WorldWideScience
1

Development of experimental verification techniques for non-linear deformation and fracture on the nanometer scale.  

Energy Technology Data Exchange (ETDEWEB)

This work covers three distinct aspects of deformation and fracture during indentations. In particular, we develop an approach to verification of nanoindentation induced film fracture in hard film/soft substrate systems; we examine the ability to perform these experiments in harsh environments; we investigate the methods by which the resulting deformation from indentation can be quantified and correlated to computational simulations, and we examine the onset of plasticity during indentation testing. First, nanoindentation was utilized to induce fracture of brittle thin oxide films on compliant substrates. During the indentation, a load is applied and the penetration depth is continuously measured. A sudden discontinuity, indicative of film fracture, was observed upon the loading portion of the load-depth curve. The mechanical properties of thermally grown oxide films on various substrates were ...

2005-11-01

2

Internal strain and texture evolution during deformation twinning in magnesium  

Energy Technology Data Exchange (ETDEWEB)

The development of a twinned microstructure in hexagonal close-packed rolled magnesium compressed in the in-plane direction has been monitored in situ with neutron diffraction. The continuous conversion of the parent to daughter microstructure is tracked through the variation of diffraction peak intensities corresponding to each. Approximately 80% of the parent microstructure twins by 8% compression. Elastic lattice strain measurements indicate that the stress in the newly formed twins (daughters) is relaxed relative to the stress field in the surrounding matrix. However, since the daughters are in a plastically 'hard' deformation orientation, they quickly accumulate elastic strain as surrounding grains deform plastically. Polycrystal modeling of the deformation process provides insight about the crystallographic ...

2005-06-15

3

Effect of microstructure and deformation conditions on hot plasticity of Ti-6Al-5Mo-5V-1Cr-1Fe titanium alloy  

International Nuclear Information System (INIS)

Results of investigation on the effect of microstructure and deformation conditions (temperature and strain rate) on flow stress and critical strain in two phase #alpha# + #beta# titanium alloy Ti-6Al-5Mo-5V-1Cr-1Fe is presented in the paper. The alloy is deformed or torsional plastometer at temperature range 1073-1173 K and at the strain rate #epsilon# = 0.04-4.0 s"-"1. Sequential deformation at 1173 K at the strain rate of 0.4 s"-"1 was also performed with holding times in the range 1-100 s. The fraction of dynamically and metadynamically recrystallized #beta# phase was determined on the basis of results of sequential deformation test. Microstructure was examined using LM and TEM techniques. (author)

2004-06-20

4

Mechanical deformation and tensile super-elastic behaviors of a Ti-Mo based shape memory alloy  

Science.gov (United States)

Ni-free shape memory alloys are promising functional materials for medical applications. A newly developed Ti-Mo based shape memory alloy shows superelasticity after thermomechanical treatment. However, the microstructure evolution and precipitation during thermomechanical processes are still not well understood. In the present paper, compressive deformation behavior at a series of temperatures of 298K - 973K and tensile deformation behavior of the alloy after aged at 573K - 973K have been investigated systematically. It is found that the compressive yield stress and ultimate compressive strength change with the deformation temperature. The ultimate tensile strength and yield stress of aged specimens also change with the aging temperature following a non-linear relationship. Microstructures of aged specimens as well as effects of lattice softening and aging-induced precipitates on ...

2011-03-01

5

Hydrogen effect or texture and deformation mechanism in #beta#-titanium alloy cold rolling  

International Nuclear Information System (INIS)

The relationships of hydrogen alloyed #beta#-titanium alloy deformation behaviour to its microstructure and texture are investigated. It is shown that plasticity increases and strain induced texture changes at low hydrogen contents (0.1-0.2 mass %). Possible mechanisms responsible for specific features of #beta#-Ti alloy deformation are discussed. The study is made using alloy VT35 doped with hydrogen

1999-09-01

6

Microstructure characterization and tensile properties of b phase containing TiAl pancake  

British Library Electronic Table of Contents (United Kingdom)

The microstructure and tensile properties of Ti-44Al-6V-3Nb-0.3Y (at.%) alloy after canned forging were investigated. SEM results showed that the TiAl pancake exhibits inhomogeneous microstructure, which can be ascribed to the temperature drop and friction between billet and outer pack during forging, as well as the intrinsic anisotropy of lamellar colony. By means of TEM observation and EBSD analysis, the microstructure in the dominant area of the pancake was further characterized. This deformation area consists of 87.7% content of g grains plus some refined lamellar colonies and the rest of B2 grains. The grain size ranges between 1mm and 8.5mm. High-angle boundaries dominate the deformation microstructure, several substructures and twins are observed as well. Additionally, current forge...

2011-01-01

7

Influence of rolling conditions on the microstructure and mechanical properties of magnesium sheet AZ31  

Energy Technology Data Exchange (ETDEWEB)

Two aspects of the deformation behavior of magnesium sheets are the subject of this paper. First it will give a mechanical characterization of a commercial magnesium with a focus on the anisotropy and the possible microstructural causes of this behavior. The rolling process will be part of the second aspect. The aim is to show the influence of the parameters on the microstructure and texture and how this could affect the anisotropy in the rolled sheets. (Abstract Copyright [2003], Wiley Periodicals, Inc.)

2003-12-01

8

Strain softening and hardening effects in Ti-6Al-4V during high temperature deformation  

International Nuclear Information System (INIS)

Effect of strain and temperature on high temperature deformation properties of an alpha + beta titanium alloy Ti-6Al-4V has been investigated in the temperature range 800 to 910 deg. C by using the method of cross head speed cycling. On the basis of flow stress strain rate-strain rate sensitivity data and microstructural studies of the undeformed and deformed regions of tensile test pieces, both strain introduced hardening and softening effects were observed during the course of deformation which could be associated with grain coarsening and refining respectively. (author)

9

Modeling grain size during hot deformation of IN 718  

Energy Technology Data Exchange (ETDEWEB)

Aerospace gas turbine disks operate in an environment of relatively high stresses caused by centrifugal forces and elevated temperatures. These severe conditions necessitate the need for materials with high temperature strength and good low cycle fatigue resistance. One class of alloys used for this task is the nickel base superalloys, out of which, IN 718 is the most widely used in the aerospace industry. The properties of IN 718 are attributed to the combined effects of the chemistry, heat treatment, and microstructure. The chemistry is tailored not only for solid solution strengthening but also for precipitation hardening developed during heat treatment, which combined with a fine grained microstructure lead to excellent mechanical properties such as low cycle fatigue resistance and elevated temperature strength. The properties of a gas turbine disk are sensitive to the microstructure, in particular the grain size, which ...

1999-12-17

10

Thin film adhesion by nanoindentation-induced superlayers. Final report  

Energy Technology Data Exchange (ETDEWEB)

This work has analyzed the key variables of indentation tip radius, contact radius, delamination radius, residual stress and superlayer/film/interlayer properties on nanoindentation measurements of adhesion. The goal to connect practical works of adhesion for very thin films to true works of adhesion has been achieved. A review of this work titled ''Interfacial toughness measurements of thin metal films,'' which has been submitted to Acta Materialia, is included.

2001-06-01

11

Effect of mean stress (stress ratio) and aging on fatigue-crack growth in a metastable beta titanium alloy, Ti-10V-2Fe-3Al  

International Nuclear Information System (INIS)

The effect of mean stress, or the stress ratio (R), on the fatigue-crack growth (FCG) behavior of #alpha#-aged and #omega#-aged microstructures of the beta titanium alloy Ti-10V-2Fe-3Al was investigated. While the mean stress had a negligible effect on the FCG behavior of the #alpha#-aged microstructure, a strong effect was observed in the #omega#-aged microstructure. In particular, the values of the threshold stress-intensity range (#DELTA#K_t_h) exhibited a strong dependence on R in the #omega#-aged microstructure, while this dependence was weak in the #alpha#-aged microstructure. These effects seem to arise primarily from fracture-surface roughness-induced crack closure. The crack closure levels for the #alpha#-aged microstructure were found to be very low compared to those for the #omega#-aged microstructure. Transmission electron ...

2000-03-01

12

Microstructures and mechanical properties of pure copper deformed severely by equal-channel angular pressing and high pressure torsion  

International Nuclear Information System (INIS)

Pure Cu of 99.98 wt.% purity has been processed at room temperature by diverse techniques of severe plastic deformation, namely equal-channel angular pressing (ECAP), high pressure torsion (HPT) and a combination of both in order to find out the evolution on the microstructural homogeneity for each of the processes and their combination. Starting with a grain size of #approx#60 #mu#m, severe plastic deformation has been introduced to the material while maintaining the sample dimensions unchanged through the processes of ECAP and HPT. A significant decrease in grain size was observed by transmission electronic microscopy (TEM). Microtensile and microhardness tests were carried out on the deformed material in the three processing conditions. A significant improvement of the tensile strength was promoted with admissible penalization on ductility.

2008-03-25

13

Relationship between microstructural evolution and low cycle fatigue behaviour at 550/sup 0/C of alloy 800 grade 2  

Energy Technology Data Exchange (ETDEWEB)

In this study, deformation modes and precipitations have been characterized in test pieces made of alloy 800, grade 2 hyper-hardened state and age-conditioned for 3000 h at 550/sup 0/C, used for steam generator tubes of the Super Phenix Reactor, after continuous fatigue and fatigue-relaxation tests in the oligocyclic range. This microstructural study has provided an interpretation of the fatigue behaviour of the material.

1989-01-01

14

Superplastic deformation of nitrogen-rich Ca-#alpha#-sialon ceramics  

International Nuclear Information System (INIS)

Nitrogen-rich Ca-#alpha#-sialon ceramics, prepared with CaH_2 as one of the starting powders, were compressively deformed in spark plasma sintering equipment. Compared with the oxygen-rich Ca-#alpha#-sialons, increasing onset deformation temperatures (about 150 K higher) were observed for nitrogen-rich Ca-#alpha#-sialons deformed at a rate of 2 x 10"-"3 s"-"1. High hardness (H_V_1_0 = 18-20 GPa) and toughness (K_I_C = 4-7 MPa m"1"/"2) were maintained after the deformation. Anisotropic grain growth was found to take place during deformation, resulting in anisotropic microstructures, containing coarse and elongated grains. The observed differences in deformation behaviour and properties between nitrogen-rich and oxygen-rich Ca-#alpha#-sialons are, as indicated by transmission electron microscopy and electron energy loss spectroscopy analysis, ...

2008-02-25

15

Microstructure of a nickel-base ODS powder after mechanical alloying. Mikrostruktur eines ODS-Pulvers auf Nickelbasis nach dem mechanischen Legieren  

Energy Technology Data Exchange (ETDEWEB)

Mechanical alloying is an important pre-requisite for the manufacturing of heat resistant oxide-dispersion-strengthened superalloys. Though the microstructure of these materials after hot extrusion and recrystallization treatment is well documented, little is known about the microstructural evolution during ball-milling. A method was tested to prepare electron transparent foils and extraction replica from powder particles for TEM investigations. The microstructure was found to consist of a Ni-Cr-Al solid solution in which submicron particles of refractory metals were embedded. The extremely fine grainize of about 50 nm is the consequence of severe plastic deformation. Yttria particles could not be detected in the powder after ball milling, but after a heat treatment at 1000 C the well-known fine dispersion of oxide particles was evident. (orig.)

1993-02-01

16

Microstructural evolution during hot rolling of an AZ31 Mg alloy  

Energy Technology Data Exchange (ETDEWEB)

The microstructural evolution of a AZ31 Mg alloy during hot rolling has been investigated using optical microscopy and texture (macro and micro) analysis as the main characterization tools. In particular, the differences between the microstructure obtained by unidirectional rolling (UR) and cross rolling (CR) are studied. Significant twinning activity is observed in both cases. Additionally, after cross rolling, a rather heterogeneous microstructure develops, with scattered regions populated by very fine grains. The strong basal fiber texture of the as-received material remains present after both hot rolling schemes. The impossibility to obtain accurate EBSD measurements within the twinned regions suggests that significant localized deformation takes place in those areas. Thus, these regions become preferential sites for the onset of recrystallization due to the increase in the local strain energy. ...

2003-07-01

17

Radiation hardening effects on localized deformation and stress corrosion cracking of stainless steels  

International Nuclear Information System (INIS)

Radiation hardening in austenitic stainless steels is shown to modify deformation characteristics and correlate well with an increased susceptibility to intergranular stress corrosion cracking (IGSCC). Available data on neutron-irradiated materials have been analyzed and correlations developed between fluence, yield strength and cracking susceptibility in high-temperature water environments. Large heat-to-heat differences in the critical fluence (0.2 to 2.5 x10"2"1 n/cm"2) for IGSCC are documented. In many cases, this variability is consistent with yield strength differences among irradiated materials. IGSCC correlates better to yield strength than to fluence for most heats suggesting a possible role of radiation-induced hardening and microstructure on cracking. Microstructural evolution during proton and heavy-ion irradiation has been characterized in low-carbon 304SSs. Hardening results from a dispersion of dislocation ...

1993-08-01

18

Mechanical property of superplastic-deformed ceramics by micro-indentation method  

Energy Technology Data Exchange (ETDEWEB)

A neutron irradiation test on superplastic ceramic materials at high temperature has been proposed as an innovative basic research on high-temperature engineering using the High Temperature Engineering Test Reactor (HTTR). We investigated mechanical properties, such as the hardness and Young's modulus, of ceramic specimens after superplastic deformation. The tested material was 3Y-TZP (3mol% Yttria stabilized Tetragonal Zirconia Polycrystal) which is one of the representative superplastic ceramics. The properties were measured by a microindentation method. We also studied the relationship between crystal microstructures and the mechanical properties of deformed 3Y-TZP by scanning electron microscope (SEM). The indentation test showed that the mechanical properties of the specimens were reduced to about 1/2 by 30% deformation and to about 1/4 by 150% deformation. The SEM ...

2001-03-01

19

Recrystallization in AZ31 magnesium alloy during hot deformation  

Energy Technology Data Exchange (ETDEWEB)

In this study, isothermal torsion tests were carried out on magnesium AZ31B alloy under constant strain rate conditions, in the range of 250 to 400 C at 0.01, 0.1, and 1.0 s{sup -1}. Alloy flow stress dependence on strain rate and temperature can be described by a power law with activation energy of 130 kJ/mol. Microstructural examination of hot deformed samples shows very fine recrystallized grains decorating grain boundaries of larger gains in the form of a necklace. These fine grains are produced by dynamic recrystallization at the grain boundaries of original grains. Microstructure evolution, based on samples quenched at different strain levels, indicates that increasing deformation strain has little effect on recrystallized grain size but widens the recrystallized region, with full recrystallization achieved at a certain high strain level. Recrystallized grain size increases with increasing ...

2005-07-01

20

Microstructure evolution and fracture behavior in superplastic deformation of hot-rolled AZ31 Mg alloy sheet  

Energy Technology Data Exchange (ETDEWEB)

Fine-grained AZ31 magnesium alloy sheets were prepared through hot rolling process. The superplastic properties of hot-rolled AZ31 Mg alloy was examined by uniaxial tensile tests at a temperature range 250{proportional_to}450 C and strain rate range 0.7 x 10{sup -3}{proportional_to}1.4 x 10{sup -1} s{sup -1}. Optical and scanning electronic microscope (SEM) were used to observe the microstructure evolution and fracture behavior in superplastic deformation of AZ31 Mg alloy and the values of deformation activation energy at various temperatures were calculated. It is demonstrated that, the hot-rolled AZ31 alloy begins to exhibit superplasticity from 300 C and a maximum elongation of 362.5% is obtained at 400 C and 0.7 x 10{sup -3} s{sup -1}. In the temperature range 300{proportional_to}400 C, the dominant superplastic deformation mechanism is grain boundary sliding (GBS) controlled by grain boundary ...

2005-07-01

21

Microstructural development inside the stress induced martensite variant in a Ti-Ni-Nb shape memory alloy  

Energy Technology Data Exchange (ETDEWEB)

The microstructural development inside the stress induced martensite (SIM) variants in Ti-Ni-Nb alloy with various degrees of deformation have been revealed by electron microscopic observations. The orientation relationship between the SIM and the parent phase has been found: [1{bar 1}0]{sub M}{parallel}[11{bar 1}]{sub B2}, (001){sub M} 5{degree} away from (101){sub B2}. The lattice invariant shear of the SIM variants at the slightly deformed stage is dominantly (11{bar 1}) Type I twin. Besides the ordinary slip, the adjustment and development of the internal secondary twinning from (11{bar 1}) Type I twin to {l_angle}011{r_angle} Type II/ or (011) Type I twin, (001)compound twin and (111) Type I twin happen concurrently or in combination inside the SIM variants with the further deformation. The corresponding deformation mechanisms include stress induced reorientation of SIM ...

2000-04-03

22

Texture development of AZ31 magnesium alloy during ECAE processing  

Energy Technology Data Exchange (ETDEWEB)

Mg-3%Al-1%Zn (AZ31) alloy was subjected to ECAE processing at 523 and 573 K. Microstructure observation and texture analysis were carried out using optical microscope and SEM-EBSD technique in order to investigate the process of microstructural changes including texture development during ECAE processing. Grain refinement during ECAE processing is enhanced by dynamic continuous recrystallization. The texture of the ECAE-processed AZ31 alloy specimens change with ECAE processing temperature, and the textural changes relate to deformation mechanisms that change with ECAE processing temperature. (orig.)

2003-07-01

23

Stress-induced martensitic transformation of metastable #beta#-titanium alloy  

International Nuclear Information System (INIS)

The constituent phases and associated deformed microstructure of the quenched Ti-xNb-(0.5-1.5) at.% Si alloy consisting of non-cytotoxicity elements, where x = 24-30 at.%, were investigated to provide pseudoelasticity for biomedical and sensor applications. Optical microscopy revealed that stress-induced martensitic transformation takes place during the deformation in the present alloys. It is confirmed from the X-ray diffraction results of the deformed specimens that the crystal structure of the stress-induced martensite phase is the orthorhombic so-called #alpha#'' structure. Within the alloys having #beta#(bcc) phase studied Nb-poor region appeared to exhibit a dominant behavior for stress-induced martensitic transformation than Nb-rich region. This result suggests that metastable #beta# phase is superior to stable #beta# phase for the occurrence of stress-induced martensitic transformation in the ...

2007-03-25

24

Microstructures of friction welded joints of AZ31 to AM60 magnesium alloys  

Energy Technology Data Exchange (ETDEWEB)

AZ31 magnesium alloy was friction-welded to AM60 and the microstructures and the friction welding process were studied. The microstructures changed near the weld interface. The AZ31 was refined to a grain size of several {mu}m near the weld interface. The nucleation occurred in the shear bands that were introduced during the welding process. On the other hand, the eutectic structure was deformed and the lamellar structure which was composed of {alpha}-Mg and Mg{sub 17}Al{sub 12} was formed near the weld interface in AM60 alloy. In the friction process, the adhesion and peel off occurred alternately between AZ31 and AM60. Eventually, bonding was completed during upset process. (orig.)

2003-07-01

25

Microstructure and mechanical properties of magnesium alloy AZ31B laser beam welds  

International Nuclear Information System (INIS)

Microstructure and properties of a Mg AZ31B laser beam weld without filler are studied using electron microscopy, X-ray diffraction and mechanical tests. The microstructure of the weld is characterized by a narrow heat affected zone, columnar grains and precipitate coarsening in the fusion zone. Texture in the fusion zone is significantly different from the texture of the base material. The residual stress distribution observed is similar at the top and the bottom of the weld, maximum tensile residual stress values are observed in the fusion zone. Tensile tests reveal differences in the mechanical behavior of the fusion zone and the parent material, which can be related to the differences of texture and the resulting deformation mechanisms.

2008-06-25

26

Microstructural characterization of plasma nitrided austenitic stainless steel  

Energy Technology Data Exchange (ETDEWEB)

The microstructure of the layers produced by plasma nitriding austenitic stainless steel at different treatment temperatures (400 and 500 C) were studied by transmission electron microscopy (TEM) together with X-ray diffraction (XRD) and scanning electron microscopy (SEM). The results show that the microstructures were composed of 'expanded austenite' ({gamma}{sub N}) and {alpha}(ferrite)+CrN following plasma nitriding at lower and higher treatment temperatures, respectively. The former contains stacking faults and deformed twin substructures, while the latter is made up of colonies displaying a lamellar structure. Kurdjumov-Sachs or Nishiyama-Wassermann orientation relationships between the {alpha} and CrN layer were observed. (orig.)

2000-10-23

27

Local thermal property analysis by scanning thermal microscopy of an ultrafine-grained copper surface layer produced by surface mechanical attrition treatment  

International Nuclear Information System (INIS)

Scanning thermal microscopy (SThM) was used to map thermal conductivity images in an ultrafine-grained copper surface layer produced by surface mechanical attrition treatment (SMAT). It is found that the deformed surface layer shows different thermal conductivities that strongly depend on the grain size of the microstructure: the thermal conductivity of the nanostructured surface layer decreases obviously when compared with that of the coarse-grained matrix of the sample. The role of the grain boundaries in thermal conduction is analyzed in correlation with the heat conduction mechanism in pure metal. A theoretical approach, based on this investigation, was used to calculate the heat flow from the probe tip to the sample and then estimate the thermal conductivities at different scanning positions. Experimental results and theoretical calculation demonstrate that SThM can be used as a tool for the thermal property and ...

2006-06-15

28

Microstructural characterization of Ti-6Al-4V metal chips by focused ion beam (FIB) and transmission electron microscopy (TEM)  

Energy Technology Data Exchange (ETDEWEB)

The microstructure of the secondary deformation zone (SDZ) near the cutting surface in metal chips of Ti-6Al-4V formed during machining was investigated using focused ion beam (FIB) specimen preparation and transmission electron microscopy (TEM) imaging. Use of the FIB allowed precise extraction of the specimen across this region to reveal its inhomogeneous microstructure resulting from the non-uniform distribution of strain, strain rate, and temperature generated during the cutting process. Initial imaging from conventional TEM foil preparation revealed microstructures ranging from heavily textured to regions of fine grains. Using FIB preparation, the transverse microstructure could be interpreted as fine grains near the cutting surface which transitioned to coarse grains toward the free surface. At the cutting surface a 10 nm thick recrystallized layer was observed capping a 20 nm ...

2011-01-01

29

Cavitation during hot-torsion testing of Ti-6Al-4V  

Science.gov (United States)

Hot-torsion testing was used to establish the cavitation behavior of a typical alpha/beta titanium alloy, Ti-6Al-4V, with a colony microstructure, during simple-shear deformation. For this purpose, sections of deformed specimens were examined by optical metallography, and by scanning and orientation-imaging microscopy (OIM). It was found that cavity nucleation occurred along prior beta boundaries as well as at triple points; in particular, most cavities nucleated along boundaries perpendicular to the axial direction of the specimen. Extensive growth was observed for cavities surrounded by both hard and soft orientations, with the soft colonies accommodating more of the imposed strain. At high degrees of deformation, dynamic globularization of the colony microstructure adjacent to the cavities was also observed. In addition, the metallographic observations revealed that the cavities ...

2005-12-01

30

Flow behaviour and microstructure of the heat-resistant steels X20CrMoV12.1 and X5NiCrTiAl32.20 (alloy 800)  

Energy Technology Data Exchange (ETDEWEB)

Flow-curve characteristics of the heat-resistant steels X 20 CrMoV 12.1 and alloy 800 (X5NiCrTiAl32.20) were measured by tensile and compression tests at temperatures between room temperature and 800 C and strain rates {epsilon}{<=}10 s{sup -1} in connection with microstructure investigations (dislocation content, carbide precipitation) by TEM and X-ray diffraction analysis (XDA). Modelling the deformation behaviour of the steels in terms of the microstructure development indicates that it cannot be explained in a simple manner. The flow curves {sigma}={sigma}({epsilon}, {epsilon}, T) lie, in general, between those predicted by the Kocks-Mecking-Estrin model and a modified (i.e. two-parameter) Roberts model. Because of the less complicated nature of the deformation process the correspondence of experiment and modelling is more satisfying in the case of the material X 20 CrMoV 12.1. (orig.) 26 refs.

1999-10-01

31

Failure analysis of CO_2 anti-freezing heater at Daya Bay Nuclear Power Station  

International Nuclear Information System (INIS)

In this paper, an investigation was performed on a failure pressure vessel, which was as an anti-freezing heater for General Gas Storage and Distribution (SGZ) system. Evident and serious deformation was observed on the body of the vessel. A metallurgical investigation was conducted to establish the mechanism and cause of deformation of the anti-freezing heater at Daya Bay PWR station in China. The investigation, which was performed on specimens cut from the most serious area deformed of the vessel, included macroscopic examination and microscopy examination. The results of the examinations showed that some lamellar pearlite in the microstructure were already spheroidized. It was confirmed that the vessel was operated at high temperature. Stress analysis for the vessel was conducted. And it was confirmed that, in ideal conditions, the vessel would be deformed at around 420 C. The ...

2002-09-23

32

The radiation hardening and microstructural defect evolution in ion irradiated Fe-Cr alloys with irradiation temperature  

International Nuclear Information System (INIS)

Generally, neutron, ion and electron Irradiations cause a substantial amount of hardening and significantly alter the deformation behavior of metals and alloys at relatively low irradiation temperatures. A radiation hardening is caused by the formation of microstructural defects such as dislocation loops, voids and precipitates under irradiation. Therefore, it is important to have a better knowledge of the irradiation induced microstructural defects under irradiation condition. As a part of the National mid- and long-term atomic energy R and D program, we are dealing with the radiation hardening behavior in Fe-Cr binary alloy. Fe-Cr binary alloy is a base alloy of Ferritic/Martensitic steel(F/M steel) planning to use for the Gen IV nuclear system. In this work, we investigated the radiation hardening and microstructural defect evolution in ion irradiated Fe-Cr alloys with irradiation temperature using ...

2009-05-01

33

The mechanical response of woven Kevlar fabric  

Energy Technology Data Exchange (ETDEWEB)

Woven Kevlar fabrics exhibit a number of beneficial mechanical properties which include strength, flexibility, and relatively low density. The desire to engineer or design Kevlar fabrics for specific applications has stimulated interest in the development of theoretical models which relate their effective mechanical properties to specific aspects of the fabric morphology and microstructure. In this work the author provides a theoretical investigation of the large deformation elastic response of a plane woven Kevlar fabric and compares these theoretical results with experimental data obtained from uniaxially loaded Kevlar fabrics. The theoretical analysis assumes the woven fabric to be a regular network of orthogonal interlaced yarns and the individual yarns are modeled as extensible elastica, thus coupling stretching and bending effects at the outset. This comparison of experiment with theory indicates that the deformation ...

1991-01-01

34

Stress measurements in welds: Problem areas  

Energy Technology Data Exchange (ETDEWEB)

There have been many stress measurements on welds by neutron diffraction over the past 20 years but there are still a number of serious experimental issues that are often not addressed. The primary fact is that the microstructure generally changes across the weld and accompanying this may be a change in the concentration of strengthening elements in solution. This will lead to a shift in lattice spacing which may be incorrectly interpreted as a strain. Secondly, a gradient of plastic deformation near the weld may be expected. Since plastic deformation by application of a stress always generates intergranular (type-2) strains this may lead to a range of intergranular effects superposed on the conventional weld-related strains. The effects are illustrated by neutron diffraction studies of Zr-4, ferritic and austenitic welds where chemistry, intergranular effects and crystallographic texture can all play a role.

2006-11-10

35

Hydrogen effect on cold rolling texture of stable #beta#-titanium alloy  

International Nuclear Information System (INIS)

A study was made into microstructure and texture of cold rolled titanium alloy VT-35 with various hydrogen content aimed to reveal hydrogen influence on the mechanism of cold plastic deformation by rolling. Experiments were carried out using sheets 1.2 mm thick hydrogenated up to hydrogen concentrations from 0.06 to 0.554 mass. %. All specimens constituted a single-phase FCC #beta#-solid solution. It is shown that small hydrogen additions have a plasticizing effect on #beta#-titanium alloys in their cold rolling. The character of texture is dependent on hydrogen concentration and determined by deformation mechanism. 6 refs.; 5 figs.

36

Capturing recrystallization of metals with a multi-scale materials model  

Energy Technology Data Exchange (ETDEWEB)

The final report for a Laboratory Directed Research and Development project entitled, ``Capturing Recrystallization of Metals in a Multiscale Materials Model'' is presented. In this project, deformation and recrystallization processes have been followed experimentally and theoretically in order to incorporate essential mechanisms from the defect (dislocation) and grain size length scales. A nonlinear rotational gradient theory has been developed which enables the incorporation of microstructural parameters. The evolution of these parameters during deformation and recrystallization has been characterized qualitatively and quantitatively, applying various electron optic techniques ranging over several length scales. The theoretical and experimental framework developed is general. It has been exemplified by an application to recrystallization in single crystals and bicrystals of aluminum. The ...

2000-04-01

37

Anomalous activity of nonbasal dislocations in AZ31 Mg alloys at room temperature  

Energy Technology Data Exchange (ETDEWEB)

AZ31 Mg alloy samples were extruded by an equal channel angular extrusion (ECAE) process and subsequently annealed to obtain fine-grained material with a low dislocation density. Tensile tests at room temperature exhibited an apparent steady-state deformation region and a large tensile elongation of 47%. The deformed microstructure at an elongation of 2% indicated a substantial cross-slip to nonbasal planes possibly induced by grain-boundary compatibility effects. The nonbasal segments of dislocations were found to consist of 40% of the total dislocation density at a yield anisotropy factor of only 1.1 instead of an expected value of 100 from single-crystal experiments. (orig.)

2003-07-01

38

Optimizing the microstructure of implant alloy TiAl5Fe2.5 by microprobe analysis  

International Nuclear Information System (INIS)

For optimizing the microstructure of the (#alpha# + #beta#)-titanium alloy TiAl5Fe2.5 the content of the two alloying elements aluminium and iron in the #alpha#- and #beta#-phase was determined by microprobe analysis. The alloys with the composition of the #alpha#- and of the #beta#-phase at 850 degC TiAl6Fe0.5 (#alpha#-phase) and TiAl3.5Fe6.5 (#beta#-phase) were prepared by arc melting and rolling at 850 degC. The mechanical properties of the '#alpha#'- and of the '#beta#'-phase-alloy are compared with the properties of the (#alpha# + #beta#)-alloy TiAl5Fe2.5 in the as rolled and swaged condition and after an additional aging at 550 degC. By this optimizing process it was possible to achieve a tensile strength of Rsub(m) = 1012 N/mm"2, an yield strength of Rsub(p0.2) 954 N/mm"2 and an elongation at fracture A = 14.5% in the TiAl5Fe2.5-alloy, although the degree of hot deformation was small. By a higher degree of ...

1985-05-13

39

Micromechanical modeling of ferrite-pearlite steels using finite element unit cell models  

Energy Technology Data Exchange (ETDEWEB)

An axisymmetric unit cell model based on a regular array of second-phase particles arranged on a BCC lattice is used to study deformation mechanisms of ferrite-pearlite structural steels. Microstructural characteristics of the steels were parameterized by the pearlite volume fraction, the aspect ratio of the pearlite particles, and the neighboring factor, which represents the ratio of interparticle spacing in the longitudinal direction to that in the transverse direction. FE analyses were carried out to investigate the macroscopic and microscopic response of unit cells with morphological features based on idealizations of the microstructures of the actual steels. Tensile properties of each constituent phase were obtained experimentally and used in the analyses. As compared to traditional axisymmetric models, the BCC tell model appears to be able to capture more realistically the behavior of the materials, and it accurately ...

2000-11-01

40

Recrystallization during and following hot working of magnesium alloy AZ31  

Energy Technology Data Exchange (ETDEWEB)

The microstructures of magnesium AZ31 are examined following hot compression testing and annealing. The grain size, fraction dynamically recrystallized and, in a couple of cases, the crystallographic texture are reported. It was found that the progress of dynamic recrystallization is strongly sensitive to processing conditions but that the dynamically recrystallized grain size was less sensitive to stress than in other metals. It was also found that, for structures containing between 80 and 95% dynamic recrystallization, abnormal grain growth occurs during annealing. The crystallographic texture produced is also sensitive to the deformation conditions. (orig.)

2003-07-01

41

Microstructure Characterization of Magnetic-Pulse-Welded AA 6061-T6 by Electron Backscattered Diffraction  

Energy Technology Data Exchange (ETDEWEB)

The grain boundary crystallographic misorientations of magnetic-pulse-welded (MPW) aluminum alloy (AA) 6061-T6 in linear and tubular configurations were examined using the electron backscattered diffraction (EBSD) technique. A refined structure of heavily deformed grains with higher grain boundary angles was observed in linear welds. Significant spalling was observed away from the joints, in the interior of tubular welds. The results show the complex interaction of shock waves with the materials during this impact welding process.

2008-08-01

42

Medium carbon vanadium micro alloyed steels for drop forging  

International Nuclear Information System (INIS)

Growing competitiveness of alternative manufacturing routes requires cost minimization in the production of drop forged components. The authors analyse the potential of medium carbon, vanadium microalloyed steels for drop forging. Laboratory and industrial experiments have been carried out emphasizing deformation and temperature cycles, strain rates and dwell times showing a typical processing path, associated mechanical properties and corresponding microstructures. The steels the required levels of mechanical properties on cooling after forging, eliminating subsequent heat treatment. The machinability of V-microalloyed steels is also improved when compared with plain medium carbon steels. (author)

43

The effect of the changing microstructure on the fatigue behaviour during cyclic rolling contact loading  

Energy Technology Data Exchange (ETDEWEB)

During rolling contact fatigue of the inner rings of ball bearings three stages of material response can be distinguished, in terms of the volume that is plastically deformed upon overrolling. After a first stage of material strengthening during which a decrease occurs for the volume that is deformed plastically, an effectively stationary, second stage is entered which is eventually succeeded by a third stage exhibiting a pronounced increase of the volume that is deformed plastically upon overrolling, which leads to failure. It is suggested that carbon diffusion induced by local temperature peaks occurring at the moment of overrolling is the key mechanism leading to fatigue damage. The amount of decomposed retained austenite is a useful, practical parameter to assess fatigue life. It is shown that published ideas about the role of certain components of residual stress in enhancing fatigue life are not correct and that the ...

1997-04-01

44

Dynamic nucleation of new grains in magnesium alloy during hot deformation  

Energy Technology Data Exchange (ETDEWEB)

Microstructure evolution under hot deformation was investigated in compression of a magnesium alloy AZ31 at 673 K (0.73T{sub m}). Two kinds of samples were machined along the parallel and transverse direction of the extruded rods. New fine grains are evolved at corrugated grain boundaries at low strains and developed rapidly in grain interiors in the medium range of strain, finally leading to a roughly full evolution of equiaxial fine grains. Kink bands are evolved at corrugated grain boundaries and in grain interiors at low strains. The boundary misorientation of kink band increases rapidly with increasing strain. These characteristics of new grain evolution process are not changed by the orientation of the samples, while the flow behaviors clearly depend on it. It is concluded that new grain evolution can be controlled by a deformation-induced continuous reaction resulting in grain fragmentation by kink bands, i.e. ...

2003-07-01

45

Determination of the stacking fault energy of austenite in a duplex stainless steel; Determinacao da energia de defeito de empilhamento da austenita de aco inoxidavel duplex  

Energy Technology Data Exchange (ETDEWEB)

Determination of stacking fault energy (SFE) of the austenite phase of a duplex stainless steel DIN W.-Nr.: 1.4462 has been carried out using transmission electron microscopy. Furthermore, cold rolling tests and microstructural analysis have been realized in order to allow a detailed discussion of the obtained SFE-values. The results of this investigation indicate that the stacking fault energy of the austenite phase within the duplex stainless steel is lower than of one-phase austenitic stainless steels. This is justified by the chemical composition, mainly by the Cr and Ni alloying contents. Nevertheless, work hardening of the austenite during cold deformation is not as accentuated as expected by the SFE-values, because at higher deformation levels the deformation mainly occurs within the ferrite phase 7 refs., 5 figs., 2 tabs.

1995-12-31

46

SEM and TEM investigations of recovery and recrystallization in technically pure molybdenum; REM- und TEM-Untersuchungen von Erholung und Rekristallisation in technisch reinem Molybdaen  

Energy Technology Data Exchange (ETDEWEB)

Beside traditional applications of refractory metals, e.g. in high temperature furnace construction, lighting or glass industry, one of the most important molybdenum products nowadays are large plates which are frequently used as targets for the sputtering of molybdenum layers in thin-film transistor liquid crystal displays. For the hot rolling of the sintered pre-material, the control over the recovery and recrystallization behavior is of particular importance. Molybdenum tends to a very recovery controlled behavior during hot deformation, at which the dislocations arrange into subcell boundaries instantaneously. These pronounced recovery processes seem to consume a large amount of the stored deformation energy for the actual recrystallization. On the other hand, recovery provides the future recrystallization nuclei. For a comprehensive characterization of these microstructural processes, electron microscopy appears to be ...

2011-07-15

47

In vitro corrosion, cytotoxicity and hemocompatibility of bulk nanocrystalline pure iron  

International Nuclear Information System (INIS)

Bulk nanocrystalline pure iron rods were fabricated by the equal channel angular pressure (ECAP) technique up to eight passes. The microstructure and grain size distribution, natural immersion and electrochemical corrosion in simulated body fluid, cellular responses and hemocompatibility were investigated in this study. The results indicate that nanocrystalline pure iron after severe plastic deformation (SPD) would sustain durable span duration and exhibit much stronger corrosion resistance than that of the microcrystalline pure iron. The interaction of different cell lines reveals that the nanocrystalline pure iron stimulates better proliferation of fibroblast cells and preferable promotion of endothelialization, while inhibits effectively the viability of vascular smooth muscle cells (VSMCs). The burst of red cells and adhesion of the platelets were also substantially suppressed on contact with the nanocrystalline pure iron in blood ...

2010-12-01

48

Study on fracture behaviour of Al?15%Mg2Si metal matrix composite with and without beryllium additions  

British Library Electronic Table of Contents (United Kingdom)

In this study, the influence of Beryllium (Be) content on the fracture behaviour of Al?15%Mg2Si composite was investigated. The results showed an increase in mechanical properties with increasing of Be content. The stress?strain curves of samples showed a same category of serrations reflecting non-uniform deformation. Scanning electron microscopy was employed to examine the crack nucleation and fracture model. The results indicate that Al?15%Mg2Si composite shows different behaviours of crack initiation and fracture for samples with and without Be. Differences observed in the fracture behaviour were attributed to microstructural changes as well as morphological aspects of primary Mg2Si particles.

2011-01-01

49

Design and characterization of a lamellar nanostructure in a low C steel  

British Library Electronic Table of Contents (United Kingdom)

A fully lamellar ferrite/cementite nanostructure was designed in a low C steel by using a specific thermal treatment. The strengthening of such microstructure has been investigated as a function of prestrain by rolling up to a deformation of 300%. As in usual pearlitic structure, its work-hardening shows no saturation and its elongation to fracture remains rather constant instead of decreasing drastically as conventional steels. The hardening by a similitude effect is thus not the privilege of pearlitic steels. Nevertheless, its lower initial work-hardening rate at low strain compared to an equivalent pearlitic steel and a lower hardening potential at high strain let us suspect major differences in the nature and the behaviour of ferrite channels in relation to the morphogenesis of the mic...

2011-01-01

50

Irradiation-assisted stress corrosion cracking in HTH Alloy X-750 and Alloy 625  

International Nuclear Information System (INIS)

In-reactor testing of bolt-loaded compact tension specimens was performed in 360 C water to determine the irradiation-assisted stress corrosion cracking (IASCC) behavior of HTH Alloy X-750 and direct-aged Alloy 625. New data confirm previous results showing that high irradiation levels reduce SCC resistance in Alloy X-750. Heat-to-heat variability correlates with boron content, with low boron heats showing improved IASCC properties. Alloy 625 is resistant to IASCC, as no cracking was observed in any Alloy 625 specimens. Microstructural, microchemical and deformation studies were performed to characterize the mechanisms responsible for IASCC in Alloy X-750 and the lack of an effect in Alloy 625. The mechanisms under investigation are: boron transmutation effects, radiation-induced changes in microstructure and deformation characteristics, and radiation-induced segregation. Irradiation of Alloy X-750 ...

1995-08-06

51

Microstructure engineering from metallic powder blends for enhanced mechanical properties  

International Nuclear Information System (INIS)

The present work focuses on the transformation of high-purity Ni powder blends of controlled volume fractions (40 and 60 %) of nanometre-sized (100 nm) and micrometre-sized (544 nm) particles into bulk samples as part of a strategy for producing ultrafine-grained materials usefully exhibiting both strength and ductility. The process involved cold isostatic pressing at 1.5 GPa and sintering. The resulting bulk samples had relative densities near 95 %, were texture-free, and exhibited two different grain size distributions with an average value of 600 #+-# 30 nm. The mechanical properties were investigated by compression and microhardness tests, both at room temperature, and compared to the behaviour of a sample processed from micrometre-sized powder only. Samples prepared from the blends exhibited high yield stresses of 440 and 550 MPa after compression, and they did sustain work hardening. Tests conducted before and after compression up to 50 % deformation showed ...

2010-07-01

52

Irradiation-assisted stress corrosion cracking of HTH Alloy X-750 and Alloy 625  

International Nuclear Information System (INIS)

In-reactor testing of bolt-loaded compact tension specimens was performed in 360 C water. New data confirms previous results that high irradiation levels reduce SCC resistance in Alloy X-750. Low boron heats show improved IASCC (irradiation-assisted stress corrosion cracking). Alloy 625 is resistant to IASCC. Microstructural, microchemical, and deformation studies were carried out. Irradiation of X-750 caused significant strengthening and ductility loss associated with formation of cavities and dislocation loops. High irradiation did not cause segregation in X-750. Irradiation of 625 resulted in formation of small dislocation loops and a fine body-centered-orthorhombic phase. The strengthening due to loops and precipitates was apparently offset in 625 by partial dissolution of #gamma# precipitates. Transmutation of boron to helium at grain boundaries, coupled with matrix strengthening, is believed to be responsible for IASCC in X-750, and the ...

