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1

Construction of the ATLAS end cap electromagnetic calorimeter and study of its performances; Construction du bouchon du calorimetre electromagnetique d'ATLAS et etudes de ses performances  

Energy Technology Data Exchange (ETDEWEB)

ATLAS is one of the four experiments which will take place at the LHC, the CERN future protons collider. This accelerator, which should start in 2007, will allow to continue the studies carried out by its predecessors, as the standard model Higgs boson and new physics searches. The very high luminosity -10 fb{sup -1} during the first three functioning years, then 100 fb{sup -1}- and the 14 TeV in the frame center will ease these studies. The Centre de Physique des Particules de Marseille took part in the ATLAS collaboration, taking in charge half of the End-cap electromagnetic calorimeter modules construction. The description of this sub-detector and the construction steps, in particular the electrical tests which allow the stacking validation, are presented in this document. These tests results, obtained for the live first production modules, are analysed. The pre-series module (module 0) performances, obtained with beam tests performed at CERN in 1999, are also presented. The ...

2002-09-01

4

Electromagnetic fields, pacemakers and defibrillators; Champs electromagnetiques, cardiostimulateurs et defibrillateurs  

Energy Technology Data Exchange (ETDEWEB)

Presentation of electromagnetic sources constituted by various radio transmitters contributing to different radio communication services in the environment. Results of a measures campaign to assess the electromagnetic field in the close neighbourhood of various stations. Analysis by frequency domains. (author)

2004-07-01

5

Calorimetric studies of the kinetic unfreezing of molecular motions in hydrated lysozyme, hemoglobin, and myoglobin.  

UK PubMed Central (United Kingdom)

Differential scanning calorimetric (DSC) studies of the glassy states of as-received and hydrated lysozyme, hemoglobin, and myoglobin powders, with water contents of < or = 0.25, < or...Full Text Available

1994-01-01

6

Thermal radiation from hot surfaces measured by optical and calorimetric methods. Master's thesis  

Energy Technology Data Exchange (ETDEWEB)

The radiative heat loss from a surface is determined by its total hemispherical emittance, which consequently plays an important role in aerospace and solar applications. This study compares emittances measured calorimetrically with values derived from near normal incidence spectral reflectance measurements. This optical derivation is based on a number of assumptions which limit the accuracy if not sufficiency fulfilled. These assumptions include sample specularity, a straybody character beyond the range of measurement, only small variations of emittance with temperature, and a perfectly smooth sample surface. The comparison of calorimetrically and optically derived emittance performed in this study not only quantifies the errors introduced by insufficient fulfillment of the assumptions but also identifies which assumption causes the dominant error. The calorimetric emissometer, constructed for this study and based on a ...

1982-01-01

7

Optical properties of A-15 thin films and single crystals  

Energy Technology Data Exchange (ETDEWEB)

Optical absorptance spectra of A-15 compounds were taken using a calorimetric technique in the range 0.2 eV to 4.0 eV. Thermomodulation spectra were taken on several A-15 sputtered films.

1980-01-01

8

Optical properties of A-15 thin films and single crystals  

International Nuclear Information System (INIS)

Optical absorptance spectra of A-15 compounds were taken using a calorimetric technique in the range 0.2 eV to 4.0 eV. Thermomodulation spectra were taken on several A-15 sputtered films.

9

Calorimetric and spectroscopic studies of the polymorphic phase behavior of a homologous series of n-saturated 1,2-diacyl phosphatidylethanolamines.  

UK PubMed Central (United Kingdom)

The polymorphic phase behavior of a homologous series of n-saturated 1,2-diacyl phosphatidylethanolamines was investigated by differential scanning calorimetry, 31P-nuclear magnetic resonance, and Fourier...Full Text Available

1993-04-01

10

Electromagnetic compatibility and power quality: engineering contribution; Compatibilite electromagnetique et qualite de l`onde: contribution de l`ingenieur-conseil  

Energy Technology Data Exchange (ETDEWEB)

Problems relating to electromagnetic compatibility and power quality were discussed, combined with a discussion of the role that consulting engineers can play in resolving them. The need for the consulting engineer to be aware of design specifications of equipment was considered essential. Similarly, the interrelationship between installations using variable speed drives, halogenous lighting systems, capacitor banks, high-voltage power lines, power transformers, etc., and the need for familiarity with the operating characteristics of different types of power systems were stressed as key ingredients to success in ascertaining events and causes of equipment failure or power system problems on the network. The main sources of disturbances, impact of voltage variations, the importance of controlling voltage imbalance, and system protection were summarized. 4 figs.

