WorldWideScience
1

Physical characteristics and solubility of long-lived airborne particulates in uranium producing and manufacturing facilities: A report upon completion of the extension to Phase I of the study. Research report No. INFO-0363-1  

Energy Technology Data Exchange (ETDEWEB)

Study of the rate of dissolution in simulated lung fluid of uranium from 3 different ore matrices and from refined uranium dioxide in an essentially all teflon extraction apparatus; the rate of dissolution of thorium from a nickel metal/2 percent thoria mixture; the effect of neutron irradiation of the studied materials upon the dissolution rates; and the adsorptions of the radioisotope tracers barium 133 (substitute for radium), lead 203 and thorium 234 upon the extraction system components.

1989-01-01

2

Property and Microstructural Nonuniformity in the Yttrium-Barium ...  

Science.gov (United States)

Pore Fraction in Yttrium-Barium-Copper-Oxide and. Other Polycrystalline. Materials ...... Properties of Yttrium Ceramic. Sov. J. LowTemp.Phys. 14:395-402 . ...

3

Chemistry of strontium  

International Nuclear Information System (INIS)

This paper describes stable strontium as composed of four stable isotopes ( Sr 88, Sr 87, Sr 86, and Sr 84), of which Sr 88 contributes more than 82% to its composition. Strontium exists in three crystalline, plymorphic forms; face-centered cubic alpha form, hexagonal beta form and body-centered cubic gamma form. Strontium occupies in many physicochemical aspects an intermediate position between calcium and barium, as does the solubility of strontium salts. As a result of its oxidation potential, strontium readily forms oxides, halides, and sulfide. The author proposes that the slight discrimination against strontium incorporation into bony tissues may be due to the difference in ionic potential (14%) between strontium and calcium. Ionic potential is an indicator of the strength of ionic bonds: strontium has a smaller ratio of ionic charge to ionic radius when compared with calcium.

4

Superconducting Properties of Epitaxial Yttrium BARIUM(2) COPPER(3) OXYGEN(7-DELTA) Thin Films and Yttrium BARIUM(2) COPPER(3) OXYGEN(7-DELTA)/PRASEODYMIUM BARIUM(2) COPPER(3) OXYGEN(7-Z)/YTTRIUM BARIUM(2) COPPER(3) OXYGEN(7 - Heterostructures Grown by Pulsed Laser Deposition  

Science.gov (United States)

The study of the intrinsic behavior of high transition temperature copper-oxide superconductors (HTSC) has proven to be challenging because of the extreme sensitivity of their transport properties on material quality. These compounds are characterized by a high degree of structural and electrical anisotropy, and a very short superconductive coherence length of the same order as the size of the crystalline unit cell (~5-30 A). As a result, microscopic defects such as oxygen vacancies, cationic disorder, and the presence of minute impurities have a significant effect on electrical transport in these materials. Therefore, much effort has been expended in synthesizing sizable samples that are homogeneous, well characterized, and emenable to the study of the anisotropic properties of the HTSC. We have demonstrated that thin films of HTSC compounds such as rm YBa_2Cu_3O_{7 -delta}, which is a 92 K superconductor, can be synthesized easily by a technique known as pulsed laser deposition, and ...

1992-01-01

7

Addition of methyl cellulose enema to double-contrast barium imaging of sigmoid diverticulosis  

Energy Technology Data Exchange (ETDEWEB)

Double-contrast barium enema has a reduced sensitivity in patients with severe sigmoid diverticulosis. Therefore a carboxy methyl cellulose enema was employed after the conventional double-contrast examination in 15 patients with sigmoid diverticulosis. A significant increase in lumen diameter and a superior removal of barium residue from the diverticulas facilitated the interpretation of the sigmoid loops. Conclusion: The addition of methyl cellulose enema to double-contrast barium imaging improves diagnostic imaging in diverticulosis by expanding the lumen and emptying the diverticulas. (orig.).

1997-01-01

8

Photoexcitation and optical pumping in a barium atomic beam  

International Nuclear Information System (INIS)

An apparatus allowing the photoexcitation of barium atomic beam over its whole surface is described. This photoexcitation is achieved by another barium spectrum emitted up steam of the beam by a cathodic out-flow produced at the exit oven. The fluorescence spectrum is studied in detail as well as the influence of different parameters, such as oven temperature, current intensity of the outflow, and excitation depth. A calculation shows how to determine Einstein coefficient, oscillator strengths and atomic lifetimes from our experimental measurements.