1995-08-06

53

High-temperature strength property evaluation of heat affected zone in boiler weldment parts of 2.25Cr-1Mo steel; 2.25Cr-1Mo ko boiler yosetsu netsu eikyobu no koon kyodo tokusei hyoka  

Energy Technology Data Exchange (ETDEWEB)

In view of the situation that aging of boiler components proceeds and some `Type IV` cracking incidents are reported recently, the development of an accurate remaining life evaluation method for boiler weldment parts is an important subject for the utilities. In this study, simulated materials with coarse and fine grain microstructures in a weldment heat affected zone were produced, and their high temperature strength properties were evaluated. The strength property of the weld joint was also discussed based on the experimental and analytical results. It was found that the creep rupture strength of the fine grain material was as low as 1/2 of the base metal and as 1/5 of the coarse grain material, and the weld joint ruptured at the fine grain region in a shorter period than the base metal as the applied stress level decreased. Many grainboundary creep cavities were also observed in the fine grain region. A creep deformation analysis by FEM ...

1998-03-15

55

DEFORMATION BEHAVIOR OF AN OMEGA HARDENED ...  

Science.gov (United States)

... Accession Number : ADD100229. Title : DEFORMATION BEHAVIOR OF AN OMEGA HARDENED ALPHA-BETA TITANIUM ALLOY,. ...

56

Effect of Yttrium on the Microstructure of Titanium Alloys,  

Science.gov (United States)

... Title : Effect of Yttrium on the Microstructure of Titanium Alloys,. ... The yttrium was added in the melting stage as an oxide or in the elemental form. ...

57

Fast and cyclic deformation and transformation behaviour of hardened phases of the steels X210Cr12 and 100Cr6 containing retained austenite; Zuegiges und zyklisches Verformungs- und Umwandlungsverhalten von gehaerteten restaustenitbehafteten Werkstoffzustaenden der Staehle X 210 Cr 12 und 100 Cr 6  

Energy Technology Data Exchange (ETDEWEB)

Alloyed steels containing retained austenite after martensitic hardening are widely applied in technical practice. Although many practical investigations have been made into the mechanical behaviour of composite microstructures with retained austenite, there is still a lack of knowledge concerning their fatigue and crack propagation behaviour. For this reason, the author investigated the effects of retained austenite concentration and stability on the transformation and deformation behaviour of hardened states of the steels X210Cr12 and 100Cr6. For this purpose, monotone tensile tests, cyclic tensile pressure tests, and supplementary crack propagation experiments were carried out. The concentrations of retained austenite were varied between 10 and 100% by volume by means of different heat treatments. [Deutsch] Legierte Staehle, die nach martensitischer Haertung noch Restaustenit enthalten, finden in der technischen Praxis verbreitete Anwendung. ...

1995-11-01

58

Effects of ductile particles on the toughness and deformation characteristics of NiAl matrix materials; Einfluss duktiler Teilchen auf die Zaehigkeit und das Verformungsverhalten von NiAl-Matrix-Werkstoffen  

Energy Technology Data Exchange (ETDEWEB)

The intermetallic phase NiAl is a potential material for high-temperature applications; however, its technical application was prevented so far by its high brittleness at room temperature. This problem may be solved by incorporating relatively high-ductility particles into the NiAl matrix. Controlled crack propagation experiments, tensile and pressure tests were carried out in order to analyze the toughness and deformation characteristics of NiAl composite materials containing niobium or molybdenum particles at room temperature and in ambient atmosphere. Both the niobium and the molybdenum particles increase the toughness as compared to the pure NiAl matrix, but no ductilisation was observed in the composite materials investigated. Model experiments in consideration of experimental data suggest, hovewer, that the toughness and ductility of NiAl may be enhanced by optimizing the microstructural and production parameters of the incorporated ...

1995-12-31

59

Deformation of CHS model  

Energy Technology Data Exchange (ETDEWEB)

We calculate mass spectrum of CHS model deformed by an exactly marginal operator, and find that there are tachyons which are not localized in the target space. Similar deformation is discussed in another CFT which corresponds to separated NS5-branes. A condensation of the tachyons is briefly argued.

2002-10-07

60

Utilization of consistency metrics for error analysis in deformable image registration  

UK PubMed Central (United Kingdom)

PurposeTo investigate the utility of consistency metrics, such as inverse consistency, in contour based deformable registration error analysis.Full Text Available

2009-09-21

61

IDSS: deformation invariant signatures for molecular shape comparison  

UK PubMed Central (United Kingdom)

BackgroundMany molecules of interest are flexible and undergo significant shape deformation as part of their function, but most existing methods of molecular shape comparison (MSC)...Full Text Available

62

Enhanced Reliability MEMS Deformable Mirrors for Space Imaging ...  

Science.gov (United States)

Sep 3, 2010 ... These higher-quality deformable mirrors will enable diffraction-limited performance for many space-based optical systems such as space-based ...

64

Deformation and seismicity of Taiwan  

UK PubMed Central (United Kingdom)

14C-dated Holocene coastal uplift, conventional and satellite geodetic measurements, and coseismic and aseismic fault slip reveal the pattern of distributed deformation at Taiwan resulting...Full Text Available

2000-10-10

65

Preliminary Investigations of Joining Technologies for Attaching Refractory Metals to Ni-Based Superalloys  

International Nuclear Information System (INIS)

In this study, a range of joining technologies has been investigated for creating attachments between refractory metal and Ni-based superalloys. Refractory materials of interest include Mo-47%Re, T-111, and Ta-10%W. The Ni-based superalloys include Hastelloy X and MarM 247. During joining with conventional processes, these materials have potential for a range of solidification and intermetallic formation-related defects. For this study, three non-conventional joining technologies were evaluated. These included inertia welding, electro-spark deposition (ESD) welding, and magnetic pulse welding (MPW). The developed inertia welding practice closely paralleled that typically used for the refractory metals alloys. Metallographic investigations showed that forging during inertia welding occurred predominantly on the refractory metal side. It was also noted that at least some degree of forging on the Ni-based superalloy side of the joint was necessary to achieve consistent bonding. Both ...

2006-01-20

70

Investigation of Destruction Mechanisms in Reactor Steels  

International Science & Technology Center (ISTC)

Investigation of Destruction Mechanisms in Reactor Steels and Alloys under Cycling Deformation

71

Investigation into superplasticity of Be alloys  

International Nuclear Information System (INIS)

Investigated are the characteristics of high-temperature plastic deformation the velocity sensitivity of flow stresses, deformation curves, flow stresses, deformation before rupture - as well as the structure of beryllium alloys containing nickel (0.5-4 %), yttrium (0.5-2 %) and aluminium (38 %). The alloys containing nickel (2%) and yttrium (0.5 %) are superplastic, however, deformation before fracture of the alloys is lower than that of the unalloyed beryllium. The singularities of high-temperature plastic flow of the alloys and the causes of deterioration of their plasticity are determined.

74

Determination of Shooting Distance from Deformation of the ...  

Science.gov (United States)

... Descriptors : *TERMINAL BALLISTICS, *WOUND BALLISTICS, VELOCITY, CONVERSION, REPRINTS, TISSUES(BIOLOGY), MANUFACTURING ...

75

A STUDY TO DETERMINE THE DEFORMATION ...  

Science.gov (United States)

... crystals and polycrystals. Nevertheless, explosive forming, magnetic forming, etc., are all high-strain-rate processes that ...

1963-04-01

81

EFFECT OF MICROSTRUCTURE ON THE STRENGTH ...  

Science.gov (United States)

... THE STRENGTH, TOUGHNESS, AND STRESS-CORROSION CRACKING SUSCEPTIBILITY OF A METASTABLE BETA TITANIUM ALLOY (Ti-11. ...

1970-02-01

82

Quantitative bone scintigraphy in the evaluation of angular deformity of the lower extremity  

International Nuclear Information System (INIS)

A technique for quantitative analysis of growth plates in varus or valgus deformity about the knee has been developed. Computer-generated regions of interest are placed on magnification scintigraphs to divide distal femoral and proximal tibial physes into four equal segments. The ratio of counts in the medial half to counts in the lateral half was studied in 31 children (22 normal, 9 with angular deformity). Normal ratios were 0.74 to 0.98 for femora and 0.98 to 1.20 for tibias. In eight of nine patients with deformity, the ratio was abnormal; in two patients the ratio returned to normal when the deformity ceased to progress.

83

Electron microscopy study of thermomechnical deformation conditions effect on the structure of two-phase (#alpha#+#beta#) titanium alloys  

International Nuclear Information System (INIS)

The methods of optical and transmission electron microscopy were used to study the influence of different programmes of hot deformation on the structure formation of (#alpha#+#beta#) titanium alloy VT9. The #beta# alloy VT-15 was studied at the same time in order to simulate the dislocation structure generated in the process of hot deformation. During the hot deformation of two-phase titanium alloys in both #beta# and (#alpha#+#beta#) ranges there is found to be an optimum range of deformation in which a homogeneous, polygonized structure is formed.

84

Effect of deformation on corrosion behavior of Ti-23Nb-0.7Ta-2Zr-O alloy  

International Nuclear Information System (INIS)

The influence of deformation on the corrosion behavior of a newly developed multifunctional beta titanium alloy Ti-23Nb-0.7Ta-2Zr-O (mol%) in Ringer's solution at 310 K was evaluated using an electron backscatter diffraction technique and electrochemical measurements. The results showed that the effect of deformation on the corrosion resistance of the beta titanium alloy is complicated. Small levels of plastic deformation are detrimental to the corrosion resistance, whereas large deformations tend to eliminate this detrimental effect.

2009-03-01

85

The Diagnostic Method of Inner Parts of Welded Joints at Nuclear Power Plant  

International Nuclear Information System (INIS)

There is no possibility to check any inner part at real welded joint at nuclear power station (NPS) during operation because any destructive test cannot be used. In practice there is checked surface of weld. There are used four methodical instructions for the check of real welds: 1. The visual inspection, 2. The measurement of hardness, 3. The chemical composition checking and 4. The microstructure replica analysis. It is necessary to know how these information of weld surface are in accordance with characteristics of inner parts of weld. If there is not any difference between surface weld microstructure and internal weld microstructure of experimental weld it is supposed to that there is not any difference in other measured properties of welds. If is changed structural characteristics of microstructure, it is changed also hardness, chemical analysis etc. It was observed that the ...

2010-06-22

86

Technical note: A physical phantom for assessment of accuracy of deformable alignment algorithms  

International Nuclear Information System (INIS)

The purpose of this study was to investigate the feasibility of a simple deformable phantom as a QA tool for testing and validation of deformable image registration algorithms. A diagnostic thoracic imaging phantom with a deformable foam insert was used in this study. Small plastic markers were distributed through the foam to create a lattice with a measurable deformation as the ground truth data for all comparisons. The foam was compressed in the superior-inferior direction using a one-dimensional drive stage pushing a flat 'diaphragm' to create deformations similar to those from inhale and exhale states. Images were acquired at different compressions of the foam and the location of every marker was manually identified on each image volume to establish a known deformation field with a known accuracy. The markers were removed digitally from corresponding images ...

2007-07-01

87

Deformed-coal structure and control to coal-gas outburst  

Energy Technology Data Exchange (ETDEWEB)

Based on techniques of organic solvent extraction and a thermal model experiments of coal-related hydrocarbon, the variation of coal structure and the character of deformed coal-related hydrocarbons were studied when the coal seam at Piagdingshan mine, China was modified by tectonic stress. The results show that the extraction ratio by n-hexane and benzene from the deformed coal approaches that form normal coal, but the extraction ratio by chloroform from the deformed coal is two times more than that from normal coal. The deformed coal has higher solvable low-molecular weight compounds than normal coal. The intermolecular force of deformed coal is relatively small. The deformed coal has low strength and high adsorption capacity, and these determine the outbreak of coal-gas outburst. The extraction yields by chloroform can be taken as an index of forecast risks ...

2007-03-15

88

3D simulations of microstructure and comparison with experimental microstructure coming from OIM analysis  

International Nuclear Information System (INIS)

This paper presents a new methodology to create realistic 3D microstructures of polycrystals. The virtual microstructures are based on statistical data describing the morphological and crystallographic textures of a sample, obtained from an EBSD analysis. In addition, the methodology can reproduce the observed surface on top of the simulated microstructure. This feature allows finite element calculations on these virtual aggregates to be compared to experimental results of mechanical tests. Such a comparison leads to the identification of the mechanical parameters of constitutive laws, such as critical resolved shear stress and strain hardening, using an optimization algorithm. Two materials were simulated in this study: TiAl and grade 702 zirconium. The first one presents twins inside the microstructure and the second one has an anisotropic texture. Based on 2D simulations, the important parameters ...

89

ROCK DEFORMATION. Final Progress Report  

Energy Technology Data Exchange (ETDEWEB)

The Gordon Research Conference (GRC) on ROCK DEFORMATION was held at II Ciocco from 5/19/02 thru 5/24/02. Emphasis was placed on current unpublished research and discussion of the future target areas in this field.

2002-05-24

90

Objective assessment of deformable image registration in radiotherapy: A multi-institution study  

UK PubMed Central (United Kingdom)

The looming potential of deformable alignment tools to play an integral role in adaptive radiotherapy suggests a need for objective assessment of these complex algorithms. Previous studies in this area...Full Text Available

2008-12-01

91

Rotational band-structures in transitional odd-A nuclei  

International Nuclear Information System (INIS)

... deformed nuclei eigenvalues even-odd nuclei gold 195 hamiltonians iridium

92

On the validity of the pseudo-spin concept for axially symmetric deformed nuclei  

International Nuclear Information System (INIS)

The average single-particle field shows a very small pseudo-spin-orbit splitting in the pseudo-spin representation. If this splitting is neglected, pseudo-spin becomes a good quantum number and the resulting scheme (the pseudo-Nilsson model) has a very simple interpretation. The pseudo-spin symmetry embodied in the realistic deformed average field is explored by comparing the single-particle energies and wave functions of the deformed Woods-Saxon model with the corresponding results of the pseudo-Nilsson model. The scheme is used to calculate the magnetic moments of deformed odd-A nuclei of the rare-earth region. (orig.).

93

Modeling Blast and High-Velocity Impact of Composite Sandwich Panels  

Science.gov (United States)

Analytical models for predicting the deformation and failure of composite sandwich panels subjected to blast and projectile impact loading are presented in this paper. The analytical predictions of the transient deformations and damage initiation in the composite sandwich panels were compared with finite element solutions using ABAQUS Explicit. For the blast model, the predicted transient deformation of the sandwich panel was within 7%of FEA results, while the predicted damage initiation using Hashin's composite failure criteria was about 15%higher than FEA results in most cases. For the high velocity impact model, the predicted transient deformations were within 20%of FEA results.

2009-01-01

94

METAL DEFORMATION PROCESSES/FRICTION AND ...  

Science.gov (United States)

... In the same year, the Revere Copper and Brass Company of America introduced the tandem cold mill, soon followed by ...

2011-05-14

95

Evidence for asymmetric shapes from high-spin odd-A spectra  

International Nuclear Information System (INIS)

... coupling deformed nuclei gold 195 high spin states iridium 187 moment of

96

Comparison of Optical and SEM BSE Imaging Techniques for Quantifying Alpha-Beta Titanium Alloy Microstructures (Preprint).  

Science.gov (United States)

Quantitative metallography is often used to confirm the proper processing of aerospace metallic materials. A microstructural feature of great importance for titanium alloys processed in the alpha-beta phase field is the volume fraction of primary alpha. S...

2006-01-01

97

Correlation between tensile property and micro-hardness in reduced activation ferritic/martensitic steel irradiated at 573 K  

International Nuclear Information System (INIS)

Full text of publication follows: Radiation hardening and embrittlement due to high-energy neutron radiation around 623 K are the important issues on reduced-activation ferritic/martensitic (RAF/M) steels. It is expected that the improvement of radiation hardening might be one of effective ways to control the mechanical properties of RAF/M after irradiation. It has been reported that the weld joint has less hardening than the base metal from the tensile test results of TIG weldments irradiated in HFIR. This report indicated that radiation hardening can be reduced by the optimization of heat treatment condition for F82H. The purposes of this study are to establish the condition of heat treatment for minimum of radiation hardening in F82H steel using Neutron/Ion-irradiation and to examine a correlation between tensile property and micro-hardness before/after irradiation. The materials used in this study were F82H IEA heat and F82H heat treatment variants. Neutron irradiation was ...

2007-12-10

98

Structural features of twins in transition class alloy Ti-Al-Mo-V-Cr  

International Nuclear Information System (INIS)

The alloy of Ti-Al-Mo-V-Cr system is studied for its structure in a strained state and specific features of #beta#-#alpha# transformation in a #beta#-matrix and deformation twins on ageing. It is determined that preliminary deformation initiates the decomposition of solid solution on aging. In a metastable #beta#-titanium alloy the substructure of deformation twins is shown to vary essentially with aluminium and chromium partial substitution for molybdenum and vanadium

1999-11-01

99

Non-supersymmetric deformations of non-critical superstrings  

Energy Technology Data Exchange (ETDEWEB)

We study certain supersymmetry breaking deformations of linear dilaton backgrounds in different dimensions. In some cases, the deformed theory has bulk closed strings tachyons. In other cases there are no bulk tachyons, but there are localized tachyons. The real time condensation of these localized tachyons is described by an exactly solvable worldsheet CFT. We also find some stable, non-supersymmetric backgrounds.

2005-12-15

100

Governor model for asymmetric deformed nuclei  

International Nuclear Information System (INIS)

The governor model is extended to include the asymmetric shape of nuclei which allows a simultaneous analysis of the data for both the ground state and the #gamma#-vibrational bands in deformed even-even nuclei. The rotationally invariant core is assumed to be a spheroid with an axis of symmetry parallel to the axis of rotation. The calculations are carried out under the assumption of no stretching. The static #gamma#-deformation results are compared with the VMI(ARM) and Krutov values, and the calculated energies are in good agreement with the experimental data.

101

Application of strength hypotheses in the creep range under multiaxial stresses  

International Nuclear Information System (INIS)

The applicability of conventional strength hypotheses in the long-term creep range was examined by means of multiaxial loaded small and large-scale specimens of 1% CrMoNiV-steel at 550deg C. The experimentally determined deformation behaviour in the primary and secondary creep range was simulated by means of a finite element analysis. The creep deformation capacity is influenced by the degree of multiaxiality. The validity of a strength hypothesis depends on the type of load and on deformation resp. failure criteria. (orig.).

102

radiation hardening and microstructure evolution in austenitic chromium-nickel steel under various type irradiation  

International Nuclear Information System (INIS)

A study was made into microstructure and hardening in austenitic stainless steel 0Kh18N10T irradiated with neon ions (230 MeV) and neutrons (E_n > 0.1 MeV). The experiments were accomplished using an external beam of U-400 cyclotron (Dubna) and EWA reactor (Poland). The dependences of tensile properties, hardening index, microstructure, dislocation density on damaging dose were determined. An attempt is made to reveal the correlation between an yield strength increment and defect cluster accumulation. The interpretation of variations of mechanical properties and microstructure under irradiation is given.

103

Microstructure, texture and mechanical properties of the magnesium alloy AZ31 processed by ECAP  

Energy Technology Data Exchange (ETDEWEB)

To investigate the influence of equal channel angular pressing on the microstructure and texture of the magnesium alloy AZ31, electron backscattering diffraction and well as neutron diffraction experiments were carried out. Through these experiments it was possible to trace the microstructure and texture evolution with strain accumulated with the increasing number of equal channel angular pressing passes. It was further demonstrated by subsequent compression tests that the microstructural changes produced by equal channel angular pressing have a beneficial effect on both the compressive strength and ductility of AZ31. (orig.)

2008-01-15

106

Influence of HNS on the Microstructure and Properties of Cast ...  

Science.gov (United States)

... The ultimate compressive strength was measured, and values for Young's modulus were calculated from the linear portion of the test curve. ...

1981-04-01

107

Image analysis of complex microstructures by texture analysis and correlation with properties by neural networks; Bildanalyse komplexer Werkstoffgefuege durch Texturanalyse und Korrelation mit den Eigenschaften durch neuronale Netze  

Energy Technology Data Exchange (ETDEWEB)

By characterising the microstructure, quantitative image analysis allows to draw conclusions on the mechanical properties of materials. On fine microstructures with low contrast, e.g. of hardened steels, texture analysis has to be applied for quantification. Feeding texture parameters according to Haralick into a trained neural network, a correlation between the microstructure and the hardness of the steels C45 and 100Cr6 can be achieved. (orig.)

2001-08-01

109

#alpha#-Sialon - new opportunities via new microstructure  

International Nuclear Information System (INIS)

Both microstructural graded and homogenous single-phase #alpha#-Sialon is obtained from Si_3N_4 powder for a broad range of compositions of practical interest. Elongated grains of #alpha#-Sialon could be developed in the monophase material by controlled mechanism of nucleation and growth. Tailoring of microstructure was realized through slow transformation reaction from Si_3N_4 to #alpha#-Sialon at lower temperature than sintering temperature when the composition is near the #alpha#-Sialon phase boundary. The mechanical properties are strongly correlated with the microstructure and are enhanced greatly in the optimized Sialon composition. (author)

2001-05-01

110

Steel microstructure engineering for large diameter tubes; Engenharia de microestrutura de acos para tubos de grande diametro  

Energy Technology Data Exchange (ETDEWEB)

High and ultra-high strength steels for pipelines are produced by properly handling the steel microstructure. The metallurgical principles involved in the microstructure control are presented, with emphasis on TMCP processing, that comprises conventional controlled rolling followed by accelerated cooling. (author)

2008-05-15

111

Effect of laser induced plasma nitriding on al surface microstructure  

Energy Technology Data Exchange (ETDEWEB)

In this paper, aluminium nitride synthesis is carried out by direct laser irradiation onto an aluminium target surface in a nitrogen containing atmosphere. The influence of various processing parameters on the microstructure of AlN thin films is investigated in order to improve their tribological properties. The main microstructural characteristics: nature, concentration, in depth distribution and morphology of various phases are studied versus processing parameters by TEM and GIXD. (author). 2 refs., 1 fig., 2 photos.

1996-12-31

112

Effect of laser induced plasma nitriding on al surface microstructure  

International Nuclear Information System (INIS)

In this paper, aluminium nitride synthesis is carried out by direct laser irradiation onto an aluminium target surface in a nitrogen containing atmosphere. The influence of various processing parameters on the microstructure of AlN thin films is investigated in order to improve their tribological properties. The main microstructural characteristics: nature, concentration, in depth distribution and morphology of various phases are studied versus processing parameters by TEM and GIXD. (author). 2 refs., 1 fig., 2 photos.

113

Analysis of Ground Deformation Detected Using the SBAS-DInSAR Technique in Umbria, Central Italy  

British Library Electronic Table of Contents (United Kingdom)

Ground deformation affecting the Umbria region (central Italy) in the 9-year period from 1992 to 2000 was investigated through multi-temporal Differential Synthetic Aperture Radar Interferometry (DInSAR). For the purpose, the Small BAseline Subset (SBAS) technique was adopted, which allows studying the temporal evolution of the detected deformation at two spatial scales: a low-resolution (regional) scale, and a full-resolution (local) scale. For the analysis, SAR data acquired by the European Remote Sensing (ERS-1/2) satellites along ascending and descending orbits were used. The detected deformation was analysed to investigate its relevance to geophysical, geomorphologic, and human-induced processes that may result in hazardous conditions to the population of Umbria. Low-resolution deform...

2009-01-01

114

Consolidation settlement analysis of pile foundations; Kui kiso no atsumitsu chinka kaiseki  

Energy Technology Data Exchange (ETDEWEB)

Deformation of the ground can be considered as a sum of volume deformation and shear deformation. At circumferential ground of pile axis, simple shear type of shear deformation becomes main factor of settlement. As shear forces with reverse direction are overlapped at parallel face for pile around face of the ground between the piles, the shear deformation is relaxed. At deeper place from top of the pile, volume deformation becomes larger and component of shear deformation approaches to a pure shear type. In case of the land surface loading type consolidation settlement calculation, a method adopting one dimensional consolidation calculating method using only vertical component within stress obtained by elasticity theory even when investigating multi dimensionally is used widely. In Japanese design standards, the method calculating the ...

1997-02-01

115

Water Repellency Microstructure Oligomer Formulation Cured with Electron Beam  

International Nuclear Information System (INIS)

Water repellency en the microstructure super-hydrophobic cured surface is important for research and industrial purposes. This microstructure film can be cured on polyethylene terephthalate PET surface by electron beam (EB) at different irradiation doses 10-100 kGy. The microstructure formulation composed from hydrophobic acrylate oligomer (EB 244) and monomer (SR 440). The irradiation induced cross linking of the prepared microstructure was proved by FTIR spectroscopy and the adhesion force by abrasion test. Some factors affecting the adhesion force of the prepared microstructure film such as oligomer/monomer composition ratio and the thickness of the microstructure cured film were studied. The contact angles (8) were measured on cured surfaces before and after adding the super hydrophobic nanoparticles (Zonyl 9361). The super-hydrophobic cured surface showed ...

116

Dislocation plasticity and complementary deformation mechanisms in polycrystalline Mg alloys  

Energy Technology Data Exchange (ETDEWEB)

Deformation mechanisms of Mg-Al-Zn (AZ31) alloys were investigated by performing tensile test at room temperature. In fine grain Mg alloys deformed at room temperature, nonbasal slip systems were found to be active as well as basal slip systems because of grain-boundary compatibility effect. Slip-induced grain-boundary sliding occurred as a complementary deformation mechanism to give rise to c-axis component of strain. With increasing grain size, the activation of the nonbasal slip systems was limited near grain boundaries. Instead of grain-boundary sliding, twinning occurred as a complementary deformation mechanism in large grained samples. Orientation analysis of twins indicated that twinning is induced by stress concentration due to the pile up of basal dislocations. The grain-size dependence on deformation mechanism was found to affect yielding behavior both microscopically and ...

2004-07-01

117

Direct observation of radial distribution change during tensile deformation of metallic glass by high energy X-ray diffraction method  

International Nuclear Information System (INIS)

The purpose of this research is to investigate the micro-mechanism of deformation behavior of metallic glasses. We report the results of direct observations of short-range and medium-range structural change during tensile deformation of metallic glasses by high energy X-ray diffraction method. Cu50Zr50 and Ni30Zr70 metallic glass samples in the ribbon shape (1.5 mm width and 25 ?m) were made by using rapid quenching method. Tensile deformation added to the sample was made by using special equipment adopted for measuring the high energy X-ray diffraction. The peaks in pair distribution function g(r) for Cu50Zr50 and N30iZr70 metallic glasses move zigzag into front and into rear during tensile deformation. These results of direct observation on atomic distribution change for Cu50Zr50 and Ni30Zr70 metallic glass ribbons during tensile deformation suggest that the micro-relaxations ...

2009-08-26

118

Structural transformations of metastable #alpha#''-phase during cold deformation  

International Nuclear Information System (INIS)

Phase transformations occuring during cold deformation in hardened #alpha#+#beta# titanium alloy of the Ti-Al-Mo-Zr-Sn-Si system with 10% summary content of alloying elements are studied by X-ray diffraction analysis. Two stages of trapsformation of metastable #alpha#''-phase are found. A conclusiop is made that ability of the alloy containing #alpha#''-phase to cold deformation is determined by the presence of favourable texture, by high degree of metastability and by volume portion of #alpha#''-phase in the alloy structure.

119

Lifetime in {sup 181}Ir and {sup 187}Au: enhanced deformation of the {pi}i {sub 13/2} intruder orbital  

Energy Technology Data Exchange (ETDEWEB)

Lifetimes have been measured in the {pi}h{sub 9/2} (yrast) and {pi}i{sub 13/2} (excited) bands in the nuclei {sup 181}Ir and {sup 187}Au using the Recoil Distance Method (RDM). The results clearly indicate that the {pi}i{sub 13/2} band exhibits an increased deformation over the {pi}h{sub 9/2} band, in keeping with the premise that the delayed crossing in this band is due to enhanced quadrupole deformation. (author). 3 refs, 1 fig, 2 tab.

1995-02-01

120

Lifetime in "1"8"1Ir and "1"8"7Au: enhanced deformation of the #pi#i _1_3_/_2 intruder orbital  

International Nuclear Information System (INIS)

Lifetimes have been measured in the #pi#h_9_/_2 (yrast) and #pi#i_1_3_/_2 (excited) bands in the nuclei "1"8"1Ir and "1"8"7Au using the Recoil Distance Method (RDM). The results clearly indicate that the #pi#i_1_3_/_2 band exhibits an increased deformation over the #pi#h_9_/_2 band, in keeping with the premise that the delayed crossing in this band is due to enhanced quadrupole deformation. (author). 3 refs, 1 fig, 2 tab.

1994-09-05

121

Fractal analysis of deformation-induced dislocation patterns  

Energy Technology Data Exchange (ETDEWEB)

The paper reports extensive analyses of the fractal geometry of cellular dislocation structures observed in Cu deformed in multiple-slip orientation. Several methods presented for the determination of fractal dimensions are shown to give consistent results. Criteria are formulated which allow the distinguishing of fractal from non-fractal patterns, and implications of fractal dislocation patterning for quantitative metallography are discussed in detail. For an interpretation of the findings a theoretical model is outlined according to which dislocation cell formation is associated to a noise-induced structural transition far from equilibrium. This allows relating the observed fractal dimensions to the stochastic properties of deformation by collective dislocation glide.

1999-06-22

122

Electron microscopy analysis of grain boundary structure and composition in superplastically deformed Al-Mg alloys  

Energy Technology Data Exchange (ETDEWEB)

Evaluation of grain boundary composition and structure in superplastically deformed AA5083-based alloys (Al-4.5Mg-1.6Mn-0.2Zr) was carried out in a field-emission gun transmission electron microscope (FEG-TEM). During superplastic deformation at high homologous temperatures materials undergo extensive grain boundary sliding (GBS) which creates a flow of defects in the near-boundary region. Recent literature has shown that the grain-boundary composition in Al-Mg alloys is not necessarily the same as the matrix, and that these differences can have an effect on GBS.

1996-12-31

123

Microstructure design of dielectric ceramics; Yudentai seramikkusu no bikozo sekkei  

Energy Technology Data Exchange (ETDEWEB)

In order to design the microstructure of ceramics with desired dielectric property, an estimation method of dielectric constant of ceramics taking into account the characteristics of microstructure of the ceramics is proposed. In the estimation model, the microstructure of ceramics is represented by the assembly of unit cells comprising of grain, pore and grain boundary. The sizes of grain and pore and the thickness of grain boundary in each unit cell were determined exactly according to their size and thickness distributions in a real ceramic. The dielectric constant of the assembly can be calculated on the basis of equivalent circuit theory. The estimated values of dielectric constant of ceramic BaTiO{sub 3} using the proposed estimation method agree well with experimental ones. The dependence of characteristics of microstructure on the dielectric constant was clarified by the estimation of dielectric ...

2000-11-10

124

What is the heritable component of spinal deformities in the European sea bass (Dicentrarchus labrax)?  

British Library Electronic Table of Contents (United Kingdom)

Malformations in farmed fish are a prime research topic as it has a major impact on fish welfare and on the economical value of the product. In this study, the genetic component of spine deformities was estimated in European sea bass, a major species of Mediterranean aquaculture, with the use of a posteriori reconstruction of pedigree with microsatellites. Our population exhibited a very high malformation rate (81%), probably due to intense swimming of fish during pre-growing. The heritability of global spine deformities was evaluated to be 0.21?0.04 on the underlying scale (0.33?0.06 for lordosis, 0.13?0.04 for scoliosis). Deformities scored by an internal or external examination turned out to be genetically the same trait (genetic correlations>0.9), although phenotypic correlations were ...

2009-01-01

126

Study on the low-lying collective states of A=54-124 nuclei in 50 MeV #alpha#-particle scattering and in the "6"4Ni("3He, "3He') reaction by DWBA and coupled channel method  

International Nuclear Information System (INIS)

The analysis of elastic and inelastic scattering of #alpha# particles with energy of 50 MeV by nuclei with mass numbers A=54-124 and of "3He particles by the nucleus "6"4Ni is given in the framework of the optical model. The parameters of multipole deformations for lower states are determined. The parameters for quadrupole and octupole deformations of the potential for the nucleus "1"1"2Sn are extracted, the values of the hexadecupole deformation #beta#_4 of the potential for nuclei "9"4Zr, "1"2"0","1"2"4Sn are found. Information is extracted on the ratio of deformation parameters for the neutron and proton components in lower collective states (2_1"+, 3_1"-) of nuclei with A=90-124.

127

Study of Contemporary Electronic Components under a Fluid ...  

Science.gov (United States)

... The effects of these voids were more noticeable for tantalum and aluminum electrolytic capacitors, which usually exhibited severe case deformation ...

1973-03-01

128

Structure and properties of a metastable #beta#-alloy aged after plastic deformation  

International Nuclear Information System (INIS)

Phase and structural transformations in a multicomponent (5.05 mas.% Mo-4.95V-3.00Cr-3.05Al) metastable #beta#-titanium alloy on aging after plastic deformation are studied using methods of electron microscopy and X-ray diffraction analysis. The alloy is deformed by twinning in a #left brace#332#right brace# system, and even at initial stages the formation of a twin skeleton takes place in the structure, on further loading the deformation of the skeleton is by secondary twinning resulting in a high plasticity of the alloy. On annealing mechanical twins transform into #alpha#-phase - a ductile twin skeleton is replaced by a rigid skeleton of #alpha#-phase plates. The aging enhances the yield strength of the alloy but decreases sharply its plasticity

2004-12-01

129

Structure and morphology changes during nylon 66 fiber deformation via synchrotron x-ray scattering techniques  

Energy Technology Data Exchange (ETDEWEB)

Morphological and structural changes of nylon 66 were evaluated during a continuous heat-draw process. Results are discussed.

1996-12-31

130

Structure and Mechanical Properties of Boron-Doped Cubic ...  

Science.gov (United States)

... by the boron doping in most of the alloys except for Al66Mn9Zr25 + 50 ppm B alloy; permanent deformation at ultimate compressive strength is not ...

131

Resonances in gravitational scenario given by deformed branes  

Science.gov (United States)

In this work we examine a five-dimensional brane-world model with brane structure driven by a real scalar field. From the deformation of a kink-like defect we find a new class of brane solutions containing internal structures which have implications for the way the background space-time is constructed and the way its curvature behaves. Initially, for spin 0 scalar field, we find a zero mode which can be localized on the deformed brane. However, this result can change by the gravitational interaction with the brane internal structure. Analyzing the massive modes of the scalar field, using two different methods, we find resonance structures similar to those found in the study of gravity localization. The main objective here is to observe the contributions of the deformation procedure to the resonances and to the well known field localization methods.

2011-08-01

132

Quantization of the Lie algebra so(2n+1) and of the Lie superalgebra osp(1/2n) with preoscillator generators  

CERN Document Server

The Lie algebra so(2n+1) and the Lie superalgebra osp(1/2n) are quantized in terms of 3n generators, called preoscillator generators. Apart from n "Cartan" elements the preoscillator generators are deformed para-Fermi operators in the case of so(2n+1) and deformed para-Bose operators in the case of osp(1/2n). The corresponding deformed universal enveloping algebras U_q[so(2n+1)] and U_q[osp(1/2n)] are the same as those defined in terms of Chevalley operators. The name "preoscillator" is to indicate that in a certain representation these operators reduce to the known deformed Fermi and Bose operators.

1994-01-01

133

Positive energy representations of the conformal quantum algebra  

International Nuclear Information System (INIS)

The positive-energy unitary irreducible representations of the q-deformed conformal algebra #delta#C_q = U_q(su(2,2)) are obtained by appropriate deformation of the classical ones. When the deformation parameter q is N -th root of unity, all these unitary representations become finite-dimensional. For his case we discuss in some detail the massless representations, which are also irreducible representations of the q-deformed Poincare subalgebra of #delta#C_q. Generically, their dimensions are smaller than the corresponding finite-dimensional non-unitary representation of su(2,2), except when N = 2 modul h + 1, where h is the helicity of the representations. The latter cases include the fundamental representations with h = #+-#1/2. (author). 10 refs.

1985-05-22

134

Nonlinear creep deformation analysis of a radiation-cured wood-polymer composite  

International Nuclear Information System (INIS)

A wood-polymer composite has been produced by impregnating the wood with the monomer and subsequently polymerizing it by exposure to a gamma radiation source. To compare the improvement in creep deformation of the wood due to the polymer impregnation, a nonlinear Norton-Bailey isothermal mathematical function has been used to model the bending creep deformation of the wood-polymer composites. Results show that the impregnation significantly improves the creep resistance of the wood. The maximum creep resistance is obtained when the amount of polymer impregnation exceeds about 30%. An interfacial interaction between the wood cell wall and the polymer could explain the creep deformation improvement, as well as the maximum impregnation level beyond which little improvement occurs. The results indicate that polymer impregnation is a viable method for improving the poor creep properties of wood. (author).

1989-01-01

136

Evaluation of the long-term mechanical behavior in the near-fields considering chemical transitions of barrier materials  

International Nuclear Information System (INIS)

An analysis system for the long-term mechanical behavior of barrier materials (MACBECE: Mechanical Analysis system considering Chemical transitions of BEntonite-based and CEment-based materials) was developed in order to improve the reliability of the evaluation of the hydraulic field which is one of the important environmental conditions in the safety assessment of the TRU waste disposal. MACBECE is the system that calculates the deformation of barrier materials using their chemical property changes as inputs, and subsequently calculates their hydraulic conductivity taking both their chemical property changes and deformation into consideration. By using MACBECE, the long-term deformation and the transition of hydraulic field for the round-type disposal cavities were evaluated, assuming some sets of chemical evolution data as input. Based on the analysis result, it is considered that the influence of the long-term ...

2007-04-22

138

Effect of electrostimulated deformation on thin structure and mechanical properties of polycrystalline molybdenum  

Energy Technology Data Exchange (ETDEWEB)

To clarify the effect of electrostimulated deformation on the fine structure and mechanical properties of polycrystalline molybdenum the experiments on the flattening of wire 0.8 mm in diameter into a strip 0.4 mm thick and its further rolling to 0.1 mm thickness using the electric current of high density in the deformation zone and without it, are carried out. As a result of the electric current use the strip density has increased by more than 20%, the same plasticity being preserved. The changes above are explained by the transformations in the fine structure of the deformed metal, which are manifested in more uniform distribution of dislocations and impurities in the grain boundaries in wide angles of the disoriented subgrains.

1981-01-01

139

Double decoupling and pseudo-spin alignment  

Energy Technology Data Exchange (ETDEWEB)

Doubly decoupled structures in doubly odd deformed nuclei are reexamined and shown to be composed of a pseudo-spin aligned neutron and a decoupled proton. (orig.).

1992-04-16

140

Double decoupling and pseudo-spin alignment  

International Nuclear Information System (INIS)

Doubly decoupled structures in doubly odd deformed nuclei are reexamined and shown to be composed of a pseudo-spin aligned neutron and a decoupled proton. (orig.).

141

Dislocation structure and mechanical properties of. cap alpha. -iron in dependence on plastic deformation conditions  

Energy Technology Data Exchange (ETDEWEB)

Investigations of dislocation structure and mechanical properties of iron after rolling deformation in shaped rolls and after hydroextrusion are conducted. It is shown that dislocation iron structure slightly changes with deformation degree after rolling in shaped rolls and annealing and it is characterized by low density of screw dislocations. Cold brittleness temperature decreases in the result of rolling and the succeeding recrystallization and impact strength increases both at room temperature and at low temperatures. Screw dislocations having high Peierls barrier prevail in the structure after hydroextrusions. The iron deformed by hydroextrusion at 400 mPa and higher after annealing has high cold brittleness temperature and low impact strength.

1982-03-01

142

Deformation of "5"6Fe from 104 MeV #alpha#-particle scattering  

International Nuclear Information System (INIS)

(1 Apr 1975). United Kingdom Gils, HJ Rebel, H. Nowicki, G. Ciocanel, A.

143

Deformable spanners and applications  

UK PubMed Central (United Kingdom)

For a set S of points in ℝd, an s-spanner is a subgraph of the complete graph with node set S such that...Full Text Available

2006-08-01

144

CoSpell CheckSpell Checkherent Charge Qubits Based on ...  

Science.gov (United States)

... We considered spontaneous radiation of quanta and acoustic phonons (both due to deformational and piezoelectric electron-phonon interaction ...

2000-06-23

145

Analytical Summary. Part 4. The Theory of Armor Penetration  

Science.gov (United States)

... F ? (28.3)(108) in an isotherme.l deformation with stationary principal axes of strain rate, but the component might be as small as F2= (19-3)(100) ...

1946-05-01

146

Transmission electron microscopy of simulated DWPF high level nuclear waste glasses following gamma irradiation  

International Nuclear Information System (INIS)

Thermal analysis testing revealed slight weight changes, which were a function of gamma irradiation, in a highly reduced Defense Waste Processing Facility (DWPF) simulated waste glass. Transmission electron microscopy (TEM) was performed on this glass to determine if the weight change corresponded to microstructural variations. TEM analyses showed that no microstructural changes were attributable to gamma irradiation. Exposure of the samples to the electron beam in the TEM did cause changes in the glass microstructures in some cases. These changes were likely due to localized heating of the glass due to interactions with the transmitted electrons.

1994-04-25

147

Property and Microstructural Nonuniformity in the Yttrium-Barium ...  

Science.gov (United States)

Pore Fraction in Yttrium-Barium-Copper-Oxide and. Other Polycrystalline. Materials ...... Properties of Yttrium Ceramic. Sov. J. LowTemp.Phys. 14:395-402 . ...

148

Nitride Fuel for Fast Neutron Nuclear Reactors  

International Science & Technology Center (ISTC)

Development of Technology for Producing High-Effective Nitride Fuel UN with Controlled Microstructure for Advanced Fast Neutron Nuclear Reactors

150

Microstructure and fracture toughness of hot pressed zirconia-toughened sialon  

International Nuclear Information System (INIS)

Zirconia-toughened sialon composites have been fabricated using conventional hot-pressing techniques. The fracture toughness and microstructure were determined for CeO_2- and Y_2O_3-stabilized ZrO_2 additives and also as a function of volume percent ZrO_2. The Yttria system showed a linear increase in fracture toughness with increasing volume fraction zirconia content while the ceria-stabilized system exhibited a peak in fracture toughness at 20 vol% ZrO_2 content. The fracture toughness at 800 C was measured and correlated with the microstructure. High-temperature stability was determined and it was found that the deleterious nitride phases of zirconium could be precluded from the microstructure.

151

Metallurgical instabilities during the high temperature low cycle fatigue of nickel-base superalloys  

Energy Technology Data Exchange (ETDEWEB)

In this letter, examples of microstructural instabilities that can significantly affect the low crystal fatigue (LCF) life are pointed out.

