique. It is found that the magnitudes of the tensile longitudinal stresses decrease along the plate due to progressive heating up of the plate ahead of the arc during welding, so that steady-state conditions are not achieved. Comparison of the data with a finite element model indicates that softening of the heat-affected region must be included to simulate the resulting stress field. The FE model is found to be in good agreement with the data especially in the vicinity of the weld slope-out

  17. Study of microstructural evolutions of the 6061-T6 aluminium alloy under irradiation

    International Nuclear Information System (INIS)

    Flament, Camille

    2015-01-01

    The 6061-T6 Aluminium alloy, whose microstructure contains Al(Fe,Mn,Cr)Si dispersoids and hardening needle-shaped β'' precipitates (Mg, Si), has been chosen as the structural material for the core vessel of the Material Testing Jules Horowitz Nuclear Reactor. Because it will be submitted to high neutron flux at a temperature around 50 C, it is necessary to study microstructural evolutions induced by irradiation and especially the stability of the second phase particles. In this work, an analytical study by in-situ and ex-situ electron and ion irradiations has been performed, as well as a study under neutron irradiation. The precipitate characterization by Transmission Electron Microscopy demonstrates that Al(Fe,Mn,Cr)Si dispersoids are driven under irradiation towards their equilibrium configuration, consisting of a core/shell structure, enhanced by irradiation, with a (Fe, Mn) enriched core surrounded by a Cr-enriched shell. In contrast, the (Mg,Si) β'' precipitates are destabilized by irradiation. They dissolve under ion irradiation in favor of a new precipitation of (Mg,Si,Cu,Cr,Al) rich clusters resulting in an increase of the alloy's hardness. β'' precipitates tend towards a transformation to cubic precipitates under neutron irradiation. (author) [fr

  18. Oxide growth on aluminium alloys in the presence of ammonium fluoborate

    International Nuclear Information System (INIS)

    Oliver, J.; Paterson, P.; Flavell, T.; Biddle, G.

    1996-01-01

    The aim of this study as to determine the mechanisms involved in using ammonium fluoborate as a reducing atmosphere when preheating a high magnesium content aluminium alloy. Rutherford Backscattering (RBS) has been the major technique used in the analysis of samples, it revealed significant reduction in both the diffusion of magnesium to the surface and the calculated oxide thickness in the presence of NH 4 BF 4 . At temperatures above 500 deg C in air, SEM images revealed depressions and voids due to incipient melting at various stages, around the grain boundaries. Grain boundaries effectively acted as pipes aiding the diffusion of magnesium to the surface. These results have been verified through compositional analysis with both RBS and auger electron spectroscopy (AES). Results from NH 4 BF 4 atmosphere preheat conditions showed significant improvements. It was verified experimentally that above 500 deg C , AA5182 alloys undergo incipient melting at the grain boundaries with magnesium diffusing through to the surface. 5 refs., 1 fig

  19. Oxide growth on aluminium alloys in the presence of ammonium fluoborate

    Energy Technology Data Exchange (ETDEWEB)

    Oliver, J.; Paterson, P.; Flavell, T. [Royal Melbourne Inst. of Tech., VIC (Australia); Biddle, G. [Alcoa Rolled Products (Australia)

    1996-12-31

    The aim of this study as to determine the mechanisms involved in using ammonium fluoborate as a reducing atmosphere when preheating a high magnesium content aluminium alloy. Rutherford Backscattering (RBS) has been the major technique used in the analysis of samples, it revealed significant reduction in both the diffusion of magnesium to the surface and the calculated oxide thickness in the presence of NH{sub 4}BF{sub 4}. At temperatures above 500 deg C in air, SEM images revealed depressions and voids due to incipient melting at various stages, around the grain boundaries. Grain boundaries effectively acted as pipes aiding the diffusion of magnesium to the surface. These results have been verified through compositional analysis with both RBS and auger electron spectroscopy (AES). Results from NH{sub 4}BF{sub 4} atmosphere preheat conditions showed significant improvements. It was verified experimentally that above 500 deg C , AA5182 alloys undergo incipient melting at the grain boundaries with magnesium diffusing through to the surface. 5 refs., 1 fig.

  20. Modeling and Simulating Material Behavior during Hot Blank - Cold Die (HB-CD) Stamping of Aluminium Alloy Sheets

    Science.gov (United States)

    Zhang, Nan; Abu-Farha, Fadi

    2016-08-01

    Hot blank - cold die (HB-CD) stamping, non-isothermal hot stamping, of aluminium alloy sheets offers great opportunities for high production rates at low cost, while overcoming limited material formability issues. Yet developing an accurate model that can describe the complex material behavior over the wide ranging conditions of HB-CD stamping (temperatures ranging between 25 and 350 °C) is challenging. Moreover, validation of the developed models under transient conditions is problematic. This work presents he results of a comprehensive characterization, material modeling, FE simulation and experimental validation effort to capture the behavior of an aluminium alloy sheet during HB-CD stamping. In particular, we highlight the integration between temperature measurements (thermography) and strain measurements (digital image correlation) for the accurate validation of model predictions of non-isothermal material deformation.

  1. Probabilistic thermal-mechanical fatigue criterion for lost foam casting aluminium alloys based on 2D/3D porosities distribution

    Directory of Open Access Journals (Sweden)

    Szmytka F.

    2014-06-01

    Full Text Available A thermal-mechanical fatigue criterion is proposed to assess the lifetime of aluminium alloys produced by a lost foam casting process. It is based on the observed size distribution of pores sizes which are considered as critical zones for cracks initiation and gives reliable results when both pores sizes are identified from X-ray tomography and mean stresses are taken into account. Lifetime probabilities are finally successfully compared with experimental results.

  2. Evaluation of the performance of coated and uncoated carbide tools in drilling thick CFRP/aluminium alloy stacks

    OpenAIRE

    MONTOYA , Maxime; CALAMAZ , Madalina; GEHIN , Daniel; GIROT , Franck

    2013-01-01

    This paper aims to establish the wear mechanisms of coated and uncoated tungsten carbide drills when drilling carbon fibre reinforced plastics (CFRP)/aluminium alloy (Al) stacks. During the drilling experiments, thrust forces were measured. A scanning electron microscope (SEM) and a numerical microscope, provided with a scanning device, were periodically used to analyse tool wear mechanisms and to measure wear progression of the tool cutting edges. For both coated and uncoated drills, abrasio...

  3. The effect of palm kernel shell ash on the mechanical properties of as-cast aluminium alloy matrix composites

    Directory of Open Access Journals (Sweden)

    Isiaka Oluwole OLADELE

    2016-06-01

    Full Text Available The present work describes the effect of palm kernel shell ash (PKSA as reinforcement on the mechanical properties of As-cast aluminium alloy. Recycled aluminium alloy from cylinder of an automotive engine block was degreased by using premium motor spirit (PMS also known as petrol, washed thoroughly with soap and water and sun dried for 5 days. The palm kernel shell was screened of dirt and other unwanted foreign materials before being roasted in furnace. The ash was further pulverized by laboratory ball mill machine followed by sieving to obtain particle sizes of 106 µm and divided into two parts. One portion was treated with NaOH solution while the other part was left as untreated before they are used to reinforced molten aluminium alloy in predetermined proportions. The newly developed composites were characterized with respect to their mechanical properties in response to the tests that were carried out on them. The results indicate that palm kernel shell ash can be used as potential reinforcing material for automobile applications.

  4. Weldability of AA 5052 H32 aluminium alloy by TIG welding and FSW process - A comparative study

    Science.gov (United States)

    Shanavas, S.; Raja Dhas, J. Edwin

    2017-10-01

    Aluminium 5xxx series alloys are the strongest non-heat treatable aluminium alloy. Its application found in automotive components and body structures due to its good formability, good strength, high corrosion resistance, and weight savings. In the present work, the influence of Tungsten Inert Gas (TIG) welding parameters on the quality of weld on AA 5052 H32 aluminium alloy plates were analyzed and the mechanical characterization of the joint so produced was compared with Friction stir (FS) welded joint. The selected input variable parameters are welding current and inert gas flow rate. Other parameters such as welding speed and arc voltage were kept constant throughout the study, based on the response from several trial runs conducted. The quality of the weld is measured in terms of ultimate tensile strength. A double side V-butt joints were fabricated by double pass on one side to ensure maximum strength of TIG welded joints. Macro and microstructural examination were conducted for both welding process.

  5. Study of Dissimilar Welding AA6061 Aluminium Alloy and AZ31B Magnesium Alloy with ER5356 Filler Using Friction Stir Welding

    Science.gov (United States)

    Mahamud, M. I. I.; Ishak, M.; Halil, A. M.

    2017-09-01

    This paper is to study of dissimilar welding AA6061 aluminium alloy and AZ31B magnesium alloy with ER5356 filler using friction stir welding. 2 mm thick plates of aluminium and magnesium were used. Friction stir welding operations were performed at different rotation and travel speeds and used the fixed tilt angle which is 3°. The rotation speeds varied from 800 to 1100 rpm, and the travel speed varied from 80 to 100 mm/min. In the range rotation speed of 800 to 1000 rpm and welding speed of 80 to 100 mm/min there are no defect at the weld. Tensile test show the higher tensile strength is 198 MPa and the welding efficiency is about 76%.

  6. Sintering behaviour of Alumix 321 and 6061 aluminium alloys; Sinterizacion de las aleaciones Alumix 321 y 6061

    Energy Technology Data Exchange (ETDEWEB)

    Romano, P.; Fogagnolo, J. B.; Garcia, A.; Ruiz-Navas, E. M.

    2005-07-01

    The sintering behaviour of two aluminium alloys, Alumix 321 and 6061, was studied in this paper. Both have a similar Mg, Cu and Si contents, but have been obtained by different methods. the Alumix 321 alloy is produced by mixing the initial elements as powders and the 6061 is obtained by water atomization. The work carried out includes the study of the green properties, the determination of the compressibility and green strength curves as well as the microstructural characterization of the powders. Thermal analyses (DTAs and Dilatometries) were performed in order to study the behaviour of both alloys with temperature. furthermore, different sintering temperatures were studied by characterizing the mechanical properties of the sintered materials. It can be concluded that the 6061 alloys has better properties than the Alumix 321, when both were sintered at 600 degree centigree. (Author) 27 refs.

  7. Accelerated growth of oxide film on aluminium alloys under steam: Part I: Effects of alloy chemistry and steam vapour pressure on microstructure

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Gudla, Visweswara C.; Jellesen, Morten S.

    2015-01-01

    of the oxide layeras well as the compactness increased with steam vapour pressure. The increase in vapour pressure also resulted in a better coverage over the intermetallic particles. Oxide layer showed a layered structure with more compact layer at the Al interface and a nano-scale needle like structure...... of alkaline etching pre-treatment influenced the thickness and growth of theoxide. Moreover the steam treatment resulted in the partial oxidation of second phase intermetallic particles present in the aluminium alloy microstructure....

  8. Processing and characterization of aluminium alloys or composites exhibiting low-temperature or high-rate superplasticity

    International Nuclear Information System (INIS)

    Huang, J. C.

    1997-01-01

    Wide applications of superplastic forming still face several problems, one is the high temperature that promotes grain growth, another is the low forming rate that makes economically inefficient. The current study is intended to develop a series of fabrication and thermomechanical processing, so as to result in materials possessing either low temperature superplasticity (LTSP) or high rate superplasticity (HRSP). The former has been achieved in the cast Al alloys, while the latter was accomplished in powder-metallurgy aluminium matrix composites. The aluminium alloys, after special thermomechanical processes, exhibited LTSP from 300 to 450 degree C with elongations varying from 300 to 700 %. The LTSP sheets after 700 % elongation at 350 degree C still possessed fine grains 3.7 μm size and narrow surface solute depletion zones 11 μm in with, resulting in a post-SP T6 strength of 500 MPa, significantly higher than that of the HTSP superplasticity alloys tested at 525 degree C or above. Meanwhile, it was found that LTSP materials may be transferred into HTSP materials simply by adding a preloading at 300-400 degree C for a small amount of work. As for the endeavor in making HRSP materials, 2024Al/SiC, 6061Al/SiC and Al/Al 3 Ti systems processed by powder metallurgy or mechanical alloying methods are under investigation. The average sizes of the reinforcing SiC or A13Ti particles, as well as the grain size are all around 1 μm. The aluminium composites have exhibited HRSP at 525-620 degree C and 10 -2 -10 -1 s -l , with elongations varying from 150 to 350 %. This ultimate goal is to produce an alloy or composite exhibiting low temperature and high strain rate superplasticity (LT and HRSP). (author)

  9. Effects of surface treatment of aluminium alloy 1050 on the adhesion and anticorrosion properties of the epoxy coating

    Energy Technology Data Exchange (ETDEWEB)

    Sharifi Golru, S., E-mail: samanesharifi@aut.ac.ir [Department of Polymer Engineering and Color Technology, Amirkabir University of Technology, P.O. Box 15875-4413 Tehran (Iran, Islamic Republic of); Attar, M.M., E-mail: attar@aut.ac.ir [Department of Polymer Engineering and Color Technology, Amirkabir University of Technology, P.O. Box 15875-4413 Tehran (Iran, Islamic Republic of); Ramezanzadeh, B. [Department of Surface Coating and Corrosion, Institute for Color Science and Technology, No. 59,Vafamanesh St, Hosainabad Sq, Lavizan, Tehran (Iran, Islamic Republic of)

    2015-08-01

    Highlights: • Aluminium alloy 1050 was treated by zirconium-based (Zr) conversion coating. • The surface morphology and surface free energy of the samples were obtained. • The adhesion properties of the epoxy coating was studied on the treated samples. • The corrosion resistance of the epoxy coating was enhanced on treated samples. - Abstract: The objective of this work is to investigate the effects of zirconium-based (Zr) conversion coating on the adhesion properties and corrosion resistance of an epoxy/polyamide coating applied on the aluminium alloy 1050 (AA1050). Field emission scanning electron microscope (FE-SEM), energy dispersive X-ray spectrum (EDS), atomic force microscope (AFM) and contact angle measuring device were employed in order to characterize the surface characteristics of the Zr treated AA1050 samples. The epoxy/polyamide coating was applied on the untreated and Zr treated samples. The epoxy coating adhesion to the aluminium substrate was evaluated by pull-off test before and after 30 days immersion in 3.5% w/w NaCl solution. In addition, the electrochemical impedance spectroscopy (EIS) and salt spray tests were employed to characterize the corrosion protection properties of the epoxy coating applied on the AA1050 samples. Results revealed that the surface treatment of AA1050 by zirconium conversion coating resulted in the increase of surface free energy and surface roughness. The dry and recovery (adhesion strength after 30 days immersion in the 3.5 wt% NaCl solution) adhesion strengths of the coatings applied on the Zr treated aluminium samples were greater than untreated sample. In addition, the adhesion loss of the coating applied on the Zr treated aluminium substrate was lower than other samples. Also, the results obtained from EIS and salt spray test clearly revealed that the Zr conversion coating could enhance the corrosion protective performance of the epoxy coating significantly.

  10. Effects of surface treatment of aluminium alloy 1050 on the adhesion and anticorrosion properties of the epoxy coating

    International Nuclear Information System (INIS)

    Sharifi Golru, S.; Attar, M.M.; Ramezanzadeh, B.

    2015-01-01

    Highlights: • Aluminium alloy 1050 was treated by zirconium-based (Zr) conversion coating. • The surface morphology and surface free energy of the samples were obtained. • The adhesion properties of the epoxy coating was studied on the treated samples. • The corrosion resistance of the epoxy coating was enhanced on treated samples. - Abstract: The objective of this work is to investigate the effects of zirconium-based (Zr) conversion coating on the adhesion properties and corrosion resistance of an epoxy/polyamide coating applied on the aluminium alloy 1050 (AA1050). Field emission scanning electron microscope (FE-SEM), energy dispersive X-ray spectrum (EDS), atomic force microscope (AFM) and contact angle measuring device were employed in order to characterize the surface characteristics of the Zr treated AA1050 samples. The epoxy/polyamide coating was applied on the untreated and Zr treated samples. The epoxy coating adhesion to the aluminium substrate was evaluated by pull-off test before and after 30 days immersion in 3.5% w/w NaCl solution. In addition, the electrochemical impedance spectroscopy (EIS) and salt spray tests were employed to characterize the corrosion protection properties of the epoxy coating applied on the AA1050 samples. Results revealed that the surface treatment of AA1050 by zirconium conversion coating resulted in the increase of surface free energy and surface roughness. The dry and recovery (adhesion strength after 30 days immersion in the 3.5 wt% NaCl solution) adhesion strengths of the coatings applied on the Zr treated aluminium samples were greater than untreated sample. In addition, the adhesion loss of the coating applied on the Zr treated aluminium substrate was lower than other samples. Also, the results obtained from EIS and salt spray test clearly revealed that the Zr conversion coating could enhance the corrosion protective performance of the epoxy coating significantly

  11. The effect of natural pre-ageing on the mechanical properties of Rheo-High pressure die cast aluminium alloy 2139

    CSIR Research Space (South Africa)

    Chauke, L

    2015-07-01

    Full Text Available -high pressure die casting process (R-HPDC). Alloy 2139 is a Ag-containing aluminium alloy from the Al-Cu-Mg 2xxx series family. The addition of Ag enhances the age hardening response through the formation of co-clusters that act as precursors to the formation...

  12. Contribution to the grain refinement of hypoeutectic aluminium-silicon casting alloys: application of a new grain refiner and experience from practice; Beitrag zur Kornfeinung von untereutektischen Aluminium-Silicium-Gusslegierungen: Anwendung eines neuen Kornfeiners und Erfahrungen aus der Praxis

    Energy Technology Data Exchange (ETDEWEB)

    Koch, H. [Aluminium Rheinfelden GmbH, Rheinfelden (Germany)

    2000-10-01

    This paper describes the application of a master alloy on the basis of aluminium-titanium-boron, that is designed for hypoeutectic aluminium-silicon casting alloys. The efficiency of the grain refiner was measured using thermal analysis and sand and permanent mould casted samples. The grain size was measured using metallographic technique. In addition, casting trials using a spiral sand mould were carried out to estimate the influence on the flowing behaviour of the melt. To compare the results, a standard AlTi5B1 rod was used under the same test conditions. Finally, results from practice are shown. The grain refinement mechanism is discussed. (orig.)

  13. The effect of heat treatment conditions on the structure evolution and mechanical properties of two binary Al-Mg aluminium alloys

    Directory of Open Access Journals (Sweden)

    P. Snopiński

    2017-01-01

    Full Text Available The presented investigation results were carried out on two binary aluminium-magnesium alloys. The article focuses on the influence of heat treatment conditions on the precipitation response of AlMg3 and AlMg5 aluminium alloy, microstructure evolution and strength of the alloys. The microstructure variation was analysed using a scanning electron microscope and an optical microscope in order to characterise the microstructure in a heat treated condition. Tensile tests and hardness measurements were carried out to investigate the effect of heat treatment on the mechanical properties.

  14. Investigation on wear and corrosion behavior of equal channel angular pressed aluminium 2014 alloy

    Science.gov (United States)

    Divya, S. P.; Yoganandan, G.; Balaraju, J. N.; Srinivasan, S. A.; Nagaraj, M.; Ravisankar, B.

    2018-02-01

    Aluminium 2014 alloy solutionized at 495°C, aged at 195°C was subjected to Equal Channel Angular Pressing (ECAP). Dry sliding wear tests were conducted using pin on disc tribometer system under nominal loads of 10N and 30N with constant speed 2m/s for 2000m in order to investigate their wear behavior after ECAP. The Co-efficient of friction and loss in volume were decreased after ECAP. The dominant wear mechanism observed was adhesion, delamination in addition to these wear mechanisms, oxidation and transfer of Fe from the counter surface to the Al 2014 pin were observed at higher loading condition. The corrosion behavior was evaluated by potentiodynamic polarization (PDP) and electrochemical impedance spectroscopy (EIS) in 3.5% NaCl solution. The results obtained from PDP showed higher corrosion potential and lower corrosion density after ECAP than base. Electrochemical impedance spectroscopy (EIS) showed higher charge transfer resistance after ECAP. Surface morphology showed decreased pit size and increased oxygen content in ECAP sample than base after PDP.

  15. Design and Analysis of Wind Turbine Blade Hub using Aluminium Alloy AA 6061-T6

    Science.gov (United States)

    Ravikumar, S.; Jaswanthvenkatram, V.; Sai kumar, Y. J. N. V.; Sohaib, S. Md.

    2017-05-01

    This work presents the design and analysis of horizontal axis wind turbine blade hub using different material. The hub is very crucial part of the wind turbine, which experience the loads from the blades and the loads were transmitted to the main shaft. At present wind turbine is more expensive and weights more than a million pounds, with the nacelle, rotor hub and blades accounting for most of the weight. In this work Spheroidal graphite cast iron GGG 40.3 is replaced by aluminium alloy 6061-T6 to enhance the casting properties and also to improve the strength-weight ratio. This transition of material leads to reduction in weight of the wind turbine. All the loads caused by wind and extreme loads on the blades are transferred to the hub. Considering the IEC 61400-1 standard for defining extreme loads on the hub the stress and deflection were calculated on the hub by using Finite element Analysis. Result obtained from ANSYS is compared and discussed with the existing design.

  16. Strain Measurement in Aluminium Alloy during the Solidification Process Using Embedded Fibre Bragg Gratings

    Directory of Open Access Journals (Sweden)

    Klaus Weraneck

    2016-11-01

    Full Text Available In recent years, the observation of the behaviour of components during the production process and over their life cycle is of increasing importance. Structural health monitoring, for example of carbon composites, is state-of-the-art research. The usage of Fibre Bragg Gratings (FBGs in this field is of major advantage. Another possible area of application is in foundries. The internal state of melts during the solidification process is of particular interest. By using embedded FBGs, temperature and stress can be monitored during the process. In this work, FBGs were embedded in aluminium alloys in order to observe the occurring strain. Two different FBG positions were chosen in the mould in order to compare its dependence. It was shown that FBGs can withstand the solidification process, although a compression in the range of one percent was measured, which is in agreement with the literature value. Furthermore, different lengths of the gratings were applied, and it was shown that shorter gratings result in more accurate measurements. The obtained results prove that FBGs are applicable as sensors for temperatures up to 740 °C.

  17. Fatigue crack propagation in an ECAP-processed aluminium alloy - influence of shear plane orientation

    Energy Technology Data Exchange (ETDEWEB)

    Hockauf, M.; Wagner, M.F.X.; Lampke, T.; Halle, T. [Technische Universitaet Chemnitz, Institut fuer Werkstoffwissenschaft und Werkstofftechnik, Erfenschlager Strasse 73, 09125 Chemnitz (Germany); Hockauf, K.

    2012-07-15

    In this work, the orientation-dependent fatigue crack propagation behaviour in an ECAP-processed aluminium alloy is investigated. For a bimodal condition with elongated structures as well as for a homogeneous condition with equiaxed ultrafine grains, the tendency for crack path deviation was evaluated for different sample orientations. In the case of elongated structures, the crack path is deflected towards the elongation plane. However, the angle of deviation differs, depending on whether the fatigue crack propagation rate was in the near-threshold and lower Paris-Erdogan regime (higher angle of deviation) or the upper Paris-Erdogan regime (smaller angle of deviation). Especially in the near-threshold region, the crack path deviation is linked to higher crack growth rates when compared to ideally straight crack propagation. This effect can be explained by the effects of processing-induced damage and local stress fields along the elongated structures. (Copyright copyright 2012 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

  18. Micromechanical aspects of fatigue in a MIG welded aluminium airframe alloy

    International Nuclear Information System (INIS)

    Lefebvre, F.; Sinclair, I.

    2005-01-01

    Short crack fatigue behaviour of a metal inert gas (MIG) welded 2024-T351 aluminium alloy has been studied in terms of crack initiation and propagation, and the microstructural features of the weld. Extensive crack initiation was noted within the weld fusion zone. Relatively small interdentritic defects are seen to be more damaging (in initiating cracks) than the larger gas bubble defects that exist in this region. Cracks were also seen to initiate within the weld heat affected zone where tensile residual stresses were found to be high, however, rapid crack growth and coalescence within the fusion zone is seen to dominate failure. Multiple crack interactions are seen to have a significant effect on failure up to relatively large crack lengths (of the order of the fusion zone width), enhancing the variability in short crack growth. Secondary electron and back-scattered electron imaging, in association with electron back-scattered diffraction (EBSD) mapping, were carried out on failed samples to assess the associated microstructural interactions

  19. Anisotropic work-hardening behaviour ofstructural steels and aluminium alloys at large strains

    Science.gov (United States)

    Bouvier, S.; Teodosiu, C.; Haddadi, H.; Tabacaru, V.

    2003-03-01

    Sheet metal forming processes may often involve intense forming sequences, leading to large strains and severe strain-path changes. Optimizing such technologies requires a good understanding and description of the anisotropic plastic behaviour of the deformed material, in connection with the evolution of its texture and microstructure. In this paper, we present the predictions provided by a model involving isotropic and kinematioc hardening and by a physically-based microstructural model, which introduces additional internal variables taking into accounthe directional strength of dislocation structures and their polarity. These models have been identified by using sequences of uniaxial traction and simple shear experiments, carried out on various steels (DC06, DP600, HSLA340) and aluminium alloys (AA5182-O, AA6016-T4). The microstructural model proved able predict the complex hardening behaviour displayed, especially by the ferritic steels, namely the transient work-hardening stagnation during reversed deformation in Bauschinger tests, the temporary work-softening during orthogonal tests, and the grain fragmentation at large monotonie strains.

  20. Deep surface rolling for fatigue life enhancement of laser clad aircraft aluminium alloy

    Science.gov (United States)

    Zhuang, W.; Liu, Q.; Djugum, R.; Sharp, P. K.; Paradowska, A.

    2014-11-01

    Deep surface rolling can introduce deep compressive residual stresses into the surface of aircraft metallic structure to extend its fatigue life. To develop cost-effective aircraft structural repair technologies such as laser cladding, deep surface rolling was considered as an advanced post-repair surface enhancement technology. In this study, aluminium alloy 7075-T651 specimens with a blend-out region were first repaired using laser cladding technology. The surface of the laser cladding region was then treated by deep surface rolling. Fatigue testing was subsequently conducted for the laser clad, deep surface rolled and post-heat treated laser clad specimens. It was found that deep surface rolling can significantly improve the fatigue life in comparison with the laser clad baseline repair. In addition, three dimensional residual stresses were measured using neutron diffraction techniques. The results demonstrate that beneficial compressive residual stresses induced by deep surface rolling can reach considerable depths (more than 1.0 mm) below the laser clad surface.

  1. Microstructural evolution and mechanical properties of oil jet peened aluminium alloy, AA6063-T6

    International Nuclear Information System (INIS)

    Arun Prakash, N.; Gnanamoorthy, R.; Kamaraj, M.

    2010-01-01

    Grain size refinement by severe surface plastic deformation is one way of improving the surface properties. This paper describes the microstructural evolution due to severe surface plastic deformation by oil jet peening in aluminium alloy, AA6063-T6. Detail characterization of the treated surfaces using X-ray diffraction analysis and transmission electron microscopy revealed the formation of submicron size grains at and near the surface. The nozzle-traveling velocity decides the peening intensity and coverage and affects the surface properties. The specimen peened at low nozzle-traveling velocity exhibited an ultrafine grain size (∼210 nm) with high surface hardness (∼0.88 GPa), compressive residual stress (-102 ± 7 MPa) and dislocation density. The hardness is high at the surface and the depth of hardened layer is ∼400 μm. Formation of high-density dislocations and associated grain refinement resulted in increased surface hardness. Presence of surface modified layer will be beneficial in improving the fatigue and tribo behavior.

  2. Influence of transport mechanisms on nucleation and grain structure formation in DC cast aluminium alloy ingots

    Science.gov (United States)

    Bedel, M.; Založnik, M.; Kumar, A.; Combeau, H.; Jarry, P.; Waz, E.

    2012-01-01

    The grain structure formation in direct chill (DC) casting is directly linked to nucleation, which is generally promoted by inoculation. Inoculation prevents defects, but also modifies the physical properties by changing the microstructure. We studied the coupling of the nucleation on inoculant particles and the grain growth in the presence of melt flow induced by thermosolutal convection and of the transport of free-floating equiaxed grains. We used a volume-averaged two-phase multiscale model with a fully coupled description of phenomena on the grain scale (nucleation on grain refiner particles and grain growth) and on the product scale (macroscopic transport). The transport of inoculant particles is also modeled, which accounts for the inhomogeneous distribution of inoculant particles in the melt. The model was applied to an industrial sized (350mm thick) DC cast aluminium alloy ingot. A discretised nuclei size distribution was defined and the impact of different macroscopic phenomena on the grain structure formation was studied: the zone and intensity of nucleation and the resulting grain size distribution. It is shown that nucleation in the presence of macroscopic transport cannot be explained only in terms of cooling rate, but variations of composition, nuclei density and grain density, all affected by transport, must be accounted for.

  3. Elastic and plastic properties of iron-aluminium alloys. Special problems raised by the brittleness of alloys of high aluminium content; Proprietes elastiques et plastiques des alliages fer-aluminium. Problemes particuliers poses par la fragilite des alliages a forte teneur en aluminium

    Energy Technology Data Exchange (ETDEWEB)

    Mouturat, P. [Commissariat a l' Energie Atomique, Saclay (France). Centre d' Etudes Nucleaires

    1966-06-01

    The present study embodies the results obtained with iron-aluminium alloys whose composition runs from 0 to nearly 50 atoms per cent aluminium. Conditions of elaboration and transformation have been studied successively, as well as the Young's modulus and the flow stress; the last chapter embodies, a study of the Portevin-le-Chatelier effect in alloys of 40 atoms per cent of aluminium. I) The principal difficulty to clear up consisted in the intergranular brittleness of ordered alloys; this brittleness has been considerably reduced with appropriate conditions of elaboration and transformation. II) The studies upon the Young's modulus are in connection with iron-aluminium alloys; transformation temperatures are well shown up. The formation of covalent bonds on and after 25 atoms per cent show the highest values of the modulus. III) The analysis of variations of the flow stress according to the temperature show some connection with ordered structures, the existence of antiphase domains and the existence of sur-structure dislocations. IV) In the ordered Fe Al domain the kinetics of the Portevin-le-Chatelier effect could be explained by a mechanism of diffusion of vacancies. The role they play has been specified by the influence they exert upon the dislocations; this has led us to the inhomogeneous Rudman order; this inhomogeneous order could explain the shape of the traction curves. (author) [French] Cette etude comporte les resultats obtenus avec des alliages fer-aluminium dont la composition s'etend de 0 a pres de 50 atomes pour cent d'aluminium. Nous avons etudie successivement les conditions d'elaboration et de transformation, le module elastique et la limite elastique; un dernier chapitre est consacre a l'etude du phenomene Portevin-le-Chatelier dans les alliages a 40 atomes pour cent d'aluminium. I) La principale difficulte a resoudre residait dans la fragilite intergranulaire des alliages ordonnes; celle-ci a ete

  4. Experimental investigations of visco-plastic properties of the aluminium and tungsten alloys used in KE projectiles

    Directory of Open Access Journals (Sweden)

    Magier M.

