WorldWideScience
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Web Policies & Notices  

Science.gov (United States)

Resources & Guides Schools Airmen Testing FAA Academy Federal Aviation Administration Web Policies & Notices Print Email | Updated: 4:46 pm ET March 2, 2011 Employment...

2011-10-08

2

Ultrasensitive fluorescence detection of DNA  

Science.gov (United States)

Progress on Ultrasensitive fluorescence detection of DNA is briefly described. (CBS)

1991-01-01

3

Radionuclide X-ray fluorescence analysis. 3: Examples of application in practice  

Science.gov (United States)

Examples are given of the applicability and importance of radionuclide fluorescence analysis as a

1973-01-01

4

Fluorescent Silicate Materials for the Detection of Paraoxon  

Science.gov (United States)

... significantly lower limits of detection. The complex fluorescence spectra of these constructs indicated that only a portion ...

2010-03-19

5

ASE FILE  

Science.gov (United States)

radionuclide X-ray fluorescence analysis: the resolving power of the ... The radiation detectors used in radionuclide X-ray fluorescence ...

7

Free amino acid distribution in plasma and liver of juvenile cobia (Rachycentron canadum) fed increased levels of lizardfish silage  

British Library Electronic Table of Contents (United Kingdom)

Abstract Juvenile cobia (Rachycentron canadum) (100-g) were fed four moist diets (447-476-g-kg-1-dry-wt) where 0, 130, 260 or 390-g-kg-1 of concentrated lizardfish (Saurida undosquamis) silage replaced fresh lizardfish, respectively. Blood and livers were sampled at 0, 6, 12, 24 and 48-h postfeeding at the end of the 3-week experiment. At 6-h postfeeding in all groups, maximum concentrations of most plasma essential amino acids were observed, while significantly lower levels of most non-essential amino acid levels were recorded compared to the other sampled times. At 6 and 12-h after feeding, the concentration of most plasma free amino acid (FAA) increased with an increase in dietary fish silage levels. Most FAA in livers of all groups peaked at 12 and 24-h postfeeding. However, at 48-h po...

2011-01-01

8

Analysis of tritium mission FMEF/FAA fuel handling accidents  

Energy Technology Data Exchange (ETDEWEB)

The Fuels Material Examination Facility/Fuel Assembly Area is proposed to be used for fabrication of mixed oxide fuel to support the Fast Flux Test Facility (FFTF) tritium/medical isotope mission. The plutonium isotope mix for the new mission is different than that analyzed in the FMEF safety analysis report. A reanalysis was performed of three representative accidents for the revised plutonium mix to determine the impact on the safety analysis. Current versions computer codes and meterology data files were used for the analysis. The revised accidents were a criticality, an explosion in a glovebox, and a tornado. The analysis concluded that risk guidelines were met with the revised plutonium mix.

1997-11-18

9

Realistic Probability Estimates For Destructive Overpressure Events In Heated Center Wing Tanks Of Commercial Jet Aircraft  

Energy Technology Data Exchange (ETDEWEB)

The Federal Aviation Administration (FAA) identified 17 accidents that may have resulted from fuel tank explosions on commercial aircraft from 1959 to 2001. Seven events involved JP 4 or JP 4/Jet A mixtures that are no longer used for commercial aircraft fuel. The remaining 10 events involved Jet A or Jet A1 fuels that are in current use by the commercial aircraft industry. Four fuel tank explosions occurred in center wing tanks (CWTs) where on-board appliances can potentially transfer heat to the tank. These tanks are designated as ''Heated Center Wing Tanks'' (HCWT). Since 1996, the FAA has significantly increased the rate at which it has mandated airworthiness directives (ADs) directed at elimination of ignition sources. This effort includes the adoption, in 2001, of Special Federal Aviation Regulation 88 of 14 CFR part 21 (SFAR 88 ''Fuel Tank System Fault Tolerance Evaluation ...

2007-02-07

10

Radionuclide X-ray fluorescence analysis. 2: Detection of the X-ray fluorescence radiation excited by radionuclide radiation  

Science.gov (United States)

This investigation describes the technique for the detection of the X-ray fluorescent radiation

1972-01-01

11

Radiation streaming analysis of horizontal penetrations in calandria vault of TAPP-3, 4  

International Nuclear Information System (INIS)

This paper consists the radiation streaming analysis of Horizontal penetrations in Calandria Vault of 540 MWe PHWR. There are total 19 penetrations, penetrating east and west walls of calandria vault of 540 MWe PHWR. These penetrations are provided to accommodate ion chambers. HFUs and SDS - 2. Penetrations described here are not present in 220 MWe units except for ion chamber penetrations. As these penetrations are in accessible area, a detailed analysis has been carried out to find out the neutron and gamma dose rates around these penetrations when reactor is operating. Analysis has been carried out using computer code DOT-III and MCNP. Predictions by this method compare well with the measurements at ion chamber locations at KGS-1,2. (author)

2006-11-13

12

Vessel elements present in the secondary xylem of Trochodendron and Tetracentron (Trochodendraceae)  

British Library Electronic Table of Contents (United Kingdom)

For almost 150 years, the two monotypic genera Trochodendron and Tetracentron (Trochodendraceae) have been considered to share an unusual and primitive feature in angiosperms - the lack of vessels in their wood. Therefore, they have been classified in a basal position in the angiosperms. Our observations by light microscopy, low-vacuum environmental scanning electron microscopy (ESEM) and high-vacuum scanning electron microscopy (SEM) both in fresh and FAA-fixed materials consistently showed the presence of tracheary elements differentiated into two types in both genera. In Trochodendron, the tracheary elements can be divided into perforate vessel elements and imperforate fiber-tracheids and tracheids. The vessel elements show end and lateral walls. The pits on the end walls are elongate- ...

2011-01-01

13

The fluorescence properties and NMR analysis of protopine and allocryptopine  

International Nuclear Information System (INIS)

The fluorescence properties of protopine and allocryptopine in aqueous and organic environments are described for the first time. The fluorescence of alkaloids and their pH-dependent interconversion to cationic forms (transannular interaction) were studied using steady-state and time-resolved fluorescence techniques. For the analysis of tricyclic base and cis/trans tetracyclic cations of the alkaloids, NMR and X-ray crystallography were used. - Highlights: ? We describe fundamental fluorescence characteristics of alkaloids protopine and allocryptopine. ? We analyzed the pH-dependent transitions and cis/trans isomerization. ? These two alkaloids can be better distinguished by their fluorescence decay characteristics. ? The fluorescence parameters are related to the NMR and crystallographic structural data.

2011-07-01

16

Investigation of subsurface exploration methods for prevailing geologic conditions in South Carolina  

Science.gov (United States)

Subsurface conditions at sites in the coastal plains region of South Carolina were investigated using standard penetration and mechanical quasi-static cone penetration tests. The penetration test results are compared with measured static axial pile capacity. The cone penetration test results are compared with stratigraphy and soil types encountered at each site. Results show that with certain limitations, cone penetration test results can be used to assess general stratigraphy and soil type and predict static axial pile capacity with reasonable accuracy.

1985-11-01

17

Detection and Analysis of Tumor Fluorescence Using a Two-Photon Optical Fiber Probe  

UK PubMed Central (United Kingdom)

The utility of a two-photon optical fiber fluorescence probe (TPOFF) for sensing and quantifying tumor fluorescent signals was tested in vivo. Xenograft tumors were developed in athymic mice using MCA207...Full Text Available

2004-06-01

18

x - NASA Technical Reports Server  

Science.gov (United States)

Mar 1, 2011 ... Radionuclide X-ray fluorescence analysis. 2: Detection of the X-ray fluorescence radiation excited by radionuclide radiation ...

19

Radionuclide X-ray fluorescence analysis. 1: Excitation of X-ray fluorescense radiation by nuclear radiation  

Science.gov (United States)

The principles of radionuclide excitation of X-ray fluorescence radiation and its application in

1972-01-01

20

Observation of Fluorescence for some lanthanides in LiCl-KCl molten salt media at high temperature  

Energy Technology Data Exchange (ETDEWEB)

To our knowledge, the fluorescence studies of lanthanides in LiCl-KCl eutectic molten salt at a high temperature are not reported yet. The fluorescence of the lanthanide-ions was generally decreased when the temperature was increased. Moreover, the fluorescence of the lanthanides was strong when the sample was solidified to or from the melt. The temperature, where the fluorescence was decreased, was identified to be different depending on the species of the lanthanides and the substrates was considered to possibly be from quenching of the fluorescence due to either the collisions of melted samples induced by high temperature media or the re-absorption of fluorescence by the samples. Several comparison experiments were performed to explain and understand this phenomenon and improve the fluorescence. In this way, an on-line monitoring of ...

2008-08-15

21

NASA Technical Reports Server - Radionuclide X-ray fluorescence ...  

Science.gov (United States)

Aug 1, 1972 ... The principles of radionuclide excitation of X-ray fluorescence radiation and its application in analytic chemistry are discussed.

23

Shielding augmentation for HFU penetration in calandria vault of 540 MWe PHWR  

International Nuclear Information System (INIS)

This paper consists the radiation streaming analysis of Horizontal Flux Unit (HFU) penetrations in Calandria Vault of 540 MWe PHWR. There are total 7 HFU penetrations on west wall of calandria vault. As these penetrations are in accessible area, a detailed analysis has been carried out to find the neutron and gamma dose rates around these penetrations when reactor is operating. Analysis has been carried out Using the computer code MCNP and DOT-III. Based on the predictions at HFU penetrations, shielding arrangement was recommended. Neutron and gamma dose rate higher than estimated were observed at TAPS-4. This was because of installed shield not being similar to recommended one due to site conditions. Subsequently semi-empirical calculations using measured data were carried out by MCNP to further augment the existing shield taking into consideration the space limitations at site. ...

2006-11-13

24

A combined numerical and theoretical study on the penetration of a jacketed rod into semi-infinite targets  

British Library Electronic Table of Contents (United Kingdom)

A combined numerical and theoretical study is conducted herein on the penetration of semi-infinite targets by jacketed rods with different r"j"0/r"c"0 ratios where r"j"0 and r"c"0 are the radii of the jacket and the core, respectively. The numerical results show that for smaller r"j"0/r"c"0 ratios the u-v relationship changes only a little compared to that of unitary long rod penetrator of the same core material, hence, the u-v relationship of unitary (homogeneous) long rod penetration is also applicable for jacketed rod penetration. Model for cratering in semi-infinite targets by jacketed rods is then suggested by using the laws of conversation of mass, momentum and energy, together with the u-v relationship of unitary (homogeneous) long rod penetration and an analytical model for predict...

2011-01-01

28

Radionuclide X-ray fluorescence analysis  

International Nuclear Information System (INIS)

Slovak 1973. 164 p. Czechoslovakia Havranek, E. Bumbalova, A. Svitel,

1973-01-01

29

Preparation and Characterization of Fe3O4/CdTe Magnetic/Fluorescent Nanocomposites and their Applications in Immuno-labeling and Fluorescent Imaging of Cancer Cells  

UK PubMed Central (United Kingdom)

The synthesis of a new kind of magnetic, fluorescent multifunctional nanoparticles (~30 nm in diameter) was demonstrated, where multiple fluorescent CdTe quantum dots (QDs) are covalently linked...Full Text Available

2010-01-19

30

NONDESTRUCTIVE DETERMINATION OF AIRBORNE LEAD ...  

Science.gov (United States)

... NONDESTRUCTIVE DETERMINATION OF AIRBORNE LEAD PARTICULATES BY THE RADIONUCLIDE X-RAY FLUORESCENCE ANALYSIS. ...

32

Lidar techniques for search and rescue  

Energy Technology Data Exchange (ETDEWEB)

Four techniques for using LIDAR in Search and Rescue Operations will be discussed. The topic will include laser retroreflection, laser-induced fluorescence in the visible, laser-induced fluorescence during daylight hours, and laser-induced fluorescence in the uv. These techniques use high-repetition rate lasers at a variety of frequencies to induce either fluorescence in dye markers or retroreflection from plastic corner cubes on life preservers and other emergency markers.

1985-01-01

37

Endoscopic treatment of persistent thoracobiliary fistulae after penetrating liver trauma  

UK PubMed Central (United Kingdom)

Background:This study evaluated the outcomes of patients with complex or persistent thoracobiliary fistulae following penetrating liver trauma, who underwent endoscopic biliary intervention...Full Text Available

2009-03-01

38

Retrieval of chlorophyll a concentration from a fluorescence enveloped area using hyperspectral data  

British Library Electronic Table of Contents (United Kingdom)

It is acknowledged that fluorescence line height (FLH) algorithms are still hampered by the uncertainty of fluorescence peak position. The fluorescence peak moves to longer wavelengths with the increase of chlorophyll a concentration. In this article, the fluorescence enveloped area (FEA), which integrates the fluorescence height and the fluorescence peak position, was used to estimate the chlorophyll a concentration in the coastal waters of the Pearl River Estuary. The FEA algorithm was developed from in situ data of chlorophyll a concentration, total suspended matter (TSM) concentration and above-water remote sensing reflectance, which were collected at 37 sampling stations in the Pearl River Estuary during two cruises. The results showed that the FEA algorithm made a better estimation o...

2011-01-01

39

Penetrants for hot surfaces in welding inspection: experimental work and first results; Penetrants pour le controle de surfaces chaudes lors du soudage: etude experimentale et premiers resultats obtenus  

Energy Technology Data Exchange (ETDEWEB)

Preliminary results of studies into penetrant testing at high surface temperature (up to 200 deg.C), are presented. Tests were performed to assess the effectiveness of red dye penetrants using Al and NiCr samples containing artificial as well as natural discontinuities. The test results will be used in due course to formulate a specification for non-destructive testing procedure qualification at non-standard (i.e. outside 16-52 deg.C) temperatures.

2000-04-01

40

Radionuclide X-ray fluorescence analysis  

International Nuclear Information System (INIS)

The author's achievements in the title field are summarized and discussed. The following topics are dealt with: (i) principles of radionuclide X-ray fluorescence analysis; (ii) mathematical methods in X-ray fluorescence analysis; (iii) Ross differential filters; (iv) application of radionuclide X-ray fluorescence analysis in the coal industry (with emphasis on the determination of the ash content, sulfur content, and arsenic content of coal); and (v) evaluation of the X-ray fluorescence analyzer from the radiological safety point of view. (P.A.).

1994-01-01

41

Analytic description of X-ray fluorescence intensity as a function of the particle size in powder samples and pulp upon X-ray fluorescence analysis  

International Nuclear Information System (INIS)

Analytic expression is derived for X-ray fluorescence dependence on the particle size of powder and slurry media. The expression is obtained for a model of powder medium containing particles of different size and random distribution in the bulk of the sample. Limiting cases of homogeneous and slurry-like media are considered and expressions for calculation of the fluorescence intensity are derived. The results reasonably match the experiment for binary powder mixtures and thus provide evaluation of the powder particle size on the fluorescence intensity for multicomponent polydisperse powder medium

2007-11-01

42

Downward penetration of hot UO/sub 2/ into basalt concrete  

Energy Technology Data Exchange (ETDEWEB)

Following a postulated meltdown accident, the integrity of containment building structural material under attack by hot molten core debris and the safeguard of environment against radiological releases constitutes the final line of defense in PAHR safety assessment. Such assessment requires a good knowledge of UO/sub 2//interaction and penetration with different types of concrete. The present study focuses on the phenomena associated with core debris interaction/penetration with substrate basalt concrete.

1983-01-01

43

Intrinsic fluorescence of the amniotic fluid  

International Nuclear Information System (INIS)

The intrinsic fluorescence of clear amniotic fluid from third-trimester pregnancy is reported. The fluorescence intensity peaked at 405 nm when excited by ultraviolet light in the range of 310 to 360 nm. All of the 33 samples tested fluoresced, and their emission spectrum had the same shape, varying only in magnitude. Changing sample temperature (20 to 50 C) and sample pH (7.2 to 7.7) had little effect on the emission spectrum. The same fluorescence, with higher intensity, was observed when some newborn urine was tested. The fluorescence of amniotic fluid may provide a new tool to determine fetal age, fetal organ maturation, and fetal distress. (author).

1981-01-01

44

The efflux of a fluorescent probe is catalyzed by an ATP-driven extrusion system in Lactococcus lactis.  

UK PubMed Central (United Kingdom)

Many bacteria, both gram positive and gram negative, extrude in an energy-dependent manner the fluorescent pH indicator 2',7'-bis-(2-carboxyethyl)-5[and -6]-carboxyfluorescein (BCECF) (D. Molenaar,...Full Text Available

1992-05-01

45

Six orders of magnitude dynamic range in capillary electrophoresis with ultrasensitive laser-induced fluorescence detection  

UK PubMed Central (United Kingdom)

An ultrasensitive laser-induced fluorescence detector was used with capillary electrophoresis for the study of 5-carboxy-tetramethylrhodamine. The raw signal from the detector provided roughly...Full Text Available

2009-12-15

46

Real-Time Assessment of Cardiac Perfusion, Coronary Angiography, and Acute Intravascular Thrombi Using Dual-Channel Near-Infrared Fluorescence Imaging  

UK PubMed Central (United Kingdom)

ObjectivesWe have developed an image-guided surgery system based on invisible near-infrared (NIR) fluorescent light. Presently, the only clinically-available NIR...Full Text Available

2009-07-01

47

Rate of allosteric change in hemoglobin measured by modulated excitation using fluorescence detection.  

UK PubMed Central (United Kingdom)

We have measured the forward and reverse rates of the allosteric transition of hemoglobin A with three CO molecules bound by using modulated excitation coupled with fluorescence quenching of the DPG...Full Text Available

1989-10-01

48

Radionuclide X-ray fluorescence analysis of waste water from the production of citric acid  

Energy Technology Data Exchange (ETDEWEB)

Radionuclide X-ray fluorescence analysis was used for the determination of iron, calcium, potassium, copper, manganese and zinc in waste water from the production process of citric acid.

1982-02-18

49

Radionuclide X-ray fluorescence analysis of waste water from the production of citric acid  

International Nuclear Information System (INIS)

Radionuclide X-ray fluorescence analysis was used for the determination of iron, calcium, potassium, copper, manganese and zinc in waste water from the production process of citric acid. (author).

1982-02-01

50

Photophysics and optical switching in green fluorescent protein mutants  

UK PubMed Central (United Kingdom)

We demonstrate by using low-temperature high-resolution spectroscopy that red-shifted mutants of green fluorescent protein are photo-interconverted among three conformations and are, therefore, not...Full Text Available

2000-03-28

51

Near Infrared-Fluorescent and Magnetic Resonance Imaging Molecular Probe with High T1 Relaxivity for In Vivo Multimodal Imaging  

UK PubMed Central (United Kingdom)

A new gadolinium chelating NIR fluorescent molecular probe increases T1 relaxivity of water protons, facilitating combined optical and magnetic resonance imaging.

2010-06-07

52

Improved DNA Sequencing Accuracy and Detection of Heterozygous Alleles Using Manganese Citrate and Different Fluorescent Dye Terminators  

UK PubMed Central (United Kingdom)

The use of dideoxynucleotide triphosphates labeled with different fluorescent dyes (dye terminators) is the most versatile method for automated DNA sequencing. However, variation in peak heights reduces...Full Text Available

1999-06-01

53

Electron Transport-Dependent Chlorophyll-a Fluorescence Quenching by O2 in Various Algae and Higher Plants  

UK PubMed Central (United Kingdom)

A comparison of chlorophyll-a fluorescence in brown algae (Macrocystis integrifolia, Fucus vesiculosis), green algae (Scenedesmus obliquus, Ulva sp.)...Full Text Available

1983-12-01

54

Early Detection of Bronchial Lesions Using Lung Imaging Fluorescence Endoscope  

UK PubMed Central (United Kingdom)

The performance of the Lung Imaging Fluorescence Endoscope (LIFE) system was compared with conventional bronchoscopy in 158 patients: 68 patients with invasive cancer, 42 patients with abnormal sputum...Full Text Available

1999-01-01

55

Coupling of Pressure-Induced Structural Shifts to Spectral Changes in a Yellow Fluorescent Protein  

UK PubMed Central (United Kingdom)

AbstractX-ray diffraction analysis of pressure-induced structural changes in the Aequorea yellow fluorescent protein Citrine reveals the structural basis for the continuous...Full Text Available

2009-09-16

56

Contribution to the radionuclide x-ray fluorescence analysis of human blood and plasma  

International Nuclear Information System (INIS)

A photon-induced x-ray fluorescence method allowing the simultaneous determination of iron, copper, zinc, bromine and rubidium in human blood and blood plasma samples is described. The method is reliable and has a good sensitivity for a wide range of elements. (author).

1986-04-01

57

Binding of a Fluorescent Lipid Amphiphile to Albumin and its Transfer to Lipid Bilayer Membranes  

UK PubMed Central (United Kingdom)

Kinetics and thermodynamics of the binding of a fluorescent lipid amphiphile, Rhodamine Green™-tetradecylamide (RG-C14:0), to bovine serum albumin were characterized in an equilibrium...Full Text Available

2003-01-01

58

A novel fluorescent pH probe for expression in plants  

UK PubMed Central (United Kingdom)

BackgroundThe pH is an important parameter controlling many metabolic and signalling pathways in living cells. Recombinant fluorescent pH indicators (pHluorins) have come into vogue...Full Text Available

59

8. Application of radionuclide X-ray fluorescence analysis in other fields of science and technology  

International Nuclear Information System (INIS)

Certain applications are described of radionuclide X-ray fluorescence analysis in the ore dressing industry, in the manufacture of building materials, in metallurgy, pharmacy, in the chemical, photographic and paper industries, in space exploration, in archeology and for measuring the thicknesses of thin layers of coatings. (ES).

1983-12-01

60

Synthesis of histidine-stabilized cadmium sulfide quantum dots: Study of their fluorescence behaviour in the presence of adenine and guanine  

British Library Electronic Table of Contents (United Kingdom)

Cadmium sulfide particles have been synthesized in the aqueous medium using the amino acid histidine as a stabilizing agent. These particles demonstrate the phenomenon of size quantization effect. The fluorescence of histidine-stabilized CdS was found to be enhanced and quenched by the addition of DNA bases adenine and guanine, respectively. The fluorescence enhancement of CdS in the presence of adenine has been explained on the basis of interaction between the quantum dot stabilizer and the amino group of adenine. Quenching of CdS fluorescence by guanine occurs due to interaction of the substrate with the quantum dot surface.

2010-01-01

61

Radionuclide X-ray fluorescence analysis using semiconductor detectors  

International Nuclear Information System (INIS)

Czech May 1979. p. 32-33. Czechoslovakia Benada, J. Spacek, B. Ustav

1979-05-01

62
63

Microcomputers in radionuclide X-ray fluorescence analysis  

International Nuclear Information System (INIS)

Czech Apr 1986. p. 51. Czechoslovakia Cechak, T. Kluson, J. Ceske

1986-04-01

64

Ion Transport Measurements in a Multi-Dipole Argon Plasma by Broadband Laser Induced Fluorescence  

International Nuclear Information System (INIS)

Argon ion laser induced fluorescence measurements were carried out in a multipolar filament discharge with a broadband diode laser centered on 668 nm, which stimulated a transition from the metastable state in Ar(II) 3d4F7/2 to 4p4D05/2. The intensity of the induced fluorescence at 442 nm was maximized by the optimization of the discharge parameters and the laser power. From the recovery of the background fluorescence after the laser was turned off, the ion diffusion coefficient was deduced and compared with the result inferred from the experiments of ion acoustic wave (IAW) damping.

2009-06-01

65

Development of time-resolved laser fluorescence spectrometry for on-line uranium checking in solutions of the Purex reprocessing process; Developpement de la spectrofluorimetrie laser a resolution temporelle pour le controle en ligne de l`uranium dans les solutions du procede de retraitement purex  

Energy Technology Data Exchange (ETDEWEB)

The Purex process and the fluorescence spectrometry are first recalled, then uranyl fluorescence is studied in a pure nitric medium without other elements to establish a theoretical model, allowing the description of uranium fluorescence signal with a general equation. The influence of different parameters (temperature, inhibitors, dynamic quenching of iron and cerium) is investigated to develop the model. A quantitative analysis method without addition of reagents is proposed to validate the model.

1992-02-25

66

Determination of ash content in coal by means of backscattered X-ray radiation and X-ray fluorescence analysis, and devices manufactured by the PAR company  

Energy Technology Data Exchange (ETDEWEB)

Discusses methods for determining ash content in coal using backscattering in X-ray fluorescence. The following aspects are evaluated: principle of ash content determination, energy sources, factors that influence measurement accuracy, reliability. Types of X-ray fluorescence analyzers developed in Czechoslovakia and manufactured in the Czech Republic are comparatively evaluated. Operation of the RPM 113.1 radionuclide X-ray fluorescence analyzer developed by the PAR company and used for measuring ash content in coal and coal calorific value is discussed. 7 refs.

1993-09-01

67

3. Physical foundations and methodology of radionuclide X-ray fluorescence analysis  

International Nuclear Information System (INIS)

The physical foundations are described of radionuclide X-ray fluorescence analysis (RXFA) and the table shows the values of K- and L-absorption thresholds and the K- and L-line energies of elements. The calculation of the intensity of characteristic radiation during RXFA proceeds from relations derived for conventional X-ray fluorescence analysis. The choice of the radionuclide source is ruled by the nature of the analysed substance and the used detection technique. The diagram shows the areas of radionuclide sources and the energy of the fluorescence radiation of elements. The table shows the spectra of radionuclide sources suitable for the purposes of RXFA measured by semiconductor Si(Li) and Ge(Li) detectors. (ES).

1983-12-01

68

Utilization of Fluorescent Microspheres and a Green Fluorescent Protein-Marked Strain for Assessment of Microbiological Contamination of Permafrost and Ground Ice Core Samples from the Canadian High Arctic  

UK PubMed Central (United Kingdom)

Fluorescent microspheres were applied in a novel fashion during subsurface drilling of permafrost and ground ice in the Canadian High Arctic to monitor the exogenous microbiological contamination of...Full Text Available

2005-02-01

69

Radionuclide X-ray fluorescence determination of Mn, Fe, Cu, Zn and Pb in wastewaters and sludges from wastewater treatment plants in Bratislava (SR)  

International Nuclear Information System (INIS)

Radiometric X-ray fluorescence analysis was used for the determination of Mn, Fe, Cu, Zn and Pb in wastewater and sludges from three wastewater treatment plants in Bratislava (SR). Metals were determined in wastewaters after preconcentration by 8-hydroxyquinoline and in sludges by drying and pressing to pellets. "2"3"8Pu and "1"0"9Cd was used for excitation of fluorescence radiation. (author).

1997-01-01

70

Radionuclide X-ray fluorescence analysis of components of the environment  

International Nuclear Information System (INIS)

The physical foundations and methodology are described of radionuclide X-ray fluorescence analysis. The sources are listed of air, water and soil pollution, and the transfer of impurities into biological materials is described. A detailed description is presented of the sampling of air, soil and biological materials and their preparation for analysis. Greatest attention is devoted to radionuclide X-ray fluorescence analysis of the components of the environment. (ES).

1983-01-01

71

Present state of radionuclide X-ray fluorescence analysis in coal mining  

International Nuclear Information System (INIS)

Applications of X-ray fluorescence analysis in coal mining and geology are briefly described based on results published in Czechoslovakia as well as abroad over the past 3 years. Particular attention is paid to the rapid determination of the ash content of coal using portable radionuclide X-ray fluorescence analyzers that are being developed in Czechoslovakia. (author).

1990-01-01

72

Pharmaceutics | Special Issue: Molecular Imaging  

Wastenet

...) Abstract: Fluorescence microscopic imaging is widely used in biomedical research to study molecular and cellular processes in cell culture or tissue samples. This is motivated by the high inherent sensitivity of fluorescence techniques, the spatial resolution that compares favorably with cellular dimensions, the stability of the fluorescent labels used and the sophisticated strategies that have been developed for selectively labeling target molecules. More recently, two and ...

73

Laser induced fluorescence measurements of the mixing of fuel oil with air  

Energy Technology Data Exchange (ETDEWEB)

We report on measurements of the mixing of fuel oil with air at atmospheric pressure in an industrial premixed gas turbine burner. The concentration of the vaporized fuel oil was measured with laser induced fluorescence. We reason that the fuel oil concentration can be considered with good accuracy as proportional to the fluorescence intensity. (author) 6 fig., 3 refs.

1999-08-01

74

Contribution to the in vitro multielement X-ray fluorescence analysis of human soft tissues  

International Nuclear Information System (INIS)

Determination of Mn, Fe, Ni, Cu, Zn, and Pb in human soft tissues by radionuclide X-ray fluorescence analysis (using "2"3"8Pu and "1"0"9Cd sources) is described. The results of multielement XRS analysis of selected human tissues are tabulated. They are in good agreement with the literature data. It is concluded that X-ray fluorescence technique is a suitable method for trace element determination. (author).

1986-11-01

75

Barrier filter for fluorescence microscopy of strongly autofluorescent plant tissues. Application to actin cables in Chara.  

Science.gov (United States)

A liquid barrier filter for use in fluorescence microscopy of strongly autofluorescent plant tissues is described. The filter consists of a methanol solution of cupric chloride and ferric chloride and isolates fluorescein fluorescence from the strong red autofluorescence of photosynthetic plant tissues. Subcortical actin cables in the giant alga Chara are being visualized through use of this filter together with heavy meromyosin labeling. PMID:90068

1979-05-01

76

Behavior at under-film corrosion tips of Zn-Fe alloy coated steel sheets. Zn-Fe gokin mekki koban no tomakushita fushoku ni okeru fushoku sentanbu no kyodo  

Energy Technology Data Exchange (ETDEWEB)

From a macroscopic point of view, corrosion of Zn alloy coated steel sheet occurs by the coating preceding corrosion mechanism; microscopically, however, the coated layer corrosion velocity in the tip of corrosion is different. In order to find the main factors of under-film corrosion of Zn and Zn-Fe alloy coatings in the salt water spray atmospheric exposure test, the correlation between point inflation-exfoliation width and chlorine penetration behavior, point adhesion, and the difference in chlorine penetration behavior due to alloy coating components were investigated. Consequently, the following results were obtained: 1. The better correlation was observed between chlorine penetration distance and point inflation-point exfoliation width. 2. The durability of coating against chlorine penetration improved by increase in point adhesion and Zn content in the coating layer. 3. Zn-Fe (10-20%) alloy ...

1990-09-01

77

Study of penetration depth for V"+ with low energy implanted in peanut seeds  

International Nuclear Information System (INIS)

The penetration depth and concentration distribution for vanadium ions with low energy implanted into the dry peanut seeds is determined by scanning electron microscope and X-ray energy dispersion spectrometer. The results show that the depth-concentration distribution is a Gaussian distribution with a long tail and the maximum penetration depth is about 13.6 #mu#m for V"+ with 200 keV in cotyledon of the peanut. The experimental result of the implanted V"+ range in the peanut seeds is compared with the calculating value of the TRIM95

2002-11-01

78

Inland penetration of sea breeze around Wolsung NPP site  

Energy Technology Data Exchange (ETDEWEB)

A three dimensional sea-land breeze model has been employed for the study on the inland penetration of sea breeze around Wolsung NPP site. In this study, the sea breeze simulation was carried out under the weak northwesterly geostrophic wind (3.2 m/s, 339 .deg.) at 850 hPa in Spring. The results showed that sea breezes developed near Wolsung site penetrated into about 20 km inland under the weak northwesterly geostrophic wind in Spring. This result agreed with observation data around Wolsung site on May 1996.

1997-07-01

79

Inland penetration of sea breeze around Wolsung NPP site  

International Nuclear Information System (INIS)

A three dimensional sea-land breeze model has been employed for the study on the inland penetration of sea breeze around Wolsung NPP site. In this study, the sea breeze simulation was carried out under the weak northwesterly geostrophic wind (3.2 m/s, 339 .deg.) at 850 hPa in Spring. The results showed that sea breezes developed near Wolsung site penetrated into about 20 km inland under the weak northwesterly geostrophic wind in Spring. This result agreed with observation data around Wolsung site on May 1996.

1997-11-06

80

W-7405 - NASA Technical Report Server (NTRS)  

Science.gov (United States)

W. Wayne Scott and R. G. Alsmiller, Jr. ABSTRACT. Comparisons of the results obtained for a hypothetical problem with four different proton penetration ...

81

Strikingly different penetrance of LHON in two Chinese families with primary mutation G11778A is independent of mtDNA haplogroup background and secondary mutation G13708A  

British Library Electronic Table of Contents (United Kingdom)

The penetrance of Lebers hereditary optic neuropathy (LHON) in families with primary mitochondrial DNA (mtDNA) mutations is very complex. Matrilineal and nuclear genetic background, as well as environmental factors, have been reported to be involved in different affected pedigrees. Here we describe two large Chinese families that show a striking difference in the penetrance of LHON, in which 53.3% and 15.0% of members were affected (Pin vivo mitochondrial oxidative metabolism as described in a previous study. Evolutionary analysis failed to indicate any putatively pathogenic mutation that cosegregated with G11778A in these two pedigrees. Our results suggest that the variable penetrance of LHON in the two Chinese families is independent of both their mtDNA haplotype background and a seconda...

2008-01-01

82

SPACE STATION INTEGRATED WALL DESIGN AND PENETRATION  

Science.gov (United States)

screens of fine wire was placed between the gun barrel and the panel to determine whether the gun performance was repeatable. The transducers were placed ...

83

Potassium Transport in Corn Roots 1  

UK PubMed Central (United Kingdom)

The relative transport capabilities of the cells of the root periphery and cortex were investigated using a variety of experimental techniques. Brief (30 seconds to 1 minute) exposures with the penetrating...Full Text Available

1983-10-01

84

On penetration effect in M1 component of 70.45 keV #gamma#-transition in "1"7"7Ta  

International Nuclear Information System (INIS)

... gamma radiation l conversion m conversion mev range 10-100 mixing ratio

1987-04-14

85

Investigation of drug delivery by iontophoresis in a surgical wound utilizing microdialysis  

UK PubMed Central (United Kingdom)

Purpose:This study investigated the penetration of lidocaine around and through a sutured incision following the application of iontophoretic and passive patches...Full Text Available

2008-08-01

86

Discrete Element Method for Modeling Penetration  

Science.gov (United States)

... In fact, for dynamic loading, the ultimate compressive strength can be more than doubled (Bischoff and Perry 1991), whereas the ultimate uniaxial ...

2006-07-01

87

Analytical Summary. Part 4. The Theory of Armor Penetration  

Science.gov (United States)

... F ? (28.3)(108) in an isotherme.l deformation with stationary principal axes of strain rate, but the component might be as small as F2= (19-3)(100) ...

1946-05-01

88

Ultrafast fluorescence dynamics of Sybr Green I/DNA complexes  

British Library Electronic Table of Contents (United Kingdom)

The ultrafast dynamics of the DNA fluorescent dye Sybr Green I (SG) has been studied in buffer, single-stranded (ssDNA), double-stranded (dsDNA) and triple-stranded DNA (tsDNA). The fluorescence quantum yield of SG increases dramatically when bound to DNA (including tsDNA). The fluorescence dynamics of the free SG has shown two decay components with 0.15-0.4ps and 1.3-2.1ps time constants, depending on the fluorescence wavelength. Upon binding to DNA, the dynamics becomes slower exhibiting four decay components. This is mainly due to the restriction of the internal motions of the dye caused by the relatively rigid environment of the dye complexed with DNA.

2010-01-01

89

Spatial fluorescence cross correlation spectroscopy by means of a spatial light modulator  

CERN Document Server

Spatial Fluorescence Cross Correlation Spectroscopy is a rarely investigated version of Fluorescence Correlation Spectroscopy, in which the fluorescence signals from differ-ent observation volumes are cross-correlated. In the reported experiments, two observation volumes, typically shifted by a few $\\mu$m, are produced, with a Spatial Light Modulator and two adjustable pinholes. We illustrated the feasibility and potentiality of this technique by: i) measuring molecular flows, in the range 0.2 - 1.5 $\\mu$m/ms, of solutions seeded with fluorescent nanobeads or rhodamine molecules (simulating active transport phenomenons); ii) investigating the perme-ability of phospholipidic membrane of Giant Unilamellar Vesicles versus hydrophilic or hydrophobic molecules (in that case the laser spots were set on both sides of the mem-brane). Theoretical descriptions are proposed together with a discussion about FCS ...

2008-01-01

90

Weakly penetrating radiation monitoring and assessment at Daya Bay Nuclear Power Plant  

International Nuclear Information System (INIS)

Weakly penetrating radiation monitoring and investigating with area monitors and individual dosimeters were carried out at Daya Bay nuclear power plant during its refueling outages. This paper introduces monitoring methods, measuring results, data analysis and assessment, presents some suggestions for monitoring plan and protection measures in the future as well. (authors)

2006-05-01

91

Spontaneous radiation emission during penetration of ions in solids  

International Nuclear Information System (INIS)

In this work, the principal continuum radiative emission processes, which occur during the penetration of ions in solids or gases, are resumed. The characteristics of the following processes are discussed: secondary electron bremsstrahlung (SEB), atomic bremsstrahlung (AB), and internuclear bremsstrahlung (INB). Recent advances of the ion channeling effects in crystal solids on the spontaneous radiative spectra are exposed. (A.C.A.S.).

1988-09-25

92

Penetration effect in the M1 component of "1"7"7Ta #gamma#-transition with energy of 70.45 keV  

International Nuclear Information System (INIS)

The magnetic #beta#-spectrometer of the #pi# #sq root#2 type with 0.07% pulse resolution is used to measure the intensities of interval conversion electrons on L- and M-subshells of 70.45 keV "1"7"7 Ta gamma-transition. The results are analyzed and the values of mixing parameter #sigma#(E2/M1) and penetration parameter #lambda# are obtained.

93

Numerical error analysis of direct integration method  

Energy Technology Data Exchange (ETDEWEB)

Numerical errors of PALLAS calculation due to spatial mesh sizes are examined for a typical deep penetration shielding problem of isotropic incident fission neutrons penetrating a 200-cm-thick water slab. The exponential approximation for the source spatial distribution to solve the transport equation based on the direct integration method is verified to be effective for radiation transport in attenuating medium, while the linear approximation employed in the old PALLAS code is found to produce large errors for calculations with large mesh sizes.

1986-01-01

94

Detection of constitutive heterodimerization of the integrin Mac-1 subunits by fluorescence resonance energy transfer in living cells  

International Nuclear Information System (INIS)

Macrophage differentiation antigen associated with complement three receptor function (Mac-1) belongs to #beta#_2 subfamily of integrins that mediate important cell-cell and cell-extracellular matrix interactions. Biochemical studies have indicated that Mac-1 is a constitutive heterodimer in vitro. Here, we detected the heterodimerization of Mac-1 subunits in living cells by means of two fluorescence resonance energy transfer (FRET) techniques (fluorescence microscopy and fluorescence spectroscopy) and our results demonstrated that there is constitutive heterodimerization of the Mac-1 subunits and this constitutive heterodimerization of the Mac-1 subunits is cell-type independent. Through FRET imaging, we found that heterodimers of Mac-1 mainly localized in plasma membrane, perinuclear, and Golgi area in living cells. Furthermore, through analysis of the estimated physical distances between cyan ...

2006-08-04

95

X-ray fluorescence analysis as auxiliary method of restorers  

International Nuclear Information System (INIS)

The principle is described of X-ray fluorescence analysis and the manner of detecting the emitted characteristic radiation. The advantages are presented of radionuclide X-ray fluorescence analysis which consist primarily in the possibility of conducting a totally non-destructive analysis, and of accurate and relatively narrow localization of the analyzed area, the simultaneous qualitative and quantitative determinations of a large number of elements in the order of concentrations 10"1 to 10"-"4%, stability of excitation radiation flux, simple design and relatively low capital costs. The so-called matrix effect is pointed to. A number of examples is given of the use of the cited method, including its use in the analysis of art objects. (J.B.).