9

Trichoderma-fortified compost extracts for the control of choanephora wet rot in okra production  

British Library Electronic Table of Contents (United Kingdom)

The potential of water extracts produced from rice straw (RST) and empty fruit bunch of oil palm (EFB) composts fortified with Trichoderma harzianum for the control of Choanephora wet rot of okra caused by Choanephora cucurbitarum was studied under field conditions. Disease severity was lowest in plants treated with Trichoderma-fortified RST extracts (9.56%) with a disease index of 1, mancozeb (Dithane M-45 (2gl-1 of water), Trichoderma-fortified EFB compost extracts, extracts of RST and EFB, and an aqueous suspension of T. harzianum recorded disease severity values of 10.25%, 19.38%, 37.56%, 53.71% and 56.36%, with a disease index of 1, 1, 2, 3 and 3, respectively. There was a reduction of 85.04% in Choanephora wet rot severity on okra treated with Trichoderma-fortified RST extracts durin...

2008-01-01

10

Attenuation of heavy metal leaching from hazardous wastes by co-disposal of wastes  

Energy Technology Data Exchange (ETDEWEB)

The potential hazard of landfill wastes was previously evaluated by examining the extraction procedures for individual waste, although various wastes were co-disposed of in actual landfills. This paper investigates the reduction of extraction-procedure toxicity by co-disposing various combinations of two wastes. When two wastes are mixed homogeneously, the extraction of heavy metals from the waste mixture is critically affected by the extract pH. Thus, co-disposal wastes will have a resultant pH between the pH values of its constituent. The lower the resultant pH, the lower the concentrations of heavy metals in the extract. When these wastes are extracted sequentially, the latter extracted waste has a stronger influence on the final concentration of heavy metals in the extract. Small-scale lysimeter ...

1996-12-31

11

Oral administration of purple passion fruit peel extract attenuates blood pressure in female spontaneously hypertensive rats and humans  

British Library Electronic Table of Contents (United Kingdom)

Hypertension is one of the most important modifiable risk factors for cardiovascular and cerebrovascular diseases. We investigated the potential antihypertensive effect of the purple passion fruit peel (PFP) extract, a mixture of bioflavonoids, phenolic acids, and anthocyanins, in spontaneously hypertensive rats and human. A high-performance liquid chromatography analysis was performed to identify the active ingredients of the PFP extract. In a rat liver toxicity assay, no hepatotoxicity was observed after 9 hours incubation in the presence of PFP extract (20 ?g/mL). The PFP extract also revealed hepatoprotection against chloroform (1 mmol/L)-induced liver injury. In the experimental model, 24 spontaneously hypertensive rats were divided into 3 treatment groups for a period of 8weeks: cont...

2007-01-01

12

Solvent extraction of well defined astatine species  

International Nuclear Information System (INIS)

During solvent extraction of At"-, [At(H_2O)_2]"+, AtCl, AtCl_2"- as well as of astatine compounds with higher oxidation states like AtO_n"-, the astatine species are changed into astatine of the oxidation state zero at the phase boundary independent on the organic solvent used. At(O) probably reacts with components of the organic phase or with decomposition products formed by chemical reactions or by radiolysis. The extraction coefficients of the astatine species depend on the experimental conditions applied, the redox potential, and on complex forming reactions or associations, resp., occuring in the aqueous phase. (author).

13

BARIUM RELEASES at ALTITUDES BET\\VEEN 200 and 1000 - NASA ...  

Science.gov (United States)

Zinn, John;. Hoerlin,. Herman; and Petschek,. Albert. G.: The Motion of Bomb. Debris. Following the Starfish. Test. Radiation. Trapped in the Earth's ...

15

A DETAILED SAFETY ASSESSMENT OF A SAW PALMETTO EXTRACT  

UK PubMed Central (United Kingdom)

BackgroundSaw palmetto is commonly used by men for lower urinary tract symptoms. Despite its widespread use, very little is known about the potential toxicity of...Full Text Available

2008-06-01

16

Strong-Weak Coupling Duality in Quantum Mechanics  

CERN Document Server

We present a strong-weak coupling duality for quantum mechanical potentials. Similarly to what happens in quantum field theory, it relates two problems with inverse couplings, leading to a mapping of the strong coupling regime into the weak one, giving information from the nonperturbative region of the parameters space. It can be used to solve exactly power-type potentials and to extract deep information about the energy spectra of polynomial ones. We present a strong-weak coupling duality for quantum mechanical potentials. Similarly to what happens in quantum field theory, it relates two problems with inverse couplings, leading to a mapping of the strong coupling regime into the weak one, giving information from the nonperturbative region of the parameters space. It can be used to solve exactly power-type potentials and to extract deep information about the ...