    2012-08-01

    Full Text Available The main aim of studies on dynamic behaviour of construction materials at high strain rates is to determine the variation of mechanical properties (strength, plasticity in function of the strain rate and temperature. On the basis of results of dynamic tests on the properties of constructional materials the constitutive models are formulated to create numerical codes applied to solve constructional problems with computer simulation methods. In the case of military applications connected with the phenomena of gunshot and terminal ballistics it’s particularly important to develop a model of strength and armour penetration with KE projectile founded on reliable results of dynamic experiments and constituting the base for further analyses and optimization of projectile designs in order to achieve required penetration depth. Static and dynamic results of strength investigations of the EN AW-7012 aluminium alloy (sabot and tungsten alloy (penetrator are discussed in this paper. Static testing was carried out with the INSTRON testing machine. Dynamic tests have been conducted using the split Hopkinson pressure bars technique at strain rates up to 1,2 ⋅ 104s−1 (for aluminium alloy and 6 ⋅ 103s−1 (for tungsten alloy.

  5. Experimental investigations of visco-plastic properties of the aluminium and tungsten alloys used in KE projectiles

    Science.gov (United States)

    Kruszka, L.; Magier, M.

    2012-08-01

    The main aim of studies on dynamic behaviour of construction materials at high strain rates is to determine the variation of mechanical properties (strength, plasticity) in function of the strain rate and temperature. On the basis of results of dynamic tests on the properties of constructional materials the constitutive models are formulated to create numerical codes applied to solve constructional problems with computer simulation methods. In the case of military applications connected with the phenomena of gunshot and terminal ballistics it's particularly important to develop a model of strength and armour penetration with KE projectile founded on reliable results of dynamic experiments and constituting the base for further analyses and optimization of projectile designs in order to achieve required penetration depth. Static and dynamic results of strength investigations of the EN AW-7012 aluminium alloy (sabot) and tungsten alloy (penetrator) are discussed in this paper. Static testing was carried out with the INSTRON testing machine. Dynamic tests have been conducted using the split Hopkinson pressure bars technique at strain rates up to 1,2 ṡ 104s-1 (for aluminium alloy) and 6 ṡ 103s-1 (for tungsten alloy).

  6. In-vitro characterization of stress corrosion cracking of aluminium-free magnesium alloys for temporary bio-implant applications.

    Science.gov (United States)

    Choudhary, Lokesh; Singh Raman, R K; Hofstetter, Joelle; Uggowitzer, Peter J

    2014-09-01

    The complex interaction between physiological stresses and corrosive human body fluid may cause premature failure of metallic biomaterials due to the phenomenon of stress corrosion cracking. In this study, the susceptibility to stress corrosion cracking of biodegradable and aluminium-free magnesium alloys ZX50, WZ21 and WE43 was investigated by slow strain rate tensile testing in a simulated human body fluid. Slow strain rate tensile testing results indicated that each alloy was susceptible to stress corrosion cracking, and this was confirmed by fractographic features of transgranular and/or intergranular cracking. However, the variation in alloy susceptibility to stress corrosion cracking is explained on the basis of their electrochemical and microstructural characteristics. Copyright © 2014 Elsevier B.V. All rights reserved.

  7. Modification of aluminium alloys with rare metals – the basis for advanced materials in construction and transport

    Directory of Open Access Journals (Sweden)

    Skachkov Vladimir Mikchaylovich

    2016-06-01

    Full Text Available The method of process powder injection into aluminum melt shows much promise. Scandium is injected by the high-temperature exchange reaction between the salt melt and aluminum. The best salt compositions were selected. The results of the process are considered to depend on the initial salts. A series of fusions was performed under production conditions at the Kamensk-Uralskii metallurgical plant. It was shown that the injection method for production of aluminoscandium master alloys is technologically feasible. To protect intellectual property of authors, employees of the Institute of Solid State Chemistry, Ural branch of RAS (Russia a patent «Method of alloying of aluminium or alloys on its basis» RU № 2534182 of 27.11.2014 was registered.

  8. Industrial based volume manufacturing of lightweight aluminium alloy panel components with high-strength and complex-shape for car body and chassis structures

    Science.gov (United States)

    Anyasodor, Gerald; Koroschetz, Christian

    2017-09-01

    To achieve the high volume manufacture of lightweight passenger cars at economic cost as required in the automotive industry, low density materials and new process route will be needed. While high strength aluminium alloy grades: AA7075 and AA6082 may provide the alternative material solution, hot stamping process used for high-strength and ultrahigh strength steels such as boron steel 22mnb5 can enable the volume manufacture of panel components with high-strength and complex-shape for car body and chassis structures. These aluminium alloy grades can be used to manufacture panel components with possible yield strengths ≥ 500 MPa. Due to the differences in material behaviors, hot stamping process of 22mnb5 cannot be directly applied to high strength aluminium alloy grades. Despite recorded successes in laboratories, researches and niche hot forming processes of high strength aluminium alloy grades, not much have been achieved for adequate and efficient volume manufacturing system applicable in the automotive industry. Due to lack of such system and based on expert knowledge in hot stamping production-line, AP&T presents in this paper a hot stamping processing route for high strength aluminium alloys been suitable for production-line development and volume manufacturing.

  9. Examination of the effect of Sc on 2000 and 7000 series aluminium alloy castings: for improvements in fusion welding

    International Nuclear Information System (INIS)

    Norman, A.F.; Hyde, K.; Costello, F.; Thompson, S.; Birley, S.; Prangnell, P.B.

    2003-01-01

    It has been reported that small additions of scandium (Sc) can improve the weldability and mechanical properties of some aluminium aerospace alloys that are normally considered to be 'unweldable'. In order to determine the mechanisms by which these improvements occur, and more rapidly arrive at optimum Sc addition levels, small wedge-shaped castings have been used to simulate the cooling rates found in MIG/TIG welds. Using this technique, a range of Sc addition levels have been made to two typical Al-aerospace alloys, 2024 and 7475. It has been found that when the Sc level exceeds a critical concentration, small Al 3 Sc primary particles form in the melt and act as very efficient grain nucleants, resulting in simulated fusion zone grain sizes as fine as 15 μm. This exceptional level of grain refinement produced an unusual grain structure that exhibited no dendritic, or cellular, substructure and a large increase in strength and ductility of the castings. Sc also produced changes in the alloy's freezing paths, which cannot yet be fully explained, but led to the appearance of the W phase in the 2024 alloy and, in both alloys, an overall reduction in the amount of eutectic formed during solidification. When coupled with the high level of grain refinement, this behaviour could be used to explain the increased strength and ductility of the castings. In 2000 and 7000 series aluminium alloys, it is therefore, anticipated that optimised Sc bearing filler wires will significantly improve the mechanical properties of the weld metal, as well as reducing the tendency for solidification cracking

  10. Circular economy: To be or not to be in a closed product loop? A Life Cycle Assessment of aluminium cans with inclusion of alloying elements

    DEFF Research Database (Denmark)

    Niero, Monia; Olsen, Stig Irving

    2016-01-01

    Packaging, representing the second largest source of aluminium scrap at global level, deserves a key role in the transition towards the circular economy. Life Cycle Assessment (LCA) of aluminium products has been typically based on one life cycle considering pure aluminium flows and neglecting...... the presence of alloying elements and impurities. However, this simplification undermines the potentials of using LCA to quantify the environmental performances of products in multiple loops, as required in the circular economy. This study aims to investigate the effects of including the actual alloy...... recycling scenario using mixed Al packaging scrap. The main recommendation from an LCA methodological point of view is to include the idea of multiple co-functions in the functional unit definition. To further improve the environmental performances of the aluminium beverage can sector towards circular...

  11. Influence of friction stir welding process and tool parameters on strength properties of AA7075-T6 aluminium alloy joints

    International Nuclear Information System (INIS)

    Rajakumar, S.; Muralidharan, C.; Balasubramanian, V.

    2011-01-01

    The aircraft aluminium alloys generally present low weldability by traditional fusion welding process. The development of the friction stir welding has provided an alternative improved way of satisfactorily producing aluminium joints, in a faster and reliable manner. In this present work, the influence of process and tool parameters on tensile strength properties of AA7075-T 6 joints produced by friction stir welding was analysed. Square butt joints were fabricated by varying process parameters and tool parameters. Strength properties of the joints were evaluated and correlated with the microstructure, microhardness of weld nugget. From this investigation it is found that the joint fabricated at a tool rotational speed of 1400 rpm, welding speed of 60 mm/min, axial force of 8 kN, using the tool with 15 mm shoulder diameter, 5 mm pin diameter, 45 HRc tool hardness yielded higher strength properties compared to other joints.

  12. Influence of ECAP on Densification Behaviour in the PM Aluminium Al-Mg-Si-Cu-Fe Alloy

    Science.gov (United States)

    Bidulská, Jana; Kvačkaj, Tibor; Kočiško, Róbert; Bidulský, Róbert; Grande, Marco Actis

    2010-09-01

    The main aim of this paper is to show how ECAP influences the densification behaviour of PM aluminium alloys. An aluminium based powder (Al-Mg-Si-Cu-Fe) was used as material to be investigated. After applying different compacting pressures, specimens were dewaxed in a ventilated furnace at 400 °C for 60 min. Sintering was carried out in a vacuum furnace at 610 °C for 30 min. The specimens were ECAPed for 1 pass. Optical characterization was carried out on the minimum of 10 different image fields. The results were measured for each pore individually in order to describe the dimensional and morphological porosity characteristics. ECAP influences the porosity distribution in terms of the severe shear deformation involved.

  13. Effect of tool profile and fatigue loading on the local hardness around scratches in clad and unclad aluminium alloy 2024

    International Nuclear Information System (INIS)

    Khan, M.K.; Fitzpatrick, M.E.; Hainsworth, S.V.; Edwards, L.

    2009-01-01

    Nanoindentation has been used to study the hardness changes produced by scratching of aluminium alloy AA2024, with and without a clad layer of pure aluminium. The hardness was mapped around scratches made with diamond tools of different profiles. One tool produced significant plastic damage with associated hardening at the scratch root, whilst the other produced a 'cleaner' cut with no hardening. The different behaviours are attributed to whether the tool makes the scratch by a 'cutting' or a 'ploughing' mechanism. The degree of plastic damage around the scratches has been correlated with peak broadening data obtained using synchrotron X-ray diffraction. There was no change observed in the local hardness around the scratch with fatigue loading.

  14. Tribological Properties of Aluminium Alloy Composites Reinforced with Multi-Layer Graphene-The Influence of Spark Plasma Texturing Process.

    Science.gov (United States)

    Kostecki, Marek; Woźniak, Jarosław; Cygan, Tomasz; Petrus, Mateusz; Olszyna, Andrzej

    2017-08-10

    Self-lubricating composites are designed to obtain materials that reduce energy consumption, improve heat dissipation between moving bodies, and eliminate the need for external lubricants. The use of a solid lubricant in bulk composite material always involves a significant reduction in its mechanical properties, which is usually not an optimal solution. The growing interest in multilayer graphene (MLG), characterised by interesting properties as a component of composites, encouraged the authors to use it as an alternative solid lubricant in aluminium matrix composites instead of graphite. Aluminium alloy 6061 matrix composite reinforced with 2-15 vol % of MLG were synthesised by the spark plasma sintering process (SPS) and its modification, spark plasma texturing (SPT), involving deformation of the pre-sintered body in a larger diameter matrix. It was found that the application of the SPT method improves the density and hardness of the composites, resulting in improved tribological properties, particularly in the higher load regime.

  15. Effect of friction time on the properties of friction welded YSZ‐alumina composite and 6061 aluminium alloy

    Directory of Open Access Journals (Sweden)

    Uday M. Basheer

    2012-03-01

    Full Text Available The aim of this work was to study the effect of friction time on the microstructure and mechanical properties of alumina 0, 25, 50 wt% yttria stabilized zirconia (YSZ composite and 6061 aluminium alloy joints formed by friction welding. The alumina-YSZ composites were prepared through slip casting in plaster of Paris molds (POP and subsequently sintered at 1600°C, while the aluminium rods were machined down using a lathe machine to the dimension required. The welding process was carried out under different rotational speeds and friction times, while friction force (0.5 ton-force was kept constant. Scanning electron microscopy was used to characterize the interface of the joints structure. The experimental results showed that the friction time has a significant effect on joint structure and mechanical properties.

  16. Hydrogen analysis and effect of filtration on final quality of castings from aluminium alloy AlSi7Mg0,3

    Directory of Open Access Journals (Sweden)

    M. Brůna

    2011-01-01

    Full Text Available The usage of aluminium and its alloys have increased in many applications and industries over the decades. The automotive industry is the largest market for aluminium castings and cast products. Aluminium is widely used in other applications such as aerospace, marine engines and structures. Parts of small appliances, hand tools and other machinery also use thousands of different aluminium castings. The applications grow as industry seeks new ways to save weight and improve performance and recycling of metals has become an essential part of a sustainable industrial society. The process of recycling has therefore grown to be of great importance, also another aspect has become of critical importance: the achievement of quality and reliability of the products and so is very important to underst and the mechanisms of the formation of defects in aluminium melts, and also to have a reliable and simple means of detection.

  17. Analysis of the tool plunge in friction stir welding - comparison of aluminium alloys 2024 T3 and 2024 T351

    Directory of Open Access Journals (Sweden)

    Veljić Darko

    2016-01-01

    Full Text Available Temperature, plastic strain and heat generation during the plunge stage of the friction stir welding (FSW of high-strength aluminium alloys 2024 T3 and 2024 T351 are considered in this work. The plunging of the tool into the material is done at different rotating speeds. A three-dimensional finite element (FE model for thermomechanical simulation is developed. It is based on arbitrary Lagrangian-Eulerian formulation, and Johnson-Cook material law is used for modelling of material behaviour. From comparison of the numerical results for alloys 2024 T3 and 2024 T351, it can be seen that the former has more intensive heat generation from the plastic deformation, due to its higher strength. Friction heat generation is only slightly different for the two alloys. Therefore, temperatures in the working plate are higher in the alloy 2024 T3 for the same parameters of the plunge stage. Equivalent plastic strain is higher for 2024 T351 alloy, and the highest values are determined under the tool shoulder and around the tool pin. For the alloy 2024 T3, equivalent plastic strain is the highest in the influence zone of the tool pin. [Projekat Ministarstva nauke Republike Srbije, br. TR 34016 i br. TR 35006

  18. Electrochemical and DFT studies of quinoline derivatives on corrosion inhibition of AA5052 aluminium alloy in NaCl solution

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Dapeng; Yang, Dong [Shanghai Key Laboratory of Materials Protection and Advanced Materials in Electric Power, School of Environmental and Chemical Engineering, Shanghai University of Electric Power, Shanghai 200090 (China); Zhang, Daquan, E-mail: zhangdaquan@shiep.edu.cn [Shanghai Key Laboratory of Materials Protection and Advanced Materials in Electric Power, School of Environmental and Chemical Engineering, Shanghai University of Electric Power, Shanghai 200090 (China); Li, Kang; Gao, Lixin [Shanghai Key Laboratory of Materials Protection and Advanced Materials in Electric Power, School of Environmental and Chemical Engineering, Shanghai University of Electric Power, Shanghai 200090 (China); Lin, Tong [Institute for Frontier Materials, Deakin University, Geelong, VIC 3216 (Australia)

    2015-12-01

    Graphical abstract: - Highlights: • 8-AQ and 8-NQ have a good anti-corrosion effect acting as anodic inhibitor. • The inhibition mechanism is dominated by geometric covering effect. • The p-orbital of reactive site of inhibitor and sp-orbital of Al are hybridizing. - Abstract: Two quinoline derivatives, 8-aminoquinoline (8-AQ) and 8-nitroquinoline (8-NQ), have been used as inhibitors to examine their corrosion protection effect on AA5052 aluminium alloy in 3% NaCl solution. The weight-loss and electrochemical measurement have indicated that 8-AQ and 8-NQ play as anodic inhibitor to retard the anodic electrochemical process. SEM/EDS analysis clearly shows that 8-AQ and 8-NQ form a protective film on the AA5052 alloy surface. Density functional theory (DFT) calculation confirmed the formation of strong hybridization between the p-orbital of reactive sites in the inhibitor molecules and the sp-orbital of the Al atom. 8-aminoquinoline and 8-nitroquinoline may be useful as effective corrosion inhibitors for aluminium alloys.

  19. Evolution of mechanical behavior of 6XXX aluminium alloy due to the precipitation state during a thermo-mechanical process

    International Nuclear Information System (INIS)

    Bardel, Didier; Perez, Michel; Nelias, Daniel; Chaise, Thibaut; Garnier, Jerome; Bourlier, Florent

    2014-01-01

    The aim of this research is to link the microstructural state and the mechanical properties of an age hardening alloy during a fast heat treatment such as encountered during welding. A coupled model between precipitation state and mechanical properties is used to predict the yield strength and hardening behavior that can be observed experimentally. The method permits the identification of the kinematic and isotropic contributions in the hardening model. The methodology is applied to a 6061-T6 aluminium alloy which is used in the Jules Horowitz reactor vessel. The general idea of this methodology is to couple an efficient microstructural model to a mechanical one based on the dislocation theory and ad'hoc experiments. The theoretical background is based on the work of Kampmann and Wagner, known as the KWN model, to account for nucleation, growth/dissolution and coarsening of precipitates. This analysis requires transient thermo-mechanical experimental data. The efficiency of these models and their coupling are shown for a series 6XXX aluminium alloy which contains β'' and β' precipitates. Ultimately these models are coupled to a FEA model and allows to predict the distribution of precipitates within each element of the mesh, and subsequently its mechanical behavior. (authors)

  20. Accelerated growth of oxide film on aluminium alloys under steam: Part II: Effects of alloy chemistry and steam vapour pressure on corrosion and adhesion performance

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Bordo, Kirill; Jellesen, Morten Stendahl

    2015-01-01

    The steam treatment of aluminium alloys with varying vapour pressure of steamresulted in the growth of aluminium oxyhydroxide films of thickness range between 450 - 825nm. The surface composition, corrosion resistance, and adhesion of the produced films was characterised by XPS, potentiodynamic...... polarization, acetic acid salt spray, filiform corrosion test, and tape test. The oxide films formed by steam treatment showed good corrosion resistance in NaCl solution by significantly reducing anodic and cathodic activities. The pitting potential of the surface treated with steam was a function...... of the vapour pressure of the steam. The accelerated corrosion and adhesion tests on steam generated oxide films with commercial powder coating verified that the performance of the oxide coating is highly dependent on the vapour pressure of the steam....

  1. Studies of the subsurface zone created in aluminium and its alloys by means of positron annihilation and complementary methods

    International Nuclear Information System (INIS)

    Dryzek, E.

    2008-01-01

    There are presented the results of the studies of the subsurface zone created in aluminium and its alloys during sliding or other surface modification treatments. The application of the positron annihilation techniques due to their high sensitivity to crystal lattice defects enabled to determine defects profiles in the subsurface zone. The positron annihilation studies were correlated with other conventional measurements applied in tribology, i.e. microhardness measurements, scanning electron microscopy, X-ray diffraction and in a special case stress distribution calculated theoretically. It was shown that the positron annihilation spectroscopy is a useful tool for profiling of the subsurface zone created during sliding even for light metals their alloys and composites. The total range of the subsurface zone detected by the positron annihilation extends from 50 μm to 450 μm depending on the material studied and surface modification treatment. Additionally, the type of the main defects can be determined. The studies of the pure aluminium samples after dry sliding enabled to find the defect concentration of vacancy type in the depth less then 1 μm and to correlate its value with the size of crystallites. It supports the conclusion on recovery processes taking place in this layer. There was made the attempt to apply the Doppler broadening coincidence spectroscopy to the studies of aluminium alloy and composite. In view of the interdisciplinary character the present thesis enclose also the review of the basic issues of tribology, measurement methods applied to the subsurface zone studies and positron annihilation experimental techniques. (author)

  2. Electromagnetic Gauge Study of Laser-Induced Shock Waves in Aluminium Alloys

    Science.gov (United States)

    Peyre, P.; Fabbro, R.

    1995-12-01

    The laser-shock behaviour of three industrial aluminum alloys has been analyzed with an Electromagnetic Gauge Method (EMV) for measuring the velocity of the back free surface of thin foils submitted to plane laser irradiation. Surface pressure, shock decay in depth and Hugoniot Elastic Limits (HEL) of the materials were investigated with increasing thicknesses of foils to be shocked. First, surface peak pressures values as a function of laser power density gave a good agreement with conventional piezoelectric quartz measurements. Therefore, comparison of experimental results with computer simulations, using a 1D hydrodynamic Lagrangian finite difference code, were also in good accordance. Lastly, HEL values were compared with static and dynamic compressive tests in order to estimate the effects of a very large range of strain rates (10^{-3} s^{-1} to 10^6 s^{-1}) on the mechanical properties of the alloys. Cet article fait la synthèse d'une étude récente sur la caractérisation du comportement sous choc-laser de trois alliages d'aluminium largement utilisés dans l'industrie à travers la méthode dite de la jauge électromagnétique. Cette méthode permet de mesurer les vitesses matérielles induites en face arrière de plaques d'épaisseurs variables par un impact laser. La mise en vitesse de plaques nous a permis, premièrement, de vérifier la validité des pressions d'impact superficielles obtenues en les comparant avec des résultats antérieurs obtenus par des mesures sur capteurs quartz. Sur des plaques d'épaisseurs croissantes, nous avons caractérisé l'atténuation des ondes de choc en profondeur dans les alliages étudiés et mesuré les limites d'élasticité sous choc (pressions d'Hugoniot) des alliages. Les résultats ont été comparés avec succès à des simulations numériques grâce à un code de calcul monodimensionnel Lagrangien. Enfin, les valeurs des pressions d'Hugoniot mesurées ont permis de tracer l'évolution des contraintes d

  3. Fatigue crack growth resistance of gas tungsten arc, electron beam and friction stir welded joints of AA2219 aluminium alloy

    International Nuclear Information System (INIS)

    Malarvizhi, S.; Balasubramanian, V.

    2011-01-01

    AA2219 aluminium alloy square butt joints without filler metal addition were fabricated using gas tungsten arc welding (GTAW), electron beam welding (EBW) and friction stir welding (FSW) processes. The effect of three welding processes on fatigue crack growth behaviour is reported in this paper. Transverse tensile properties of the welded joints were evaluated. Microstructure analysis was also carried out using optical and electron microscopes. It was found that the FSW joints are exhibiting superior fatigue crack growth resistance compared to EBW and GTAW joints. This was mainly due to the formation of very fine, dynamically recrystallised grains and uniform distribution of fine precipitates in the weld region.

  4. Optimization of squeeze casting parameters for non symmetrical AC2A aluminium alloy castings through Taguchi method

    International Nuclear Information System (INIS)

    Senthil, P.; Amirthagadeswaran, K. S.

    2012-01-01

    This paper reports a research in which an attempt was made to prepare AC2A aluminium alloy castings of a non symmetrical component through squeeze casting process. The primary objective was to investigate the influence of process parameters on mechanical properties of the castings. Experiments were conducted based on orthogonal array suggested in Taguchi's offline quality control concept. The experimental results showed that squeeze pressure, die preheating temperature and compression holding time were the parameters making significant improvement in mechanical properties. The optimal squeeze casting condition was found and mathematical models were also developed for the process

  5. Experimental and numerical investigation on under-water friction stir welding of armour grade AA2519-T87 aluminium alloy

    Directory of Open Access Journals (Sweden)

    S. Sree Sabari

    2016-08-01

    Full Text Available Friction stir welding (FSW is a promising welding process that can join age hardenable aluminium alloys with high joint efficiency. However, the thermal cycles experienced by the material to be joined during FSW resulted in the deterioration of mechanical properties due to the coarsening and dissolution of strengthening precipitates in the thermo-mechanical affected zone (TMAZ and heat affected zone (HAZ. Under water friction stir welding (UWFSW is a variant of FSW process which can maintain low heat input as well as constant heat input along the weld line. The heat conduction and dissipation during UWFSW controls the width of TMAZ and HAZ and also improves the joint properties. In this investigation, an attempt has been made to evaluate the mechanical properties and microstructural characteristics of AA2519-T87 aluminium alloy joints made by FSW and UWFSW processes. Finite element analysis has been used to estimate the temperature distribution and width of TMAZ region in both the joints and the results have been compared with experimental results and subsequently correlated with mechanical properties.

  6. Local zone-wise elastic-plastic constitutive parameters of Laser-welded aluminium alloy 6061 using digital image correlation

    Science.gov (United States)

    Bai, Ruixiang; Wei, Yuepeng; Lei, Zhenkun; Jiang, Hao; Tao, Wang; Yan, Cheng; Li, Xiaolei

    2018-02-01

    The mechanical properties of aluminium alloys can be affected by the local high temperature in laser welding. In this paper, an inversion identification method of local zone-wise elastic-plastic constitutive parameters for laser welding of aluminium alloy 6061 was proposed based on full-field optical measurement data using digital image correlation (DIC). Three regions, i.e., the fusion zone, heat-affected zone, and base zone, of the laser-welded joint were distinguished by means of microstructure optical observation and micrometer hardness measurement. The stress data were obtained using a laser-welded specimen via a uniaxial tensile test. Meanwhile, the local strain data of the laser-welded specimen were obtained by the DIC technique. Thus, the stress-strain relationship for different local regions was established. Finally, the constitutive parameters of the Ramberg-Osgood model were identified by least-square fitting to the experimental stress-strain data. Experimental results revealed that the mechanical properties of the local zones of the welded joints clearly weakened, and these results are consistent with the results of the hardness measurement.

  7. Study of surface interactions of ionic liquids with aluminium alloys in corrosion and erosion-corrosion processes

    Energy Technology Data Exchange (ETDEWEB)

    Bermudez, Maria-Dolores [Grupo de Ciencia de Materiales e Ingenieria Metalurgica, Departamento de Ingenieria de Materiales y Fabricacion, Universidad Politecnica de Cartagena, C/ Doctor Fleming s/n, Campus Muralla del Mar, 30202 Cartagena (Spain)]. E-mail: mdolores.bermudez@upct.es; Jimenez, Ana-Eva [Grupo de Ciencia de Materiales e Ingenieria Metalurgica, Departamento de Ingenieria de Materiales y Fabricacion, Universidad Politecnica de Cartagena, C/ Doctor Fleming s/n, Campus Muralla del Mar, 30202 Cartagena (Spain); Martinez-Nicolas, Gines [Grupo de Ciencia de Materiales e Ingenieria Metalurgica, Departamento de Ingenieria de Materiales y Fabricacion, Universidad Politecnica de Cartagena, C/ Doctor Fleming s/n, Campus Muralla del Mar, 30202 Cartagena (Spain)

    2007-06-30

    Surface interactions of alkylimidazolium ionic liquids (ILs) with aluminium alloy Al 2011 have been studied by immersion tests in seven neat ILs [1-n-alkyl-3-methylimidazolium X{sup -} (X = BF{sub 4}; n = 2 (IL1), 6 (IL2), 8 (IL3). X = CF{sub 3}SO{sub 3}; n = 2 (IL4). X = (4-CH{sub 3}C{sub 6}H{sub 4}SO{sub 3}); n = 2 (IL5). X PF{sub 6}; n = 6 (IL6)] and 1-butyl-3-methylpyridinium bis(trifluoromethylsulfonyl)imide (IL7)]. Immersion tests for Al 2011 have also been carried out in 1 wt.% and 5 wt.% solutions of 1-ethyl,3-methylimidazolium tetrafluoroborate (IL1) in water. No corrosion of Al 2011 by neat ILs is observed. The highest corrosion rate for Al 2011 in water is observed in the presence of a 5 wt.% IL1 due to hydrolysis of the anion with hydrogen evolution and formation of aluminium fluoride. Erosion-corrosion processes have been studied for three aluminium alloys (Al 2011, Al 6061 and Al 7075) in a 90 wt.% IL1 solution in water in the presence of {alpha}-alumina particles. The erosion-corrosion rates are around 0.2 mm/year or lower, and increase with increasing copper content to give a corrosion resistance order of Al 6061 > Al 7075 > Al 2011. Results are discussed on the basis of scanning electron microscopy (SEM) observations, energy dispersive spectroscopy (EDS) analysis, X-ray diffraction (XRD) patterns and X-ray photoelectron spectroscopy (XPS) determinations.

  8. Ejection Performance of Coated Core Pins Intended for Application on High Pressure Die Casting Tools for Aluminium Alloys Processing

    Directory of Open Access Journals (Sweden)

    P. Terek

    2017-09-01

    Full Text Available In high pressure die casting (HPDC process of aluminium alloys cast alloy soldering severely damages tool surfaces. It hampers casting ejection, reduces the casting quality and decreases the overall production efficiency. Thin ceramic PVD (physical vapor deposition coatings applied on tool surfaces successfully reduce these effects. However, their performance is still not recognised for surfaces with various topographies. In this investigation, soldering tendency of Al-Si-Cu alloy toward EN X27CrMoV51 steel, plasma nitrided steel, CrN and TiAlN duplex PVD coatings is evaluated using ejection test. The coatings were prepared to a range of surface roughness and topographies. After the tests sample surfaces were analysed by different microscopy techniques and profilometry. It was found that the ejection performance is independent of the chemical composition of investigated materials. After the ejection, the cast alloy soldering layer was found on surfaces of all tested materials. This built-up layer formed by effects of mechanical soldering, without corrosion reactions. Coated samples displayed a pronounced dependence of ejection force on surface roughness and topography. By decreasing roughness, ejection force increased, which is a consequence of intensified adhesion effects. Presented findings are a novel information important for efficient application of PVD coatings intendent for protection of HPDC tools.

  9. Fatigue performance of matching and dissimilar joints in aluminium alloys 5083-H111 and 6061-T651 after fully automatic pulsed GAMW using ER5356 filler wire

    CSIR Research Space (South Africa)

    Mutombo, K

    2010-08-31

    Full Text Available The tensile strength and fatigue properties of Al5083-H111 welded with aluminium-magnesium alloyed ER5356 filler wire appeared similar to those of the base metal. This joint failed in the weld metal as a result of a slight reduction in hardness...

  10. Improvement of the surface properties of aluminium by the formation of intermetallic phases and metal matrix composites during laser surface alloying

    CSIR Research Space (South Africa)

    Mabhali, Luyolo AB

    2011-05-01

    Full Text Available , beam spot size, laser scan speed and powder feed rate have to be controlled to achieve the desired surface properties. This research project is a preliminary investigation into laser surface alloying of aluminium AA1200 using a 4.4 kW Rofin Sinar Nd...

