WorldWideScience
2

Neutron magnetic scattering studies on ferromagnetism in potassium nanoclusters arrayed in zeolite A-Trial experiments  

Energy Technology Data Exchange (ETDEWEB)

Potassium clusters arrayed in zeolite A are known to show ferromagnetic properties at low temperature. The origin of the spontaneous magnetization has been explained by a model of spin-canting in an antiferromagnetically ordered state. The direct information for the magnetic structure, however, has not been obtained so far. In the present work, we measure the neutron powder diffraction by using pulsed neutron source at KEK-KENS below and above the Curie temperature. No significant temperature-dependence was, however, obtained within the statistical errors, namely, magnetic scattering could not be detected separately. We also estimate the intensity of magnetic scattering by assuming some possible magnetic structures with considering the magnetic form factor of the cluster wave function. The intensity of magnetic ...

2009-02-21

3

Neutron magnetic scattering studies on ferromagnetism in potassium nanoclusters arrayed in zeolite A-Trial experiments  

International Nuclear Information System (INIS)

Potassium clusters arrayed in zeolite A are known to show ferromagnetic properties at low temperature. The origin of the spontaneous magnetization has been explained by a model of spin-canting in an antiferromagnetically ordered state. The direct information for the magnetic structure, however, has not been obtained so far. In the present work, we measure the neutron powder diffraction by using pulsed neutron source at KEK-KENS below and above the Curie temperature. No significant temperature-dependence was, however, obtained within the statistical errors, namely, magnetic scattering could not be detected separately. We also estimate the intensity of magnetic scattering by assuming some possible magnetic structures with considering the magnetic form factor of the cluster wave function. The intensity of magnetic ...

2009-02-21

4

Magnetic phase transition in UPd_2Si_2  

International Nuclear Information System (INIS)

... fields magnetic moments neel temperature neutron diffraction order-disorder

6

Diffraction Experiments at the IBR-2 Pulsed Reactor with Methane Cold Neutron Source  

CERN Document Server

A new methane cold neutron source has been tested at the IBR-2 pulsed reactor at the Frank Laboratory of Neutron Physics. In a paper the results of experiments at neutron diffractometers HRFD and DN-2 which are placed at the IBR-2 from the methane moderator side are given. A comparison with the results obtained with the conventional water comb-like moderator is performed. The perspectives of the cold source for various kinds of neutron diffraction experiments, including atomic and magnetic structural analysis and real time experiments are discussed. It is shown, that for a huge number of the experiments which are performing at both HRFD and DN-2 the methane cold neutron source provides the better conditions than water comb-like moderator.

2000-01-01

7

Upgrade of X-ray Magnetic Diffraction Experimental System and Its Application to Ferromagnetic Material  

International Nuclear Information System (INIS)

We have performed X-ray magnetic diffraction (XMD) experiment of ferromagnets at the Photon Factory (PF) of the High Energy Accelerator Research Organization (KEK) in Tsukuba. In this study, we have upgraded the XMD experimental system in order to apply this method to as many samples as possible. Upgrade was made for (1) the X-ray counting system and related measurement program, (2) the electromagnet, and (3) the refrigerator. The performance of the system was enhanced so that (1) the counting rate capability was improved from 104cps to 105cps, (2) the maximum magnetic field was increased from 0.85T to 2.15T, and (3) the lowest sample temperature was reduced from 15K to 5K. The new system was applied to an orbital ordering compound of YTiO3, and we obtained spin magnetic form factor for the reflection plane (010) perpendicular to the b axis. The magnetic field ...

2007-01-19

9

Remodeling of the free electron laser with the L-band linac at Osaka University  

International Nuclear Information System (INIS)

The far infrared free electron laser (FEL) has been being developed since 1990 using the L-band electron linac at the Institute of Scientific and Industrial Research, Osaka University. The first lasing was obtained in 1994 at wavelengths from 32 to 40 #mu#m. The FEL is now being modified suitable for user experiments. The wiggler with a fixed magnet gap used in the original FEL has been remodeled to make the magnet gap variable. In order to optimize the variable range of the gap, the gain and the diffraction loss were calculated. The peak gain is calculated to be 270% and the diffraction loss to be 22% at 150 #mu#m. The wavelength is expected to be variable from 25 up to at least 150 #mu#m. The two bending magnets in the optical resonator have been remodeled and the vacuum chambers with larger vertical sizes for them have been newly made so that the ...

1997-02-28

10

Magnetic ordering in CeM_2Si_2 (M = Ag,Au,Pd,Rh) compounds as studied by neutron diffraction  

International Nuclear Information System (INIS)

We report the results of neutron-diffraction experiments on CeM_2Si_2 (M = Ag,Au,Pd,Rh) which were performed to explore the role of valence fluctuations and 4f hybridization in the magnetic ordering of cerium compounds. All four order antiferromagnetically, the first three exhibiting structures consisting of ferromagnetic layers with moments perpendicular to the layers, which are believed to be characteristic of 4f-4f interactions mediated through hybridization with conduction electrons. CePd_2Si_2 has an anomalously small moment (0.62#mu#/sub B/) in the ordered state. CeAg_2Si_2 exhibits an incommensurate longitudinal, static magnetization wave with moment and propagation direction along the a axis. The fourth compound, CeRh_2Si_2, has the highest known transition temperature (39 K) reported for cerium ordering; it exhibits another second-order transition at 27 K to a complex commensurate structure ...

11

Magnetic ordering in CeM/sub 2/Si/sub 2/ (M = Ag,Au,Pd,Rh) compounds as studied by neutron diffraction  

Energy Technology Data Exchange (ETDEWEB)

We report the results of neutron-diffraction experiments on CeM/sub 2/Si/sub 2/ (M = Ag,Au,Pd,Rh) which were performed to explore the role of valence fluctuations and 4f hybridization in the magnetic ordering of cerium compounds. All four order antiferromagnetically, the first three exhibiting structures consisting of ferromagnetic layers with moments perpendicular to the layers, which are believed to be characteristic of 4f-4f interactions mediated through hybridization with conduction electrons. CePd/sub 2/Si/sub 2/ has an anomalously small moment (0.62..mu../sub B/) in the ordered state. CeAg/sub 2/Si/sub 2/ exhibits an incommensurate longitudinal, static magnetization wave with moment and propagation direction along the a axis. The fourth compound, CeRh/sub 2/Si/sub 2/, has the highest known transition temperature (39 K) reported for cerium ordering; it exhibits another second-order transition at 27 ...

1984-03-01

12

Studies of interlayer magnetic coupling in all-semiconductor superlattices by means of neutron scattering techniques  

International Nuclear Information System (INIS)

An overview on neutron scattering studies of ferromagnetic and antiferromagnetic all-semiconductor superlattices is presented. Diffraction experiments on MnTe/CdTe, MnTe/ZnTe and EuTe/PbTe superlattices show pronounced correlations between the MnTe and EuTe layers across the non-magnetic spaces, even though these layers are antiferromagnetic and the systems are nearly-insulating. Current theory status of these systems is discussed. Diffractometry and reflectometry data from EuS/PbS superlattices reveal pronounced antiferromagnetic coupling between the ferromagnetic EuS block. First polarized neutron reflectometry data from superlattices prepared of a novel ferromagnetic 'spintronics' material, Ga(Mn)As are also presented. (author)

2001-09-23

13

Magnetic Levitation of MC3T3 Osteoblast Cells as a Ground-Based Simulation of Microgravity  

UK PubMed Central (United Kingdom)

Diamagnetic samples placed in a strong magnetic field and a magnetic field gradient experience a magnetic force. Stable magnetic levitation occurs when the magnetic force exactly counter balances...Full Text Available

2009-11-01

14

Double umbrella structure in terbium iron garnet  

International Nuclear Information System (INIS)

The umbrella magnetic structure of the terbium iron garnet (TbIG) has been studied using neutron diffraction experiments peformed in the 4.2 to 650 K temperature range which covers both the Neel temperature (Tsub(N) = 550 +- 10 K) and the compensation temperature (Tsub(comp) = 244 +- 2 K). When T > Tsub(N), the observed peak intensities originate from nuclear contribution only. When Tsub(comp) < T < Tsub(N), the results have been interpreted in the Neel theory of ferrimagnetism. Below Tsub(comp), three salient features have been observed: there appears superstructure lines forbiden by the cubic space group Ia3d, whereas the other superstructure peaks are found absent contrary to other heavy rare earth garnets; the strongest reflexion (110) vanishes near Tsub(comp). The magnetic modes associated to the rhombohedral symmetry space group R(-3)c have been calculated; the two inequivalent ...

1984-04-10

16

Diffraction studies of nanocrystals: theory and experiment  

International Nuclear Information System (INIS)

Based on theoretical calculations of powder diffraction data it is shown that the assumption of the infinite crystal lattice for small particles is not justified, leads to significant changes of the diffraction patterns, and may lead to erroneous interpretation of the experimental results. An alternate evaluation of diffraction data of nanoparticles, based on the so-called 'apparent lattice parameter', alp, is proposed. (author)

2001-09-23

17

Teaching electron diffraction and imaging of macromolecules.  

UK PubMed Central (United Kingdom)

Electron microscopic analysis can be used to determine the three-dimensional structures of macromolecules at resolutions ranging between 3 and 30 A. It differs from nuclear magnetic resonance spectroscopy...Full Text Available

1993-05-01

18

Spin-polarized Auger-electron diffraction study of the magnetic poisoning of Fe(001) by sulfur  

International Nuclear Information System (INIS)

Spin-polarized angle-resolved sulfur L_2_,_3VV Auger-electron spectra have been recorded for the c(2x2)S/Fe(001) system. The data show the modulation of the sulfur Auger spin polarization as a function of emission angle, which represents an observation of spin-polarized Auger-electron diffraction (SPAED), a potentially powerful tool for the study of local magnetic structure at surfaces, interfaces, and thin films. Theoretical modeling of the SPAED data indicates a large decrease in the magnetization of the top iron layer, suggesting a magnetic poisoning induced by the sulfur overlayer. These findings are independently supported by the observation of a large decrease of secondary electron spin polarization upon sulfur adsorption.

19

Magnetic properties of ErPd_2Si_2 from magnetization Moessbauer and neutron diffraction measurements  

International Nuclear Information System (INIS)

Magnetization, neutron diffraction and "1"6"6Er Moessbauer measurements on ErPd_2Si_2 are reported. Below 4.8 K ErPd_2Si_2 orders AF with complex modulated magnetic structures, where the Er moments are aligned along the c-axis. At 1.5 K a squared structure with #mu#_E_r #approx# 7.8(1)#mu#_B is found while a saturation Er moment of 8.2(2)#mu#_B is inferred from the hyperfine field data. The temperature dependence of the Moessbauer spectra in the paramagnetic region is explained in the framework of a relaxation model implying excited crystal field levels. Its analysis is used to estimate the B"m_n CEF parameters. (orig.).

20

Microstructure Characterization of Magnetic-Pulse-Welded AA 6061-T6 by Electron Backscattered Diffraction  

Energy Technology Data Exchange (ETDEWEB)

The grain boundary crystallographic misorientations of magnetic-pulse-welded (MPW) aluminum alloy (AA) 6061-T6 in linear and tubular configurations were examined using the electron backscattered diffraction (EBSD) technique. A refined structure of heavily deformed grains with higher grain boundary angles was observed in linear welds. Significant spalling was observed away from the joints, in the interior of tubular welds. The results show the complex interaction of shock waves with the materials during this impact welding process.

2008-08-01

21

/sup 239/PuN powder neutron diffraction study  

Energy Technology Data Exchange (ETDEWEB)

A powder neutron diffraction study has been carried out on /sup 239/PuN, which was reported to be antiferromagnetic below T = 13 K. No magnetic ordering has been detected at 4 K, the limit of the magnetic ordering which could be detected being ..mu..sub(ord) = 0.25 ..mu..sub(B) per Pu atom. Moreover a neutron scattering length determination of /sup 239/Pu was performed which gave a value of bsub(239Pu) = (0.81 +- 0.05) x 10/sup -12/ cm at a neutron wavelength lambda = 1.219 A.

1984-10-01

22

Magnetic structure of Ce(Ru_0_._9_6Pd_0_._0_4)_2Si_2  

International Nuclear Information System (INIS)

The magnetic structure of a tetragonal Ce(Ru_0_._9_6Pd_0_._0_4)_2Si_2 single crystal, determined by neutron diffraction measurements, is similar to that observed in Rh doped alloys. The magnetic moments are oriented and modulated along the c-axis. Here the wave vector is incommensurate: k=(0,0,0.38). At 1.5 K, the moment is estimated to about 0.3 #mu#_B. Magnetization, magnetoresistance and Hall effect measurements performed on this alloy are also reported. (orig.).

23

Structure of molten alkali halides  

Energy Technology Data Exchange (ETDEWEB)

The results of X-ray and neutron diffraction experiments on molten alkali halides in which some data of our experiments by X-ray diffraction such as those of molten LiCl, NaCl, KCl, LiBr and KBr are included were summarized. The first peak positions in the radial distribution function in molten alkali halides by X-ray or neutron diffraction experiments are always longer than those by computer simulations and the differences of 0.1 -- 0.3 A exceed the experimental error. It seems to be due to the deformation of the electron shell. In the computer simulation, the shell model which has the spherical deformation was expected to have a closer value of the first peak position to the experimental one than the rigid ion model by taking the polarization of ions. However, no change in the first peak position was found. Therefore, the non-spherical deformation of electron ...

1982-06-01

24

Structure of molten alkali halides  

International Nuclear Information System (INIS)

The results of X-ray and neutron diffraction experiments on molten alkali halides in which some data of our experiments by X-ray diffraction such as those of molten LiCl, NaCl, KCl, LiBr and KBr are included were summarized. The first peak positions in the radial distribution function in molten alkali halides by X-ray or neutron diffraction experiments are always longer than those by computer simulations and the differences of 0.1 -- 0.3 A exceed the experimental error. It seems to be due to the deformation of the electron shell. In the computer simulation, the shell model which has the spherical deformation was expected to have more closer value of the first peak position to the experimental one than the rigid ion model by taking the polarization of ions. However, no change in the first peak position was found. Therefore, the non-spherical deformation of ...

1982-01-01

25

Magnetization reversal phenomena and domain wall behaviours in nanostructured magnetic systems  

International Nuclear Information System (INIS)

Several recent experiments on micro- (or nano-) structured samples of ferromagnetic materials are introduced. Magnetization reversal phenomena are investigated on submicron wire samples of trilayer structure using the giant magnetoresistance effect. Domain wall movements are sensitively monitored by resistivity measurements and the velocity of propagation is determined. The contribution of domain wall to the resistivity is argued from the results on artificially designed samples of a spring-magnet system. In circular dots of permalloy, the existence of vortex magnetization is confirmed and the reversal of the vortex core magnetization is studied from magnetic force microscopy measurements. (author)

2001-09-23

26

Structural relaxation and crystallization in the Fe-Cr-Si-B and Fe-Cu-Cr-Si-B amorphous alloys  

International Nuclear Information System (INIS)

Structural relaxation, crystallization and optimisation processes in soft magnetic amorphous alloys based on iron are examined by applying different experimental techniques: X-ray diffraction analysis, high-resolution electron microscopy, measurements of magnetic and electric properties (permeability, after-effect resistivity). The presented results are discussed in terms of annealing out of microvoids, formation of nanocrystalline phase and changes of effective magnetostriction constant. (author)

2001-09-23

27

Smith-Purcell radiation in the highly relativistic regime  

International Nuclear Information System (INIS)

An electron moving over the surface of a diffraction grating will transfer a part of its kinetic energy to radiation via a velocity synchronous coupling with a slow space harmonic component of the field. Since the phase velocity of a slow space harmonic is less than the speed of light, the slow components decay exponentially, or evanesce, with distance above the grating and the evanescence scale is determined by the product of the relative velocity, #beta#, the relative energy, #gamma#, and the wavelength #lambda#. Thus, in the relativistic regime, good electron - grating coupling can be maintained at beam heights that are greater than the emitted wavelength. In order to explore this regime a series of experiments have been carried out with moderately energetic beams and an experiment with the 70-MeV beam at the Accelerator Test Facility is in the planning stage. The work has two basic goals: the first is to explore the ...

1995-08-21

28

Moessbauer diffraction measurements on polycrystalline bcc iron  

Energy Technology Data Exchange (ETDEWEB)

In the early days of Moessbauer spectroscopy, it was demonstrated that coherent scattering of photons emitted by a Moessbauer source can be observed. In spite of the fact that scattering experiments could give information not accessible by the absorption method, they are not widely used. The reasons for this are, on the one hand, experimental difficulties, and on the other hand, the form of the samples, which should be large single crystals in most cases. In this work, we present a Moessbauer diffraction measurement on polycrystalline bcc iron where these problems have been overcome. We demonstrate that using the kinematical theory of gamma-ray diffraction, useful information on the relative orientation of the crystallographic axis to the hyperfine field directions can be subtracted. (orig.)

1994-11-01

29

FELIX Experiments: Measurements of Electromagnetic Effects.  

Science.gov (United States)

Three major series of experiments have been conducted with the FELIX facility at ANL. Experiments on the coupling between eddy currents and angular displacements of loops and plates in crossed constant and changing magnetic fields demonstrated that the co...

1985-01-01

30

Changes in the profile structure of the sarcoplasmic reticulum membrane induced by phosphorylation of the Ca2+ ATPase enzyme in the presence of terbium: a time-resolved x-ray diffraction study.  

UK PubMed Central (United Kingdom)

The design of the time-resolved x-ray diffraction experiments reported in this and an accompanying paper was based on direct measurements of enzyme phosphorylation using [gamma-32P]ATP that were employed...Full Text Available

1994-05-01

31

Neutron diffraction study of quasi-one-dimensional spin-chain compounds Ca3Co2-xFexO6  

International Nuclear Information System (INIS)

We report the results of the DC magnetization, neutron powder diffraction and neutron depolarization studies on the spin-chain compounds Ca3Co2-xFexO6 (x = 0, 0.1, 0.2 and 0.4). Rietveld refinement of neutron powder diffraction patterns at room temperature confirms the single-phase formation for all the compounds in rhombohedral structure with space group R3-barc. Rietveld refinement also confirms that Fe was doped at the trigonal prism site, 6a (0, 0, 1/4) of Co. The high temperature magnetic susceptibility obeys the Curie-Weiss law; the value of the paramagnetic Curie temperature (?p) decreases as the concentration of iron increases and it becomes negative for x = 0.4. No extra Bragg peak as well as no observable enhancement in the intensity of the fundamental (nuclear) Bragg peaks has been observed in the neutron diffraction patterns down to 30 K. No depolarization of neutron ...

2008-11-01

32

Neutron diffraction and magnetization studies of pseudoternary HoRh_2_-_xPd_xSi_2 solid solutions (0#<=#x<2)  

International Nuclear Information System (INIS)

Neutron powder diffraction and magnetometric studies of the HoRh_2_-_xPd_xSi_2 series of solid solutions (x=0, 0.5, 0.75, 1.0, 1.5, 1.8) are reported. The intermetallics investigated crystallize in the body-centred-tetragonal ThCr_2Si_2-type structure (space group I4/mmm). All the samples order antiferromagnetically at low temperatures. For low values of the dilution parameter x a simple collinear antiferromagnetic structure of the AFI type is stable. Below T_N the magnetic moments are parallel to the c-axis and then, below T_t, deflect forming an angle #psi# with the c-axis. Further replacement of Rh by Pd results in the development of a sine-wave-modulated magnetic structure with one two-component propagation vector and magnetic moments in the basal plane. For x=1.8 a sine-wave-modulated structure similar to that reported for HoPd_2Si_2 (i.e. with a two-component propagation vector and ...

2002-06-03

33

Refrigerator operating experience on whole body MRI magnet systems  

International Nuclear Information System (INIS)

Several refrigerators for liquid helium and liquid nitrogen systems have been integrated successfully into IGC manufactured whole body Magnetic Resonance Imaging (MRI) magnet systems. The refrigerators have been tested in systems with magnetic fields of 0.6T to 1.5T. Tests were performed to study the effectiveness of the refrigerators, the magnetic field effects on the refrigerators, the effect of the refrigerators on the field uniformity and magnetic resonance image quality. The interface between the refrigerator and the whole body MRI magnet system cryostat was specifically designed to allow retrofit to the existing IGC magnet systems, while ensuring good heat transfer characteristics and good vibration isolation from the cryostat. The interface between the refrigerator and the cryostat and the refrigerator test results are presented.

1985-08-01

34

Progress on the Design and Fabrication of the MICE Focusing Magnets  

Energy Technology Data Exchange (ETDEWEB)

The Muon Ionization Cooling Experiment (MICE) focusing solenoid magnets focus the muon beam within the MICE cooling channel on a liquid or solid absorber that is within the warm bore of solenoid. The focusing magnet has a warm bore of 470 mm. his magnet consists of two coils 210-mm long that is separated by an aluminum mandrel that is 200 mm long. Each of the coils has its own leads. The coils may be operated in either the non-flip mode (solenoid mode with both coils at the same polarity) or the lip mode (quadrupole focusing mode where both coils are at opposite polarity). This report describes the focusing solenoid magnet design that will be built by the vendor. The progress on the construction of the first of the focusing magnets will also be discussed in this report. Ultimately three of these magnets will be built. These ...

2009-10-19

35

Microstructure, texture and mechanical properties of the magnesium alloy AZ31 processed by ECAP  

Energy Technology Data Exchange (ETDEWEB)

To investigate the influence of equal channel angular pressing on the microstructure and texture of the magnesium alloy AZ31, electron backscattering diffraction and well as neutron diffraction experiments were carried out. Through these experiments it was possible to trace the microstructure and texture evolution with strain accumulated with the increasing number of equal channel angular pressing passes. It was further demonstrated by subsequent compression tests that the microstructural changes produced by equal channel angular pressing have a beneficial effect on both the compressive strength and ductility of AZ31. (orig.)

2008-01-15

36

Polarized neutron diffraction study of CePd{sub 3}  

Energy Technology Data Exchange (ETDEWEB)

We have performed polarized neutron diffraction measurements on the intermediate valence compound CePd{sub 3} using the D3 spectrometer at the ILL. The results show that at low temperatures, 1.7 K, as well as at 100 K, the field-induced magnetic amplitudes measured in a field of 4.6 T could be interpreted in terms of two contributions: a 4f-type contribution with a Ce{sup 3+} form factor, and an extra delocalized contribution (relatively narrow in q-extent). In particular, we find that the values of the 4f moment deduced from the extrapolation of the neutron data to Q=0 are systematically lower than the values deduced from bulk magnetization measurements performed on the same sample. This difference can be ascribed to a possible positive polarization of the conduction band which is similar at both temperatures.

2004-07-15

37

Magnetism of DyPd_2Si_2 and ErPd_2Si_2  

International Nuclear Information System (INIS)

Neutron diffraction and magnetometric measurements on polycrystalline samples of DyPd_2Si_2 and ErPd_2Si_2 were carried out in the temperature range from 2 to 293 K. Both compounds show tetragonal ThCr_2Si_2 type crystal structure and order at 12 K in a sine modulated magnetic structure with propagation vectors k=[0.609,0,0.155] and [0.575, 0, 0.083] respectively. The oscillatory character of magnetic order found in RPd_2Si_2 (R=Tb-Er) compounds suggests exchange interaction described by the RKKY model to be dominant, but the non-monotonic dependence of respective Neel temperatures on the number of f-electrons indicates the influence of a crystalline electric field (CEF) on the magnetic behaviour in this series. (orig.).

38

Gamma irradiation induced damage creation on the cation distribution, structural and magnetic properties in Ni-Zn ferrite  

International Nuclear Information System (INIS)

Ferrite of system, namely Ni_1_-_xZn_xFe_2O_4 with x = (0.0, 0.2, 0.4, 0.6, 0.8, 1.0), have been prepared by solid state reaction to investigate the effect of gamma rays irradiations using Co"6"0 source on the cation distribution, structural and magnetic properties. The unirradiated and irradiated samples were then subjected to characterization techniques such as X-ray diffraction, magnetization and AC susceptibility. The results of these characterizations are found to be different for irradiated from that of the pristine sample. The modifications in respect of irradiated samples are explained in terms of the ion-induced disorder. The important result of #gamma#-irradiation on the cation distribution, structural and magnetic properties is the change of ratio Fe"2"+/Fe"3"+. Possible reasons on the results are proposed.

2010-09-01

39

Effects of velocity-dependent force on the magnetic form factors of odd-Z  

International Nuclear Information System (INIS)

We investigate the effects of the velocity-dependent force on the magnetic form factors and magnetic moments of odd-Z nuclei. The form factors are calculated with the harmonic-oscillator wavefunctions. It is found that the contributions of the velocity-dependent force manifest themselves in the very large momentum transfer region (q?4 fm-1). In the low and medium q region the contributions of the velocity-dependent force are very small compared with those without this force. However, in the high-q region the contributions of the velocity-dependent force are larger than the normal form factors. The diffraction structures beyond the existing experimental data are found after the contributions of the velocity-dependent force are included. The formula of the correction to the single particle magnetic moment due to the velocity-dependent force is reproduced exactly in the long-wavelength limit (q=0) of the ...

2008-03-01

40

Spin-resolved magnetic studies of focused ion beam etched nano-sized magnetic structures  

International Nuclear Information System (INIS)

Scanning ion microscopy with polarization analysis (SIMPA) is used to study the spin-resolved surface magnetic structure of nano-sized magnetic systems. SIMPA is utilized for in situ topographic and spin-resolved magnetic domain imaging as well as for focused ion beam (FIB) etching of desired structures in magnetic or non-magnetic systems. Ultra-thin Co films are deposited on surfaces of Si(1 0 0) substrates, and ultra-thin, tri-layered, bct Fe(1 0 0)/Mn/bct Fe(1 0 0) wedged magnetic structures are deposited on fcc Pd(1 0 0) substrates. SIMPA experiments clearly show that ion-induced electrons emitted from magnetic surfaces exhibit non-zero electron spin polarization (ESP), whereas electrons emitted from non-magnetic surfaces such as Si and Pd exhibit zero ESP, which can be used to calibrate ...

2005-04-01

41

Furnace for rapid change of temperature for neutron diffraction  

International Nuclear Information System (INIS)

A new furnace for neutron diffraction experiments is capable of heating and cooling a sample very rapidly. The rapid heating is done by two circular infrared lamps placed over and under a sample, whose radiation is roughly focused on the sample by a reflector. The rapid cooling is done by high-pressure gas blows against the sample from two circular nozzles which are also placed over and under the sample. This system enables us to obtain the heating rate of over 1000"0C/min and cooling rate of -500"0C/min for an alloy of 10 mm diameter and 30 mm length. The performance is sufficient to carry out some kinetics measurements in real-time neutron diffraction by the use of a position-sensitive detector. This kind of experiment is demonstrated by the observation of the relaxation process of order--disorder transitions in CuZn and Ni_3Mn alloys.

42

Diffraction applications using the energy dispersive beamline X6A at the National Synchrotron Light Source  

Energy Technology Data Exchange (ETDEWEB)

The energy dispersive beamline X6A at the National Synchrotron Light Source employs a curved crystal monochromator (polychromator) which focuses a range ([similar to]1 keV) of x-ray energies into a narrow (100--120 [mu]m) line image. Although this beamline was constructed primarily for time-dependent EXAFS experiments, we have begun to explore the use of this instrument for energy dispersive diffraction experiments with different types of sample including macromolecular crystals. The tunability ([ital E]=6.5 to 21 keV) and flexibility ([Delta][ital E]=100--1000 eV) of the instrument makes the beamline ideal as a test bed for the application of polychromatic single-crystal diffraction techniques to different chemical or biological materials.

1995-02-01

43

Magnetization and 61Ni Moessbauer effect study of the ternary arsenide CrNiAs  

International Nuclear Information System (INIS)

The results of x-ray diffraction, dc magnetization, and 61Ni Moessbauer spectroscopy studies of the ternary arsenide CrNiAs are reported. This compound crystallizes in the orthorhombic Fe2P-type structure (space group P6-bar2m) with the lattice parameters a 6.1128(2) A and c = 3.6585(1) A. CrNiAs is a mean-field ferromagnet with Curie temperature TC = 171.9(1) K and the critical exponents ? 0.514(18), ? = 1.010(16), and ? = 2.922(10). The temperature dependence of the magnetic susceptibility above TC follows the modified Curie-Weiss law with a paramagnetic Curie temperature of 176.0(3) K and effective magnetic moment per transition metal atom of 2.42(1) ?B. The magnetic moment per formula unit at 4.2 K is found to be 1.114(33) ?B. The hyperfine magnetic field at 61Ni nuclei at 4.2 K of 41.5(1.0) kOe implies that the Ni atoms carry a magnetic ...

2008-08-13

44

Preliminary Calculations of the Radiation Damage of the Permanent Magnets for TRADE (TRiga Accelerator Driven Experiment)  

CERN Document Server

Monte Carlo calculations of proton irradiation of permanent magnets for the TRADE experiment have been performed. An irradiation dose of about 4´106 Gy/yr/mA has been estimated due to beam losses in normal operating conditions. Existing experimental results indicate that this irradiation level may induce a considerable demagnetization: in fact, a dose of 6´107 Gy induces a remanence loss of 0.3 % on samples of Sm2Co17 magnets, which are the most resistant type. More detailed calculations with the final design of the magnets and of the beam line are suggested, to determine if the irradiation levels allowed a reliable operation of the permanent magnets for the entire duration of the TRADE experiment. Damage and gas production rates have also been calculated; the values obtained are very low, thus confirming that the demagnetization process is in great part ...

2002-01-01

45

Magnetic response of ultrathin Fe on MgO: A polarized neutron reflectometry study  

Energy Technology Data Exchange (ETDEWEB)

The magnetization of ultrathin bcc Fe films (two and three monolayers) on MgO was measured and compared with the behavior predicted for a two-dimensional ferromagnet. The experiment indicated that no hysteresis was present in the magnetization. Instead, the magnetization at low temperature was affected by a marked field cooling effect. These observations lead to the conclusion that films of Fe on MgO of such thickness exhibit superparamagnetic behavior as if they were not entirely continuous. In contrast, films thicker than five monolayers exhibit a magnetic response close to that of bulk iron.

1994-11-15

46

Direct observation of ordered orbital of YTiO_3 by the X-ray magnetic diffraction technique  

International Nuclear Information System (INIS)

X-ray magnetic diffraction (XMD) technique was applied to an orbital ordering compound of ferromagnetic YTiO_3 for the first time. The orbital-magnetic form factor #mu# _L(k) and the spin-magnetic form factor #mu# _S(k) were independently measured by utilizing the LS separation ability of the XMD. The #mu# _L(k) was measured for ten reciprocal-lattice points. No significant values of the #mu# _L(k) were observed for most of the reciprocal-lattice points within the estimated statistical errors, which suggested quenching of the orbital moment. The #mu# _S(k) was measured for 22 reciprocal-lattice points. Fourier synthesis of the #mu# _S(k) gave the spin density distribution m _S(r) in the real space. The obtained m _S(r) map shows the characteristic feature of the electron distribution of 3d electron in the t_2_g state of a Ti atom coordinated by O"2"- ions, in which the electrons are distributed away ...

2005-08-01

47

Application of neutron diffraction in chemistry. Pt. 2  

Energy Technology Data Exchange (ETDEWEB)

This article provides a survey of neutron scattering experiments in condensed matter research, which are of interest to chemistry. The theoretical background has been treated in a previous issue. The present article consists of two parts. The first part exhibits the range of experimental possibilities by means of a few selected examples. The starting point is classical neutron diffraction by which the position of atomic nuclei may be determined. Additional information on the spatial distribution in the outer electron shells may be obtained via combined X-ray/neutron-diffraction experiments or via the diffraction of polarized neutrons. Progress in instrumentation, due to the development of more intense sources, has influenced especially the fields of small angle scattering and spectroscopy. The second part features domains of research of current interest, where a combination of ...

1982-01-01

48

Neutron diffraction study of 5f itinerant antiferromagnet UPtGa{sub 5} and UNiGa{sub 5}  

Energy Technology Data Exchange (ETDEWEB)

Magneto-striction and magnetic form factors in 5f itinerant antiferromagnets UNiGa{sub 5} and UPtGa{sub 5} are studied by means of neutron scattering. Remarkable magneto-striction was observed around T{sub N}, indicating large spin-orbit coupling in the itinerant system. The orbital magnetic moment is found to be strongly suppressed due to the hybridization of uranium 5f with Ga-4p electron.

2003-05-01

49

Nanocrystallization of the amorphous Fe_1_4Ni_4_0Zr_7B_1_2 alloys studied by the Moessbauer spectroscopy  

International Nuclear Information System (INIS)

Formation of the soft magnetic nanostructure in amorphous Fe_1_4Ni_4_0Zr_7B_1_2 alloy due to heat treatment is studied by the Moessbauer, differential scanning calorimetry, and X-ray diffraction techniques. Annealing at temperatures 520-580 "oC leads to the formation of extremely soft nanocrystalline alloy as revealed by the rf-Moessbauer measurements. The superparamagnetic behaviour was observed for the alloy annealed at 620-640 "oC. At higher annealing temperatures good soft magnetic properties deteriorate. (author)

2001-09-23

50

Ferroelectric and magnetic properties of Ho{sub 2}CuTiO{sub 6} double perovskite  

Energy Technology Data Exchange (ETDEWEB)

Ho{sub 2}CuTiO{sub 6} double pervoskite is synthesized by solid state reaction method and the phase formation was confirmed by X-ray diffraction. Ho{sub 2}CuTiO{sub 6} crystallizes in space group P63 cm and are isostructural in AMnO{sub 3} structure. We have investigated the effect of the presence of a magnetic ion (Ho{sup 3+}{approx}10.4{mu}{sub B}) in Ho{sub 2}CuTiO{sub 6}, on the magnetic properties, compared to that of an isostructural double perovskite containing Y-ion (non-magnetic), i.e., Y{sub 2}CuTiO{sub 6}. Magnetization measurements on Ho{sub 2}CuTiO{sub 6} showed paramagnetic moment of 0.026{mu}{sub B}/Ho at room temperature in an applied field of 7 T although no saturation is observed at room temperature, whereas, at 5 K, the paramagnetic moment was 0.3{mu}{sub B}/Ho in the same field. Since this compound is non-centrosymmetric, it is of interest to look into the ...

2006-08-15

51

Experimental Verification of the Hall Effect during Magnetic Reconnection in a Laboratory Plasma  

Energy Technology Data Exchange (ETDEWEB)

In this letter we report a clear and unambiguous observation of the out-of-plane quadrupole magnetic field suggested by numerical simulations in the reconnecting current sheet in the Magnetic Reconnection Experiment (MRX). Measurements show that the Hall effect is large in collisionless regime and becomes small as the collisionality increases, indicating that the Hall effect plays an important role in collisionless reconnection.

2005-06-16

52

The addition of trim coils to the Tandem Mirror Experiment magnet system to improve the magnetic field mapping  

International Nuclear Information System (INIS)

The mapping of the magnetic flux bundle from the center cell to the Plasma Potential Control plates (PPC) on the end fan of the Tandem Mirror Experiment Upgrade (TMX-U), was improved by the addition of trim coils (12,000 amp-turns) on each side of each end fan next to the pump beam magnetic shields. The coils' axes are oriented perpendicular to the machine centerline. These coils made the necessary corrections to the field-line mapping, while keeping the field in the nearby pump beam magnetic shield below the saturation threshold. This paper briefly describes the problem, discusses the design as it evolved, and presents the results of the field testing. A brief description of the improvement in the machine performance is also included.

53

Real time neutron diffraction experiments using Bragg edges  

Energy Technology Data Exchange (ETDEWEB)

Time resolved phase transition and strain experiments have been performed on the millisecond time scale using a Bragg-edge transmission technique that has been developed at the Los Alamos National Laboratory. The precision with which lattice parameters can be determined from edge positions is sufficient to perform high-resolution strain measurements in uniaxial stress.

1995-12-31

54

Real time neutron diffraction experiments using Bragg edges  

International Nuclear Information System (INIS)

Time resolved phase transition and strain experiments have been performed on the millisecond time scale using a Bragg-edge transmission technique that has been developed at the Los Alamos National Laboratory. The precision with which lattice parameters can be determined from edge positions is sufficient to perform high-resolution strain measurements in uniaxial stress.

1994-12-02

55

Identification of fatigue damage in cortical bone by diffraction enhanced imaging  

International Nuclear Information System (INIS)

In an effort to explore Diffraction Enhanced Imaging of bone tissue, experiments were performed to determine if it was possible to use Diffraction Enhanced Imaging to detect microdamage in bovine cortical bone. Measurements were made at the National Synchrotron Light Source where pre- and post-fatigue rocking curve widths of the bone were studied. The rocking curve widths were then compared. Since no consistent pattern of narrowing or broadening of the rocking curve emerged, it is likely that the ultra-small-angle X-ray scattering present in the bone overshadowed any additional changes to rocking curve caused by microdamage of the bone. Larger bone structures were able to be visualized which suggests that microdamage may be visualized with a higher resolution detector.

2005-08-11

56

Ammonium azide: a commented example of an Ab initio structure (Re-) determination from X-ray powder diffraction  

Energy Technology Data Exchange (ETDEWEB)

The structure of ammonium azide (NH{sub 4})N{sub 3} was (re-)determined ab initio from x-ray powder diffraction experiment using synchrotron radiation. We tried to detail and comment the different steps involved in the structure determination. The compound crystallize in the orthorhombic Pmna space group (no.53) with a = 8.937(1) A, b= 3.8070(5) A, c = 8.664(1) A, V = 294.79(7) A{sup 3}; Z= 4. It was possible to locate and refine the hydrogen coordinates, in two different approaches, and to establish the H-bonds. The final structural parameters are in good agreement with previous results based on three-dimensional neutron diffraction. (Author)

2002-07-01

57

Ammonium azide: a commented example of an Ab initio structure (Re-) determination from X-ray powder diffraction  

International Nuclear Information System (INIS)

The structure of ammonium azide (NH_4)N_3 was (re-)determined ab initio from x-ray powder diffraction experiment using synchrotron radiation. We tried to detail and comment the different steps involved in the structure determination. The compound crystallize in the orthorhombic Pmna space group (no.53) with a = 8.937(1) A, b= 3.8070(5) A, c = 8.664(1) A, V = 294.79(7) A"3; Z= 4. It was possible to locate and refine the hydrogen coordinates, in two different approaches, and to establish the H-bonds. The final structural parameters are in good agreement with previous results based on three-dimensional neutron diffraction. (Author)

58

NMR at earth's magnetic field using para-hydrogen induced polarization  

British Library Electronic Table of Contents (United Kingdom)

A method to achieve NMR of dilute samples in the earth's magnetic field by applying para-hydrogen induced polarization is presented. Maximum achievable polarization enhancements were calculated by numerically simulating the experiment and compared to the experimental results and to the thermal equilibrium in the earth's magnetic field. Simultaneous 19F and 1H NMR detection on a sub-milliliter sample of a fluorinated alkyne at millimolar concentration (1018 nuclear spins) was realized with just one single scan. A highly resolved spectrum with a signal/noise ratio higher than 50:1 was obtained without using an auxiliary magnet or any form of radio frequency shielding.

2011-01-01

59

Crystalline electric field of the rare-earth nickelates RniO{sub 3} (R = Pr, ND, Sm, Eu, and Pr{sub 1-x}La{sub x},0 {le} X {le} 0.7) determined by inelastic neutron scattering.  

Energy Technology Data Exchange (ETDEWEB)

The rare-earth based nickelates RNiO{sub 3} (R = Pr, Nd, Sm, Eu, and Pr{sub 1-x}La{sub x}, 0{<=}x{<=}0.7) were studied by inelastic neutron scattering. Energy splittings due to the crystalline-electric-field (CEF) interaction at the R{sup 3+} site within the electronic ground-state J multiplet (for R = Pr, Nd, and Pr{sub 1-x}La{sub x}) as well as within the two lowest-lying J multiplets (for R = Sm and Eu) were directly observed, and the corresponding CEF energy-level schemes were reconstructed. The latter were rationalized in terms of CEF parameters, which vary smoothly over the rare-earth series and give magnetic properties associated with the R sublattice in agreement with results from neutron powder diffraction experiments. Across the metal-insulator transition, a continuous change in the electronic part of the CEF parameters is observed. However, an attempt to quantify a charge transfer from the observed ...

1999-12-01

60

Crystalline electric field of the rare-earth nickelates RNiO{sub 3} (R=Pr, Nd, Sm, Eu, and Pr{sub 1-x}La{sub x}, 0{<=}x{<=}0.7) determined by inelastic neutron scattering  

Energy Technology Data Exchange (ETDEWEB)

The rare-earth based nickelates RNiO{sub 3} (R=Pr, Nd, Sm, Eu, and Pr{sub 1-x}La{sub x}, 0{<=}x{<=}0.7) were studied by inelastic neutron scattering. Energy splittings due to the crystalline-electric-field (CEF) interaction at the R{sup 3+} site within the electronic ground-state J multiplet (for R=Pr, Nd, and Pr{sub 1-x}La{sub x}) as well as within the two lowest-lying J multiplets (for R=Sm and Eu) were directly observed, and the corresponding CEF energy-level schemes were reconstructed. The latter were rationalized in terms of CEF parameters, which vary smoothly over the rare-earth series and give magnetic properties associated with the R sublattice in agreement with results from neutron powder diffraction experiments. Across the metal-insulator transition, a continuous change in the electronic part of the CEF parameters is observed. However, an attempt to quantify a charge transfer from the observed ...

