Energy Technology Data Exchange (ETDEWEB)

The use of cement based systems for solidification and stabilization of hazardous wastes has been proposed. The stabilization of Cr contaminated paint removal wastes in ordinary Portland cement and in a Portland cement and blast furnace slag matrix was investigated. A loading by volume of 75% waste and 25% cement (or cement + slag) was used. The expression of pore solution was utilized to determine the chemical environment encountered by the waste species in the cement matrix. The highly alkaline conditions of ordinary Portland cement determined the stability of the metal species, with Cr being highly soluble. The replacement of 25% of the Portland cement by blast furnace slag was found to decrease the [OH-] of the pore solution resulting ...

Energy Technology Data Exchange (ETDEWEB)

Roller compacted concretes (RCC) were developed for the Norwegian Skjerka hydropower project. RCCs were developed to have a high-volume fly ash content to address environmental issues, including the reduction of carbon dioxide emissions associated with dam construction. They also makes good use of waste product and conserve natural resources. This study examined a series of mixtures to determine the appropriateness of using RCC as a competing alternative to the traditional rock fill dam proposed for the Skjerka hydropower project. The main advantage of RCC is speed, allowing a relatively large dam to be constructed in just one summer season, saving financial costs and providing early return on the investment. In addition, fly ash can be used in the structure, using clean and renewable energy. Several procedures to proportion RCC mixtures were proposed, including the optimal paste volume method which is based on the assumption that an optimal RCC should have just enough paste to fill ...

Energy Technology Data Exchange (ETDEWEB)

The main objectives of Phase 2 are to determine the feasibility of using cements with controlled particle size distributions (CPSD cements) in practical concrete applications, and to refine our estimates of the potential energy savings that may ensue from such use. The work in Phase 2 is divided into two main tasks, some parts of which will be carried out simultaneously: Task 1 will continue cement paste studies to optimize cement performance similar to those of Phase 1, but with particular emphasis on gypsum requirements, blended cements, and water-reducing admixtures. This task will also include preparation of sufficient CPSD cements for use in all Phase 2 work. Task 2 will be a comprehensive examination of the properties of concretes made with CPSD cements. This will include optimization of concrete mix designs to obtain the best possible ...

Energy Technology Data Exchange (ETDEWEB)

Presented are the results from a laboratory test program conducted to identify and evaluate materials for converting hazardous geothermal residues to a non-hazardous and potentially usable form. Results indicate that the residues can be effectively incorporated, as a fine aggregate, into portland cement-based composites. Five geothermal residues obtained from sites in the Salton Sea area of California were evaluated. Three of these were classified as hazardous. After mixing with cement, the leach rates were all well below specified levels. Although structural-grade composites were produced, gradual reductions in properties with time up to 1 yr were noted. This indicates ongoing chemical reactions between the cement paste and the constituents of the residues. Further research is necessary before the composites could be considered for use in structural applications. 3 refs., 8 tabs.

International Nuclear Information System (INIS)

When clinoptilolite is immobilized in cement-based composites, a series of reactions occur, leading to release of Cs. These reactions occur in three overlapping stages: a rapid ion exchange, followed by a somewhat slower reaction between clinoptilolite and principally the Ca(OH)_2 component of cement, and, in the longer term, slower reactions with C-S-H leading either to formation of low-lime C-S-H at temperatures below 100"0C or 11 A (1.1 nm) tobermorite at higher temperatures. Kinetic data are presented to evaluate the rate of physical consumption of the zeolites at 70 and 150"0C. Reactions occurring above 100"0C appear to result in the development of extensive microcracking of cement-zeolite composites containing 50% zeolite.

Energy Technology Data Exchange (ETDEWEB)

Red mud from HINDALCO (Hindustan Aluminium Corporation) Industries Limited, Renukoot, India, contains significant quantities of alumina, iron oxide and silica. Presence of the said constituents makes it a suitable ingredient for the preparation of special cements. Preparation of three varieties of cements was investigated, namely: (a) aluminoferrite (C{sub 4}AF)-belite ({beta}-C{sub 2}S) using lime + red mud + fly ash; (b) aluminoferrite-ferrite (C{sub 2}F)-aluminates (C{sub 3}A and C{sub 12}A{sub 7}) utilizing lime + red mud + bauxite; and (c) sulfoaluminate (C{sub 4}A{sub 3}{bar S})-aluminoferrite-ferrite using lime + red mud + bauxite + gypsum. The effects of composition (proportions of lime, red mud, fly ash, bauxite and gypsum), firing temperature and duration on the properties of cements produced were studied in detail. Cements made from lime + red mud + bauxite or lime + red mud + bauxite + ...

Environmental Research Database

ObjectivesTo determine the reaction rate of slag during curing and factors affecting reactivity.~%~~%~To measure the rates of chloride ingress into concrete and the extent of chloride binding.~%~~%~To determine conditions for pitting corrosion and the nature of corrosion products.~%~~%~To characterise the reactions in slag-calcium alumina cement hydration and the nature of the products.~%~DescriptionBlast-furnace slag has latent hydraulic properties, giving considerable potential for commercial use in addition to its widespread use as a partial replacement for Portland cement, notably in alkali-activated slag (AAS) and slag-calcium alumina cement (CAC) concretes. Use of AAS concretes is already well-established in China and the former USSR, but their further application is hindered by lack of research into setting, hydration and durability, Slag/CAC ...

Energy Technology Data Exchange (ETDEWEB)

The rate of corrosion of hardened cement paste in solutions of nitric, hydrochloric, sulfuric, acetic and formic acids was compared. Corrosion in solutions of acetic and nitric acids with different concentrations was studied in more detail. The results made it possible to obtain the relationships expressing the influence of concentration and the time of action of acid solutions on the depth of corrosion. The rates of corrosion in nitric acid solutions during the first 3 years were about 2 to 4 times that in acetic acid solutions, depending on the concentration.

Energy Technology Data Exchange (ETDEWEB)

The Rocky Flats Plant (RFP) generates large volumes of a low level aqueous waste stream high in nitrate salts. The aqueous waste is concentrated by evaporation and then mixed with Portland cement prior to transport and disposal. Planned process upgrades include a new horizontal thin film evaporator. Temperature of brine at discharge end of the new evaporator will be near boiling point. Introduction of hot water to cement can degrade the monolithic waste form. However, the RFP salt waste contains high concentrations of compounds known to retard hydration. This paper discusses impact of introducing high temperature waste to cement. The study evaluated three waste compositions: (1) highest probable nitrate composition, (2) highest probable chloride composition, and (3) current composition. Results showed that compressive strength of final waste form increased with brine temperature, and waste forms from ...

British Library Electronic Table of Contents (United Kingdom)

The shrinkage of the cement paste with low water-cement ratio at different relative humidity was observed and analyzed with ESEM and deformation map technique. The crack morphology was observed with different magnification with SEM and FESEM, and the formation of the crack was observed with AFM between two C-S-H nano particles. The observation by multi technique at multi scale indicated that the shrinkage was increase with the decrease of the humidity due to the increase of the pressure of the capillary pressure, the morphology of the crack in smaller scale was similar to that in the bigger scale, the smaller crack distributed in the latticework of the bigger ones, and the crack propagated along the gap between two nano particles of C-S-H with weaker bonding.

Energy Technology Data Exchange (ETDEWEB)

The authors investigate the feasibility of constructing walls and partitions with enhanced heat storage capability from cement blocks permeated with an organic phase change material (pressed stearic acid). The blocks are lightweight, easy to produce and are cured in the same way as cement or concrete. The ratio of components (cement, stearic acid (SA) and water) was optimized with respect to compressive strength. With normal portland cement, the best compressive strength 2.2 MPa was obtained with a ratio C:SA:W of 1:0.8:0.65 (i.e. 32% stearic acid) after 28 days of curing. This was increased to 4.4 MPa when high early strength cement was used, about as strong as Sipporex, lightweight concrete or lightweight clay bricks. As expected, the compressive strength decreased linearly with temperature between 25/sup 0/C and 100/sup 0/C, at a rate of 15 kPa//sup 0/C. The ...

International Nuclear Information System (INIS)

Immobilization of a model liquid organic pollutant, i.e. the 2-chloroaniline (2-CA), into a cement matrix using organoclays as pre-sorbent agents was investigated. Five cement-clay pastes were prepared with different nominal water-to-cement ratios (w/c=0.40, 0.25 and 0.15 wt/wt) and various amounts of waste (waste-to-cement o/c=0.20, 0.60 and 1.00 wt/wt); for comparison, a neat cement paste was also prepared. Dynamic leach tests were performed on solidified monoliths in order to assess the successful immobilization of the 2-CA. In monoliths at constant w/c ratio (0.40) the total amount of pollutant released increases with its initial content, and ranges from 15 to 35% with respect to it. By lowering w/c from 0.40 to 0.15 at constant o/c, the performances improved (<25% released). The microstructure of the hardened cement-clay pastes was ...

Energy Technology Data Exchange (ETDEWEB)

Samples from three mine tailings, the Hemlo Mine (located in Northern Ontario), the Louvicourt Mine, and the Laronde Mine (both located in Northwestern Quebec) and four different types of hydraulic binder in three different proportions (3, 4.5, 6 per cent of total dry weight of tailings) were used to prepare 33 recipes for cement caulk. The sulphur content of the three tailings is, respectively, 5 per cent, 16 per cent, and 32 per cent. Three of the four hydraulic binders are in fact a mix of two cement types: binder based on Portland cement (CP), binder based on fly ash (FA), and binder based on dross (CL). The fourth binder is based mainly on dross. The coupons of caulk dykes were flushed at 14, 28, 56, and 91 days in a humid chamber. At each of these steps, the samples were characterized for chemical, geochemical, physical, microstructural, and mechanical attributes to better understand the ...

Energy Technology Data Exchange (ETDEWEB)

The primary objective of this task was to perform a variability study of the high activity waste (HAW) acidic feed to determine the impact of feed variability on the quality of the final grout and on the mixability of the salt solution into the dry powders. The HAW acidic feeds were processed through the neutralization/pH process, targeting a final pH of 12. These fluids were then blended with the dry materials to make the final waste forms. A secondary objective was to determine if elemental substitution for cost prohibitive or toxic elements in the simulant affects the mixing response, thus providing a more economical simulant for use in full scale tests. Though not an objective, the HAW simulant used in the full scale tests was also tested and compared to the results from this task. A statistically designed test matrix was developed based on the maximum molarity inputs used to make the acidic solutions. The maximum molarity inputs were: 7.39 HNO{sub 3}, 0.11618 gallium, 0.5423 ...

Energy Technology Data Exchange (ETDEWEB)

'Improvement in understanding of the deposition of ambient dust particles on ECAM (Environmental Continuous Air Monitor) filters, reduction of the alpha-particle interference of radon progeny and other radioactive aerosols in different particle size ranges on filters, and development of ECAM''s with increased sensitivity under dusty outdoor conditions. As of May 1, 1998 (1/2 year into the project) the research-prototype 30-cm pulsed ionization chamber (PIC) is assembled and operational with an alpha particle energy resolution of better than 45 keV for 5-MeV alpha particles. Measurements of spectral resolution for alpha particles from radon decay products have been made as a function of filter type and dust loading conditions. So far, a study of ten filter types has found that the best combination of resolution and throughput is obtained with 3.0 \\265m Millipore fluoropore and 1.0 \\265m Corning FNMB filters. Experiments with gypsum and ...

Energy Technology Data Exchange (ETDEWEB)

No abstract prepared

Science.gov (United States)

Sensitivity to Dental Cements; Dental Crowns; Dental Three-unit Bridges

Science.gov (United States)

... Accession Number : ADD100229. Title : DEFORMATION BEHAVIOR OF AN OMEGA HARDENED ALPHA-BETA TITANIUM ALLOY,. ...

International Nuclear Information System (INIS)

Radioactive "1"4C sucrose was found to be an ideal marker for microleakage because it did not penetrate tooth tissue, dental cement, or mounting resin. The main finding is that the adhesive cements--the glass-ionomer and polycarboxylate--are significantly more effective at preventing microleakage than are the traditional phosphate cements--silicate and zinc phosphate. The differences can be as high as two orders of magnitude. The adhesive cements provide almost perfect and reliable seals. By contrast, the nonadhesive cements are erratic sealants with most of the restorations leaking.

UK PubMed Central (United Kingdom)

Background:Cemented hip arthroplasty is an established treatment for femoral neck fracture in the mobile elderly. Cement pressurization raises intramedullary pressure and...Full Text Available

Science.gov (United States)

The Federal Highway Administration (FHWA) has put a high priority on the use of existing dynamic message signs (DMS) to provide travel time estimates to the public. The Oregon Department of Transportation (ODOT) has three DMS in the Portland metropolitan ...

KoreaScience (Korea)

Full Text Available

International Nuclear Information System (INIS)

A total dose hardening treatment is applied to SIMOX buried oxides. Total ionizing dose radiation testing is performed on fully-depleted transistors fabricated on both hardened and non-hardened substrates. At 200 krads x-ray dose, the front gate shift is reduced from -0.7 to -0.2 V for FETs built on the hardened wafers.

Science.gov (United States)

Graft copolymers of methyl methacrylate and biodegradable, biocompatible bacterial poly([R]-3-hydroxybutyrate) (PHB) blocks were synthesized and evaluated as possible constituents in acrylic bone cements for use in orthopaedic applications. The copolymers were produced by conventional free radical copolymerization and incorporated in one commercially available acrylic bone cement brand, Antibiotic Simplex (AKZ). Cements with formulations containing 6.7 and 13.5 wt % of PMMA-graft-PHB were prepared. The morphology of the graft copolymer particles was suggested to influence the ability of the modified cement to be processed. Formulations containing more than about 20 wt % of the graft copolymer resulted in cement doughs that, both after first preparation and several hours later, were either sandy or soft spongy in texture and, thus, would be unacceptable for use in orthopaedic ...

International Nuclear Information System (INIS)

Short communication.

International Nuclear Information System (INIS)

Short communication.

International Nuclear Information System (INIS)

Results on defect structure study and degree of molybdenum radiation hardening irradiated by fission neutrons and medium energy alpha-particles are presented. It is shown that molybdenum irradiation by alpha-particles and neutrons leads to different degree of material hardening for the same damage level. It is established that molybdenum radiation hardening is mainly defined by radiation defect clusters visible in electron microscope whose coefficient of rigidity depends on their size. 5 refs.; 6 figs.; 2 tabs. (author).

Wastenet

complex -agriculture sector in a local community -blast furnace -cokes oven -cement kiln

Energy Technology Data Exchange (ETDEWEB)

In this study, we investigate an inter-industrial and inter-regional recycling system for industrial waste by the cement industry in Japan. We develop a linear programming model that represents cement production processes and waste transportation of all cement factories in Japan. We simulate cost and CO{sub 2}-minimizing systems. The result implies that making waste transportation more efficient in cost is an effective means for CO{sub 2} reduction. (author)

International Nuclear Information System (INIS)

Radon appears mainly by diffusion processes from the point of origin following #alpha#- decay of "2"2"6Ra in underground soil and building materials used, in the construction of floors, walls, and ceiling. The transport phenomenon of radon through diffusion is a significant contributor to indoor radon entry. In the present study radon diffusion through sand, cement, mixtures of sand + cement (1:1), sand + cement (2:1), sand + cement (3:1), sand + cement (4:1) has been carried out using LR-115 type II solid state nuclear track detectors (SSNTDs). The radon diffusion coefficient and diffusion lengths have been calculated for different materials. The effect of compaction, which changes the porosity and permeability of the materials, on radon diffusion has also been studied. (author)

Energy Technology Data Exchange (ETDEWEB)

The Cement Bond Log Advisor is an expert system being developed to assist users in the design, evaluation, and interpretation of cement bond logs (CBL's). CBL's are produced by sonic tools run after the casing is cemented in a well to determine how well the cement is bonded to the casing and formation and whether a cement squeeze jog should be attempted. During the development of program, two particular challenges were encountered and resolved in ways that might be of general interest to developers of expert system applications for the petroleum industry. The first challenge was to find an efficient and effective method for guiding the user in correlating and interpreting the relationships between multiple sources of continuous visual data (the various waveforms making up the log output). Second, the nomographs, which correlate log amplitudes with ...