  11. Characterization of friction stir welded joints of the aluminium alloy AA 2024-T3 by laser extensometry; Reibruehrschweissungen aus Aluminium charakterisieren. Lokale Dehnungsmessung mit Laserextensometer

    Energy Technology Data Exchange (ETDEWEB)

    Biallas, G. [Paderborn Univ. (Germany). Lehrstuhl fuer Werkstoffkunde; Dalle Donne, C. [DLR Deutsches Zentrum fuer Luft- und Raumfahrt e.V., Koeln (Germany). Inst. fuer Werkstoff-Forschung

    2000-07-01

    Friction stir welding (FSW) is a simple, clean and innovative solid state joining process for light metals. In contrast to conventional welding, FSW is performed at temperatures below the melting point. Therefore, detrimental microstructural changes and cracking during the solidification of the weld pool are avoided. Within certain limits, the excellent mechanical properties of friction stir welds are further improved by an increase of the welding or transverse speed. This is shown by localized strain measurements during tensile tests of friction stir welded sheet material of the aluminium alloy AA 2024-T3. The local strains are measured in the welding region and in the heat affected zone by a laser extensometer. It turned out that the increase in strength with increasing weld speed has to be related to the more homogeneous strain distribution in the welding region and heat affected zone. (orig.) [German] Das Reibruehrschweissen oder Friction Stir Welding (FSW) ist ein einfaches und sauberes Fuegeverfahren fuer Leichtmetalle. Im Gegensatz zu konventionellen Schmelz-Schweissverfahren erfolgt der FSW-Prozess bei Temperaturen unterhalb des Schmelzpunktes von Leichtmetalllegierungen, was Gefuegeveraenderungen und Rissbildungen beim Erstarren der Schmelze vermeidet. Die guten mechanischen Eigenschaften reibruehrgeschweisster Verbindungen lassen sich durch eine Erhoehung des Vorschubs weiter verbessern, wie Zugversuche an geschweissten Blechen der Aluminiumlegierung AA 2024-T3 zeigen. Ueber lokale Dehnungsmessungen im Nahtbereich wird mit dem Laserextensometer nachgewiesen, dass die Ursache der gleichzeitigen Zunahme von Festigkeit und Verformbarkeit in einem homogenen Verformungszustand liegt. (orig.)

  12. Overload effects on a ferritic-baintic steel and a cast aluminium alloy: two very different behaviours

    Energy Technology Data Exchange (ETDEWEB)

    Saintier, N. [Arts et Metiers Paris Tech, I2M, UMR CNRS, Universite Bordeaux 1, Talene Cedex (France); El Dsoki, C.; Kaufmann, H.; Sonsino, C.M. [Fraunhofer-Institute for Structural Durability and System Reliability LBF, Darmstadt (Germany); Dumas, C. [RENAULT, Technocentre, Guyancourt Cedex (France); Voellmecke, F.J. [BORBET GmbH, Hallenberg-Hesborn (Germany); Palin-Luc, T.; Bidonard, H.

    2011-10-15

    Load controlled fatigue tests were performed up to 10{sup 7} cycles on flat notched specimens (K{sub t} = 2.5) under constant amplitude and variable amplitude loadings with and without periodical overloads. Two materials are studied: a ferritic-bainitic steel (HE400M steel) and a cast aluminium alloy (AlSi7Mg0.3). These materials have a very different cyclic behaviour: the steel exhibits cyclic strain softening whereas the Al alloy shows cyclic strain hardening. The fatigue tests show that, for the steel, periodical overload applications reduce significantly the fatigue life for fully reversed load ratio (R{sub {sigma}} = -1), while they have no influence under pulsating loading (R{sub {sigma}} = 0). For the Al alloy overloads have an effect (fatigue life decreasing) only for variable amplitude loadings. The detrimental effect of overloads on the steel is due to ratcheting at the notch root which evolution is overload's dependent. (Copyright copyright 2011 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

  13. Design of Laser Welding Parameters for Joining Ti Grade 2 and AW 5754 Aluminium Alloys Using Numerical Simulation

    Directory of Open Access Journals (Sweden)

    Mária Behúlová

    2017-01-01

    Full Text Available Joining of dissimilar Al-Ti alloys is very interesting from the point of view of weight reduction of components and structures in automotive or aerospace industries. In the dependence on cooling rate and chemical composition, rapid solidification of Al-Ti alloys during laser welding can lead to the formation of metastable phases and brittle intermetallic compounds that generally reduce the quality of produced weld joints. The paper deals with design and testing of welding parameters for preparation of weld joints of two sheets with different thicknesses from titanium Grade 2 and AW 5754 aluminium alloy. Temperature fields developed during the formation of Al-Ti butt joints were investigated by numerical simulation in ANSYS software. The influence of laser welding parameters including the laser power and laser beam offset on the temperature distribution and weld joint formation was studied. The results of numerical simulation were verified by experimental temperature measurement during laser beam welding applying the TruDisk 4002 disk laser. The microstructure of produced weld joints was assessed by light microscopy and scanning electron microscopy. EDX analysis was applied to determine the change in chemical composition across weld joints. Mechanical properties of weld joints were evaluated using tensile tests and Vickers microhardness measurements.

  14. The effect of dispersoids on the grain refinement mechanisms during deformation of aluminium alloys to ultra-high strains

    International Nuclear Information System (INIS)

    Apps, P.J.; Berta, M.; Prangnell, P.B.

    2005-01-01

    The effect of fine dispersoids on the mechanisms and rate of grain refinement has been investigated during the severe deformation of a model aluminium alloy. A binary Al-0.2Sc alloy, containing coherent Al 3 Sc dispersoids, of ∼20 nm in diameter and ∼100 nm spacing, has been deformed by equal channel angular extrusion to an effective strain of ten. The resulting deformation structures were quantitatively analysed using high-resolution electron backscattered diffraction orientation mapping, and the results have been compared to those obtained from a single-phase Al-0.13Mg alloy, deformed under identical conditions. The presence of fine, non-shearable, dispersoids has been found to homogenise slip, retard the formation of a cellular substructure and inhibit the formation of microshear bands during deformation. These factors combine to reduce the rate of high-angle grain boundary generation at low to medium strains and, hence, retard the formation of a submicron grain structure to higher strains during severe deformation

  15. Cr(VI)-free pre-treatments for adhesive bonding of aerospace aluminium alloys

    NARCIS (Netherlands)

    Abrahami, S.T.

    2016-01-01

    For more than six decades, chromic acid anodizing (CAA) has been the central process in the surface pre-treatment of aluminium for adhesively bonded aircraft structures in Europe. Unfortunately, this electrolyte contains hexavalent chromium (Cr(VI)), a compound known for its toxicity and

  16. Laser surface alloying of aluminium with WC+Co+NiCr for improved wear resistance

    CSIR Research Space (South Africa)

    Nath, S

    2012-03-01

    Full Text Available In the present study, laser surfac ealloying of aluminium with WC + Co + NiCr (in the ratio of 70:15:15) has been conducted using a 5 kW continuous wave (CW) Nd:YAG laser (at a beam diameter of 0.003 m), with the output power ranging from 3 to 3.5 k...

  17. Effects of mechanical heterogeneity on the tensile and fatigue behaviours in a laser-arc hybrid welded aluminium alloy joint

    International Nuclear Information System (INIS)

    He, Chao; Huang, Chongxiang; Liu, Yongjie; Li, Jiukai; Wang, Qingyuan

    2015-01-01

    Highlights: • Full field strain evolution was characterized using DIC method in fatigue test. • The differences of fatigue failure mechanism between HAZ and FZ were discussed. • Porosity in FZ significantly influenced high cycle fatigue behaviours of the weld. - Abstract: The effects of mechanical heterogeneity on the tensile and high cycle fatigue (10 4 –10 7 cycles) properties were investigated for laser-arc hybrid welded aluminium alloy joints. Tensile–tensile cyclic loading with a stress ratio of 0.1 was applied in a direction perpendicular to the weld direction for up to 10 7 cycles. The local mechanical properties in the tensile test and the accumulated plastic strain in the fatigue test throughout the weld’s different regions were characterized using a digital image correlation technique. The tensile results indicated heterogeneous tensile properties throughout the different regions of the aluminium welded joint, and the heat affected zone was the weakest region in which the strain localized. In the fatigue test, the accumulated plastic strain evolutions in different subzones of the weld were analyzed, and slip bands could be clearly observed in the heat affected zone. A transition of fatigue failure locations from the heat affected zone caused by accumulated plastic strain to the fusion zone induced by fatigue crack at pores could be observed under different cyclic stress levels. The welding porosity in the fusion zone significantly influences the high cycle fatigue behaviour

  18. Multi-Objective Optimization of Friction Stir Welding of Aluminium Alloy Using Grey Relation Analysis with Entropy Measurement Method

    Directory of Open Access Journals (Sweden)

    SAURABH KUMAR GUPTA

    2015-01-01

    Full Text Available The present research focus on optimization of Friction Stir Welding (FSW process parameters for joining of AA6061 aluminium alloy using hybrid approach. The FSW process parameters considered are tool rotational speed, welding speed and axial force. The quality characteristics considered are tensile strength (TS and percentage of tensile elongation (TE. Taguchi based experimental design L9 orthogonal array is used for determining the experimental results. The value of weights corresponding to each quality characteristic is determined by using the entropy measurement method so that their importance can be properly explained. Analysis of Variance (ANOVA is used to determine the contribution of FSW process parameters. The confirmation tests also have been done for verifying the results.

  19. Microstructure, local and global mechanical properties of friction stir welds in aluminium alloy 6005A-T6

    International Nuclear Information System (INIS)

    Simar, A.; Brechet, Y.; Meester, B. de; Denquin, A.; Pardoen, T.

    2008-01-01

    The effect of the welding speed on the microstructure, local and overall mechanical properties of friction stir welded joints has been investigated in the aluminium alloy 6005A-T6. The fine hardening precipitation within the heat-affected zone has been characterized by differential scanning calorimetry (DSC) and transmission electron microscopy (TEM). Post-welding heat treatments have been applied to obtain indications on the level of solid solution supersaturation in the as welded state. The local mechanical behaviour was determined using thin specimens extracted from various regions of the weld. The overall properties were measured on samples cut perpendicular to the weld. Specific attention was devoted to the relationship between the local microstructure and local hardening properties in the weakest region, which govern the overall strength and ductility of the welds

  20. Electrochemical corrosion characteristics of aluminium alloy 6061 T6 in demineralized water containing 0.1 % chloride ion

    International Nuclear Information System (INIS)

    Zaifol Samsu; Muhammad Daud; Siti Radiah Mohd Kamarudin; Mohd Saari Ripin; Rusni Rejab; Mohd Shariff Sattar

    2012-01-01

    Direct current electrochemical method is one of the techniques has been used to study the corrosion behaviour of metal/alloy in its environment. This paper attempts to investigate the corrosion behaviour of Al 6061 T6 immersed in Reactor TRIGA Mark II pool water containing about 0.1% NaCl content. The result shown that the corrosion rate value of the aluminium 6061 T6 increased with the presence of 0.1 % Ion Chloride content in the demineralized water reactor pool as compared to normal demineralized water. This is due to aggressiveness of chloride ion attack to metal surface. Beside corrosion rate analysis, the further tests such as corrosion behaviour diagram, cyclic polarization have been carried and the results have been reported. (author)

  1. Prediction of shear and tensile strength of the diffusion bonded AA5083 and AA7075 aluminium alloy using ANN

    International Nuclear Information System (INIS)

    Sagai Francis Britto, A.; Raj, R. Edwin; Mabel, M. Carolin

    2017-01-01

    Diffusion bonding is a pressure welding technique to establish bonds by inter diffusion of atoms. Bonding characteristics were generated by varying the significant process conditions such as the bonding temperature, the pressing load and the duration of pressure while bonding the aluminium alloys AA5083 and AA7075. Deriving analytical correlation with the process variables to weld strength is quite involved due to the non-linear dependency of the process variables with the mechanical strength of the joints. An arbitrary function approximation mechanism, the artificial neural network (ANN) is therefore employed to develop the models for predicting the mechanical properties of the bonded joints. Back propagation technique, which alters the network weights to minimize the mean square error was used to develop the ANN models. The models were tested, validated and found to be satisfactory with good prediction accuracy.

  2. Characterization of AA7050 aluminium alloy processed by ECAP; Caracterizacao da liga de aluminio AA7050 processada por ECAP

    Energy Technology Data Exchange (ETDEWEB)

    Cardoso, K.R.; Guido, V. [Universidade do Vale do Paraiba (UNIVAP), Sao Jose dos Campos, SP (Brazil). Inst. de Pesquisa e Desenvolvimento; Travessa, D.N. [Empresa Brasileira de Aeronautica (EMBRAER), Sao Jose dos Campos, SP (Brazil); Jorge Junior, A.M. [Universidade Federal de Sao Carlos (DEMa/UFSCar), SP (Brazil). Dept. de Engenharia de Materiais

    2010-07-01

    The commercial AA7050 aluminium alloy in the solution heat treated condition (W) was processed by ECAP through route A. Two pressing temperatures (room and 150 deg C and velocities (5 and 30mm/min) were used, as well as different number of passes. The effect of such variables on the microstructure evolution was evaluated using optical and transmission electron microscopy with EDX microanalysis, and xray diffraction. It was found that the microstructure has been refined by ECAP, as a result of subgrains formed within deformation bands. ECAP at 150 deg C resulted in intense precipitation of plate like {eta} phase, which evolves to equiaxial morphology as the number of passes increases. (author)

  3. Analysis of Thermo-Elastic Fracture Problem during Aluminium Alloy MIG Welding Using the Extended Finite Element Method

    Directory of Open Access Journals (Sweden)

    Kuanfang He

    2017-01-01

    Full Text Available The thermo-elastic fracture problem and equations are established for aluminium alloy Metal Inert Gas (MIG welding, which include a moving heat source and a thermoelasticity equation with the initial and boundary conditions for a plate structure with a crack. The extended finite element method (XFEM is implemented to solve the thermo-elastic fracture problem of a plate structure with a crack under the effect of a moving heat source. The combination of the experimental measurement and simulation of the welding temperature field is done to verify the model and solution method. The numerical cases of the thermomechanical parameters and stress intensity factors (SIFs of the plate structure in the welding heating and cooling processes are investigated. The research results provide reference data and an approach for the analysis of the thermomechanical characteristics of the welding process.

  4. Effect of weld morphology on mechanical response and failure of friction stir welds in a naturally aged aluminium alloy

    International Nuclear Information System (INIS)

    Imam, Murshid; Biswas, Kajal; Racherla, Vikranth

    2013-01-01

    Highlights: ► Friction stir welds of AA 6063-T4 are obtained using three tool pin profiles. ► Signature of weld defects in mechanical response of welds is investigated. ► Correlation between peak temperatures in HAZs and their hardness is studied. ► Reasons for strengthening of WNZ and softening of HAZs are found using TEM and XRD. ► A FEM model for the weld zone is developed and validated. -- Abstract: Friction stir butt welds in 6063-T4 aluminium alloy were obtained using square and two tapered tool pin profiles. Tensile tests at 0°, 45°, and 90° to the weld line, hardness contours in the weld cross-section, temperatures in the heat affected zones, cross-sectional macrographs, transmission electron micrographs, and X-ray diffraction studies were used to characterize the welds. In transverse weld specimen, tunnel defects appearing at higher weld speeds for tapered pin profiles, were found to result in mechanical instabilities, i.e. sharp drops in load–displacement curves, much before macroscopic necking occured. Further, in comparison to the base metal, a marked reduction in ductility was observed even in transverse specimen with defect free welds. Hardness contours in the weld cross-section suggest that loss in ductility is due to significant softening in heat affected zone on the retreating side. Transmission electron microscopy images demonstrate that while recovery and overaging are responsible for softening in the heat affected zone, grain size refinement from dynamic recrystallization is responsible for strengthening of the weld nugget zone. X-ray diffraction studies in the three weld zones: weld nugget zone, heat affected zone, and the base metal corroborate these findings. A weld zone model, for use in forming simulations on friction stir welded plates of naturally aged aluminium alloys, was proposed based on mechanical characterization tests. The model was validated using finite element analysis.

  5. Determination of Optimal Parameters for Diffusion Bonding of Semi-Solid Casting Aluminium Alloy by Response Surface Methodology

    Directory of Open Access Journals (Sweden)

    Kaewploy Somsak

    2015-01-01

    Full Text Available Liquid state welding techniques available are prone to gas porosity problems. To avoid this solid state bonding is usually an alternative of preference. Among solid state bonding techniques, diffusion bonding is often employed in aluminium alloy automotive parts welding in order to enhance their mechanical properties. However, there has been no standard procedure nor has there been any definitive criterion for judicious welding parameters setting. It is thus a matter of importance to find the set of optimal parameters for effective diffusion bonding. This work proposes the use of response surface methodology in determining such a set of optimal parameters. Response surface methodology is more efficient in dealing with complex process compared with other techniques available. There are two variations of response surface methodology. The one adopted in this work is the central composite design approach. This is because when the initial upper and lower bounds of the desired parameters are exceeded the central composite design approach is still capable of yielding the optimal values of the parameters that appear to be out of the initially preset range. Results from the experiments show that the pressing pressure and the holding time affect the tensile strength of jointing. The data obtained from the experiment fits well to a quadratic equation with high coefficient of determination (R2 = 94.21%. It is found that the optimal parameters in the process of jointing semi-solid casting aluminium alloy by using diffusion bonding are the pressing pressure of 2.06 MPa and 214 minutes of the holding time in order to achieve the highest tensile strength of 142.65 MPa

  6. INFLUENCE OF MECHANICAL ALLOYING AND LEAD CONTENT ON MICROSTRUCTURE, HARDNESS AND TRIBOLOGICAL BEHAVIOR OF 6061 ALUMINIUM ALLOYS

    Directory of Open Access Journals (Sweden)

    M. Paidpilli

    2017-03-01

    Full Text Available In the present work, one batch of prealloyed 6061Al powder was processed by mixing and another one was ball milled with varying amount of lead content (0-15 vol. %. These powders were compacted at 300MPa and sintered at 590˚C under N2. The instrumented hardness and the young’s modulus of as-sintered 6061Al-Pb alloys were examined as a function of lead content and processing route. The wear test under dry sliding condition has been performed at varying loads (10-40 N using pin-on-disc tribometer. The microstructure and worn surfaces have been investigated using SEM to evaluate the change in topographical features due to mechanical alloying and lead content. The mechanically alloyed materials showed improved wear characteristics as compared to as-mixed counterpart alloys. Delamination of 6061Al-Pb alloys decreases up to an optimum lead composition in both as-mixed and ball-milled 6061Al-Pb alloys. The results indicated minimum wear rate for as-mixed and ball-milled 6061Al alloy at 5 and 10 vol. % Pb, respectively.

  7. Investigations into the corrosion resistance of copper aluminium alloys. Effect of phosphorus as corrosion resistant third alloying element in the ternary system CuAl20P1

    International Nuclear Information System (INIS)

    Allwardt, A.

    1997-01-01

    The effect of phosphorus on the corrosion resistance of Al-bronzes is studied in detail in this work. A literature review showed that there are a lot of things known about the microstructure and the mechanical properties of Al-bronzes. In spite of their corrosion resistance the corrosion properties and the structure of the protective oxide films of Al-bronzes were seldom a matter of interest. Systematic studies of the influence of different alloying elements on the oxide film and the corrosion properties are rare. Therefore, it is not possible to predict the corrosion resistance of Al-bronzes, made by alloying particular elements. The high corrosion resistance of the new alloy CuAl 20 P 1 was the reason to investigate the influence of phosphorus on the corrosion properties of Al-bronzes in more detail. A systematic study of the microstructure and the corrosion properties of Cu, CuP x , CuAl 20 and CuAl 20 P x offers an insight into the effect of aluminium and phosphorus on the formation of the oxide film on Al-bronzes. It was found that there exists a critical amount of 1 at.-% of phosphorus. Above and below this amount the corrosion resistance becomes worse. This behaviour could be explained by XPS-and electrochemical measurements. Although there are still some questions about the influence of phosphorus on the corrosion resistance of Al-bronzes, this work has produced some important results, which in the future may be helpful to develop new high corrosion resistant Al-bronzes more efficiently: - on clean surface Al-bronze, the oxidation of Al and Cu takes place simultaneously, - Al promotes the formation of Cu 2 O but impedes the formation of Cu(II)-oxide/-hydride in neutral solutions, - P impedes the formation of Cu 2 O and as a consequence promotes the formation of aluminium oxide. This results in a higher amount of Al in the oxide film on the surface of the alloy, which leads to a better corrosion resistance. (author) figs., tabs., 106 refs

  8. Effect of Lubrication on Sliding Wear of Red Mud Particulate Reinforced Aluminium Alloy 6061

    OpenAIRE

    N. Panwar; R.P. Poonia; G. Singh; R. Dabral; A. Chauhan

    2017-01-01

    In present study, Red mud, an industrial waste, has been utilized as a reinforcement material to fabricate Aluminium 6061 matrix based metal matrix composite. Taguchi L18 orthogonal array has been employed for fabrication of composite castings and for conducting the tribological experimentation. ANOVA analysis has been applied to examine the effect of individual parameters such as sliding condition: dry and wet, reinforcement weight fraction, load, speed, and sliding distance on specific wear...

  9. Recycling of Uranium from Uranium-Aluminium alloys by Chlorination with HCl(g)

    OpenAIRE

    MEIER ROLAND; SOUCEK Pavel; MALMBECK Rikard; FANGHAENEL Thomas

    2012-01-01

    Much attention has been paid to the handling of metallic nuclear fuel, which can offer a safe and more secure fuel cycle. To ensure this, it is essential to gain a thorough understanding of the related fundamental processes to scientifically assess the safety aspects. To this aim, a pyrochemical process for the recycling of actinides is being investigated in ITU. It is consisting of anodic dissolution of all actinides to a molten salt bath and electrochemical reduction on solid aluminium cath...

  10. Effect of Mg, Si and Cu content on the microstructure of dilute 6000 series aluminium alloys

    Energy Technology Data Exchange (ETDEWEB)

    Jaafar, Aiza, E-mail: cnaizza@gmail.com [School of Materials and Mineral Resources Engineering, Universiti Sains Malaysia, 14300 Nibong Tebal, Penang (Malaysia); Rahmat, Azmi [School of Materials Engineering, Universiti Malaysia Perlis, Taman Muhibah, 02600 Jejawi, Arau Perlis (Malaysia); Hussain, Zuhailawati [School of Materials and Mineral Resources Engineering, Universiti Sains Malaysia, 14300 Nibong Tebal, Penang (Malaysia); Zainol, Ismail [Chemistry Department, Faculty of Science and Mathematics, Universiti Pendidikan Sultan Idris, 35900 Tanjung Malim, Perak (Malaysia)

    2011-09-01

    Highlights: > The main precipitates formed in the artificially aged dilute alloys are needle-shaped. > The ageing temperature of 100 deg. C is found to be too low to form precipitates. > The number density of precipitates increases with increasing solute contents. > There is a correlation between Mg{sub 2}Si, Si and Cu content and alloys microstructure. > The precipitates kinetics is faster in the less dilute alloys. - Abstract: The effect of Mg, Si and Cu content on the microstructural development during ageing treatment of dilute 6000 series alloys have been investigated using transmission electron microscopy (TEM). Four dilute alloys were used in this study. These alloys were subjected to quenching and artificial ageing at 100 deg. C, 185 deg. C and 300 deg. C. The microstructural developments of the precipitates formed were monitored by TEM. The ageing temperature of 100 deg. C was found to be too low to form precipitates. It was found that needle or rod-shaped precipitates were formed in the alloys after ageing at 185 and 300 deg. C. Prolong ageing up to 1000 h at 300 deg. C resulted in the formation of Mg{sub 2}Si precipitate that coexists with the type of AlFeSi and Si precipitates. The results show a correlation between the Mg{sub 2}Si, Si and Cu content on the microstructure of the four dilute alloys after ageing treatment.

  11. Effect of Mg, Si and Cu content on the microstructure of dilute 6000 series aluminium alloys

    International Nuclear Information System (INIS)

    Jaafar, Aiza; Rahmat, Azmi; Hussain, Zuhailawati; Zainol, Ismail

    2011-01-01

    Highlights: → The main precipitates formed in the artificially aged dilute alloys are needle-shaped. → The ageing temperature of 100 deg. C is found to be too low to form precipitates. → The number density of precipitates increases with increasing solute contents. → There is a correlation between Mg 2 Si, Si and Cu content and alloys microstructure. → The precipitates kinetics is faster in the less dilute alloys. - Abstract: The effect of Mg, Si and Cu content on the microstructural development during ageing treatment of dilute 6000 series alloys have been investigated using transmission electron microscopy (TEM). Four dilute alloys were used in this study. These alloys were subjected to quenching and artificial ageing at 100 deg. C, 185 deg. C and 300 deg. C. The microstructural developments of the precipitates formed were monitored by TEM. The ageing temperature of 100 deg. C was found to be too low to form precipitates. It was found that needle or rod-shaped precipitates were formed in the alloys after ageing at 185 and 300 deg. C. Prolong ageing up to 1000 h at 300 deg. C resulted in the formation of Mg 2 Si precipitate that coexists with the type of AlFeSi and Si precipitates. The results show a correlation between the Mg 2 Si, Si and Cu content on the microstructure of the four dilute alloys after ageing treatment.

  12. Comparative Investigation on Modal analysis of LM25 Aluminium alloy with other Aluminim alloys using Finite element analysis software

    Science.gov (United States)

    Arunkumar, S.; Baskaralal, V. P. M.; Muthuraman, V.

    2017-03-01

    The rudimentary steps of the modal analysis and simulation are carried out. The modal analysis is carried out on the different Aluminum Alloys cantilever beam. The cantilever beam is designed in the graphical environment of the ANSYS. The cantilever beam was fine-tuned on one end with all degree of liberation on this end were taken, beam cannot move and rotate. Mode shapes and natural frequencies are premeditated in platforms ANSYS with arithmetical formulation of the direct solver including the block Lanczos method. Aluminum alloys are widely utilized in much application due to their estimable weight to vigor property. Many examination works have been distributed out to make developments the mechanical properties of aluminum alloys. The composition of alloying elements plays a consequential role in deciding the properties of an alloy. In this study a numerical analysis implement i.e., finite element analysis (FEA) is utilized. The work obtainable in this paper is aimed at the study of effect of modal analysis of different aluminum alloys. The modeling and analysis is carried out utilizing ANSYS FEA software. A modal analysis is carried out to understand the modes of frequency demeanor of the material considered. The modal analysis play a vital role in the design of components subjected to high vibration.

  13. Crystalline textures in aluminium-uranium alloys determined by neutron diffraction

    International Nuclear Information System (INIS)

    Azevedo, Adriana M.V. de

    1979-08-01

    Textures of hot-rolled aluminum-uranium alloys and aluminum were determined by neutron diffraction. Sheets of alloys containing 8.0, 21.5 and 23.7 wt pct U, as well as pure aluminum, were obtained in a stepped rolling process, 15% reduction each step, 75% total reduction. During the rolling the temperature was 600 deg C. Alloys with low uranium contents are two phase systems in which an intermetallic compound UAl 4 , orthorhombic, is dispersed in a pure aluminum matrix. The addition of a few percent of Si in such alloys leads to the formation of UAl 3 , simple cubic, instead of UAl 4 . The Al - 23.7 wt pct U alloy was prepared with 2,2 wt pct of Si. The (200), (040) and (121) pole figures of the phase UAl 4 of the Al-21.5 wt pct U alloy show a high degree of orientation defined as (010) |100|. The (111) reflection of the phase UAl 3 of the Al-23.7 wt pct U alloy showed no preferred orientations. The (111) pole figures of the matrix of the alloys 21.5 and 23.7 wt pct U can be described satisfactorily by the same weakly developed texture, namely {113} . The (111) pole figure for the matrix of the Al-8.0 wt pct U alloy has the texture {113} , which is an intermediate case between the {110} texture of aluminum and the texture of the higher uranium-bearing alloys. For pure aluminum and the 8.0pct alloy the degree of the textures is still weak however higher than in the preceding cases. The (200) and (121) pole figures for the UAl 4 of the 8.0 pct alloy show the same texture as the 21,5 pct alloy though with considerable more spread. The results indicate that the texture of the matrix is more dependent on the uranium concentration than on the texture of the intermetallic phases. This work also presents an improvement in the technique applied to texture measurements by using a sample fully bathed in the neutron beam. The method takes advantage of the low neutron absorption of the studied materials as well as of the negligible variation in the multiple scattering which

  14. Influence of Welding Process and Post Weld Heat Treatment on Microstructure and Pitting Corrosion Behavior of Dissimilar Aluminium Alloy Welds

    Science.gov (United States)

    Venkata Ramana, V. S. N.; Mohammed, Raffi; Madhusudhan Reddy, G.; Srinivasa Rao, K.

    2018-03-01

    Welding of dissimilar Aluminum alloy welds is becoming important in aerospace, shipbuilding and defence applications. In the present work, an attempt has been made to weld dissimilar aluminium alloys using conventional gas tungsten arc welding (GTAW) and friction stir welding (FSW) processes. An attempt was also made to study the effect of post weld heat treatment (T4 condition) on microstructure and pitting corrosion behaviour of these welds. Results of the present investigation established the differences in microstructures of the base metals in T4 condition and in annealed conditions. It is evident that the thickness of the PMZ is relatively more on AA2014 side than that of AA6061 side. In FS welds, lamellar like shear bands are well noticed on the top of the stir zone. The concentration profile of dissimilar friction stir weld in T4 condition revealed that no diffusion has taken place at the interface. Poor Hardness is observed in all regions of FS welds compared to that of GTA welds. Pitting corrosion resistance of the dissimilar FS welds in all regions was improved by post weld heat treatment.

  15. Effect of turning parameters on surface roughness of A356/5% SiC composite produced by electromagnetic stir casting

    Energy Technology Data Exchange (ETDEWEB)

    Dwivedi, S. P.; Kumar, Sudhir; Kumar, Ajay [Noida Institute of Engineering Technology, U.P (India)

    2012-12-15

    In the present investigation, A356 alloy 5 wt% SiC composite is fabricated by electromagnetic stir casting process. An attempt has been made to investigate the effect of CNC lathe process parameters like cutting speed, depth of cut, and feed rate on surface roughness during machining of A356 alloy 5 wt% SiC particulate metal-matrix composites in dry condition. Response surface methodology (Box Behnken Method) is chosen to design the experiments. The results reveal that cutting speed increases surface roughness decreases, whereas depth of cut and feed increase surface roughness increase. Optimum values of speed (190 m/min), feed (0.14 mm/rev) and depth of cut (0.20 mm) during turning of A356 alloy 5 wt% SiC composites to minimize the surface roughness (3.15>m) have been find out. The mechanical properties of A356 alloy 5 wt% SiC were also analyzed.

  16. XPS Study of Chemical Changes on the La/Ce Treated Surface of A361 Aluminium Alloy Exposed to Air at Temperatures up to 500∘C

    Directory of Open Access Journals (Sweden)

    A. Pardo

    2009-01-01

    Full Text Available The chemical changes that take place on the rare earth treated surface of the A361 aluminium alloy exposed to air at temperatures between 100 and 500∘C have been examined using X-ray photoelectron spectroscopy (XPS. The most notable features discussed in this work are the disappearance of Mg and Si signals at the tested temperatures and disappearance of the Ce signal at temperatures of 400–500∘C. The biphasic microstructure of the A361 alloy, constituted by close to 12 wt% Si and the Al matrix, plays an important role in many of the results obtained. The notable growth of aluminium oxide across the conversion coating in the case of the Ce-treated surface is related to the structural transformation experienced by the cerium oxide coating at 400–500∘C.

  17. Effect of titanium or/and aluminium on 1 MeV electron swelling of low chromium Fe-Cr10-Ni20-25 type alloys

    International Nuclear Information System (INIS)

    Seran, J.L.

    1985-10-01

    Simulation swelling results with 1 MeV electrons at 500 0 C and 600 0 C on many low chromium steels hardened in solid solution or by γ' phase precipitation by titanium or/and aluminium additions. These new steels, for some chemical compositions, may have a resistance to swelling upper than the classical reference materials such as 316 Ti type materials. The alloys hardened by precipitation and then highly doped in titanium and/or aluminium do not seem very propositions because cavity germination is important at medium temperatures. In the contrary, the under-stabilized steels are also to rule-out because their swelling speed is prohibitive. Between these two extremes, 10-25 alloys hardened in solid solution by some tenth per cent of titanium could be the most interesting one, at least at temperatures higher than 500 0 C [fr

  18. The positron annihilation technique applied to the study of inhomogeneous solids: aluminium alloys, layered compound 1T-TaS2

    International Nuclear Information System (INIS)

    Boileau, F.