1983-01-01

154

Dual-ion irradiation effects on microstructure of austenitic alloys  

International Nuclear Information System (INIS)

An Fe-15Cr-20Ni ternary model alloy and a Type 316 stainless steel were irradiated by dual-ions at 1 to 50 appm of He/dpa ratios, to investigate the helium effects on microstructural development in austenitic alloys under irradiation. Quantitative analysis on resultant microstructures revealed that the Frank loop nucleation rate and the network dislocation density positively correlate and Frank loop growth rate negatively correlate with the He/dpa ratio, while the cavity growth rate has its peak at an intermediate helium injection rate. Although He/dpa dependence of various microstructural features were similar for the model alloy and the 316SS, the rates of their development and the mechanism which had assisted cavity growth were significantly different in these two materials. (orig.).

155

Design and microstructural analysis of magnesium alloys for dynamical applications  

British Library Electronic Table of Contents (United Kingdom)

A microanalytical characterization of cast magnesium alloys of eutectic origin based on the Mg?Al?Ca ternary matrix system has been carried out in order to investigate the influence of alloying elements on their microstructure as well as microchemistry-processing-microstructural relations using structure-sensitive techniques of electron microscopy, mechanical spectroscopy (internal friction), X-ray diffractometry, and advanced microanalytical methods including electron probe compositional analysis. Following the data obtained here there is direct correlation of microstructure with creep properties of the new experimental magnesium alloys. The creep and heat-induced properties of the multicomponent magnesium alloys containing low range of inexpensive additions of titanium (0.07?0.2%) or str...

2011-01-01

156

:z:..... \\ - NASA Technical Report Server (NTRS)  

Science.gov (United States)

A common reinforced liner material is a cloth formed of PTFE fibers and fiber of ... and ablation protection provided. All of these methods of thermal ..... The influence of fiber content on the microstructures of the composites is ...

157

Void growth and softening of a single crystal with strain gradient effects  

Energy Technology Data Exchange (ETDEWEB)

The strain gradient crystal plasticity theory is applied to study the deformation of planar single crystal with a void under a nominally uniaxial tension. The crystal theory assumes elevated strain hardening due to slip gradients and has a constitutive length scale. The effects of the void size with respect to the constitutive length scale on the single crystal deformation are investigated.

1997-02-06

158

Shape coexistence and extreme deformations near A =80  

Energy Technology Data Exchange (ETDEWEB)

The neutron deficient Sr and Zr nuclei are studied in the relativistic mean-field approach. Large deformations and shape coexistence are predicted for these nuclei in the vicinity of the proton drip line. The charge radii are found to increase with the removal of neutrons from the semimagic {sup 88}Sr and {sup 90}Zr, in close agreement with the recent isotopic-shift measurements.

1992-10-01

159

Recent plate motions and crustal deformation  

Energy Technology Data Exchange (ETDEWEB)

Reports by U.S. workers on geodetic measurements of recent plate motions or crustal deformation published in 1987-1990 are reviewed. The review begins with global plate motions, proceeds through plate boundaries in California, Alaska, and the Pacific Northwest, and finishes with volcanic phenomena, monument stability and longevity, and GPS relative position measurements. 184 refs.

1991-01-01

160

Quantum deformation of BRST algebra  

International Nuclear Information System (INIS)

We investigate the q-deformation of the BRST algebra, the algebra of the ghost, matter and gauge fields on one spacetime point using the result of the bicovariant differential calculus. There are two nilpotent operations in the algebra, the BRST transformation #delta#_B and the derivative d. We show that one can define the covariant commutation relations among the fields and their derivatives consistently with these two operations as well as the *-operation, the antimultiplicative inner involution. (orig.).

1993-01-01

161

Grain boundaries structure and mechanical properties of aluminium alloys  

Energy Technology Data Exchange (ETDEWEB)

The paper discusses the problem of influence of grain boundaries structure on mechanical properties of aluminium alloys at elevated temperatures. Showed the data amount of grain boundaries close to special and a random of grain boundaries. The results of calculation of contribution of different mechanisms of deformation to the total deformation for alloys with different types of grain boundaries are given. (orig.)

1996-08-01

162

Effect of #beta#_4 deformations on decoupled rotational bands in odd-A nuclei  

International Nuclear Information System (INIS)

Calculations for a single-j nucleon coupled to an axially symmetric core with both #beta#_2 and #beta#_4 deformation have been performed for "1"8"7Ir. Using #beta#_4=-0.08, consistent with previously measured and predicted values of #beta#_4, the calculated spectrum is competitive with recent calculations assuming an asymmetric core.

163

Dynamic Deformation and Recovery Response of Red Blood Cells to a Cyclically Reversing Shear Flow: Effects of Frequency of Cyclically Reversing Shear Flow and Shear Stress Level  

UK PubMed Central (United Kingdom)

Dynamic deformation and recovery responses of red blood cells (RBCs) to a cyclically reversing shear flow generated in a 30-μm clearance, with the peak shear stress of 53, 108,...Full Text Available

2006-09-01

164

Differences of the deformation parameter #beta# for 2"+_1 states of even-even spherical nuclei from electromagnetic excitation and proton scattering  

International Nuclear Information System (INIS)

Differences of the deformation parameters for the 2"+_1 states of even-even spherical nuclei extracted from electromagnetic excitation #beta#sup(em)_2 and from proton scattering #beta#sup(pp')_2 are discussed. It is found that the ratio #beta#sup(pp')_2/#beta#sup(em)_2 is equal to about unity and that there is a small isotope dependence for several incomplete shell nuclei. (orig.).

165

Study on seismic stability of seawall in man-made island. Pt. 4. Deformation analysis of seawall during earthquake by DEM-FEM coupled analysis method (SEAWALL-2D)  

Energy Technology Data Exchange (ETDEWEB)

In the development of the man-made island siting technology of nuclear power plants, assessing the stability of the seawall against large ocean waves and earthquakes is indispensable. Concerning with the seismic stability of the seawall, prediction of the deformation like sliding and settlement of the seawall during earthquake including the armour units in front of the caisson becomes important factor. For this purpose, the authors have developed the two-dimensional DEM-FEM coupled analysis method (SEAWALL-2D) to predict the deformation of the seawall covered with the armour units during earthquake. In this method, movements of the armour units are calculated in DEM analysis part and deformation of the caisson, rubble moundsand seabed and back fill are calculated in FEM analysis part taking the nonlinearity of the soil materials based on the effective stress into account. Numerical simulations of dynamic centrifuge model ...

1999-02-01

166

High temperature deformation behavior of AZ31 Mg alloy  

Energy Technology Data Exchange (ETDEWEB)

High temperature deformation behavior of AZ31 Mg alloy was investigated in this study on the basis of a processing map ({epsilon} {approx} 0.6). To construct a processing map, compression tests were carried out at various temperatures and strain rates. Two regions of high deformation efficiency ({eta}) were identified as: (1) a dynamic recrystallization (DRX) domain at 250 C and 1/s and (2) a superplasticity domain at 450 C and 10{sup -4}/s. The average grain size observed in the DRX region was considerably smaller (2.9{mu}m) than in any other region. In the superplastic condition, tensile elongation to failure approached to 1040%. At the high Z regions, flow softening occurred resulting from the dynamic recrystallization but below 10{sup 10} of Z value, flow hardening occurred due to the grain growth. Possible deformation mechanisms operating at high temperature were discussed in relation to the activation energy. A ...

2005-07-01

167

The Relationship between the Microstructure and Age Hardening Response in the Metastable Beta Titanium Alloy Ti-11.5Mo-6Zr-4.5Sn (Beta III).  

Science.gov (United States)

The effect of solution treatment temperature and oxygen content on the microstructure and age hardening response of the metastable beta alloy Ti-11.5Mo-6Zr-4.5Sn have been studied. Kinetics of formation of the equilibrium alpha-phase and the metastable om...

1977-01-01

168

Microstructural modifications and high-temperature strength of monocrystalline nickel-base superalloys  

Energy Technology Data Exchange (ETDEWEB)

The examples discussed demonstrate that in order to improve further the high-temperature strength properties of (monocrystalline) nickel-base superalloys, it is expedient to follow two parallel routes, namely alloy development, on the one hand, and suitable modifications of the microstructure by appropriate thermal and mechanical treatments, on the other hand. (orig.)

2000-07-01

169

Microstructural evolution in several casts of alloy 800 during creep tests  

International Nuclear Information System (INIS)

The creep behaviour of different casts of Alloy 800, supplied by different sources, has been determined in multispecimen furnaces at 650, 750 and 800"0C and at different stress levels up to about 14,000 hs; the environment was initially helium and then air. The microstructural investigations were carried out by transmission electron microscopy. (Auth.).

170

Magnetization and magnetostriction curves for highly magnetostrictive materials  

Energy Technology Data Exchange (ETDEWEB)

The macroscopic behavior of magnetostrictive materials results from domain evolutions occurring at a microscopic scale. The author shows how to compute magnetization and magnetostriction curves by appraising the behavior of the underlying microstructures. The method hinges on an averaging device (Young measures), which allows one to pass from the microscopic to the macroscopic scale. He takes into account the kinematical constraints on the accommodation of elastic effects, and he highlights the role of material symmetry in the selection of energetically optimal microstructures.

1994-12-31

171

Analysis of microstructure of materials using a combination of a focused ion beam and transmission electron microscopy  

Energy Technology Data Exchange (ETDEWEB)

Recent development in application of a focused ion beam (FIB) technique to preparation of thin foil specimens for transmission electron microscopy (TEM) observation has been reviewed. Combined technique of FIB/TEM enables one to analyze those microstructures which have been almost impossible or very difficult to analyze so far. (author)

2002-03-01

172

Microstructure and mechanical properties of a high strength bearing steel SAE 52100 produced by spray deposition; Gefuege und mechanische Eigenschaften eines durch Spruehkompaktieren hergestellten Stahles 100Cr6  

Energy Technology Data Exchange (ETDEWEB)

Spray depositing allows the production of steels having a structure which is free of any macro-segregation, homogeneous and equiaxed. Nevertheless the spray deposition of steels shows some effects that have to be regarded as disadvantages. A porous region at the billet border and a rather coarse-grained microstructure can be noticed. As a result, in the presented work the influence of a subsequent hot rolling and a following heat treatment on microstructure and mechanical properties has been investigated. For this purpose the bearing steel SAE 52100 has been used as master material. The initial microstructure has been transformed to a homogeneous equiaxed fine-grained pearlitic microstructure without any remaining porosity. To get use of the characteristic properties of this high-strength steel an isothermal bainitic hardening has been carried out. Information about the mechanical properties of this ...

2001-07-01

173

Microstructural evolution of WC-Co alloys  

Energy Technology Data Exchange (ETDEWEB)

The microstructural development and grain-coarsening behavior of WC-Co alloys, with and without a VC additive, were investigated. The primary goal was to determine the mechanism through which VC acts as a grain-growth inhibitor. The study involved long-time sintering experiments (1 to 100 hours) on fully dense material, nascent stage sintering (90 to 1,320 seconds) starting with the green compact, and surrogate liquid phase experiments to characterize the WC powder prior to sintering. Quantitative microstructural analysis using intercept length distributions was performed for the long-term sintering. The nascent stage experiments involved the measurement of the specific surface area (S{sub v}) of each type of interface separately allowing the determination of the contribution of each developing entity to the overall microstructural evolution. The VC addition has been found to enhance the breakup of multigrained particles in ...

1991-01-01

174

Microstructural evolution of WC-Co alloys  

International Nuclear Information System (INIS)

The microstructural development and grain-coarsening behavior of WC-Co alloys, with and without a VC additive, were investigated. The primary goal was to determine the mechanism through which VC acts as a grain-growth inhibitor. The study involved long-time sintering experiments (1 to 100 hours) on fully dense material, nascent stage sintering (90 to 1,320 seconds) starting with the green compact, and surrogate liquid phase experiments to characterize the WC powder prior to sintering. Quantitative microstructural analysis using intercept length distributions was performed for the long-term sintering. The nascent stage experiments involved the measurement of the specific surface area (S_v) of each type of interface separately allowing the determination of the contribution of each developing entity to the overall microstructural evolution. The VC addition has been found to enhance the breakup of multigrained particles in the ...

175

Local composition analysis of SiC microstructures formed by ion projection in silicon using energy filtered TEM in combination with FIB specimen preparation  

International Nuclear Information System (INIS)

Buried silicon carbide (SiC) microstructures with lateral dimensions in the #mu#m range were formed by high-dose projection of 1.5 MeV C"2"+ ions in Si(100) at different doses and temperatures and subsequent annealing for 10 h at 1250 deg. C. Sections of individual SiC microstructures were prepared for cross-sectional transmission electron microscopy (TEM) analysis using a focused ion beam (FIB). Besides the possibility to select an individual microstructure, the FIB technique has the advantage of producing specimen foils of uniform thickness. Therefore, it was possible to map the carbon concentration of microstructures by energy filtered TEM (EFTEM) using the C_K absorption edge without the need of any sample thickness correction. Local overstoichiometric (>50%) carbon concentrations are shown to be correlated to the formation of an amorphous phase in the SiC and to significant swelling visible at ...

2003-09-15

176

Influence of microstructural characteristics on the mechanical properties of silicon nitride with Al{sub 2}O{sub 3}, Y{sub 2}O{sub 3} and Nd{sub 2}O{sub 3} as sintering aids  

Energy Technology Data Exchange (ETDEWEB)

Silicon nitride based ceramics have attracted considerable attention as good candidates for structural applications due to their excellent mechanical properties including strength, hardness, fracture toughness, and high temperature strength. These properties are strongly influenced by grain size and morphology, and by the degree of crystallinity and chemistry of grain boundary phases. In this work, the microstructure of Si{sub 3}N{sub 4} densified with Nd{sub 2}O{sub 3}, Y{sub 2}O{sub 3} and Al{sub 2}O{sub 3} sintering additives was studied. Sintered samples were polished and plasma etched for microstructural analysis using scanning electron microscope. Quantitative evaluation of materials microstructure was accomplished using Quantikov software. Fracture toughness was measured by Vickers indentation method. The observed microstructure is typical of silicon nitride based materials and is characterized ...

2003-07-01

177

cap alpha. decay of fission isomers  

Energy Technology Data Exchange (ETDEWEB)

The theory of ..cap alpha.. decay in first-order perturbation theory is presented. The theory is designed for a strongly deformed nucleus in an isomeric state which changes its deformation dynamically through decay from a very deformed to an almost spherical shape. It is shown that other channels are not coupled to the ..cap alpha.. channel in first-order perturbation theory. The collective degrees of freedom of the daughter nucleus are described by shape vibrational states, eigenstates of a Hamiltonian whose potential has two minima. The parent nucleus is described by dynamically coupling the vibrational degrees of freedom to the ..cap alpha..-particle motion and also taking rotations into account. The ..cap alpha.. particle is taken to be a point-like particle. The theory is applied to the ..cap alpha.. decay of the isomeric state of /sub 95//sup 242/Am.

1984-10-01

178

Split anterior tibial tendon transfer for varus equinus spastic foot deformity  

British Library Electronic Table of Contents (United Kingdom)

Spastic equinovarus foot deformity commonly occurs after stroke or head trauma. Management by split anterior tibial tendon transfer to the lateral border of the foot was chosen by the authors. The purpose of that work was to assess the reliability of this method to improve patient's functional autonomy and investigate the relationship between the initial clinical examination findings and the quality of the functional results. 84 feet, operated in 82 patients out of 130, of mean age 46 years, were reviewed at a mean follow-up of 65 months. Very few complications were observed. Toe deformities remain a commonly associated problem. 80 patients were able to walk barefoot, 74 reported an increase in their walking distance, and 73 could regularly wear normal shoes. There is a strong relationship...

2011-01-01

179

Pressure-induced structural transitions in multi-walled carbon nanotubes  

British Library Electronic Table of Contents (United Kingdom)

We demonstrate a novel cross-sectional deformation, called the radial corrugation, of multi-walled carbon nanotubes (MWNTs) under hydrostatic pressure. Theoretical analyses based on the continuum elastic approximation have revealed that MWNTs consisting of more than ten concentric walls undergo elastic deformations at critical pressure Formula Not Shown , above which the circular shape of the cross-section becomes radially corrugated. Various corrugation modes have been observed by tuning the innermost tube diameter and the number of constituent walls, which is a direct consequence of the core-shell structure of MWNTs. Cross-sectional views of MWNT under high hydrostatic pressure: elliptic deformation with the mode index n = 2 (left), and radial corrugations with n = 5 (center), and n = 6 ...

2009-01-01

180

Numerical modeling of a MEMS actuator considering several magnetic force calculation methods  

British Library Electronic Table of Contents (United Kingdom)

Purpose - The purpose of this paper is to investigate the accuracy of different force calculation methods and their impact on mechanical deformations. For this purpose, a micrometer scaled actuator is considered, which consists of a micro-coil and of a permanent magnet (PM) embedded in a deformable elastomeric layer. Design/methodology/approach - For the magnetic field evaluation a hybrid numerical approach (finite element method/boundary element method (FEM/BEM) coupling and a FEM/BEM/Biot-Savart approach) is used, whereas FEM is implemented for the mechanical deformation analysis. Furthermore, for the magneto-mechanical coupling several force calculation methods, namely the Maxwell stress tensor, the virtual work approach and the equivalent magnetic sources methods, are considered and co...

2011-01-01

181

Hydrogen effect on the deformation and annealing textures in the #beta# titanium alloy VT35  

International Nuclear Information System (INIS)

A study is made into textures of deformation and primary recrystallization forming in a #beta#-titanium alloy doped with hydrogen in amounts from 0.04 to 0.55 mass. %, on cold rolling with a 70%-reduction and dehydrogenating annealing at 860 deg C. It is shown that a volume fraction of recrystallization texture components is determined by the nature of corresponding deformation texture, in its turn, depending on hydrogen concentration in the alloy. At low hydrogen contents the main texture components are #left brace#111#right brace# and #left brace#001#right brace#. A hydrogen content increase up to 0.09 - 0.18 mass. % results in formation of dominant components of #left brace#111#right brace# and #left brace#112#right brace#

2003-12-01

182

High temperature deformation behaviour of Ti-10V Alloy and associated activation energy  

International Nuclear Information System (INIS)

High temperature deformation behaviour of an experimental Beta-titanium alloy Ti-10V has been studied in the temperature range 800 to 945 degree C by using the method of crosshead speed cycling. Although subgrain formation was observed but the alloy did not exhibit superplastic behaviour in the entire temperature range studied. A very large initial grain size and elongation of grains during the deformation are considered the main factors responsible for absence of superplastic behaviour. The activation energy values for regions II and III of the ln sigma vs. ln small epsilon plots are close to the lower of the two activation energy values proposed together to describe self diffusion in beta-phase suggesting that the rate controlling mechanism is that for lattice diffusion rather then grain boundary diffusion. (author)

2004-06-01

183

GIS for combined storage and analysis of data from terrestrial and synthetic aperture radar remote sensing deformation measurements in hard coal mining  

British Library Electronic Table of Contents (United Kingdom)

In this paper we demonstrate the capabilities of our ArcGIS-based software development that includes an adapted database system and a GIS tool for storage, combined analysis and visualization of leveling data and interferometric synthetic aperture radar (SAR) deformation measurements. Preprocessed remote sensing image data are stored with metadata that include all processing routines and parameters. This allows reproduction and traceability of all processing steps. Deformation monitoring is supported through data searching and selection based on a variety of criteria. A methods toolbox allows spatio-temporal analyses for points, lines and areas (e.g. subsidence basins) in a graphical manner.

2011-01-01

184

Effect of defect local piles and dislocation multiplication on radiation hardening of metals  

International Nuclear Information System (INIS)

Computer experiments imitating specimen strain on tension with constant deformation rate have been carried out. A formation possibility of atmosphere from defects around gliding dislocations (I) and a work of Frank-Read sources (II) have been accounted for. In result deformation curves until stresses do not exceed a critical shear stress were calculated. Influence of effects (I) and (II) was analyzed. It is determined that both by pass of dislocations over defect ''atmospheres'' and dislocation multiplication can cause a peak in flow stress occurrence on the deformation curves. Reasons and conditions of such peak occurrence have been studied. 12 refs.; 9 figs. (author).

1990-05-22

185

Activation energy for high temperature deformation of Ti-10V alloy on the basis of second strain rate cycles  

International Nuclear Information System (INIS)

Activation energy values for high temperature deformation of a beta -titanium alloy Ti-10V were determined from the flow stress strain rate data taken from the second increasing strain rate cycles, in order to find the rate controlling mechanism. Although the data obtained from first increasing strain rate cycles are considered most appropriated by the author in a previous study due to obvious reasons, the values obtained in present work are again indicative of lattice self diffusion in beta -phase as the rate controlling mechanism for this alloy and nevertheless suggest that two different activation energy values for a deformation process could be possible in a given temperature range, depending upon the data. (author)

2007-12-01

186

Similarities and differences of microstructure and macro properties between portland and blended cement  

Energy Technology Data Exchange (ETDEWEB)

The relationship between microstructure and macro properties of different cementitious materials has been investigated. This study consists of the following tasks: using NMR and IR to better characterize the amorphous and poorly crystalline phases that occur in blended cements; characterizing the microstructure of the hydration products of modified Portland cement as a function of different percentages of pozzolan replacements by ESEM, SEM, and EDS; comparing the properties of blended cement pastes with a control group of normal Portland cements; and studying the engineering aspects of blended cement that are important for identifying and characterizing fundamental phenomena that are responsible for their durability. The overall influence of the nanoscale and microscale structure of blended and Portland cement on the properties of the resultant composite will be discussed.

1997-10-01

187

Pitting susceptibility of a pipeline steel with banded microstructure of martensite, ferrite and pearlite  

International Nuclear Information System (INIS)

Early failure of an induction-hardening carbon steel pipe, which was used to transport tailing slurry, was caused by pitting corrosion. The microstructure on the internal pipe surface layer was found being a mixture of martensite, pearlite and ferrite. In this work, the pitting corrosion behavior of each constitute in the microstructure of steel is investigated with electrochemical noise analyses; the electronic properties of passive films were studied with Mott-Schottky relationship. It is found that the passive films formed on the materials under investigation are highly disordered n-type semiconductors. The high-to-low pitting susceptibility is ferrite > martensite > pearlite. The pitting resistance is related to the semiconductive nature of the passive film formed on each constitute. The pitting susceptibility increases with the donor concentration in the passive films. (author)

2003-08-24

188

Morphology evolution of Ir-Nb-X (X = Hf, Ta, or Ti) ternary alloys  

Energy Technology Data Exchange (ETDEWEB)

The microstructure evolution of nine samples from three Ir-base ternary systems, Ir-Nb-Hf, Ir-Nb-Ta, and Ir-Nb-Ti, was investigated by microstructure observation using scanning electron microscopy (SEM), composition map-analysis using electron probe microscopy analysis (EPMA), and phase determination using X-ray diffraction (XRD) patterns. The fcc/L1{sub 2} two-phase structure was detected in all the samples. Lattice misfits between fcc and L1{sub 2} phases were calculated. Ir-Nb-Ta and Ir-Nb-Ti alloys exhibited a microstructure quite similar to that of Ni-base superalloys, and the cuboidal L1{sub 2} precipitates in Ir-Nb-Ta and Ir-Nb-Ti alloys could maintain up to 1900 {sup o}C.

2007-01-31

189

Microstructure and mechanical behaviour of an elevated temperature Mg-rare earth based alloy  

International Nuclear Information System (INIS)

AM-SC1 is a heat treatable magnesium alloy that has been specifically developed to achieve the elevated temperature strength and creep properties necessary for engine block applications. This paper describes the interrelationship between the microstructure and the mechanical properties of AM-SC1. The compressive and tensile strengths are relatively insensitive to temperature up to and including 450 K and the tensile yield behaviour deviates from a standard Hall-Petch relationship at grain sizes below 200 ?m. The microstructural features contributing to the creep resistance are both inter- and intra-granular in nature and are on length scales from nanometers to micrometers. The creep behaviour at 423 K and 450 K is diffusion controlled, with any contribution from the grain boundaries being negligible.

2009-04-15

190

Microstructural features in sintered Si_3N_4/SiC platelets systems  

International Nuclear Information System (INIS)

Analytical TEM and high resolution TEM were used in the microstructural characterization of hot-press sintered Si_3N_4-SiC platelets composites. The quantity of sintering additives, Er_2O_3 and AlN, was varied to produce different matrices, e. g. Si_3N_4, #beta#'+#alpha#'-Sialon and #alpha#'-Sialon. Detailed analysis of platelet-sialon matrix interfaces revealed the presence of AlN polytypoids. The polytypoids nucleate preferentially onto the (0001) plane of SiC and growth epitaxially in several ten nanometer layers contributing in this way to crystallize, partially, the matrix intergranular glass pockets contacting the platelets. Possible applications of the phenomena to microstructural control, grain boundary phase control and enhanced creep resistance are discussed. (orig.).

1993-10-04

191

Microstructural characteristics and creep rupture behavior of electron beam and laser welded AISI 316L stainless steel  

Energy Technology Data Exchange (ETDEWEB)

AISI 316L stainless steel was welded by the electron beam (EB) and laser techniques. Microstructural characteristics, hardness profile, creep rupture properties and creep damage of the welds were investigated. Fully austenitic microstructure was obtained in the two welds. The solidification structure of the welds consisted of the cellular and equiaxed dendrites. The creep rupture lives of the two welds were almost the same, and they were reduced by a factor of about two compared to the base metal. Moreover, the rupture elongation of the welds was lower than that of the base metal. Creep damage was observed in the ``parting`` region of the welds and in the heat-affected zone (HAZ), respectively. Final creep fracture occurred in the ``parting`` region of the welds. (orig.).

1995-12-01

192

Microstructural characteristics and creep rupture behavior of electron beam and laser welded AISI 316L stainless steel  

International Nuclear Information System (INIS)

AISI 316L stainless steel was welded by the electron beam (EB) and laser techniques. Microstructural characteristics, hardness profile, creep rupture properties and creep damage of the welds were investigated. Fully austenitic microstructure was obtained in the two welds. The solidification structure of the welds consisted of the cellular and equiaxed dendrites. The creep rupture lives of the two welds were almost the same, and they were reduced by a factor of about two compared to the base metal. Moreover, the rupture elongation of the welds was lower than that of the base metal. Creep damage was observed in the ''parting'' region of the welds and in the heat-affected zone (HAZ), respectively. Final creep fracture occurred in the ''parting'' region of the welds. (orig.).

193

Influence of annealing on the microstructure of commercial Mg alloy AZ31 after mechanical forming  

International Nuclear Information System (INIS)

The microstructure of commercial rolled magnesium alloy AZ31B (nominal composition Mg-3Al-0.9Zn-0.15Mn in wt.%) was investigated with the help of light microscopy, electron backscatter diffraction (EBSD) and X-ray diffraction technique after annealing in the temperature range from room temperature (RT) to 400 deg. C. Tensile tests at RT were performed to show the influence of the microstructure on mechanical properties. Static recrystallization (SRX) was observed during annealing of as-received alloy at and above 150 deg. C. Twins play an important role during SRX and serve as nucleation sites and preferred paths for growth of grains. The strong basal texture caused by rolling was weakened by SRX. Significant differences in the stress strain curves were observed for as-received and annealed specimens.

2006-09-25

194

Formation of Bimodal-Sized Structure and Its Tensile Properties in a Warm-Rolled and Annealed Ultrafine-Grained Ferrite/Cementite Steel  

British Library Electronic Table of Contents (United Kingdom)

An ultrafine-grained ferrite/cementite (UGF/C) steel with a local high density of cementite particles was fabricated through caliber-warm-rolling followed by annealing and resulted in a bimodal-sized microstructure. The characteristic bimodal-sized microstructure was attributed to the original ferrite-pearlite structure and cementite spacing, and reflected the original ferrite-pearlite structure. The smaller-sized clusters corresponded to the former pearlite regions and the larger-sized clusters to the proeutectoid ferrite regions. The cementite particles naturally localized within the former pearlite region. Most of the ferrite coarsening did not occur until the cementite particle spacing reached a critical value. The UGF/C microstructure with a bimodal grain size showed a yield strength ...

2008-01-01

195

Effect of hydroxyapatite content on the microstructure, thermal and mechanical properties of Ti-based glassy alloy/hydroxyapatite composite prepared by spark plasma sintering  

British Library Electronic Table of Contents (United Kingdom)

In the present paper, the effects of hydroxyapatite (HA) content on the microstructure, thermal and mechanical properties of Ti-based glassy alloy/HA composite prepared by spark plasma sintering (SPS) are investigated. The microstructure of the composites is homogeneous when the HA is lower than 2 wt%. When the HA content is higher than 3 wt%, the crystalline precipitates with size of less than 5 nm are distributed in the glassy matrix. HA decomposes during sintering procedure for the composite with high HA content. With increasing HA addition, compressive strength decreases. Especially for the HA content is over 2 wt%, the strength decreases sharply because of partial crystallization of glassy alloy matrix.

2011-01-01

196

Bonding and microstructural stability in Ni55Ti45 studied by experimental and theoretical methods  

Energy Technology Data Exchange (ETDEWEB)

Spiral orbit tribometry friction tests performed on Ni-rich Ni55Ti45 titanium ball bearings indicate that this alloy is a promising candidate for future aerospace bearing applications. Microstructural characterization of the bearing specimens was performed using transmission electron microscopy and energy dispersive spectroscopy, with NiTi, Ni4Ti3, Ni3Ti, and Ni2Ti4Ox phases identified within the microstructure of the alloy. Density functional theory was applied to predict the electronic structure of the NixTiy phases, including the band structure and site projected density of states. Ultraviolet photoemission spectroscopy was used to verify the density of states results from the density functional theory calculations, with good agreement observed between experiment and theory.

2010-11-25

197

Thermal dislocation depinning in a deformed crystal  

Energy Technology Data Exchange (ETDEWEB)

The temperature dependence of the dislocation mobility threshold is investigated on the basis of a dislocation model suggested by Frenkel-Kontorova. The critical value is obtained for the stress/temperature, corresponding to the dislocation depinning from its equilibrium position. The universal behaviour of a barrier height at finite stress and temperature is revealed and investigated.

2008-01-14

198

Safety and efficacy of botox injection in alleviating post-operative pain and improving quality of life in lower extremity limb lengthening and deformity correction  

UK PubMed Central (United Kingdom)

BackgroundDistraction osteogenesis is the standard treatment for the management of lower limb length discrepancy of more than 3 cm and bone loss secondary to congenital anomalies,...Full Text Available

199

SEGMENTING CT PROSTATE IMAGES USING POPULATION AND PATIENT-SPECIFIC STATISTICS FOR RADIOTHERAPY  

UK PubMed Central (United Kingdom)

This paper presents a new deformable model using both population and patient-specific statistics to segment the prostate from CT images. There are two novelties in the proposed method. First,...Full Text Available

2009-08-07

200

Role of surface degrees of freedom in grazing heavy ion collisions  

Energy Technology Data Exchange (ETDEWEB)

A survey is given of the influence of surface deformations on heavy ion reactions. Emphasis is put on the effect of zeropoint fluctuations in the entrance channel and on the effect on grazing collisions in terms of an imaginary part of the scattering potential.

1983-11-14

201

Role of surface degrees of freedom in grazing heavy ion collisions  

International Nuclear Information System (INIS)

A survey is given of the influence of surface deformations on heavy ion reactions. Emphasis is put on the effect of zeropoint fluctuations in the entrance channel and on the effect on grazing collisions in terms of an imaginary part of the scattering potential. (orig.).

202

Retrosternal Percutaneous Tracheostomy: An Approach for Predictably Impossible Classic Tracheostomy  

UK PubMed Central (United Kingdom)

Percutaneous tracheostomy is a routine procedure in intensive care units. In cases of very low position of the larynx, cervical spine deformation, morbid obesity, or neck tumor, performance of the classic...Full Text Available

2010-01-01

203

Research on deformation characteristic of AZ31Mg alloy and its constitutive equations  

Energy Technology Data Exchange (ETDEWEB)

Superplasticity of polycrystalline metallic materials is a phenomenon which shows hundreds to thousands of percents of large plastic deformation without necking in a steady state of low stress, when the uni-axial tensile loading is done in some special thermo-mechanical conditions (some limited ranges of properly high temperature and low strain rate). The main mechanism of superplastic phenomenon is the grain boundary sliding, while the main mechanism of usual plastic deformation is the trans-granular sliding. In this research, the possibility of superplastic deformation in a magnesium alloy (AZ31Mg alloy) was experimentally investigated, because generally speaking, the magnesium alloy whose atomic structure is hexagonal does not have enough formability in a form of trans-granular sliding mechanism. In this paper, the detail of experimental results are shown and discussed. Moreover, the constitutive equations of Mg alloy ...

2004-07-01

204

Relativistic mean field theory and applications in finite nuclei  

Energy Technology Data Exchange (ETDEWEB)

Relativistic mean field (RMF) theory is applied to modern problems of nuclear structure, such as the description of rotating bands in super-deformed nuclei or the investigation of neutron halos in light exotic nuclei. (orig.)

1997-05-01

205

Quantifying the accuracy of automated structure segmentation in 4D CT images using a deformable image registration algorithm  

UK PubMed Central (United Kingdom)

Four-dimensional (4D) radiotherapy is the explicit inclusion of the temporal changes in anatomy during the imaging, planning, and delivery of radiotherapy. One key component of 4D radiotherapy planning...Full Text Available

2008-04-01

206

Performance evaluation of an automatic anatomy segmentation algorithm on repeat or four-dimensional CT images using a deformable image registration method  

UK PubMed Central (United Kingdom)

PurposeAuto-propagation of anatomical region-of-interests (ROIs) from the planning CT to daily CT is an essential step in image-guided adaptive radiotherapy. The...Full Text Available

2008-09-01

207

New deformation mechanisms in fine-grain Mg alloys  

Energy Technology Data Exchange (ETDEWEB)

Deformation mechanisms were investigated in fine-grain (d=7 {mu}m) AZ31 Mg alloy in order to understand their excellent room-temperature ductility. Dislocation cross slip from basal to non-basal planes was found to occur easily at room temperature at a plastic anisotropy factor of only 1.5 instead of several tens to 100 expected from the single crystal CRSS data. Enhanced grain-boundary sliding (GBS) was also found to occur at room temperature. The contribution of GBS strain was found to be approximately 8% of total strain. The enhanced activity of non-basal dislocation slip and GBS was attributed to grain-boundary compatibility effects. Moreover, dynamic recovery was found to occur during deformation at room temperature associated with the formation of recovery twins and small-angle grain boundaries. The occurrence of these deformation mechanisms at room temperature was considered to be a major reason for an excellent ...

2003-07-01

208

Multiple neural tube defects in the same patient with no neurological deficit  

UK PubMed Central (United Kingdom)

Congenital deformities involving the coverings of the nervous system are called neural tube defects (NTDs). NTD can be classified as neurulation defects, which occur by stage 12, and postneurulation...Full Text Available

2010-01-01

209

MR findings in acute Lyme disease affecting the knee. A case report  

Energy Technology Data Exchange (ETDEWEB)

In this paper we report a case with primarily unspecific arthralgia after surgical therapy of hallux valgus deformity and consecutive reflex sympathetic dystrophy in which MR led to the diagnosis of Lyme disease. (orig.)

2002-07-01

210

Localized deformation and IASCC initiation in austenitic stainless steels  

International Nuclear Information System (INIS)

Localized deformation may play a key role in the underlying mechanism of irradiation assisted stress corrosion cracking (IASCC) in light water reactor core components. In this study, four austenitic alloys, 18Cr8Ni, 15Cr12Ni, 13Cr15Ni and 21Cr32Ni, with different stacking fault energies were irradiated to 1 and 5 dpa at 360 deg. C using 3.2 MeV protons. Interrupted constant extension rate tensile (CERT) tests were conducted in a simulated BWR environment to determine IASCC susceptibility. In order to characterize the localized deformation in slip channels and grain boundaries, parallel CERT experiments were also performed in an argon atmosphere. Results show that the IASCC susceptibility of the tested alloys increases with increasing irradiation dose and decreasing stacking fault energy. IASCC tends to initiate at locations where slip channels intersect grain boundaries. Localized deformation in the form of grain boundary ...

2008-12-01

211

Lifetimes of superdeformed nuclei in the mass region A {approx}150 with the Eurogam multidetector array; Durees de vie de noyaux superdeformes de la region de masse A {approx}150 mesurees avec le multicompteur Eurogam  

Energy Technology Data Exchange (ETDEWEB)

This work concerns the study of the nuclear superdeformation phenomenon in the rare earth region (A {approx} 150). The superdeformed (SD) states in Gadolinium and Dysprosium isotopes were produced via heavy-ion induced reactions and studied with the (EUROGAM EUROpean GAmma-ray Microscope) gamma multidetector array. Precise level attenuation method (DSAM). From the derived quadrupole moments, we find large differences in deformation between the yrast bands in neighbour nuclei explained in terms of the case of nuclei corresponding to an axis ratio of 2:1, the shell gaps are not fixed at a specific particle number and deformation. Furthermore the present results indicate that the deformations associated with identical bands are different supporting the picture that mass and deformation changes tend to compensate in SB bands with the same moments of inertia. (author). 114 refs.

1996-05-13

212

Induction of mortality and malformation in Xenopus laevis embryos by water sources associated with field frog deformities.  

UK PubMed Central (United Kingdom)

Water samples from several ponds in Minnesota were evaluated for their capacity to induce malformations in embryos of Xenopus laevis. The FETAX assay was used to assess the occurrence of malformations...Full Text Available

1998-12-01

213

In-pile measurements of fuel rod deformation and verification of the finite element model FEMAXI  

International Nuclear Information System (INIS)

For safety evaluations and licensing procedures, fuel rod performance is predicted through model calculations. Due to the complexity of fuel rod performance and the insufficient availability of experimental data, such calculations necessarily reflect inaccuracies and conservatism. For verification and development of more realistic models and submodels, acquisition of reliable on-line data on fuel rod performance characteristics is imperative. The present paper describes the instruments and equipment applied in the Halden Reactor for on-line measurements of fuel rod and assembly power and power distribution, and fuel rod axial and diameter deformation. Recent results from evaluation of such fuel rod deformation measurements, covering fuel rods with different designs, subjected to various modes of operation, including startup ramps, steady state, and power shock, are presented. It is also shown how these data are used for verification and ...

1976-09-13

214

Grain refinement in magnesium alloy AZ31 during hot deformation  

Energy Technology Data Exchange (ETDEWEB)

The deformation behavior and structure changes of magnesium alloy AZ31 were studied in compression at temperatures ranging from 523 K to 673 K and at a strain rate of 3 x 10{sup -3} s{sup -1}. They depend sensitively on deformation temperature. At high temperatures, grain fragmentation takes place due to frequent formation of kink bands initially at corrugated grain boundaries and then in grain interiors, followed by full development of new grains in high strain. At lower temperatures, in contrast, twinning takes place in rather coarse grains and kink bands are formed mainly in finer original ones in low strain. It is concluded that new grain evolution can be controlled by a deformation-induced continuous reaction resulting in grain fragmentation by kink bands, i.e. continuous dynamic recrystallization (cDRX). The latter is discussed comparing with conventional, i.e. discontinuous, DRX. (orig.)

2004-07-01

215

Fixation Techniques for Split Anterior Tibialis Transfer in Spastic Equinovarus Feet  

UK PubMed Central (United Kingdom)

Equinovarus of the foot is the most common lower extremity deformity following traumatic brain injury. We evaluated outcomes of the split anterior tibialis tendon transfer (SPLATT) for correction of...Full Text Available

2008-10-01

216

Evaluation of press formability in magnesium alloy  

Energy Technology Data Exchange (ETDEWEB)

A press formability of magnesium alloy sheet cannot be evaluated by only general characteristics in tensile test; tensile strength, elongation n-value and r-value. For example, AZ31-alloy elongates about 20% in room temperature but breaks easily at shallow stage in deep drawing, which is caused by little local elongation (local necking). Crystallographic restriction of slip deformation in this alloy produces high strength, which almost equal to macroscopic fracture strength. In press forming, the bending under high tension requires a large deformability. A great difference in the deformability between AZ31 magnesium alloy and a strain hardened A1100 Aluminum (only 5% in elongation) is shown by static bending test with V-notch. In a rolled plate of AZ31, a crack is produced by stress concentration and propagates with reduced load at all testing temperature up to 453 K. In contrast, the point of notch in A1100 is dulled by ...

2003-07-01

217

Electric-field-induced deformation of biological cells  

Energy Technology Data Exchange (ETDEWEB)

The cell is modeled as an ellipsoid with shell and the surface stress distribution calculated by means of the Maxwell Stress Tensor. The cell membrane is treated as incompressible material having both bending and shear energies of deformation. Employing the principle of virtual work, cell volume (and hence shape) is computed as a function of the external field strength and orientation with respect to the field. The following results were obtained: (1) The surface stresses that develop or the cell membrane are distributed having both normal and tangential components that act together to produce a rounding of the cell. (2) If the tangential component of the stress is ignored, then higher field strengths are needed to produce similar deformation (shape change) of cells. (3) The threshold value of the applied field, i.e, the field strength at which the volume (shape) of the cell changes abruptly, occurs at approximately 55V/cm. Above the threshold ...

1989-01-01

218

Effect of Particle Size on Compaction of Materials with Different Deformation Mechanisms with and without Lubricants  

UK PubMed Central (United Kingdom)

This work investigates the effect of excipient particle size on compaction properties of brittle, plastic and viscoelastic materials with and without added lubricants. Sieve cuts of Microcrystalline...Full Text Available

219

Discovering and mapping low-amplitude dislocations by employing radioscopy methods  

Energy Technology Data Exchange (ETDEWEB)

Methodologies are given for conducting studies to discover and map break deformations in coal strata using various modifications on radiometry, together with the field for their use. Results that were obtained using the IKS-50 device are given.

1981-01-01

220

Deformed Wing Virus Implicated in Overwintering Honeybee Colony Losses ?  