Science.gov (United States)

Polymethlylmethacrylate (PMMA) is the most frequently used cement for percutaneous vertebroplasty and kyphoplasty. To aid visualisation during surgery cements are doped with radiopacifying agents such as Barium sulphate (Ba(2)SO(4)) or Zirconium Dioxide (ZiO(2)). Mounting research suggests that these agents may impair the biocompatibility of the cements. However, incorporating an alternative radiopacifier agent with excellent biocompatibility would be a significant step forward. Bioactive radiopaque glasses incorporating elements such as strontium (Sr) and zinc (Zn), known to have beneficial and therapeutic effects on bone, are of great interest in this respect. In this study, the Ba(2)SO(4) of the commercially available Spineplex was incrementally replaced with a radiopaque therapeutic glass composition. The resulting effects on cement setting time, peak isotherm, ultimate compressive strength, Young's ...

International Nuclear Information System (INIS)

Experimental results on study of helium concentration influence on degree of molybdenum radiation hardening for various method of cyclotron doping differing in degree and damage character are presented. It is established that accumulation of helium atoms in molybdenum for simultaneous formation of radiation defects caused by low energetic primary-knocked atoms leads to higher degree of hardening than for high energetic ion irradiation. It is shown that with increase of helium atom concentration the degree of radiation hardening for the same level of damage increases. 4 refs.; 3 figs. (author).

Energy Technology Data Exchange (ETDEWEB)

Controlling acid mine drainage is one of the most important challenges facing the mining industry. One of the solutions to this problem is the use of soil covers. In this poster presentation, the author described the development of a soil barrier composed of cement kiln dust and fly ash. In the study, four different cement kiln dust were associated to three different fly ash types, for a total of twelve different mix. The objective was to develop a stable environmental barrier. The origin of the cement kiln dust was described, followed by the characterization and preparation of the different mix, and the monitoring of the hydration process. The results were discussed, and indicated that a barrier composed of cement kiln dust and fly ash seemed to have great potential. The results also indicated that the fly ash improve the properties of the cement kiln dust, but that the improvement ...

International Nuclear Information System (INIS)

2D MEDICI simulator is used to investigate hardening solutions to single-event burnout (SEB). SEB parametric dependencies such as carrier lifetime reduction, base enlargement, and emitter doping decrease have been verified and a p"+ plug modification approach for SEB hardening of power MOSFETs is validated with simulations on actual device structures.

International Nuclear Information System (INIS)

A patent is claimed for the invention of a hardening (ionizing radiation resistance) process for MOS type components and CMOS or bipolar type components. The ionizing radiation effect on those systems is the electron-hole pair production, which induces interference phenomena. The MOS main structure is successively composed of a silicon substrate layer, a layer of an irradiation resistant material and a layer of partially monocrystalline silicon.

Energy Technology Data Exchange (ETDEWEB)

This document reports the results of testing of spent ion exchange media pretreatment technologies. Emphasis of the testing activities has been on screening pretreatment technologies, such as drying and emulsification, which are compatible with vitrification, cementation, and incineration. Ion exchange media tested for cementation and incineration pretreatment technologies were typical organic ion exchange resins and inorganic zeolites. The ion exchange medium tested for vitrification pretreatment technologies was inorganic zeolite. The results of testing activities are discussed in detail in this report.

Science.gov (United States)

... MPS) Advanced Liquid Crystalline Optical Materials Superconductivity Computation and Visualization ... Cement-Based Materials Synthesis, Growth, and Analysis of Electronic Materials Photoinduced Charge ...

British Library Electronic Table of Contents (United Kingdom)

Normally, concrete technologists attribute salt weathering, salt crystallization or physical attack to the deterioration of concrete that is partially exposed to sulfate environment. However, there are few convincing evidences supporting this view. The purpose of this paper is to check by means of extensive micro-analysis if traces of sulfate crystals are present in the paste. This would enable to verify in a direct way whether salt weathering really causes cement paste damage or not.In this research, cement paste and cement?fly ash paste specimens were partially exposed to sodium sulfate and magnesium sulfates solution under a constant storage condition (20 ? 2 ?C, and 60 ? 5% RH) and a sharply fluctuating environment (40 ? 2 ?C and 35 ? 5% RH for 24 h, then 10 ? 1 ?C and 85 ? 5% RH, also...

Energy Technology Data Exchange (ETDEWEB)

In the new system presented in this paper, the cement clinker is sintered, not in a rotary kiln, but in two different furnaces: a spouted bed kiln and a fluidized bed kiln. The heat generated in the process of cooling the cement clinker is recovered by a fluidized bed cooler and a packed bed cooler, which are more efficient than the conventional coolers. Compared with the rotary kiln system, the new technology significantly reduces NO{sub x} emissions, appreciably cuts energy consumption, and reduces CO{sub 2} emissions as well. Thus, the new system is an efficient cement sintering system that is friendly to the global environment. In this paper, we describe this new technology as one of the applied technologies at an industrial level that is being developed in the Clean Coal Technology Project, and we present the results from test operations at our pilot plant.

International Nuclear Information System (INIS)

Neutron irradiation embrittlement of reactor pressure vessel (RPV) steels is one of the critical issues on aging management for long term operation of nuclear power plants. Mechanistic understanding of embrittlement is a key to accurate prediction of embrittlement, especially after long term operation where the mechanical test data are sparse. Since matrix hardening is the source of the embrittlement, we focus on matrix hardening of A533B bainitic pressure vessel steel. Bainitic matrix is composed of lath structure made by ferrite and carbides, therefore it is important to understand how this structure affects hardening behavior, and to understand irradiation response of each phase. As the typical dimension of lath structure of A533B is about one micron, nanoindentation technique is suitable for the estimation of hardening of each phase. MV ion accelerators were used for controlled irradiation because ...

Energy Technology Data Exchange (ETDEWEB)

This report contains detailed information of the research program entitled "Development of Bulk Nanocrystalline Cemented Tungsten Carbide Materials for Industrial Applications". The report include the processes that were developed for producing nanosized WC/Co composite powders, and an ultrahigh pressure rapid hot consolidation process for sintering of nanosized powders. The mechanical properties of consolidated materials using the nanosized powders are also reported.

Energy Technology Data Exchange (ETDEWEB)

This report summarizes the research conducted during Budget Period One on the project ''Improved Natural Gas Storage Well Remediation''. The project team consisted of Furness-Newburge, Inc., the technology developer; TechSavants, Inc., the technology validator; and Nicor Technologies, Inc., the technology user. The overall objectives for the project were: (1) To develop, fabricate and test prototype laboratory devices using sonication and underwater plasma to remove scale from natural gas storage well piping and perforations; (2) To modify the laboratory devices into units capable of being used downhole; (3) To test the capability of the downhole units to remove scale in an observation well at a natural gas storage field; (4) To modify (if necessary) and field harden the units and then test the units in two pressurized injection/withdrawal gas storage wells; and (5) To prepare the project's final report. This report ...

Scientific Electronic Library Online (English)

Abstract in english The rate of copper II/zinc cementation from copper sulphate solutions in the absence and in the presence of methanol (CH3OH) and dimethyl sulphoxide (DMSO) has been studied and the reaction was found to follow first-order kinetics. The influence of several parameters on the course of the reaction, such as cylinder rotation speed, initial concentration of Cu2+ ions, temperature and concentration of organic solvent, was investigated. In the case of CH3OH, rotating zinc cyli (more) nder was used, while in the presence of DMSO stationary zinc sheet and rotating zinc cylinder were used. It was found that (1) the percentage inhibition caused by methanol ranged from 10.70 to 58.38 depending on the concentration of the alcohol used; (2) the rate of cementation in the presence of DMSO using rotating zinc cylinder > the rate of cementation in the presence of DMSO using stationary zinc sheet; (3) the rate of ...

Energy Technology Data Exchange (ETDEWEB)

The aim of this paper is to investigate the possible displacement of natural gypsum (CaSO{sub 4}2H{sub 2}O) in cement with an alternative setting retarder, such as the industrial by-product derived from flue gas desulfurization process called FGD gypsum. These calcium-sulfate-bearing materials (CSBM), alone or in mixtures, were ground with clinker both in laboratory and industrial scale to examine their influence on the physical and mechanical properties of cement, as well as on the industrial production line of cement. From the present work, it is extracted that the use of mixtures of sulfate-bearing materials with gypsum seems to be advantageous for the actual control of setting time. The addition of FGD gypsum increases setting time without affecting compressive strength profile. During the industrial trial, the formation of hemihydrate form of calcium sulfate dihydrate has a profound regulatory effect on the setting and ...

International Nuclear Information System (INIS)

Irradiation of ferritic steels with neutrons in the temperture range of room temperature to #propor to# 450deg C results in lattice hardening, which causes an increase in strength and a decrease in ductility. Eight reduced-activation Cr-W-V stels with chromium concentration varying from 2.25 to 12% were irradiated at 365deg C to #propor to# 7 dpa in the Fast Flux Test Facility. A steel with 2.25% Cr and the combination of 2% W and 0.25% V hardened less than those containing vanadium or tungsten alone or a steel with 1% W and 0.25% V. The amount of hardening was similar for Cr-W-V steels with constant vanadium and tungsten concentrations and containing 2.,25, 5, and 9% Cr; a steel with 12% Cr hardened considerably more. Specimens of two conventional Cr-Mo steels, 9Cr-1MoVNb and 12Cr-1MoVW, were also irradiated, and the hardening of these steels was similar to analogous ...

International Nuclear Information System (INIS)

A study was made into microstructure and hardening in austenitic stainless steel 0Kh18N10T irradiated with neon ions (230 MeV) and neutrons (E_n > 0.1 MeV). The experiments were accomplished using an external beam of U-400 cyclotron (Dubna) and EWA reactor (Poland). The dependences of tensile properties, hardening index, microstructure, dislocation density on damaging dose were determined. An attempt is made to reveal the correlation between an yield strength increment and defect cluster accumulation. The interpretation of variations of mechanical properties and microstructure under irradiation is given.

International Nuclear Information System (INIS)

This chapter is an overview of total-ionizing-dose and single-event hardening techniques and should be used as a guide to a range of research publications. It should be stressed that there is no clear and simple route to a radiation-tolerant silicon integrated circuit. What works for one fabrication process may not work for another, and there are many complex interactions within individual processes and designs. The authors have attempted to highlight the most important factors and those process changes which should bring improved hardness. The main point is that radiation-hardening as a procedure must be approached in a methodical fashion and with a good understanding of the response mechanisms involved.

International Nuclear Information System (INIS)

The notion of hardened systems can be found in several applications (nuclear power plants, alarm systems, research installations..). Their development correspond to the functional necessity to take into account a specific radiative environment. The starting point of each hardening study is the definition of the radiative environmental constraints representative of the application. In addition to these external constraints, the specific functional characteristics of each system are considered: control or interface systems in nuclear industry, in-board control systems, remote handling systems, etc. This paper summarizes the methodology followed according to the experience gained in previous studies and anticipating the future needs. (J.S.). 6 refs., 5 figs.

International Nuclear Information System (INIS)

Titanium base 'alpha'-alloys (Pt-7M, RK-20 and Ti-5Al-2Zr-1.5V) are considered for their behaviour under neutron irradiation. The role of alloying elements in radiation hardening is discussed depending of neutron fluence and irradiation temperature. For PK-20 alloy three stages of change in mechanical properties are revealed which are following: incubation period and weak hardening, intense radiation hardening, radiation hardening attenuation. Irradiation temperature rise results in an increase of incubation period and threshold neutron fluence. A special attention is paid to hydrogen absorption in #alpha#-titanium alloys under irradiation. It is concluded that titanium base 'alpha'-alloys are serviceable as structural materials in nuclear plants with allowance made for peculiar features of their radiation behaviour. 4 refs.; 7 figs.; 1 tab.

International Nuclear Information System (INIS)

(Dec 1971). United States Olson, RJ Alexander, DR Antinone, RJ Durham,

International Nuclear Information System (INIS)

High temperature deformation behavior of an alpha + beta titanium alloy Ti-3Al-2.5V has been investigated in the temperature range 830 deg. C to 910 deg. C by using the method of cross head speed cycling. On the basis of flow stress-strain rate and strain rate sensitivity data, it was found that the alloy exhibits a hardening effect in the entire temperature range studied, amount of hardening being significant at the highest test temperature of 910 deg. C which resulted in a degradation of superplastic properties of the alloy. Grain growth in beta-phase due to strain was considered responsible for the hardening effect observed.

International Nuclear Information System (INIS)

... Industry, Material Science Research Laboratory, Yokosuka, Kanagawa (Japan)

Energy Technology Data Exchange (ETDEWEB)

In this study, the cytocompatibility of new 'iron-modified/alpha-tricalcium phosphate (IM/alpha-TCP) and calcium sulfate dihydrate (CSD)' bone cement (IM/alpha-TCP/CSD-BC) intended for spinal applications has been approached. The objective was to investigate by direct-contact osteoblast-like cell cultures (from 1 to 14 days) the in vitro cell adhesion, proliferation, morphology and cytoskeleton organization of MG-63 cells seeded onto the new cements. The results were as follows: (a) quantitative MTT-assay and scanning electron microscopy (SEM) showed that cell adhesion, proliferation and viability were not affected with time by the presence of iron in the cements; (b) double immunofluorescent labeling of F-actin and alpha-tubulin showed a dynamic interaction between the cell and its porous substrates sustaining the locomotion phenomenon on the cements' surface, which favored ...

British Library Electronic Table of Contents (United Kingdom)

In the paper, the effect of Ni content, WC grain size and Mo2C addition on WC-6.25wt%TiC-9.3wt%Ni cemented carbide were investigated to improve the properties of Ni-bonded cemented carbides. The results show that the decrease of Ni content will result in the decrease of transverse rupture strength and increase of hardness; with the decrease of WC particle size, hardness increases due to the refinement of WC grains, however, the transverse rupture strength decrease due to the decrease of Ni binder thickness; Mo2C proves to be an effective grain growth inhibitor. With the increase of Mo2C content, the WC grains are refined and the hardness and transverse rupture strength are improved. Generally, when the Ni content is decreased to 8.4wt%, 13.45mm WC is used and 1.2wt% Mo2C is added, a higher...

Energy Technology Data Exchange (ETDEWEB)

Preliminary studies were preformed to determine whether thermal conductivity of cementitious grouts used to backfill heat exchanger loops for geothermal heat pumps could be improved, thus improving efficiency. Grouts containing selected additives were compares with conventional bentonite and cement grouts. Significant enhancement of grout alumina grit, steel fibers, and silicon carbide increased the thermal conductivity when compared to unfilled, high solids bentonite grouts and conventional cement grouts. Furthermore, the developed grouts retained high thermal conductivity in the dry state, where as conventional bentonite and cement grouts tend to act as insulators if moisture is lost. The cementitious grouts studied can be mixed and placed using conventional grouting equipment.

British Library Electronic Table of Contents (United Kingdom)

Two grades of WC-10wt.%Co cemented carbide with or without addition of Cr3C2/VC grain growth inhibitor during liquid phase sintering were produced with the goal to investigate their reciprocating sliding friction and wear behaviour against WC-6wt.%Co cemented carbide under unlubricated conditions. The tribological characteristics were obtained on a Plint TE77 tribometer using distinctive normal contact loads. The generated wear tracks were analyzed by scanning electron microscopy and quantified topographically using surface scanning equipment. The post-mortem obtained wear volumes were compared to the online assessed wear. Correlations between wear volume, wear rate and coefficient of friction on the one hand and sliding distance and microstructural properties on the other hand were determ...