    1983-01-01

    This thesis is an experimental investigation of inhomogeneous solids using the standard positron annihilation techniques (angular correlation of annihilation γ-rays, Doppler broadening, lifetime). The investigations are concerned with different types of more or less extended defects. The effect of impurities on the migration properties of the vacancy-type defects is first studied in electron irradiated and quenched aluminium alloys. The affinity of the positron for precipitates formed in supersatured aluminium alloys is shown experimentally and explained. The effects of low dimensionality on the behaviour of the positron are then studied in the layered dichalcogenide 1T-TaS 2 where the presence of charge density waves modifies the electronic properties. An experimental and theoretical insight on the Fermi surface of this compound has been successfully undertaken [fr

  19. Effect of post weld heat treatment on tensile properties and microstructure characteristics of friction stir welded armour grade AA7075-T651 aluminium alloy

    Directory of Open Access Journals (Sweden)

    P. Sivaraj

    2014-03-01

    Full Text Available This paper reports the effects of post weld heat treatments, namely artificial ageing and solution treatment followed by artificial ageing, on microstructure and mechanical properties of 12 mm thick friction stir welded joints of precipitation hardenable high strength armour grade AA7075-T651 aluminium alloy. The tensile properties, such as yield strength, tensile strength, elongation and notch tensile strength, are evaluated and correlated with the microhardness and microstructural features. The scanning electron microscope is used to characterie the fracture surfaces. The solution treatment followed by ageing heat treatment cycle is found to be marginally beneficial in improving the tensile properties of friction stir welds of AA7075-T651 aluminium alloy.

  20. Effect of post annealing temperatures on microstructures and mechanical properties of cryorolled 5052 aluminium sheet alloy

    Science.gov (United States)

    Anas, N. M.; Umar, Z. A. A.; Zuhailawati, H.; Anasyida, A. S.

    2017-07-01

    The effect of post annealing temperature of cryorolled 5052 Al alloy after cryorolling process at 30% thickness reduction was investigated, focusing on the evolution of microstructures and mechanical properties. The evolution of microstructure was investigated using optical microscopy (OM). The mechanical behaviour of the samples have been evaluated through Vickers hardness and tensile test performed at room temperature. The results showed that the post annealing on cryorolled 5052 Al alloy have enhanced the ductility with sacrificing the hardness and strength. The lattice strain of post annealed 5052 Al alloy decreased with increasing of annealing temperatures. The evolution of microstructure of the post annealed 5052 Al alloy showed equiaxed grains at 200°C and grain coarsening as post annealing temperature increases to 350°C. The result of crystallite size confirmed the grain size increased as the post annealing temperature rises.

  1. Research of gas release during crystallization of aluminium and its alloys

    OpenAIRE

    Трегубенко, Геннадий Николаевич

    2015-01-01

    The problem of gas porosity formation in the manufacture of aluminum structural or cast porous alloys is discussed and some results of our research in this area are shown in the article. The main aim of the research is to investigate the influence of various technological, physical and chemical factors on the process of hydrogen gas release during crystallization of aluminum and its alloys. Using system simulation allows a scientist to investigate fully the flow of a process. In this paper to...

  2. Fatigue behavior of GMAW welded Aluminium alloy AA7020; Comportamiento a fatiga de uniones soldadas GMAW de la aleacion de aluminio AA 7020

    Energy Technology Data Exchange (ETDEWEB)

    Bloem, C. A.; Salvador, M. D.; Amigo, V.; Vicente, A.

    2007-07-01

    The aim of this investigation is to evaluate the influence on the fatigue behavior by the finishing of the bulge in a welded aluminium-zinc-magnesium alloy AA7020. It was determined that total or partial elimination of the bulge has very little influence on its behavior, giving a very similar result on both cases, where one is better than the other by only 3%. (Author) 20 refs.

  3. Effect of 1.0% Ni on high-temperature impression creep and hardness of recycled aluminium alloy with high Fe content

    Science.gov (United States)

    Faisal, M.; Mazni, Noor; Prasada Rao, A. K.

    2018-03-01

    Reported work focusses on the effect of 1.0% Ni addition on the microstructure, high- temperature impression creep and thereby the hardness of recycled Al-alloy containing >2wt% Fe, obtained from automotive scrap. Present studies have shown that the addition of 1.0% Ni have supress the formation of α-phase (Al5FeSi) by supressing the peritectic transformation of β-phase (Al8Fe2Si). Such suppression is found to improve the hardness and high-temperature impression creep of the recycled aluminium alloy.

  4. Effect of Al–5Ti–1B grain refiner on the microstructure, mechanical properties and acoustic emission characteristics of Al5052 aluminium alloy

    OpenAIRE

    Pattnaik, Amulya Bihari; Das, Satyabrat; Jha, Bharat Bhushan; Prasanth, Nedumbilly

    2015-01-01

    In the present investigation, the effect of Al–5Ti–1B grain refiner on the microstructure, mechanical properties and acoustic emission characteristics of Al 5052 aluminium alloy have been studied. Microstructural analysis showed the presence of primary α solid solution. No Al–Mg phase was found to be formed due to the presence of magnesium in the solid solution. The results indicated that the addition of Al–5Ti–1B grain refiner into the alloy caused a significant improvement in ultimate tensi...

  5. Light-weight steels based on iron-aluminium - influence of micro alloying elements (B, Ti, Nb) on microstructures, textures and mechanical properties

    Energy Technology Data Exchange (ETDEWEB)

    Bruex, U.; Frommeyer, G. [Dept. of Materials Technology, Max-Planck-Inst. fuer Eisenforschung GmbH, Duesseldorf (Germany); Jimenez, J. [Centro Nacional de Investigaciones Metalurgicas (C.S.I.C.), Madrid (Spain)

    2002-12-01

    The influence of the micro alloying elements B, Ti and Nb on the recrystallization texture and mechanical properties of iron aluminium light-weight steels, particularly with reference to their improved deep drawing properties was investigated. Depending on the combination of the alloying elements the microstructures of the investigated micro alloyed Fe-6Al steels are influenced by grain refinement. Likewise, variable combinations of micro alloying elements differently affect the texture. Generally, the mechanical properties are improved. However, small amounts of B, Ti and Nb cause superior deep drawing and stretch forming properties of these iron aluminium light-weight steels. The microstructures of various micro alloyed cold rolled Fe-6Al steel sheets were evaluated by optical microscopy, scanning electron microscopy (SEM) inclusively EDAX and X-ray diffraction. Texture measurements were performed using a goniometer with a closed Eulerian cradle and analysed by ODF calculations. Tensile tests were carried out at room temperature and 200 C, respectively. The deep drawing behaviour was determined by performing cupping tests and digitalised strain analysis. (orig.)

  6. APPLICATION OF CHEMICAL PRE-TREATMENT ON THE POLISHED SURFACE OF ALUMINIUM ALLOYS

    Directory of Open Access Journals (Sweden)

    Pavel Kraus

    2016-12-01

    Full Text Available This paper reports the preparation and characterization of thin transparent nanolayers with phase composition ZrF4 and different modification of SiO2 with special focus on affecting the surface roughness of the material and the way of exclusion of the thin nanolayer on the surface of the polished aluminium material. The thin nanolayer was prepared by the sol-gel method. The final treatment based on PTFE was applied on the surface of some samples. This treatment is suitable for increasing wear resistance. The films were characterized with help of SEM microscopy and EDS analysis. The surface roughness was measured with classical surface roughness tester. The results on this theme have already published but not on the polished surface of the aluminium material. The results from the experiment show the problems with application of these nanolayers because a cracks were found on the surface of the material and deformations of the layer after application of the PTFE final layer. The surface layer formation is discussed.

  7. Biochemical analysis of the Hormoconis resinae fungal mycelium in the corrosion of aeronautical aluminium alloys

    International Nuclear Information System (INIS)

    Araya, R.; Bobadilla, C.; Vera, R.; Rosales, B. M.

    2007-01-01

    Biochemical analyses of the Hormoconis resinae fungal mycelium would explain behaviour differences of corrosive and non-corrosive strains of Al and its aeronautical alloys. In previous works its aggressiveness had been studied through SEM-EDX surface analysis, electrochemical techniques and immersion testing. In this paper separation of the proteins of the mycelium produced by a non-corrosive strain and its culture along three generations was performed. cultures were prepared in batch in the presence and absence of pure Al and AA 2024, AA 7005 and AA 7075 alloys. The mycelia grown throughout the three generations increasingly recovered usual characteristics at the third replication, included their corrosiveness on Al and its alloys previously shown by all out strains. Among the bio-molecule fractions isolated and analysed during this preliminary study only the proteins revealed changes with the generation grown. When this fungal strain was cultured in the presence of alloy metal sheets electrophoresis of the protean fraction was correlative with the distinct mycelia behaviour observed, including corrosiveness on Al and its alloys. (Author) 30 refs

  8. Determination of crystalline texture in aluminium - uranium alloys by neutron diffraction

    International Nuclear Information System (INIS)

    Azevedo, A.M.V. de.

    1978-01-01

    Textures of hot-rolled aluminum-uranium alloys and of aluminum were determined by neutron diffraction. Sheets of alloys containing 8.0, 21.5 and 23.7 wt pct U, as well as pure aluminum, were obtained in a stepped rolling process, 15% reduction each step, 75% total reduction. During the rolling the temperature was 600 0 C. Alloys with low uranium contents are two phase systems in which an intermetallic compound UAl 4 , orthorhombic, is dispersed in a pure aluminum matrix. The addition of a few percent of Si in such alloys leads to the formation of UAl 3 , simple cubic, instead of UAl 4 . The Al -- 23.7 wt pct U alloy was prepared with 2,2 wt pct of Si. The results indicate that the texture of the matrix is more dependent on the uranium concentration than on the texture of the intermetallic phases. An improvement in the technique applied to texture measurements by using a sample fully bathed in the neutron beam is also presented. The method takes advantage of the low neutron absorption of the studied materials as well as of the neglibible variation in the multiple scattering which occurs in a conveniently shaped sample having a weakly developed texture. (Author) [pt

  9. Fatigue crack growth rate behaviour of friction-stir aluminium alloy AA2024-T3 welds under transient thermal tensioning

    International Nuclear Information System (INIS)

    Ilman, M.N.; Kusmono,; Iswanto, P.T.

    2013-01-01

    Highlights: • FSW enables unweldable aircraft material AA2024-T3 to be welded without cracking. • FSW applied to aircraft structure is required to have superior fatigue resistance. • Transient thermal tensioning (TTT) is being developed for stress relieving in FSW. • The fatigue crack growth rates of FSW joints under TTT are studied. - Abstract: Friction stir welding (FSW) has become a serious candidate technology to join metallic fuselage panels for the next generation of civil aircrafts. However, residual stress introduced during welding which subsequently affects fatigue performance is still a major problem that needs to be paid attention. The present investigation aims to improve fatigue crack growth resistance of friction stir aluminium alloy AA2024-T3 welds using transient thermal tensioning (TTT) treatment. In this investigation, aluminium alloy AA2024-T3 plates were joined using FSW process with and without TTT. The welding parameters used including tool rotation speed (Rt) and the plate travelling speed (v) were 1450 rpm and 30 mm/min respectively. The TTT treatments were carried out by heating both sides of friction stir weld line using moving electric heaters ahead of, beside and behind the tool at a heating temperature of 200 °C. Subsequently, a sequence of tests was carried out including microstructural examination, hardness measurement, tensile test and fatigue crack growth rate (FCGR) test in combination with fractography using scanning electron microscopy (SEM). The FCGR test was carried out using a constant amplitude fatigue experiment with stress ratio (R) of 0.1 and frequency (f) of 11 Hz whereas specimens used were centre-crack tension (CCT) type with the initial crack located at the weld nugget. Results of this investigation showed that at low ΔK, typically below 9 MPa m 0.5 , the friction stir welds under TTT treatments lowered fatigue crack growth rate (da/dN) and the lowest (da/dN) was achieved as the heaters were located ahead of

  10. A bottom-up approach for optimization of friction stir processing parameters; a study on aluminium 2024-T3 alloy

    International Nuclear Information System (INIS)

    Nadammal, Naresh; Kailas, Satish V.; Suwas, Satyam

    2015-01-01

    Highlights: • An experimental bottom-up approach has been developed for optimizing the process parameters for friction stir processing. • Optimum parameter processed samples were tested and characterized in detail. • Ultimate tensile strength of 1.3 times the base metal strength was obtained. • Residual stresses on the processed surface were only 10% of the yield strength of base metal. • Microstructure observations revealed fine equi-axed grains with precipitate particles at the grain boundaries. - Abstract: Friction stir processing (FSP) is emerging as one of the most competent severe plastic deformation (SPD) method for producing bulk ultra-fine grained materials with improved properties. Optimizing the process parameters for a defect free process is one of the challenging aspects of FSP to mark its commercial use. For the commercial aluminium alloy 2024-T3 plate of 6 mm thickness, a bottom-up approach has been attempted to optimize major independent parameters of the process such as plunge depth, tool rotation speed and traverse speed. Tensile properties of the optimum friction stir processed sample were correlated with the microstructural characterization done using Scanning Electron Microscope (SEM) and Electron Back-Scattered Diffraction (EBSD). Optimum parameters from the bottom-up approach have led to a defect free FSP having a maximum strength of 93% the base material strength. Micro tensile testing of the samples taken from the center of processed zone has shown an increased strength of 1.3 times the base material. Measured maximum longitudinal residual stress on the processed surface was only 30 MPa which was attributed to the solid state nature of FSP. Microstructural observation reveals significant grain refinement with less variation in the grain size across the thickness and a large amount of grain boundary precipitation compared to the base metal. The proposed experimental bottom-up approach can be applied as an effective method for

  11. Corrosion characteristics of an aluminium alloy in the H3PO4 - CO2 mixture

    International Nuclear Information System (INIS)

    Aljinovic, Lj.; Smith, M.; Gotovac, V.

    1998-01-01

    The Al 6063 alloy examined in this work contains silicon and magnesium capable of forming Mg 2 Si and iron, which can form an intermetallic second phase (FeAl 3 ). In order to examine the influence of temperature on the corrosion behaviour of the Al 6063 alloy, examinations were carried out in aerated H 3 PO 4 and in H 3 PO 4 saturated with CO 2 at temperatures of 20, 30, 40, and 50 C. The following electrochemical methods were applied: determination of dependence of E OCP on time, recording of anodic and cathodic polarization curves, and cyclic voltammetry. It has been observed that corrosion parameters obtained are strongly temperature dependent. They also depend on CO 2 dissolved in H 3 PO 4 . CO 2 retards cathodic and anodic reactions at all temperatures, which can be attributed to formation of a kind of mechanical passivity as alloy components react with CO 2 . (orig.)

  12. Irradiation-induced creep and microstructural development in precipitation-hardened nickel-aluminium alloys

    International Nuclear Information System (INIS)

    Ansari, I.

    1985-04-01

    Irradiation-induced creep in solid-solution Ni-8.5 at% AL and precipitation-hardened Ni-13.1 at% Al alloys was studied by bombarding miniaturized specimens with 6.2 MeV protons at 300 0 C under different tensile stresses. After irradiation transmission electron microscopic (TEM) investigations were made to observe the precipitate structure under irradiation for different experimental parameters. Moreover, the irradiation-induced changes in precipitate structure and changes of Al-concentrations in the matrix in Ni-13.1 at% Al alloys were studied by electrical resistivity measurements during irradiation. For comparison, the electrical resistivity of unirradiated specimens was also measured after thermal aging for different times. For correlation, TEM analysis was performed on irradiated and unirradiated aged specimens. Tensile tests on annealed and aged Ni-Al alloys were also done at various temperatures. (orig./RK)

  13. Fracture performance of high strength steels, aluminium and magnesium alloys during plastic deformation

    Directory of Open Access Journals (Sweden)

    Yu Haiyan

    2015-01-01

    Full Text Available A series of uniaxial tension tests were performed for 5052 and 6061 aluminum alloys, AZ31B magnesium alloy, TRIP600 and DP600 steels, to obtain a better understanding of their fracture performance. Scanning electron microscope (SEM observation of the microstructure evolution was conducted. The dimple structure, orientation relationship between the fracture surface and tensile direction, necking behavior were analyzed. The fracture mechanism and fracture mode of each material was discussed in detail. The results show that TRIP600 steel is subject to a typical inter-granular ductile fracture combined by shear fracture. DP600 steel belongs to mainly ductility mixed with normal fracture. Both 5052 and 6061 aluminum alloys are subject to a mixed ductility fracture and brittle fracture. AA5052 and AA6061 belong to a typical shear fracture and a normal fracture, respectively. Magnesium AZ31B is typical of a brittle fracture combined with normal fracture.

  14. Preparation of A356 Foam Aluminum by Means of Titanium Hydride

    Science.gov (United States)

    Sarajan, Zohair

    2017-09-01

    The effect of heating temperature and stirring time during preparation of foam aluminum alloy A356 on its relative porosity is studied. The optimum amount of the foam-forming agent, i.e., titanium hydride TiH2, facilitating uniform distribution of pores throughout the whole cross section of a hardened casting is determined. Optimum conditions are established for foam formation in a melt during stirring using a mixer are described.

  15. Reducing non value adding aluminium alloy in production of parts through high pressure die casting

    CSIR Research Space (South Africa)

    Pereira, MFVT

    2010-10-01

    Full Text Available alloy able to withstand high temperature process conditions without the welding problems experienced by standard die construction materials, such as H13, was examined in an extensive series of casting trials. The importance of operating dies at elevated...

  16. Galvanostatic response of AA2024 aluminium alloy in 3.5% NaCl ...

    Indian Academy of Sciences (India)

    Galvanostatic responses of AA2024T3 alloy in de-aerated and naturally aerated 3.5% NaCl solution have been investigated. In the de-aerated condition, two distinct stages of polarization were revealed. From the first stage, the relationships between the pitting incubation time, pitting potential and applied current density for ...

  17. T5 heat treatment of semi-solid metal processed aluminium alloy F357

    CSIR Research Space (South Africa)

    Moller, H

    2009-04-01

    Full Text Available The T5 heat treatment of semi-solid metal (SSM) processed alloy F357 was investigated by considering the effects of cooling rate and natural aging after casting, as well as artificial aging parameters on tensile properties. In addition, the tensile...

  18. Galvanostatic response of AA2024 aluminium alloy in 3.5% NaCl ...

    Indian Academy of Sciences (India)

    Abstract. Galvanostatic responses of AA2024T3 alloy in de-aerated and naturally aerated 3.5% NaCl solution have been investigated. In the de-aerated condition, two distinct stages of polarization were revealed. From the first stage, the relationships between the pitting incubation time, pitting potential and applied current ...

  19. Effect of alloying with zinc on SFE of aluminium by study of lattice ...

    Indian Academy of Sciences (India)

    '' are absent in the cold worked state and twin fault is found to be slightly present in the deformed lattice of the two initial compositions of the alloys. Similar to the effect of solute germanium and copper, respectively in Al–Ge and Al–Cu ...

  20. Behaviour and modelling of aluminium alloy AA6060 subjected to a wide range of strain rates and temperatures

    Directory of Open Access Journals (Sweden)

    Vilamosa Vincent

    2015-01-01

    Full Text Available The thermo-mechanical behaviour in tension of an as-cast and homogenized AA6060 alloy was investigated at a wide range of strains (the entire deformation process up to fracture, strain rates (0.01–750 s−1 and temperatures (20–350 ∘C. The tests at strain rates up to 1 s−1 were performed in a universal testing machine, while a split-Hopkinson tension bar (SHTB system was used for strain rates from 350 to 750 s−1. The samples were heated with an induction-based heating system. A typical feature of aluminium alloys at high temperatures is that necking occurs at a rather early stage of the deformation process. In order to determine the true stress-strain curve also after the onset of necking, all tests were instrumented with a digital camera. The experimental tests reveal that the AA6060 material has negligible strain-rate sensitivity (SRS for temperatures lower than 200 ∘C, while both yielding and work hardening exhibit a strong positive SRS at higher temperatures. The coupled strain-rate and temperature sensitivity is challenging to capture with most existing constitutive models. The paper presents an outline of a new semi-physical model that expresses the flow stress in terms of plastic strain, plastic strain rate and temperature. The parameters of the model were determined from the tests, and the stress-strain curves from the tests were compared with the predictions of the model. Good agreement was obtained over the entire strain rate and temperature range.

  1. Analysis of Structure and Shear/Peel Strength of Refill Friction Stir Spot Welded 7075-T6 Aluminium Alloy Joints

    Directory of Open Access Journals (Sweden)

    Rafał Kluz

    2017-09-01

    Full Text Available The article presents an analysis of the macrostructure and mechanical properties of spot welds of joints made by Refill Friction Spot Stir Welding (RFSSW method. RFSSW is a relatively new technology that gaining wider use in not only the automotive and aviation industries because it is a less energy intensive method than resistance spot welding. The primary focus of the article is the effect of welding time on the quality of the welded joints of sheet metal using the aforementioned method. The research was conducted on a joint between two pieces of sheet metal of various thicknesses (1.6mm and 0.8mm made of the common aviation grade aluminium alloy 7075-T6 Alclad. Metallographic sections of select variants were made in order to analyze the structure of the joint. Strength tests with a static load were conducted in different loading configurations. A traditional tensile strength test was conducted on the lap joint, which revealed a complex stress state within the joint and an analogous test was conducted with the use of a stiffening holder that ensured a pure shear state in the joint. Peel tests were also performed on the lap joints with using a special holder.

  2. Recovery of actinides from actinide-aluminium alloys by chlorination: Part III - Chlorination with HCl(g)

    Science.gov (United States)

    Meier, Roland; Souček, Pavel; Walter, Olaf; Malmbeck, Rikard; Rodrigues, Alcide; Glatz, Jean-Paul; Fanghänel, Thomas

    2018-01-01

    Two steps of a pyrochemical route for the recovery of actinides from spent metallic nuclear fuel are being investigated at JRC-Karlsruhe. The first step consists in electrorefining the fuel in molten salt medium implying aluminium cathodes. The second step is a chlorination process for the separation of actinides (An) from An-Al alloys formed on the cathodes. The chlorination process, in turn, consists of three steps; the distillation of adhered salt (1), the chlorination of An-Al by HCl/Cl2 under formation of AlCl3 and An chlorides (2), and the subsequent sublimation of AlCl3 (3). In the present work UAl2, UAl3, NpAl2, and PuAl2 were chlorinated with HCl(g) in a temperature range between 300 and 400 °C forming UCl4, NpCl4 or PuCl3 as the major An containing phases, respectively. Thermodynamic calculations were carried out to support the experimental work. The results showed a high chlorination efficiency for all used starting materials and indicated that the sublimation step may not be necessary when using HCl(g).

  3. Effect of temperature and frequency of dynamic loading in the viscoelastic properties of aluminium alloy 7075-T6

    Energy Technology Data Exchange (ETDEWEB)

    Rojas, Jose I.; Aguiar, Albert; Crespo, Daniel [Escola d' Enginyeria de Telecomunicacio i Aeroespacial de Castelldefels (EPSC), Universitat Politecnica de Catalunya (UPC Barcelona Tech), Castelldefels, Barcelona (Spain)

    2011-11-15

    The viscoelastic response of a material offers an alternative method for analyzing its microstructure, phase transformations and fatigue behaviour. In this work, the viscoelastic properties of commercial aluminium alloy (AA) 7075-T6 are studied with a Dynamic-Mechanical Analyzer (DMA), and results are combined with Transmission Electron Microscopy (TEM) and Differential Scanning Calorimetry (DSC) data. In accordance with this analysis, we propose an analytical model for the storage modulus E' as a function of temperature, frequency of the dynamic loading and the concentration of Guinier-Preston Zones (GPZ). The latter parameter is obtained as a function of temperature after integration and fitting of the model. It is shown that the proposed model fits the experimental data for the storage modulus reasonably well in the prescribed region, and that this fact supports the hypothesis that the change in the storage modulus slope at about 130-160 C is due to GPZ decomposition. (copyright 2011 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

  4. Influence of process parameters on physical dimensions of AA6063 aluminium alloy coating on mild steel in friction surfacing

    Directory of Open Access Journals (Sweden)

    B. Vijaya Kumar

    2015-09-01

    Full Text Available An attempt is made in the present study to obtain the relationships among process parameters and physical dimensions of AA6063 aluminium alloy coating on IS2062 mild steel obtained through friction surfacing and their impact on strength and ductility of the coating. Factorial experimental design technique was used to investigate and select the parameter combination to achieve a coating with adequate strength and ductility. Spindle speed, axial force and table traverse speed were observed to be the most significant factors on physical dimensions. It was observed that the thickness of the coating decreased as the coating width increased. In addition, the width and thickness of the coatings are higher at low and high torques. At intermediate torque values, when the force is high, the width of the coating is high, and its thickness is thin; and when the force is low, the width and thickness are low. The interaction effect between axial force (F – table traverse speed (Vx and spindle speed (N – table traverse speed (Vx produced an increasing effect on coating width and thickness, but other interactions exhibited decreasing influence. It has also been observed that sound coatings could be obtained in a narrow set of parameter range as the substrate-coating materials are metallurgically incompatible and have a propensity to form brittle intermetallics.

  5. Experimental investigation on the effects of cooling system on surface quality in high speed milling of an aluminium alloy

    Science.gov (United States)

    Chirita, B.; Tampu, N. C.; Brabie, G.; Radu, M. C.

    2016-08-01

    Surface quality is often an important feature of industrial products, not only from the impact it has on the aesthetic aspect but also for the functional role of the parts. High quality surface increases corrosion resistance, assures a longer life cycle for the product and lowers the wear. For a machined part, surface quality is influenced by a series of factors such as the material of the part, the process type, tool geometry, cutting parameters or the cooling system. The choice of the cooling system is especially important, taking into account that the proper conditions will not only assure a superior surface quality, but will also lower the costs and reduce the environmental impact and health risks. The present study aims to investigate the performance of the cooling system and the effect of the cutting parameters on the characteristics of the surfaces resulted from high speed face milling of some parts made of Al 7050-T7451 aluminium alloy. Dry cutting conditions and minimum quantity lubrication (MQL) where used. The results were analysed using analysis of variance (ANOVA).

  6. Effect of retrogression and re-ageing heat treatment on microstructure and microhardness of aluminium 7010 alloy

    Directory of Open Access Journals (Sweden)

    Nandana M. S.

    2018-01-01

    Full Text Available Aluminium alloy 7010 is subjected to retrogression and re-ageing (RRA heat treatment to study the influence of microstructural changes on hardness. Retrogression is performed at 190 °C for different time intervals ranging from 10 to 60 minutes. Optimum time for retrogression treatment is estimated based on the retrogression time that result with equivalent mechanical properties as that of peak aged (T6 condition. Retrogression performed for 30 minutes resulted with micro hardness of 203 HV, which is equivalent to that obtained by following T6 treatment. Microstructural characterization done with the help of transmission electron microscope (TEM indicates RRA treatment results with the coarsened and discontinuous precipitates along the grain boundary which is similar to over aged (T7 condition, where as fine and densely populated precipitates in the matrix similar to T6 condition. Coarse and discontinuous grain boundary precipitates (GBP’s improves resistance to stress corrosion cracking. Fine and dense precipitates in the matrix ensures hardness equivalent to that of T6.

  7. Study of Relation between Shot Peening Parameters and Fatigue Fracture Surface Character of an AW 7075 Aluminium Alloy

    Directory of Open Access Journals (Sweden)

    Libor Trško

    2018-02-01

    Full Text Available Shot peening is a well-known surface treatment method used for fatigue life improvement of cyclically loaded structural components. Since three main variables are considered in the peening process (peening intensity, coverage and peening media type, there is no direct way to choose the best combination of treatment parameters for the best performance, thus it has to be based on experience and laboratory tests. When shot peening is performed with inadequate parameters, or the peening process is not stable in time (decrease of the peening pressure, deterioration of the peening media and so on, it can result in significant degradation of the treated component fatigue properties, what is commonly called as the “overpeening” effect. When a premature fatigue fracture occurs in operation, the fracture surface analysis is usually the most important method of revealing the damage mechanism. This work is aimed at the study of the relation between the shot peening parameters and the fatigue fracture surface character on an AW 7075 aluminium alloy with an objective of identifying marks of overpeening and investigating the fatigue crack initiation mechanism. After performing the tests, it was observed that shot peening with optimized parameters creates a surface layer that is able to change the mechanism of the fatigue crack propagation and improve fatigue strength. On the other hand, using extensive peening parameters decrease the fatigue strength due to the creation of surface cracks and surface layer delamination.

  8. Microstructure and mechanical properties of similar and dissimilar joints of aluminium alloy and pure copper by friction stir welding

    Directory of Open Access Journals (Sweden)

    V.C. Sinha

    2016-09-01

    Full Text Available In the present study, the microstructure and mechanical properties of similar and dissimilar friction stir welded joints of aluminium alloy (AlA and pure copper (Cu were evaluated at variable tool rotational speeds from 150 to 900 rpm in steps of 150 rpm at 60 mm/min travel speed and constant tilt angle 2°. The interfacial microstructures of the joints were characterised by optical and scanning electron microscopy. The Al4Cu9, AlCu, Al2Cu and Al2Cu3 intermetallic compounds have been observed at the interface and stir zone region of dissimilar Al/Cu FSWed joints. Variation in the grain size was observed in the stir zone depending upon the heat input value. Axial force, traverse force and torque value were analysed with variation in tool rotational speed. Residual stresses were measured at the stir zone by X-ray diffraction technique. Maximum ultimate tensile strength of ∼75% of AlA strength for AlA–AlA joints has been obtained at 750 rpm and for Cu–Cu joint tensile strength of ∼100% of tensile strength of Cu was obtained at 300 rpm. However, for Cu–AlA joint when processed at 600 rpm tool rotational speed achieved maximum ultimate tensile strength of ∼77% of AlA.

  9. Study of corrosion of aluminium alloys of nuclear purity in ordinary water, пart one

    Directory of Open Access Journals (Sweden)

    Pešić Milan P.

    2004-01-01

    Full Text Available Effects of corrosion of aluminum alloys of nuclear purity in ordinary water of the spent fuel storage pool of the RA research reactor at VINČA Institute of Nuclear Sciences has been examined in the frame work of the International Atomic Energy Agency Coordinated Research Project "Corrosion of Research Reactor Aluminum-Clad Spent Fuel in Water" since 2002. The study presented in this paper comprises activities on determination and monitoring of chemical parameters and radio activity of water and sludge in the RA spent fuel storage pool and results of the initial study of corrosion effects obtained by visual examinations of surfaces of various coupons made of aluminum alloys of nuclear purity of the test racks exposed to the pool water for a period from six months to six years.