1999-12-01

61

Crystalline electric field of the rare-earth nickelates RNiO_3 (R=Pr, Nd, Sm, Eu, and Pr_1_-_xLa_x, 0#<=#x#<=#0.7) determined by inelastic neutron scattering  

International Nuclear Information System (INIS)

The rare-earth based nickelates RNiO_3 (R=Pr, Nd, Sm, Eu, and Pr_1_-_xLa_x, 0#<=#x#<=#0.7) were studied by inelastic neutron scattering. Energy splittings due to the crystalline-electric-field (CEF) interaction at the R"3"+ site within the electronic ground-state J multiplet (for R=Pr, Nd, and Pr_1_-_xLa_x) as well as within the two lowest-lying J multiplets (for R=Sm and Eu) were directly observed, and the corresponding CEF energy-level schemes were reconstructed. The latter were rationalized in terms of CEF parameters, which vary smoothly over the rare-earth series and give magnetic properties associated with the R sublattice in agreement with results from neutron powder diffraction experiments. Across the metal-insulator transition, a continuous change in the electronic part of the CEF parameters is observed. However, an attempt to quantify a charge transfer from the observed variation of the CEF parameters in an ...

1999-12-01

62

Structure and magnetic properties of the Al1-xGaxFeO3 family of oxides: A combined experimental and theoretical study  

International Nuclear Information System (INIS)

Magnetic properties of the Al1-xGaxFeO3 family of oxides crystallizing in a non-centrosymmetric space group have been investigated in detail along with structural aspects by employing X-ray and neutron diffraction, Moessbauer spectroscopy and other techniques. The study has revealed the occurrence of several interesting features related to unit cell parameters, site disorder and ionic size. Using first-principles density functional theory based calculations, we have attempted to understand how magnetic ordering and related properties in these oxides depend sensitively on disorder at the cation site. The origin and tendency of cations to disorder and the associated properties are traced to the local structure and ionic sizes. -- Graphical abstract: We have studied both experimentally and theoretically the important role of disorder at the cation site on magnetic and related properties of the Al1-xGaxFeO3 ...

2011-03-01

63

AUTOMATED TECHNOLOGY KNOWLEDGE BASE  

Science.gov (United States)

MAGNETIC FORMING .............. MAGNETIC INDUCTION ............ MAGNETIC MATERIALS ............ MAGNETIC MEASUREMENT .......... MAGNETIC PERMEABILITY . ...

64

Synthesis of colloidal silver iron oxide nanoparticles--study of their optical and magnetic behavior.  

Science.gov (United States)

Silver iron oxide nanoparticles of fairly small size (average diameter approximately 1 nm) with narrow size distribution have been synthesized by the interaction of colloidal beta- Fe2O3 and silver nanoparticles. The surface morphology and size of these particles have been analyzed by using atomic force microscopy (AFM), field emission scanning electron microscopy (FESEM) and transmission electron microscopy (TEM). Their structural analysis has been carried out by employing x-ray diffraction (XRD), selected-area electron diffraction (SAED), optical and infrared (IR) spectroscopic techniques. The ageing of these particles exhibits the formation of self-assembly, possibly involving weak supramolecular interactions between Ag(I)O4 and Fe(III)O4 species. These particles display the onset of absorption in the near-infrared region and have higher absorption coefficient in the visible range compared to that of its precursors. ...

2009-07-01

65

Large orbital magnetic moment and its quenching in the itinerant uranium intermetallic compounds UTGa_5 (T=Ni, Pd, Pt)  

International Nuclear Information System (INIS)

The crystal structure, lattice strain due to the antiferromagnetic ordering, and magnetic form factor in the itinerant 5f compounds UTGa_5 (T=Ni, Pd, Pt) have been studied by neutron scattering. High-resolution powder diffraction revealed that the tetragonality of the U-Ga layers increases down to the series of the transition metal element T. The integrated intensities of the antiferromagnetic reflections can be well explained with the Neel-type structure for UNiGa_5, whereas UPtGa_5 has the antiferromagnetic stacking of the ferromagnetically ordered uranium moments in the c plane. In both compounds the uranium moments orient along the c axis with moments of 0.75(5) and 0.32(5) #mu#_B for UNiGa_5 and UPtGa_5, respectively. No magnetic peak could be observed in the powder diffraction pattern of UPdGa_5 due to the small magnetic moment less than the experimental sensitivity. The ...

2003-12-01

66

Design and experimental results on a terawatt magnetically controlled plasma opening switch  

Energy Technology Data Exchange (ETDEWEB)

The magnetically controlled plasma opening switch (MCPOS) is an advanced plasma opening switch that utilizes magnetic fields to improve operation. Magnetic fields always dominate terawatt, pulsed power plasma opening switches. For that reason, the MCPOS uses controlled applied magnetic fields with magnitude comparable to the self-magnetic field of the storage inductor. One applied field holds the plasma in place while energy accumulates in the storage inductor, then another applied field pushes the plasma away from the cathode to allow energy to flow downstream. Over a ten month period, an MCPOS was designed, built, and tested on DECADE Module 2 at Physics International. The peak drive current was 1.8 MA in 250 ns. The output parameters were up to 1 MA into an electron beam load. The radiation temporal pulse width averaged 60 nanoseconds full-width at half-maximum. The peak load ...

1998-05-01

67

Magnetic Moments and Electromagnetic Radii of Nucleon and ?(1232) in an Extended Goldstone-Boson-Exchange Model  

International Nuclear Information System (INIS)

We derive the exchange currents of pseudoscalar, vector, and scalar mesons from Feynman diagrams, and use them to calculate the magnetic form factors of nucleon and ?(1232). The magnetic moments and electromagnetic radii are obtained by using those form factors and the parameters determined from the masses of nucleon and ?(1232). We find the magnetic moments and electromagnetic radii of nucleon and ?(1232) can be produced very well in the extended Goldstone-Boson-exchange model in which all of pseudoscalar, vector, and scalar meson nonet are included. The magnetic moments of ?(1232) are closer to experiment values and results from lattice calculation than the results obtained by the model without other mesons except for pion and sigma.

2005-01-15

68

Structural, electronic and magnetic properties of splat-quenched FeCsub(x) alloys (x<0.05)  

International Nuclear Information System (INIS)

The results of a combined investigation of splat-quenched Fe-Csub(x) (x<0.05) alloys by resistivity, X-ray diffraction and Moessbauer spectroscopy are presented. The residual resistivity increases linearly with the carbon content (#DELTA#rho=5#mu##OMEGA#cm/at.%) with a slope identical to that observed in the dilute ferritic phase. X-ray diffraction reveals the presence of a martensite structure in addition to a small fraction of residual austenite; the dependence of the a and c lattice parameters on xsub(c) agrees with earlier measurements. A detailed investigation of the relative reflexion intensities shows that the as-quenched martensites consist of a mixing of massive martensite and tetragonal martensite for low carbon content and of tetragonal martensite only for xsub(c) approximately 0.05. The Moessbauer spectra reveal 3 or 4 magnetically non equivalent iron sites. From a detailed analysis of the intensity ...

2006-01-01

69

A facile method for the room-temperature synthesis of water-soluble magnetic Fe3O4 nanoparticles: Combination of in situ synthesis and decomposition of polymer hydrogel  

British Library Electronic Table of Contents (United Kingdom)

We propose and demonstrate a facile room-temperature synthetic method for obtaining water-soluble magnetic Fe3O4 nanoparticles (NPs) by combining the in situ synthesis and decomposition of a magnetic polymer hydrogel. The Fe3O4 NPs with average diameters of 6.3-8.3nm were synthesized in a cross-linked polyacrylamide (PAAm) hydrogel by coprecipitating iron ions. The decomposition of the magnetic polymer hydrogel by an aqueous solution of sodium hydroxide led to the transfer of Fe3O4 NPs into the aqueous medium. The NPs can be dispersed stably in water for more than three months. The Fe3O4 NPs were characterized by X-ray photoelectron spectra (XPS), X-ray powder diffraction (XRD), transmission electron microscope (TEM), and Fourier transform infrared spectroscopy (FT-IR). The saturation magn...

2011-01-01

70

Synthesis and characterization of Fe3O4Gg nanocomposites and their antibacterial performance  

British Library Electronic Table of Contents (United Kingdom)

We synthesized Fe3O4Gg nanocomposites through a combination of solvothermal, hydrothermal, and chemical redox reactions. Characterization of the resulting samples by X-ray diffraction, Fourier-transform infrared spectroscopy, field-emission scanning and transmission electron microscopy, and magnetic measurement is reported. Compared to Fe3O4g nanocomposites, the Fe3O4Gg nanocomposites showed enhanced antibacterial activity. The Fe3O4Gg nanocomposites were able to almost entirely prevent growth of Escherichia coli when the concentration of Ag nanoparticles was 10mg/mL. Antibacterial activity of the Fe3O4Gg nanocomposites was maintained for more than 40h at 37^oC. The intermediate carbon layer not only protects magnetic core, but also improves the dispersion and antibacterial activity of the...

2011-01-01

71

Documentation and evaluation of Moessbauer data for minerals  

Energy Technology Data Exchange (ETDEWEB)

More than 2,500 Moessbauer spectroscopic studies on minerals have been published since 1960. These papers contain approximately 8,000 sets of Moessbauer mineral data on at least 400 different minerals. This information has been compiled into a database that includes isomer shifts, quadrupole splittings, and magnetic hyperfine interactions at room, liquid nitrogen, and liquid helium temperatures. The database provides a profile of the Moessbauer research performed to date on minerals, including type and locality of minerals investigated, significance of the studies and results, and location of the research facilities. The data and information are available both in printed and magnetic form.With the establishment of this resource, the Moessbauer Effect Data Center has begun a systematic evaluation of the Moessbauer mineral data. It is anticipated that this resource can be used for the identification of minerals as powder X-ray ...

1998-12-15

72

Antiferromagnetic Kondo lattice: CePdSi_2  

International Nuclear Information System (INIS)

The compounds CePdSi_2, CeIrSi_2 and CeRhSn_2 have been synthesized and studied by X-ray diffraction, electrical resistivity and magnetic susceptibility. The magnetic susceptibility of CePdSi_2 exhibits two peaks at 6.8 K and 2.5 K, respectively, indicating two antiferromagnetic phase transitions, while that of CeIrSi_2 shows a broad maximum at 150 K, characteristic of valence fluctuating Ce-compounds. CeRhSn_2 remains paramagnetic down to 5 K. The resistivity of CeIrSi_2 exhibits a T"2 dependence at low temperatures, indicating a Fermi-liquid ground state, while those of CePdSi_2 and CeRhSn_2 shows the presence of Kondo and crystal field effects. (orig.).

1996-08-19

73

Structural and magnetic studies on the enhancement of the giant magnetoimpedance by ion irradiation  

British Library Electronic Table of Contents (United Kingdom)

The mechanism of abrupt increase of the giant magneto impedance (GMI) ratio in the ion irradiated Co-based amorphous ribbon has been investigated. The grazing incident X-ray diffraction and transmission electron microscope were used to characterize the samples before and after ion irradiation. The GMI-ratio considerably increased in the ion irradiated samples and the GMI response showed strong dependence on the driving frequencies. The Barkhausen noise (BN) signals are increased for the Ar ion irradiated sample with dose of 1x10^1^7 ion/cm^2. The results are interpreted in terms of GMI variation associated with domain wall dynamics.

2011-01-01

74

Finite element stress analysis of the CMS magnet coil  

CERN Document Server

The Compact Muon Solenoid (CMS) is one of the experiments which are being designed in the framework of the Large Hadron Collider (LHC) project at CERN. The design field of the CMS magnet is 4 T, the magnetic length is 12.38 m and the aperture is 6.36 m. This is achieved with a 4 layer-5 module superconducting Al-stabilized coil energised at a nominal current of 20 kA. The finite element analysis (FEA) carried out is axisymmetric elasto-plastic. FEA has also been carried out on the suspension system and on the conductor. (8 refs).

2000-01-01

75

Neurobehavioral effects of power-frequency electromagnetic fields.  

UK PubMed Central (United Kingdom)

Some laboratory experiments have suggested that power-frequency electric and magnetic fields (EMF) may be capable of influencing calcium efflux from cell membranes, pineal function, and circadian rhythms....Full Text Available

1993-12-01

76

X-point model for magnetic susceptibility of A-15 compounds  

Science.gov (United States)

The X-point linear chain model for electronic structure of A-15 compounds is shown to lead to a weakly temperature dependent magnetic susceptibility ?(T) = 3micro2?N(0) tanh (?~ / T) is serious disagreement with experiment. Supported in part by NSF-DMR76-20641; AROD-DAHCO4-75-G-0052; and FRAP-CUNY 11453.

1977-11-01

77

Measurement of the Self-Diffusion Coefficient of Water as a Function of Position in Wheat Grain Using Nuclear Magnetic Resonance Imaging  

UK PubMed Central (United Kingdom)

A pulsed field gradient spin echo sequence has been incorporated in a nuclear magnetic resonance (NMR) imaging experiment to provide an image contrast dependent on local molecular self-diffusion. The...Full Text Available

1988-01-01

78

Design study of copper toroidal field coils with bow shaping, demountable sliding joints, and active liquid-nitrogen cooling  

International Nuclear Information System (INIS)

The motivation for this design study has been to identify magnet designs for useful magnetic fusion experiments which minimize capital cost. Some possibly useful novel design features have been identified. 5 refs., 6 figs., 3 tabs.

1996-06-16

79

Noncollinear magnetism in surfaces and interfaces of transition metals  

Energy Technology Data Exchange (ETDEWEB)

Noncollinear (NC) magnetism is common in nature, especially when there exist geometrical frustration and chemical imparity in the system. In this work we studied the NC magnetism and the response to external magnetic fields in surfaces and interfaces of transition metals by using an semi-empirical tight-binding (TB) method that parameterized to the ab initio TB-LMTO calculations. We implemented this method to study two systems. The first one is the system of 6 Mn monolayers on Fe(001) substrate. Due to the complex structure and magnetic properties of Mn, we found 23 collinear magnetic configurations but only one NC configuration. The collinear ground state has a layered antiferromagnetic (AFM) coupling which agrees with previous experiments and calculations. In the NC configuration the local AFM coupling in the Mn layers is preserved, but the surface is 90 ...

2009-09-15

80

Polynomial curve fitting method for refraction-angle extraction in diffraction enhanced imaging  

International Nuclear Information System (INIS)

X-ray diffraction enhanced imaging (DEI) is applied to inspect internal structures of weakly absorbing low-Z sample. How to extract phase information from raw images measured in different positions of rocking curve is the key problem of DEI. In this paper, we present an effective extraction method called polynomial curve fitting method, in order to extract accurate information angular in a fast speed. It is com- pared with the existing methods such as multiple-images statistical method and Gaussian curve fitting method. The experiments results on a plastic cylinder and a black ant at the Beijing Synchrotron Radiation Facility prove that the polynomial curve fitting method can obtain most approximate refraction-angle values and its computation speed is 10 times faster than the Gaussian curve fitting method. (authors)

2009-11-01

81

Extraction methods of phase information for X-ray diffraction enhanced imaging  

Energy Technology Data Exchange (ETDEWEB)

X-ray diffraction enhanced imaging (DEI) is one of X-ray phase-contrast imaging methods, which is applied to inspect internal structures of weakly absorbing low-Z samples. The key problem of the DEI is how to extract phase information which is expressed by refraction-angle images from a series of DEI images measured in different positions of the rocking curve of the analyzer. Three effective extraction methods are presented in this paper: the statistical geometric-optics-approximation method, the maximum refraction-angle method and the Gaussian curve fitting method. They are compared with the existing methods, such as the D. Chapman's geometric optics approximation method and the multiple-images statistical method. A 2D computer simulation experiment is performed to draw comparisons of these methods. The experimental results prove that the above three methods have more precision of refraction-angle values than existing methods.

2007-08-21

82

Extraction methods of phase information for X-ray diffraction enhanced imaging  

International Nuclear Information System (INIS)

X-ray diffraction enhanced imaging (DEI) is one of X-ray phase-contrast imaging methods, which is applied to inspect internal structures of weakly absorbing low-Z samples. The key problem of the DEI is how to extract phase information which is expressed by refraction-angle images from a series of DEI images measured in different positions of the rocking curve of the analyzer. Three effective extraction methods are presented in this paper: the statistical geometric-optics-approximation method, the maximum refraction-angle method and the Gaussian curve fitting method. They are compared with the existing methods, such as the D. Chapman's geometric optics approximation method and the multiple-images statistical method. A 2D computer simulation experiment is performed to draw comparisons of these methods. The experimental results prove that the above three methods have more precision of refraction-angle values than existing methods.

2007-08-21

83

Direct observation of ordered orbital of YTiO{sub 3} by the X-ray magnetic diffraction technique  

Energy Technology Data Exchange (ETDEWEB)

X-ray magnetic diffraction (XMD) technique was applied to an orbital ordering compound of ferromagnetic YTiO{sub 3} for the first time. The orbital-magnetic form factor {mu} {sub L}(k) and the spin-magnetic form factor {mu} {sub S}(k) were independently measured by utilizing the LS separation ability of the XMD. The {mu} {sub L}(k) was measured for ten reciprocal-lattice points. No significant values of the {mu} {sub L}(k) were observed for most of the reciprocal-lattice points within the estimated statistical errors, which suggested quenching of the orbital moment. The {mu} {sub S}(k) was measured for 22 reciprocal-lattice points. Fourier synthesis of the {mu} {sub S}(k) gave the spin density distribution m {sub S}(r) in the real space. The obtained m {sub S}(r) map shows the characteristic feature of the electron distribution of 3d electron in the t{sub 2g} state of a Ti atom coordinated by O{sup 2-} ...

2005-08-15

84

Spectrograph for free-electron laser experiments  

International Nuclear Information System (INIS)

The design and construction of a Browne-Buechner type round pole face magnetic electron spectrograph is described. The design is based on the first order transfer properties of the bending magnet including the focal surface, dispersion, magnification and resolution. Second order aberrations are compared wit numerical ray tracing results using measured field data to simulate the magnet. The numerical results are also compared with floating wire measurements on the system. Agreement is within one part in 10"4. Data extraction from the instrument is done with an array of copper detectors placed along the focal surface. The spectrograph has been successfully employed in free-electron laser (FEL) experiments for over a year.

1983-03-21

85

A polarized neutron reflectometry study of the spin glass freezing in a 29 nm thick AuFe film  

Energy Technology Data Exchange (ETDEWEB)

We performed polarized neutron reflectometry (PNR) experiments on a 29 nm thick Au{sub 93}Fe{sub 7} film in a temperature range from 295 K down to 2 K in a vertical magnetic field up to 6 T. These high-field experiments were performed on the C5 spectrometer in Chalk River, Canada, using a split-pair cryomagnet. The magnetization as determined by PNR can be described with a Brillouin function from 295 K down to 50 K assuming the magnetic moment of isolated Fe atoms, i.e. 4{mu}{sub B} per Fe atom. Below 50 K the onset of the spin-glass freezing is observed as a strong deviation from this Brillouin type behavior of isolated atoms.

2007-07-15

86

Tracking failure of gamma-ray irradiated polybutylene polymers under magnetic field  

British Library Electronic Table of Contents (United Kingdom)

Polymer insulating materials used in radioactive environments are subjected to a risk of surface degradation caused by tracking. The tracking behavior becomes more complex with the presence of magnetic field. This paper presents investigation of tracking failure of gamma-ray irradiated polybutylene naphthalate (PBN) and polybutylene terephthalate (PBT) under magnetic field. The samples were irradiated in air up to 100 kGy and then up to 1000 kGy with dose rate of 10 kGy/h by using a 60Co gamma-source. Magnetic field Formula Not Shown with flux density of 250 mT was assembled perpendicularly to electric field Formula Not Shown , which gave rise to relative angle between Formula Not Shown and surface normal vector Formula Not Shown of 0degree, 90degree and 180degree, respectively. The experi...

2011-01-01

87

Magnetic properties of laminated perovskite-like ferroelectromagnetics  

International Nuclear Information System (INIS)

Magnetic properties of layer ferromagnets against the thickness are investigated. Two new compounds served for studies: Bisub(6)Tisub(2)Nbsub(0,5)Fesub(2,5)Osub(18) and Bi_7Ti_3Fe_3O_2_1. The Moessbauer effect and the magnetic susceptibility measurements were applied in the experiment. The Faraday method was used in magnetic measurements in fields from 1 to 9,5 kOe. The results of Moessbauer measurements show that temperature dependence of the spectra is typical for compounds with superparamagnetic properties. The magnetic fields Hsub(n) on Fe"5"7 nuclei in Bisub(6)Tisub(2)Nbsub(0,5)Fesub(2,5)Osub(18) and Bi_7Ti_3Fe_3O_2_1 are similar and equal to 520+-10 kOe. Therefore it may be concluded that relaxation times of nuclear spins in these compounds are equal or close to each other. The lines of quadrupole splitting appear in spectra together at 20 K. The results of ...

1975-01-01

88

Crystal electric field excitations in the cerium compound CeRh{sub 3}B{sub 2} studied by inelastic neutron scattering  

Energy Technology Data Exchange (ETDEWEB)

We have performed inelastic neutron scattering (INS) experiments on CeRh{sub 3}B{sub 2} at various temperatures to obtain direct information on the crystal electric field (CEF) in this compound, which exhibits some very peculiar magnetic properties for a Ce system: it is ferromagnetic with an unusually high Curie temperature (115 K), which contrasts with a strongly reduced and anisotropic magnetization (0.4 {mu}{sub B}/fu within the c-plane of the hexagonal structure). Measurements with high incident energies show only one well defined magnetic excitation around 150 meV, its exact position varying with the temperature. These results, combined with our previous data of magnetization and magnetic form factor, have permitted us to determine the CEF energy level scheme taking into account the two J multiplets of the Ce{sup 3+} ion. Information on the ground state ...

2007-12-19

89

Crystal electric field excitations in the cerium compound CeRh_3B_2 studied by inelastic neutron scattering  

International Nuclear Information System (INIS)

We have performed inelastic neutron scattering (INS) experiments on CeRh_3B_2 at various temperatures to obtain direct information on the crystal electric field (CEF) in this compound, which exhibits some very peculiar magnetic properties for a Ce system: it is ferromagnetic with an unusually high Curie temperature (115 K), which contrasts with a strongly reduced and anisotropic magnetization (0.4 #mu#_B/fu within the c-plane of the hexagonal structure). Measurements with high incident energies show only one well defined magnetic excitation around 150 meV, its exact position varying with the temperature. These results, combined with our previous data of magnetization and magnetic form factor, have permitted us to determine the CEF energy level scheme taking into account the two J multiplets of the Ce"3"+ ion. Information on the ground state (quasielastic ...

2007-12-19

90

Structure and magnetic properties of nanocrystalline Fe-Mo alloys prepared by mechanosynthesis  

International Nuclear Information System (INIS)

Nanocrystalline samples of Fe_8_0Mo_2_0 and Fe_5_0Mo_5_0 alloys were prepared by the mechanical milling method. The structure, lattice parameters, and crystallite size were determined by the X-ray diffraction. The magnetic properties of the milled products were determined by the Moessbauer spectroscopy. It was observed that in the case of the Fe_8_0Mo_2_0 alloy a solid solution of Mo in Fe was formed with the lattice parameters of the Fe increasing from 0.28659 nm to 0.29240 nm and the crystallite size decreasing from 250 nm to 20 nm. In the case of the Fe_5_0Mo_5_0 alloy there were no clear changes in values of the lattice parameters of Fe and Mo during the milling process, but the crystallite size decreased from 200 to 15 nm. Moessbauer spectra revealed different magnetic phases in the machanosynthesized Fe_Mo samples. In the case of the Fe_8_0Mo_2_0 alloy, the spectrum for the milled mixture indicated the formation of ...

2001-09-23

91

Structure and magnetic properties of RE_4CoCd and RE_4RhCd (RE = Tb, Dy, Ho)  

International Nuclear Information System (INIS)

New rare earth metal rich cadmium compounds RE_4CoCd and RE_4RhCd (RE = Tb, Dy, Ho) were prepared by high-frequency melting of the elements in sealed tantalum tubes. The samples were studied by x-ray powder and single-crystal diffraction. All the compounds crystallize with Gd_4RhIn-type structure, with space group F4-bar3m. The structures are built up from rigid three-dimensional networks of condensed, cobalt (rhodium) centred trigonal RE_6 prisms. The voids left by these networks are filled by Cd_4 cluster units and the coordination number 14 polyhedra of the RE1 atoms. The terbium and dysprosium compounds in both series undergo antiferromagnetic ordering, whereas the holmium compounds exhibit ferromagnetic ordering. The magnetic ordering in these compounds is characterized by broad peaks around the transition temperatures. The results of detailed crystallographic investigations and preliminary magnetic and specific heat ...

2007-02-21

92

Magnetic properties of the Mn{sub 1-x}Fe{sub x}In{sub 2}S{sub 4} spinel compounds  

Energy Technology Data Exchange (ETDEWEB)

Mn{sub 1-x}Fe{sub x}In{sub 2}S{sub 4} spinel compounds (x=0.3, 0.8) were grown by the chemical vapor transport method. The analysis of the X-ray diffraction data suggest that both the compounds crystallize in a cubic structure under the space group Fd3m. The magnetic study done between 300 and 2 K showed a paramagnetic behavior for the intermediate concentration sample x=0.3. A good fitting to the Curie-Weiss law allows us to calculate the paramagnetic Curie temperature. They are negative indicating predominant antiferromagnetic interactions. However, in sample with high Fe concentration, x=0.8, it was possible to observe a peak at around T{sub sg} congruent with 10 K. From ac magnetic susceptibility data at different driving frequencies f, it is found that the peak at T{sub sg} shifts to lower temperatures with decreasing frequency suggesting an spin-glass behavior.

2004-04-28

93

Evolution of magnetic structures in the UNi{sub 2}Si{sub 2}-UPd{sub 2}Si{sub 2} system  

Energy Technology Data Exchange (ETDEWEB)

The influence of Pd-Ni substitution on the formation of magnetic phases in the tetragonal U(Ni{sub 1-x}, Pd{sub x}){sub 2}Si{sub 2} system and the concentration magnetic phase diagram are presented. A series of different substitutions was prepared and detailed studies by powder neutron diffraction were performed for x=0.25, 0.5 and 0.75. All compounds order antiferromagnetically and form ferromagnetic basal planes stacked along the c axis (q=(0,0,q{sub z}) propagation). The ground-state phase (AF3) of UNi{sub 2}Si{sub 2} is an uncompensated AF structure (++- stacking (q{sub z}=2/3)). In UPd{sub 2}Si{sub 2} the ground-state phase corresponds to the simple AF structure AF2 (+-+-(q{sub z}=1)). In solid solutions, no traces of the AF3 phase were found for x=0.25 and the ground-state powder patterns correspond to AF2 for x{>=}0.25. (orig.)

2002-07-01

94

Evolution of magnetic structures in the UNi_2Si_2-UPd_2Si_2 system  

International Nuclear Information System (INIS)

The influence of Pd-Ni substitution on the formation of magnetic phases in the tetragonal U(Ni_1_-_x, Pd_x)_2Si_2 system and the concentration magnetic phase diagram are presented. A series of different substitutions was prepared and detailed studies by powder neutron diffraction were performed for x=0.25, 0.5 and 0.75. All compounds order antiferromagnetically and form ferromagnetic basal planes stacked along the c axis (q=(0,0,q_z) propagation). The ground-state phase (AF3) of UNi_2Si_2 is an uncompensated AF structure (++- stacking (q_z=2/3)). In UPd_2Si_2 the ground-state phase corresponds to the simple AF structure AF2 (+-+-(q_z=1)). In solid solutions, no traces of the AF3 phase were found for x=0.25 and the ground-state powder patterns correspond to AF2 for x#>=#0.25. (orig.)

95

Electronic structure and nesting-driven enhancement of the RKKY interaction at the magnetic ordering propagation vector in Gd_2PdSi_3 and Tb_2PdSi_3  

International Nuclear Information System (INIS)

We present first-time measurements of the Fermi surface and low-energy electronic structure of intermetallic compounds Gd_2PdSi_3 and Tb_2PdSi_3 by means of angle-resolved photoelectron spectroscopy (ARPES). We show that the Fermi surface in both compounds consists of an electron barrel at the #GAMMA# point surrounded by spindle-shaped electron pockets originating from the same band, with the band bottom of both features lying at 0.5 eV below the Fermi level. From the experimentally measured band structure, we estimate the momentum-dependent RKKY coupling strength and demonstrate that it is peaked at the 1/2#GAMMA# K wave vector. Comparison with neutron diffraction data from the same crystals shows perfect agreement of this vector with the propagation vector of the low-temperature in-plane magnetic order, thereby demonstrating the decisive role of the Fermi surface geometry in explaining the complex magnetically ordered ...

2009-03-22

96

STEM nanodiffraction technique for structural analysis of CoPt nanoparticles  

Energy Technology Data Exchange (ETDEWEB)

Studying the structure of nanoparticles as a function of their size requires a correlation between the image and the diffraction pattern of single nanoparticles. Nanobeam diffraction technique is generally used but requires long and tedious TEM investigations, particularly when nanoparticles are randomly oriented on an amorphous substrate. We bring a new development to this structural study by controlling the nanoprobe of the Bright and Dark Field STEM (BF/DF STEM) modes of the TEM. The particularity of our experiment is to make the STEM nanoprobe parallel (probe size 1 nm and convergence angle <1 mrad) using a fine tuning of the focal lengths of the microscope illumination lenses. The accurate control of the beam position offered by this technique allowed us to obtain diffraction patterns of many single nanoparticles selected in the digital STEM image. By means of this technique, we demonstrate ...

2008-06-15

97

STEM nanodiffraction technique for structural analysis of CoPt nanoparticles  

International Nuclear Information System (INIS)

Studying the structure of nanoparticles as a function of their size requires a correlation between the image and the diffraction pattern of single nanoparticles. Nanobeam diffraction technique is generally used but requires long and tedious TEM investigations, particularly when nanoparticles are randomly oriented on an amorphous substrate. We bring a new development to this structural study by controlling the nanoprobe of the Bright and Dark Field STEM (BF/DF STEM) modes of the TEM. The particularity of our experiment is to make the STEM nanoprobe parallel (probe size 1 nm and convergence angle <1 mrad) using a fine tuning of the focal lengths of the microscope illumination lenses. The accurate control of the beam position offered by this technique allowed us to obtain diffraction patterns of many single nanoparticles selected in the digital STEM image. By means of this technique, we demonstrate size ...

2008-06-01

98

A novel semidry flue gas desulfurization process with the magnetically fluidized bed reactor.  

Science.gov (United States)

The magnetically fluidized bed (MFB) was used as the reactor in a novel semidry flue gas desulfurization (FGD) process to achieve high desulfurization efficiency. Experiments in a laboratory-scale apparatus were conducted to reveal the effects of approach to adiabatic saturation temperature, Ca/S molar ratio and applied magnetic field intensity on SO(2) removal. Results showed that SO(2) removal efficiency can be obviously enhanced by decreasing approach to adiabatic saturation temperature, increasing Ca/S molar ratio, or increasing applied magnetic field intensity. At a magnetic field intensity of 300Oe and a Ca/S molar ratio of 1.0, the desulfurization efficiency (excluding desulfurization efficiency in the fabric filter) was over 80%, while spent sorbent appeared in the form of dry powder. With the SEM, XRD and EDX research, it can be found that the increase of DC ...

2009-03-18

99

Structure properties and magnetic susceptibility of diluted magnetic semiconductor Y_2_-_xHo_xO_3  

International Nuclear Information System (INIS)

The polycrystalline samples of Y_2_-_xHo_xO_3 (0.10#<=#x#<=#1.80) were synthesized by ceramic technology. The X-ray powder diffraction data were collected and the crystal structures were refined by the Rietveld method for the samples Y_2_-_xHo_xO_3 (x=0.00, 0.20, 0.40, 1.20, 1.80, 2.00). Holmium ions Ho"3"+ were randomly distributed over two cationic sites 8b and 24d in the space group Ia3 in all refined structures. Cation-anion-cation bonds important for superexchange interaction were determined. Magnetic susceptibility measurements were done by the Faraday method in the temperature range 290 to 620 K and a behaviour in accordance with the Curie-Weiss law was obtained. The molar Curie's constants linearly depend on concentration. The effective magnetic moments of Ho"3"+ ions were smaller than the free ion value. The Curie-Weiss paramagnetic temperatures indicated antiferromagnetic interaction. The gram ion ...

1995-01-01

100

Magnetic and thermal properties of cubic single-crystal PrCu_4Ag  

International Nuclear Information System (INIS)

We succeeded in synthesizing a new cubic intermetallic compound PrCu_4Ag in a fcc structure. Measurements of X-ray diffraction, magnetic susceptibility, magnetization, specific heat, electrical resistivity, thermal expansion, and elastic constants have been performed on single crystals of PrCu_4Ag. A maximum value of #chi#(T) with a corresponding peak in C(T) suggests that an antiferromagnetic phase transition occurs at T_N=2.4 K, where a sudden decrease in #rho#_4_f(T) and a sharp peak in the thermal expansion coefficient #alpha#(T) were observed. Characteristic Curie-type softening was observed in the temperature dependence of the transverse mode for (C_1_1 - C_1_2)/2 and C_4_4 from 70 K down to T_N, which implies that the crystalline electric field (CEF) ground state is the magnetic triplet #GAMMA#_5. The anisotropic properties in M(T,H) and C(T,H) are studied when the external ...

2010-11-01

101

The first insertion devices at SSRL - some personal recollections  

Energy Technology Data Exchange (ETDEWEB)

The author recounts his experiences with insertion devices at the Stanford Synchrotron Radiation Laboratory. His first experiences with wigglers occured at the Cambridge Electron Accelerator, and was carried over to SSRL with the proposal for a six pole electromagnetic wiggler. Most modern undulators, and many wigglers are now designed around permanent magnets, and the origin of this transition at SSRL was rather fortuitous and humorous. It reflects some of the personality characteristics of Klaus Halbach.

1995-02-01

102

Real time closed orbit correction system  

Energy Technology Data Exchange (ETDEWEB)

We describe a global closed orbit feedback experiment, based upon a real time harmonic analysis of both the orbit movement and the correction magnetic fields. The feedback forces the coefficients of a few harmonics near the betatron tune to vanish, and significantly improves the global orbit stability. We present the results of the experiment in the UV ring using 4 detectors and 4 trims, in which maximum observed displacement was reduced by a factor of between 3 and 4. 4 refs., 3 figs.

1989-01-01

103

Synthesis, structure and characterisation of the n=4 Aurivillius phase Bi5Ti3CrO15  

International Nuclear Information System (INIS)

The n=4 Aurivillius phase, Bi5Ti3CrO15, was synthesised by solid state reaction. Rietveld analysis of high resolution neutron diffraction data demonstrated this material to adopt the polar space group A21am at room temperature, transforming to the aristotype I4/mmm structure above 650 oC. This phase transition is coincident with an anomaly in DSC signal and relative permittivity, which are characteristic of a ferroelectric-paraelectric phase transition. Bi5Ti3CrO15 exhibits paramagnetic behaviour at low temperature, with short range antiferromagnetic interactions, but no evidence for long range magnetic ordering. This is considered a consequence of significant disorder of Ti and Cr over the available octahedral sites, as demonstrated by analysis of neutron diffraction data. -- Graphical abstract: We report here the synthesis, structure and characterisation of the n=4 Aurivillius phase Bi5Ti3CrO15. Analysis of neutron powder ...

2011-02-01

104

Free electron laser experiments using a long pulse induction linac  

International Nuclear Information System (INIS)

The NRL Long Pulse Induction Linac is being employed in a Free Electron Laser (FEL) experiment. The authors present results of beam transport and focusing experiments as well as measurements of the output radiation generated by various magnetic wigglers. The electron gun of the accelerator presently has a 17-cmdiam. cold cathode which is located in a nearly zero magnetic field (B /SUB z/ less than or equal to 5 G). The gun voltage is flat to within approx. = + or - 5% for 1.5 #mu#sec with this graphite brush cathode. The beam is focused by a series of solenoidal coils as it propagates through the 4-m-long accelerator."2 A solenoidal field which can be varied from 1-10 kG confines the beam in the FEL interaction region. Previous experiments were limited by poor beam transport, focusing, and matching into the relatively large solenoidal field in the FEL region. By smoothing the axial ...

105

Crystal growth, structural and optical characterization of a semi-organic single crystal for frequency conversion applications  

International Nuclear Information System (INIS)

Single crystals of semi-organic L-histidine hydrobromide have been grown by slow evaporation technique from a mixture of L-histidine and hydrobromic acid in aqueous solution at ambient temperature. From high-resolution X-ray diffraction analysis, the crystalline perfection of the grown crystal has been studied. Single crystal X-ray diffraction analyses, Nuclear Magnetic Resonance spectral analysis, Thermo-Gravimetry (TG), Differential Thermal Analysis (DTA) and hardness test have been employed to characterize the as-grown crystals. The UV cutoff wavelength of the grown crystal is below 300 nm and has a wide transparency window, which is suitable for second harmonic generation of laser in the blue region. Nonlinear optical characteristics have been studied using Q switched Nd:YAG laser (#lambda#=1064 nm). The second harmonic generation conversion efficiency of the grown crystals confirms their suitability for frequency ...

2010-12-15

106

Optical Diffraction Studies of Muscle Fibers  

UK PubMed Central (United Kingdom)

A new technique to monitor light diffraction patterns electrically is applied to frog semitendinosus muscle fibers at various levels of stretch. The intensity of the diffraction lines, sarcomere length...Full Text Available

1973-09-01

107

Coal demineralization with Ca(OH)2. Hydrothermal reaction between Ca(OH)2 and quartz; Ca(OH)2 wo mochiita sekitan no kagakuteki dakkai. Ca(OH)2 to sekitan no suinetsu hanno  

Energy Technology Data Exchange (ETDEWEB)

Coal demineralization mechanism and its optimum condition were studied by hydrothermal reaction between Ca(OH)2 and quartz as a coal demineralization model. In experiment, the mixture of powder quartz and Ca(OH)2 water slurry was subjected to reaction in an autoclave under spontaneous pressure at 175-340{degree}C. After dried in N2 gas atmosphere at 105{degree}C, the reaction product was analyzed by X-ray diffraction, thermo-balance and differential thermal analysis. In measurement of quartz conversion, the specimen was analyzed by X-ray diffraction after removal of bound water by heat treatment at 850{degree}C. The mixture of clean coal deashed by NaOH and a fixed amount of quartz was also used as specimen for experiment. As the experimental result, dicalcium silicate hydrate was mainly produced at 175{degree}C, and the product changed into xonotlite through tobermorite by longer treatment at higher ...

1996-10-28

108

Change in pore structure of coals by activation with KOH; KOH fukatsushita sekitan no saiko kozo  

Energy Technology Data Exchange (ETDEWEB)

Three typical Japanese coals of non-coking coal, coking coal and anthracite were heat-treated with KOH, and change in their pore structure was examined by absorption of N2, X-ray diffraction and TEM observation. In addition, the relation between a coal rank and pore structure was also studied by absorption experiment of N2. In experiment, the mixture of coal and KOH in a nickel holder was heat-treated in N2 gas flow at heating rate of 2{degree}C/min, and held at a fixed temperature for one hour. To clarify the pore structure, N2 absorption isotherms were measured at -196{degree}C under nearly 76cmHg using a commercially available full-automatic absorption measurement equipment. Based on the X-ray diffraction and TEM observation results on activated coals, the relation between the N2 absorption and pore structure was studied. The results are summarized as follows: (1) The yield and absorption ability of ...

1996-10-28

109

Electrical breakdown at low pressure in the presence of a weak magnetic field  

Energy Technology Data Exchange (ETDEWEB)

Electron trapping in crossed electric and magnetic fields is an important mechanism by which electrical discharges can develop in low pressure gases. The authors report observations of discharges produced by this mechanism around a spherical anode in two space simulation chambers, namely the Space Plasma Interaction Experiment (SPIE) at the University of Maryland, and the NASA-Lewis B-2 chamber. They have identified two types of discharges in these experiments. In the B-2 chamber, the breakdown takes the form of a runaway dischage with spherical topology, limited only by the ability of the power supply to provide the current. In the SPIE chamber this type of discharge also occurs, in addition to a low current toroidal discharge which is observed at higher magnetic fields. They present measurements of both types of discharge and show how the trapping effect of the magnetic field ...

1990-05-01

110

Temperature evolution of the internal magnetic hyperfine field of Metglas: amorphous and crystallized phases  

International Nuclear Information System (INIS)

We present differential scanning calorimetry (DSC), X-ray diffractometry, in situ Moessbauer spectroscopy (MS), and transmission electron microscopy (TEM) studies in Metglas ribbons subjected to different heat treatments. The temperature evolution of the hyperfine field H_h_f(T) and the Curie temperature (T_c) of the amorphous phase are determined. The magnetic field originally present in the amorphous phase has a 'normal' behavior, in the sense that it can be described by the Weiss molecular field theory. The total angular momentum of the iron atoms turns out to be 5/2 and this implies Fe"3"+ in which the electronic spins are uncoupled. When the samples are maintained near T_c (#approx#673 K), three new magnetic phases are detected in the Moessbauer spectra, indicating an onset of a crystallization process well below the first crystallization temperature (T_X_1), as determined by DSC (#approx#820 K). The magnetic behavior ...