UK PubMed Central (United Kingdom)

Osteoporotic vertebral fractures often lead to pain and disability. They can be successfully treated, and possibly prevented, by injecting cement into the vertebral body, a procedure known as vertebroplasty....Full Text Available

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An experiment was conducted on the structure of mesoscopic calculating method for cement-based composite materials. The purpose was utilization for the simulation of mesoscale failure processes and the development of new composite materials. Mesh split based on Voronoi polygons was applied as the discrete limit analysis of the cement-based composite materials containing aggregate particles taking the arrangement of random particles into consideration, and a two-dimensional rigid-body/spring model was employed as the model. The nonhomogeneity of concrete was represented by three kinds of different spring parameters which were aggregate, mortar matrix and their interfaces. The simulation results were summarized as follows: The stress-strain curve went into a non-linear state from the 30% of the maximum stress. The generation of interfacial crack started on the side of the aggregate, but the propagation of the crack was stable. Deformation became ...

International Nuclear Information System (INIS)

Red mud is a by-product of the alkaline extraction of aluminum from the bauxite and represents a renewed environmental problem due the significant annual throughput by the plants. In the present work, the pozzolanic properties of Brazilian red mud fired at 600, 700, 800 and 900 deg C were investigated by monitoring lime consumption using DTA analysis and Brazilian standard methodology NBR 5772 (1992). Products and kinetics of hydration were determined in cement pastes produced with 5 and 15% red mud using x-ray diffraction and DTA analysis. Compressive strength and capillary absorption tests were realized on mortars constituted by 5, 10 and 15% red mud in replacement of cement. When calcined at 600 deg C, the red mud develops good pozzolanic properties, and the compressive strength of mortars produced with this waste meet values in accordance with regulatory standard. These results shown than red mud can be used, in partial replacement of ...

International Nuclear Information System (INIS)

The role of helium in a process of embrittlement and hardening of RAFM steels was investigated in EUROFER97 based experimental heats, ADS2, ADS3 and ADS4, that were doped with different contents of natural B and the separated 10B-isotope (0.008-0.112 wt.%). The neutron irradiation of the boron doped and the reference RAFM steels was performed in the Petten High Flux Reactor up to 16.3 dpa at different temperatures between 250 and 450 deg. C. The embrittlement behaviour and hardening was investigated by instrumented Charpy-V tests with subsize specimens. Irradiation lead to generation of 84, 432 and 5580 appm He in ADS2, ADS3 and ADS4 steels, respectively. At irradiation temperatures Tirr ? 350 deg. C the boron doped steals show progressive embrittlement and reduction of toughness with increasing helium amount. The analysis of the hardening vs. embrittlement behaviour at Tirr ? 350 deg. C reveals ...

International Nuclear Information System (INIS)

A study is made of the mechanical properties of vanadium irradiated with fast neutrons up to dose 8.6.10"-"4 dpa, as a function of the temperature of post-radiation annealing. The radiation-annealing hardening (RAH) effect is observed at 300"oC, in agreement with previous studies. It is established for the first time that RAH is accompanied by fall in ductility. A phenomenological model is described which explains the dependence of RAH on radiation dose and temperature, as well as on the content of chemically active alloying impurities. (author).

International Nuclear Information System (INIS)

SGS-Thomson and CNES significantly hardened a power MOSFET transistor against heavy ions and cobalt 60 total dose. The influence of the major technological steps on the component radiation sensitivity has been analyzed. Then the optimization has been carried out, using booth computerized simulation and experimental data. (D.L.). 5 refs., 8 figs.

International Nuclear Information System (INIS)

Power devices such as MOSFETSs and IGBTs, include parasitic structures that can give rise to destructive failures such as breakdown and latch-up. To determine a suitable strategy for device radiation hardening, simulation software like MEDICI-2D can be used to model the effects of technological modifications and device parameters that are difficult to measure experimentally. (authors).

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This work contains 27 chapters which cover recent advances in fracture mechanics applied to cement-based composites: concrete, reinforced concrete, and fiber reinforced concrete. The book, based on a NATO Advanced Study Institute, is a comprehensive survey of treating nonlinearity associated with crack growth in brittle materials such as cement composites, rocks and ice. The book is divided into 8 major themes: advances in nonlinear fracture mechanics; fracture processes; numerical modelling of fracture; experimental methods of determining fracture parameters; damage and continuum modelling; strain-rate and dynamic effects of crack propagation; stress-corrosion, time and temperature effects on fracture; and implications for concrete structures.

International Nuclear Information System (INIS)

Irradiation response on the tensile properties of 9Cr-2W steels has been investigated following FFTF/MOTA irradiations at temperatures between 646 and 873 K up to doses between 10 and 59 dpa. The largest irradiation hardening accompanied by the largest decrease in the elongation is observed for the specimens irradiated at 646 K at doses between 10 and 15 dpa. The irradiation hardening appears to saturate at a dose of around 10 dpa at the irradiation temperature. No hardening but softening was observed in the specimens irradiated at above 703 K to doses of 40 and 59 dpa. Microstructural observation by transmission electron microscope (TEM) revealed that the dislocation loops with the a left angle 100 right angle type Burgers vector and small precipitates which were identified to be M_6C type carbides existed after the irradiation at below 703 K. As for the void formation, the average size of voids increased with increasing ...

International Nuclear Information System (INIS)

This research report discusses the radiation hardening of a commercially available mobile robot, the REMOTEC ANDROS. This hardening effort is culminating in the availability of a megarad hardened mobile platform to access areas in nuclear facilities with extremely high levels of radiation (0.1 to 1 Mrad). These radiation levels may be encountered both during routine repair and monitoring activities and accident situations. The project has completed a phase-I U.S. Department of Energy Small Business Innovative Research contract and is now in a phase-II effort with completion scheduled in early 1995. The research involves the evaluation of the material and electrical components of an ANDROS robot to determine the anticipated radiation hardness of the current production version and evaluation of the components that must be replaced or modified to harden the system to higher radiation levels. The work being ...

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The Nuclear Regulatory Commission stipulates in 10 CFR 61 that disposed low-level radioactive waste (LLW) be stabilized. To provide guidance to disposal vendors and nuclear station waste generators for implementing those requirements, the NRC developed the Technical Position on Waste Form, Revision 1. That document details a specified set of recommended testing procedures and criteria, including several tests for determining the biodegradation properties of waste forms. Information has been presented by a number of researchers, which indicated that those tests may be inappropriate for examining microbial degradation of cement-solidified LLW. Cement has been widely used to solidify LLW; however, the resulting waste forms are sometimes susceptible to failure due to the actions of waste constituents, stress, and environment. The purpose of this research program was to develop modified microbial degradation test procedures that would be more ...

International Nuclear Information System (INIS)

A large matrix of simple alloys and complex commercial type steels was irradiated over a range of fluxes at 60 FC up to a fast fluence of about 3 x 10"2"2 n/m"2. Combined with data in the literature, these results show a negligible effect of flux on irradiation hardening in the range of 2 x 10"1"3 to 5 x 10"1"8 n/m"2-s. This observation lends indirect support to the proposal that the accelerated embrittlement in the High Flux Isotope Reactor surveillance steels was due to an anomalously high level of damage from gamma rays. A weak dependence of hardening on a number of elements, including copper, nickel, phosphorus, molybdenum and manganese, can be described by a simple empirical chemistry factor. Particular combinations of elements resulted in hardening differences of up to about 60% in the complex commercial type steels and up to about 100% in simple model alloys. Direct effects of microstructure appear to be minimal. ...

British Library Electronic Table of Contents (United Kingdom)

The age hardening behavior of Al-4.5%Cu alloy composite reinforced with zircon sand particulates and produced by stir casting route has been investigated in different quenching media viz, water, oil, and salt brine solution (7wt%). Optical microscopy of the as cast alloy composite indicates that the matrix of the composite has the cellular structure. Copper rich CuAl2 precipitates have been found near particle matrix interface. The results of ageing demonstrate that the microhardness of age hardenable Al-Cu based alloy composites depend on the quenching medium in which they are heat treated. Salt brine quenching is faster as compared to water and oil, even if higher strength is obtained but cannot be used for complex shapes and thin sections where oil quenching is the alternative due to mi...

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Due to size and costs of big slewing rings, the common methods of experimental trial and error together with destructive test methods for verification of the inductive hardening process are limited. Thereby it is essential to simulate the hardening process in addition to the tests. With these simulations, it should be possible to get conclusions for the hardening pattern, the residual stress and distortion. With actually existing methods a fully three dimensional simulation is extremely time consuming. For that reason, a new method was developed that combines two dimensional with three dimensional simulation to shorten the time for calculation tremendously. (orig.)

British Library Electronic Table of Contents (United Kingdom)

Bent specimens of A533B steel (0.16wt% Cu) were irradiated at 290degreeC to 1dpa with 6.4MeV Fe3+ ions. Calculated tensile stresses at the irradiated surface were set to 0, 250, 500 and 750MPa. The specimens were subjected to hardness measurements, transmission electron microscopy (TEM) observations and three-dimensional atom probe (3DAP) analysis. The radiation-induced hardening decreased with increasing stress to 500MPa which was near the yield strength. TEM and 3DAP results showed that well-defined dislocation loops and solute clusters were formed. The diameter of dislocation loops increased and the number density decreased when the stress was applied, whereas the diameter and number density of solute clusters decreased. The hardening was mainly attributed to solute cluster formation. A...

International Nuclear Information System (INIS)

Precipitation-hardened single crystals of a beta (bcc) Ti--40 at. percent V--1.0 at. percent Si alloy were deformed in compression at 77 and 298"0K. The dependence of the yield stress upon aging time at 843"0K for solution-treated crystals shows two maxima which are caused by silicide precipitates. The orientation dependence of the yield stress and of the active macroscopic slip plane were determined as a function of aging time. The solution-treated as well as aged crystals exhibit an asymmetry of both the yield stress and the plane of slip, the degree of asymmetry being larger at 77 than at 298"0K. The asymmetry of slip and yielding is not affected by the presence of precipitation hardening. Results indicate that the effect of the dislocation core structure on dislocation motion is independent of the presence of precipitates. (auth).

Science.gov (United States)

In this study, we propose a new bioactive bone cement (BBC), composed of natural bone powder (hydroxyapatite; HA), chitosan powder, and the currently available polymethylmethacrylate (PMMA) bone cement, for use in orthopedic surgeries such as vertebroplasty or as bone filler. Three types of BBCs (BBC I, BBC II, and BBC III) were prepared with different composition ratios. In vitro tests and animal studies were performed with the new BBCs, and with a currently available commercial PMMA bone cement. Surface morphology, chemical composition, changes in pH over time, exothermic temperatures, intrusion, and cellular responses were investigated in vitro. Scanning electron microscopy (SEM) and radiological and histological examinations were performed in animal studies. The results showed that the major components of the BBCs were C, O, Ca, P, Cl, Si, S, Ba, and Mg. The pH values of the BBCs decreased after 1 day, but eventually ...

Science.gov (United States)

The Nuclear Regulatory Commission stipulates in 10 CFR 61 that disposed low-level radioactive waste (LLW) be stabilized. To provide guidance to disposal vendors and nuclear station waste generators for implementing those requirements, the NRC developed the Technical Position on Waste Form, Revision 1. That document details a specified set of recommended testing procedures and criteria, including several tests for determining the biodegradation properties of waste forms. Cement has been widely used to solidify LLW; however, the resulting waste forms are sometimes susceptible to failure due to the actions of waste constituents, stress, and environment. The purpose of this research program is to develop modified microbial degradation test procedures that will be more appropriate than the existing procedures for evaluating the effects of microbiologically influenced chemical attack on cement-solidified LLW. Groups of microorganisms indigenous to ...

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In large samples, the {gamma}-ray count rate of a prompt gamma neutron activation analysis system is a multi-variable function of the elemental dry composition, density, water content and thickness of the material. The experimental calibration curves require tremendous laboratory work, using a great number of standards with well-known compositions. Although a Monte Carlo simulation study does not avoid the experimental calibration work, it reduces the number of experimental calibration standards. This paper is part of a feasibility study for a PGNAA system for on-line continuous characterisation of cement raw material conveyed on a belt (Oliveira, C., Salgado, J. and Carvalho, F. G. (1997) Optimisation of PGNAA instrument design for cement raw materials using the MCNP code. J. Radioanal. Nucl. Chem. 216(2), 191-198; Oliveira, C., Salgado, J., Goncalves, I. F., Carvalho, F. G. and Leitao, F. (1997a) A Monte Carlo study of the influence of ...

Science.gov (United States)

The objective of this study was to simplify the opacifying mixing process of the bone cement and contrast used for percutaneous vertebroplasty (PVP). We performed a biomechanical study of polymethyl methacrylate (PMMA) (Corinplast 3) using three different mixtures of PMMA, monomer, and contrast: group I, 2:1; group II, 3:2; group III, 3:2:1 ratio of powder/monomer/iodinated contrast (Omnipaque). In vitro biomechanical testing of ultimate compressive strength was carried out in all samples. Following the conclusion of a proper bone cement mixture regimen drawn from the in vitro study, PVP was performed in 125 patients: 58 with cancer, 12 with hemangioma, and 54 with osteoporotic fracture. The ultimate compressive strength in group III was decreased by 38% compared to groups II and I. Proper fluoroscopic visualization was achieved in all PVP procedures using this mixture. There were no major complications associated with injection of the ...

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Simultaneous nitriding and ageing heat treatments of precipitation hardenable tool steel was carried out inside a DC-pulsed plasma nitriding reactor. A single heat treatment cycle was done, as the plasma nitriding and age hardening processes occur approximately at the same ranges of temperatures and times. Specimens of Cr-Ni-Mo-Al age hardenable steel, in the solubilized and solubilized and aged conditions, were tested. Plasma nitriding and ageing, carried out at 500 deg. C for times ranging between 2 and 8 h, increased the surface hardness up to 1000 HV, producing case depths between 100 and 200 {mu}m. The core hardness of solubilized samples increased from 30 to 39 Rockwell C after the plasma nitriding treatment proving the possibility of nitriding and ageing at the same treatment cycle. The pre-aged samples did not show any overageing after the simultaneous plasma nitriding and ageing treatments. The corrosion resistance ...

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An overview of the operations of Sandia`s Microelectronics Development Lab (MDL) is to develop radiation hardened IC, but techniques used for IC processing have been applied to a variety of related technologies such as micromechanics, smart sensors, and packaging.

International Nuclear Information System (INIS)

Effect of strain and temperature on high temperature deformation properties of an alpha + beta titanium alloy Ti-6Al-4V has been investigated in the temperature range 800 to 910 deg. C by using the method of cross head speed cycling. On the basis of flow stress strain rate-strain rate sensitivity data and microstructural studies of the undeformed and deformed regions of tensile test pieces, both strain introduced hardening and softening effects were observed during the course of deformation which could be associated with grain coarsening and refining respectively. (author)

International Nuclear Information System (INIS)

The Joint Work Session of the ITER CDA (Conceptual Design Activities) by four parties, (eg. Japan, USA, USSR and EC), which has continued during 3 years from May 1988 to December 1990 was completed successfully. During the CDA, overall diagnostic systems for the next generation machine was performed for the first time and the principal tasks of Diagnostic research and development (R and D) are identified. In this paper, radiation hardening problems, which should be solved for the period 1991 through 1996 of the ITER EDA (Engineering Design Activities), are described. (author).

International Nuclear Information System (INIS)

Some results on mechanical property study of copper and titanium subjected to impact load and next to neutron irradiation are presented. It was shown that shock wave influence involves a substantial shape change of the stress-strain diagram and of respective mechanical characteristics. Yield- and ultimate strength were substantially increased, as well as hardness with a considerable drop of plasticity. Also a heat stability of copper and titanium specimens was studied after being treated with shock-waves and neutron radiation. Results are given of electron microscope study of titanium structure sfter explosion hardening, which caused decomposition of hydride segregations in titanium and increased dislocation density.