  10. Corrosion behaviour of ion implanted aluminium alloy in 0.1 M NaCl electrolyte

    Energy Technology Data Exchange (ETDEWEB)

    Chu, J.W.; Evans, P.J. [Australian Nuclear Science and Technology Organisation, Lucas Heights, NSW (Australia); Sood, D.K. [Royal Melbourne Inst. of Tech., VIC (Australia)

    1993-12-31

    Aluminum and its alloys are widely used in industry because of their light weight, high strength and good corrosion resistance which is due to the formation of a protective oxide layer. However, under saline conditions such as those encountered in marine environments, this group of metals are vulnerable to localised degradation in the form of pitting corrosion. This type of corrosion involves the adsorption of an anion, such as chlorine, at the oxide solution interface. Ion implantation of metal ions has been shown to improve the corrosion resistance of a variety of materials. This effect occurs : when the implanted species reduces anion adsorption thereby decreasing the corrosion rate. In this paper we report on the pitting behavior of Ti implanted 2011 Al alloy in dilute sodium chloride solution. The Ti implanted surfaces exhibited an increased pitting potential and a reduced oxygen uptake. 5 refs., 3 figs.

  11. Continuous sodium modification of nearly-eutectic aluminium alloys. Part II. Experimental studiem

    Directory of Open Access Journals (Sweden)

    Białobrzeski A.

    2007-01-01

    Full Text Available One of the possible means of continuous sodium modification of nearly-eutectic alloys may be continuous electrolysis of sodium compounds (salts, taking place directly in metal bath (in the crucible. For this process it is necessary to use a solid electrolyte conducting sodium ions. Under the effect of the applied direct current voltage, sodium salt placed in a retort made from the solid electrolyte undergoes dissociation, and next - electrolysis. The retort is immersed in liquid metal. The anode is sodium salt, at that temperature occurring in liquid state, connected to the direct current source through, e.g. a graphite electrode, while cathode is the liquid metal. Sodium ions formed during the sodium salt dissociation and electrolysis are transported through the wall of the solid electrolyte (the material of the retort and in contact with liquid alloy acting as a cathode, they are passing into atomic state, modifying the metal bath.

  12. Continuous sodium modification of nearly-eutectic aluminium alloys. Part I. Theoretical backgrounds of the process

    Directory of Open Access Journals (Sweden)

    Białobrzeski A.

    2007-01-01

    Full Text Available One of the possible techniques of continuous sodium modification of nearly-eutectic alloys is continuous electrolysis of sodium compounds (salts, taking place directly in metal bath (in crucible. For this process it is necessary to use a solid electrolyte conducting sodium ions. The main properties and methods to obtain solid electrolyte of „beta alumina” were highlighted, along with the possibilities of its application in foundry metallurgical processes.

  13. The analysis of initiation and growth of cracks in diffusion aluminium coatings on ZS6U alloy in conditions of thermal fatigue

    International Nuclear Information System (INIS)

    Ciesla, M.; Swadzba, L.; Supernak, W.

    2002-01-01

    The paper deals with the analysis of thermal fatigue of nickel based ZS6U super alloy with 'Si-Ai' and 'Cr-Al' aluminium diffusion coatings. The processes of initiation and growth of cracks in diffusion coating in the conditions of cyclic changing temperature (500 o C - 950 o C) and simultaneous F o constant axial force loading have been analysed. The results of numerical calculations of stress distribution in the specimen with aluminium coatings have been presented. They enabled to elaborate the models of mechanical behaviour of coatings, which in turn helped to explain different character of cracks in the assumed experimental conditions. Thermal fatigue tests performed at lower static component of F o loading spectrum proved that aluminium coatings obtained in course of 'Si-Al' process show the highest lifetime respectively of their thickness. Moreover, the lifetime of 'Si-Al' aluminium coatings decreases together with the increase of static component of load fatigue spectrum unlike in case of 'Cr-Al' coatings. (author)

  14. Material properties of Al-Si-Cu aluminium alloy produced by the rotational cast technology

    Directory of Open Access Journals (Sweden)

    Muhammad Syahid

    2017-03-01

    Full Text Available The aim of the present study is to explore microstructural and mechanical properties of cast Al-Si-Cu aluminum alloy (ADC12. To obtain excellent material properties, the cast Al alloys were produced by an originally developed mold rotational machine, namely liquid aluminum alloy is solidified during high speed rotating. The casting process was conducted under various casting conditions, in which the following factors were altered, e.g., melt temperature, metal mold temperature and different rotational speed. Microstructural characteristics were examined by direct observation using an optical microscope and a scanning electron microscope (SEM, and the secondary dendrite arm spacing of alpha-Al phase (SDAS and the size of Si eutectic phase were identified. Mechanical properties were investigated by micro-hardness and tensile tests. Rotation speed and melt temperature were directly attributed to the SDAS, and severe shear stress arising from the rotation made fine and complicated grain structure, leading to the high mechanical properties. The extent of the shear stress was altered depending on the area of the sample due to the different shear stress. Furthermore, high melt temperature and high rotational speed decrease the size of Si eutectic phases. The high mechanical properties were detected for the cast samples produced by the casting condition as follows: melt temperature 700oC, mold temperature 400oC and rotation speed 400 rpm

  15. Emission of nanoparticles during friction stir welding (FSW) of aluminium alloys.

    Science.gov (United States)

    Gomes, J F; Miranda, R M; Santos, T J; Carvalho, P A

    2014-01-01

    Friction stir welding (FSW) is now well established as a welding process capable of joining some different types of metallic materials, as it was (1) found to be a reliable and economical way of producing high quality welds, and (2) considered a "clean" welding process that does not involve fusion of metal, as is the case with other traditional welding processes. The aim of this study was to determine whether the emission of particles during FSW in the nanorange of the most commonly used aluminum (Al) alloys, AA 5083 and AA 6082, originated from the Al alloy itself due to friction of the welding tool against the item that was being welded. Another goal was to measure Al alloys in the alveolar deposited surface area during FSW. Nanoparticles dimensions were predominantly in the 40- and 70-nm range. This study demonstrated that microparticles were also emitted during FSW but due to tool wear. However, the biological relevance and toxic manifestations of these microparticles remain to be determined.

  16. Friction Stir Welding of three dissimilar aluminium alloy used in aeronautics industry

    Science.gov (United States)

    Boşneag, A.; Constantin, M. A.; Niţu, E.; Iordache, M.

    2017-10-01

    Friction Stir Welding (FSW) is an innovative solid-state joining process. This process was, in first time, develop to join the similar aluminum plates but now the technology can be used to weld a large area of materials similar or dissimilar. Taking these into account FSW process, for dissimilar materials are increasingly required, more than traditional arc welding, in industrial environment. More than that FSW is used in aeronautics industry because of very good result and very good weldability between aluminum alloy used at building of airplanes, where the body of airplane are 20% aluminum alloy and this percent can be increaser in future. In this paper is presented an experimental study which includes welding three dissimilar aluminum alloy, with different properties, used in aeronautics industry, this materials are: AA 2024, AA6061 and AA7075. After welding with different parameters, the welding join and welding process will be analyzed considering process temperature, process vertical force, and roughnessof welding seams, visual aspect and microhardness.

  17. A simplified design of clamping system and fixtures for friction stir welding of aluminium alloys

    Directory of Open Access Journals (Sweden)

    Mohammed. M. Hasan

    2015-12-01

    Full Text Available Sound friction stir welds could be attained by using an active design of backing/clamping system with a proper selection of the welding parameters. This work presented a simplified design of fixtures and backing plates to be used for friction stir welding of aluminum alloys. The test-rig was constructed to prevent dispersal or lifting of the specimens throughout the joining process and to ensure uniform distribution of temperature along the plates. The workpieces were subjected to uniform lateral and vertical pressures by means of bolts and nuts. Compound backing plates and pressure bars with additional side plates were included to increase the heat sink. Several coupons of dissimilar aluminum alloys AA7075 and AA6061 were joined to inspect the validity of this design. The tests showed promising results with defects-free welds, good strength and smooth surface finish without geometric imperfection and gap creation between the welded specimens. Efficiency of the joint reached its maximum value of about 82% with respect to the ultimate strength of the AA6061 alloy at 1100 rpm rotation speed and 300 mm/min feed. These results encourage using and improving the present design for future studies of friction stir welding.

  18. Computational prediction of the refinement of oxide agglomerates in a physical conditioning process for molten aluminium alloy

    International Nuclear Information System (INIS)

    Tong, M; Jagarlapudi, S C; Browne, D J; Patel, J B; Stone, I C; Fan, Z

    2015-01-01

    Physically conditioning molten scrap aluminium alloys using high shear processing (HSP) was recently found to be a promising technology for purification of contaminated alloys. HSP refines the solid oxide agglomerates in molten alloys, so that they can act as sites for the nucleation of Fe-rich intermetallic phases which can subsequently be removed by the downstream de-drossing process. In this paper, a computational modelling for predicting the evolution of size of oxide clusters during HSP is presented. We used CFD to predict the macroscopic flow features of the melt, and the resultant field predictions of temperature and melt shear rate were transferred to a population balance model (PBM) as its key inputs. The PBM is a macroscopic model that formulates the microscopic agglomeration and breakage of a population of a dispersed phase. Although it has been widely used to study conventional deoxidation of liquid metal, this is the first time that PBM has been used to simulate the melt conditioning process within a rotor/stator HSP device. We employed a method which discretizes the continuous profile of size of the dispersed phase into a collection of discrete bins of size, to solve the governing population balance equation for the size of agglomerates. A finite volume method was used to solve the continuity equation, the energy equation and the momentum equation. The overall computation was implemented mainly using the FLUENT module of ANSYS. The simulations showed that there is a relatively high melt shear rate between the stator and sweeping tips of the rotor blades. This high shear rate leads directly to significant fragmentation of the initially large oxide aggregates. Because the process of agglomeration is significantly slower than the breakage processes at the beginning of HSP, the mean size of oxide clusters decreases very rapidly. As the process of agglomeration gradually balances the process of breakage, the mean size of oxide clusters converges to a

  19. Reoxidation Processes Prediction in Gating System by Numerical Simulation for Aluminium Alloys

    Directory of Open Access Journals (Sweden)

    Brůna M.

    2017-09-01

    Full Text Available Pouring of liquid aluminium is typically accompanied by disturbance of the free surface. During these disturbances, the free surface oxide films can be entrained in the bulk of liquid, also pockets of air can be accidentally trapped in this oxide films. The resultant scattering of porosity in castings seems nearly always to originate from the pockets of entrained air in oxide films. Latest version of ProCast software allows to identify the amount of oxides formed at the free surface and where they are most likely to end-up in casts. During a filling calculation, ProCast can calculate different indicators which allow to better quantify the filling pattern. The fluid front tracking indicator “Free surface time exposure” has the units [cm2*s]. At each point of the free surface, the free surface area is multiplied by the time. This value is cumulated with the value of the previous timestep. In addition, this value is transported with the free surface and with the fluid flow. Experiments to validate this new functions were executed.

  20. Investigation of microstructural and mechanical properties of cell walls of closed-cell aluminium alloy foams

    Energy Technology Data Exchange (ETDEWEB)

    Islam, M.A.; Kader, M.A.; Hazell, P.J.; Brown, A.D. [School of Engineering and Information Technology, UNSW Canberra, ACT 2610 (Australia); Saadatfar, M. [Department of Applied Mathematics, Australian National University, Canberra ACT 0200 (Australia); Quadir, M.Z [Electron Microscope Unit, Mark Wainwright Analytical Centre (MWAC), The University of New South Wales, Sydney, NSW 2052 (Australia); Microscopy and Microanalysis Facility (MMF), John de Laeter Centre (JdLC), Curtin University, WA 6102 (Australia); Escobedo, J.P., E-mail: J.Escobedo-Diaz@adfa.edu.au [School of Engineering and Information Technology, UNSW Canberra, ACT 2610 (Australia)

    2016-06-01

    This study investigates the influence of microstructure on the strength properties of individual cell walls of closed-cell stabilized aluminium foams (SAFs). Optical microscopy (OM), micro-computed X-ray tomography (µ-CT), electron backscattering diffraction (EBSD), and energy dispersive X-ray spectroscopy (EDS) analyses were conducted to examine the microstructural properties of SAF cell walls. Novel micro-tensile tests were performed to investigate the strength properties of individual cell walls. Microstructural analysis of the SAF cell walls revealed that the material consists of eutectic Al-Si and dendritic a-Al with an inhomogeneous distribution of intermetallic particles and micro-pores (void defects). These microstructural features affected the micro-mechanism fracture behaviour and tensile strength of the specimens. Laser-based extensometer and digital image correlation (DIC) analyses were employed to observe the strain fields of individual tensile specimens. The tensile failure mode of these materials has been evaluated using microstructural analysis of post-mortem specimens, revealing a brittle cleavage fracture of the cell wall materials. The micro-porosities and intermetallic particles reduced the strength under tensile loading, limiting the elongation to fracture on average to ~3.2% and an average ultimate tensile strength to ~192 MPa. Finally, interactions between crack propagation and obstructing intermetallic compounds during the tensile deformation have been elucidated.

  1. The effect of pre-straining and pre-ageing on a novel thermomechanical treatment for improving the mechanical properties of AA2139 aerospace aluminium alloys

    Science.gov (United States)

    Bakare, F.; Alsubhi, Y.; Ragkousis, A.; Ebomwonyi, O.; Damisa, J.; Okunzuwa, S.

    2017-07-01

    The novel thermomechanical treatment employed by Wang Z et al (2014 Mater. Sci. Eng. A 607 313-7) in enhancing the mechanical and microstructure properties of 6000 series aluminium alloys has been replicated for AA2139 aerospace aluminium alloys. The novel route which involves under-ageing, cold-rolling reductions and re-ageing at a fixed temperature has been carried out focusing on the effect of pre-straining and pre-ageing on the alloy properties. The influence of varying cold-rolling reductions and pre-ageing has been examined by tensile testing, hardness testing, differential scanning calorimetry, thermoelectric power measurements and scanning electron microscope (SEM). Further analyses were conducted with DSC and TEP measurements to check for precipitation sequence and solute retention respectively. On comparing the hardness and strength of the non pre-aged to the pre-aged samples, there is a remarkable increase in the hardness and strength of the aerospace alloy showing the huge influence of both pre-ageing and pre-straining stage of the novel thermomechanical treatment as observed in the 6000 series alloy, albeit at a higher rate. The treatments that exhibited the most promising mechanical properties (hardness, yield and ultimate tensile strength, elongation to failure) were found to be at a pre-ageing temperature of 175 °C for 1.5 h, 40% cold-rolling and re-ageing at 150 °C. The material was found to have yield strength of 590 MPa and 8.1% uniform elongation, which is well above the 5% acceptable value for structural applications and with strength levels adaptable for aerospace industries. The presence of higher volume fraction of well dispersed precipitates observed in the SEM further shows that intermediate cold-rolling reductions combines well with pre-ageing to give the best mechanical properties in this alloy.

  2. Microstructure and composition of rare earth-transition metal-aluminium-magnesium alloys

    Directory of Open Access Journals (Sweden)

    Lia Maria Carlotti Zarpelon

    2008-03-01

    Full Text Available The determination of the microstructure and chemical composition of La0.7-xPr xMg0.3Al 0.3Mn0.4Co0.5 Ni3.8 (0 < x < 0.7 metal hydride alloys has been carried out using scanning electron microscopy (SEM, energy dispersive X ray analysis (EDX and X ray diffraction analysis (XRD. The substitution of La with Pr changed the grain structure from equiaxial to columnar. The relative atomic ratio of rare earth to (Al, Mn, Co, Ni in the matrix phase was 1:5 (LaNi5-type structure. Magnesium was detected only in two other phases present. A grey phase revealed 11 at.% Mg and the concentration ratios of other elements indicated the composition to be close to PrMgNi4. A dark phase was very heterogeneous in composition, attributed to the as-cast state of these alloys. The phases identified by XRD analysis in the La0.7Mg0.3Al0.3Mn0.4Co 0.5Ni3.8 alloy were: La(Ni,Co5, LaAl(Ni,Co4, La2(Ni,Co7 and AlMn(Ni,Co2. Praseodymium favors the formation of a phase with a PuNi3-type structure. Cobalt substituted Ni in the structures and yielded phases of the type: Pr(Ni,Co5 and Pr(Ni,Co3.

  3. Laser surface alloying (LSA) of aluminium (AA 1200) with TiB2 for hardness improvement

    CSIR Research Space (South Africa)

    Popoola, AP

    2010-10-01

    Full Text Available and D, from these profiles secondary phases were identified, phases present in the alloyed layer are: TiB2, AlTi, AlB2, Al, Ti, B. The Al and Ti belong to the same crystal system and the same space group, and as such their peaks are overlapping.... The same for TiB2 and AlB2 � they belong to the same space group and peaks are overlapping. However, the XRD result of sample D also showed the presence of Al3Ti, this is an intermetallic phase that exhibits high hardness, high melting and also very...

  4. Studies and research on the crack testing for brazed aluminium alloys specimens

    Science.gov (United States)

    Dimitescu, A.; Babiş, C.; Niţoi, D. F.; Radu, C.

    2017-08-01

    The scope of this paper is the identification of an optimum technological solution for brazing aluminum alloys using crack tested specimens. To obtain conclusive results, these tests are conducted on two sets of different specimens. Thus, we get two sets of data which we will compare. These tests are part of the standardized series of tests required by the ASME standards. These are called exfoliation tests. They are used to determine where the crack occurs: in the base material or in the filler material. Thus, we can determine whether the cracking is cohesive or adhesive.

  5. Cutting Forces Parametric Model for the Dry High Speed Contour Milling of Aerospace Aluminium Alloys

    OpenAIRE

    SALGUERO , JORGE; BATISTA , MOISES; CALAMAZ , Madalia; GIROT , Franck; MARCOS , MARIANO

    2013-01-01

    International audience; Cutting forces is one of the most important outputs in material removal machining processes. Their values depend on a large number of parameters, such as the cutting tool material and geometry, the workpiece material or the cutting parameters, among others. In this paper, cutting forces behavior have been analyzed as a function of feedrate and cutting speed, for the high-speed peripheral milling of UNS A92024-T3 (Al-Cu) stacks. This alloy is widely used in the manufact...

  6. Effect of surface roughness on ultrasonic echo amplitude in aluminium-copper alloy castings

    International Nuclear Information System (INIS)

    Ambardar, R.; Pathak, S.D.; Prabhakar, O.; Jayakumar, T.

    1996-01-01

    In the present investigation, the influence of test surface roughness on ultrasonic back-wall echo (BWE) amplitude in Al-4.5%Cu alloy cast specimens has been studied. The results indicate that as the value of surface roughness of the specimen increases, the value of relating BWE amplitude at a given probe frequency decreases. However, under the present set of experimental conditions, the decrease in BWE amplitude with the increase in surface roughness of the test specimen is found to be appreciable at 10 MHz probe frequency. (author)

  7. Observations on infiltration of silicon carbide compacts with an aluminium alloy

    Science.gov (United States)

    Asthana, R.; Rohatgi, P. K.

    1992-01-01

    The melt infiltration of ceramic particulates permits an opportunity to observe such fundamental materials phenomena as nucleation, dynamic wetting and growth in constrained environments. Experimental observations are presented on the infiltration behavior and matrix microstructures that form when porous compacts of platelet-shaped single crystals of alpha- (hexagonal) silicon carbide are infiltrated with a liquid 2014 Al alloy. The infiltration process involved counter gravity infiltration of suitably tamped and preheated compacts of silicon carbide platelets under an external pressure in a special pressure chamber for a set period, then by solidification of the infiltrant metal in the interstices of the bed at atmospheric pressure.

  8. Best Cutting Conditions for Pocket Milling in Aluminium Alloy Body Parts

    Directory of Open Access Journals (Sweden)

    S. V. Grubyy

    2015-01-01

    Full Text Available Essentially, new constructive solutions, among which there are such as application of highstrength aluminum alloys for large-size case parts with the wafer design of the shell (WDS characterize modern and perspective products of the missile and space equipment (MSE. To define optimum strategy of WDS pocket treatment, the paper presents a strategy analysis of penetration and treatment in CAID "ADEM". Based on the performed optimization a combination "spiral" and penetration "spiral on a contour" has been accepted as a strategy of the pocket treatment.To optimize the cutting modes, taking into consideration an elimination of the WDS element deformations, are calculated the hard-alloy mill forces, temperatures, wear rate, size of wear, and tool life, when milling a pocket as a standard element of WDS. A calculation technique which distinctive feature is to take into account the forces and pressure from the face edge of a mill tooth is used. In particular, there is functional relationship between the wear rate of a back surface of the tool and the generalized parameter, i.e. the cutting speed relation to hardness of the wearing tool surface as a function of the cutting temperature for milling conditions of aluminum alloys on the modern CN equipment.The paper presents a sequence of formulas implemented as a calculating algorithm and appropriate calculating program. It shows power and polynomial equations obtained to establish relations of the tool life and a torque of cutting with the variable parameters, i.e. the speed, depth, feed, mill diameter and width.Modeling and optimization results show that for rough treatment of grooves, a technological restriction is machine spindle power. With fine finish and penetration a feed of the tool has to be restricted to prevent deformation of a pocket bottom.During treatment of pockets in large-size parts with WDS a lag effect of the linear drives of equipment has to be taken into consideration, when feeding

  9. Evaluation of microstructure of A356 aluminum alloy casting ...

    Indian Academy of Sciences (India)

    Grain refinement was obtained through mold vibration. Metallurgical properties were examined through optical microstructure, tensile fracture scanning electron microscope (SEM) and SEM image of test specimens prepared under different conditions of solidification. Results indicate that mold vibration effectively modified ...

  10. [Comporison Sduty of Microstructure by Metallographicalk on the Polarized Light and Texture by XRD of CC 5083 and CC 5182 Aluminium Alloy after Cold Rolling and Recrystallization].

    Science.gov (United States)

    Chen, Ming-biao; Li, Yong-wei; Tan, Yuan-biao; Ma, Min; Wang, Xue-min; Liu, Wen-chang

    2015-03-01

    At present the study of relation between microstructure, texture and performance of CC 5083 aluminium alloy after cold tolling and recrystallization processes is still finitude. So that the use of the CC 5083 aluminium alloy be influenced. Be cased into electrical furnace, hot up with unlimited speed followed the furnace hot up to different temperature and annealed 2h respectively, and be cased into salt-beth furnace, hot up quickly to different temperature and annealed 30 min respectively for CC 5083 and CC 5182 aluminum alloy after cold roling with 91.5% reduction. The microstructure be watched use metallographic microscope, the texture be inspected by XRD. The start temperature of recrystallization and grain grow up temperature within annealing in the electric furnace of CC 5083 aluminum alloy board is 343 degrees C, and the shap of grain after grow up with long strip (the innovation point ); The start temperature of recrystallization within annealling in the salt bath furnace of CC 5083 is 343 degrees C. The start temperature and end temperature of recrystallization within annealling of CC 5083 and CC 5182 aluminum alloy is 371 degrees C. The grain grow up outstanding of cold rooled CC 5152 aluminum alloy after annealed with 454 degrees C in the electric furnace and salt bath furnace. The start temperature of grain grow up of CC 5083 alluminurn alloy annealed in the electric furnace and salt bath furnace respectively is higher than the start temperature of grain grow up of CC 5182 alluminum alloy annealed in the electric furnace and salt bath furnace respectively. The strat temperature of recrystallization grain grow up is higher than which annealled with other three manner annealing process. The recrystallization temperature of CC 5182 annealed in the salt bath furnace is higher than which annealed in the electric furnace. The recrystallization temperature of the surface layer of CC 5083 and CC 5182 aluminum alloy is higher than the inner layer (the innovation

  11. Influence of heat treatment on the microstructure, texture and formability of 2024 aluminium alloy

    Energy Technology Data Exchange (ETDEWEB)

    Moy, Charles K.S., E-mail: cloo8000@uni.sydney.edu.au [Australian Centre for Microscopy and Microanalysis, University of Sydney, NSW 2006 (Australia); ARC Centre of Excellence for Design in Light Metals, University of Sydney, NSW 2006 (Australia); School of Civil Engineering, University of Sydney, NSW 2006 (Australia); Weiss, Matthias [Centre for Materials and Fibre Innovation, Deakin University, VIC 3217 (Australia); Xia, Junhai [Australian Centre for Microscopy and Microanalysis, University of Sydney, NSW 2006 (Australia); Sha, Gang; Ringer, Simon P. [Australian Centre for Microscopy and Microanalysis, University of Sydney, NSW 2006 (Australia); ARC Centre of Excellence for Design in Light Metals, University of Sydney, NSW 2006 (Australia); Ranzi, Gianluca [Australian Centre for Microscopy and Microanalysis, University of Sydney, NSW 2006 (Australia); ARC Centre of Excellence for Design in Light Metals, University of Sydney, NSW 2006 (Australia); School of Civil Engineering, University of Sydney, NSW 2006 (Australia)

    2012-08-30

    We have investigated the effect of heat treatment on the microstructure, texture and formability of high-strength aluminium Al2024 sheets of gauge thicknesses 1.27 mm and 2.03 mm. Both optical and electron microscopy were employed to characterise the microstructure. Tensile tests performed at 0 Degree-Sign , 45 Degree-Sign and 90 Degree-Sign to the rolling direction were used as an indication of the anisotropic behaviour of the sheets. The formability of the sheets was assessed by performing stretch forming tests over a hemispherical punch. Comparison of microstructure and material properties indicated an effect of precipitation hardening on the overall anisotropy of the investigated materials. We report an improvement in the total elongation under uniaxial tension with a loss in strength for 2.5 h and 2 days ageing while the ageing treatment for 1 week (peak hardness) resulted in increased strength with a decline in total elongation. The 1.27 mm thick sheet showed better drawability and least tendency to earing than the thicker sheet. The drawability was the highest at 45 Degree-Sign to the rolling direction for the as-received material and those that had been aged for 2.5 h and 2 days. Forming limit diagrams derived from the stretch forming tests showed that the 2 days aged sample had the highest plane strain limit making it the most appropriate condition considering that the plane strain is usually the most critical forming strain in stamping applications. In addition, the 2 days aged sample had its plane strain shifted towards the biaxial stretching area which is likely to have a positive effect on some sheet forming applications. Finally, a formability index was calculated and compared against the hardness plot.

  12. Atomic-scale simulation study of some bulk and interfacial properties of iron aluminium ordered alloys

    International Nuclear Information System (INIS)

    Besson, Remy

    1997-01-01

    A semi-empirical potential was designed for B 2 and DO 3 iron aluminides and used to study point defects and grain boundaries in these compounds. At low temperature, departure from B 2 stoichiometry is accommodated with antisite defects; when T increases, iron vacancies appear and defects have a trend to form clusters, the structure of which is very sensitive to this departure. Our calculations, relying on T = 0 K formation energies, predict the nature of major defects, but lead to underestimated quantitative results, which may point out the essential role of atomic vibrations. In the stoichiometric B 2 compound, the diffusion of both species is induced by four-jump cycles involving iron vacancies. Although the agreement between our calculated activation energies and other experiments is good, the calculated diffusion coefficients are below the experimental ones. Here again, this discrepancy may be put down to the overlooking of phonon contributions. The second application concerns the atomic structures of the [001] (310) symmetric tilt grain boundary in the B 2 and DO 3 compounds. At low temperature, in the stoichiometric B 2 compound, we obtain an iron-rich single stable structure (pseudo-symmetric), whose structure is strongly influenced by the bulk composition (with intergranular segregation of the major element). In the stoichiometric DO 3 compound, many energetically equivalent structures exist, all being systematically aluminium-rich. The study of the B 2 grain boundary structure at high temperature shows a phase transition favouring a symmetric structure. Its high excess energy at low temperature emphasizes the influence of atomic vibrations in the interfacial properties of B 2 Fe-Al compounds. (author) [fr

  13. Process-scale modelling of microstructure in direct chill casting of aluminium alloys

    Science.gov (United States)

    Bedel, M.; Heyvaert, L.; Založnik, M.; Combeau, H.; Daloz, D.; Lesoult, G.

    2015-06-01

    The mechanical properties of an alloy being related to its microstructure, the understanding of the mechanisms responsible for the grain structure formation in direct chill casting is crucial. However, the grain size prediction by modelling is difficult since a variety of multi-scale coupled phenomena have to be considered. Nucleation and growth of the grains are interrelated, and the macroscopic transport phenomena such as the motion of grains and inoculant particles with the flow impact the nucleation-gowth competition. Thus we propose to study the grain size distribution of a 5182 alloy industrial scale slab of 510 mm thickness, both non-inoculated and inoculated with Al-3Ti-1B, for which experimental grain size measurements are available. We use a volume-averaged two-phase multi-scale model that describes nucleation from inoculant particles and grain growth, fully coupled with macroscopic transport phenomena: fluid flow induced by natural convection and solidification shrinkage, heat, mass and solute mass transport, grains and inoculant particles motion. We analyze the effect of liquid and grain motion as the effect of grain morphology on microstructure formation and we show in which extent those phenomena are responsible for the grain size distribution observed experimentally. The effect of the refiner level is also studied.

  14. The Generation of AlmFe in Dilute Aluminium Alloys with Different Grain Refining Additions

    Science.gov (United States)

    Meredith, M. W.; Greer, A. L.; Evans, P. V.; Hamerton, R. G.

    Al13Fe4, Al6Fe and AlmFe are common intermetallics in commercial AA1XXX series Al alloys. Grain-refining additions (based on either Al-Ti-B or Al-Ti-C) are usually added to such alloys during solidification processing to aid the grain structure development. They also influence the favoured intermetallic and, hence, can affect the materials' properties. This work simulates commercial casting practices in an attempt to determine the mechanisms by which one intermetallic phase is favoured over another by the introduction of grain-refining additions. Directional solidification experiments on Al-0.3wt.%Fe-0.15wt.%Si with and without grain refiner are conducted using Bridgman apparatus. The type, amount and effectiveness of the grain-refining additions are altered and the resulting intermetallic phase selection followed. The materials are characterised using optical microscopy, scanning electron microscopy and X-ray diffraction. AlmFe is seen to form when Al-Ti-B grain-refiner is introduced but only when the refinement is successful; reducing the effectiveness of the refiner led to Al6Fe forming under all conditions. Al-Ti-C refiners are seen to promote AlmFe at lower solidification velocities than when Al-Ti-B was used even though the grain structure was not as refined. These trends can be explained within existing eutectic theory, by considering growth undercooling.

  15. Laser beam welding and friction stir welding of 6013-T6 aluminium alloy sheet

    International Nuclear Information System (INIS)

    Braun, R.; Dalle Donne, C.; Staniek, G.

    2000-01-01

    Butt welds of 1.6 mm thick 6013-T6 sheet were produced using laser beam welding and friction stir welding processes. Employing the former joining technique, filler powders of the alloys Al-5%Mg and Al-12%Si were used. Microstructure, hardness profiles, tensile properties and the corrosion behaviour of the welds in the as-welded condition were investigated. The hardness in the weld zone was lower compared to that of the base material in the peak-aged temper. Hardness minima were measured in the fusion zone and in the thermomechanically affected zone for laser beam welded and friction stir welded joints, respectively. Metallographic and fractographic examinations revealed pores in the fusion zone of the laser beam welds. Porosity was higher in welds made using the filler alloy Al-5%Mg than using the filler metal Al-12%Si. Transmission electron microscopy indicated that the β '' (Mg 2 Si) hardening precipitates were dissolved in the weld zone due to the heat input of the joining processes. Joint efficiencies achieved for laser beam welds depended upon the filler powders, being about 60 and 80% using the alloys Al-5%Mg and Al-12%Si, respectively. Strength of the friction stir weld approached over 80% of the ultimate tensile strength of the 6013-T6 base material. Fracture occurred in the region of hardness minima unless defects in the weld zone led to premature failure. The heat input during welding did not cause a degradation of the corrosion behaviour of the welds, as found in continuous immersion tests in an aqueous chloride-peroxide solution. In contrast to the 6013-T6 parent material, the weld zone was not sensitive to intergranular corrosion. Alternate immersion tests in 3.5% NaCl solution indicated high stress corrosion cracking resistance of the joints. For laser beam welded sheet, the weld zone of alternately immersed specimens suffered severe degradation by pitting and intergranular corrosion, which may be associated with galvanic coupling of filler metal and

  16. Fatigue crack growth behaviour of the aluminium-lithium alloy 2090

    International Nuclear Information System (INIS)

    Tabrett, C.P.; McKeighan, P.C.; Smith, D.J.