1987-09-07

96

State analysis of sulfur in coal and coal fly ash by double-crystal X-ray fluorescence spectrometry  

Energy Technology Data Exchange (ETDEWEB)

Double-crystal high-resolution x-ray fluorescence spectrometry was applied to the state analysis of sulfur in coal and related fly ash. For total sulfur, a proportional relationship exists between fluorescence intensities and the analytical values obtained by the oxygen-combustion method. Two oxidation states of sulfur were identified by a least square curve fitting method, by assuming that the spectrum profile is identical for each sulfur state but the intensity and position are different. The chemical state of sulfur in coal and remaining in fly ash is discussed.

1983-01-01

97

X-Ray Fluorescence Analysis of Composite Propellants for ...  

Science.gov (United States)

... The constancy of the X-ray intensity ratio for each element in Table 8 as the X-ray tube settings were changed shows the excellent compensating ...

1977-06-03

99

Stress Tolerance of Photosystem II in Vivo  

UK PubMed Central (United Kingdom)

The in vivo photochemical activity of photosystem II was inferred from modulated chlorophyll fluorescence and photoacoustic measurements in intact leaves of several plant species (Lycopersicon...Full Text Available

1992-09-01

100

SHORT PULSE LASERS  

Science.gov (United States)

... main in this state only for 10-8 secs., after which they decay to the meta- stable state (fluorescent level) because of spontaneous radiation or other ...

1962-10-01

103

Photophysical properties of new psoralen derivatives: psoralens linked to adenine through polymethylene chains  

International Nuclear Information System (INIS)

The model compounds, 8-methoxypsoralen-CH_2O(CH_2)_n-adenine (MOPCH_2OC_nAd, n=2,3,5,6,8, and 10) in which 5 position of 8-methoxypsoralen (8-MOP) is linked by various lengths of polymethylene bridge to N"9 of adenine. UV absorption spectra are identical with the sum of MOPCH_2OC3 and adenine absorption spectra. Solvent effect on the UV absorption and fluorescence emission spectra indicate that the lowest excited singlet state is the (#pi##->##pi#"*) state. The spectral characteristics of the fluorescence of MOPCH_2OC_nAd are strongly dependent upon the nature of the solvents. The fluorescence emission spectra in aprotic solvents are broad and structrueless due to the excimer formation through the folded conformation accelerated by hydrophobic #pi#-#pi# stacking interaction. Increasing polarity of the protic solvents leads to higher population of unfolded conformation stabilized through favorable solvation and H-bonding, ...

2002-10-01

104

Phase-Sensitive Fluorescence Study of Mono-L-Aspartyl ...  

Science.gov (United States)

... of perylene were measured with the Shimadzu UV-2500 UV-VIS spectrophotometer (Kyoto, Japan) to determine their molar extinction coefficients. ...

2001-10-25

105

PRICES SUBJECT To CHq.G - NASA Technical Report Server (NTRS)  

Science.gov (United States)

by the radionuclide X-ray fluorescence analysis into several groups according to the atomic number of the determined element. Table I documents this. ...

106

N94- 31026 - NASA Technical Report Server (NTRS)  

Science.gov (United States)

in early 1992 from Lord Corporation, were also found. For both the reflective and absorptive polyurethanes, the fresh paint fluoresces significantly ...

108

Color Fluorescence Ratio for Detection of Bronchial Dysplasia and Carcinoma In situ  

UK PubMed Central (United Kingdom)

BackgroundAutofluorescence bronchoscopy is more sensitive than conventional bronchoscopy for detecting early airway mucosal lesions. Decreased specificity can lead...Full Text Available

2009-07-15

110

Application of laser fluorimetry for determining the influence of a single amino-acid substitution on the individual photophysical parameters of a fluorescent form of a fluorescent protein mRFP1  

International Nuclear Information System (INIS)

Individual photophysical parameters of the chromophore of a fluorescent protein mRFP1 and its two mutants (amino-acid substitution at position 66 - mRFP1/ Q66C and mRFP1/Q66S proteins) are determined. For this purpose, apart from conventional methods of fluorimetry and spectrophotometry, nonlinear laser fluorimetry is used. It is shown that the individual extinction coefficients of the chromophore of proteins correlate (correlation coefficient above 0.9) with the volume of the substituted amino-acid residue at position 66 (similar to the positions of the absorption, fluorescence excitation and emission maxima). (laser biology and medicine)

2009-03-31

111
112

 

UK PubMed Central (United Kingdom)

Enteropathogenic E. coli were sought routinely by the fluorescent antibody technique, using monovalent and polyvalent conjugates (rhodamine sulfonyl· chloride, fluorescein and rhodamine isothiocyanate)....Full Text Available

1962-11-03

113

Effect of applied tensile stress on intergranular corrosion of AA2024-T3  

International Nuclear Information System (INIS)

The effect of uniaxial tensile stress on intergranular corrosion (IGC) of AA2024-T3 was studied using the foil penetration technique. Standard ASTM G49 fixed-displacement jigs were modified to allow the use of sheet samples, which were then attached to an electrochemical cell as in the foil penetration setup. The time for IGC to penetrate samples of varying thickness was monitored. This method provides a new approach to bridge the gap between IGC and intergranular stress corrosion cracking (IGSCC). Samples with various orientations relative to the rolling direction were studied in 1.0 M NaCl at controlled anodic potentials. Potentiodynamic polarization measurements indicated that the two breakdown potentials typically observed for AA2024-T3 were lower for stressed samples than for unstressed samples, and the current at a given potential was higher. The penetration rate depended on potential and was ...

2004-02-01

114

Revisited the mathematical derivation wall thickness measurement of pipe for radiography  

Energy Technology Data Exchange (ETDEWEB)

Wall thickness measurement of pipe is very important of the structural integrity of the industrial plant. However, the radiography method has an advantage because the ability of penetrating the insulated pipe. This will have economic benefit for industry. Moreover, the era of digital radiography has more advantages because the speed of radiographic work, less exposure time and no chemical used for film development. Either the conventional radiography or digital radiology, the wall thickness measurement is using the tangential radiography technique (TRT). In case, of a large diameter, pipe (more than inches) the determination maximum penetration wall thickness must be taken into the consideration. This paper is revisited the mathematical derivation of the determination of wall thickness measurement based on tangential radiography technique (TRT). The mathematical approach used in this derivation is the Pythagoras theorem and geometrical ...

2007-07-01

115

Development of sealing insulator for electric penetration assemblies  

International Nuclear Information System (INIS)

Electrical penetration assemblies mounted on the containment wall are used to carry electrical power and signals from the equipment inside this containment (e.g. recirculation pumps, control rod position indications etc.) Todays BWR nuclear power plants apply epoxy resin sealed electric penetration. Contrariwise, the epoxy resin (organic sealant) was replaced with sodium barium glass (inorganic) by way of trial in search for a quality sealant. The glass sealant has been proved to have high temperature airtightness at 300 degC above from an evaluation test involving full-scale model parts. Environmental tests were conducted continuously as to heat cycle, vibration and LOCA etc. the specimens (module) of five types. They were made certain of conformity to the design requirements for boiling water operation. (author).

116

Characterization of radon penetration of different structural domains of concrete. Final project report  

International Nuclear Information System (INIS)

This report documents the research activities by Rogers and Associates Engineering Corporation on grant DE-FG03-93ER61600 during the funded project period from August 1993 to April 1996. The objective of this research was to characterize the mechanisms and rates of radon gas penetration of the different structural domains of the concrete components of residential floor slabs, walls, and associated joints and penetrations. The research was also to characterize the physical properties of the concretes in these domains to relate their radon resistance to their physical properties. These objectives support the broader goal of characterizing which, if any, concrete domains and associated properties constitute robust barriers to radon and which permit radon entry, either inherently or in ways that could be remediated or avoided.

117

Time-resolved confocal fluorescence spectroscopy reveals the structure and metabolic state of epithelial tissue  

Science.gov (United States)

Autofluorescence spectroscopy has been a widely explored technique for in vivo and noninvasive diagnosis of pre-cancer lesions in epithelium where 90% cancers originate. For extracting more accurate fluorescence information for cancer diagnosis, depth-resolved fluorescence measurements are crucial to assess NADH and FAD in non-keratinized epithelial layer and collagen in stromal layer, respectively. In this study, we achieved the depth-resolved fluorescence spectral measurements of squamous epithelial tissue based on confocal technique. We found that in non-keratinized epithelial layer the fluorescence signals excited at 405 nm were the combination of NADH and FAD fluorescence and could be used for evaluating the redox ratio. Moreover, we found that confocal time-resolved autofluorescence measurements of epithelial tissue with 405 nm excitations could provide the information on the ...

2007-03-01

118

Theoretical transition energies, lifetimes and fluorescence yields of multiply ionized silicon  

Energy Technology Data Exchange (ETDEWEB)

Theoretical x-ray transition energies, lifetimes and partial multiplet fluorescence yields are presented for all spectroscopic terms of electron configurations with a single K-shell vacancy and varying number of electrons in the L-shell and M/sub 1/-subshell for multiply-ionized silicon. 9 tables.

1982-01-01

119

The fatty acid analogue 11-(dansylamino)undecanoic acid is a fluorescent probe for the bilirubin-binding sites of albumin and not for the high-affinity fatty acid-binding sites.  

UK PubMed Central (United Kingdom)

1. The fluorescent fatty acid probe 11-(dansylamino)undecanoic acid (DAUDA) binds with high affinity to bovine and human serum albumin (BSA and HSA) at three sites. 2. The Kd of the primary binding...Full Text Available

1990-08-15

120

Structural basis of binding of fluorescent, site-specific dansylated amino acids to human serum albumin  

UK PubMed Central (United Kingdom)

Human serum albumin (HSA) has two primary binding sites for drug molecules. These sites selectively bind different dansylated amino acid compounds, which—due to their intrinsic fluorescence—have...Full Text Available

2011-04-01

121

Rubidium 5"2P fine-structure transitions induced by collisions with potassium and caesium atoms  

International Nuclear Information System (INIS)

A diode-laser fluorescence experiment was performed in order to study fine-structure transitions between 5"2P states of rubidium atoms colliding with ground-state potassium or caesium atoms. The Rb(5"2P_3_/_2) state was optically excited and the intensity ratio of sensitized to direct fluorescence was measured. (author).

122

Radionuclide X-ray fluorescence determination of Cr, Fe, Cu, Zn,and Pb in industrial wastewaters after preconcentration of determined elements  

International Nuclear Information System (INIS)

Radionuclide X-ray fluorescence analysis was used for the determination of Cr, Fe, Cu, Zn and Ph in industrial wastewaters (from surface treatment of metals and glasses) after precipitation of determined elements by 8-hydroxyquinoline. (author).

1997-01-01

123

Radionuclide X-ray fluorescence analysis of solid aerosol particles on Synpor 4 collection filters  

International Nuclear Information System (INIS)

The feasibility was studied of the application of radionuclide X-ray fluorescence analysis to the identification and determination of chemical elements in the air. A description of the method is presented, the main stages of the analysis are discussed (sample preparation and standards, selection of radioactive radiation sources, geometry of measurement and evaluation of results). The method is illustrated on the determination of elements Fe, Cu, Zn, Br, and Pb in air samples taken in the city of Prague. (author) 2 tabs., 2 figs., 14 refs.

1992-01-01

124

Nondestructive determination of airborne lead particulates by the radionuclide X-ray fluorescence analysis  

International Nuclear Information System (INIS)

Airborne lead particulates collected on a membrane filter were determined by the nondestructive X-ray fluorescence method. The gamma/X radionuclide source "2"4"1Am/Ag and a scintillation detector with a NaI/Tl crystal were used for the excitation and detection, respectively, of L X-rays of Pb. One can say, with reference to the obtained results, that the sensitivity and accuracy of the measurement is more than adequate for monitoring the Pb level in air. (author).

1980-01-01

125

Heavy metals in industrial wastewater determined by radionuclide x-ray fluorescence analysis and their effects on Allium cepa root tip cells  

International Nuclear Information System (INIS)

Radionuclide x-ray fluorescence method was used in the determination of Cr, Ni and other heavy metals content in wastewater of an engineering plant taken both before and after chemical treatment. Toxic effects of the wastewaters using Allium cepa root tip cells were tested. (author) 8 refs.; 2 tabs.

1994-05-01

126

Heavy metals and some other elements in medicinal plants. Determined by X-ray fluorescence analysis  

International Nuclear Information System (INIS)

Determination of Mn, Fe, Cu, Zn, Hg, Pb, Br, Se, Rb, Sr and Cd in the medicinal plants by radionuclide X-ray fluorescence analysis (using "2"3"8Pu, "2"4"1Am/Ag and "1"2"5I) is described. (author). 12 refs., 2 tabs.

1995-01-01

127

Heavy element contamination of surface waters in the region Banska Stiavnica (SR) measured by radionuclide X/ray fluorescence analysis  

International Nuclear Information System (INIS)

Heavy metals (Pb, Cd, Mn, Cu, Zn, Fe) were determined in surface waters in the surroundings of the depositories of the mining shrubs in the region of Banska Stiavnica (SR) by radionuclide X-ray fluorescence analysis. Allowed concentrations of the determined metals are exceeded numerously (multiplicity in some cases was 10"3-10"6). (author).

1997-01-01

128

Evaluation of adhesive plasters by radionuclide X-ray fluorescence analysis  

International Nuclear Information System (INIS)

A radiometric method was elaborated for surface density determinations of the adhesive layer of plasters by radionuclide X-ray fluorescence using the 17.47 keV bremsstrahlung of "1"4"7Pm/Mo. The bremsstrahlung line excites the 8.63 keV characteristic K#alpha# line of Zn contained in the adhesive layer of the plaster as a filling material in the form of ZnO. In homogeneous adhesive layers the Zn content is proportional to surface density. (author).

1976-01-01

129

Determination of cesium and selenium in cultivated mushrooms using radionuclide X-ray fluorescence technique  

International Nuclear Information System (INIS)

Cesium and selenium intake of cultivated mushrooms (Agaricus bisporus), with these elements previously added to culture medium, has been examined from the viewpoint of health- and environmental protection. The process of measuring has been carried out by the radionuclide X-ray fluorescence technique. Treatments of the elementary substance with Se salt appears to influence the Se content of the mushrooms to a significant extent. Cs intake is of considerable importance, as this element is accumulated by mushrooms. (author)

2000-09-01

130

Determination of ash in coal by X-ray backscattering and X-ray fluorescence analysis and apparatus by the PAR company  

International Nuclear Information System (INIS)

The basic principles of determination of the ash content of coal by the title methods are outlined. A brief technical characteristic of the ash meters and radionuclide X-ray fluorescence analyzers manufactured by the PAR company is presented. (Z.S.). 4 figs., 7 refs.

1993-01-01

131

Determination of Y, Ba and Cu in superconductor films by x-ray fluorescence analysis  

International Nuclear Information System (INIS)

Radionuclide x-ray fluorescence analysis was used for the determination of Y, Ba and Cu in thin high-temperature superconducting films. Atomic emission ICP spectrometry was used to estimate the precision and accuracy of analytical results. Reasonable agreement between both methods was obtained when a polynomial calibration curve was applied. (author) 4 refs.; 4 tabs.

1994-06-01

132

Determination of Mn, Fe, Ni, Cu, Zn and Pb contents in samples of apple trees by radionuclide X-ray fluorescence analysis  

Energy Technology Data Exchange (ETDEWEB)

The applicability of the radionuclide X-ray fluorescence analysis (RXFA) for qualitative and quantitative evaluation of environmental plant samples is discussed and examples of determination of Mn, Fe, Ni, Cu, Zn, Pb in samples of apple trees are given. The instrumentation, the standard and sample preparation are also presented.

1982-12-01

133

Determination of Fe and Zn in healing plants by radionuclide X-ray fluorescence analysis  

International Nuclear Information System (INIS)

Radionuclide X-ray fluorescence method was used for the determination of Fe and Zn in healing plants (Sage, Peppermint, Stinging, Common Agrimony, Milfoil, Ribwort, Tansy, White Dead-Nettle). "2"3"8Pu exciting source and Si/Li semiconductor detector were used for the determination. (author)

1999-06-01

134

Determination of Fe and Zn in agricultural plants with special cultivation by radionuclide x-ray fluorescence analysis  

International Nuclear Information System (INIS)

Fe and Zn were determined in various parts of maize (Zea mays) in dependence on quantity of organic substrate EKOFERT as organic fertilizer in soil, using radionuclide X-ray fluorescence analysis. The increase of quantity of organic substrate EKOFERT in soil causes a decrease of heavy metal concentrations in certain parts of the plant. (author). 4 refs., 1 tab.

1996-01-01

135

Determination of Cu, Ni, Zn and Pb contents in taraxacum officinale near the highway D-61 Bratislava-Trnava (SR) by radionuclide X-ray fluorescence analysis  

International Nuclear Information System (INIS)

Radionuclide X-ray fluorescence method with Si/Li semiconductor detector and "2"3"8Pu exciting source was used for the determination of Cu, Ni, Zn and Pb in plant samples (Taraxacum officinale) from various localities near the highway D-61 Bratislava-Trnava (SR). (author) 2 refs.; 1 fig.; 1 tab.

1993-12-01

136

Determination of Cu, Ni, Zn and Pb contents in soil near the D-61 Bratislava-Trnava Highway by radionuclide X-ray fluorescence analysis  

International Nuclear Information System (INIS)

Radionuclide X-ray fluorescence method with Si/Li semiconductor detector and "2"3"8Pu exciting source was used for the determination of Cu, Ni, Pb, and Zn in soil samples from various localities near the D-61 Bratislava-Trnava highway (CSFR). (author) 1 ref.; 1 tab.

1993-01-01

137

Analysis of high-temperature superconducting films by x-ray fluorescence analysis  

International Nuclear Information System (INIS)

Radionuclide X-ray fluorescence analysis was used for the determination of Cu, Y and Ba in very thin high-temperature superconducting films. The precision of the method is better than 3% for about 1 #mu#m thick films. The atomic emission ICP spectrometry was used to testify results of XRF analysis. An acceptable agreement of both methods was obtained. (author) 4 refs.; 2 tabs.

1991-09-01

138

7. Overview of radionuclide X-ray fluorescence analysis of components of the environment  

International Nuclear Information System (INIS)

A survey is presented of studies dealing with radionuclide X-ray fluorescence analysis (RXFA) of impurities in the air, water, soil, sediments and biological materials, mainly blood, urine, hair, soft tissues and bones. Tabulated are lists of published works on RXFA of the air, water and biological materials. (ES).

1983-12-01

139

Uptake and Intracellular Activity of Moxifloxacin in Human Neutrophils and Tissue-Cultured Epithelial Cells  

UK PubMed Central (United Kingdom)

The penetration by moxifloxacin of human neutrophils (polymorphonuclear leukocytes [PMN]) and tissue-cultured epithelial cells (McCoy cells) was evaluated by a fluorometric assay. At...Full Text Available

1999-01-01

140

Topical Application of 5-Aminolevulinic Acid Hexyl Ester and 5-Aminolevulinic Acid to Normal Nude Mouse Skin: ...  

Science.gov (United States)

... J. W. and R. A. de Zeeuw. 1990. Transdermal drug delivery: efficacy and potential applications of the penetration enhancer ... ...

141

Thermal stress cracking and the enhancement of heat extraction from fractured geothermal reservoirs  

Science.gov (United States)

Given sufficient time, the extraction of heat from geothermal reservoirs formed by the hydraulic fracturing of competent rock will eventually result in the formation of thermal stress cracks in the reservoir. These cracks penetrate the rock in a manner such that the penetration-to-spacing ratio is approximately one. The penetration depends upon the extent of cooling and the square root of time. Initially then, the cracks are closely spaced and penetrate but little, so that a crazing pattern is apparent; but with increasing time some of these cracks, now more widely spaced, grow deeper. Eventually these larger cracks attain a critical aperture such that significant rates of water flow can be established within them and thus the newly created heat transfer area becomes useful for heat extraction. At the same time that cracks are forming within the main reservoir, thermal cracking also occurs in the ...

1978-04-01

142

The role of skin absorption as a route of exposure for volatile organic compounds (VOCs) in drinking water.  

UK PubMed Central (United Kingdom)

Assessments of drinking water safety rely on the assumption that ingestion represents the principal route of exposure. A review of the experimental literature revealed that skin penetration rates for...Full Text Available

1984-05-01

143

Potential for containment leak paths through electrical penetration assemblies under severe accident conditions  

International Nuclear Information System (INIS)

The leakage behavior of containments beyond design conditions and knowledge of failure modes is required for evaluation of mitigation strategies for severe accidents, risk studies, emergency preparedness planning, and siting. These studies are directed towards assessing the risk and consequences of severe accidents. An accident sequence analysis conducted on a Boiling Water Reactor (BWR), Mark I (MK I), indicated very high temperatures in the dry-well region, which is the location of the majority of electrical penetration assemblies. Because of the high temperatures, it was postulated in the ORNL study that the sealants would fail and all the electrical penetration assemblies would leak before structural failure would occur. Since other containments had similar electrical penetration assemblies, it was concluded that all containments would experience the same type of failure. The results of this study, however, show that ...

144

Over-the-scope clip closure of two chronic fistulas after gastric band penetration  

UK PubMed Central (United Kingdom)

Gastrointestinal perforations are conservatively managed at endoscopy by through-the-scope endoclips and covered self expandable stents, according to the size and tissue features of the perforation....Full Text Available

2010-04-07

145

Jet initiation and penetration of explosives  

Energy Technology Data Exchange (ETDEWEB)

The two-dimensional Eulerian hydrodynamic code 2DE, with the shock initiation of heterogeneous explosive burn model called Forest Fire, is used to model numerically the interaction of jets of steel, copper, tantalum, aluminum, and water with steel, water, and explosive targets. The calculated and experimental critical condition for propagating detonation may be described by the Held V/sup 2/d expression (jet velocity squared times the jet diameter). In PBX 9502, jets initiate an overdriven detonation smaller than the critical diameter, which either fails or enlarges to greater than the critical diameter while the overdriven detonation decays to the C-J state. In PBX 9404, the jet initiates a detonation that propagates only if it is maintained by the jet for an interval sufficient to establish a stable curved detonation front. The calculated penetration velocities into explosives, initiated by a low-velocity jet, are significantly less than for non-reactive solids ...

1983-01-01

146

Jet initiation and penetration of explosives  

Energy Technology Data Exchange (ETDEWEB)

The two-dimensional Eulerian hydrodynamic code 2DE with the shock initiation of heterogeneous explosive burn model called Forest Fire, is used to model numerically the interaction of jets of steel, copper, tantalum, aluminum, and water with steel, water, and explosive targets. The calculated and experimental critical condition for propagating detonation may be described by the Held V/sup 2/d expression (jet velocity squared times the jet diameter). In PBX 9502, jets initiate an overdriven detonation smaller than the critical diameter, which either fails or enlarges to greater than the critical diameter while the overdriven detonation decays to the C-J state. In PBX 9404, the jet initiates a detonation that propagates only if it is maintained by the jet for an interval sufficient to establish a stable curved detonation front. The calculated penetration velocities into explosives, initiated by a low-velocity jet, are significantly less than for non-reactive solids of ...

1983-01-01

147

Do energetic heavy nuclei penetrate deeply into Earth's atmosphere?  

UK PubMed Central (United Kingdom)

We calculate the expected fluxes of cosmic ray nuclei with charge 5 ≤ Z ≤ 28 at various depths in the earth's atmosphere, taking into account the initial charge distribution,...Full Text Available

1980-01-01

148

CENTRAL CORNEAL OPACIFICATION RESULTING FROM RECENT CHEMOTHERAPY IN CORNEAL DONORS  

UK PubMed Central (United Kingdom)

PurposeOcular surface disease following penetrating keratoplasty has been shown to increase patient morbidity and adversely affect graft survival. Five cases of dense central subepithelial...Full Text Available

2007-12-01

149

A model for fuel spray penetration  

Energy Technology Data Exchange (ETDEWEB)

A new model for fuel spray penetration (location of spray tip) is suggested and validated against available experimental data. Simple analytical expressions for fuel spray penetration are derived in two limiting cases: the initial stage and the two-phase flow regime. At the initial stage, the effects of droplet drag and entrainment of air are accounted for. In the case of the two-phase flow, it is assumed that the spray droplets have the same velocities as the entrained air. The characteristic time of droplet break-up in the spray is estimated for both bag and stripping break-up mechanisms. For realistic diesel spray parameters, the droplet break-up takes place almost immediately after the droplets leave the nozzle. This leads to a considerable shortening of the initial stage and a rapid conversion of the flow to the two-phase stage. This allows the analysis to be restricted to the two-phase flow approximation for this type of spray. The ...

2001-12-05

150

A radionuclide analyzer of total sulfur in coal  

International Nuclear Information System (INIS)

The devised radionuclide analyzer for the determination of total sulfur in coal includes two radionuclide sources with different energies, which are accommodated in collimators fitted with adjustable diaphramgs. The sample compartment is located between the two sources. Moreover, an X-ray fluorescence standard can be slid into the sample compartment. A proportional detector for X-ray fluorescence and scattered gamma radiation is located off the sample compartment. The input of the proportional detector is interfaced to the output of a high-voltage supply, the output, to the information input of a control-and-evaluation unit. One of the control outputs of the control-and-evaluation unit is connected to the input of the sliding mechanism for the X-ray fluorescence standard. This arrangement enables automatic energy calibration of the analyzer. The analyzer can measure not only total sulfur in coal by radionuclide X-ray ...

1987-05-13

151

Clean ferrous casting technology research. Final technical report, September 29, 1993--December 31, 1995  

Energy Technology Data Exchange (ETDEWEB)

This is the final report covering work performed on research into methods of attaining clean ferrous castings. In this program methods were developed to minimize the formation of inclusions in steel castings by using a variety of techniques which decreased the tendency for inclusions to form during melting, casting and solidification. In a second project, a reaction chamber was built to remove inclusions from molten steel using electromagnetic force. Finally, a thorough investigation of the causes of sand penetration defects in iron castings was completed, and a program developed which predicts the probability of penetration formation and indicates methods for avoiding it.

1996-01-31

152

Characterization of jet breakup mechanisms observed from simulant experiments of molten fuel penetrating coolant  

Science.gov (United States)

The goal of this research program has been to add to our understanding of the breakup of molten fuel jets penetrating reactor coolant. Easily handled working fluids are used to simulate fuel jet breakup, so that detailed observations may be obtained from a relatively large number of experiments. The tools used for observing this behavior are high speed notion picture photography, Flash X-radiography, and X-ray cine. Jet breakup lengths are determined from motion pictures; the mechanisms by which the jets are fragmented may be inferred from radiographs.

1992-01-01

153

BURST STRENGTH AND NON-DESTRUCTIVE EVALUTION OF COMPOSITE PIPES AND PIPE COUPLINGS WITH DEFECTS (TOP 48)  

Environmental Research Database

ObjectivesObjectives Not AvailableDescriptionTo determine the effects of water penetration on the burst strength of filament wound composite pipes which have been damaged by impact and then subjected to long term pressurisation with sea water. ~%~ To monitor and characterise the damage and effects of sea water penetration using ultrasonic NDT. To determine the burst strength of bonded composite pipe joints with and without defects and to see whether the defects can be detected using ultrasonic NDT. [continued...

1996-01-31

154

Strikingly different penetrance of LHON in two Chinese families with primary mutation G11778A is independent of mtDNA haplogroup background and secondary mutation G13708A  

Energy Technology Data Exchange (ETDEWEB)

The penetrance of Leber's hereditary optic neuropathy (LHON) in families with primary mitochondrial DNA (mtDNA) mutations is very complex. Matrilineal and nuclear genetic background, as well as environmental factors, have been reported to be involved in different affected pedigrees. Here we describe two large Chinese families that show a striking difference in the penetrance of LHON, in which 53.3% and 15.0% of members were affected (P < 0.02), respectively. Analysis of the complete mtDNA genome of the two families revealed the presence of the primary mutation G11778A and several other variants suggesting the same haplogroup status G2a. The family with higher penetrance contained a previously described secondary mutation G13708A, which presents a polymorphism in normal Chinese samples and does not affect in vivo mitochondrial oxidative metabolism as described in a previous study. Evolutionary analysis failed ...

2008-08-25

155

Strikingly different penetrance of LHON in two Chinese families with primary mutation G11778A is independent of mtDNA haplogroup background and secondary mutation G13708A  

International Nuclear Information System (INIS)

The penetrance of Leber's hereditary optic neuropathy (LHON) in families with primary mitochondrial DNA (mtDNA) mutations is very complex. Matrilineal and nuclear genetic background, as well as environmental factors, have been reported to be involved in different affected pedigrees. Here we describe two large Chinese families that show a striking difference in the penetrance of LHON, in which 53.3% and 15.0% of members were affected (P < 0.02), respectively. Analysis of the complete mtDNA genome of the two families revealed the presence of the primary mutation G11778A and several other variants suggesting the same haplogroup status G2a. The family with higher penetrance contained a previously described secondary mutation G13708A, which presents a polymorphism in normal Chinese samples and does not affect in vivo mitochondrial oxidative metabolism as described in a previous study. Evolutionary analysis failed to indicate ...

2008-08-25

156

Resistance study of packaging materials to rice insects pest  

International Nuclear Information System (INIS)

The resistance of several packaging materials to penetration by 4 species of rice insect pests was determined. Five insects of adult or larval stage were confined in pouches made from 9 different packaging materials with or without irradiated rice. It was observed that both adults and larvae of species Tribolium castaneum Herbst., Sitophilus zeamais L., Oryzaephilus surinamensis L. and Cocyra cephalonica Stainton, were incapable of penetrating pouches made from white polyvinychloride of 0.175mm thickness, low density polyethylene of 0.130mm thickness and 0.150mm thick low density polyethylene. However, penetrations marks were found in pouches made from hard paper with a thickness of 0.155mm, clear polivinylchloride of 0.130mm thickness, low density polyethylene of 0.085mm thickness, low density polyethylene 0.100mm thick, high density polyethylene of 0.06mm thickness and 0.080mm thick polypropylene. Tribolium castaneum ...

157

Liver trauma from penetrating injuries. Miscellanea, personal series, clinical and CT findings  

International Nuclear Information System (INIS)

Penetrating liver wounds are related to many causes and rank second after blunt abdominal and liver trauma. In this report are examined the clinical and radiological findings of personal series of patients with penetrating trauma, especially by firearms and stab and cut wounds. It will also tried to define the diagnostic workup of these traumas, which is especially based on CT signs of liver damage and associated changes and which is of basic importance for following treatment, both surgical or conservative. In the last seven years it was retrospectively reviewed 31 cases of penetrating liver trauma. The patients were 19 men and 12 women, ranging in age 18 to 73 (mean 42), with penetrating liver injuries from firearms (16 patients) and stab (9 cases) wounds; 6 patients had injuries from different cases. Abdominal CT was carried out in emergency with the CT Angiography (CTA) technique in all patients. In ...

2000-12-01

158

State analysis of sulfur in coal and coal fly ash by double-crystal X-ray fluorescence spectrometry  

Energy Technology Data Exchange (ETDEWEB)

Double-crystal high-resolution X-ray fluorescence spectrometry was applied to the state analysis of sulfur in coal and related fly ash. For total sulfur, a proportional relationship exists between fluorescence intensities and the analytical values obtained by the oxygen-combustion method. Two oxidation states of sulfur were identified by a least square curve fitting method, by assuming that the spectrum profile is identical for each sulfur state but the intensity and the position are different. Sulfur in coal mainly consists of S/sup 2 -/, whereas that in coal fly ash mainly consists of S/sup 6 +/. As much as 0.04-0.08% of S/sup 2 -/ remains in fly ash.

1983-01-01

159

Research on improving utilization efficiency of photoelectric cell by using fluorescence material  

Energy Technology Data Exchange (ETDEWEB)

This paper proves that it is practicable to build a new power model which can work efficiently at night by using a type of fluorescence material. The utilization efficiency of photovoltaic cell is improved by prolonging the actual working hours of the cell within 24 hours. Both theoretical analysis and experiment on this model are carried out, and base on which the current-time curve (I-t curve) is depicted. It shows that the model which applies the fluorescence material to photovoltaic system is available. According to the analysis and comparison between the attenuating curve of the material and I-t curve of the power system, we can conclude that the weak illumination and the mismatch on wavelength are primary reasons for the low current. Finally, several improved measures of this power model for practical application are given, and it is expected to provide a new thought for photovoltaic study. (orig.)

2008-07-01

160

PKH26 as a fluorescent label for live human umbilical mesenchymal stem cells  

British Library Electronic Table of Contents (United Kingdom)

To determine whether PKH26 labeling affects the morphologies, phenotypes, proliferation, and secretion abilities of human umbilical mesenchymal stromal cells (HUMSCs) were investigated. Isolated HUMSCs were labeled with PKH26, and cell morphology was observed under microscope. Cell cycle, apoptotic cell death, expression of PKH26, and the proliferation rate were evaluated. Additionally, fluorescence intensity of PKH26 labeling at different passage times was quantified. There were no detectable differences in cell morphology, cell growth, and proliferation rate after PKH26 labeling. In addition, fluorescence intensity of PKH26 labeling was gradually reduced with increase of the passage times. The PKH26 labeling disappeared after passage six times. In summary, PKH26 labeling is a safe and ef...

2011-01-01

161

Multielement analysis of air samples. Determination of iron, zinc, lead, and bromine content by the radionuclide X-ray fluorescence analysis  

Energy Technology Data Exchange (ETDEWEB)

Radionuclide X-ray fluorescence analysis for nondestructive determination of Fe, Zn, Pb, and Br in air samples collected on nitrocellulose membrane filter Synpor 4 is described. A /sup 238/Pu source for the excitation and a semiconductor Si/Li detector for the detection of characteristic and L-fluorescent radiation of the above elements were used. A correction method based upon the measurements of simple or multiple Compton scattering for compensation of varying mass per unit area values in sample deposits was theoretically proposed and experimentally tested. The results obtained both with and without the correction were compared and good agreement with those given by atomic absorption spectrometry was observed.

1981-01-01

162

Mitochondrial sequestration of BCECF after ester loading in the giant alga Chara australis  

British Library Electronic Table of Contents (United Kingdom)

Summary. Ratiometric fluorescent dyes are often used to monitor free ion concentrations in vivo, especially in cells that are recalcitrant to transformation with genetically encoded fluorescent markers. Although intracellular dye distributions are often found to be cytosolic, dye localisation has often not been examined in detail. We began exploring the use of BCECF (2?,7?-bis(2-carboxyethyl)-5(6)-carboxyfluorescein) to monitor pH in the giant alga Chara australis and discovered that younger leaf cells could be loaded using the acetoxymethyl ester of BCECF. However, we were puzzled to find in microphotometric measurements that the fluorescence ratio appeared insensitive to manipulations affecting cytosolic pH. Confocal imaging of C. australis cells loaded with BCECF showed an accumulation ...

2007-01-01

163

Micro-patterning of chemical functionality of anthracene-bis-resorcinol film using focused ion beam  

International Nuclear Information System (INIS)

Anthracene-bis-resorcinol is an interesting molecule as it forms a hydrogen-bonded network when guest molecules with weak polarity are included. Focused ion beam (FIB) was irradiated on a part of its amorphous film with low dose, and the film was exposed to the vapor of guest molecules. From fluorescence and AFM analyses of this film, it was found that no inclusion compound was formed in FIB irradiated area, i.e. FIB irradiation suppresses the ability to form the inclusion compounds. By utilizing this phenomenon, we succeeded in a microfabrication of relief structures consisting of inclusion compounds which has different fluorescence from its surrounding. Morphology, fluorescence, and IR absorption analyses indicated that hydroxyl or resorcin groups are damaged by ion beams, and consequently a formation of hydrogen-bonded networks, which play a role of a lattice caging guest molecules, becomes impossible.

2005-12-15

164

Influence of alloying effect on X-ray fluorescence parameters of Co and Cu in CoCuAg alloy films  

British Library Electronic Table of Contents (United Kingdom)

In this study, Kb/Ka X-ray intensity ratios, Formula Not Shown , Formula Not Shown production cross-sections and K fluorescence yields of Co and Cu and Lb/La X-ray intensity ratios, Formula Not Shown , Formula Not Shown production cross-sections and Formula Not Shown average fluorescence yields of Ag in pure metals and in different alloy compositions were measured. In this study, alloying effects on the Formula Not Shown production cross-sections of Co and Cu were investigated and changes interpreted according to the rearrangement of valance state electrons and the charge transfer process between the 3d elements (Co and Cu) and Ag.

2009-01-01

165

Exciplex processes involving trans naphthylethylenes. Implications of ground-state conformeric equilibria  

Energy Technology Data Exchange (ETDEWEB)

Five arylethylenes with 1-naphthyl, 2-naphthyl, and phenyl groups in 1,2-positions have been studied for singlet-mediated charge-transfer interactions with several amines and paraquat dication. 1-Phenyl-2-(2-naphthyl)ethylene and 1,2-di(2-naphthyl)ethylene exhibit distinct dependence of exciplex emission maxima and lifetimes, and fluorescence quenching constants, on excitation and/or monitoring wavelengths; this is in conformity with the existence of ground-state rotamers for these systems, wtih distinguishable absorption-emission spectra and fluorescence lifetimes. The fluorescence quenching by aromatic amines and paraquat dication occurs with rate constants in the limit of diffusion control and is accompanied by the formation of radical ions in polar solvents (acetonitrile). The transient spectra and kinetics associated with the radical ions, observed by 337.1- and 355-nm laser flash photolysis, are also reported. 10 ...

1983-05-12

166

Detection of Fluorescence for Lanthanides in LiCl-KCl Molten Salt Medium  

Energy Technology Data Exchange (ETDEWEB)

In the electrorefining step of the pyrochemical process, actinide ions dissolved in the LiCl-KCl eutectic salt are recovered as pure actinide metals at a cathode for a re-use as a nuclear fuel from the aspect of its nonproliferation of the nuclear fuel cycles. The lanthanide species dissolved in the LiCl-KCl eutectic salt play an important role in an effective metal purification during the electrorefining step, so it is necessary to understand the chemical and physical behaviors of lanthanides in molten salt. The in situ spectroscopic measurement system and studies according to temperature changes are essential for better understandable information. To our knowledge, the absorption studies of lanthanides at high temperatures have been reported before, but the fluorescence studies of those at high temperature are not reported yet. We will discuss here the fluorescence behaviors of lanthanides in LiCl-KCl molten salt medium according to a ...

2007-10-15

167

Detection of Fluorescence for Lanthanides in LiCl-KCl Molten Salt Medium  

International Nuclear Information System (INIS)

In the electrorefining step of the pyrochemical process, actinide ions dissolved in the LiCl-KCl eutectic salt are recovered as pure actinide metals at a cathode for a re-use as a nuclear fuel from the aspect of its nonproliferation of the nuclear fuel cycles. The lanthanide species dissolved in the LiCl-KCl eutectic salt play an important role in an effective metal purification during the electrorefining step, so it is necessary to understand the chemical and physical behaviors of lanthanides in molten salt. The in situ spectroscopic measurement system and studies according to temperature changes are essential for better understandable information. To our knowledge, the absorption studies of lanthanides at high temperatures have been reported before, but the fluorescence studies of those at high temperature are not reported yet. We will discuss here the fluorescence behaviors of lanthanides in LiCl-KCl molten salt medium according to a ...

2007-10-01

168

A dual-emissive-materials design concept enables tumour hypoxia imaging  

British Library Electronic Table of Contents (United Kingdom)

Luminescent materials are widely used for imaging and sensing owing to their high sensitivity, rapid response and facile detection by many optical technologies. Typically materials must be chemically tailored to achieve intense, photostable fluorescence, oxygen-sensitive phosphorescence or dual emission for ratiometric sensing, often by blending two dyes in a matrix. Dual-emissive materials combining all of these features in one easily tunable molecular platform are desirable, but when fluorescence and phosphorescence originate from the same dye, it can be challenging to vary relative fluorescence/phosphorescence intensities for practical sensing applications. Heavy-atom substitution alone increases phosphorescence by a given, not variable amount. Here, we report a strategy for modulating ...