1996-08-01

11

Calorimetric measurements of emittance of pipe surfaces: influence of enclosure diameter, test pipe length, and an argon atmosphere  

Energy Technology Data Exchange (ETDEWEB)

Additional results using a calorimetric technique for measuring the total hemispherical emittance of pipe surfaces from 400 to 600 K are described. Two different Pyrex pipe enclosures were used, one of 15 cm i.d. and the other of 30 cm i.d. An error analysis showed that the larger diameter Pyrex pipe should have a smaller error, but the difference was negligible for the 4.4-cm test pipe diameter used. Measurements on a short length of a previously-measured pipe agreed with earlier measurements, but only over the temperature range of the measurements. While the technique normally uses a vacuum to minimize nonradiative heat transfer, measurements were done succesfully with an argon atmosphere in a closed system. A nickel-plated pipe, measured first in a vacuum and then in an argon atmosphere, allowed calculation of an effective convective heat-transfer coefficient for use with test pipes of unknown emittances. Measurements done with an atmosphere have larger ...

1981-10-01

12

Total hemispherical emittance measured at high temperatures by the calorimetric method  

Energy Technology Data Exchange (ETDEWEB)

A calorimetric vacuum emissometer (CVE) capable of measuring total hemispherical emittance of surfaces at elevated temperatures was designed, built, and tested. Several materials with a wide range of emittances were measured in the CVE between 773 to 923 K. These results were compared to values calculated from spectral emittance curves measured in a room temperature Hohlraum reflectometer and in an open-air elevated temperature emissometer. The results differed by as much as 0.2 for some materials but were in closer agreement for the more highly-emitting, diffuse-reflecting samples. The differences were attributed to temperature, atmospheric, and directional effects, and errors in the Hohlraum and emissometer measurements ({+-} 5 percent). The probable error of the CVE measurements was typically less than 1 percent.

1994-09-01

13

The thermochromic properties of La{sub 1-x}Sr{sub x}MnO{sub 3} compounds  

Energy Technology Data Exchange (ETDEWEB)

La{sub 1-x}Sr{sub x}MnO{sub 3} (LSMO) compounds (0.175{<=}x{<=}0.30) were prepared by conventional solid-state reaction method. Temperature dependence of the total hemispherical emittance ({epsilon}{sub H}) of the compounds from 173 to 373 K was measured on a calorimetric emissometer (CE) which was constructed based on the steady-state calorimetric method. The compounds show thermochromic properties and {epsilon}{sub H}'s have low value at low temperature and have high value at high temperature, because the compounds are dominated by metallic phase and insulator phase, respectively. We use the phase separation model to interpret the temperature dependence of {epsilon}{sub H}. (author)

2008-10-15

14

Calorimetric sensors for energy deposition measurements  

Energy Technology Data Exchange (ETDEWEB)

A calorimetric sensor with several novel design features has been developed. These sensors will provide an accurate sampling of thermal power density and energy deposition from proton beams incident on target components of accelerator-based systems, such as the Accelerator Production of Tritium Project (APT) and the Spallation Neutron Source (SNS). A small, solid slug (volume = 0.347 cc) of target material is suspended by kevlar fibers and surrounded by an adiabatic enclosure in an insulating vacuum canister of stainless steel construction. The slug is in thermal contact with a low-mass, calibrated, 100-k{Omega} thermistor. Power deposition caused by the passage of radiation through the slug is calculated from the rate of temperature rise of the slug. The authors have chosen slugs composed of Pb, Al, and LiAl.

1998-12-31

15

Which neuro-physiologic effects at low level 2.45 GHz RF exposure?; Quels effets neurophysiologiques pour un champ electromagnetique de faible puissance a 2,45 GHz?  