1996-01-01

17

Antitumor and Antiviral Activity of Colombian Medicinal Plant Extracts  

Scientific Electronic Library Online (English)

Abstract in english Extracts of nine species of plants traditionally used in Colombia for the treatment of a variety of diseases were tested in vitro for their potential antitumor (cytotoxicity) and antiherpetic activity. MTT (Tetrazolium blue) and Neutral Red colorimetric assays were used to evaluate the reduction of viability of cell cultures in presence and absence of the extracts. MTT was also used to evaluate the effects of the extracts on the lytic activity of herpes simplex virus type (more) 2 (HSV-2). The 50% cytotoxic concentration (CC50) and the 50% inhibitory concentration of the viral effect (EC50) for each extract were calculated by linear regression analysis. Extracts from Annona muricata, A. cherimolia and Rollinia membranacea, known for their cytotoxicity were used as positive controls. Likewise, acyclovir and heparin were used as positive ...

1999-07-01

18

SU(2) potentials in quantum gravity  

CERN Document Server

We present investigations of the potential between static charges from a simulation of quantum gravity coupled to an SU(2) gauge field on 6^{3}\\times 4 and 8^{3}\\times 4 simplicial lattices. In the well-defined phase of the gravity sector where geometrical expectation values are stable, we study the correlations of Polyakov loops and extract the corresponding potentials between a source and sink separated by a distance R. In the confined phase, the potential has a linear form while in the deconfined phase, a screened Coulombic behavior is found. Our results indicate that quantum gravitational effects do not destroy confinement due to non-abelian gauge fields.

1994-01-01

19

Reactivity of ceramic superconductors with palladium alloys  

Science.gov (United States)

This paper reports Palladium alloy compositions investigated for suitability as a nonreactive material for the processing of ceramic superconductors. Barium-based superconductors were tested on Pd-Au and Pd-Ag alloys for reactivity. Bismuth-based superconductors were tested on a Pd-Ag alloy. The least reactive was found to be 70% Pd-30% Ag for the barium-based high-temperature superconductors (HTSC), whereas 30% Pd-70% Ag was found to be least reactive for bismuth-based HTSC.

1990-06-01

20

Raney-platinum film electrodes for potentially implantable glucose fuel cells. Part 1: Nickel-free glucose oxidation anodes  

British Library Electronic Table of Contents (United Kingdom)

We present a novel fabrication route yielding Raney-platinum film electrodes intended as glucose oxidation anodes for potentially implantable fuel cells. Fabrication roots on thermal alloying of an extractable metal with bulk platinum at 200^oC for 48h. In contrast to earlier works using carcinogenic nickel, we employ zinc as potentially biocompatible alloying partner. Microstructure analysis indicates that after removal of extractable zinc the porous Raney-platinum film (roughness factor ~2700) consists predominantly of the Pt3Zn phase. Release of zinc during electrode operation can be expected to have no significant effect on physiological normal levels in blood and serum, which promises good biocompatibility. In contrast to previous anodes based on hydrogel-bound catalyst particles the ...

2010-01-01

21

Activation of rapid signaling pathways and the subsequent transcriptional regulation for the proliferation of breast cancer MCF-7 cells by the treatment with an extract of Glycyrrhiza glabra root.  

Science.gov (United States)

Glycyrrhiza glabra root is one of the common traditional Chinese medicines and used as flavoring and sweetening agents for tobaccos, chewing gums, candies, toothpaste and beverages. While glycyrrhizin is one of the main components in the extract of G. glabra root and has been characterized, the other components have not been well characterized. The mechanism of growth activation of breast cancer MCF-7 cells, including the activation of Erk1/2 and Akt, and the transcriptional regulation of estrogen-responsive genes, was examined by means of sulforhodamine B, luciferase reporter gene, real-time RT-PCR and Western blotting assays after the induction of the cells with the extract of G. glabra root. The extract has similar activity to that induced by 17beta-estradiol (E(2)), although glycyrrhizin did not show such an activity. Moreover, the estrogen receptor alpha-dependent neurite outgrowth induced by the ...