2009-01-01

169

Model experiment on change of seismic properties of a fracture caused by injecting/draining water; Chusui/haisui ni yoru kison kiretsu no dansei denpa tokusei no henka ni kansuru model jikken  

Energy Technology Data Exchange (ETDEWEB)

Effect of water injection/draining on elastic waves penetrating through cracks is examined by measuring elastic waves before, during, and after the injection/draining of water into/from cracks in presence in granite. Two blocks of rock, with their crack-containing surfaces in contact with each other, are placed in a vessel, and water injection/draining is done through a hole on a vessel bottom side so that water will penetrate into the cracks. When the blocks are dry, there is almost no contact between the cracks, and so no crack penetrating waves are observed. Crack penetrating waves are produced when water is injected, and the position of the receiver sensing the penetrating waves changes as the water level rises. When the water level is lowered from the high water level, the waveform changes again as the level changes. The change in waveform is not so remarkable, however, as that ...

1997-05-27

170

Failure criteria and fission products trapping effect at containment penetrations under severe accident conditions (2)  

Energy Technology Data Exchange (ETDEWEB)

Since the integrity of the containment penetrations was confirmed under accident management (AM) conditions in the former test, failure criteria tests and aerosol trapping tests were carried out using low-voltage modules and flange gaskets of an actual plant under severe accident (SA) conditions, without AM. The safety margin for failure temperature of the penetrations and the credit for fission product (FP) aerosol trapping effect along the leakage paths of the degraded penetrations were evaluated in the present tests. Failure temperature of the penetrations ranged from 270 to 300degC for low-voltage modules and 300 to 350degC for flange gaskets under 0.4 to 1.0 MPa conditions. Pressure dependency on failure temperature was small. This means that the safety margin of failure temperature under AM condition is more than 70degC. By introducing a equivalent leak area for the damaged test pieces, total leak ...

1999-07-01

171

Width of the 1.836-MeV level in "8"8Sr  

International Nuclear Information System (INIS)

Using bremsstrahlung, the resonance fluorescence yield has been measured for the 1.836-MeV 2"+_1 level in "8"8Sr. The observed yield corresponds to a level width GAMMA = 2.94 +- 0.15 meV.

172

Understanding Enzyme Activity Using Single Molecule Tracking (Poster)  

Energy Technology Data Exchange (ETDEWEB)

This poster describes single-molecule tracking and total internal reflection fluorescence microscopy. It discusses whether the carbohydrate-binding module (CBM) moves on cellulose, how the CBM binds to cellulose, and the mechanism of cellulosome assembly.

2009-06-01

173

The Arabidopsis ref2 Mutant Is Defective in the Gene Encoding CYP83A1 and Shows Both Phenylpropanoid and Glucosinolate Phenotypes  

UK PubMed Central (United Kingdom)

The Arabidopsis ref2 mutant was identified in a screen for plants having altered fluorescence under UV light. Characterization of the ref2 mutants showed that they...Full Text Available

2003-01-01

174

Site-specific modification of albumin by free radicals. Reaction with copper(II) and ascorbate.  

UK PubMed Central (United Kingdom)

Exposure of albumin to Cu(II) (10-100 microM) and ascorbate (0.1-2 mM) results in extensive molecular modifications, indicated by decreased fluorescence and chain breaks. The rate of utilization of...Full Text Available

1986-06-01

175

STS-83 - Johnson Space Center - NASA  

Science.gov (United States)

Radiation Measurement in Crew Compartment. DTO 805: .... spacecraft and aircraft propulsion, and hazardous waste disposal. ...... combustion reactions in a turbulent chemical kinetic flow reactor using laser induced fluorescence and ...

176

Role of Methoxypolyethylene Glycol on the Hydration, Activity, Conformation and Dynamic Properties of a Lipase in a Dry Film  

UK PubMed Central (United Kingdom)

A combined approach based on the use of ATR-FT/IR and steady-state fluorescence spectroscopy allowed to shed light on the effects of the additive methoxypolyethylene glycol (MePEG) on the hydration,...Full Text Available

2008-10-01

177

Ring opening reaction dynamics of a photochromic diarylethene derivative dye  

International Nuclear Information System (INIS)

Ring opening dynamics of diarylethene derivative (BTF6) in n-hexane are studied by femtosecond transient absorption and time resolved spontaneous fluorescence techniques. Cyclo-reversion time constant is obtained.

2001-11-01

178

Probing the Mechanisms of an Air Amplifier using a LTQ-FT-ICR-MS and Fluorescence Spectroscopy  

UK PubMed Central (United Kingdom)

We report the first quantitative assessment of electrosprayed droplet/ion focusing enabled by the use of a voltage-assisted air amplifier between an electrospray ionization emitter and a hybrid...Full Text Available

2007-11-01

179

Phagocytic response of bovine polymorphonuclear leukocytes to different incubation conditions and following exposure to some effectors of phagocytosis and different anticoagulants in vitro.  

UK PubMed Central (United Kingdom)

The ability of bovine polymorphonuclear leukocytes (PMN) to phagocytose fluorescent beads in vitro was studied using flow cytometry. The effects of varying laboratory conditions (bead:PMN ratio, length...Full Text Available

2001-01-01

180

Nitric Oxide-Mediated Tumoricidal Activity of Murine Microglial Cells12  

UK PubMed Central (United Kingdom)

Experimental metastases in the brain of mice are infiltrated by microglia, and parabiosis experiments of green fluorescent protein (GFP+) and GFP- mice revealed that these microglia...Full Text Available

181

Measurements and elimination of Cherenkov light in fiber-optic scintillating detector for electron beam therapy dosimetry  

International Nuclear Information System (INIS)

In this study, a miniature fiber-optic radiation detector has been developed using a water-equivalent organic scintillator for electron beam therapy dosimetry. Usually, two kinds of light signals such as fluorescent and Cherenkov lights are generated in a fiber-optic radiation detector when a high-energy electron beam is irradiated. The fluorescent light signal is produced in the scintillator and is transmitted through a plastic optical fiber to a remote light-measuring device such as a PMT or a photodiode. The Cherenkov light could be also produced in the plastic optical fiber itself and be detected by a light-measuring device. Therefore, it could cause problems or limit the accuracy of the detection of a fluorescent light signal that is proportional to dose. The objectives of this study are to measure, characterize and eliminate Cherenkov light generated in a plastic optical fiber used as a component of a fiber-optic ...

2007-08-21

182

Measurement of reactor tube cladding thickness by x-ray fluorescence spectrometry  

International Nuclear Information System (INIS)

An x-ray fluorescence spectrometer was designed and fabricated which nondestructively determines the thickness of aluminum cladding at small suspected thin spots in the inner or outer surface of actinide reactor tubes. The analysis method is based on the difference in absorption of actinide L/sub #alpha#/ and L/sub #beta#/ fluorescent x-rays in passing through the cladding. Calibration plots of the logarithm of the L/sub #beta#//L/sub #alpha#/ x-ray intensity ratio versus cladding thickness are linear to at least 40 mils for U-Al, U_3O_8-Al, and PuO_2-Al substrates. Accuracy and precision of the experimentally determined cladding thickness and evaluated for both uranium and plutonium substrates. Experimental thickness data are reported for 618 quality assurance analyses on six Mark 41 PuO_2-Al target tubes. An x-ray fluorescence cladding thickness monitor operated with a computer-controlled fluoroscope holds considerable ...

1978-01-01

183

Mapping the Spatiotemporal Dynamics of Calcium Signaling in Cellular Neural Networks Using Optical Flow  

UK PubMed Central (United Kingdom)

An optical flow gradient algorithm was applied to spontaneously forming networks of neurons and glia in culture imaged by fluorescence optical microscopy in order to map functional calcium signaling...Full Text Available

2010-08-01

184

Lysozyme dimer formation on lysozyme oxidation with B./2 as studied by fluorescence evolution  

International Nuclear Information System (INIS)

Lysozyme dimers produced on oxidation of lysozyme with Br_2anion radicals in aqueous solutions exhibit a fluorescence spectrum (lambdasub(max) = 400 nm) closely similar to that of bi-tyrosine. This suggests that the dimer is likely to have a tyrosine-tyrosine bond resulting from the combination of tyrosine phenoxy radicals of two lysozyme molecules. Kinetic studies on dimer formation were made by measuring time-dependent fluorescence after pulsed-electron irradiation over wide pH range. The results lead to the following conclusions. The second-order growth of the dimer fluorescence observed at pH 10.7-12.5 reflects the combination process of the lysozyme radicals, which is rate-determining in the pH range. On the other hand, the first-order growth observed at pH 6.8-10.2 is attributable to the enolization of the keto-form of the dimer. A tentative reaction scheme is proposed for the dimer formation. (author).

185

Imaging of calcium transients in skeletal muscle fibers.  

UK PubMed Central (United Kingdom)

Epifluorescence images of Ca2+ transients elicited by electrical stimulation of single skeletal muscle fibers were studied with fast imaging techniques that take advantage of the large fluorescence...Full Text Available

1991-01-01

186

Images of photoreceptors in living primate eyes using adaptive optics two-photon ophthalmoscopy  

UK PubMed Central (United Kingdom)

In vivo two-photon imaging through the pupil of the primate eye has the potential to become a useful tool for functional imaging of the retina. Two-photon excited fluorescence images...Full Text Available

187

Identification and In Vivo Characterization of NvFP-7R, a Developmentally Regulated Red Fluorescent Protein of Nematostella vectensis  

UK PubMed Central (United Kingdom)

BackgroundIn recent years, the sea anemone Nematostella vectensis has emerged as a critical model organism for comparative genomics and developmental biology. Although...Full Text Available

188

Human Lymphatic Architecture and Dynamic Transport Imaged Using Near-infrared Fluorescence12  

UK PubMed Central (United Kingdom)

BACKGROUND: Although the importance of lymphatic function is well recognized, the lack of real-time imaging modalities limits our understanding of its role in many diseases. In a phase...Full Text Available

189

High-Sensitivity Analysis of Naturally Occurring Sugar Chains, Using a Novel Fluorescent Linker Molecule  

UK PubMed Central (United Kingdom)

To analyse the binding of sugar chains to proteins, viruses and cells, the surface plasmon resonance (SPR) technique is very convenient and effective because it is a real-time, non-destructive detection...Full Text Available

2009-07-01

190

Fluorimetric study of the interaction between nicotinamide adenine dinucleotide phosphate and tetracycline-europium complex and its application  

Energy Technology Data Exchange (ETDEWEB)

A new spectrofluorimetric method was developed for the determination of trace amount of nicotinamide adenine dinucleotide phosphate (NADP). Using europium (Eu{sup 3+})-tetracycline (TC) complex as a fluorescent probe, in the buffer solution of pH 7.60. NADP can remarkably enhance the fluorescence intensity of the Eu{sup 3+}-TC complex at {lambda} = 612 nm and the enhanced fluorescence intensity of Eu{sup 3+} ion is in proportion to the concentration of NADP. Optimum conditions for the determination of NADP were also investigated. The dynamic range for the determination of NADP is 4.4 x 10{sup -7} to 2.2 x 10{sup -6} mol l{sup -1} with detection limit of 6.9 x 10{sup -8} mol l{sup -1}. This method is simple, practical and relatively free interference from coexisting substances and can be successfully applied to determination of NADP in synthetic water samples and in serum samples. Moreover, the enhancement mechanisms of the ...

2005-09-06

191

Fluorescence amplified fragment length polymorphism for subtyping of genotypes of Acanthamoeba isolated from patients with keratitis  

UK PubMed Central (United Kingdom)

Background & objectives:Acanthamoeba keratitis (AK) is a painful and vision-threatening ocular infection. The differentiation of Acanthamoeba...Full Text Available

2011-01-01

192

Evaluation of Multiplexed Fluorescent Microsphere Immunoassay for Detection of Autoantibodies to Nuclear Antigens  

UK PubMed Central (United Kingdom)

Antibodies to extractable nuclear antigens (ENA) are found in a variety of collagen vascular diseases. Determining the individual specificities of these antibodies is extremely useful in establishing...Full Text Available

2004-11-01

193

Enantioselective Fluorescent Recognition of Chiral Acids by Cyclohexane-1,2-diamine-Based Bisbinaphthyl Molecules  

UK PubMed Central (United Kingdom)

The cyclohexane-1,2-diamine-based bisbinaphthyl macrocycles (S)-/(R)-5 and their cyclic and acyclic analogs are synthesized. The interactions of...Full Text Available

2007-06-22

194

Electronic absorption and emission spectra of Alq3 in solution with special attention to a delayed fluorescence  

International Nuclear Information System (INIS)

Tris(8-quinolinolato)aluminum(III) (Alq3) shows electronic absorption bands at 378, 360 (in a 1:1 mixed solvent of methanol and ethanol (ME) at 77 K), 334, 316, 300, 263, 255.8, and 233 nm in ethanol at room temperature. According to the polarized fluorescence excitation spectrum together with MO calculations, for instance, the 360 nm band is assigned to an LL CT transition (an intramolecular charge transfer transition between two ligands), and the 378 nm band to an LM/ML CT one (an intramolecular charge transfer transition between ligand and metal). Alq3 shows a broad fluorescence band peaking at around 478 nm in the ME matrix at 77 K. The emission spectrum measured with a phosphoroscope has two emission bands at 567 and 478 nm. The 567 nm band accompanies vibronic bands at 578 and 605 nm, being safely assigned to a phosphorescence of Alq3. The lifetimes of the 478 and 567 nm bands are both 5.4 ms. The lifetime of the 478 nm band together with ...

2008-08-01

195

Dual-channel imaging system for singlet oxygen and photosensitizer for PDT  

UK PubMed Central (United Kingdom)

A two-channel optical system has been developed to provide spatially resolved simultaneous imaging of singlet molecular oxygen (1O2) phosphorescence and photosensitizer (PS) fluorescence...Full Text Available

196

Drug-binding properties of human alpha-foetoprotein.  

UK PubMed Central (United Kingdom)

The drug-binding properties of human alpha-foetoprotein (alpha FP) were investigated by a fluorescence-spectral method. Human alpha FP was shown to bind to albumin's site I marker (warfarin, phenylbutazone),...Full Text Available

1985-10-01

197

Distance-dependent interactions between gold nanoparticles and fluorescent molecules with DNA as tunable spacers  

International Nuclear Information System (INIS)

Using stoichiometrically controlled 1:1 functionalization of gold nanoparticles with fluorescent dye molecules in which the dye molecule is held away from the particle surface by a rigid DNA spacer allows precise determination of the distance-dependent effect of the metal nanoparticles on fluorescence intensity. Two dyes were studied, Cy3 and Cy5, with two sizes of nanoparticles, 5 and 10 nm. The larger the particle, the more quenching of the photoluminescence (PL) intensity, due to increased overlap of the dye's emission spectrum with the Au surface plasmon resonance. Fluorescence is quenched significantly for distances somewhat larger than the particle diameter, in good agreement with the predictions of an electrodynamics model based on interacting dipoles. The distance dependence of surface energy transfer behavior, i.e. quenching efficiency, is proportional to 1/d4, which involves no consideration of the size of the ...

2009-12-02

198

Determination of trace elements in Syrian medicinal plants and their infusions by energy dispersive X-ray fluorescence and total reflection X-ray fluorescence spectrometry  

Energy Technology Data Exchange (ETDEWEB)

X-ray fluorescence (XRF) and total-reflection X-ray fluorescence (TXRF) techniques suited well for a multi-element determination of K, Ca, Mn, Fe, Cu, Zn, Rb, and Sr in some Syrian medicinal plant species. The accuracy and the precision of both techniques were verified by analyzing the Standard Reference Materials (SRM) peach-1547 and apple leaves-1515. A good agreement between the measured concentrations of the previously mentioned elements and the certified values were obtained with errors less than 10.7% for TXRF and 15.8% for XRF. The determination of Br was acceptable only by XRF with an error less than 24%. Furthermore, the XRF method showed a very good applicability for the determination of K, Ca, Mn, Fe, Cu, Zn, Rb, Sr, and Br in infusions of different Syrian medicinal plant species, namely anise (Anisum vulgare), licorice root (Glycyrrhiza glabra), and white wormwood (Artemisia herba-alba)

2009-07-15

200

Determination of heptacaine hydrochloride in solution using nuclear analytical methods  

Energy Technology Data Exchange (ETDEWEB)

The applicability of two nuclear analytical methods: radionuclide X-ray fluorescence analysis and radiometric titrations based on precipitate formations was studied in order to determine the heptacaine hydrochloride in solutions. The applied methods were evaluated based on the obtained sensitivity values.

1984-01-20

201

Determination of heptacaine hydrochloride in solution using nuclear analytical methods  

International Nuclear Information System (INIS)

The applicability of two nuclear analytical methods: radionuclide X-ray fluorescence analysis and radiometric titrations based on precipitate formations was studied in order to determine the heptacaine hydrochloride in solutions. The applied methods were evaluated based on the obtained sensitivity values. (author).

1984-01-01

202

Comprehensive molecular cytogenetic analysis of sorghum genome architecture: distribution of euchromatin, ...  

Science.gov (United States)

Cyteogenetic maps of sorghum chromosomes 3-7, 9, and 10 were constructed on the basis of the fluorescence in situ hybridization (FISH) of ~ ... regions of heterchromatin were delimited for all 10 sorghum chrom...

203

Compact Image Slicing Spectrometer (ISS) for hyperspectral fluorescence microscopy  

UK PubMed Central (United Kingdom)

An image slicing spectrometer (ISS) for microscopy applications is presented. Its principle is based on the redirecting of image zones by specially organized thin mirrors within a custom fabricated...Full Text Available

2009-07-20

204

Calcium gradients and buffers in bovine chromaffin cells.  

UK PubMed Central (United Kingdom)

1. Digital imaging and photometry were used in conjunction with the fluorescent Ca2+ indicator, Fura-2, to examine intracellular Ca2+ signals produced by depolarization of single adrenal chromaffin...Full Text Available

1992-05-01

205

Analyzing the Light Energy Distribution in the Photosynthetic Apparatus of C4 Plants Using Highly Purified Mesophyll and Bundle-Sheath Thylakoids.  

UK PubMed Central (United Kingdom)

The chlorophyll fluorescence characteristics of mesophyll and bundle-sheath thylakoids from plant species with the C4 dicarboxylic acid pathway of photosynthesis were investigated using flow cytometry....Full Text Available

1996-11-01

206

A post-labeling method for multiplexed and multicolored genotyping analysis of SSR, indel and SNP markers in single tube with bar-coded split tag (BStag)  

UK PubMed Central (United Kingdom)

BackgroundGenotyping analysis using capillary DNA sequencing with fluorescently labeled primer pairs obtained by polymerase chain reaction (PCR) is widely used, but is expensive....Full Text Available

207

A Software System for Data Analysis in Automated DNA?Sequencing  

UK PubMed Central (United Kingdom)

Software for gel image analysis and base-calling in fluorescence-based sequencing consisting of two primary programs, BaseFinder and GelImager, is described. BaseFinder is a framework for trace processing,...Full Text Available

1998-06-01

208

Zinc determination in medicinal powders by radionuclide X-ray fluorescence analysis  

International Nuclear Information System (INIS)

X-ray fluorescence analysis was used to determine the zinc content of the ''Perilacin'' powder and the ZnO content of the ''Epiderman-pix'' powder. The characteristic Ksub(#alpha#) line of zinc was excited using a "1"4"7Pm/Mo source (10"7 s"-"1) and the molybdenum Ksub(#alpha#) line (17.47 keV). 4 to 5% Zn and 45 to 49% ZnO were determined with a NaI(Tl) scintillation detector. The radiation intensity was found to decrease with particle size. (M.K.).

1977-01-01

209

Use of X-ray fluorescence analysis in the study of archeological samples  

International Nuclear Information System (INIS)

Radionuclide X-ray fluorescence analysis (XFA) was used in the determination of the contents of metal residues in dosing plates for coin minting. XFA was also used for the determination of the strontium/calcium ratio in bone samples of different animals with the aim to obtain information on the food composition of these animals. It was found that bones of different animals can be distinguished based on the Sr/Ca ratio. No significant differences in the Sr/Ca ratio were observed in human bones of individuals from different social groups. (author). 1 fig., 5 tabs., 4 refs.

1988-09-26

210

The use of x-ray fluorescence in the detection of inorganic elements in medicines drugs  

International Nuclear Information System (INIS)

Based on the instrumental wavelength dispersive X-ray fluorescence technique of analysis (W D-X R F), the inorganic elements in four samples of commercial medicines drugs were analyzed. The samples were used without any chemical separation of the elements or chemical pre-treatment. Eleven elements could be identified, namely Si, P, S, Cl, K, Ca, Ti, Mn, Fe, Cu and Zn. However, Si, Ti and Mn have not been mentioned in the printed instructions for the use of the medicines drugs by the producers. (author)

211

Plasma-edge studies in ISX-B and EBT-S using surface probes and laser-induced fluorescence  

Energy Technology Data Exchange (ETDEWEB)

Surface probe and laser-induced fluorescence measurements in ISX-B and EBT-S have made significant contributions to the understanding of plasma edge characteristics and plasma-surface interactions in these devices. Where comparison is possible, these techniques have led to results which are consistent with plasma diagnostics. Charge-exchange neutral sputtering and self-ion sputtering have been identified as the dominent heavy impurity release mechanisms in ISX-B and EBT-S, respectively.

1982-08-01

212

Multielement analysis of air samples  

International Nuclear Information System (INIS)

Radionuclide X-ray fluorescence analysis for nondestructive determination of Fe, Zn, Pb, and Br in air samples collected on nitrocellulose membrane filter Synpor 4 is described. A "2"3"8Pu source for the excitation and a semiconductor Si/Li detector for the detection of characteristic and L-fluorescent radiation of the above elements were used. A correction method based upon the measurements of simple or multiple Compton scattering for compensation of varying mass per unit area values in sample deposits was theoretically proposed and experimentally tested. The results obtained both with and without the correction were compared and good agreement with those given by atomic absorption spectrometry was observed. (author).

1981-01-01

213

Measurement of M shell X-ray production cross sections and fluorescence yields for the elements in the atomic range 70#<=#Z#<=#92 at 5.96 keV  

International Nuclear Information System (INIS)

Total M X-ray cross sections for 12 elements in atomic range 70#<=#Z#<=#92 were measured at 5.96 keV Mn K X-ray photon energy. The average M shell fluorescence yields (anti #omega#_M) of these elements have also been observed using the presently measured cross section values and the theoretical M shell photoionisation cross section values. (orig.).

214

Inner-shell excitation of intrinsic luminescence and resonantly excited X-ray fluorescence at Be 1s edge in oriented BeO crystals  

International Nuclear Information System (INIS)

The results of studies of the time-resolved luminescence of self-trapped excitons (STE) with different multiplicity as well as the X-ray emission in oriented BeO crystals under excitation in the vicinity of the 1 s Be photoabsorption edge are presented. The branching of the electronic excitations relaxation depends strongly on the crystal orientation after the inner-shell excitation. The common features between the processes of the STE luminescence and resonantly excited X-ray fluorescence have been discussed.

2007-05-21

215

Identification of elements in plant drugs and their water infusion using X-ray fluorescence analysis  

International Nuclear Information System (INIS)

The present work gives preliminary results of analysis of drug mixtures (NEPHROSAL tea bag) and its water infusion. In a sample of dried drugs the elements K, Ca, Mn, Fe, Ni, Cu, Zn, Br, Rb, Sr, Pb were identified, whereas in their water infusion only Ca, Mn, Zn and Sr were found. The method applied was radionuclide X-ray fluorescence analysis using a radionuclide source "1"0"9Cd, a Si/Li semiconductor detector and a multichannel analyzer Canberra 8100. (author) 6 refs.; 3 figs.

8100-01-01

216

Fluorescence resonance energy transfer using lanthanide-ion doped oxide nanoparticles as donors  

Science.gov (United States)

We have demonstrated fluorescence resonance energy transfer (FRET) between lanthanide-ion doped oxide nanoparticles acting as donors and organic acceptor molecules (Cy5). Due to the long nanoparticle lifetime and the large Stokes shift between nanoparticle absorption and emission, unambiguous and precise FRET measurements can be performed despite the presence of large free acceptor oncentrations. We determined FRET efficiencies as a function of Cy5 concentration which are in very good agreement with a multiple acceptor-multiple donor calculation.

2006-03-01

217

Diagnosing hepatocellular carcinoma with the intensity and the lifetime of two-photon red autofluorescences  

Science.gov (United States)

We demonstrated that the intensity levels and lifetimes of two-photon autofluorescences (2PAF) in human liver tissues can be exploited to diagnose hepatocellular carcinoma (HCC). Excited by an infrared femtosecond laser, we suppressed the two-photon autofluorescences of most endogenous fluorophores and made red autofluorescences more specific to particular molecules in the cryo-sectioned human livers. Using such fluorescence contrast, we found HCC tissues have reduced levels of 2PAF and longer fluorescence lifetime.

2011-02-01

218

Determination of concentration distribution of admixtures by radionuclide X-ray fluorescence analysis  

International Nuclear Information System (INIS)

A theoretical analysis is presented for the method of determining the concentration distribution of admixtures in zone melting and in the study of diffusion in melts. Continuous mode X-ray fluorescence analysis is considered. The convolution integral interpreting the analog output of the ratemeter was solved applying the mathematical apparatus of Z transformation. The feasibility of the method is tested on an example of the determination of tin distribution in tungsten. With respect to the statistical error (#delta#<1.5%), the maximum integration constant (100 s) and a very slow sample feed (0.025 mm/s) were used. The calculated transfer function reflects the total transfer function of the ratemeter and the recorder used. (M.D.).

1985-01-01

219

Determination of Mn, Fe, Cu, Zn, and Pb in particulate matter, raw and final materials of a brick factory by radionuclide X-ray fluorescence analysis  

International Nuclear Information System (INIS)

Radionuclide X-ray fluorescence method with a Si/Li semiconductor detector and "2"3"8Pu exciting source was used in the study of Mn, Fe, Cu, Zn, and Pb content of solid emissions, raw and final materials of a brick factory. From the point of view of metal content, the working environment if the brick factory is safe for workers. (author) 2 refs.; 2 figs.; 1 tab.

1994-01-01

220

Three-dimensional simulation study of compact toroid plasmoid injection into magnetized plasmas  

Energy Technology Data Exchange (ETDEWEB)

Three-dimensional dynamics of a compact toroid (CT) plasmoid, which is injected into a magnetized target plasma region is investigated by using magnetohydrodynamic (MHD) numerical simulations. It is found that the process of the CT penetration into this region is much more complicated than what has been analyzed so far by using a conducting sphere (CS) model. The injected CT suffers from a tilting instability, which grows with the similar time scale as the CT penetration. The instability is accompanied by magnetic reconnection between the CT magnetic field and the target magnetic field, which disrupts the magnetic configuration of the CT. Magnetic reconnection plays a role to supply the high density plasma initially confined in the CT magnetic field into the target region. Also, the penetration depth of the CT high density plasma is examined. It is shown to be shorter than that estimated from the CS model. The CT high ...

1999-04-01

221

The Proposed Yucca Mountain Repository From A Corrosion Perspective  

Energy Technology Data Exchange (ETDEWEB)

Corrosion is a primary determinant of waste package performance at the proposed Yucca Mountain Repository and will control the delay time for radionuclide transport from the waste package. Corrosion is the most probable and most likely degradation process that will determine when packages will be penetrated and the shape, size, and distribution of those penetrations. The general issues in corrosion science, materials science and electrochemistry are well defined, and the knowledge base is substantial for understanding corrosion processes. In this paper, the Yucca Mountain Repository is viewed from a corrosion perspective. A major component of the long-term strategy for safe disposal of nuclear waste at the Yucca Mountain Repository is first to completely isolate the radionuclides in the waste packages for long times and to greatly retard the egress and transport of radionuclides from penetrated packages. Therefore, ...

2005-04-12

222

Root Architecture of Jarrah (Eucalyptus marginata) Trees in Relation to Post-Mining Deep Ripping in Western Australia  

British Library Electronic Table of Contents (United Kingdom)

Abstract This research aimed to investigate coarse root systems of Jarrah (Eucalyptus marginata Donn ex Sm.) trees at a 13-year-old restored bauxite mine site in south-western Australia. Excavations in an area with small trees (low-quality site) revealed that deep ripping equipment failed to penetrate the cemented lateritic subsoil, restricting coarse roots (roots >5 mm in diameter) to the top 0.5 m of the soil profile, resulting in fewer (1,344 stems/ha) and smaller (mean height 4.5 m) Jarrah trees. An adjacent area within the same pit (high-quality site), with a stand density of 3,256 stems/ha and a mean height of 8.0 m, had a kaolinitic clay subsoil which coarse roots penetrated to the average ripping depth (1.5 m). Trees at the low-quality site did not penetrate the subsoil with their ...

2007-01-01

223

Reverse time migration for ground penetrating radar using finite difference time domain method; Jikan ryoiki yugenn sabunho ni yoru chichu reda no ribasu taimu maigureshon  

Energy Technology Data Exchange (ETDEWEB)

The reversion time migration, as one of reflection seismic prospecting migration, reverse propagates a wave equation by reverse promoting the differential time, and conducts the migration. The method has such merits as no limit to the inclined angle of a reflection, correspondence to a complex topography etc. And, there is a finite difference time domain (FDTD) that uses the Maxwell equation as it is and makes a difference approximation in the methods differentiating and resolving electro-magnetic fields. It is also possible to apply the reverse time migration onto it. In this speech, using an explosive reflection face, a slope 2 layer structure and models of its reflection points are synthesized by a ground penetrating radar using the FDTD, and reverse time migration is conducted. As a result, it is clarified that the reverse time migration is valid for the ground penetrating radar recording. And, the cases including a diffusion item in the ...

1999-02-01

224

Modeling jet penetration in glass  

Energy Technology Data Exchange (ETDEWEB)

It is well known that composite armors, consisting of glass elements confined with metallic tampers, are extraordinarily effective against shaped charge attack. Early experiments showed that jets fired against glass targets appeared to be bombarded by tiny fragments that destroyed alignment and reduced residual jet penetration. This result was attributed to an elastic rebound effect in which the outward radial motion of the target around the jet periphery was supposed to be arrested by tensile hoop stresses which developed behind the divergent shock front. Glass fragments were then accelerated radially inward and these destabilized the jet. To sustain the large tensile hoop stresses required, the glass must not have been fractured by the initial shock, behind which the stress state is typically well above the Hugoniot elastic limit. Modeling the penetration of a jet into glass requires not only determining the spall strength, i.e., the tensile ...

1990-04-05

225

Coal-mine-hazard detection using in-seam ground-penetrating-radar transillumination. Report of Investigations/1987  

Energy Technology Data Exchange (ETDEWEB)

The Bureau of Mines recently completed peliminary studies to demonstrate the feasibility of using Ground-Penetrating Radar (GPR) for in-seam hazard detection. Investigations included air and coal tests for the purpose of checking equipment accuracy, coal penetration, and other factors such as the effects of receiver orientation. Further investigations involved using both a short pulse and a new prototype synthetic-pulse system to locate a clay vein in a coal seam using transillumination. Data were gathered on multiple travel paths, and a back-projection processing technique was then used to create a tomographic image using the calculated velocities. A computer model of the same coal seam was subsequently processed using the same tomogrpahic technique, and the results were compared with those of the actual data. Results of these preliminary studies show that GPR is feasible for use in in-seam hazard detection and point the direction that future ...

1987-01-01

226

The influence of electron-beam irradiation on some mechanical properties of commercial multilayer flexible packaging materials  

International Nuclear Information System (INIS)

The influence of electron-beam irradiation on mechanical properties of commercial multilayer flexible packaging materials based on coextruded and laminated polypropylene (PP), low-density polyethylene (LDPE), ethylene vinyl alcohol copolymer (EVOH) and poly(ethylene terephthalate) (PET), irradiated with doses up to 120 kGy, was studied. The tensile strength and elongation at break of the irradiated PET/PP film increase, while the penetration and sealing resistance decreased. In addition, the irradiated PET/LDPE/EVOH/LDPE film presented increase in the tensile strength on some radiation doses and decrease of the penetration and sealing resistance, except for sealing resistance at radiation dose of 15 kGy that resulted in a slight increase of ca 4%.

2008-09-21

227

Studies of alloy 800 in HTR helium by the Dragon project  

International Nuclear Information System (INIS)

Several heats of Alloy 800 are included in a survey of materials being creep tested in a simulated HTR helium atmosphere in the temperature range 650 to 800degC. The results are, as yet, incomplete, but indicate wide variations in the influence of the atmosphere on creep properties. Some heats appear, from results so far available up to 10,000 hours duration, to have greater creep strength in helium than in air, but others have the strength reduced by as much as 20%. Metallographic examination of terminated creep test bars and of unstressed samples indicates that oxidation of reactive constituents takes place, forming a surface scale and sub-surface oxide penetration. Carburisation can also occur and at 750 to 800degC this can penetrate to a depth of up to 800 #mu# m after 5000 h. (author).

228

Retinue of the beans roots growth by using neutron radiography technique  

International Nuclear Information System (INIS)

Agricultural practices frequently cause the development of a soil compacted layer below the surface. These compacted layers restrict the root penetration into deeper layers of soil, in search for water. It is proposed to monitor, using Non Destructive Test, the roots growth due to the planting of standard seeds in different agricultural soils, in function of their compactness and humidity. It will be used the neutrons beams derived from an irradiation channel called J-9 of the Reactor Argonauta (IEN/CNEN), so that the neutron radiographic images of the soil-plant system can be obtained. Each root can be evaluated for its ability to penetrate into compacted soil layers; this fact would mean an optimization of agricultural harvests. (author)

2002-08-11

229

Neutron and gamma-ray penetrations in thick iron  

Energy Technology Data Exchange (ETDEWEB)

Measurements of neutron and gamma-ray penetrations in an iron shield were performed up to a 60-cm depth in a tightly coupled source shield configuration with the fast-neutron reactor YAYOI as a source. Rates of neutron reactions and gamma-ray dose rates in the iron shield were obtained using activation foils and thermoluminescent dosimeters. Analyses of the experiments were made by using the DOT-III code with coupled neutron and gamma-ray cross sections from ENDF/B-IV and POPOP4 libraries. To obtain the source condition for the iron shield analyses, the calculated spectrum was adjusted to the measured reaction rates at the reactor shield boundary. The calculated neutron and gamma-ray distributions in the iron shield show fairly good agreement with the experiments. The effect of difference in Bondarenko-type self-shielding factors on the analyses of the iron shield is also shown.

1980-03-01

230

Group structure and weighting function effects on neutron penetration through thick sodium-iron shields  

Energy Technology Data Exchange (ETDEWEB)

The effects of group structures and weighting functions on neutron penetration through a thick Na-Fe geometry are studied. The recommended broad-group (61-neutron/23-gamma-ray) and few-group (22-neutron/10-gamma-ray) structures are tailored to the sodium and iron resonances, windows, and capture gamma-ray spectra. The best weighting functions are shown to be fine-group fluxes selected from a few key locations in the geometry. These group structures and weighting functions, relative to existing group structures and conventional weighting functions, improve the accuracy of the computed 61-neutron-group Bonner ball responses by up to one hundred percent and of the computed 22-neutron-group results by up to six hundred percent.

1987-01-01

231

Fourier transform IR studies on the interaction of selected chemicals with isolated cuticles  

International Nuclear Information System (INIS)

It is known that the plant cuticle represents the first barrier that must be overcome by any chemical reaching the plant surface from the atmosphere before entering the plant. Because of the importance of the cuticle as a barrier to penetration of a wide variety of compounds, its morphology, chemistry, and permeability have been extensively studied. However, only limited information is available on the nature of functional chemical groups present and their interaction and role during the penetration process. The usefulness of in situ Fourier transform infrared spectroscopy studies in identifying functional groups present in isolated cuticles is described and their relationships to the structure of the cuticular membrane are discussed. Applications of infrared spectroscopy on the presence and role of phenolics in the cuticle structure and during the cuticle development, nitrogen oxide binding to isolated cuticles, and the interactions between ...

232

Explosives solve downhole problems  

Energy Technology Data Exchange (ETDEWEB)

Shaped charges were first used more than 30 years ago to perforate casing, cement sheath and reservoir to provide selective communication between the reservoir and well bore. Since then, advances have been made in design of shaped charge sand ancillary equipment. Penetration has increased considerably. Miniaturization of equipment allows passing through relatively small restrictions and effectively communicating with reservoirs. Gun debris has been drastically reduced and in some designs eliminated. Deep reservoirs can be effectively penetrated under down-hole environments exceeding 500 F and 20,000 psi. This work covers the problems encountered and reviews successful devices employing shaped charge and explosive technology.

1981-11-01

233

Enhanced carbon dioxide removal by promoted hot potassium carbonate in a split-flow absorber  

Energy Technology Data Exchange (ETDEWEB)

In this work, a comprehensive model has been developed for the absorption of carbon dioxide into promoted hot potassium carbonate solution. The model, which is based on penetration theory, incorporates an extensive set of important reactions and takes into account the coupling between mass transfer and chemical kinetics. The penetration theory provides an appropriate absorption rate and enhancement factor for the chemical absorption. Operating data for carbon dioxide absorption into DEA-hot potassium carbonate solution has been compared with model predictions. The impact of parameters such inlet temperature of lean solution, promoter concentration, liquid split fraction, hot feed location and type of promoter on the performance of a split-flow absorber have been examined. The use of other promoters is an efficient way to enhance the carbon dioxide absorption, which has been discussed in this paper.

2004-07-01

234

Effects of spray characteristics on engine performance in a small direct injection diesel engine  

Energy Technology Data Exchange (ETDEWEB)

The engine performance test was studied at high load in a small direct injection diesel engine by measuring fuel spray travel of three nozzles having different nozzle length/nozzle diameter(L/D) and by changing parameters such as piston cavity diameter and intake swirl. Hydrocarbon(HC) and the brake specific fuel comsumption(BSFC) were mainly influenced by spray characteristics due to L/D compared with piston cavity diameter and intake swirl. The piston cavity diameter optimal to BSFC corresponds to the fuel spray travel(fuel penetration) in each nozzle. The exhaust smoke was improved by reducing piston cavity diameter and by promoting the intake swirl. NOx increased with the decrease of piston cavity diameter at the identical nozzle and also increased in case of larger piston cavity diameter owing to the utilization of intense spray penetration. (13 figs, 4 refs)

1988-06-25

235

Development of the Weapon Borne Sensor parachute system  

Energy Technology Data Exchange (ETDEWEB)

A parachute system was designed and prototypes built to deploy a telemetry package behind an earth-penetrating weapon just before impact. The parachute was designed to slow the 10 lb. telemetry package and wire connecting it to the penetrator to 50 fps before impact occurred. The parachute system was designed to utilize a 1.3-ft-dia cross pilot parachute and a 10.8-ft-dia main parachute. A computer code normally used to model the deployment of suspension lines from a packed parachute system was modified to model the deployment of wire from the weapon forebody. Results of the design calculations are presented. Two flight tests of the WBS were conducted, but initiation of parachute deployment did not occur in either of the tests due to difficulties with other components. Thus, the trajectory calculations could not be verified with data. Draft drawings of the major components of the parachute system are presented.

1998-06-01

236

Computational modeling of dynamic-failure mechanisms in armor/anti-armor materials. Final report, 1 Oct 88-30 Sep 91  

Energy Technology Data Exchange (ETDEWEB)

The purpose of this project was to develop improved dynamic failure models for brittle materials (primarily ceramics). The approach to developing these failure models was to establish a database (ACERAM) in which fundamental material properties and processing information could be directly correlated with ballistic performance data. Under this contract, a comprehensive literature search was conducted, many contacts were established in the armor/anti-armor research and development community, and database development was undertaken. A more limited project was also undertaken to assess and compare the effects of material properties and penetration mechanisms on the ballistic performance of depleted uranium and tungsten alloy penetrators.