2000-11-01

111

The study of thermal characteristics of high temperature oven for atomic spectroscopy  

International Nuclear Information System (INIS)

We present a high temperature heat oven with merits of conventional heat pipe oven and study ots thermal characteristics. The oven consists of stainless steel body and heating part of three layers of ceramic tubes. We obtained the maximum temperature of about 1350. deg. C at the center which was measured by thermocouple and infrared thermometer. And we compared the heating characteristics in the cases of external heating and no extent heating. It was applied to self diffraction experiment in the samarium gas which was one of the high melting point material.

1997-11-01

112

The ANL X6B beamline at NSLS: A versatile facility  

Energy Technology Data Exchange (ETDEWEB)

We have described the x-ray optics and beamline performance of the ANL X6B beam line at the NSLS. Considerable flexibility has been built into the beam line to accommodate a wide range of x-ray diffraction, scattering, and spectroscopy experiments with various requirements. We presented selected examples of experimental results and showed that with the high intensity, high energy resolution, high-q resolution, and energy tunability, the X6B beam line has become a versatile facility.

1994-07-01

113

Surface modification of 17-4PH stainless steel by DC plasma nitriding and titanium nitride film duplex treatment  

Energy Technology Data Exchange (ETDEWEB)

17-4PH stainless steel was modified by direct current (DC) plasma nitriding and titanium nitride film duplex treatment in this study. The microstructure, wear resistance and corrosion resistance were characterized by X-ray diffraction (XRD), pin-on-disk tribological test and polarization experiment. The results revealed that the DC plasma nitriding pretreatment was in favor of improving properties of titanium nitride film. The corrosion resistance and wear resistance of duplex treatment specimen was more superior to that of only coated titanium nitride film.

2007-04-15

114

Surface modification of 17-4PH stainless steel by DC plasma nitriding and titanium nitride film duplex treatment  

International Nuclear Information System (INIS)

17-4PH stainless steel was modified by direct current (DC) plasma nitriding and titanium nitride film duplex treatment in this study. The microstructure, wear resistance and corrosion resistance were characterized by X-ray diffraction (XRD), pin-on-disk tribological test and polarization experiment. The results revealed that the DC plasma nitriding pretreatment was in favor of improving properties of titanium nitride film. The corrosion resistance and wear resistance of duplex treatment specimen was more superior to that of only coated titanium nitride film.

2007-04-01

115

Structural Phase Transition in AuZn Alloys  

Energy Technology Data Exchange (ETDEWEB)

AuxZn1-x alloys undergo a shape memory martensitic transformation whose temperature and nature (continuous or discontinuous) is strongly composition dependent. Neutron diffraction experiments were performed on single crystals of x=50 and 52 to explore the structural changes occurring at the transition temperature. A transverse modulation with wavevector q0=(1/3,1/3,0) develops below the transition temperature, with no observable change in lattice parameter. However, the Bragg peak width shows a broadening suggesting an unresolved rhombohedral distortion similar to what has been observed in NiTi-Fe alloys.

2009-05-03

116

Plasma nitriding of low alloy steels at floating and cathodic potentials  

International Nuclear Information System (INIS)

The low alloy steels were nitrided in the plasma atmosphere generated by using hollow cathode discharge. For comparison, specimens of 40 Cr steel were in two different potential states. One kind is isolated from cathode and anode between them the discharge was created. The other kind is placed on the plate which is connected to the cathode. The nitriding was carried out at different temperatures. The surface morphology, phase of compound layers and microhardness profiles were analyzed. The optical microscopy observation and X-ray diffraction showed that the compound layers were formed in all experiments. The results of the nitriding treatment are weakly dependent on the potentials applied on the specimens.

2008-08-15

117

Forward Physics with the CMS experiment at the Large Hadron Collider  

CERN Document Server

multi-parton interactions and underlying event structure, $\\gamma$-mediated processes and luminosity determination, Monte Carlo tuning and even MSSM Higgs discovery in central exclusive production. In this article, the forward detector instrumentation around the CMS interaction point is described and the prospects for diffractive and forward physics using the CMS forward detectors are summarized. In addition, first observation of forward jets as well as early measurements of the forward energy flow in the pseudorapidity range $3.15

2010-01-01

118

High coercivity in Nd-Fe-Al-Co-B alloys prepared by mechanical milling  

Energy Technology Data Exchange (ETDEWEB)

Nd{sub 40}Fe{sub 30}Al{sub 10}Co{sub 15}B{sub 5} alloys were fabricated by high energy ball milling method under various conditions. Microstructure of the alloys was investigated by X-ray diffraction and electron microscopy techniques. Magnetic properties were characterized by hysteresis and thermomagnetic measurements. The high coercive fields up to 2.36 T have been observed on the samples consisting of Nd{sub 2}(Fe,Co,Al){sub 14}B, Nd{sub 6}(Fe,Co,Al){sub 14} and Nd crystallites imbedded in a residual amorphous matrix.

2008-02-15

119

Enhancement in transition temperature and upper critical field of CeO0.8F0.2FeAs by yttrium doping  

Science.gov (United States)

We report significant enhancement in superconducting properties of yttrium substituted Ce1-xYxOFFeAs superconductors. The polycrystalline samples were prepared by two step solid state reaction technique. X-ray diffraction confirmed tetragonal ZrCuSiAs structure with decrease in both a and c lattice parameters on increasing yttrium substitution (with fixed F content). With smaller ion Y in place of Ce, the transition temperature increased by 6 K. Yttrium doping also lead to higher critical fields as well as broader magnetization loops, particularly at elevated temperature.

2009-12-01

120

Ferrofluid flow for TOUGH2  

Energy Technology Data Exchange (ETDEWEB)

We have developed EOS7M, a ferrofluid flow and transport module for TOUGH2. EOS7M calculates the magnetic forces on ferrofluid caused by an external magnetic field and allows simulation of flow and advective transport of ferrofluid-water mixtures through porous media. Such flow problems are strongly coupled and well suited to the TOUGH2 framework. Preliminary applications of EOS7M to some simple pressure and flow problems for which experiments were carried out in the lab show good qualitative agreement with the laboratory results.

1998-03-24

121

COBE confounds the cosmologists  

Energy Technology Data Exchange (ETDEWEB)

The validity of the Big Bang theory is evaluated. The basis of the Big Band theory and the supercluster observations of Tully, which conflict with the Big Band theory, are discussed. Various explanations for the existence of supercluster observations are proposed. The cosmic background explorer (COBE) is being utilized to detect energetic processes. The COBE contains a far IR absolute spectrometer, a differential microwave radiometer, and a diffuse IR background experiment. The hypothesis of the evolution of the universe of Hannes Alfven, which emphasizes the importance of electricity and magnetism, is presented and research illustrating the importance of electric currents and magnetic fields in space is examined.

1990-03-01

122

A modular and extensible data acquisition and control system for testing superconducting magnets  

Energy Technology Data Exchange (ETDEWEB)

The Magnet Test Facility at Fermilab tests a variety of full-scale and model superconducting magnets for both R and D and production. As the design characteristics and test requirements of these magnets vary widely, the magnet test stand must accommodate a wide range of Data Acquisition (DAQ) and Control requirements. Such a system must provide several functions, which includes: quench detection, quench protection, power supply control, quench characterization, and slow DAQ of temperature, mechanical strain gauge, liquid helium level, etc. The system must also provide cryogenic valve control, process instrumentation monitoring, and process interlock logic associated with the test stand. A DAQ and Control system architecture that provides the functionality described above has been designed, fabricated, and put into operation. This system utilizes a modular approach that provides both extensibility and ...

2001-07-20

123

Transverse-field Formula Not Shown SR and magnetic disorder in Formula Not Shown  

British Library Electronic Table of Contents (United Kingdom)

We have carried out transverse-field ( Formula Not Shown ) Formula Not Shown SR experiments in Formula Not Shown for temperatures from 300 down to 2.2K. The muon-decay asymmetry can be fit to a stretched exponential relaxation function: Formula Not Shown . The exponent Formula Not Shown for Formula Not Shown , but drops continuously below this temperature (being Formula Not Shown for Formula Not Shown and reaching Formula Not Shown near 2K). The characteristic relaxation rate Formula Not Shown grows six-fold in the experimental temperature range (from Formula Not Shown for Formula Not Shown to Formula Not Shown for Formula Not Shown ). Independently of theoretical models, the behavior of these parameters is consistent with strong magnetic disorder. Although the magnetic susceptibility of F...

2008-01-01

125

High Magnetic Field NMR Studies of LiVGe$_2$O$_6$, a quasi 1-D Spin $S = 1$ System  

CERN Document Server

We report $^{7}$Li pulsed NMR measurements in polycrystalline and single crystal samples of the quasi one-dimensional S=1 antiferromagnet LiVGe$_2$O$_6$, whose AF transition temperature is $T_{\\text{N}}\\simeq 24.5$ K. The field ($B_0$) and temperature ($T$) ranges covered were 9-44.5 T and 1.7-300 K respectively. The measurements included NMR spectra, the spin-lattice relaxation rate ($T_1^{-1}$), and the spin-phase relaxation rate ($T_2^{-1}$), often as a function of the orientation of the field relative to the crystal axes. The spectra indicate an AF magnetic structure consistent with that obtained from neutron diffraction measurements, but with the moments aligned parallel to the c-axis. The spectra also provide the $T$-dependence of the AF order parameter and show that the transition is either second order or weakly first order. Both the spectra and the $T_1^{-1}$ data show that $B_0$ has at most a small effect on the alignment of the AF ...

2001-01-01

126

Crystal structure and magnetic properties of Sm{sub 3}ReO{sub 7}  

Energy Technology Data Exchange (ETDEWEB)

Crystals of a new ternary samarium rhenium oxide, Sm{sub 3}ReO{sub 7} were obtained by subsolidus reaction of samariumsesquioxide and rheniumdioxide (ratio 1.5:1) in sealed Pt-10Rh-tubes at 1673 K. The structure was determined by single-crystal X-ray diffraction. Sm{sub 3}ReO{sub 7} crystallizes in the orthorohombic system with unit cell dimensions a = 10.736(5), b = 7.392(3), and c = 7.519(3) in space group Cmcm (No. 63) with Z = 4. The structure consists of ReO{sub 6} octahedra, distorted SmO{sub 6} octahedra, and SmO{sub 8} prisms that are interconnected to each other to form a three-dimensional network. Rhenium has the formal oxidation state of +5 but no metal-metal bond is observed in this compound. The observed magnetization in the temperature range 4 K < T < 52 K is explained by a Curie-Weiss law modified by a temperature independent Van Vleck paramagnetism of samarium (3+).

1996-08-01

127

Antiferromagnetic Kondo lattice: CePdSi{sub 2}  

Energy Technology Data Exchange (ETDEWEB)

The compounds CePdSi{sub 2}, CeIrSi{sub 2} and CeRhSn{sub 2} have been synthesized and studied by X-ray diffraction, electrical resistivity and magnetic susceptibility. The magnetic susceptibility of CePdSi{sub 2} exhibits two peaks at 6.8 K and 2.5 K, respectively, indicating two antiferromagnetic phase transitions, while that of CeIrSi{sub 2} shows a broad maximum at 150 K, characteristic of valence fluctuating Ce-compounds. CeRhSn{sub 2} remains paramagnetic down to 5 K. The resistivity of CeIrSi{sub 2} exhibits a T{sup 2} dependence at low temperatures, indicating a Fermi-liquid ground state, while those of CePdSi{sub 2} and CeRhSn{sub 2} shows the presence of Kondo and crystal field effects. (orig.). 5 refs.

1997-02-01

128

Testing measurements at horizontal channels of the MARIA reactor performed using neutron spectrometers; Pomiary testowe przy kanalach poziomych reaktora MARIA wykonane przy uzyciu spektrometrow neutronow  

Energy Technology Data Exchange (ETDEWEB)

By means of neutron diffraction, using the standard polycrystalline sample of Al{sub 2}O{sub 3}, measurements on three (of four spectrometers) already installed in the front of horizontal channels of MARIA reactor have been performed. Basing on these experiments as well as on activation measurements carried out earlier, the fluxes of monoenergetic neutrons have been estimated. These experiments allowed to determine (for a given geometry and kind of monochromators chosen) the resolution efficiency of instruments and high order contamination in the reflected beam. With the help of polycrystalline vanadium and TbBr{sub 3} sample, the possibility of studies using the inelastic scattering process have been tested. (author) 7 refs, 15 figs, 7 tabs

1997-12-31

129

Pencil-like mm-size electron beams produced with linear inductive voltage adders  

International Nuclear Information System (INIS)

We present the design, analysis, and results of the high brightness electron beam experiments currently under investigation at Sandia National Laboratories. The anticipated beam parameters are the following: energy 12 MeV, current 35 endash 40 kA, rms radius 0.5 mm, and pulse duration 40 ns full width at half-maximum. The accelerator is SABRE, a pulsed linear inductive voltage adder modified to higher impedance, and the electron source is a magnetically immersed foilless electron diode. 20 endash 30 T solenoidal magnets are required to insulate the diode and contain the beam to its extremely small-sized (1 mm) envelope. These experiments are designed to push the technology to produce the highest possible electron current in a submillimeter radius beam. Design, numerical simulations, and experimental results are presented. copyright 1997 American Institute of Physics.

130

Ion temperature anisotropy in high power helium neutral beam fuelling experiments in JET  

Energy Technology Data Exchange (ETDEWEB)

During helium beam fuelling experiments in JET, distinctive anisotropic features have been observed in the velocity distribution function describing both fast and thermal alpha particle populations. During the initial fuelling phase the central helium ion temperature observed perpendicular to the magnetic field is higher than the central electron temperature, while the central helium ion temperature observed parallel to the magnetic field is lower than or equal to the central electron temperature. In order to verify temperature measurements of both perpendicular and parallel lines of sight, other independent methods of deducing the ion temperature are investigated: deuterium ion temperature, deuterium density, comparison with neutron rates and profiles (influence of a possible metastable population of helium). 6 refs., 7 figs.

1994-07-01

131

Ternary stannides RE_3Ru_4Sn_1_3 (RE = La, Ce, Pr, Nd). Structure, magnetic properties, and "1"1"9Sn Moessbauer spectroscopy  

International Nuclear Information System (INIS)

The ternary stannides RE_3Ru_4Sn_1_3 (RE = La, Ce, Pr, Nd) were obtained by arc-melting of the elements. The polycrystalline samples were characterized by powder X-ray diffraction. The structures of three compounds were refined from single-crystal diffractometer data: Yb_3Rh_4Sn_1_3 type, Pm anti 3n, a = 977.74(3) pm, wR2 = 0.0379, 280 F"2 values for La_3Ru_4Sn_1_3, a = 971.34(9) pm, wR2 = 0.0333, 274 F"2 values for Ce_3Ru_4Sn_1_3, a = 970.68(8) pm, wR2 = 0.0262, 272 F"2 values for Nd_3Ru_4Sn_1_3 with 13 variables per refinement. The structures consist of three-dimensional networks of condensed RuSn_6_/_2 trigonal prisms with the RE (CN 16) and Sn2 (CN 12) atoms in two different types of cavities of the networks. The two crystallographically independent tin sites have been resolved by "1"1"9Sn Moessbauer spectroscopy. Temperature-dependent magnetic susceptibility measurements of Ce_3Ru_4Sn_1_3 gave a reduced magnetic moment ...

2011-07-01

132

Magnetic and transport properties of Ba_2Co_9O_1_4 and Ba_1_._9A_0_._1Co_9O_1_4 (A=La or Na)  

International Nuclear Information System (INIS)

The valence and spin-state distributions of Co ions and the complex structure of antiferromagnetic Ba_2Co_9O_1_4 have led to the suggestion that doped Ba_2Co_9O_1_4 compounds may be good thermoelectric materials. We have checked this suggestion by measuring the magnetic properties as well as the transport properties of nominal Ba_1_._9A_0_._1Co_9O_1_4 (A=La or Na). We show that although all compounds are indicated to be single phase by powder X-ray diffraction analysis, they are all p-type polaronic conductors with low mobile-hole concentrations. Magnetic-susceptibility data of the parent and La-doped compounds give evidence of a second magnetic phase with ferromagnetic order setting in below 215 K; but this second phase is not seen in the Na-doped sample. We conclude that the structure is stabilized by oxidation and that cation exolution from the Ba_2Co_9O_1_4 structure creates cation vacancies that ...

2010-11-01

133

Initial results from 50mm short SSC dipoles at Fermilab  

Energy Technology Data Exchange (ETDEWEB)

Several short model SSC 50 mm bore dipoles are being built and tested at Fermilab. Mechanical design of these magnets has been determined from experience involved in the construction and testing of 40 mm dipoles. Construction experience includes coil winding, curing and measuring, coil end part design and fabrication, ground insulation, instrumentation, collaring and yoke assembly. Fabrication techniques are explained and construction problems are discussed. Similarities and differences from the 40 mm dipole tooling and management components are outlined. Test results from the first models are presented. 19 refs., 12 figs.

1991-03-01

135

Synchrotron resource of the Howard Hughes Medical Institute  

Energy Technology Data Exchange (ETDEWEB)

The Synchrotron Resource of the Howard Hughes Medical Institute will be dedicated to structural analyses of biological macromolecules, primarily through crystallography. This facility is under construction at the X4 port of the National Synchrotron Light Source at Brookhaven National Laboratory, and it will comprise three beamlines. The first line to be built has been devised to apply the multiwavelength anomalous diffraction method which provides direct estimates for the phases of reflections. The second line will be devoted to rapid and essentially routine diffraction measurements, mainly through the rotation method. These two experimental stations are contained within refrigerated radiation enclosures that will maintain clean environments, narrowly defined constant temperatures, and protection against biohazard at biosafety level BL-2. At the same time as the second line will be developed, the swath center is planned to first serve as a ...

1989-07-01

136

Magnified x-ray phase imaging using asymmetric Bragg reflection: Experiment and theory  

International Nuclear Information System (INIS)

X-ray imaging using asymmetric Bragg reflection in the hard x-ray regime opens the way to improve the spatial resolution limit below 1 #mu#m by magnifying the image before detection, simultaneously providing a strong phase contrast. A theoretical formalism of the imaging process is established. Based on this algorithm, numerical simulations are performed and demonstrate that both Fresnel propagation and Bragg diffraction contribute to contrast formation. The achievable resolution of this technique is investigated theoretically; the results obtained can be used to improve future experimental setups. Furthermore, the minimum detectable phase gradient is estimated, for comparison with other phase sensitive imaging techniques. Results from biological objects demonstrate that the technique is viable for imaging both in two and three dimensions. Refraction contrast images are extracted from experimental projection images by an algorithm similar to ...

2006-08-01

137

Recent activites on electromagnetic processing of materials in Japan  

Energy Technology Data Exchange (ETDEWEB)

Application of electromagnetic forces to materials processing, so-called {open_quotes}electromagnetic processing of materials (EPM){close_quotes} has been recognized as cutting edge technology, especially in the fields of steelmaking and advanced materials processing in Japan. The history of EPM in Japan is mentioned and the background to promote EPM is described. The current status of research and development of EPM is shown briefly introducing several examples. Regarding the application of high-frequency magnetic field, two topics are dealt with. The first is the improvement of the surface quality of cast steel where an alternating magnetic field is imposed on the molten steel from the outside of the mold, and the second is the induction cold crucible where a considerably large amount of molten intermetallic compound is levitated. Examples of the application of DC magnetic field are the control of molten steel flow in a ...

1995-01-01

138

Neutrino emission in neutron matter from magnetic moment interactions  

CERN Document Server

Neutrino emission drives neutron star cooling for the first several hundreds of years after its birth. Given the low energy ($\\sim$ keV) nature of this process, one expects very few nonstandard particle physics contributions which could affect this rate. Requiring that any new physics contributions involve light degrees of freedom, one of the likely candidates which can affect the cooling process would be a nonzero magnetic moment for the neutrino. To illustrate, we compute the emission rate for neutrino pair bremsstrahlung in neutron-neutron scattering through photon-neutrino magnetic moment coupling. We also present analogous differential rates for neutrino scattering off nucleons and electrons that determine neutrino opacities in supernovae. Employing current upper bounds from collider experiments on the tau magnetic moment, we find that the neutrino emission rate can exceed the rate through neutral ...

2004-01-01

139

Problems and solutions of the IFSMTF power and switch system  

Energy Technology Data Exchange (ETDEWEB)

Solutions have been found for the problems encountered with the coil power and switching systems of the International Fusion Superconducting Magnet Test Facility (IFSMTF). The coil power system provides the filtered dc sources (+- 12 V dc; 25,000 A) for charging and discharging the coils of the IFSMTF experiment. The switching system provides the means of transferring the coil current into a dump resistor when a rapid discharge of a coil is required due to a coil failure (quench) or other system abnormalities.

1985-01-01

140

P and e identification capabilities CAPRICE  

Energy Technology Data Exchange (ETDEWEB)

The cosmic antiparticle ring imaging Cherenkov experiment (CAPRICE) flew on a stratospheric balloon 8-9 August 1994 over northern Canada and collected data for more than 21 hours with less than 5 g/cm{sup 2} of residual atmosphere. The instrument includes a solid radiator RICH detector and an electromagnetic calorimeter for particle identification in the magnetic spectrometer. Preliminary antiproton and positron identification capabilities are presented.

1995-09-01

141

Kinetic energy accumulators. Application to electric cars  

Energy Technology Data Exchange (ETDEWEB)

The development of electric cars always met with the difficulty in storing energy and in recovering it in the form of electric power. Research work done for the last two decades in the field of materials and of new technologies oriented mainly towards aeronautical and space applications have led to designing, realizing and experimenting with flywheels rotating at high speed in magnetic bearings. The results obtained represent openings that, now, fall in with different industrial fields and in particular with application to electric cars.

1982-12-01

142

Electron phonon properties of A-15 compounds and Chevrel phases  

International Nuclear Information System (INIS)

A review of the information on the electron and phonon spectra in the A-15 compounds and Chevrel phase superconductors obtained from nuclear magnetic resonance, heat capacity, and Moessbauer effect experiments is presented. Relationships of the Fermi energy electrons and the soft phonons to the strength of the electron-phonon interaction are discussed.

143

Electron and phonon properties of A-15 compounds and Chevrel phases  

International Nuclear Information System (INIS)

A review of the information on the electron and phonon spectra in the A-15 compounds and Chevrel phase superconductors obtained from nuclear magnetic resonance, heat capacity, and Moessbauer effect experiments is presented. Relationships of the Fermi energy electrons and the soft phonons to the strength of the electron-phonon interaction are discussed.

144

Radiation-hardening of magnet coils  

International Nuclear Information System (INIS)

The first essential before embarking on the radiation-hardening of electrical insulation - mostly magnet coils - in any beam line application is to obtain a reliable estimate of the dose to the components. These are examples ( switchyards at SLAC and LAMPF) where the degree of hardness specified was much higher than was required. Although experience shows that the cost premium for substantial radiation - hardening is of the order of 10%, it has also become clear that well - designed beam line have negligible losses: hardening is required only in the vicinity of targets, collimators or other beam - intercepting devices. Where the beam is deliberately scraped, local shielding will minimize the associated radiation in the surroundings. Electron machines have their own special problems due to synchrotron radiation, so certainly coils and other electrical equipment should be kept away from the beam bend - plane. Because proton beams interact with ...

1989-03-01

145

Radiation imposed limits on superconducting magnets: A data base for copper stabilizers  

Energy Technology Data Exchange (ETDEWEB)

Two of eight differently prepared copper stabilizer samples, previously irradiated in the RTNS-II at LLNL, the IPNS-1 and the BSR at ORNL, have been irradiated to a fluence of 1.33 /times/ 10/sup 22/ n/m/sup 2/ at RTNS-II. During the course of the irradiation the samples were periodically removed (without warming) for measurements of the transverse magnetoresistance and returned for continued irradiation. This experiment extends the range of neutron-irradiation-induced resistivity by a factor of five over the previous experiments. A simple model is developed which reproduces the magnetoresistance results of all the experiments to an accuracy of 2.5%. 13 refs., 6 figs.

1987-10-28

146

Radionuclide adsorption characteristics around coastal water  

Energy Technology Data Exchange (ETDEWEB)

The adsorption capacity of radionuclides onto suspended sediment was experimented on each of the coastal seawater sampled around the Kori and the Wolsung nuclear power plant. During the experiment the quantity and size fraction of suspended sediment were adjusted and the seawater and sediment chemistry is approximated to the expected field condition. Because the sorption capacity depends on the specific minerals, ocean chemistry and radionuclide involved, it is necessary to analyze sediment mineralogy. Clay mineral is dominant in seabed mineral and suspended sediment as the result of x-ray diffraction. Radionuclide sorbed to silty-clay mineral can be rather transported to ocean than scavenged to seabed because of low quantity and fine grained suspended sediment in the coast around the Kori and the Wolsung. The result of adsorption examinations shows that {sup 139}Ce and {sup 51}Cr and {sup 110m}Ag are strongly sorbed to ...

1999-07-01

147

Radionuclide adsorption characteristics around coastal water  

International Nuclear Information System (INIS)

The adsorption capacity of radionuclides onto suspended sediment was experimented on each of the coastal seawater sampled around the Kori and the Wolsung nuclear power plant. During the experiment the quantity and size fraction of suspended sediment were adjusted and the seawater and sediment chemistry is approximated to the expected field condition. Because the sorption capacity depends on the specific minerals, ocean chemistry and radionuclide involved, it is necessary to analyze sediment mineralogy. Clay mineral is dominant in seabed mineral and suspended sediment as the result of x-ray diffraction. Radionuclide sorbed to silty-clay mineral can be rather transported to ocean than scavenged to seabed because of low quantity and fine grained suspended sediment in the coast around the Kori and the Wolsung. The result of adsorption examinations shows that "1"3"9Ce and "5"1Cr and "1"1"0"mAg are strongly sorbed to suspended ...

1999-11-04

148

Growth characteristics of ZrO_2 insulation coatings on Ag/AgMg sheathed Bi-2212 superconducting tapes  

International Nuclear Information System (INIS)

We have investigated the growth behaviors of high temperature compatible ZrO_2 insulation coatings on Ag and AgMg sheathed Bi_2Sr_2Ca_1Cu_2O_x superconducting tapes depending on number of dipping and thermal conditions. The coatings were fabricated on long-length superconducting tape substrates using a solution derived from Zr tetrabutoxide, solvent and chelating agent for high magnetic field magnets. The layer-on-layer growth behaviors were characterized by environmental scanning electron microscope (ESEM), energy dispersive spectroscopy (EDS), X-ray maps and X-ray diffraction (XRD). This research showed that the ZrO_2 coatings were regularly grown on Ag-based tape substrates and coating thickness increased with increasing number of dipping. It was found that ceramic oxides formed at temperature range 450 and 550 deg. C. The final coating thickness changed between 6 and 8 #mu#m after annealing process. Resistance of ...

2004-07-15

149

Solubility of AmOHCO{sub 3} in aqueous solution under atmospheric conditions  

Energy Technology Data Exchange (ETDEWEB)

Modeling calculations on the solubility of americium have indicated that basic americium carbonate, and not americium trihydroxide, is the solubility-controlling solid in the pH range from 6 to 10 under the influence of atmospheric CO{sub 2}. The solubility of crystalline {sup 243}AmOHCO{sup 3} has been investigated in batch experiments in near-neutral and basic solutions as a function of dissolution time in 0.1 M NaClO{sup 4} at room temperature under oxic conditions. After the solutions reached steady-state conditions, the influence of dissolved solids on the americium concentration in the supernatant solution was studied by utilizing several experimental methods to separate the solution phase from the solid. The solids were characterized by X-ray powder diffraction analysis.

1987-12-01

150

Preparation and photocatalytic property of pyrochlore Bi2Ti2O7 and (Bi, La) 2Ti2O7 films  

British Library Electronic Table of Contents (United Kingdom)

Dopant-free Bi2Ti2O7 thin films with pyrochlore structure and La-doped bismuth titanate thin films have been fabricated by means of chemical solution decomposition, and characterized by X-ray diffraction, atomic force microscopy, scanning electron microscopy and UV?Vis spectrophotometry in this study. Their photocatalytic activities have been evaluated by photodegrading methyl orange solution, and the optimum processing parameters for the highest photocatalytic activity have been found. Moreover, the effects of La-doping on the phase transformation and the photocalalytic activity have been studied. It has been deduced from the experiment result that substituted La3+ ions can act as a stabilizer of Aurivillus phase BLT and a grain?growth inhibitor in BLT thin films.

2008-01-01

151

Position sensitive detection of individual nuclear particle scintillations using image intensifier tubes  

International Nuclear Information System (INIS)

An imaging position sensitive detector for charged particles, neutrons, X-and gamma rays has been developed. The novel feature of this scintillation imaging radiation detector is its ability to detect individual nuclear particle scintillations with a h igh degree of spatial resolution. The key elements of this detector system are a high gain, low noise image intensifier tube, a CCD camera and commercially available image processing hardware and software. This detector system is highly effective for applications such as low fluence and real time neutron radiography, mapping of radioactive contamination in nuclear reactor fuel rods, X-ray diffraction imaging, high speed autoradiography and in general position sensitive detection of nuclear radiation. Results of some of the exploratory experiments carried out using this detector system are presented in this paper. (orig.).

1996-01-01

152

PLZT spatial light modulator for a 1-D hologram memory.  

Science.gov (United States)

A 100-bit slitlike aperture array spatial light modulator has been developed using 8.8/65/35 PLZT for a high-bit-density 1-D hologram memory. The most desirable characteristics, such as distortion-free diffraction-limited Fourier transform patterns and good uniformity of displayed bit patterns over 100 bits, have been realized. The lowest SNR was 86, and rise time and fall time have been 30 microsec and 8 microsec, respectively, at 190-V halfwave voltage. One-dimensional holographic storage experiments have been successfully performed using this PLZT spatial light modulator. PMID:20216813

1980-01-01

153

Inelastic excitation in the collisions of relativistic heavy ions  

International Nuclear Information System (INIS)

The penumbra of the profile function describing the nuclear collisions of relativistic heavy ions is related to the cross section for their producing a specific target-nucleus #gamma#-ray, sigmasub(#gamma#). The analysis assumes that the diffuse-edge diffraction model suffices to calculate the inelastic cross sections to the particle-stable states of the target nucleus. When the deformation lengths, deltasub(L) = #beta#sub(L)R, characterizing all important excitations are available from other experiments and the #gamma#-branching of these states is also known, the only unknown quantity determining sigmasub(#gamma#) is found to be the ratio of the diffuseness parameter of the profile function, d, to its radius, R. The most reliably determined values of d/R, for the target "4"0Ca, imply a rather wide penumbra, consistent with microscopic calculations. (orig.).

154

Generation and relaxation of microstrains in GaN nanocrystals under extreme pressures  

International Nuclear Information System (INIS)

Nanocrystalline powders of GaN with grain sizes ranging from 2 to 30 nm were examined under high external pressures by in situ diffraction techniques in a diamond anvil cell at DESY (HASYLAB, Station F3). The experiments on densification of pure powders under high pressure were performed without a pressure medium. The mechanism of generation and relaxation of internal strains and their distribution in nanoparticles was deduced from Bragg reflections recorded in situ under high pressures at room temperature. The microstrain was calculated from the full-width at half-maximum (FWHM) values of the Bragg lines. It was found that microstrains in GaN crystallites are generated and subsequently relaxed by two mechanisms: generation of stacking faults and change of the size and shape of the grains occurring under external stress. (author)

2001-09-23

155

Frequency upconversion properties of Ag: TeO2?ZnO nanocomposites codoped with Yb3+ and Tm3+ ions  

British Library Electronic Table of Contents (United Kingdom)

Yb3+?Tm3+ codoped tellurite glasses containing silver nanoparticles (NPs) were synthesized and characterized using transmission electron microscopy and optical techniques. The samples? composition and the nucleation of NPs were investigated using electron diffraction and energy dispersive spectroscopy. For the optical experiments, the samples were excited using a diode laser operating at 980?nm, in resonance with the Yb3+ transition 2F7/2?2F5/2. Photoluminescence (PL) bands corresponding to Tm3+ transitions were observed at 480, 650, and 800?nm due to the Yb3+? Tm3+ energy transfer. PL enhancement was achieved by heat-treatment of the samples at 325?C during different time intervals. The growth of the PL bands correlates with the increase of the silver NPs concentration. The relevant mecha...

2011-01-01

156

Feathery grain growth during solidification under forced flow conditions  

British Library Electronic Table of Contents (United Kingdom)

The grain morphology developed during solidification of an Al-4.5% Cu alloy is represented generally by columnar or equiaxed dendrites. Twinned feathery grains are found in the structure formed under certain heat and flow conditions during solidification. In this work, these conditions were achieved during solidification in a cavity under forced flow. Feathery grain formation is studied by means of fluid dynamics simulations with solidification included and by experiments. In order to determine the crystallographic orientation of feathery grains, electron backscattered diffraction measurements were performed. The growth features of feathery grains were analyzed by observations made normal and parallel to the growth direction. Some correlations between twinned feathery morphology, flow and ...

2007-01-01

157

Adhesion studies of Au films on GaAs using ion-assisted deposition techniques  

International Nuclear Information System (INIS)

This paper reports on a series of experiments performed to examine the ability of ion beam assisted thermal deposition to produce good adhesion of Au metallization on GaAs left-angle 100 right-angle substrates. A study of the influence of Ar ion-assisted thermal deposition of the Au films as well as in situ pre-sputtering of the GaAs surface with low-energy Ar ions prior to thermal deposition, shows that strong adhesion can be achieved without resorting to chemical cleaning. The substrate temperature and the relative flux of Ar ions to incident Au atoms were varied in order to correlate these parameters with film adhesion. The interfaces of films processed under these various conditions were examined by XTEM, RBS and XPS. Orientation texture was studied by x-ray diffraction (XRD).

158

The effect of neutrals on the performance of plasma opening switches  

Energy Technology Data Exchange (ETDEWEB)

The authors address the question of the limitations on voltage and current transfer to loads in magnetic storage systems utilizing microsecond conduction time plasma opening switches. They propose that the limitation of performance results from neutral atoms that are not entrained into the ionized material that is driven by the magnetic field of the rising generator current. Evidence in support of this proposition is gathered from experiments performed on the Ace-4 and Hawk generators. They set forth a theory to describe the effect of neutrals on the electrical performance of plasma opening switches. The neutral gas is assumed to be present in the region between the moving plasma mass and the generator, primarily in the region in which the plasma is injected initially. The essential elements of the theory are a weak photoionization source to seed the gas with a low concentration of electrons, and joule heating accompanied ...

1996-12-31

159

Precipitation of ions induced by nonadiabatic motion in the outer cusp region  

Science.gov (United States)

The transport of magnetospheric particles in the outer cusp region is examined by means of three-dimensional single particle codes. It is shown that, at high altitudes, particles can experience nonadiabatic motions leading to significant magnetic moment changes. It is demonstrated that this nonadiabatic behavior can be interpreted, at least partly, by the action of an impulsive centrifugal force perturbing the particle gyromotion. Systematic trajectory calculations reveal that plasma sheet ions which ExB convert toward the magnetopause from low L-shells in the dayside sector are subjected to such nonadiabatic motions. As a result of magnetic moment damping, a number of them are injected into the loss cone and subsequently precipitate near the cusp equatorward edge.

160

Andreev reflection spectroscopy in MgB{sub 2}  

Energy Technology Data Exchange (ETDEWEB)

Our Andreev reflection measurements (Phys. Rev. Lett. 87 (2001) 137005) along with other experiments have led to a general consensus that MgB{sub 2} is a multiband superconductor with two main superconducting gaps closing at the same T{sub c}. Here we show the behavior of the small gap as a function of the temperature and magnetic field. This gap is isotropic with T{sub c} of the bulk material but with a specific small (crossover) critical magnetic field of about 1 T much lower than the real H{sub c2}. The latter field is anisotropic and is rather governed by the large gap and strongly anisotropic Fermi surface of the material.

2003-04-01

161

Magnetic properties and low temperature X-ray studies of the weak ferromagnetic monoclinic and trigonal chromium tellurides Cr_5Te_8  

International Nuclear Information System (INIS)

Monoclinic and trigonal Cr_5Te_8 show a transition into the ferromagnetic state with a Curie temperature T_c, which sensitively depends on the actual composition. Monoclinic samples exhibit a lower T_c despite their higher Cr content. This observation is explained on the basis of less effective ferromagnetic superexchange in the monoclinic compounds and the larger number of Cr atoms being antiferromagnetically coupled. Magnetization experiments performed at 5 K demonstrate that the compounds saturate already at rather low magnetic fields. In addition, small values are estimated for the coercitive field H_c as well as for the remanence magnetization both being typical for weak ferromagnetic materials. The values for the saturation magnetization amount to about 72% and 65% for monoclinic and trigonal Cr_5Te_8, respectively. These low values can partially be explained on the basis of ...

2004-03-01

162

High-Performance, Superparamagnetic, Nanoparticle-Based Heavy Metal Sorbents for Removal of Contaminants from Natural Waters  

Energy Technology Data Exchange (ETDEWEB)

We describe the synthesis and characterization of superparamagnetic iron oxide nanoparticle based heavy metal sorbents with various surface chemistries that demonstrate an excellent affinity for the separation of heavy metals in contaminated water systems (i.e. spiked Columbia river water). The magnetic nanoparticle sorbents are prepared from an easy to synthesize iron oxide precursor, followed by a simple, one-step ligand exchange technique to introduce the organic surface functionality of interest chosen to target either specific or broader classes of heavy metals. Functionalized superparamagnetic nanoparticles are excellent sorbent materials for the extraction of heavy metal contaminants from environmental and clinical samples since they are easily removed from the media once bound to the contaminant by simply applying a magnetic field. These engineered magnetic nanoparticle sorbents have an inherently high active ...

2010-06-01

163

Design and operating experience of a 40 MW, highly-stabilized power supply  

Energy Technology Data Exchange (ETDEWEB)

Four 10 MW, highly-stabilized power supply modules have been installed at the National High Magnetic Field Laboratory in Tallahassee, FL, to energize water-cooled, resistive, high-field research magnets. The power supply modules achieve a long term current stability if 10 ppM over a 12 h period with a short term ripple and noise variation of <10 ppM over a time period of one cycle. The power supply modules can operate independently, feeding four separate magnets, or two, three or four modules can operate in parallel. Each power supply module consists of a 12.5 kV vacuum circuit breaker, two three-winding, step-down transformers, a 24-pulse rectifier with interphase reactors, and a passive and an active filter. Two different transformer tap settings allow rated dc supply output voltages of 400 and 500 V. The rated current of a supply module is 17 kA and each supply module has a one-hour overload capability of 20 kA. The ...

1995-07-01

164

Structure and properties of a novel cobaltate La0.30CoO2  

British Library Electronic Table of Contents (United Kingdom)

The layered cobaltate La0.30CoO2 was prepared from NaxCoO2 precursor by a solid-state ionic exchange and was characterized by means of X-ray and neutron diffraction, magnetic, thermal and electric transport measurements. The compound consists of hexagonal sheets of edge-sharing CoO6 octahedra interleaved by lanthanum monolayers. Compared to Na+ in the parent system, the La3+ ions occupy only one-third of available sites, forming a 2-dimensional superstructure. The deviation from the ideal stoichiometry La1/3CoO2 introduces extra hole carriers into the diamagnetic LS Co3+ matrix making the sample Pauli paramagnetic. The temperature dependence of the electrical conductivity in La0.30CoO2 follows Mott's T?1/3 law up to about 400K, which is in contrast w...

2011-01-01

165

Properties of superconducting Cu-rich composites containing V_3Si or V_3Ga  

International Nuclear Information System (INIS)

Superconducting Cu-rich composites containing the A-15 compounds V_3Si or V_3Ga were made by the ''Tsuei'' process (melting into ingots followed by cold working and heat treatment). Superconducting transition temperatures of the composites were measured. X-ray diffraction analyses were performed. Microstructures were studied using both the optical metallograph and the scanning electron microscope. For some composites containing V_3Ga, the critical current densities as functions of transverse magnetic field up to 60 kG, and as functions of temperature from 4.2 to 12"0K were measured. It was found that the Tsuei process does not work for the composites containing V_3Si, but works satisfactorily for V_3Ga; reasons are discussed. Relations between measured properties and various metallurgical factors such as alloy compositions, cross-section reduction ratios, and heat treatment are discussed. The mechanism for the observed superconductivity in the ...

166

Novel non-discoid chiral copper(II)-salen type [N2O2] donor Schiff base complexes with a cyclohexane diamine spacer: synthesis, electrochemistry, columnar mesomorphism and DFT study  

British Library Electronic Table of Contents (United Kingdom)

A series of new non-discoid chiral copper(ii)-salen type complexes, [Cu((4-CnH2n+1O)2salen)], n = 14, 16, 18 and salen = N,N'-cyclohexane bis (salicylideneiminato), containing 4-substituted alkoxy tails in the side aromatic rings and a cyclohexane spacer, have been prepared and their mesogenic properties investigated. The compounds were characterised by Fourier transform infra-red spectroscopy, 1H and 13C nuclear magnetic resonance spectroscopy, UV-vis spectroscopy and fast atom bombardment mass spectrometry. Mesomorphic properties of these compounds were studied by polarising optical microscopy, differential scanning calorimetry and X-ray diffraction (XRD). The ligands are non-mesogenic but the complexes exhibited enantiotropic rectangular columnar mesophases (Colr) with extended temperat...