    1993-01-01

    The fatigue crack growth (FCG) behavior of the aluminum lithium (Al-Li) alloy 2090-T84 has been investigated from a series of constant amplitude FCG tests. The influence of in plane orientation (L-T, T-L+45) and sheet thickness (1.6 and 6 mm) on the FCG rates for the rolled product has been examined. In general, the T-L orientation possess superior FCG resistance for both thicknesses and the 6 mm thick sheet material showed improved FCG resistance when compared to the 1.6 mm thick material for all orientations. It is believed this trend is related to the greater roughness and larger asperities found on the fatigue crack surfaces for the 6 mm thick material. Closure corrected FCG data suggests that much of the difference between the L-T and T-L orientation for the 6 mm thick sheet arise from variations in crack closure levels. (author)

  17. Formation of an A1N continuous layer by nitrogen ion implantation in aluminium alloys

    International Nuclear Information System (INIS)

    Denanot, M.F.; Delafond, J.; Grilhe, J.

    1986-01-01

    Nitrogen ion implantations at doses from 10 17 ions cm -2 up to 6 x 10 17 ions cm -2 in pure A1 and an Au 4 G industrial alloy are studied by electron microscopy investigations. In these two materials, we observe the formation of AlN precipitates with an orientation relationship between the two lattices. The highest dose leads to the formation of a continuous layer of AlN with a very good crystallographic quality, but there are blisters due to gas bubbles. It seems that the dose of 3 x 10 17 ions cm -2 is optimum to have a good AlN continuous layer and thus to improve the surface qualities of the materials. (author)

  18. RETRACTED ARTICLE: Comparison on grain refinement efficiency of peritectic and eutectic alloying elements on pure aluminium

    Science.gov (United States)

    Haghayeghi, R.; Kapranos, P.

    2014-07-01

    The work investigated the grain refining efficiency of peritectic forming solutes as well as eutectic solutes on pure Al. Significant grain refinement for peritectic and small refinement for the eutectic elements were achieved and the mechanisms of refinement were studied. In order to investigate the grain structure and solidification phenomena for each set of alloys, a TP-1 test, as well as thermal analysis, was performed and back scattered images were used to analyze the phases that may contribute to the grain refinement. It appears that the significant grain refinement of peritectic elements is due to the formation of in-situ properitectic particles and their appropriate constitutional undercooling. The results suggest that the availability of potent nuclei and exogenous particles play major roles in the grain refinement efficiency. However, in the case of eutectic elements only segregation power contributes to refinement whilst the availability of potent nuclei is of paramount importance.

  19. On the melt infiltration of copper coated silicon carbide with an aluminium alloy

    Science.gov (United States)

    Asthana, R.; Rohatgi, P. K.

    1992-01-01

    Pressure-assisted infiltration of porous compacts of Cu coated and uncoated single crystals of platelet shaped alpha (hexagonal) SiC was used to study infiltration dynamics and particulate wettability with a 2014 Al alloy. The infiltration lengths were measured for a range of experimental variables which included infiltration pressure, infiltration time, and SiC size. A threshold pressure (P(th)) for flow initiation through compacts was identified from an analysis of infiltration data; P(th) decreased while penetration lengths increased with increasing SiC size (more fundamentally, due to changes in interparticle pore size) and with increasing infiltration times. Cu coated SiC led to lower P(th) and 60-80 percent larger penetration lengths compared to uncoated SiC under identical processing conditions.

  20. Strobloy — The New Combined Grain Refiner and Modifier for Hypoeutectic AlSi Foundry Alloys

    Science.gov (United States)

    Bondhus, Eivind; Sagstad, Trond

    Hydelko presents a new combination alloy for use in hypoeuctectic aluminium silicon foundry alloys. Strobloy simplifies today's addition practice of grain refiner and modifier by reducing the number of additions from two to one. Strobloy is a combination product between the well-established TiBloy, and strontium. The alloy contains nucleating particles in the form of the mixed boride (Al, Ti)B2, which is beneficial regarding settling and grain refining efficiency. Strontium is present as fast-dissolving AL4Sr particles. Trials carried out indicate that Strobloy shows very good performance compared to separate additions of TiBloy/AlTi5B1 and AlSr master alloy. The grain refining efficiency and modification level is the same or better. This paper displays results collected from tests done with different strontium levels in an A356 alloy. Comparisons to separate additions of TiBloy and AlSr are presented.

  1. Pre-aging effects in thermo mechanically treated 6201 aluminium alloy

    International Nuclear Information System (INIS)

    Martinova, Zlatanka P.

    2003-01-01

    In this work the aging characteristics of aluminum alloy 6201 (Al-0, 62%Mg-O, 56%Si), subjected to new dimension of thermomechanical treatment (TMT) was investigated. TMT employed stepped, aging according to the scheme: solution treatment, water quenching, pre-aging at low to intermediate temperatures, cold working with 75-95% deformation and final artificial aging at 170 o C - 200 o C. Differential thermal analysis (DTA) and differential scanning calorimetry (DSC) analysis to examine the precipitation and dissolution reactions during continuous heating of samples with different pre-aging treatments were used. The main commonality between each DSC curve obtained from pre-aged and deformed samples at 20 o Cmin -1 was the appearance of broad exothermic peak, centered at approximately 250 o C. This suggests an overlap of several reactions, occurring within the same temperature interval. Most likely, these are the precipitation of strengthening β , β' phases, recovery/ recrystallization and some reversion of GPI zones. The tensile properties and electrical conductivity of the wires were determined after deformation and after isothermal artificial aging. The changes of the properties are discussed in terms of structure development at every stage of TMT and according to the current two-stepped aging theories. (Original)

  2. Evaluation of casting defects in aluminium alloys by CT and US

    International Nuclear Information System (INIS)

    Silva, Ivan L.M.; Lopes, Ricardo T.; Jesus, Edgar F.O. de

    2000-01-01

    This work shows the development of a methodology in the comparative analyze between the Computerized Tomography and the ultrasound technique. These techniques were utilized in non-destructive essays in casting pieces in aluminum alloy with the aim of analyzing all kinds of defects aroused in the casting process. The results show that the computerized tomography gives a more precise and easier information to be interpreted. On the other hand, the ultrasound technique is a more sensitive technique that can be utilized as an auxiliary tool for choosing the parameters used in the computerized tomography. The results with the X-ray transmission tomography technique show results of spatial resolution of the order of 0.8 mm. The ultra-sound technique was capable of detecting defects of the order of 0.5 mm of diameter, with resolution of 0.4 mm in the x direction and 0.39 in y direction, besides being sensitive to the porosity presence. (author)

  3. Effect of zinc addition on the performance of aluminium alloy sacrificial anode for marine application

    Science.gov (United States)

    Khan, Bharvez; Rosli, M. U.; Jahidi, H.; Ishak, Muhammad Ikman; Zakaria, M. S.; Jamalludin, Mohd Riduan; Khor, C. Y.; Faizal, W. M.; Rahim, W. M.; Nawi, M. A. M.

    2017-09-01

    In this work, the effect of zinc addition on the performance of aluminum-based sacrificial anode in seawater was investigated. The parameters used in assessing the performance of the cast anodes are anodic efficiency, protection efficiency and polarized potential. The content of zinc in the anodes was varied after die casting. The alloys produced were tested as sacrificial anode for the protection of mild steel for marine application at room temperature. Factors such as reactivity of zinc particles in the seawater, corrosion activity during the period of experiment, pH of seawater and the electronegativity potential of zinc were collected for analysis. Overall findings shows addition of zinc increases rate of corrosion to the sacrificial anode and the protection offered by the sacrificial anodes measured and collected in PIT shows the seawater react to sacrificial anode and no porosity reaction between the anodes. The microstructure showed the intermetallic structures of β-phase which breakdown the alumina passive film, thus enhancing the anode efficiency.

  4. Market Opportunity of Some Aluminium Silicon Alloys Materials through Changing the Casting Process

    Directory of Open Access Journals (Sweden)

    Delfim SOARES

    2012-08-01

    Full Text Available Fatigue is considered to be the most common mechanism by which engineering components fail, and it accounts for at least 90% of all service failures attributed to mechanical causes. Mechanical properties (tensile strength, tensile strain, Young modulus, etc as well as fatigue properties (fatigue life are very dependent on casting method. The most direct effects of casting techniques are on the metallurgical microstructure that bounds the mechanical properties. One of the important variables affected by the casting technique is the cooling rate which is well known to strongly restrict the microstructure. In the present research has been done a comparison of fatigue properties of two aluminum silicon alloys obtained by two casting techniques. It was observed that the fatigue life is increasing with 24% for Al12Si and 31% for AL18Si by using centrifugal casting process instead of gravity casting. This increasing in fatigue life means that a component tailored from materials obtained by centrifugal casting will stay longer in service. It was made an estimation of the time required to recover the costs of technology in order to use the centrifuge process that will allow to obtain materials with improved properties. The amortization can be achieved by using two different marketing techniques: through the release of the product at the old price and with much longer life of the component which means "same price - longer life", or increasing price, by highlighting new product performance which means "higher price - higher properties".

  5. Investigation of Corrosion Behaviour of Aluminium Alloy Subjected to Laser Shock Peening without a Protective Coating

    Directory of Open Access Journals (Sweden)

    U. Trdan

    2015-01-01

    Full Text Available The effect of shock waves and strain hardening of laser shock peening without protective coating (LSPwC on alloy AA 6082-T651 was investigated. Analysis of residual stresses confirmed high compression in the near surface layer due to the ultrahigh plastic strains and strain rates induced by multiple laser shock waves. Corrosion tests in a chloride environment were carried out to determine resistance to localised attack, which was also verified on SEM/EDS. OCP transients confirmed an improved condition, that is, a more positive and stable potential after LSPwC treatment. Moreover, polarisation resistance of the LSPwC treated specimen was by a factor of 25 higher compared to the untreated specimen. Analysis of voltammograms confirmed an improved enhanced region of passivity and significantly smaller anodic current density of the LSPwC specimen compared to the untreated one. Through SEM, reduction of pitting attack at the LSPwC specimen surface was confirmed, despite its increased roughness.

  6. Wear behaviour and morphology of stir cast aluminium/SiC nanocomposites

    Science.gov (United States)

    Tanwir Alam, Md; Arif, Sajjad; Husain Ansari, Akhter

    2018-04-01

    Wear and friction play a vital role in the service life of components. Aluminium matrix nanocomposites possess tremendous potential for a number of applications in addition to their present uses. It is valuable to the field of newer materials for better performance in tribological applications. In this work, dry sliding wear, friction coefficient and morphology of aluminium alloy (A356) reinforced with silicon carbide nanoparticles (SiCn) were investigated. A356/SiCn nanocomposites (AMNCs) containing 1–5 weight percentage of SiCn were prepared through two-step stir casting process via mechanical ball milling. The wear test was conducted on pin-on-disc test apparatus. Regression analysis was performed to develop mathematical functions to fit the experimental data points. Morphological studies of Al and SiCn as-received, wear debris and worn surfaces were further analysed by SEM along with EDS. The occurrence of oxide layers was observed on worn surfaces. Iron trace was identified by wear debris. It was found that the wear loss and friction coefficient were strongly influenced by mechanical milling and SiCn content. The results exhibited that the friction coefficient reduces with the addition of SiCn as well as with the increase in load. However, wear resistance increases as the reinforcement content increases because of the embedding and wettability effects.

  7. Optimization of Coolant Technique Conditions for Machining A319 Aluminium Alloy Using Response Surface Method (RSM)

    Science.gov (United States)

    Zainal Ariffin, S.; Razlan, A.; Ali, M. Mohd; Efendee, A. M.; Rahman, M. M.

    2018-03-01

    Background/Objectives: The paper discusses about the optimum cutting parameters with coolant techniques condition (1.0 mm nozzle orifice, wet and dry) to optimize surface roughness, temperature and tool wear in the machining process based on the selected setting parameters. The selected cutting parameters for this study were the cutting speed, feed rate, depth of cut and coolant techniques condition. Methods/Statistical Analysis Experiments were conducted and investigated based on Design of Experiment (DOE) with Response Surface Method. The research of the aggressive machining process on aluminum alloy (A319) for automotive applications is an effort to understand the machining concept, which widely used in a variety of manufacturing industries especially in the automotive industry. Findings: The results show that the dominant failure mode is the surface roughness, temperature and tool wear when using 1.0 mm nozzle orifice, increases during machining and also can be alternative minimize built up edge of the A319. The exploration for surface roughness, productivity and the optimization of cutting speed in the technical and commercial aspects of the manufacturing processes of A319 are discussed in automotive components industries for further work Applications/Improvements: The research result also beneficial in minimizing the costs incurred and improving productivity of manufacturing firms. According to the mathematical model and equations, generated by CCD based RSM, experiments were performed and cutting coolant condition technique using size nozzle can reduces tool wear, surface roughness and temperature was obtained. Results have been analyzed and optimization has been carried out for selecting cutting parameters, shows that the effectiveness and efficiency of the system can be identified and helps to solve potential problems.

  8. Experimental and Numerical Study of Needle Peening Effects in Aluminium Alloy 2024-T3 Sheets

    Science.gov (United States)

    Mendez Romero, Julio Alberto

    Montreal as part of previous shot peening research. Saturation tests were done to determine the deflection at saturation for different peening parameters. The specimen deflection was measured using the standard Almen gauge used as part of routinary process control. Due to the aluminium magnetic incompatibility with the Almen gauge, the deformed specimen profile was measured using a Coordinate Measuring Machine (CMM). Repeatability of the process was demonstrated and the deflection at saturation, as well as the saturation time, was obtained. The indentation diameters created by impacts for different operating pressures were measured using microscopic photography. It was determined that the specimen deformation, as well as the indentation diameter, is larger when the operating pressure increases. Treatment of the test samples using the same peening parameters resulted in a variable indentation diameter. This is explained by the velocity variations detected during the equipment characterization. The added value that needle peening could provide to existing peening techniques is that, in principle, uniformity in the indentation diameters is easier to achieve as all impacts are normal and there is no loss of energy due to media interaction. The last experimental test was to determine the induced residual stress by means of X-ray Diffraction (XRD) for one specimen at saturation. An FE model heavily inspired by previous shot peening modeling was developed to simulate needle peening. The parameters obtained during the characterization of the equipment were taken as boundary conditions. Initially, the case of a single impacts was studied. Good accordance between the simulated and the average experimental indentation diameters was obtained, except for the lowest pressure studied. The overestimation of the indentation diameter could stem from the method used to measure the simulated diameter. Coverage estimation, and therefore indentation diameters remain an open line of research in

  9. Behaviour and fatigue damage study of cast aluminium alloys; Etude du comportement et de l'endommagement en fatigue d'alliages d'aluminium de fonderie

    Energy Technology Data Exchange (ETDEWEB)

    Barlas, B.

    2004-02-15

    This study is aimed at determining the influence of chemical composition and heat treatment of cast aluminium alloys Al-Si-Cu-Mg on mechanical behaviour and fatigue life of structures. The industrial frame of this study concerns cylinder-heads of high efficiency diesel engines, for Renault and Montupet companies. The experimental means involved in this work are as well microscopic (TEM, microhardness, image analysis), mechanical (LCF and aniso-thermal tests, macro-hardness) and numerical (simulation of the stability of the hardening phases, behaviour and damage model identification, cylinder-head life time calculation). The link between micro and macro approaches is provided by the means of an internal microscopic variable representing thermal aging through coarsening of the precipitates and implemented into the macroscopic model. (author)

  10. Design and operation of an aluminium alloy tank using doped Na3AlH6 in kg scale for hydrogen storage

    Science.gov (United States)

    Urbanczyk, R.; Peinecke, K.; Meggouh, M.; Minne, P.; Peil, S.; Bathen, D.; Felderhoff, M.

    2016-08-01

    In this publication the authors present an aluminium alloy tank for hydrogen storage using 1921 g of Na3AlH6 doped with 4 mol% of TiCl3 and 8 mol% of activated carbon. The tank and the heat exchangers are manufactured by extrusion moulding of Al-Mg-Si based alloys. EN AW 6082 T6 alloy is used for the tank and a specifically developed alloy with a composition similar to EN AW 6060 T6 is used for the heat exchangers. The three heat exchangers have a corrugated profile to enhance the surface area for heat transfer. The doped complex hydride Na3AlH6 is densified to a powder density of 0.62 g cm-3. The hydrogenation experiments are carried out at 2.5 MPa. During one of the dehydrogenation experiments approximately 38 g of hydrogen is released, accounting for gravimetric hydrogen density of 2.0 mass-%. With this tank 15 hydrogenation and 16 dehydrogenation tests are carried out.

  11. In situ monitoring of corrosion mechanisms and phosphate inhibitor surface deposition during corrosion of zinc-magnesium-aluminium (ZMA) alloys using novel time-lapse microscopy.

    Science.gov (United States)

    Sullivan, James; Cooze, Nathan; Gallagher, Callum; Lewis, Tom; Prosek, Tomas; Thierry, Dominique

    2015-01-01

    In situ time-lapse optical microscopy was used to examine the microstructural corrosion mechanisms in three zinc-magnesium-aluminium (ZMA) alloy coated steels immersed in 1% NaCl pH 7. Preferential corrosion of MgZn(2) lamellae within the eutectic phases was observed in all the ZMA alloys followed by subsequent dissolution of Zn rich phases. The total extent and rate of corrosion, measured using time-lapse image analysis and scanning vibrating electrode technique (SVET) estimated mass loss, decreased as Mg and Al alloying additions were increased up to a level of 3 wt% Mg and 3.7 wt% Al. This was probably due to the increased presence of MgO and Al(2)O(3) at the alloy surface retarding the kinetics of cathodic oxygen reduction. The addition of 1 × 10(-2) mol dm(-3) Na(3)PO(4) to 1% NaCl pH 7 had a dramatic influence on the corrosion mechanism for a ZMA with passivation of anodic sites through phosphate precipitation observed using time-lapse image analysis. Intriguing rapid precipitation of filamentous phosphate was also observed and it is postulated that these filaments nucleate and grow due to super saturation effects. Polarisation experiments showed that the addition of 1 × 10(-2) mol dm(-3) Na(3)PO(4) to the 1% NaCl electrolyte promoted an anodic shift of 50 mV in open circuit potential for the ZMA alloy with a reduction in anodic current of 2.5 orders of magnitude suggesting that it was acting primarily as an anodic inhibitor supporting the inferences from the time-lapse investigations. These phosphate additions resulted in a 98% reduction in estimated mass loss as measured by SVET demonstrating the effectiveness of phosphate inhibitors for this alloy system.

  12. Recovery in aluminium

    DEFF Research Database (Denmark)

    Gundlach, Carsten

    2006-01-01

    In the present thesis the development of a unique experimental method for volume characterisation of individual embedded crystallites down to a radius of 150 nm is presented. This method is applied to in-situ studies of recovery in aluminium. The method is an extension of 3DXRD microscopy, an X...... by the combined use of X-ray micro focusing optics, new scanning algorithms and the use of foils. The ratio of foil thickness to crystallite size should be at least 10 such that the central ones are situated in a bulk environment. To avoid thermal drifts, gold reference markers are deposited onto the sample...... are represented as strings. To identify the strings a combination of a 5D connected component type algorithm and multi-peak fitting was found to be superior. The first use of the method was a study of recovery of a deformed aluminium alloy (AA1050). The aluminium alloy was deformed by cold rolling to a thickness...

  13. The effect of surface pre-conditioning treatments on the local composition of Zr-based conversion coatings formed on aluminium alloys

    International Nuclear Information System (INIS)

    Cerezo, J.; Vandendael, I.; Posner, R.; Wit, J.H.W. de; Mol, J.M.C.; Terryn, H.

    2016-01-01

    Graphical abstract: - Highlights: • Field Emission Auger Electron Spectroscopy was used for local elemental analysis. • Acid and alkaline pre-conditioning treatments induces Cu-enrichment on AA6014. • A Cu-containing Zr-based conversion treatment for aluminium alloys was evaluated. • Cu-rich areas enhance the local formation of Zr-based conversion films on AA6014. • Thermal pre-conditioning treatments inhibits the formation of Zr-based coatings. - Abstract: This study investigates the effect of different alkaline, acidic and thermal pre-conditioning treatments applied to different Al alloy surfaces. The obtained results are compared to the characteristics of Zr-based conversion coatings that were subsequently generated on top of these substrates. Focus is laid on typical elemental distributions on the sample surfaces, in particular on the amount of precipitated functional additives such as Cu species that are present in the substrate matrix as well as in the conversion bath solutions. To this aim, Field Emission Auger Electron spectra, depth profiles and surface maps with superior local resolution were acquired and compared to scanning electron microscopy images of the sample. The results show how de-alloying processes, which occur at and around intermetallic particles in the Al matrix during typical industrial alkaline or acidic cleaning procedures, provide a significant source of crystallization cores for any following coating processes. This is in particular due for Cu-species, as the resulting local Cu structures on the surface strongly affect the film formation and compositions of state-of-the-art Zr-based films. The findings are highly relevant for industrial treatments of aluminium surfaces, especially for those that undergo corrosion protection and painting process steps prior to usage.

  14. Activation Analysis of Aluminium

    Energy Technology Data Exchange (ETDEWEB)

    Brune, Dag

    1961-01-15

    An analysis of pure aluminium alloyed with magnesium was per- formed by means of gamma spectrometry , Chemical separations were not employed. The isotopes to be determined were obtained in conditions of optimum activity by suitably choosing the time of irradiation and decay. The following elements were detected and measured quantitatively: Iron, zinc, copper, gallium, manganese, chromium, scandium and hafnium.

  15. The effects of reactive elements on the oxidation of alumina-forming iron-chromium-aluminium alloys at high temperature

    International Nuclear Information System (INIS)

    Deakin, J.; Prunier, V.; Wood, G.C.; Stott, F.H.

    1995-01-01

    A study is being undertaken into the influence of sulphur and reactive elements on the growth and adhesion of alumina scales on iron-chromium-base alloys during thermal cycling in air from 1300 C. A low-sulphur- (< 10 ppm) containing alloy has shown considerable improvements in scale adhesion compared with an alloy containing a higher concentration of sulphur. Additions of reactive elements to the low sulphur-containing alloy had little further effect on scale adhesion, although second-phase precipitates facilitated preferential inward growth of the scale and the development of a very irregular scale/alloy interface. All the alloys showed evidence for stress development during scale growth, but this was often relieved by flow of the weak alloy. Although not extensive, all the low sulphur-containing alloys exhibited some scale failure, involving both a decohesion, buckling and tensile cracking route and a shear cracking and wedging route. (orig.)

  16. Effect of Al–5Ti–1B grain refiner on the microstructure, mechanical properties and acoustic emission characteristics of Al5052 aluminium alloy

    Directory of Open Access Journals (Sweden)

    Amulya Bihari Pattnaik

    2015-04-01

    Full Text Available In the present investigation, the effect of Al–5Ti–1B grain refiner on the microstructure, mechanical properties and acoustic emission characteristics of Al 5052 aluminium alloy have been studied. Microstructural analysis showed the presence of primary α solid solution. No Al–Mg phase was found to be formed due to the presence of magnesium in the solid solution. The results indicated that the addition of Al–5Ti–1B grain refiner into the alloy caused a significant improvement in ultimate tensile strength (UTS and elongation values from 114 MPa and 7.8% to 185 MPa and 18% respectively. The main mechanisms behind this improvement were found to be due to the grain refinement during solidification and segregation of Ti at primary α grain boundaries. Acoustic emission (AE results indicated that intensity of AE signals increased with increase in Al–5Ti–1B master alloy content, which had been attributed to the combined effect of dislocation motion and grain refinement. The field emission scanning electron microscopy (FESEM and energy dispersive X-ray (EDX analysis were used to study the microstructure and fracture surfaces of the samples.

  17. Effect of grain refiner on the tensile and impact properties of Al–Si–Mg cast alloys

    International Nuclear Information System (INIS)

    Samuel, E.; Golbahar, B.; Samuel, A.M.; Doty, H.W.; Valtierra, S.; Samuel, F.H.

    2014-01-01

    The present study aims to investigate the influence of the addition of Ti and B in the form of five different grain refiners/aluminium master alloys (Al–10%Ti, Al–5%Ti–1%B, Al–2.5%Ti–2.5%B, Al–1.7%Ti–1.4%B and Al–4%B) in conjunction with that of Sr (as modifier) added in the form of Al–10%Sr master alloy to A356.2 alloy. Grain refinement of an A356.2 alloy with Ti and B additions in the ranges of 0.02–0.5% and 0.01–0.5%, respectively, was examined using these different types of grain refiners. Strontium additions of 30 and 200 ppm were made. All alloys were T6-heat treated before mechanical testing. Tensile and impact tests were conducted to evaluate the influence of the interaction between grain refiner and modifier on the mechanical properties. The properties were determined for both the as-cast and heat-treated conditions. - Highlights: • Grain refining of 356 alloys using five types of grain refiners. • Interaction between the added grain refiner and amount of modifier used (i.e. 30 or 200ppm Sr). • Role of the added amount of Ti and/or B on the eutectic Si particle characteristics. • Role of Ti/B on the impact toughness of 356 alloys modified with Sr (30 or 200ppm)

  18. Finite element modelling of shot peening and peen forming processes and characterisation of peened AA2024-T351 aluminium alloy

    Science.gov (United States)

    Gariepy, Alexandre

    The main purpose of this thesis was to develop and validate finite element (FE) simulation tools for shot peening and peen forming. The specific aim was to achieve quantitatively accurate predictions for both processes and demonstrate the potential of reliable FE modelling for scientific investigation and industrial applications. First, an improved dynamic impact model that takes into account the stochastic nature of shot peening was proposed by carefully studying its dimensions, introducing a dispersion of shot sizes and significantly reducing its computational cost. In addition, cyclic mechanical testing was conducted to define a suitable material constitutive theory for aluminium alloy (AA) 2024-T3/T351 subjected to shot peening. By combining a realistic shot peening model with an appropriate material law, fairly good residual stress predictions were achieved for three different sets of shot peening parameters. Second, an experimental and numerical characterization of AA2024-T351 shot peened with parameters representative of fatigue life improvement applications was conducted. Multiple techniques, such as micro-indentation, residual stress determination and electron backscatter diffraction, were combined to gain a better understanding of the influence of shot peening on the material. The potential uses of finite element simulation to complement experimental data were also studied. The material heterogeneity arising from the random impact sequence was investigated and it was found that the impact modelling methodology could provide useful information on such heterogeneities. Third, a novel peen forming simulation methodology was introduced. The impact model provided the necessary input data as part of a multiscale approach. Numerically calculated unbalanced induced stress profiles were input into shell elements and the deformed shape after peen forming was computed as a springback analysis. In addition, a simple interpolation method was proposed to model the

  19. Study of the thermal diffusion of ion-alloyed cesium in aluminium, silicon and titanium by the Rutherford backscattering method

    International Nuclear Information System (INIS)

    Bulgakov, Yu.V.; Savel'eva, L.M.

    1987-01-01

    Thermal diffusion of cesium implanted at 120 keV energy in monocrystal silicon and in polycrystal aluminium and titanium is investigated by the method of Rutherford backscattering (RBS). Parameters of temperature dependence of the cesium diffusion coefficient in materials given above are determined. Cesium is shown to be one of the most movable impurities

  20. Effect of post-weld aging treatment on mechanical properties of Tungsten Inert Gas welded low thickness 7075 aluminium alloy joints

    International Nuclear Information System (INIS)

    Temmar, M.; Hadji, M.; Sahraoui, T.

    2011-01-01

    Highlights: → The effects of post-weld aging treatment on the properties of joints is studied. → The post-weld aging treatment increases the tensile strength of TIG welded joints. → The strengthening is due to a balance of dissolution, reversion and precipitation. → Simple post-weld aging at 140 o C enhances the properties of the welded joints. -- Abstract: This paper reports the influence of post-weld aging treatment on the microstructure, tensile strength, hardness and Charpy impact energy of weld joints low thickness 7075 T6 aluminium alloy welded by Tungsten Inert Gas (TIG). Hot cracking occurs in aluminium welds when high levels of thermal stress and solidification shrinkage are present while the weld is undergoing various degrees of solidification. Weld fusion zones typically exhibit microstructure modifications because of the thermal conditions during weld metal solidification. This often results in low weld mechanical properties and low resistance to hot cracking. It has been observed that the mechanical properties are very sensitive to microstructure of weld metal. Simple post-weld aging treatment at 140 o C applied to the joints is found to be beneficial to enhance the mechanical properties of the welded joints. Correlations between microstructures and mechanical properties were discussed.

  1. The effect of extrusion temperature on the development of deformation microstructures in 5052 aluminium alloy processed by equal channel angular extrusion

    Energy Technology Data Exchange (ETDEWEB)

    Chen, Y.C.; Huang, Y.Y.; Chang, C.P.; Kao, P.W

    2003-04-18

    Commercial 5052 aluminium alloy was used to study the effect of extrusion temperature on the development of deformation microstructures processed by equal channel angular extrusion (ECAE). The extrusion temperatures used were between 50 and 300 deg. C, and the cumulative equivalent strain was 5.6. Transmission electron microscopy was adopted to characterize quantitatively the metallographical parameters, namely grain size, grain aspect ratio, and boundary disorientation. Raising extrusion temperature causes grain size to increase, grain shape to become more equiaxed-like, and a dramatic increase of low angle boundaries. Both grain and subgrain boundaries with low disorientations are formed at elevated temperatures. Comments on disorientation measuring techniques in transmission electron microscope are also given.