International Nuclear Information System (INIS)

The procedure of charge-coupled devices (CCD) are investigated by using MOS capacitors for enhancing their ionizing radiation tolerance. Authors have found that the gate oxidation temperature, thickness of SiO_2 gate insulator and high temperature processes after gate oxidation are crucial for determining the radiation tolerance of the devices, and proposed to decrease the thickness of gate insulator, perform gate oxidation at 1000 deg C by means of dry oxidation and minimize the number of high temperature procedure steps after gate oxidation. All stated above is a necessary preparation for priducing radiation hardened charge-coupled devices.

International Nuclear Information System (INIS)

Full text of publication follows: Radiation hardening and embrittlement due to high-energy neutron radiation around 623 K are the important issues on reduced-activation ferritic/martensitic (RAF/M) steels. It is expected that the improvement of radiation hardening might be one of effective ways to control the mechanical properties of RAF/M after irradiation. It has been reported that the weld joint has less hardening than the base metal from the tensile test results of TIG weldments irradiated in HFIR. This report indicated that radiation hardening can be reduced by the optimization of heat treatment condition for F82H. The purposes of this study are to establish the condition of heat treatment for minimum of radiation hardening in F82H steel using Neutron/Ion-irradiation and to examine a correlation between tensile property and micro-hardness before/after irradiation. The materials ...

International Nuclear Information System (INIS)

Hardened CMOS/SOI 29101 microprocessor, elementary cells and transistor shave been irradiated at levels between 10 Mrad(SiO_2) and 1 Grad(SiO_2) ("6"0Co and 10 keV x-rays). SIMOX buried oxide behavior in the range of 100 Mrad(SiO_2) and a channel-stopped MOS/SOI structure avoiding lateral leakage current are presented. These two items indicate the feasibility of a CMOS/SOI technology operating in the hundred Mrad(SiO_2) range.

International Nuclear Information System (INIS)

Analyses of the roles of cement-based barriers in radioactive waste isolation show that models used to estimate their characteristics during the lifetime of the repository must consider the alteration of material properties with time due to degradation processes. Reinforced concrete barriers at repositories shall be designed in such manner that they fulfil besides isolative capabilities also the required functions of mechanical resistance and stability. Key elements of safety evaluation are mainly the correct selection of materials for mineral composites with cement binder (cements, aggregates, mineral additives and chemical admixtures) and their design, execution of construction works and production of precast concrete containers (continuous casting of concrete - no cold joints, limited number of construction joints, proper placing and consolidation, finishing and curing), strict control of used materials and inspection of ...

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Biomass and nutrient dynamics of black spruce seedlings during the hardening phase of the greenhouse rotation were examined after four pre-hardening fertilization regimes - conventional, constant-rate loading, exponential loading, and high exponential loading (delivering respectively 15, 40, 40 and 60 mg N seedling{sup -1}) - in order to assess nutrient dilution and steady-state nutrition. Although height growth of seedlings had virtually ceased during hardening, shoot biomass increased 99-142% and root biomass increased five- to tenfold depending on treatment. The biomass increase compromised steady-state nutrient status by diluting internal nutrient pools as nutrient supply was unable to keep up with growth. Soil nutrient levels were rapidly depleted during this period because of plant uptake and lack of fertilizer supplementation. Pre-hardening nutrient loading partly countered and delayed dilution ...

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This international conference brought together representatives from industry, academia and government agencies to present the latest developments on the subject of chemical admixtures and superplasticizers in concrete. Recent technological advances in the development of superplasticizers were reviewed, as well as new approaches to manufactured aggregates. The influence of new materials on the rheology of cement systems was discussed, as well as the influence of superplasticizers on various types of aggregates. The addition of hydrophobic admixtures in corrosion prevention strategies were reviewed. Various interactions between cements and superplasticizers were evaluated. Issues concerning adsorption and concrete materials were also investigated. A total of 70 papers were presented at the conference, of which 3 have been catalogued separately for inclusion in this database. refs., tabs., figs.

International Nuclear Information System (INIS)

This report summarizes the results of a research programme which involves the development of a laboratory experimental facility for the simulation and study of hydro-thermo-mechanical processes in saturated geomaterials with low permeability. The experimentation involves a synthetic cement based porous material made of cement grout which possesses permeabilities in the range of dense unfractured sandstones or shale. Specially manufactured pore-pressure transducers were installed within the cylindrical block at locations adjacent to a plane free boundary. The block was saturated with the periodic application of a vacuum. In its saturated state the plane boundary of the block was subjected to heating via a circular heater the temperature of which was maintained constant. The resulting pore pressure generation along with temperature at these locations was monitored continuously. The results of a series of experiments are documented and further ...

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Red mud is a waste generated by the aluminum industry, and its disposal is a major problem for this industry. Very rich in iron, it can be used as cheap pigment for colored concrete. The red coloration can be enhanced by calcination in the range of 600 to 800 C. Such operation also transforms the aluminum hydroxides (goethite and boehmite) and clays minerals into pozzolanic admixtures that are able to consume the calcium hydroxide produced by cement hydration. Thus, it is possible to develop a new admixture for concrete: a pozzolanic pigment. The pozzolanic properties of calcined red mud were investigated by monitoring lime consumption of different mixtures of OPC and red mud. The main products of hydration were C-S-H and mono-carboaluminate (C{sub 4}A{bar C}H{sub 11}). A uniform and durable colored concrete was obtained using white cement interground with 11% of burnt red mud.

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This paper shows some considerations about the cost of wood, steel and cement support pillars in rural power distribution systems. The life span, mechanical properties, cost estimation and general durability of each type of pillar was evaluated, aiming a better selection of the desired one. 6 figs., 8 tabs., 4 refs.

International Nuclear Information System (INIS)

Numerous mercury intrusion porosimetry (MIP) studies have been carried out to investigate the pore structure in cement-based materials. However, the standard MIP often results in an underestimation of large pores and an overestimation of small pores because of its intrinsic limitation. In this paper, an innovative MIP method is developed in order to provide a more accurate estimation of pore size distribution. The new MIP measurements are conducted following a unique mercury intrusion procedure, in which the applied pressure is increased from the minimum to the maximum by repeating pressurization-depressurization cycles instead of a continuous pressurization followed by a continuous depressurization. Accordingly, this method is called pressurization-depressurization cycling MIP (PDC-MIP). By following the PDC-MIP testing sequence, the volumes of the throat pores and the corresponding ink-bottle pores can be determined at every pore size. These values are used to ...

International Nuclear Information System (INIS)

An experimental investigation of the effect of nickel content on irradiation hardening of reactor pressure vessel steels was conducted. The alloys studied, with nickel contents ranging from 0 to 1.7%, included five sets of steels representing variations in copper contents and other metallurgical variables. Various subsets of the alloys were irradiated at selected combinations of flux, fluence, and irradiation temperature. Irradiation hardening was measured by either changes in the uniaxial yield stress or diamond pyramid hardness. Higher hardening rates with increasing nickel were observed in controlled experiments on commercial-type steels containing high copper concentrations (0.4% Cu). The effect of nickel increased with increasing fluence and decreasing temperature. At high fluence (>10"1"9 n/cm"2) the hardening increased with nickel at an average rate of about 100 MPa/%Ni. There also appeared to ...

International Nuclear Information System (INIS)

The first essential before embarking on the radiation-hardening of electrical insulation - mostly magnet coils - in any beam line application is to obtain a reliable estimate of the dose to the components. These are examples ( switchyards at SLAC and LAMPF) where the degree of hardness specified was much higher than was required. Although experience shows that the cost premium for substantial radiation - hardening is of the order of 10%, it has also become clear that well - designed beam line have negligible losses: hardening is required only in the vicinity of targets, collimators or other beam - intercepting devices. Where the beam is deliberately scraped, local shielding will minimize the associated radiation in the surroundings. Electron machines have their own special problems due to synchrotron radiation, so certainly coils and other electrical equipment should be kept away from the beam bend - plane. Because proton ...

Science.gov (United States)

Al2O3-based ceramic is one of the most widely used materials for tools employed in hardened steel turning applications due to its high hardness, wear resistance, heat resistance and chemical stability. The objective of this work is to predict the lives of Al2O3-(W, Ti)C ceramic tools in intermittent turning of hardened AISI 1045 steel by means of damage evolution model taking into account the mechanical loading and thermal effect in the cutting process. A damage evolution model analyzing the RVE with uniformly distributed interacting cracks is constructed based on micromechanics. The calculated results of the proposed damage evolution model are compared with the lives of two kinds of Al2O3-(W, Ti)C ceramic tools obtained through experiments. It is found that the proposed model can be used to predict the lives of the ceramic cutting tools in intermittent turning operation.

Energy Technology Data Exchange (ETDEWEB)

Hard surface finishing represents the final manufacturing step for functional areas of machine elements in state-of-the-art production. Raceways of rolling bearing rings are ground and honed to the required low roughness. Plastic deformation is restricted to a narrow edge zone of the hardened steel. Reheating of the machined components below the martensite tempering or bainite transformation temperature results in a marked decrease of the XRD line width on the surface. The investigated samples are made of through-hardened standard bearing steel 100Cr6 (international denotation: SAE 52100). On the basis of a material model that explains the effect as a complex diffusion process of dislocational carbon segregation, i.e. static strain aging, the measured kinetics of the XRD line width reduction is simulated by an Arrhenius-type equation, which describes the rate-controlling reaction step of temper carbide dissolution. The formation of a small ...

International Nuclear Information System (INIS)

Ten different alloys of zirconium have been tested with regard to the effect of irradiation on their mechanical properties and their sensitivity to environmentally induced failure. Two different environments were used: iodine vapour and liquid cesium with an addition of 2% cadmium. The neutron dose was 10"2"1n/cm"2 (E>1MeV) and the irradiation temperature was about 300 degrees C. All alloy additions increased the irradiation hardening. Especially notable was the large effect of titanium and tin on irradiation hardening. A limited amount of transmission electron microscopy was carried out in order to find an explanation to the effects. The testing in different environments showed that there is no clear correlation between environmental sensitivity and yield stress. For materials of similar yield stress an alloyed material tends to be more sensitive to environmental cracking than a material which only contains oxygen as an impurity. There also ...

International Nuclear Information System (INIS)

Tensile properties of reduced-activation 10Cr-30Mn austenitic steels with carbon levels from 0.003 to 0.55% were investigated over the temperature range from room temperature to 873 K after neutron irradiation in the Japan Materials Testing Reactor at 573 K to 8.5x10"2"2 n/m"2. Irradiation-induced increase in yield stress increased significantly with carbon concentration up to about 0.1% and it was constant above 0.1% carbon. A high density of dislocation loops with small (below 10 nm) and large (20-30 nm) sizes formed during irradiation. The high density, small loops caused a large irradiation hardening, while the large loops contributed only slightly to irradiation hardening. It was considered that carbon atoms formed the small loops together with irradiation defects. The deformation channeling was observed in the irradiated high carbon steels, 0.11 and 0.55% carbon, but not in the very low carbon steel, 0.003% carbon, after deformation near ...

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Alloy 800 from three different commercial heats have been continuously cycled and cycled with a hold period at 922/sup 0/K. The starting microstructures of these heats reflects an inherently wide spectrum of possibilities for Alloy 800. The amounts and morphologies of the TiC and M/sub 23/C/sub 6/ carbides are different among the heats. During cycling, M/sub 23/C/sub 6/ forms intragranularly in a solution annealed heat. This precipitation contributes to the cyclic hardening. Both mill annealed heats of Alloy 800 are stable to carbide precipitation during cycling. The heat with the lower carbon content formed ..gamma..' during cycling but the volume fraction was too low to contribute to hardening. The inclusion of hold periods caused the dislocation substructure to become more diffuse in the mill annealed heats. The cyclic hardening was enhanced with the inclusion of the hold periods but this was not due to any ...

International Nuclear Information System (INIS)

This paper provides a physically-based engineering model to estimate radiation hardening of 9%Cr-steels under both displacement damage (dpa) and helium. The model is essentially based on the dispersed barrier hardening theory and the dynamic re-solution of helium under displacement cascades but incorporating a number of assumptions and simplifications [Trinkaus, J. Nucl. Mater. 318 (2003) 234-340]. As a result, the kinetics of the damage accumulation kept fixed, its amplitude is fitted on one experimental condition. The model was rationalized on an experimental database that mainly consists of ?9%Cr-steels irradiated in the range of 50-600 deg. C up to 50 dpa and with a He-content up to 5000 appm. The test temperature effect is taken into account through a normalization procedure based on the change of the Young's modulus and the anelastic deformation that occurs at high temperature. Despite the large experimental scatter, inherent to the ...

International Nuclear Information System (INIS)

Magnesium alloys have been increasingly used in automotive and electronic industries because of their excellent strength to weight ratio and EMI shielding properties. However, magnesium alloys have low formability at room temperature due to their unique mechanical behavior (twinning and untwining), prompting for forming at an elevated temperature. In this study, a temperature dependent constitutive model for magnesium alloy (AZ31B) sheet is developed. A hardening law based on non linear kinematic hardening model is used to consider Bauschinger effect properly. Material parameters are determined from a series of uni-axial cyclic experiments (T-C-T or C-T-C) with the temperature ranging 150-250 deg. C. The influence of temperature on the constitutive equation is introduced by the material parameters assumed to be functions of temperature. Fitting process of the assumed model to measured data is presented and the results are compared.

Science.gov (United States)

A separation phenomenon occurring during the Charpy impact test of API X80 pipeline steels was investigated in the present study. A detailed microstructural analysis of fractured impact specimens showed that the band structure of bainite elongated along the rolling direction worked as prior initiation sites for separations, and that the number and length of the separations increased with the increasing volume fraction of bainite. In the steels having high work hardenability, tearing-shaped separations were found because the hammer-impacted region was seriously hardened during the impact test, which led to the reduction in the impact toughness. As the test temperature decreased, the tendency toward separations increased, but separations were not found when the cleavage fracture prevailed at very low temperatures. These findings suggested that the formation of bainite and secondary phases should be minimized for preventing or minimizing ...

International Nuclear Information System (INIS)

Microprocessor based ''smart'' pressure, level, and flow transmitters were tested to determine the radiation hardness of this class of electronic instrumentation for use in reactor building applications. Commercial grade Complementary Metal Oxide Semiconductor (CMOS) integrated circuits used in these transmitters were found to fail at total gamma dose levels between 2500 and 10,000 rad. This results in an unacceptably short lifetime in many reactor building radiation environments. Radiation hardened integrated circuits can, in general, provide satisfactory service life for normal reactor operations when not restricted to the extremely low power budget imposed by standard 4--20 mA two-wire instrument loops. The design of these circuits will require attention to vendor radiation hardness specifications, dose rates, process control with respect to radiation hardness factors, and non-volatile programmable memory technology. 3 refs., 2 figs.

British Library Electronic Table of Contents (United Kingdom)

The RD50 collaboration has been exploring the development of radiation hard semiconductor devices for very high-luminosity colliders since 2002. The target fluence to qualify detectors set by the anticipated dose for the innermost tracking layers of the future upgrade of the CERN large hadron collider (LHC) is 1016 1MeV neutron equivalent (neq) cm-2. This is about an order of magnitude higher than the maximum dose for the most exposed silicon detectors in the current machine. RD50 investigates the radiation hardening of silicon sensors from many angles: improvement of the intrinsic tolerance of the substrate material, optimisation of the readout geometry and study of novel design of detectors. A review of some of the recent activities within RD50 is here presented.