1991-02-01

237

Apparatus for measuring the decontamination factor of a multiple filter air-cleaning system  

Energy Technology Data Exchange (ETDEWEB)

An apparatus for measuring the overall decontamination factors of first and second filters located in a plenum. The first filter separates the plenum's upstream and intermediate chambers. The second filter separates the plenum's intermediate and downstream chambers. The apparatus comprises an aerosol generator that generates a challenge aerosol. An upstream collector collects unfiltered aerosol which is piped to first and second dilution stages and then to a laser aerosol spectrometer. An intermediate collector collects challenge aerosol that penetrates the first filter. The filtered aerosol is piped to the first dilution stage, diluted, and then piped to the laser aerosol spectrometer which detects single particles. A downstream collector collects challenge aerosol that penetrates both filters. The twice-filtered aerosol is piped to the aerosol spectrometer. A pump and several valves control the movement of aerosol within the ...

1985-07-03

238

Uranium isotopic assay instrument  

International Nuclear Information System (INIS)

Full text: The isotopic assay instrument under development at Pacific Northwest National Laboratory (PNNL) is capable of rapid prescreening to detect small and rare particles containing high concentrations of uranium in a heterogeneous sample. The isotopic measurement concept is based on laser vaporization of solid samples followed by sensitive isotope-specific detection using either uranium atomic fluorescence emission or uranium atomic absorbance. Both isotopes are measured concurrently, following a single ablation laser pulse using two external-cavity violet diode lasers. The simultaneous measurement of both isotopes enables the correlation of the fluorescence and absorbance signals on a shot-to-shot basis. This measurement approach demonstrated negligible channel crosstalk between isotopes. Scanning the heterogeneous samples provides high-resolution imagery of sample isotopic fluorescence and absorbance. Isotopically ...

2006-10-16

239

[Heart injuries: diagnosis and therapy].  

Science.gov (United States)

The clinical manifestation of wounds of the heart is determined by the mode, site and size of the injury as well as the structure of the pericardial and myocardial lesion. Diagnosis can be confirmed by ECG and echocardiography. Only 20% of the patients with penetrating wounds of the heart live for more than 30 minutes. Pericardio-centesis should be used only to gain time for a safe sternotomy, cardiac decompression and suture of the wound of the heart. An aggressive surgical approach is mandatory. Cardiopulmonary bypass is necessary only to correct of concomitant lesions. PMID:1983618

1990-01-01

240

The combined transduction of copper, zinc-superoxide dismutase and catalase mediated by cell-penetrating peptide, PEP-1, to protect myocardium from ischemia-reperfusion injury  

UK PubMed Central (United Kingdom)

BackgroundOur previous studies indicate that either PEP-1-superoxide dismutase 1 (SOD1) or PEP-1-catalase (CAT) fusion proteins protects myocardium from ischemia-reperfusion-induced...Full Text Available

241

Stratigraphic drilling report - GSQ Taroom 17  

Energy Technology Data Exchange (ETDEWEB)

GSQ Taroom 17 was drilled 18 km northeast of Injune, adjacent to the type of section of the Hutton Sandstone, in the Surat Basin. The bore penetrated sedimentary rocks of the Surat Basin overlying Triassic sedimentary rocks of the Bowen Basin, and is situated in an area that has been subjected to faulting, possibly since the Late Carboniferous-early Permian. The bore provided core material for detailed petrographic, clay analysis, petrophysical and source-rock determinations. 23 references.

1986-01-01

242

On protecting steel pile foundations of oil field structures from corrosion  

Energy Technology Data Exchange (ETDEWEB)

In the area of seasonally thawing soil, porous or broken coatings cannot significantly retard the process of pile metal destruction, since it will occur through electroosmotic penetration of the base electrolyte to the metal surface. Such processes can be prevented by electrochemical protective methods. Systems based on grid cathode stations with power control and distribution units are recommended for use for cathode protection of steel pile foundations.

1980-01-01

243

Identification of physochemical factors controlling the capacity of nano-particles to penetrate cells of the respiratory epithelium  

Environmental Research Database

Objectives1) To establish a protocol for transfection of immortalised type I cells with SiRNA and its effect on cell viability; 2) To optimise silencing of genes involved in endocystosis using SiRNA and confirm successful transfection with western blotting; 3) To investigate the effect of gene silencing on uptake of flourescently-labelled latex nanoparticles.DescriptionTo investigate the mechanisms of particle uptake.

2009-01-31

244

Finding two-dimensional peaks  

CERN Document Server

Two-dimensional generalization of the original peak finding algorithm suggested earlier is given. The ideology of the algorithm emerged from the well known quantum mechanical tunneling property which enables small bodies to penetrate through narrow potential barriers. We further merge this ``quantum'' ideology with the philosophy of Particle Swarm Optimization to get the global optimization algorithm which can be called Quantum Swarm Optimization. The functionality of the newborn algorithm is tested on some benchmark optimization problems.

2004-01-01

245

Experimental study of nanoparticles penetration through commercial filter media  

Energy Technology Data Exchange (ETDEWEB)

In this study, nanoparticle penetration was measured with a wide range of filter media using silver nanoparticles from 3 nm to 20 nm at three different face velocities in order to define nanoparticle filtration characteristics of commercial fibrous filter media. The silver particles were generated by heating a pure silver powder source via an electric furnace with a temperature of 870 deg. C, which was found to be the optimal temperature for generating an adequate amount of silver nanoparticles for the size range specified above. After size classification using a nano-DMA, the particle counts were measured by an Ultrafine Condensation Particle Counter (UCPC) both upstream and downstream of the test filter to determine the nanoparticle penetration for each specific particle size. Particle sampling time continued long enough to detect more than 10{sup 5} counts at the upstream and 10 counts at the downstream sampling point so that 99.99% ...

2007-01-15

246

Eulerian simulation of the perforation of aluminum plates by nondeforming projectiles  

Energy Technology Data Exchange (ETDEWEB)

A new algorithm for the treatment of sliding interfaces between solids with or without friction in an Eulerian wavecode is described. The algorithm has been implemented in the two-dimensional version of the CTH code. The code was used to simulate penetration and perforation of aluminum plates by rigid, conical-nosed tungsten projectiles. Comparison with experimental data is provided.

1992-03-01

247

Depth of origin of the gas content in thermal waters  

Energy Technology Data Exchange (ETDEWEB)

The gas composition of recent thermal waters is in perfect conformity with their geologic-tectonic positions. The composition of gas-liquid inclusions in the basic-hyperbasic xenoliths of basaltoid lavas depends on the depth from which xenoliths are supplied. (The depth is determined by using the methods of geological thermobarometers). By comparing available data the conclusion was drawn that the gas compositions of thermal waters reflect the depth of generation of deep fluid which heats them and depends on the penetration depth of the fluid-conducting fissure zones.

1980-01-01

248

Photovoltaic lighting for outdoor telephone booth  

Energy Technology Data Exchange (ETDEWEB)

A free standing outdoor telephone booth is provided with a photovoltaic (PV) array, one or more rechargeable storage batteries and electrical control circuit which includes a temperature compensated control for limiting the supply of electrical energy from the PV array to the rechargeable battery to avoid over charging the battery, an ambient light (solar insolation) sensing circuit for controlling the electrical lamp load, to turn the lamp ON during dark ambient and OFF during light ambient conditions. In addition, the total discharge limit of the storage battery is controlled to a safe operating limit and a means is disclosed to power a fluorescent lamp at energy conserving intensities with energy derived from the rechargeable storage battery. The lamp control circuitry is preferably constituted by a high frequency power inverter with regulated output power to energize a low wattage fluorescent lamp and to dim the ...

1984-04-03

249

Measurements of K-shell x-ray production cross sections and K to L and M-shell radiative vacancy transfer probabilities for Nd, Eu, Gd, Dy and Ho at excitation with 59.5 keV photons in an external magnetic field  

International Nuclear Information System (INIS)

The effect of the #+-# 0.75 T external magnetic field on the K_#alpha#_1, K_#alpha#_2, K_#beta#_'_1 and K_#beta#_'_2 x-ray production cross sections and radiative vacancy transfer probabilities from K-shell to L2 and L3 subshells and M-shell for ferromagnetic Nd, Gd and Dy and paramagnetic Eu and Ho have been investigated, using the 59.5 keV incident photons. K-shell fluorescence yields and K x-ray intensity ratios for these elements have been determined in the external magnetic field also. The K x-rays from different targets were detected using a high-resolution Si(Li) semiconductor detector. For B = 0, the present experimental results were compared with the experimental and theoretical data in the literature. The results show that K-shell fluorescence parameters such as photoionization cross section, fluorescence yield, radiation rates, vacancy transfer probabilities and spectral linewidth can change owing to the applied ...

2006-06-19

250

Fluorescence quantum yields and cascade-free lifetimes of state selected CO_2"+, COS"+, CS_2"+ and N_2O"+ determined by photoelectron-photon coincidence spectroccopy  

International Nuclear Information System (INIS)

The details and principles of an apparatus built for measurements of fluorescence quantum yields and cascade-free lifetimes of open-shell cations are reported. These rely on the detection of coincidences between energy selected photo-electrons and undispersed photons. The results of such measurements for CO"+_2,COS"+,CS"+_2 and N_2O"+ in selected vibrational levels of their excited states are presented. Non-unity fluorescence quantum yields are found for some vibronic levels of CO"+_2(B), COS"+(A), N_2O"+(A) and a non-exponential decay is observed for CS"+_2(B). The data yield the following values for the radiative lifetimes: CO"+_2(A) 124 +- 6 ns,CO"+_2(B) 140 +- 7 ns, COS"+(A) 550 +- 50 ns and N_2O"+(A) 240 +- 12 ns. (orig.).

1980-10-01

251

Fluorescence based molecular in vivo imaging; Fluoreszenzgestuetzte molekulare Bildgebung in vivo  

Energy Technology Data Exchange (ETDEWEB)

Molecular imaging represents a modern research area that allows the in vivo study of molecular biological process kinetics using appropriate probes and visualization methods. This methodology may be defined- apart from the contrast media injection - as non-abrasive. In order to reach an in vivo molecular process imaging as accurate as possible the effects of the used probes on the biological should not be too large. The contrast media as important part of the molecular imaging can significantly contribute to the understanding of molecular processes and to the development of tailored diagnostics and therapy. Since more than 15 years PTB is developing optic imaging systems that may be used for fluorescence based visualization of tissue phantoms, small animal models and the localization of tumors and their predecessors, and for the early recognition of inflammatory processes in clinical trials. Cellular changes occur during many diseases, thus the molecular imaging ...

2008-12-15

252

A fluorescent aminolipid from a green photosynthetic bacterium  

Energy Technology Data Exchange (ETDEWEB)

A preliminary chemical characterization is presented of phosphate-free aminolipids isolation from Chlorobium limicola f. thiosulfatophilum. The lipid contains no phosphorus, glycerol, sugar, ornithine, or lysine. Ultraviolet absorption and fluorescence spectra indicate that the amino moiety of the lipid is an aromatic heterocyclic compound. Infrared spectra indicate that the lipid is a secondary or tertiary amide, and gas chromatograhic analysis of the hydrolyzed lipid shows that for each 1100 g of lipid, 1 mol of myristic acid (C/sub 14:0/) is linked in an amide bond. Acid hydrolysis of the lipid yields two fluorescent substances, A (ninhydrine positive) and B (negative), in addition to myristic acid. Proton nuclear magnetic resonance (NMR) studies indicate that substance A contains a butyl groups attached to a conjugated ring carbon, two equivalent ethyl groups attached to one or two nitrogen atoms, and two downfield protons (8.4 ppm), ...

1983-04-12

253

X-ray fluorescence in research on Czech cultural monuments  

Energy Technology Data Exchange (ETDEWEB)

Radionuclide X-ray fluorescence analysis (RXRFA), as a non-destructive method, relatively simple and allowing measurements to be carried out in situ, is an excellent tool in research on various objects of art. A range of artefacts have been investigated by our laboratory, in part for the purposes of history of art and in part as a basis for restoration works - medieval frescoes in some Czech castles and churches, metal sculptures and objects of applied art, paints and inks of old manuscripts, paintings. Some of these are among the most valuable monuments in the Czech cultural heritage. The contribution of the results of the tests to the investigation of their 'life story' and, in some cases, to their conservation, is not negligible. Later additions and repairs can be recognised, and materials and technologies that are close to their historic counterparts can be used in restoration work.

2004-01-01

254

X-ray fluorescence in research on Czech cultural monuments  

International Nuclear Information System (INIS)

Radionuclide X-ray fluorescence analysis (RXRFA), as a non-destructive method, relatively simple and allowing measurements to be carried out in situ, is an excellent tool in research on various objects of art. A range of artefacts have been investigated by our laboratory, in part for the purposes of history of art and in part as a basis for restoration works - medieval frescoes in some Czech castles and churches, metal sculptures and objects of applied art, paints and inks of old manuscripts, paintings. Some of these are among the most valuable monuments in the Czech cultural heritage. The contribution of the results of the tests to the investigation of their 'life story' and, in some cases, to their conservation, is not negligible. Later additions and repairs can be recognised, and materials and technologies that are close to their historic counterparts can be used in restoration work.

2004-01-01

255

Unfolding analysis of the mature and unprocessed forms of Bacillus licheniformis ?-glutamyltranspeptidase  

British Library Electronic Table of Contents (United Kingdom)

Bacillus licheniformis ?-glutamyltranspeptidase (BlGGT) undergoes an autocatalytic process to generate 44.9 and 21.7?kDa subunits; however, a mutant protein (T399A) loses completely the processing ability and mainly exists as a precursor. For a comprehensive understanding of their structural features, the biophysical properties of these two proteins were investigated by circular dichroism and fluorescence spectroscopy. Tryptophan fluorescence and circular dichroism spectra were nearly identical for BlGGT and T399A, but unfolding analyses revealed that these two proteins had a different sensitivity towards temperature- and guanidine hydrochloride (GdnHCl)-induced denaturation. BlGGT and the unprocessed T399A displayed T m values of 61.4?C and 68.1?C, respectively, and thermal unfolding of b...

2011-01-01

256

Transmission nuclear resonance fluorescence measurements of "2"3"8U in thick targets  

International Nuclear Information System (INIS)

Transmission nuclear resonance fluorescence measurements were made on targets consisting of Pb and depleted U with total areal densities near 86g/cm"2. The "2"3"8U content in the targets varied from 0% to 8.5% (atom fraction). The experiment demonstrates the capability of using transmission measurements as a non-destructive technique to identify and quantify the presence of an isotope in samples with thicknesses comparable to the average thickness of a nuclear fuel assembly. The experimental data also appear to demonstrate the process of notch refilling with a predictable intensity. Comparison of measured spectra to previous backscatter "2"3"8U measurements indicates general agreement in observed excited states. Evidence of two new "2"3"8U excited states and possibly a third state have also been observed.

2011-05-15

257

Total M shell X-ray production cross sections and average fluorescence yields in 11 elements from Tm to U at photon energy of 5.96 keV  

International Nuclear Information System (INIS)

Total M shell X-ray production cross section for 11 elements with 69 #<=# Z #<=# 92 have been measured using an incident photon energy of 5.96 keV. Measurements have been performed using an "5"5Fe annular source and a Si(Li) detector. Average M shell fluorescence yield at each incident photon energy has been deduced, using the experimental total M X-ray production cross section and theoretical M shell photoionization cross section. Present experimental results are compared with other experimental and theoretical values. Reasonable agreement (to within 0.3-28%) is typically obtained between present and other experimental and theoretical values.

2005-04-01

258

The investigations on K and L X-ray fluorescence parameters of gold compounds  

British Library Electronic Table of Contents (United Kingdom)

The study aimed to determine the chemical effects on the K and L X-ray intensity ratios and the K and L X-ray production cross sections for gold compounds. The K shell fluorescence yields and L shell average yields were also investigated. The samples were excited by 59.5keV ?-rays from an 241Am annular radioactive source and 123.6keV ?-rays from a 57Co annular radioactive source. K and L X-rays emitted from samples were counted by an Ultra-LEGe detector with a resolution of 0.150keV at 5.9keV. The experimental values were compared with theoretical, the semi-empirical and other experimental values.

2010-01-01

259

Synthesis of reversible fluorescent organogel containing 2-(2prime-hydroxyphenyl)benzoxazole: fluorescence enhancement upon gelation and detecting property for nerve gas simulant  

British Library Electronic Table of Contents (United Kingdom)

A new low molecular mass organogelator 1 containing 2-(2prime-hydroxyphenyl)benzoxazole (HPB) group with long alkyl chain was synthesized by the reaction with 5-amino-2-(2prime-hydroxy-4prime-methylphenyl)benzoxazole and dodecyl isocyanate in THF at room temperature. The reversible gelation ability of 1 was investigated using a heating-cooling method in various organic solvents. The stable organogel was formed from carbon tetrachloride or from cyclohexane at the concentration as low as 0.9%. The self-assembled supramolecular gel structure formed by non-covalent bonding was confirmed with field emission-scanning electron microscope (FE-SEM) exhibiting fibril- or ribbon-shaped structure depending on the solvent used. Regarding the aggregation-induced emission enhancement (AIEE) phenomenon, t...

2010-01-01

260

Structural characterization of liposomes made of diether archaeal lipids and dipalmitoyl-L-a-phosphatidylcholine  

British Library Electronic Table of Contents (United Kingdom)

The physicochemical properties of binary lipid mixtures of diether C25,25 lipids and dipalmitoyl-L-a-phosphatidylcholine (DPPC) were studied using photon correlation, fluorescence and electron paramagnetic resonance spectroscopy, and transmission electron microscopy. These two types of lipids can be mixed at all molar ratios to form unilamellar and multilamellar liposomes. Fluorescence anisotropy of 1,6-diphenyl-1,3,5-hexatrien in mixed liposomes indicates that the abrupt changes in order parameter in the hydrophobic part of bilayer membranes made of DPPC lipids disappears with increasing mol%C25,25 lipids. Electron paramagnetic resonance spectroscopy shows that at temperatures below 50^oC, the interfacial regions of membrane bilayer of mixed liposomes is more fluid than for pure DPPC lipo...

2011-01-01

261

Spatial distribution of arsenic and heavy metals in willow roots from a contaminated floodplain soil measured by X-ray fluorescence spectroscopy  

British Library Electronic Table of Contents (United Kingdom)

Under changing redox conditions some plants create plaques at their root surface, which may affect the mobility and uptake of As and heavy metals but it is unknown to what extent this also holds true for willows in contaminated floodplain soils. Therefore, willow roots were sampled from a phytoremediation trial in the contaminated floodplain of the river Elbe (Germany), cryofixed, freeze-dried, and cross sections were mapped for the distribution of As, Ca, Cu, Fe, K, Mn, Ni, S and Zn by synchrotron based X-ray fluorescence spectroscopy. The elements Ca, Cu, Ni, S and Zn were concentrated in the aerenchymatic tissue, and not associated with Fe and Mn. Mixed Fe-Mn plaques covered the surface of the willow roots and As was accumulated in these plaques. The observed association pattern between...

2011-01-01

262

Solution state hybridization detection using time-resolved fluorescence anisotropy of quantum dot-DNA bioconjugates  

British Library Electronic Table of Contents (United Kingdom)

In this Letter, we demonstrate the application of time-resolved fluorescence anisotropy measurements to detect solution state hybridization of streptavidin conjugate (CdSe)ZnS quantum dots (QD). The study was performed on samples containing 10nM QD incubated with 800nM DNA. We show that the rotational correlation time of QD-DNA constructs increases significantly upon hybridization with values of 330ns (QD-ssDNA) and 1.3ms (QD-dsDNA), corresponding to a diameter of 14nm and 23nm respectively. The present study opens a new modality for hybridization detection using quantum dots.

2010-01-01

263

Sequential injection system for phospholipase A2 activity evaluation: Studies on liposomes using an environment-sensitive fluorescent probe  

British Library Electronic Table of Contents (United Kingdom)

This work reports the development of an automatic methodology based on the use of 1-anilinonaphthalene-8-sulfonate (ANS) as an interfacial fluorescent probe for detecting the hydrophobic environment shift around the probe, caused by the hydrolytic action of PLA2 on the liposomes. The implementation of this reaction in a sequential injection analysis (SIA) system along with the use of the mixing chambers permitted the evaluation of PLA2 activity and assessment of the inhibitory effect of the non-steroidal anti-inflammatory drugs (NSAIDs) on PLA2 activity. Several studies were performed with the aim of establishing the appropriate flow system configuration: the liposome substrate; PLA2 and ANS optimum concentrations and incubation times before and after the enzyme addition. Based on these st...

2009-01-01

264

Programmable radionuclide X-ray fluorescence multi-channel spectrometric analyzer, type 123-1  

International Nuclear Information System (INIS)

The whole equipment consists of three separate portable parts: a detector case, a microprocessor and a graphic TV monitor. Magnetic tape memory and an x-y recorder can be connected for recording the measured spectra. The analyzer contains two built-in exchangeable excitation radionuclides. Fluorescence and scattered radiation is detected using a proportional detector. The detected pulses are analyzed by a 256-channel analyzer and the results are shown on the display. The device may be used in mining laboratories, coal and ore dressing plant control rooms or in mining fields of open cast mines for quick detection of the quality of mined or dressed raw materials. (E.S.). 1 fig.

1988-01-01

265

Laser-fluorescence determination of trace uranium in hot spring water, geothermal water and tap water in Xi'an Lishan region  

International Nuclear Information System (INIS)

Using the Laser-Fluorescence technique, an investigation was made, adopting the standard mix method, on trace uranium concentrations in hot spring water and geothermal water from Lishan region, and in tap water from some major cities in Shanxi province. Totally 40 samples from 27 sites were investigated. Measurement showed that the tap water contains around 10"-"6 g/L of uranium, whose concentrations in both hot spring water and geothermal water are 10"-"5 g/L. Most of samples are at normal radioactive background level, some higher contents were determined in a few samples

2002-03-01

266

Interaction of insulin with a triblock copolymer of PEG-(fumaric-sebacic acids)-PEG: Thermodynamic and spectroscopic studies  

British Library Electronic Table of Contents (United Kingdom)

A comparative study on the interaction of (PEG-co-P(FA/SC)-co-PEG) triblock copolymer with bovine and human insulins was carried out using isothermal titration calorimetry (ITC), circular dichroism (CD), and fluorescence spectroscopy. ITC data show that the copolymer has a low affinity for both proteins, with an association constant of about 7?9?103?M ?1. Results also show that binding is enthalpically driven, and disfavored by conformational entropy. CD spectroscopy studies reveal a small increase in the helical content and a decrease in ?-structure as well as random coil in both proteins. Acrylamide quenching experiments display reduced accessibility of tyrosines, while intrinsic fluorescence spectra show lower tyrosine emission. Furthermore, thermal unfolding experiments, studied by far...

2007-01-01

267

Instruments for X-ray fluorescence analysis and spectrometry  

International Nuclear Information System (INIS)

The radionuclide X-ray fluorescence analyzer consists of a source changer and a sample changer. "5"5Fe, "1"0"9Cd and "2"4"1Am are used as excitation sources. The radiation is detected with a semiconductor Si(Li) detector. The complete assembly of the apparatus consists of an imagine unit, a keyboard, a floppy disc drive, a printer, a console and a rack with analog and digital electronics. Its multichannel amplitude analyzer consists of power supplies, a high voltage supply, a linear amplifier, an analog-to-digital converter and a computer. The technical specifications are given. The control and data processing system is controlled with an MHB 8080A microprocessor. Software for semiconductor gamma spectrometry and for quantitative gamma spectrometry will be supplied with the equipment. (E.S.). 3 figs., 4 refs.

268

Identification of a functional nuclear export signal in the green fluorescent protein asFP499  

International Nuclear Information System (INIS)

The green fluorescent protein (GFP) asFP499 from Anemonia sulcata is a distant homologue of the GFP from Aequorea victoria. We cloned the asFP499 gene into a mammalian expression vector and showed that this protein was expressed in the human lymphoblast cell line Ramos RA1 and in the embryonic kidney 293T cell line (HEK 293T). In HEK 293T cells, asFP499 was localized mainly in the cytoplasm, suggesting that the protein was excluded from the nucleus. We identified _1_9_4LRMEKLNI_2_0_1 as a candidate nuclear export signal in asFP499 and mutated the isoleucine at position 201 to an alanine. Unlike the wildtype form, the mutant protein was distributed throughout the cytoplasm and nucleus. This is First report of a GFP that contains a functional NES.

2006-04-21

269

Human cDNA mapping using fluorescence in situ hybridization  

Energy Technology Data Exchange (ETDEWEB)

Genetic mapping is approached using the techniques of high resolution fluorescence in situ hybridization (FISH). This technology and the results of its application are designed to rapidly generate whole genome as tool box of expressed sequence to speed the identification of human disease genes. The results of this study are intended to dovetail with and to link the results of existing technologies for creating backbone YAC and genetic maps. In the first eight months, this approach generated 60--80% of the expressed sequence map, the remainder expected to be derived through more long-term, labor-intensive, regional chromosomal gene searches or sequencing. The laboratory has made significant progress in the set-up phase, in mapping fetal and adult brain and other cDNAs, in testing a model system for directly linking genetic and physical maps using FISH with small fragments, in setting up a database, and in establishing the validity and throughput of the system.

1993-03-04

270

Groundtruth approach to accurate quantitation of fluorescence microarrays  

Energy Technology Data Exchange (ETDEWEB)

To more accurately measure fluorescent signals from microarrays, we calibrated our acquisition and analysis systems by using groundtruth samples comprised of known quantities of red and green gene-specific DNA probes hybridized to cDNA targets. We imaged the slides with a full-field, white light CCD imager and analyzed them with our custom analysis software. Here we compare, for multiple genes, results obtained with and without preprocessing (alignment, color crosstalk compensation, dark field subtraction, and integration time). We also evaluate the accuracy of various image processing and analysis techniques (background subtraction, segmentation, quantitation and normalization). This methodology calibrates and validates our system for accurate quantitative measurement of microarrays. Specifically, we show that preprocessing the images produces results significantly closer to the known ground-truth for these samples.

2000-12-01

271

Determination of selected elements by radionuclide X-ray fluorescence analysis after the separation on different kinds of sorption materials  

International Nuclear Information System (INIS)

This paper aimed to the evaluation of different kinds of sorbent material preparation and to the evaluation of their characteristics at different pH conditions by X-ray fluorescence analysis. This method is suitable for identification and determination of elements in samples of different character, state and origin because it is a polycomponent, non-destructive, fast and simple analytical method. Moreover, it allows timeadvantageous and reliable measurements. This paper studies problems concerning the determination of some selected elements (Mn, Fe, Ni, Cu, Zn, Pb) in pharmaceutical samples of sodium chloride in the solid state as well as in its solution by sorption on chelating extraction membrane 3M Empore"T"M and on the strongly acidic ion-exchanger Dowex 50Wx8. Conditions for the most effective sorption of determined elements are also interpreted. (author)

2008-03-01

272

Determination of selected elements by radionuclide X-ray fluorescence analysis after the separation on different kinds of sorption materials  

British Library Electronic Table of Contents (United Kingdom)

This paper aimed to the evaluation of different kinds of sorbent material preparation and to the evaluation of their characteristics at different pH conditions by X-ray fluorescence analysis. This method is suitable for identification and determination of elements in samples of different character, state and origin because it is a polycomponent, non-destructive, fast and simple analytical method. Moreover, it allows time-advantageous and reliable measurements. This paper studies problems concerning the determination of some selected elements (Mn, Fe, Ni, Cu, Zn, Pb) in pharmaceutical samples of sodium chloride in the solid state as well as in its solution by sorption on chelating extraction membrane 3M Empore? and on the strongly acidic ion-exchanger Dowex 50Wx8. Conditions for the most ef...

2008-01-01

273

Comparison of fluorescence in situ hybridisation using peptide nucleic acid probes, Gram stain/acridine orange leukocyte cytospin and differential time to positivity methods for detection of catheter related bloodstream infection in patients after haematopoietic stem cell transplantation  

British Library Electronic Table of Contents (United Kingdom)

Abstract In 46 febrile neutropenic patients who had undergone haematopoietic stem cell transplantation, the fluorescence in situ hybridisation using peptide nucleic acid probes (PNA FISH), Gram stain/acridine orange leukocyte cytospin (Gram/AOLC), and differential time to positivity (DTP) methods were performed for detection of catheter related bloodstream infections (CRBSIs). As compared with the DTP method (which detected 11 patients with CRBSI), the PNA FISH and the Gram/AOLC methods detected ten of 11 CRBSI patients, resulting in a sensitivity, specificity, negative predictive value and positive predictive value of 91%, 100%, 97% and 100%, respectively, for the PNA FISH method as well as for the Gram/AOLC method.

2010-01-01

274

Amyloid oligomers: spectroscopic characterization of amyloidogenic protein states  

British Library Electronic Table of Contents (United Kingdom)

It is assumed that protein fibrils manifested in amyloidosis result from an aggregation reaction involving small misfolded protein sequences being in an `oligomeric' or `prefibrillar' state. This review covers recent optical spectroscopic studies of amyloid protein misfolding, oligomerization and amyloid fibril growth. Although amyloid fibrils have been studied using established protein-characterization techniques throughout the years, their oligomeric precursor states require sensitive detection in real-time. Here, fluorescent staining is commonly performed using thioflavin T and other small fluorescent molecules such as 4-(dicyanovinyl)- julolidine and 1-amino-8-naphtalene sulphonate that have high affinity to hydrophobic patches. Thus, populated oligomeric intermediates and related `pre...

2010-01-01

275

XRF and PIXE method as trols for the element analysis of metallic glasses  

International Nuclear Information System (INIS)

The radionuclide X-ray fluorescence and particle induced X-ray emission methods were used for rapid and nondestructive analysis of metallic glasses. The methods were compared for accuracy and precision with the atomic absorption method. Some results of the analyses of Fe_xNi_8_0_-_xB_2_0 materials are briefly reviewed. The distribution of elements along the width as well as the length and a qualitative analysis of the composition of material surfaces are considered. (author).

1986-01-01

276

XRF and PIXE analysis of metallic glasses  

International Nuclear Information System (INIS)

Radionuclide X-ray fluorescence and particle induced X-ray emission methods were used for a rapid and nondestructive analysis of metallic glasses. The methods are compared in accuracy and precision with the atomic absorption method. Some results of analyses of Fe_xNi_8_0_-_xB_2_0 materials are briefly reviewed. The distribution of elements along the width and length, and a qualitative analysis of the composition of material surfaces are considered. (author) 3 refs.

1987-05-01

277

X-ray spectral microanalysis of component redistribution in finely dispersed two-phase alloys  

International Nuclear Information System (INIS)

It is shown that it is necessary to take into account locality of the analysis and to introduce additional corrections for partial capture of matrix and fluorescent subexcitation by matrix during quantitative X-ray spectral microanalysis of finely dispersed materials. Cast two-phase (#alpha#+#beta#) titanium alloy VT3-1 is chosen as an investigation object.

278

Width of the 1. 836-MeV level in /sup 88/Sr  

Science.gov (United States)

Using bremsstrahlung, the resonance fluorescence yield has been measured for the 1.836-MeV 2/sup +//sub 1/ level in /sup 88/Sr. The observed yield corresponds to a level width GAMMA = 2.94 +- 0.15 meV.

1977-06-01

279

Unique Properties of Thermally Tailored Copper: Magnetically Active Regions and Anomalous X-ray Fluorescence Emissions  

UK PubMed Central (United Kingdom)

When high-purity copper (≥99.98%wt) is melted, held in its liquid state for a few hours with iterative thermal cycling, then allowed to resolidify, the ingot surface is found to have...Full Text Available

2009-12-24

280

The Effects of Surface Chemistry on the Properties of Proteins Confined in Nano-porous Materials  

Energy Technology Data Exchange (ETDEWEB)

The entrapment of proteins using the sol-gel route provides a means to retain its native properties and artificially reproduce the molecular crowding and confinement experienced by proteins in the cell allowing investigation of the physico-chemical and structural properties of biomolecules at the biotic/abiotic interface. The biomolecules are spatially separated and 'caged' in the gel structure but solutes can freely permeate the matrix. Thus, properties such as the folding of ensembles of individual molecules can be examined in the absence of aggregation effects that can occur in solution studies. Green fluorescent protein from Aequorea coerulescens was used as a model protein to examine the unfolding/re-folding properties of protein in silica gels. The recombinant protein was isolated and purified from Escherichia coli extracts by cell lysis, three-phase partitioning, dialysis, and anion exchange chromatography. The purity of the protein was ...

2007-09-01

281

Standard deviation of measurement results in x-ray fluorescence spectrometry  

International Nuclear Information System (INIS)

The standard deviation of measurement results of a given element in XRF spectrometry depends on three factors: concentration and concentration region, atomic number and matrix. The effects of these factors were investigated by an XRF instrument type ARL 72.000 for aluminium metal, bauxite-red mud and aluminium using computerized data processing. A comparison of linear and nonlinear relation between concentration and the result of XRF analysis was made for the determination of standard deviation. (R.P.).

1984-11-13

282

Spectroscopic studies of the Sm_3Ga_5O_1_2 monocrystals  

International Nuclear Information System (INIS)

The fluorescence, absorption, infrared and Raman spectra of Sm_3Ga_5O_1_2 have been investigated. The energy-level schemes in the energy range 3000-16000 cm"-"1 have been determined. The number and symmetries of the Sm_3Ga_5O_1_2 crystal normal mode have been obtained by the molecular site group analysis and their comparison with the experiment has been made.

283

Some relationships between ultraviolet light and heme-protein-induced peroxidative lipid breakdown in liposomes, as reflected by fluorescence changes: the effect of negative surface charge  

International Nuclear Information System (INIS)

The water soluble, photolabile nitrene precursor, azidonaphthalene-2,7-disulfonic acid (ANDS) was encapsulated in small unilamellar, isoelectric (egg PC) or negatively charged (egg PC + dihexadecylphosphate) liposomes. The individual and combined effects of heme-proteins and UV irradiation on the fluorescence of these vesicles under aerobic conditions were studied. Consistent with the catalytic action of heme-proteins on lipid peroxidation and peroxide decomposition, addition of cytochrome c (positively charged) or catalase (negatively charged) to the vesicles elicited immediate formation of a fluorescence band at 470 nm, characteristic of Schiff bases that form from aldehyde byproducts of decomposing hydroperoxides. Ultraviolet irradiation of liposomes caused no significant changes in the fluorescence spectrum, in spite of the radiolysis of ANDS inside the vesicles with consequent formation of nitrene radicals. When ...

284

Some optimization measurements and parameters of a radionuclide X-ray fluorescence spectrometer  

International Nuclear Information System (INIS)

An irradiation head with sample holders is described and measurement geometry is reported. Measurements were made for optimizing the distance between the source and the sample and for optimizing the sample diameter. The optimal distance between the source and the sample does not depend on the collimator diameter. The sample diameter should not exceed 30 - 35 mm. Sensitivity and detection limits were determined for Zn, Pb and Br and calibration curves were plotted. (M.D.) 6 figs., 2 tabs., 4 refs.

1986-01-01

285

Remote measurement of methane in coal mines: a review  

Energy Technology Data Exchange (ETDEWEB)

The authors identify a need for a device which can remotely measure methane in coal mines. Similar techniques which have been used to measure atmospheric pollutants are discussed. These techniques include adsorption, Raman scattering and fluorescence. While differential adsorption and Raman scattering techniques have potential there are a number of problems to be resolved before they could be applied effectively. It is felt that an area which may provide suitable technology sometime in the future is in the field of laser sources. 6 refs., 4 tabs.

1987-02-01

286

Radionuclide X-ray fluorescence analysis of drinking water using preconcentration of trace metals on chelating cellulose exchanger ostsorb-oxin  

International Nuclear Information System (INIS)

Determination of Cr, Fe, Cu, Zn and Pb in drinking water preconcentrated on a chelating ion exchanger of Czechoslovak production is described. The analytical system consisted of a radionuclide source "2"3"8Pu, a Si/Li semiconductor detector and a multichannel analyzer. Results are compared with trehshold limit values recommended for drinking water. (author) 9 refs.; 2 figs.

1992-04-01

287

Radioanalytical chemistry. Vol. 2  

International Nuclear Information System (INIS)

This volume of the monograph covers the following topics: activation analysis, non-activation interaction analysis (elastic scattering of charged particles, absorption and backscattering of beta radiation and photons, radionuclide X-ray fluorescence analysis, thermalization, scattering and absorption of neutrons, use of ionization caused by nuclear radiation, use of ionization by alpha or beta radiation for the measurement of pressure, density and flow rate of gases), and automation in radioanalytical chemistry. (P.A.).

1989-01-01

288

Photoexcitation and optical pumping in a barium atomic beam  

International Nuclear Information System (INIS)

An apparatus allowing the photoexcitation of barium atomic beam over its whole surface is described. This photoexcitation is achieved by another barium spectrum emitted up steam of the beam by a cathodic out-flow produced at the exit oven. The fluorescence spectrum is studied in detail as well as the influence of different parameters, such as oven temperature, current intensity of the outflow, and excitation depth. A calculation shows how to determine Einstein coefficient, oscillator strengths and atomic lifetimes from our experimental measurements.

289

Near-Infrared Fluorescence Labeled Anti-TAG-72 Monoclonal Antibodies for Tumor Imaging in Colorectal Cancer Xenograft Mice  

UK PubMed Central (United Kingdom)

Anti-TAG-72 monoclonal antibodies target the tumor-associated glycoprotein (TAG)-72 in various solid tumors. This study evaluated the use of anti-TAG-72 monoclonal antibodies, both murine CC49...Full Text Available

2009-01-01

290

Measurement of time of travel in streams by dye tracing  

Energy Technology Data Exchange (ETDEWEB)

The US Geological survey is active in measuring time of travel in streams using dye tracers. This manual describes methods of measuring time of travel of water and waterborne solutes by dye tracing. The fluorescent dyes, measuring equipment used, and field and laboratory procedures are also described. Methods of analysis and presentation to illustrate time of travel of streams are provided.

1989-01-01

291

Measurement of K x-ray intensity ratio of tin, gadolinium and dysprosium  

International Nuclear Information System (INIS)

Full text: Measurement of K_#beta# to K_#alpha# x-ray intensity ratios are important not only in the field of atomic physics, radiation physics and medical physics, but also to test the validity of assumptions made in the theoretical prediction. The intensity ratios can also give information on the effect of physical and chemical environment of the element in the compound. Many investigators have adopted a single and double reflection geometries to measure the K_#beta# to K_#alpha# x ray intensity ratios to understand the effect of physical and chemical environment on x-ray fluorescence. The targets are excited by a radioactive source of having activity of the order 100 MBq. in order to carry out accurate measurement K_#beta# to K_#alpha# x-ray intensity ratios, we have develop 2#pi# geometrical configuration method : placing a target right on the surface of the detector facing the target to measure the K shell fluorescence parameters such as ...

2003-11-01

292

Laser-induced fluorescence measurement of sup(6,7)lithium isotope shift  

Energy Technology Data Exchange (ETDEWEB)

Values of frequency splittings in the lithium isotopes have been determined with the aid of laser-induced fluorescene in a supersonic beam, perpendicularly irradiated by a CW ring dye laser. The residual 2s-2p isotope shift has been found to bw 4721.8 +- 2.0 MHz, leading to a specific mass shift for the 2p level of -3610.8 +- 5 MHz.

1986-07-01

293

Identification and determination of elements in Taraxacum officinale plant from different Bratislava localities  

Energy Technology Data Exchange (ETDEWEB)

Elements Ti, Mn, Fe, Ni, Cu, Zn, Pb, Br, Rb and Sr were determined by the method of radionuclide X-ray fluorescence analysis with semiconductor detection in samples of Taraxacum officinale from various localities of Bratislava. The dependence of their content on the source and the degree of the air pollution was found out.

1983-01-01

294

Identification and determination of elements in Taraxacum officinale plant from different Bratislava localities  

International Nuclear Information System (INIS)

Elements Ti, Mn, Fe, Ni, Cu, Zn, Pb, Br, Rb and Sr were determined by the method of radionuclide X-ray fluorescence analysis with semiconductor detection in samples of Taraxacum officinale from various localities of Bratislava. The dependence of their content on the source and the degree of the air pollution was found out. (author).