UK PubMed Central (United Kingdom)

The worldwide decline in honeybee colonies during the past 50 years has often been linked to the spread of the parasitic mite Varroa destructor and its interaction with certain honeybee...Full Text Available

2009-11-01

221

Deformation study of separator pellets for thermal batteries  

Energy Technology Data Exchange (ETDEWEB)

The deformation characteristics of pellets of electrolyte-binder (EB) mixes based on MgO were measured under simulated, thermal-battery conditions. Measurements (using a statistically designed experimental strategy) were made as a function of applied pressure, temperature, and percentage of theoretical density for four molten-salt electrolytes at two levels of MgO. The EB mixes are used as separators in Li-alloy thermal batteries. The electrolytes included LiCl-KCI eutectic, LiCl-LiBr-KBr eutectic, LiBr-KBr-LiF eutectic, and a LiCl-LiBr-LiF electrolyte with a minimum-melting composition. The melting points ranged from 313 C to 436 C. The experimental data were used to develop statistical models that approximate the deformation behavior of pellets of the various EB mixes over the range of experimental conditions we examined. This report, discusses the importance of the deformation response surfaces to thermal-battery design.

1995-05-01

222

Accelerated interleaflet transport of phosphatidylcholine molecules in membranes under deformation.  

UK PubMed Central (United Kingdom)

Biological membranes are lamellar structures composed of two leaflets capable of supporting different mechanical stresses. Stress differences between leaflets were generated during micromechanical experiments...Full Text Available

1996-09-01

223

A self-oscillating biophysical computer model of the elongated vocal fold  

UK PubMed Central (United Kingdom)

A new 3D model is developed to simulate the self-oscillation of the elongated vocal folds. This model allows for large deformation and longitudinal displacement. The displacement boundary condition...Full Text Available

2008-01-01

224

``Q-deformation and energy deficit in liquid helium phonon spectrum``  

Energy Technology Data Exchange (ETDEWEB)

The instability of the phonon spectrum in liquid Helium for T < 1 K is a well established experimental fact. We discuss the role of q-deformation as a possible mechanism to supply the energy deficit that forbidden one-phonon decay into two phonons when the constant {gamma} in the phonon anomalous dispersion relation ({omega}{sup ph} = c{sub 0} p(1 - {gamma}p{sup 2})) is positive, through the analysis of three-phonon processes in a q-phonons gas. (author). 19 refs.

1996-09-01

225

Wilson loops in warped resolved deformed conifolds  

CERN Document Server

We calculate quark-antiquark potentials using the relationship between the expectation value of the Wilson loop and the action of a probe string in the string dual. We review and categorize the possible forms of the dependence of the energy on the separation between the quarks. In particular, we examine the possibility of there being a minimum separation for probe strings which do not penetrate close to the origin of the bulk space, and derive a condition which determines whether this is the case. We then apply these considerations to the flavoured resolved deformed conifold background of Gaillard et al. We suggest that the unusual behaviour we observe in this solution is likely to be related to the IR singularity which is not present in the unflavoured case.

2011-01-01

226

The effect of ductile connectors on the behaviour of timber-concrete composite beams  

British Library Electronic Table of Contents (United Kingdom)

The load-carrying capacity and ultimate deformation capacity of timber-concrete composite systems can be significantly influenced by the ductility of the connection between the two materials. The use of more ductile connections can increase the load-carrying capacity of the composite system as well as its ultimate deformation capacity. In this work, the potential increase that might be expected for these two parameters due to the use of ductile connections will be assessed through numerical simulations, taking the non-linear behaviour of the connections into account. Furthermore, the connection ductility required to achieve the maximum load capacity depends on the mechanical properties of the connection as well as on the geometric and mechanical properties of the composite system. There ar...

2011-01-01

227

String theory, black holes, and SL(2,R) current algebra  

International Nuclear Information System (INIS)

We analyse in detail the SL(2, R) black hole by extending standard techniques of Kac-Moody current algebra to the non-compact case. We construct the elements of the ground ring and exhibit W_#infinity# type structure in the fusion algebra of the discrete states. As a consequence, we can identify some of the exactly marginal deformations of the black hole. We show that these deformations alter not only the spacetime metric but also turn on non-trivial backgrounds for the tachyon and all of the massive modes of the string. (orig.).

1993-05-01

228

Stress corrosion cracking of Alloy 600 using the constant strain rate test  

International Nuclear Information System (INIS)

Nuclear grade production tubing of Alloy 600 was evaluated for stress corrosion cracking (SCC) susceptibility in high purity water at 365, 345, 325, and 290 C. Reverse tube U-bend specimens provided crack initiation data and constant extension rate tests were employed to determine the crack velocities experienced in th crack propagation stage. Initial results indicate that a linear extrapolation of data received from high temperature tests can be used to predict the service life of steam generator tubing that has been plastically deformed or is continually deforming by ''denting.''.

229

Schematic model for the differences between neutron and proton quadrupole deformation parameters in open-shell nuclei  

Energy Technology Data Exchange (ETDEWEB)

The schematic model is extended to open-shell nuclei. The quasiparticle random-phase approximation plus core polarization are used to calculate multipole matrix elements M/sub n/ and M/sub p/. Calculated trends in the ratio of deformation parameters ..beta../sub n//..beta../sub p/ are compared with experimental ratios for several sets of isotopes and isotones. The systematics indicate a rather abrupt change toward equality of ..beta../sub n/ and ..beta../sub p/ when N or Z is changed from a closed-shell value.

1984-01-16

230

Relativistic mean field study of light nuclei  

International Nuclear Information System (INIS)

Bulk properties such as the binding energies, r.m.s. radii and deformation parameters are calculated for the light (Z=2-8) even-mass nuclei using deformed relativistic mean-field theory. A comparison between L1, NL1 and NL2 parameter sets are given. The effects of pairing for open-shell nuclei have been investigated. The calculation is extended to nuclei near the proton- and neutron-drip line. Reasonable agreement with experiment is achieved for NL1 and NL2 parameter sets. (orig.).

231

Posttraumatic tibia valga: a case demonstrating asymmetric activity at the proximal growth plate on technetium bone scan  

Energy Technology Data Exchange (ETDEWEB)

Posttraumatic tibia valga is a well-recognized complication following fracture of the upper tibial metaphysis in young children. We present a case of a child who developed a valgus deformity following fracture of the proximal tibia and fibula in which quantitative bone scintigraphy at 5 months after injury demonstrated increased uptake at the proximal tibial growth plate with proportionally greater uptake on the medial side. This finding suggests that the valgus deformity in this patient was due to a relative increase in vascularity and consequent overgrowth of the medial portion of the proximal tibial physis.

1987-07-01

232

Posttraumatic tibia valga: a case demonstrating asymmetric activity at the proximal growth plate on technetium bone scan  

International Nuclear Information System (INIS)

Posttraumatic tibia valga is a well-recognized complication following fracture of the upper tibial metaphysis in young children. We present a case of a child who developed a valgus deformity following fracture of the proximal tibia and fibula in which quantitative bone scintigraphy at 5 months after injury demonstrated increased uptake at the proximal tibial growth plate with proportionally greater uptake on the medial side. This finding suggests that the valgus deformity in this patient was due to a relative increase in vascularity and consequent overgrowth of the medial portion of the proximal tibial physis.

233

Nuclear tetrahedral configurations at spin zero  

CERN Document Server

The possibility of the existence of stable tetrahedral deformations at spin zero is investigated using the Skyrme-HFBCS approach and the generator coordinate method (GCM). The study is limited to nuclei in which the tetrahedral mode has been predicted to be favored on the basis of non self-consistent models. Our results indicate that a clear identification of tetrahedral deformations is unlikely as they are strongly mixed with the axial octupole mode. However, the excitation energies related to the tetrahedral mode are systematically lower than those of the axial octupole mode in all the nuclei included in this study.

2008-01-01

234

Effects of focused ion beam milling on the nanomechanical behavior of a molybdenum-alloy single crystal  

International Nuclear Information System (INIS)

Nanoindentation was performed on a Mo-alloy single crystal to investigate effects of focused ion beam (FIB) milling on mechanical behavior. On a non-FIB-milled surface, pop-ins were observed on all load-displacement curves corresponding to a transition from elastic to plastic deformation. Similar pop-ins were not detected on surfaces subjected to FIB milling. This difference indicates that FIB milling introduces damage that obviates the need for dislocation nucleation during subsequent deformation. A second effect of FIB milling is that it increased the surface hardness. Together, these effects could be the source of the size effects reported in the literature on micropillar tests.

2007-09-10

235

Dynamic stability and vibration monitoring for No. 9 mine, M-1 dump  

Energy Technology Data Exchange (ETDEWEB)

This study examines the effects of blasting on waste dumps at open pit mining operations. Of specific concern were mining operations at the base of a five hundred foot high waste dump such as the operation at the South Pit of the Smoky-River Coal Ltd. property near Grande Cache, Alberta. An assessment of waste dump stability including factors such as quasi-static deformation behaviour, historical dump deformation behaviours and potential blasting effects was undertaken. It is concluded that safe blasting may be carried out in proximity to waste dumps, but monitoring of dump behaviour is recommended to ensure operational safety. 22 refs., 4 apps.

1988-11-01

236

Structure of first- and second-stage mineralized elements in teeth of the sea urchin Lytechinus variegatus  

UK PubMed Central (United Kingdom)

Microstructure of the teeth of the sea urchin Lytechinus variegatus was investigated using optical microscopy, SEM (scanning electron microscopy) and SIMS (secondary ion mass...Full Text Available

2009-12-01

237

Monotonic and Low-Cycle Fatigue Response of a Maraging Steel and Metastable Beta Titanium Alloy under Torsional Loading.  

Science.gov (United States)

This study deals with the torsional response of Ti-8823 and 18Ni (200) maraging steel. The effect of different heat treatments and the subsequent change in microstructure are investigated. In the case of the Ti-8823, a comparison was made between the solu...

1977-01-01

238

Mechanistic fracture criteria for the failure of human cortical bone  

Energy Technology Data Exchange (ETDEWEB)

A mechanistic understanding of fracture in human bone is critical to predicting fracture risk associated with age and disease. Despite extensive work, a mechanistic framework for describing how the underlying microstructure affects the failure mode in bone is lacking.

2002-12-13

239

Evaluation of microstructures and mechanical properties in the HAZ of SA 508 Gr.4N Low Alloy Steel  

International Nuclear Information System (INIS)

In the heat-affected zones (HAZ) of low alloy steels used for nuclear pressure vessel, microstructural changes, such as grain coarsening, carbide precipitation, and martensite formation, generally occur and cause a deterioration of toughness and an increase in sensitivity to brittle fracture. Metallographic analyses of low alloy steel welds reveal significantly different regions in HAZ microstructures. In 2-pass welds, there were seven characteristic regions in the HAZ determined by the peak temperature, to which the region was exposed during the weld thermal cycle: a coarse-grained region, a fine-grained region, an intercritical region, and subcritical region. The coarse-grained region can be categorized into four zones according to the reheating temperature as follows : an unaltered coarse-grained zone (UCGHAZ), a supercritically reheated coarse grained zone (SCRCGHAZ), an intercritically reheated coarse-grained zone (ICRCGHAZ), and an ...

2006-11-02

240

Effect of rolling conditions on microstructure and mechanical properties of AZ31 Mg alloy  

Energy Technology Data Exchange (ETDEWEB)

The effect of warm rolling under various conditions on the microstructure and mechanical property was investigated using an AZ31 Mg alloy sheet. Several processing parameters such as initial thickness, thickness reduction by a single pass rolling, rolling temperature, roll speed, and roll temperature were varied to elicit an optimum condition for the warm rolling process of AZ31 Mg alloy. Microstructure and mechanical properties were measured for specimens subjected to rolling experiments of various conditions. Warm rolling of 30% thickness reduction per pass was possible without any side-crack at temperatures as low as 200 C under the roll speed of 30 m/min. The initial microstructure before rolling was the mixed one consisting of partially recrystallized and cast structures. Grain refinement was found to occur actively during the warm rolling, producing a very fine grain size of 7 {mu}m after 50% reduction in single pass ...

2005-07-01

241

Effect of orientation on the in vitro fracture toughness ofdentin: The role of toughening mechanisms  

Energy Technology Data Exchange (ETDEWEB)

A micro-mechanistic understanding of bone fracture thatencompasses how cracks interact with the underlying microstructure anddefines their local failure mode is lacking, despite extensive research nthe response of bone to a variety of factors like aging, loading, and/ordisease.

2003-01-28

243

Development of tough #alpha#-SiAlON  

International Nuclear Information System (INIS)

The development of tough #alpha#-SiAlON with elongated grains in the last five years is summarized. This progress has been guided by the improved understanding of phase relations and nucleation/growth kinetics in SiAlON ceramics. Although most #alpha#-SiAlON compositions can be processed to contain some elongated grains, their microstructure, fracture toughness and R-curve behavior vary greatly. Such variability is due to the different phase stability of #alpha#-SiAlONs and the varying physical chemistry of the competing phases, including the transient/residual liquid. For this reason, microstructure control of #alpha#-SiAlON must pay close attention to the composition, starting powder and heating schedule. Seeding with single crystals of an appropriate #alpha#-SiAlON composition provides an attractive alternative that simplifies the task of microstructure control, since such seeds are thermodynamically stable and they ...

244

Age- and Gender-Related Differences in the Geometric Properties and Biomechanical Significance of Intracortical Porosity in the Distal Radius and Tibia  

UK PubMed Central (United Kingdom)

Cortical bone contributes the majority of overall bone mass and bears the bulk of axial loads in the peripheral skeleton. Bone metabolic disorders often are manifested by cortical microstructural changes...Full Text Available

2010-05-01

245

The effect of cold deformation on the structure, texture and properties of yttrium high temperature superconducting powders and strips  

Energy Technology Data Exchange (ETDEWEB)

Cold deformation of YBa{sub 2}Cu{sub 3}O{sub 7-x}(phase 123, T{sub c} = 88.5-92 K) powders and strips causes partial decomposition of the 123 phase, a reduction in the degree of orthorhombicity of the structure up to almost complete degradation, and a decrease in T{sub c}. When they are deformed, yttrium high temperature superconductors acquire basal (001) (110) texture with high pole density (13-15 arbitrary units), low scattering angle ({+-} 6deg--7deg from the normal direction), and a weak preference for a, b or a + b in the rolling direction; traces of (139) orientations may also be found. This texture is known to be favourable for increasing j{sub k}. The combined effect of cold deformation and a carbon-containing binder leads, however, to a complete loss of superconductivity at 77 K or above. Depending on the regime of subsequent annealing, the following effects may be observed: degradation of the orthorhombic ...

1991-09-20

246

Summary on performance study of corrosion resistance of zirconium alloys  

International Nuclear Information System (INIS)

Zirconium-base alloys are used primarily as fuel cladding material and other core structure material in water cooled nuclear power reactors. Main research achievements and problems about corrosion of zirconium alloys are reviewed; the present theories and challenge are summarized. In the 1980s, great progress had been made towards correlating alloy composition, microstructure and irradiation with corrosion resistance. In the 1990s, main researches are focused on exploring actual mechanism of corrosion, optimizing both alloy composition and microstructure in order to minimize the fuel cycle costs through burnup optimization.

247

Mixed structures in continuously cooled low-carbon automotive steels  

Energy Technology Data Exchange (ETDEWEB)

Mixed microstructures have been studied in low- carbon microalloyed steels suitable for automotive applications, after continuous cooling from the hot-rolled condition. Microstructural features such as polygonal ferrite, bainitic and acicular ferrite and microphase constituent are identified using transmission electron microscopy. The influence of these mixed structures on the tensile strength, impact toughness and fracture behaviour is examined. It is found that improvements in impact toughness as compared with microalloyed medium- carbon ferrite/pearlite steels can be achieved from these predominantly acicular structures developed by controlling alloy composition and continuous cooling of these lower carbon steels. (orig.).

1993-11-01

248

Mixed structures in continuously cooled low-carbon automotive steels  

International Nuclear Information System (INIS)

Mixed microstructures have been studied in low- carbon microalloyed steels suitable for automotive applications, after continuous cooling from the hot-rolled condition. Microstructural features such as polygonal ferrite, bainitic and acicular ferrite and microphase constituent are identified using transmission electron microscopy. The influence of these mixed structures on the tensile strength, impact toughness and fracture behaviour is examined. It is found that improvements in impact toughness as compared with microalloyed medium- carbon ferrite/pearlite steels can be achieved from these predominantly acicular structures developed by controlling alloy composition and continuous cooling of these lower carbon steels. (orig.).

1993-06-01

249

Microstructure/Mechanical property relationships in bar products of Beta-C trademark (Ti-3Al-8V-6Cr-4Mo-4Zr)  

International Nuclear Information System (INIS)

Beta-C trademark is a metastable beta titanium alloy which can be heat treated to achieve a good combination of properties such as tensile strength, fatigue strength, ductility and toughness, such as needed in aircraft fasteners. Variations in hot and cold processing parameters and solution heat treatment can affect the resultant grain structure which in turn affects subsequent aging response and mechanical properties. Several processing/heat treating routes on round bar are explored in this study to determine the effects on microstructure and various mechanical properties.

1993-02-21

250

Hot workability, microstructural control and rate-controlling mechanisms in cast-homogenized AZ31 magnesium alloy  

Energy Technology Data Exchange (ETDEWEB)

Optimum conditions for microstructural control in industrial hot working of cast and homogenized AZ31 magnesium alloys are evaluated by using a processing map. The recommended window for bulk metal working of this alloy is the domain in the temperature range 300-450 C and strain rate range 1-10 s{sup -1}, and the optimum processing parameters are 400 C and 10 s{sup -1}, where grain-boundary self diffusion is the rate-controlling mechanism. (Abstract Copyright [2009], Wiley Periodicals, Inc.)

2009-03-15

251

Effect of mineralizer on the nitridation of sialon-bonded silicon carbide products  

International Nuclear Information System (INIS)

The effect of a mineralizer, magnesium silicate, on the nitridation of compacts consisting of silicon, clay, silica and silicon carbide was examined in terms of their reaction depth, density, porosity, phase composition and microstructure. It was found that addition of mineralizer slowed down the nitridation significantly. The kinetic process of isothermal nitridation in the presence of magnesium silicate obeys a parabolic rate law. Otherwise it obeys a linear rate law. The results suggest that nitrogen transportation is the limiting step during nitridation when mineralizer is added. The mechanism of nitridation is discussed in terms of phase composition and microstructure. Copyright (2000) The Australian Ceramic Society

252

Effect of intense plastic straining on microstructure and mechanical properties of an Al-Mg-Sc alloy  

International Nuclear Information System (INIS)

An Al-5%Mg-0.18%Mn-0.2%Sc-0.08%Zr-0.002%Be was subjected to equal-channel angular extrusion up to true strains of #approx#3 and #approx#8, that resulted in the formation of partially recrystallized and fully recrystallized structure, respectively. It was shown that the alloy with partially recrystallized structure exhibits highest strength and ductility. The material with fully recrystallized structure showed lowest fatigue crack growth rate and highest value of fracture toughness. Reasons of this unusual effect of microstructure on crack propagation resistance under fatigue are discussed.

2010-07-01

253

Correlation of coke microstructure and properties  

Science.gov (United States)

Coke petrography could be useful for improving blast furnace coke properties and for solving cokemaking production problems. To do this, quantitative correlations between coke structure, coal properties and carbonization conditions, and coke properties are useful, if not essential. Some examples of correlations of this type were presented in this paper. Specifically, microstructural parameters of cokes produced in Inland Steel Company's pilot scale coke oven were correlated with the rank and blend proportions of the parent coal, with the reactivity of the coke, and with the ASTM stability of cokes prepared from single coals.

1982-01-01

254

Characterization and evaluation of type 316LN stainless steel/alloy 800 joint  

Energy Technology Data Exchange (ETDEWEB)

The effect of aging on the microstructure and tensile properties of a type 316LN stainless steel/Alloy 800 joint, welded with 16-8-2 stainless steel consumable, has been studied to characterize and evaluate the joint for long-term elevated temperature service. The joint was subjected to accelerated againg heat treatments at 873 K up to 5000 h to simulate long-term service exposures. Analysis of the results from this investigation shows that this joint has adequate stability of microstructure and tensile properties even after prolonged exposure at elevated temperatures. (orig.)

1994-12-01

255

Durability of cement-based materials: modeling of the influence of physical and chemical equilibria on the microstructure and the residual mechanical properties; Durabilite des materiaux cimentaires: modelisation de l'influence des equilibres physico-chimiques sur la microstructure et les proprietes mecaniques residuelles  

Energy Technology Data Exchange (ETDEWEB)

A large part of mechanical and durability characteristics of cement-based materials comes from the performances of the hydrated cement, cohesive matrix surrounding the granular skeleton. Experimental studies, in situ or in laboratory, associated to models, have notably enhanced knowledge on the cement material and led to adapted formulations to specific applications or particularly aggressive environments. Nevertheless, these models, developed for precise cases, do not permit to specifically conclude for other experimental conclusions. To extend its applicability domain, we propose a new evolutive approach, based on reactive transport expressed at the microstructure scale of the cement. In a general point of view, the evolution of the solid compounds of the cement matrix, by dissolutions or precipitations, during chemical aggressions can be related to the pore solution evolution, and this one relied to the ionic exchanges with the external environment. By the ...

2004-09-15

256

Study of the Photon Strength Functions for Gadolinium Isotopes with the DANCE Array  

Science.gov (United States)

The gadolinium isotopes are interesting for reactor applications as well as for medicine and astrophysics. The gadolinium isotopes have some of the largest neutron capture cross sections. As a consequence they are used in the control rod in reactor fuel assembly. From the basic science point of view, there are seven stable isotopes of gadolinium with varying degrees of deformation. Therefore they provide a good testing ground for the study of deformation dependent structure such as the scissors mode. Decay gamma rays following neutron capture on Gd isotopes are detected by the DANCE array, which is located at flight path 14 at the Lujan Neutron Scattering Center at Los Alamos National Laboratory. The high segmentation and close packing of the detector array enable gamma-ray multiplicity measurements. The calorimetric properties of the DANCE array coupled with the neutron time-of-flight technique enables one to gate on a specific resonance of a ...

2009-03-10

257

Structure of molten alkali halides  

Energy Technology Data Exchange (ETDEWEB)

The results of X-ray and neutron diffraction experiments on molten alkali halides in which some data of our experiments by X-ray diffraction such as those of molten LiCl, NaCl, KCl, LiBr and KBr are included were summarized. The first peak positions in the radial distribution function in molten alkali halides by X-ray or neutron diffraction experiments are always longer than those by computer simulations and the differences of 0.1 -- 0.3 A exceed the experimental error. It seems to be due to the deformation of the electron shell. In the computer simulation, the shell model which has the spherical deformation was expected to have a closer value of the first peak position to the experimental one than the rigid ion model by taking the polarization of ions. However, no change in the first peak position was found. Therefore, the non-spherical deformation of electron shell at the point where ions are in contact with each other ...

1982-06-01

258

Structure of molten alkali halides  

International Nuclear Information System (INIS)

The results of X-ray and neutron diffraction experiments on molten alkali halides in which some data of our experiments by X-ray diffraction such as those of molten LiCl, NaCl, KCl, LiBr and KBr are included were summarized. The first peak positions in the radial distribution function in molten alkali halides by X-ray or neutron diffraction experiments are always longer than those by computer simulations and the differences of 0.1 -- 0.3 A exceed the experimental error. It seems to be due to the deformation of the electron shell. In the computer simulation, the shell model which has the spherical deformation was expected to have more closer value of the first peak position to the experimental one than the rigid ion model by taking the polarization of ions. However, no change in the first peak position was found. Therefore, the non-spherical deformation of electron shell at the point where ions are in contact with each other ...

1982-01-01

259

Plastic zone and pileup around large indentations  

International Nuclear Information System (INIS)

Mechanical properties of cold-worked molybdenum, grade 4 titanium, and an #alpha#-#beta# titanium alloy are measured with tensile tests and by indentations using conical indenters with 105, 120, and 137 deg included angles. The extent of plastic deformation and pileup around an indentation is measured using profilometry. Various models predicting the extent of plastic deformation and pileup are compared to the actual measured values. As inferred from indentation, the calculated yield strength of the material from the mean pressure does not correlate well to the yield strength measured by tensile testing. The plastic zone size surrounding an indentation can also be used to determine the yield strength of the material, and this does correlate to the yield strength measured by tensile tests. Furthermore, the extent of plastic deformation is relatively independent of the included angle of the indenter for the range of materials ...

260

Optical potentials and isoscalar transition rates from 104 MeV alpha-particle scattering by the N=28 isotones _4_8Ca, _5_0Ti and _5_2Cr  

International Nuclear Information System (INIS)

Precisely measured differential cross sections for elastic and inelastic scattering from 104 MeV alpha-particles by _4_8Ca, _5_0Ti and _5_2Cr are reported. The analyses aim primarily at the determination of strength, radial shapes and deformation of the scattering potentials, looking for isotonic differences of N=28 isotones. The mean square radii of the (real) potentials are discussed in terms of mean square radius differences of the matter distributions. The isoscalar transition rates derived by coupled channel analyses of the measured cross sections are compared with electromagnetic rates. In addition to the analyses on the basis of a slightly generalized extended optical model a semi-microscopic deformed folding model has been applied, using a density-dependent effective alpha-bound nucleon interaction. Though an excellent description of the data over the full angular range is obtained the resulting values of the ...

261

Optical potentials and isoscalar transition rates from 104 MeV alpha-particle scattering by the N=28 isotones /sup 48/Ca, /sup 50/Ti and /sup 52/Cr  

Energy Technology Data Exchange (ETDEWEB)

Precisely measured differential cross sections for elastic and inelastic scattering from 104 MeV alpha-particles by /sup 48/Ca, /sup 50/Ti and /sup 52/Cr are reported. The analyses aim primarily at the determination of strength, radial shapes and deformation of the scattering potentials, looking for isotonic differences of N=28 isotones. The mean square radii of the (real) potentials are discussed in terms of mean square radius differences of the matter distributions. The isoscalar transition rates derived by coupled channel analyses of the measured cross sections are compared with electromagnetic rates. In addition to the analyses on the basis of a slightly generalized extended optical model a semi-microscopic deformed folding model has been applied, using a density-dependent effective alpha-bound nucleon interaction. Though an excellent description of the data over the full angular range is obtained the resulting values of the ...

1983-08-01

262

Nanomechanical properties of vimentin intermediate filament dimers  

International Nuclear Information System (INIS)

The cell's cytoskeleton, providing the cell with structure and shape, consists of a complex array of structural proteins, including microtubules, microfilaments and intermediate filaments. Intermediate filaments play a crucial role in mechanotransduction and in providing mechanical stability to cells, in particular under large deformation. By utilizing molecular simulation, here we report a nanomechanical analysis of vimentin intermediate filament dimers, the basic building blocks of intermediate filaments. We describe a detailed analysis of the mechanical properties and associated deformation mechanisms, and find that mechanical stretch induces a transition from alpha-helices to beta-sheets, a phenomenon known as alpha-beta transition. A comparison of the Young's modulus predicted from simulation with experimental measurements is provided, and good agreement is found. We present an analysis of structural changes during ...

2009-10-21

263

Fluid pressure arrival time tomography: Estimation and assessment in the presence of inequality constraints, with an application to a producing gas field at Krechba, Algeria  

Energy Technology Data Exchange (ETDEWEB)

Deformation in the overburden proves useful in deducing spatial and temporal changes in the volume of a producing reservoir. Based upon these changes we estimate diffusive travel times associated with the transient flow due to production, and then, as the solution of a linear inverse problem, the effective permeability of the reservoir. An advantage an approach based upon travel times, as opposed to one based upon the amplitude of surface deformation, is that it is much less sensitive to the exact geomechanical properties of the reservoir and overburden. Inequalities constrain the inversion, under the assumption that the fluid production only results in pore volume decreases within the reservoir. We apply the formulation to satellite-based estimates of deformation in the material overlying a thin gas production zone at the Krechba field in Algeria. The peak displacement after three years of gas production is approximately ...

2010-04-01

264

Fault-related-folding structure and reflection seismic sections. Construction of earth model using balanced cross section; Danso ga kaizaisuru shukyoku kozo no keitai to jishin tansa danmen. 1. Balanced cross section wo mochiita chika model no kochiku  

Energy Technology Data Exchange (ETDEWEB)

Pre-stacking depth migration treatment is studied for the estimation of the fold configuration from seismic survey cross sections. The estimation of a velocity structure is necessary for the execution of such treatment, and the utilization of structural-geological knowledge is required for its interpretation. The concept of balanced cross section in relation to the fault-bend fold constructs a stratum structure model under conditions that the deformation during fold and fault formation is a planar strain, that there is no change in volume due to deformation, and that a fold is a parallel fold. In addition to the above geometric and kinetic approach, there is another fold formation process simulation model using a Newtonian fluid for study from the viewpoint of dynamics. This simulation stands on the presumption that the boundary contains a ramp that had been in presence before fold formation and that an incompressible viscous matter is mounted ...

1997-05-27

265

Edge-drop control of hot and cold rolled strip by tapered-crown work roll shifting mill. Kata taper tsuki work roll shifting mill ni yoru hakkoban no edge-drop seigyo tokusei  

Energy Technology Data Exchange (ETDEWEB)

Together with an investigation on the deformation behavior of hot and cold rolled strip edge, the edge-drop control was explained in characteristics and result of application to the commercial mill by the tapered-crown work roll (WR) shifting mill. From a cold rolling experiment, three-dimensional material flow was known to be generated in the vicinity of edge also at the time of rolling the strip, and which generation influences that of edge-drop. Almost linearly relative to the flattened deformation of WR, the edge-drop enlarges with enlargement in that deformation. The number of stands to be applied to the tapered-crown WR shifting mill in the tandem cold mill is determined by the location as far as which the strip is to be controlled in edge-drop. In case of improving it to obtain the edge-drop-free strip, all the stands are required to be equipped with tapered-crown WR shifting mill. By applying a tapered-crown WR ...

1992-01-01

266

Deforming the Maxwell-Sim algebra  

International Nuclear Information System (INIS)

The Maxwell algebra is a noncentral extension of the Poincare algebra, in which the momentum generators no longer commute, but satisfy [P?,P?]=Z??. The charges Z?? commute with the momenta, and transform tensorially under the action of the angular momentum generators. If one constructs an action for a massive particle, invariant under these symmetries, one finds that it satisfies the equations of motion of a charged particle interacting with a constant electromagnetic field via the Lorentz force. In this paper, we explore the analogous constructions where one starts instead with the ISim subalgebra of Poincare, this being the symmetry algebra of very special relativity. It admits an analogous noncentral extension, and we find that a particle action invariant under this Maxwell-Sim algebra again describes a particle subject to the ordinary Lorentz force. One can also deform the ISim algebra to DISimb, where b is a nontrivial dimensionless parameter. We find that the ...

2010-09-15

267

Crushed Salt Constitutive Model  

Energy Technology Data Exchange (ETDEWEB)

The constitutive model used to describe the deformation of crushed salt is presented in this report. Two mechanisms -- dislocation creep and grain boundary diffusional pressure solution -- are combined to form the basis for the constitutive model governing the deformation of crushed salt. The constitutive model is generalized to represent three-dimensional states of stress. Upon complete consolidation, the crushed-salt model reproduces the Multimechanism Deformation (M-D) model typically used for the Waste Isolation Pilot Plant (WIPP) host geological formation salt. New shear consolidation tests are combined with an existing database that includes hydrostatic consolidation and shear consolidation tests conducted on WIPP and southeastern New Mexico salt. Nonlinear least-squares model fitting to the database produced two sets of material parameter values for the model -- one for the shear consolidation tests and one for a ...

1999-02-01

268

Atomic spectroscopy study of nuclear properties of francium and cesium isotopes; Etude par spectroscopie atomique de proprietes nucleaires d'isotopes de francium et de cesium  

Energy Technology Data Exchange (ETDEWEB)

This work is based on the study of cesium ({sup 118,146}Cs) and francium ({sup 207-213}Fr,{sup 220-228}Fr) isotopes by hyperfine atomic spectroscopy and on the interpretation of these results from the nuclear physics point of view. The measured nuclear quantities are: the spin, the magnetic moment, the electric quadrupole moment and the mean square charge radius. The experimental method which is based on hyperfine optical pumping with a tunable laser, followed by magnetic analysis of the atoms is described in the first part. Results related to atomic physics are also presented. In the second part, these data are interpreted in the framework of nuclear models. The deformation of light cesium isomers are compared to values obtained from a theoretical self-consistent calculation. Heavy francium isotopes are situated in an area where the existence of static octupole deformations have been predicted. The odd-even staggering measured on the mean ...

1986-04-15

269

A laboratory study on the thermomechanical behaviour of clayey soils  

Energy Technology Data Exchange (ETDEWEB)

The thermomechanical behaviour of clayey soils was examined in a laboratory study because of their importance in some engineering applications such as hydrocarbon extraction from oil-bearing sands and radioactive waste disposal. The slightest temperature variations have been known to have an impact on the mechanical behaviour of clayey soils. In this study, tests were conducted on reconstituted and natural clayey soils using triaxial cells modified to control temperatures. Changes of temperature and stress state were not applied simultaneously. Instead, the tests were divided into two separate sections aimed at studying the thermal and mechanical behaviour of clays. The thermal behaviour tests examined the deformations induced by drainage temperature changes as well as pore-pressure generation and consolidation phenomena. The mechanical behaviour tests, focused on the influence of temperature and temperature history on compressibility, ...

2000-08-04

270

Study on warm caliber rolling of magnesium alloy  

Energy Technology Data Exchange (ETDEWEB)

The warm caliber rolling was experimented using the AZ31 magnesium alloy round bar of 20 mm in diameter machined from cast ingot materials. In warm caliber rolling in final size of 10 mm in diameter at 623 K via 8passes, each width-spreading, the change of each microstructure, X-ray analysis of final texture and final mechanical properties were investigated. Microstructure, texture and mechanical properties of warm caliber rolled round bar at 473 K via latter 4passes were compared with those at 623 K consistently. Obtained results are as follows: (1) The width-spreading in caliber rolling of round bar is relatively large, compared with that in flat rolling of the flat bar. The largeness of width-spreading of round bar makes the shape control of cross section difficult, and causes the cracks around the free surface. (2) Finer microstructure and inclined c axis of hexagonal lattice of 10 degrees to vertical direction of the ...

2003-07-01

271

Stress-assisted crystallisation in anodic titania  

International Nuclear Information System (INIS)

Research highlights: ? Correlations between microstructure and internal stress during Ti anodising are established. ? Large internal compressive stresses are accumulated in the film during anodising upto 12 V. ?A transition from compressive to tensile stress is observed when the cell voltage exceeds 12 V. ? At 40 V, the oxide films consist of two regions with different compositions and microstructures. Crystallisation of amorphous to anatase TiO2 contributes to the compressive stress relaxation. - Abstract: The relationship between the microstructural and internal stress evolution during Ti anodising is discussed. Samples anodised galvanostatically to 12 V and 40 V, corresponding to different stages of the internal stress evolution, were examined by in-plane and cross-section transmission electron microscopy. Electron diffraction patterns have been complemented with stoichiometry data obtained from energy loss near edge ...

2011-04-01

272

Microstructure of the gravitationally settled region in a liquid-phase sintered dilute tungsten heavy alloy  

Energy Technology Data Exchange (ETDEWEB)

A dilute tungsten heavy alloy consisting of 50W-35Ni-15Fe (wt pct) was liquid phase sintered at 1,500 C for times ranging from 30 to 960 minutes. This alloy corresponds to a nominal solid content of 20 vol pct at the sintering temperature. Because of the excess liquid, the alloy densified easily and exhibited extensive liquid-solid separation due to the density difference between the phases. The solid content at the compact bottom ranged from 45 to 70 vol pct over position and time. The microstructure of the settled region was quantified for volume fraction of tungsten, grain size, connectivity, and settled solid angle of repose. These results provide a basis for extending the microstructural parameters to possible microgravity conditions. The grain growth rate constant varies with the inverse 2/3 power of the volume fraction of liquid, possibly reflecting combined coalescence and solution-reprecipitation processes. This volume-fraction effect ...

1995-02-01

273

Microstructure of the gravitationally settled region in a liquid-phase sintered dilute tungsten heavy alloy  

International Nuclear Information System (INIS)

A dilute tungsten heavy alloy consisting of 50W-35Ni-15Fe (wt pct) was liquid phase sintered at 1,500 C for times ranging from 30 to 960 minutes. This alloy corresponds to a nominal solid content of 20 vol pct at the sintering temperature. Because of the excess liquid, the alloy densified easily and exhibited extensive liquid-solid separation due to the density difference between the phases. The solid content at the compact bottom ranged from 45 to 70 vol pct over position and time. The microstructure of the settled region was quantified for volume fraction of tungsten, grain size, connectivity, and settled solid angle of repose. These results provide a basis for extending the microstructural parameters to possible microgravity conditions. The grain growth rate constant varies with the inverse 2/3 power of the volume fraction of liquid, possibly reflecting combined coalescence and solution-reprecipitation processes. This volume-fraction effect ...

274

Microstructure modifications and modulated piezoelectric responses in PLZT/Al{sub 2}O{sub 3} composites  

Energy Technology Data Exchange (ETDEWEB)

Piezoelectric ceramics for acoustic applications have been prepared by mixing the piezoelectric phase Pb{sub 1-1.5x}La{sub x}{open_square}{sub x/2}(Ti{sub 1-y}Zr{sub y})O{sub 3} (PLZT) with variable fractions of Al{sub 2}O{sub 3}. The samples are in form of pellets and polarized at high temperature. After thermal treatment, X-ray diffraction and scanning electron microscopy have been used to determine the phase and morphological modifications. The morphotropic PLZT initial phase disproportionates into modified PLZT and ZrO{sub 2} phases. Using electrical impedance spectroscopy, the resonance frequencies of the composite system have been determined and analyzed. As the Al{sub 2}O{sub 3} volume fractions increase, the resonance frequency and the amplitude of the electrical response both decrease. An interpretation of the role of Al{sub 2}O{sub 3} additions is proposed in terms of phase and microstructure modifications. Using LRC electrical equivalent circuits, the ...

2003-01-15

275

Microstructure fracture toughness and fatigue crack growth rate in titanium alloys; Proceedings of the 1987 TMS-AIME Annual Symposium, Denver, CO, Feb. 24, 25, 1987  

Science.gov (United States)

The papers contained in this volume provide an overview of recent theoretical and experimental research related to the fracture toughness and fatigue crack growth characteristics of titanium alloys. Topics discussed include room temperature fatigue crack propagation in beta-titanium alloys, fatigue crack growth rate acceleration in alpha+beta Ti alloys, influence of transformed beta microstructures on fatigue crack growth rates in Ti-6Al-4V, and the role of inclusion and pore content on the fracture toughness of powder processed blended elemental Ti-10V-2Fe-3Al. Papers are also presented on fatigue crack growth measurements in an alpha-beta titanium alloy, the effects of thermal processing variation on the properties of Ti-6Al-4V, and the effect of microstructure on ductility and fracture toughness of alpha+beta titanium alloys.

1987-01-01

276

In-situ focused ion beam (FIB) microscopy at high temperature  

International Nuclear Information System (INIS)

Materials Scientists need information on the kinetics of the microstructural evolution processes that determine the finished microstructure, and hence the properties, of any material. E.g. recrystallisation, grain growth and phase changes. Such kinetic information requires reliable discrimination of differently oriented crystallites and/or different crystal phases coupled with useful spatial resolution and temporal resolution (i.e. high frame rates). These imaging results must be realised from a hot and changing specimen, in an instrument that is compatible with that hot specimen and with a practical specimen heater. Focused Ion Beams (FIB) offer strong contrast between crystallites and phases, and hence offer the ability to discriminate between these features even while imaging at fast frame rates, however their compatibility with hot specimens was unproven. Here we report results from a novel combination of FIB with an in-situ heating stage, ...

2008-08-01

277

In Vitro Fracture of Human Cortical Bone: Local Fracture Criteria and Toughening Mechanisms  

Energy Technology Data Exchange (ETDEWEB)

A micro-mechanistic understanding of bone fracture that encompasses how cracks interact with the underlying microstructure and defines their local failure mode is lacking, despite extensive research on the response of bone to a variety of factors like aging, loading, and/or disease. Micro-mechanical models for fracture incorporating such local failure criteria have been widely developed for metallic and ceramic materials systems; however, few such deliberations have been undertaken for the fracture of bone. In fact, although the fracture event in mineralized tissues such as bone is commonly believed to be locally strain controlled, until recently there has been little experimental evidence to support this widely held belief. In the present study, a series of in vitro experiments involving a double-notch bend test geometry are performed in order to shed further light on the nature of the local cracking events that precede catastrophic fracture in bone and to define ...

2004-08-18

278

High performance ultra-steels with recyclable design  

Energy Technology Data Exchange (ETDEWEB)

The global production of steel is predicted to increase rapidly to meet future demands. In order to conserve the natural resources, certain measures must be taken. These include perfecting the recycling of steel, improving the performance to extend the life of the material, and reduce the need for massive production of steel by increasing the strength of the material. This paper presented a design concept for ultrafine complex microstructure steel. The National Research Institute for Metals in Japan has worked on a project which investigated 800 MPa ferrite steel for welded structures with a chemical composition similar to 400 MPa-class plain carbon steel. The doubled strength was attributed to grain refinement. Novel welding techniques were also used for joining the ultrafine microstructure. In this study, low carbon Si-Mn ferrite-pearlite steels were subjected to a thermo-mechanical treatment to produce a microstructure ...

2000-07-01

279

Factors influencing the microstructural development of Ca -#alpha#-sialon exhibiting elongated grains  

International Nuclear Information System (INIS)

Ca #alpha#-sialon is a high hardness material that exhibits in-situ growth of elongated grains during pressureless sintering. This potentially gives the material very good fracture toughness. This paper examined the effects of a number of variables on microstructural development during sintering. The effect of composition was investigated by studying seven different compositions. Densification was seen to be hindered in compositions that produced only small quantities of liquid phase during sintering. Elongated #alpha#-sialon was observed in all the compositions. It was in combination with equiaxed #alpha#--sialon in low liquid compositions, but only elongated #alpha#-sialon was present in the liquid rich compositions. The effects of using P-Si_3N_4 instead of #alpha#-Si_3N_4 starting powders were also examined. Compositions using only #alpha#-S_3N_4 and those that used a 50:50 #alpha#:#beta# mix displayed similar development during sintering. However, compositions ...