  2. Simulation calculations for the positron annihilation in aluminium alloys for the study of the segregate formation; Simulationsrechnungen zur Positronenannihilation in Aluminiumlegierungen zur Untersuchung der Ausscheidungsbildung

    Energy Technology Data Exchange (ETDEWEB)

    Korff, Bjoern

    2010-11-29

    Highly solid aluminium alloys owe their properties to small, finely distributed segregations of alloy atoms. For the better understanding of the temperature treatment, which is required in order to control the segregate formation, it is important, to determine informations on the first early stages from few atoms. In the positron-annihilation spectroscopy (PAS) positrons are trapped in the vacancies of a solid and yield at their annihilation with surrounding electrons informations from their direct environment. because the formation of segregates requires a diffusion of the extraneous atoms by means of the vacancies, the PAS represents one of the few examination methods, by which already the formation of smallest segregations can be observed. By the comparison of measurement quantities of the PAS with simulations for different possible arrangements of extraneous atoms around the vacancy the atomic environment of the vacancy can be identified. In order to make this possible also in aluminium alloys, in which the number of the possible defect types is relatively large, a good description of the measurement values by the simulation is especially important. In the framework of this thesis the program AB2D was developed, by which the Doppler shift of the annihilation radiation can be determined. Contrarily to already existing approaches here valence-electron wave functions are used, which were calculated with the program ABINIT. By this way the main uncertainty by the description of the valence electrons in atomic superposition is cancelled. Because ABINIT is based on pseudopotentials, the projector augmented-wave method is used in order to describe the higher momenta of the electrons near the nuclei more realistically. With AB2D simulations for vacancy-extraneous-atom complexes and segregation phases in the alloy systems Al-Cu, Al-Mg-Cu, and Al-Mg-Si were performed. A comparison with measurements on samples, which were only few minutes stored at room temperature

  3. The role of solidification rate in the corrosion resistance of a directionally solidified novel aluminium-lanthanum alloy

    Energy Technology Data Exchange (ETDEWEB)

    Dzib-Perez, L. [Programa de Corrosion del Golfo de Mexico, Universidad Autonoma de Campeche, Av. Agustin Melgar s/n, Col. Buenavista, CP 24030 Campeche, Campeche (Mexico); Gonzalez-Sanchez, J. [Programa de Corrosion del Golfo de Mexico, Universidad Autonoma de Campeche, Av. Agustin Melgar s/n, Col. Buenavista, CP 24030 Campeche, Campeche (Mexico)]. E-mail: jagonzal@uacam.mx; Perez, T. [Programa de Corrosion del Golfo de Mexico, Universidad Autonoma de Campeche, Av. Agustin Melgar s/n, Col. Buenavista, CP 24030 Campeche, Campeche (Mexico); Bartolo-Perez, P. [Programa de Corrosion del Golfo de Mexico, Universidad Autonoma de Campeche, Av. Agustin Melgar s/n, Col. Buenavista, CP 24030 Campeche, Campeche (Mexico); CINVESTAV-Merida, Applied Physics Department, Carr. antigua a Progreso, km 6, CP 97310 Merida, Yucatan (Mexico); Juarez, A. [CIATEQ. Calzada del Retablo 150, CP 76150 Queretaro, Queretaro (Mexico)

    2006-08-15

    The corrosion resistance of a novel Al-12.6 wt.%La alloy manufactured using unidirectional solidification was studied by sensitive electrochemical techniques. It was found that the electrochemical behaviour of the alloy depends upon the formation of non-passive corrosion product layers. Different solidification rates produced dissimilar microstructures which promoted selective dissolution when the alloy was anodically polarized in distilled water. A model for the electrochemical behaviour of this alloy was proposed based on an equivalent circuit that simulated the impedance results.

  4. Study of the aqueous corrosion mechanisms and kinetics of the AlFeNi aluminium based alloy used for the fuel cladding in the Jules Horowitz research reactor

    International Nuclear Information System (INIS)

    Wintergerst, M.

    2009-05-01

    For the Jules Horowitz new material-testing reactor (JHR), an aluminium base alloy, called AlFeNi, will be used for the cladding of the fuel plates. This alloy (Al - 1% Fe - 1% Ni - 1 % Mg), which is already used as fuel cladding, was developed for its good corrosion resistance in water at high temperatures. However, few studies dealing with the alteration process in water and the relationships with irradiation effects have been performed on this alloy. The conception of the JHR fuel requires a better knowledge of the corrosion mechanisms. Corrosion tests were performed in autoclaves at 70 C, 165 C and 250 C on AlFeNi plates representative of the fuel cladding. Several techniques were used to characterize the corrosion scale: SEM, TEM, EPMA, XRD, Raman spectroscopy. Our observations show that the corrosion scale is made of two main layers: a dense amorphous scale close to the metal and a porous crystalline scale in contact with the water. More than the morphology, the chemical compositions of both layers are different. This duplex structure results from a mixed growth mechanism: an anionic growth to develop the inner oxide and a cationic diffusion followed by a dissolution-precipitation process to form the outer one. Dynamic experiments at 70 C and corrosion kinetics measurements have demonstrated that the oxide growth process is controlled by a diffusion step associated to a dissolution/precipitation process. A corrosion mechanism of the AlFeNi alloy in aqueous media has been proposed. Then post-irradiation exams performed on irradiated fuel plates were used to investigate the effects of the irradiation on the corrosion behaviour in the reactor core. (author)

  5. Chemical Changes at the Interface Between Low Carbon Steel and an Al-Si Alloy During Solution Heat Treatment

    OpenAIRE

    Zhe, M.; Dezellus, O.; Gardiola, B.; Braccini, M.; Viala, J.C.

    2011-01-01

    International audience; The aim of this work was to characterize the chemical changes during solid state solution heat treatment of a metallurgically bonded steel/Al-Si interface. For this purpose, low carbon steel plates covered with the A-S7G03 aluminium alloy (7wt%Si, 0.3wt%Mg analogous to A356) were prepared by dip coating, water-quenching to room temperature and reheating in the solid state at 480-560°C for 3 to 160 hours. Upon reheating at 535 °C, a reaction layer was observed to grow a...

  6. Mechanical properties of friction stir welded butt joint of steel/aluminium alloys: effect of tool geometry

    Science.gov (United States)

    Syafiq, W. M.; Afendi, M.; Daud, R.; Mazlee, M. N.; Majid, M. S. Abdul; Lee, Y. S.

    2017-10-01

    This paper described the mechanical properties from hardness testing and tensile testing of Friction Stir Welded (FSW) materials. In this project, two materials of aluminium and steel are welded using conventional milling machine and tool designed with different profile and shoulder size. During welding the temperature along the weld line is collected using thermocouples. Threaded pins was found to produce stronger joints than cylindrical pins. 20 mm diameter shoulder tool welded a slightly stronger joint than 18 mm diameter one, as well as softer nugget zone due to higher heat input. Threaded pins also contributed to higher weld temperature than cylindrical pins due to increase in pin contact surface. Generally, higher temperatures were recorded in aluminium side due to pin offset away from steel.

  7. Aluminium in foodstuff and the influence of aluminium foil used for food preparation or short time storage.

    Science.gov (United States)

    Ertl, Kathrin; Goessler, Walter

    2018-02-28

    Aluminium is an omnipresent part of everyday life. It is widely used in industry and furthermore in products like cosmetics, sun creams or it can be applied for instance as aluminium foil by consumers during food preparation in households. However, over the last decades the toxicity of aluminium for humans has been heavily discussed and is still not completely clarified. Therefore, food aluminium concentrations were investigated in different untreated foodstuff as well as a possible aluminium transfer from aluminium foil to food. The results show that untreated food is not significantly contaminated. Furthermore, short time contact to aluminium foil increases the food aluminium concentration only marginal. Nevertheless, as soon as the food is in contact to aluminium foil and at the same time in contact with metals (alloys) with a higher standard electrode potential than aluminium (-1.66 V) high aluminium contaminations were observed.

  8. An improved billet on billet extrusion process of continuous aluminium alloy shapes for cryogenic applications in the Compact Muon Solenoid experiment

    CERN Document Server

    Tavares, S S

    2003-01-01

    The Compact Muon Solenoid (CMS) is one of the experiments being designed in the framework of the Large Hadron Collider accelerator at CERN. CMS will contain the largest and the most powerful superconducting solenoid magnet ever built in terms of stored energy. It will work at 4.2 K, will have a magnetic length of 12.5 m, with a free bore of 6m and will be manufactured as a layered and modular structure of NbTi cables embedded in a high purity (99.998%) Al- stabiliser. Each layer consists of a wound continuous length of 2.55 km. In order to withstand the high electromagnetic forces, two external aluminium alloy reinforcing sections are foreseen. These reinforcements, of 24 mm multiplied by 18 mm cross-section, will be continuously electron beam (EB) welded to the pure Al-stabiliser. The alloy EN AW-6082 has been selected for the reinforcements due to its excellent extrudability, high strength in the precipitation hardened state, high toughness and strength at cryogenic temperatures and ready EB weldability. Ea...

  9. Increasing strength, ductility and impact toughness of ultrafine-grained 6063 aluminium alloy by combining ECAP and a high-temperature short-time aging

    Energy Technology Data Exchange (ETDEWEB)

    Meyer, L W; Schoenherr, R; Hockauf, M, E-mail: robert.schoenherr@mb.tu-chemnitz.d [Chemnitz University of Technology, Materials and Impact Engineering, D-09107 Chemnitz (Germany)

    2010-07-01

    Since fully-dense ultrafine or nanocrystalline bulk materials can be processed, there has been an increasing scientific interest in several plastic deformation (SPD) procedures, particularly in the last decade. Especially the equal-channel angular pressing (ECAP) has widely been investigated due to its ability of producing billets sufficiently large for industrial applications in functional or structural components. The significant strength increase based on grain refinement is typically accompanied by a significant decrease in ductility and toughness. Within this work, a new methodology was applied for combining ECAP with a subsequent high-temperature short-time aging for the 6063 aluminium alloy. An increase in strength, ductility as well as impact toughness regarding its coarse grained counterparts was reached. More precisely, ultimate tensile strength, elongation to failure and impact toughness were increased by 46%, 21% and 40% respectively. This was observed after only one run of ECAP at room temperature in a solid-solution treated condition and an aging at 170{sup 0} C for 18 minutes. The regular aging time for maximum strength at 170{sup 0} C is around 6 hours. Longer exposure times lead to recrystallisation and, as for regular aging, it leads to overaging, both causing a decrease of properties. The work demonstrates a strategy for an efficient processing of commercial Al-Mg-Si alloys with outstanding mechanical properties.

  10. Increasing strength, ductility and impact toughness of ultrafine-grained 6063 aluminium alloy by combining ECAP and a high-temperature short-time aging

    Science.gov (United States)

    Meyer, L. W.; Schönherr, R.; Hockauf, M.

    2010-07-01

    Since fully-dense ultrafine or nanocrystalline bulk materials can be processed, there has been an increasing scientific interest in several plastic deformation (SPD) procedures, particularly in the last decade. Especially the equal-channel angular pressing (ECAP) has widely been investigated due to its ability of producing billets sufficiently large for industrial applications in functional or structural components. The significant strength increase based on grain refinement is typically accompanied by a significant decrease in ductility and toughness. Within this work, a new methodology was applied for combining ECAP with a subsequent high-temperature short-time aging for the 6063 aluminium alloy. An increase in strength, ductility as well as impact toughness regarding its coarse grained counterparts was reached. More precisely, ultimate tensile strength, elongation to failure and impact toughness were increased by 46%, 21% and 40% respectively. This was observed after only one run of ECAP at room temperature in a solid-solution treated condition and an aging at 170° C for 18 minutes. The regular aging time for maximum strength at 170° C is around 6 hours. Longer exposure times lead to recrystallisation and, as for regular aging, it leads to overaging, both causing a decrease of properties. The work demonstrates a strategy for an efficient processing of commercial Al-Mg-Si alloys with outstanding mechanical properties.

  11. The effect of surface pre-conditioning treatments on the local composition of Zr-based conversion coatings formed on aluminium alloys

    Science.gov (United States)

    Cerezo, J.; Vandendael, I.; Posner, R.; de Wit, J. H. W.; Mol, J. M. C.; Terryn, H.

    2016-03-01

    This study investigates the effect of different alkaline, acidic and thermal pre-conditioning treatments applied to different Al alloy surfaces. The obtained results are compared to the characteristics of Zr-based conversion coatings that were subsequently generated on top of these substrates. Focus is laid on typical elemental distributions on the sample surfaces, in particular on the amount of precipitated functional additives such as Cu species that are present in the substrate matrix as well as in the conversion bath solutions. To this aim, Field Emission Auger Electron spectra, depth profiles and surface maps with superior local resolution were acquired and compared to scanning electron microscopy images of the sample. The results show how de-alloying processes, which occur at and around intermetallic particles in the Al matrix during typical industrial alkaline or acidic cleaning procedures, provide a significant source of crystallization cores for any following coating processes. This is in particular due for Cu-species, as the resulting local Cu structures on the surface strongly affect the film formation and compositions of state-of-the-art Zr-based films. The findings are highly relevant for industrial treatments of aluminium surfaces, especially for those that undergo corrosion protection and painting process steps prior to usage.

  12. Increasing strength, ductility and impact toughness of ultrafine-grained 6063 aluminium alloy by combining ECAP and a high-temperature short-time aging

    International Nuclear Information System (INIS)

    Meyer, L W; Schoenherr, R; Hockauf, M

    2010-01-01

    Since fully-dense ultrafine or nanocrystalline bulk materials can be processed, there has been an increasing scientific interest in several plastic deformation (SPD) procedures, particularly in the last decade. Especially the equal-channel angular pressing (ECAP) has widely been investigated due to its ability of producing billets sufficiently large for industrial applications in functional or structural components. The significant strength increase based on grain refinement is typically accompanied by a significant decrease in ductility and toughness. Within this work, a new methodology was applied for combining ECAP with a subsequent high-temperature short-time aging for the 6063 aluminium alloy. An increase in strength, ductility as well as impact toughness regarding its coarse grained counterparts was reached. More precisely, ultimate tensile strength, elongation to failure and impact toughness were increased by 46%, 21% and 40% respectively. This was observed after only one run of ECAP at room temperature in a solid-solution treated condition and an aging at 170 0 C for 18 minutes. The regular aging time for maximum strength at 170 0 C is around 6 hours. Longer exposure times lead to recrystallisation and, as for regular aging, it leads to overaging, both causing a decrease of properties. The work demonstrates a strategy for an efficient processing of commercial Al-Mg-Si alloys with outstanding mechanical properties.

  13. Influence of Sludge Particles on the Fatigue Behavior of Al-Si-Cu Secondary Aluminium Casting Alloys

    Directory of Open Access Journals (Sweden)

    Lorella Ceschini

    2018-04-01

    Full Text Available Al-Si-Cu alloys are the most widely used materials for high-pressure die casting processes. In such alloys, Fe content is generally high to avoid die soldering issues, but it is considered an impurity since it generates acicular intermetallics (β-Fe which are detrimental to the mechanical behavior of the alloys. Mn and Cr may act as modifiers, leading to the formation of other Fe-bearing particles which are characterized by less harmful morphologies, and which tend to settle on the bottom of furnaces and crucibles (usually referred to as sludge. This work is aimed at evaluating the influence of sludge intermetallics on the fatigue behavior of A380 Al-Si-Cu alloy. Four alloys were produced by adding different Fe, Mn and Cr contents to A380 alloy; samples were remelted by directional solidification equipment to obtain a fixed secondary dendrite arm spacing (SDAS value (~10 μm, then subjected to hot isostatic pressing (HIP. Rotating bending fatigue tests showed that, at room temperature, sludge particles play a detrimental role on fatigue behavior of T6 alloys, diminishing fatigue strength. At elevated temperatures (200 °C and after overaging, the influence of sludge is less relevant, probably due to a softening of the α-Al matrix and a reduction of stress concentration related to Fe-bearing intermetallics.

  14. Nd:YAG laser welding aluminum alloys

    Energy Technology Data Exchange (ETDEWEB)

    Jimenez, E. Jr.

    1992-02-01

    Autogenous Nd:YAG laser welding wrought 4047, 1100, 3003, 2219, 5052, 5086, 5456, and 6061 and cast A356 aluminum alloys to cast A356 aluminum alloy in restrained annular weld joints was investigated. The welds were 12.7 mm (0.375 in.) and 9.5 mm (0.375 in.) diameter with approximately 0.30 mm (0.012 in.) penetration. This investigation determined 4047 aluminum alloy to be the optimum alloy for autogenous Nd:YAG laser welding to cast A356 aluminum alloy. This report describes the investigation and its results.

  15. Effect of Cold Rolling Reduction Rate on Corrosion Behaviour of Twin-roll Cast 8006 Aluminium Alloys

    OpenAIRE

    KÜÇÜK, İsrafil

    2018-01-01

    Utilization of aluminum alloys in automotive industry takes a crucial role in recent years due to their excellent properties such as corrosion resistance and light weight. 3003 and 8006 aluminum alloys have been particularly used as a heat exchanger compartment due to their corrosion resistance feature which has a perfect match for a heat exchanger fin stocks and a destructive salty environment in this car’s part. In the present work, an effect of cold rolling reduction (CRR) rate on the corr...

  16. Study of the uniform corrosion of an aluminium alloy used for the fuel cladding of the Jules Horowitz experimental reactor; Etude de la corrosion uniforme d'un alliage d'aluminium utilise comme gainage du combustible nucleaire du reacteur experimental Jules Horowitz

    Energy Technology Data Exchange (ETDEWEB)

    Wintergerst, M. [CEA Saclay, Dept. des Materiaux pour le Nucleaire (DEN/DANS/DMN/SEMI), 91 - Gif-sur-Yvette (France)

    2008-07-01

    For the Jules Horowitz new material testing reactor, an aluminium base alloy, AlFeNi, will be used for the cladding of the fuel plates. Taking into account the thermal properties of the alloy and of its oxide, the corrosion of the fuel cans presents many problems. The aim of this thesis is to provide a growing kinetic of the oxide layer at the surface of the AlFeNi fuel can in order to predict the life time of fuel element. Thus the mechanism of degradation of the cladding will be describe in order to integrate the different parameters of the operating reactor. (A.L.B.)

  17. Real-time synchrotron x-ray observations of equiaxed solidification of aluminium alloys and implications for modelling

    Science.gov (United States)

    Prasad, A.; Liotti, E.; McDonald, S. D.; Nogita, K.; Yasuda, H.; Grant, P. S.; StJohn, D. H.

    2015-06-01

    Recently, in-situ observations were carried out by synchrotron X-ray radiography to observe the nucleation and growth in Al alloys during solidification. The nucleation and grain formation of a range of Al-Si and Al-Cu binary alloys were studied. When grain refiner was added to the alloys, the location of the nucleation events was readily observed. Once nucleation began it continued to occur in a wave of events with the movement of the temperature gradient across the field of view due to cooling. Other features observed were the settling of the primary phase grains in the Al-Si alloys and floating in the Al-Cu alloys, the effects of convection with marked fluctuation of the growth rate of the solid-liquid interface in the Al-Si alloys, and an absence of fragmentation. The microstructures are typical of those produced in the equiaxed zone of actual castings. These observations are compared with predictions arising from the Interdependence model. The results from this comparison have implications for further refinement of the model and simulation and modelling approaches in general. These implications will be discussed.

  18. Fabrication of Carbon Nanofibers/A356 Nanocomposites by High-Intensity Ultrasonic Processing

    Science.gov (United States)

    Wu, Qing-Jie; Yan, Hong

    2018-03-01

    A356 alloy reinforced with carbon nanofibers (CNFs) was fabricated by high-intensity ultrasonic vibration processing. The microstructure and mechanical properties were investigated. The distribution of CNFs became more and more uniform with the increase of ultrasonic power, and the mechanical properties of nanocomposites were significantly enhanced accordingly. The yield strength (YS), ultimate tensile strength (UTS), and microhardness of the nanocomposite increased by 38.3, 21.9, and 43.2 pct, respectively, at a CNF content of 0.9 wt pct compared with the matrix without CNF addition. The improvement in mechanical properties was the effect of CNFs on the thermal expansion mismatch strengthening of the nanocomposite, the grain refinement of the nanocomposite, and the load transfer from the matrix to the nanofibers.

  19. Investigation on the of effect of self assembling molecules on the corrosion resistance of the 1050 aluminium alloy

    International Nuclear Information System (INIS)

    Szurkalo, Margarida

    2009-01-01

    Surface treatments are widely used to increase the corrosion resistance of metallic materials. Specifically for aluminum and aluminum alloys, treatment with hexavalent chromium is one of the most used, due to its efficiency and ease of application. However, because of environmental restrictions and the high cost involved in the treatments of waste generated in this process, alternative methods for its replacement are necessary. In this context, this study investigated the effect of the surface treatment with self-assembling molecules (SAM) based on phosphonate compounds on the corrosion of the 1050 aluminum alloy. The conditions adopted for the SAM treatment were determined by conductivity and contact angle measurements, besides electrochemical experiments. Electrochemical techniques, specifically: measurement of the open circuit potential (OCP) variation with time, electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization curves were used to evaluate the corrosion resistance of the 1050 aluminum alloy exposed to SAM treatment The experimental impedance diagrams were interpreted using equivalent electrical circuit models that simulate film that is formed on the alloy surface. The results of the samples treated with SAM were compared with those of samples either without any treatment or treated with chromatizing conversion coating with Cr(VI) and showed that the first treatment significantly increased the corrosion resistance of the aluminum alloy and approached that of chromatizing with Cr(VI) process. (author)

  20. Rapidly solidified aluminium for optical applications

    NARCIS (Netherlands)

    Gubbels, G.P.H.; Venrooy, B.W.H. van; Bosch, A.J.; Senden, R.

    2008-01-01

    This paper present the results of a diamond turning study of a rapidly solidified aluminium 6061 alloy grade, known as RSA6061. It is shown that this small grain material can be diamond turned to smaller roughness values than standard AA6061 aluminium grades. Also, the results are nearly as good as

  1. Electron Conditioning of Technical Aluminium Surfaces

    Energy Technology Data Exchange (ETDEWEB)

    Le Pimpec, F

    2004-09-02

    The effect of electron conditioning on commercially aluminium alloys 1100 and 6063 were investigated. Contrary to the assumption that electron conditioning, if performed long enough, can reduce and stabilize the SEY to low values (= 1.3, value of many pure elements [1]), the SEY of aluminium did not go lower than 1.8. In fact, it reincreases with continued electron exposure dose.

  2. Characterization of surface liquid segregation in SSM-HPDC aluminium alloys 7075, 2024, 6082 and A201

    CSIR Research Space (South Africa)

    Moller, H

    2010-09-01

    Full Text Available analysis. Chemical profiles of the main alloying elements were plotted for the cross-section of the plates in the as-cast and T6 (after solution treatment) temper conditions. Vickers hardness profiles from the surface to the centre of the plates were...

  3. The effect of scandium, transition metals and in purities on hardening of aluminium alloys upon decomposition of solid solutions

    International Nuclear Information System (INIS)

    Zakharov, V.V.; Rostova, T.D.

    2007-01-01

    Strengthening of aluminum alloys of the Al-Sc system in ingots due to decomposition of the solid solution of scandium in aluminum is studied as a function of the content of scandium (varied from 0.14 to 0.55%), the presence of Zr, Ti, Hf, V, and Co additives at the same content of scandium (0.2%), of the Sc/Zr proportion at the same total content of Sc + Zr, and as a function of iron and silicon admixtures. Zirconium addition produces the highest effect, increasing the hardness and stabilizing the strengthening, extending it to a wider temperature range of aging. Additions of Ti, Hf produce a similar, though a less pronounced effect. Vanadium addition decreases the hardness of Al-0.2%Sc alloy. The presence of zirconium neutralizes the negative effect of vanadium. Cobalt addition does not effect the hardness of Al-0.2%Sc. The greatest strengthening during decomposition of solid solution in the Al-Sc-Zr system alloys is achieved at equal content of Sc and Zr. In this case, the maximum saturation of the solid solution with scandium and zirconium occurs during melting of ingots and as a result of subsequent heating, judging by the alloy location in the phase diagram, the phase Al 3 (Sc 1-x , Zr x ), where scandium atoms are replaced with zirconium atoms to utmost extent, is separated [ru

  4. Influence of surface liquid segregation on corrosion behavior of semi-solid metal high pressure die cast aluminium alloys

    CSIR Research Space (South Africa)

    Masuku, EP

    2010-09-01

    Full Text Available of the major advantages of SSM processing is that high strength wrought alloys such as 7075 and 2024 can be used to produce near-net shape products. Corrosion is a surface phenomenon, and since the surface compositions of the SSM-processed components...

  5. Spot welding of aluminium alloy sheets to coated steel sheets. Kakushu mekki koban to arumi gokin no spot yosetsusei

    Energy Technology Data Exchange (ETDEWEB)

    Inoue, S.; Fukumura, K.; Soga, S. (Nisshin Steel Co. Ltd., Tokyo (Japan))

    1994-03-31

    Welding aluminum alloy sheets with coated steel sheets has become used frequently in association with weight reduction in automobiles. This paper describes investigations on the effects of spot welding aluminum alloy sheets with different kinds of coated steel sheets on optimal welding conditions and weld strength. An AC single-phase spot welding machine was used for an experiment using an aluminum alloy(5052)with a thickness of 1 mm(referred to as A)and different coated steel sheets with a thickness of 0.8 mm(referred to as B). The result may be summarized as follows: the weldable value of the electric current is closer to that for between the B steel sheets than the middle of that for between the As and between Bs; while the weldable current range is affected little by the coating materials when a CF electrode is used, it grows greater in aluminum coated steel sheets and hot-dip galvanized steel sheets than in alloyed hot-dip galvanized steel sheets and cold-rolled steel sheets when an R-type electrode is used; influence of the coating materials was observed in tensile shear strength and cross tensile shear strength; and any combination of metals shows fatigue strength lower than that in the A-A combination in a fatigue test of cross tensile system. 5 refs., 12 figs., 6 tabs.

  6. Effect of Welding Speed on Microstructure and Mechanical Properties due to The Deposition of Reinforcements on Friction Stir Welded Dissimilar Aluminium Alloys

    Directory of Open Access Journals (Sweden)

    Baridula Ravinder Reddy

    2017-01-01

    Full Text Available The strength of the welded joint obtained by solid state stir welding process was found to be improved as compared to fusion welding process. The deposition of reinforcements during friction stir welding process can further enhance the strength of the welded joint by locking the movement of grain boundaries. In the present study, the aluminium alloys AA2024 and AA7075 were welded effectively by depositing the multi-walled carbon nanotubes in to the stir zone. The mechanical properties and microstructures were studied by varying the traverse speed at constant rotational speed. The results show that rotating tool pin stirring action and heat input play an important role in controlling the grain size. The carbon nanotubes were found to be distributed uniformly at a welding speed (traverse speed of 80mm/min. This enhanced the mechanical properties of the welded joint. The microstructure and Electron dispersive X-ray analysis (EDX studies indicate that the deposition of carbon nanotubes in the stir zone was influenced by the traverse speed.

  7. Experimental and Mathematical Modeling for Prediction of Tool Wear on the Machining of Aluminium 6061 Alloy by High Speed Steel Tools

    Directory of Open Access Journals (Sweden)

    Okokpujie Imhade Princess

    2017-12-01

    Full Text Available In recent machining operation, tool life is one of the most demanding tasks in production process, especially in the automotive industry. The aim of this paper is to study tool wear on HSS in end milling of aluminium 6061 alloy. The experiments were carried out to investigate tool wear with the machined parameters and to developed mathematical model using response surface methodology. The various machining parameters selected for the experiment are spindle speed (N, feed rate (f, axial depth of cut (a and radial depth of cut (r. The experiment was designed using central composite design (CCD in which 31 samples were run on SIEG 3/10/0010 CNC end milling machine. After each experiment the cutting tool was measured using scanning electron microscope (SEM. The obtained optimum machining parameter combination are spindle speed of 2500 rpm, feed rate of 200 mm/min, axial depth of cut of 20 mm, and radial depth of cut 1.0mm was found out to achieved the minimum tool wear as 0.213 mm. The mathematical model developed predicted the tool wear with 99.7% which is within the acceptable accuracy range for tool wear prediction.

  8. Experimental and Mathematical Modeling for Prediction of Tool Wear on the Machining of Aluminium 6061 Alloy by High Speed Steel Tools

    Science.gov (United States)

    Okokpujie, Imhade Princess; Ikumapayi, Omolayo M.; Okonkwo, Ugochukwu C.; Salawu, Enesi Y.; Afolalu, Sunday A.; Dirisu, Joseph O.; Nwoke, Obinna N.; Ajayi, Oluseyi O.

    2017-12-01

    In recent machining operation, tool life is one of the most demanding tasks in production process, especially in the automotive industry. The aim of this paper is to study tool wear on HSS in end milling of aluminium 6061 alloy. The experiments were carried out to investigate tool wear with the machined parameters and to developed mathematical model using response surface methodology. The various machining parameters selected for the experiment are spindle speed (N), feed rate (f), axial depth of cut (a) and radial depth of cut (r). The experiment was designed using central composite design (CCD) in which 31 samples were run on SIEG 3/10/0010 CNC end milling machine. After each experiment the cutting tool was measured using scanning electron microscope (SEM). The obtained optimum machining parameter combination are spindle speed of 2500 rpm, feed rate of 200 mm/min, axial depth of cut of 20 mm, and radial depth of cut 1.0mm was found out to achieved the minimum tool wear as 0.213 mm. The mathematical model developed predicted the tool wear with 99.7% which is within the acceptable accuracy range for tool wear prediction.

  9. Impact properties of the aircraft cast aluminium alloy Al-7Si0.6Mg (A357

    Directory of Open Access Journals (Sweden)

    Alexopoulos N.D.

    2010-06-01

    Full Text Available The impact mechanical properties of the widely used in the aeronautics A357 cast aluminum alloy were investigated by exploiting experiments on an instrumented Charpy impact testing machine. The evaluated impact properties for 25 different artificial aging heat treatment conditions were analyzed and discussed in conjunction with the respective tensile properties. Correlations are proposed to establish useful relationships between impact resistance and tensile strain energy density properties. The established correlations, which are well supported by the performed experiments, can be used to estimate the tensile ductility and toughness of the A357 cast aluminum alloy from the Charpy impact test. Performed fractographic analyses were supporting the physically arbitrary correlation between tensile strain energy density and impact resistance.

  10. Synergy of the Plastic Treatment HPT and Shot Peening in Aluminium Alloy Al-Mg-Mn-Sc-Zr

    Directory of Open Access Journals (Sweden)

    Stegliński M.

    2016-06-01

    Full Text Available An improvement in fatigue strength is one of the main factors enabling the use of high-durability Al-Mg-Mn-Sc-Zr alloys in functional components of mobile robots. As part of this study, a computer simulation was carried out using ANSYS LS-DYNA software that involved the hybridization of high pressure torsion (HPT and shot peening (SP forming processes. The numerical analysis was aimed at determining residual stresses and strains that affect the durability and stress characteristics of the analyzed Al alloy. Results of the study indicate that tensile stresses of σ = 300 MPa generated as a result of HPT are transformed into a beneficial stress of σ = 25 MPa resulting from plastic strains caused by SP surface treatment.

  11. Delayed and prompt gamma-ray neutron activation analysis of saudi aluminium and iron alloys using isotopic neutron sources

    International Nuclear Information System (INIS)

    Abu-Talib, M.; Alamoudi, Z.; Hassan, A.M.