British Library Electronic Table of Contents (United Kingdom)

Modifications of the structure and mechanical properties in LiF crystals irradiated with MeV-energy Au ions have been studied using nanoindentation, atomic force microscopy and optical spectroscopy. The nanostructuring of crystals under a high-fluence irradiation (above 1013 ions/cm2)?was?observed. Nanoindentation tests show a strong ion-induced increase of hardness (up?to 150?200%), which is related to the high volume concentration of complex color centers, defect aggregates, dislocation loops and grain boundaries acting as strong barriers for dislocations. From the?depth profiling of the hardness and energy loss it follows that both nuclear and electronic stopping mechanisms of MeV Au ions contribute to the creation of damage and hardening. Whereas the electronic stopping is dominating i...

International Nuclear Information System (INIS)

The introduction of tolerance to radiation (''radiation-hardness'') into large electronic systems is one of the major tasks to which this Handbook will be put. The practices recommended here for inculcating radiation-tolerance in equipment require advanced physical modeling techniques, precise engineering procedures, and firm assurance procedures. The degree to which these procedures should be used in an equipment project can be measured by the severity of the raw radiation environment, the desired reliability of the system, and the requirement of that project for radiation-sensitive technologies. The balance of device/circuit design versus shielding will depend on whether the radiation is highly penetrating -- as in isotope handling or military environments -- or readily attenuated, as in space. In this chapter the authors have attempted to summarize the essential features of the radiation hardening of large assemblies of equipment and how effective control of ...

Energy Technology Data Exchange (ETDEWEB)

Underground injection, compared to other waste disposal methods, is considered to have the advantages of isolating wastes in a confined brine aquifer well below the horizon of human activity and underground sources of drinking water (USDWs). While most of injected wastes move laterally in the injection zone, posing a long-term concern to the human health and environment, a small amount can migrate upward to the upper aquifers, causing a greater threat to the quality of USDWs. Both the dual porosity and the single porosity models were used to investigate the migration of injected wastes through these hydrologic conduits. The results indicate that regional upward migration through an extensive confining formation is a slow process. Nevertheless, injected wastes can move upward rapidly through microannuli and channels in the cement sheath and spread over a distance in the upper aquifer. The wastes can also migrate fast through fractures in the disturbed zone. The ...

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The {sup 176}Ybn,{gamma}{sup 177}Yb-{beta}{sup -}{yields}{sup 177}Lu process was investigated to provide no-carrier-added (nca) {sup 177}Lu. The radiochemical separation of the {sup 177}Lu from the macro-amounts of the ytterbium target based on the cementation process, i.e. the selective extraction of Yb by Na(Hg) amalgam from Cl{sup -}/CH{sub 3}COO{sup -} electrolytes, followed by a final cation exchange purification. The cementation separation process provides a decontamination factor of Yb(III) of 10{sup 4}, the cation exchange purification adding a decontamination factor of >10{sup 2}. The nca {sup 177}Lu is available in radiochemically pure form despite the chemical similarity of the lanthanides with 75{+-}5% overall separation yield within 4-5 h. It can be used to synthesise nca {sup 177}Lu labelled radiotherapeuticals.

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A testing program has been conducted by the Westinghouse Hanford Company to confirm the baseline waste form selection for use in Waste Receiving and Processing (WRAP) Module 2A. WRAP Module 2A will provide treatment required to properly dispose of containerized contact-handled, mixed low-level waste at the US Department of Energy Hanford Site in south-central Washington State. Solidification/stabilization has been chosen as the appropriate treatment for this waste. This work is intended to test cement-based, thermosetting polymer, and thermoplastic polymer solidification media to substantiate the technology approach for WRAP Module 2A. Screening tests were performed using the major chemical constituent of each waste type to measure the gross compatibility with the immobilization media and to determine formulations for more detailed testing. Surrogate materials representing each of the eight waste types were prepared in the laboratory. These surrogates were then ...

International Nuclear Information System (INIS)

Different concrete waste packages have been designed by Electricite de France (EDF) for the long-term storage of radioactive Low Level Waste (LLW). Their main function is to confine radionuclides from the biosphere for three hundred years in a near-surface disposal. According to the transport regulations, a Type-B package is needed for some waste like water filters. The water filters from EDF nuclear power plants are encapsulated in mortar and placed in a concrete container. Transport regulations for these containers have required the development of a methodology for safety assessment. The reference scenario of container degradation during transport considers a 9 m drop and a 800"oC fire for 30 min. First, the different chemical and physical processes involved in the containment of radionuclides are analysed. In particular, the radionuclide transport mechanisms in cement-based materials have been reviewed. Secondly, the effects of a container drop on the mortar and ...

Energy Technology Data Exchange (ETDEWEB)

Acid mine drainage is a serious environmental problem caused by the oxidation of sulfide minerals that releases highly acidic, sulfate, and metals-rich drainage. In this study, alkaline industrial wastes were mixed with acid mine tailings in order to obtain neutral conditions. A series of column leaching tests were performed to evaluate the behavior of reactive mine tailings amended with alkaline-additions under dynamic conditions. Column tests were conducted of oxidized mine tailings combined with cement kiln dust, red mud bauxite, and mixtures of cement kiln dust with red mud bauxite. The pH results show the addition of 10% of alkaline materials permits the maintenance of near neutral conditions. In the presence of 10% alkaline material, the concentration of toxic metals such as Al, Cu, Fe, Zn are significantly reduced as well as the number of viable cells (Thiobacillus ferrooxidans) compared to control samples.

Energy Technology Data Exchange (ETDEWEB)

The strain gradient crystal plasticity theory is applied to study the deformation of planar single crystal with a void under a nominally uniaxial tension. The crystal theory assumes elevated strain hardening due to slip gradients and has a constitutive length scale. The effects of the void size with respect to the constitutive length scale on the single crystal deformation are investigated.

Energy Technology Data Exchange (ETDEWEB)

Stress relaxation was studied at 408 K on AZ31 reinforced by ceramic foam produced by in situ foaming of filler loaded preceramic polymer melt. Reinforcement causes significant enhancement of the resistance against stress relaxation compared to AZ91. It is correlated with hardening by the ceramic skeleton as well as ceramic particles formed in the AZ31-matrix. (orig.)

International Nuclear Information System (INIS)

The influence of additionally injected short-wavelength photobleaching light on the radiation hardness of Ge-doped graded index fibers working at 1,300 nm wavelength is investigated. Predictions are complicated by the fact that more efficient shortwave bleaching light experiences higher radiation-induced loss. Promising results are found for low fiber temperatures (approx-lt -50 C) and bleaching light of about 835 nm wavelength.

International Nuclear Information System (INIS)

The influence of RTA (Rapid Thermal Anneal) treatment on MOS radiation hardness is demonstrated and compared with classical furnace treatment. In the case of the RTA, the oxide trapped charge is found to depend on: (i) the anneal temperature as expected, data are in good agreement with a recently developed model of oxygen out-diffusion; (ii) the location across the wafer with a radial dependence, results could be related to stress induced by thermal gradient.

Energy Technology Data Exchange (ETDEWEB)

Carbide reactions occurring in a precipitation-hardening gamma/gamma-prime Ni-Cr alloy during prolonged high-temperature aging are investigated experimentally. It is found that the decomposition of primary MC carbides, which is accompanied by the precipitation of M23C6 particles, may lead to void nucleation and growth. The effect of carbide transformations on the residual properties of the material at temperatures above the equicohesion temperature is observed at the late stages of aging only. 6 references.

Science.gov (United States)

An instrument has been constructed for the measurement of residual stress in steel. If necessary, large objects can be examined in situ. An account is given of the principles and construction. A special stressing frame provides for calibration. An application to residual stress in gear blanks has established a systematic variation of surface stress with nickel content and confirmed the overall effect of the surface hardening treatment.

Energy Technology Data Exchange (ETDEWEB)

This report describes initial work on the development of solidification systems for sodium nitrate waste and compacted waste. Sodium nitrate waste has been solidified in three types of materials: polyethylene, polyester-styrene (PES), and latex cement. Evaluations of the properties of the waste form, such as the ANS 16.1 leaching test, water immersion test and compressive strength measurements were performed on the waste forms containing various amounts of sodium nitrate. 9 refs., 9 figs., 7 tabs.

Energy Technology Data Exchange (ETDEWEB)

This book provided a set of supplementary papers provided to delegates at the eighth international CANMET/ACI conference on superplasticizers and chemical admixtures in concrete. Recent research on chemical admixtures and superplasticizers was presented along with new approaches to the practical application of concrete admixtures. The presentations highlighted technological advances in the development of superplasticizers and new approaches to the manufacture and implementation of aggregates. Issues regarding the application of plasticizers with various aggregates were addressed, and interactions between cements and superplasticizers were evaluated. Four of the supplementary papers have been catalogued separately for inclusion in this database. refs., tabs., figs.

International Nuclear Information System (INIS)

The article is an overview on atmospheric pollution in Lebanon. It presents an analysis of sources of pollution in the country and their impacts on local and global environment and describes their control. Air pollution is mainly due to the industrial, electrical and transportation sectors. Pollutants from fuel combustion are analyzed. It is estimated that in 2010, CO_2 emissions will reach 5987250 tons, SO_2 emissions is estimated to be 182950 tons, Nox to 105180 and dusts to 4965 tons. CFC consumption and measures of control according to Montreal protocol are described. Consumption of primary energy, consumption of petroleum products, quantity of petroleum in refineries and production of cement in Lebanon are also presented in tables

Energy Technology Data Exchange (ETDEWEB)

The geothermal well-cost model developed by Sandia National Laboratories is being used to analyze the sensitivity of well costs to improvements in geothermal drilling technology. Three interim results from this modeling effort are discussed. The sensitivity of well costs to bit parameters, rig parameters, and material costs; an analysis of the cost reduction potential of an advanced bit; and a consideration of breakeven costs for new cementing technology. All three results illustrate that the well-cost savings arising from any new technology will be highly site-dependent but that in specific wells the advances considered can result in significant cost reductions.

Science.gov (United States)

This construction curriculum guide on masonry for secondary students is one of six developed for inservice teachers at Marianas High School in Saipan. The guide provides the rationale, description, goals, and objectives of the program; the program of studies and performance objectives by levels; samples of lesson plans for effective delivery of instruction; and a listing of references. Concepts covered include orientation to masonry construction, safety, tools and equipment, cement, concrete, concrete block masonry, concrete forms, and concrete reinforcement. Appended materials include transparency copies, tests and answer keys, information sheets, and student activities. (CT)

Energy Technology Data Exchange (ETDEWEB)

A hose lining process, used widely for underground service structures, such as for city gas, and water and sewerage pipes, was adopted to repair interiors of underground wire raceways, and improvements were made for power cable pipe use, including long size construction, inner diameter assurance, and flame retardation. The sealing hose as a lining material consists of a fabric layer woven by warps of polybutylene terephthalate (PBT) and wefts of combined PBT fibers and glassfibers, the fabric being coated with polyurethane resin on one side. The other side of the fabric is coated with heat hardening resin made of epoxy resin as the main ingredient and aromatic amine as the hardening agent to assure close adhesion of the sealing hose onto the pipe interior. Mimic raceways were used to verify the lining material for its abrasion coefficient, mechanical strength, wear resistance, water cut-off performance, chemical resistance, and shape retention ...

International Nuclear Information System (INIS)

Radiation damage of the final optical components in an Inertial Confinement Fusion (ICF) reactor is a crucial issue for development of a laser-fusion reactor. To some extent, this problem will be encountered in the National Ignition Facility (NIF), but there, the integrated radiation dose will be considerably less than that encountered in a future reactor. This extremely harsh radiation environment necessitates shielding the ICF optics from direct neutron and x-ray bombardment. Several approaches have been suggested, such as the use of grazing incidence metal mirrors or fused silica wedge deflectors. While metal mirrors can withstand a larger radiation dose, their focusing qualities pose problems. Therefore wedge deflectors, originally suggested by Lawrence Livermore National Laboratory (LLNL) staff, represent a promising alternative. Radiation hardening of the fused silica deflectors using a new combined thermal/optical annealing approach is examined here as a ...

International Nuclear Information System (INIS)

Total-dose irradiation seriously damages MOS devices and their circuit performance. Threshold voltage shifts, transconductance degradation and increase in off-state leakage current are generally observed for irradiated devices. These instabilities are essentially due to positive and/or negative charge trapping in SiO_2 and interface trap generation at the SiO_2/Si interface. Radiation hardening of CMOS VLSIs is to eliminate these trapping effects, and for this purpose, special considerations for fabrication processes and layout design are necessary. In this paper, basic mechanisms for radiation-induced charge trapping and related effects on MOS devices are reviewed. Also discussed are radiation-hardening technologies from both fabrication-process and layout-design viewpoints. Using these technologies, 1 #mu#m radiation-hard CMOS gate arrays have been successfully developed. Experimental data taken for 2k-gate test chips indicate that radiation ...

Energy Technology Data Exchange (ETDEWEB)

The objective of this program is to tool-harden and make commercially available an existing wireless MWD tool to reliably operate in an air, air-mist, or air-foam environment during Appalachian Basin oil and gas directional drilling operations in conjunction with downhole motors and/or (other) bottom-hole assemblies. The application of this technology is required for drilling high angle (holes) and horizontal well drilling in low-pressure, water sensitive, tight gas formations that require air, air-mist, and foam drilling fluids. The basic approach to accomplishing this objective was to modify GEC's existing electromagnetic (e-m) CABLELESS''{trademark} MWD tool to improve its reliability in air drilling by increasing its tolerance to higher vibration and shock levels (hardening). Another important aim of the program is to provide for continuing availability of the resultant tool for use on DOE-sponsored, and other, ...

International Nuclear Information System (INIS)

Contrary to previous plans for the preparation of diagnostic systems for D-T break-even experiments in the Tokamak Fusion Test Reactor (TFTR), it now appears that a limited Q#approx#1 demonstration can be carried out without constructing a close-fitting igloo radiation shield around the tokamak. In order to assess the impact of D-T operation of TFTR without an igloo shield, particularly with regard to hardening of diagonstic systems, we have mapped neutron and gamma fluxes inside the test cell and test cell basement, using a variety of radiation measurements. The measurements are sufficiently detailed to resolve massive hardware components, such as neutral beams and shielded diagnostic systems, and can be used to predict local fluxes. By comparing the measurements with transport code calculations for the case of a bare tokamak, we conclude that the models have substantially overestimated fluxes both inside and outside the TFTR shield walls. It may be possible to ...

International Nuclear Information System (INIS)

For an assessment of the future US spallation neutron source (SNS) target performance, radiation induced hardening and microstructural evolution were investigated as a function of ion dose for EC316LN stainless steel. Irradiation was carried out using 3.5 MeV Fe"+, 360 keV He"+, and 180 keV H"+ simultaneous ion-beams at 200 deg. C to simulate the damage, He and H production in the SNS target vessel wall. At low dose (< 1 dpa), the predominant defects were black dots whose number density saturated rapidly within a few dpa. This was followed by the evolution of interstitial loops whose number density saturated below 15 dpa. Although He-bubbles were not visible, severely scalloped loops suggested that the implanted He/H atoms existed in the form of small clusters. Comparison with reported neutron irradiation data showed that hardening and ductility loss occurred mostly in the black dot regime (< 1 dpa), but that good ductility (>20% ...

Energy Technology Data Exchange (ETDEWEB)

Effect of the coverage of shot peening, the surface roughness and shot shape, etc. on the stress corrosion cracking (SCC) of Alloy 800 in alkaline solutions was studied. Alloy 800 specimens were cracked in boiling alkaline solutions at the potntial range of {minus} 100 to 0mV in the boiling 50%NaOH+0.3%SiO {sub 2} solution. U bend specimens were tested under the polarized condition at the controlled potential to 0mV, showing that shot peened specimens cracked more easily. Tests of specimens with the same hardness showed that specimens hardened by cold working showed the higher susceptivity than that of surface hardened specimens. In these connections, U bend specimens of higher shot peened coverage were cracked at conditions of 593K and 10%NaOH solution. O-ring specimens of smaller stress level did not show any cracks independent of surface treatments. 8 refs., 9 figs., 5 tabs.