2011-01-01

167

Enhanced corrosion resistance of Fe_4_0Ni_3_8Mo_4B_1_8 and Nd_1_5Fe_7_7B_8 by laser glazing  

International Nuclear Information System (INIS)

Laser glazing, using a KrF excimer laser (> = 248 nm, >a = 22 ns), has been used to improve the corrosion resistance properties of crystallized Fe_4_0Ni_3_8Mo_4B_1_8 (Metglas 2826 MB) and the permanent magnet material Nd_1_5Fe_7_7B_8. The formation of an amorphous layer was confirmed by conversion-electron Mossbauer Spectroscopy (CEMS), and the thickness of the amorphous layer was determined from the attenuation of the x-rays diffracted from the underlying crystalline material. The variation with laser fluence of the amorphous layer thickness on the Metglas were measured. The corrosion properties of the original, crystalline and laser glazed Metglas were measured potentiodynamically in acid electrolyte. Similar voltametric characteristics were obtained for the laser glazed surface and original Metglas, both showing a lower current in the passive region than the crystalline material. Laser glazing of the Nd_1_5Fe_7_7B_8 also produced a ...

1988-09-21

168

Complex permittivity and complex permeability of Sr ions substituted Ba ferrite at X-band  

International Nuclear Information System (INIS)

M-type hexagonal ferrite composition, Ba(1-x)SrxFe12O19 (x=0.0, 0.2, 0.4, 0.6, 0.8 and 1.0), was prepared by a two route ceramic method. Complex permittivity (?'-j?'') and complex permeability (?'-j?'') have been measured using a network analyzer from 8.2 to 12.4 GHz X-ray diffraction confirmed the M-type hexagonal structure and a scanned electron micrograph was used to analyze the grain size distribution of ferrite. Substitution of Sr2+ ions causes an increase in porosity that deteriorates the electromagnetic and microstructural properties in the doped samples. Both dielectric constant and dielectric loss are enhanced in comparison to the permeability and magnetic loss over the entire frequency region. This is due to a resistivity variation and the formation of Fe2+ ions, which increases the hopping mechanism between Fe2+ and Fe3+ ions.

2008-05-01

169

Chemistry of tervalent uranium. Preparation and properties of NH sub 4 UBr sub 4. 1. 5CH sub 3 CN. 6H sub 2 O  

Energy Technology Data Exchange (ETDEWEB)

The paper presents the preparation, X-ray powder diffraction data as well as some magnetic and spectroscopic properties of a new uranium(III) complex bromide of the formula NH{sub 4}UBr{sub 4}.1.5CH{sub 3}CN.6H{sub 2}O. The compound crystallizes in the monoclinic system with a=11.877 A, b=6.385 A, c=6.815 A, {beta}=101.29deg and Z=2. In the 60-240 K range it follows the Curie-Weiss law with {theta}=-37.24 K and {mu}{sub eff}=3.20 B.M. The IR and UV-VIS absorption spectra were recorded in the 80-4000 cm{sup -1} and 4000-26000 cm{sup -1} spectral ranges respectively. Thermal decomposition at a non-static high vacuum enabled the conversion of the compound into pure and anhydrous UBr{sub 3}. (orig.).

1990-07-01

170

Characterization and reactivity of Fe3O4/FeMnOx core/shell nanoparticles for methylene blue discoloration with H2O2  

British Library Electronic Table of Contents (United Kingdom)

A magnetic core/shell Fe3O4/FeMnOx catalyst was prepared by a simple oxidation-precipitation method. The catalyst was characterized by X-ray diffraction, transmission electron microscope, X-ray photoelectron spectroscopy, Fourier transform infrared spectroscopy, thermogravimetric analysis and cyclic voltammetry. The characterization studies verified that Fe3O4 core was coated with a layer of Fe-Mn oxide. The Fe3O4/FeMnOx was found to be an effective and stable heterogeneous catalyst for the discoloration of methylene blue (MB) in aqueous solution by H2O2. The high catalytic activity is due to the FeMnOx shell, which not only increased the surface hydroxyl groups, but also enhanced the interfacial electron transfer. The discoloration of MB could be due to the decomposition of H2O2 into ?OH ...

2011-01-01

171

Refining the Magnetic Forming Capability.  

Science.gov (United States)

... Title : Refining the Magnetic Forming Capability. ... Abstract : The purpose of this project was to refine the in-house magnetic forming capability. ...

1972-04-01

173

BIOMAGNETIC RESPONSE OF SIMPLE BIOLOGICAL ...  

Science.gov (United States)

... Examples include magnetic forming tools, magnetic shielding, magnetohydrodynamic propulsion systems, and various magnetic containment ...

1970-01-01

174

/22k : - NASA Technical Reports Server  

Science.gov (United States)

in pulse applications such as magnetic forming. ... In magnetic-forming electric circuitry, the ..... Aspects of Electrohydraulic land Magnetic Forming. ...

175

Electron Diffraction Examination of Gun Barrel Coatings.  

Science.gov (United States)

... Accession Number : ADA954164. Title : Electron Diffraction Examination of Gun Barrel Coatings. Descriptive Note : Special rept.,. ...

1942-10-20

176

Smith-Purcell free-electron laser  

International Nuclear Information System (INIS)

The term Smith-Purcell free electron laser can be employed generally to describe any coherent radiation source in which a diffraction grating is used to couple an electron beam with the electromagnetic field. To date, most practical developments of this concept have focused on devices which operate in the millimeter spectral regime. In this paper construction of a Smith-Purcell free-electron laser operating in the far-infrared (FIR) region using a novel resonator cavity design and the electron beam from a low energy (0.5-5 MeV) radio-frequency accelerator will be discussed. A tunable source in this region would have many applications and since the beam energy is low, the small size and low overall cost of such a device would make it a laboratory instrument. Current projects which are progressing towards developing a FIR source are the programs at Stanford and CREOL. Both of these projects are using permanent magnet undulators to couple the ...

1995-08-21

177

MAGNETIC RESONANCE IMAGING DEVICE  

J-STORE (Japan)

Full Text Available

2010-08-31

178

Neutron scattering studies of mixed-valence semiconductors  

Energy Technology Data Exchange (ETDEWEB)

Neutron scattering experiments on the mixed-valence (MV) compounds SmB{sub 6} are reported. The inelastic magnetic response of SmB{sub 6} at T = 2 K, measured on a double-isotope single crystal,displays a strongly damped peak at 35 meV corresponding to the inter multiplet transition of Sm{sup 2+}. At lower energies ( h.{omega} {approx_equal} 14 meV), a narrow magnetic excitation is observed, with remarkable scattering-vector and temperature dependences of its intensity. This novel feature is discussed in terms of recent theoretical works describing the formation of an anisotropic local bound state in semiconducting MV materials. If the average samarium valence is decreased by substituting La for Sm, a peak is found to appear at high energies. The elastic magnetic form factor of SmB{sub 6} was determined using polarised neutrons and no significant difference is observed in its Q-dependence with respect ...

1994-12-31

179

Characteristic Of Induction Magnetic Field On The Laboratory Scale Superconducting Fault Current Limiter Circuit  

International Nuclear Information System (INIS)

Model construction of the laboratory scale superconducting fault current limiter circuit (SFCL) has been performed. The SFCL is fault current limiter and used as electric network security. It mainly consists of a copper coil, a superconducting ring and an iron core that are concentrically arranged. The SFCL circuit is essentially a transformer where the secondary windings are being replaced by the ring of YBa_2Cu_3O_7_-_x superconductor (HTS). The ring has critical transition temperature Tc = 92 K and critical current Ic = 3.61 A. Characterization of the SFCL circuit is simulated by ANSYS version 5.4 software. The SFCL circuit consists of load and transformer impedances. The results show that the inductions of magnet field flux in the iron core of primer windings and ring disappear to one other before fault state. It means that impedance of the transformer is zero. After the condition a superconductivity behavior of the ring is disappear so that the impedance of ...

2004-06-01

180

Nanofocusing refractive X-ray lenses  

Energy Technology Data Exchange (ETDEWEB)

This thesis is concerned with the optimization and development of the production of nanofocusing refractive X-ray lenses. These optics made of either silicon or diamond are well-suited for high resolution X-ray microscopy. The goal of this work is the design of a reproducible manufacturing process which allows the production of silicon lenses with high precision, high quality and high piece number. Furthermore a process for the production of diamond lenses is to be developed and established. In this work, the theoretical basics of X-rays and their interaction with matter are described. Especially, aspects of synchrotron radiation are emphasized. Important in X-ray microscopy are the different optics. The details, advantages and disadvantages, in particular those of refractive lenses are given. To achieve small X-ray beams well beyond the 100 nm range a small focal length is required. This is achieved in refractive lenses by moving to a compact lens design where several single lenses ...

2010-02-05

181

Studies on the development of mossy zinc electrodeposits from flowing alkaline electrolytes  

Energy Technology Data Exchange (ETDEWEB)

The initiation and characteristics of mossy zinc electrodeposits have been investigated. Batteries with zinc electrodes are candidates for electric vehicle applications; however, this electrode is prone to form non-compact deposits that contribute to capacity loss and battery failure. Moss is deposited when the current density is far from the limiting current. This morphology first appears only after the bulk deposit is approximately 1 {mu}m thick. In this investigation, the effects of flow rate (Re=0--4000), current density (0--50 mA/cm{sup 2}), concentration of the electroactive species (0.25 and 0.5 M), and the concentration of supporting electrolyte (3, 6, and 12 M) on the initiation of moss were examined. The rotating concentric cylinder electrode was employed for most of the experiments; and a flow channel was used to study the development of morphology. After the experiment, the deposit was characterized using microscopic, x-ray ...

1991-07-01

182

Research by ESS Division for the Nevada Nuclear Waste Storage Investigations: Progress report, January-June 1985  

Energy Technology Data Exchange (ETDEWEB)

Petrographic research for the Nevada Nuclear Waste Storage Investigations focused on xenolithic variability in the Topopah Spring Member and on variations of clinoptilolite composition at Yucca Mountain. Zeolite and smectite occurrences were considered in terms of their relation to a disturbed zone beneath the potential repository, and mineral stability experiments have produced a new clinoptilolite structure as a result of prolonged heating at low temperature. Limitations were defined on the abundance of erionite and of sulfur. X-ray diffraction studies lead to improved analytical methods. Progress was made in the comparative study of mineralogy in sand ramps and in faults. Geological modeling considered the differences of the diffusion of nonsorbing tracers in vertically and in horizontally fractured rock. Modeling also treated the diffusion of a nonsorbing tracer in devitrified and in zeolitized rock. The results of these ...

1987-10-01

183

Manganese removal using an aerated granular filter  

Energy Technology Data Exchange (ETDEWEB)

Experiments on manganese removal using an aerated granular filter with mean particle size of 3.68 mm and 5.21 mm anthracite were conducted at a filtration rate of 100 m d{sup -1}. Air, with a rate of 0 to 366 m d{sup -1}, was supplied through nozzles positioned 100 mm above the filter column bottom. From the experiments that were conducted, it was found that manganese removal is completed at a pH of 9.6 or above. In addition, the oxidation and removal rate of dissolved manganese were expressed as a first-order reaction. The smaller the filter media particles were, the higher the manganese removal efficiency was. The aeration rate of dissolved oxygen in raw water is sufficient for the manganese removal process. The manganese removal rate increased with time due to the catalytic effect of manganese dioxide (MnO{sub 2}) attached to the media. The x-ray diffraction analysis showed that the solids attached to the filter media ...

2007-09-15

184

Formation of Si-nanoparticles in a microwave reactor: Comparison between experiments and modelling  

International Nuclear Information System (INIS)

The formation and growth of silicon-nanoparticles from silane in a microwave reactor was investigated. Experiments were performed for the following conditions: precursor concentration 380-2530 ppm, pressures of 20-30 mbar, microwave powers 120-300 W. The formed particles were examined in-situ with a particle mass spectrometer. Additionally, particles were collected on grids and analyzed by transmission electron microscopy, X-ray diffraction, and by determining the specific surface area by BET. The particle size was found to be in the range of 5-8 nm in diameter. A simple model was used to simulate the particle formation processes taking place inside the reactor. The microwave energy coupled into the reactor flow was treated as a spatially distributed energy source resulting in a local temperature increase. The particles were assumed to have a monodisperse size distribution. To allow an approximation of their shape they were characterized by ...

2005-02-01

185

The magnetic spectrometer PAMELA for the study of cosmic antimatter in space  

Energy Technology Data Exchange (ETDEWEB)

In the framework of the RIM (Russian Italian mission) program, PAMELA is the experiment devoted to the accurate measurement of the positron and antiproton spectra from the very low energy thresh-old of 100 MeV up to more than 50 GeV, and to hunt antinuclei with sensitivity better than 10{sup -7} in the helium/helium ratio. A permanent magnet equipped by microstrip silicon sensors, measures the particle momentum with MDR=400 GV/c on GF=25 cm{sup 2} sr. An accurate ToF system, a 19 X{sub o} deep imaging calorimeter, an aerogel Cherenkov counter and a TRD detector complement the spectrometer in order an efficient e{sup +-}/p{sup +-} separation and some light isotope identification capability. The PAMELA experiment will be carried out on a 700 km high polar orbit, on board of the Earth-observation meteor-3A satellite, to be launched at the end of 1988.

1995-09-01

186

Moderately heavy, heavy-fermion compound YbPd_2Si_2 at low temperatures  

International Nuclear Information System (INIS)

The available experimental data on the specific heat, magnetic susceptibility, magnetization, valence, NMR Knight shift and relaxation rate, and the quadrupolar moment of YbPd_2Si_2 are examined within the framework of the single-ion Anderson model. Such an analysis has previously given excellent agreement between theory and experiment for numerous other light heavy-fermion compounds, where crystalline fields do not play a dominant role. For YbPd_2Si_2, substantial crystalline-field splittings make difficult a quantitative comparison with existing exact solutions of the Anderson model. Inconsistencies with the interpretation that a nearly degenerate ground quadruplet determines the low-temperature thermodynamics are pointed out. It is concluded that at least three of the four Kramers doublets participate in the low-T properties. These three doublets should have a splitting of the order of the Kondo temperature, i.e., about ...

187

Moderately heavy, heavy-fermion compound YbPd sub 2 Si sub 2 at low temperatures  

Energy Technology Data Exchange (ETDEWEB)

The available experimental data on the specific heat, magnetic susceptibility, magnetization, valence, NMR Knight shift and relaxation rate, and the quadrupolar moment of YbPd{sub 2}Si{sub 2} are examined within the framework of the single-ion Anderson model. Such an analysis has previously given excellent agreement between theory and experiment for numerous other light heavy-fermion compounds, where crystalline fields do not play a dominant role. For YbPd{sub 2}Si{sub 2}, substantial crystalline-field splittings make difficult a quantitative comparison with existing exact solutions of the Anderson model. Inconsistencies with the interpretation that a nearly degenerate ground quadruplet determines the low-temperature thermodynamics are pointed out. It is concluded that at least three of the four Kramers doublets participate in the low-{ital T} properties. These three doublets should have a splitting of the order of the ...

1992-07-01

188

First plasma experiment on spherical tokamak device UTST  

International Nuclear Information System (INIS)

The UTST (University of Tokyo Spherical Tokamak) device was constructed for the purpose of exploring the formation of ultra-high beta ST (Spherical Tokamak) plasma using the double null plasma merging method. When two plasmas merge together to form a single plasma, magnetic field lines reconnect, and the magnetic field energy is converted to the plasma kinetic energy, increasing the plasma beta. The merging start-up has been demonstrated in the TS-3/4, START and MAST devices using coils inside the vacuum vessel and TS-3 plasma obtained 50% beta. In order to demonstrate the start-up in a more reactor relevant situation, UTST has all poloidal field coils outside the vacuum vessel. The first plasma experiment on the UTST was performed from December, 2007. In the result, the plasma obtained 10 kA by using only outer PF coils and single ST was generated at the lower area (z=-0.3 - -1.0[m]) close to a washer gun. This result ...

2009-04-01

189

New Forming Limits For Light Alloys By Means Of Electromagnetic Forming And Numerical Simulation Of The Process  

Science.gov (United States)

It is well known that one of the main advantages of the high speed forming (HSF) processes is the improvement in the forming limits of the used materials.Using the Electromagnetic Forming (EMF) technology two materials have been tested with different mechanical and physical properties: the AA5754 aluminium and the AZ31B magnesium alloys.The EMF process principle can be described as follows: A significant amount of electrical energy is stored in a bank of capacitors which are suddenly discharged releasing all the stored energy. This electric discharge runs through a coil which generates an intense transient magnetic field. At the same time transient Eddy currents are induced in the electrically conductive part placed some millimetres far from the coil. Another intense magnetic field is generated due to those Eddy currents but on the opposite direction as the one generated by the coil. A big magnetic repulsion force is ...

2007-04-07

190

New Forming Limits For Light Alloys By Means Of Electromagnetic Forming And Numerical Simulation Of The Process  

International Nuclear Information System (INIS)

It is well known that one of the main advantages of the high speed forming (HSF) processes is the improvement in the forming limits of the used materials.Using the Electromagnetic Forming (EMF) technology two materials have been tested with different mechanical and physical properties: the AA5754 aluminium and the AZ31B magnesium alloys.The EMF process principle can be described as follows: A significant amount of electrical energy is stored in a bank of capacitors which are suddenly discharged releasing all the stored energy. This electric discharge runs through a coil which generates an intense transient magnetic field. At the same time transient Eddy currents are induced in the electrically conductive part placed some millimetres far from the coil. Another intense magnetic field is generated due to those Eddy currents but on the opposite direction as the one generated by the coil. A big magnetic repulsion force is ...

2007-04-07

191

In-beam #gamma#-ray spectroscopy of fast beams at the NSCL  

International Nuclear Information System (INIS)

With the development of an array of highly-segmented germanium detectors, it now becomes possible to perform in-flight #gamma#-ray spectroscopy experiments on intermediate energy beams with unprecedented #gamma#-ray energy resolution. Presented in this report are examples of two techniques in which SeGA, the most highly-segmented operational germanium array for in-flight spectroscopy with fast beams, was used for the detection of #gamma# rays. SeGA used in conjunction with a high-resolution magnetic spectrograph (S800) to detect the reaction residues in coincidence represents a powerful combination for in-beam #gamma#-ray studies.

2004-04-05

192

Improved SSAMS performance  

British Library Electronic Table of Contents (United Kingdom)

We operate a new NEC 250kV single-stage accelerator mass spectrometer (SSAMS) next to our established 5MV tandem. This permits good comparison of 14C-AMS and challenges SSAMS performance. Initial SSAMS ion-optical deficiencies have been addressed by shimming the injection magnet and 3permil 14C/13C measurement with background limited by sample chemistry is routine. Higher-precision analysis is also achievable. A problematic measurement interference remains, however. The small spectrometer was procured to add measurement capacity, and for experiments with positive ions, but is now the preferred instrument for both convenience and measurement quality.

2010-01-01

193

Expansion Rate Measurements at Moderate Pressure of Nonneutral Electron Plasmas in the Electron Diffusion Gauge (EDG) Experiment  

Energy Technology Data Exchange (ETDEWEB)

Measurements of the expansion rate of pure-electron plasmas have been performed on the Electron Diffusion Gauge (EDG) device at background helium gas pressures in the 5 x 10(superscript -8) Torr to 1 x 10(superscript -5) Torr range, where plasma expansion due to electron-neutral collisions dominates over plasma expansion due to trap asymmetries. It is found that the expansion rate, defined as the time rate of change of the particles' mean-square radius, scales approximately linearly with pressure and inversely as the square of the magnetic field strength in this regime, in agreement with classical predictions.

2001-05-18

194

Enriched lithium collection from lithium plasma flow  

International Nuclear Information System (INIS)

In order to understand the physical processes concerned with the selective heating by ion cyclotron resonance and with the subsequent collection of heated particles, experiments were carried out with the extraction of lithium samples, enriched with "6Li isotopes. Probe and integral extractors allow to collect enriched Li at the end of the selective heating region. Surface density distribution on the collector and local isotopic content of lithium are measured, as a function of the screen height and the retarding potential. Dependence of the collected amount of lithium and of its isotopic content on the value of the magnetic field is also measured. 4 figs., 2 tabs., 5 refs.

195

Determination of the #pi#1g/sub 9/2/ orbit size in "8"8Sr, "9"0Zr, and "9"2Mo from inelastic electron scattering  

International Nuclear Information System (INIS)

A study of the #pi#1g/sub 9/2/ orbit size in "8"8Sr, "9"0Zr, and "9"2Mo is presented. The rms radius for the point-proton density is extracted by studying transitions to 8"+ states in these nuclei. The radii are consistently larger than a value determined in a magnetic electron scattering experiment on "9"3Nb. A qualitative discussion of the ground state occupation of the #pi#1g/sub 9/2/ orbit based on the transition amplitudes to the 8"+ states is given.

196

Automatic beam position control at Los Alamos Spallation Radiation Effects Facility (LASREF)  

Energy Technology Data Exchange (ETDEWEB)

Historically the Los Alamos Spallation Radiation Effects Facility (LASREF) has used manual methods to control the position of the 800 kW, 800 MeV proton beam on targets. New experiments, however, require more stringent position control more frequently than can be done manually for long periods of time. Data from an existing harp is used to automatically adjust steering magnets to maintain beam position to required tolerances.

1997-08-01

197

The PAMELA space experiment: first year of operation  

Energy Technology Data Exchange (ETDEWEB)

On the 15th of June 2006 the PAMELA experiment, mounted on the Resurs DK1 satellite, was launched from the Baikonur cosmodrome and it has been collecting data since July 2006. PAMELA is a satellite-borne apparatus designed to study charged particles in the cosmic radiation, to investigate the nature of dark matter, measuring the cosmic-ray antiproton and positron spectra over the largest energy range ever achieved, and to search for antinuclei with unprecedented sensitivity. The apparatus comprises a time-of-flight system, a silicon-microstrip magnetic spectrometer, a silicon-tungsten electromagnetic calorimeter, an anticoincidence system, a shower tail catcher scintillator and a neutron detector. The combination of these devices allows charged particle identification over a wide energy range.

2008-05-15

198

Strong fields and recycled accelerator parts as a laboratory for fundamental physics  

International Nuclear Information System (INIS)

Over the last few years it has become increasingly clear that low energy, but high precision experiments provide a powerful and complementary window to physics beyond the Standard Model. In this note we illuminate this by using minicharged particles as an example. We argue that minicharged particles arise naturally in extensions of the Standard Model. Compatibility with charge quantization arguments suggests that minicharged particles typically arise together with a massless hidden sector U(1) gauge field. We present several low energy experiments employing strong lasers, electric and magnetic fields that can be used to search for (light) minicharged particles and their accompanying U(1) gauge boson.

2009-12-01

199

Retroperitoneoscopic partial adrenalectomy for small adrenal tumours (<=1 cm): the Ruijin clinical experience in 88 patients  

British Library Electronic Table of Contents (United Kingdom)

Study Type - Therapy (case series)Level of Evidence 4 OBJECTIVE To present our experience of retroperitoneoscopic partial adrenalectomy (RPA) for small adrenal tumours, as with modern imaging methods small adrenal lesions are being diagnosed more commonly, and retroperitoneoscopic adrenal surgery for small adrenal tumours (PATIENTS AND METHODS We retrospectively reviewed the records of 389 consecutive retroperitoneoscopic adrenalectomies from September 2005 to December 2008, 88 of which were small adrenal tumours and treated by RPA. Ultrasonography and computed tomography (CT) were used in all patients before RPA, and magnetic resonance imaging or positron emission tomography/CT in some patients. We used RPA for adrenal tumours and total adrenalectomy for adrenal cancer. During the surgery...

2010-01-01

200

Multi-GeV electron spectrometer  

Energy Technology Data Exchange (ETDEWEB)

The advance in laser-plasma acceleration techniques pushes the regime of the resulting accelerated particles to higher energies and intensities. In particular the upcoming experiments with the FLAME laser at LNF will enter the GeV regime with almost 1nC of electrons. From the current status of understanding of the acceleration mechanism, relatively large angular and energy spreads are expected. There is therefore the need to develop a device capable to measure the energy of electrons over three orders of magnitude (few MeV to few GeV) under still unknown angular divergences. Within the PlasmonX experiment at LNF a spectrometer is being constructed to perform these measurements. It is made of an electro-magnet and a screen made of scintillating fibers for the measurement of the trajectories of the particles. The large range of operation, the huge number of particles and the need to focus the divergence present unprecedented ...

2010-11-11

203

Synthesis and crystal structure of a new open-framework iron phosphate (NH4)4Fe3(OH)2F2[H3(PO4)4]: Novel linear trimer of corner-sharing Fe(III) octahedra  

International Nuclear Information System (INIS)

A new iron phosphate (NH4)4Fe3(OH)2F2[H3(PO4)4] has been synthesized hydrothermally at HF concentrations from 0.5 to 1.2 mL. Single-crystal X-ray diffraction analysis reveals its three-dimensional open-framework structure (monoclinic, space group P21/n (No. 14), a=6.2614(13) A, b=9.844(2) A, c=14.271(3) A, ?=92.11(1)o, V=879.0(3) A3). This structure is built from isolated linear trimers of corner-sharing Fe(III) octahedra, which are linked by (PO4) groups to form ten-membered-ring channels along [1 0 0]. This isolated, linear trimer of corner-sharing Fe(III) octahedra, [(FeO4)3(OH)2F2], is new and adds to the diverse linkages of Fe polyhedra as secondary building units in iron phosphates. The trivalent iron at octahedral sites for the title compound has been confirmed by synchrotron Fe K-edge XANES spectra and magnetic measurements. Magnetic measurements also show that this compound exhibit a strong antiferromagnetic ...

2010-12-01

204

Study of nanocrystallization in FINEMET alloy by active screen plasma nitriding  

International Nuclear Information System (INIS)

The nanocrystallization process of amorphous Fe_7_3_._5Si_1_3_._5B_9Nb_3Cu_1 was investigated by active screen plasma nitriding (ASPN) treatment at temperatures ranging from 410 "oC to 560 "oC for 3 h in two gas mixtures of 75% N_2-25% H_2 and 25% N_2-75% H_2 at 5 mbar atmosphere. The amorphous ribbons were then annealed under vacuum at the same time and temperatures mentioned above. The structure of the samples was analyzed using various techniques such as X-ray diffraction (XRD), atomic force microscopy (AFM) and differential scanning calorimetry (DSC). Microhardness measurements, electrical resistivity and Vibrating Sample Magnetometer (VSM) were used to study mechanical, electrical and magnetic properties of the samples, respectively. It was observed that the ASPN treatment leads to finer grain size and higher crystalline volume fraction and modifies the structural features of Fe(Si) phase. The Fe(Si) lattice parameter for the nitrided ...

2010-02-18

205

Intrinsic magnetism in Fe doped SnO2 nanoparticles  

International Nuclear Information System (INIS)

Iron doped semiconducting nanoparticles Sn1-xFexO2 with x=0, 0.001, 0.002, 0.003, 0.004, 0.01 and 0.03 were prepared by a sol-gel method. The X-ray diffraction, Transmission Electron Microscopy measurements confirm the rutile structure with no impurity phase. The three characteristic lines of electron spin resonance (ESR) are observed in the doped samples for all compositions, which is a clear evidence for rhombic Fe3+ in rutile phase. The line width of ESR increases with increase in Fe concentration due to induced disorder. The spin-pumping effect is observed at temperatures below 250 K for the samples with x=0.01 and 0.03. However, based on the Curie-Weiss susceptibility, iron is in paramagnetic state and is subject to weak antiferromagnetic interaction. Blue shift in the optical band gap is observed with increase in the Fe content. -- Graphical abstract: The ESR spectra reveal that the nature of Fe in Sn1-xFexO2 samples is isolated rhombic Fe3+-ion in rutile ...

2011-01-01

206

Crystal structure and magnetic properties of Sm{sub 2}ReO{sub 5}  

Energy Technology Data Exchange (ETDEWEB)

Crystals of disamarium rhenium (IV) pentoxide, Sm{sub 2}ReO{sub 5}, were obtained by subsolidus reaction of samariumsesquioxide and rheniumdioxide (ratio 1:1) in sealed Pt 10Rh tubes at 1673 K. The structure was determined by single-crystal X-ray diffraction. Sm{sub 2}ReO{sub 5} crystallizes in the tetragonal system with unit cell dimensions a = 8.646(3) {angstrom} and c = 5.747(2) {angstrom} and space group P4/n (no. 85) with Z = 4. The structure consists of isolated RE{sub 2}O{sub 8} groups and the (Sm{sub 4}O) chains are inter-connected by common oxygen atoms to form a three-dimensional network. Each Re{sub 2}O{sub 8} group is composed of a pair of rhenium each surrounded by four oxygens with a short Re-Re distance of 2.251(1) {angstrom} indicating a metal-metal bond. Rhenium has the formal oxidation state of +4. The observed magnetizations in the temperature range 1.8 < T < 100 K exhibits antiferromagnetic ordering below 2.4(1) K and ...

1997-08-01

207

Specification of the steel sheet for the 300 GeV magnet system  

CERN Document Server

Specification of the steel sheet for the 300 GeV magnet system

1971-01-01

208

Radial Halbach Magnetic Bearings  

Science.gov (United States)

Radial Halbach magnetic bearings have been investigated as part of an effort to develop increasingly

2009-01-01

209

Magnetic forming of resistive materials  

Science.gov (United States)

Necessary theoretical foundation is given for the treatment of magnetic stresses applied to

1969-01-01

210

Magnetic forming coil design and development summary report  

Science.gov (United States)

Magnetic forming coil design and development

1964-01-01

212

Large scale magnetic field measurements and mapping  

CERN Document Server

Large scale magnetic field measurements and mapping

1984-01-01

213

ELECTRICAL AND DIAGNOSTIC ASPECTS OF ELECTROHYDRAULIC AND MAGNETIC FORMING  

Science.gov (United States)

Discussion of an electrohydraulic and magnetic forming process

1963-01-01

215

Magnetic separation of antibiotics by electrochemical magnetic seeding  

Energy Technology Data Exchange (ETDEWEB)

Magnetic separation of several classes of antibiotics was investigated using electrochemical magnetic seeding. Electrocoagulation with a sacrificial anode followed by addition of magnetite particles was applied for the magnetic seeding of antibiotics. With electrochemical magnetic seeding using an iron anode, tetracycline antibiotics (oxytetracycline, chlortetracycline, doxycycline and tetracycline) and cephalosporin antibiotic (cefdinir) were rapidly removed from synthetic wastewater by magnetic separation using a neodymium magnet. Iron and aluminium anodes were suitable for magnetic seeding of the antibiotics. The results indicated that the ability of antibiotics to form strong complex with iron and aluminium allowed the higher removal by magnetic separation. This method would be appropriate for rapid treatment of ...

2009-03-01

216

Results of Compact Stellarator Engineering Trade Studies  

Energy Technology Data Exchange (ETDEWEB)

number of technical requirements and performance criteria can drive stellarator costs, e.g., tight tolerances, accurate coil positioning, low aspect ratio (compactness), choice of assembly strategy, metrology, and complexity of the stellarator coil geometry. With the completion of a seven-year design and construction effort of the National Compact Stellarator Experiment (NCSX) it is useful to interject the NCSX experience along with the collective experiences of the NCSX stellarator community to improving the stellarator configuration. Can improvements in maintenance be achieved by altering the stellarator magnet configuration with changes in the coil shape or with the combination of trim coils? Can a mechanical configuration be identified that incorporates a partial set of shaped fixed stellarator coils along with some removable coil set to enhance the overall machine maintenance? Are there other ...

2009-05-27

217

Results of Compact Stellarator Eengineering Trade Studies  

Energy Technology Data Exchange (ETDEWEB)

A number of technical requirements and performance criteria can drive stellarator costs, e.g., tight tolerances, accurate coil positioning, low aspect ratio (compactness), choice of assembly strategy, metrology, and complexity of the stellarator coil geometry. With the completion of a seven-year design and construction effort of the National Compact Stellarator Experiment (NCSX) it is useful to interject the NCSX experience along with the collective experiences of the NCSX stellarator community to improving the stellarator configuration. Can improvements in maintenance be achieved by altering the stellarator magnet configuration with changes in the coil shape or with the combination of trim coils? Can a mechanical configuration be identified that incorporates a partial set of shaped fixed stellarator coils along with some removable coil set to enhance the overall machine maintenance? Are there other ...

2009-09-25

218

Optical Feshbach Resonances in Alkaline Earth Atoms  

Science.gov (United States)

Recent proposals have shown that a quantum degenerate gas of alkaline earth atoms can be used for a number of novel quantum computing and quantum simulation experiments. Strontium is a good candidate for such experiments because it can be controlled with high precision, as demonstrated in recent atomic clock experiments. Unfortunately, the small scattering length of strontium is not amenable to evaporative cooling techniques that are used to reach quantum degeneracy. Furthermore, increasing the scattering length of alkaline earths with a magnetic Feshbach resonance is not possible due to their spinless electronic ground state configuration. However, recent theoretical and experimental work suggests the possibility of changing scattering lengths in alkaline earths with laser light. Using this optical Feshbach resonance near strontium's narrow ^1S0->^3P1 intercombination transition might allow its ...

2009-10-01

219

Launch of the Space experiment PAMELA  

CERN Document Server

PAMELA is a satellite borne experiment designed to study with great accuracy cosmic rays of galactic, solar, and trapped nature in a wide energy range protons: 80 MeV-700 GeV, electrons 50 MeV-400 GeV). Main objective is the study of the antimatter component: antiprotons (80 MeV-190 GeV), positrons (50 MeV-270 GeV) and search for antimatter with a precision of the order of 10^-8). The experiment, housed on board the Russian Resurs-DK1 satellite, was launched on June, 15, 2006 in a 350*600 km orbit with an inclination of 70 degrees. The detector is composed of a series of scintillator counters arranged at the extremities of a permanent magnet spectrometer to provide charge, Time-of-Flight and rigidity information. Lepton/hadron identification is performed by a Silicon-Tungsten calorimeter and a Neutron detector placed at the bottom of the device. An Anticounter system is used offline to reject false triggers coming from the ...

2007-01-01

220

Front-End-Electronics Communication software for multiple detectors in the ALICE experiment  

Energy Technology Data Exchange (ETDEWEB)

In the ALICE experiment at CERN, the Detector Control System (DCS) employs several interacting software components to accomplish its task of ensuring the correct operation and monitoring of the experiment. This paper describes the Front-End-Electronics Communication (FeeCommunication) software and its role within the DCS. The FeeCommunication software's central task is passing configuration and monitoring data between the top level DCS process control and the field devices of several detectors within ALICE. The lowest level of the FeeCommunication software runs on the DCS boards, specialized embedded systems which are in direct contact with the field devices and are physically located within the detector. The middle and upper layers run on standard PC hardware located in the counting room or other external locations. This paper focuses on the design and implementation of the FeeCommunication software and the steps that were taken to ...

2006-02-15

221

Data Compression on Zero Suppressed High Energy Physics Data  

CERN Document Server

Future High Energy Physics experiments will produce unprecedented data volumes (up to 1 GB/s [1]). In most cases it will be impossible to analyse these data in real time and they will have to be stored on durable mostly magnetic linear media (e.g. tapes) for later analysis. This threatens to become a major cost factor for the running of these experiments. Here we present some ideas developed together with the Institute of Computer Graphics, Department for Algorithms and Programming on how this volume and the related cost can be reduced significantly. The algorithms presented are not general ones but aimed in particular to physics experiments data. Taking advantage of the knowledge of the data they are highly superior to general ones (Huffman, LZW, arithmetic coding) both in compression rate but more importantly in speed as to keep up with the output rate to modern tape drives. Above standard algorithms ...

1996-01-01

222

Analysis of the Semileptonic Decay D0 --> anti-K0 pi- mu+ nu  

Energy Technology Data Exchange (ETDEWEB)

This thesis describes the analysis of the semileptonic decay D{sup 0} {yields} {bar K}{sup 0} {pi}{sup -} {mu}{sup +}{nu} using FOCUS data. FOCUS is a fixed target experiment at Fermilab that studies the physics of the charm quark. Particles containing charm are produced by photon-gluon fusion from the collision of a photon beam on a BeO target. The experiment is characterized by excellent vertex resolution and particle identification. The spectrometer consists of three systems for track reconstruction (two silicon systems and one multiwire proportional chamber system) and two magnets of opposite polarity. The polarity of the magnet is such that the events of e{sup +}e{sup -} pairs produced in the target (which constitutes the main background) travel through a central opening in the detectors without interactions. Particle momentum is measured from the deflection angle in the ...

2004-11-01

223

Hybrid Simulations of Mini Magnetospheres in the Laboratory  

Science.gov (United States)

We use a massively parallel 3D hybrid particle code, dHybrid, to simulate the deflection of plasma beams by a dipole like magnetic field in a laboratory environment. Dipole magnetic fields, along with a plasma injection source to inflate the magnetic field, are now being studied as means of deflecting solar wind and Energetic Particles away from spacecrafts [1,2,3]. We have considered three setups, consistent with the experiments, with a plasma beam fired at i) a dipole field with no plasma injection, ii) a plasma injection source with no dipole field and iii) a dipole field with a plasma injection source. The hybrid simulations help understand the relevant physical phenomena, and enable extrapolation to space plasma scenarios, where setups are similar but plasma parameters differ significantly. The simulation results consistently show the plasma beam being deflected by the dipole field, in the first ...

2007-11-01

224

Use of clays as liners in solar ponds  

Energy Technology Data Exchange (ETDEWEB)

An alternative to synthetic materials for use in solar pond liners is to select clayey soils as hydraulic barriers. This option reduces the cost of construction and the risk of contamination of subsoil and groundwater by hot brines. This paper deals with the physical, chemical and hydraulic properties of different soils tested mainly as compacted clay liners. The underdeveloped nations have the option to use this type of liner, but before doing so several tests are recommended, including those for soil and water composition, permeability, plasticity and X-ray diffraction analysis. In this investigation the following samples are analyzed: native clayey soils with illite, montmorillonite and halloysite, treated and non-treated bentonites in powder and granulated form, a mixture of zeolite and sodium bentonite, and industrial minerals composed largely of halloysite, kaolinite and attapulgite selected clays. Neutral salt aqueous solutions (NaCl and KCl) at different ...

2009-06-15

225

Thermodynamics and stability of the mixed-conducting Sr-Fe-Co-O system.  

Energy Technology Data Exchange (ETDEWEB)

Mixed-conducting Sr-Fe-Co oxides have potential applications in dense ceramic membranes for high-purity oxygen separation and/or methane conversion to produce syngas (CO + H{sub 2}), because of their combined high electronic/ionic conductivity and significant oxygen permeability. We studied the crystal structure and microstructure of the system in X-ray diffraction experiments and by using scanning electron microscopy, respectively. Thermogravimetric analysis was conducted on the SrFeCo{sub 0.5}O{sub x} sample in environments of various oxygen partial pressures (pO{sub 2}). Conductivity increased while weight decreased with increasing temperature. Activation energy decreased while conductivity increased with increasing pO{sub 2}. The pO{sub 2}-dependent conducting behavior of the SrFeCo{sub 0.5}O{sub x} system can be understood by considering the trivalent-to-divalent transition of transition-metal ions.

1999-04-28

226

Synthesis and photo-degradation application of WO3/TiO2 hollow spheres  

British Library Electronic Table of Contents (United Kingdom)

A WO3/TiO2 composite, hollow-sphere photocatalyst with average diameter of 320nm and shell thickness of 50nm was successfully prepared using a template method. UV-vis diffuse reflectance spectra illustrated that the main absorption edges of the WO3/TiO2 hollow spheres were red-shifted compared to the TiO2 hollow spheres, indicating an extension of light absorption into the visible region of the composite photocatalyst. The WO3 and TiO2 phases were confirmed by X-ray diffraction analysis. BET isotherms revealed that the specific surface area and average pore diameter of the hollow spheres were 40.95m^2/g and 19nm, respectively. Photocatalytic experiments indicate that 78% MB was degraded by WO3/TiO2 hollow spheres under visible light within 80min. Under the same conditions, only 24% MB can ...

2011-01-01

227

Some computer simulations of semiconductor thin film growth and strain relaxation in a unified atomistic and kinetic model  

Energy Technology Data Exchange (ETDEWEB)

An overview is provided of an evolving atomistic and kinetic model of semiconductor growth that unifies the main features of strain relaxation in low and high lattice misfit heteroepitaxy. The model reveals a kinetic pathway for dislocation formation during growth with little or no energy cost at low misfits, thus providing a way out of the longstanding dilemma of too high dislocation nucleation energies predicted by classical theories of the equilibrium behavior of a fixed number of particles at low misfits. The essential kinetic process underlying the model are identified on the basis of comparison of the predictions of kinetic Monte-Carlo simulations of growth with real-time or in-situ data obtained in such experiments as reflection high-energy electron diffraction (RHEED) and scanning probe microscopy (SPM). Relative significance of these atomistic kinetic processes is shown to naturally lead to strain relaxation via defect initiation at ...