Energy Technology Data Exchange (ETDEWEB)

The LS electromagnetic band (1-4 GHz) is widely used both in domestic and industrial domains. Several studies suggested that the biological systems would exhibit a specific sensitivity to the 2.45 GHz microwaves (water resonance frequency). Potential human health hazards and especially a disruption of the cholinergic system have been reported, due to exposure to microwaves even at low power density. This work presents a multi-parametric study of freely moving rat where neuro-physiology was investigated during 70 hours using neurochemical (micro-dialysis technique), electrophysiological, behavioral (vigilance stages quantification) and thermo-physiological approaches. The rats were exposed 24 hours to a 2.45 GHz pulsed electromagnetic field at low power density. In this exposure conditions, no significant effect have been reported. (authors)

2007-06-15

16

[Experimental and kinetic modeling of acid/base and redox reactions over oxide catalysts  

Energy Technology Data Exchange (ETDEWEB)

The research has involved the characterization of catalyst acidity, [sup 2]D NMR studies of Bronsted acid sites, and kinetic, calorimetric, and spectroscopic studies of methylamine synthesis and related reactions over acid catalysts. Approach of this work was to explore quantitative correlations between factors that control the generation, type, strength, and catalytic properties of acid sites on zeolite catalysts. Microcalorimetry, thermogravimetric analysis, IR spectroscopy, and NMR spectroscopy have provided information about the nature and strength of acid sites in zeolites. This was vital in understanding the catalytic cycles involved in methylamine synthesis and related reactions over zeolite catalysts.

1993-01-01

17

The CTOF measurements and Monte Carlo analyses of neutron spectra for backward direction from iron target irradiated by protons with energies from 400 to 1200 MeV  

CERN Document Server

A calorimetric-time-of-flight (CTOF) technique was used for real-time, high-precision measurement of neutron spectrum at the angle of 175 degrees from the initial proton beam direction, which hits a face plane of a cylindrical iron target of 20 cm in diameter and 25 cm thick. A comparison was performed between the neutron spectra predicted by the MARS and the MCNPX code systems and measured by experiments for 0.4-, 0.6-, 0.8-, 1.0-, and 1.2-GeV protons.

2009-01-01

18

High emittance coverglass  

International Nuclear Information System (INIS)

The authors describe measurements of emittance made on samples of solar cell coverglasses incorporating new coatings both on C-7940 fused silica and on CMX ceria doped microsheet. Samples of a conventional, MgF_2 coating on the same two types of coverglass substrates were included in the measurements as controls. Measurements were made by the calorimetric method of total hemispherical emittance within a cooled chamber as well as by the more common infrared reflectance method. Emittance enhancements from 1 to 4% were measured for the new coatings.

1988-09-26

19

Thermodynamic study of systems with lower critical solution temperatures: H_2O + (C_2H_5)_3N, D_2O + (C_2H_5)_3N  

International Nuclear Information System (INIS)

Molar excess enthalpies and molar excess volumes are reported for the systems H_2O + (C_2H_5)_3N and D_2O + (C_2H_5)_3N at temperatures below and above their lower critical solution temperatures. The molar excess enthalpies are slightly less exothermic for the D_2O system. The molar excess volumes of the H_2O and D_2O systems are within experimental error of one another. Compositions of conjugate solutions estimated from the calorimetric and volumetric measurements agree with those obtained from published liquid-liquid phase diagrams. (Auth.).

1979-01-01

20

Neutrino tagging through secondary beam scraping  

CERN Document Server

We discuss an experimental technique aimed at tagging electron neutrinos in multi-GeV artificial sources on an event-by-event basis. It exploits in a novel manner calorimetric and tracking technologies developed in the framework of the LHC experiments and of rare kaon decay searches. The setup is based on an instrumented decay tunnel equipped with tagging units that intercept secondary and tertiary leptons from the bulk of undecayed pi+ and protons. We show that the taggers are able to reduce the nue contamination originating from K_e3 decays by about one order of magnitude. Only a limited suppression (~60%) is achieved for nue produced by the decay-in-flight of muons; for moderate beam powers, similar performance as for K_e3 can be reached supplementing the tagging system with an instrumented beam dump.