    2005-01-01

    The delayed and prompt gamma-ray spectra due to neutron capture in two aluminum and four iron Saudi alloys using 252Cf and 226Ra/Be isotopic neutron sources have been measured. Elemental investigations of each sample lead to identification of many elements by both methods. The elemental concentration values in percent for some elements in each sample are presented. The results were compared and discussed with those obtained by different techniques for the same samples

  12. Aluminium bridges, aluminium bridge decks

    NARCIS (Netherlands)

    Soetens, F.; Straalen, IJ.J. van

    2003-01-01

    Applications of aluminium have grown considerably in building and civil engineering the last decade. In building and civil engineering the increase of aluminium applications is due to various aspects like light weight, durability and maintenance, use of extrusions, and esthetics. The paper starts

  13. Light-weight aluminium bridges and bridge decks. An overview of recent applications

    NARCIS (Netherlands)

    Maljaars, J.; Soetens, F.; Kluyver, D. de

    2008-01-01

    The last decades have shown a large increase in the application of aluminium alloys for light-weight bridges. For bridge construction, aluminium alloys have some specific advantages, but also some points of attention. This paper deals with some recent projects of aluminium bridges, and for these

  14. Equal-channel angular pressing of medium- to high-strength precipitation hardening aluminium wrought alloys; ECAP-Umformung mittel- und hochfester ausscheidungshaertbarer Aluminiumknetlegierungen

    Energy Technology Data Exchange (ETDEWEB)

    Hockauf, M.; Schoenherr, R.; Wagner, S.; Meyer, L.W. [Technische Universitaet Chemnitz, Lehrstuhl Werkstoffe des Maschinenbaus, Erfenschlager Str. 73, 09125 Chemnitz (Germany); Podlesak, H.; Muecklich, S.; Wielage, B.; Weber, D. [Technische Universitaet Chemnitz, Professur fuer Verbundwerkstoffe (Germany); Krueger, L. [Technische Universitaet Bergakademie Freiberg, Institut fuer Werkstofftechnik (Germany); Hahn, F. [Hochschule Mittweida, Fachbereich Maschinenbau/Feinwerktechnik (Germany)

    2009-07-15

    The study deals with the optimisation of medium- to high-strength aluminium wrought alloys. The goal is to define processing routes in order to improve the mechanical properties if compared to their commercial counterparts. It is shown for the Al-Mg-Si and the Al-Cu-Mg-Si system that the application of ECAP enables a significant increase in strength. The strengthening as well as the grain size reduction respectively, benefit from increasing alloying as well as from the degree of aging. It is also shown that the presence of a considerably fine particulate reinforcement hardens the material tremendously during ECAP. The combination of a pre- or post-ECAP heat treatment enables the improvement of the workability on the one hand, reducing the loads on the die, and also gives a better ductility on the other hand. This positive effect is particularly pronounced for low alloying contents and high aging temperatures and can be attributed to the interaction of deformation induced defects and the precipitation activity. The combination of an appropriate set of ECAP parameters (heat treatment condition, ECAP-strain, -temperature, -backpressure) enables the efficient production of outstanding properties. Due to the low workability of AA7075 (Al-Zn-Mg-Cu system) no significant improvement in properties was achieved. (Abstract Copyright [2009], Wiley Periodicals, Inc.) [German] Die Studie befasst sich mit der Eigenschaftsoptimierung verschiedener mittel- und hochfester Aluminiumknetlegierungen. Im Fokus steht die Optimierung von Prozessabfolgen mit denen im Vergleich zu den kommerziell verfuegbaren Referenzzustaenden deutlich bessere mechanische Eigenschaften eingestellt werden koennen. Fuer das Al-Mg-Si- und das Al-Cu-Mg-Si-System wird gezeigt, dass die ECAP-Umformung sehr hohe Festigkeiten ermoeglicht. Je groesser der Legierungsgehalt bzw. Aushaertegrad ist, desto hoehere Festigkeiten und geringere Korngroessen koennen durch ECAP erreicht werden. Ebenso extrem verfestigend

  15. Solid state recycling of aluminium alloys via a porthole die hot extrusion process: Scaling up to production

    Science.gov (United States)

    Paraskevas, Dimos; Kellens, Karel; Deng, Yelin; Dewulf, Wim; Kampen, Carlos; Duflou, Joost R.

    2017-10-01

    Whereas industrial symbiosis has led to increased energy and resource efficiency in process industries, this concept has not yet been applied in discrete product manufacturing. Metal scrap is first conventionally recycled, for which substantial energy and resource efficiency losses have been reported. Recent research has however proven the feasibility of `meltless' recycling of light metal scrap, yielding a first glimpse of potential industrial symbiosis. Various solid state recycling techniques (such as recycling via hot extrusion or Spark Plasma Sintering) have been proposed for scrap consolidation directly into bulk products or semis by physical disruption and dispersion of the oxide surface film by imposing significant plastic and shear strain. Solid State Recycling (SSR) methods can omit substantial material losses as they bypass the metallurgical recycling step. In this context the case of direct production of bulk aluminium profiles via hot extrusion at industrial scale is demonstrated within this paper. The extrusion tests were performed directly into the production line, highlighting the scaling up potentials and the industrial relevance of this research. A significant amount of machining chips were collected, chemically cleaned and cold compacted into chip based billets with ˜80% relative density. Afterwards the scrap consolidation was achieved by imposing significant plastic and shear deformation into the material during hot extrusion through a modified 2-porthole extrusion die-set. The production process sequence along with microstructural investigations and mechanical properties comparison of the cast based profile used as reference versus the chip based profile are presented.

  16. Multiaxial fatigue of cast aluminium EN AC-42000 T6 (G-AlSi7Mg0.3 T6 for automotive safety components under constant and variable amplitude loading

    Directory of Open Access Journals (Sweden)

    C.M. Sonsino

    2016-07-01

    Full Text Available Regarding the fatigue behaviour of EN AC-42000 T6 (A 356 T6, which is the most frequently used cast aluminium alloy for automotive safety components, especially under non-proportional constant and variable normal and shear stress amplitudes with changing principal stress directions, a poor level of knowledge was available. The reported investigations show that, under non-proportional normal and shear stresses, fatigue life is increased in contrast to ductile steels where life is reduced due to changing principal stress directions. This behaviour caused by the low ductility of this alloy (e < 10% compared to quenched and tempered steels suggests the application of the Normal (Principal Stress Hypothesis (NSH. For all of the investigated stress states under multiaxial constant and variable (Gaussian spectrum amplitudes without and with mean stresses, the NSH was able to depict the life increase by the non-proportionality and delivered, for most cases, conservative but non-exaggerated results.

  17. Application of in situ thermography for evaluating the high-cycle and very high-cycle fatigue behaviour of cast aluminium alloy AlSi7Mg (T6).

    Science.gov (United States)

    Krewerth, D; Weidner, A; Biermann, H

    2013-12-01

    The present paper illustrates the application of infrared thermal measurements for the investigation of crack initiation point and crack propagation in the high-cycle and the very high-cycle fatigue range of cast AlSi7Mg alloy (A356). The influence of casting defects, their location, size and amount was studied both by fractography and thermography. Besides internal and surface fatigue crack initiation as a further crack initiation type multiple fatigue crack initiation was observed via in situ thermography which can be well correlated with the results from fractography obtained by SEM investigations. In addition, crack propagation was studied by the development of the temperature measured via thermography. Moreover, the frequency influence on high-cycle fatigue behaviour was investigated. The presented results demonstrate well that the combination of fractography and thermography can give a significant contribution to the knowledge of crack initiation and propagation in the VHCF regime. Copyright © 2013 Elsevier B.V. All rights reserved.

  18. Influence of initial microstructure of aluminium alloy charge after its melting on the hard metal inherited structure

    Directory of Open Access Journals (Sweden)

    Г. О. Іванов

    2016-07-01

    Full Text Available Metal properties heredity in the chain- initial hard state > liquid state > final solidified state has always been interesting for metallurgists. It is known that after the primary melting of charge there occurs microheterogenеous non-equilibrium melt with crystal-like groups of atoms and disordered area in it. With increase in temperature the melt approaches the equilibrium microhomogeneous state. The aim of this work is to study the charge microstructure influence on melt fluidity in the light of quasi-crystal model of liquid structure. Influence of isothermal heating on fluidity of aluminium melt, smelted from fine-grained and coarse-grained charge has been investigated. It has been stated that for coarse-grained metal additional melting of crystallization «genes» takes place in 1,4-quick time, as compared to fine-grained. The coefficients of exponential function for our experimental data have been calculated. It has been stated that the exponent depends on the charge microstructure, and multiplier depends on the soaking temperature. On the basis of A. Einstein equation for the calculation of liquid viscosity from the known fraction of admixtures and clean liquid viscosity an analogical equation for fluidity and calculation of quasi-crystals volume share in the melt have been derived. It has been found that the charge grain size affects the speed of quasi-crystals additional melting in the melt. The reference amount of quasi-crystals at the initial moment of large- and fine-grained charge melting has been calculated from our metallographic, experimental and estimated data

  19. The ‘full sleeve’ application in the horizontal cold-chamber machine for pressure die casting of aluminium alloys

    Directory of Open Access Journals (Sweden)

    Z. Konopka

    2008-04-01

    Full Text Available The ‘full sleeve’ construction has been designed and accomplished in the horizontal cold-chamber pressure die casting machine. Main part of this solution is a counter plunger placed in a movable die half which allows for full filling of the shot sleeve and precisely fixes the metal quantity needed for casting. The purpose of this new construction solution is mainly the reduction of the casting porosity caused by air entrapment and the improvement of both castability and accuracy of the die cavity reproduction. For such a redesigned machine there have been performed examinations consisting in pressure casting of AlSi9Cu alloy (EN AC-46000 at varying plunger velocity in the second stage of injection and varying intensification pressure. The alloy castability (the die filling ability has been measured for each parameter setting. For the purpose of comparison, similar measurements have been performed also for the conventional system without a counter plunger. The castability examination has been done by means of a specially designed die with an impression of a trial casting of variable wall thickness. The experiments have been held according to the assumed factor design 22, what allowed for determining the mathematical models describing the influence of die filling parameters on the castability and the die cavity reproduction level. Both alternatives of the experiment confirmed the positive influence of plunger velocity and intensification pressure increase on the improvement of castability, the measure of the latter being the filled length of the impression. Applying of the new ‘full sleeve’ solution has improved castability for each experiment by about 20% as compared with conventional alternative. Castability in the ‘full sleeve’ system has been increased even for low values of plunger velocity and intensification pressure. For both alternative systems the influence of plunger velocity has been found, as an average, by four times

  20. Effect of tool shape and welding parameters on mechanical properties and microstructure of dissimilar friction stir welded aluminium alloys

    Directory of Open Access Journals (Sweden)

    Chetan Aneja

    2016-07-01

    Full Text Available In the present experimental study, dissimilar aluminum alloy AA5083 and AA6082 were friction stir welded by varying tool shape, welding speed and rotary speed of the tool in order to investigate the effect of varying tool shape and welding parameters on the mechanical properties as well as microstructure. The friction stir welding (FSW process parameters have great influence on heat input per unit length of weld. The outcomes of experimental study prove that mechanical properties increases with decreasing welding speed. Furthermore mechanical properties were also found to improve as the rotary speed increases and the same phenomenon was found to happen while using straight cylindrical threaded pin profile tool. The microstructure of the dissimilar joints revealed that at low welding speeds, the improved material mixing was observed. The similar phenomenon was found to happen at higher rotational speeds using straight cylindrical threaded tool.

  1. Influence of annealing and deformation on optical properties of ultra precision diamond turned and anodized 6060 aluminium alloy

    DEFF Research Database (Denmark)

    Tabrizian-Ghalehno, Naja; Hansen, Hans Nørgaard; Hansen, P.E.

    2010-01-01

    Influence of cold forging, and subsequent heat treatment and diamond turning on optical quality of anodized film on 6060 (AlMgSi) alloy was investigated and compared with microstructural changes. Heat treatment of the samples was carried out either prior to forging, post-forging, or both....... The surface of the forged material was then diamond turned to a mirror like finish. The diamond turned samples were subsequently anodized in a sulphuric acid bath. The microstructure of the samples was analysed using optical microscopy (LOM), scanning electron microscopy (SEM) and energy dispersive X......-ray spectroscopy (EDX). Colour/brightness measurements were carried out using CIE Lab system. An optical method was used to measure the thickness of the oxide film and roughness of the surface was measured before and after anodizing using stylus, a mechanical instrument, and bidirectional reflection distribution...

  2. Tailored Aluminium based Coatings for Optical Appearance and Corrosion Resistance

    DEFF Research Database (Denmark)

    Aggerbeck, Martin

    The current project investigated the possibility of designing aluminium based coatings focusing on the effect of composition and surface finish on the optical appearance and on the alkaline corrosion properties using titanium as the main alloying element. The main results and discussions...... of these applications, but the use of recycled aluminium compromises this due to the presence of increased levels of impurity and alloying elements. Knowledge on how different alloying elements affect the optical appearance might therefore increase the applicability of recycled aluminium. It was investigated how...... the optical appearance is affected by the alloy composition, surface morphology, and the microstructure. Four commercial aluminium alloys were studied before and after polishing, etching, anodisation, and hot water sealing, giving an overview on how the alloy composition affects the appearance. It was found...

  3. Study of the behavior to corrosion of samples of nuclear grade aluminium sheathed in nickel-phosphorous alloys obtained autocatalytically

    International Nuclear Information System (INIS)

    Castro, Maria Eugenia; Barbero, Jose Alfredo; Bubach, Ernesto

    2006-01-01

    One of the ways to protect an industrially important metallic material against corrosion is by covering the piece with an approximately 1 μm layer of a material whose resistance to corrosion is greater than the element being protected. The mechanism by which the anticorrosive protection is obtained is with the formation of a pore free physical barrier without defects that impedes the arrival of the agents responsible for the electrochemical attack. Other sacrifice anodes such as aluminum or zinc have protective forms based on their dissolution as a consequence of their less electrochemically noble behavior to preserve the material. This work studies the resistance to the corrosion of metallic coatings on nuclear grade aluminum substrates. The focus is on coating nickel-phosphorous (ni-P) alloys obtained autocatalytically from aluminum 6061. A comparative study is carried out of a series of electroless nickel coatings containing different amounts of the latter element, but without surpassing the threshold of 12%. The work includes the study of another nickel coating, Vitrovac 0080 (without phosphorous content) in order to compare structures and anticorrosive properties. These materials are also compared with the Al6061 substrate without any kind of coating. The study is carried out with surface characterization of each one of the samples with or without coating using a series of complementary techniques, such as chemical and electrochemical techniques (linear-sweep voltammetry, cyclic voltammetry, determination of the polarization resistance) and physical techniques (SEM microscopy, determination of micro-hardness). The correlation of variables is carried out later as a function of the phosphorous content of the test samples. The structures obtained from the coatings are amorphous. They have no pores or faults and have high hardness values. The electrochemical study proves that the anticorrosive protection capacity of the Ni-P alloy increases along with the

  4. Influence of Microstructure and Composition Changes on Mechanical Characteristics of Aluminium Alloy After Heating and Cooling Treatment

    International Nuclear Information System (INIS)

    Sigit; Nuraini, E; Martoyo

    1998-01-01

    Influences of microstructure and chemical composition changes on mechanical characteristics of AIMg2 which were heated at 85-500 0 C and cooled with sands, water or air have been studied. Microstructure observation was carried out using optical microscope, while chemical composition determination by atomic absorption spectrophotometry (AAS). AIMg2 which has been heated at the relatively low temperature i. e, 200 0 C during 6 hours and cooled using sands showed a small change microstructure, but those will be clearly observed on the treatment at 300 0 C. The microstructure change is in agreement with the change of mechanical characteristic, I. e., the decreasing of tensile strength and hardness and increasing of elongation. After the temperature of treatment is higher than 300 0 C, the decreasing of the tensile strength was relatively constant, while the hardness increased. The microstructure of AIMg2 resulted from the heat treatment at temperature of 500 0 C was different with that of 300 0 C. Heat treatment at 500 0 C following by cooling in the sands, water or air respectively gave similar microstructure. Those also caused the change of alloying element content which was in agreement with decreasing of mechanical characteristics

  5. Experimental Investigations of the In-Die Quenching Efficiency and Die Surface Temperature of Hot Stamping Aluminium Alloys

    Directory of Open Access Journals (Sweden)

    Kailun Zheng

    2018-04-01

    Full Text Available The in-die quenching is a key stage in the hot stamping volume production chain which determines the post-formed strength of lightweight alloy components, tool life, and hot stamping productivity. In this paper, the performance of in-die quenching, reflected by the quenching efficiency (the time of work-piece held within stamping dies and die surface temperature during the simulated hot stamping process of AA6082, was experimentally and analytically investigated. A range of in-die quenching experiments were performed for different initial work-piece and die temperatures, quenching pressures, work-piece thickness, and die clearances, under hot stamping conditions. In addition, a one-dimensional (1D closed-form heat transfer model was used to calculate the die surface temperature evolution that is difficult to obtain during practical manufacture situations. The results have shown that the in-die quenching efficiency can be significantly increased by decreasing the initial work-piece and die temperatures. Die clearances are required to be designed precisely to obtain sufficiently high quenching rates and satisfying post-formed strength for hot-stamped panel components. This study systematically considered an extensive variety of influencing factors on the in-die quenching performance, which can provide practical guides for stamping tool designers and manufacture systems for hot-stamping volume production.

  6. Effects of as-cast and wrought Cobalt-Chrome-Molybdenum and Titanium-Aluminium-Vanadium alloys on cytokine gene expression and protein secretion in J774A.1 macrophages

    DEFF Research Database (Denmark)

    Jakobsen, Stig Storgaard; Larsen, Agnete; Stoltenberg, Meredin

    2007-01-01

    the cell viability. Surface properties of the discs were characterised with a profilometer and with energy dispersive X-ray spectroscopy. We here report, for the first time, that the prosthetic material surface (non-phagocytable) of as-cast high carbon CoCrMo reduces the pro-inflammatory cytokine IL-6......Insertion of metal implants is associated with a possible change in the delicate balance between pro- and anti-inflammatory proteins, probably leading to an unfavourable predominantly pro-inflammatory milieu. The most likely cause is an inappropriate activation of macrophages in close relation...... to the metal implant and wear-products. The aim of the present study was to compare surfaces of as-cast and wrought Cobalt-Chrome-Molybdenum (CoCrMo) alloys and Titanium-Aluminium-Vanadium (TiAlV) alloy when incubated with mouse macrophage J774A.1 cell cultures. Changes in pro- and anti-inflammatory cytokines...

  7. Relation between feeding mechanisms and solidification mode in 380 aluminium alloy with different iron contents; Relacion entre los mecanismos de alimentacion y el modo de solidificacion en una aleacion de aluminio 380 con distintos contenidos de hierro

    Energy Technology Data Exchange (ETDEWEB)

    Tovio, D. O.; Gonzalez, A.C.; Mugica, G. W.; Cuyas, J. C.

    2003-07-01

    In the present work the effect of iron (0.15, 0.42 and 0.86%) content in feeding mechanisms for 380 aluminium alloy has been studied. The feeding capacity has been evaluated by a device that produces a barrier removable to allowing the movement of the inter dendritic liquid. The results show the flow of different quantity of liquid, it depends of the temperature of operating the device and of the iron content. For minimum and maximum iron content, the inter dendritic and bursts feeding mechanisms are fundamentally involved, for 0.42% of iron the feeding mechanisms was the inter dendritic. The authors establish this behavior by the solidification mode of alloy, which promotes the presence of particles of Si or plates of b-Al{sub 3}FeDi phase, in the inter dendritic channels and produce the different feeding mechanisms. (Author) 15 refs.

  8. Hydrogen diffusion into fatigue cracks of aluminium alloy 6013 in a corrosive environment; Wasserstoffeinlagerung an Ermuedungsrissen der Aluminiumlegierung 6013 unter korrosiver Umgebung

    Energy Technology Data Exchange (ETDEWEB)

    Lenk, Christian Alexander

    2009-08-13

    The author attempted a time-resolved detection of raised hydrogen concentrations in the plastic deformation region of fatigue cracks in an aluminium test piece deformed by cyclic stress in a corrosive environment. Mechanical material parameters like the crack propagation velocity under cyclic stress change dramatically in a corrosive environment. This is assumed to be caused by hydrogen diffusion, but so far there is no method that reliably measures additional hydrogen from the corrosive environment. For this reason, a special analytical configuration was set up which makes use of the thermal desorption method. First, chips with a thickness of about 20 micrometers are sawed out of the test specimen in high-vacuum conditions. The chips fall into a hot melting vessel in a UHV chamber, where the hydrogen contained in the chips is released. The resulting pressure increase is recorded by a mass spectrometer. A hydrogen profile of the test specimen is obtained by assigning the chip position to the signal. For the corrosive medium in which the test specimen is immersed during crack initiation, i.e. NaCl solution, heavy water was used. This makes it possible to distinguish between the hydrogen contained in a piece of technical aluminium alloy (AA6013) and the deuterium diffusing in from the corrosive fluid. The deuterium is found exclusively in the test piece volume in the strongly plastically deformed region surrounding the fatigue crack. (orig.) [German] Das Ziel der vorliegenden Arbeit besteht im ortsaufgeloesten Nachweis einer erhoehten Wasserstoffkonzentration im plastisch deformierten Bereich von Ermuedungsrissen einer unter korrosiver Umgebung zyklisch verformten Aluminiumprobe. Mechanische Materialparameter wie z.B. die Rissausbreitungsgeschwindigkeit unter zyklischer Belastung aendern sich drastisch in korrosiver Umgebung. Als Ursache fuer dieses Verhalten wird eine Eindiffusion von Wasserstoff vermutet, jedoch gibt es bisher keine Messung die den zusaetzlichen

  9. Investigation of the aluminium-aluminium oxide reversible transformation as observed by hot stage electron microscopy.

    Science.gov (United States)

    Grove, C. A.; Judd, G.; Ansell, G. S.

    1972-01-01

    Thin foils of high purity aluminium and an Al-Al2O3 SAP type of alloy were oxidised in a specially designed hot stage specimen chamber in an electron microscope. Below 450 C, amorphous aluminium oxide formed on the foil surface and was first detectable at foil edges, holes, and pits. Islands of aluminium then nucleated in this amorphous oxide. The aluminium islands displayed either a lateral growth with eventual coalescence with other islands, or a reoxidation process which caused the islands to disappear. The aluminium island formation was determined to be related to the presence of the electron beam. A mechanism based upon electron charging due to the electron beam was proposed to explain the nucleation, growth, coalescence, disappearance, and geometry of the aluminium islands.

  10. Effect of Duration on Ti Grain Refinement of A356 and Melt Quality

    Science.gov (United States)

    Gürsoy, Özen; Erzi, Eray; Yüksel, Çağlar; Dispinar, Derya

    Grain refinement of aluminium alloys increases fluidity and feedability; and thus higher mechanical properties and decreased porosity is achieved. Typically, various ratios of Ti-B is used as grain refiner. It is well known that due to the sedimentation, the effectiveness of the grain refinement decreases which is called the fading effect. In this work, this effect has been investigated by means of melt quality. Two different melting temperatures were selected (725 and 750C) and samples were cast into die and sand mould. After the addition of grain refiners, samples were collected at 10 minutes of interval. Metallographic examinations were carried out where microstructural change and porosity distribution were investigated. The results were correlated with bifilm index (i.e. melt quality).

  11. Industrial heat treatment of R-HPDC A356 automotive brake callipers

    CSIR Research Space (South Africa)

    Chauke, L

    2012-10-01

    Full Text Available Heat treatment of rheo-high pressure die cast (R-HPDC) A356 brake callipers has produced good mechanical properties on the laboratory scale. An industrial heat treatment is required to evaluate the applicability and conformance of the R-HPDC A356...

  12. Industrial heat treatment of R-HPDC A356 automotive brake callipers [Conference paper

    CSIR Research Space (South Africa)

    Chauke, L

    2012-10-01

    Full Text Available Heat treatment of rheo-high pressure die cast (R-HPDC) A356 brake callipers has produced good mechanical properties on the laboratory scale. An industrial heat treatment is required to evaluate the applicability and conformance of the R-HPDC A356...

  13. Effects of Process Conditions on the Mechanical Behavior of Aluminium Wrought Alloy EN AW-2219 (AlCu6Mn Additively Manufactured by Laser Beam Melting in Powder Bed

    Directory of Open Access Journals (Sweden)

    Michael Cornelius Hermann Karg

    2017-01-01

    Full Text Available Additive manufacturing is especially suitable for complex-shaped 3D parts with integrated and optimized functionality realized by filigree geometries. Such designs benefit from low safety factors in mechanical layout. This demands ductile materials that reduce stress peaks by predictable plastic deformation instead of failure. Al–Cu wrought alloys are established materials meeting this requirement. Additionally, they provide high specific strengths. As the designation “Wrought Alloys” implies, they are intended for manufacturing by hot or cold working. When cast or welded, they are prone to solidification cracks. Al–Si fillers can alleviate this, but impair ductility. Being closely related to welding, Laser Beam Melting in Powder Bed (LBM of Al–Cu wrought alloys like EN AW-2219 can be considered challenging. In LBM of aluminium alloys, only easily-weldable Al–Si casting alloys have succeeded commercially today. This article discusses the influences of boundary conditions during LBM of EN AW-2219 on sample porosity and tensile test results, supported by metallographic microsections and fractography. Load direction was varied relative to LBM build-up direction. T6 heat treatment was applied to half of the samples. Pronounced anisotropy was observed. Remarkably, elongation at break of T6 specimens loaded along the build-up direction exceeded the values from literature for conventionally manufactured EN AW-2219 by a factor of two.

  14. Influence of stirring speed on SiC particles distribution in A356 liquid

    Directory of Open Access Journals (Sweden)

    Yao Shasha

    2012-05-01

    Full Text Available A straight-blade mechanical stirrer was designed to stir A356-3.5vol%SiCp liquid in a cylindrical crucible with the capability of systematically investigating the influence of rotating speed of stirrer on the distribution of SiC particles in A356 liquid. The experimental results show that the vertical distribution of SiC particles in A356 liquid can be uniform when the rotating speed of stirrer is 200 rpm, but the radial distribution of SiC particles in A356 liquid is always nonhomogeneous regardless of the rotating speed of stirrer. The radial centrifugalization ratio of SiC particles in A356 liquid between the center and the periphery of crucible increases with the rotating speed of stirrer. The results were explained in the light of SiC particles motion subject to a combination of stirring and centrifugal effect.

  15. Influence of energy input in friction stir welding on structure evolution and mechanical behaviour of precipitation-hardening in aluminium alloys (AA2024-T351, AA6013-T6 and Al-Mg-Sc)

    Energy Technology Data Exchange (ETDEWEB)

    Weis Olea, Cesar Afonso [GKSS-Forschungszentrum Geesthacht GmbH (Germany). Inst. fuer Werkstofforschung

    2008-12-04

    Aluminium alloys AA2024 T351, AA6013 T6 and the recently developed Al-Mg-Sc for aircraft industry applications, which are usually considered difficult to weld by conventional fusion welding processes, demonstrate outstanding performance when joined by friction stir welding (FSW). The main feature of the process is to produce solid-state welds, where the maximum temperatures attained during the process are about 80 % that of the melting temperature of the base material. The process generates substantial plastic deformation, due to the solid-state stirring, and consequently creates a high dislocation density, which is a precursor to dynamic recrystallization, a metallurgical feature that characterizes the stir zone (weld centre). A relevant aspect considered, regarding precipitation-hardening aluminium alloys, is the deterioration of the mechanical properties in the weld zones, which are fundamentally attributed to changes in the characteristics of strengthening precipitates. Among the strengthening mechanisms acting in these aluminium alloys, the most important is basically dependent on the morphology, size and population of the precipitates. The thermal cycle and deformation generated during the FSW process alter the precipitation characteristics previously present in the base material. FSW input energy regulates the magnitude of the thermal cycle and the intensity of deformation taking place during the process, and it can be controlled by the welding parameters, affecting the precipitates evolution and consequently the mechanical properties of the joint. Nevertheless, there remains a lack of knowledge about the substructural evolution of these alloys during FSW, and its correlation with weld energy input and their respective mechanical properties, particularly for the Al-Mg-Sc alloy. The main objective of this work is to explain the micro and substructural evolution (emphasizing precipitates evolution) of AA2024- T351, AA6013-T6 and Al-Mg-Sc alloys in similar

  16. Enhanced corrosion protection by microstructural control of aluminium brazing sheet

    NARCIS (Netherlands)

    Norouzi Afshar, F.

    2013-01-01

    Aluminium brazing sheet is a sandwich material made out of two aluminium alloys (AA4xxx/AA3xxx) and is widely used in automotive heat exchangers. One of the main performance criteria for heat exchanger units is the lifetime of the product. The lifetime of the heat exchanger units is determined by

  17. Laser deposition of (Cu + Mo) alloying reinforcements on AA1200 substrate for corrosion improvement

    CSIR Research Space (South Africa)

    Popoola, API

    2011-10-01

    Full Text Available Poor corrosion performance of aluminium alloys in marine environment has been a subject of intensive research recently. Aluminium substrate was alloyed with a combination of two metallic powders (Cu + Mo) using an Nd: YAG solid state laser...

  18. The Hamlet dilemma for aluminium cans in the circular economy: to be or not to be in a closed loop?

    OpenAIRE

    Niero, Monia; Hoffmeyer, Simon B.; Langen, Håkon; Olsen, Stig Irving

    2015-01-01

    In the context of circular economy the focus is not only on recycling from a quantitative point of view, but also on improving the quality of materials. We considered the case of aluminium cans, and quantified the influence of alloying elements on the overall environmental performances of aluminium can recycling. We performed a Life Cycle Assessment (LCA) comparing different sources of aluminium: primary aluminium and mixed scraps, Used Beverage Can (UBC) scrap, mixed aluminium packaging scra...

  19. Crack growth behaviour of the aluminium alloy AlMg4.5Mn at proportional and non-proportional fatigue loading; Risswachstumsverhalten der Aluminiumlegierung AlMg4.5Mn unter proportionaler und nichtproportionaler Schwingbelastung

    Energy Technology Data Exchange (ETDEWEB)

    Zerres, Patrick; Vormwald, Michael [Technische Univ. Darmstadt (Germany). Fachgebiet Werkstoffmechanik; Bruening, Jutta [TUEV NORD SysTec, Hamburg (Germany). Gruppe Mechanische Analyse/Bruchmechanik

    2011-07-01

    In the present investigations a series of fatigue crack growth experiments has been conducted using thin-walled, hollow cylinders with a notch. The cylinders are made of Aluminium alloy AlMg4.5Mn. Cyclic tension- compression, torsion and proportional as well as non-proportional combinations of both loadings have been applied. For these experiments the crack growth lives, the crack growth curves and the crack paths have been identified. Depending on the loading type initiation of two to four cracks at different positions of the notch has been observed. Using the nominal stress as a load parameter, only very small differences concerning the crack growth lives could be determined. Using the local elastic notch stress as a load parameter, significant differences between the five loading types could be determined. (orig.)

  20. IEC 61267: Feasibility of type 1100 aluminium and a copper/aluminium combination for RQA beam qualities.

    Science.gov (United States)

    Leong, David L; Rainford, Louise; Zhao, Wei; Brennan, Patrick C

    2016-01-01

    In the course of performance acceptance testing, benchmarking or quality control of X-ray imaging systems, it is sometimes necessary to harden the X-ray beam spectrum. IEC 61267 specifies materials and methods to accomplish beam hardening and, unfortunately, requires the use of 99.9% pure aluminium (Alloy 1190) for the RQA beam quality, which is expensive and difficult to obtain. Less expensive and more readily available filters, such as Alloy 1100 (99.0% pure) aluminium and copper/aluminium combinations, have been used clinically to produce RQA series without rigorous scientific investigation to support their use. In this paper, simulation and experimental methods are developed to determine the differences in beam quality using Alloy 1190 and Alloy 1100. Additional simulation investigated copper/aluminium combinations to produce RQA5 and outputs from this simulation are verified with laboratory tests using different filter samples. The results of the study demonstrate that although Alloy 1100 produces a harder beam spectrum compared to Alloy 1190, it is a reasonable substitute. A combination filter of 0.5 mm copper and 2 mm aluminium produced a spectrum closer to that of Alloy 1190 than Alloy 1100 with the added benefits of lower exposures and lower batch variability. Copyright © 2015 Associazione Italiana di Fisica Medica. Published by Elsevier Ltd. All rights reserved.