1996-12-31

228

Removal of Cr(III) from aqueous solutions using zeolite NaY prepared from rice husk ash  

International Nuclear Information System (INIS)

The efficiency of the synthesized zeolite NaY from rice husk ash (RHA) in the removal of Cr(III) from aqueous solution was studied. Zeolite NaY was synthesized from RHA via seeding technique and the identification of its structure was done by X-ray Diffraction (XRD) technique and the elemental analysis was carried out by X-ray Fluorescence (XRF). The physicochemical properties which were related to the use of the zeolite NaY as a sorbent was also investigated. The synthesized zeolite NaY has higher cation exchange capacity (CEC) than the commercial zeolite NaY due to the higher amount of sodium content in the synthesized as well as the lower ratio of silica to alumina. The synthesized zeolite NaY together with the commercial one as comparison was used in the sorption of the Cr(III) in aqueous solution by batch sorption experiments. The kinetic study showed that the Cr(III) uptake by both zeolites were based on the pseudo second order model. ...

2007-01-01

229

Properly synchronized measurements of droplet sizes for high-pressure intermittent coal-water slurry fuel sprays  

Energy Technology Data Exchange (ETDEWEB)

Experiments were completed to study intermittent coal-water slurry (CWS) fuel sprays injected from an electronically-controlled accumulator injector system. A new synchronization technique was developed using the light extinction signal as a triggering source for the data taking initiation with a laser diffraction particle analyzing (LDPA) technique. This technique allowed measurement of SMDs near the spray tip where the light extinction was low and the data were free from the multiscattering bias. Coal-water slurry fuel with 50% coal loading in mass containing 5 {mu}m mass median diameter coal particulates was considered. A correlation of the SMD with the injection conditions was determined which should show a satisfactory agreement with the measured SMD data. The spray SMD showed an increase with the distance of the axial measurement location and with the ambient gas density, and showed a decrease with increasing injection pressure.

1993-12-31

230

Preparation and photocatalytic property of pyrochlore Bi{sub 2}Ti{sub 2}O{sub 7} and (Bi, La) {sub 2}Ti{sub 2}O{sub 7} films  

Energy Technology Data Exchange (ETDEWEB)

Dopant-free Bi{sub 2}Ti{sub 2}O{sub 7} thin films with pyrochlore structure and La-doped bismuth titanate thin films have been fabricated by means of chemical solution decomposition, and characterized by X-ray diffraction, atomic force microscopy, scanning electron microscopy and UV-Vis spectrophotometry in this study. Their photocatalytic activities have been evaluated by photodegrading methyl orange solution, and the optimum processing parameters for the highest photocatalytic activity have been found. Moreover, the effects of La-doping on the phase transformation and the photocalalytic activity have been studied. It has been deduced from the experiment result that substituted La{sup 3+} ions can act as a stabilizer of Aurivillus phase BLT and a grain-growth inhibitor in BLT thin films.

2008-11-28

231

Modeling paraxial wave propagation in free-electron laser oscillators  

International Nuclear Information System (INIS)

Modeling free-electron laser (FEL) oscillators requires calculation of both the light-beam interaction within the undulator and the light propagation outside the undulator. We have developed a paraxial optical propagation code that can be combined with various existing models of gain media, for example, Genesis 1.3 for FELs, to model oscillators with full paraxial wave propagation within the resonator. A flexible scripting interface is used both to describe the optical resonator and to control the codes for propagation and amplification. To illustrate its capabilities, we numerically investigate two significantly different FEL oscillators: the free-electron laser for infrared experiments (FELIX) system and the vacuum-ultraviolet (VUV)-FEL oscillator of the proposed high-gain fourth generation light source. For the FELIX system, we find that diffraction losses are a considerable part of the single-pass cavity loss (at a wavelength of 40 #mu#m). ...

2006-11-01

232

Influence of bias voltage on the formation and properties of iron-based nitrides produced by plasma nitriding  

Energy Technology Data Exchange (ETDEWEB)

A series of experiments have been conducted on AISI 5140 low alloy steel using a hollow cathode discharge-assisted plasma nitriding apparatus with the aim of elucidating the role of substrate bias voltages in plasma nitriding process. For comparison, some samples were nitrided with applied substrate bias (-50 V) while other samples were nitrided at floating potential. Treatments were carried out in NH{sub 3} atmosphere of 150 Pa at temperatures ranging from 450 {sup o}C to 550 {sup o}C for 2 h, 4 h, and 6 h. The nitrided samples were characterized by optical microscopy, X-ray diffraction and micro-hardness measurement. The corrosion behaviors were evaluated using anodic polarization tests in 3.5% NaCl solution. The results showed that the microstructure and phase constituents of the nitride layers were strongly influenced by the bias voltages. It was also demonstrated that the better corrosion resistance with a thicker nitrided layer was ...

2010-05-14

233

Influence of bias voltage on the formation and properties of iron-based nitrides produced by plasma nitriding  

International Nuclear Information System (INIS)

A series of experiments have been conducted on AISI 5140 low alloy steel using a hollow cathode discharge-assisted plasma nitriding apparatus with the aim of elucidating the role of substrate bias voltages in plasma nitriding process. For comparison, some samples were nitrided with applied substrate bias (-50 V) while other samples were nitrided at floating potential. Treatments were carried out in NH_3 atmosphere of 150 Pa at temperatures ranging from 450 "oC to 550 "oC for 2 h, 4 h, and 6 h. The nitrided samples were characterized by optical microscopy, X-ray diffraction and micro-hardness measurement. The corrosion behaviors were evaluated using anodic polarization tests in 3.5% NaCl solution. The results showed that the microstructure and phase constituents of the nitride layers were strongly influenced by the bias voltages. It was also demonstrated that the better corrosion resistance with a thicker nitrided layer was obtained on the ...

2010-05-14

234

High frequency limit of vacuum microelectronic grating free-electron laser  

International Nuclear Information System (INIS)

The dependencies that limit high frequency operation of a vacuum microelectronic grating free-electron laser are examined. The important parameters are identified as the electron beam energy, emittance, and generalized perveance. The scaling of power with emittance and frequency is studied in the far-infrared spectral range using a modified scanning electron microscope (SEM) and submillimeter diffraction gratings. The SEM is suited to the task of generating and positioning a low emittance (10"-"2#pi#-mm-mrad), low current (100 #mu#A), but high current density (50-500 A cm"-"2) electron beam. It has been used to demonstrate the spontaneous emission process known as the Smith-Purcell effect. A vacuum microelectronic grating free-electron laser has the potential of generating radiation throughout the entire far-infrared spectral range which extends from approximately 10 to 10"3#mu#m. An introduction to the theory, initial results, and details of the ...

1995-08-21

235

Fuel spray evolution; Comparison of experiment and CFD simulation of nonevaporating spray  

Energy Technology Data Exchange (ETDEWEB)

Detailed spray characteristics were obtained for a small-capacity, pressure-swirl atomizer using an Aerometrics phase-Doppler particle analyzer. Measurements included drop size and velocity distributions, liquid volume fluxes, and air velocities at four axial locations, 25,50,75, and 100 mm, with complete radial traverses at each location. Drop size results were compared with measurements from a Malvern laser-diffraction instrument, and integrated liquid volume fluxes were compared with measured flow rates to estimate measurement uncertainties. Drop sizes measured by the two independent techniques and area-weighted-averaged over the radial traverses at each of the four axial stations varied on average by less than 4 percent. Integrated volume flux measurements by the phase-Doppler instrument at four axial stations differed from the nozzle flow rate by at most 19 percent, with some of the difference due to evaporation. The phase-Doppler data were used to begin an ...

1989-01-01

236

Flow behaviour and microstructure of the heat-resistant steels X20CrMoV12.1 and X5NiCrTiAl32.20 (alloy 800)  

Energy Technology Data Exchange (ETDEWEB)

Flow-curve characteristics of the heat-resistant steels X 20 CrMoV 12.1 and alloy 800 (X5NiCrTiAl32.20) were measured by tensile and compression tests at temperatures between room temperature and 800 C and strain rates {epsilon}{<=}10 s{sup -1} in connection with microstructure investigations (dislocation content, carbide precipitation) by TEM and X-ray diffraction analysis (XDA). Modelling the deformation behaviour of the steels in terms of the microstructure development indicates that it cannot be explained in a simple manner. The flow curves {sigma}={sigma}({epsilon}, {epsilon}, T) lie, in general, between those predicted by the Kocks-Mecking-Estrin model and a modified (i.e. two-parameter) Roberts model. Because of the less complicated nature of the deformation process the correspondence of experiment and modelling is more satisfying in the case of the material X 20 CrMoV 12.1. (orig.) 26 refs.

1999-10-01

237

Facile synthesis of additive-assisted nano goethite powder and its application for fluoride remediation  

Energy Technology Data Exchange (ETDEWEB)

The present article describes a novel synthesis route for nano-sized goethite ({alpha}-FeOOH) using hydrazine sulphate as an additive. The X-ray diffraction (XRD) peaks of synthesized powder matched well with those of {alpha}-FeOOH. Transmission electron microscopy (TEM) showed the particles of irregular shape in the range of 1-10 nm. Batch adsorption experiments for fluoride uptake were performed to study the influence of various experimental parameters such as contact time (10 min to 7 h), initial fluoride concentration (10-150 mg L{sup -1}), pH (2-11.6) and the presence of competing anions. The time data fitted well to pseudo-second-order kinetic model. The fluoride removal passed through broad maxima in pH ranges of 6-8. High adsorption capacity of 59 mg g{sup -1} goethite was obtained. The isothermic data fitted well to Freundlich model. The presence of other ions namely chloride and sulphate adversely affected fluoride removal. Fluoride ...

2010-02-15

238

Develop techniques for ion implantation of PLZT [lead-lanthanum-zirconate-titanate] for adaptive optics  

International Nuclear Information System (INIS)

Research was conducted at Pacific Northwest Laboratory to develop high photosensitivity adaptive optical elements utilizing ion implanted lanthanum-doped lead-zirconate-titanate (PLZT). One centimeter square samples were prepared by implanting ferroelectric and anti-ferroelectric PLZT with a variety of species or combinations of species. These included Ne, O, Ni, Ne/Cr, Ne/Al, Ne/Ni, Ne/O, and Ni/O, at a variety of energies and fluences. An indium-tin oxide (ITO) electrode coating was designed to give a balance of high conductivity and optical transmission at near uv to near ir wavelengths. Samples were characterized for photosensitivity; implanted layer thickness, index of refraction, and density; electrode (ITO) conductivity; and in some cases, residual stress curvature. Thin film anti-ferroelectric PLZT was deposited in a preliminary experiment. The structure was amorphous with x-ray diffraction showing the beginnings of a structure at ...

239

Characterization of supported palladium catalysts II. Pd/SiO sub 2  

Science.gov (United States)

The isomerization of neopentane has been investigated over the 0.76 wt% Pd/SiO{sub 2} catalyst. It is found that after high temperature reduction (HTR, at 873 K) the selectivity for isomerization is much higher than that after low temperature reduction (LTR, at 573 K). A variety of experiments, including kinetic, chemisorption (O{sub 2}, H{sub 2}, and CO), temperature-programmed desorption of H{sub 2}, and X-ray diffraction, showed that this selectivity enhancement cannot be interpreted in terms of H{sub 2} retention by catalyst. Instead, the formation of Pd-Si compound(s) (most probably Pd{sub 3}Si) during HTR seems immediately responsible for the catalytic behavior of HTR Pd/SiO{sub 2} catalysts. A mechanism is proposed for the Pd-SiO{sub 2} interaction in which Pd atoms (or ions) are incorporated into the silica support (via oxygen vacancies) and a new phase of palladium silicide is formed. Regeneration by an oxygen treatment of the HTR ...

1989-06-01

240

Cellulose as a binding material in graphitic anodes for Li ion batteries: a performance and degradation study  

Energy Technology Data Exchange (ETDEWEB)

Four types of cellulose, in particular carboxy methyl cellulose (CMC), are tested as potential binding materials in graphitic anodes for lithium ion batteries. It is shown that a minimum content of a cellulose which gives acceptable anode properties (reversible capacity > 300 mA hg{sup -1} during the first 10 cycles, irreversible loss < 20%) is about 2 wt.%, which is less than in the case of conventional polymeric binders (5-10 wt.%). Kinetics of insertion-deinsertion and passivation processes seem not to be affected by the presence of cellulose. Explanation for the electrode failure at cellulose contents lower than 1 wt.% is given based on X-ray diffraction and microscopy investigations. Finally, the structure (distribution) of cellulose in the composite anode material is discussed and (indirectly) checked with a series of experiments. Most results are compared with the corresponding results obtained either with gelatin or ...

2003-02-20

241

A study into effects of CO2 laser melting of nitrided Ti-6Al-4V alloy  

Science.gov (United States)

Multiple treatment of engineering surfaces can provide improved surface properties that cannot be obtained by a single surface treatment. Consequently, this study investigates the effects of laser melting on the microstructures of plasma nitrided Ti-6Al-4V alloy. The study consists of two parts. In the first part, governing equations pertinent to the laser melting process are developed, and temperature variation across the melted zone is predicted. In the second, an experiment is conducted to nitride the surface of the alloy through plasma nitriding process and to melt the plasma nitrided and the untreated alloy surfaces with a CO2 laser beam. The resulting metallurgical changes are examined using x-ray diffraction (XRD), bdenergy-dispersive spectrometry (EDS), and scanning electron microscopy (SEM) techniques. It is shown that three distinct nitride layers are formed in the vicinity of the alloy surface prior to the laser melting process, and ...

1997-10-01

242

Stability and disturbance of large dc superconducting magnets  

Energy Technology Data Exchange (ETDEWEB)

This paper addresses the stability aspects of several successful dc superconducting magnets such as large bubble chamber magnets, and magnets for the Mirror Fusion Test Facility and MHD Research Facility. Specifically, it will cover Argonne National Laboratory 12-Foot Bubble Chamber magnets, the 15-foot Bubble Chamber magnets at Fermi National Laboratory, the MFTF-B Magnet System at Lawrence Livermore National Laboratory, the U-25B Bypass MHD Magnet, and the CFFF Superconducting MHD magnet built by Argonne National Laboratory. All of these magnets are cooled in pool-boiling mode. Magnet design is briefly reviewed. Discussed in detail are the adopted stability critera, analyses of stability and disturbance, stability simulation, and the final results of magnet ...

1981-11-11

243

Magnetic braking of the rotation of molecular cloud cores  

International Nuclear Information System (INIS)

We investigate the magnetic braking of the core of an axisymmetric cloud whose rotation axis is parallel to the mean direction of the magnetic field. (author).

244

LHC magnet alignment  

CERN Document Server

Checks are performed on the alignment of the magnets in the LHC tunnel. It is vital that each magnet is placed exactly where it has been designed so that the path of the beam is precisely controlled.

2007-01-01

245

Test Bed for Superconducting Materials  

Energy Technology Data Exchange (ETDEWEB)

Superconducting rf cavities are increasingly used in accelerators. Gradient is a parameter of particular importance for the ILC. Much progress in gradient has been made over the past decade, overcoming problems of multipacting, field emission, and breakdown triggered by surface impurities. However, the quenching limit of the surface magnetic field for niobium remains a hard limitation on cavity fields sustainable with this technology. Further exploration of materials and preparation may offer a path to surpassing the current limit. For this purpose, we have designed a resonant test cavity. One wall of the cavity is formed by a flat sample of superconducting material; the rest of the cavity is copper or niobium. The H field on the sample wall is 75% higher than on any other surface. Multipacting is avoided by use of a mode with no surface electric field. The cavity will be resonated through a coupling iris with high-power rf at superconducting temperature until the ...

2006-01-30

246

New correlated electron physics from new materials  

International Nuclear Information System (INIS)

Many important advances in the physics of strongly correlated electron systems have been driven by the development of new materials: for instance the filled skutterudites MT4X12 (M=alkali metal, alkaline earth, lanthanide, or actinide; T=Fe, Ru, or Os; X=P, As, or Sb), certain lanthanide and actinide intermetallic compounds such as URu2-xRexSi2 and CeTIn5 (T=Co, Rh, or Ir), and layered oxypnictides and related materials. These types of complex multinary d- and f-electron compounds have proven to be a vast reservoir of novel strongly correlated electron ground states and phenomena. In these materials, the occurrence of such a wide range of ground states and phenomena arises from a delicate interplay between competing interactions that can be tuned by partial or complete substitution of one element for another, as well as the application of pressure, and magnetic fields, resulting in rich and complex electronic phase diagrams in the hyperspace of temperature, ...

2009-10-15

247

Managing system for mounted parts and spare parts of power source facilities  

Energy Technology Data Exchange (ETDEWEB)

The power source facilities of JT-60 consist of poloidal magnetic coil power source, toroidal magnetic coil power source, the power generation facility for heating, operation power distribution facility and secondary cooling facility, and at the time of the experiment operation of JT-60, they supply 1300 MVA of instantaneous maximum power to loads. The component machinery and equipment of the power source facilities are installed in about 20 indoor and outdoor places, and their mounted parts are about 15,000 kinds. About 3,000 kinds of spare parts are preserved in 15 exclusively used stores. The managing system for mounted parts and spare parts of JT-60 power source facilities which possesses the functions of rapidly and efficiently carrying out the storage of large quantity of information, mutual relating and retrieval by making mounted parts and spare parts into a data base and doing their unified management with a ...

1995-07-01

248

Magnetic resonance imaging in patients with heart valve prostheses  

International Nuclear Information System (INIS)

Artifical valve prostheses are often regarded as a contraindication for magnetic resonance imaging (MRI), although preliminary in vitro studies suggested, that patients with these metallic implants might safely undergo MR examination. This study reports on the experience with a group of 89 patients with 100 heart valve prostheses who were examined by spin-echo MR and gradient-echo MR. MR examination was performed in all patients without complications. The spin-echo sequence showed advantages in the depiction of anatomical structures like paravalvular abcesses. Anatomical structures adjacent to the artificial valve were clearly visivle and the metal components of the valves showes no or only small artifacts. Artifacts were accentuated when using gradient-echo sequences. Gradient-echo sequences provided valuable information regarding the presence of valvular insufficiency. Physiological valvular regurgitation was easy to differentiate from ...

249

Density separation of materials by using magnetic fluids  

Energy Technology Data Exchange (ETDEWEB)

The magnetic fluid is a colloidal suspension of magnetite in kerosene, prepared by a low-cost process. Separation is accomplished in an open trough filled with magnetic fluid. A magnetic field is established in the fluid, by energizing an electromagnet having poles on each side of the trough. Due to the design of the magnet poles and air gaps, the magnetic field is strongest at the bottom, about 10,000 oersteds, and uniformly decreases in strength to about 2000 oersteds at the top of the fluid. Therefore, the magnetic field gradient increases with depth. The magnetic force attracts the entire separation medium (magnetic fluid) creating a reaction force of equal magnitude and acting in the opposite direction. This reaction created within a magnetic fluid/magnetic field combination ...

1980-03-01

250

Crack healing behavior and high-temperature strength properties in mullite/SiC composite ceramics. Muraito/SiC fukugo ceramics no kiretsu chiyu kyodo to koon kyodo tokusei  

Energy Technology Data Exchange (ETDEWEB)

Discussions were given on mullite/SiC composite ceramics as to crack size dependence of their crack healing behavior, and high-temperature strength properties. Test specimens used in the experiment are sinters of mullite powder added with SiC powder at 20% by volume, and hot-pressed under conditions of a sintering temperature of 1650 degC, time of four hours, and a pressure of 35 MPa. In the experiment, a pre-crack was introduced at the center of a test specimen by using a Vickers hardness meter, and a heat treatment was performed in atmosphere at 1300 degC for one hour. A four-point bending test was conducted in atmosphere as a strength test. Conditions in test specimens were investigated by using SEM observation, a laser microscope and X-ray diffraction. The following findings were obtained as a result of the experiment: the bending strength for the pre-cracked material is about 140 MPa against that ...

1998-05-21

251

Low temperature partly ionized plasma in magnetic fusion devices: Present status and prospects  

Energy Technology Data Exchange (ETDEWEB)

The most striking achievement in magnetic fusion experiments during last few years was the discovery of plasma detachment from material targets, a much needed effect for plasmas with high power fusion parameters. Due to the very low heat loads on the targets observed in these regimes and potentially low erosion of the targets, detached regimes look attractive from the International Thermonuclear Experimental Reactor (ITER) design point of view. Thus the author has experimental proof for the possibility for a co-existence of fusion relevant hot plasma in the core and a low temperature partly ionized plasma at the edge of magnetic fusion device. Although somewhat similar behavior of edge plasma was considered theoretically even before plasma detachment was found experimentally, it was not clear in the beginning how these theoretical and experimental findings would fit together. Now, after a few years of intensive additional ...

1998-12-31

252

Beam-induced damage on diffractive hard X-ray optics  

UK PubMed Central (United Kingdom)

The issue of beam-induced damage on diffractive hard X-ray optics is addressed. For this purpose a systematic study on the radiation damage induced by a high-power X-ray beam is carried out in both...Full Text Available

2010-11-01

253

Physical and optical properties of rare earth cobalt magnets  

Energy Technology Data Exchange (ETDEWEB)

Rare Earth Cobalt (REC) permanent magnets have unique properties that permit solutions to some optical tasks that cannot be accomplished with conventional magnets. A review of design and of performance characteristics of these magnets includes an analytical description of the three dimensional fringe fields of REC quadrupoles.

1980-08-01

259

METHOD OF FORMING THIN MAGNETIC FILM  

J-STORE (Japan)

Full Text Available

2007-10-04

265

Two dimensional NMR and NMR relaxation studies of coal structure  

Energy Technology Data Exchange (ETDEWEB)

This report covers the progress made on the title project for the project period. Four major areas of inquiry are being pursued. Advanced solid state NMR methods are being developed to assay the distribution of the various important functional groups that determine the reactivity of coals. Special attention is being paid to methods that are compatible with the very high magic angle sample spinning rates needed for operation at the high magnetic field strengths available today. Polarization inversion methods utilizing the difference in heat capacities of small groups of spins are particularly promising. Methods combining proton-proton spin diffusion with [sup 13]C CPMAS readout are being developed to determine the connectivity of functional groups in coals in a high sensitivity relay type of experiment. Additional work is aimed at delineating the role of methyl group rotation in the proton NMR relaxation behavior of coals.

1992-11-25

266

Tools and methods for implementing the control systems on the Mirror Fusion Test Facility  

Energy Technology Data Exchange (ETDEWEB)

Installation of the major hardware subsystems for MFTF is nearing completion. These subsystems include the Fusion Chamber System, the eighty KV Neutral Beam System, the Superconducting Magnet System, and the Personnel Safety System. The Local Controls group has undertaken a uniform aproach to implementing the control systems for all of these hardware subsystems. This approach has two major aspects: (1) to provide a stand-alone computer control system with a remote, portable terminal so that computer control can be provided at the site of the hardware for initial testing, (2) to provide hardware simulators so that the complicated MFTF computer control system can be tested independent of the hardware. The software and hardware tools which were developed to carry out this plan will be described. Our experiences with bringing up subsystems containing up to 900 separate channels of control and status will also be described.

1981-09-29

267

Steady particulate flows in a horizontal rotating cylinder  

Energy Technology Data Exchange (ETDEWEB)

Results of discrete element method (DEM) simulation and magnetic resonance imaging (MRI) experiments are compared for monodisperse granular materials flowing in a half-filled horizontal rotating cylinder. Because opacity is not a problem for MRI, a long cylinder with an aspect ratio {approximately}7 was used and the flow in a thin transverse slice near the center was studied. The particles were mustard seeds and the ratio of cylinder diameter to particle diameter was approximately 50. The parameters compared were dynamic angle of repose, velocity field in a plane perpendicular to the cylinder axis, and velocity fluctuations at rotation rates up to 30 rpm. The agreement between DEM and MRI was good when the friction coefficient and nonsphericity were adjusted in the simulation for the best fit. {copyright} {ital 1998 American Institute of Physics.}

1998-06-01

268

State of the art simulations of magnicon  

International Nuclear Information System (INIS)

The magnicon is a highly attractive candidate to be the RF source for a future multi-Tev linear collider. Physical models and computer codes have been developed which can provide start-to-end self-consistent simulations of a magnicon, including precise simulations of the high-convergence electron gun, RF-system, magnetic system, and beam collector. The 3-D beam dynamics simulations include realistic fields, finite beam size and transverse space charge effects. The codes allow one to provide steady-state simulations of the entire tube, so as to evaluate transient process of magnicon excitation, parasitic mode self-excitation, stability analysis, and tolerance analysis. The results of the simulations are found to be in good agreement with magnicon experiments. A brief description of the physical models and simulation codes employed will be given.

2002-12-12

269

Stabilizing effect of the electron-beam self-fields on the phase-space trajectory in a self-amplified spontaneous emission free-electron laser operating in ultraviolet and x-ray spectral ranges  

International Nuclear Information System (INIS)

A detailed treatment is introduced to measure the dynamic stability of the relativistic electrons in a self-amplified spontaneous emission free-electron laser (FEL) system, which includes the numerical approach of the Kolmogorov entropy (entropy-like quantity), the general equations of motion for a charged particle and the method of monitoring the simulation accuracy. Numerical experiments reveal a new phenomenon that there exists the possibility of the transition from chaotic to non-chaotic phase-space trajectories of the strongly relativistic electrons due to the effect of their self-fields. The adiabatic magnetic field of a one-dimensional wiggler may have a slight influence on the electron transportation in the absence of the FEL fields, but substantially affects the dynamic stability of the electrons in the process of the FEL interaction. Moreover, the laser fields diminish the dynamic stability of the electrons as the FEL interaction ...

2004-02-28

270

Results from a Prototype Chicane-Based Energy Spectrometer for a Linear Collider  

Energy Technology Data Exchange (ETDEWEB)

The International Linear Collider (ILC) and other proposed high energy e{sup +}e{sup -} machines aim to measure with unprecedented precision Standard Model quantities and new, not yet discovered phenomena. One of the main requirements for achieving this goal is a measurement of the incident beam energy with an uncertainty close to 10{sup -4}. This article presents the analysis of data from a prototype energy spectrometer commissioned in 2006-2007 in SLAC's End Station A beamline. The prototype was a 4-magnet chicane equipped with beam position monitors measuring small changes of the beam orbit through the chicane at different beam energies. A single bunch energy resolution close to 5 {center_dot} 10{sup -4} was measured, which is satisfactory for most scenarios. We also report on the operational experience with the chicane-based spectrometer and suggest ways of improving its performance.

2011-02-28

271

Overview of Cooling Water System for the KSTAR 1st Plasma Experiment  

International Nuclear Information System (INIS)

The KSTAR cooling water system (CWS) consists of a primary cooling water system (PCWS), a secondary cooling water system (SCWS), and a de-mineralizing and de-ionized water system (DIWS). The PCWS cooling loops have been made for the poloidal field (PF) and toroidal field (TF) magnet power supplies (MPS), vacuum vessel (VV), electron cyclotron heating (ECH), ion cyclotron heating (ICRH), vacuum pumps, diagnostics, helium facility, etc. The CWS had been done individual commissioning of each system to confirm the design specifications by the end of 2006 and had gradually begun operation for the KSTAR ancillary devices by March 2008

2009-05-01

272

New Measurements of the Proton Electromagnetic Form Factor Ratio at Low Q{sup 2}  

Energy Technology Data Exchange (ETDEWEB)

Polarization measurements are allowing the electric to magnetic form factor ratio of the proton to be determined with unprecedented precision. Recent results indicate that there is a large deviation from unity in the proton form factor ratio around Q{sup 2}{approx_equal}0.35 GeV{sup 2}. Furthermore, the deviation from unity is attributed to a deviation of the electric form factor from standard fits and calculations. A new, partially completed, experiment will significantly improve the existing data and will determine the presence, if any, of a narrow structure in the form factor ratio. The new measurement, combined with the expected high precision cross section measurements, will allow the extraction of individual form factors with unprecedented accuracy at low Q{sup 2}.

2009-08-15

273

Nano photonic sensors for microdamage detection : an exploratory simulation.  

Energy Technology Data Exchange (ETDEWEB)

Nano photonic materials are synthetically manufactured crystals at the nano scale with the target of creating a microstructure with a special electro-magnetic periodicity. Such nano photonic materials have the ability to control light propagation and thus are capable of creating photonic bandgaps in the frequency domain. We propose using nano photonic crystals as sensors to detect microdamage in composite materials. We demonstrate using a simulation model that a nano photonic sensor attached to a composite bar experiences a significant change in its bandgap profile when damage is induced in the composite bar. The model predicts the frequency response of the nano photonic sensor using the transfer matrix method. A damage metric to evaluate the change in the frequency response is developed. Successful developments of nano photonic sensors allow damage identification at scales not attainable using current sensing technologies.

2005-04-01

274

Inflammatory spine disease as a cause of back pain  

International Nuclear Information System (INIS)

The aim of this review is to evaluate the role of inflammatory spine disease in patients with chronic back pain. The contribution of imaging modalities for the diagnostic evaluation of back pain is discussed. A systematic literature search based on the classification of seronegative spondyloarthropathies and rheumatoid arthritis was performed. The results of this search and the experiences in a large collective of rheumatological patients are analyzed. The prevalence of rheumatoid arthritis (1-2%) is comparable to that of spondyloarthropathies (1.9%). The etiology of these entities is not fully elucidated. Magnetic resonance imaging is increasingly used for early detection and surveillance of therapy with TNF-#alpha# antagonists. Bone marrow edema, which is only detectable with MRI, represents an early sign of inflammation. Therapy with TNF-#alpha# antagonists is based on clinical and laboratory criteria, and signs of inflammation in MRI. MRI ...

2006-06-01

275

Hyperfine Interactions in USb2 Crystal  

CERN Document Server

The hyperfine interactions at the uranium site in the antiferromagnetic USb2 compound were calculated within the density functional theory (DFT) employing the augmented plane wave plus local orbital (APW+lo) method. We investigated the dependence of the nuclear quadruple interactions to the magnetic structure in USb2 compound. The investigation were performed applying the so called band correlated LDA+U theory self consistently. The self consistent LDA+U calculations were gradually added to the performed generalized gradient approximation (GGA) including scalar relativistic spin orbit interactions in a second variation scheme. The result, which is in agreement with experiment, shows that the 5f-electrons have the tendency to be hybridized with the conduction electrons in the ferromagnetic uranium planes.

2006-01-01

276

Experimental parameterization of an energy function for the simulation of unfolded proteins  

DEFF Research Database (Denmark)

The determination of conformational preferences in unfolded and disordered proteins is an important challenge in structural biology. We here describe an algorithm to optimize energy functions for the simulation of unfolded proteins. The procedure is based on the maximum likelihood principle and employs a fast and efficient gradient descent method to find the set of parameters of the energy function that best explain the experimental data. We first validate the method by using synthetic reference data, and subsequently apply the algorithms to data from nuclear magnetic resonance spin-labeling experiments on the Delta 131 Delta fragment of Staphylococcal nuclease. A significant strength of the procedure that we present is that it directly uses experimental data to optimize the energy parameters, without relying on the availability of high resolution structures. The procedure is fully general and can be applied to a range of experimental data and ...

2008-01-01

277

Effect of Two-Boson Exchange on Parity-Violating e-p Scattering  

Science.gov (United States)

We compute the corrections from two-photon and {gamma}-Z exchange in parity-violating elastic electron-proton scattering, used to extract the strange form factors of the proton. We use a hadronic formalism that successfully reconciled the earlier discrepancy in the proton's electron to magnetic form factor ratio, suitably extended to the weak sector. Implementing realistic electroweak form factors, we find effects of the order 2%-3% at Q{sup 2} < or approx. 0.1 GeV{sup 2}, which are largest at backward angles and have a strong Q{sup 2} dependence at low Q{sup 2}. Two-boson contributions to the weak axial current are found to be enhanced at low Q{sup 2} and for forward angles. We provide corrections at kinematics relevant for recent and upcoming parity-violating experiments.

2008-02-29

278

Determination of the. pi. 1g/sub 9/2/ orbit size in /sup 88/Sr, /sup 90/Zr, and /sup 92/Mo from inelastic electron scattering  

Energy Technology Data Exchange (ETDEWEB)

A study of the ..pi..1g/sub 9/2/ orbit size in /sup 88/Sr, /sup 90/Zr, and /sup 92/Mo is presented. The rms radius for the point-proton density is extracted by studying transitions to 8/sup +/ states in these nuclei. The radii are consistently larger than a value determined in a magnetic electron scattering experiment on /sup 93/Nb. A qualitative discussion of the ground state occupation of the ..pi..1g/sub 9/2/ orbit based on the transition amplitudes to the 8/sup +/ states is given.

1985-09-01

279

Biopolymer system for permeability modification in porous media  

Energy Technology Data Exchange (ETDEWEB)

New technologies are needed to reduce the current high rate of well abandonment. Improved sweep efficiency, reservoir conformance, and permeability modification can have a significant impact on oil recovery processes. Microorganisms can be used to selectively plug high-permeability zones to improve sweep efficiency and impart conformance control. Studies of a promising microbial system for polymer production were conducted to evaluate reservoir conditions in which this system would be effective. Factors which can affect microbial growth and polymer production include salinity, pH, temperature, divalent ions, presence of residual oil, and rock matrix. Flask tests and coreflooding experiments were conducted to optimize and evaluate the effectiveness of this system. Nuclear magnetic resonance imaging (NMRI) was used to visualize microbial polymer production in porous media. Changes in fluid distribution within the pore system of the core were ...

1995-12-31

280

Aurivillius phases of PbBi4Ti4O15 doped with Mn3+ synthesized by molten salt technique: Structure, dielectric, and magnetic properties  

International Nuclear Information System (INIS)

Doping of manganese (Mn3+/Mn4+) into the Aurivillius phase Pb1-xBi4+xTi4-xMnxO15 was carried out using the molten salt technique for various Mn concentrations (x=0, 0.2, 0.4, 0.6, 0.8, and 1). Single phase samples could be obtained in the composition range with x up to 0.6 as confirmed by X-ray and neutron diffraction analysis. Dielectric measurements show a peak at 801, 803, 813 and 850 K for samples with x=0, 0.2, 0.4, and 0.6, respectively, related to the ferroelectric transition temperature (Tc). The main contribution of the in-plane polarization for x?0.2 which was calculated from the atomic positions obtained by the structure analysis is the dipole moment in the Ti(1)O6 layer; however, for x?0.4 the polarization originates from the dipole moment in the Ti(2)O6 layer. Mn doping in the Pb1-xBi4+xTi4-xMnxO15 does not show any long range magnetic ordering. -- Graphical abstract: The dipole moment of TiO6 dependence of x in ...

2011-05-01

281

NASA TECH BRIEF  

Science.gov (United States)

Magnetic Forming Studies. The use of transient high magnetic-field devices has made possible the generation of very large accurately ...

283

Magnetic properties of single crystalline RE_2PdSi_3 intermetallic compounds  

International Nuclear Information System (INIS)

... susceptibility magnetization magnetoresistance monocrystals order-disorder

284

Finite Element Analysis of Magnetoelastic Plate Problems.  

Science.gov (United States)

... in the design of such devices as fusion reactors, magnetohydrodynamic generators, magnetically levitated vehicles, magnetic forming devices, and ...

1981-08-01

285

Design of a kW, DC Magnetically Contained Electrothermal ...  

Science.gov (United States)

... magnetic containment field lines which is zero on the center line of the toroidal containment tube and increases in magnitude with ...

1988-07-01

286

An investigation of the decoupling effects in a magnetic forming beryllium coil assembly.  

Science.gov (United States)

Decoupling force exerted by magnetic forming Be coil assembly on metallic plate during forming

1968-01-01

288

Structure analysis of ferrite in deformed pearlitic steel by means of X-ray diffraction method with synchrotron radiation  

Energy Technology Data Exchange (ETDEWEB)

Structure of ferrite in drawn pearlitic steel containing 0.9 mass% C was investigated with X-ray diffraction technique using synchrotron radiation. In the detailed analysis of diffraction peaks of ferrite during the drawing process, it was experimentally revealed that the transformation of ferrite from bcc to bct due to the supersaturation of carbon in ferrite of heavily drawn pearlitic steel.

2004-07-15

289

Structure analysis of ferrite in deformed pearlitic steel by means of X-ray diffraction method with synchrotron radiation  

International Nuclear Information System (INIS)

Structure of ferrite in drawn pearlitic steel containing 0.9 mass% C was investigated with X-ray diffraction technique using synchrotron radiation. In the detailed analysis of diffraction peaks of ferrite during the drawing process, it was experimentally revealed that the transformation of ferrite from bcc to bct due to the supersaturation of carbon in ferrite of heavily drawn pearlitic steel.

2004-07-01

290

Reflective diffraction grating  

Energy Technology Data Exchange (ETDEWEB)

Reflective diffraction grating. A focused ion beam (FIB) micromilling apparatus is used to store color images in a durable medium by milling away portions of the surface of the medium to produce a reflective diffraction grating with blazed pits. The images are retrieved by exposing the surface of the grating to polychromatic light from a particular incident bearing and observing the light reflected by the surface from specified reception bearing.

2003-06-24

291

Null field method in wave diffraction problems  

British Library Electronic Table of Contents (United Kingdom)

Diffraction by an impermeable scatterer in ?3 with a Dirichlet boundary condition is considered. It is shown that the null field equation is equivalent to the original diffraction problem. The general theoretical constructions are illustrated by analyzing the excitation of a sphere by a point source. The evolution of the residual of the null field equation as the scatterer surface is approached by an auxiliary surface is estimated.

2011-01-01

292

Progress of magnetic-suspension systems and magnetic bearings in the USSR  

International Nuclear Information System (INIS)

This paper traces the development and progress of magnetic suspension systems and magnetic bearings in the USSR. The paper describes magnetic bearings for turbomachines, magnetic suspension systems for vibration isolation, some special measuring devices, wind tunnels, and other applications. The design, principles of operation, and dynamic characteristics of the system are presented.

1992-05-01

293

International Symposium on Magnetic Suspension Technology. Part 2  

International Nuclear Information System (INIS)

In order to examine the state of technology of all areas of magnetic suspension and to review related recent developments in sensors and controls approaches, superconducting magnet technology, and design/implementation practices, a symposium was held. The proceedings are presented. The sessions covered the areas of bearings, sensors and controls, microgravity and vibration isolation, superconductivity, manufacturing applications, wind tunnel magnetic suspension systems, magnetically levitated trains (MAGLEV), space applications, and large gap magnetic suspension systems.

1991-08-19

294

Equatorial scintillation model. Technical report, 1 February 1983-30 April 1985  

Energy Technology Data Exchange (ETDEWEB)

Radiowave scintillation in the presence of natural and/or high-altitude nuclear disturbances has the potential to disrupt numerous transionospheric radio and radar systems. This report develops a model characterizing the plasma-density irregularities that produce scintillation in the naturally disturbed equatorial F layer. The model is incorporated into Program WBMOD along with subroutines for computing both link geometry and scintillation indices, the latter by means of phase screen diffraction theory. The model is based on similarly extensive analysis of wideband data from two equatorial stations. It describes irregularities at an effective height of 350 km that are isotropic across the geomagnetic field and elongated by a factor of 50 along the field and whose one-dimensional spatial power spectrum obeys a single-regime power law with a (negative) spectral index of 1.5. The height-integrated spectral strength of the irregularities is modeled as a function of ...

1985-09-30

295

Application of Bayer red mud for iron recovery and building material production from alumosilicate residues  

Energy Technology Data Exchange (ETDEWEB)

Red mud is a solid waste produced in the process of alumina extraction from bauxite. In this paper, recovery iron from Bayer red mud was studied with direct reduction roasting process followed by magnetic separation, and then building materials were prepared from alumosilicate residues. After analysis of chemical composition and crystalline phase, the effects of different parameters on recovery efficiency of iron were carried out. The optimum reaction parameters were proposed as the following: ratio of carbon powder: red mud at 18:100, ratio of additives: red mud at 6:100, roasting at 1300 deg. C for 110 min. With these optimum parameters, total content of iron in concentrated materials was 88.77%, metallization ratio of 97.69% and recovery ratio of 81.40%. Then brick specimens were prepared with alumosilicate residues and hydrated lime. Mean compressive strength of specimens was 24.10 MPa. It was indicated that main mineral phase transformed from nepheline ...

2009-01-15

296

The Pamela Cosmic Ray Space Observatory: Detector, Objectives and First Results  

CERN Document Server

PAMELA is a satellite borne experiment designed to study with great accuracy cosmic rays of galactic, solar, and trapped nature in a wide energy range (protons: 80 MeV-700 GeV, electrons 50 MeV-400 GeV). Main objective is the study of the antimatter component: antiprotons (80 MeV-190 GeV), positrons (50 MeV-270 GeV) and search for antimatter with a precision of the order of $10^{-8}$). The experiment, housed on board the Russian Resurs-DK1 satellite, was launched on June, 15 2006 in a $350\\times 600 km$ orbit with an inclination of 70 degrees. The detector is composed of a series of scintillator counters arranged at the extremities of a permanent magnet spectrometer to provide charge, Time-of-Flight and rigidity information. Lepton/hadron identification is performed by a Silicon-Tungsten calorimeter and a Neutron detector placed at the bottom of the device. An Anticounter system is used offline to reject false triggers ...