2010-01-01

 
 
 
 
21

Low-temperature radiation polymerization of triethylene glycol. cap alpha. ,. omega. -dimethacrylate. [Gamma radiation  

Energy Technology Data Exchange (ETDEWEB)

Kinetics of postradiation polymerization of triethylene glycol ..cap alpha.., ..omega..-dimethacrylate has been studied by calorimetric method. The low-temperature radiolysis has been studied by ESR method. The radiation-chemical yield of radicals on ..gamma..-irradiation by /sup 60/Co is determined being equal to 6+-1 1/100 ev. Transformation of the radicals spectrum into the spectrum of propagating macroradicals proceeds at 140 K. After the transition from glassy to liquid state (Tsub(g)=193 K) the intensive postpolymerization begins. During the polymerization the disappearance of radicals is observed. For the low-temperature region the effective activation energy of polymerization is determined beina equal to 50.7+-0.8 kJ/mol.

1984-04-01

22

Investigation of the local hardening effect produced by various low-Z materials in a Si/(Fe, Pb) electromagnetic calorimeter  

International Nuclear Information System (INIS)

The condition for obtaining a calorimetric response linear with energy for hadronic showers and an energy resolution that improves as the incident energy increases is the equalization of the electromagnetic (e) and the hadronic (#pi#) signal responses. This equalization is obtained by exploiting a local hardening effect realized through the insertion of low-Z thin plates between the high-Z absorbers and the active material in a hadronic calorimeter with silicon readout. This effect, which allows the reduction of the calorimeter response to the electromagnetic component of the incoming hadronic showers, has been investigated for different low-Z materials. The relevance of some aspects of this study to the radiation hardness of the calorimeters is also addressed. (orig.).

23

High pressure in situ diffraction studies of metal-hydrogen systems  

British Library Electronic Table of Contents (United Kingdom)

''Hybrid'' hydrogen storage, where hydrogen is stored in both the solid material and as a high pressure gas in the void volume of the tank can improve overall system efficiency by up to 50% compared to either compressed hydrogen or solid materials alone. Thermodynamically, high equilibrium hydrogen pressures in metal-hydrogen systems correspond to low enthalpies of hydrogen absorption-desorption. This decreases the calorimetric effects of the hydride formation-decomposition processes which can assist in achieving high rates of heat exchange during hydrogen loading-removing the bottleneck in achieving low charging times and improving overall hydrogen storage efficiency of large hydrogen stores. Two systems with hydrogenation enthalpies close to -20kJ/mol H2 were studied to investigate the h...

2011-01-01

24

Design and operation of an apparatus for calorimetric emittance measurements of pipe surfaces  

Energy Technology Data Exchange (ETDEWEB)

A technique for the measurement of the total hemispherical emittance of pipe surfaces is described, and design and operational details are given. The technique is conceptually simple. A long test pipe (e.g., 3.4 m) is mounted concentrically inside a Pyrex glass pipe. The system is evacuated, and the test pipe is heated by means of an electrical resistance heater. Heat transfer from the test pipe to the enclosure is almost solely radiative, allowing an average emittance for the test pipe and the Pyrex pipe and the electrical power input to the heater. By varying the electrical power level, one can measure the test pipe emittance as a function of temperature. By using a simple correction to account for the finite length of the test pipe, one can calculate the results using the simple expression for infinite, concentric cylinders. Results agree with measurements by reflectance techniques and have a nominal relative error of less than 10%.

1981-10-01

25

Apparatus for total hemispherical emittance measurements of full-scale receiver pipes from 100 to 300 C  

Energy Technology Data Exchange (ETDEWEB)

An apparatus is described for measuring the total hemispherical emittance of pipes of a length suitable for use in a prototype solar collector. The calorimetric method used requires measurements of the temperatures of the surface of the test pipe and of a concentric outer cylinder and measurement of the electrical power used to heat the test pipe. Measurements were made of the total hemispherical emittance of black chrome, nickel, and bare steel pipes as a function of temperature. The emittance of the black chrome surfaces increased significantly from an extrapolated value of about 0.1 at 25 deg C to values on the order of 0.3-0.4 at 300 deg C. The extrapolated values for black chrome agreed with measurements made using other techniques at room temperature. The results for the nickel-plated pipe agreed with total emittance calculated from spectral reflectance data.