International Nuclear Information System (INIS)

Plasma nitriding is a powerful technique for modifying the phase-structure of the material surface layers, which affect the mechanical, physical and chemical properties of material. The effect of plasma nitriding on the surface properties of three types of steel (low carbon, AISI-304 and H13 (hardened)) has been investigated. The steel samples were plasma nitrided in vacuum of 10"-"1Pa with gas mixture of (N_2, H_2) at 530 Centigrade degree for a duration of 14 hours. Vickers microhardness measurements and XRD phase analysis of the treated and untreated samples were carried out. The diffraction patterns of treated steels revealed that new phases of #gamma#-Fe_4N, #epsilon#-Fe_3N and (Fe,Cr)_2N were formed. The maximum treated depths were about 5, 6 and 45 #mu#m for low carbon, AISI-304 and H13 (hardened) nitrided steel respectively. The microhardness was increased by about 150%, 200% and 140% for low carbon, AISI-304 and H13 nitrided samples ...

International Nuclear Information System (INIS)

The theoretical hardness against total dose of the six-transistor SRAM cell is investigated in detail. An explicit analytical expression of the maximum tolerable threshold voltage shift is derived for two cross-coupled inverters. A numerical method is used to explore the hardness of the read and write operations. Both N- and P-channel access transistors designs are considered and their respective advantages are compared. The study points out that the radiation hardness mainly relies on the technology. Results obtained with the very robust Gate-All-Around process are finally presented.

International Nuclear Information System (INIS)

Generally, Hardening and irradiated brominating phenomena are occurred in the reactor vessel under operation conditions by atomic cavities and creation of impurity atoms which are led by high fast neutron flux. To assure the mechanical integrity of pressure vessel until the end of power plant life after monitoring the sample specimens on the vessel inside, a series of tests is performed over the retrieved surveillance capsule to examine the changes according to the plant operation in accordance with regulations. Monitoring surveillance capsules attached to neutron shield wall of outer core are consists of impact sample, tensile sample and temperature monitor

International Nuclear Information System (INIS)

SP-700, an emerging #beta#-rich #alpha#+#beta# titanium alloy, is designed to improve superplastic formability as well as mechanical properties over Ti-6Al-4V alloy. Owing to its fine microstructure and low #beta#-transus temperature, it is superplastic-formable at temperature below 1,073K (800 C) with low flow stress. Remarkable workability of this alloy is also retained in conventional Manufacturing processes. Another advantage of SP-700 is heat treatment response which includes deep hardenability and quick aging kinetics. Corrosion resistance and machinability are equivalent to or better than Ti-6Al-4V alloy.

British Library Electronic Table of Contents (United Kingdom)

Simplified strain-based fracture mechanics equations, established for external surface cracked pipelines subjected to an external bending load, are presented and used in probabilistic assessment of a pipeline girth weld. The model takes into account several parameters, such as variation in crack depth, crack length, internal pressure and material hardening. The critical strain from ductile tearing in the cracked pipeline is found by using the tangency criterion. The reliability problem is solved using first and second order reliability methods for different pipe dimensions and load levels.

Science.gov (United States)

Deformation experiments performed in-situ in the transmission electron microscope have led to an increased understanding of dislocation dynamics. To illustrate the capability of this technique two examples will be presented. In the first example, the processes of work hardening in Mo at room temperature will be presented. These studies have improved our understanding of dislocation mobility, dislocation generation, and dislocation-obstacle interactions. In the second example, the interaction of matrix dislocations with grain boundaries will be described. From such studies predictive criteria for slip transfer through grain boundaries have been developed.

Energy Technology Data Exchange (ETDEWEB)

The production of many important commercial materials involves the evolution of a complex fluid through a cooling phase into a hardened product. Textile fibers, high-strength fibers(KEVLAR, VECTRAN), plastics, chopped-fiber compounds, and fiber optical cable are such materials. Industry desires to replace experiments with on-line, real time models of these processes. Solutions to the problems are not just a matter of technology transfer, but require a fundamental description and simulation of the processes. Goals of the project are to develop models that can be used to optimize macroscopic properties of the solid product, to identify sources of undesirable defects, and to seek boundary-temperature and flow-and-material controls to optimize desired properties.

International Nuclear Information System (INIS)

Remote-controlled handling systems are required for work to be done in the decommissioning and dismantling of nuclear facilities. These systems are equipped with electronic devices suitable for use in working environments affected by ionizing radiation. The publication explains the step-wise progress achieved for improving the radiation resistance of electronic devices with the example of a four-quadrant controlling device for the motors of a manipulator. The radiation resistance of the device could be enhanced to radiation energies of 5.500 Gy. This means that a manipulator vehicle equipped with this controlling device can take up to approx. 15 kGy all in all, taking into account its own shielding properties. (DG).

International Nuclear Information System (INIS)

Radiation hardening and radiation-induced chromium (Cr) depletion were related to intergranular stress corrosion cracking (IGSCC) response among various stainless steels (SS). Available data on neutron-irradiated materials were analyzed and correlations developed between fluence, yield strength, grain-boundary Cr concentration, and cracking susceptibility in high-temperature water environments. Large heat-to-heat differences in the critical fluence (0.2 neutrons/cm"2 to 2.5 x 10"2"1 neutrons/cm"2) for IGSCC were documented. Variability often was consistent with yield strength differences among irradiated materials. IGSCC correlated better to yield strength than to fluence for most heats, suggesting a possible role for radiation-induced hardening (and microstructure) on cracking. However, isolated heats revealed a wide range of yield strengths (450 MPa to 800 MPa) necessary to promote IGSCC which could not be explained by strength effects alone. ...

Energy Technology Data Exchange (ETDEWEB)

Alloyed steels containing retained austenite after martensitic hardening are widely applied in technical practice. Although many practical investigations have been made into the mechanical behaviour of composite microstructures with retained austenite, there is still a lack of knowledge concerning their fatigue and crack propagation behaviour. For this reason, the author investigated the effects of retained austenite concentration and stability on the transformation and deformation behaviour of hardened states of the steels X210Cr12 and 100Cr6. For this purpose, monotone tensile tests, cyclic tensile pressure tests, and supplementary crack propagation experiments were carried out. The concentrations of retained austenite were varied between 10 and 100% by volume by means of different heat treatments. [Deutsch] Legierte Staehle, die nach martensitischer Haertung noch Restaustenit enthalten, finden in der technischen Praxis verbreitete Anwendung. ...

International Nuclear Information System (INIS)

Effects of helium and hydrogen production on irradiation hardening of martensitic steel F82H (Fe-8Cr-2W-0.2V-0.04Ta-0.1C) were examined by dual or triple beam experiments. The effects of tempering and cold working were also examined. The irradiations were performed at about 500degC to 50 dpa under simultaneous dual beams of 10.5 MeV Fe"3"+ and 1.05 MeV He"+ or triple beams of those and 380 keV H"+ ions. The value of appm-He/dpa for the dual ion beams was about 15, and the values of appm-He/dpa and appm-H/dpa for the triple ion beams were 15 and 15 (or 150), respectively. The hardness of the irradiated specimens measured at room temperature using a micro indentation after the irradiations. Irradiation softening and hardening was observed in F82H-std, F82H+20%CW and a non-tempered F82H steels irradiated at about 500degC to 18 and 50 dpa, respectively, by dual ion beams. The hardness of the specimens irradiated at about 500degC to 18 dpa under ...

International Nuclear Information System (INIS)

Full text of publication follows: Low activation ferritic/martensitic steels are receiving a high priority in the European long term materials research. Although extensively investigated, the available experimental data do not cover all required parameter ranges and cannot unambiguously be used to produce hardening/embrittlement trend curves. Therefore, the main objective of this work is to provide a physically-based engineering model offering a rational to experimental observations. From the literature, experimental data were selected to establish a database that mainly consists of 8 to 9Cr-steels irradiated in the range of 50 to 600 deg. C up to 30 dpa and with a He-content up to 5000 appm. The database includes neutron and proton irradiations, He-implanted as well as B- and Ni-doped steels. Because of the difficulty of interpretation inherent to the Charpy impact test, only tensile data were considered. The difficulty stems from the large range of specimen sizes ...

British Library Electronic Table of Contents (United Kingdom)

Abstract Incomplete dispersion of aggregates is a well known difficulty when analyzing soil texture of Andosols, particularly if no fresh soil material is available. To facilitate such investigations, several dispersion procedures were carried out on air dried samples rich in short range order minerals, originating from selected Andosol profiles (S Mexico). As a result, we propose an improved method based on a sequential chemical treatment with K oxalate, NH4 oxalate, and oxalic acid that reliably removes cementing agents and allows for a stable dispersion of soil particles after addition of Na pyrophosphate. This method was proved to be well reproducible and highly reliable for routine grain size determinations. The potential error caused by the inherent risk of dissolving primary mineral...

International Nuclear Information System (INIS)

The document presents an overview on atmospheric pollution in Lebanon, with an analysis of sources of pollution, their impact on local and global environment and their control.Local causes of pollution are mainly: -Thermal power plants of electric power production which produce 75% SO_2 emission and 60% dust - Industries, especially cement industry - Land transportation which produces 70% NOX emission and 50% CO_2 A description of air pollution caused by these three sectors is revealed. Pollutants derived from fuel combustion are analyzed. It is estimated that in 2010, Co_2 emission will reach 5204450 tons, SO_2 emission will be 136470 tons, NOX emissions 96870 and dust estimated to 4130 tons. CFC consumption and measures of control according to Montreal Protocol are described. Recommendations for control of air pollution in Lebanon within a national policy are presented.

British Library Electronic Table of Contents (United Kingdom)

Abstract The Jebel Ressas Pb-Zn deposits in North-Eastern Tunisia occur mainly as open-space fillings (lodes, tectonic breccia cements) in bioclastic limestones of the Upper Jurassic Ressas Formation and along the contact of this formation with Triassic rocks. The galena-sphalerite association and their alteration products (cerussite, hemimorphite, hydrozincite) are set within a calcite gangue. The Triassic rocks exhibit enrichments in trace metals, namely Pb, Co and Cd enrichment in clays and Pb, Zn, Cd, Co and Cr enrichment in carbonates, suggesting that the Triassic rocks have interacted with the ore-bearing fluids associated with the Jebel Ressas Pb-Zn deposits. The 18O content of calcite associated with the Pb-Zn mineralization suggests that it is likely to have precipitated from a fl...

Energy Technology Data Exchange (ETDEWEB)

Shaped charges were first used more than 30 years ago to perforate casing, cement sheath and reservoir to provide selective communication between the reservoir and well bore. Since then, advances have been made in design of shaped charge sand ancillary equipment. Penetration has increased considerably. Miniaturization of equipment allows passing through relatively small restrictions and effectively communicating with reservoirs. Gun debris has been drastically reduced and in some designs eliminated. Deep reservoirs can be effectively penetrated under down-hole environments exceeding 500 F and 20,000 psi. This work covers the problems encountered and reviews successful devices employing shaped charge and explosive technology.

Energy Technology Data Exchange (ETDEWEB)

A survey is given by the authors of methods of removing the sulphur dioxide content of fumes which can be linked together with producing useful final products. From these technologies those suppling well utilizable gypsum, the Walther process, producing ammonium sulphate, the Wellman-Lord and Bergbau-Forschung processes, respectively adapted to produce sulphuric acid or sulphur, may be of interest. Also in the method of fumes desulphurisation by catalysis by manganese, developed in KBFI, utilizable final products are given. Background of the work of developing this method. Detailed description of the manganese catalytic method based on the use of a red mud desulphurizing agent. By this process, in addition to desulphurizing fumes, enriched red mud with reduced Na/sub 2/O content is produced, which as an iron carrier, is to be reckoned with, or to be used in the cement industry for replacing imported calcined pyrites.

Energy Technology Data Exchange (ETDEWEB)

The first task for remediation actions against underground contamination should be an effective confinement of contamination plumes. Some conventional barrier techniques have been already proved to have sufficient features to prevent such plumes from extending horizontally, but further technical development is required to construct a bottom barrier to stop plumes going deeper. Superjet{sup {trademark}} is a powerful version of the jet grouting method (1) and is characterized by prompt construction of an underground cement pile when exceeds 5 meter in diameter. Its application to a case of construction of underground lapping beams has shown satisfactory completion to sustain underground open space. The results and some basic experiments indicate that this method is technically feasible to build a bottom barrier with a certain mechanical strength.

Energy Technology Data Exchange (ETDEWEB)

Olive field is oil productive from a thin stratigraphically trapped sandstone within the Upper Cretaceous lower Tuscaloosa Formation. The discovery of Olive in 1981 led to renewed interest in the Mid-Dip Tuscaloosa Trend that continues today. Discovery and development was based on the correlation of the B sandstone to a mappable soft seismic event at a depth of 10,500 ft. The field was developed by 25 wells on 40-acre spacing. Olive has been waterflooded since 1983 and is a target for enhanced recovery using carbon dioxide. A total of 7.5 million stock tank bbl or approximately 75% of the original oil in place is estimated to be recoverable by conventional and enhanced recovery methods. The B sandstone was deposited by a northwest to southeast-flowing high-sinuosity meandering river system. Point bar, channel, and channel abandonment deposits are present. The point bar formed from the lateral migration of the river system from west to east, and channel abandonment is evident at the ...

Energy Technology Data Exchange (ETDEWEB)

This report describes work accomplished in the project, titled ''Development of Appropriate Resistance Spot Welding Practice for Transformation-Hardened Steels.'' The Phase 1 of the program involved development of in-situ temper diagrams for two gauges of representative dual-phase and martensitic grades of steels. The results showed that tempering is an effective way of reducing hold-time sensitivity (HTS) in hardenable high-strength sheet steels. In Phase 2, post-weld cooling rate techniques, incorporating tempering, were evaluated to reduce HTS for the same four steels. Three alternative methods, viz., post-heating, downsloping, and spike tempering, for HTS reduction were investigated. Downsloping was selected for detailed additional study, as it appeared to be the most promising of the cooling rate control methods. The downsloping maps for each of the candidate steels were used to locate the conditions ...

International Nuclear Information System (INIS)

The effect of W and V on the high temperature strength properties of 12%Cr-15%Mn austenitic steels was studied from the view point of precipitation hardening and internal stress. The contribution of W addition to the tensile and creep-rupture strength was not so large. By contrast the combined addition of W and V increased the strength considerably. These are resulted from the precipitation of fine vanadium nitride (VN) within grains and the enhancement of M_2_3C_6 type carbide precipitation at grain boundaries. The V added material had large internal stress value which is considered to be due to dislocation movement disturbed by fine vanadium nitrides. (author).

British Library Electronic Table of Contents (United Kingdom)

Irradiation of EP-823 (16Cr12MoWsiVNbB) ferritic-martensitic steel with 7-MeV Ni++ ions and with 30- and 70-keV He+ ions at a temperature of 500?C was followed by an increase in the microhardness, which was due to both radiation point defects and changes in the phase composition and the dislocation structure of the steel. It was found that the dependence of the largest relative increase in the microhardness on the concentration of radiation-induced point defects in the near-surface region of the steel under irradiation with different ions correlated with an analogous dependence of the surface segregation of silicon and chromium.

British Library Electronic Table of Contents (United Kingdom)

Plastic injection molds are an important economic sector due to the increasing use of injection molded plastic components. The selection of mold steel material, its processing conditions, and the way it is machined and hardened all have an impact on how it performs during use across its lifecycle for injection molding. For this study, injection molding conditions seen during high volume manufacturing were used to induce wear that would be typical during processing. A 50wt.% glass fiber reinforced Polybutylene Terephthalate (PBT) was used for the research. After 3000 injection operations, surface damage was found only on the steel used for the stationary half of the mold cavity and the corresponding surface of the molded parts. In contrast, the moving half showed no surface damage or increa...