2009-01-01

297

Preshock desensitization of PBX explosives  

Energy Technology Data Exchange (ETDEWEB)

Preshocking delays initiation of PBX-9404 and PBX-9501, relative to unshocked material. In PBX-9404 preshock experiments, a first shock of 2.3 GPa was followed 0.65 {mu}s later by a second shock of 5.6 GPa. In PBX-9501, a preshock of 2.8 GPa and 0.32 us duration was followed by an initiating shock of 6.0 GPA. Both PBX explosives show clear desensitization while the preshock persists. In PBX-9404, initiation of detonation occurs nearly as anticipated for the material, after coalescence of the preshock and main shock into a single wave. Multiple embedded magnetic gauges were used to measure the shock histories. Our data indicates a slightly longer run to detonation than expected, even though a single wave is initiating the material. A slight stress reduction at coalescence, as required by the shock dynamics, may be responsible for the overrun. A reactive waste is clearly evident while the preshock persists. The long run to detonation indicates ...

1993-08-01

298

Paul Trap Simulator Experiment to Model Intense Beam Propagation in Alternating-gradient Transport Systems  

Energy Technology Data Exchange (ETDEWEB)

The results presented here demonstrate that the Paul Trap Simulator Experiment (PTSX) simulates the propagation of intense charged particle beams over distances of many kilometers through magnetic alternating-gradient (AG) transport systems by making use of the similarity between the transverse dynamics of particles in the two systems. Plasmas have been trapped that correspond to normalized intensity parameters s = wp2 (0)/2wq2 * 0.8, where wp(r) is the plasmas frequency and wq is the average transverse focusing frequency in the smooth-focusing approximation. The measured root-mean-squared (RMS) radius of the beam is consistent with a model, equally applicable to both PTSX and AG systems that balances the average inward confining force against the outward pressure-gradient and space-charge forces. The PTSX device confines one-component cesium ion plasmas for hundreds of milliseconds, which is equivalent to over 10 km of beam propagation.

2004-01-29

299

Measurement of the antiproton/proton ratio at few-TeV energies with the ARGO-YBJ experiment  

CERN Document Server

Cosmic ray antiprotons provide an important probe for the study of cosmic-ray propagation in the interstellar space and to investigate the existence of Galactic dark matter. Cosmic rays are hampered by the Moon, therefore a deficit of cosmic rays in its direction is expected (the so-called "Moon shadow"). The Earth-Moon system acts as a magnetic spectrometer. In fact, due to the geomagnetic field the center of the Moon shifts westward by an amount depending on the primary cosmic ray energy. Paths of primary antiprotons are therefore deflected in an opposite sense in their way to the Earth. This effect allows, in principle, the search of antiparticles in the opposite direction of the observed Moon shadow. The ARGO-YBJ experiment, in stable data taking since November 2007 with an energy threshold of a few hundreds of GeV, is observing the Moon shadow with high statistical significance. Using about 1 year data, an upper limit of the antip/p flux ...

2009-01-01

300

High voltage high brightness electron accelerator with MITL voltage adder coupled to foilless diode  

International Nuclear Information System (INIS)

The design and analysis of a high brightness electron beam experiment under construction at Sandia National Laboratory is presented. The beam energy is 12 MeV, the current 35 endash 40 kA, the rms radius 0.5 mm, and the pulse duration FWHM 40 ns. The accelerator is SABRE [J. Corley, J. A. Alexander, P. J. Pankuch, C. E. Heath, D. L. Johnson, J. J. Ramirez, and G. J. Denison, in Proceedings of the Eighth International IEEE Pulsed Power Conference, San Diego, California, 1991 (IEEE, New York, 1991), p. 920], a pulsed inductive voltage adder, and the electron source is a magnetically immersed foilless diode. This experiment has as its goal to stretch the technology to the edge and produce the highest possible electron current in a submillimiter radius beam. copyright 1996 American Institute of Physics.

1995-10-13

301

Eddy current inspection of superconducting cable during manufacturing  

Energy Technology Data Exchange (ETDEWEB)

The downstream failure of cable during winding, insulating, coil winding, and coil assembly is a significant issue in magnet production. The impact of these failures are costly both financially, and from the time to recover from this downstream failure. The current approach to cabling has been to visually inspect the cable for any gross defects during cabling. To date this has been effective in finding small defects such as crossovers for example, which drastically reduce the mechanical integrity of the strand, and thus the cable itself. But because of the large volume of cable which will be manufactured an automated flaw detection system which can inspect the cable and detect these type of defects will be needed. We have recently done an on-line experiment using an Eddy current system, and specialized Eddy current probes to inspect cable during manufacturing. We will present the results of our inspection demonstrating detection of crossovers, ...

1992-03-01

302

Eddy current inspection of superconducting cable during manufacturing  

International Nuclear Information System (INIS)

The downstream failure of cable during winding, insulating, coil winding, and coil assembly is a significant issue in magnet production. The impact of these failures is costly both financially and because of the time needed to recover from them. The current approach to cabling has been to visually inspect the cable for any gross defects during cabling. To date this has been effective in finding small defects such as crossovers, which drastically reduce the mechanical integrity of the strand and thus of the cable itself. But because of the large volume of cable that will be manufactured, an automated flaw detection system that can inspect the cable and detect these types of defects will be needed. We have recently done an on-line experiment using an Eddy current system and specialized Eddy current probes to inspect cable during manufacturing. We will present the results of our inspection, demonstrating detection of crossovers and cold welds. ...

1992-03-04

303

Consideration of some fundamental erosion processes encountered in hypervelocity electromagnetic propulsion  

Energy Technology Data Exchange (ETDEWEB)

Experimental and theoretical research has been conducted jointly at the Livermore and Los Alamos National laboratories on dc electromagnetic railgun Lorentz accelerators. Pellets weighing a few grams to tens of grams have been launched at velocities up to better than 11 km/s. The research is addressed to attaining repeated launches of samples at hypervelocity in target impact experiments. In these experiments, shock-induced pressures in the tens of megabars range are obtained for high pressure equation-of-state research. Primary energy sources of the order of several hundred kJ to a MJ and induction currents of the order of 1 or more MA are necessary for these launches. Erosion and deformation of the conductor rails and the accelerated sample material are continuing problems. The heating, stress, and erosion resulting from simultaneous imposition of rail induction current, dense plasma (armature) interaction, current distribution, ...

1982-09-30

304

A superconducting solenoidal spectrometer for a balloon-borne experiment  

Energy Technology Data Exchange (ETDEWEB)

The BESS detector is a new type of balloon-borne spectrometer which utilizes various technologies recently developed for collider experiments. The principal scientific objectives include a measurement of cosmic-ray antiproton spectrum, search for anti-nuclei in cosmic radiation, and precise measurements of cosmic-ray primaries. A thin superconducting solenoidal coil produces a uniform magnetic field of 1 T. Cylindrical drift chambers are located inside and outside the coil and perform continuous tracking. The momentum resolution is 0.5% at 1 GeV/c. i.e., the maximum detectable rigidity is 200 GV. Scintillation counter hodoscopes, placed above and below the solenoid, provide timing and dE/dx measurements and trigger generation. The timing resolution is 80 ps/counter. This cylindrical configuration achieves a large geometrical acceptance of 0.35 m{sup 2} sr which is essential to detect rare cosmic-ray particles. In order to cope with high trigger ...

2000-03-21

305

A new measurement of the antiproton-to-proton flux ratio up to 100 GeV in the cosmic radiation  

CERN Document Server

A new measurement of the cosmic ray antiproton-to-proton flux ratio between 1 and 100 GeV is presented. The results were obtained with the PAMELA experiment, which was launched into low-earth orbit on-board the Resurs-DK1 satellite on June 15th 2006. PAMELA is equipped with a silicon-microstrip magnetic spectrometer and a silicon-tungsten imaging calorimeter and has been collecting data since July 2006. During 500 days of data collection a total of about 1000 antiprotons have been identified, including 100 above an energy of 20 GeV. The high-energy results are a ten-fold improvement in statistics with respect to all previously published data. The antiproton-to-proton flux ratio increases smoothly with energy up to about 10 GeV, in agreement with previous experiments, and then levels off. The data follow the trend expected from secondary production calculations and significantly constrain contributions from exotic sources, ...

2008-01-01

306

Self-consistent full-potential linearized-augmented-plane-wave local-density electronic-structure studies of magnetism and superconductivity in C15 compounds: ZrZn_2 and ZrV_2  

International Nuclear Information System (INIS)

The electronic structure and properties of the cubic Laves phase (C15) compounds ZrZn_2 and ZrV_2 have been determined using our all-electron full-potential linearized-augmented-plane-wave (FLAPW) method for bulk solids. The computations were performed in two stages: (i) self-consistent warped muffin tin and (ii) self-consistent full potential. Spin-orbit coupling was included after either stage. The effects of the inclusion of the nonspherical terms inside the muffin tins on the eigenvalues is found to be small (of order 1 mRy). However, due to the fact that some of the bands near the Fermi level are flat, this effect leads to a much higher value of the density of states at E/sub F/ in ZnZr_2. The most important difference between the materials ZrZn_2 and ZrV_2 is the position of the d bands derived from the Zr and V atoms. Consequently, these materials have completely different Fermi surfaces. We have investigated the magnetic properties of these compounds by ...

307

Self-consistent full-potential linearized-augmented-plane-wave local-density electronic-structure studies of magnetism and superconductivity in C15 compounds: ZrZn/sub 2/ and ZrV/sub 2/  

Energy Technology Data Exchange (ETDEWEB)

The electronic structure and properties of the cubic Laves phase (C15) compounds ZrZn/sub 2/ and ZrV/sub 2/ have been determined using our all-electron full-potential linearized-augmented-plane-wave (FLAPW) method for bulk solids. The computations were performed in two stages: (i) self-consistent warped muffin tin and (ii) self-consistent full potential. Spin-orbit coupling was included after either stage. The effects of the inclusion of the nonspherical terms inside the muffin tins on the eigenvalues is found to be small (of order 1 mRy). However, due to the fact that some of the bands near the Fermi level are flat, this effect leads to a much higher value of the density of states at E/sub F/ in ZnZr/sub 2/. The most important difference between the materials ZrZn/sub 2/ and ZrV/sub 2/ is the position of the d bands derived from the Zr and V atoms. Consequently, these materials have completely different Fermi surfaces. We have investigated the magnetic properties ...

1988-03-01

308

Nonaqueous synthesis of metal oxide nanoparticles: Short review and doped titanium dioxide as case study for the preparation of transition metal-doped oxide nanoparticles  

Science.gov (United States)

The liquid-phase synthesis of metal oxide nanoparticles in organic solvents under exclusion of water is nowadays a well-established alternative to aqueous sol-gel chemistry. In this article, we highlight some of the advantages of these routes based on selected examples. The first part reviews some recent developments in the synthesis of ternary metal oxide nanoparticles by surfactant-free nonaqueous sol-gel routes, followed by the discussion of the morphology-controlled synthesis of lanthanum hydroxide nanoparticles, and the presentation of structural peculiarities of manganese oxide nanoparticles with an ordered Mn vacancy superstructure. These examples show that nonaqueous systems, on the one hand, allow the preparation of compositionally complex oxides, and, on the other hand, make use of the organic components (initially present or formed in situ) in the reaction mixture to tailor the morphology. Furthermore, obviously even the crystal structure can differ from the corresponding ...

2008-07-15

309

NMR studies of the partially disordered state in a triangular antiferromagnet UNi_4B  

International Nuclear Information System (INIS)

A triangular antiferromagnet UNi_4B experiences a partially disordered state, in which two-thirds of U 5f moments order in a vertex-like structure and one-third of U 5f moments remain paramagnetic. Magnetization and NMR measurements of UNi_4B have been performed to study the dynamical properties of U magnetic moments in the partially disordered state. The value of the effective moment above T_N derived from the fitting of the Curie-Weiss law suggests a significant crystal field splitting and the Kondo effect. The Weiss temperature was also estimated to be -28 K, which suggests that the exchange interaction is antiferromagnetic. Furthermore, the exchange interaction estimated from the relaxation rate T_1"-"1 above 50 K is 18 K, which is close to the Weiss temperature. These results suggest that the dominant interactions between U moments are antiferromagnetic in the basal plane. The relaxation rate T_1"-"1 decreases abruptly ...

2007-04-11

310

Magnetic excitations in R_2PdSi_3 studied by inelastic neutron scattering  

International Nuclear Information System (INIS)

R_2PdSi_3 compounds have been found to exhibit rich magnetic phenomena arising from the interplay between RKKY interaction, crystal electric field effects and geometric frustration due to the derived hexagonal AlB_2 structure. The observed crystallographic superstructure further complicates the CEF level scheme. Inelastic neutron scattering measurements on single crystals of Tm_2PdSi_3 and Er_2PdSi_3 have been performed at the cold triple axis spectrometer PANDA in FRM-II. Both compounds order antiferromagnetically at T_N=7 K and 2.1 K respectively; Er_2PdSi_3 undergoes a second phase transition at T_2=2 K. Several low lying CEF excitations (below 10 meV) were observed. The intensity of the lowest excitation show strong directional dependence (in HK0 plane for Er_2PdSi_3 and in HHL plane for Tm_2PdSi_3), from which the details of the transitional matrix could be deduced. Measurements in magnetic fields up to 13 T show Zeeman splitting of the ...

2009-03-22

311

Design of a magnetic braking system  

International Nuclear Information System (INIS)

A non-contact method, using magnetic drag force principle, was proposed to design the braking systems to improve the shortcomings of the conventional braking systems. The extensive literature detailing all aspects of the magnetic braking is briefly reviewed, however little of this refers specifically to upright magnetic braking system, which is useful for industries. One of the major issues to design upright magnetic system is to find out the magnetic flux. The changing magnetic flux induces eddy currents in the conductor. These currents dissipate energy in the conductor and generate drag force to slow down the motion. Therefore, a finite element model is developed to analyze the phenomena of magnetic flux density when air gap and materials of track are varied. The verification shows the predicted magnetic flux is within ...

2006-09-01

312

Thermal annealing effect on optical properties of electrodeposited ZnO thin films  

Energy Technology Data Exchange (ETDEWEB)

ZnO thin films were electrodeposited in aqueous solution on gilded p-type Si wafer substrates. Thermal treatments were carried out on different films in Ar atmosphere at different temperatures, between 200 and 600 {sup 0}C. Surface morphology studies using scanning electron microscopy and atomic force microscopy show a smooth surface for an annealing temperature of 400 {sup 0}C with a roughness mean square value of about 15 nm and a precipitation of ZnO microcrystals on the deposit surface at 600 {sup 0}C. X-ray diffraction experiments reveal a decrease in the c-parameter value from 5.223 to 5.206 A after treatment at 600 {sup 0}C, due to the removal of hydrogen from the film. Raman spectroscopy analyses show an improvement in the crystal quality of the film and a decrease in the compressive stress inside the deposit. Photoluminescence observations reveal an important change in the UV emission band after annealing at 200 {sup 0}C. A visible ...

2008-10-07

313

Review of High Gain FELs  

Science.gov (United States)

For understanding on basic radiation mechanism of the high-gain FEL based on SASE, the author presents electron-crystal interpretation of FEL radiation. In the electron-crystal, electrons are localized at regularly spaced multi-layers, which represents micro-bunching, whose spacing is equal to the radiation wavelength, and the multi-layers are perpendicular to beam axis, thus, diffracted wave creates Bragg's spots in forward and backward directions. Due to the Doppler's effect, frequency of the back-scattered wave is up-converted, generates forwardly focused X-ray. The Bragg's effect contributes focusing the X-ray beam into a spot, thus peak power becomes extremely higher by factor of typically 107. This is the FEL radiation. As well known, the total numbers of scattered photons in Bragg's spots is equal to the total elastic scattering photons from the atoms contained in the crystal. Therefore, total power in the FEL laser is ...

2007-01-19

314

Optical Properties and Wave Propagation in Semiconductor-Based Two-Dimensional Photonic Crystals  

Energy Technology Data Exchange (ETDEWEB)

This work is a theoretical investigation on the physical properties of semiconductor-based two-dimensional photonic crystals, in particular for what concerns systems embedded in planar dielectric waveguides (GaAs/AlGaAs, GaInAsP/InP heterostructures, and self-standing membranes) or based on macro-porous silicon. The photonic-band structure of photonic crystals and photonic-crystal slabs is numerically computed and the associated light-line problem is discussed, which points to the issue of intrinsic out-of-lane diffraction losses for the photonic bands lying above the light line. The photonic states are then classified by the group theory formalism: each mode is related to an irreducible representation of the corresponding small point group. The optical properties are investigated by means of the scattering matrix method, which numerically implements a variable-angle-reflectance experiment; comparison with experiments is ...

2002-12-31

315

Seven years of operating experience with amorphous metal transformers  

Energy Technology Data Exchange (ETDEWEB)

Amorphous metals have an atomic structure resembling that of glass, and have high strength, toughness, and excellent magnetic properties for transformer applications. This type of metal has the potential to reduce the core losses of electromagnetic apparatus by 70-75% compared to the best grain-oriented silicon iron currently used. If all 4 million distribution transformers now in service in Canada were replaced by the more efficient amorphous units, it is estimated that over 5.25 billion kWh of energy could be saved annually. The experience of the General Electric (GE) Company and other researchers with operation of amorphous transformers is described. GE first tried operating amorphous metal transformers on a utility distribution system in April 1982. The shell-type cruciform design showed stable, low-loss performance over eight years of service. GE and the Electric Power Research Institute cooperated on manufacturing and installing 25 ...

1991-05-01

316

Nuclear magnetic resonance spectroscopy in biomedicine. Course organized by the Istituto Superiore di Sanita`. Marciana Marina (Isola d`Elba), September 18-23, 1995; Spettroscopia di risonanza magnetica nucleare in biomedicina. Corso organizzato dall`Istituto Superiore di Sanita`. Marciana Marina (Isola d`Elba), 18-23 settembre 1995  

Energy Technology Data Exchange (ETDEWEB)

Nuclear magnetic resonance is a powerful technique that can be used in a wide range of applications, such as the structural characterization of high molecular weight molecules, conformational studies on enzymes in solution, enzyme-substrate or DNA-protein interactions, monitoring of cell metabolism in vivo, and for diagnostic purposes, employing spectroscopic and imaging techniques. This course was organized in order to introduce the participants to the fundamentals of NMR spectroscopy, and offer practical advice on performing NMR experiments on cell systems, cell and tissue extracts and animal models. The main implications regarding human experiments were also discussed. Finally the quantification of information and the interpretation of data were considered with regard to the main nuclei observed. [Italiano] La risonanza magnetica nucleare e` una delle tecniche spettroscopiche che meglio risponde all`ampio spettro di ...

1997-12-01

317

Luminescent unit computerization to research spectral characteristics of fine film alkali halide crystal  

International Nuclear Information System (INIS)

The fundamental optical absorption of ion crystals characterizes the creation of different free low energetic electronic excitation (the excitons and electron-hole pairs), but their straight registration is not possible because of incommensurable big absorption factor of alkali halide monocrystals. So to registration the spectrums of alkali halide monocrystal very fine layers are necessary. We have received fine films of Nal and KCl in system of KCl-Nal-KCl, KCl-KI-KCl on the base of universal vacuum post VUP-4, VUP-5 by thermal evaporation. A unique spectral unit has been created For this on the basic the SDL-2 complex. Complex consists of radiator, systems of condensers, monochromators MDR-12 and MDR-23, receivers of radiation, controller by unit. Connect and control of monochromators by means of IBM-compatible computer has been created. Kinematics schemes of monochromators provide consequent removing on output slot of monochromatic radiation in operating range of each ...

318

The Daya Bay reactor neutrino experiment  

CERN Document Server

The Daya Bay reactor neutrino experiment

2008-01-01

319

Statistical Analysis of Designed Experiments  

CERN Document Server

Statistical Analysis of Designed Experiments

2010-01-01

320

Comparison and Physical Interpretation of MCNP and TART Neutron and Gamma Monte Carlo Shielding Calculations for a Heavy-Ion ICF System  

Energy Technology Data Exchange (ETDEWEB)

For heavy-ion beam driven inertial fusion ''liquid-protected'' reactor designs such as HYLIFE-II, a mixture of molten salts made of F{sup 10}, Li{sup -6}, Li{sup 7} and Be{sup 9} (called flibe) allows small chambers and final-focus magnets closer to the target with superconducting coils suffering higher radiation damage, though they can stand only a certain amount of energy deposited before quenching. This work has been primarily focusing on verifying that total energy deposited by fusion neutrons and induced gamma rays remain under such limit values and the final purpose is the optimization of the shielding of the magnetic lens system from the points of view of the geometrical configuration and of the physical nature of the materials adopted. The system is analyzed in terms of six geometrical models going from simplified up to much more realistic representations of a system of 192 beam lines, each focused by ...

2002-07-01

321

Experimental Study of Hypernuclei Electroproduction by High Precision Spectroscopy  

Energy Technology Data Exchange (ETDEWEB)

Jlab experiment E01-011, carried out in 2005 in JLab Hall C, is the second generation of the hypernuclear spectroscopy experiments by the (e,e{prime}K{sup +}) reaction. The (e,e{prime}K{sup +}) reaction is complimentary to the associated production reactions (K{sup -},{pi}{sup -}), ({pi}{sup +},K{sup +}) since, due to a larger momentum transfer to a hyperon, excitations of both spin-non-flip and spin-flip states are possible. The experiment uses high quality and continuous primary electron beam to produce neutron rich hypernuclei on various targets by the electroproduction. The experimental setup consists of splitter magnet, high resolution kaon spectrometer (HKS) and electron spectrometer (Enge) implemented in new configuration, the so called 'Tilt Method'. Production data was taken on multiple targets: CH{sub 2}, {sup 6}Li, {sup 7}Li, {sup 9}Be, {sup 10}B, {sup 12}C and {sup 28}Si. ...

2009-12-01

322

Chemistry of transuranium elements and compounds  

International Nuclear Information System (INIS)

Studies are made in this program to enhance our understanding of the role of 5f electrons in chemical bonding. Most of our studies on the macroscopic scale emphasize certain isotopes available from the National Transplutonium Production Program centered at HFIR/TRU -namely, _9_6"2"4"8Cm, _9_7"2"4"9Bk, _9_8"2"4"9Cf, _9_9"2"5"3Es, and _9_9"2"5"4Es. Particular classes of compounds, such as hydrides, chalcogenides, and pnictides are often selected for study on the basis of their utility in bringing out significant chemical differences between the lanthanides and the actinides. High temperature/high pressure experiments on actinide metals and compounds reveal characteristics about the degree of 5f electron localization as a function of atomic number in the series. Magnetic properties of metals and compounds are investigated using ultra-sensitive methods and hydration numbers of ions in solution are investigated by neutron scattering at HFIR. As a ...

1986-05-01

323

Magnetic fluctuation measurement in Sino United Spherical Tokamak plasma  

International Nuclear Information System (INIS)

To investigate the magnetic fluctuations and for further transport study, the poloidal and radial magnetic field measurement is conducted on the Sino United Spherical Tokamak (SUNIST). Auto-power spectral density indicates that the magnetic fluctuation energy mainly concentrates in the frequency region lower than 10 kHz. The magnetic field oscillations, which are characterized by harmonic frequencies of 40 kHz, are observed in the scrape-off layer; by contrast, in the plasma core, the magnetic fluctuations are of Gaussian type. The time-frequency profiles show that the poloidal magnetic fluctuations are temporally intermittent. The autocorrelation calculation indicates that the fluctuations in decorrelation time vary between the core and the edge. (authors)

2007-07-01

324

Hydration of swelling clay and bacteria interaction. An experimental in situ reaction study; Hydratation des argiles gonflantes et influence des bacteries. Etude experimentale de reaction in situ  

Energy Technology Data Exchange (ETDEWEB)

This study reports on the physical-chemical behaviour of swelling di-octahedral clays (smectites) and their interaction with aqueous solutions and bacteria (Shewanella putrefaciens). Experimental results are presented for compacted clays, hydrated under confined volume conditions, using a new type of reaction-cell (the 'wet-cell' of Warr and Hoffman, 2004) that was designed for in situ X-ray diffraction (XRD) measurement. For comparison, dispersed clay systems were studied using standard batch solutions subjected to varying degrees of agitation. The combination of time-dependent in situ XRD measurements with gravimetric measurements and calculated diffraction patterns using the CALCMIX software (Plancon and Drits, 1999) allowed to successful quantification of the dynamics of water uptake and storage. This analytical procedure combined with published water vapour adsorption data enabled determination of the abundance of ...

2008-01-15

325

Mapping Strain in Nanocrystalline Nitinol: an X-ray Diffraction Method (SULI paper)  

Energy Technology Data Exchange (ETDEWEB)

Understanding the mechanical properties of biomedical devices is critical in predicting and preventing their failure in the body. Such knowledge is essential, for example, in the design of biomedical stents, which must undergo repeated strain over their ten year lifetimes without breaking. Computational models are used to predict mechanical response of a device, but these models are not complete; there are significant deviations from the predictions, especially when devices are subjected to repeated multi-axial loads. Improving these models requires comparisons with actual measurements of strained nitinol. Local measurements of the full strain tensor can be made using X-ray diffraction techniques, but they are currently limited to materials whose grain size is larger than the X-ray beam size or require several diffraction patterns produced by rotation of the sample. Nitinol stents are nanocrystalline, with grains smaller than any available ...

2006-01-04

326

Three-dimensional simulation study of compact toroid plasmoid injection into magnetized plasmas  

Energy Technology Data Exchange (ETDEWEB)

Three-dimensional dynamics of a compact toroid (CT) plasmoid, which is injected into a magnetized target plasma region is investigated by using magnetohydrodynamic (MHD) numerical simulations. It is found that the process of the CT penetration into this region is much more complicated than what has been analyzed so far by using a conducting sphere (CS) model. The injected CT suffers from a tilting instability, which grows with the similar time scale as the CT penetration. The instability is accompanied by magnetic reconnection between the CT magnetic field and the target magnetic field, which disrupts the magnetic configuration of the CT. Magnetic reconnection plays a role to supply the high density plasma initially confined in the CT magnetic field into the target region. Also, the penetration depth of the CT high density plasma is ...

1999-04-01

327

Magnetic properties of materials  

Energy Technology Data Exchange (ETDEWEB)

A number of interactions between magnetic fields and matter is reviewed. The resulting forces range in magnitude from the very large, obtained in high-energy fields, to the weak ones caused by the magnetostriction of ferromagnets. The fundamentals of these interactions are highlighted, and the examples discussed are forces on dipoles, particle alignment, magnetostrictive forces, magnetic forming, magnetic stirring, levitation melting, and magnetic pulsing of tool steels. (orig.)

2000-08-15

328

Magnetic flocculation and filtration  

Energy Technology Data Exchange (ETDEWEB)

A model is available in predicting flocculation frequencies between particles of various properties under the influence of a magnetic field. This model provides a basic understanding of fundamental phenomena, such as particle-particle and particle-collector interactions, occurring in HGMF (high gradient magnetic field), and will be extended to describe experimental data of particle flocculation and filtration and predict the performance of high- gradient magnetic filters. It is also expected that this model will eventually lead to a tool for design and optimization of magnetic filters for environmental, metallurgical, biochemical, and other applications.

1996-10-01

329

Transformation of the ATOMKI-ECRIS into a Plasma Device  

International Nuclear Information System (INIS)

Complete text of publication follows. In order to extend the capabilities of the electron cyclotron resonance (ECR) ion source (ECRIS) of ATOMKI it has been transformed into a special plasma facility [1,2]. The transformation is reversible and was simply done by changing several main components of the ion source by new ones, namely: the hexapole magnet, the plasma chamber and the microwave source. The basic requirements of the transformation were: (1) most parts of the present ECRIS should be used in the new assembly in the same way and (2) the transformation time between the two operation modes should not be more than 2-3 days (in both directions). The following sub-systems are used identically in both configurations: solenoid coils, vacuum system, gas dosing system, ovens, probes. The extraction optics and beam transport system can also be used in the new configuration to check the components and charge-state of the plasma. A new, large, but unusually thin ...

2006-01-01

330

The effective longitudinal dielectric constant for plasmas in inhomogeneous magnetic fields  

Scientific Electronic Library Online (English)

Abstract in english We present a detailed derivation of the effective dielectric constant to be used in the dispersion relation for electrostatic waves in the case of a plasma immersed in a inhomogeneous magnetic field, with inhomogeneity perpendicular to the direction of the magnetic field.

2004-09-01

331

Magnetic mirror fusion systems: Characteristics and distinctive features  

Energy Technology Data Exchange (ETDEWEB)

A tutorial account is given of the main characteristics and distinctive features of conceptual magnetic fusion systems employing the magnetic mirror principle. These features are related to the potential advantages that mirror-based fusion systems may exhibit for the generation of economic fusion power.

1987-08-10

332

Magnetic fields of x-ray pulsars  

Energy Technology Data Exchange (ETDEWEB)

An analytic model of magnetic torques applied to an accreting neutron star is employed to evaluate the magnetic dipole moments of x-ray pulsars. A new type of close binary system containing a neutron star is suggested.

1982-09-01

333

Magnetic excitations studied with time-of-flight spectroscopy  

Energy Technology Data Exchange (ETDEWEB)

An introduction to time-of-flight neutron spectroscopy is presented in the context of the study of magnetic materials. Examples are taken from the class of rare earth and actinide magnetic materials known as `strongly correlated electron` systems. (author) 11 figs., 24 refs.

1996-11-01

334

Eddy Current Inspection of Mildly Ferromagnetic Tubing.  

Science.gov (United States)

The past decade has seen the development of eddy current probes for inspection of the mildly ferro-magnetic alloy Monel 400. Due to the rapid advances in permanent magnet technology similar probes have been upgraded to magnetically saturate, and hence ins...

1984-01-01

335

Active magnetic regenerator  

Energy Technology Data Exchange (ETDEWEB)

The disclosure is directed to an active magnetic regenerator apparatus and method. Brayton, Stirling, Ericsson, and Carnot cycles and the like may be utilized in an active magnetic regenerator to provide efficient refrigeration over relatively large temperature ranges.

1982-01-01

336

Effects of FIB milling and pre-straining on the microstructure of directionally solidified Mo pillars: a Laue diffraction analysis  

Energy Technology Data Exchange (ETDEWEB)

White beam Laue micro-diffraction was performed on directionally solidified, single-crystal Mo pillars in the as-grown state, after focused ion beam (FIB) milling and after pre-straining. The Laue diffraction peaks from the as-grown pillars are very sharp and show no broadening, similar to those from single-crystal Si wafers. Significant broadening and streaking of the peaks occurred after FIB milling and pre-straining, indicative of the damage these treatments induce in the nearly perfect crystal structure of the directionally solidified Mo pillars.

2010-05-01

337

Brain mechanisms supporting the modulation of pain by mindfulness meditation.  

Science.gov (United States)

The subjective experience of one's environment is constructed by interactions among sensory, cognitive, and affective processes. For centuries, meditation has been thought to influence such processes by enabling a nonevaluative representation of sensory events. To better understand how meditation influences the sensory experience, we used arterial spin labeling functional magnetic resonance imaging to assess the neural mechanisms by which mindfulness meditation influences pain in healthy human participants. After 4 d of mindfulness meditation training, meditating in the presence of noxious stimulation significantly reduced pain unpleasantness by 57% and pain intensity ratings by 40% when compared to rest. A two-factor repeated-measures ANOVA was used to identify interactions between meditation and pain-related brain activation. Meditation reduced pain-related activation of the contralateral primary somatosensory cortex. ...

2011-04-01

338

Nanocrystalline permanent magnets with enhanced properties  

International Nuclear Information System (INIS)

Parameters of permanent magnets result from the combination of intrinsic properties such as saturation magnetization, magnetic exchange, and magnetocrystalline energy, as well as microstructural parameters such as phase structure, grain size, and orientation. Reduction of grain size into nanocrystalline regime (#approx# 50 nm) leads to the enhanced remanence which derives from ferromagnetic exchange coupling between highly refined grains. In this study the fundamental phenomena, quantities, and structure parameters, which define nanophase permanent magnets are presented and discussed. The theoretical considerations are confronted with experimental data for nanocrystalline Sm-Fe-N type permanent magnets. (author)

2001-09-23

339

Transurethral Ultrasound Diffraction Tomography  

Science.gov (United States)

... [5] GT Gullberg, RH Huesman, DNG Roy, J. Qi and BW Reutter, Esti- mation of the parameter covariance matrix for a one-compartment cardiac ...

2007-03-01

341

Integrated Optics Interdigitated-Electrode Switches  

Science.gov (United States)

... thus can function as switches -6 ... Akkari, "Optical Channel Waveguide Switch and Coupler ... Wide-Band Guided Wave Acousto-Optic Bragg Diffraction ...

1989-12-31

342

Enhanced Reliability MEMS Deformable Mirrors for Space Imaging ...  

Science.gov (United States)

Sep 3, 2010 ... These higher-quality deformable mirrors will enable diffraction-limited performance for many space-based optical systems such as space-based ...

343

Collaborative Research and Development (CR&D). Delivery ...  

Science.gov (United States)

... 7 Page 11. Figure 5. Diffraction pattern shown a and ~ slip directions with the associated misalignment for single colonies of Ti6242 [2]. 8 Page 12. -- ...

2005-10-01

345

Rare earth metal rich magnesium compounds RE4NiMg (RE=Y, Pr-Nd, Sm, Gd-Tm, Lu)-Synthesis, structure, and hydrogenation behavior  

International Nuclear Information System (INIS)

The rare earth metal rich compounds RE4NiMg (RE=Y, Pr-Nd, Sm, Gd-Tm, Lu) were synthesized from the elements in sealed tantalum tubes in an induction furnace. All compounds were investigated by X-ray diffraction on powders and single crystals: Gd4RhIn type, space group F4-bar 3m, Z=16, a=1367.6(2) pm for Y4NiMg, a=1403.7(3) pm for Pr4NiMg, a=1400.7(1) pm for Nd4NiMg, a=1386.5(2) pm for Sm4NiMg, a=1376.1(2) pm for Gd4NiMg, a=1362.1(1) pm for Tb4NiMg, a=1355.1(2) pm for Dy4NiMg, a=1355.2(1) pm for Ho4NiMg, a=1354.3(2) pm for Er4NiMg, a=1342.9(3) pm for Tm4NiMg, and a=1336.7(3) pm for Lu4NiMg. The nickel atoms have trigonal prismatic rare earth coordination. These NiRE6 prisms are condensed via common edges to a three-dimensional network which leaves voids for Mg4 tetrahedra and the RE1 atoms which show only weak coordination to the nickel atoms. The single crystal data indicate two kinds of solid solutions. The RE1 positions reveal small RE1/Mg mixing and some ...

2009-02-01

346

Phase diagram of SrO-InO1.5-CoOx and a new compound Sr3In0.9Co1.1O6  

International Nuclear Information System (INIS)

Sr3In0.9Co1.1O6, isostructural to Ca3Co2O6, is revealed by the study of the phase relations in the system SrO-InO1.5-CoOx (1000 oC). The structure of Sr3In0.9Co1.1O6 is refined by the combination of powder X-ray and neutron diffraction. Sr3In0.9Co1.1O6 crystallizes in a trigonal lattice with the cell parameters a=b=9.59438(3) A, c=11.02172(4) A with the space group R-3c. Its structure possesses 1D (In/Co)O3 chains running along the c-axis constructed by alternating face-sharing CoO6 octahedra and (In0.9Co0.1)O6 trigonal prisms. The co-occupation of In3+ and Co3+ at the trigonal prismatic site is evidenced by elementary analysis and determined by the structure refinement. Sr3In0.9Co1.1O6 is paramagnetic, and the susceptibility is consistent with the occupation of Co3+ at 10% of the trigonal prismatic positions in a high spin state (HS, S=2). The HS Co3+ is well separated by diamagnetic CoO6 octahedra and InO6 trigonal prisms and shows a g factor of 2.0 in the ...

2011-04-01

347

Untitled - NASA Technical Report Server (NTRS)  

Science.gov (United States)

Principle advantages of magnetic forming for part manufacture appear to lie ... to be an area of great potential for the magnetic forming process. We have a ...

348

Symptoms of the musculoskeletal system and exposure to magnetic fields in an aluminium plant.  

UK PubMed Central (United Kingdom)

OBJECTIVE--The study was performed to examine the influence of the exposure to magnetic fields in the potrooms of an electrolysis plant on the occurrence of musculoskeletal symptoms among the employees....Full Text Available

1995-08-01

349

Possible observation of the coexistence of superconductivity and long-range magnetic order in NdRh_4B_4  

International Nuclear Information System (INIS)

The ternary rare earth compound NdRh_4B_4 has been studied by means of critical field, low temperature heat capacity, and static magnetic susceptibility measurements. Features in the upper critical field and heat capacity data at 1.31 K and 0.89 K suggest the occurrence of long-range magnetic order in the superconducting state. The temperature dependence of the static magnetic susceptibility follows a Curie-Weiss law with an effective magnetic moment #mu#sub(eff) = 3.58 +- 0.05 #mu#sub(B) and a Curie-Weiss temperature thetasub(p) = -6.2 +- 1.0 K between 20 K and room temperature. However, magnetization vs. applied magnetic field isotherms suggest the development of a ferromagnetic component in the Nd"3"+ magnetization at low temperatures. (author).

1979-01-01

350

PLASMA JET WELDING, COATING, AND CUTTING: AN ...  

Science.gov (United States)

... 31. New electric forming methods offer potentials for light metals; magnetic forming and plasma forming. ... 3, 25 Magnetic Forming ..... ...

1963-02-01

351

Ordered magnetic nanohole and antidot arrays prepared through replication from anodic alumina templates  

Energy Technology Data Exchange (ETDEWEB)

Highly ordered arrays of Ni nanoholes and Fe{sub 20}Ni{sub 80} antidots have been prepared, respectively, by replica/antireplica processing and sputtering techniques using nanoporous alumina membranes as templates. Geometrical characteristics as nanohole/antidot diameter, interpore distance and the overall hexagonal symmetry of arrays are controlled through the original templates. Experimental data on their hysteresis and magnetic domain structure have been taken by vibrating sample magnetometry and magnetic force microscopy, respectively. An analysis of the magnetization process, resulting magnetic anisotropy and magnetic domain structure is summarized considering the influence of those geometry aspects. In particular, the hexagonal symmetry and the density of nanohole/antidots determine the overall magnetic behavior, which is of interest in future high-density ...

2008-07-15

352

Ordered magnetic nanohole and antidot arrays prepared through replication from anodic alumina templates  

International Nuclear Information System (INIS)

Highly ordered arrays of Ni nanoholes and Fe20Ni80 antidots have been prepared, respectively, by replica/antireplica processing and sputtering techniques using nanoporous alumina membranes as templates. Geometrical characteristics as nanohole/antidot diameter, interpore distance and the overall hexagonal symmetry of arrays are controlled through the original templates. Experimental data on their hysteresis and magnetic domain structure have been taken by vibrating sample magnetometry and magnetic force microscopy, respectively. An analysis of the magnetization process, resulting magnetic anisotropy and magnetic domain structure is summarized considering the influence of those geometry aspects. In particular, the hexagonal symmetry and the density of nanohole/antidots determine the overall magnetic behavior, which is of interest in future high-density ...

2008-07-01

353

Mechanism of viscosity effect on magnetic island rotation  

Energy Technology Data Exchange (ETDEWEB)

It is shown that plasma viscosity does not influence the magnetic island rotation directly. Nevertheless, it leads to nonstationarity of the plasma velocity. This nonstationarity is the reason of the viscosity effect on island rotation. (author)

2000-04-01

354

Magnetic Properties of Ni Nanoparticles Embedded in ...  

Science.gov (United States)

... M(TH) in applied magnetic fields up to ± 7 T and for temperatures ranging from 2 to 300 K. The superparamagnetic (SPM) behavior of these metallic ...

2011-05-14

355

Localization of small magnets against a noisy background  

Science.gov (United States)

Effective localization of small magnets against a noisy, real world background can involve various methods to first identify the magnetic fields produced by the magnet of interest, then to filter out background noise, and then to analyze the available magnetic field data to localize the magnet. Here we discuss low cost techniques which allow localization of small magnets with field strengths in the milliGauss range against real world background fields in the range of hundreds of mG, which may be fluctuating by up to tens of mG. Such techniques allow magnet tracking to be used to localize catheters in place of more invasive and expensive methods, e.g. fluoroscopy, for a variety of applications, including drug infusion with peripherally inserted central catheters (PICCs), laser ablation (TMR, PTMR) and introduction of pacemaker leads.

2001-05-01

356

Hypoxia and Magnetic Therapy for Personnel Radiation Protection  

International Science & Technology Center (ISTC)

Development of Portable Normobaric Hypoxia and Pulsed Magnetic Field Firmware System for Enhancement of Radio- and Non-specific Resistance in Workers of Environmentally Hazardous Industries

357

Geometry effects in the pulsed magnetization of high-temperature superconductor bulk parts  

International Nuclear Information System (INIS)

The dynamic response of cylindrical and ring-shaped YBaCuO bulk parts to pulsed magnetic fields is calculated by using small sets of finite elements. Some comparisons with experimental results are provided, and they give confidence in the modelling of the superconducting properties. Transient magnetizations as a function of time and space as well as shapes and absolute values of trapped magnetic flux profiles are presented. The influence of the sample geometry is investigated for different millisecond pulsed magnetization processes. Results are reported for different radial thicknesses and heights, different pulse durations, peak magnetic fields and pulse sequences with and without stepwise cooling. Comparisons concerning the achievable trapped magnetic field and flux are made, and implications for the use of high-temperature superconductor bulk parts as ...