1981-01-01

26

Study of the Photon Strength Functions for Gadolinium Isotopes with the DANCE Array  

Science.gov (United States)

The gadolinium isotopes are interesting for reactor applications as well as for medicine and astrophysics. The gadolinium isotopes have some of the largest neutron capture cross sections. As a consequence they are used in the control rod in reactor fuel assembly. From the basic science point of view, there are seven stable isotopes of gadolinium with varying degrees of deformation. Therefore they provide a good testing ground for the study of deformation dependent structure such as the scissors mode. Decay gamma rays following neutron capture on Gd isotopes are detected by the DANCE array, which is located at flight path 14 at the Lujan Neutron Scattering Center at Los Alamos National Laboratory. The high segmentation and close packing of the detector array enable gamma-ray multiplicity measurements. The calorimetric properties of the DANCE array coupled with the neutron time-of-flight technique enables one to gate on a specific resonance of a specific isotope in ...

2009-03-10

27

Performance of the AMS-02 Experiment for High Energy Gamma Ray Astrophysics  

CERN Document Server

AMS is a particle detector designed to perform high precision measurements of the cosmic rays fluxes with the main goals of searching for anti-nuclei, as remnants of primordial anti-matter, and of measuring the faintest components of the cosmic flux, anti- protons, positrons and high energy photons. To fulfill the requirements of large acceptance, long exposure time and excellent particle identification needed to achieve the intended results, AMS will operate in space as an attached payload to the International Space Station (ISS), being the first full featured particle physics experiment to operate in the Earth orbit. The AMS-02 accurate measurements of cosmic-ray nuclei, protons, antiprotons, electrons and positrons will be completed by high energy gamma rays detection. The experiment will detect gamma-rays, either by reconstructing e+e? pairs generated by photons converted upstream the tracker (conversion mode), or based on direct identification of electromagnetic showers in ECAL ...

2007-01-01

28

Fabrication, structure and consolidation of NiAl-Al_2O_3 mechanically alloyed nanocomposite powders  

International Nuclear Information System (INIS)

Reactive milling of NiO + Al powder mixture resulted in the formation of NiAl-Al_2O_3 nanocomposite powders, with a crystallite size of about 20 nm. The Hall-Williamson analysis revealed that NiAl showed an orientation dependent crystallite size after short processing time and orientation dependent internal strain after long milling time. Both anisotropies were removed by heating the powders in the differential scanning calorimetry. Calorimetric studies showed one exothermic effect attributed to the reduction reaction of NiO and endothermic one associated with melting of Al. Two methods were applied for powders compaction: resistance sintering and pulse electric discharge. In both cases the densities of abut 90% of the theoretical value were achieved. A significant increase in average NiAl crystallites size in compacted samples was observed, up to several hundreds of nanometers.(author)

2001-09-23

29

Automatic Gamma-Scanning System for Measurement of Residual Heat in Spent Nuclear Fuel  

International Nuclear Information System (INIS)

In Sweden, spent nuclear fuel will be encapsulated and placed in a deep geological repository. In this procedure, reliable and accurate spent fuel data such as discharge burnup, cooling time and residual heat must be available. The gamma scanning method was proposed in earlier work as a fast and reliable method for the experimental determination of such spent fuel data. This thesis is focused on the recent achievements in the development of a pilot gamma scanning system and its application in measuring spent fuel residual heat. The achievements include the development of dedicated spectroscopic data-acquisition and analysis software and the use of a specially designed calorimeter for calibrating the gamma scanning system. The pilot system is described, including an evaluation of the performance of the spectrum analysis software. Also described are the gamma-scanning measurements on 31 spent PWR fuel assemblies performed using the pilot system. The results obtained for the determination ...

30

Automatic Gamma-Scanning System for Measurement of Residual Heat in Spent Nuclear Fuel  

Energy Technology Data Exchange (ETDEWEB)

In Sweden, spent nuclear fuel will be encapsulated and placed in a deep geological repository. In this procedure, reliable and accurate spent fuel data such as discharge burnup, cooling time and residual heat must be available. The gamma scanning method was proposed in earlier work as a fast and reliable method for the experimental determination of such spent fuel data. This thesis is focused on the recent achievements in the development of a pilot gamma scanning system and its application in measuring spent fuel residual heat. The achievements include the development of dedicated spectroscopic data-acquisition and analysis software and the use of a specially designed calorimeter for calibrating the gamma scanning system. The pilot system is described, including an evaluation of the performance of the spectrum analysis software. Also described are the gamma-scanning measurements on 31 spent PWR fuel assemblies performed using the pilot system. The results obtained for the determination ...