1983-01-01

295

Heavy metals in welding fumes  

Energy Technology Data Exchange (ETDEWEB)

Fe, Mn, Ni, V, Ti and Mo were determined in aerosols from manual arc welding. Samples of welding aerosols were trapped on a Synpor 4 filter. The amount of determined elements in aerosols was detected using the method of radionuclide X-ray fluorescence analysis. A /sup 241/Am annular source was used as the source of excitation radiation and radiation was processed using a Si(Li) spectrometer.

1984-10-01

296

Heavy metals in welding fumes  

International Nuclear Information System (INIS)

Fe, Mn, Ni, V, Ti and Mo were determined in aerosols from manual arc welding. Samples of welding aerosols were trapped on a Synpor 4 filter. The amount of determined elements in aerosols was detected using the method of radionuclide X-ray fluorescence analysis. A "2"4"1Am annular source was used as the source of excitation radiation and radiation was processed using a Si(Li) spectrometer. (E.S.).

1984-01-01

297

Fusion of GFP to the M.EcoKI DNA methyltransferase produces a new probe of Type I DNA restriction and modification enzymes  

UK PubMed Central (United Kingdom)

AbstractWe describe the fusion of enhanced green fluorescent protein to the C-terminus of the HsdS DNA sequence-specificity subunit of the Type I DNA modification methyltransferase M.EcoKI....Full Text Available

2010-07-23

298

Effect of Elicitation and Changes in Extracellular pH on the Cytoplasmic and Vacuolar pH of Suspension-Cultured Soybean Cells 1  

UK PubMed Central (United Kingdom)

We have employed both 31P nuclear magnetic resonance spectroscopy and two intracellular fluorescent pH indicator dyes to monitor the pH of the vacuole and cytoplasm of suspension-cultured...Full Text Available

1992-02-01

299

Determination of the Sr/Ca ratio in bones by XRFA  

International Nuclear Information System (INIS)

Radionuclide X-ray fluorescence analysis was used for the determination of Sr/Ca ratio in bones to test the influence of a diet on this ratio. Significant differences were observed for Sr/Ca ratio in bones of various animals. Only small differences in the Ca/Sr ratio were observed for the samples of various prehistoric human bones. (author) 4 refs.; 4 tabs.

1989-11-01

300

Determination of heavy metals in welders' working environment using nuclear analytical methods  

International Nuclear Information System (INIS)

Technological processes of welding are significant sources of pollution in the working area. Evaluation of chemical quality of working area was made by means of radionuclide x-ray fluorescence analysis and activation analysis with fast neutrons. Welding aerosols were sampled by filtration method on Synpor 4 membrane ultra-filters. For selected types of welding filter metals, determination of heavy metals in aerosols was performed. (author).

1985-01-01

301

Determination of heavy metals in welders' working environment using nuclear analytical methods  

Energy Technology Data Exchange (ETDEWEB)

Technological processes of welding are significant sources of pollution in the working area. Evaluation of chemical quality of working area was made by means of radionuclide x-ray fluorescence analysis and activation analysis with fast neutrons. Welding aerosols were sampled by filtration method on Synpor 4 membrane ultra-filters. For selected types of welding filter metals, determination of heavy metals in aerosols was performed.

1985-01-03

302

Determination of heavy metals in industrial wastewaters and their influence on activated sludge biocenose  

International Nuclear Information System (INIS)

Radionuclide X-ray fluorescence method with a Si/Li semiconductor detector and "2"3"8Pu exciting source was used in the determination of Cr, Fe, Ni, Cu, and Zn content in industrial wastewaters. Simultaneously, the effects of the wastewaters on activated sludge biocenose were evaluated. (author) 6 refs.; 1 fig.; 1 tab.

1994-03-01

303

Determination of Mg, Al, Si, Cl and K in some medicinal plants by NAA and REA methods  

Energy Technology Data Exchange (ETDEWEB)

Trace elements have been determined in biological samples including pepperwort, thyme, plantain, blessed thistle and common comfrey as well as cabbage leaves and milk powder. Concentrations of Al, Si, and Cl have been determined by fast neutron activation analysis while, in the case of Mg-, K, and Cl the X-ray fluorescence method was used.

1982-07-26

304

Detection device for high explosives  

Energy Technology Data Exchange (ETDEWEB)

A portable fiber optic detector that senses the presence of specific target chemicals by electrostatically attracting the target chemical to an aromatic compound coating on an optical fiber. Attaching the target chemical to the coated fiber reduces the fluorescence so that a photon sensing detector records the reduced light level and activates an appropriate alarm or indicator.

1992-01-01

306

Contribution to the sample preparation in the radionuclide X-ray fluorescence analysis of hair  

International Nuclear Information System (INIS)

Methods of sample treatment in XRF analysis of hair are studied in view of the effect on analytical results. A new method is proposed based on the incomplete ashing of hair followed by pellet preparation. Its suitability is estimated on the XRF analysis of real hair samples collected from 4 healthy adults. (author) 12 refs.; 4 figs.; 1 tab.

1989-03-01

307

Application of isotope-excitation x-ray fluorescence (XRF) analysis for aluminium production  

International Nuclear Information System (INIS)

An energy sensitive Si(Li) detector XRF analyzer built by ATOMKI, Hungary, has been applied for various analytical purposes in alumina production at the Almasfuezitoe Alumina Company, Hungary. Specifically, the CaO content in red mud was determined by the new XRF technique using isotope excitation sources. The analysis of other components is under way. (R.P.).

308

Analysis of titanium and zirconium in red mud with energy dispersive x-ray spectrometry  

Energy Technology Data Exchange (ETDEWEB)

An energy dispersive x-ray fluorescence technique was used for the determination of Titanium (Ti) and Zirconium (Zr) in red mud by using a standard addition method. An annular {sup 241}Am source is employed for excitation of K shells of elements. 13 refs., 2 figs., 1 tab.

1996-11-01

309

A study of the interactions of some polypyridylruthenium (II) complexes with DNA using fluorescence spectroscopy, topoisomerisation and thermal denaturation.  

UK PubMed Central (United Kingdom)

The nature of binding of Ru(phen) 2+ (I), Ru(bipy) 2+ (II), Ru(terpy) 2+ (III) (phen = 1,10-phenanthroline, bipy 3 = 2,2'-bipyridyl, 3 terpy = 2,2'2," - 2 terpyridyl) to DNA, poly[d(G-C)] and poly[d(A-T)]...Full Text Available

1985-09-11

310

A simple system of instruments for radionuclide X-ray fluorescence analysis in nonferrous metallurgy  

International Nuclear Information System (INIS)

Proceeding from commercially available instruments, a simple measuring system has been established, which renders possible fast and simple discontinuous analysis of individual elements. This measuring system is described, giving some examples of utilization in nonferrous metallurgy (mining, ore dressing, metallurgical treatment), and specific details, such as error of measurement, ranges of measurement and limits of utilization. (author).

1979-01-01

311

2. Nuclear analytical methods and environmental protection  

International Nuclear Information System (INIS)

The first step in the protection of the environment is the control of pollutant level in the components of the environment. The application is compared of radionuclide X-ray fluorescence analysis (RXFA) used for this purpose with polarographic and nuclear analytical techniques. The advantage of RXFA is its high sensitivity and selectivity, its low time and cost exactingness. The origins and development of RXFA are described. (Ha).

1983-12-01

312

Proposition for execution control of bearing stratum in bored precast pile method. Umekomi kui koho ni okeru shijiso kakunin no tame no seko kanri hoho no teian  

Energy Technology Data Exchange (ETDEWEB)

As a parameter for execution control of confirming a bearing stratum, which is most important in a bored precast pile method, discussions were made on the relativity between the product AT'' of a load current value A'' in an electric motor driving an auger used to drill pit holes with an excavation time T'' and a value N,'' a result of the standard penetration test of the ground. As a result, although the relativity of the N'' value has some variance in the ground of diluvial clay, they correspond well to each other in other kinds of ground. In pile bearing strata in particular, they correspond very well to each other regardless of soil textures of the ground, proving clearly that the AT'' value can be used as an effective parameter for confirmation of and penetration into the bearing stratum. Therefore, tips of all the piles used in one ...

1991-07-25

313

Modeling of spray combustion in Direct-injection diesel engine. Final report, January 1984-December 1987  

Energy Technology Data Exchange (ETDEWEB)

A mathematical model was developed to predict the penetration of a transient fuel spray, the temporal and spatial distribution of air-fuel mixture before the end of ignition delay and the subsequent pressure rise during combustion in a Direct-Injection Diesel Engine with and without swirl. The model accounts for the non-isothermal and non-isobaric character of processes during fuel injection resulting from continuous motion of the piston. The effects of various engine operating variables on spray were studied and graphically presented. The calculated spray penetration with and without crossflow of air is compared with the available experimental data of other researchers with good agreement. The model can predict the rate of combustible-mixture formation, the rate of heat release and cylinder pressure as a function of time in direct injection (DI) diesel engine. A single-cylinder D.I. research diesel engine was operated with N-hexadecane as the ...

1988-01-30

314

Geothermal Heat Pump research and development studies at Sandia National Laboratories  

Energy Technology Data Exchange (ETDEWEB)

The Geothermal Heat Pump (GHP) concept was originally developed in the 1940`s. Recently, because of increasing energy costs, utility interest, and the development of simple and durable ground source heat exchangers, GHP`s have gained international attention as a proven means of energy conservation and electrical peak power demand reduction. GHP systems require installation of a buried heat exchanger to utilize the nearly constant ground temperature making them more efficient than conventional air source heat pumps. However, the high installation cost for both residential and commercial applications is a major obstacle to their market penetration. Sandia National Laboratories (SNL) through its sponsors, the Department of Energy (DOE), and the Department of Defense (DOD), has embarked on a research program to find ways to reduce GHP installation costs and improve performance, thereby increasing their market penetration. The major elements of the ...

1994-08-01

315

Fragmentation mechanisms of a single molten copper jet penetrating a sodium pool. Transition from thermal to hydrodynamic fragmentation in instantaneous contract interface temperatures below its freezing point  

International Nuclear Information System (INIS)

To clarify the fragmentation mechanism of a molten metallic fuel jet in a sodium pool under high-ejection-velocity conditions that correspond to the medium- and high-burnup conditions in the metallic fuel core of liquid-metal-cooled fast breeder reactors, a series of experiments with molten copper as a metallic fuel simulant and a sodium pool was carried out. Under low-ejection-velocity conditions in the range of an ambient Weber number (Wea) a ? 200, the size of the fragments is confirmed to be almost independent of the initial superheating of the jet. Furthermore, the size of the fragments agrees well with that evaluated using the Rayleigh-Taylor instability model, in which the fragment size is assumed to be equal to half the fastest growing wavelength. This result is qualitatively consistent with the characteristics that the molten jet column with large inertia force owing to the high ejection velocity, which transports enthalpy downwards, can penetrate the ...

2010-03-01

316

Effects of gamma irradiation on the physical properties of laminated packaging materials. 2. polypropylene-polypropylene, polypropylene-polyethylene, and polyester-polyethylene  

International Nuclear Information System (INIS)

This experiment was done to determine the effects of irradiation on the physical properties of three kinds of laminated packaging materials, i.e. polypropylene-polypropylene, polypropylene-polyethylene, polyester-polyethylene. Observations were made on pinhole production, leakage, oil resistance, resistance against insect penetration, colour, odour tensile strength, elongation at break, seal strength and tear resistance. The samples were irradiated with doses of 0, 5 and 10 kGy, then stored at room temperature and examined after 0, 3, 6 and 12 months of storage. The results showed that irradiation doses up to 10 kGy, as well as storage up to 12 months, did not create pinholes, or leakage in pouches prepared from laminated films. The resistance of the films to oil and insect penetration, the colour, and the odour were also unchanged. Both irradiation and storage treatments had a significant effect on physical properties of the laminated films. ...

317

Damage to metallic samples produced by measured lightning currents  

Energy Technology Data Exchange (ETDEWEB)

A total of 10 samples disks of 2024-T3 aluminum and 4130 ferrous steel were exposed to rocket-triggered lightning currents at the Kennedy Space Center test site in Florida during the summer of 1990. The experimental configuration was arranged so that the samples were not exposed to the preliminary streamer, wire-burn, or following currents that are associated with an upward-initiated rocket-triggered flash but which are a typical of naturally initiated lightning. Return-stroke currents and continuing currents actually attaching to the sample were measured, augmented by close-up video recordings of approximately 3 feet of the channel above the sample and by 16-mm movies with 5-ms resolution. From these data it was possible to correlate individual damage spots with streamer, return-stroke, and continuing currents that produced them. Substantial penetration of 80-mil aluminum was produced by a continuing current of submedian amplitude and duration, and full ...

1991-01-01

318

Characteristics of deep penetration laser welding of dissimilar metal Ni-based cast superalloy K418 and alloy steel 42CrMo  

Science.gov (United States)

Experimental trials of autogenous deep penetration welding between dissimilar cast Ni-based superalloy K418 and alloy steel 42CrMo flat plates with 5.0 mm thickness were conducted using a 3 kW continuous wave (CW) Nd:YAG laser. The influences of laser output power, welding velocity and defocusing distance on the morphology, welding depth and width as well as quality of the welded seam were investigated. Results show that full keyhole welding is not formed on both K418 and 42CrMo side, simultaneously, due to the relatively low output power. Partial fusion is observed on the welded seam near 42CrMo side because of the large disparity of thermal physical and high-temperature mechanical properties of these two materials. The microhardness of the laser-welded joint was also examined and analyzed. It is suggested that applying negative defocusing in the range of Raylei length can increase the welding depth and improve the coupling efficiency of the laser materials ...

2007-09-01

319

Bacterial Pili exploit integrin machinery to promote immune activation and efficient blood-brain barrier penetration.  

Science.gov (United States)

Group B Streptococcus (GBS) is the leading cause of meningitis in newborn infants. Bacterial cell surface appendages, known as pili, have been recently described in streptococcal pathogens, including GBS. The pilus tip adhesin, PilA, contributes to GBS adherence to blood-brain barrier (BBB) endothelium; however, the host receptor and the contribution of PilA in central nervous system (CNS) disease pathogenesis are unknown. Here we show that PilA binds collagen, which promotes GBS interaction with the ?(2)?(1) integrin resulting in activation of host chemokine expression and neutrophil recruitment during infection. Mice infected with the PilA-deficient mutant exhibit delayed mortality, a decrease in neutrophil infiltration and bacterial CNS dissemination. We find that PilA-mediated virulence is dependent on neutrophil influx as neutrophil depletion results in a decrease in BBB permeability and GBS-BBB penetration. Our results suggest that the bacterial pilus, ...

2011-09-06

320

[Fundamental biological model for trials of wound ballistics].  

Science.gov (United States)

The aim of our experiment was the testing of effects of common ammunition on usable and slightly accessible biological tissue thereby to create fundamental simple biological model for trials of wounded ballistic. Like objective tissue was elected biological material - pork and beef hind-limbs, pork head, pork bodily cavity. It was discovered that objective tissue is able to react to singles types of shots in all spectrum results namely simple smooth penetration wound as well as splintery fracture in dependence on kind of using ammunition. Pork hind-limb was evaluated like the most suitable biological material for given object. PMID:17172163

2006-10-01

321

Wood-polymer composites obtained by gamma radiation  

International Nuclear Information System (INIS)

It has been prepared composites materials by means of monomer penetration in pores of wood samples and later curing by means of gamma irradiation. The studied species were Hura crepitans L. (catahua), Aniba puchury-minor (C. Martinez) (mohena amarilla), and Calycophyllum spruceanum (Benth.) (capirona). These new materials exhibit smaller water absorption and better mechanical properties in comparison with native wood. The test tubes of catahua treated with the styrene-polyester mixture absorb only up to 10% humidity compared to the native species whereas its hardness is increased in a 100%. (author).

2006-01-01

322

Wilson loops in warped resolved deformed conifolds  

CERN Document Server

We calculate quark-antiquark potentials using the relationship between the expectation value of the Wilson loop and the action of a probe string in the string dual. We review and categorize the possible forms of the dependence of the energy on the separation between the quarks. In particular, we examine the possibility of there being a minimum separation for probe strings which do not penetrate close to the origin of the bulk space, and derive a condition which determines whether this is the case. We then apply these considerations to the flavoured resolved deformed conifold background of Gaillard et al. We suggest that the unusual behaviour we observe in this solution is likely to be related to the IR singularity which is not present in the unflavoured case.

2011-01-01

323

Use of high energy radiation component as a reference source for radiometric testing  

International Nuclear Information System (INIS)

The possibility of providing high accuracy of absorption and albedo methods of radiometric testing due to the use of high-energy radiation component that has passed through a barrier and gone from it in the opposite direction as a reference source, is considered. It is shown that the use of high-energy component of penetrating radiation as a reference source decreases the device response to the main interference in a much larger degree than its response to the change of measured parameter. Experiments are performed using steel pipes and plates. "2"4"1Am, "1"3"7Cs and "6"0Co are used as sources.

324

The use of combustible metals in explosive incendiary devices  

Energy Technology Data Exchange (ETDEWEB)

We have investigated tailoring damage effects of explosive devices by addition of unconventional materials, specifically combustible metals. Initial small-scale as well as full-scale testing has been performed. The explosives functioned to disperse and ignite these materials. Incendiary, enhanced-blast, and fragment-damage effect have been identified. These types of effects can be used to extend the damage done to hardened facilities. In other cases it is desirable to disable the target with minimal collateral damage. Use of unconventional materials allows the capability to tailor the damage and effects of explosive devices for these and other applications. Current work includes testing of an incendiary warhead for a penetrator.

1996-08-01

325

Technetium complexes as potential brain imaging agents  

International Nuclear Information System (INIS)

Single photon tomography using lipophilic tracers provides tomographic representations of regional blood flow. To penetrate a healthy blood-brain barrier requires that radiotracers either are fat-soluble or have an affinity for one of the selective blood-brain barrier transport systems. In recent years there has been an increasing interest to explore the ideal physical characteristics of "9"9"mTc for diagnostic problems of brain diseases. The development of radiopharmaceuticals for brain imaging including the intensively studied "9"9"mTc-propyleneamineoxime derivatives is discussed. (author).

326

Single parameter analysis of hysteretic magnetic flux trapping in high T{sub c} superconductor ribbon  

Energy Technology Data Exchange (ETDEWEB)

This paper described the application of an AC surface probe, similar to presently used eddy current probes, to the measurement of DC transport critical currents and critical state dissipation in high {Tc} superconductors. It has been shown that the probe can provide quantitative measurement of the full field penetration in superconducting samples by measuring the response of AC induced screening currents for superconducting materials in the form of tapes with overlayers of silver. In this manner, the AC probe can be used to replace the contact DC probe for determining critical currents in a noncontacting and local manner suitable for scanning over or along the sample.

1992-10-01

327

Single parameter analysis of hysteretic magnetic flux trapping in high T_c superconductor ribbon  

International Nuclear Information System (INIS)

This paper described the application of an AC surface probe, similar to presently used eddy current probes, to the measurement of DC transport critical currents and critical state dissipation in high T_c superconductors. It has been shown that the probe can provide quantitative measurement of the full field penetration in superconducting samples by measuring the response of AC induced screening currents for superconducting materials in the form of tapes with overlayers of silver. In this manner, the AC probe can be used to replace the contact DC probe for determining critical currents in a noncontacting and local manner suitable for scanning over or along the sample.

1992-07-19

328

Single parameter analysis of hysteretic magnetic flux trapping in high T[sub c] superconductor ribbon  

Energy Technology Data Exchange (ETDEWEB)

This paper described the application of an AC surface probe, similar to presently used eddy current probes, to the measurement of DC transport critical currents and critical state dissipation in high [Tc] superconductors. It has been shown that the probe can provide quantitative measurement of the full field penetration in superconducting samples by measuring the response of AC induced screening currents for superconducting materials in the form of tapes with overlayers of silver. In this manner, the AC probe can be used to replace the contact DC probe for determining critical currents in a noncontacting and local manner suitable for scanning over or along the sample.

1992-01-01

329

Rapid Tools for Joint Inversion and Imaging. Final report  

Energy Technology Data Exchange (ETDEWEB)

The activities and results of a Small Business Innovation Research Phase II project entitled ''Rapid Tools for Joint Inversion and Imaging'' are presented. Research and development on three-dimensional methods to recover distributions of material property values from sparse data are reported. Innovations using artificial neural networks and extended Kalman filtering are described. The report also covers investigations on upscaling and downscaling, segmentation for data processing, and applications to ground penetrating radar and geohydraulic tomography.

2000-08-02

330

Nondestructive Technique Survey for Assessing Integrity of Composite Firing Vessel  

Energy Technology Data Exchange (ETDEWEB)

The repeated use and limited lifetime of a composite tiring vessel compel a need to survey techniques for monitoring the structural integrity of the vessel in order to determine when it should be retired. Various nondestructive techniques were researched and evaluated based on their applicability to the vessel. The methods were visual inspection, liquid penetrant testing, magnetic particle testing, surface mounted strain gauges, thermal inspection, acoustic emission, ultrasonic testing, radiography, eddy current testing, and embedded fiber optic sensors. It was determined that embedded fiber optic sensor is the most promising technique due to their ability to be embedded within layers of composites and their immunity to electromagnetic interference.

2000-08-01

331

Mineral analysis in experimental corneal scars. An EDAX study  

Energy Technology Data Exchange (ETDEWEB)

Central penetrating excisional wounds were made in the corneas of 12 rabbits and 10 trout. The scar tissue and the surrounding cornea were compared using a new method for assessing inorganic elements in the cornea: the scanning electron microscopy and energy dispersive analysis of x-ray (EDAX). Semiquantitative determination of inorganic elements within the range of atomic numbers 9-93 in the periodic system was performed, comparing the relative concentration of those elements in the scar tissue to the surrounding cornea. Results showed that calcium was the only element higher in the healing wound than in the surrounding cornea.

1988-01-01

332

Long-term monitoring of microleakage of dental cements by radiochemical diffusion  

International Nuclear Information System (INIS)

Radioactive "1"4C sucrose was found to be an ideal marker for microleakage because it did not penetrate tooth tissue, dental cement, or mounting resin. The main finding is that the adhesive cements--the glass-ionomer and polycarboxylate--are significantly more effective at preventing microleakage than are the traditional phosphate cements--silicate and zinc phosphate. The differences can be as high as two orders of magnitude. The adhesive cements provide almost perfect and reliable seals. By contrast, the nonadhesive cements are erratic sealants with most of the restorations leaking.

333

Hydrothermal industrialization electric-power systems development. Final report  

Energy Technology Data Exchange (ETDEWEB)

The nature of hydrothermal resources, their associated temperatures, geographic locations, and developable capacity are described. The parties involved in development, required activities and phases of development, regulatory and permitting requirements, environmental considerations, and time required to complete development activities ae examined in detail. These activities are put in proper perspective by detailing development costs. A profile of the geothermal industry is presented by detailing the participants and their operating characteristics. The current development status of geothermal energy in the US is detailed. The work on market penetration is summarized briefly. Detailed development information is presented for 56 high temperature sites. (MHR)

1982-03-01

334

Geothermal heat pump performance  

Energy Technology Data Exchange (ETDEWEB)

Geothermal heat pump systems are a promising new energy technology that has shown rapid increase in usage over the past ten years in the United States. These systems offer substantial benefits to customers and utilities in energy (kWh) and demand (kW) savings. The purpose of this study was to determine what existing monitored data was available mainly from electric utilities on heat pump performance, energy savings and demand reduction for residential, school, and commercial building applications. Information was developed on the status of electric utility marketing programs, barriers to market penetration, incentive programs, and benefits.

1995-12-31

335

Back-up for high voltage cable pressurizing system  

Energy Technology Data Exchange (ETDEWEB)

A back-up system is provided for a pumping plant or a pressure reservoir system used to maintain insulating oil under pressure in high voltage submarine power cables which includes a gas driven membrane pump to insure a small outflow of oil at a rupture point in the power cable to prevent water from penetrating the cable. The proper operation of the membrane pump is insured by introducing degasified oil at the drive side of the pump during the stand-by and test modes of operation of the back-up system. 11 drawings.

1982-07-19

336

Application of the neutron television fluoroscopic system to neutron computed tomography  

Energy Technology Data Exchange (ETDEWEB)

Recently the real-time neutron radiography system of the Kyoto University Reactor (KUR) has been developed and practically applied to penetrating the side plates of the MTR type reactor fuels and investigation of moving objects. In this paper an application of the KUR neutron TV system to neutron computed tomography (NCT) is described. By using the NTV system, projection data can be acquired in a single measurement and simultaneously the projection image can be observed on a CRT monitor. The Fourier-convolution technique is used to produce the reconstructed image and its image has a good enough quality for revealing water in a small hole of 1.5 mm in diameter. (orig.).

1984-10-01

337

Application of the neutron television fluoroscopic system to neutron computed tomography  

Energy Technology Data Exchange (ETDEWEB)

Recently the real-time neutron radiography system of the Kyoto University Reactor (KUR) has been developed and practically applied to penetrating the side plates of the MTR type reactor fuels and investigation of moving objects. In this paper an application of the KUR neutron TV system to neutron computed tomography (NCT) is described. By using the NTV system, projection data can be acquired in a single measurement and simultaneously the projection image can be observed on a CRT monitor. The Fourier-convolution technique is used to produce the reconstructed image and its image has a good enough quality for revealing water in a small hole of 1.5 mm in diameter.

1984-10-01

338

An application of the neutron television fluoroscopic system to neutron computed tomography  

International Nuclear Information System (INIS)

Recently the real-time neutron radiography system of the Kyoto University Reactor (KUR) has been developed and practically applied to penetrating the side plates of the MTR type reactor fuels and investigation of moving objects. In this paper an application of the KUR neutron TV system to neutron computed tomography (NCT) is described. By using the NTV system, projection data can be acquired in a single measurement and simultaneously the projection image can be observed on a CRT monitor. The Fourier-convolution technique is used to produce the reconstructed image and its image has a good enough quality for revealing water in a small hole of 1.5 mm in diameter. (orig.).

1984-10-01

339

A new solution of 150 KV overhead compact line  

Energy Technology Data Exchange (ETDEWEB)

Environmental considerations have led the Italian electric utility, ENEL, to use an advanced compact design for the reconstruction of a 60kV power line on the outskirts of Rome. This solution has achieved the following aims: minimisation of the visual impact by reducing the size of the supports; reduction of the occupation of the area especially during construction; reduction of damage due to the degree of penetration into the soil. The use of one stem tubular supports and bored pile foundations is described. The scheme has been shown to be viable in terms of planning and low environmental impact and also cost-effective and is likely to be adopted by ENEL in other situations. (UK)

1997-12-31

340

The enhanced genomic instability was induced by alpha particle and low-energy ion irradiation in somatic cells of Arabidopsis thaliana  

International Nuclear Information System (INIS)

Although low-energy ion radiation has been proven to have a wide range of biological effects and led to fruitful achievements as a new mutagenic source for genetic modification, there still exist some disputes about its mutagenic mechanisms because of its short-penetrating property. In present research, Arabidopsis thaliana transgenic for GUS recombination substrate was used to evaluate the genomic instability induced by irradiations of alpha particle (3.3MeV) and Low-energy-Argon ion (30 KeV). A pronounced effects of alpha particle irradiation to Arabidopsis thaliana seedlings and Argon ion irradiation to seeds on the somatic homologous recombination frequency (sHRF) were reported. The sHRFs increased 1.88-fold and 2.42-fold, respectively, which indicated that the short-penetrating radiation could effectively induce the plant genomic instability in either dry seeds or seedlings with active metabolism. The local alpha particle irradiation of ...

2008-08-12

341

Spectroscopic investigation of the charge dynamics of heavy ions penetrating solid and gaseous targets  

Energy Technology Data Exchange (ETDEWEB)

This thesis presents the study of the slowing down process of fast heavy ions inside matter. In the framework of this research, the influence of the target density on the stopping process is investigated. Experiments on the interaction of {sup 48}Ca{sup 6+}-{sup 48}Ca{sup 10+} and {sup 26}Mg{sup 5+} ion beams with initial energies of 11.4 MeV/u and 5.9 MeV/u with solid and gaseous targets have been carried out. A novel diagnostic method, X-ray spectroscopy of K-shell projectile radiation, is used to determine the ion charge state in relation to its velocity during the penetration of fast heavy ions inside the stopping material. A spatially resolved analysis of the projectile and target radiation in solids is achieved for the first time. The application of low-density silica aerogels as stopping media provided a stretching of the ion stopping length by 20 - 100 times in comparison with solid quartz. The Doppler Effect observed on the projectile K-shell spectra is ...

2007-01-15

342

Improving the mechanical properties of steels using low energy, high temperature nitrogen ion implantation  

Energy Technology Data Exchange (ETDEWEB)

The use of nitrogen ion implantation to increase the surface hardness of structural steels is well documented. Traditionally this involves the use of high energy nitrogen ion beams (approximately 100 keV), with a relatively low beam current density because high energy beams are necessary to produce the required penetration into the material to achieve a significant depth of hardened material. Hardening needs to occur in a region whose size is comparable with the scale of the deformation associated with the tribocontact. 100 keV nitrogen ions typically penetrate into steels only about 0.1 {mu}m and the range of possible tribological applications is thus restricted by this shallow treatment depth. In plasma nitriding processes the nitrogen ions approach the substrate with much lower energies but the ion currents are sufficiently high to cause considerable substrate heating. In this study an ion beam process has been used which more closely ...

1996-09-01

343

Dissimilar autogenous full penetration welding of superalloy K418 and 42CrMo steel by a high power CW Nd:YAG laser  

Energy Technology Data Exchange (ETDEWEB)

Experiments of autogenous laser full penetration welding between dissimilar cast Ni-based superalloy K418 and alloy steel 42CrMo flat plates with 3.5 mm thickness were conducted using a 3 kW continuous wave (CW) Nd:YAG laser. The influences of laser welding velocity, flow rate of side-blow shielding gas, defocusing distance were investigated. Microstructure of the welded seam was characterized by optical microscopy (OM), scanning electron microscopy (SEM) and X-ray diffraction (XRD) and energy dispersive spectrometer (EDS). Mechanical properties of the welded seam were evaluated by microhardness and tensile strength testing. Results show that high quality full penetration laser-welded joint can be obtained by optimizing the welding velocity, flow rate of shielding gas and defocusing distance. The laser-welded seam have non-equilibrium solidified microstructures consisting of {gamma}-FeCr{sub 0.29}Ni{sub 0.16}C{sub 0.06} austenite solid solution ...

2007-06-30

344

Dissimilar autogenous full penetration welding of superalloy K418 and 42CrMo steel by a high power CW Nd:YAG laser  

International Nuclear Information System (INIS)

Experiments of autogenous laser full penetration welding between dissimilar cast Ni-based superalloy K418 and alloy steel 42CrMo flat plates with 3.5 mm thickness were conducted using a 3 kW continuous wave (CW) Nd:YAG laser. The influences of laser welding velocity, flow rate of side-blow shielding gas, defocusing distance were investigated. Microstructure of the welded seam was characterized by optical microscopy (OM), scanning electron microscopy (SEM) and X-ray diffraction (XRD) and energy dispersive spectrometer (EDS). Mechanical properties of the welded seam were evaluated by microhardness and tensile strength testing. Results show that high quality full penetration laser-welded joint can be obtained by optimizing the welding velocity, flow rate of shielding gas and defocusing distance. The laser-welded seam have non-equilibrium solidified microstructures consisting of #gamma#-FeCr_0_._2_9Ni_0_._1_6C_0_._0_6 austenite solid solution ...

2007-06-30

345

Dissimilar autogenous full penetration welding of superalloy K418 and 42CrMo steel by a high power CW Nd:YAG laser  

Science.gov (United States)

Experiments of autogenous laser full penetration welding between dissimilar cast Ni-based superalloy K418 and alloy steel 42CrMo flat plates with 3.5 mm thickness were conducted using a 3 kW continuous wave (CW) Nd:YAG laser. The influences of laser welding velocity, flow rate of side-blow shielding gas, defocusing distance were investigated. Microstructure of the welded seam was characterized by optical microscopy (OM), scanning electron microscopy (SEM) and X-ray diffraction (XRD) and energy dispersive spectrometer (EDS). Mechanical properties of the welded seam were evaluated by microhardness and tensile strength testing. Results show that high quality full penetration laser-welded joint can be obtained by optimizing the welding velocity, flow rate of shielding gas and defocusing distance. The laser-welded seam have non-equilibrium solidified microstructures consisting of ?-FeCr0.29Ni0.16C0.06 austenite solid solution dendrites as the ...

2007-06-01

346

X-Ray Fluorescence in Research on the Cultural Heritage  

Energy Technology Data Exchange (ETDEWEB)

Radionuclide X-ray fluorescence analysis is a method, which has many advantages for analysing various historic artefacts, as it is relatively cheap, sensitive and non-destructive, and it allows measurements in-situ. However, this analysis has also certain limitations especially concerning sensitivity to chemical elements only, irrespective of the compounds or chemical forms in which these elements have been bonded. In addition, light elements emitting very soft X-rays cannot be measured, and in order to detect a wide range of elements, it is necessary to carry out repeated measurements with different radiation sources. Despite these limitations, valuable information can be obtained about the composition of historic materials and data about the origin and age of these artefacts can be derived. Analyses of wall paintings, ancient metal sculptures or other objects of art provide the basis for historic considerations documented in our results for some objects belonging ...

2001-09-15

347

X-Ray Fluorescence in Research on the Cultural Heritage  

International Nuclear Information System (INIS)

Radionuclide X-ray fluorescence analysis is a method, which has many advantages for analysing various historic artefacts, as it is relatively cheap, sensitive and non-destructive, and it allows measurements in-situ. However, this analysis has also certain limitations especially concerning sensitivity to chemical elements only, irrespective of the compounds or chemical forms in which these elements have been bonded. In addition, light elements emitting very soft X-rays cannot be measured, and in order to detect a wide range of elements, it is necessary to carry out repeated measurements with different radiation sources. Despite these limitations, valuable information can be obtained about the composition of historic materials and data about the origin and age of these artefacts can be derived. Analyses of wall paintings, ancient metal sculptures or other objects of art provide the basis for historic considerations documented in our results for some objects belonging ...

2001-09-01

348

Theoretical modelling of X-ray fluorescence signals for different lunar compositions and dependence on solar activity  

British Library Electronic Table of Contents (United Kingdom)

We present a forward modelling technique for calculating the surface X-ray spectra for a variety of lunar terrains. Our calculations considered variations in solar fluxes from solar quiescent condition to large flare activity (M1 flare), and expected elemental concentrations in the target, as well as yield, instrumental, and viewing geometry parameters for X-ray induced fluorescence from the lunar surface. Additionally, we present estimates of anticipated XRF signals from prominent Ka lines observable by a collimated 14cm2 X-ray detector from a 100km lunar orbit with 20km spatial resolution. Our results show that Mg, Al and Si characteristic Ka lines can be observed for all solar conditions. The Ca Ka lines line can be differentiated from a fixed background during more energetic solar cond...

2010-01-01

349

The influence of treatment with thiotepa, thyroxine and D3 vitamin and the effect of fast neutron radiolysis on walker tumor chromatin  

International Nuclear Information System (INIS)

Anticancer drug thyotepa (10 mg/ kg) hormonal compound thyroxine (40 mg / kg) and D3 vitamin (30,000 IU / kg) have been administrated simply or associated to Wistar rats bearing Walker carcinosarcoma. The chromatin (the complex of DNA and proteins from nuclei) has been extracted from Walker tumor and submitted to fast neutron beams produced by deuterons (13 MeV) on thick Be target at an IPNE U-120 Cyclotron, in doses of 5-100 Gy. Thermal transition of chromatin fluorescence intensity of chromatin-ethidium bromide complexes and intrinsic fluorescence of chromatin have been analysed. Association of thiotepa with thyroxine and D3 vitamin produced a diminution of chromatin lesions induced by the cytostatic. Thus in the effects of fast neutrons radiolysis in chromatin significant differences occurred. These results could help to improve the methodology of associated chemotherapy-radiotherapy in clinical applications. (author).

1995-12-02

350

Radioanalytical determination of chromium in welding fumes  

International Nuclear Information System (INIS)

Radionuclide X-ray fluorescence analysis and fast neutron activation analysis were used for the determination of chromium. The excitation source for X-ray fluorescence analysis was a ring-shaped "2"4"1Am source with an activity of 18.5x10"9 Bq. SYNPOR filters of 35 mm in diameter were used for the measurement. The 5.414 keV Cr peak was measured with a Si(Li) detector. The sensitivity was 0.05 mg for a period of measurement of 1000 s. A neutron generator with an emission of 10"9 s"-"1 was used as the source of fast neutrons. "5"2V and "5"3V, the products of nuclear reaction with Cr, were measured gamma spectrometrically with a Ge(Li) detector. The sensitivity for Cr is 0.015 mg, in the presence of Mn which causes interference the sensitivity is a mere 0.075 mg. The mentioned methods were used to determine total Cr and Cr(VI) in welding aerosols. It was found that the most toxic form, i.e., Cr(VI), is released during manual arc welding of high ...

1985-01-01

351

Radiation methods in research of ancient monuments  

Energy Technology Data Exchange (ETDEWEB)

A 'Laboratory of Quantitative Methods in Monument Research' is being built at the CTU Prague. Its primary orientation is the investigation of historic architecture, although other objects of art can also be investigated. In the first phase, two radiation methods are being established, but it is set up in such a way, that various other methods can readily be added in its future development. The radiation methods chosen for the initial development of the laboratory are: thermoluminescence dating and X-ray fluorescence analysis. The design of the automated TL-reader, built in our laboratories, is adjusted for the purpose of dating of historic brick architecture (which, of course, does not exclude applications for ceramics and other materials). The investigation of renaissance architecture in southern Bohemia and Moravia is under preparation as the first large campaign of this kind in the Czech Republic. Radionuclide X-ray ...

2000-11-15

352

Radiation methods in research of ancient monuments  

International Nuclear Information System (INIS)

A 'Laboratory of Quantitative Methods in Monument Research' is being built at the CTU Prague. Its primary orientation is the investigation of historic architecture, although other objects of art can also be investigated. In the first phase, two radiation methods are being established, but it is set up in such a way, that various other methods can readily be added in its future development. The radiation methods chosen for the initial development of the laboratory are: thermoluminescence dating and X-ray fluorescence analysis. The design of the automated TL-reader, built in our laboratories, is adjusted for the purpose of dating of historic brick architecture (which, of course, does not exclude applications for ceramics and other materials). The investigation of renaissance architecture in southern Bohemia and Moravia is under preparation as the first large campaign of this kind in the Czech Republic. Radionuclide X-ray fluorescence analysis has ...

2000-11-15

353

Photophysical characteristics of 4,4'-bis(N-carbazolyl)tolan derivatives and their application in organic light emitting diodes  

International Nuclear Information System (INIS)

4,4'-bis(N-carbazolyl)tolan (BCT) and 4,4'-bis[N-(3,6-di-t-butyl)carbazolyl]tolan (BCT-t-Bu) were synthesized as ?-expanded analogs of 4,4'-bis(N-carbazolyl)biphenyl. Their photophysical characteristics both in solution and films were thoroughly investigated. Interestingly, the phosphorescence spectrum of BCT was significantly medium-dependent, and the emission maximum was red-shifted by 131 nm from 489 nm in solution at 77 K to 620 nm in a deposited film at 5 K, suggesting the presence of strong intermolecular interactions in the film. BCT and BCT-t-Bu were found to be useful as host materials for fluorescence-based organic light emitting diodes (OLEDs). However, their low triplet energy levels in films negated their potential to act as hosts in phosphorescence-based OLEDs. - Research highlights: ? We synthesized N-carbazolyl-tolan derivatives (BCT) as ?-expanded analogues of CBP. ? We found that BCT derivatives are useful as host materials for ...