280

Evaluation of Mechanical Properties and Microstructure in Ion-Irradiated Surface Layer  

Science.gov (United States)

Target vessel materials used in spallation neutron source will be exposed to proton and neutron irradiation and mercury immersion environments. In order to evaluate the surface degradation of the vessel candidate materials due to such environment, the triple-ion beam irradiation taking the spallation reaction into account and mercury immersion tests were carried out. Mechanical properties of the gradient surface layer were evaluated by the inverse analysis with multi-layer model that considers distribution of surface characteristic was applied to the load and depth curves measured by using the instrumented indentation machine. Transmission electron microscopic observations were performed to evaluate the changes of microstructure in irradiated surface layer using focused ion-beam cut micro-specimen. The mechanical properties distributions in the surface layer were evaluated quantitatively and the changes in microstructures were correspondent to ...

2005-01-01

281

Effect of energy and dose on transient-enhanced diffusion and defect microstructure in low energy high dose As{sup +} implanted Si  

Energy Technology Data Exchange (ETDEWEB)

(001) CZ silicon wafers were implanted with arsenic (As{sup +}) at energies of 10--50 keV to doses of 2 {times} 10{sup 14} to 5 {times} 10{sup 15}/cm{sup 2}. All implants were amorphizing in nature. The samples were annealed at 700 C for 16 hrs. The resultant defect microstructures were analyzed by XTEM and PTEM and the As profiles were analyzed by SIMS. The As profiles showed significantly enhanced diffusion in all of the annealed specimens. The diffusion enhancement was both energy and dose dependent. The lowest dose implant/annealed samples did not show As clustering which translated to a lack of defects at the projected range. At higher doses, however, projected range defects were clearly observed, presumably due to interstitials generated during As clustering. The extent of enhancement in diffusion and its relation to the defect microstructure is explained by a combination of factors including surface recombination of point defects, As ...

1997-11-01

282

Effect of energy and dose on transient-enhanced diffusion and defect microstructure in low energy high dose As"+ implanted Si  

International Nuclear Information System (INIS)

(001) CZ silicon wafers were implanted with arsenic (As"+) at energies of 10--50 keV to doses of 2 x 10"1"4 to 5 x 10"1"5/cm"2. All implants were amorphizing in nature. The samples were annealed at 700 C for 16 hrs. The resultant defect microstructures were analyzed by XTEM and PTEM and the As profiles were analyzed by SIMS. The As profiles showed significantly enhanced diffusion in all of the annealed specimens. The diffusion enhancement was both energy and dose dependent. The lowest dose implant/annealed samples did not show As clustering which translated to a lack of defects at the projected range. At higher doses, however, projected range defects were clearly observed, presumably due to interstitials generated during As clustering. The extent of enhancement in diffusion and its relation to the defect microstructure is explained by a combination of factors including surface recombination of point defects, As precipitation, As clustering and ...

1996-12-02

283

Correlation of mechanical properties with microstructure of Alloy 800 after annealing at 800 - 1000 "0C  

International Nuclear Information System (INIS)

The microstructures of so called high temperature alloys, which have been developed for service temperatures up to 800"0C, are not necessarily stable at higher temperatures. The mobility of alloying elements is very high in FeCrNi alloys at 950 "0C e.g. iron, chromium or nickel can diffuse up to 0.1 mm distance in one year, which is about a grain diameter. Interstitials like carbon or nitrogen show a four orders of magnitude higher diffusivity than the alloying elements. In addition, the carbon solubility in this type of alloy is reported to be very low. Therefore the alloys are supersaturated with carbon after heat treatment above 1100 "0C and water quenching although the absolute carbon content is very low. At service temperatures around 800"0C the solubility of carbon is still about one order of magnitude lower than at heat treatment temperature. This will lead, together with the high mobility of elements, to precipitation of carbides even after short times and ...

1981-05-01

284

Cell behaviour on chemically microstructured surfaces  

Energy Technology Data Exchange (ETDEWEB)

Micropatterned surfaces with different chemical topographies were synthesised in order to investigate the influence of surface chemistry and topography on cell behaviour. The microstructured materials were synthesised by photoimmobilising natural Hyaluronan (Hyal) and its sulphated derivative (HyalS), both adequately functionalised with a photorective moiety, on glass substrates. Four different grating patterns (10, 25, 50 and 100 {mu}m) were used to pattern the hyaluronan. The micropatterned samples were analysed by Secondary Ions Mass Spectrometry, Scanning Electron Microscopy (SEM) and Atomic Force Microscopy to investigate the chemistry and the topography of the surfaces. The spectroscopic and microscopic analysis of the microstructured surfaces revealed that the photoimmobilisation process was successful, demonstrating that the photomask patterns were well reproduced on the sample surface. The influence of chemical topographies on the cell ...

2003-03-03

285

An Assessment of Through Thickness Mechanical Properties in Forged Thick Section Mod. 9Cr-1Mo Steel  

International Nuclear Information System (INIS)

Ferritic/martensitic steel, modified 9Cr-1Mo steels have been used most extensively in the power generation industry throughout the world due to having superior high temperature properties such as high strength, creep resistance, and good microstructure stability. These steels are also the primary candidate for the RPVs(Reactor Pressure Vessels) of High Temperature Gas-Cooled Reactors. Currently, many studies has been conducted in laboratory-scale for mod. 9Cr-1Mo steels. However, there is a lack of the study on forged thick- section for RPVs. The differences in characteristics including the through thickness microstructure and mechanical properties between internal and external locations may occur during cooling after austenitization, because the thickness of RPVs is over about 200mm. Therefore, in order to use ferritic/martensitic steel as RPVs, a detailed assessment of the through thickness properties is needed. The purpose of this study is ...

2010-10-01

286

X-ray Microdiffraction and Strain Gradient Crystal Plasticity Studies of Geometrically Necessary Dislocations Near a Ni Bicrystal Grain Boundary  

Energy Technology Data Exchange (ETDEWEB)

We compare experimental measurements of inhomogeneous plastic deformation in a Ni bicrystal with crystal-plasticity simulations. Polychromatic X-ray microdiffraction, orientation imaging microscopy and scanning electron microscopy, were used to characterize the geometrically necessary dislocation distribution of the bicrystal after uniaxial tensile deformation. Changes in the local crystallographic orientations within the sample reflect its plastic response during the tensile test. Elastic strain in both grains increases near the grain boundary. Finite element simulations were used to understand the influence of initial grain orientation and structural inhomogeneities on the geometrically-necessary dislocations arrangement and distribution and to understand the underlying materials physics.

2009-01-01

287

Wavelength shift of lasing from a dye-doped asymmetrically deformed liquid jet  

International Nuclear Information System (INIS)

We examined the spectral behaviors of lasing from a asymmetrically deformed liquid jet (a ? 14 ?m) which is induced by a laterally flowing gas. Th liquid sample was methanols which contains DCM dye. When n distortion is induced, the lasing spectrum appears as two periodic peaks which are corresponding to the resonance modes of cylindrical cavity. As the distortion parameter exceeds about 4%, the lasing spectrum shifts continuously to short wavelength. When the distortion parameter reaches ? 10%, the amount of blue shift was ? 30 nm. The blue shift can be explained as the shift of optimum wavelength of threshold curves. From the absorption and fluorescence curve of liquid sample, we estimated the spoiled Q with the distortion parameter.

1997-11-01

288

Torsional responses of double-walled carbon nanotubes via molecular dynamics simulations  

Energy Technology Data Exchange (ETDEWEB)

The buckling behaviors of double-walled carbon nanotubes (DWCNTs) under torsion are investigated by using molecular dynamics (MD) simulations. The effect of length on the torsional buckling behaviors of DWCNTs is examined for the first time. The simulation results show that the DWCNTs experience gradual or simultaneous buckling deformations depending on their lengths. In addition, the effect of the inner tube in a DWCNT on its torsional buckling behavior is also examined. The presence of the inner tube triggers van der Waals (vdW) interactions between it and the outer tube and thus leads to a stiffening effect of the DWCNT against torsional deformation. Whether the ends of the inner tube are free or fixed and whether it is subject to a torque or not, the critical torque and the critical torsional angle of the outer tube are only marginally affected.

2008-11-12

289

The deformation behavior of DyCu ductile intermetallic compound under compression  

British Library Electronic Table of Contents (United Kingdom)

In this study polycrystalline specimens of as-cast DyCu with B2 crystal structure were compressed to different strains at room temperature to test if stress-induced phase transformation and twinning occur during deformation. In these tests DyCu exhibited high ductility with plastic strain as high as 35% and ultimate compressive strength of ~790MPa. X-ray diffraction and transmission electron microscopy (TEM) showed no indications that DyCu had undergone stress-induced phase transformation or twinning. -type dislocations have been observed to play an important role for imparting the ductile behavior. TEM analyses showed the presence of second phases, Dy2O3 and DyCu2 within the DyCu. The mechanisms of ductility and impurity phase formation are discussed.

2011-01-01

290

Sub-barrier fusion reactions for synthesis of "2"9"8114  

International Nuclear Information System (INIS)

Favorable reaction channels are searched for in order to obtain the superheavy element "2"9"8114. The interaction energy is supposed to comply with the adiabatic hypothesis. Concerning the deformation energy, a very complete binary macroscopic-microscopic energy method is used to perform calculations. Deformed two-center shell model provides the energy level schemes for shell effects. Yukawa-plus-exponential model gives the macroscopic (liquid drop) part of the total energy. The mass tensor is obtained by the Werner-Wheeler irrotational flow hypothesis. Finally the minimization of the multidimensional action integral produces the highest penetrability values. Kr-projectile reactions provide the best pairs, although generally the presentabilities are very low. (author)

2005-01-01

291

Seismic tests of post-tensioned self-centering building frames with column and slab restraints  

British Library Electronic Table of Contents (United Kingdom)

Post-tensioned (PT) self-centering moment frames have been developed as an alternative to typical moment-resisting frames (MRFs) for earthquake resistance. When a PT frame deforms laterally, gaps between the beams and columns open. However, the gaps are constrained by the columns and the slab in a real PT self-centering building frame. This paper presents a methodology for evaluating the column restraint and beam compression force based on the column deformation and gap openings at all stories. The method is verified by cyclic tests of a full-scale, two-bay by one-story PT frame. Moreover, a sliding slab is proposed to minimize restraints on the expansion of the PT frame. Shaking table tests were conducted on a reduced-scale, two-by-two bay one-story specimen, which comprises one PT frame ...

2011-01-01

292

Reinforced concrete beam-column joints with crossed inclined bars under cyclic deformations  

British Library Electronic Table of Contents (United Kingdom)

This experimental study investigates the effectiveness of crossed inclined bars (X-bars) as joint shear reinforcement in exterior reinforced concrete beam-column connections under cyclic deformations. Test results of 20 joint subassemblages with various reinforcement ratios and arrangements including X-bars in the joint area are presented. The X-type, non-conventional reinforcement is examined as the only joint reinforcement and in combination with common stirrups or vertical bars. The experimental results reported herein include full loading cycle curves, energy dissipation values and a categorization of the observed damage modes. Based on the comparisons between the overall hysteretic responses of the tested specimens, it is deduced that joints with X-bars exhibited enhanced cyclic perfo...

2008-01-01

293

Probing the origin of inertia behind spacetime deformation  

CERN Document Server

To investigate the origin and nature of inertia, we introduce a new concept of hypothetical 2D, so-called, "master-space" (MS), subject to certain rules. The MS, embedded in the background 4D-spacetime, is an indispensable individual companion to the particle of interest, without relation to every other particle. We argue that a deformation/(distortion of local internal properties) of MS is the origin of inertia. With this perspective in sight, we construct the alternative relativistic theory of inertia (RTI), which allows to compute the relativistic inertial force acting on an arbitrary point-like observer due to its "absolute acceleration". We go beyond the hypothesis of locality with an emphasis on distortion of MS, which allows to improve essentially the standard metric and other relevant geometrical structures related to the noninertial reference frame of an arbitrary accelerated observer. We compute the inertial force exerted on the photon in a gravitating ...

2011-01-01

294

Petrography, geochemistry and regional significance of crystalline klippen in the Garhwal Lesser Himalaya, India  

British Library Electronic Table of Contents (United Kingdom)

Uphalda gneisses (UG) is a crystalline klippe located near Srinagar in Garhwal Himalaya. These gneisses are compared with Debguru porphyroids (DP) (?Ramgarh group) of Garhwal?Kumaun Himalaya and Baragaon mylonitic gneisses (BMG) of Himachal Himalaya. Petrographic study reveals that the deformation of UG was initiated at higher temperature (above 350?C) and continued till lowering of temperature and deformation led to the mylonitization. Geochemically, these granitic gneisses (UG, DP and BMG) exhibit similar composition. Features such as high molecular A/CNK value (>1), presence of normative corundum and absence of normative diopside, enhanced Rb/Sr, Rb/Zr ratios, enrichment of Th and containing rounded zircons support their crustally-derived S-type granitic nature. The linear plot in major...

2011-01-01

295

Numerical Algorithms for Two-Dimensional Dry Granular Flow with Deformable Elastic Grain  

Energy Technology Data Exchange (ETDEWEB)

The authors consider the dynamics of interacting elastic disks in the plane. This is an experimentally realizable two-dimensional model of dry granular flow where the stresses can be visualized using the photoelastic effect. As the elastic disks move in a vacuum, they interact through collisions with each other and with the surrounding geometry. Because of the finite propagation speed of deformations inside each grain it can be difficult to capture computationally even simple experiments involving just a few interacting grains. The goal of this project is to improve our ability to simulate dense granular flow in complex geometry. They begin this process by reviewing some past work, how they can improve upon previous work. the focus of this project is on capturing the elastic dynamics of each grain in an approximate, computationally tractable, model that can be coupled to a molecular dynamics scheme.

2005-08-11

296

Measurement of dynamic fracture toughness and failure behavior for explosive mock materials  

British Library Electronic Table of Contents (United Kingdom)

In this work, a pre-cracked semi-circular shaped explosive simulant was loaded using a split Hopkinson pressure bar (SHPB). A high-speed camera was used to capture the deformation and fracture process of the specimen in situ. The digital images were processed using the digital image correlation (DIC) method. Next, full displacement and strain fields were obtained. The displacement vector field shows that the specimen fractured under tensile stress action. The strain field can be used to predict the crack propagation. Results show that the method of combined DIC and SHPB is effective to study the dynamic deformation and fracture behavior of explosive simulants. In addition, the specimen was loaded using a drop weight. The fracture toughness of the specimen was preliminary measured.

2011-01-01

297

Manufacturing of oxide-dispersion-strengthened steels with the use of preliminary surface oxidation  

British Library Electronic Table of Contents (United Kingdom)

Regularities of deformation-induced dissolution of a surface layer of iron oxides in matrixes of iron-based alloys with bcc and fcc lattices have been studied by the methods of M?ssbauer spectroscopy, transmission electron microscopy, and X-ray diffraction. A method of producing iron alloys strengthened by dispersed oxide nanoparticles and alloyed with elements possessing a high affinity to oxygen (titanium and yttrium) has been proposed, which implies a dynamic dissolution of a surface layer of iron oxides upon strong cold deformation and a precipitation of secondary yttrium and titanium nanooxides upon a subsequent high-temperature sintering of mechanically alloyed powders. There has been demonstrated a possibility of oxide strengthening of pure iron upon its interaction with air without...

2011-01-01

298

Laser-assisted asymmetric incremental sheet forming of titanium sheet metal parts  

British Library Electronic Table of Contents (United Kingdom)

Asymmetric Incremental Sheet Forming (AISF) is a relatively new manufacturing process. In AISF, a CNC driven forming tool imposes a localized plastic deformation as it moves along the contour of the desired part. Thus, the final shape is obtained by a sequence of localized plastic deformations. AISF is suitable for small series production of sheet metal parts as needed in aeronautical and medical applications. Two main process limits restrict the range of application of AISF in these fields. These are the low geometrical accuracy of parts made from titanium alloys or high strength steels and, for titanium alloys, the limited formability at room temperature. In this paper a new concept for laser-assisted AISF is introduced including the required components. Furthermore, the CAX tools used f...

2011-01-01

299

Interlattice displacements and elastic constants of the A-15 compounds V_3Si, V_3Ge and Nb_3Sn  

International Nuclear Information System (INIS)

General expressions for the interlattice displacements of the A-15 structure compounds are obtained in terms of the strain components making use of the deformation theory. The nature of the interlattice displacements of all the 8 atoms in the unit cell is discussed. It is found that the interlattice displacements occur in such a way that the pair of atoms along any linear chain move in opposite directions with equal magnitudes. Expression for the strain energy of these compounds is developed using deformation theory and this is compared with the strain energy expression from continuum theory to obtain the elastic constants. The theoretical values of the elastic constants fairly agree with the experimental values for V_3Si, V_3Ge and Nb_3Sn. (author).

300

Interlattice displacements and elastic constants of the A-15 compounds V3Si, V3Ge and Nb3Sn  

Science.gov (United States)

General expressions for the interlattice displacements of the A-15 structure compounds are obtained in terms of the strain components making use of the deformation theory. The nature of the interlattice displacements of all the 8 atoms in the unit cell is discussed. It is found that the interlattice displacements occur in such a way that the pair of atoms along any linear chain move in opposite directions with equal magnitudes. Expression for the strain energy of these compounds is developed using deformation theory and this is compared with the strain energy expression from continuum theory to obtain the elastic constants. The theoretical values of the elastic constants fairly agree with the experimental values for V3Si, V3Ge and Nb3Sn.

1978-03-01

301

Impact of Hight Velocity Cold Spray Particles  

Energy Technology Data Exchange (ETDEWEB)

This paper presents experimental data and an computational model of the cold spray solid particle impact process. Copper particles impacting onto a polished stainless steel substrate are examined. The high velocity impact causes significant plastic deformation of both the particle and the sub- strate, but no melting is observed. The plastic deformation exposes clean surfaces that, under the high impact pressures, result in significant bond strengths between the particle and substrate. Experimental measurements of the splat and crater sizes compare well with the numerical calculations. It is shown that the crater depth is significant and increases with impact velocity. However, the splat diameter is much less sensitive to the impact velocity. It is also shown that the geometric lengths of the splat and crater scale linearly with the diameter of the impacting particle. It is hoped that the results presented will allow better understanding of the ...

1998-12-01

302

Hydrogen in titanium alloy with 16 at% Mo  

International Nuclear Information System (INIS)

The effect of various hydrogen concentrations on the crystal lattice period and the hardness of titanium alloy was examined, the alloy containing about 16 at.% Mo (27.5 wt. % Mo) and having #beta# structure. The peculiar features of the mechanism of plastic deformation of the alloy were studied after adding hydrogen to it. A dependence of the crystal lattice period on the concentration of hydrogen was obtained for TixMoxH_2 alloy. It has been established that the hardness of the Ti-Mo alloy does not change when hydrogen is added to it. The presence of hydrogen introduces changes into the mechanism of deformation of #beta#-titanium alloy. The configuration of the inverse pole figures after rolling proves that the transverse slip process in an alloy with hydrogen is hampered, and that the coplanar slip process is developing in it.

303

Hardening effect in Ti-3Al-2.5V during high temperature deformation  

International Nuclear Information System (INIS)

High temperature deformation behavior of an alpha + beta titanium alloy Ti-3Al-2.5V has been investigated in the temperature range 830 deg. C to 910 deg. C by using the method of cross head speed cycling. On the basis of flow stress-strain rate and strain rate sensitivity data, it was found that the alloy exhibits a hardening effect in the entire temperature range studied, amount of hardening being significant at the highest test temperature of 910 deg. C which resulted in a degradation of superplastic properties of the alloy. Grain growth in beta-phase due to strain was considered responsible for the hardening effect observed.

304

Grain size effects on the tensile properties and deformation mechanisms of a magnesium alloy, AZ31B, sheet  

International Nuclear Information System (INIS)

The grain size dependence of the tensile properties and the deformation mechanisms responsible for those properties are examined for Mg alloy, AZ31B, sheet. Specifically, the Hall-Petch effect and strain anisotropy (r-value) are characterized experimentally, and interpreted using polycrystal plasticity modeling. {1 0 . 2} extension twins, {1 0 . 1} contraction twins, and so-called 'double-twins' are observed via microscopy and diffraction-based techniques, and the amount of twinning is found to increase with increasing grain size. For the sheet texture and tensile loading condition examined, {1 0 . 2} extension twinning is not expected, yet the polycrystal plasticity model predicts the observed behavior, including this 'anomalous' tensile twinning. The analysis shows that the Hall-Petch strength dependence, of the polycrystal as a whole, is primarily determined by the grain size dependence of the strength of the prismatic slip systems.

2008-07-15

305

Gene Regulation of Extracellular Matrix Remodeling in Human Bone Marrow Stem Cell-Seeded Tissue-Engineered Grafts  

British Library Electronic Table of Contents (United Kingdom)

Tissue-engineered heart valves are prone to early structural deterioration. We hypothesize that cell?scaffold interaction and mechanical deformation results in upregulation of genes related to osteogenic/chondrogenic differentiation and thus changes extracellular matrix (ECM) composition in human bone marrow mesenchymal stem cell (hBMSC)-derived tissue-engineered grafts. hBMSC were expanded and seeded onto poly-glycolic acid/poly-lactic acid scaffold for 14 days. Seeded tissue-engineered constructs (TEC) were subjected to cyclic flexure for 24?h, whereas control TEC was maintained in roller bottles for the same duration. hBMSC, TEC, and mechanically deformed TEC were subjected to gene-array and histological analysis. Expression levels of RNA and/or protein markers related to chondrogenesis...

2011-01-01

306

Friction welding of AZ31 magnesium alloy  

Energy Technology Data Exchange (ETDEWEB)

In this paper, for an acceleration of utilization of magnesium alloy which is being interested in recent years, friction welding of AZ31 magnesium alloy was carried out, and the joint performance was discussed in relation to the deformation heat input in the upset stage and upset loss as a evaluation factor. Where, the deformation heat input in the upset stage is mechanical work represented by the product of upset speed and axial pressure. As a result, it was made clear that the friction welding of AZ31 magnesium alloy was easy in the atmosphere, and good welded joints without a non- adhesion area at the weld interface could de obtained. Moreover, the evaluation factors discussed were possible to evaluate to joint performance. (orig.)

2003-07-01

307

Friction in ultra-thin conjunction of valve seals of pressurised metered dose inhalers  

British Library Electronic Table of Contents (United Kingdom)

In many drug dispensing devices, such as syringes and inhalers, an elatomeric gasket is used to prevent the formulation from leaking from the chamber. During device actuation, the seal is subjected to friction, which in turn causes its deformation and can cause unintentional leakage, thus dose variability. Additionally, friction of seal is responsible for a host of potential problems such undue effort required for actuation and potential wear. The mechanism of friction generation in the seal conjunction is complex, arising from adhesion of rubber in contact with the moving interface, viscous action of a thin film of fluid and deformation of seal asperities. Therefore, the first step in understanding the conjunctional behaviour of rubber seals is a fundamental study of mechanisms of frictio...

2010-01-01

308

Facial reconstruction in the developing world: a complicated matter  

British Library Electronic Table of Contents (United Kingdom)

Around the world there is a small industry of non-governmental organisations that provide health care in niche areas that cannot be met by national health care provision. One topic is facial deformity that can have a dramatic effect on quality of life. In this study we investigate the morbidity and outcome of a British surgical team working for a 2-week period in Ethiopia. Thirty-five patients who presented with facial deformities had 47 operations during a 2-week period. Data were recorded for a minimum of 3 weeks postoperatively. Operative techniques were classified as simple or complex. Postoperative complications were assessed and classified as major, intermediate, and minor. In addition, the character of each complication was recorded and the cause elucidated. After 3 weeks the clinic...

2011-01-01

309

Experimental evidence for intraplate deformation controlled by netlike plastic-flow in central-eastern Asia  

British Library Electronic Table of Contents (United Kingdom)

The experimental results of brittle/ductile two-layer analogue models verify that intraplate tectonic deformation in central-eastern Asia is controlled mainly by the netlike plastic-flow (NPF) occurring in the lower lithosphere, including the lower crust and lithospheric mantle. The ductile lower layer in the model, corresponding to the lower lithosphere in the natural prototype, is made of a mixture of gum rosin and turpentine oil and the brittle upper one, to the upper crust, is formed by the consolidation of talc-powder slurry. The NPF hypothesis for continental dynamics can be regarded as a combination and development of two kinds of seemingly mutually exclusive ones, which are based on the theories of slip-line field and viscous (plastic) flow, respectively. In contrast to "homogeneou...

2007-01-01

310

Effect of matrix strength on pullout behavior of steel fiber reinforced very-high strength concrete composites  

British Library Electronic Table of Contents (United Kingdom)

This paper presents the results of single-fiber pullout tests for deformed and smooth steel fibers embedded in the newly developed very-high strength concrete (VHSC) matrixes. The pullout test program involved four types of steel fibers, eight compressive strengths of VHSC matrixes, and two normal concrete strengths. Test results have shown that pullout behavior of different steel fiber reinforced VHSC composites is influenced by the matrix strength and fiber end condition (smooth, flat end, or hooked). Results reveal that both maximum pull-out load and total pullout energy increases as matrix strength increases for all deformed fibers that did not rupture. The test results also indicated that the increase in total pullout energy is more significant than that in peak load.

2011-01-01

311

Effect of austenitizing and hot deformation temperatures on structure and mechanical properties of 40KhN2MA steel  

Energy Technology Data Exchange (ETDEWEB)

The effect of tsub(A) austenitization temperature in heating for quenching as well as in the cycle of high-temperature thermomechanical treatment (HTMT) on structure, mechanical properties and fracture mode of 40KhN2MA structural steel is investigated. It is shown that heating up to 1200 deg C does not affect essentially sigmasub(b) and sigmasub(0.2) of a quenched material but increases fracture toughness of 200 deg C - tempered precracked specimens and is accompanied by a decrease of impact strength and plasticity of vee-notched specimens. The optimum complex of mechanical properties is attained upon combined treatment comprising heating up to 1200 deg C and HTMT with deformation at 850 deg C.

1982-01-01

312

Deformations of topological open strings  

International Nuclear Information System (INIS)

Deformations of topological open string theories are described, with an emphasis on their algebraic structure. They are encoded in the mixed bulk-boundary correlators. They constitute the Hochschild complex of the open string algebra - the complex of multilinear maps on the boundary Hilbert space. This complex is known to have the structure of a Gerstenhaber algebra (Deligne theorem), which is also found in closed string theory. Generalising the case of function algebras with a B-field, we identify the algebraic operations of the bulk sector, in terms of the mixed correlators. This gives a physical realisation of the Deligne theorem. We translate to the language of certain operads (spaces of d-discs with gluing) and d-algebras, and comment on generalisations, notably to the AdS/CFT correspondence. The formalism is applied to the topological A- and B-models on the disc. (author)

2001-01-01

313

Corrosion resistance of Ultra-Low-Carbon 19% Cr-11% Ni stainless steel for nuclear fuel reprocessing plants in nitric acid  

International Nuclear Information System (INIS)

An Ultra-Low-Carbon 19% Cr-11% Ni Stainless Steels used in nuclear fuel reprocessing plants where highly corrosion resistance in nitric acid is required has been developed. This steel has optimized the chemistry composition to decrease inclusions and deformation-induced martensitic transformation. The formation of deformation-induced martensite has the potential danger of accelerating corrosion in nitric acid. In this paper, effects of cold reduction and martensitic transformation on corrosion resistance of Ultra-Low-Carbon Stainless Steels in nitric acid are discussed. The developed steel showed excellent corrosion resistance during long-term exposure to nitric acid. (author).

314

Control of quench distortion for steel parts  

Energy Technology Data Exchange (ETDEWEB)

There are two types in quench distortion of steel parts: thermal distortion and transformation distortion. Quench distortion is caused mainly by uneven cooling rate of steel parts from Austenitising temperature. The rapid cooled side is lengthened (convex deformation); the slow cooled side is shortened (concave deformation). So, to control the quench distortion, it is necessary to regulate the cooling rate of steel parts during quenching. TWO COMPONENTS produce the quench distortion of steel parts: the thermal stress and transformation stress. Generally, the effect of the thermal stress on the quench distortion is stronger than the transformation stress. The quench distortion is caused by uneven cooling rate of the steel parts, from Austenitising temperature to Ms point and Ms-Mf range. So, to control the quench distortion, it is very important to regulate the cooling rate of the steel parts during quenching. The purpose of this paper is to ...

1996-12-31

315

Computer simulation of the initial rafting process of a nickel-base single-crystal superalloy  

Energy Technology Data Exchange (ETDEWEB)

Rafting of the {gamma}/{gamma}{prime} morphology of nickel-base superalloys is a well-known phenomenon during high-temperature deformation. The initial stages of this type of directional coarsening were modeled two-dimensionally by the method of finite elements (FEs) using an energy-perturbation approach. In addition to the elastic energy density, the effect of the local difference of the hydrostatic stresses in {gamma} and {gamma}{prime} in combination with the different lattice parameters of the two phases was considered in the calculations as a further driving force. From the results of modeling, the deformation-induced internal stresses and strains were determined and used to evaluate the direction-dependent lattice parameters and lattice misfits of the two phases. The results agree well with experimentally determined values.

2000-03-01

316

Calculation of electromagnetic force in electromagnetic forming process of metal sheet  

International Nuclear Information System (INIS)

Electromagnetic forming (EMF) is a forming process that relies on the inductive electromagnetic force to deform metallic workpiece at high speed. Calculation of the electromagnetic force is essential to understand the EMF process. However, accurate calculation requires complex numerical solution, in which the coupling between the electromagnetic process and the deformation of workpiece needs be considered. In this paper, an appropriate formula has been developed to calculate the electromagnetic force in metal work-piece in the sheet EMF process. The effects of the geometric size of coil, the material properties, and the parameters of discharge circuit on electromagnetic force are taken into consideration. Through the formula, the electromagnetic force at different time and in different positions of the workpiece can be predicted. The calculated electromagnetic force and magnetic field are in good agreement with the numerical and experimental ...

2010-06-15

317

Brown diamonds from an eclogite xenolith from Udachnaya kimberlite, Yakutia, Russia  

British Library Electronic Table of Contents (United Kingdom)

Abstract: We have performed petrographic and spectroscopic studies of brown diamonds from an eclogite xenolith from the Udachnaya pipe (Yakutia, Russia). Brown diamonds are randomly intermixed with colorless ones in the rock and often located at the grain boundaries of clinopyroxene and garnet. Brown diamonds can be characterized by a set of defects (H4, N2D and a line at 490.7nm) which are absent in colorless diamonds. This set of defects is typical for plastically deformed diamonds and indicates that diamonds were likely annealed for a relatively short period after deformation had occurred. Excitation of brown colored zones with a 632.8nm He-Ne laser produced the typical diamond band plus two additional bands at 1730cm^-^1 and 3350cm^-^1. These spectral features are not genuine Raman ban...

2011-01-01

318

Alignment and alignment dynamics of nematic liquid crystals on Langmuir-Blodgett mono-layers  

CERN Document Server

Mono-layers of stearic and behenic acids deposited with the Langmuir-Blodgett technique, were used as aligning films in nematic liquid crystal cells. During the filling process the liquid crystal adopts a deformed quasi-planar alignment with splay-bend deformation and preferred orientation along the filling direction. This state is metastable and transforms with time into homeotropic once the flow has ceased. The transition is accompanied by formation of disclination lines which nucleate at the edges of the cell. The lifetime of the metastable splay-bend state was found to depend on the cell thickness. On heating, anchoring transition from quasi-homeotropic to degenerate tilted alignment in form of circular domains takes place near the transition to the isotropic phase. The anchoring transition is reversible with a small hysteresis.

1998-01-01

319

Complexity of the microstructure evolution for optimization cBN growth in a four-step ion-assisted deposition process  

International Nuclear Information System (INIS)

The changes in microstructure of a specially prepared boron nitride (BN) film as a function of film depth were studied by high resolution transmission electron microscopy (HRTEM) and other materials analysis tools. These changes were then correlated to the changes in processing parameters during film growth. The analyzed film was fabricated by the four-step ion-assisted deposition procedure known to be effective in film-stress engineering for the formation and retention of a thick cubic BN (cBN) layer with a three-step buffer-layer deposition. In this deposition, the energy of the ions assisting cBN formation was increased stepwise from 200 to 280, and then to 360 eV [S.F. Wong, C. W. Ong, G.K.H. Pang, K.Z. Baba-Kishi, W. M. Lau, J. Vac. Sci. Technol. A 22 (2004) 676]. The nominal thickness of the cBN layer was 650 nm and that for each of the three buffer layers was about 160 nm. Both the HRTEM and electron diffraction results confirmed that the top cBN layer, with ...

2005-10-01

320

Transmission electron microscopy study of plasma nitriding of electroplated chromium coating  

Energy Technology Data Exchange (ETDEWEB)

In this paper, the influence of plasma nitriding at temperature 720 deg. C for 20 h on the surface microstructure and interface microstructure of electroplated chromium coating was investigated. In these conditions, interdiffusion, mixing and reaction phenomena of elements originating from the substrate and coating material are more likely to occur, thus increasing the bonding strength between the coating and carbon steel substrate. The change of the structures from the substrate side to the coating surface, and the effect of the substrate steel on the interface structure were studied by cross-sectional transmission electron microscope observation (XTEM). The nitride layer formed on the surface was analyzed by X-ray diffraction method (XRD). After treatment at above conditions a 6-7 {mu}m thick nitride compound layer was formed in surface region and the same thick carbide compound layer was also formed in the interface region between ...

2003-02-28

321

Transmission electron microscopy study of plasma nitriding of electroplated chromium coating  

International Nuclear Information System (INIS)

In this paper, the influence of plasma nitriding at temperature 720 deg. C for 20 h on the surface microstructure and interface microstructure of electroplated chromium coating was investigated. In these conditions, interdiffusion, mixing and reaction phenomena of elements originating from the substrate and coating material are more likely to occur, thus increasing the bonding strength between the coating and carbon steel substrate. The change of the structures from the substrate side to the coating surface, and the effect of the substrate steel on the interface structure were studied by cross-sectional transmission electron microscope observation (XTEM). The nitride layer formed on the surface was analyzed by X-ray diffraction method (XRD). After treatment at above conditions a 6-7 #mu#m thick nitride compound layer was formed in surface region and the same thick carbide compound layer was also formed in the interface region between ...

2003-02-28

322

Transmission electron microscopy characterization of laser welding cast Ni-based superalloy K418 turbo disk and alloy steel 42CrMo shaft  

Energy Technology Data Exchange (ETDEWEB)

Microstructure characterization is important for controlling the quality of laser welding. In the present work, a detailed microstructure characterization by transmission electron microscopy was carried out on the laser welding cast Ni-based superalloy K418 turbo disk and alloy steel 42CrMo shaft and an unambiguous identification of phases in the weldment was accomplished. It was found that there are {gamma}-FeCrNiC austenite solid solution dendrites as the matrix, (Nb, Ti) C type MC carbides, fine and dispersed Ni{sub 3} Al {gamma}' phase as well as Laves particles in the interdendritic region of the seam zone. A brief discussion was given for their existence based on both kinetic and thermodynamic principles.

2008-08-11

323

Transmission electron microscopy characterization of laser welding cast Ni-based superalloy K418 turbo disk and alloy steel 42CrMo shaft  

International Nuclear Information System (INIS)

Microstructure characterization is important for controlling the quality of laser welding. In the present work, a detailed microstructure characterization by transmission electron microscopy was carried out on the laser welding cast Ni-based superalloy K418 turbo disk and alloy steel 42CrMo shaft and an unambiguous identification of phases in the weldment was accomplished. It was found that there are #gamma#-FeCrNiC austenite solid solution dendrites as the matrix, (Nb, Ti) C type MC carbides, fine and dispersed Ni_3 Al #gamma#' phase as well as Laves particles in the interdendritic region of the seam zone. A brief discussion was given for their existence based on both kinetic and thermodynamic principles.

2008-08-11

324

Transformation kinetics and microstructures of Ti17 titanium alloy during continuous cooling  

International Nuclear Information System (INIS)

We have investigated the microstructure evolutions in the Ti17 near #beta# titanium alloy during heat treatments. The phase transformation has first been studied experimentally by combining X-ray diffraction analysis, electrical resistivity and microscopy observations. From a series of isothermal treatments, a IT diagram has been determined, which takes into account the different morphologies. Then, a Johnson-Mehl-Avrami-Kolmogorov (JMAK) model has been successfully used to describe the phase transformation kinetics during either isothermal or cooling treatments. Finally, the coupling of the JMAK model to the finite element software ZeBuLoN allowed us to investigate the evolution of the spatial distribution of the different morphologies during the cooling of an aircraft engine shaft disk after forging.

2007-03-15

325

Thermal processing effects on the functional properties and microstructure of lentil, chickpea, and pea flours  

British Library Electronic Table of Contents (United Kingdom)

Pulses are rich in nutrients. The existence of anti-nutritional components and the length of time required for preparation have, however, limited their frequency of use compared to recommended intake levels. Anti-nutritional components in pulses can be largely removed by heat treatment. Additionally pre-treatment of pulses with heat and processing of seeds into flour could further enhance their use by decreasing processing and preparation times. In this study, trypsin inhibitor activity, functional properties, and microstructural characteristics of flours prepared from different varieties of lentil, chickpea, and pea as affected by roasting and boiling were evaluated. Both thermal treatments resulted in significant reduction (p<0.05) in trypsin inhibitor activity ranging from -95.6% to -37...

2011-01-01

326

Superplastic forming behaviors and microstructure characters of magnesium alloy sheet AZ31B  

International Nuclear Information System (INIS)

An experimental study on superplastic forming behaviors and microstructure characters of commercial magnesium alloy sheet AZ31B is presented in this paper. The main experimental results show that the commercial magnesium alloy AZ31B sheet has superplastic capability. For the received sheet without any pre-processing, the maximum elongation is 295%. The dynamic recrystallization and grain refinement can be found, In the case of temperature =# 350 deg. C. The superplastic behaviors can be improved by controlling the dynamic recrystallization and grain refinement. Some experimental results of free superplastic bulging are presented in this paper. The results show that influence of temperature on forming capability is much less than the influences of temperature on elongation. In addition, the maximum principle strain.

2004-06-10

327

Studies of the reduction mechanism of selenium dioxide and its impact on the microstructure of manganese electrodeposit  

British Library Electronic Table of Contents (United Kingdom)

The influence of selenium dioxide (SeO2) on the microstructure and electrodeposition of manganese coatings obtained from a sulfate based neutral solution was investigated by material characterization methods and electrochemical techniques. The crystal structure and surface morphology of these coatings were studied by scanning electron microscopy (SEM) and powder X-ray diffraction spectroscopy (XRD), respectively. The SEM and XRD data showed that SeO2 could effectively accelerate phase transformation, and facilitate leveled and fine grain growth. The electrochemical results indicated that SeO2 could inhibit hydrogen evolution reaction and promote manganese deposition. The action of selenium dioxide in manganese deposition was found to be a reduction and adsorption mechanism. The process cou...

2011-01-01

328

Strength and toughness tradeoffs for an ultrafine-grain size ferrite/cementite steel produced by warm-rolling and annealing  

British Library Electronic Table of Contents (United Kingdom)

For an ultrafine grain ferrite/cementite (UGF/C) steel, the Charpy impact energy was measured at temperatures from 373K to 4.2K, and tensile tests were carried out at temperatures between 323K and 77K. For the steel with annealed microstructure, the ductile-to-brittle transition appearance temperature (DBTT) was lower than the Charpy transition temperature (CTT). With increasing annealing time at 873K, the DBTT and the CTT increased, and the DBTT approached the CTT. The DBTT decreased with decreasing effective grain size. The effective grain size correlated to the grain size of the larger grain size peak in the distribution of grains with {100} planes. The annealed microstructures had higher yield strength for equivalent toughness (including upper shelf energy, DBTT and CTT) compared to th...

2011-01-01

329

Significance of microstructure for a MOCVD-grown YSZ thin film gas sensor  

Energy Technology Data Exchange (ETDEWEB)

The authors report the fabrication and characterization of a low temperature (200--400 C) thin film gas sensor constructed from a MOCVD-grown yttria-stabilized zirconia (YSZ) layer sandwiched between two platinum thin film electrodes. A reproducible gas-sensing response is produced by applying a cyclic voltage which generates voltammograms with gas-specific current peaks and shapes. Growth conditions are optimized for preparing YSZ films having dense microstructures, low leakage currents, and maximum ion conductivities. In particular, the effect of growth temperature on film morphology and texture is discussed and related to the electrical and gas-sensing properties of the thin film sensor device.

1996-11-01

330

Quantitative analysis of X-Ray Microtomography images of metal powders in the course of sintering  

Energy Technology Data Exchange (ETDEWEB)

In situ X-Ray microtomography offers new opportunities for analysing sintering mechanisms since it allows 3D observation of the microstructural evolution of the powder all along a sintering cycle. With synchrotron radiation at ESRF, a 3D image with a resolution of 2 {mu}m can be obtained in about one minute. In addition to the visual examination of the images, relevant microstructural parameters can be measured through quantitative image analysis using recently developed tools. In this paper the results obtained with two materials, loose copper powder and compacted steel powder, are resumed. For copper powder, the dispersion of local parameters such as particle co-ordination number and porosity is investigated. Concerning steel compacts, data about pore morphology evolution and on local strains provides clues for understanding the anisotropic shrinkage of such compacts. (authors)

2005-07-01

331

Production of powder titanium alloys with Mo, Zr, Nb additions and their properties  

International Nuclear Information System (INIS)

In order to substitute expensive cast titanium alloys by powder ones the possibility of introduction of powder additions by mechanical stock mixing is studied. It is shown that microstructure of powder alloys of Ti-Zr(1-9%) system is typical for one-phase cast #alpha#-alloys. The Ti-Mo(1-9%) and Ti-Nb(1-9%) system alloys have microstructure typical for two-phase (#alpha#+#beta#)-alloys. For homogeneous structure to be obtained the high temprature annealing is advisable after hot pressing. Alloying with Mo, Zr and Nb permits to increase considerable the strength of powder titanium products (at 9% Mo more than two times).

332

Observation of the microstructural changes in lithium titanate by multi-ion irradiation  

Energy Technology Data Exchange (ETDEWEB)

The irradiation behavior of Li{sub 2}TiO{sub 3} under a fusion reactor environment was simulated by simultaneous irradiation of Li{sub 2}TiO{sub 3} by the triple ion beams and the respective single ion beams of O{sup 2+}, He{sup +} and H{sup +}. The microstructural changes in Li{sub 2}TiO{sub 3} caused by the irradiation were measured by Raman spectroscopy and FT-IR photoacoustic spectroscopy. The results suggest that the formation of TiO{sub 2} due to displacements by irradiation occurs, and the irradiation defects generated by irradiation trap hydrogen and increase the amount of hydroxyl near the surface. Such phenomena are believed to significantly affect the chemical form of the released tritium and the tritium inventory in the breeding materials of a fusion reactor.