2007-03-15

31

An enzyme-amplified microtiter plate assay for ethanol: Its application to the detection of peanut ethanol and alcohol dehydrogenase  

Energy Technology Data Exchange (ETDEWEB)

A calorimetric microliter plate assay for ethanol amplified by aldehyde dehydrogenase (ALDH) was developed. In the assay ethanol from a sample took part in a chain-reaction catalyzed by alcohol dehydrogenase (ADH) and amplified by ALDH in the presence of NAD{sup +}, diaphorase, and p-ibdonitrotetrazolium-violet (INT-violet)(a precursor of red product). The resultant reaction gave a red color, the intensity of which was proportional to the amount of ethanol present. Using the technique, the content of activity from peanuts of differing maturity and curing stages were determined respectively. Data showed that immature peanuts had a higher level of ethanol and a lower ADH activity than mature peanuts, and that the level of ethanol and ADH activity decreased with the curing time. This indicates that peanut maturity and curing have an effect on ethanol. Also, this implies that other peanut volatiles could be affected in the same way as ethanol, a major volatile in ...

1995-12-01

32

Two-gigawatt burst-mode operation of the intense microwave prototype (IMP) free-electron laser (FEL) for the microwave tokamak experiment (MTX)  

Energy Technology Data Exchange (ETDEWEB)

The MTX explored the plasma heating effects of 140 GHz microwaves from both Gyrotrons and from the IMP FEL wiggler. The Gyrotron was long pulse length (0.5 seconds maximum) and the FEL produced short-pulse length, high-peak power, single and burst modes of 140 GHZ microwaves. Full-power operations of the IMP FEL wiggler were commenced in April of 1992 and continued into October of 1992. The Experimental Test Accelerator H (ETA-II) provided a 50-nanosecond, 6-MeV, 2--3 kAmp electron beam that was introduced co-linear into the IMP FEL with a 140 GHz Gyrotron master oscillator (MO). The FEL was able to amplify the MO signal from approximately 7 kW to peaks consistently in the range of 1--2 GW. This microwave pulse was transmitted into the MTX and allowed the exploration of the linear and non-linear effects of short pulse, intense power in the MTX plasma. Single pulses were used to explore and gain operating experience in the parameter space of the IMP FEL, and finally evaluate ...

1993-10-06

33

Structural, morphological and surface chemical features of Al{sub 2}O{sub 3} catalyst supports stabilized with CeO{sub 2}  

Energy Technology Data Exchange (ETDEWEB)

Two families of CeO{sub 2}/Al{sub 2}O{sub 3} (ACE) catalyst supports, containing 3 and 20 % wt CeO{sub 2} respectively, have been examined and compared with the pure oxides CeO{sub 2} and (transition-phase) Al{sub 2}O{sub 3}. Structural data indicate that, also in the presence of CeO{sub 2}, the Al{sub 2}O{sub 3} support undergoes all phase transitions at the usual temperatures. Electron micrographs show that particles morphology and crystals size are mainly imposed by the Al{sub 2}O{sub 3} support. The porosimetric texture indicates a more pronounced meso-porosity in the ACE systems than in pure Al{sub 2}O{sub 3}, especially in the case of low CeO{sub 2} loadings. FTIR spectra and volumetric/calorimetric data of the adsorption of CO at {approx}300 K show that the surface Lewis acidity of aluminas is severely modified by the presence of CeO{sub 2}: the overall CO uptake is increased, there is the formation of one additional family of Lewis acid sites (Ce{sup 4+} ...