2011-07-01

354

Photochemical reactivity of the homologous proteins. cap alpha. -lactalbumin and lysozyme  

Energy Technology Data Exchange (ETDEWEB)

The fluorescent behaviour and the photodynamic effect was studied in native and structurally modified lysozyme and ..cap alpha..-lactalbumin. The Tyr residues in lysozyme and ..cap alpha..-lactalbumin show different sensitivities to the photodynamic effect. The effect is zero in the case of Tyr from native lysozyme. In contrast, the Tyr residues in ..cap alpha..-lactalbumin are susceptible to photooxidation, which indicates a greater degree of exposure to the solvent. The three His residues of ..cap alpha..-lactalbumin have different degrees of exposure and show two different kinetics of photooxidation whereas the His residue of lysozyme is photooxidized with a single kinetic. Two photooxidation kinetics were obtained for the Trp residues of both native proteins, an indication that in both cases there are Trp residues that are differently exposed to the solvent. The wavelengths of maximum fluorescent emission of the Trp residues were different ...

1985-04-01

355

Mercury-free fluorescent lighting  

Energy Technology Data Exchange (ETDEWEB)

A brief comparative review of possible mercury free fluorescent lighting technologies is presented, including rare-gas positive column discharges, molecular discharges, and dielectric barrier discharges. Detailed experimental results on xenon positive column discharges will then be considered. In order to judge whether xenon-based discharges are a viable UV source it is necessary to measure the radiant emittance (power per unit area) for the vacuum ultraviolet (VUV) resonance xenon emission at 147 nm. Two techniques to determine the VUV radiant emittance have been developed and applied to xenon discharges. One method combines the measured resonance level density using absorption spectroscopy and a calculation of the trapped decay rate for the resonance radiation to arrive at the radiant emittance at 147 nm. A second method utilizes a direct measurement of the radiance (power per unit area per unit solid angle) at 147 nm using a calibrated VUV photodiode, and a ...

1996-05-01

356

Measuring head for radionuclide X-ray fluorescence analyzer  

International Nuclear Information System (INIS)

The design of a gaging head for a portable radionuclide X-ray fluorescence analyzer is described. The gaging head is designed as a construction unit system which enables the application of lateral reflexion geometry as well as of coaxial geometry. It is designed so that adjustment from one geometry to the other is labour and time saving. The selection of characteristic radiation is performed by a couple of Ross' differential filters. These filters are prepared by a novel technique developed by our laboratory. The filter exchange is effected by the longitudinal move of the couple of filters encapsulated in a holder. The shift of the filters is controlled by means of a triggering mechanism situated in the body of the gaging head handle. This design makes is possible to handle the gaging head during measurements with one hand. A simple interchange of the absorption filter for the transmissive filter allows the operator to avoid any unwanted shift of the head during ...

1976-05-21

357

Measurement of L X-ray fluorescence cross-sections for elements with 45 Z50 using synchrotron radiation at 8keV  

British Library Electronic Table of Contents (United Kingdom)

The L shell fluorescence cross-sections of the elements in range 45Z50 have been determined at 8keV using Synchrotron radiation. The individual L X-ray photons, Ll, La, LbI, LbII, LgI and LgII produced in the target were measured with high resolution Si(Li) detector. The experimental set-up provided a low background by using linearly polarized monoenergetic photon beam, improving the signal-to-noise ratio. The experimental cross-sections obtained in this work were compared with available experimental data from Scofield [1,2] Krause [3,4] and Scofield and Puri et al. [5,6]. These experimental values closely agree with the theoretical values calculated using Scofield and Krause data, except for the case of Lg, where values measured of this work are slighter higher.

2011-01-01

358

Luminescent determination of zirconium and hafnium with myricetin  

International Nuclear Information System (INIS)

Reaction of formation of 3, 5, 7, 3', 4', 5' - hexaoxiflavone - myricetin complexes with zirconium and hafnium ions has been the basis for development of luminescent method of determining these elements. Optimum conditions for complexing have been determined. For Hf they are : 8-9 HCl concentration, maximum fluorescence wave length (lambda fl.)of 520 nm, wave length of exciting light (lambda el) of 436 nm, for Zr lambda fl = 536nm, lambda el = 436 nm. Stable fluorescence establishes after 25 min. for Zr and after 15 min for Hf in the presence of 40% ethanol. Usage of various camouflage agents has permitted to attain high selectivity of the method. Possibility for determination of Zr with myricetin in the presence of a 10-time excess of Hf, Cr, Cu, 50-time excess of Mo and Ti is shown. Sensitivity of Zr determination is 2.0x10 #mu#g"-"2/ml, for Hf it is 9.0x10 #mu#g"-"3 and mineral waters.

359

Human cDNA mapping using fluorescence in situ hybridization. Progress report, April 1, 1992--December 31, 1992  

Energy Technology Data Exchange (ETDEWEB)

Genetic mapping is approached using the techniques of high resolution fluorescence in situ hybridization (FISH). This technology and the results of its application are designed to rapidly generate whole genome as tool box of expressed sequence to speed the identification of human disease genes. The results of this study are intended to dovetail with and to link the results of existing technologies for creating backbone YAC and genetic maps. In the first eight months, this approach generated 60--80% of the expressed sequence map, the remainder expected to be derived through more long-term, labor-intensive, regional chromosomal gene searches or sequencing. The laboratory has made significant progress in the set-up phase, in mapping fetal and adult brain and other cDNAs, in testing a model system for directly linking genetic and physical maps using FISH with small fragments, in setting up a database, and in establishing the validity and throughput of the system.

1993-03-04

360

High-efficiency RF suppression circuit for fluorescent lamp inverters using charge pump and partial smoothinf capacitors; Chagi ponpu shiki korikiritsu bubun heikatsu hoshiki wo mochiita keikoto inbatayo kochoha teigen kairo  

Energy Technology Data Exchange (ETDEWEB)

A highly efficiency partial smoothing method is proposed to be used for inverters for 40W class household fluorescent inverters. In this system, the input current from the commercial AC power source is accumulated in a capacitor with comparatively small capacity as the electric charge, and then the lamp circuit is driven by the inverter utilizing the charging voltage of the capacitor and the charging voltage of the separately prepared partial smoothing capacitor. By this method, the RF harmonic components in the supply current can be decreased to improve the power factor with no complicated feedback controlling device. In addition, comparatively small capacity coils and capacitors can be used. The structure of the circuit and the operation of this proposed method are described, and the operational characteristic of the prototype circuit and the result of analysis are shown. Furthermore, problems and improving method of the actual circuit are investigated by an ...

1997-06-20

361

Fabrication of single nanofluidic channels in poly(methylmethacrylate) films via focused-ion beam milling for use as molecular gates  

International Nuclear Information System (INIS)

Focused-ion beam (FIB) milling provides rapid fabrication of individual cylindrical submicrometer channels with reproducible dimensions (#+-#5% diameters) through 8-#mu#m thick poly(methylmethacrylate) (PMMA) films. PMMA films are spincast on sacrificial Si carriers and sputter-coated with Au before the 30-kV gallium FIB milling process. By adding a trace amount of poly(ethyleneoxide) and poly(dimethylsiloxane) to the PMMA solution before casting, the films can be released for subsequent mounting in microfluidic devices to create hybrid microfluidic-nanofluidic multilevel architectures. In situ FIB sectioning demonstrates the smooth cylindrical surface within the pore. Placing a milled film in contact with an aqueous fluorescein solution fills the channel by capillary action, as verified by confocal fluorescence microscopy. Confocal fluorescence of dyed films reveals that the pores span the thickness of the PMMA film. Small arrays of channels ...

2004-08-16

362

Development of lidar techniques for environmental studies  

Energy Technology Data Exchange (ETDEWEB)

The lidar group in Lund has performed many DIAL measurements with a mobile lidar system that was first described in 1987. The lidar system is based on a Nd:YAG-pumped dye laser. During the last few years the lidar group has focused on fluorescence imaging and mercury measurements in the troposphere. In 1994 we performed two campaigns: one fluorescence imaging measurement campaign outside Avignon, France and one unique lidar campaign at a mercury mine in Almaden, Spain. Both campaigns are described in this thesis. This thesis also describes how the mobile lidar system was updated with the graphical programming language LabVIEW to obtain a user friendly lidar system. The software controls the lidar system and analyses measured data. The measurement results are shown as maps of species concentration. All electronics and the major parts of the program are described. A new graphical technique to estimate wind speed from plumes is also discussed. ...

1996-09-01

363

Determination of small amounts of elements by radionuclide X-ray fluorescence analysis  

International Nuclear Information System (INIS)

The determination of small amounts of elements by radionuclide X-ray fluorescence analysis is described. Samples containing 5x10"-"4 to 5x10"-"6 g of elements were fixed on a suitable carrier. For a coaxial configuration a low-energy source of the #gamma#/X type was used, namely an annular "2"4"1Am/Ag source with an activity of 7.4x10"8 s"-"1 (20 mCi), and for a configuration with side reflection source of the #beta#/X type was used, namely "1"4"7Pm/Sm with the activity of Pm(OH)_3 approximately 3.7x1O"1"0 s"-"1 (1 Ci). Cs, Ba, La, Pr, Nd, and Ag were determined by means of the Ksub(#alpha#) line and Hg, W, Er, and Pr by means of the Lsub(#alpha#) line. For all elements studied a detection limit of the order of 10"-"7 g was achieved. (author).

1975-01-01

364

Clinical and tomographic aspects of macular microholes; Aspectos clinicos e tomograficos dos microburacos maculares  

Energy Technology Data Exchange (ETDEWEB)

Purpose: To describe the clinical aspects and evaluate optical coherence tomography of macular microholes. Methods: Seven patients were assessed (8 eyes) with microholes of the macula. All patients underwent complete eye examination, fundus photography, fluorescent angiography and OCT-3 imaging. Results: Ages ranged from 26 to 69 years. Six patients were female (85.7%) and five of them had microhole in the right eye. The presenting symptom was decrease in visual acuity (71.3%) and central scotoma in (14.3%). Five eyes (71.4%) had no defects shown by fluorescent angiography. A defect in the outer retina was demonstrated in all eyes on optical coherence tomography. The lesions were nonprogressive. Conclusion: Macular microholes are small lamellar defects in the outer retina. The condition is nonprogressive, generally unilateral and compatible with good visual acuity. Fundus biomicroscopy associated with an optical coherence tomography are the ...

2009-07-01

365

Behaviour of atomic oxygen in a pulsed dielectric barrier discharge measured by laser-induced fluorescence  

International Nuclear Information System (INIS)

Atomic oxygen is measured in a pulsed dielectric barrier discharge (DBD) using two-photon absorption laser-induced fluorescence (TALIF). The ground-level atomic oxygen is excited to the 3p "3P state by two-photon absorption at 226 nm. Negative (-40 kV) or positive (+30 kV) pulsed DBD occurs in an O_2-N_2 mixture at atmospheric pressure. The pulse width of the DBD current is approximately 50 ns. The TALIF experiment shows that the decay rate of atomic oxygen increases linearly with O_2 concentration. This result proves that atomic oxygen decays mainly by the third-body reaction, O + O_2 + M #-># O_3 + M. The rate coefficient of the third-body reaction is estimated to be 2.2 x 10"-"3"4 cm"6 s"-"1 in the negative DBD and 0.89 x 10"-"3"4 cm"6 s"-"1 in the positive DBD. It is shown that the decay rate of atomic oxygen increases linearly with humidity. This can explain the well-known fact that ozone production in DBD is suppressed by increasing humidity.

2005-08-21

366

Spectroscopic studies of the Sm/sub 3/Ga/sub 5/O/sub 12/ monocrystals  

Energy Technology Data Exchange (ETDEWEB)

The fluorescence, absorption, infrared and Raman spectra of Sm/sub 3/Ga/sub 5/O/sub 12/ have been investigated. The energy-level schemes in the energy range 3000-16000 cm/sup -1/ have been determined. The number and symmetries of the Sm/sub 3/Ga/sub 5/O/sub 12/ crystal normal mode have been obtained by the molecular site group analysis and their comparison with the experiment has been made.

1984-11-01

367

Radionuclide X-ray fluorescence analysis with environmental application  

International Nuclear Information System (INIS)

The purpose of this work is to present a comprehensive, instructive analysis of the basis of radionuclide XRFA, to describe methods of sample preparation for environmental analysis and to make the reader more familiar with the procedures, methods and instrumentation of radionuclide XRFA used in this field. This book discusses the use of radionuclide XRFA for solving analytical problems of the environment and information is presented concerning the current state of research and use of radionuclide XRFA in this significant area. The present volume will serve as a basic source of data and also as a laboratory handbook. refs.; figs.; tabs.

1990-01-01

368

Quantum electrodynamic and semiclassical interference effects in spontaneous radiation  

International Nuclear Information System (INIS)

The theory of spontaneous decay is studied using both quantum electrodynamics (QED) and semiclassical theories of radiation. There are qualitative differences between the theories in the prediction of interference phenomena. In QED, systems which were excited with pulsed laser light do not exhibit quantum interference effects associated with lower state splittings. On the other hand, semiclassical treatments of spontaneous decay do indicate the existence of interference effects not present in QED. In addition to this, differences are found between the predictions of fluorescence intensity in the presence of lower-state level crossings under continuous excitation. (U.S.).

1975-01-01

369

Preparation and Properties of New Ester-Linked Cleavable Gemini Surfactants  

British Library Electronic Table of Contents (United Kingdom)

We have prepared a series of novel gemini surfactants having ester bonds in their structures. These surfactants possess two identical hydrophilic polyethylene glycol moieties, two hydrophobic alkyl group moieties, and an anionic spacer. The structures of these compounds were confirmed through infrared and nuclear magnetic resonance spectroscopic and elemental analyses. The novel gemini surfactants exhibit excellent surface activity in terms of their surface tension, low-foaming, wetting power, and fluorescence properties. The presence of the ester linkages made these structures cleavable surfactants.

2011-01-01

370

Nondestructive testing of metal coating thickness and control of chemical composition using radionuclide X-ray fluorescence analysis  

International Nuclear Information System (INIS)

The principle is described of a method using low-activity emitters as the primary radiation source for analysis. The selection of the radiation source and the detection methods including the assessment of the applicability of various radiation detectors are discussed. The benefits and the constraints of the method are considered. Practical examples are presented showing the application possibilities of the method for testing the thickness of bearing layers, piston ring coats, lead layers, etc. The possibility is shown of applying the rapid test for the composition of tungsten and chromium alloyed metal materials in testing complex systems. (J.K.).

1974-12-03

371

New coumarin-based sensor molecule for magnesium and calcium ions  

British Library Electronic Table of Contents (United Kingdom)

A new coumarin-based sensor molecule (L1) has been synthesized and this was found to bind calcium and magnesium ions more effectively as compared to other alkali/alkaline earth/lanthanide and certain transition metal ions. A significant enhancement in fluorescence intensity was observed on binding to Ca2+ and Mg2+ ions; while a minor quenching was observed for weakly bound Hg2+, Ni2+, Fe3+, and Co2+ ions. PET process, coupled with the ICT process, is proposed to explain the observed spectral response.

2009-01-01

372

Neutron radiography with the cyclotron, 5  

International Nuclear Information System (INIS)

Reliable facility of cyclotron-based real time neutron radiography system has been developed and applied to some industrial components. The equipment for neutron fluoroscopy is based on a sub-compact cyclotron and a LiF/ZnS (Ag) fluorescent screen viewed by a silicon intensifier target TV camera. The real time image is monitored on a CRT, recorded with a standard video recorder and processed by a digital image processor. The effectiveness of our real time neutron radiograph has been demonstrated to be applicable to not only the dynamic observation but also the magnifying and stereoscopic observation of fluoroscopic images. (author).

1987-01-01

373

Multielement XRF-analysis of blood from patients with dilated cardiomyopathy  

International Nuclear Information System (INIS)

Radionuclide x-ray fluorescence analysis was used for the determination of Fe, Zn, Br and Rb levels in whole blood from dilated cardiomyopathy patients and from a control group. The XRF-system consisted of a radionuclide source "1"0"9Cd, a semiconductor Si/Li detector connected to a multichannel analyzer. Fe content in blood of patients was significantly lower than that of the control. Zn content showed no deviation from normal range. Values for Br and Rb in patients highly exceed the range reported for them. (author) 4 tabs.; 9 refs.

1991-03-01

374

Labeled cells as research, diagnostic and therapeutic tools  

Energy Technology Data Exchange (ETDEWEB)

Scientists at JPL have developed chemical and biological techniques using microspheres filled with drugs, electron-opaque metals, or radioactive, fluorescent, magnetic or electrically charged materials to label specific groups of cells. Synthetic polymeric microspheres are coupled with specific antibodies to form reagents called immunomicrospheres, which can seek out and attach themselves to any specific group of cells. These cell-labeling techniques, therefore, open new avenues not only to the basic study of cells but also to the diagnosis and treatment of many diseases, including cancer.

1983-09-01

375

Functionalized luminescent oxide nanoparticles for sodium channel imaging at the single molecule level  

Science.gov (United States)

Lanthanide-ion doped oxide nanoparticles were functionalized for use as fluorescent biological labels. These nanoparticles are synthesized directly in water which facilitates their functionalization, and are very photostable without emission intermittency. Nanoparticles functionalized with guanidinium groups act as artificial toxins and specifically target sodium channels. They are individually detectable in cardiac myocytes, revealing a heterogeneous distribution of sodium channels. Functionalized oxide nanoparticles appear as a novel tool particularly well adapted to long-term single-molecule tracking.

2005-04-01

376

Flow cytogenetics methodology and applications  

Energy Technology Data Exchange (ETDEWEB)

Flow cytogenetics is a rapidly developing technology which complements rather than supplants the traditional methods of cytogenetic analysis. As an adjunctive approach to chromosome classification, flow systems measurements of isolated chromosomes give new information relative to the enrichment of A-T or G-C base sequences on specific chromosomes. As a result, chromosomal fluorescence polymorphisms both within and among individuals that are not always associated with banding polymorphisms can be detected. Finally, flow sorting provides bulk quantities of highly purified chromosomes for use in biochemical studies. Methodology is detailed. (PSB)

1982-10-17

377

Estimation of X-rays dose in the crystals of final thickness  

International Nuclear Information System (INIS)

A calculation method of the X-ray radiation dose (energy of gamma- radiation remains in the range of energies where the mechanism of photoelectric absorption is the prevailing one) absorbed in the absorbers of final thickness is suggested. Calculations of resorption of secondary radiation (characteristic fluorescences) in the substance and kinetic energy of photoelectrons caused by this resorption (it would be enough to consider one or two hard series) are presented. Calculation of the spectrum of photoelectron energy yield in TeInSe_2 monocrystal for 0.1-0.5 A range of X-ray radiation is conducted by the developed methods.

378

Elemental concentration analysis in some plant samples by EDXRF at Trabzon  

International Nuclear Information System (INIS)

The elemental analysis of some plant samples have been carried out in Trabzon region (Turkey) using energy-dispersive X-ray fluorescence (EDXRF) spectrometry. We have analyzed plant samples for nine stations using 1.85 GBq 55Fe radioactive sources. We have found that potassium and calcium within 0.3-1.4% and 0.3-2.8% were present in concentration in plants for every station, respectively. The concentration of Cl and Ti generally changed according to the plant species and the sampling station.

2006-12-01

379

Dimensionally dependent luminescence of boron difluoride ?-diketonates  

International Nuclear Information System (INIS)

The results of the study of dimensionally dependent fluorescence of boron difluoride ?-diketonates of general formula (R1COCHCOR2)BF2 are presented. The fact that for most of the compounds studied a noticeable hypsochrome shift of the luminescence band maximum is characteristic during transition from bulk crystals to microcrystals was detected. However, for boron difluoride dibenzoylmethanate having a unique supramolecular structure, a bathochromic shift of luminescence due to the crustal size reduction is observed. The dimensionally dependent luminescence properties of the complexes have been analyzed within the exciton mechanism

2008-06-01

380

Cutaneous leishmaniasis associated with jungle training.  

Science.gov (United States)

In November 1977, 627 soldiers belonging primarily to the First Battalion, 82nd Airborne Division, stationed at Fort Bragg, were sent to the Canal Zone, Panama, for jungle warfare training. A medical surveillance program incorporating pre- and post-evaluations over a 6-month period with dermatologic examinations, questionnaires, and serologic tests was established. Ten cases of cutaneous leishmaniasis (1.6/100 men) were diagnosed by positive Leishmania culture. The demonstrated lack of sensitivity and specificity of the indirect fluorescent antibody test and the direct agglutination test render these serological methods useless as diagnostic screening methods in the early stages of this disease. PMID:7406101

1980-07-01

381

Coincidence measurements of M-shell excitation in slow Xe-Xe collisions  

Energy Technology Data Exchange (ETDEWEB)

Ion-photon and ion-Auger-electron coincidence measurements have been performed to study the impact parameter dependence of Xe M-shell excitation in 1.05 MeV Xe/sup 3 +/-Xe collisions. The experimental results are found to be consistent with the prediction of the molecular orbital model of atomic collisions. The average fluorescence yield for the Xe M shell is found to be strongly dependent on the impact parameter. This is ascribed to the production of highly charged Xe ions in close collisions.

1982-07-14

382

Chromosomal localization and cDNA sequence of human BTEB, a GC box binding protein  

Energy Technology Data Exchange (ETDEWEB)

Human BTEB cDNA clones have been isolated, sequenced, and the corresponding gene has been assigned to human chromosome 9, region q13, by fluorescent in situ hybridization and DNA blot analysis using DNAs from hybrid cell clones containing a single human chromosome. The cDNA clone encodes a polypeptide of 244 amino acids whose sequence shows a high sequence similarity with the rat BTEB (98% amino acid identity).

1993-09-01

383

Application of radionuclide X-ray fluorescence analysis in determining lanthanum content in tungsten and in iron by internal standard technique  

Energy Technology Data Exchange (ETDEWEB)

The use of the method is described on powder samples before and after sintering with a La content of up to 1%. For excitation of the K series of La a /sup 241/Am source with an activity of 1.11 GBq was used. The obtained results showed that the method is sufficiently accurate (error 7%) at a short period of measurement (100 s). It gives satisfactory results even in the comparison of the experimental relative count rate and the theoretically calculated value despite the fact that the analytical signal comes from the sample surface.

1983-05-01

384

Application of radionuclide X-ray fluorescence analysis in determining lanthanum content in tungsten and in iron by internal standard technique  

International Nuclear Information System (INIS)

The use of the method is described on powder samples before and after sintering with an La content of up to 1%. For excitation of the K series of La a _2_4_1Am source with an activity of 1.11 GBq was used. The obtained results showed that the method is sufficiently accurate (error 7%) at a short period of measurement (100 s). It gives satisfactory results even in the comparison of the experimental relative count rate and the theoretically calculated value despite the fact that the analytical signal comes from the sample surface. (Ha).

1983-01-01

385

Analysis of o-tyrosine as a method for the identification of irradiated chicken and the comparison with other methods (analysis of volatiles and ESR-spectroscopy)  

Energy Technology Data Exchange (ETDEWEB)

With the mentioned method to analyse O-tyrosine with HPLC/fluorescence-detection, the irradiation of chicken meat can be determined in a simple and fast way. The formation of o-tyrosine is proportional to the applied dose but because it is also depending on the applied dose rate and the temperature during the irradiation, it is not possible to control the irradiation dose. Since unirradiated chicken can contain little amounts of o-tyrosine and to confirm some results, a second method is needed. Together with one of the other mentioned methods (analysis of the volatiles or esr-spectroscopy) it is possible to recognize irradiated chicken with a high security. (author).

1990-01-01

386

An Apparent Hard X-ray Decline of CH Cygni  

CERN Document Server

CH Cygni is a symbiotic star consisting of an M giant and an accreting white dwarf, which is known to be a highly variable X-ray source with a complex, two-component, spectra. Here we report on two Suzaku observations of CH Cyg, taken in 2006 January and May, during which the system was seen to be in a soft X-ray bright, hard X-ray faint state. Based on the extraordinary strength of the 6.4 keV fluorescent Fe K-alpha line, we show that the hard X-rays observed with Suzaku are dominated by scattering.

2006-01-01

387

A Virtual Young's Double Slit Experiment for Hard X-ray Photons  

CERN Document Server

We have implemented a virtual Young's double slit experiment for hard X-ray photons with micro-fabricated bi-prisms. We observe fringe patterns with a scintillator, and quantify interferograms by detecting X-ray fluorescence from a scanned 30nm Cr metal film. The observed intensities are best modeled with a near-field, Fresnel analysis. The maximum fringe number in the overlap region is proportional to the ratio of real to imaginary parts refractive index of the prism material. The horizontal and vertical transverse coherence lengths at beamline APS 8-ID are measured.

2009-01-01

388

6. Sample preparation for determining pollutants in components of the environment  

International Nuclear Information System (INIS)

Examples are given of reference materials for radionuclide X-ray fluorescence analysis (RXFA) of the environment processed by the National Bureau of Standards and the IAEA. Methods are described used for preparing standard materials for RXFA. For determining air pollutants the sample is prepared by dry or wet mineralization. Water samples have to be preserved prior to analysis. Insoluble components are separated by filtration or centrifugation. Biological materials must be dehydrated and homogenized. Samples of soil, sludges, sediments and solid wastes will sometimes have to be converted into a solution in some cases a leachate will have to be obtained. (ES).

1983-12-01

389

Supramolecular selectivity of [60]-fullerene among equivalently photoactive porphyrins  

International Nuclear Information System (INIS)

The photophysical investigation of different para-substituted tetraphenylporphyrins (TP), viz., meso-tetra(4'-hydroxyphenyl)-21H-23H-porphyrin(1),meso-tetrakis (4'-hex-5-enyloxyphenyl)-21H-23H-porphyrin(2), meso-tetrakis(4'-oct-7-enyloxyphenyl)-21H-23H-porphyrin(3) and meso-tetrakis(4'-undecyloxyphenyl)-21H-23H-porphyrin (4) revealed that except for quantum yield (#phi#) the para-substitution has little effect on any other photophysical properties like lifetime, excitation, emission wavelength, etc. The host-guest type interactions of these tetraarylporphyrins (TP 1-4), with [60]-fullerene (F) have been studied with "1H NMR and fluorescence spectrometric techniques in carbon tetrachloride medium. Fluorescence studies revealed that the Q band of the TPs was sufficiently quenched upon addition of F. All the fullerene/porphyrin systems were found to produce stable complexes with 1:1 stoichiometry. Binding constants (K) of all the ...

2010-10-01

390

Silencing of SARS-CoV spike gene by small interfering RNA in HEK 293T cells  

International Nuclear Information System (INIS)

Two candidate small interfering RNAs (siRNAs) corresponding to severe acute respiratory syndrome-associated coronavirus (SARS-CoV) spike gene were designed and in vitro transcribed to explore the possibility of silencing SARS-CoV S gene. The plasmid pEGFP-optS, which contains the codon-optimized SARS-CoV S gene and expresses spike-EGFP fusion protein (S-EGFP) as silencing target and expressing reporter, was transfected with siRNAs into HEK 293T cells. At various time points of posttransfection, the levels of S-EGFP expression and amounts of spike mRNA transcript were detected by fluorescence microscopy, flow cytometry, Western blot, and real-time quantitative PCR, respectively. The results showed that the cells transfected with pEGFP-optS expressed S-EGFP fusion protein at a higher level compared with those transfected with pEGFP-S, which contains wildtype SARS-CoV spike gene sequence. The green fluorescence, mean ...

2004-11-26

391

Rapid laser fluorometric method for the determination of uranium in soil, ultrabasic rock, plant ash, coal fly ash and red mud samples  

International Nuclear Information System (INIS)

A simple and rapid laser fluorometric determination of trace and ultra trace level of uranium in a wide variety of low uranium content materials like soil, basic and ultra basic rocks, plant ash, coal fly ash and red mud samples is described. Interference studies of some common major, minor and trace elements likely to be present in different geological materials on uranium fluorescence are studied using different fluorescence enhancing reagents like sodium pyrophosphate, orthophosphoric acid, penta sodium tri-polyphosphate and sodium hexametaphosphate. The accurate determination of very low uranium content samples which are rich in iron, manganese and calcium, is possible only after the selective separation of uranium. Conditions suitable for the quantitative single step extraction of 25 ng to 20 #mu#g uranium with tri-n-octylphosphine oxide and single step quantitative stripping with dilute neutral sodium pyrophosphate, which also acts as ...

1999-10-01

392

Mitochondrial sequestration of BCECF after ester loading in the giant alga Chara australis.  

Science.gov (United States)

Ratiometric fluorescent dyes are often used to monitor free ion concentrations in vivo, especially in cells that are recalcitrant to transformation with genetically encoded fluorescent markers. Although intracellular dye distributions are often found to be cytosolic, dye localisation has often not been examined in detail. We began exploring the use of BCECF (2',7'-bis(2-carboxyethyl)-5(6)-carboxyfluorescein) to monitor pH in the giant alga Chara australis and discovered that younger leaf cells could be loaded using the acetoxymethyl ester of BCECF. However, we were puzzled to find in microphotometric measurements that the fluorescence ratio appeared insensitive to manipulations affecting cytosolic pH. Confocal imaging of C. australis cells loaded with BCECF showed an accumulation of the dye in two locations: (1) on the outside of the chloroplasts in irregularly shaped stationary bodies; (2) within 1-1.5 mum structures that ...

2007-12-19

393

M-shell x-ray production by 0.6--4.0-MeV protons in ten elements from hafnium to thorium  

International Nuclear Information System (INIS)

M-shell x-ray production cross sections for selected heavy elements, namely, _7_2Hf, _7_3Ta, _7_4W, _7_5Re, _7_6Os, _7_7Ir, _7_8Pt, _7_9Au, _8_3Bi, and _9_0Th, were measured for protons of energy 0.6--4.0 MeV. The experimental results are compared with the predictions of the first Born and semiclassical approximations for M-shell ionization; these data are also compared with the theory that accounts for the projectile's energy loss and Coulomb deflection as well as for the target's M-shell electron perturbed stationary state and relativistic nature (ECPSSR). Generally, fair agreement between the data and the ECPSSR theory is found. Some systematical discrepancies observed for the lightest elements (Hf, Ta, and W) are explained as possible ambiguities in the M-shell Coster-Kronig factors and fluorescence yields, which were used to convert theoretical M-subshell ionization cross sections to the total M-x-ray production cross sections. The experimental total M-shell ...

394

Luminescence studies of Nd3+- and Yb3+-doped ?-Y(IO3)3 and ?-Y(IO3)3, transparent host matrix in the mid- and beginning of the far-infrared  

International Nuclear Information System (INIS)

?-Y(IO3)3 and ?-Y(IO3)3 are transparent until 12.8 and 13.4 ?m, respectively; thus they are interesting as a potential laser matrix in the mid- and beginning of the far-infrared. So, in order to investigate the properties of lanthanides- doped anhydrous yttrium iodate, polycrystalline samples of ?-Y1-xNdx(IO3)3 (0.01?x?0.05), ?-Y1-xNdx(IO3)3 (0.001?x?0.1), ?-Y1-xYbx(IO3)3 (0.01?x?0.33) and ?-Y1-xYbx(IO3)3 (0.01?x?0.25) were synthesized. For Nd3+ ions, fluorescent emissions from the 4F3/2 multiplet were observed at 300 K under pulsed laser excitations at 750 nm and for Yb3+, fluorescent emissions from the 2F5/2 multiplet were observed at 300 K under pulsed laser excitations at 980 nm. The decays of all these emissions were measured. They are exponential and the fluorescence lifetimes are in the range 0.093-0.193 ms for Nd3+ and 0.370-0.541 ms for Yb3+, depending on the nature of the host and the concentration of doping.

2009-03-01

395

Determination of Cinchona alkaloids and Vitamin B_6 by high-performance liquid chromatography with fluorescence detection  

International Nuclear Information System (INIS)

A simple and specific method has been developed for the simultaneous determination of the four major Cinchona alkaloids and their dihydroderivatives and pyridoxine hydrochloride (Vitamin B_6) by high-performance liquid chromatography (HPLC) with fluorescence detection (#lambda#_e_m=420 nm with #lambda#_e_x=330 nm). The chromatographic separation was performed on a Phenomenex Prodigy ODS column (5 #mu#m, 250 mmx3.2 mm i.d.), recommended for basic compounds, under isocratic reversed-phase conditions. The method allowed a good peak shape and an effective resolution of the tested compounds. The extraction of alkaloids from the Cinchona succirubra bark was carried out in mild and fast conditions (ambient temperature, 20 min) by ultrasonication. The procedure showed to be advantageous respect to a reference method, which involved Soxhlet extraction. The results were compared statistically by means of the Student's t-test and the variance ratio F-test; no significant ...

2004-06-04

396

Assignment of the human aggrecan gene (AGC1) to 15q26 using fluorescence in situ hybridization analysis  

Energy Technology Data Exchange (ETDEWEB)

The large aggregating proteoglycan aggrecan is a major structural component of the extracellular matrix of articular cartilage. Recent cDNA cloning of the human aggrecan gene (AGC1) reveals a core protein of at least 2316 amino acids characterized by several distinct structural domains. Two globular domains, termed G1 and G2, are present at the amino terminus of the molecule and a third, termed G3, is present at the carboxy terminus. The G1 domain is homologous in structure to the cartilage link protein and accounts for the aggregating potential of aggrecan through its ability to interact with hyaluronic acid. The aggrecan gene is known to consist of 15 exons, with each exon encoding a distinct functional region of the mature protein. However, while the link protein gene is known to reside on chromosome 5 in the human, the location of the aggrecan gene is currently undetermined in any species. The probe (pAGG2) for the aggrecan gene was mapped on chromosome band 15q26, most likely in ...

1993-05-01

397

mtDNA mutation C1494T, haplogroup A, and hearing loss in Chinese  

British Library Electronic Table of Contents (United Kingdom)

Mutation C1494T in mitochondrial 12S rRNA gene was recently reported in two large Chinese families with aminoglycoside-induced and nonsyndromic hearing loss (AINHL) and was claimed to be pathogenic. This mutation, however, was first reported in a sample from central China in our previous study that was aimed to reconstruct East Asian mtDNA phylogeny. All these three mtDNAs formed a subclade defined by mutation C1494T in mtDNA haplogroup A. It thus seems that mutation C1494T is a haplogroup A-associated mutation and this matrilineal background may contribute a high risk for the penetrance of mutation C1494T in Chinese with AINHL. To test this hypothesis, we first genotyped mutation C1494T in 553 unrelated individuals from three regional Chinese populations and performed an extensive search ...

2006-01-01

398

[Pulmonary vascular manifestations in hereditary hemorrhagic telangiectasia].  

Science.gov (United States)

Hereditary hemorrhagic telangiectasia (Osler-Rendu-Weber disease) is a genetic disorder with autosomal dominance, variable penetrance, and an estimated prevalence of 1/10,000 inhabitants in France. Diagnosis is based on clinical criteria including epistaxis, telangiectasia, visceral manifestations, and familial occurrence. Pulmonary arteriovenous malformations, present in 15-33% of patients, are its primary visceral complications. The disease may be revealed by infectious and ischemic neurological manifestations due to paradoxical embolism. The high frequency of neurologic complications even in asymptomatic patients justifies systematic screening for pulmonary arteriovenous malformations. Treatment of these malformations is based on percutaneous transcatheter coil embolization of the feeding artery. Pulmonary arterial hypertension is rare in this disease. It may be due to systemic arteriovenous shunting in the liver, which increases cardiac output, or be similar to ...

2005-11-01

399

Water-seal vacuum pumps as compact units for deaeration of steam turbine condensers in conventional and nuclear plants  

International Nuclear Information System (INIS)

On all steam turbines operating with condensation the air leakage penetrating from the part of the plant which is under vacuum must be eliminated, in order to maintain the vacuum created by physical conditions. In order to attain effective air bleed-off, the water-steam-air mixture is conveyed via the super-cooling bundles in the condenser. In this way the steam partial pressure decreases and the air partial pressure increases at a constant condenser pressure. In this procedure the mixture is supercooled by about 4"0C compared with the saturate steam temperature appertaining to the condenser pressure. The values of volume of air leakage are the result of a year's experience on existing plant. (orig.).

400

Treatment of hepatocellular carcinoma (HCC) with radiolabeled Lipiodol: a preliminary report  

Energy Technology Data Exchange (ETDEWEB)

Fatty acid esters such as Lipiodol or Ethiodol are known to selectively localize in vascular hepatocellular carcinomas (HCC), following intraarterial hepatic administration. Lipiodol was labeled with radioactive /sup 131/I and administered in 47 patients with HCC for both imaging and therapy. The short term preliminary results suggest radiolabeled Lipiodol is effective in eliminating ascites, shrinking the tumor by a high internal radiation dose, and in improving symptomatology of these tumors. In the future, /sup 90/Y, which is a stronger pure beta-emitter (maximum beta energy of 2.27 MeV, a half life of 64 h, and a maximum penetration or beta range of 11mm), than /sup 131/I will be used for more effective treatment of HCC.

1987-12-01

401

Thrust faults and associated structures in the Deep River Basin: Evidence for post-extensional compression  

Energy Technology Data Exchange (ETDEWEB)

Thrust faulting, folding, and penetrative compressional fabrics (e.g. spaced cleavage, pencils, and coal cleats) have been found in several outcrops within the central Deep River Basin (the southern Durham subbasin to the northern Wadesboro subbasin). The trend of these structures is nearly parallel to the basin, and may locally control the present geometry of the basin boundaries. These features are distributed throughout the stratigraphic section and across the entire width of the basin. In outcrops where relative timing can be determined, the compressional structures post-date all extensional and intrusive features associated with basin formation. In particular, thrusts cut across and displace basin-parallel normal faults and basin-normal cross-faults. All thrusts found to date verge northwest, and displacements of cross-fault boundaries indicate that transport was approximately 325[degree].

1994-03-01

402

Three-dimensional particle simulation of plasma instabilities and collisionless reconnection in a current sheet  

Energy Technology Data Exchange (ETDEWEB)

Generation of anomalous resistivity and dynamical development of collisionless reconnection in the vicinity of a magnetically neutral sheet are investigated by means of a three-dimensional particle simulation. For no external driving source, two different types of plasma instabilities are excited in the current layer. The lower hybrid drift instability (LHDI) is observed to grow in the periphery of current layer in an early period, while a drift kink instability (DKI) is triggered at the neutral sheet in a late period as a result of the nonlinear deformation of the current sheet by the LHDI. A reconnection electric field grows at the neutral sheet in accordance with the excitation of the DKI. When an external driving field exists, the convective electric field penetrates into the current layer through the particle kinetic effect and collisionless reconnection is triggered by the convective electric field earlier than the DKI is excited. It is also found that the ...

1999-06-01

403

The impact of solar flares and magnetic storms on humans  

International Nuclear Information System (INIS)

Three classes of solar emanations, namely, photon radiation from solar flares, solar energetic particles, and inhomogeneities in the solar wind that drive magnetic storms, are examined, and their effects on humans and technological systems are discussed. Solar flares may disrupt radio communications in the HF and VLF ranges. Energetic particles pose a special hazard at low-earth orbit and above, where they can penetrate barriers such as spacesuits and aluminum and destroy cells and solid state electronics. Energetic solar particles also influence terrestrial radio waves propagating through polar regions. Magnetic storms may disturb the operation of navigation instruments, power lines and pipelines, and satellites; they give rise to ionospheric storms which affect radio communication at all latitudes. There is also a growing body of evidence that changes in the geomagnetic field affect biological systems. 3 refs.

404

The compatibility of alloy 800 in HTR atmospheres  

International Nuclear Information System (INIS)

A thermodynamic analysis of the behaviour of Alloy 800 in helium based atmospheres relevant to the High Temperature Gas Cooled Reactor indicates that, depending upon the precise gas composition, oxidation and carburisation, or carburisation alone may be expected. The prime influence appears to be the moisture level. The morphology and structure of the reaction products are discussed. It is shown that the 'reactive' elements chromium, manganese, titanium and silicon are concentrated in the oxide scale which is normally duplex in structure. Aluminium oxide is formed at grain boundaries and in an internal oxidation zone together with titanium and sometimes silicon. In carburising conditions, mixed titanium-chromium carbides are formed. When this occurs, intergranular penetration is maximised. Weight gain data are assessed and briefly described and a tentative model for the mechanism of corrosion of Alloy 800 in HTR helium is proposed. Areas for further work are ...