2005-02-01

358

Formulation development and evaluation of metronidazole magnetic nanosuspension as a magnetic-targeted and polymeric-controlled drug delivery system  

Energy Technology Data Exchange (ETDEWEB)

A nanosuspension of magnetically tagged metronidazole was developed by the solvent displacement method coupled with ultrasonication and was evaluated for its physicochemical properties. The drug release from metronidazole magnetic nanosuspension at pH 1.2 and 7.0 shows maximum correlation coefficient for zero order and Higuchi model, respectively. The anthelmintic activity of the formulated metronidazole magnetic nanosuspension was evaluated on Indian earthworms (Pheretima poi). Metronidazole magnetic nanosuspension at a dose of 10 and 50 mg/ml shortened by 31% and 34%, respectively, the mean time to death of the earthworms when compared against a non-magnetic metronidazole suspension. Thus, the developed metronidazole magnetic nanosuspension showed potent, controlled and targeted drug action and might be a good therapeutic avenue in combating infectious GI ...

2009-05-15

359

Evaluation of Commercial Magnetic Descalers.  

Science.gov (United States)

With the increased costs of maintaining boilers and chillers entrepreneurs around the country have offered magnetic and similar devices to facilities as viable alternatives to their maintenance program. This report gives a brief history of some of the pre...

1984-01-01

360

Develop Magnetic Coil Design and Manufacturing Capability.  

Science.gov (United States)

... design, and manufacturing knowledge have been acquired and used to develop an 'in-house' capability for the fabrication of magnetic forming coils ...

1974-11-01

362

CONTRACT: NAS 8-11811 DESIGN, DEVELOPMENT, MANUFACTURE, AND ...  

Science.gov (United States)

has been generally related to magnetic forming. One of the methods suggested was the following: A "pancake" magnetic coil is placed over a thin aluminum ...

363

Application of the grazing angle polarized neutron reflectometry to study the magnetism in thin films and stratified media  

Energy Technology Data Exchange (ETDEWEB)

From optical point of view and due to the magnetic interaction of the cold neutrons with the unpaired electron shell, magnetic materials hae a neutron spin-dependent refractive index n[sup +] [spin up] and n[sup -] [spin down]. Magnetic media such as Fe, Co and Ni react like birefringent uniaxial crystals in ordinary optica. n[sup +] and n[sup -] are the equivalent of the ordinary and extraordinary refractive indices. The specular reflection of spin polarized neutrons which is due to the discontinuity of the magnetic induction at the surface of the ferromagnet is a sensitive probe of surface and interface magnetism. We shall first give the background of the art of polarized neutron optics. Secondly, some recent examples from surface and interface magnetism will be given to illustrate the power of this technique such as the magnetic coupling ...

1992-12-01

364

Anisotropic forming of magnetic powders mixed with ultraviolet resin; Shigaisen koka jushi wo mochiita jisei funmatsu no haiko seikei  

Energy Technology Data Exchange (ETDEWEB)

For the purpose of solving the limitations such as shape and dimension for magnetic compact fabricated by conventional anisotropic forming under magnetic orienting field, the feasibility of a new magnetic forming process was studied. Ferrite powder mixed with UV resin was compacted in the die mold and followed by alignment under the magnetic field. Effects of viscosity of UV resin and forming condition on magnetic characteristics of the compact was investigated. Maximum degree of alignment for the ferrite powder reached to 0.826. It was predicted that the proposed method had make it possible to fabricate a high performance magnet having the anisotropic alignment of the magnetic powder. The UV resin is desirable to have low viscosity, good properties such as formability and configuration stability for the compact and also parting- ability ...

1999-01-15

365

An Advance in Superconducting Magnet Technology Opens the Door...  

Science.gov (United States)

magnet research at several national laboratories through its Advanced Accelerator Technology Program. The HEP Conductor Development Program, a collaboration among national...

2011-08-20

366

40th Anniversary of the First Proton-Proton Collisions in the CERN Intersecting Storage Rings (ISR)  

ScienceCinema

...and ...and ? ...and ...and and ...and sent to discuss results ...and the moment that ...and ...and ...and and it's a great pleasure to ...and ...and because ...and ...? and ...and ...and ...? and ...? yes yes and ...and ...techniques and ...those who don't know and and i ...and ...? and ...and ...and and ...and ...and ...and ...and january nineteen seventy one and ...and ...and ...ejected johnson ? and ...saw this and that ...and the ...and ...? and ...the problem of the following talks that and ...physics and ...um and finally ...and ...and ...disposal them but that's ...and and ...and ...and that's ...and ...and ...and ...and on the physics results by michael ...and ...and evolution of detectors ...and ...and ...and ...? folks and ...and all ...and and ...and the ...and ...and ...and ...and and ...and ...and ...would be a coffee and h ? and that ...and the physics still go to forgetfulness ...and the and website and ...give you some physicists and ...and ...and ...out what the ...

367

The effect of hydrogen peroxide solution on SO2 removal in the semidry flue gas desulfurization process.  

Science.gov (United States)

The present study attempts to use hydrogen peroxide solution to humidify Ca(OH)(2) particles to enhance the absorption of SO(2) to achieve higher removal efficiency and to solve the valuable reuse of the reaction product in the semidry flue gas desulfurization (FGD) process. Experiments were carried out to examine the effect of various operating parameters including hydrogen peroxide solution concentration, Ca/S molar ratio and approach to adiabatic saturation temperature on SO(2) removal efficiency in a laboratory scale spray reactor. The product samples were analyzed to obtain semi-quantitative measures of mineralogical composition by X-ray diffraction (XRD) with reference intensity ratio (RIR) method and the morphology of the samples was examined by scanning electron microscope (SEM). Compared with spraying water to humidify Ca(OH)(2), SO(2) removal efficiency was improved significantly by spraying hydrogen peroxide solution of 1-3 wt.% to ...

2009-04-24

368

Synthesis and photo-degradation application of WO3/TiO2 hollow spheres.  

Science.gov (United States)

A WO(3)/TiO(2) composite, hollow-sphere photocatalyst with average diameter of 320 nm and shell thickness of 50 nm was successfully prepared using a template method. UV-vis diffuse reflectance spectra illustrated that the main absorption edges of the WO(3)/TiO(2) hollow spheres were red-shifted compared to the TiO(2) hollow spheres, indicating an extension of light absorption into the visible region of the composite photocatalyst. The WO(3) and TiO(2) phases were confirmed by X-ray diffraction analysis. BET isotherms revealed that the specific surface area and average pore diameter of the hollow spheres were 40.95 m(2)/g and 19 nm, respectively. Photocatalytic experiments indicate that 78% MB was degraded by WO(3)/TiO(2) hollow spheres under visible light within 80 min. Under the same conditions, only 24% MB can be photodegraded by TiO(2). The photocatalytic mineralization of MB, catalyzed by TiO(2) and WO(3)/TiO(2), proceeded at a ...

2011-02-22

369

Research on laser welding of cast Ni-based superalloy K418 turbo disk and alloy steel 42CrMo shaft  

Energy Technology Data Exchange (ETDEWEB)

Exploratory experiments of laser welding cast Ni-based superalloy K418 turbo disk and alloy steel 42CrMo shaft were conducted. Microstructure of the welded seam was characterized by optical microscopy (OM), scanning electron microscopy (SEM), X-ray diffraction (XRD), energy-dispersive spectrometer (EDS). Mechanical properties of the welded seam were evaluated by microhardness and tensile strength testing. The corresponding mechanisms were discussed in detail. Results showed that the laser-welded seam had non-equilibrium solidified microstructures consisting of FeCr{sub 0.29}Ni{sub 0.16}C{sub 0.06} austenite solid solution dendrites as the dominant and some fine and dispersed Ni{sub 3}Al {gamma}' phase and Laves particles as well as little amount of MC short stick or particle-like carbides distributed in the interdendritic regions. The average microhardness of the welded seam was relatively uniform and lower than that of the base metal ...

2008-04-03

370

Research on laser welding of cast Ni-based superalloy K418 turbo disk and alloy steel 42CrMo shaft  

International Nuclear Information System (INIS)

Exploratory experiments of laser welding cast Ni-based superalloy K418 turbo disk and alloy steel 42CrMo shaft were conducted. Microstructure of the welded seam was characterized by optical microscopy (OM), scanning electron microscopy (SEM), X-ray diffraction (XRD), energy-dispersive spectrometer (EDS). Mechanical properties of the welded seam were evaluated by microhardness and tensile strength testing. The corresponding mechanisms were discussed in detail. Results showed that the laser-welded seam had non-equilibrium solidified microstructures consisting of FeCr_0_._2_9Ni_0_._1_6C_0_._0_6 austenite solid solution dendrites as the dominant and some fine and dispersed Ni_3Al #gamma#' phase and Laves particles as well as little amount of MC short stick or particle-like carbides distributed in the interdendritic regions. The average microhardness of the welded seam was relatively uniform and lower than that of the base metal due to partial ...

2008-04-03

371

Properties of dust particles sampled from windboxes of an iron ore sintering plant: Surface structures of unburned carbon  

Energy Technology Data Exchange (ETDEWEB)

Aiming to understand the formation mechanism of dioxins in the iron ore sintering process, dust samples obtained from some windboxes of a commercial iron ore sintering plant have been characterized with a powder X-ray diffraction (XRD), by the transmission electron microscope (TEM) equipped with an electron energy loss spectroscopy (EELS), and by the temperature-programmed desorption (TPD) and temperature-programmed oxidation (TPO) techniques. The elemental and XRD analyses reveal that the content of the Cl present in the samples ranges from 0.075 mass%-dry to 5.1 mass%-dry and tends to be higher at smaller dust particles, and that some of the Cl exists as KCl with the average crystalline size between 40 nm and 50 nm. Dust samples also contain a significant amount of unburned carbon, and the smallest dust particles, < 500 {mu}m, show the highest C contents in many cases and consist partly of C, K, and Cl elements. The TPD and TPO ...

2006-07-01

372

Processing of LiBH{sub 4} from its elements by ball milling method  

Energy Technology Data Exchange (ETDEWEB)

Investigations of alternative renewable energy resources continue, with many studies concentrating on hydrogen storage. However, there are a few problems such as storage, transportation, delivery to the user and usage safely, to be addressed to facilitate commercialization and wide usage of the hydrogen. The absorbed form within the metal hydrides seems to be the best solution of this problem. Since Li is the lightest metal, it has the advantage as the stored amount of hydrogen mass ratio. LiBH{sub 4} production process was investigated using elemental Li, B and H{sub 2}. Spex type ball milling with tungsten carbide, stainless steel and zirconia type vessels, was used to mix the different amount of Li and B under argon atmosphere. X-ray diffraction pattern demonstrated that the LiB was obtained. A system was designed to provide a hydrogen atmosphere of 60 bars to force hydrogen into the LiB structure. FTIR analysis strongly indicated the LiBH{sub 4} compound when ...

2008-11-15

373

Physical and electrochemical characterization of CdS hollow microspheres prepared by a novel template free solution phase method  

International Nuclear Information System (INIS)

Novel CdS hollow microspheres have been successfully synthesized via a facile template-free solution-phase reaction from cadmium nitrate and thioacetamide precursors. The morphology of CdS hollow microspheres depends strongly on the ratio between the precursors, cadmium nitrate to thioacetamide ratio. The physical properties of the hollow microspheres have systematically been studied by different characterization methods. The stoichiometry of the hollow microspheres studied by the energy dispersive X-ray diffraction spectroscopy confirmed that the synthesized CdS hollow microspheres are nearly stoichiometric bulk like CdS. The morphology of the hollow microspheres studied by high resolution scanning electron microscopy and transmission electron microscopy observations showed that the CdS hollow microspheres of the size of 2.5 ?m have hollow structure and are constructed by several nanoparticles of the size between 30 and 40 nm. The UV-visible diffuse reflectance ...

2010-12-15

374

In situ texture analysis under applied load  

International Nuclear Information System (INIS)

The in-situ measurement of a crystallographic texture is a special type of a non-destructive measurement, which need special equipments. Due to the high photon flux and the excellent brilliance high energetic synchrotron radiations are a fantastic tool particular in fast experimentation. Moreover, a high penetration power allows the investigation of standard tensile sample of the DIN-norm. A loading device with a power up to 20 kN was installed at the hard wiggler beamline BW5 (HASYLAB-DESY) to perform in-situ strain and in-situ texture analysis. Using 100keV X-rays one gets short wavelength so that a 2D image-plate detector offers a wide range of diffraction pattern within the first 10 degree in 2 theta. Thermal neutron is another radiation with a high penetration power, which is the standard method for global texture analysis of bulk samples. As an example rectangular extruded Mg- Az31 was investigated by an in-situ. tensile experiment. ...

375

Fabrication of zircon for disposition of weapons plutonium  

International Nuclear Information System (INIS)

This is the final report of a one-year, Laboratory-Directed Research and Development (LDRD) project at the Los Alamos National Laboratory (LANL). In an effort to address the problems of long term storage and nuclear waste minimization, zircon has been proposed as a host medium for plutonium and other actinides recovered from dismantled nuclear weapons. The objective of this work is to investigate the feasibility of large scale fabrication of Pu-bearing zircon. Since PuO_2 is thermodynamically less stable than ZrO_2, it is expected that the process parameters determined for synthesizing ZrSiO_4 (zircon) would be applicable to those for PuSiO_4 (Pu-zircon). Furthermore, since the foremost concern in plutonium processing is the potential for contamination release, this work emphasizes the development of process parameters, using zircon first, to anticipate potential material problems in the containment system for reaction mixtures during processing. Stoichiometric mixtures of ZrO_2 and ...

376

Dissimilar autogenous full penetration welding of superalloy K418 and 42CrMo steel by a high power CW Nd:YAG laser  

Energy Technology Data Exchange (ETDEWEB)

Experiments of autogenous laser full penetration welding between dissimilar cast Ni-based superalloy K418 and alloy steel 42CrMo flat plates with 3.5 mm thickness were conducted using a 3 kW continuous wave (CW) Nd:YAG laser. The influences of laser welding velocity, flow rate of side-blow shielding gas, defocusing distance were investigated. Microstructure of the welded seam was characterized by optical microscopy (OM), scanning electron microscopy (SEM) and X-ray diffraction (XRD) and energy dispersive spectrometer (EDS). Mechanical properties of the welded seam were evaluated by microhardness and tensile strength testing. Results show that high quality full penetration laser-welded joint can be obtained by optimizing the welding velocity, flow rate of shielding gas and defocusing distance. The laser-welded seam have non-equilibrium solidified microstructures consisting of {gamma}-FeCr{sub 0.29}Ni{sub 0.16}C{sub 0.06} austenite solid solution ...

2007-06-30

377

Dissimilar autogenous full penetration welding of superalloy K418 and 42CrMo steel by a high power CW Nd:YAG laser  

International Nuclear Information System (INIS)

Experiments of autogenous laser full penetration welding between dissimilar cast Ni-based superalloy K418 and alloy steel 42CrMo flat plates with 3.5 mm thickness were conducted using a 3 kW continuous wave (CW) Nd:YAG laser. The influences of laser welding velocity, flow rate of side-blow shielding gas, defocusing distance were investigated. Microstructure of the welded seam was characterized by optical microscopy (OM), scanning electron microscopy (SEM) and X-ray diffraction (XRD) and energy dispersive spectrometer (EDS). Mechanical properties of the welded seam were evaluated by microhardness and tensile strength testing. Results show that high quality full penetration laser-welded joint can be obtained by optimizing the welding velocity, flow rate of shielding gas and defocusing distance. The laser-welded seam have non-equilibrium solidified microstructures consisting of #gamma#-FeCr_0_._2_9Ni_0_._1_6C_0_._0_6 austenite solid solution ...

2007-06-30

378

Dissimilar autogenous full penetration welding of superalloy K418 and 42CrMo steel by a high power CW Nd:YAG laser  

Science.gov (United States)

Experiments of autogenous laser full penetration welding between dissimilar cast Ni-based superalloy K418 and alloy steel 42CrMo flat plates with 3.5 mm thickness were conducted using a 3 kW continuous wave (CW) Nd:YAG laser. The influences of laser welding velocity, flow rate of side-blow shielding gas, defocusing distance were investigated. Microstructure of the welded seam was characterized by optical microscopy (OM), scanning electron microscopy (SEM) and X-ray diffraction (XRD) and energy dispersive spectrometer (EDS). Mechanical properties of the welded seam were evaluated by microhardness and tensile strength testing. Results show that high quality full penetration laser-welded joint can be obtained by optimizing the welding velocity, flow rate of shielding gas and defocusing distance. The laser-welded seam have non-equilibrium solidified microstructures consisting of ?-FeCr0.29Ni0.16C0.06 austenite solid solution dendrites as the ...

2007-06-01

379

Two dimensional NMR and NMR relaxation studies of coal structure. Progress report, July 1, 1992--September 30, 1992  

Energy Technology Data Exchange (ETDEWEB)

This report covers the progress made on the title project for the project period. Four major areas of inquiry are being pursued. Advanced solid state NMR methods are being developed to assay the distribution of the various important functional groups that determine the reactivity of coals. Special attention is being paid to methods that are compatible with the very high magic angle sample spinning rates needed for operation at the high magnetic field strengths available today. Polarization inversion methods utilizing the difference in heat capacities of small groups of spins are particularly promising. Methods combining proton-proton spin diffusion with {sup 13}C CPMAS readout are being developed to determine the connectivity of functional groups in coals in a high sensitivity relay type of experiment. Additional work is aimed at delineating the role of methyl group rotation in the proton NMR relaxation behavior of coals.

1992-11-25

380

Seiberg duality and e+e- experiments  

Energy Technology Data Exchange (ETDEWEB)

Seiberg duality in supersymmetric gauge theories is the claim that two different theories describe the same physics in the infrared limit. However, one cannot easily work out physical quantities in strongly coupled theories and hence it has been difficult to compare the physics of the electric and magnetic theories. In order to gain more insight into the equivalence of two theories, we study the ''e{sup +}e{sup -}'' cross sections into ''hadrons'' for both theories in the superconformal window. We describe a technique which allows us to compute the cross sections exactly in the infrared limit. They are indeed equal in the low-energy limit and the equality is guaranteed because of the anomaly matching condition. The ultraviolet behavior of the total ''e{sup +}e{sup -}'' cross section is different for the two theories. We comment on proposed nonsupersymmetric ...

1998-10-02

381

Proton G{sub E}/G{sub M} from beam-target asymmetry  

Science.gov (United States)

The ratio of the proton's electric to magnetic form factor, G{sub E}/G{sub M}, can be extracted in elastic electron-proton scattering by measuring cross sections, beam-target asymmetry, or recoil polarization. Separate determinations of G{sub E}/G{sub M} by cross sections and recoil polarization observables disagree for Q{sup 2}>1 (GeV/c){sup 2}. Measurement by a third technique might uncover an unknown systematic error in either of the previous measurements. The beam-target asymmetry has been measured for elastic electron-proton scattering at Q{sup 2} = 1.51 (GeV/c){sup 2} for target spin orientation aligned perpendicular to the beam momentum direction. This is the largest Q{sup 2} at which G{sub E}/G{sub M} has been determined by a beam-target asymmetry experiment. The result, {mu}G{sub E}/G{sub M}=0.884{+-}0.027{+-}0.029, is compared to previous world data.

2006-09-15

382

Plasma dynamics in the PF-1000 device under full-scale energy storage: II. Fast electron and ion characteristics versus neutron emission parameters and gun optimization perspectives  

International Nuclear Information System (INIS)

Electron and ion beam dynamics of the PF-1000 facility were investigated for the first time at its upper energy limit (?1 MJ) in relation to neutron emission, the pinch's plasma ('target') characteristics and some other parameters with the help of a number of diagnostics with ns temporal resolution. Special attention was paid to the temporal and the spatial cross correlations of different phenomena. Results of these experiments are in favour of a neutron emission model based on ion beam-plasma interaction with three important features: (1) the plasma target is hot and confined during a few 'inertial confinement times'; (2) the ions of the main part of the beam are magnetized and entrapped around the pinch plasma target for a period longer than the characteristic time of the plasma inductive storage system and (3) ion-ion collisions (both fusion collisions, due to head-on impacts and Coulomb collisions) are responsible for neutron emission. ...

2007-06-21

383

Nuclear magnetic resonance spectroscopy in the structure elucidation and biosynthesis of natural products  

Energy Technology Data Exchange (ETDEWEB)

Examination of a chloroform extract of Dracaena loureiri Gagnep (Agavaceae), a Thia medicinal plant possessing antibacterial activity, has led to the isolation of fifteen flavenoids. The biogenic relationships among these flavenoids isolated were briefly discussed. Definition of the skeleton and the unambiguous assignment of all of the protons of the isolates was achieved through extensive 2D-homonuclear chemical shift correlation, nuclear Overhauser effect (NOE) difference spectroscopy and 2D-NOE experiments. The {sup 1}H and {sup 13}C NMR spectra of staurosporine, a potent biologically active agent from Streptomyces staurosporeus, were unambiguously assigned by using 2D homonuclear chemical shift correlation, NOE, {sup 1}H-detected heteronuclear multiple-quantum coherence via direct coupling and via multiple-bond coupling for resonance assignments of protonated and nonprotonated carbons, respectively. S. Staurosporeus was found to utilize endogenous and exogenous ...

1988-01-01

384

New real-time MR image-guided surgical robotic system for minimally invasive precision surgery  

Energy Technology Data Exchange (ETDEWEB)

To investigate the usefulness of a newly developed magnetic resonance (MR) image-guided surgical robotic system for minimally invasive laparoscopic surgery. The system consists of MR image guidance [interactive scan control (ISC) imaging, three-dimensional (3-D) navigation, and preoperative planning], an MR-compatible operating table, and an MR-compatible master-slave surgical manipulator that can enter the MR gantry. Using this system, we performed in vivo experiments with MR image-guided laparoscopic puncture on three pigs. We used a mimic tumor made of agarose gel and with a diameter of approximately 2 cm. All procedures were successfully performed. The operator only advanced the probe along the guidance device of the manipulator, which was adjusted on the basis of the preoperative plan, and punctured the target while maintaining the operative field using robotic forceps. The position of the probe was monitored continuously with 3-D ...

2008-04-15

385

NATIONAL HIGH MAGENTIC FIELD LABORATORY FEL INJECTOR DESIGN CONSIDERATION  

Energy Technology Data Exchange (ETDEWEB)

A Numerical study of beam dynamics was performed for two injector systems for the proposed National High Magnetic Field Laboratory at the Florida State University (FSU) Free Electron Laser (FEL) facility. The first considered a system consisting of a thermionic DC gun, two buncher cavities operated at 260 MHz and 1.3 GHz and two TESLA type cavities, and is very similar to the injector of the ELBE Radiation Source. The second system we studied uses a DC photogun (a copy of JLab FEL electron gun), one buncher cavity operated at 1.3 GHz and two TESLA type cavities. The study is based on PARMELA simulations and takes into account operational experience of both the JLab FEL and the Radiation Source ELBE. The simulations predict the second system will have a much smaller longitudinal emittance. For this reason the DC photo gun based injector is preferred for the proposed FSU FEL facility.

2007-06-25

386

Mechanism of adenylate kinase. Dose adenosine 5'-triphosphate bind to the adenosine 5'-monophosphate site  

Energy Technology Data Exchange (ETDEWEB)

Although the subtrate binding properties of adenylate kinase (AK) have been studied extensively by various biochemical and biophysical techniques, it remains controversial whether uncomplexed adenosine 5'-triphosphate (ATP) binds to the adenosine 5'-monophosphate (AMP) site of AK. The authors present two sets of experiments which argue against binding of ATP to the AMP site. (a) /sup 31/P nuclear magnetic resonance titration of ATP with AK indicated a 1:1 stoichiometry on the basis of changes in coupling constants and line widths. This ruled out binding of ATP to both sites. (b) ATP and MgATP were found to behave similarly by protecting AK from spontaneous inactivation while AMP showed only a small degree of protection. Such inactivation could also be protected or reversed by dithioerythritol and is most likely due to oxidation of sulfhydryl groups, one of which (cysteine-25) is located near the MgATP site. The results support ...

1987-10-06

387

Measurement of the Electron Affinities of Indium and Thallium  

Energy Technology Data Exchange (ETDEWEB)

The electron affinities of indium and thallium were measured in separate experiments using the laser-photodetachment electron spectroscopy technique. The measurements were performed at the University of Nevada, Reno. Negative ion beams of both indium and thallium were extracted from a cesium-sputter negative ion source, and mass analyzed using a 90{sup o} bending magnet. The negative ion beam of interest was then crossed at 90{sup o} with a photon beam from a cw 25-Watt Ar{sup +} laser. The resulting photoelectrons were energy analyzed with a 160{sup o} spherical-sector spectrometer. The electron affinity of In({sup 2}P{sub 1/2}) was determined to be 0.404 {+-} 0.009 eV and the electron affinity of thallium was determined to be 0.377 {+-} 0.013 eV. The fine-structure splittings in the ground states of the negative ions were also determined. The experimental measurements will be compared to several recent theoretical predictions.

1999-03-20

388

Large area electron beam pumped krypton fluoride laser amplifier  

International Nuclear Information System (INIS)

Nike is a recently completed multi-kilojoule krypton fluoride (KrF) laser that has been built to study the physics of direct drive inertial confinement fusion. This paper describes in detail both the pulsed power and optical performance of the largest amplifier in the Nike laser, the 60 cm amplifier. This is a double pass, double sided, electron beam-pumped system that amplifies the laser beam from an input of 50 J to an output of up to 5 kJ. It has an optical aperture of 60 cm x 60 cm and a gain length of 200 cm. The two electron beams are 60 cm high x 200 cm wide, have a voltage of 640 kV, a current of 540 kA, and a flat top power pulse duration of 250 ns. A 2 kG magnetic field is used to guide the beams and prevent self-pinching. Each electron beam is produced by its own Marx/pulse forming line system. The amplifier has been fully integrated into the Nike system and is used on a daily basis for laser-target experiments. copyright 1997 ...

389

Free electron laser  

International Nuclear Information System (INIS)

The present article outlines major features of the free electron laser (FEL) and reviews research and development of FEL. Relations among the oscillation frequency, electron beam parameters and wiggler parameters, the physical mechanism of amplification and the physical process of saturation are discussed to identify the difference between FEL and other lasers. The report also outlines techniques for accelerators which are used to generate high-quality, high-energy electron beams required for FEL experiments. Techniques to achieve a short wavelength, high output and high efficiency, and applications of FEL are also discussed. FEL consists of an electron accelerator, wiggler and optical resonator. In FEL, electron beams with a relativistic energy interact resonantly with an electromagnetic field to generate coherent electromagnetic waves. Unlike conventional lasers, FEL does not surfer from restrictions on its oscillation frequency associated with atomic, molecular ...

390

Extremely low frequency electric and magnetic fields and cancer: A literature review  

Energy Technology Data Exchange (ETDEWEB)

Epidemiologic studies suggest a weak link between occupational or residential exposure to extremely low frequency electromagnetic fields and cancer, especially tumors of the central nervous and hematopoietic systems. This report discusses these studies with reference to basic research on ELF EMF bioeffects relevant to cancer-promoting mechanisms. Many of the studies suggest a possible interaction of ELF EMF with the immune system, endocrine system, or growth-regulatory signals and morphogenic movements that involve calcium flux through cell membranes. Many bioeffects have been reported only with certain specific combinations of frequency, amplitude, and orientation of the EMF signal with respect to the geomagnetic field. The possibility of signal-specific effects raises a complication in dosimetry for both epidemiologic and experimental studies since ELF EMF effects may not be directly related to field strength. The report concludes with a discussion of design considerations for ELF ...

1989-12-01

391

Design of the ZTH vacuum liner  

Energy Technology Data Exchange (ETDEWEB)

The current status of the ZTH vacuum liner design is covered by this report. ZTH will be the first experiment to be installed in the CPRF (Confinement Physics Research Facility) at the Los Alamos National Laboratory and is scheduled to be operational at the rated current of 4 MA in 1992. The vacuum vessel has a 2.4 m major radius and a 40 cm minor radius. Operating parameters which drive the vacuum vessel mechanical design include a 300 C bakeout temperature, an armour support system capable of withstanding 25 kV, a high toroidal resistance, 1250 kPa magnetic loading, a 10 minute cycle time, and high positional accuracy with respect to the conducting shell. The vacuum vessel design features which satisfy the operating parameters are defined. The liner is constructed of Inconel 625 and has a geometry which alternates sections of thin walled bellows with rigid ribs. These composite sections span between pairs of the 16 diagnostic stations to ...

1987-01-01

392

Construction and Calibration of the Laser Alignment System for the CMS Tracker  

CERN Document Server

The CMS detector (Compact Muon Solenoid) is under construction at one of the four proton-proton interaction points of the LHC (Large Hadron Collider) at CERN, the European Organization for Nuclear Research (Geneva, Switzerland). The inner tracking system of the CMS experiment consisting of silicon detectors will have a diameter of 2.4 m and a length of 5.4 m representing the largest silicon tracker ever. About 15000 silicon strip modules create an active silicon area of 200 m2 to detect charged particles from proton collisions. They are placed on a rigid carbon fibre structure, providing stability within the working conditions of a 4 T solenoid magnetic field at ?10oC. Knowledge of the position of the silicon detectors at the level of 100 ?m is needed for an efficient pattern recognition of charged particle tracks. Metrology methods are used to survey tracker subdetectors and the integrated Laser Alignment System (LAS) provides absolute ...

2006-01-01

393

Aspects of Stability Related to the Colliding Beam Fusion = Reactor  

Science.gov (United States)

Recent experiments with TFTR, D-III-D and JET involving the injection and trapping of low density beams of high energy large orbit ions indicate that large orbit non-adiabatic ions slow down and diffuse classically in the presence of anomalous fluctuations and transport of adiabatic majority particles. Accordingly, we consider conceptual fusion reactors(N. Rostoker, M.W. Binderbauer and H.J. Monkhorst, Science) 278, 1419 (1997). based on classical confinement of fuel ions and fusion products(M.W. Binderbauer and N. Rostoker, J. Plasma Phys.) 56, 451 (1996).. The magnetic confinement geometry of the proposed designs is a Field Reversed Configuration. A survey of experimental results on instabilities and their characteristics as related to these reactor concepts is presented. Particular focus will be given to long wavelength (as compared to gyro-radius) and low frequency (?<< c/r_o, r_o=3D major radius of annular current ring) instabilities ...

1998-11-01

394

Application of realistic meson-exchange forces in the broken-pair model  

Energy Technology Data Exchange (ETDEWEB)

A G-matrix, derived from a meson-exchange potential in nuclear matter, is applied to finite, semi-magic nuclei. For the open shell the broken-pair model, which can accommodate many single-particle levels, is used. The excitations of the closed shell are treated as particle-hole states. Energy spectra and electromagnetic transition densities are calculated for /sup 88/Sr and /sup 58/Ni. The energies of the non-collective states are well described. Pairing correlations in the ground state have almost the correct strength in a multishell model space. To improve the energies of the collective 2/sup +/ and 3/sup -/ states the inclusion of core-polarisation effects in the force is required. Transition charge densities for collective states become strongly surface-peaked by core-polarisation effects, as is observed in experiments. The effects of pairing correlations and core polarisation on the magnetic form factor of the 3.486 MeV 1/sup +/ state in ...

1985-03-11

395

Application of realistic meson-exchange forces in the broken-pair model  

International Nuclear Information System (INIS)

A G-matrix, derived from a meson-exchange potential in nuclear matter, is applied to finite, semi-magic nuclei. For the open shell the broken-pair model, which can accommodate many single-particle levels, is used. The excitations of the closed shell are treated as particle-hole states. Energy spectra and electromagnetic transition densities are calculated for "8"8Sr and "5"8Ni. The energies of the non-collective states are well described. Pairing correlations in the ground state have almost the correct strength in a multishell model space. To improve the energies of the collective 2"+ and 3"- states the inclusion of core-polarisation effects in the force is required. Transition charge densities for collective states become strongly surface-peaked by core-polarisation effects, as is observed in experiments. The effects of pairing correlations and core polarisation on the magnetic form factor of the 3.486 MeV 1"+ state in "8"8Sr are found to be ...

396

A singlet - triplet T_+ based qubit  

International Nuclear Information System (INIS)

We theoretically model a nuclear-state preparation scheme that increases the coherence time of a two-spin qubit in a double quantum dot. The two-electron system is tuned repeatedly across a singlet-triplet level-anticrossing with alternating slow and rapid sweeps of an external bias voltage. Using a Landau-Zener-Stueckelberg model, we find that in addition to a small nuclear polarization that weakly affects the electron spin coherence, the slow sweeps are only partially adiabatic and lead to a weak nuclear spin measurement and a nuclear-state narrowing which prolongs the electron spin coherence. This resolves some open problems brought up by a recent experiment. We also show that the electronic two-spin states singlet and triplet T_+ are promising candidates for the implementation of a qubit in GaAs double quantum dots (DQD). A coherent superposition of the two-spin states is obtained by finite time Landau-Zener-Stueckelberg interferometry and the single qubit ...

2010-03-21

397

A magnetically levitated electrode ionization chamber of the noncontact measurement type  

Energy Technology Data Exchange (ETDEWEB)

A new type of ionization chamber with levitated electrode has been developed. In this ionization chamber, an ion-collection electrode levitates in the air without getting any physical support from the insulator. The electrode is charged by an electrostatic charger without physical contact. The charge of the electrode is read out at a Faraday cage periodically at a given time interval without physical contact. Because its electrode levitates, the ionization chamber produces no background current caused by leaks or piezo current. In addition, as the charging of its electrode and the read-out of its charge are carried out without physical contact, no irregular charge or contact potential difference due to the chattering between electrode and contact point occurs. Through experiments, it was found that this ionization chamber was able to measure the {gamma}-ray dose such as the environmental radiation with a high degree of sensitivity. The minimum detectable value of ...

2002-04-01

398

A look ahead: PET/MR versus PET/CT  

Energy Technology Data Exchange (ETDEWEB)

Integration of positron emission tomography (PET) and magnetic resonance (MR) has become a topic of increasing interest to the imaging community over the past two years. In this text, the authors attempt to distinguish facts from fiction concerning such integrated systems. Analysis of existing information of combined imaging on existing brain PET/MR systems and imaging experience with PET-computed tomography (CT) is reviewed. Various types of system integration of PET and MR are discussed with completely independent systems on one hand and completely integrated systems with the possibility of simultaneous data acquisition on the other hand. Furthermore, it is discussed, what simultaneous data acquisition with nuclear imaging systems combined with MR or CT really means, as technical simultaneity may not be relevant in light of the pharmacokinetics of the nuclear tracers used. The authors conclude that combining PET/MR is an interesting research ...

2009-03-15

399

Spin freezing in the re-entrant spin glass FeNiMn close to the frustration limit  

Energy Technology Data Exchange (ETDEWEB)

In the invar alloy (Fe{sub 0.65}Ni{sub 0.35}){sub 1-} {sub x} Mn {sub x} we measured the magnetic form factor s(Q) and the intermediate scattering function s(Q,t) for a sample close to the critical Mn concentration (x {sub c}=0.139), at which the sample turns to a re-entrant spin glass phase. The aim was to check whether the magnetic behaviour would approach the Q-independent relaxation behaviour of a classical spin glass when x=x {sub c}. The experiment showed a quite similar spin freezing as for a more ferromagnetic sample with x=0.113. The intermediate scattering function and the form factor were determined by paramagnetic NSE. The normalized scattering function S(Q,t)=s(Q,t)/s(Q)=exp[(-{gamma}t) {sup n}] was fitted by stretched exponential decay. As a function of temperature T<200 K the inverse time constant {gamma} showed the change of more than four orders of magnitude from frozen spin glass (T=60 K to T=100 ...

2007-07-15

400

Nucleon electromagnetic form factors from lattice QCD using 2+1 flavor domain wall fermions on fine lattices and chiral perturbation theory  

Science.gov (United States)

We present a high-statistics calculation of nucleon electromagnetic form factors in N{sub f}=2+1 lattice QCD using domain wall quarks on fine lattices, to attain a new level of precision in systematic and statistical errors. Our calculations use 32{sup 3}x64 lattices with lattice spacing a=0.084 fm for pion masses of 297, 355, and 403 MeV, and we perform an overdetermined analysis using on the order of 3600 to 7000 measurements to calculate nucleon electric and magnetic form factors up to Q{sup 2{approx_equal}}1.05 GeV{sup 2}. Results are shown to be consistent with those obtained using valence domain wall quarks with improved staggered sea quarks, and using coarse domain wall lattices. We determine the isovector Dirac radius r{sub 1}{sup v}, Pauli radius r{sub 2}{sup v} and anomalous magnetic moment {kappa}{sub v}. We also determine connected contributions to the corresponding isoscalar observables. We extrapolate these observables to the ...

2010-02-01

401

New correlated electron physics from new materials  

Energy Technology Data Exchange (ETDEWEB)

Many important advances in the physics of strongly correlated electron systems have been driven by the development of new materials: for instance the filled skutterudites MT{sub 4}X{sub 12} (M=alkali metal, alkaline earth, lanthanide, or actinide; T=Fe, Ru, or Os; X=P, As, or Sb), certain lanthanide and actinide intermetallic compounds such as URu{sub 2-x}Re{sub x}Si{sub 2} and CeTIn{sub 5} (T=Co, Rh, or Ir), and layered oxypnictides and related materials. These types of complex multinary d- and f-electron compounds have proven to be a vast reservoir of novel strongly correlated electron ground states and phenomena. In these materials, the occurrence of such a wide range of ground states and phenomena arises from a delicate interplay between competing interactions that can be tuned by partial or complete substitution of one element for another, as well as the application of pressure, and magnetic fields, resulting in rich and complex electronic phase diagrams in ...

2009-10-15

402

Magnetic resonance imaging of stents. Quantitative in vitro examination at 3 Tesla; Magnetresonanztomographie von Stents. Quantitative MR-Untersuchungen in vitro bei 3 Tesla  

Energy Technology Data Exchange (ETDEWEB)

The aim of this study was to qualitatively and quantitatively study MR artifacts of various stents on the basis of in vitro experiments. We were particularly interested whether sequence type and orientation of the stent with respect to the static magnetic field influences the artifact. We examined 18 stents of different material (nitinol, stainless steel, cobalt alloy), different design of the stent meshes (AccuLink, OmniLink, DynaLink, Xact, Protoge, Wallstent Monorail), different diameter (5-10 mm) and different length (18-58 mm) with a turbo spin echo (TSE), a 2D-fast low angle shot (FLASH) and a 3D-FLASH sequence. The MR images were examined qualitatively with respect to possible artifacts. Furthermore we examined the MR data quantitatively: The contrast-noise-ratio (CNR) was determined both within the stent and outside (within the tube); based on these values we calculated the transparency factor P, furthermore we calculated the apparent ...

2009-07-01

403

Magnetic properties of a SmNiSn single crystal  

Energy Technology Data Exchange (ETDEWEB)

The magnetic properties of a single crystal of SmNiSn with the orthorhombic {epsilon}-TiNiSi-type crystal structure have been investigated by magnetic susceptibility, magnetization and electrical resistivity measurements from 1.5 K to room temperature. Two anomalies have been found in the magnetic susceptibility, indicating an antiferromagnetic phase transition at T{sub N}=9.4 K and a second transition at 4.4 K. A large magnetic anisotropy has been found at low temperatures in the temperature and field dependencies of magnetic susceptibility and magnetization. Below 80 K, the easy axis of the magnetization is the c-axis. At T=2.0 K, the c-axis magnetization curve exhibits metamagnetic-like behavior at H{sub c}=42 kOe and reaches 0.54 emu/g at H=55 kOe, whereas for the a- and b-axis the ...

2003-04-01

404

Development of magnetic drive packless valves for commercial purpose  

Energy Technology Data Exchange (ETDEWEB)

A study on development of magnetic drive packless valves for commercial purpose showed the results as follows; 1. Study on the radial rays effecting to the permanent magnets -Measurement of the strength of Nd-magnets according to irradiation of radial rays. 2. Effects of temperature on the magnetic driving device -Temperature dependency of the Nd-casting magnets. -Effects of temperature on the heat releasing fins of high-temperature valve. 3. Optimization of torque -Arranging method of permanent magnets -Measuring method and results of torque. 4. Design, manufacture and test for the pressure-resisting structure of magnetic power transmitting device -Calculation and design for the flat circular plates under pressure of the magnetic power transmitting device -Design, manufacture and test for the pressure-resisting ...

1995-09-01

405

Challenges in fabrication of 180deg magnet chamber  

International Nuclear Information System (INIS)

180 deg magnet chamber is used in Folded Tandem Ion Accelerator for passage and 180 deg bending of ion beam. The chamber is placed between 180 deg terminal magnet (Electro-magnet), which is used for bending, and analysing the beams. Magnet with a particular magnetic field strength bends ions of only specified mass energy product through a precise path. There is also a space limitation in the direction of magnetic field. Both of them require the magnet chamber to be of a close tolerance. Accuracy of center distance between inlet and outlet port of the magnet chamber has to be at par with the concentricity of high energy and low energy beam line. To achieve this we started the fabrication of magnet chamber by following two methods: a) Circular rolling and bending of rectangular tube for 180 deg sector ...