2004-08-01

333

Observation of the microstructural changes in lithium titanate by multi-ion irradiation  

International Nuclear Information System (INIS)

The irradiation behavior of Li_2TiO_3 under a fusion reactor environment was simulated by simultaneous irradiation of Li_2TiO_3 by the triple ion beams and the respective single ion beams of O"2"+, He"+ and H"+. The microstructural changes in Li_2TiO_3 caused by the irradiation were measured by Raman spectroscopy and FT-IR photoacoustic spectroscopy. The results suggest that the formation of TiO_2 due to displacements by irradiation occurs, and the irradiation defects generated by irradiation trap hydrogen and increase the amount of hydroxyl near the surface. Such phenomena are believed to significantly affect the chemical form of the released tritium and the tritium inventory in the breeding materials of a fusion reactor.

2004-08-01

334

Modelling the effects of measured anode triple-phase boundary densities on the performance of micro-tubular hollow fiber SOFCs  

British Library Electronic Table of Contents (United Kingdom)

The percolated or active triple phase boundary (TPB) length per unit volume of Ni-YSZ anode hollow fibers (HFs) containing 60wt.% initial NiO and a spatially varying microstructure were measured using a focused ion beam (FIB)-SEM technique. The measured values of contiguous TPB density were interfaced with a 2-D distributed finite element model of a hollow fiber solid oxide fuel cell. The model was applied to simultaneously solve the ionic and electronic charge balances in the electrodes, which were modelled as overlying continuum materials with effective electronic and ionic conductivities. The model was used to predict the effects of anode microstructure on the distribution of current density, and anode activation polarization. Active TPB lengths of 2.63-8.63 m^-^2 were measured for the ...

2011-01-01

335

Microstructure-property relationships in beryllia-ceramics sintered to near theoretical density  

Energy Technology Data Exchange (ETDEWEB)

The use of selective additives such as MgO as a sintering aid and a rare earth oxide as a grain growth inhibitor, has allowed the manufacture of beryllia ceramics having close to theoretical density. The grain size and grain size distribution can be controlled by an optimum firing schedule leaving a remnant porosity which is extremely fine (0.2 {mu}m). This structure is compared with conventional BeO ceramics, densified by liquid phase sintering, which develops a glassy grain boundary and retains large pores up to 3 {mu}m. The significantly improved strength properties, extremely fine pores,the 'pinning effect' of rare earth oxide, and the superior surface finish both in the as-fired and polished state are discussed in relation to the micro-structure. (orig.).

1989-01-01

336

Microstructure, mechanical properties and fracture behavior of #alpha# particle irradiated type 316 stainless steel  

International Nuclear Information System (INIS)

The present work is a research of the effect of helium on the microstructure, mechanical properties and fracture behaviors of a type 316 austenitic steel. Helium implantation was performed by 30-MeV #alpha#-particle injection on very small size specimens, using a cyclotron. Average helium content in a He-deposited region was up to 2000 appm He. In the case of 2000appm He implantation, intergranular fracture was sometimes observed on the helium deposited region after tensile test at room temperature. At elevated temperature test, however, this material showed the transition of fracture mode from transgranular-ductile fracture at 773K to intergranular fracture at 873. In the case of 500 appm He implantation, the transition of fracture mode was recognized at a temperature range of 873K to 973K. (author).

337

Microstructure and tool electrode erosion in EDMed of TiN/Si_3N_4 composites  

International Nuclear Information System (INIS)

Conductive TiN/Si_3N_4 ceramic composites were processed by electrical discharge machining (EDM) and their microstructure and conductivity were investigated. The whole process of tool electrode wear is evaluated by sinker-EDM. The machined surfaces of TiN/Si_3N_4 ceramic composites were examined by scanning electron microscopy (SEM) and profilometry to determine the surface finish. The electrode wear rate of brass is higher than copper electrode for all EDMed tests. The surface texture was found to have greater dependence on pulse energy. It was observed that the sinker-EDM at higher pulse energy caused severe microdamage in the surface. The surface roughness (Ra) values also increase with increasing pulse energy.

2003-12-20

338

Microstructure and properties of ultrafine WC-10Co composites with chemically doped VC  

British Library Electronic Table of Contents (United Kingdom)

Vanadium carbide is the most effective grain growth inhibitor for ultrafine WC-Co composites due to its high solubility and mobility in the cobalt phase at relatively low temperatures; however, there are still some debates over the best way to introduce it into the WC-Co formulation. In this paper, the differences between admixed and chemically doped grain growth inhibitors on the microstructural development and properties of an ultrafine WC-10Co composite are discussed. The densification rate of chemically doped samples is slower in the early stage of sintering and the WC grain sizes of the sintered alloys are finer than those of admixed samples, leading to the increase of hardness and transverse rupture strength of the sintered alloys. The effectiveness of the chemically doped inhibitor ...

2011-01-01

339

Microstructure and emission properties of nanometer Ce-W material  

International Nuclear Information System (INIS)

Nanometer Ce-W composite materials have been prepared by the method of freeze-drying. Microstructure and surface properties of materials were investigated by SEM and 'in situ' AES and emission characteristics have been determined. It is found that the nanometer materials have relatively small crystal particles with average dimensions in the order of 50 nm. Due to the results of matrix analysis, the cerium in the materials is uniformly distributed on submicron scale, which proves that the diffusion ability of cerium has been increased. Under high temperature, the active layer on the surface thickens simultaneously with the increase of cerium and oxygen. As a result, nanometer Ce-W materials exhibit excellent emission characteristics compared with those of micron-sized Ce-W materials.

2007-07-12

340

Microstructure analysis of nanocrystalline powders by X-ray diffraction  

International Nuclear Information System (INIS)

The use of X-ray diffraction line profile analysis for the study of nanocrystalline powders is described. The fundamentals of the theory are presented in terms of crystallite/domain size, size distribution, lattice distortion, dislocations density and stacking faults. Line profile parameters and the methods of pattern fitting introduced to overcome the diffraction-line overlap problem are discussed. The approaches based of the integral breadth of the measured line profiles and the Fourier method are discussed. In addition, simplified approaches are also commented. Representative examples are selected to illustrate various cases of microstructure, such as nanomaterials with strain-free spherical nano crystallites, strain-free crystallites with anisotropic crystallite shape, anisotropic crystallites with microstrains and spherical crystallites with dislocation densities and crystallite size distributions. (author)

2001-09-23

341

Microstructural changes of stearic acid films by immersion in salt solution  

Energy Technology Data Exchange (ETDEWEB)

X-Ray reflectivity has been used to investigate the microstructural changes of solution-cast stearic acid films before and after immersion in CoCl{sub 2} solutions. Before immersion, the films possess a well-defined layered structure with an interlayer spacing of 4.01{+-}0.05 nm. After the films were immersed in the CoCl{sub 2} solutions, a new set of equidistant diffraction peaks emerge, the corresponding interlayer spacing of which is 5.13{+-}0.05 nm. The X-ray photoelectron spectra of the films indicate the existence of cobalt ions inside the films after immersion. It is concluded that the permeation of the cobalt ions into the hydrophilic interlayer causes the stearic acid molecules to reorient perpendicular to the films, resulting in the increase of interlayer spacing and the roughening of the interfaces.

2003-11-01

342

Mechanical properties of B-modified Ti-6Al-4V alloys  

International Nuclear Information System (INIS)

Minor addition of B to the Ti-6Al-4V alloy reduces the prior #beta# grain size by more than an order of magnitude. TiB formed in-situ in the process has been noted to decorate the grain boundaries. This microstructural modification influences the mechanical behavior of the Ti-6Al-4V alloy significantly. In this paper, an overview of our current research on tensile properties, fracture toughness as well as notched and un-notched fatigue properties of Ti-6Al-4V-xB with x varying between 0.0 to 0.55 wt.% is presented. A quantitative relationship between the microstructural length scales and the various mechanical properties have been developed. Moreover, the effect of the presence of hard and brittle TiB has also been studied.

2010-07-01

343

Mechanical Properties and Thermal Shock Resistance of Refractory Self-Reinforced -SiAlONs Using Barium Aluminosilicate as an Additive  

British Library Electronic Table of Contents (United Kingdom)

Yb-, Y-, Yb/Y-, and Yb/Nd-doped -SiAlON ceramics with 5-wt% barium aluminosilicate (BAS) were synthesized by hot pressing. Typical self-reinforced microstructures were obtained in all investigated -SiAlONs in spite of the type of doped cations. This is attributed to the incorporation of BAS, which could supply suitable liquid phase to promote the anisotropic growth of the -SiAlON grains. All the composites exhibited excellent high-temperature mechanical properties and thermal shock resistance due to the formation of a self-reinforced microstructure and the complete crystallization of BAS additive.

2011-01-01

344

Measurement of the bead profile and microstructural characterization of a CO2 laser welded AISI 904 L super austenitic stainless steel  

British Library Electronic Table of Contents (United Kingdom)

Laser welding of AISI 904 L super austenitic stainless steel using a diffusion cooled slab 3.5kW CO2 laser and employing two different shielding gases, namely argon and helium, was carried out. The laser weld bead profile depends on various parameters such as beam power (BP), travel speed (TS) and focal position (FP) of the laser spot. These parameters have to be selected suitably to obtain the desirable output. The cross sectioned area of the bead profiles measured using an optical microscope to determine the bead width and depth of penetration. X-ray diffraction used for phase identification confirmed that the weld structure was fully austenitic and dendritic. Hardness was observed to increase in the weld bead with respect to the parent metal and it was related to the microstructural ref...

2010-01-01

345

Mapping subcortical diffusivity. Application to brain development. Presidential award proceeding  

International Nuclear Information System (INIS)

We studied age-related microstructural changes in the subcortical white matter from adolescence to middle age in 16 healthy male subjects (age range: 12 to 47 years) using diffusion-weighted magnetic resonance (MR) imaging (DWI). Mean diffusivity (MD) of subcortical white matter was mapped onto the overlying cortical surface using our original method. The mean MD values within 76 cortical regions were measured using atlas-based gray matter segmentation and then correlated with age. A significant negative correlation with age was observed in subcortical MD values in several cortical regions, primarily over the bilateral temporal and occipital lobes. Our results demonstrated subcortical microstructural change in postadolescence that may reflect continuing myelination. (author)

2007-01-01

346

Locally resonant acoustic metamaterials with 2D anisotropic effective mass density  

British Library Electronic Table of Contents (United Kingdom)

A two-dimensional (2D) lattice model with anisotropic resonant microstructures is found to provide an anisotropic band gap structure. A 2D continuum with anisotropic effective mass density is introduced to represent this lattice system. Two methods are proposed to derive the equivalent continuum. In the first method, the effective mass density of the equivalent continuum is obtained by matching the dispersion relations for harmonic waves propagating in the principal directions. The second approach employs an approximate estimation of the effective mass density by volume-averaging an effective mass that represents the resonant microstructure. For both equivalent continuum models, the effective mass density is frequency-dependent and may become negative in certain frequency ranges. Subsequen...

2011-01-01

347

Isothermal sheet formability and microstructure study of rolling processed magnesium alloy AZ31  

Energy Technology Data Exchange (ETDEWEB)

Applications of magnesium alloys are motivated mainly by their lightweight. However, manufacturing cost should also be evaluated when considering applying them. From this point of consideration, adoption of sheet forming processes, which previously have not been heavily researched, should be an option. This paper is intended to pioneer the study of the formability of magnesium alloy AZ31 out of rolled sheets at elevated temperatures. The rolled microstructures are examined and correlated with their formability. Post-forming conditions will also be investigated. The tool employed to perform the sheet forming experiments was a punchless die-setting which used pressurized gas to press the sheet into a female die cavity. This technique applied to Mg-alloy is unconventional and warrants attention for its potential utilization in the industry. (orig.)

2003-07-01

348

Influence of sputtering parameters and nitrogen on the microstructure of chromium nitride thin films deposited on steel substrate by direct-current reactive magnetron sputtering  

International Nuclear Information System (INIS)

Chromium nitride thin films were deposited on SA-304 stainless steel substrates by using direct-current reactive magnetron sputtering. The influence of process conditions such as nitrogen content in the fed gas, substrate temperature, and different sputtering gases on microstructural characteristics of the films was investigated. The films showed (200) preferred orientation at low nitrogen content (< 30%) in the fed gas. The formation of Cr_2N and CrN phases was observed when 30% and 40% N_2 were used, with a balance of Ar, respectively. Field emission scanning electron microscopy and atomic force microscopy were used to characterize the morphology and surface topography of the thin films, respectively. Microhardness tests showed a maximum hardness of 16.95 GPa for the 30% nitrogen content.

2010-08-02

349

Experimental characterisation and modelling of crack initiation and short crack propagation for fatigue life prediction of a #beta#-titanium alloy  

International Nuclear Information System (INIS)

Up to 90% of the life time of cyclically loaded components is determined by short crack initiation and propagation. This stage of the fatigue damage process is strongly influenced by microstructural features, e.g. grain boundaries and crystallographic grain orientation. Therefore LEFM can not be applied in a reasonable manner explaining the demand for a mechanism-related modelling method. The present study deals with mechanical testing and microstructural examinations applied to the relatively new #beta#-titanium alloy LCB. The results are used as data base to develop a new short crack model that is based on the model of Navarro and de los Rios. By using various techniques such as electron back-scattered diffraction and finite-element calculations the origin of crack initiation is revealed and the characteristics of crack propagation is determined. (orig.)

2000-02-24

350

Effects of modification on microstructure and properties of ultrahigh carbon (1.9wt.% C) steel  

British Library Electronic Table of Contents (United Kingdom)

The effects of a modifier that contains Rare Earths (RE), low melting point alloy (Al-Bi-Sb) and Ca-Si alloy on an ultrahigh carbon steel containing 1.9wt.% C were studied. Microstructure characterization was carried out with optical microscopy (OM) and scanning electronic microscopy (SEM) combined with energy-dispersive spectrometry (EDS). Upon modification, the continuous eutectic carbide network structure was broken up and changed to a partly isolated and finer blocky structure in the as-cast alloy. Differential scanning calorimetry (DSC) revealed that the eutectoid temperature increased and the eutectic temperature decreased for the modified alloy. Modification also improved the impact toughness of the tempered steel, with a significant increase from 6.5 to 12.6Jcm^-^2, despite the har...

2011-01-01

351

Effect of intergranular glass on phase relation of Nd-#alpha#-sialon  

International Nuclear Information System (INIS)

Quantitative analytical electron microscopy study of dopant distribution in the microstructure of selected Nd-#alpha#-sialon samples revealed the presence of relatively large amounts of glassy phase at quadruple pockets, which exhibited a common composition similar to a melilite solution. Al segregants were depleted from adjacent grain boundaries to satisfy the 'stoichiometry' of such glass. Existence of this glass results in significant deviation of the Nd-#alpha#-sialon composition from the expected values, which shifts the #alpha#-#beta#-sialon phase boundary. Only extra Nd_2O_3 additives enable a monolithic #alpha#-sialon microstructure. The absence of similar glass in Yb-#alpha#-sialon materials keeps the phase relations from such deviations.

2006-04-01

352

Effect of heat treatment on tensile properties and fracture toughness of two-phase #alpha#+#beta# titanium alloy Ti-6Al-2Mo-2Cr  

International Nuclear Information System (INIS)

In the paper results of the investigation on the effect of microstructure on room temperature tensile properties and fracture toughness of two-phase #alpha#+#beta# titanium alloy Ti-6Al-2Mo-2Cr have been presented. Microstructure has been varied by changes in the cooling rate from the solution treatment temperature and aging time and temperature. Mechanical properties examined show dependence on the treatment conditions, especially aging conditions. It has been attributed mainly to the amount and morphology of #alpha# phase obtained after heat treatment. The higher volume fraction of lamellar #alpha# structure, the higher fracture toughness. (author)

1998-05-17

353

Effect of Alcohol Solvent on Mixing of Fine Ceramic Powders and Some Properties of Ceramic-Based Composites; Seramikkusu fukugokei ni okeru bifunmatsu kongo ni oyobosu arukoru youbai no eikyo to shoketsutai no seishitsu  

Energy Technology Data Exchange (ETDEWEB)

Effect of alcohol solvent in mixing process on process on the microstructure and sintering behavior of ceramic-based composites was inestigated in detail. The mixture of fine ceramic powders was prepared through the conventional ball-milling method with various alcohol media. The particle distributions of fine ceramic powders were strongly dependent on the kind of alcohol employed during ball-milling. Ceramic-based composites were fabricated by hot-pressing the mixture of fine ceramic powders. Their microstructures and some mechanical properties of the ceramic-based composites were evaluated. It was found that the viscosity of alcohol, surface tension and contat angle greatly affect the sinterbility and some of the mechanical properties of ceramic-based somposites. (author)

1999-07-01

354

Effect of Al and AlP on the microstructure of Mn-30 wt.%Si alloy  

Energy Technology Data Exchange (ETDEWEB)

Effect of Al and AlP particles on the microstructure of near eutectic Mn-Si alloy (Mn-30 wt.%Si) was studied by Electron Probe Micro-analyzer (EPMA) and Differential Scanning Calorimeter (DSC). Crystal lattice correspondence analyses show that both Al and AlP have good lattice matching coherence relationships with MnSi phase, and the addition of Al and AlP particles results in an abnormal eutectic structure, i.e. the eutectic constitution MnSi and Mn{sub 5}Si{sub 3} precipitate separately: MnSi precipitates firstly, and then the Mn{sub 5}Si{sub 3} phase.

2008-04-15

355

Development of plasticity processing of magnesium alloys  

Energy Technology Data Exchange (ETDEWEB)

Recent developments on plastic forming technology of magnesium alloys are presented. Attempts have been undergoing with an aim at forming magnesium alloy parts at lower temperatures. It is believed that fine microstructure magnesium alloys usually have much higher plasticity at lower temperatures and even room temperatures. Extrusion is a method to form magnesium profile products and tube products, which is also one of the effective ways to make fine microstructure magnesium alloys. Superplasticity forming is another method to form high plasticity magnesium alloys. Hot forming of magnesium sheet parts is an important process to form magnesium products. Some developments related to above issues are discussed in the present paper. (orig.)

2003-07-01

356

Development of a new Pb-free solder: Sn-Ag-Cu  

Energy Technology Data Exchange (ETDEWEB)

With the ever increasing awareness of the toxicity of Pb, significant pressure has been put on the electronics industry to get the Pb out of solder. This work pertains to the development and characterization of an alloy which is Pb-free, yet retains the proven positive qualities of current Sn-Pb solders while enhancing the shortcomings of Sn-Pb solder. The solder studied is the Sn-4.7Ag-1.7Cu wt% alloy. By utilizing a variety of experimental techniques the alloy was characterized. The alloy has a melting temperature of 217{degrees}C and exhibits eutectic melting behavior. The solder was examined by subjecting to different annealing schedules and examining the microstructural stability. The effect of cooling rate on the microstructure of the solder was also examined. Overall, this solder alloy shows great promise as a viable alternative to Pb-bearing solders and, as such, an application for a patent has been filed.

1995-02-10

357

Creep performance and microstructure of the iron alloy Alloy 800 HT  

International Nuclear Information System (INIS)

The examination of the high-temperature properties of the alloy Alloy 800HT has shown that both the creep performance and the microstructure of the material can be purposefully set by the initial heat treatment. At the high temperatures applied, (700-900 C), a rapid softening process sets in induced by carbide precipitation, stabilization, and coarsening. This softening process causes creep velocities strongly accelerating as a function of duration of the heat treatment prior to the creep test. The identified cause of the softening effect is a change in particle size that could be verified by SEM and TEM. It is shown that two different carbide precipitate size classes are responsible for the softening effect. While the precipitates dectable by TEM become effective primarily via interactions with dislocations, the carbide precipitates detectable only by SEM contribute to a hardening of the grain boundaries and the matrix.(orig./CB)

1997-11-28

358

Creating bulk nanocrystalline metal.  

Energy Technology Data Exchange (ETDEWEB)

Nanocrystalline and nanostructured materials offer unique microstructure-dependent properties that are superior to coarse-grained materials. These materials have been shown to have very high hardness, strength, and wear resistance. However, most current methods of producing nanostructured materials in weapons-relevant materials create powdered metal that must be consolidated into bulk form to be useful. Conventional consolidation methods are not appropriate due to the need to maintain the nanocrystalline structure. This research investigated new ways of creating nanocrystalline material, new methods of consolidating nanocrystalline material, and an analysis of these different methods of creation and consolidation to evaluate their applicability to mesoscale weapons applications where part features are often under 100 {micro}m wide and the material's microstructure must be very small to give homogeneous properties across the feature.

2008-10-01

359

Anisotropic properties of magnesium sheet AZ31  

Energy Technology Data Exchange (ETDEWEB)

Car weight corresponds directly to fuel consumption and driving performance. So in order to improve the fuel efficiency and performance of a car the weight has to be reduced. Magnesium as a light metal offers a wide range of weight saving opportunities, especially Magnesium wrought alloys with their improved mechanical properties have a high potential for structural applications. Mechanical properties in terms of their quality and anisotropy are dependent on the microstructure of the material and can be characterized by their degree of inhomogeneity, their grain size distribution and their crystallographic texture. Therefore the orientation distribution of grains, the grain size, its size distribution, the chemical composition (precipitates) itself influence the mechanical parameters and their anisotropy. In this presentation first results of mechanical anisotropy are given: differences in yield stress, r-values and their relation to the texture. This correlation ...

2003-07-01

360

(#alpha#+#beta#) - Sialon ceramic composites  

International Nuclear Information System (INIS)

(#alpha#+#beta#)-SiALON ceramic composites are industrially important materials. Due to their unique chemistry, crystal structure and microstructural features, #alpha#-SiAlON has superior hardness while #beta#-SiALON offers high strength and toughness. The combination of the two phases enables materials engineers to design a ceramic where the physical properties of the composite can be tailored to a particular application. This article presents a general review of the crystal structures, fabrication and properties of the (#alpha#+#beta#)-SiALON composites with special highlights outlining how microstructural tailoring can control the properties of these advanced ceramic alloys. Copyright (1997) Institute of Metals and Materials Australasia Ltd.

361

The triaxial motion in Mo isotopes  

Energy Technology Data Exchange (ETDEWEB)

The nuclear shapes of transitional Mo isotopes are calculated by means of a model based on the cranking approximation and the Strutinksy method. The recent experimental results of the high-spin spectroscopy and lifetime measurement of [sup 87]Mo are studied in detail and explained by the evolution of the [gamma]-deformation with the quasiparticle configurations. The shape calculations with the modified-harmonic-oscillator potential give a critical neutron number N [>=] 47 for the spherical shape of the Mo isotopes. (orig.)

1993-11-22

362

The triaxial motion in Mo isotopes  

International Nuclear Information System (INIS)

The nuclear shapes of transitional Mo isotopes are calculated by means of a model based on the cranking approximation and the Strutinksy method. The recent experimental results of the high-spin spectroscopy and lifetime measurement of "8"7Mo are studied in detail and explained by the evolution of the #gamma#-deformation with the quasiparticle configurations. The shape calculations with the modified-harmonic-oscillator potential give a critical neutron number N #>=# 47 for the spherical shape of the Mo isotopes. (orig.).

363

Supersonic flutter of composite sandwich panels  

Science.gov (United States)

A flutter-motion equation is presently derived for a 2D composite sandwich panel considering the total lateral displacement of the plate as the sum of the displacement due to bending of the plate, and that which is due to shear deformation at the core. The effects of core thickness and stacking sequence of the faces on the flutter boundary of the plate are discussed; it is shown that the sandwich panel greatly improves the flutter boundary over that of a composite laminate panel, provided it has sufficient core thickness.

1992-12-01

364

Superconducting properties and structural transition in compounds with an A-15 lattice  

International Nuclear Information System (INIS)

The dependence of Tsub(c) on composition and deformation is calculated and compared with the corresponding dependence for Tsub(m). It is shown that superconducting and structural properties of A-15 compounds can be described, at least qualitatively, by the quasi-one-dimensional model previously developed by the authors. The superconductivity mechanism is assumed to be analogous to the BCS theory. The upper critical field Hsub(c2) of the V_3Si or Nb_3Sn compounds is found to be much greater than that in V or Nb.

365

Structure analysis of ferrite in deformed pearlitic steel by means of X-ray diffraction method with synchrotron radiation  

Energy Technology Data Exchange (ETDEWEB)

Structure of ferrite in drawn pearlitic steel containing 0.9 mass% C was investigated with X-ray diffraction technique using synchrotron radiation. In the detailed analysis of diffraction peaks of ferrite during the drawing process, it was experimentally revealed that the transformation of ferrite from bcc to bct due to the supersaturation of carbon in ferrite of heavily drawn pearlitic steel.

2004-07-15

366

Structure analysis of ferrite in deformed pearlitic steel by means of X-ray diffraction method with synchrotron radiation  

International Nuclear Information System (INIS)

Structure of ferrite in drawn pearlitic steel containing 0.9 mass% C was investigated with X-ray diffraction technique using synchrotron radiation. In the detailed analysis of diffraction peaks of ferrite during the drawing process, it was experimentally revealed that the transformation of ferrite from bcc to bct due to the supersaturation of carbon in ferrite of heavily drawn pearlitic steel.

2004-07-01

367

Solution of Bohr's collective Hamiltonian for transitional odd-mass nuclei  

International Nuclear Information System (INIS)

A numerically feasible method, based on the use of deformed phonons, is developed for the diagonalization of the collective quadrupole Hamiltonian for a system with an odd particle coupled to an anharmonic even core. Examples: the transition from prolate to oblate via #gamma#-unstable shapes and furthermore the hsub(9/2) spectra of the nuclei "1"8"7Ir and "1"9"7Tl. (Auth.).

368

Slow strain-rate testing of Alloy 800 in molten-nitrate salts  

Energy Technology Data Exchange (ETDEWEB)

An experimental technique has been developed to examine the interaction between deformation and the exposure of certain high temperature structural alloys to oxidizing molten salt environments. The experimental program involved performing a series of long-term tensile tests over a wide range of strain rates. Fracture strain reduction in area and ultimate strength (UTS) were monitored as parameters indicative of an alloy's susceptibility to environmental degradation. For Incoloy Alloy 800 tested at 600/sup 0/C in the salt medium and at initial strain rates between 2 x 10/sup -7/ sec/sup -1/ and 1 x 10/sup -5/ sec/sup -/1 no appreciable loss of ductility, as measured by reduction in area, was observed relative to control specimens tested in air at the same temperature and strain rates. Similarly, fracture strain and UTS were essentially unaffected by exposure to the oxidizing environment. The structure of the oxide film formed by contact of the specimens to ...

1982-01-01

369

On the triaxial deformation in transitional odd-A nuclei  

International Nuclear Information System (INIS)

The essential difference as well as the apparent identity between the triaxial-rotor model and the gamma-vibrational model have been discussed. From the gamma decay mode, the [19/2"-]_1 states of the j = 11/2"- family in "1"8"7Ir and "1"8"9Ir have been identified as the K = j + 4 states, the presence of which contradicts the particle plus triaxial-rotor model. (author).

370

On the relation between Tsub(c) and structural properties of the A-15 compounds  

International Nuclear Information System (INIS)

It is shown that both the Tsub(c) and Tsub(m) dependences on the deformations and composition for the A-15 compounds can be described at least qualitatively in the quasi-one-dimensional model developed by the authors previously. The mechanism for the superconductivity is supposed to be the same as in the BCS theory. The upper critical field near Tsub(c) is obtained. (author).

371

New approach to the design of LMFBR liners  

Energy Technology Data Exchange (ETDEWEB)

The reconstruction of steel lining of the FFTF reactor building is described. The cold part of the lining has a simple structure and represents a steel sheet of 6.35 mm thickness welded to I-shaped imbedded in concrete, the hot part is meant for resisting the hot sodium contacting with it. The reconstruction has been reduced to the substitution of usual lining, the sheets of which are fixed in such a way that dangerous strains in metal arising at evaporation are excluded by the new structure admitting sheet deformation.

1981-01-01

372

Modelling of gravity changes in mining areas  

Energy Technology Data Exchange (ETDEWEB)

The numerical modelling of gravity changes resulting from the simultaneous effects of mass relocation and rock deformation is described. The method is supported by FEMMA (Finite Element Method for Multipurpose Applications) software, and has been used for modelling expected gravity changes in a large open pit coal mine in Poland. The results are in good agreement with conventional calculations of gravity changes for a simple geometry of relocated mass. 10 refs., 6 figs., 2 tabs.

1995-10-01

373

Measurement of the electrical resistivity of the lithium isotopes at low temperatures  

Energy Technology Data Exchange (ETDEWEB)

The electrical resistivity at low temperatures (T = 10 to 90 K) of the lithium isotopes /sup 6/Li and /sup 7/Li and of an isotopic mixture /sup 7 +6/Li has been studied. The specimens contained a small amount of chemical impurities. An appreciable difference was observed in the temperature dependence of the resistivity produced both by deformation of the phonon spectrum, related to the change in isotopic composition, and by the presence of chemical impurities making the nonequilibrium part of the electron distribution function more isotropic.

1982-03-01

374

Lithology and evolution of the crust-mantle boundary region in the southwestern Basin and Range province  

Energy Technology Data Exchange (ETDEWEB)

Seismic transects in this area show a strongly reflective Moho of generally low relief, which, in the area of modern transects, consists of a thin zone (< 2 km thick) of short reflectors. The upper mantle is transparent and has a P{sub n} of 7.8-8.0 km/s similar to much of the western US. A lower crustal zone, 2-13 km thick, has variable internal reflectivity and a relatively low velocity of 6.6-6.8 km/s. Upper mantle peridotite xenoliths show both ductile and brittle deformational features and have structures and composition affected by magmatic intrusion; intrusions form complex dike systems and extensive zones of grain boundary infiltration in peridotite xenoliths. Whereas melt infiltration preceded and followed ductile deformation, brittle deformation, represented by closely spaced joint systems and faults, followed ductile deformation and is related to the youngest magmatic episodes. Lower ...

1990-01-10

375

Laboratory test on soil-structure interaction with backfill soil using non-linear material (embedment effect tests on soil-structure interaction)  

International Nuclear Information System (INIS)

A series of Model Tests of Embedment Effect on Reactor Buildings has been carried out by the Nuclear Power Engineering Corporation (NUPEC), under the sponsorship of the Ministry of International Trade and Industry (MITI) of Japan. Seismic response of an embedded reactor building is greatly affected by the non-linearity of the backfill soil. However, quite few experimental data have been obtained so far. The objective of this study is to qualitatively evaluate the non-linear behavior of the backfill soil through shaking table tests. Its effects to the seismic response of a reactor building constructed at a soft rock site can be made clear through the tests. Non-linear effects of the backfill soil on the seismic response of the embedded reactor building model were evaluated experimentally. Based on the sinusoidal and seismic wave excitation tests, the following conclusions were obtained regarding the changes in vibrational characteristics of the building model which occurred according to ...

1993-08-15

376

Investigation of lifetimes in the dipole band of {sup 139}Sm  

Energy Technology Data Exchange (ETDEWEB)

Lifetimes have been measured for a dipole band in {sup 139}Sm using DSAM. The deduced B(M1) and B(E2) values as well as B(M1)/B(E2) ratios are compared with calculations in the framework of the TAC (Tilted Axis Cranking) and SPAC (Shears mechanism with Principal Axis Cranking) models. The dipole band in {sup 139}Sm can be considered as a magnetic rotational band with a prolate or triaxial nuclear deformation. (orig.)

2008-09-15

377

Factors affecting the tensile ductility of a metastable beta titanium alloy  

International Nuclear Information System (INIS)

The ductility of extruded heavy-section Ti-base--Mo--V--Fe--Al alloy was studied. Metallographic evidence for the large effect of grain size on ductility is presented. Fracture was found to occur in large-grain material after less deformation than in smaller grain size specimens.

378

Fabrication of magnesium alloy (AZ31) sheet by extrusion  

Energy Technology Data Exchange (ETDEWEB)

In order to investigate the extrusion characteristics of magnesium alloy (AZ31), a computer simulation was attempted. Tensile properties of as-cast billet with different strain rates were incorporated into the simulation. The results showed a great change in distribution of stress and strain at near die region by the ram travel. It was found that the average grain size at longitudinal edge of the extruded sheet was smaller than that at center region, which might be attributed to recrystallization caused by severe plastic deformation. (orig.)

2004-07-01

379

Characterization of Adaptive Optics at Keck Observatory  

Energy Technology Data Exchange (ETDEWEB)

In this paper, the adaptive optics (AO) system at Keck Observatory is characterized. The AO system is described in detail. The physical parameters of the lenslets, CCD and deformable mirror, the calibration procedures and the signal processing algorithms are explained. Results of sky performance tests are presented: the AO system is shown to deliver images with an average Strehl ratio of up to 0.37 at 1.59 {micro}m using a bright guide star. An error budget that is consistent with the observed image quality is presented.

2003-07-24

380

Battery side terminal  

Energy Technology Data Exchange (ETDEWEB)

A side terminal battery is described comprising: a casing having a side wall made from a moldable material; and a plug formed of relatively deformable, electrically conductive, corrosion resistant material molded into the side wall to form a seal between the interior and exterior of the casing and including a battery terminal insert embedded therein so as to be exposed at the exterior of the casing and isolated, by the plug, from the interior of the casing.

1988-03-08

381

Anelastic strain recovery of amorphous metals. [80 Pd--20 Si; 80 Fe--13 P--7 C; 60 Cu--40 Zr  

Science.gov (United States)

This paper describes the anelastic strain recovery and the strain hardening of amorphous metals and presents the experimental result that creep deformation is represented by a viscoelastic model consisting of rheological elements. Materials studied were 80Pd--20Si, 80Fe--13P--7C, and 60 Cu--40 Zr. (DLC)

1976-08-01

382

Alignments of multi-quasiparticle bands and seniority-dependent reduced pairing  

Energy Technology Data Exchange (ETDEWEB)

Pairing correlations in multi-quasiparticle states in deformed nuclei are expected to be reduced because of blocking. New intrinsic states and their associated rotational bands have been identified allowing comparisons to be made as a function of seniority and between nuclei. The possible effects of the reduced pairing on the collective rotation, and its manifestation in terms of alignment, are discussed. 13 refs., 2 figs.

1994-09-01

383

26 years of operating experience with a boiler drum manufactured from a high-temperature copper-nickel-molybdenum steel. 26 Jahre Betriebserfahrungen mit einer Kesseltrommel aus einem warmfesten Kupfer-Nickel-Molybdaen-Stahl  

Energy Technology Data Exchange (ETDEWEB)

The creep behaviour of boiler drums of CuNiMo steels depends on the ratio of the alloys, the heat treatment and the processing technology. Reduction in deformability must be expected but, under optimum conditions, this does not lead to a critical material condition. The appropriate material tests are indispensable. (orig.)

1993-05-01

384

Triple ion-beam studies of radiation damage effects in a 316LN austenitic alloy for a high power spallation neutron source  

Energy Technology Data Exchange (ETDEWEB)

Austenitic 316LN alloy was ion-irradiated using the unique Triple Ion Beam Facility (TIF) at ORNL to investigate radiation damage effects relevant to spallation neutron sources. The TIF was used to simulate significant features of GeV proton irradiation effects in spallation neutron source target materials by producing displacement damage while simultaneously injecting helium and hydrogen at appropriately high gas/dpa ratios. Irradiations were carried out at 80, 200, and 350 C using 3.5 MeV Fe{sup ++}, 360 keV He{sup +}, and 180 keV H{sup +} to accumulate 50 dpa by Fe, 10,000 appm of He, and 50,000 appm of H. Irradiations were also carried out at 200 C in single and dual ion beam modes. The specific ion energies were chosen to maximize the damage and the gas accumulation at a depth of {approximately} 1 {micro}m. Variations in microstructure and hardness of irradiated specimens were studied using transmission electron microscopy (TEM) and a nanoindentation ...

1997-09-01

385

Through Weld Inspection of Wrought Stainless Steel Piping Using Phased Arrays  

Energy Technology Data Exchange (ETDEWEB)

Outline: Discuss far-side weld problem and phased array techniques applied. Describe laboratory work on flawed piping specimens using L- and S-wave arrays and provide synopsis of results. Discuss conclusions ofr capability of phased array as applied to austenitic welds. Research Approach: Evaluate phased arrays on unifornly-welded piping specimens. Apply best methods to non-uniform welds. Correlate acoustic responses as function of weld microstructures.

2004-12-31

386

The influence of process parameters on forged magnesium alloys  

Energy Technology Data Exchange (ETDEWEB)

Two extruded magnesium alloys, AZ31 and AZ61 were selected to evaluate the influence of process parameters on the material forgeability. The processing parameters considered for forging magnesium alloys were: compression load in the range 55 KN to 60 KN and forging temperature, in the range of ambient temperature to 300 C. Uniaxial compression tests were conducted to establish the strain-temperature relationship. The influences of process parameters on the microstructure were also evaluated. (orig.)

2003-07-01

387

The influence of inclusion spacing and microstructure on the fracture toughness of the secondary hardening steel AF1410  

Energy Technology Data Exchange (ETDEWEB)

An approach to the ductile fracture of ultra high strength steels has been evaluated. According to this approach the critical crack tip opening, delta/sub IC/, will scale with X/sub 0/(R/sub V//R/sub I/vertical bar/sub R//sub 0/. X/sub 0/ is an average inclusion spacing and (R/sub V/R/sub I/)vertical bar/sub R//sub 0/ is the void radius divided by the radius of the inclusion nucleating the void evaluated at the average inclusion size. AF1410 was selected to test this approach because it has exceptionally high fracture toughness on aging at 510/sup 0/C and because its toughness varies markedly with aging temperature. The results from this and earlier work showed a linear relationship exists between delta/sub IC/ and X/sub 0/(R/sub V//R/sub I/)vertical bar /sub R//sub 0/ for values of delta/sub IC/ ranging from about 8 ..mu..m to 60 ..mu..m. The values of (R/sub V//R/sub I/)vertical bar /sub R//sub 0/ for AF1410 aged at 425/sup 0/C and 510/sup 0/C differed by a factor of two. Because the ...

1987-07-01

388

The influence of compound admixtures on the properties of high-content slag cement  

Energy Technology Data Exchange (ETDEWEB)

Based on the activation theory of alkali and sulfate, the influence of compound admixtures on the properties of high-content slag cement was studied by testing the strength, pore structure, hydrates, and microstructure, Test results show that compound admixtures can obviously improve the properties of high-content slag cement. The emphasis of the present research is two-fold: substituting gypsum with anhydrite and calcining gypsum. These both can improve early and later performance.

2000-01-01

389

TEM-investigations of erosion craters caused by electrical discharge; TEM-Untersuchungen an Erosionskratern, die durch elektrische Entladungen erzeugt werden  

Energy Technology Data Exchange (ETDEWEB)

Craters were produced in the surface of a Pt-specimen by plasma discharge. Using a Focussed Ion Beam (FIB), TEM-foils of the cross section of the craters were prepared in order to examine the microstructural changes occurring as a result of the discharge impact. The molten material pushed to the edge of the craters was able to be identified. The grains beneath the craters reached the surface of the crater by a mechanism of epitaxial growth. (orig.)

2005-11-01

390

Strontium as modifier for AlSi and AlSiCu alloys  

International Nuclear Information System (INIS)

The optimum of strontium amount for good modification of AK7, AK9, AK11, AK52, AK104 alloys was determined on the base of the analysis of microstructural changes. The stability of the modifier was investigated on the way of successive remelting of billets. The influence of amount of modifier on the impact strength of the alloys was established. (author)

391

Radial distribution of bonded fission gas in mixed carbide fuel pins  

International Nuclear Information System (INIS)

The fission gas xenon bonded in bubbles, in pore, and in the lattice of mixed carbide fuels is measured by electron-probe microanalysis. Radial xenon distribution and release curves are determined and are calibrated by gas chromatography of the bonded fission gas and by burnup analysis in the respective pin sections of the irradiation experiments FR2 6A and 6C, Mol 11/K 2, and DFR 330/1. The results are correlated to the microstructure of the fuel, bonding medium, temperature, and burnup. (Auth.).

1979-01-01

392

Plan-view transmission electron microscopy of crack tips in bulk materials  

Energy Technology Data Exchange (ETDEWEB)

A focused ion beam (FIB) system has been applied to prepare a thin foil specimen of Si, MgO and alumina which contained cracks in the plan of foil. It was possible to observe a much larger area at and near a crack tip than has been hitherto possible. FIB was also applied to observation of microstructure near a crack tip evolved during severe rolling contact fatigue in a steel.

1996-12-01

393

Microstructure evolution and strength-reduction in area balance of ultrafine-grained steels processed by warm caliber rolling  

British Library Electronic Table of Contents (United Kingdom)

Ultrafine grained steels with different carbon contents were produced through warm caliber rolling and evaluated for their stress-strain behavior along with the reduction in area. It was found that the reduction in area-tensile strength balance is far better than the conventional ferrite+pearlite steels and even superior to bainitic steels for all materials tested in the present study.

2006-01-01

394

Metallographic preparation and characterisation of the As-cast Ni-based superalloy GMR 235; Metallographische Praeparation und Charakterisierung der Nickelbasis-Superlegierung GMR 235 im Gusszustand  

Energy Technology Data Exchange (ETDEWEB)

In this work a Ni-based superalloy GMR 235 was investigated. We determined convenient metallographic methods for preparation of bulk metallographic specimens, extraction carbon replicas, transparent metallic foils and minor phase extraction. In addition, the alloy microstructure was characterised using different metallographic techniques. (orig.)

2004-08-01

395

In situ observation of fatigue crack retardation in banded ferrite?pearlite microstructure due to crack branching  

British Library Electronic Table of Contents (United Kingdom)

This paper reports the results of in situ observation of fatigue crack growth in a ferrite?pearlite steel. Stress intensity factor range (?K) decreasing/increasing and constant-?K fatigue tests have been carried out. In banded pearlite orientation, intense crack branching was observed which leads to fatigue crack retardation. Crack closure during the test was monitored to understand the fatigue crack growth behaviour.