1995-12-31

34

Optical absorptance and thermomodulation studies of several A-15 compounds  

Energy Technology Data Exchange (ETDEWEB)

The purpose of this work was to investigate the optical properties of several high T/sub c/ compounds in the form of sputtered films. The measurements are used toward this end: optical absorptance (using a calorimetric technique near 4.2K), which yields (after Kramers-Kronig analysis) the complex dielectric function, and thermoreflectance (which measures the change in reflectance in the optical range when a 1 to 10/sup 0/K temperature wave is applied), performed at two ambient temperatures (80 and 300/sup 0/K), yielding the differential dielectric function. The sputtered films included Nb/sub 3/Ge, Nb/sub 3/Al, V/sub 3/Ga and Nb/sub 3/Ir. It is noted that Nb/sub 3/Ir is not a high T/sub c/ superconductor. The thermoreflectance on the bulk samples V/sub 3/Si, V/sub 3/Ge and single crystal Cr/sub 3/Si were not performed because the samples were not in the form of thin films. The thermomodulation studies are correlated with the absorptance measurements in comparison ...

1983-06-01

35

Optical absorptance and thermomodulation studies of several A-15 compounds  

International Nuclear Information System (INIS)

The purpose of this work was to investigate the optical properties of several high T/sub c/ compounds in the form of sputtered films. The measurements are used toward this end: optical absorptance (using a calorimetric technique near 4.2K), which yields (after Kramers-Kronig analysis) the complex dielectric function, and thermoreflectance (which measures the change in reflectance in the optical range when a 1 to 10_0K temperature wave is applied), performed at two ambient temperatures (80 and 300_0K), yielding the differential dielectric function. The sputtered films included Nb"3Ge, Nb"3Al, V"3Ga and Nb"3Ir. It is noted that Nb"3Ir is not a high T/sub c/ superconductor. The thermoreflectance on the bulk samples V"3Si, V"3Ge and single crystal Cr"3Si were not performed because the samples were not in the form of thin films. The thermomodulation studies are correlated with the absorptance measurements in comparison to band structure calculations. When ...

36

Design of spacecraft thermal control materials on polyimide film; Polyimide film ni yoru uchuyo netsuseigyo zairyo no kaihatsu  

Energy Technology Data Exchange (ETDEWEB)

Two types of thermal control materials based on polyimide film UPILEX-R are designed. One of thermal control material R/Al is coated with Al on the back surface. The other of thermal control material TCC/R/Al is coated with transparent conductive coating on the font surface and is coated with Al on the balk surface. The solar absorptance is measured spectroscopically with an integrating sphere in the wavelength region of 0.26 - 2.50 {mu}m and the total hemispherical emittance is measured calorimetrically in the temperature range of -100-+100{degree}C for the present thermal control materials. To evaluate the space degradation of optical properties (refractive index, extinction coefficient, absorption coefficient) on UPILEX-R film and solar absorptance on thermal control materials, space environment simulation tests are performed on the ground with independent radiation and combined radiation by UV, electrons, and protons. An onboard simultaneous measurement ...

1996-01-20

37

A low-temperature calorimetric study of synthetic (forsterite+fayalite) {(Mg2SiO4+Fe2SiO4)} solid solutions: An analysis of vibrational, magnetic, and electronic contributions to the molar heat capacity and entropy of mixing  

International Nuclear Information System (INIS)

The molar heat capacities (Cp,m) of a series of synthetic forsterite (Fo)-fayalite (Fa), (Mg2SiO4+Fe2SiO4), olivines have been measured between 5K and 300K on milligram-sized samples with the Physical Properties Measurement System (Quantum Design(R)). Sharp, ?-type heat capacity anomalies are observed in the Fe-rich compositions fayalite, Fo10Fa90, Fo20Fa80, Fo30Fa70, and Fo40Fa60. The corresponding Neel temperatures TN decrease linearly from 64.5K in fayalite to 32.8K in Fo40Fa60 following the relationship TN=79.02.xFa-14.07. Fo50Fa50 and Mg-richer olivines show weak broad features in the heat capacity data around 15K to 20K that decrease in magnitude with increasing forsterite content. In order to derive and separate molar electronic, magnetic and vibrational heat capacity contributions, Cel,m, Cmag,m, and Cvib,m from the experimental heat capacities (Ctot,m), we used a single-parametric phonon dispersion model to calculate Cvib,m for the solid-solution members and fayalite. The ...

2007-06-01