2006-11-01

406

AC loss measurements of model and full size 50mm SSC collider dipole magnets at Fermilab  

Energy Technology Data Exchange (ETDEWEB)

Tests have recently been performed at Fermilab in order to measure the energy losses due to eddy currents and iron and superconductor magnetization. These measurements were performed on six 1.5m long model magnets and eight 15m long full scale collider dipole magnets. AC losses were measured as a function of ramp rate using sawtooth ramps from 500, to 5000 Amps for both types of magnets, while bipolar studies were additionally performed on some of the short magnets. The measured magnet voltage and current for a complete cycle are digitally integrated to yield the energy loss per cycle. Measurement reproducibility is typically 5%, with good agreement between long magnet measurements and extrapolations from short magnet measurement results. Magnetization loss measurements among similar ...

1992-09-01

407

Interaction of antimicrobial peptides with lipid membranes  

International Nuclear Information System (INIS)

This study aims to investigate the difference in the interaction of antimicrobial peptides with two classes of zwitterionic peptides, phosphatidylethanolamines (PE) and phosphatidylcholines (PC). Further experiments were performed on model membranes prepared from specific bacterial lipids, lipopolysaccharides (LPS) isolated from Salmonella minnesota. The structure of the lipid-peptide aqueous dispersions was studied by small-and wide-angle X-ray diffraction during heating and cooling from 5 to 85 C. The lipids and peptides were mixed at lipid-to-peptide ratios 10-10000 (POPE and POPC) or 2-50 (LPS). All experiments were performed at synchrotron soft condensed matter beamline A2 in Hasylab at Desy in Hamburg, Germany. The phases were identified and the lattice parameters were calculated. Alamethicin and melittin interact in similar ways with the lipids. Pure POPC forms only lamellar phases. POPE forms lamellar phases at low ...

408

X-ray diffraction studies of palladium silicide thin films  

Energy Technology Data Exchange (ETDEWEB)

The solid state reaction between a Pd thin film and a Si substrate produces a single new phase, Pd/sub 2/Si, for temperatures <700/sup 0/C. When the substrate is a single crystal of (111) surface orientation, this process is particularly interesting because the silicide grows epitaxially. Growth of epitaxial interfacial Pd/sub 2/Si was the focus of this study using X-ray diffraction techniques.

1985-01-01

409

The influence of self-diffraction on two-wave mixing for counterpropagating geometry  

Science.gov (United States)

Two-wave mixing in sillenite crystals such as bismuth silicon oxide (Bi12SiO20) and bismuth titanium oxide (Bi12TiO20) of (001)- and (221)-cuts for counterpropagating geometry was studied within the frame of slowly varying amplitude approximation. Electrooptic, photoelastic, piezoelectric, self-diffraction effects and optical activity were taken into account.

2005-06-01

410

The different structural scales of the breast and their impact on time-of-flight and diffraction tomography  

Energy Technology Data Exchange (ETDEWEB)

Ultrasound tomography is an attractive imaging method for the detection of breast cancer. The complex anatomy of the breast with its different spatial scales and material property contrasts make accurate reconstructions very challenging. This paper proposes a hybrid approach whereby Travel-of-Flight and Diffraction Tomography are combined together to achieve high-resolution and high-accuracy sound-speed reconstructions. The method is validated with several numerical phantoms.

2010-01-01

411

Correlation between the microstructure and the physical properties of HTSC single crystals and films. Final report; Korrelation zwischen der Realstruktur und den physikalischen Eigenschaften von HTSL-Einkristallen und -Schichten. Abschlussbericht  

Energy Technology Data Exchange (ETDEWEB)

1. In order to carry out isothermic crystal growth experiments of YBCO the 123 primary crystallization field was determined by means of phase diagram investigations and crystal growth experiments at different oxygen partial pressure. 2. YBCO single crystals of high crystallographic perfection were grown and conclusions on the flux pinning mechanism were drawn. 3. By means of Liquid Phase Epitaxy (LPE) single crystalline (Tc{approx}90 K; {Delta}T{<=}0.5 K) c- and a,b- YBCO fils have been prepared on NdGaO{sub 3} and LaGaO{sub 3} substrates. The films were characterized structurally and magnetically. 4. Our fist melt textured YBCO ``single crystals`` possess intracrystalline critical current densities >10{sup 4} A/cm{sup 2} at B{<=}2T. The irreversibility inductions are {<=}6 T at 77 K. A simple demonstrator was constructed together with the IFW Dresden and a growth model was developed. 5. Using above all torque ...

1993-06-01

414

The Effect of Static Magnetic Forces on Water Contents and Photosynthetic Pigments in Sweet Basil Ocimum basilicum L. (Lamiaceae)  

International Nuclear Information System (INIS)

Three different magnetic regimes; aerial, surface and buried; each with three different forces, have been used to investigate their effects on the water contents and photosynthetic pigments of sweet basil plants (Ocimum basilicum L.). Two groups of sweet basil seeds, Ocimum basilicum L. have been cultivated, one under normal conditions and the second has been subdivided into three portion (aerial, surface and buried) to examine the effect of different magnetic forces coming from the three directions on the resulted plants. At all directions of magnets, water contents have been significantly affected by the magnetic forces. Chlorophyll A and carotene contents have been affected, as well, according to the three magnetic forces coming from soil surface regime only. Chlorophyll B did not significantly affected by differences magnetic forces in the three regimes, but ...

415

THE APPLICATION OF STEEP PULSE CURRENTS TO THE ...  

Science.gov (United States)

... Title : THE APPLICATION OF STEEP PULSE CURRENTS TO THE ELECTROHYDRAULIC AND MAGNETIC FORMING OF METALS. ...

1966-04-01

422

Recovery Effects of a 180?mT Static Magnetic Field on Bone Mineral Density of Osteoporotic Lumbar Vertebrae in Ovariectomized Rats  

UK PubMed Central (United Kingdom)

The effects of a moderate-intensity static magnetic field (SMF) on osteoporosis of the lumbar vertebrae were studied in ovariectomized rats. A small disc magnet (maximum magnetic flux density 180 mT)...Full Text Available

2011-01-01

423

QCCM - Center for NMR Quantum Information Processing  

Science.gov (United States)

... decoherence. Descriptors : *QUANTUM COMPUTING, NUCLEAR MAGNETIC RESONANCE, JOSEPHSON JUNCTIONS. Subject ...

2011-02-16

424

Perpendicular magnetic anisotropy of ultrathin FeCo alloy films on Pd(0 0 1) surface: First principles study  

International Nuclear Information System (INIS)

Using the full potential linearized augmented plane wave (FLAPW) method, thickness dependent magnetic anisotropy of ultrathin FeCo alloy films in the range of 1 monolayer (ML) to 5 ML coverage on Pd(0 0 1) surface has been explored. We have found that the FeCo alloy films have close to half metallic state and well-known surface enhancement in thin film magnetism is observed in Fe atom, whereas the Co has rather stable magnetic moment. However, the largest magnetic moment in Fe and Co is found at 1 ML thickness. Interestingly, it has been observed that the interface magnetic moments of Fe and Co are almost the same as those of surface elements. The similar trend exists in orbital magnetic moment. This indicates that the strong hybridization between interface FeCo alloy and Pd gives rise to the large magnetic moment. Theoretically calculated ...

2009-06-01

426

Optimization of soft magnetic properties in Fe-B and Fe-B-Si amorphous alloys obtained by melt spinning method  

International Nuclear Information System (INIS)

In the present paper the progress of optimization of soft magnetic properties have been studied by applying different experimental techniques (magnetic measurements, electric measurements, X-ray analysis, and high-resolution electron microscopy observation). It has been shown that an increase in magnetic permeability after optimization annealing can be mainly attributed to annealing out of microvoids. (author)

2001-09-23

427

NASA Technical Reports Server - Magnetic forming coil design and ...  

Science.gov (United States)

Site Error There's a problem with your browser or settings. ...

432

Magnetic forming studies  

Science.gov (United States)

Elastodynamic approach to measuring stress-strain relationship of uniaxially stressed wire, and

1967-01-01

434

Magnetic excitations in amorphous ferromagnets  

Science.gov (United States)

Neutron scattering techniques have been used to measure the static structure and magnetic excitations in amorphous magnets. Sum rules and computer models are used to discuss the relationship between the static disorder and the shape of the excitation spectrum. Polarized beam measurements of chi''(Q,E) are compared to analytical theories and computer calculations for the magnetic excitations in amorphous ferromagnets.

1978-03-01

435

Magnetic electronic lenses, quadrupole and octupole for microsystem electron beam techniques  

International Nuclear Information System (INIS)

The MOS-technology allows to make tiny electronic lenses for multibeam electron systems. In the paper results of research and principles of designing of tiny magnetic electron lenses are submitted. Electronic lenses with a nonconventional configuration of tiny magnetic circuit and electronic lenses with coincident electric and magnetic fields in nonconventional tiny performance are considered

2006-09-01

439

Influence of rotation and magnetic field on the minimum mass of a main-sequence star  

Energy Technology Data Exchange (ETDEWEB)

The influence of rigid-body and differential rotation and of a fine-scale chaotic magnetic field and a poloidal magnetic field on the minimum mass of a main-sequence star is investigated. It is shown that rotation and a magnetic field with an energy equal to 10--20% of the star's gravitational energy increase the minimum mass of a main-sequence star by 1.5--2 times.

1980-11-01

456

A STUDY TO DETERMINE THE DEFORMATION ...  

Science.gov (United States)

... crystals and polycrystals. Nevertheless, explosive forming, magnetic forming, etc., are all high-strain-rate processes that ...

1963-04-01

457

A HELICAL MAGNET DESIGN FOR RHIC.  

Energy Technology Data Exchange (ETDEWEB)

Helical dipole magnets are required in a project for the Relativistic Heavy Ion Collider (RHIC) to control and preserve the beam polarization in order to allow the collision of polarized proton beams. Specifications are for low current superconducting magnets with a 100 mm coil aperture and a 4 Tesla field in which the field rotates 360 degrees over a distance of 2.4 meters. A magnet meeting the requirements has been developed that uses a small diameter cable wound into helical grooves machined into a thick-walled aluminum cylinder.

1997-05-12

459

Magnetocaloric and magnetoresistance studies of GdPd{sub 2}Si  

Energy Technology Data Exchange (ETDEWEB)

The compound GdPd{sub 2}Si, which is reported to order antiferromagnetically at 13 K, has been investigated by heat capacity and electrical resistivity measurement in the presence of external magnetic fields. In contrast to an earlier report, the zero-field heat capacity and resistivity data indicate two magnetic transitions at 13 and 17 K. The external magnetic field substantially influences the resistivity and heat capacity of the compound around the magnetic ordering temperature. The magnetocaloric effect, which is calculated from in-field heat capacity data, is quite large around the magnetic transition temperature. The magnetoresistance is also large near the magnetic ordering temperature. The metamagnetic transition is observed for 10 kOe magnetic field both in magnetocaloric and in magnetoresistance data. The metamagnetic transition ...

2001-01-22

460

Magnetocaloric and magnetoresistance studies of GdPd_2Si  

International Nuclear Information System (INIS)

The compound GdPd_2Si, which is reported to order antiferromagnetically at 13 K, has been investigated by heat capacity and electrical resistivity measurement in the presence of external magnetic fields. In contrast to an earlier report, the zero-field heat capacity and resistivity data indicate two magnetic transitions at 13 and 17 K. The external magnetic field substantially influences the resistivity and heat capacity of the compound around the magnetic ordering temperature. The magnetocaloric effect, which is calculated from in-field heat capacity data, is quite large around the magnetic transition temperature. The magnetoresistance is also large near the magnetic ordering temperature. The metamagnetic transition is observed for 10 kOe magnetic field both in magnetocaloric and in magnetoresistance data. The metamagnetic transition ...

2001-01-22

461

Magnetic separation anxiety  

International Nuclear Information System (INIS)

This paper reports that only a few years ago superconducting magnetic separation was viewed as the next major market for superconducting magnets. The first commercial units had been installed, worked flawlessly, and demonstrated real economic viability. The potential market was seen as quite large, and many people believed that superconducting magnetic separation would soon show the same rapid growth that MRI had demonstrated after its initial success. These hopes even prompted IGC, one of the top MRI magnet builders, to form a separate division devoted to magnetic separation. Despite the existence of Magstream, IGC has not been overly active in the market. As a technology that has applications from the clay on the Earth to the soil on the moon, superconducting magnetic separation has yet to become widely used.

1992-01-01

462

High-mode-number ballooning modes in a heliotron/torsatron system: 1, Local magnetic shear  

Energy Technology Data Exchange (ETDEWEB)

The characteristics of the local magnetic shear, a quantity associated with high-mode-number ballooning mode stability, are considered in heliotron/torsatron devices that have a large Shafranov shift. The local magnetic shear is shown to vanish even in the stellarator-like region in which the global magnetic shear is positive. The reason for this is that the degree of the local compression of the poloidal magnetic field on the outer side of the torus, which maintains the toroidal force balance, is reduced in the stellarator-like region of global magnetic shear because the global rotational transform in heliotron/torsatron systems is a radially increasing function. This vanishing of the local magnetic shear is a universal property in heliotron/torsatron systems with a large Shafranov shift since it results from toroidal force balance in the stellarator-like ...

1996-05-01

463

Effect of the induced magnetic field on peristaltic flow of a couple stress fluid  

Science.gov (United States)

We have analyzed the MHD flow of a conducting couple stress fluid in a slit channel with rhythmically contracting walls. In this analysis we are taking into account the induced magnetic field. Analytical expressions for the stream function, the magnetic force function, the axial pressure gradient, the axial induced magnetic field and the distribution of the current density across the channel are obtained using long wavelength approximation. The results for the pressure rise, the frictional force per wave length, the axial induced magnetic field and distribution of the current density across the channel have been computed numerically and the results were studied for various values of the physical parameters of interest, such as the couple stress parameter ?, the Hartmann number M, the magnetic Reynolds number R and the time averaged mean flow rate ?. Contour plots for the stream and ...

2008-06-01

464

Eddy current probe development based on a magnetic sensor array; Developpement d'un imageur magnetique pour le controle non destructif par courants de Foucault  

Energy Technology Data Exchange (ETDEWEB)

This research deals with in the study of the use of innovating magnetic sensors in eddy current non destructive inspection. The author reports an analysis survey of magnetic sensor performances. This survey enables the selection of magnetic sensor technologies used in non destructive inspection. He presents the state-of-the-art of eddy current probes exploiting the qualities of innovating magnetic sensors, and describes the methods enabling the use of these magnetic sensors in non destructive testing. Two main applications of innovating magnetic sensors are identified: the detection of very small defects by means of magneto-resistive sensors, and the detection of deep defects by means of giant magneto-impedances. Based on the use of modelling, optimization, signal processing tools, probes are manufactured for these both applications.

2007-06-15

465

On the temperature dependence of the magnetic excitations  

International Nuclear Information System (INIS)

We compare experimental data for temperature dependence of the magnetic order parameter and the magnetic excitations (spin waves) in materials with a quenched orbital moment and a well-defined spin quantum number. It is observed that the thermal decrease of the two quantities proceeds according to the same analytical function of the type y(T)=1-cT"#epsilon# with an identical exponent #epsilon#. This power function applies not only asymptotically for T->0 but holds over a wide temperature range. The exponent #epsilon# is universal, i.e. independent of spin order type and lattice symmetry and depends only on the dimensionality of the relevant interactions and on whether the spin quantum number is integer or half-integer. The different T"#epsilon# functions are identified as representations of stable universality classes. The fact that order parameter and magnetic excitations follow the same T"#epsilon# function shows that ...

2005-07-15

466

Theory of zwitterionic molecular-based organic magnets  

British Library Electronic Table of Contents (United Kingdom)

We describe a class of organic molecular magnets based on zwitterionic molecules (betaine derivatives) possessing donor, p bridge, and acceptor groups. Using extensive electronic structure calculations we show the electronic ground-state in these systems is magnetic. In addition, we show that the large energy differences computed for the various magnetic states indicate a high Neel temperature. The quantum mechanical nature of the magnetic properties originates from the conjugated p bridge (only p electrons) in cooperation with the molecular donor-acceptor character. The exchange interactions between electron spin are strong, local, and independent on the length of the p bridge.

2011-01-01

467

Occurrence of magnetism in superconductors  

Science.gov (United States)

We discuss how magnetic phenomena affect superconductivity in simple metals, transition metals and alloys thereof, and dilute Rare-Earth alloys. It is shown both qualitatively and quantitatively that superconductors are sensitive probes for studying itinerant spin excitations, local spin excitations associated with nearly magnetic impurities, the effect of the atomic environment on the stability of local magnetic moments, and the nature of the spin order in Rare-Earth alloys. Also, we discuss how magnetic impurities can be used to study the electronic configuration which is responsible for superconductivity in Laves-phase crystals like A-15 compounds and ..beta..-W crystals, for example.

1970-12-14

468

Magnetic properties of glasses from geothite industrial wastes recycling (FeOOH)  

International Nuclear Information System (INIS)

It has been carried out the magnetic properties determination for high iron oxide content glasses series obtained from a geothite red mud waste from the zinc hydrometallurgy and dolomite and glass cullet as main raw materials. It has been determined the magnetic susceptibility and magnetization values for the glasses here investigated. The results suggest that the magnetic behaviour are depending on the glass chemical composition, so that glasses can be differently classified like ferrimagnetic, ferromagnetic, superparamagnetic and paramagnetic. (Author) 6 refs.

469

Magnetic fluctuations in paramagnetic Mn{sub 0.81}Ni{sub 0.19}  

Energy Technology Data Exchange (ETDEWEB)

Magnetic fluctuations present in the paramagnetic Mn{sub 0.81}Ni{sub 0.19} system have been investigated by measuring inelastic magnetic neutron scattering from a single crystal at temperatures of 450, 585 and 700 K. Antiferromagnetic correlations are observed to be present at all the temperatures studied. The spectral width of the magnetic scattering has been observed to increase with temperature, while the spatial range of the magnetic correlations is seen to decrease as the temperature is raised. The wave-vector-dependent susceptibility is found to follow a Curie-Weiss law near the (1 0 0) position, in agreement with theoretical predictions.

2006-11-15

470

Hydromagnetic rotational braking of magnetic stars  

International Nuclear Information System (INIS)

It is suggested that the magnetic Ap stars can be rotationally decelerated to long periods by the braking action of the associated magnetic field on time scales of order 10"7--10"1"0 years depending on whether the star's dipole field is aligned perpendicular or parallel to the rotation axis. Rotation includes a toroidal magnetic field in the plasma surrounding a star, and the accompanying magnetic stresses produce a net torque acting to despin the star. These results indicate that it is not necessary to postulate mass loss or mass accretion for this purely hydromagnetic braking effect.

471

Correlation between Magnetic Field Quality and mechanical components of the Large Hadron Collider Main Dipoles  

CERN Document Server

The homogeneity of the magnetic field in the LHC dipoles strongly depends on the correct position of the superconducting cables: this is related to the quality of the dipole components, such as the dimension of the coil spacers (copper wedges), of the cable and of the collars. The performance in operational conditions is also affected by the magnetization of the cables. In this work, we analyse the measurements of these quantities during the production of the 1276 LHC dipoles, their trends, and the relation to the measured magnetic field. A novel mtehod to locate electrical shorts based on the analysis of magnetic measurements is also presented, and applications to 15 dipoles reascued during the production is given.

2006-01-01

472

Theory of low voltage annular beam free-electron lasers  

Energy Technology Data Exchange (ETDEWEB)

An nonlinear analysis of an annular beam propagating through a cylindrical waveguide in the presence of a helical wiggler and an axial guide field is presented. The analysis is based upon the ARACHNE simulation which is a non-wiggler-averaged slow-time-scale simulation code in which the electromagnetic field is represented as a superposition of the TE and TM modes in a vacuum waveguide, and the beam space-charge waves are represented as a superposition of Gould-Trivelpiece modes. The DC self-electric and self-magnetic fields are also included in the model. ARACHNE has been extensively benchmarked against experiments at MIT and NRL in the past with good agreement, but all of these experiments have dealt with solid electron beams and beam voltages in excess of 200 kV. In seeking to reduce the beam voltage requirements we now consider the effect of operation with an annular beam. One advantage to be obtained by using an ...

1995-12-31

473

Outcome of moderately dosed radiosurgery for limited brain metastases. Report of a single-center experience  

International Nuclear Information System (INIS)

Purpose: Efficacy and safety of the own single-center experience with moderately dosed radiosurgery (SRS) for limited (one to four) brain metastases were analyzed and correlated with patient- and treatment-related variables. Patients and Methods: Between 05/1998 and 10/2006, 93 patients received SRS for a total of 142 brain metastases. The median number of brain metastases treated per patient was one (range, one to four). 46 patients (49%) received initial SRS alone, 13 patients (14%) SRS with up-front whole-brain radiotherapy (WBRT), and 34 patients (37%) SRS for recurrent metastases after WBRT. Median dose was 16 Gy (range, 10-20 Gy). Results: Median overall survival (OS) was 7.5 months. The actuarial 6- and 12-month data for OS were 60% and 35%, for local brain control (LBC) 87% and 79%, and for distant brain control (DBC) 48% and 37%, respectively. Only ten of 46 patients (22%) with initial SRS alone ultimately received WBRT. Ten patients suffered from seizures ...

2010-02-01

474

K/sub. beta. //K/sub. cap alpha. / transition probability ratios from the measurement of fluorescent X-ray intensities of some lanthanide compounds  

Energy Technology Data Exchange (ETDEWEB)

The effect that different chemical and physical atomic environments can have on the relative intensities of radiative electron transitions from the filling of K shell vacancies was investigated. The method used involved the detection of photoionization induced X-ray fluorescence. An experimental system based on a hyper pure germanium detector (HPGE) was used to measure the relative K-L and K-M X-ray yields from the photofluorescence of a series of lanthanide elements and compounds. A background subtraction and peak integration strategy was employed which accounted for scattering in the samples and scattering of the flux from the radioisotope photoionization sources. Analysis of the data resulted in a tabulation of relative K/sub ..beta..//K/sub ..cap alpha../ X-ray intensity ratios. The measured relative K/sub ..beta..//K/sub ..cap alpha../ X-ray intensity ratios were compared to the calculated values predicted by the theoretical development of Scofield and the average of previous ...

1987-01-01

475

K/sub #beta#//K/sub #alpha#/ transition probability ratios from the measurement of fluorescent X-ray intensities of some lanthanide compounds  

International Nuclear Information System (INIS)

The effect that different chemical and physical atomic environments can have on the relative intensities of radiative electron transitions from the filling of K shell vacancies was investigated. The method used involved the detection of photoionization induced X-ray fluorescence. An experimental system based on a hyper pure germanium detector (HPGE) was used to measure the relative K-L and K-M X-ray yields from the photofluorescence of a series of lanthanide elements and compounds. A background subtraction and peak integration strategy was employed which accounted for scattering in the samples and scattering of the flux from the radioisotope photoionization sources. Analysis of the data resulted in a tabulation of relative K/sub #beta#//K/sub #alpha#/ X-ray intensity ratios. The measured relative K/sub #beta#//K/sub #alpha#/ X-ray intensity ratios were compared to the calculated values predicted by the theoretical development of Scofield and the average of previous experimental values ...

1987-01-01

476

Experimental estimation of the hot spot size in Nb-based Josephson tunnel junctions using Abrikosov vortices  

Energy Technology Data Exchange (ETDEWEB)

We report on a new experimental approach to the size estimation of the hot spot induced by ionizing particles in a Josephson tunnel junction. Here, in contrast to the case of a superconducting strip, it is possible to investigate the hot spot dynamics in absence of effects due to the heating induced by the bias current. The reported experiment is based on the motion of Abrikosov vortices, trapped in the thin films constituting the junction electrodes, under 5.6 MeV {alpha}-particle irradiation. The fast time evolution of a hot spot, combined with the presence of Abrikosov vortices, produces a change of the static magnetic field in the junction area and thus a change of the critical current value, I{sub c}. Measurements of I{sub c} during the {alpha}-particle irradiation and in presence of trapped Abrikosov vortices allow to determine the rate of appearance of those I{sub c} changes. The behavior of the average appearance rate as function of the ...

1997-11-01

477

How the Performance of a Superconducting Magnet is affected by theConnection between a small cooler and the Magnet  

Energy Technology Data Exchange (ETDEWEB)

As low temperature cryocoolers become more frequently used to cool superconducting magnets, it becomes increasingly apparent that the connection between the cooler and the magnet has an effect on the design and performance of the magnet. In general, the use of small coolers can be considered in two different temperature ranges; (1) from 3.8 to 4.8 K for magnet fabricated with LTS conductor and (2) from 18 to 35 K for magnets fabricated using HTS conductor. In general, both temperature ranges call for the use of a two-stage cooler. The best method for connecting a cooler to the magnet depends on a number of factors. The factors include: (1) whether the cooler must be used to cool down the magnet from room temperature, (2) whether the magnet must have one or more reservoirs of liquid cryogen to keep the ...

2005-09-08

478

Anisotropic Nd{endash}Fe{endash}B bonded magnets made from HDDR powders (invited)  

Energy Technology Data Exchange (ETDEWEB)

Anisotropic Nd{endash}Fe{endash}B magnet powders can be produced by the hydrogenationdecomposition-desorption-recombination (HDDR) process from Nd{endash}Fe@ xnB{endash}Co{endash}M ({ital M}=Ga, Zr, Nb, Hf, and Ta) alloys. The present status of those HDDR powders and the bonded magnets made from them are reviewed with regards to the powder particle size dependence of their magnetic properties, their magnetic thermal stability, and their magnetization behavior. The results of a mechanistic study on the recombination step are also presented. The magnetic properties of the anisotropic HDDR powder depend relatively little on the powder particle size. Bonded magnets with a density of {approximately}6.20 g/cm{sup 3} and a BH{sub max} of 18.5{endash}20.5 MGOe can be produced from anisotropic HDDR powders with particle sizes of below 300 {mu}m diam. ...

1996-04-01

479

Summary of Dissimilar Metal Joining Trials Conducted by Edison Welding Institute  

International Nuclear Information System (INIS)

Under the direction of the NASA-Glenn Research Center, the Edison Welding Institute (EWI) in Columbus, OH performed a series of non-fusion joining experiments to determine the feasibility of joining refractory metals or refractory metal alloys to Ni-based superalloys. Results, as reported by EWI, can be found in the project report for EWI Project 48819GTH (Attachment A, at the end of this document), dated October 10, 2005. The three joining methods used in this investigation were inertia welding, magnetic pulse welding, and electro-spark deposition joining. Five materials were used in these experiments: Mo-47Re, T-111, Hastelloy X, Mar M-247 (coarse-grained, 0.5 mm to several millimeter average grain size), and Mar M-247 (fine-grained, approximately 50 (micro)m average grain size). Several iterative trials of each material combination with each joining method were performed to determine the best practice joining method. ...

480

Summary of Dissimilar Metal Joining Trials Conducted by Edison Welding Institute  

Energy Technology Data Exchange (ETDEWEB)

Under the direction of the NASA-Glenn Research Center, the Edison Welding Institute (EWI) in Columbus, OH performed a series of non-fusion joining experiments to determine the feasibility of joining refractory metals or refractory metal alloys to Ni-based superalloys. Results, as reported by EWI, can be found in the project report for EWI Project 48819GTH (Attachment A, at the end of this document), dated October 10, 2005. The three joining methods used in this investigation were inertia welding, magnetic pulse welding, and electro-spark deposition joining. Five materials were used in these experiments: Mo-47Re, T-111, Hastelloy X, Mar M-247 (coarse-grained, 0.5 mm to several millimeter average grain size), and Mar M-247 (fine-grained, approximately 50 {micro}m average grain size). Several iterative trials of each material combination with each joining method were performed to determine the best practice joining method. ...

2005-11-18

481

Kondo effect and impurity-impurity interaction in (La, Ce)B_6 alloys  

International Nuclear Information System (INIS)

Measurements of the magnetic susceptibility betweeen 0.03 and 300 K and of the magnetization between 0.05 and 10 K for magnetic fields up to 60kOe have been used to investigate effects from the interaction between the conduction electrons and local magnetic moments in (Lasub(1-x)Cesub(x))B_6 alloys (0.0007<=x<=0.10). For Ce concentrations x<0.006 the data show Kondo-type single impurity behaviour at low temperatures with a transition from a magnetic to a non-magnetic regime of the Ce ions. In the magnetic regime the impurity susceptibility follows a Curie-Weiss law, and in the non-magnetic regime it varies with T"2. An external magnetic field gradually restores the free-ion behaviour of the Ce impurities. For more concentrated alloys interactions between the impurities are observed. The RKKY ...

1978-01-01

482

Development of magnetic separation system of magnetoliposomes  

Energy Technology Data Exchange (ETDEWEB)

The magnetic separation technology using sub-microsized ferromagnetic particle is indispensable in many areas of medical biosciences. For example, ferromagnetic particles (200-500 nm) are widely used for cell sorting in stem cell research with the use of cell surface-specific antigens. Nanosized ferromagnetic particles (10-20 nm) have been suggested as more suitable in drug delivery studies given their efficiency of tissue penetration, however, the magnetic separation method for them has not been established. One of the major reasons is that magnetic force acting on the object particles decreases drastically as a particle diameter becomes small. In this study, magnetic force acting on the targets was enhanced by the combination of superconducting magnet and the filter consisting of ferromagnetic particle. By doing so, we confirmed that Fe{sub 3}O{sub 4} of 20 nm in diameter was ...

2009-10-15

483

Anti-cancer drug loaded iron-gold core-shell nanoparticles (Fe@Au) for magnetic drug targeting.  

Science.gov (United States)

Magnetic drug targeting, using core-shell magnetic carrier particles loaded with anti-cancer drugs, is an emerging and significant method of cancer treatment. Gold shell-iron core nanoparticles (Fe@Au) were synthesized by the reverse micelle method with aqueous reactants, surfactant, co-surfactant and oil phase. XRD, XPS, TEM and magnetic property measurements were utilized to characterize these core-shell nanoparticles. Magnetic measurements showed that the particles were superparamagnetic at room temperature and that the saturation magnetization decreased with increasing gold concentration. The anti-cancer drug doxorubicin (DOX) was loaded onto these Fe@Au nanoparticle carriers and the drug release profiles showed that upto 25% of adsorbed drug was released in 80 h. It was found that the amine (-NH2) group of DOX binds to the gold shell. An in vitro apparatus simulating the human ...

2010-09-01

484

"1"5"1Eu-Moessbauer study of complex magnetism in Eu_2PdSi_3: Effect of Eu"2"+ substitution by Y"3"+ and of high pressure  

International Nuclear Information System (INIS)

With "1"5"1Eu-Moessbauer spectroscopy and other methods the complex magnetic properties of Eu_2PdSi_3, arising from the two crystallographically different lattice sites of the Eu"2"+ ions, have been already studied. Here we study the impact of magnetic dilution of the magnetic Eu"2"+ sites by non-magnetic Y"3"+ ions. A previous specific heat study has found reduced magnetic ordering temperatures with strong indication of disorder effects like in magnetic spin glasses. Here we provide from "1"5"1Eu-Moessbauer spectroscopy detailed information of the impact of Y"3"+ substitution on the magnetic properties of the two lattice sites, well distinguishable in the "1"5"1Eu-spectra. Since the substitution of the larger Eu"2"+ ions by the smaller Y"3"+ ions is connected with a lattice contraction, we also applied high pressure to the Eu_2PdSi_3 sample ...

2010-03-01

486

CERN's 'Big Bang' experiment given green light  

CERN Document Server

CERN's 'Big Bang' experiment given green light

2008-01-01

487

Big Bang experiment given green light  

CERN Document Server

Big Bang experiment given green light

2008-01-01

488

Transverse Imaging of the Proton in Exclusive Diffractive pp Scattering  

Energy Technology Data Exchange (ETDEWEB)

In a forthcoming paper we describe a new approach to rapidity gap survival (RGS) in the production of high-mass systems (H = dijet, Higgs, etc.) in exclusive double-gap diffractive pp scattering, pp -> p + H + p. It is based on the idea that hard and soft interactions are approximately independent (QCD factorization), and allows us to calculate the RGS probability in a model-independent way in terms of the gluon generalized parton distributions (GPDs) in the colliding protons and the pp elastic scattering amplitude. Here we focus on the transverse momentum dependence of the cross section. By measuring the ''diffraction pattern'', one can perform detailed tests of the interplay of hard and soft interactions, and even extract information about the gluon GPD in the proton from the data.

2006-04-20

489

Time-resolved neutron diffraction study of the superconducting phase formation process in the Bi(PB)-Sr-Ca-Cu-O system  

Energy Technology Data Exchange (ETDEWEB)

The results of real-time neutron diffraction measurements during the superconducting phase formation process in the Bi(Pb)-Sr-Ca-Cu-O system are reported. A Sr-Ca-Cu-O type precursor, with the same stoichiometry as the 2223 phase, was used as starting material, and the temperature range favorable to the formation of the 2223 phase was investigated. The diffraction patterns were processed by a multiphase Rietveld refinement. The formation and decomposition of the 2201 and 2212 phases were directly observed. Experimental evidence on the existence of a partially melted phase in the range 855-860[degrees]C, involved in the formation of the 2223 phase, is discussed. 14 refs., 9 figs., 1 tab.

1993-08-01

490

Time-resolved neutron diffraction study of the superconducting phase formation process in the Bi(PB)-Sr-Ca-Cu-O system  

International Nuclear Information System (INIS)

The results of real-time neutron diffraction measurements during the superconducting phase formation process in the Bi(Pb)-Sr-Ca-Cu-O system are reported. A Sr-Ca-Cu-O type precursor, with the same stoichiometry as the 2223 phase, was used as starting material, and the temperature range favorable to the formation of the 2223 phase was investigated. The diffraction patterns were processed by a multiphase Rietveld refinement. The formation and decomposition of the 2201 and 2212 phases were directly observed. Experimental evidence on the existence of a partially melted phase in the range 855-860 degrees C, involved in the formation of the 2223 phase, is discussed. 14 refs., 9 figs., 1 tab.

491

The application of the neutron time-of-flight technique for real-time diffraction studies  

Energy Technology Data Exchange (ETDEWEB)

Real-time neutron powder diffraction and small-angle scattering techniques have been developed on the TOF diffractometer DN-2 at the IBR-2 pulsed reactor at JINR (Dubna) with a total flux on the sample of 10{sup 7} neutrons cm{sup -2}s{sup -1} and a resolution of about 1%. A special arrangement of the detector system ensures a high counting rate of diffracted neutrons. Depending upon sample type and experimental conditions, the measuring time t{sub s} of one neutron pattern varies from a few minutes to several seconds. The performance of the diffractometer is discussed and typical data are shown to demonstrate current achievements using real-time techniques at a pulsed reactor. (orig.).

1991-12-01

492

The application of the neutron time-of-flight technique for real-time diffraction studies  

International Nuclear Information System (INIS)

Real-time neutron powder diffraction and small-angle scattering techniques have been developed on the TOF diffractometer DN-2 at the IBR-2 pulsed reactor at JINR (Dubna) with a total flux on the sample of 10"7 neutrons cm"-"2s"-"1 and a resolution of about 1%. A special arrangement of the detector system ensures a high counting rate of diffracted neutrons. Depending upon sample type and experimental conditions, the measuring time t_s of one neutron pattern varies from a few minutes to several seconds. The performance of the diffractometer is discussed and typical data are shown to demonstrate current achievements using real-time techniques at a pulsed reactor. (orig.).

1991-12-01

493

Microstructure analysis of nanocrystalline powders by X-ray diffraction  

International Nuclear Information System (INIS)

The use of X-ray diffraction line profile analysis for the study of nanocrystalline powders is described. The fundamentals of the theory are presented in terms of crystallite/domain size, size distribution, lattice distortion, dislocations density and stacking faults. Line profile parameters and the methods of pattern fitting introduced to overcome the diffraction-line overlap problem are discussed. The approaches based of the integral breadth of the measured line profiles and the Fourier method are discussed. In addition, simplified approaches are also commented. Representative examples are selected to illustrate various cases of microstructure, such as nanomaterials with strain-free spherical nano crystallites, strain-free crystallites with anisotropic crystallite shape, anisotropic crystallites with microstrains and spherical crystallites with dislocation densities and crystallite size distributions. (author)

2001-09-23

494

Gauging film thickness: A comparison of an x-ray diffraction technique with Rutherford backscattering spectrometry  

Energy Technology Data Exchange (ETDEWEB)

An x-ray diffraction technique for determining thin-film thickness is presented which should prove to be a valuable alternative to the array of spectroscopies (Rutherford backscattering spectrometry, Auger electron spectroscopy, etc.) currently favored for these measurements. Some of the virtues of this x-ray diffraction approach are its nondestructive nature, fast data acquisition rate (enabling in situ observations), thickness resolution better than 5 nm, and conventional equipment requirements. Results are shown for Pd/sub 2/Si thin films grown during isothermal annealing of Pd coatings (100 nm) on Si at 200 /sup 0/C for various amounts of time. A comparison of these x-ray measurements with Rutherford backscattering spectrometry data taken from the same specimens is used to demonstrate the validity of the x-ray technique.

1985-01-15

495

Diffusion examined by diffraction  

Science.gov (United States)

X-ray diffraction offers a unique combination of advantages for kinetic study which include the non-destructive nature of the measurement, the use of bulk crystals, and the convenience of the experimental arrangements. These attributes and the availability of position-sensitive detectors and high-flux synchrotron radiation sources make this technique most useful for in situ, dynamical investigations. When using diffraction techniques to determine a diffusion coefficient, the principle of analysis entails a scattering theory and a kinetic model. The former allows the kinetic parameter(s) to be extracted from measured intensity, while the latter relates the kinetic parameter(s) to the diffusion coefficient(s). Three examples are demonstrated: (1) Palladium Silicide (Pd{sub 2}Si) Layer Growth on Silicon, (2) Decomposition of an Ni-12.5at%Si Superalloy, and (3) Short-range Ordering in Cu-Au Solid Solutions.

496

Resistivity, Hall effect, and magnetic susceptibility of UPd_2Si_2  

International Nuclear Information System (INIS)

The electrical resistivity, Hall effect, and magnetic susceptibility of single-crystal UPd_2Si_2 have been studied between 4.2 and 300 K. A large anisotropy was observed in both the magnetic and transport properties. There is a quadratic temperature dependence of the resistivity for a range of temperatures between 4.2 and 80 K. At higher temperatures, the resistivity indicates a Kondo-type behavior. The behavior of these quantities is accounted for by the magnetic phase transitions at 108 and 136 K reported from neutron-scattering studies. At high temperatures, the magnetic susceptibility of UPd_2Si_2 is Curie-Wiess-like along the c axis. The temperature dependence of the Hall coefficient above 108 K is accounted for by a theoretical model invoking skew scattering of conduction electrons by localized magnetic moments.

497

Recycler model magnet test on temperature compensation for strontium ferrite  

Energy Technology Data Exchange (ETDEWEB)

The Recycler ring magnet will be made of Strontium ferrite permanent magnets. A strontium ferrite permanent magnet without compensation has a temperature coefficient of -0.2 % in dB/dT. To compensate this effect, we are utilizing 30 % Ni 70 % Fe alloy, a temperature compensation ferromagnetic material with a low Curie point. To search for optimum commercially available material and optimum condition, we made a couple of simple model magnets, and tested with several different compensating material. The test results are reported and its optimal conditions are shown. Several different configurations were tested including a possible 2 kG magnet configuration.

1995-10-01

498

Effect of On-Chip Magnetic Shielding for TES Microcalorimeters  

British Library Electronic Table of Contents (United Kingdom)

We investigated the magnet field dependence of the X-ray pulse height and the critical current of a Ti/Au bilayer TES micro-calorimeter. The pulse height was strongly affected by the magnetic field intensity applied perpendicularly to the TES surface. We found that the critical current at zero temperature, I c0, decreased by a factor of two by applying a magnet field of ?10??T. Our data are consistent with a TES sensitivity proportional to (I/I c0)?2/3, as predicted by the Ginzburg-Landau theory. This fact implies that the shape of the R?T curve of the TES is partly determined by the critical current of the superconductor. In order to make our TES microcalorimeters less sensitive to the external magnetic field, we fabricated devices equipped with on-chip magnetic shielding. One device has ...

2008-01-01

499

Design, Performance and Series Production of Superconducting Trim Quadrupoles for the Large Hadron Collider  

CERN Document Server

The Large Hadron Collider (LHC) will be equipped with several thousands of superconducting corrector magnets. Among the largest ones are the superconducting trim quadrupoles (MQTL). These twin-aperture magnets with a total mass of up to 1700 kg have a nominal gradient of 129 T/m at 1.9 K and a magnetic length of 1.3 m. Sixty MQTL are required for the LHC, 36 operating at 1.9 K in and 24 operating at 4.5 K. The paper describes the design features, and reports the measured quench performance and magnetic field quality of the production magnets. The MQTL magnet production is shared between CERN and industry. This sharing is simplified due to the modular construction, common to all twin-aperture correctors.

2006-01-01