2006-01-01

396

High resolution transmission electron microscopy of a #beta#'-sialon-TiN nanocomposite  

International Nuclear Information System (INIS)

TEM and HRTEM have been used to characterise the microstructures of materials formed by hot-pressing silicon nitride with an Al_2O_3-SiO_2-TiO_2 densification aid system, to form #beta#'-sialon-TiN composites in which the TiN particles are of 20-100 nm dimension. (orig.).

1992-06-21

397

Effects of initial microstructure and helium production on radiation hardening in F82H Steels  

International Nuclear Information System (INIS)

Full text of publication follows: Fission neutron irradiation to steels doped with isotope boron-10 is frequently conducted to study effects of the helium production on mechanical properties. The intrinsic mechanical properties of F82H steels could have been changed due to the boron doping. Recently, we reported that co-doping with boron and nitrogen to F82H (F82H+B+N) improved the mechanical properties of F82H doped only with boron. The mechanical properties of F82H+B+N are successfully comparable with the non-doped F82H before irradiation. In order to evaluate the effects of initial microstructure and helium production on radiation hardening, F82H and F82H+B+N were irradiate d Specimens used in this study were standard F82H martensitic steels, F82H steels doped with 60 mass ppm 10B and 200 ppm N (F82H+10B+N) and F82H steels doped with 60 mass ppm 11B and 200 ppm N (F82H+11B+N). Initial microstructures were changed by tempering conditions, and ...

2007-12-10

398

Effect of grain boundary microstructures of brittle fracture in polycrystalline molybdenum  

Energy Technology Data Exchange (ETDEWEB)

Superplasticity can be generally achieved by grain boundary sliding (GBS). The GBS in polycrystalline materials sometimes accompanies with intergranular fracture because of stress concentrations at triple points and/or GB irregularities. To develop the superplastic flow, it is necessary to suppress the intergranular cracking. In the present study, therefore, polycrystalline molybdenum with distinct GB microstructures, such as grain boundary character distribution (GBCD), has been employed to clarify the relationship between fracture behaviour and GB microstructures. Microstructures were analyzed using a FE-SEM/EBSP/OIM system prior to 4-points bending tests at 77K, thereafter, crack propagation was observed. The main results obtained are as follows. Stress fluctuations on stress - strain curves were observed for specimens with random oriented grains, whereas such behaviour rarely occurred for ones with textured grains. ...

1999-07-01

399

Effect of aging on the pitting corrosion behavior in Al-Li alloys  

Energy Technology Data Exchange (ETDEWEB)

In the present work, electrochemical measurements and corrosion tests in NaCl solutions were carried out to study the effect of aging treatments on pitting corrosion behavior in a 8090 alloy and its high purity Al-Li binary alloy analogue. The pitting corrosion characteristics and corrosion resistance of the 8090 alloy have been determined in relation to precipitation microstructures. (orig.).

1990-06-01

400

Computer simulation of martensitic transformations  

Energy Technology Data Exchange (ETDEWEB)

The characteristics of martensitic transformations in solids are largely determined by the elastic strain that develops as martensite particles grow and interact. To study the development of microstructure, a finite-element computer simulation model was constructed to mimic the transformation process. The transformation is athermal and simulated at each incremental step by transforming the cell which maximizes the decrease in the free energy. To determine the free energy change, the elastic energy developed during martensite growth is calculated from the theory of linear elasticity for elastically homogeneous media, and updated as the transformation proceeds.

1993-11-01

401

A study of the effect of Yttria additions on densification of #beta#-sialon  

International Nuclear Information System (INIS)

In this paper the effect of adding commercially pure yttria concentrate and yttrium carbonate concentrate (NUCLEMON) on the densification of #beta#-Sialon has been studied. The specimens were sintered in graphite furnace at 1720 and 175 deg C, for 1 hour in a nitrogen atmosphere. Densities of up to 99% of the theoretical density were obtained. Microstructural analyses of the specimens were carried out with the aid of an X ray diffractometer and a scanning electron microscope. (author)

1995-06-10

402

A study of palladium silicide formed by focused ion beam implantation of palladium ions  

Science.gov (United States)

The formation and properties of Pd{sub 2}Si formed by focused ion beam implantation of Pd ions into Si is presented in this thesis. An extensive microstructural study using transmission electron microscopy was undertaken and the as-implanted as well as annealed microstructure is shown. Results of other analysis techniques such as Rutherford back scattering and secondary ion mass spectrometry etc. are also presented. Kinetic information on the growth of Pd{sub 2}Si obtained by both microstructural and resistance measurements indicates that the activation energy for growth of the silicide is around 0.36 to 0.39 eV. This can be compared with the normally reported value of 1.5 eV for Pd{sub 2}Si formed by annealing thin film Pd on Si. The growth of the silicide was found to follow t{sup 1/2} kinetics. Microstructural observation of the as-implanted samples showed extensive in-situ formation of Pd{sub 2}Di ...

1989-01-01

403

A study of palladium silicide formed by focused ion beam implantation of palladium ions  

International Nuclear Information System (INIS)

The formation and properties of Pd_2Si formed by focused ion beam implantation of Pd ions into Si is presented in this thesis. An extensive microstructural study using transmission electron microscopy was undertaken and the as-implanted as well as annealed microstructure is shown. Results of other analysis techniques such as Rutherford back scattering and secondary ion mass spectrometry etc. are also presented. Kinetic information on the growth of Pd_2Si obtained by both microstructural and resistance measurements indicates that the activation energy for growth of the silicide is around 0.36 to 0.39 eV. This can be compared with the normally reported value of 1.5 eV for Pd_2Si formed by annealing thin film Pd on Si. The growth of the silicide was found to follow t"1"/"2 kinetics. Microstructural observation of the as-implanted samples showed extensive in-situ formation of Pd_2Di and also surprisingly ...

404

q-Virasoro algebra, q-conformal dimensions and free q-superstring  

International Nuclear Information System (INIS)

The commutators of standard Virasoro generators and fields generate various representations of the centreless Virasoro algebra depending on a conformal dimension J of the field in question (J is related to the Bargmann index of SU(1,1) generated by L_m, m=0,#+-#1). We introduce the notion of q-conformal dimension for various oscillator realizations of q-deformed Virasoro (super)algebras proposed earlier. We use the field theoretical approach introduced recently in which the q-Virasoro currents L"#alpha# (z) are expressed as Schwinger-like point-split normally ordered quadratic expressions in elementary fields. We extend this approach and probe the elementary fields A(z) (the q-superstring coordinate, momentum and fermionic field) and their powers by the q-Virasoro generators L"#alpha#_m (i.e. we calculate the commutators [L"#alpha#_m,A(z)]) and show that to all of them can be assigned just the standard non-deformed conformal dimension. (orig.).

1996-12-01

405

Trishear fault-propagation folding  

Energy Technology Data Exchange (ETDEWEB)

Previous models of fault-propagation folding used kink-band geometries to approximate folding in front of propagating thrusts. However, kink-band kinematics cannot replicate the curved fold surfaces and complex strain patterns innatural and experimental fault-propagation folds, which also occur in front of steeper reverse and normal faults. Fault-propagation fold hinges tighten and converge downward, forming a triangular zone of penetrative deformation focused on the tip of the propagating fault. The downward convergence of deformation in fault-propagation folds can be modeled as triangular shear zones. Trishear, here defined as distributed, strain-compatible shear in a triangular (in profile) shear zone, provides an alternate kinematic model for fault-propagation folds. Trishear is analogous to simple shear in a tabular shear zone except that area balance in a triangular shear zone requires curved displacement oblique to the fault slip ...

1991-06-01

406

Three-Dimensional Wing Kinematics and Aerodynamic Characteristics of a Beetle in Free Flight  

Science.gov (United States)

Detailed three dimensional wing kinematics and aerodynamic characteristics are experimentally presented for the free flight of a beetle, Allomyrina dichotoma, which has a pair of elytra (fore wings) and hind wings. The kinematic parameters of the wing motion, such as the wing tip trajectory, angle of attack, torsion angle, and camber deformation, are obtained from a 3D reconstruction technique that involves the use of two or three synchronized high-speed cameras to digitize various points marked on the wings. Our data show outstanding characteristics of wing deformation and flexibility in the free flight of the beetle. To find out the mechanism of aerodynamic force, the leading edge vortex (LEV) and trailing edge vortex (TEV) on both elytron and hind wing were observed by using smoke wire visualization and digital particle image velocimetry (DPIV) technique. Qualitative smoke lines in the region of the most intent vortex shedding demonstrate ...

2010-11-01

407

Thermal imaging on simulated faults during frictional sliding  

CERN Document Server

Heating during frictional sliding is a major component of the energy budget of earthquakes and represents a potential weakening mechanism. It is therefore important to investigate how heat dissipates during sliding on simulated faults. We present results from laboratory friction experiments where a halite (NaCl) slider held under constant load is dragged across a coarse substrate. Surface evolution and frictional resistance are recorded. Heat emission at the sliding surface is monitored using an infra-red camera. We demonstrate a link between plastic deformations of halite and enhanced heating characterized by transient localized heat spots. When sand 'gouge' is added to the interface, heating is more diffuse. Importantly, when strong asperities concentrate deformation, significantly more heat is produced locally. In natural faults such regions could be nucleation patches for melt production and hence potentially initiate weakening during ...

2008-01-01

408

The mouse formin (Fmn) gene: Genomic structure, novel exons, and genetic mapping  

Energy Technology Data Exchange (ETDEWEB)

Mutations in the mouse formin (Fmn) gene, formerly known as the limb deformity (ld) gene, give rise to recessively inherited limb deformities and renal malformations or aplasia. The Fmn gene encodes many differentially processed transcripts that are expressed in both adult and embryonic tissues. To study the genomic organization of the Fmn locus, we have used Fmn probes to isolate and characterize genomic clones spanning 500 kb. Our analysis of these clones shows that the Fmn gene is composed of at least 24 exons and spans 400 kb. We have identified two novel exons that are expressed in the developing embryonic limb bud as well as adult tissues such as brain and kidney. We have also used a microsatellite polymorphism from within the Fmn gene to map it genetically to a 2.2-cM interval between D2Mit58 and D2Mit103. 36 refs., 6 figs., 1 tab.

1997-02-01

409

The effects of gaseous environments on the mechanical failure of polyethylene pipe materials. Annual technical report 1 Nov 80-31 Oct 81  

Energy Technology Data Exchange (ETDEWEB)

Polyethylene gas piping is expected to be in service for times on the order of 50 years depending on service conditions. Therefore research research on piping materials and pipes has two principal objectives: (a) developing methods for predicting when a pipe will fail and (b) improving the material for piping. The prediction of long time failure hinges on the development of short time test methods which relate to long time failure. The improvement in the behavior of current materials also hinges on the use of test methods of short duration relative to the anticipated life time of the pipe in service. One of the primary criterion for an acceptable test method is that it produces the same type of failure as is observed after long time failure in service. It has been found that P.E. pipe material fails in a brittle mode after long periods of time. The failure mode is called brittle because there is little microscopic deformation throughout the pipe; however ...

1981-10-01

410

Structural analysis of piping after a large pipe break in a WWER-440 type reactor  

International Nuclear Information System (INIS)

In the WWER-440 reactor the primary piping consists of six horizontal loops going radially from the pressure vessel, each loop having a horizontal steam generator. In this reactor type the relatively long primary piping with many curved sections requires special attention in order to successfully eliminate the consequences of the design basis accident. Emergency supports are located in appropriate places to restrict the movements of the pipe in 1, 2, 3 or 4 directions depending on the geometry of the pipe near the support. Under normal conditions there is a gap of some centimeters between the pipe and a support so that the pipe can be deformed freely under changing loads. In order to analyse the behaviour of the broken piping system with the support structures a computer code called PIPEBREAK has been written. The main objects in the analyses have been to calculate the deformations of the supports and to evaluate the stresses in the pipe. The ...

1975-09-01

411

Sprengel deformity in a nine-year-old boy: diagnosis and therapy; Sprengel-Deformitaet bei einem neunjaehrigen Jungen: Diagnostik und Therapie  

Energy Technology Data Exchange (ETDEWEB)

Sprengel deformity is a congential malformation with usually unilateral elevation and medial rotation of the scapula. An omovertebral bone is generally present. Associated skeletal malformations are frequently present. Though functional impairment is mild, the cosmetic and psycho-social impairment can be considerable. The prognosis of early surgical therapy is good. The presented case also justifies surgical correction in the older child. (orig.) [German] Die Sprengel-Deformitaet ist eine angeborene Fehlbildung mit meist einseitiger Elevation und Medialrotation der Skapula. Meist ist ein Os omovertebrale vorhanden. Assoziierte skelettale Fehlbildungen sind haeufig. Obgleich funktionell wenig einschraenkend, ist die kosmetische und psycho-soziale Beeintraechtigung oft erheblich. Die Prognose der fruehen operativen Therapie ist gut. Der vorliegende Fall ermutigt zur operativen Therapie auch im hoeheren Kindesalter. (orig.)

2003-02-01

412

Respect distances. Rationale and means of computation  

Energy Technology Data Exchange (ETDEWEB)

Canisters with spent nuclear fuel can obviously not be located within deformation zones as this might jeopardise their long term mechanical stability and thereby constitute a potential hazard to the biosphere. Less apparent, but equally important, is the fact that earthquakes trigger reactivation, slip, of structures some distance from their hypocentres due to, among many other factors, stress redistribution. Fault slip across a deposition hole might damage the isolation capacity of the canister and thereby jeopardise the overall integrity of the barrier system. Therefore, the following question might be posed: What is the distance from a deformation zone beyond which a canister can be safely emplaced? This respect distance cannot be readily computed because, unknown future events aside, there are some complicated aspects that need to be addressed e.g. degree of conservatism, scale, our ability to model ice sheets and earthquakes, etc. In this ...

2004-12-01

413

Resonance ionization spectroscopy at {sup 240f,242f}Am fission isomers  

Energy Technology Data Exchange (ETDEWEB)

Optical Isotope shift measurements have been performed for the {sup 240f,242f}Am fission isomers to test the stability of nuclear deformation as function of the neutron number. The method is based on resonance ionization spectroscopy (RIS) in a buffer gas cell with fission detection of the ionization process. The {sup 240f,242f}Am fission isomers have been produced by {sup 242}Pu(p, 3n), {sup 242}Pu(d, 2n) reactions, respectively. Relative isotope shift ratios X{sub exp}{sup 242f}(500 nm)=IS{sup 242f,241}/IS{sup 243,241}=41.4(8) and X{sub exp}{sup 240f}(500 nm)=IS{sup 240f,241}/IS{sup 243,241}=39.2(8) were measured. From these ratios a small difference {delta}{beta}{sub 2}{sup 242f,240f}=0.0076(14) of the deformation parameter {beta}{sub 2} can be deduced assuming that the isotope shift between the reference isotopes {sup 241,243}Am is caused by a pure volume change. (orig.)

1997-10-01

414

Plastic instability in an omega forming Ti-l5% Mo alloy  

International Nuclear Information System (INIS)

The plastic flow behavior of a #beta#-titanium alloy (Ti-15% Mo) was investigated over a wide range of temperatures and strain rates covering those conditions where the #omega#-phase forms dynamically. Portevin-Le Chatelier (PLC) effect was observed in this alloy at temperatures between 575 and 775 K at a strain rate of 1.31 x 10"-"4 s"-"1. The serrated flow behavior of this alloy could be suppressed by rendering the matrix #beta#-phase more stable against the #beta# to #omega# transformation. PLC bands formed in this alloy, studied at different levels of magnification using light, scanning electron and transmission electron microscopy, showed a high density of deformation bands within the macroscopic PLC band. The following mechanism of serrated flow is proposed; the load drop is ascribed to the sudden flow associated with the formation of deformation bands within which #omega#-particles were destroyed while the subsequent load rise results ...

415

Pipe whip studies  

Energy Technology Data Exchange (ETDEWEB)

An experimental and analytical study was performed to improve understanding of the dynamic impact behavior of carbon steel pipes. The test program addressed two types of pipe impact scenarios using both 2- and 4-in. Sch-80 pipes and elbows. Projectile-on-pipe tests simulated the behavior of a stationary target pipe which is impacted at its center by a larger, more rigid whipping pipe. These target pipes, which contained non-flowing water at about 290{degree}C temperature and ca 8.5 megapascals pressure, exhibited a peak deformation of up to 45% reduction in their diameter. For each test condition, the local deformation at the impact zone is a function of the peak impact force and impact velocity. Pipe-on-wall tests simulated the impact of an elbow at the free end of a cantilevered whipping pipe with a rigid barrier. The peak crush of the impact zone of the elbows was a function of peak impact force. Numerical analyses of dynamic impact tests ...

1984-06-01

416

Non-Abelian Duality and Confinement: from N=2 to N=1 Supersymmetric QCD  

CERN Document Server

Recently we discovered and discussed non-Abelian duality in the quark vacua of N=2 super-Yang-Mills theory with the U(N) gauge group and N_f flavors (N_f>N). Both theories from the dual pair support non-Abelian strings which confine monopoles. Now we introduce an N=2-breaking deformation, a mass term \\mu{\\mathcal A}^2 for the adjoint fields. Starting from a small deformation we eventually make it large which enforces complete decoupling of the adjoint fields. We show that the above non-Abelian duality fully survives in the limit of N=1 SQCD, albeit some technicalities change. For instance, non-Abelian strings which used to be BPS-saturated in the N=2 limit, cease to be saturated in N=1 SQCD. Our duality is a distant relative of Seiberg's duality in N=1 SQCD. Both share some common features but have drastic distinctions. This is due to the fact that Seiberg's duality apply to the monopole rather than quark vacua. More specifically, in our ...

2011-01-01

417

Microscopic analysis of the /sup 88/Sr(p,p') reaction at E/sub p/ = 201. 5 MeV  

Energy Technology Data Exchange (ETDEWEB)

Differential cross sections for 201.5 MeV proton scattering form /sup 88/Sr were measured. From the analysis of the elastic data, no unique optical-model potential could be obtained, but the radial moments are well determined. In a macroscopic analysis of the collective states it turns out that if the optical potential and transition potential are chosen consistently, unambiguous potential deformation lengths can be obtained even though the optical potential is not unique. Taking into account the range and density dependence of the underlying effective interaction reliable neutron deformation lengths can be obtained. For inelastic transitions of various character microscopic distorted-wave calculations with a density-dependent interaction based on the Paris potential were performed. The nuclear structure was taken from one broken-pair calculations in a large model space, calibrated by (e,e') data. In general a good description is ...

1988-04-25

418

Microscopic analysis of the "8"8Sr(p,p') reaction at E_p = 201.5 MeV  

International Nuclear Information System (INIS)

Differential cross sections for 201.5 MeV proton scattering form "8"8Sr were measured. From the analysis of the elastic data, no unique optical-model potential could be obtained, but the radial moments are well determined. In a macroscopic analysis of the collective states it turns out that if the optical potential and transition potential are chosen consistently, unambiguous potential deformation lengths can be obtained even though the optical potential is not unique. Taking into account the range and density dependence of the underlying effective interaction reliable neutron deformation lengths can be obtained. For inelastic transitions of various character microscopic distorted-wave calculations with a density-dependent interaction based on the Paris potential were performed. The nuclear structure was taken from one broken-pair calculations in a large model space, calibrated by (e,e') data. In general a good description is obtained for ...

419

Mechanical properties of Fe -10Ni -7Mn martensitic steel subjected to severe plastic deformation via cold rolling and wire drawing  

Energy Technology Data Exchange (ETDEWEB)

Fe-Ni-Mn martensitic steels are one of the major groups of ultra-high strength steels that have good mechanical properties and ductility in as annealed condition but they suffer from severe inter-granular embitterment after aging. In this paper, the effect of heavy shaped cold rolling and wire drawing on the mechanical properties of Fe-Ni-Mn steel was investigated. This process could provide a large strain deformation in this alloy. The total strain was {epsilon} {approx}7. Aging behavior and tensile properties of Fe-10Ni-7Mn were studied after aging at 753 K. The results showed that the ultimate tensile strength and ductility after cold rolling, wire drawing and aging increased up to 2540 MPa and 7.1 %, respectively, while the conventional steels show a premature fracture stress of 830 MPa with about zero ductility after aging.

2010-07-01

420

Mechanical properties of Fe -10Ni -7Mn martensitic steel subjected to severe plastic deformation via cold rolling and wire drawing  

International Nuclear Information System (INIS)

Fe-Ni-Mn martensitic steels are one of the major groups of ultra-high strength steels that have good mechanical properties and ductility in as annealed condition but they suffer from severe inter-granular embitterment after aging. In this paper, the effect of heavy shaped cold rolling and wire drawing on the mechanical properties of Fe-Ni-Mn steel was investigated. This process could provide a large strain deformation in this alloy. The total strain was #epsilon# #approx#7. Aging behavior and tensile properties of Fe-10Ni-7Mn were studied after aging at 753 K. The results showed that the ultimate tensile strength and ductility after cold rolling, wire drawing and aging increased up to 2540 MPa and 7.1 %, respectively, while the conventional steels show a premature fracture stress of 830 MPa with about zero ductility after aging.

2010-07-01

421

Mechanical Properties of Bamboo-like Boron Nitride Nanotubes by In Situ TEM and MD Simulations: Strengthening Effect of Interlocked Joint Interfaces.  

Science.gov (United States)

Understanding the influence of interfacial structures on the nanoarchitecture mechanical properties is of particular importance for its mechanical applications. Due to a small size of constituting nanostructural units and a consequently high volume ratio of such interfacial regions, this question becomes crucial for the overall mechanical performance. Boron nitride bamboo-like nanotubes, called hereafter boron nitride nanobamboos (BNNBs), are composed of short BN nanotubular segments with specific interfaces at the bamboo-shaped joints. In this work, the mechanical properties of such structures are investigated by using direct in situ transmission electron microscopy tensile tests and molecular dynamics simulations. The mechanical properties and deformation behaviors are correlated with the interfacial structure under atomic resolution, and a geometry strengthening effect is clearly demonstrated. Due to the interlocked joint interfacial structures and compressive ...

2011-08-10

422

Large deformation change in iridium isotopes from laser spectroscopy  

International Nuclear Information System (INIS)

Laser spectroscopy measurements have been performed on neutron-deficient iridium isotopes. The hyperfine structure and isotope shift of the optical Ir I transition 5d"76s"2 "4F_9_/_2#->#5d"76s6p "6F_1_1_/_2 have been studied for the "1"8"2"-"1"8"9Ir, "1"8"0Ir"m and "1"9"1","1"9"3Ir isotopes. The nuclear magnetic and quadrupole moments were obtained from the hyperfine splitting measurements and the changes of the mean square charge radii from the isotope shift measurements. A large deformation change between "1"8"7Ir and "1"8"6Ir and between "1"8"6Ir"m and "1"8"6Ir"g has been observed.

1999-11-16

423

Isothermal, total strain-controlled cyclic deformation of GGG-60 at temperatures of 20 C {<=}T {<=}500 C. Pt. 1; Isotherme totaldehnungskontrollierte Wechselverformung von GGG-60 im Temperaturbereich 20 C {<=}T {<=}500 C. T. 1  

Energy Technology Data Exchange (ETDEWEB)

The paper examines the influence of various total strain amplitudes and mean strains on the cyclic deformation processes in GGG-60 at temperatures of 20 C, 350 C, and 500 C ,the total strain amplitudes being varied between 1.0 permille {<=}{epsilon}{sub a,t}{<=}3.8 permille , and the mean strains between -4.0 permille {<=}{epsilon}{sub m,t}{<=}4.0 permille . - [Deutsch] In der Arbeit wird der Einfluss unterschiedlicher Totaldehnungsamplituden und Mitteldehnungen auf das Wechselverformungsverhalten von GGG-60 bei Temperaturen von 20 C, 350 C und 500 C untersucht. Dabei werden die Totaldehnungsamplituden zwischen 1,0 permille {<=} {epsilon}{sub a,t} {<=} 3,8 permille und die Mitteldehnungen zwischen -4,0 permille {<=} {epsilon}{sub m,t} {<=} 4,0 permille variiert. (orig./MM)

1995-01-01

424

Indentation plastic displacement field: Part II. The case of hard films on soft substrates  

Energy Technology Data Exchange (ETDEWEB)

The plastic displacements around Knoop indentations made in hard titanium/aluminum multilayered films on soft aluminum alloy substrates have been studied. Indentations were cross-sectioned and imaged using the focused-ion-beam (FIB) milling and high-resolution scanning electron microscopy (SEM), respectively. The FIB milling method has the advantage of removing material in a localized region without producing mechanical damage to the specimen. The micrographs of the cross-sectioned indentations indicate that most of the plastic deformation around the indentation is dominated by the soft aluminum substrate. There is a very small change in the multilayered film thickness around the indentation{emdash}less than 10{percent}. The plastic deformation of the thin film resembles a membrane being deflected by a localized pressure gradient across the membrane. Stress-induced voids are also observed in the multilayered film, especially in the area around ...

1999-06-01

425

Improvement of folding endurance of molded hinge parts by actuating the movable pin in a mold. Katanai oshikomi hinge seikei ni yoru hinge tokusei kaizen koka  

Energy Technology Data Exchange (ETDEWEB)

Improvement of hinge forming performance was tried in the injection molding of plastic. At first, pushing hinge forming in a mold was made by a movable pin with the die built-in an actuator, and thin hinges of 0.07mm and 0.1mm thickness which were greatly less than the conventional forming limit (0.2mm and 0.6mm respectively) of polyacetal (POM) and polybutylene terephthalate (PBT) could be formed. Hinge characteristics of POM (hinge thickness t < 0.4mm) and PBT (t < 0.7mm) which were made by the conventional forming and failed after 1 time, were improved respectively to 30,000 times or more and 300,000 times or more by pushing forming in the mold. The hinge characteristics were greatly affected by the plastic deformability of the hinge part resin and the improvement of deformability by the pushing forming were caused by the elimination of oriented layer and the expansion of hemispherical layer of the hinge part. 6 refs., 13 figs., 1 tab.

1990-06-01

426

GENERALIZED ATOMIC MASS LAW  

Science.gov (United States)

Least-squares analyses were performed on a set of atomic masses using standard and generalized senaiempirical mass laws. Presumably because of errors in the assured form of the standand mass law, its least-squares coefficients can be determined at best to an accuracy of about 10%, and masses are predicted with an uncertainty of several Mev/c/sup 2/. The standard mass law was generalized by addition of shell effect and deformation terms. While the least-squares fitting of the generalized mass law is better than for the standard mass law, it is still not possible to predict atomic masses to an accuracy better than a few Mev/c/sup 2/. The nuclear deformations and the well depth . of the nuclear interaction obtained from the additional mass-law terms are in reasonable agreement with more accurate determinations by other methods. A similar statement applies to the nuclear radius constant as obtained from the ...

1959-11-15

427

Experimental studies of pipe whip and impact: Final report  

Energy Technology Data Exchange (ETDEWEB)

An experimental and computational study was undertaken to estimate the effects of pipe rupture and induced pipe whip impact on surround structures considered either as rigid or deformative such as concrete slabs. This program included sixteen tests using 3 inch schedule 80 (or 10) pipes made of carbon steel similar to A106 grade B. The study consisted of tests on rigid target and on concrete slab. The investigation of whip phase and impact phase was done separately for each test. For pipe impact on rigid targets, the impact forces are found to be directly related to the crush strength of the pipe and the general pipe deformation following the impact. For pipe impact on concrete slabs, the response of the target to the pipe impact needs to take into account the local effect such as penetration and localized damage on the slab. The test matrix covered a broad range of geometric parameters. It provides a significant data base for studying pipe ...

1987-02-01

428

Experimental investigation on the fretting wear of alloy 800 in room remperature water  

Energy Technology Data Exchange (ETDEWEB)

Fretting wear test in room temperature water was performed to evaluate the wear coefficient of CANDU (CANadian Deuterium Uranium) steam generator (SG) tube material (Alloy 800) against 410 type martensitic stainless steels. The main focus is to compare the wear behaviors between Alloy 800 and Inconel 690. Test conditions are 10{approx}30N of normal load, 200{approx}450mm of sliding amplitude and 30Hz of frequency. The result indicated that the wear rate of Alloy 800 was higher than those of Inconel 690 at various test condition such as normal loads, sliding amplitudes etc. From the results of SEM observation, there was little evidence of plastic deformation layer that were dominantly formed on the worn surfaces of Inconel 690. Also, wear particles in Alloy 800 were released from contacting asperities deformed by severe plastic flow during fretting wear. Main cause of wear rate between Alloy 800 and Inconel 690 may be due to the difference of ...

2002-05-01

429

Experimental investigation on the fretting wear of alloy 800 in room remperature water  

International Nuclear Information System (INIS)

Fretting wear test in room temperature water was performed to evaluate the wear coefficient of CANDU (CANadian Deuterium Uranium) steam generator (SG) tube material (Alloy 800) against 410 type martensitic stainless steels. The main focus is to compare the wear behaviors between Alloy 800 and Inconel 690. Test conditions are 10#approx#30N of normal load, 200#approx#450mm of sliding amplitude and 30Hz of frequency. The result indicated that the wear rate of Alloy 800 was higher than those of Inconel 690 at various test condition such as normal loads, sliding amplitudes etc. From the results of SEM observation, there was little evidence of plastic deformation layer that were dominantly formed on the worn surfaces of Inconel 690. Also, wear particles in Alloy 800 were released from contacting asperities deformed by severe plastic flow during fretting wear. Main cause of wear rate between Alloy 800 and Inconel 690 may be due to the difference of ...

2002-05-01

430

Evaluation of fetal brain development by magnetic resonance imaging. Subependymal germinal matrix layer and cerebral ventricle  

International Nuclear Information System (INIS)

Three dimensional data of brain from the formalin-fixed fetuses were collected without isolation, by the 4.7 tesla super high magnetic field MRI and the developmental process of the cerebral parenchyma was studied by 3D images. Subjects were 13 fetal brain and MRI was performed using 3D-steady-state free precession sequence. The isolated brain is very soft and fragile and is deformed by its weight at the imaging. However 3D-MRI can be obtained without isolation, and the deformation is remarkably small. The subependymal germinal matrix layer did not be observed in 7 weeks-old fetus, appeared at 9 weeks-old and increased gradually. Then it rapidly reduced from 28 weeks-old. The volume calculated, from 3D-MRI, increased rapidly from 9 weeks-old to 23 weeks-old, and reached the maximum (2.346 mm"3) at 23 weeks-old. The relation between fetal ages and volume of cerebral ventricle also showed similar pattern. This method will be useful to examine the ...

1999-10-01

431

Elasto-plastic analysis of settlement of pile foundations. Part 2. ; Prediction of immediate settlement of building. Kui kiso no dansosei chinka kaiseki. 2. ; Kenchikubutsu no sokuji chinka yosoku hoho  

Energy Technology Data Exchange (ETDEWEB)

When the foundations of the building are designed and worked, the prediction calculation of immediate settlement of the building exercised practically is to calculate assuming the earth is a linear elastic body, but the actual stress-strain relationship of the earth is nonlinear and rigidity of the earth becomes lower as strain (or stress) increases. Hence in order to grasp the actual settling behavior of the earth, it is necessary to elucidate the nonlinear relationship between stress and strain. In this article, a prediction method of building settlement is introduced which uses an analytical technique of the multi-layered earth by the linear elasticity theory and takes into consideration strain dependency of rigidity of the earth. Part of the conclusion is as follows which has been obtained by studying the settling behaviors observed in examples of vertical loading tests of the pile foundations and the elasto-plastic settlement analytical method of the pile foundations; the settling ...

1992-12-25

432

Effect of carbon on irradiation hardening of reduced-activation 10Cr-30Mn austenitic steels  

International Nuclear Information System (INIS)

Tensile properties of reduced-activation 10Cr-30Mn austenitic steels with carbon levels from 0.003 to 0.55% were investigated over the temperature range from room temperature to 873 K after neutron irradiation in the Japan Materials Testing Reactor at 573 K to 8.5x10"2"2 n/m"2. Irradiation-induced increase in yield stress increased significantly with carbon concentration up to about 0.1% and it was constant above 0.1% carbon. A high density of dislocation loops with small (below 10 nm) and large (20-30 nm) sizes formed during irradiation. The high density, small loops caused a large irradiation hardening, while the large loops contributed only slightly to irradiation hardening. It was considered that carbon atoms formed the small loops together with irradiation defects. The deformation channeling was observed in the irradiated high carbon steels, 0.11 and 0.55% carbon, but not in the very low carbon steel, 0.003% carbon, after deformation near ...

433

Deep-crustal structure of the continental margin adjacent to the eastern Aleutian trench  

Energy Technology Data Exchange (ETDEWEB)

Onshore and marine seismic-reflection data obtained near the Trans-Alaskan Crustal Transect (TACT), in the region of the eastern Aleutian trench and lower Cook Inlet, reveal highly reflective midcrustal layering that begins at a depth of 10-15 km within the upper plate of the Aleutian subduction zone. Beneath the continental shelf, midcrustal reflections were recorded over broad areas and occur in subhorizontal bands that are 1 to 3 s thick. The reflections extend beneath complexly deformed late Mesozoic and early Cenozoic accreted rocks that are exposed at the surface. Preliminary interpretation of seismic refraction data indicates that under the shelf the top of the reflections corresponds in depth with a sharp increase in rock velocity, from 5.9 km/s to 6.6 km/s. North and northwest of the shelf, beneath the Chugach and Kenai mountains, midcrustal features dip 20{degree}-30{degree} north or northwest, and below the Chugach Mountains, the top of the reflections ...

1990-06-01

434

Crystallography of grain boundary #alpha# precipitates in a #beta# titanium alloy  

International Nuclear Information System (INIS)

The crystallography of #alpha#(hcp) precipitates formed on the #beta#(bcc) matrix grain boundaries has been studied with transmission electron microscopy (TEM) in a Ti-15V-3Cr-3Sn-3Al alloy. The #alpha# precipitates have a near-Burgers orientation relationship with respect to at least one of the adjacent #beta# grains. Among the possible 12 variants in this orientation relationship, the variant that [11 bar 20]_#alpha# is parallel to the _#beta# closest to the grain boundary plane tends to be preferred by the #alpha# precipitates. Additionally, further variant selections are made so as to minimize the deviation of orientation relationship with respect to the ''opposite'' #beta# grain from the Burgers one. Such rules in variant selection often result in the formation of precipitates with a single variant at a planar grain boundary. Prior small deformation of #beta# matrix changes the variant of #alpha# precipitates at the deformed portion of ...

1994-10-03

435

Analysis of in-pile heat transfer tests: Final report  

Energy Technology Data Exchange (ETDEWEB)

This report presents the results of analysis of selected data from the NRU test series dealing with heatup and reflood heat transfer during postulated PWR LOCA conditions. These tests used nuclear fuel rods and some considered clad ballooning and rupture. Also included was an electrically-heated rod ballooning test, REBEKA-6. The COBRA-TF computer program, renamed PYTHONS, was modified and used for the analytical tool. Modifications included provisions for fuel rod gas flow and pressure, creep deformation and rupture, channel blockage, and blockage heat transfer. Calculated clad temperatures for NRU unpressurized rods show quite good agreement with experimental data. The calculated amount and axial extent of clad ballooning for pressurized rods agrees reasonably well with post-test examinations of the NRU bundles. Time to failure was underpredicted in the MT-3 test as a result of the high strength of NRU clad material which was not represented in the PYTHONS creep ...

1986-11-01

436

A mechanistic understanding of the formability of magnesium: examining the role of temperature on the deformation mechanisms  

Energy Technology Data Exchange (ETDEWEB)

The possibility of improving the cold formability of wrought magnesium alloys is considered in light of their good hot forming characteristics. Magnesium alloy AZ31B sheet is selected as a model system. Parameters affecting formability, such as strain hardening rate, strain rate sensitivity, and the degree of anisotropy are examined systematically by conducting tensile tests over a range of temperatures (room temperature to 250 C) and strain rates (1 x 10{sup -5} to 0.1 s{sup -1}). The plastic anisotropy and deformation texture evolution are examined in samples aligned with the sheet rolling and transverse directions. Polycrystal plasticity simulations using a viscoplastic self-consistent (VPSC) formulation are used to model the observed anisotropy and texture evolution. The adjustable parameters in the model are the relative critical resolved shear stresses of the dislocation mechanisms known to operate within magnesium. The experimental results suggest that an ...

2003-07-01

437

np-nh bands in the N=28 isotones  

CERN Document Server

The existence of n-particle n-hole deformed yrare bands in the N=28 isotones is explored using full pf-shell diagonalizations and the Lanczos Strength Function method. We find different 2p-2h and 4p-4h collective bands that, when allowed to mix, more often disappear. Only the 2p-2h yrare band in Cr-52 and the 4p-4h yrare band in Ni-56 survive, and only in this latter case, due to the reduced density of 2p-2h states, can the band be seen as a gamma-cascade.

2002-01-01

438

Theoretical investigations of strength of a flexible tube made of NiTi; Festigkeitstheoretische Untersuchungen einer flexiblen Huelse aus NiTi  

Energy Technology Data Exchange (ETDEWEB)

A flexible, steerable tube (distal end) of an endoscope for the application in the laparoscopic surgery has been analyzed by means of the finite-element-method (FEM). The unusual mechanical and thermal features of the used shape memory alloy (SMA) of NiTi were taken in account. The analyses showed that the strains remain in the super-elastic region up to the maximum bending of 90 and no plastic deformations occur. The application of the shape optimization (CAO) made possible finding the optimal structure of the distal end and therefore powerful reducing the maximum strains in the critical regions. (orig.)

2000-04-01

439

The identical bands in [sup 177]Ta  

Energy Technology Data Exchange (ETDEWEB)

The 4025/2 bands in [sup 177]Ta which are ''identical'' to the neighboring even-even [sup 176]Hf groundstate band have been extended to higher angular momentum. These bands in the two nuclei are seen to diverge from each other in the region of the first i[sub 13/2] neutron alignment. The lower observed crossing frequency for the 4025/2 bands indicates a lower deformation for these bands compared to [sup 176]Hf. Extensions to the h[sub 9/2] 5411/2 yrast band are also reported. (orig.)

1993-10-01

440

The identical bands in "1"7"7Ta  

International Nuclear Information System (INIS)

The [402]5/2 bands in "1"7"7Ta which are ''identical'' to the neighboring even-even "1"7"6Hf groundstate band have been extended to higher angular momentum. These bands in the two nuclei are seen to diverge from each other in the region of the first i_1_3_/_2 neutron alignment. The lower observed crossing frequency for the [402]5/2 bands indicates a lower deformation for these bands compared to "1"7"6Hf. Extensions to the h_9_/_2 [541]1/2 yrast band are also reported. (orig.).

441

The crack of harden cement paste observed with multi-technique  

British Library Electronic Table of Contents (United Kingdom)

The shrinkage of the cement paste with low water-cement ratio at different relative humidity was observed and analyzed with ESEM and deformation map technique. The crack morphology was observed with different magnification with SEM and FESEM, and the formation of the crack was observed with AFM between two C-S-H nano particles. The observation by multi technique at multi scale indicated that the shrinkage was increase with the decrease of the humidity due to the increase of the pressure of the capillary pressure, the morphology of the crack in smaller scale was similar to that in the bigger scale, the smaller crack distributed in the latticework of the bigger ones, and the crack propagated along the gap between two nano particles of C-S-H with weaker bonding.

2010-01-01

442

Superplastic behaviour in Ti-3Al-4V  

International Nuclear Information System (INIS)

Superplastic deformation behavior in an alpha + beta titanium alloy Ti-3A-4V has been investigated by using the method of cross head speed cycling in the temperature range 750-910 /sup 0/C. On the basis of flow stress-strain rate-strain rate sensitivity data, the alloy was found to be superplastic in the entire temperature range studied. Optimum superplasticity was observed in the strain-rate range 3 x 10/sup -5/ sec./sup -1/ to 6 x 10/sup -5/ and at the highest temperature of 910 deg. C. (author).

443

Subsidence model of spoil bank surface  

Energy Technology Data Exchange (ETDEWEB)

Evaluates a mathematical model that describes subsidence of spoil banks in surface brown coal mines. The model is based on the results of geodetic surveys carried out in 1974-1985. Twelve spoil banks from 4 to 61 m high were considered. Ground subsidence and deformation along 12 measuring lines and 6 measuring networks were measured. Ground subsidence during a period of 18 to 241 months was evaluated using regression analysis. The mathematical model considered effects of spoil bank design (number and thickness of rock layers), rock mechanical and physical properties and service time. 6 refs.

1989-01-01

444

Study on reactor building structures using ultrahigh strength materials - Part 8: Results of mixed structure tests  

International Nuclear Information System (INIS)

The mixed structure of a nuclear reactor building is composed of SC-columns, S-beams, S-joints and PCa-panels. Following the last report (Part 7)[1], the main test results of the mixed structure, that is, the deformation mode, strain distribution and shear strength, are described. The S-joints using ultrahigh strength materials had no buckling nor shear slipping. The proposed mixed structure resisted the external horizontal forces under integrated uniformity among SC-columns, S-joints and PCa-panels. It could be confirmed that the mixed structure can be established. (author)

1993-08-15

445

Strain induced hardening in Ti-3Al-4V at 910 deg. C  

International Nuclear Information System (INIS)

High temperature deformation behavior of an alpha + beta titanium alloy Ti-3Al-4V has been investigated at 910 deg. C. by using the method of cross head speed cycling. On the basis of flow stress, strain rate and strain rate sensitivity data, the alloy was found to exhibit strain hardening at this temperature which resulted in degradation in superplastic properties of the alloy. A high beta-phase volume fraction and grain-growth in both alpha and beta phases were considered responsible for the observed hardening effect. (author)

446

Static and dynamic muonic-atom codes-MUON and RURP  

International Nuclear Information System (INIS)

Muonic-atom energy levels and wave functions are calculated. The results are corrected for nearly all important static effects, including finite nuclear size as produced by a user-specified nuclear charge distribution. Fourth-order Runge-Kutta integration of the radial Dirac equations, with the secant method determining the eigenvalues. Corrections are either included as potentials in the Dirac equations or computed as first-order perturbations. The code assumes spherical symmetry, so that effects of nuclear deformation may be treated only as static first-order perturbations. Dynamic muon-electron and muon-nuclear effects are neglected (the latter are calculated by RURP). (Auth.).