405

Submitochondrial distribution of cAMP in its incubation with rat liver mitochondria  

Energy Technology Data Exchange (ETDEWEB)

When labeled cAMP is incubated with isolated mitochondria from rat liver, it penetrates not only through the outer membrane of the mitochondria but also into the mitoplasts, where it is accumulated chiefly in the matrix. Damage to the mitochondrial membrane by freezing-thawing promotes not an influx but an efflux of cAMP out of the mitoplasts. A substantial part of the labeled nucleotide in all the investigated submitochondrial fractions was identified as intact cAMP by the method of thin-layer chromatography. The transport of cAMP into the mitochondria can explain the activation of their functions by the hormones that activate cytoplasmic adenylate cyclase and by extramitochondrial (cytosol) cAMP, as well as the presence of cAMP-dependent protein kinase and cAMP-phosphodiesterase in the mitochondria.

1986-03-20

406

Sub-barrier fusion reactions for synthesis of "2"9"8114  

International Nuclear Information System (INIS)

Favorable reaction channels are searched for in order to obtain the superheavy element "2"9"8114. The interaction energy is supposed to comply with the adiabatic hypothesis. Concerning the deformation energy, a very complete binary macroscopic-microscopic energy method is used to perform calculations. Deformed two-center shell model provides the energy level schemes for shell effects. Yukawa-plus-exponential model gives the macroscopic (liquid drop) part of the total energy. The mass tensor is obtained by the Werner-Wheeler irrotational flow hypothesis. Finally the minimization of the multidimensional action integral produces the highest penetrability values. Kr-projectile reactions provide the best pairs, although generally the presentabilities are very low. (author)

2005-01-01

407

Spray, combustion, and heat transfer studies in a Ricardo hydra direct-injection diesel engine  

Energy Technology Data Exchange (ETDEWEB)

The spray and combustion development in a single-cylinder, direct-injection diesel engine equipped with optical access was examined using a number of complementary techniques. A laser imaging system, based around a pulsed copper-vapour laser synchronised to an intensified CCD camera, was used to obtain images of the four fuel sprays prior to combustion, and to determine the tip penetration of each spray as a function of crankangle. The surface heat flux to the wall of the piston bowl was measured by placing a fast-response thermocouple at the impingement point of one of the sprays, and a two-colour imaging system was used to obtain digital images of the flame temperature and equivalent soot distribution in the cylinder. (author)

1996-12-31

408

Rondonia Deforestation (WMS)  

Science.gov (United States)

Throughout much of the 1980s, deforestation in Brazil eliminated more than 15,000 square kilometers (9000 square miles) of forest per year. Data gathered by several satellites in the Landsat series of spacecraft shows enormous tracts of forest disappearing in Rondonia, Brazil from 1975 through 2001. The human phenomenon of deforestation starts, especially in the dense tropical forests of Brazil, when systematic cutting of a road opens new territory to potential deforestation by penetrating into new areas. Clearing of vegetation along the sides of those roads then tends to fan out to create a pattern akin to a fish skeleton. As new paths appear in the woods, more areas become vulnerable. Finally, the spaces between the skeletal bones fall to defoliation.

2005-02-17

409

Rethinking development assistance for wind power  

Energy Technology Data Exchange (ETDEWEB)

Electricity generation from wind turbines is now cost competitive for grid and off-grid applications in many developing regions, and close to competitive in others. Wind resources could generate thousands of megawatts of badly-needed power in Asia, North Africa, and Latin America. Barriers to penetrating power generation markets remain, however, including unequal access to investment capital, energy price and other market distortions, and often weak institutions for commercializing new technologies. Recognizing the potential economic and environmental benefits of wind power, bilateral and multilateral assistance organizations have for several years offered financial and technical assistance to promote its diffusion. Based on this experience and assistance for other renewable electric technologies, lessons and recommendations can be drawn regarding how assistance could more effectively overcome persistent market and policy barriers, especially in light of the ...

1995-12-31

410

Renewable Energy in Danish Municipalities - an Evaluation of The Planning Framework for Wind Power  

DEFF Research Database (Denmark)

Wind power is a maturing technology that in a number of countries is likely to contribute a major share to fully renewable energy systems. Denmark has a comparably long history of wind power development and is planning to continue expanding the existing capacity. If a large-scale penetration of wind power is to be achieved, an integrated framework is needed that can respond to the associated challenges. This paper argues for adopting an integrated macro perspective when evaluating and building frameworks to support wind power development. This macro perspective is applied to the case of Denmark, and more specifically to concrete wind power projects in the region of Northern Jutland. The results suggest although certain elements in the legislation have been improved, the feasibility of wind power projects cannot be guaranteed, and there is a tendency to exclude smaller turbines from the development.

2009-01-01

411

Real-time imaging for neutron radiography at KURRI  

International Nuclear Information System (INIS)

For neutron radiography (NR), photographic techniques have been mainly used for many years. To observe a dynamic event and to test many samples, the real-time neutron radiography (i.e. neutron television - NTV) system has been introduced at the E-2 experimental tube of the Kyoto University Research Reactor (KUR). The NTV system has been practically applied to penetrating the side plates containing boron burnable poison to test MTR type reactor fuel, to investigation of moving objects and to neutron computed tomography (NCT). New approaches using some advanced neutron converters, a high sensitive and resolution TV camera and a high performance image processing system are being undertaken for standard indicators, visualization on air-water two-phase flow, NCT and so on. (author).

1987-07-01

412

Progress and problems in the chemistry of technetium-99m tracers  

International Nuclear Information System (INIS)

The recent acceleration of effort to elucidate and explore the coordination chemistry of technetium has been prompted mainly by the need for a new generation of radiotracers in nuclear medicine, preferentially for tomograhic studies. Current approaches and their limitations in designing "9"9"mTc complexes capable of penetrating cell membranes of the target organs, and remaining there sufficiently long, are reviewed. With the predominance of Tc(V) oxo compounds, especially for brain imaging agents, new N4 and N2S2 coordinate complexes have been developed by shifting from bidentate to tetradentate ligands with a variable side chain or other adjustable reactivity. The search for myocardial imaging agents has focused on a variety of mixed ligand complexes of Tc(III) and most promising [Tc(CNR)_6]"+ complexes of Tc(I). 64 refs. (author).

413

Potential impacts assessment of plug-in electric vehicles on the Portuguese energy market  

British Library Electronic Table of Contents (United Kingdom)

Electric vehicles (EVs) and plug-in hybrid electric vehicles (PHEVs), which obtain their fuel from the grid by charging a battery, are set to be introduced into the mass market and expected to contribute to oil consumption reduction. In this research, scenarios for 2020 EVs penetration and charging profiles are studied integrated with different hypotheses for electricity production mix. The impacts in load profiles, spot electricity prices and emissions are obtained for the Portuguese case study. Simulations for year 2020, in a scenario of low hydro production and high prices, resulted in energy costs for EVs recharge of 20cents/kWh, with 2 million EVs charging mainly at evening peak hours. On the other hand, in an off-peak recharge, a high hydro production and low wholesale prices'...

2011-01-01

414

Possible control scenario of radial electric field by loss-cone-particle injection into helical device  

Energy Technology Data Exchange (ETDEWEB)

The possibility of controlling the radial electric field of toroidal plasmas by injecting high energy electrons along the reversible loss cone orbit of the helical magnetic traps is investigated. It is well known that the radial electric field plays an important role in the confinement improvement scenario especially in the low collisional regime under the physics picture of neoclassical theory. For this purpose, it is made clear that the most suitable particles are transit particles, which show a transition from helically trapped orbits to blocked ones. It is also found that a parallel AC electric field launched from outside assists this transition and makes it possible for particles to penetrate deeply into the plasma. In addition we clarify that the viscosity of the plasma coupled with the helical field configuration provide a bifurcation of plasma states and its stable solution results in confinement improvement. (author)

1999-08-01

415

Policy development for solar water heaters: the case of Lebanon  

International Nuclear Information System (INIS)

Full text.The electric energy demand in Lebanon is estimated to grow at an average of 3-5% per year for the coming 10 years. Such an increase in energy demand is problematic for Lebanon since its economy is almost totally dependent on imported fuel which contributes to 97% of the overall energy requirements. Solar water heaters (SWH) are regarded as the most important element in a long term energy conservation and management strategy for this country, but their promotion is a national issue requiring the participation of many stake holders and decision makers. Additionally, the success of solar energy penetration into the existing energy market is constrained by many factors such as technical and financial limitations, decision criteria and policy instruments. This paper will explore the feasibility of SWH, and will work out, using the Analytic Hierarchy Process technique, a policy to ensure a large scale diffusion of SWH in the energy market

2000-11-23

416

Photocatalytic degradation of gaseous pyridine over zeolite-supported titanium dioxide  

Energy Technology Data Exchange (ETDEWEB)

The photocatalyzed degradation of pyridine in the gas phase was investigated using titanium dioxide semiconductor supported on mordenite. The complete mineralization was found to occur over a catalyst containing 75 wt% TiO{sub 2} and 25 wt% mordenite in about 180 min in the presence of saturated water vapor at O{degrees}C (4.6 Torr). Low water vapor pressure of 0.096 Torr was found to be sufficient to achieve a reasonably high percentage and rate of degradation. Diffusion of pyridine within the catalyst adversely affects the activity when the thickness of the catalyst coating exceeds the penetration depth of illumination. The activity of the zeolite-supported catalysts was higher than that of TiO{sub 2}. The photonic efficiency for the complete mineralization of pyridine to CO{sub 2} was determined to be 0.48. 29 refs., 6 refs., 1 tab.

1994-09-01

417

Performance of a diode-pumped laser repetitively Q-switched with a mechanical shutter.  

Science.gov (United States)

Repetitively Q-switched operation of an end-pumped Nd:YAG laser over the range of 200 Hz to 3 kHz using an intracavity chopper is demonstrated. Performance is shown to be comparable to that achieved with an acousto-optic Q switch under similar conditions. The advantages and limitations of the mechanical Q switch are described. Parametric variations of output coupling and pump power lead to an extended empirical description of repetitively Q-switched laser operation. The insertion loss as a function of aperture-edge penetration into the resonator is reported, and a definition of the mechanical Q-switch opening time is provided. Q-switched pulsewidths as short as 35 ns were obtained for the Nd:YAG laser, with a peak power-enhancement factor in excess of 300. PMID:20862099

1994-02-20

418

Oxidation/sulfidation of material candidates for distributed solar receiver thermochemical transport program in SO/sub 2//O/sub 2/  

Energy Technology Data Exchange (ETDEWEB)

Metals for potential use in the dissociator and the synthesizer reactors of a distributed solar receiver thermochemical transport loop utilizing SO/sub 3//SO/sub 2//O/sub 2/ molecular chemistry were tested in SO/sub 2//O/sub 2/ mixtures at 500/sup 0/C and 900/sup 0/C, respectively, for times of up to four weeks. They included titanium, aluminum and nickel, and iron-base, nickel-base and cobalt-base superalloys. Weight gain measurements determine the oxidation/sulfidation kinetics. Electron microprobe analysis identifies any possible penetration of oxygen and sulfur into the metal and the formation of internal oxides and sulfides. The most promising candidates as a result of these tests are the cobalt-base superalloys.

1985-06-01

419

Mechanism of solubilization in detergent solutions  

Energy Technology Data Exchange (ETDEWEB)

The kinetics of the solubilization of lauric acid, palmitic acid, stearic acid, and monopalmitin have been studied in detergent solutions as a function of concentration, temperature, and fluid flow. The detergents used were sodium dodecyl sulfate (an anionic surfactant), decyltrimethylammonium bromide (a cationic surfactant), sodium taurocholate (a trihydroxy bile salt), sodium taurodeoxycholate (a dihydroxy bile salt), and triton X-100 (a nonionic surfactant). At low temperature, solubilization can be described by a five-step mechanism is which micelle desorption and diffusion are rate controlling. At temperatures above the fatty acid penetration temperature, solubilization is governed by formation of a liquid crystalline phase at the fatty acid-detergent solution interface.

1981-11-01

420

Mechanical properties of SiAlON glass surface after swift heavy-ion bombardment  

International Nuclear Information System (INIS)

A Y-Mg-Si-Al-O-N glass was submitted to swift heavy-ion bombardment at GANIL (Caen, France) and the influence of irradiation on the mechanical properties was studied. The mechanical properties of the glass were characterized both before and after irradiation. Changes in hardness, elastic modulus and fracture toughness of the near-surface irradiated layer were determined using indentation techniques. SRIM calculations allowed to estimate the ions penetration range and the energy deposition relative to electronic and nuclear interactions, which can be correlated to the experimental damaged depth. Meyer's hardness and Young's modulus decrease by about 30 %, while fracture toughness is increased by more than 40 %. (authors)

421

Measurements of bragg curve for 75 MeV/u "1"2C ion beam and its inactivation effect on melanoma cells  

International Nuclear Information System (INIS)

Relative doses of 75 MeV/u "1"2C ion beam after passing through different thickness of degraders were measured with the double ionization chamber method. The degrader's thickness equalized to penetration depth of the beam in water and its Bragg curve were obtained. The measured Bragg curve is compared with that calculated based on a model set up by the authors. Meanwhile, the inactivation effect of the ion beam passing through different thickness of degraders on melanoma (B_1_6) cells was measured, and the corresponding survival fraction data for B_1_6 cells were acquired

1998-08-01

422

Measurement of the bead profile and microstructural characterization of a CO2 laser welded AISI 904 L super austenitic stainless steel  

British Library Electronic Table of Contents (United Kingdom)

Laser welding of AISI 904 L super austenitic stainless steel using a diffusion cooled slab 3.5kW CO2 laser and employing two different shielding gases, namely argon and helium, was carried out. The laser weld bead profile depends on various parameters such as beam power (BP), travel speed (TS) and focal position (FP) of the laser spot. These parameters have to be selected suitably to obtain the desirable output. The cross sectioned area of the bead profiles measured using an optical microscope to determine the bead width and depth of penetration. X-ray diffraction used for phase identification confirmed that the weld structure was fully austenitic and dendritic. Hardness was observed to increase in the weld bead with respect to the parent metal and it was related to the microstructural ref...

2010-01-01

423

MCNP study for epithermal neutron irradiation of an isolated liver at the Finnish BNCT facility  

International Nuclear Information System (INIS)

A successful boron neutron capture treatment (BNCT) of a patient with multiple liver metastases has been first given in Italy, by placing the removed organ into the thermal neutron column of the Triga research reactor of the University of Pavia. In Finland, FiR 1 Triga reactor with an epithermal neutron beam well suited for BNCT has been extensively used to irradiate patients with brain tumors such as glioblastoma and recently also head and neck tumors. In this work we have studied by MCNP Monte Carlo simulations, whether it would be beneficial to treat an isolated liver with epithermal neutrons instead of thermal ones. The results show, that the epithermal field penetrates deeper into the liver and creates a build-up distribution of the boron dose. Our results strongly encourage further studying of irradiation arrangement of an isolated liver with epithermal neutron fields.

2004-11-01

424

Lung scintigraphy following inhalation of the new ultrafine aerosol 'Technegas'  

International Nuclear Information System (INIS)

Evaporation of "9"9"mTc-pertechnetate at about 2500"0C on a carbon surface generates an ultrafine aerosol of labelled carbon clusters. Its particle size of about 2-5 nm enables the aerosol to behave similarly to a gas regarding the ability of penetration. After inhalation, the radioactive particles adhere to the walls of the respiratory bronchioli and alveoli. The high concentration of the radioactivity in the argon carrier gas makes it possible to record a scintigram after a single deep breath. We studied four healthy volunteers and 79 patients including 34 with a tentative diagnosis of pulmonary embolism, 20 with bronchus carcinoma, and 15 with various other lung diseases. Ten of these patients were infants, the youngest being nine months old. All patients also had a perfusion scintigraphy. (orig.).

425

Leaching characteristics of paraffin waste package with pinhole  

International Nuclear Information System (INIS)

An Effect of pinhole(perforation or pit penetration) that might be formed outside the package on the nuclide leaching from paraffin waste form was investigated. In case of single pinhole, the leached mass and cumulative fraction leached (CFL) increased with the larger diameter of pinhole, but they were not in direct proportion to the size or area of pinhole. If the total area of multiple pinholes was fixed, the leached mass showed a tendency to increase as each size was smaller and the number was more. It was also found that the leached mass was not in direct proportion to the number of pinhole in case of constant size. In order to analyze the test results, the shrinking core model(SCM) was derived from the diffusion-controlled dissolution reaction and compared with previous diffusion model.

2001-05-01

426

Laboratory evaluation of pipeline girth weld imperfections to determine their acceptability in sour gas service  

Energy Technology Data Exchange (ETDEWEB)

The influence of common welding defects such as internal under-cut, incomplete penetration of the root bead, internal concavity and hollow bead have been evaluated in a sour environment. Tests were performed on samples cut from actual pipeline welds. The individual defects were subjected to slow strain rate testing. The samples were then examined by metallography, scanning electron microscopy, and hardness testing. It was established that a threshold stress intensity exists for sulphide stress cracking. The test results were compared to those obtained from samples of the weld and pipe which did not contain any defects. This comparison indicated that the metallurgical variations associated with the presence of a weld are the main factor for sulphide stress cracking rather than any specific defects or geometry. 5 tabs., 9 figs.

1992-12-31

427

Interactions at the cofired interface of Ag/Pd electrode and lead-based ferroelectrics  

Energy Technology Data Exchange (ETDEWEB)

In the present study, element interdiffusions at the cofired interface of 9/1 Ag/Pd electrode and lead magnesium niobate (PMN)-based ferroelectrics were investigated using Auger Electron Spectroscopy (AES). Intense interdiffusions at the interface were observed while Ag and Pd could penetrate into the ceramics for about 1 {mu}m. Ag-doping experiments were carried out to further study the effects of Ag diffusion on electrical properties of the ceramics. The results showed that Ag could be incorporated into solid solution of the ceramics as Ag{sup +}. As a whole, the Curie temperature (Tc) and dielectric constant of the ceramics decreased with Ag addition. However, Ag addition had no obvious effect on the insulation resistivity. The results inferred that Ag{sup +} could substitute for Pb{sup 2+} at A site of ABO{sub 3} lattice, thereby oxygen vacancies were generated.

2003-05-25

428

Integrated method of RS and GPR for monitoring the changes in the soil moisture and groundwater environment due to underground coal mining  

British Library Electronic Table of Contents (United Kingdom)

Mining affects the environment in different ways depending on the physical context in which the mining occurs. In mining areas with an arid environment, mining affects plants? growth by changing the amount of available water. This paper discusses the effects of mining on two important determinants of plant growth?soil moisture and groundwater table (GWT)?which were investigated using an integrated approach involving a field sampling investigation with remote sensing (RS) and ground-penetrating radar (GPR). To calculate and map the distribution of soil moisture for a target area, we initially analyzed four models for regression analysis between soil moisture and apparent thermal inertia and finally selected a linear model for modeling the soil moisture at a depth 10?cm; the relative error o...

2009-01-01

429

In situ synthesis of silver chloride nanoparticles into bacterial cellulose membranes  

British Library Electronic Table of Contents (United Kingdom)

In situ synthesis of silver chloride (AgCl) nanoparticles was carried out under ambient conditions in nanoporous bacterial cellulose (BC) membranes as nanoreactors. The growth of the nanoparticles was readily obtained by alternating dipping of BC membranes in the solution of silver nitrate or sodium chloride followed by a rinse step. X-ray diffraction (XRD) patterns indicated the existence of AgCl nanoparticles in the BC and scanning electron microscopy (SEM) images showed that the AgCl nanoparticles well dispersed on the surface of BC and penetrated into the BC network. The AgCl nanoparticle-impregnated BC membranes exhibited high hydrophilic ability and strong antimicrobial activity against Escherichia coli (Gram-negative) and Staphylococcus aureus (Gram-positive). The preparative proced...

2009-01-01

430

Extension of energy acceptance of Bragg curve counter at the high-energy end  

Energy Technology Data Exchange (ETDEWEB)

We have developed an energy-extension method of a Bragg curve counter (BCC) at the high-energy end for the measurements of double-differential cross-sections (DDXs) of fragment productions induced by tens of MeV protons. In this method, we estimate the incident energies of the fragments penetrating a BCC on the basis of the energy loss and atomic number (Z). We applied this method to the DDX measurements of the {sup nat}C(p, Li) and {sup nat}C(p, Be) reactions induced by 70 MeV protons. The validity of this method has been confirmed by comparing the DDXs of beryllium with theoretical predictions of the PHITS code and the two-body kinematics. This method improves the energy acceptance of the BCC for light fragments twice as wide as that of a conventional method without remodeling of the BCC and any loss of the original advantages.

2008-07-11

431

Equipment hardening and hardness assurance  

International Nuclear Information System (INIS)

The introduction of tolerance to radiation (''radiation-hardness'') into large electronic systems is one of the major tasks to which this Handbook will be put. The practices recommended here for inculcating radiation-tolerance in equipment require advanced physical modeling techniques, precise engineering procedures, and firm assurance procedures. The degree to which these procedures should be used in an equipment project can be measured by the severity of the raw radiation environment, the desired reliability of the system, and the requirement of that project for radiation-sensitive technologies. The balance of device/circuit design versus shielding will depend on whether the radiation is highly penetrating -- as in isotope handling or military environments -- or readily attenuated, as in space. In this chapter the authors have attempted to summarize the essential features of the radiation hardening of large assemblies of equipment and how effective control of ...

432

Enhanced inactivation of bacteria by metal-oxide nanoparticles combined with visible light irradiation  

British Library Electronic Table of Contents (United Kingdom)

AbstractBackground In recent years nano-metaloxides which easily penetrate into the cells with special interest due to their higher chemical reactivity as compared to that of similar materials in the bulk form. Of particular interest are nano-TiO2 and ZnO, which have been widely used for their bactericidal and anticancerous properties. Purpose The aim of the present study was to examine the bactericidal properties of nano-TiO2 and ZnO combined with visible light on S. aureus and S. epidermitis, known for their high prevalence in infected wounds. Study Using the technique of electron-spin resonance (ESR) coupled with spin trapping, we examined the ability of TiO2 and ZnO nanoparticle suspensions in water to produce reactive oxygen species (ROS) with and without visible light irradiation. Th...

2011-01-01

433

Efficacy and safety of certolizumab pegol in an unselected crohn's disease population: 26-week data of the FACTS II survey  

British Library Electronic Table of Contents (United Kingdom)

AbstractBackground: Certolizumab pegol (Cimzia, CZP) was approved for the treatment of Crohn's disease (CD) patients in 2007 in Switzerland as the first country worldwide. This prospective phase IV study aimed to evaluate the efficacy and safety of CZP over 26 weeks in a multicenter cohort of practice-based patients. Methods: Evaluation questionnaires at baseline, week 6, and week 26 were completed by gastroenterologists in hospitals and private practices. Adverse events were evaluated according to World Health Organization (WHO) guidelines. Results: Sixty patients (38F/22M) were included; 53% had complicated disease (stricturing or penetrating), 45% had undergone prior CD-related surgery. All patients had prior exposure to systemic steroids, 96% to immunomodulators, 73% to infliximab, and...

2011-01-01

434

Corrosion experiments and materials developed for the Japanese HLM systems  

British Library Electronic Table of Contents (United Kingdom)

The static corrosion tests in lead-bismuth eutectic (LBE) were conducted from 450degreeC to 600degreeC to understand corrosion behavior and develop corrosion resistant materials for heavy liquid metal systems. While increase of Cr content in steels enhances corrosion resistance in LBE, the effect approaches a constant value above 12wt% of Cr. Corrosion depth in LBE increases with increasing temperature and corrosion attack becomes severe above 550degreeC even under the condition of high oxygen concentration. Nickel dissolution and Pb-Bi penetration occur in 316SS and JPCA above 550degreeC under the condition of high oxygen concentration. When oxygen concentration decreases below the level of Fe oxide formation, corrosion attack on these steels also becomes violent due to dissolution of var...

2011-01-01

435

Colour contrast in ballistic gelatine  

British Library Electronic Table of Contents (United Kingdom)

Gelatine is a reliable tissue simulant in wound ballistic experiments. The projectile penetrating the gelatine transfers energy and causes radial cracks according to the temporary cavity. Thus the crack length is a function of the energy spent in the medium. In practice the fissures are poorly contrasted for which reason an enhancement of contrast was searched. A series of six shoots with expanding bullets (9mmx19 Action-5, 9mmx19 Quick Defense 1, 5.56mmx45 Styx Action) was realized on 10% gelatine blocks at 4^oC temperature. Three blocks were marked with acryl paint on the front, three blocks were shot native. The blocks were cut in slices of 1cm thickness and optically scanned. The evaluation was performed according to Fackler's wound profile, the total crack length method and the polygo...

2010-01-01

436

Coloring of cultured pearls by gamma-rays irradiation  

International Nuclear Information System (INIS)

Changing cream pearls into bluish-grey by #gamma# ray irradiation is a technique in coloring of pearls. Irradiated pearls are similar in color to cultured blue pearls. The pearl layers hardly change their color but the nuclei change into dark brown by irradiation. Visible light (500 - 700 nm) penetrating the pearl layer is absorbed by dark brown nucleus. The intensity of reflecting light between 400 and 500 nm at pearl surface, therefore, becomes stronger than that between 500 and 700 nm; therefore color of irradiated pearls look bluish-grey. The density of bluish-grey color increases with increasing absorbed doses, but their luster at surface diminishes owing to the deterioration of the pearl layer by prolonged irradiation; high doses irradiation should be avoided. Irradiated pearls show no substantial fading of their color in a year and the rate of the fading is found to be lower than that for cultured blue pearls. (author).

437

Code case to substitute the allowable crack angle in rules on fitness-for-service codes of JSME  

International Nuclear Information System (INIS)

The new Code Case to substitute the allowable crack angle for a circumferential surface crack in 'Rules on Fitness-for-Service (FFS)' published from The Japan Society of Mechanical Engineers (JSME). Until now, the angle of a circumferential surface crack was limited below 60deg. This is the limitation with consideration to the stability of the crack if the deep crack penetrates wall of the pipe. Therefore, a long crack (such like an SCC) was obliged to repair or replace even if it was shallow enough. Weld Overlay (WOL) repair in which strength of the original piping is ignored is also inapplicable for the same reason. In order to solve this irrationality, the new Code Case applying to the crack stability assessment when the crack angle exceeds 60deg was established, and allowable crack depth according to the crack angle were defined in it. (author)

2008-07-01

438

Coal fire interferometry  

Energy Technology Data Exchange (ETDEWEB)

This BCRS project demonstrates the use of SAR interferometry for measuring and monitoring land subsidence caused by underground coal fires and underground mining in a remote area of north west China. China is the largest producer and consumer of coal in the world. Throughout the N.W., N. and N.E. of China, the coal-seams are very susceptible to spontaneous combustion, causing underground coal fires. As the thick coal seams are burned out, the overburden collapses, causing land subsidence, and producing new cracks and fissures, which allow more air to penetrate and continue the fire to spread. SAR interferometry, especially differential interferometry has been shown to be able to measure small differences in surface height caused by such land subsidence. This report describes the problems, the test area, the procedures and techniques used and the results obtained. It concludes with a description of some of the problems encountered during the project plus provides ...

2000-07-01

439

Chemical absorption of carbon dioxide with aqueous sodium hydroxide solution spray  

Energy Technology Data Exchange (ETDEWEB)

Measurements of local mass fluxes of liquid, local number fluxes of the drop and local drop size distributions at various locations in the test column were made for wide ranges of liquid flow rates and gas flow rates. An empirical correlation for the volume mean diameter of the drop at the nozzle exit was proposed. Measurements of the rates of absorption of carbon dioxide from carbon dioxide-air mixtures with water sprays (physical absorption) and aqueous sodium hydroxide sprays (chemical absorption) were made for wide range so fluid flow rates, feed gas concentrations, and initial alkali concentrations. The observed dimensionless rates of absorption were compared with the theoretical values by assuming penetration model with second-order irreversible reaction. 11 refs., 7 figs.

1996-12-31

440

Changes in the soils of solonetzic associations in 30 years after their reclamation with the use of moldboard plowing, deep tillage with a three-tier plow, and deep rotary tillage  

British Library Electronic Table of Contents (United Kingdom)

Changes in the properties of solonetzic soil associations (chestnut solonetzic soils and chestnut solonetzes) in the dry steppe after their reclamation have been studied for 30 years. The reclamation included the deep three-tier plowing and the approach of rotary tillage. A single rotary tillage operation resulted in the formation of fine aggregates of equal sizes in the plow layer; any morphological features of the restoration of solonetzic pedogenesis are absent. The atmospheric moisture easily penetrates into the soil, and soluble salts are leached off to a great depth. In 30 years since the soil amelioration with the use of a PMS-70 rotary tiller, the humus content has increased up to 3.3% in the upper 20-cm-thick layer and up to 2.4% in the layer of 20?40 cm. The content of adsorbed N...

2011-01-01

441

CO2 CAPTURE BY ABSORPTION WITH POTASSIUM CARBONATE  

Energy Technology Data Exchange (ETDEWEB)

The objective of this work is to improve the process for CO{sub 2} capture by alkanolamine absorption/stripping by developing an alternative solvent, aqueous K{sub 2}CO{sub 3} promoted by piperazine. CO{sub 2} mass transfer rates are second order in piperazine concentration and increase with ionic strength. Modeling of stripper performance suggests that 5 m K{sup +}/2.5 m PZ will require 25 to 46% less heat than 7 m MEA. The first pilot plant campaign was completed on June 24. The CO{sub 2} penetration through the absorber with 20 feet of Flexipac{trademark} 1Y varied from 0.6 to 16% as the inlet CO{sub 2} varied from 3 to 12% CO{sub 2} and the gas rate varied from 0.5 to 3 kg/m{sup 2}-s.

2004-07-29

442

Brane-world cosmology with black strings  

CERN Document Server

We consider the simplest scenario when black strings (cigars) penetrate the cosmological brane. As a result, the brane has a Swiss-cheese structure, with Schwarzschild black holes immersed in a Friedmann-Lema\\^{\\i}tre-Robertson-Walker brane. There is no dark radiation in the model, the cosmological regions of the brane are characterized by a cosmological constant $\\Lambda$ and flat spatial sections. Regardless of the value of $\\Lambda$, these brane-world universes forever expand and forever decelerate. The totality of source terms in the modified Einstein equation sum up to a dust, establishing a formal equivalence with the general relativistic Einstein-Straus model. However in this brane-world scenario with black strings the evolution of the cosmological fluid strongly depends on $\\Lambda$. For $\\Lambda$ less or equal to zero it has positive energy density $\\rho$ and negative pressure $p$ and at late times it behaves as in the Einstein-Straus model. For ...

2006-01-01

443

Basic characteristics of centrifuges, (2)  

International Nuclear Information System (INIS)

The presence of an extraneous light gas must be taken into account in consideration of centrifugal separation of uranium isotopes, when there is inevitable leakage of such a gas through the gas sealant and/or leaking in from the atmosphere. Consideration is first given to the influence of the presence of the light gas on the maximum separative power. Then the basic equation for isotope separation containing a light gas is derived from Hirschfelder's diffusion equations. This equation is solved and the separative performance is expressed in terms of the shape factor and reflux parameter. The formulas for expressing the flow configurations of the gases are obtained for a simple model in which inflow and outflow prevail throughout the centrifuge. The corresponding equation for a model in which the gases flow in two concentric thin streams is also derived. It is concluded that the influence provided by the presence of a light gas is quite significant if the gas ...

444

Application of the grazing angle polarized neutron reflectometry to study the magnetism in thin films and stratified media  

Energy Technology Data Exchange (ETDEWEB)

From optical point of view and due to the magnetic interaction of the cold neutrons with the unpaired electron shell, magnetic materials hae a neutron spin-dependent refractive index n[sup +] [spin up] and n[sup -] [spin down]. Magnetic media such as Fe, Co and Ni react like birefringent uniaxial crystals in ordinary optica. n[sup +] and n[sup -] are the equivalent of the ordinary and extraordinary refractive indices. The specular reflection of spin polarized neutrons which is due to the discontinuity of the magnetic induction at the surface of the ferromagnet is a sensitive probe of surface and interface magnetism. We shall first give the background of the art of polarized neutron optics. Secondly, some recent examples from surface and interface magnetism will be given to illustrate the power of this technique such as the magnetic coupling in thin films and multilayers and flux penetration in superconductors. (orig.).

1992-12-01

445

All sliding element journal bearing rock bit  

Energy Technology Data Exchange (ETDEWEB)

For years rock bit performance has been progressively improved by many innovative changes to the design of both the bit cutting structure and the bearing. The changes have offered increased footage per bit and reduced cost per foot of hole through longer bit life and/or faster penetration rate. Efforts to assist the industry in drilling deeper thru hard abrasive rocks such as cherts of West Texas, conglomerated of the Rockies and bromides of Oklahoma led to a major breakthrough in rock bit design - the development of the tungsten carbide cutting structure. When properly applied the bit far exceeded that of the non-sealed ball and roller bearing being used at the time. The bearing failure mode was one of severe race spalling and abrasive wear influenced by the drilling fluid entering the bearing.

1983-08-01

446

Adsorption behavior of strontium on kaolinite and montmorillonite and their mixtures  

Energy Technology Data Exchange (ETDEWEB)

{sup 90}Sr, with a long half-life of 28.5 years, is the most dangerous strontium isotope. The adsorption behavior of radionuclides in the environment are closely related to the safe disposal of radioactive wastes. Since various types of minerals may exist in and around the repositories used for ultimate disposal of nuclear waste, the adsorption behavior of certain radionuclides onto and from these minerals and similar adsorbents should be studied in order to estimate the rates of transport of the nuclides in the event of water penetration into and through the repository. Information on the adsorption properties of the purified individual clay minerals may not be sufficient to predict the adsorption properties of a corresponding mixture, because these clay minerals may interact with each other and lead to modification of the adsorption properties of the mixture as compared to the pure minerals. The adsorption behavior of strontium on kaolinite and montmorillonite ...

2004-07-01

447

Acid gas absorption in aqueous solutions of mixed amines  

Energy Technology Data Exchange (ETDEWEB)

A mass transfer model has been developed to describe the rate of absorption (or desorption) of H{sub 2}S and CO{sub 2} in aqueous blends of a tertiary and a secondary or a primary amine. The model is based on penetration theory, and all significant chemical reactions are incorporated in the model. The reactions are taken to be reversible, with reactions involving only a proton transfer considered to be at equilibrium. The particular amines studied in this research were methyldiethanolamine (MDEA), a tertiary amine, and diethanolamine (DEA), a secondary amine. Key physicochemical data needed in the model, such as diffusion coefficients, kinetic rate constants, and gas solubilities, were measured. Experimental absorption rates of CO{sub 2} and H{sub 2}S were measured in a model gas-liquid contacting device and were compared with model predictions. Experiments were carried out for single amine solutions (both MDEA and DEA) and for amine blends.

1996-12-31

448

A small direct injection diesel engine with a swirl nozzle  

Energy Technology Data Exchange (ETDEWEB)

A new combustion system for a small direct injection diesel engine has been developed, with a spheroidal cavity and swirl nozzle characterized by weak spray penetration and wide spray angle. This system is intended to realize air-borne mixture formation and good combustion processes over wide operating ranges. In-cylinder observations of the system reveal that droplets are easily bent in the direction of air movement, ignition occurs near the spray tip, and the flame is hard to envelop the spray. In a single cylinder engine of 460 cm/sup 3/ swept volume, the system realizes active diffusion burning and mild premixed burning despite of long ignition delay, and provides low fuel consumption and low smoke emission, especially at low speeds.

1987-01-01

449

A liquid chromatography?fluorimetric method for the in vitro estimation of the skin penetration of disodium phenyldibenzimidazole tetrasulfonate from sunscreen formulations through human skin  

British Library Electronic Table of Contents (United Kingdom)

Disodium phenyldibenzimidazole tetrasulfonate (PDT) is a new organic UV filter with hydrophilic properties used in modern sunscreen spray formulations. The aim of this work was to develop and validate an analytical method that can be used to study skin absorption of PDT from sunscreens. Results obtained in vitro for human skin showed a low level of absorption. The proposed in vitro method employs a diffusion cell. Sunscreen lotion was applied onto pretreated human skin, which was then placed in the cell. PDT was collected in a receptor liquid, the surface of which was in contact with the skin. The solutions obtained were diluted appropriately and analyzed by liquid chromatography without any interference. The analytical features of chromatographic determination with fluorimetic detection w...

2006-01-01

450

A compensating method of an imaging plate response to clinical proton beams  

Energy Technology Data Exchange (ETDEWEB)

For charged particle irradiations, the response of an imaging plate (IP) changes around the Bragg peak. Therefore, an appropriate compensation is necessary for the evaluation of dose distribution formed by charged particles such as protons. In this paper, the response of IPs to clinical proton beams is investigated. An experimentally-obtained depth-dose distribution (an ordinary Bragg curve) by a silicon semiconductor detector (SSD) is employed to evaluate the compensation factors as a function of proton penetrating depth, i.e. residual range. A typical dose distribution in a water phantom formed by an L-shaped bolus is measured by IPs and corrected by using the information of those compensation factors; the residual proton range is successfully calculated by the pencil beam algorithm at an arbitrary point. The results show a good agreement with the measurements by the SSD within the rms error of 3.0%.

2002-04-01

451

UMTRA project disposal cell cover biointrusion sensitivity assessment, Revision 1  

International Nuclear Information System (INIS)

This study provides an analysis of potential changes that may take place in a Uranium Mill Tailings Remedial Action (UMTRA) Project disposal cell cover system as a result of plant biointrusion. Potential changes are evaluated by performing a sensitivity analysis of the relative impact of root penetrations on radon flux out of the cell cover and/or water infiltration into the cell cover. Data used in this analysis consist of existing information on vegetation growth on selected cell cover systems and information available from published studies and/or other available project research. Consistent with the scope of this paper, no new site-specific data were collected from UMTRA Project sites. Further, this paper does not focus on the issue of plant transport of radon gas or other contaminants out of the disposal cell cover though it is acknowledged that such transport has the potential to be a significant pathway for contaminants to reach the environment during ...

2004-06-22

452

UMTRA project disposal cell cover biointrusion sensitivity assessment, Revision 1  

Energy Technology Data Exchange (ETDEWEB)

This study provides an analysis of potential changes that may take place in a Uranium Mill Tailings Remedial Action (UMTRA) Project disposal cell cover system as a result of plant biointrusion. Potential changes are evaluated by performing a sensitivity analysis of the relative impact of root penetrations on radon flux out of the cell cover and/or water infiltration into the cell cover. Data used in this analysis consist of existing information on vegetation growth on selected cell cover systems and information available from published studies and/or other available project research. Consistent with the scope of this paper, no new site-specific data were collected from UMTRA Project sites. Further, this paper does not focus on the issue of plant transport of radon gas or other contaminants out of the disposal cell cover though it is acknowledged that such transport has the potential to be a significant pathway for contaminants to reach the environment during ...

1995-10-01

453

Time-temperature-precipitation and time-temperature-sensitization behavior of highly corrosion resistant nickel-chromium-molybdenum alloys. Das Zeit-Temperatur-Ausscheidungs- und das Zeit-Temperatur-Sensibilisierungs-Verhalten von hochkorrosionsbestaendigen Nickel-Chrom-Molybdaen-Legierungen  

Energy Technology Data Exchange (ETDEWEB)

The time-temperature-precipitation diagrams and the resulting time-temperature-sensitization diagrams have been established and are presented for today's current nickel-chromium-molybdenum alloys C-4, C-276, 22 and the recently developed alloy 59. Compared to those materials alloy 625 behaves differently due to its high niobium content. In addition, also the precipitation and sensitization of alloy G-3 has been established. Under the materials considered alloy C-276 has the strongest tendency to precipitate the intermetallics Mu and P together with the carbide M{sub 6}C at intermediate temperatures, followed by the alloys 22 and 59. The tendency to sensitization in the sense of the 50{mu}m (2 mils) intercrystalline penetration criterion when exposed to the ASTM G-28, method A test solution is greatest with alloy C-276, and decreases over the alloys 22, 59 and G-3 to alloy 625. Sensitization is caused by precipitation of the intermetallics {mu} and P and ...