International Nuclear Information System (INIS)

Weld metal, base material and stainless steel overlay specimens for Charpy tests and static tensile tests were irradiated for a year in a power reactor of the Bohunice nuclear power plant in place of the evaluated surveillance specimens. The material of the specimens was identical with that of the WWER-440 reactor pressure vessels, and was exposed to a fluence of (1.2 - 4.5) x 10"2"3 m"-"2 (E > 0.5 MeV) at approximately 270 degC. Some of the irradiated as well as unirradiated specimens were subjected to regeneration annealing at 475 degC for 168 h. The behavior of the materials after irradiation and annealing was evaluated. (author). 33 tabs., 32 figs., 8 refs.

International Nuclear Information System (INIS)

Early failure of an induction-hardening carbon steel pipe, which was used to transport tailing slurry, was caused by pitting corrosion. The microstructure on the internal pipe surface layer was found being a mixture of martensite, pearlite and ferrite. In this work, the pitting corrosion behavior of each constitute in the microstructure of steel is investigated with electrochemical noise analyses; the electronic properties of passive films were studied with Mott-Schottky relationship. It is found that the passive films formed on the materials under investigation are highly disordered n-type semiconductors. The high-to-low pitting susceptibility is ferrite > martensite > pearlite. The pitting resistance is related to the semiconductive nature of the passive film formed on each constitute. The pitting susceptibility increases with the donor concentration in the passive films. (author)

Energy Technology Data Exchange (ETDEWEB)

The present conference discusses plasma-assisted surface coating/modification processes, the applications to date of ion nitriding, the effects of nitrogen on metal surfaces, ion nitriding mechanisms in Cr, Al and Cr + Al-containing 1040 steel, ion nitriding of Al and its alloys, life enhancement for forging dies, novel anode plasma nitriding developments, and a comparative study of the pulsed and dc ion-nitriding behavior in specimens with blind holes. Also discussed are the influence of heating method on ion nitriding, surface hardening of marage steels by ion nitriding without core hardness reduction, plasma nitriding of nodular cast iron sput gears, NbN composites for superconductors, the carburization of tungsten in a glow discharge methane plasma, economic considerations concerning plasma nitriding, and the corrosion properties obtained by ion nitriding.

Energy Technology Data Exchange (ETDEWEB)

Results of strain controlled fatigue and tensile tests are presented for two nickel base solution hardened alloys which are reference structural alloys for use in several high temperature gas cooled reactor concepts. These alloys, Hastelloy X Inconel 617, were tested at temperatures ranging from room temperature to 871/sup 0/C in air and impure helium. Materials were tested in the solution annealed as well as in the pre-aged condition where aging consisted of isothermal exposure at one of several temperatures for periods of up to 20,000 h. Comparisons are also given between the strain controlled fatigue lives of these alloys and several other commonly used alloys all tested at 538/sup 0/C.

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The conference proceedings contains 30 papers of which five are abstracted separately. The subjects covered include fatigue crack growth in aircraft materials, fractographic measurements, fatigue cracks in nylon 66 blends, cyclic inelastic deformation aspects, prestressing, tensile cracks in creeping solids, creep-crack-growth in 304 stainless steel, high-temperature fatigue, parallel impact loading, numerical fracture dynamic code, J-resistance curves, specimen geometry effects, reactor piping systems, temperature dependence of fracture toughness, small-scale yielding, compact specimens, power hardening materials, semi-empirical fracture analyses, pipeline girth welds, wrought steels, and A36 bridge steels.

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Effect of final temperature and duration of coking on the properties of formed coke from weakly-caking Donetsk and Kuznetsk coals was studied. An increase of the final temperature to 850 C produced significant changes in the mechanical and chemical properties of the coke. Increasing the temperature beyond this point did not affect the mechanical strength significantly, but did increase hardness, real density and electroconductivity of the coke and decrease reactivity. Increasing the period of coking at final temperatures in the 650 and 750 C range, produced insignificant hardening of the formed coke. An objective evaluation of the effect of final temperature can be performed by a series of tests which characterize the resistivity of the formed coke to impact and abrasion and the fine structure of the matter in coke. 9 references.

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The phase transformations and properties of a precipitation-hardened Ni-Cr-based alloy are investigated as a function of C, B, Nb, and Cr contents. It is found that the primary role of Nb consists in the formation of an independent phase, delta-Ni3Nb, a part of a gamma/gamma-prime-delta eutectoid (for high C and B concentrations) and in stimulating the gamma-sigma reaction consecutively with the gamma double prime-delta reaction (for low C and B concentrations). In both cases, the long-term strength characteristics of the Nb-alloyed system are relatively low. The substitution of boron for carbon contributes to a reduction in the number of nucleation sites for topologically close-packed phases and to the formation of more stable (with respect to excess compounds) M3B2 and MB2 borides. The high-boron material exhibits better properties and phase stability under mechanical and thermal loading. 13 references.

Energy Technology Data Exchange (ETDEWEB)

Problems can sometimes occur during the construction of cast in-situ concrete piles. These foundations are formed by drilling a substantial hole into the ground and subsequently filling it with steel reinforcement and wet concrete. Several well-documented cases exist where concrete has not filled the hole and substantial voids have been left in the apparently completed pile. A theory has been developed by which it is possible to identify the nature, size and position of a finite defect within a suspect pile. The technique is based on the concept of receptances, and requires information obtained from vibration tests performed on piles after the concrete has hardened, and the nominal dimensions and material properties of the pile. The application of the theory is demonstrated using data relating to a pile with a known defect. The theory described in this paper ignores the effect of the surrounding soil; this can be included by further development of the theory.

International Nuclear Information System (INIS)

The examination of the high-temperature properties of the alloy Alloy 800HT has shown that both the creep performance and the microstructure of the material can be purposefully set by the initial heat treatment. At the high temperatures applied, (700-900 C), a rapid softening process sets in induced by carbide precipitation, stabilization, and coarsening. This softening process causes creep velocities strongly accelerating as a function of duration of the heat treatment prior to the creep test. The identified cause of the softening effect is a change in particle size that could be verified by SEM and TEM. It is shown that two different carbide precipitate size classes are responsible for the softening effect. While the precipitates dectable by TEM become effective primarily via interactions with dislocations, the carbide precipitates detectable only by SEM contribute to a hardening of the grain boundaries and the matrix.(orig./CB)

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The performance of advanced ceramics under cavitation loading in distilled water was studied by using a laboratory test with vibration-induced cavitation following the pattern of the ASTM standard G32-92. The hardened and tempered martensitic steel 100Cr6 was used as a reference. The aim was to identify mechanisms and the effects of important microstructural parameters on damage of polished Al{sub 2}O{sub 3}, Al{sub 2}O{sub 3}-ZrO{sub 2}, ZrO{sub 2} and SiC ceramics. Results showed that surface damage of brittle ceramics was mainly dominated by intergranular fracture, followed by detachment of single grains or fragments of them. Both incubation time and erosion rate were affected by the amount of initial surface cavities, grain sizes and secondary phases at grain boundaries. (orig.)

Energy Technology Data Exchange (ETDEWEB)

The transport of radon in concrete takes place through the complicated network of interconnected pores that is, at any time, the result of the process of hydration of cement and of moisture distribution and transport. Initially the microstructure of concrete depends on the mix proportions and curing conditions, its time-evolution being conditioned by its surrounding environment. Radon transport will be consequently a function of time, as it is influenced by the changing microstructure (total porosity and its distribution) and by the amount and distribution of the moisture contained in the pore system. A selection of information from the large amount of literature available on concrete is presented in chapter 2. A model that describes the process of hydration, of microstructure development and of moisture transport is presented in chapter 3. The physics of radon diffusion in homogeneous porous materials is outlined in chapter 4. The coupling of the numerical ...

International Nuclear Information System (INIS)

Several metallurgical coatings have been developed that provide good tribological performances in high-temperature liquid sodium and that are relatively unaffected by neutron fluences to 6 X 10/sup 22/ n/cm/sup 2/ (E > 0.1 MeV). The coatings that have consistently provided the best tribological performance have been the nickel aluminide diffusion coatings created by the pack cementation process, chromium carbide or Tribaloy 700 trade mark (a nickel-base hardfacing alloy) applied by the detonation-gun process, and chromium carbide and other hardfacing alloy) applied by the detonation-gun process, and chromium carbide and other hardfacing materials applied by the electro-spark deposition process. The latter process is a relatively recent development for nuclear applications and is expected to find wide usage. Other coating processes, such as plasma-spray coating, sputtering, and chemical vapor deposition, were candidates for use on various components, but the ...

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A review of the various solidification agents and techniques that are currently available or potentially applicable for the solidification of low-level radioactive wastes is presented. An overview of the types and quantities of low-level wastes produced is presented. Descriptions of waste form matrix materials, the wastes types for which they have been or may be applied and available information concerning relevant waste form properties and characteristics follow. Also included are descriptions of the processing techniques themselves with an emphasis on those operating parameters which impact upon waste form properties. The solidification agents considered in this survey include: hydraulic cements, thermoplastic materials, thermosetting polymers, glasses, synthetic minerals and composite materials. This survey is part of a program supported by the United States Department of Energy's Low-Level Waste Management Program (LLWMP). This work provides input into ...

Energy Technology Data Exchange (ETDEWEB)

Nanocrystalline cemented tungsten carbide has attracted considerable interests for use in cutting tool because of its superior mechanical properties. In this study, nano-sized powders of mixed WC and Co were prepared from attrition-milled oxides by a gas reduction-carburization process. The effects of compacting pressure, heating schedule, additional ball-milling, and the presence of a grain growth inhibitor on the sintering properties of the nano-sized WC-Co powders were examined. The grain size and phases in WC-Co alloy were clearly affected by compacting pressure. Because of the trapped gases and the lower melting point of the cobalt binder, when a compact of nano-sized WC-Co powder was sintered through a heating schedule with holding steps, the sintered alloy maintained the small size of WC grains without any {eta} phase. In addition, the additional ball-milling improved the microstructure and mechanical properties of the nano-sized WC-Co powder by producing a ...

British Library Electronic Table of Contents (United Kingdom)

Abstract This research aimed to investigate coarse root systems of Jarrah (Eucalyptus marginata Donn ex Sm.) trees at a 13-year-old restored bauxite mine site in south-western Australia. Excavations in an area with small trees (low-quality site) revealed that deep ripping equipment failed to penetrate the cemented lateritic subsoil, restricting coarse roots (roots >5 mm in diameter) to the top 0.5 m of the soil profile, resulting in fewer (1,344 stems/ha) and smaller (mean height 4.5 m) Jarrah trees. An adjacent area within the same pit (high-quality site), with a stand density of 3,256 stems/ha and a mean height of 8.0 m, had a kaolinitic clay subsoil which coarse roots penetrated to the average ripping depth (1.5 m). Trees at the low-quality site did not penetrate the subsoil with their ...

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In the framework of the feasibility study of radioactive waste disposal in deep geologic formations, a clay formation (named 'argilite de l'Est') has been selected in the Meuse-Haute Marne region (France) for the construction of an underground laboratory. The percolation of alkaline solutions through the argilite has been studied using column experiments with short residence times (30 min). These experiments simulate the leaching of a cement which could be used in the building materials of the laboratory. The alkaline solutions used are mono-cationic solutions of calcium, sodium and strontium. The behaviour of calcium is differentiated from the other cations. For all alkaline solutions (NaOH, Ca(OH){sub 2} or Sr(OH){sub 2}) chemical reactions consuming both hydroxide ions and their associated cations have been evidenced. These reactions are heterogenous reactions of surface adsorption by site ionization. The calcium has a different ...

International Nuclear Information System (INIS)

The broad objective of the engineered barriers studies was to demonstrate and qualify the use of different materials and techniques for sealing water flow paths in the Stripa granite, the mine excavations and the excavation disturbed zones. As may be anticipated from the application of the observational method that forms the basis for design of geotechnical structures, the programme evolved with the finding being made at Stripa and other underground laboratories. During phase 1, the engineered barriers investigations focussed on the heat affected zone of the repository. Specifically, the response of clay buffers and the interactions between waste containers, clay buffer materials and the rock were studied. The phase 2 investigations examined the feasibility of sealing boreholes shafts and tunnels with clay sealants. The phase 3, studies of the ability to grout and seal fractured granite including the excavation disturbed zone were effected and specific studies into the longevity of ...

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Clay-based materials can be cold-stabilized using binder and formed by extrusion. This paper deals with the properties of such materials under the influence of silico-aluminous flying ashes addition. Flying ashes are solid industrial wastes produced by coal combustion. Characteristics of ashes bearing clay-based products, such as dimensional stability, water and mechanical resistance, accelerated aging, are considerably improved with respect to simple clay-binder mixtures. This is principally due to a better hydration of the binder in ashes-bearing mixtures because of: a higher free-water availability as a consequence of the smaller specific surface of ash grains, the filler effect of ash grains which do not participate to the reactions, the specific property of silico-aluminous ashes that can fix the lime in presence of water to produce hydrated compounds. These ashes-bearing clay based materials can have the same qualities as classical building materials but their manufacturing ...

International Nuclear Information System (INIS)

Introduction: There are many problems in the radiological diagnosis of aseptic loosening in total hip arthroplasty. Computed tomography (CT) and magnetic resonance tomography (MRT) are not usable for metallic implants (stainless steel, cobalt alloy, titanium alloy). Material and Methods: From April 1993 to December 1993 15 CFRP non-cemented hip prostheses have been implanted. In a prospective clinical study plane radiographs, CT and MRT have been analysed. Results: Three stems were revised (1 femoral fracture, 1 severe thigh pain, 1 aseptic loosening). CFRP are not visible in plane radiographs. There was a complete (two-third of the cases) or nearly complete (one-third of the cases) small sclerotic interface between the prosthesis and the bone, these were apparent in CT and MRT in stable implant cases and did not have any clinical correlations. Discussion: The small sclerotic interface is quite different in comparison to so called 'Reactive lines'. In one case of ...

Energy Technology Data Exchange (ETDEWEB)

An approach to the ductile fracture of ultra high strength steels has been evaluated. According to this approach the critical crack tip opening, delta/sub IC/, will scale with X/sub 0/(R/sub V//R/sub I/vertical bar/sub R//sub 0/. X/sub 0/ is an average inclusion spacing and (R/sub V/R/sub I/)vertical bar/sub R//sub 0/ is the void radius divided by the radius of the inclusion nucleating the void evaluated at the average inclusion size. AF1410 was selected to test this approach because it has exceptionally high fracture toughness on aging at 510/sup 0/C and because its toughness varies markedly with aging temperature. The results from this and earlier work showed a linear relationship exists between delta/sub IC/ and X/sub 0/(R/sub V//R/sub I/)vertical bar /sub R//sub 0/ for values of delta/sub IC/ ranging from about 8 ..mu..m to 60 ..mu..m. The values of (R/sub V//R/sub I/)vertical bar /sub R//sub 0/ for AF1410 aged at 425/sup 0/C and 510/sup 0/C differed by a factor of two. Because the ...

International Nuclear Information System (INIS)

Post-irradiation annealing was used to help identify the role of radiation-induced segregation (RIS) in irradiation-assisted stress corrosion cracking (IASCC) by preferentially removing dislocation loop damage from proton-irradiated austenitic stainless steels while leaving the RIS of major and minor alloying elements largely unchanged. The goal of this study is to better understand the underlying mechanisms of IASCC. Simulations of post-irradiation annealing of RIS and dislocation loop microstructure predicted that dislocation loops would be removed preferentially over RIS due to both thermodynamic and kinetic considerations. To verify the simulation predictions, a series of post-irradiation annealing experiments were performed. Both a high purity 304L (HP-304L) and a commercial purity 304 (CP-304) stainless steel alloy were irradiated with 3.2 MeV protons at 360 deg. C to doses of 1.0 and 2.5 dpa. Following irradiation, post-irradiation anneals were performed at temperatures ranging ...