1979-02-01

447

Shell effects in the symmetric-modal fission of pre-actinide nuclei  

International Nuclear Information System (INIS)

Mass distributions of fragments in the low-energy fission of nuclei from "1"8"7Ir to "2"1"3At have been analysed. This analysis has shown that shell effects in symmetric-mode fragment mass yields from the fission of pre-actinide nuclei could be described if one assumes the existence of two strongly deformed neutron shells in the arising fragments with neutron numbers N_1#approx#52 and N_2#approx#68. A new method has been proposed for quantitatively describing the mass distributions of the symmetric fission mode for pre-actinides with A#approx#180-220. (orig.)

1998-09-21

448

Reversible Movement of Homogenously Nucleated Dislocations in a #beta#-Titanium Alloy  

International Nuclear Information System (INIS)

We demonstrate reversible movement of (1/2)[110](110) dislocation loops generated from nanodisturbances in a #beta#-titanium alloy. High resolution transmission electron microscope observations during an in situ tensile test found three reversible deformation mechanisms, nanodisturbances, dislocation loops and martensitic transformation, that are triggered in turn with increasing applied stress. All three mechanisms contribute to the nonlinear elasticity of the alloy. The experiments also revealed the evolution of the dislocation loops to disclination dipoles that cause severe local lattice rotations.

2009-01-30

449

Principal geological results of petroleum and gas prospecting on Southern Sakhalin  

Energy Technology Data Exchange (ETDEWEB)

Results are given for deep-level petroleum and gas drilling probes in various coastal zones of Southern Sakhalin covering the Poronai depression and the Aniv Bay trough. The exploratory probes indicate that the Middle Miocence deposits of the Boundary trough contain commercial-size deposits of petroleum, that commercial-size gas deposits are in the upper Myocene deposits of the Aliv Bay trough, and that the upper Cretaceous and Cenozoic deposits of the eastern section of Southern Sakhalin lack folded deformations. 7 references, 2 figures.

1981-01-01

450

Perturbing the ground ring of 2D string theory  

Energy Technology Data Exchange (ETDEWEB)

In this paper, the authors use free field techniques in D = 2 string theory t calculate the perturbation of the special state algebras when the cosmological constant is turned on. In particular, the authors find that the 'ground cone' preserved by the ring structure is promoted to a three-dimensional hyperboloid as conjectured by Witten. On the other hand, the perturbed (1,1) current algebra of moduli deformations is computed completely, and no simple geometrical interpretation is found. The authors also quote some facts concerning the Liouville matrix a model dictionary in this class of theories.

1992-12-10

451

On the Generic vanishing of certain Koszul cohomology groups  

CERN Document Server

We propose a new approach to study Koszul cohomology of general $g^r_d$'s on general curves via degenerations and deformations. As an application of this new method, we prove projective normality for general line bundles $L$ on general curves with $h^1(L)\\le1$ and degree greater than roughly $(5/4)g$. This improves the bound in a classical theorem of Green and Lazarsfeld. Also we give some partial results on vanishing of higher syzygies for line bundles with $h^1(L)=1$.

2011-01-01

452

Observation of dislocation dynamics in the electron microscope  

Science.gov (United States)

Deformation experiments performed in-situ in the transmission electron microscope have led to an increased understanding of dislocation dynamics. To illustrate the capability of this technique two examples will be presented. In the first example, the processes of work hardening in Mo at room temperature will be presented. These studies have improved our understanding of dislocation mobility, dislocation generation, and dislocation-obstacle interactions. In the second example, the interaction of matrix dislocations with grain boundaries will be described. From such studies predictive criteria for slip transfer through grain boundaries have been developed.

2001-01-17

453

Nuclear spectroscopy, ch. 8  

International Nuclear Information System (INIS)

Energy level schemes are derived from gamma spectroscopy of several medium-mass deformed nuclei by studying the decay or proton and #alpha# nuclear spectroscopic data. Some new isomeric studies are established among which is the 31 y "1"7"8Hf isomeric state for which Isup(#pi#), K was determined to be 16"+, 16. A four quasi-particle configuration was assigned to this state at 2447.5 +- 2.5 KeV. Atomic masses have been calculated from various measurements and, on the basis of mass formulae extrapolated to neighboring mass regions.

454

Neutron irradiation effects in austenitic alloys  

International Nuclear Information System (INIS)

The post (neutron) -irradiation high-temperature tensile and creep-rupture properties, deformation and fracture characteristics of austenitic alloys, particularly solution annealed Type 316 steel, are surveyed and correlated with the damage structures developed as a function of irradiation temperature (and dose). The mechanisms proposed to explain the irradiation-induced changes in properties and behaviour are summarised. The factors responsible for the observed differences in the post-irradiation and 'in-reactor' creep-rupture properties and behaviour of an austenitic steel are discussed in terms of the helium gas and stress driven growth of small intergranular bubbles and the atom plating associated with their growth and coalescence. (author).

1980-03-01

455

Magnetic Properties of a Material Used to Estimate Elastic and Plastic Strains of Ferrite?Pearlite Steels  

British Library Electronic Table of Contents (United Kingdom)

The effect of elastic and plastic strains on the magnetic properties of ferrite-pearlite steels has been studied. It has been shown that the sensitivity to elastic-tensile and bending strains is four to five times greater for remnant magnetization than for coercive force. In order to determine the degree of cold plastic deformation of high-carbon steels, a two-parametric testing technique based on the use of remnant magnetization and coercive force was suggested. An MMT-2 device was recommended for measurement of the required parameters.

2005-01-01

456

Local lattice structure, crystal field and energy level patterns in CsCdBr_3:Tm"3"+ crystals  

International Nuclear Information System (INIS)

In CsCdBr_3, Tm"3"+ substitutes for Cd"2"+. It predominately forms symmetric dimer centers and single-ion centers, both of trigonal symmetry. The energy level schemes of both centers were determined by EPR and site-selective laser spectroscopy. To describe the spectra term dependent crystal-field parameters were deduced on the basis of a microscopic model taking into account the local lattice deformation induced by the impurity centers and the quasi-resonant virtual scattering of intrinsic lattice excitations by the Tm"3"+ ions. (orig.)

1998-07-24

457

Level density parameter and fission probability calculations in heavy-ion-induced fission reactions  

International Nuclear Information System (INIS)

Based on the single-particle levels given by Nilsson, the intrinsic and effective (with collective effects) level density parameters as a function of the excitation energy for the "1"8"6Os, "1'8"7Ir, "1"8"9Os and "1"9"3Au deformation nuclei have been calculated in the range of the excitation energy up to 150 MeV. The calculated fission probabilities P_f (U) are consistent satisfactorily with the experimental data when a nonadiabatic estimation of the collective effects was used to calculated the nuclear level density parameters.

458

Large-scale absolute dent evaluation campaign  

International Nuclear Information System (INIS)

Steam generator tube denting is primarily caused by build-up of corrosion products at the tubesheet and the tube support plates. The mechanism of dent growth and the identification of tubes which should be removed from service have been studied. The practical outcome has been to prevent in-service tube leaks and to avoid unnecessary plugging of large numbers of tubes. A finite element study of tubesheet deformation (of pulled leaking tubes from reactors) was undertaken. Profilometry results for characterizing dents are given. Although several modifications have been made the high resolution profilometry system performance and the results obtained have proved satisfactory. (U.K.).

459

In-situ TEM study of dislocation-twin boundaries interaction in nanotwinned Cu films  

British Library Electronic Table of Contents (United Kingdom)

Epitaxial thin films of nanotwinned face-centered cubic metals such as Cu possess an unprecedented combination of high hardness and high electrical conductivity due to the unique structure of nanometer-spaced coherent twin boundaries. Recent studies of in-situ nanoindentation in a transmission electron microscope have provided new insights on the deformation behavior of nanotwins that are reviewed here. In particular, two unit processes are highlighted: first, stress-induced migration of ?3 {112} incoherent twin boundary that leads to de-twinning of nanotwins; second, twinning dislocation can be multiplied at ?3 {111} coherent twin boundary.

2011-01-01

460

Hyperfine structure studies with the COMPLIS facility  

International Nuclear Information System (INIS)

COMPLIS is an experimental facility designed to carry out spectroscopic studies on radioisotopes produced by disintegration of elements available at CERN's Booster-ISOLDE on-line isotope separator. During recent series of experimental runs, hyperfine structure measurements have yielded information on nuclear moments and deformations of platinum and iridium isotopes. For the first time, population by #alpha#-decay from Hg was exploited to investigate "1"7"8"-"1"8"1Pt--the most neutron-deficient Pt isotopes yet studied. Successful measurements have recently been carried out on "1"8"2"-"1"8"9Ir.

1998-12-16

461

Geological setting of the Paleoproterozoic Rosebel gold district, Guiana Shield, Suriname  

British Library Electronic Table of Contents (United Kingdom)

The Rosebel gold district is hosted in a Paleoproterozoic greenstone belt of the Guiana Shield and has many characteristics that enable classification of the ores as an orogenic gold deposit. Host rocks have undergone several phases of deformation. However, gold deposition occurred late in the structural history of the belt, and is considered part of a late regional metallogenic event with respect to the geotectonic evolution of the Guiana Shield. Economic gold mineralization is hosted in felsic to mafic volcanic rocks and two sedimentary successions that are differentiated into turbiditic and arenitic depositional packages. The detailed lithostratigraphic characterization and the geochemistry enable the correlation of the local rock types with the Paramaka, the Armina, and the Rosebel for...

2011-01-01

462

Generator coordinate method for triaxial quadrupole collective dynamics in strontium isotopes  

Energy Technology Data Exchange (ETDEWEB)

We discuss the algebraic structure of the generator coordinate method for triaxial quadrupole collective motion. The collective solutions are classified according to the representations of the permutation group of the intrinsic axes. Our method amounts to an approximate angular-momentum projection. We apply it to a study of the spherical-to-deformed-shape transition in light even strontium isotopes {sup 78-88}Sr. We find that triaxial configurations play a significant role in explaining the structure of the transitional isotopes {sup 80-82}Sr. (orig.).

1991-07-29

463

Experimental and analytical studies of four-inch pipe whip tests under PWR LOCA conditions  

Energy Technology Data Exchange (ETDEWEB)

In the tests, the effects of the overhang length on the pipe whip behavior of the pipe-restraints system were studied by measuring the strains and deformations of the test pipe and restraints, and the restraints forces. The equation for predicting the maximum strain at the outer surface of the pipe was derived using a static equilibrium condition. The calculated maximum strains at the outer surface of the pipe agree fairly well with experimental data. The dynamic response analysis of the pipe-restraints system was conducted by the finite element program ADINA. The applicability of the ADINA program to the pipe whip analysis is made clear through this analysis.

1984-01-01

464

Engineering electromagnetic response of composite terahertz metamaterial with broken symmetry  

Science.gov (United States)

We proposed and numerically investigated the influence of spatial symmetry on the terahertz frequency region response of composite planar metamaterials based on deformed split ring resonators. Compared with the original simple structures, the composite metamaterials with different spatial symmetries exhibited exotic electromagnetic properties. The electromagnetic response of a specific configuration with C4 symmetry was identical to the structure with simple lattice. Especially, for configurations with broken symmetry, very sharp Drude-like resonances with high quality factor were observed. The electric field and current distribution associated the resonances were analyzed for deep understanding of the underlying physical properties.

2011-09-01

465

Effect of porosity on the superplasticity of an alumina  

Energy Technology Data Exchange (ETDEWEB)

To evaluate the effect of porosity on superplasticity behavior, it is essential to use materials of similar initial grain sizes. This can be achieved by HIPing, which provides an effective way of reducing initial porosity while avoiding appreciable grain growth; various levels of porosity can be achieved for similar grain sizes. This note is concerned with the influence of porosity on superplasticity tensile deformation of a fine grained high-purity alumina doped with copper oxide and containing a grain growth inhibitor. Specimens were prepared by slip casting to net-shape and sintering; some presintered specimens were HIPed to reduce porosity. The subsequent superplasticity behavior is related to porosity in the material.

1994-02-01

466

Effect of cross rolling parameters on texture formation and parameters on texture formation and anisotropy of mechanical properties of (#alpha#+#beta#)-titanium alloy sheets  

International Nuclear Information System (INIS)

Formation of basis type texture at rolling of Ti + 6.0% Al + 1.5% V + 1.0% Mo system alloy with initial prismatic texture is investigated by means of X-ray techniques. Variations of mechanical features in titanium alloy sheets depending on temperature-deformation conditions of rolling are investigated. Main conditions for formation of the intensive basis textute in the investigated alloy sheets which provides for isotropic properties in sheet plane and for increased ductility are determined.

467

Displacement of a railway bridge caused by coal mining  

Energy Technology Data Exchange (ETDEWEB)

Evaluates displacement of a railway bridge element of the Walbrzych-Klodzko railway line. The bridge, consisting of three truss sections supported by two pillars made of reinforced concrete, was influenced by longwall mining. Longwalls were perpendicular to the bridge axis. Three coal seams situated in the bridge safety pillar were 550 cm thick. Ground subsidence after seam extraction was 400 cm. Ground subsidence did not cause truss section deformation, nor did it cause additional stresses in truss bridge construction. 2 refs.

1988-01-01

468

Aqueous radioactive waste bituminization  

International Nuclear Information System (INIS)

The bituminzation of decontamination and ion exchange resin stripping wastes with four grades of asphalt was investigated to determine the effects of asphalt type on the properties of the final products. All waste forms deformed readily under light loads indicating they would flow if not restrained. It was observed in all cases that product leaching rates increased as the hardness of the asphalt used to treat the waste increased. If bituminization is adopted for any Ontario Hydro aqueous radioactive wastes they should be treated with soft asphalt to obtain optimum leaching resistance and mechanical stability during interim storage should be provided by a corrosion resistant container.

5049-01-01

469

Analysis on uranium resource situations and metallogenic potential of Heyuan mineralization belt of Guangdong province  

International Nuclear Information System (INIS)

Heyuan mineralization belt is a structure-magmatic activities belt which is charcterized by strong plastic deformation and shearing. The squeeze (overthrust) structure is formed early. Later stretch produced slide shovel-shaped normal fault which control the red basin and uranium mineralization. Comprehensive study shows that this area is of favorable uranium metallogenic condition due to the rich uranium source and higher degree of geology work, it is a target for the new round resources exploration. (authors)

2008-03-01

470

A micro-compression study of shape-memory deformation in U-13at%Nb  

Energy Technology Data Exchange (ETDEWEB)

Micro-compression specimens, 1O-15{mu}m in diameter by 20-30{mu}m in height, were produced from individual parent grains in a polycrystalline U-13at%Nb shape-memory alloy using the focused ion beam (FIB) technique. The specimens were tested in a nanoindentation instrument with a flat diamond tip to investigate stress-strain behavior as a function of crystallographic orientation. The results are in qualitative agreement with a single-crystal accommodation strain (Bain strain) model of the shape-memory effect for this alloy.

2008-01-01

471

A lethal form of Gorham disease associated with extensive musculoskeletal pneumatosis: case report and review of the literature  

Energy Technology Data Exchange (ETDEWEB)

We report here the imaging findings of a rare case of a lethal form of Gorham disease in a young female patient. Multimodality imaging findings over 13 year-follow-up demonstrated progressive wide spread skeletal and soft tissue abnormalities with permeative osteolysis, pathological fractures and severe skeletal deformities. Unusual extensive osseous and soft tissue pneumatosis was illustrated on cross-sectional studies. The progressive nature of this form of Gorham disease and the subsequent complications eventually culminated in patient's death. (orig.)

2008-11-15

472

A lethal form of Gorham disease associated with extensive musculoskeletal pneumatosis: case report and review of the literature  

International Nuclear Information System (INIS)

We report here the imaging findings of a rare case of a lethal form of Gorham disease in a young female patient. Multimodality imaging findings over 13 year-follow-up demonstrated progressive wide spread skeletal and soft tissue abnormalities with permeative osteolysis, pathological fractures and severe skeletal deformities. Unusual extensive osseous and soft tissue pneumatosis was illustrated on cross-sectional studies. The progressive nature of this form of Gorham disease and the subsequent complications eventually culminated in patient's death. (orig.)

2008-11-01

473

A Geometrical Model for Non-Zero $\\theta_{13}$  

CERN Document Server

Based on Friedberg and Lee's geometric picture by which the tribimaximal PMNS leptonic mixing matrix is constructed, namely corresponding mixing angles correspond to the geometric angles among the sides of a cube. We suggest that the three realistic mixing angles which slightly deviate from the values determined for the cube, are due to a viable deformation from the perfectly cubic shape. Taking the best fitted results of $\\theta_{12}$ and $\\theta_{23}$ as inputs, we determine the central value of $\\sin^22\\theta_{13}$ should be 0.0238 with a relatively large error tolerance, this value lies in the range of measurement precision of the Daya Bay experiment.

2011-01-01

474

Treatment of low-frequency pulsating magnetic field on amorphous alloy Fe_7_8Si_9B_1_3  

International Nuclear Information System (INIS)

Effect of low-frequency pulsating magnetic field on the microstructure and magnetic properties of amorphous alloy Fe_7_8Si_9B_1_3 were investigated. The temperature rise induced by the treatment was measured by a non-contact infrared thermometer. The crystallization behavior and microstructure of specimens were studied by Moessbauer spectroscopy and transmission electron microscope (TEM). Magnetic properties of the specimens were investigated by alternating gradient magnetometer (AGM). The results show that the low-frequency pulsating magnetic field can promote the single-phase crystallization of amorphous alloy Fe_7_8Si_9B_1_3. The frequency, f of applied field is from 10 to 40 Hz, magnetic field, H is from 0.02 to 0.04 T and treatment duration, t is from 180-300 s. The volume fraction of crystallization phase (#alpha#-Fe(Si), the grain size, 2-10 nm) is 3-7%. The temperature rise less than 7 deg. C. Magnetic properties of samples are improved ...

2007-07-15

475

The nanostructure and microstructure of steels: Electrochemical Tafel behaviour and atomic force microscopy  

International Nuclear Information System (INIS)

The influence of chemical composition and heat treatment on a low-carbon steel, chromium steel and high speed steel has been examined by polarisation curves and electrochemical parameters deduced from the Tafel plots. The electrochemical corrosion resistance, which is small between the as-received steels become greater after heat treatment, following the order: carbon steel < chromium steel #approx# high speed steel. To explain these differences, the nano- and microstructure of the steels has been characterized by the ex situ techniques of atomic force microscopy and optical microscopy, before and after surface etching with Nital (a solution of 5% HNO_3 in ethanol). This causes preferential attack of the ferrite phases showing the carbide phases more clearly. From these nanostructural studies it was possible to better understand why the passive films formed on chromium steel and high speed steel have superior protective properties to those formed on carbon ...

2005-12-01

476

The influence of the binder on the properties of sintered glass-ceramics produced from industrial wastes  

Energy Technology Data Exchange (ETDEWEB)

Sintered glass-ceramics were produced from coal fly ashes, red mud from aluminum production and silica fume. The capabilities of Tuncbilek fly ash and a mixture of Orhaneli fly ash, red mud and silica fume to be vitrified and devitrified by sintering process were investigated by means of scanning electron microscopy and X-ray diffraction analysis. To determine the effect of binder in the sintering technique, glass powders were pressed without or with the addition of polyvinyl alcohol. Owing to microstructural observations, density and hardness measurements, it can be said that physical properties and the hardness of the produced samples strongly depended on the crystallization degree of the samples. Toxicity characteristic leaching procedure test results showed that glass-ceramic samples produced by using sintering technique could be considered as nonhazardous materials. Chemical durability of the sintered glass-ceramic samples was also good. ...

2009-09-15

477

SIMS and XRD measurements for the critical review of carbon diffusivity derivation from hardness profiles  

Energy Technology Data Exchange (ETDEWEB)

Microhardness decarburization profiles are often used in the industry to estimate the carbon distribution in steels. For quantitative evaluation, an analysis based on diffusion theory must be performed, the fundamentals and mathematical basics of which are presented. If the relationship between hardness and carbon content is known, microhardness-distance curves of steels can be analyzed in this way. For martensitic grades, for instance, a linearized expression holds in the concentration range from 0.15 to 0.6 m.% C. Microhardness depth profiles of higher carbon steels and other microstructures, however, are also evaluated in the literature. The applicability of quantitative diffusion modeling is discussed in detail. Through hardenable rolling bearing steel 100Cr6 (1.3505, SAE 52100) serves as model material: carbon concentration-distance curves are measured with high accuracy by secondary ion mass spectrometry (SIMS) and compared with microhardness decarburization ...

2007-07-01

478

P-LIGA: 3D-integration of microstructures with curved surfaces by deep ion irradiation  

International Nuclear Information System (INIS)

Using the advantage that the projected range of ions in matter is sharply limited, a new technique for the production of three-dimensional microstructures has been developed. Based on the P-LIGA technique (Proton-Lithographie, Galvanoformung, Abformung) this process allows the generation of structures with surfaces of almost any shape having a root mean square roughness of about #lambda#/50 for visible light wavelengths. An ion beam with diameters between 2 and 50 #mu#m is directly writing the structures and the shape is varied by geometrical manipulation of the sample in three axes during the exposure. Practically, structures have been written using protons with an energy of 1.8 MeV in a provisional experimental setup with beam diameters of 10 and 50 #mu#m, respectively. After irradiation, the parts exposed were dissolved in a liquid developer without affecting the nonirradiated parts. The shape and the rms roughness of the resulting structures were estimated by ...

1998-04-01

479

Microstructure and mechanical properties of quasi-carbon fibers and their polyacrylonitrile matrix composites  

Energy Technology Data Exchange (ETDEWEB)

Quasi-carbon fibers (QCFs) were prepared from Polyacrylonitrile (PAN) precursor by pyrolysis in the temperature range from 400{degrees}C to 950{degrees}C. The QCF-reinforced composites were fabricated by impregnating the QCFs with the PAN resin. The microstructural changes of both QCFs and their composites were characterized by the X-ray diffraction method. The stacking size and the crystallinity of the QCFs increased with the increasing heat treatment temperature (HTT). The crystallinity of the PAN matrix in a composite was also affected by various QCFs. DSC data indicated that thermal reaction mechanism of the composite could be altered due to the interaction between the fiber and the matrix. DMTA studies showed that good adhesion existed at the interface of the QCF-reinforced composites containing lower HTT fibers. The modulus magnitudes of QCFs and their composites increased with the QCF pyrolysis temperature. Although the QCFs exhibited a decreasing trend in ...

1994-12-31

480

Microstructure and crack propagation in Ti-3Al-8V-6Cr-4Mo-4Zr  

International Nuclear Information System (INIS)

Fatigue-crack growth in air and in aqueous 3.5-percent NaCl as well as fracture toughness are evaluated for the metastable beta-titanium alloy Ti-3Al-8V-6Cr-4Mo-4Zr in various microstructural conditions. Two solution heat treatments (SHT), 800 C and 927 C, were chosen to produce two different grain sizes. Approximately 20 vol pct unrecrystallized beta grains remained after SHT at the lower temperature. Yield stresses were 895 and 850 MPa, respectively. Both simplex and duplex aging treatments were performed for both grain sizes to vary the distribution of alpha precipitates while keeping the yield stress in the range of 1075-1220 MPa for all aged conditions. Unaged material exhibits significantly higher fracture toughness levels than aged material. The unrecrystallized regions were associated with a loss in ductility and toughness. 21 refs.

1990-10-07

481

Microstructural transformations and kinetics of high-temperature heterogeneous gasless reactions by high-speed x-ray phase-contrast imaging  

Science.gov (United States)

Heterogeneous gasless reactive systems, including high-energy density metal-nonmetal compositions, have seen increasing study due to their various applications. However, owing to their high reaction temperature, short reaction time, and small scale of heterogeneity, investigation of their reaction mechanisms and kinetics is very difficult. In this study, microstructural changes and the kinetics of product layer growth in the W-Si system was investigated using a high-speed x-ray phase-contrast imaging technique. Using the Advanced Photon Source of Argonne National Laboratory, this method allowed direct imaging of irreversible reactions in the W-Si reactive system at frame rates up to 36 000 frames per second with 4 {mu}s exposure and spatial resolution of 10 {mu}m. Details of the Si melt and reactions between W and Si, that are unable to be viewed with visible-light imaging, were revealed. These include processes such as the initiation of nucleated melting and other ...

2009-12-01

482

Microstructural transformations and kinetics of high-temperature heterogeneous gasless reactions by high-speed x-ray phase-contrast imaging  

International Nuclear Information System (INIS)

Heterogeneous gasless reactive systems, including high-energy density metal-nonmetal compositions, have seen increasing study due to their various applications. However, owing to their high reaction temperature, short reaction time, and small scale of heterogeneity, investigation of their reaction mechanisms and kinetics is very difficult. In this study, microstructural changes and the kinetics of product layer growth in the W-Si system was investigated using a high-speed x-ray phase-contrast imaging technique. Using the Advanced Photon Source of Argonne National Laboratory, this method allowed direct imaging of irreversible reactions in the W-Si reactive system at frame rates up to 36 000 frames per second with 4 #mu#s exposure and spatial resolution of 10 #mu#m. Details of the Si melt and reactions between W and Si, that are unable to be viewed with visible-light imaging, were revealed. These include processes such as the initiation of nucleated melting and other ...

2009-12-01

483

Microstructural characterization of dissimilar welds between alloy 800 and HP heat-resistant steel  

International Nuclear Information System (INIS)

In this study, dissimilar welds between HP heat-resistant steel and Incoloy 800 were made with four different filler materials including: 309 stainless steel and nickel-based Inconel 82, 182 and 617. The microstructure of the base metals, weld metals and their interfaces were characterized by utilizing optical and scanning electron microscopy. Grain boundaries migration in the weld metals was studied. It was found that the migration of grain boundaries in the Inconel 82 weld metal was very extensive. Precipitates of TiC and M_2_3C_6 (M = Cr and Mo) in the Inconel 617 weld metal are identified. The necessary conditions for the formation of cracks close to the fusion line of the 309-HP joints are described. Furthermore unmixed zone near the fusion line between HP steel base metal and Inconel 82 weld metal is discussed. An epitaxial growth is characterized at the fusion line of the 309-Alloy 800 and Inconel 617-Alloy 800 joints.

2008-10-01

484

Microstructural and Mechanical Characterization of Actively Brazed Alumina Specimens  

Energy Technology Data Exchange (ETDEWEB)

Alumina (94 and 99.8% grade compositions) was brazed directly to itself with gold-based active brazing alloys (ABA's) containing vanadium additions of 1,2 and 3 weight percent. The effects of brazing conditions on the joint properties were investigated. Wetting behavior, interfacial reactions, microstructure, hermeticity and tensile strength were determined. Wetting was fair to good for the ABA and base material combinations. Microanalysis identified a discontinuous Al-V-O spinel reaction product at the alumina-braze interface. Tensile strength results for 94% alumina were uniformly good and generally not sensitive to the vanadium concentration, with tensile values of 85-105 MPa. There was more variability in the 99.8% alumina strength results, with values ranging from 25-95 MPa. The highest vanadium concentration (3 wt. %) yielded the highest joint strength for the brazed 99.8% alumina. Failures in the 99.8% alumina samples occurred at the braze-alumina ...

1999-08-26

485

Microstructural Coarsening during Thermomechanical Fatigue and Annealing of Micro Flip-Chip Solder Joints  

Energy Technology Data Exchange (ETDEWEB)

Microstructural evolution due to thermal effects was studied in micro solder joints (55 {+-} 5 {micro}m). The composition of the Sn/Pb solder studied was found to be hypereutectic with a tin content of 65--70 wt%.This was determined by Energy Dispersive X-ray analysis and confirmed with quantitative stereology. The quantitative stereological value of the surface-to-volume ratio was used to characterize and compare the coarsening during thermal cycling from 0--160 C to the coarsening during annealing at 160 C. The initial coarsening of the annealed samples was more rapid than the cycled samples, but tapered off as time to the one-half as expected. Because the substrates to which the solder was bonded have different thermal expansion coefficients, the cycled samples experienced a mechanical strain with thermal cycling. The low-strain cycled samples had a 2.8% strain imposed on the solder and failed by 1,000 cycles, despite undergoing less coarsening than the annealed ...

1998-12-01

486

Magnetic microstructure of candidates for epitaxial dual Heusler magnetic tunnel junctions  

Energy Technology Data Exchange (ETDEWEB)

Heusler alloys are considered as interesting ferromagnetic electrode materials for magnetic tunnel junctions, because of their high spin polarization. We, therefore, investigated the micromagnetic properties in a prototypical thin film system comprising two different Heusler phases Co{sub 2}MnSi (CMS) and Co{sub 2}FeSi (CFS) separated by a MgO barrier. The magnetic microstructure was investigated by X-ray photoemission electron microscopy (XPEEM). We find a strong influence of the Heusler phase formation process on the magnetic domain patterns. SiO{sub 2}/V/CMS/MgO/CFS and SiO{sub 2}/V/CFS/MgO/CMS trilayer structures exhibit a strikingly different magnetic behavior, which is due to pinhole coupling through the MgO barrier and a strong thickness dependence of the magnetic ordering in Co{sub 2}MnSi.

2009-05-15

487

Influence of sigma-phase formation on the localized corrosion behavior of a duplex stainless steel  

International Nuclear Information System (INIS)

Because of their austenitic-ferritic microstructures, duplex stainless steels offer a good combination of mechanical and corrosion resistance properties. However, heat treatments can lower the mechanical strength of these stainless steels as well as render them susceptible to intergranular corrosion (IGC) and pitting corrosion. In this study, a low-carbon (0.02%) duplex stainless steel is subjected to various heat treatments at 450 to 950 C for 30 min to 10 h. The heat-treated samples than undergo ASTM IGC and pitting corrosion tests, and the results are correlated with the microstructures obtained after each heat treatment. In the absence of Cr_2_3C_6 precipitation, #sigma#-phase precipitates render this duplex stainless steel susceptible to IGC and pitting corrosion. Even submicroscopic #sigma#-phase precipitates are deleterious for IGC resistance. Longer-duration heat treatments (at 750 to 850 C) induce chromium diffusion to replenish the ...

1996-01-01

488

Fracture behavior of heat-affected zone in low alloy steels  

International Nuclear Information System (INIS)

Past elastic-plastic fracture studies for leak-before-break (LBB) assessment of low alloy steel pipings have been focused mostly on the behavior of base metals and their weld metals. In contrast, the heat-affected zone (HAZ) of a welded pipe has not been studied in detail primarily because the size of the HAZ is too small to make specimens for mechanical properties measurements. In this study, microstructural analyses, microhardness tests, tensile tests and J-R tests have been conducted as a function of distance from a fusion line and temperature for HAZ materials of SA106Gr.C low alloy piping steels. For the ferrite-pearlite steels such as SA106Gr.C, the HAZ specimens showed a higher yield strength and fracture toughness compared with those of its base metal. These characteristics, despite of grain coarsening, can be explained by cleaner microstructures of HAZ materials with a finer morphology of carbides compared with pearlitic-ferritic base ...

2001-11-01

489

Finite element analysis of stresses associated with transformations in magnesia partially stabilized zirconia  

Energy Technology Data Exchange (ETDEWEB)

Anisotropy finite element analysis was performed to study stresses associated with the tetragonal precipitates and the tetragonal to monoclinic transformation in MgO partially stabilized zirconia. Stresses were assumed to be caused by the lattice misfits between the product phase and the parent phase. In the finite element calculations, the tetragonal and monoclinic precipitates were assumed to be lenticular in shape, and the anisotropic elastic constants of the cubic, tetragonal and monoclinic phases were considered. The purpose of this paper is to obtain some knowledge about how stresses respond when the microstructure is changed, and how stress fields affect microstructure development. The finite element results show that increasing a{sub t}/a{sub c} and decreasing c{sub t}/a{sub c} can create a favorable stress field to reduce the growth rate of tetragonal precipitates during the heat treatment. Stresses associated with the single ...

1999-11-30

490

Effects of multi-ion irradiation on microstructural changes in lithium titanate  

Energy Technology Data Exchange (ETDEWEB)

The irradiation behavior of Li{sub 2}TiO{sub 3} under a fusion reactor environment was simulated by simultaneous irradiation of Li{sub 2}TiO{sub 3} by the triple ion beams and the respective single ion beams of O{sup 2+}, He{sup +} and H{sup +}. The microstructural changes in Li{sub 2}TiO{sub 3} caused by the irradiation were measured by FT-IR photoacoustic spectroscopy. The results suggest that the amount of TiO{sub 2} formed is proportional to the dpa and that the method of irradiation does not affect the dependence of formation of TiO{sub 2}. On the other hand, the amount of defects and/or radiolytic products generated by irradiation, which is considered to trap hydrogen near the surface, is found to be affected by the method of irradiation. Such phenomena are believed to affect the tritium release behavior from Li{sub 2}TiO{sub 3}, and durability of Li{sub 2}TiO{sub 3} and compatibility of Li{sub 2}TiO{sub 3} with other components of the breeder blanket such as ...

2009-04-30

491

Effects of multi-ion irradiation on microstructural changes in lithium titanate  

International Nuclear Information System (INIS)

The irradiation behavior of Li_2TiO_3 under a fusion reactor environment was simulated by simultaneous irradiation of Li_2TiO_3 by the triple ion beams and the respective single ion beams of O"2"+, He"+ and H"+. The microstructural changes in Li_2TiO_3 caused by the irradiation were measured by FT-IR photoacoustic spectroscopy. The results suggest that the amount of TiO_2 formed is proportional to the dpa and that the method of irradiation does not affect the dependence of formation of TiO_2. On the other hand, the amount of defects and/or radiolytic products generated by irradiation, which is considered to trap hydrogen near the surface, is found to be affected by the method of irradiation. Such phenomena are believed to affect the tritium release behavior from Li_2TiO_3, and durability of Li_2TiO_3 and compatibility of Li_2TiO_3 with other components of the breeder blanket such as structural materials in the fusion reactor system under operation.

2009-04-30

492

Effects of Mo, Cr, and V Additions on Tensile and Charpy Impact Properties of API X80 Pipeline Steels  

Science.gov (United States)

In this study, four API X80 pipeline steels were fabricated by varying Mo, Cr, and V additions, and their microstructures and crystallographic orientations were analyzed to investigate the effects of their alloying compositions on tensile properties and Charpy impact properties. Because additions of Mo and V promoted the formation of fine acicular ferrite (AF) and granular bainite (GB) while prohibiting the formation of coarse GB, they increased the strength and upper-shelf energy (USE) and decreased the energy transition temperature (ETT). The addition of Cr promoted the formation of coarse GB and hard secondary phases, thereby leading to an increased effective grain size, ETT, and strength, and a decreased USE. The addition of V resulted in a higher strength, a higher USE, a smaller effective grain size, and a lower ETT, because it promoted the formation of fine and homogeneous of AF and GB. The steel that contains 0.3 wt pct Mo and 0.06 wt pct V without Cr had ...

2009-08-01

493

Effects of CdCl2 treatment on properties of CdTe thin films grown by evaporation at low substrate temperatures  

International Nuclear Information System (INIS)

The structural, morphological and optical properties of vacuum-evaporated CdTe thin films were investigated as a function of substrate temperature and post-deposition annealing without and with CdCl2/treatment at 400 C for 30 min. Diffraction patterns are almost the same exhibiting higher preferential orientation corresponding to (111) plane of the cubic phase. The intensity of the (111) peak increased with the CdCl2/annealing treatment. The microstructure observed for all films following the CdCl2/annealing treatment are granular, regardless of the as-deposited microstructure. The grain sizes are increased after the CdCl2/annealing treatment but now contain voids around the grain boundaries. The optical band gaps, Eg, were found to be 1.50, 1.50 and 1.48 eV for films deposited at 200 K and annealed without and with CdCl2/treatment at 400 C for 30 min respectively. A progressive sharpening of the absorption edge upon heat treatment particularly ...

2007-09-01

494

Effect of Al and Be ions pre-implantation on formation and growth of helium bubbles in SiC/SiC composites  

Energy Technology Data Exchange (ETDEWEB)

The effect of Al and Be ions pre-implantation on microstructural change and, the formation and growth of He bubbles in SiC/SiC composite was investigated. Four kinds of ion implanted specimens were prepared with 100 appm Al, 1000 appm Al, 100 appm Be and 1000 appm Be implanted. No microstructural change was observed in the matrices and fibers of SiC/SiC composites implanted with Al or Be ions up to 1000 appm. The un-implanted and Al or Be pre-implanted SiC/SiC composites were simultaneously irradiated to 10 dpa using triple ion-beams (6.0-MeV Si{sup 2+}, 1.0-MeV He{sup +} and 340-keV H{sup +}) at 1000 deg. C. Helium bubbles were formed in every matrix and fiber irradiated by triple ion-beams. The size of He bubbles in the matrix was increased by implanting Al or Be ions and increased with increasing amount of implanted Al or Be ions. The size of He bubbles in the fiber was slightly increased by implanting Al or Be ions. These results suggest ...

2007-03-15

495

Effect of Al and Be ions pre-implantation on formation and growth of helium bubbles in SiC/SiC composites  

International Nuclear Information System (INIS)

The effect of Al and Be ions pre-implantation on microstructural change and, the formation and growth of He bubbles in SiC/SiC composite was investigated. Four kinds of ion implanted specimens were prepared with 100 appm Al, 1000 appm Al, 100 appm Be and 1000 appm Be implanted. No microstructural change was observed in the matrices and fibers of SiC/SiC composites implanted with Al or Be ions up to 1000 appm. The un-implanted and Al or Be pre-implanted SiC/SiC composites were simultaneously irradiated to 10 dpa using triple ion-beams (6.0-MeV Si"2"+, 1.0-MeV He"+ and 340-keV H"+) at 1000 deg. C. Helium bubbles were formed in every matrix and fiber irradiated by triple ion-beams. The size of He bubbles in the matrix was increased by implanting Al or Be ions and increased with increasing amount of implanted Al or Be ions. The size of He bubbles in the fiber was slightly increased by implanting Al or Be ions. These results suggest that Al or Be as ...

2007-03-01

496

Design of experiment approach applied to reducing and oxidizing tolerance of anode supported solid oxide fuel cell. Part I: Microstructure optimization  

British Library Electronic Table of Contents (United Kingdom)

The main drawback of Ni/YSZ anode supports for solid oxide fuel cell application is their low tolerance to reducing and oxidizing (RedOx) atmosphere changes, owing to the Ni/NiO volume variation. This work describes a structured approach based on design of experiments for optimizing the microstructure for RedOx stability enhancement. A full factorial hypercube design and the response surface methodology are applied with the variables and their variation range defined as: (1) NiO proportion (40-60wt% of the ceramic powders), (2) pore-former proportion (0-30wt% corresponding to 0-64vol.%), (3) NiO particle size (0.5-8mm) and (4) 8YSZ particle size (0.6-9mm). To obtain quadratic response models, 25 different compositions were prepared forming a central composite design. The measured responses...

2011-01-01

497

Creep-fatigue and temperature synergisms in alloy 800  

Energy Technology Data Exchange (ETDEWEB)

Alloy 800 from three different commercial heats have been continuously cycled and cycled with a hold period at 922/sup 0/K. The starting microstructures of these heats reflects an inherently wide spectrum of possibilities for Alloy 800. The amounts and morphologies of the TiC and M/sub 23/C/sub 6/ carbides are different among the heats. During cycling, M/sub 23/C/sub 6/ forms intragranularly in a solution annealed heat. This precipitation contributes to the cyclic hardening. Both mill annealed heats of Alloy 800 are stable to carbide precipitation during cycling. The heat with the lower carbon content formed ..gamma..' during cycling but the volume fraction was too low to contribute to hardening. The inclusion of hold periods caused the dislocation substructure to become more diffuse in the mill annealed heats. The cyclic hardening was enhanced with the inclusion of the hold periods but this was not due to any microstructural change ...

1984-01-01

498

Constant extension rate (CERT) testing of alloy 690 and 800 nuclear steam generator tubing  

Energy Technology Data Exchange (ETDEWEB)

Constant extension rate (CERT) tests were performed on Alloy 690 and Alloy 800 nuclear steam generator tubing specimens. For the Alloy 690 specimens, tests were performed in deaerated 10% sodium hydroxide solutions at 315 deg C with a +100 mV applied potential. For the Alloy 800 specimens, tests were performed in deaerated 5% sodium hydroxide solutions at 343 deg C with no applied potential. The test specimens were machined from tubing which was produced by different manufacturing processes and in different heat treated conditions. The Alloy 690 tubing was tested in six different thermomechanical conditions, while the Alloy 800 tubing was tested in four different thermomechanical conditions. The results from the test program include a complete microstructural examination using light-optical and scanning electron microscopy. The CERT test results (such as maximum stress achieved and crack morphology) are correlated to tubing microstructure, ...

1994-12-31

499

Ceramic/polymer functionally graded material (FGM) lightweight armor system  

Energy Technology Data Exchange (ETDEWEB)

This is the final report of a two-year, Laboratory Directed Research and Development (LDRD) project at the Los Alamos National Laboratory (LANL). Functionally graded material is an enabling technology for lightweight body armor improvements. The objective was to demonstrate the ability to produce functionally graded ceramic-polymer and ceramic-metal lightweight armor materials. This objective involved two aspects. The first and key aspect was the development of graded-porosity boron-carbide ceramic microstructures. The second aspect was the development of techniques for liquid infiltration of lightweight metals and polymers into the graded-porosity ceramic. The authors were successful in synthesizing boron-carbide ceramic microstructures with graded porosity. These graded-porosity boron-carbide hot-pressed pieces were then successfully liquid-infiltrated in vacuum with molten aluminum at 1,300 C, and with liquid polymers at room temperature. ...

1998-12-31

500

A personal computer based system to evaluate J-integral by a single specimen unloading compliance method: Pt. 2  

International Nuclear Information System (INIS)

A personal computer based single specimen unloading technique has been demonstrated using a nuclear grade pressure vessel material, A533B Class I steel, and an #alpha#-#beta# titanium alloy, CORONA-5. Experimental parameters investigated in the case of steel include the effect of test temperature, loading rate and neutron irradiation. Results revealed the effect of dynamic strain aging (DSA) as a drop in the critical crack initiation fracture toughness (Jsub(q)); the minimum in Jsub(q) shifts to higher temperatures at higher test speeds as predicted from DSA models. In CORONA-5, the effects of microstructure and heat treatment for two different sizes of equiaxed #alpha# morphology in a #beta#-matrix heat treated to different yield strengths were investigated. It is found that the observed higher values of Jsub(q) and tearing modulus result from a greater tortuosity of the crack path and ease of crack blunting. The largest increase in Jsub(q) occurred in fine ...