1992-05-01

454

Study on the effectiveness of some decontamination agents against skin contamination of {sup 137}Cs and {sup 60}Co  

Energy Technology Data Exchange (ETDEWEB)

In order to evaluate the effectiveness of some decontamination agents against skin contamination of {sup 60}Co and {sup 137}Cs, the experiments were carried out in this study. In the experiments, pig skin was used instead of human skin, {sup 60}CoCl{sub 2} and {sup 137}CsCl were used the liquid sources of skin contamination. To examine the effectiveness of decontamination agents, skin decontamination was tried using soup, EDTA, DAERICON which was developed for decontamination of radionuclides on the surface of building structure, and new decontamination agents such as IOCON, TRICON, and CHARCON, which were developed in this study. The absorption of radionuclides through the skin was evaluated by the gamma-ray detection on the surface of sample skin after radionuclides were penetrated into the skin during 16 hour soiling time. The results of this absorption experiment indicated that 11.5% and 3.2% of initial amounts of {sup 137}Cs and {sup 60}Co, respectively, were ...

1998-03-01

455

Study on the effectiveness of some decontamination agents against skin contamination of "1"3"7Cs and "6"0Co  

International Nuclear Information System (INIS)

In order to evaluate the effectiveness of some decontamination agents against skin contamination of "6"0Co and "1"3"7Cs, the experiments were carried out in this study. In the experiments, pig skin was used instead of human skin, "6"0CoCl_2 and "1"3"7CsCl were used the liquid sources of skin contamination. To examine the effectiveness of decontamination agents, skin decontamination was tried using soup, EDTA, DAERICON which was developed for decontamination of radionuclides on the surface of building structure, and new decontamination agents such as IOCON, TRICON, and CHARCON, which were developed in this study. The absorption of radionuclides through the skin was evaluated by the gamma-ray detection on the surface of sample skin after radionuclides were penetrated into the skin during 16 hour soiling time. The results of this absorption experiment indicated that 11.5% and 3.2% of initial amounts of "1"3"7Cs and "6"0Co, respectively, were ...

1998-03-01

456

Self-interstitial diffusion and clustering with impurities in crystalline silicon  

International Nuclear Information System (INIS)

In this work the diffusion of ion-beam-injected self-interstitials (Is) and their interaction with impurities in crystalline Si are presented. In particular, the I penetration into a molecular beam epitaxy grown Si structure was studied by means of diffusion effects induced on B spikes, analyzed by a developed simulation code. Trapping effects at sample-surface and bulk are evidenced and modeled. The B marker approach was extended to the two-dimensional (2D) I-diffusion occurring as a consequence of ion implantation through a sub-micron dimension patterned oxide mask. I-source size effects on the I penetration have been found and modeled, quantitatively describing the 2D I-diffusion. The I-substitutional carbon interactions have been also studied, showing the C ability to effectively retain Is. The I-trapping mechanism was quantitatively studied by the simulation code, showing that one I is able to deactivate about two C traps by means of ...

2004-02-01

457

Physical, biochemical and physiological effects of ultraviolet radiation on Brassica napus and Phaseolus vulgaris  

International Nuclear Information System (INIS)

In order to follow some of the changes induced by ultraviolet-B (UV-B, 280-320 nm) radiation in Phaseolus vulgaris and Brassica napus, experiments were designed to localize sites of changes in leaves and to correlate some of the physiological and biochemical changes with penetration of UV-B radiation. B.napus was exposed to 8.9 kJ m"-"2 day"-"1 biologically effective UV-B radiation (UV-B_B_E). The penetration of UV-B radiation into the leaf was followed using a quartz fibre optic microprobe. Monochromatic radiation at 310 nm was decreased by ca 50 and 34% in the adaxial and abaxial epidermis, respectively, in plants not exposed to UV-B, whereas the radiation was decreased by ca 70 and 42%, respectively, in the same region in UV-treated plants. Polychromatic radiation showed a wavelength dependent change mainly for the collimated radiation. The results correlated with the distribution of phenolic compounds analysed from 40 #mu#m paradermal leaf ...

1991-11-05

458

Modelling of fuel spray and combustion in diesel engines  

Energy Technology Data Exchange (ETDEWEB)

Fuel spray and air motion characteristics and combustion in direct injection (DI) diesel engines was studied using computational models of the commercial CFD-code FIRE. Physical subprocesses modelled included Lagrangian spray droplet movement and behaviour (atomisation, evaporation and interaction of spray droplets) and combustion of evaporated liquid spray in the gas phase. Fuel vapour combustion rate was described by the model of Magnussen and Hjertager. The standard k,{epsilon}-model was used for turbulence. In order to be able to predict combustion accurately, the fuel spray penetration should be predicted with reasonable accuracy. In this study, the standard drag coefficient had to be reduced in order to match the computed penetration to the measured one. In addition, the constants in the submodel describing droplet breakup also needed to be adjusted for closer agreement with the measurements. The characteristic time scale of fuel ...

1997-12-31

459

In situ texture analysis under applied load  

International Nuclear Information System (INIS)

The in-situ measurement of a crystallographic texture is a special type of a non-destructive measurement, which need special equipments. Due to the high photon flux and the excellent brilliance high energetic synchrotron radiations are a fantastic tool particular in fast experimentation. Moreover, a high penetration power allows the investigation of standard tensile sample of the DIN-norm. A loading device with a power up to 20 kN was installed at the hard wiggler beamline BW5 (HASYLAB-DESY) to perform in-situ strain and in-situ texture analysis. Using 100keV X-rays one gets short wavelength so that a 2D image-plate detector offers a wide range of diffraction pattern within the first 10 degree in 2 theta. Thermal neutron is another radiation with a high penetration power, which is the standard method for global texture analysis of bulk samples. As an example rectangular extruded Mg- Az31 was investigated by an in-situ. tensile experiment. ...

460

Improvement of top shield analysis technology for CANDU 6 reactor  

Energy Technology Data Exchange (ETDEWEB)

As for Wolsung NPP unit 1, radiation shielding analysis was performed by using neutron diffusion codes, one-dimensional discrete ordinates code ANISN, and analytical methods. But for Wolsung NPP unit 2, 3, and 4, two-dimensional discrete ordinates code DOT substituted for neutron diffusion codes. In other words, the method of analysis and computer codes used for radiation shielding of CANDU 6 type reactor have been improved. Recently Monte Carlo MCNP code has been widely utilized in the field of radiation physics and other radiation related areas because it can describe an object sophisticately by use of three-dimensional modelling and can adopt continuous energy cross-section library. Nowadays Monte Carlo method has been reported to be competitive to discrete ordinate method in the field of radiation shielding and the former has been known to be superior to the latter for complex geometry problem. However, Monte Carlo method had not been used for radiation streaming calculation in the ...

1996-07-01

461

Improved oil recovery using bacteria isolated from North Sea petroleum reservoirs  

Energy Technology Data Exchange (ETDEWEB)

During secondary oil recovery, water is injected into the formation to sweep out the residual oil. The injected water, however, follows the path of least resistance through the high-permeability zones, leaving oil in the low-permeability zones. Selective plugging of these their zones would divert the waterflood to the residual oil and thus increase the life of the well. Bacteria have been suggested as an alternative plugging agent to the current method of polymer injection. Starved bacteria can penetrate deeply into rock formations where they attach to the rock surfaces, and given the right nutrients can grow and produce exo-polymer, reducing the permeability of these zones. The application of microbial enhanced oil recovery has only been applied to shallow, cool, onshore fields to date. This study has focused on the ability of bacteria to enhance oil recovery offshore in the North Sea, where the environment can be considered extreme. A screen of produced water ...

1995-12-31

462

Impact characteristic analysis of ceramic/metal FGM  

Energy Technology Data Exchange (ETDEWEB)

The ceramic composite armor has been lucubrated in the past 40 years. Ceramic can provide the same protection as metal, but it has lighter weight than metal. Ceramic has excellent ability of resisting kinetic energy projectile, because it can transfer energy to a large range by its fragmented cone and has higher ability of eroding the projectile than metal. But the researches indicated the full potential of the ceramic hard face has not been achieved because the significant interface between ceramic and metal has the unfavorable impedance effects and would induce tensile failure. FGM is a new type composite with continuous transition from ceramic to metal; it has no significant discrete materials interfaces between ceramic and metal. This paper deals with the impact response of Ceramic/FGM/Metal armor by numerical and theoretical methods. Firstly, the ability of TiB{sub 2}/FGM/Metal armor resisting KE projectile is analyzed by Dytran FEM program. The comparison between TiB{sub 2}/Metal ...

2003-07-01

463

Groundwater penetrating radar and high resolution seismic for locating shallow faults in unconsolidated sediments  

Energy Technology Data Exchange (ETDEWEB)

Faults in shallow, unconsolidated sediments, particularly in coastal plain settings, are very difficult to discern during subsurface exploration yet have critical impact to groundwater flow, contaminant transport and geotechnical evaluations. This paper presents a case study using cross-over geophysical technologies in an area where shallow faulting is probable and known contamination exists. A comparison is made between Wenner and dipole-dipole resistivity data, ground penetrating radar, and high resolution seismic data. Data from these methods were verified with a cone penetrometer investigation for subsurface lithology and compared to existing monitoring well data. Interpretations from these techniques are compared with actual and theoretical shallow faulting found in the literature. The results of this study suggests that (1) the CPT study, combined with the monitoring well data may suggest that discontinuities in correlatable zones may indicate that faulting ...

1993-12-31

464

Ground penetrating radar and direct current resistivity evaluation of the desiccation test cap, Savannah River Site  

Energy Technology Data Exchange (ETDEWEB)

The Savannah River Site (SRS) has a variety of waste units that may be temporarily or permanently stabilized by closure using an impermeable cover to prevent groundwater infiltration. The placement of an engineered kaolin clay layer over a waste unit is an accepted and economical technique for providing an impermeable cover but the long term stability and integrity of the clay in non-arid conditions is unknown. A simulated kaolin cap has been constructed at the SRA adjacent to the Burial Ground Complex. The cap is designed to evaluate the effects of desiccation on clay integrity, therefore half of the cap is covered with native soil to prevent drying, while the remainder of the cap is exposed. Measurements of the continuing impermeability of a clay cap are difficult because intrusive techniques may locally compromise the structure. Point measurements made to evaluate clay integrity, such as those from grid sampling or coring and made through a soil cover, may miss cracks, joints or ...

1996-04-01

465

Fragmentation of a single molten metal droplet penetrating sodium pool I copper droplet and the relationship with copper jet  

International Nuclear Information System (INIS)

The progression of hypothetical core disruptive accidents in metallic fuel fast breeder reactors is strongly affected by the fragmentation of molten metallic fuels due to the molten fuel-coolant interaction (FCI). As a basic study of FCI, the present paper focuses on the fragmentation of a single molten copper droplet with mass from 1 to 5 g, which penetrated a sodium pool at instantaneous constant interface temperatures (Ti) from 995 to 1,342degC. Intensive fragmentation of a single molten copper droplet was clearly observed even if Ti values are below the melting point (1,083degC) of copper besides the higher Ti range. The intensive fragmentation shows that the mass median diameters (Dm) of copper droplets with a fivefold difference in mass or the same mass have little difference, i.e., they are nearly the same. Under the lower Ti condition, the Dm data of droplet fragments of both the same and different masses scatter widely. It is found that the present Dm/D0 ...

2009-05-01

466

Dual radiotracer measurement of zoobenthos-mediated solute and particle transport in freshwater sediments  

International Nuclear Information System (INIS)

#gamma# spectroscopy methods have been applied to determine the effects of two freshwater benthic macroinvertebrates, on reworking of sediments and the transfer of solutes across the sediment-water interface. Natural lake sediments and overlying water were contained in temperature-regulated rectangular plastic cells. After addition of Stylodrilus (oligochaete worms) and Pontoporeia (crustacean amphipods) to these microcosms, the vertical distribution of Cs-137 (a tracer of particle transport) and Na-22 (a tracer of solute transport) were determined. In cells with Stylodrilus, the Cs-137 layer moved downward at a rate that decreased exponentially with time. In cells with Pontoporeia, Cs-137 activity was smeared downward in time owing to eddy diffusive mixing of sediments over a small range (1-2 cm). In cells without worms, the veneer of Cs active material remained at the interface while the penetration of Na-22 into sediments was consistent with diffusion in free ...

467

C-14 release and transport from a nuclear waste repository in an unsaturated medium  

Energy Technology Data Exchange (ETDEWEB)

The release of {sup 14}C as {sup 14}CO{sub 2} from partly failed spent fuel containers has been analyzed by the flow of gases into and out of the containers. This flow of gases is driven by pressure differences, which are in turn caused by heating by the spent fuel. In this analysis, the timing and size of holes in the containers are assumed to be given. A better means of predicting the time distribution and sizes of penetrations in nuclear waste containers is needed. For the purposes of far-field transport calculations, we have adopted release rates that are shown to be bonding for the large range of hole sizes studied. The transport of released {sup 14}CO{sub 2} has been analyzed by transport in equivalent porous medium. The peak {sup 14}CO{sub 2} concentration in pore gas at 350 m above the repository does not depend on the time of hole occurrence, although the time of penetration obviously affects the arrival and duration of exposure to ...

1990-06-01

468

Ballistic performance of polyurea-coated armor grade ceramic tiles  

Science.gov (United States)

The use of ceramics as energy absorbents has been studied by many researchers and some improvements in the ballistic performance of ceramic tiles have been made by coating them with different classes of materials (e.g. E-glass/epoxy, carbon-fiber/epoxy, etc.). Using ceramics for energy absorbing applications leads to a significant weight reduction of the system. Therefore, any modification to the ceramic configuration in the system which leads to more energy absorption with the same or less areal density is significant. On the other hand, polyurea has been proved to be an excellent energy dissipating agent in many applications. Inspired by this, we are studying the effect of coating ceramics with polyurea and other materials, on the energy absorption and ballistic performance of the resulting ceramic-based composites. In this study, we investigate the effect of polyurea on ballistic efficiency of ceramic tiles. To this end, we have performed a set of penetration ...

2010-03-01

469

Analysis of load-penetration depth data using Oliver-Pharr and Cheng-Cheng methods of SiAlON-ZrO_2 ceramics  

International Nuclear Information System (INIS)

Depth sensing indentation tests were carried out to obtain load-penetration depth curves of SiAlON-ZrO_2 ceramics under different peak loads ranging from 200 to 1800 mN. The values of indentation hardness (H_O_P, H_C_C) and reduced elastic modulus (E_O_P, E_C_C) were calculated by using Oliver-Pharr (OP) and Cheng-Cheng (CC) methods. The experimental results revealed that the indentation hardness and reduced elastic modulus exhibit peak-load dependence, i.e. indentation size effect. Both indentation hardness and reduced elastic modulus values were obtained by considering indenter tip roundness and machine compliance. These values obtained from the OP method are higher than from the CC method. On the other hand, h_f/h_m ratios were used to clarify the indentation deformation behaviour of the SiAlON-ZrO_2 ceramic. The experimental h_f/h_m values were lower than the reported critical value (0.7) for all applied test loads, which is attributed to work-hardening ...

2008-02-07

470

[Study of body composition by potassium-40 measurement in patients with breast and uterine cancer].  

Science.gov (United States)

Total potassium was assayed in 150 normal weight and obese females (cervical carcinoma-52, endometrial carcinoma-25 and breast cancer-73) by measurements of 40K spontaneous radiation in a low-background chamber. Control group included 30 healthy and 25 obese females. Computations of body cell and extracellular mass and fat were carried out on the basis of the said measurements. Extracellular fluid volume was measured in 38 patients by X-ray fluorescence method using sodium bromide. The results pointed to a body cell mass deficit matched by increased extracellular mass due to a higher fat level in patients with breast, endometrial and cervical carcinoma. The said correlation was particularly pronounced in obese patients. The beneficial effect of treatment was more often observed in patients with normal body weight. PMID:3739295

1986-01-01

471

Wavelength shift of lasing from a dye-doped asymmetrically deformed liquid jet  

International Nuclear Information System (INIS)

We examined the spectral behaviors of lasing from a asymmetrically deformed liquid jet (a ? 14 ?m) which is induced by a laterally flowing gas. Th liquid sample was methanols which contains DCM dye. When n distortion is induced, the lasing spectrum appears as two periodic peaks which are corresponding to the resonance modes of cylindrical cavity. As the distortion parameter exceeds about 4%, the lasing spectrum shifts continuously to short wavelength. When the distortion parameter reaches ? 10%, the amount of blue shift was ? 30 nm. The blue shift can be explained as the shift of optimum wavelength of threshold curves. From the absorption and fluorescence curve of liquid sample, we estimated the spoiled Q with the distortion parameter.

1997-11-01

472

Synthesis, crystal structure, spectroscopic properties, antibacterial activity and theoretical studies of a novel difunctional acylhydrazone  

British Library Electronic Table of Contents (United Kingdom)

A novel difunctional acylhydrazone has been synthesized by the reaction of 5-methylisoxazole-4-carboyl hydrazine with benzaldehyde and characterized by X-ray crystallography and spectroscopy. The obtained results demonstrate the crystal belongs to triclinic, space group Formula Not Shown . Moreover, the spectroscopic properties were evaluated through density functional theory (DFT) and time-dependent density functional theory (TD DFT) calculations. The results reveal that UV-Vis absorption peaks at 194, 217.5 and 290.5nm are mainly attributed to (p, p)p*, partly (p, p)p* and partly pp*, and predominantly pp*, respectively, with intraligand charge-transfer transition (ILCT) character. The fluorescence emission peak at 485.96nm should be assigned to ILCT. In addition, the results of antibact...

2011-01-01

473

Surface modification with BSA blocking based on in situ synthesized gold nanoparticles in poly(dimethylsiloxane) microchip  

British Library Electronic Table of Contents (United Kingdom)

A stable BSA blocking poly(dimethylsiloxane) (PDMS) microchannel was prepared based on in situ synthesized PDMS-gold nanoparticles composite films. The modified microchip could successfully suppress protein adsorption. The assembly was followed by contact angle, charge-coupled device (CCD) imaging, electroosmotic flow (EOF) measurements and electrophoretic separation methods. Contact angle measurements revealed the coated surface was hydrophilic, water contact angle for coated chips was 45.2^o compared to a water contact angle for native PDMS chips of 88.5^o. The coated microchips exhibited reproducible and stable EOF behavior. With FITC-labeled myoglobin incubation in the coated channel, no fluorescence was observed with CCD image, and the protein exhibited good electrophoretic effect in ...

2010-01-01

474

Specialized Circuits from Primary Visual Cortex to V2 and Area MT  

British Library Electronic Table of Contents (United Kingdom)

SummaryPrimary visual cortex recombines inputs from magnocellular (M) and parvocellular (P) streams to create functionally specialized outputs. Understanding these input-output relationships is complicated by the fact that layer 4B, which provides outputs to dorsal visual areas, contains multiple cell types. Using a modified rabies virus that expresses green fluorescent protein, we show that layer 4B neurons projecting to MT are a majority spiny stellate, whereas those projecting to V2 are overwhelmingly pyramidal. Regardless of cell type, MT-projecting neurons have larger cell bodies, more dendritic length, and are deeper within layer 4B. Furthermore, MT-projecting pyramidal neurons are located preferentially underneath cytochrome oxidase blobs, indicating that MT-projecting neurons of bo...

2007-01-01

475

Some properties of atomic beam produced by laser induced ablation of Li target  

International Nuclear Information System (INIS)

Pulsed atomic beams produced in vacuum by laser induced ablation from a lithium target are analyzed by laser induced fluorescence (LIF). The 1-mixing processes induced in the n = 9, 10 Li Rydberg states by collisions with CO_2 molecules illustrate the application of the method. Resolution is limited by the 1 mm diameter of the probe laser beam. Combining LIF and absorption measurements gives n_L_i as a function of time at various distances from the target surface. The investigation of the Li-C0_2 1-mixing process in a heat pipe oven proved impossible due to the high reactivity of Li with C0_2. This problem was solved by renewing the Li atoms at each laser shot. Values obtained for n = 9, n = 10 are k = 17 x 10"-"8 and 15 x 10"-"8 cc/sec, respectively.

476

Selegiline-functionalized, PEGylated poly(alkyl cyanoacrylate) nanoparticles: Investigation of interaction with amyloid-b peptide and surface reorganization  

British Library Electronic Table of Contents (United Kingdom)

Alzheimer's disease (AD) is a neurodegenerative disorder for which the research of new treatments is highly challenging. Since the fibrillogenesis of amyloid-b peptide 1-42 (Ab1-42) peptide is considered as a major cause of neuronal degeneration, specific interest has been focused on aromatic molecules for targeting this peptide. In this paper, the synthesis of selegiline-functionalized and fluorescent poly(alkyl cyanoacrylate) nanoparticles (NPs) and their evaluation for the targeting of the Ab1-42 peptide are reported. The synthetic strategy relied on the design of amphiphilic copolymers by tandem Knoevenagel-Michael addition of cyanoacetate derivatives, followed by their self-assembly in aqueous solutions to give the corresponding NPs. Different cyanoacetates were used: (i) hexadecyl cy...

2011-01-01

477

Root Hairs Play a Key Role in the Endophytic Colonization of Olive Roots by Pseudomonas spp. with Biocontrol Activity  

British Library Electronic Table of Contents (United Kingdom)

The use of indigenous bacterial root endophytes with biocontrol activity against soil-borne phytopathogens is an environmentally-friendly and ecologically-efficient action within an integrated disease management framework. The earliest steps of olive root colonization by Pseudomonas fluorescens PICF7 and Pseudomonas putida PICP2, effective biocontrol agents (BCAs) against Verticillium wilt of olive (Olea europaea L.) caused by the fungus Verticillium dahliae Kleb., are here described. A gnotobiotic study system using in vitro propagated olive plants, differential fluorescent-protein tagging of bacteria, and confocal laser scanning microscopy analysis have been successfully used to examine olive roots?Pseudomonas spp. interactions at the single-cell level. In vivo simultaneous visualization...

2011-01-01

478

Rocky Mountain spotted fever in areas of high and low prevalence: survey for canine antibodies to spotted fever rickettsiae.  

Science.gov (United States)

Antibodies to Rickettsia rickettsii were detected by indirect immunofluorescence in sera from 149 of 467 dogs (32%) examined from 4 military installations located in Kentucky, North Carolina, Pennsylvania, and Virginia. The prevalence at individual installations ranged from 4.3% at Fort Knox, Ky, to 63.4% at Fort Bragg, NC. Most of the seropositive dogs were in the working and sporting groups of dogs. The difference in antibody prevalence between sexes was not significant. Serologic responses were related to R rickettsii infection, although antibodies to R montana also were detected in a few of the sera. Comparison of serodiagnostic methods indicated that the indirect fluorescent antibody test was more sensitive than was the indirect hemagglutination test for obtaining survey data on the prevalence of Rocky Mountain spotted fever in the area. PMID:6808878

1982-08-01

479

Research on Actinides in Nuclear Fuel Cycles  

International Nuclear Information System (INIS)

The electrochemical/spectroscopic integrated measurement system was designed and set up for spectro-electrochemical measurements of lanthanide and actinide ions in high temperature molten salt media. A compact electrochemical cell and electrode system was also developed for the minimization of reactants, and consequently minimization of radioactive waste generation. By applying these equipment, oxidation and reduction behavior of lanthanide and actinide ions in molten salt media have been made. Also, thermodynamic parameter values are determined by interpreting the results obtained from electrochemical measurements. Several lanthanide ions exhibited fluorescence properties in molten salt. Also, UV-VIS measurement provided the detailed information regarding the oxidation states of lanthanide and actinide ions in high temperature molten salt media

2007-04-01

480

Proteomic analysis of apoptosis induction in human lung cancer cells by recombinant MVL  

British Library Electronic Table of Contents (United Kingdom)

Lung cancer is still difficult to treat by current chemotherapeutic procedures. We recently found that MVL, an anti-HIV lectin from blue-green algae Microcystis viridis, also has antitumor activity. The objective of this study was to investigate apoptosis-inducing activity of recombinant MVL (R-MVL) and proteomic changes in A549 cells, and to identify the molecular pathways responsible for the anti-cancer action of R-MVL. We found that R-MVL induces A549 cells apoptosis in a dose-dependent manner by using MTT assay, fluorescent microscope (FM) and flow cytometry (FCM), and the IC50 was calculated to be 24.12??g/ml. Subsequently, 7 altered proteins in R-MVL-treated A549 cells were identified, including upregulated aldehyde dehydrogenase 1 and ?-actin, and five downregulated proteins: heat s...

2011-01-01

481

Photodynamic efficacy of hypericin targeted by two delivery techniques to hepatocellular carcinoma cells  

British Library Electronic Table of Contents (United Kingdom)

The photocytotoxic effect of hypericin (Hyp) targeted by two different delivery techniques, namely, liposomes and anti-hepatocyte specific antigen (anti-HSA) was investigated. Optical absorption and steady-state fluorescence were used to analyze the conjugation of Hyp with anti-HSA model and to evaluate the encapsulation capacity and drug release in a liposome model. Particle size and thermal analysis of the prepared liposomes were performed using laser-light scattering and differential scanning calorimetry (DSC), respectively. Viability study of HepG2 cells exposed to Hyp in the two delivery systems, in the dark and following visible light irradiation, was performed in comparison to free Hyp. The intracellular uptake and localization of Hyp in HepG2 cells were analyzed by means of spectro...

2010-01-01

482

Pharmaceutical applications of non-linear imaging  

British Library Electronic Table of Contents (United Kingdom)

Non-linear optics encompasses a range of optical phenomena, including two- and three-photon fluorescence, second harmonic generation (SHG), sum frequency generation (SFG), difference frequency generation (DFG), third harmonic generation (THG), coherent anti-Stokes Raman scattering (CARS), and stimulated Raman scattering (SRS). The combined advantages of using these phenomena for imaging complex pharmaceutical systems include chemical and structural specificities, high optical spatial and temporal resolutions, no requirement for labels, and the ability to image in an aqueous environment. These features make such imaging well suited for a wide range of pharmaceutical and biopharmaceutical investigations, including material and dosage form characterisation, dosage form digestion and drug rele...

2011-01-01

483

Multi-bubble sonoluminescense of europium(III) chloride in heavy water  

International Nuclear Information System (INIS)

Low fluorescence in the field of the Eu3+ photoluminescence spectrum is registered against a bach ground of the continuum of solvent emanation when multi-bubble sonolysis of EuCl3 (0.1 mol l-1) solutions saturated by the air and argon in heavy water. Distinctive sonoluminescence of europium ion is not found earlier in aqueous solutions. Possible reasons of low values of Eu3+ sonoluminescence as compared with other lanthanide ions (Ln3+), and effect of europium on the spectrum of solvent continuum connected, in particular, with the quenching of electron-excited products of the H2O* (O2O*) and Eu3+* sonolysis in the reactions of electron transfer are discussed

2008-09-01

484

Microanalytical method development for Fe, Cu and Zn determination in colorectal cancer cells  

British Library Electronic Table of Contents (United Kingdom)

Microanalytical methods suitable for the determination of Fe, Cu in HT-29 (human colon adenocarcinoma) cells treated with different iron compounds (Fe(II) sulfate, Fe(III) chloride, Fe(III) citrate and Fe(III) transferrin) and cultured in medium supplemented or not with 10% (v/v) fetal calf serum (FCS) by total reflection X-ray fluorescence spectrometry (TXRF) and simultaneous graphite furnace atomic absorption spectrometry (GF-AAS) were developed. The developed TXRF method was also suitable for Zn determination in the samples. The main advantage of the proposed methods is the execution of all sample preparation steps following incubation and prior to the elemental analysis in the same Eppendorf tubes. Sample preparation was performed at microscale (115mL sample volume) with 65% nitric aci...

2011-01-01

485

Mapping of the human cone transducin {alpha}-subunit (GNAT2) gene to 1p13 and negative mutation analysis in patients with Stargardt disease  

Energy Technology Data Exchange (ETDEWEB)

We report localization of the human cone transducin (GNAT2) gene using fluorescence in situ hybridization on chromosome 1 in band p13. The recent assignment of a gene for Stargardt disease to the same chromosomal region by linkage analysis prompted us to investigate the possible role of GNAT2 in the pathogenesis of this disease. We investigated 66 unrelated patients for mutations in the coding region of the GNAT2 gene using polymerase chain reaction-single strand conformation polymorphism analysis (SSCP) and direct sequencing. No disease-specific mutations were found, indicating that GNAT2 is probably not involved in the pathogenesis of most cases of Stargardt disease. 19 refs., 1 fig., 1 tab.

1995-01-01

486

Manganese-Induced NF-kB Activation and Nitrosative Stress Is Decreased by Estrogen in Juvenile Mice  

British Library Electronic Table of Contents (United Kingdom)

Manganese toxicity can cause a neurodegenerative disorder affecting cortical and basal ganglia structures with a neurological presentation resembling features of Parkinson's disease. Children are more sensitive to Mn-induced neurological dysfunction than adults, and recent studies from our laboratory revealed a marked sensitivity of male juvenile mice to neuroinflammatory injury from Mn, relative to females. To determine the role of estrogen (E2) in mediating sex-dependent vulnerability to Mn-induced neurotoxicity, we exposed transgenic mice expressing an NF-kB-driven enhanced green fluorescent protein (EGFP) reporter construct (NF-kB-EGFP mice) to Mn, postulating that supplementing male mice with E2 during juvenile development would attenuate neuroinflammatory changes associated with glia...

2011-01-01

487

Leishmania major ascorbate peroxidase overexpression protects cells against reactive oxygen species-mediated cardiolipin oxidation  

British Library Electronic Table of Contents (United Kingdom)

Heme peroxidases are a class of multifunctional redox-active proteins found in all organisms. We recently cloned, expressed, and characterized an ascorbate peroxidase from Leishmania major (LmAPX) that was capable of detoxifying hydrogen peroxide. Localization studies using green fluorescent protein fusions revealed that LmAPX was localized within the mitochondria by its N-terminal signal sequence. Subcellular fractionation analysis of the cell homogenate by the Percoll density-gradient method and subsequent Western blot analysis with anti-LmAPX antibody further confirmed the mitochondrial localization of mature LmAPX. Submitochondrial fractionation analysis showed that the mature enzyme (?3.6?kDa shorter than the theoretical value of the whole gene) was present in the intermembrane space ...

2008-01-01

488

Intermediate-conductance calcium-activated potassium channels participate in neurovascular coupling  

British Library Electronic Table of Contents (United Kingdom)

BACKGROUND AND PURPOSE Controlling vascular tone involves K+ efflux through endothelial cell small- and intermediate-conductance calcium-activated potassium channels (KCa2.3 and KCa3.1, respectively). We investigated the expression of these channels in astrocytes and the possibility that, by a similar mechanism, they might contribute to neurovascular coupling. EXPERIMENTAL APPROACH Transgenic mice expressing enhanced green fluorescent protein (eGFP) in astrocytes were used to assess KCa2.3 and KCa3.1 expression by immunohistochemistry and RT-PCR. KCa currents in eGFP-positive astrocytes were determined in situ using whole-cell patch clamp electrophysiology. The contribution of KCa3.1 to neurovascular coupling was investigated in pharmacological experiments using electrical field stimulatio...

2011-01-01

489

Implementation of improved interactive image analysis at the Advanced Photon Source (APC) linac.  

Energy Technology Data Exchange (ETDEWEB)

An image-analysis system, based on commercially available data visualization software (IDL [1]), allows convenient interaction with image data while still providing calculated beam parameters at a rate of up to 2 Hz. Image data are transferred from the IOC to the workstation via EPICS [2] channel access. A custom EPICS record was created in order to overcome the channel access limit of 16k bytes per array. The user can conveniently calibrate optical transition radiation (OTR) and fluorescent screens, capture background images, acquire and average a series of images, and specify several other filtering and viewing options. The images can be saved in either IDL format or APS-standard format (SDDS [3]), allowing for rapid postprocessing of image data by numerous other software tools.

1998-09-11

490

Human cDNA mapping using fluorescence in situ hybridization. Final progress report, April 1, 1994--July 31, 1997  

Energy Technology Data Exchange (ETDEWEB)

The ultimate goal of this research is to generate and apply novel technologies to speed completion and integration of the human genome map and sequence with biomedical problems. To do this, techniques were developed and genome-wide resources generated. This includes a genome-wide Mapped and Integrated BAC/PAC Resource that has been used for gene finding, map completion and anchoring, breakpoint definition and sequencing. In the last period of the grant, the Human Mapped BAC/PAC Resource was also applied to determine regions of human variation and to develop a novel paradigm of primate evolution through to humans. Further, in order to more rapidly evaluate animal models of human disease, a BAC Map of the mouse was generated in collaboration with the MTI Genome Center, Dr. Bruce Birren.

1997-12-31

491

Follow-up of pregnant women exposed to chicken pox: an audit of relationship between level of antibody and development of chicken pox  

British Library Electronic Table of Contents (United Kingdom)

The purpose of this study was to validate through natural exposure a cut-off level of varicella zoster IgG as protective against infection with varicella zoster virus (VZV). Laboratory testing to determine VZV immune status of pregnant women exposed to varicella is recommended. Quantitative assays are now available which are sensitive and specific. More than 200 consecutive requests for screening in pregnant patients with recent varicella contacts were followed-up by questionnaire. DiaSorin LIAISON and VZV time resolved fluorescence immuno assay (VZV TRFIA) were used to measure VZV antibody level. One hundred fifty out of 209 (72%) questionnaires were returned; 14 patients developed varicella, 129 did not and seven were not known. Patients who had been given VZIG and developed varicella on...

2011-01-01

492

Flow visualization II Proceedings of the Second International Symposium, Bochum, West Germany, September 9-12, 1980  

Energy Technology Data Exchange (ETDEWEB)

Applications, techniques, instrumentation, and interpretation of flow visualization are discussed. Methods of using flow visualization for the examination of combustion in furnaces, heat transfer with heat exchangers, and in fluid engines are explored, along with flow visualization in food processing, steel-casting, and process engineering. Further attention is given to pipe and channel flow, flow separation in laminar flow and around oscillating airfoils, wakes and vortices, supersonic flow and shock waves, and stratified flow and oceanography. The visualization of boundary layers is considered for various conditions, and applications for multiphase flow, rheology, and medical problems are detailed. Oil film, dry-surface coating, chemical, fluorescent, and minituft methods are presented, as well as the use of tracers, optical techniques, strobe lights, lasers, computerized data acquisition, and hot-wire anemometry.

1982-01-01

493

Flow cytometric analysis of respiratory tract cells exposed to oil shale and silica particulates. [Hamsters  

Science.gov (United States)

Flow cytometric techniques were used to measure the cytological and biochemical damage to respiratory tract cells in animals exposed to particulates. Hamsters were exposed to raw and spent oil shale particulates and silica by intratracheal instillation. Exfoliated lung cells were obtained by sacrificing the animals and lavaging the respiratory tract posterior to the trachea with saline. Cell samples were fixed in ethanol and stained with mithramycin for fluorescence analysis of DNA content. DNA content distributions from hamsters exposed to spent oil shale and silica particulates showed atypical changes 28 to 35 days later. Cell counts and total numbers of macrophages, leukocytes, and epithelial cells in the lavage fluid also showed marked changes related to time after exposure.

1979-01-01

494

Elemental analysis of savannah grass' burning ashes  

International Nuclear Information System (INIS)

In order to quantify the biomass burning emissions, the main atmospheric pollution source of tropical and subtropical regions, we carried out the analysis of ashes that are also formed during these fires. To this end, we developed analytical methods to characterize the composition of savannah grass burning ashes by using X-ray fluorescence for mineral elements and microanalysis for C, H, O and N. Samples used in this work have been collected during laboratory combustion experiments, with chemically well-defined natural savannah grasses from Ivory Coasts and South Africa. The reproducibility and efficiency of different developed procedures have been studies. The analytical relative precision is generally better than 5%. This development has allowed to establish, for the first time, the global mass balance of ashes resulting from savannah grass burning. (authors). 16 refs., 3 figs., 8 tabs.

495

Dialysis membrane for separation on microchips  

Energy Technology Data Exchange (ETDEWEB)

Laser-induced phase-separation polymerization of a porous acrylate polymer is used for in-situ fabrication of dialysis membranes inside glass microchannels. A shaped 355 nm laser beam is used to produce a porous polymer membrane with a thickness of about 15 .mu.m, which bonds to the glass microchannel and forms a semi-permeable membrane. Differential permeation through a membrane formed with pentaerythritol triacrylate was observed and quantified by comparing the response of the membrane to fluorescein and fluorescently tagging 200 nm latex microspheres. Differential permeation was observed and quantified by comparing the response to rhodamine 560 and lactalbumin protein in a membrane formed with SPE-methylene bisacrylamide. The porous membranes illustrate the capability for the present technique to integrate sample cleanup into chip-based analysis systems.

2010-07-13

496

Characterisation and use of biomass fly ash in cement-based materials  

British Library Electronic Table of Contents (United Kingdom)

This paper presents results about the characterisation of the biomass fly ashes sourced from a thermal power plant and from a co-generation power plant located in Portugal, and the study of new cement formulations incorporated with the biomass fly ashes. The study includes a comparative analysis of the phase formation, setting and mechanical behaviour of the new cement-fly ash formulations based on these biomass fly ashes. Techniques such as X-ray diffraction (XRD), X-ray fluorescence spectroscopy (XRF), thermal gravimetric and differential thermal analysis (TG/DTA), X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM) and environmental scanning electron spectroscopy (ESEM) were used to determine the structure and composition of the formulations. Fly ash F1 from the t...

2009-01-01

497

Channelrhodopsin-2 gene transduced into retinal ganglion cells restores functional vision in genetically blind rats  

British Library Electronic Table of Contents (United Kingdom)

To test the hypothesis that transduction of the channelrhodopsin-2 (ChR2) gene, a microbial-type rhodopsin gene, into retinal ganglion cells of genetically blind rats will restore functional vision, we recorded visually evoked potentials and tested the experimental rats for the presence of optomotor responses. The N-terminal fragment of the ChR2 gene was fused to the fluorescent protein Venus and inserted into an adeno-associated virus to make AAV2-ChR2V. AAV2-ChR2V was injected intravitreally into the eyes of 6-month-old dystrophic RCS (rdy/rdy) rats. Visual function was evaluated six weeks after the injection by recording visually evoked potentials (VEPs) and testing optomotor responses. The expression of ChR2V in the retina was investigated histologically. We found that VEPs could not b...

2010-01-01

498

A miniaturized spatial temperature gradient capillary electrophoresis system with radiative heating and automated sample introduction for DNA mutation detection  

British Library Electronic Table of Contents (United Kingdom)

Abstract A miniaturized spatial temperature gradient CE system with automated sample introduction for DNA mutation detection was established. Continuous electrokinetic sample injection was achieved by combining an automated slotted vial array sample introduction device to the spatial temperature gradient CE system. The temperature gradient was produced by a radiative heating system with a single graphite block heater, and the stability of the temperature gradient was investigated. The temperature variation of each measure point was 0.12 0.21% RSD (n=7) within 6 h. A 14 cm Teflon AF coated silica capillary was used both as the separation channel and as the liquid core waveguide tube of fluorescence signal. Under a temperature gradient from 54.8 to 59.5 C, a low range control mutation standa...

2010-01-01

499

A comparison of patient doses in lumbar spine radiography from various X-ray units in Poland  

Energy Technology Data Exchange (ETDEWEB)

A number of diagnostic X-ray units in Poland were subjected to analysis. The air kerma on X-ray tables was measured for the X-ray parameters used routinely during lumbo-sacral spine radiography of standard adult patient. Measurements of air kerma were performed using TLD made of lithium-fluoride. The doses received by patients in different X-ray departments can differ more than two orders of magnitude (from 0.42 mGy up to 72.11 mGy), for the same X-ray examination. The dose can be significantly reduced if fluorescent screens made from components of rare earth are used. (author). 10 refs, 1 fig., 2 tabs.

1995-12-31