Energy Technology Data Exchange (ETDEWEB)

An evaluation of eastern shale oil (ESO) residue as an asphalt additive to reduce oxidative age hardening and moisture susceptibility was conducted by Western Research Institute (WRI). The ESO residue, have a viscosity of 23.9 Pa{lg_bullet}s at 60{degree}C (140{degree}F), was blended with three different petroleum-derived asphalts, ASD-1, AAK-1, and AAM-1, which are known to be very susceptible to oxidative aging. Rheological and infrared analyses of the unaged and aged asphalts and the blends were then conducted to evaluate oxidative age hardening. In addition, the petroleum-derived asphalts and the blends were coated onto three different aggregates, Lithonia granite (RA), a low-absorption limestone (RD), and a siliceous Gulf Coast gravel (RL), and compacted into briquettes. Successive freeze-thaw cycling was then conducted to evaluate the moisture susceptibility of the prepared briquettes. The rheological analyses of the unaged ...

International Nuclear Information System (INIS)

Effect of helium and hydrogen production on radiation-hardening of F82H irradiated by dual or triple beam condition were investigated. The specimens used were four types of ferritic martensitic steels of F82H-std (Fe-8Cr-2W-0.2V-0.04Ta-0.1C) steels tempered at 750degC for 60 minutes, 20% cold worked F82H steel, F82H tempered for 10 minutes and non-tempered F82H steels. The irradiation was performed at 450degC to 50 dpa under simultaneous dual beams of 10.5 MeV Fe"3"+ and 1.05 MeV He"+ or triple beams of those and 380 keV H"+ ions. The ratios of He (appm)/dpa and H(appm)/dpa were 15 nad 15 (or 150) for dual and triple ion beams. The hardness of the irradiated specimens measured at room temperature using a micro indentation after the irradiations. The hardness in these F82H steels irradiated at 450degC to 18 dpa under triple beam irradiation was harder than that under dual beam irradiation. Irradiation softening and hardening under dual beams was ...

International Nuclear Information System (INIS)

We investigate the efficacy of mitigating radiation-based single event effects (SEE) within circuits incorporating SiGe heterojunction bipolar transistors (HBTs) built with an N-Ring, a transistor-level layout-based radiation hardened by design (RHBD) technique. Previous work of single-device ion-beam induced charge collection (IBICC) studies has demonstrated significant reductions in peak collector charge collection and sensitive area for charge collection; however, few circuit studies using this technique have been performed. Transient studies performed with Sandia National Laboratory's (SNL) 36 MeV 16O microbeam on voltage references built with N-Ring SiGe HBTs have shown mixed results, with reductions in the number of large voltage disruptions in addition to new sensitive areas of low-level output voltage disturbances. Similar discrepancies between device-level IBICC results and circuit measurements are found for the case of digital shift registers implemented ...

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Titanium alloys are characterized by poor tribological properties, and the traditional use of titanium alloys has been restricted to nontribological applications. The deposition of a well adherent diamond coating is a promising way to solve this problem. In this study, the tribological properties of diamond-coated titanium were studied using a pin-on-disk tribometer, and the results were compared with those of pure titanium and plasma nitrided titanium. The tribological behavior of pure titanium was characterized by high coefficient of friction and rapid wear of materials. Plasma nitriding improved the wear resistance only under low normal load; however, this hardened layer was not efficient in improving the wear resistance and the friction properties under high normal load. Diamond coating on pure titanium improved the wear resistance of titanium significantly. Surface profilometry measurement indicated that little or no wear of the diamond coating occurred under ...

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The effect of accelerated thermal cycling on a joint between modified 9Cr-1Mo steel (Grade 91) and Alloy 800 welded with Inconel 82 and 182 filler material is discussed. This is part of a trimetallic transition joint involving Grade 91-Alloy 800-316LN austenitic stainless steel for steam generator application. It has been shown that, during thermal cycling following the typical post-weld tempering treatment at 760 deg. C for 2 h, no carbon diffusion occurs from the ferritic steel towards the weld metal. There is, in fact, a hardness increase at the ferritic steel/weld metal interface which is probably a result of work hardening. Carbon migration sets in only after unusually long post-weld heat treatments for 20 and 50 h at 760 deg. C followed by thermal cycling. Significantly, even under the most severe thermal cycling test conditions imposed, no cracking or oxide notching could be detected, thus demonstrating the superior performance potential of modified 9Cr-1Mo ...

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By using a plasma nitriding procedure at the PUPR Mirror Cusp Plasma machine, surface hardness is increased in 302/304-type stainless steel samples by exposing them to high-ion-density plasma at high vacuum. This method successfully dopes the surface of the material with strengthening nitrogen ions, without the use of chemical procedures that sacrifice the resistance to corrosion of the given material. A 500 V negative bias is placed on the sample exposed to the nitrogen plasma, where high-energy ions are therefore attracted and immersed into the metallic matrix microns into the surface of the stainless steel. This potential maintains a constant surface temperature at approximately 800 deg. C. The plasma parameters including ion density and plasma temperature were diagnosed using single Langmuir probes. The stainless steel samples were then tested using scanning electron microscopy (SEM), and Vickers micro-hardness testing to determine the increment in the surface harness of the ...

International Nuclear Information System (INIS)

In interventional radiology (IVR) of cerebral aneurysms, it is important to understand the form and physical relationships between the cerebral aneurysm and the surrounding vessels. However, because the vessels in the head area are highly complex, it can be difficult to comprehend the structure using conventional angiography. Therefore, three-dimensional rotational angiography (3D-RA) has been used in recent years. This article discusses studies of the spatial resolution of 3D-RA. We reconstructed 3D-RA of an acrylic slit phantom (slit widths: 0.5, 0.75, 1.0, 1.5 mm) and examined spatial resolution by visual evaluation and profile curves. When the slit phantom was arranged to avoid the effect of beam hardening, the spatial resolution of 3D-RA was found to be as high as 0.75 mm. When the slit phantom was placed orthogonal to the rotational axis of the C-arm, the spatial resolution of 3D-RA was decreased because of the cone angle effect of X-rays. However, it was ...

Energy Technology Data Exchange (ETDEWEB)

Microhardness decarburization profiles are often used in the industry to estimate the carbon distribution in steels. For quantitative evaluation, an analysis based on diffusion theory must be performed, the fundamentals and mathematical basics of which are presented. If the relationship between hardness and carbon content is known, microhardness-distance curves of steels can be analyzed in this way. For martensitic grades, for instance, a linearized expression holds in the concentration range from 0.15 to 0.6 m.% C. Microhardness depth profiles of higher carbon steels and other microstructures, however, are also evaluated in the literature. The applicability of quantitative diffusion modeling is discussed in detail. Through hardenable rolling bearing steel 100Cr6 (1.3505, SAE 52100) serves as model material: carbon concentration-distance curves are measured with high accuracy by secondary ion mass spectrometry (SIMS) and compared with microhardness decarburization ...

International Nuclear Information System (INIS)

The world fusion program has advanced to the stage where it is appropriate to construct a number of devices for the purpose of burning DT fuel. In these next-generation experiments, the expected flux and fluence of 14 MeV neutrons and associated gamma rays will pose a significant challenge to the operation and diagnostics of the fusion device. Radiation effects include structural damage to materials such as vacuum windows and seals, modifications to electrical properties such as electrical conductivity and dielectric strength and impaired optical properties such as reduced transparency and luminescence of windows and fiber optics during irradiation. In preparation for construction and operation of these new facilities, the fusion diagnostics community needs to work with materials scientists to develop a better understanding of radiation effects, and to undertake a testing program aimed at developing workable solutions for this multi-faceted problem. A unique facility to help in this ...

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The aim of this work is to describe the processes during plasma nitriding of Nb-containing, powder metallurgy prepared (PM) tool steel. PM steel was studied containing 2.5% C, 3.3% Si, 6.2% Cr, 2.2% Mo, 2.6% V, 2.6% Nb and 1.0% W, produced by melt atomization and hot isostatic pressing. The hardened and tempered steel was plasma nitrided at temperatures ranging from 470 to 530 deg. C. The nitriding time was 30-180 min. Optical microscopy, electron microscopy, XRD, EDS, WDS and hardness measurements were used to study the steel's properties, microstructure, phases and chemical composition. The nitriding temperature of 470 deg. C was found to be unsuitable for practical use because the layers prepared at this temperature were non-uniform. The compound layer formed by M{sub 2,3}(C,N) and M{sub 4}N was found after nitriding at temperatures of 500 and 530 deg. C for at least 60 min. The effect of niobium on the formation of this layer was studied.

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Duplex-coating procedures consisting of plasma nitriding and Me-C:H hard coating lead to an improved performance of the devices because the Me-C:H coating is supported by the nitrided phase and, therefore, the `eggshell-effect` is avoided. Furthermore, this support leads to a higher load-bearing capacity of the thin film. Two standard procedures (classical high-pressure plasma nitriding and unbalanced magnetron sputtering of Ti-C:H) were performed subsequently to prepare the duplex coatings on X20Cr13 ferritic stainless steel. The corrosion resistance of the steel could be improved by nitriding at 450 C compared to the untreated ferritic substrate. The roughness is determined by the nitriding step. The weakest point of the coating is the transition zone between the nitrided and the untreated substrate and not the interface between the Ti-C:H coating and the nitrided substrate as shown by the Rockwell and scratch tests. The adhesion of the duplex structure (plasma nitriding and Ti-C:H ...

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The goal of this work was to develop a process flow diagram to economically produce a clean-burning fuel from fine Illinois coal. To accomplish this, the process of pelletizing fine coal with calcium hydroxide, a sulfur capturing sorbent, was investigated. Carbonation, which is the reaction of calcium hydroxide with carbon dioxide (in the presence of moisture) to produce a bonding matrix of calcium carbonate, was investigated as a method for improving pellet quality and reducing binder costs. Proper moisture level is critical to allow the reaction to occur. If too much moisture is present in a pellet, the pore spaces are filled and carbon dioxide must diffuse through the water to reach the calcium hydroxide and react. This severely slows or stops the reaction. The ideal situation is when there is just enough moisture to coat the calcium hydroxide allowing for the reaction to proceed. The process has been successfully demonstrated on a pilot-scale as a method of ...

Science.gov (United States)

The paper briefly describes the nuclear reactor facilities at Sandia Laboratories which are used for simulating nuclear weapon produced neutron environments. These reactor facilities are used principally in support of continuing R and D programs for the Department of Energy/Office of Military Application (DOE/OMA) in studying the effects of radiation on nuclear weapon systems and components. As such, the reactors are available to DOE and DOD agencies and their contractors responsible for the radiation hardening of advanced nuclear weapon systems. Emphasis is placed upon two new reactor simulation sources; the Sandia Pulse Reactor-III (SPR-III) Facility which enhances the neutron exposure volume capabilities over those presently available with the existing SPR-II Facility, and the Upgraded Annular Core Pulse Reactor (ACPR) Facility which enhances the neutron exposure capabilities over those of the former ACPR Facility.

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Aerospace gas turbine disks operate in an environment of relatively high stresses caused by centrifugal forces and elevated temperatures. These severe conditions necessitate the need for materials with high temperature strength and good low cycle fatigue resistance. One class of alloys used for this task is the nickel base superalloys, out of which, IN 718 is the most widely used in the aerospace industry. The properties of IN 718 are attributed to the combined effects of the chemistry, heat treatment, and microstructure. The chemistry is tailored not only for solid solution strengthening but also for precipitation hardening developed during heat treatment, which combined with a fine grained microstructure lead to excellent mechanical properties such as low cycle fatigue resistance and elevated temperature strength. The properties of a gas turbine disk are sensitive to the microstructure, in particular the grain size, which is dependent on the processing history. ...

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Spray depositing allows the production of steels having a structure which is free of any macro-segregation, homogeneous and equiaxed. Nevertheless the spray deposition of steels shows some effects that have to be regarded as disadvantages. A porous region at the billet border and a rather coarse-grained microstructure can be noticed. As a result, in the presented work the influence of a subsequent hot rolling and a following heat treatment on microstructure and mechanical properties has been investigated. For this purpose the bearing steel SAE 52100 has been used as master material. The initial microstructure has been transformed to a homogeneous equiaxed fine-grained pearlitic microstructure without any remaining porosity. To get use of the characteristic properties of this high-strength steel an isothermal bainitic hardening has been carried out. Information about the mechanical properties of this material has been gained by tensile and fatigue tests. For fatigue ...

International Nuclear Information System (INIS)

The problems of the thermal stress in concrete structures are roughly divided into the initial stress due to setting heat and the stress due to external temperature after hardening. The initial stress exists in every concrete structure, and it is usually neglected in beams and columns, but it must be taken into account in case of the foundation mat structures in nuclear power stations, for example. In this paper, (1) the results of measurement of temperature, strain and stress in each lift at the time of and after placing concrete in the foundation mat of a nuclear power station and the comparison of them with the results of analysis, (2) the results of measurement of the temperature and stress in a foundation mat, which was carried out to rationalize the design method for the raft type foundation mats in thermal power stations, and (3) the results of examination on the analysis model, external force conditions and boundary conditions used for the design are ...

Energy Technology Data Exchange (ETDEWEB)

Al{sub x}Ga{sub 1{minus}x}P layers (0 {le} x {le} 0.7), with thicknesses of {ge}1 {micro}m were grown on Si (100) wafers by metal-organic molecular beam epitaxy (MOMBE) at 450 C. Transmission electron micrographs of the single crystal films revealed that the microstructure contains stacking faults and microtwins especially near the interface as well as both threading and misfit dislocations. Hardness and elastic modulus were measured using a Nanotest 500 indenter, which can probe the film properties without influence from the substrate. The hardness H varies linearly according to (11.8 {minus} 2.3x) GPa. The absence of alloy hardening is due to the fact that there is no difference in atomic size of Al and Ga. The indentation modulus E/(1{minus}v{sup 2}) decreases monotonically from 136 GPa for GaP to 129 GPa for Al{sub 0.7}Ga{sub 0.3}P and bows only slightly (about 2%) below the straight line of linear interpolation.

International Nuclear Information System (INIS)

Protocols were standardized for in vitro propagation of several elite and diverse banana accessions using shoot tip explants. Tissue culture raised plants were field planted at multiple locations. Studies were undertaken for the induction of mutations using multiple shoot cultures of six selected cultivars, Shreemanti (AAA), Basrai (AAA), Lal Kela (AAA), Rasthali (AAB), Karibale Monthan (ABB) and a wild diploid (BB). These shoot cultures were irradiated at different doses of gamma rays (0-100 Gy) and subcultured thrice (up to M_1V_3) to separate shimeras, followed by induction of rooting (M_1V_4). In general, the rate of multiplication had a negative association with the dose of gamma rays. Enhanced multiplication of shoots was noticed at lower doses. The proliferation of shoots was arrested beyond 50 Gy and a dose of 70 Gy was completely lethal for all the genotypes studied. The rooted plantlets were hardened in the green house and in the early stages of field ...

Energy Technology Data Exchange (ETDEWEB)

In this paper, we define, design and test a radiation tolerant autonomous monitoring tool for nuclear embedded applications. The goal of the instrumentation system was to record the values of some parameters such as dose, temperature or vibrations appearing inside the containment building of nuclear power plants. The knowledge of these parameters will be a good help for predictive maintenance of the power plant components. For the design of the monitoring tool, we rely on commercial-off-the-shelf (COTS) low power electronic components to use battery-supplied power. A large amount of components starting from discrete transistors or logic units to memories and micro-controllers was associated to define and design a prototype. We then confirm the environment conditions tolerance estimated to up to 2 kGy of total dose and 80 C for temperature by on-line irradiation experiments for individual components and functions and prototypes. Two different sets of about 60 systems were realised as ...