2007-06-24

22

Measurement of achievable plutonium decontamination from gallium by means of Purex solvent extraction  

Energy Technology Data Exchange (ETDEWEB)

Gallium is present in surplus weapons-grade plutonium (WG-Pu) at a concentration of approximately 1 wt %. Plans are to dispose of surplus WG-Pu by converting it to UO{sub 2}-PuO{sub 2} mixed oxide (MOX) fuel and irradiating it in commercial power reactors. However, the presence of high concentrations of gallium in plutonium poses a potential corrosion problem during the process of MOX fuel irradiation. The batch experiments performed in this study were designed to measure the capability of the PUREX solvent extraction process to separate gallium from plutonium under idealized conditions. Radioactive tracing of the gallium with {sup 72}Ga enabled the accurate measurement of low concentrations of extractable gallium. The experiments approximated the proposed flowsheet for WG-Pu purification, except that only one stage was used for each process: extraction, scrubbing, and stripping. The gallium ...

2000-07-01

23

Intermediate mass Higgs study at {gamma}{gamma} colliders  

Energy Technology Data Exchange (ETDEWEB)

We present the efficient technique to extract the signal of the intermediate mass Higgs boson from the backgrounds at future {gamma}{gamma} colliders. For a clear Higgs detection, it is important to fit the original electron accelerator energy depending on the Higgs mass, to set the polarization of the photon beams and to apply the efficient b quark tagging method. we demonstrate the extraction of information of Higgs parameters and the new physics from the observable physical quantities. It is clearly shown that a future {gamma}{gamma} collider will have a rich potential for study on the new physics, as well as the Higgs physics. (author).

1995-05-01

24

Intermediate mass Higgs study at #gamma##gamma# colliders  

International Nuclear Information System (INIS)

We present the efficient technique to extract the signal of the intermediate mass Higgs boson from the backgrounds at future #gamma##gamma# colliders. For a clear Higgs detection, it is important to fit the original electron accelerator energy depending on the Higgs mass, to set the polarization of the photon beams and to apply the efficient b quark tagging method. we demonstrate the extraction of information of Higgs parameters and the new physics from the observable physical quantities. It is clearly shown that a future #gamma##gamma# collider will have a rich potential for study on the new physics, as well as the Higgs physics. (author).

1995-05-01

25

Physicochemical investigation of the behavior of elements in chloride melts in the presence of solid phases based on phosphates of polyvalent elements. II. Behavior of strontium and barium  

Energy Technology Data Exchange (ETDEWEB)

The distribution of the alkaline earth elements strontium and barium between the solid phases of phosphates of transition elements of group 4 and chloride melts was studied. The distribution coefficients of strontium and barium were found at T = 700-800/sup 0/C. Phosphates of the type NaM/sub 2//sup (IV)/(PO/sub 4/)/sub 3/, where M/sub (IV)/ represents titanium, zirconium, and hafnium, were used as the solid phases. It was established that there is an enrichment of the precipitates with the distributed components. The distribution coefficient depends on the nature of the solid phase and the temperature. It was suggested that M/sup (II)/ x M/sub 4//sup (IV)/(PO/sub 4/)/sub 6/ is formed in processes of distribution, where M/sup (II)/ represents Sr, Ba.

1987-07-01

26

Inhibition of barium sulfate deposition by polycarboxylates of various molecular structures  

Energy Technology Data Exchange (ETDEWEB)

To establish a relationship between the molecular structure of polycarboxylates and their growth-retarding influence on barium sulfate, seeded-suspension-growth experiments were performed at various inhibitor concentrations and pH values. Two types of polycarboxylates with a molecular structure based on their polyacrylic or maleic acid were studied. The molecular structure of these compounds were varied by particle substitution with monomers containing hydroxyl, amide, and sulfonic acid, as well as hydrophobic groups. Hydrophobic groups are detrimental to good inhibitor performance, whereas the introduction of OH, NH {sub 2}, or SO {sub 3} H groups presents opportunities to enhance the inhibitor effectiveness. The sequence in performance of the compounds on barium sulfate was compared with the sequence formerly obtained for calcium sulfate dihydrate.

1990-02-01

27

Coupling of magnetostriction and electrostriction in the porous rheological composite  

Energy Technology Data Exchange (ETDEWEB)

The production method of the elastic composite containing ferrous particles and titanium barium particles dispersed in the porous silicone matrix is described in this article. Since it contains ferrous and titanium barium particles, this composite shows magnetorheological and also electrorheological properties. The electrostriction of composite samples in the electric field with maximal intensity 1.5x10{sup 6} V/m was investigated. The magnetostriction in the magnetic field with maximal induction 1 T was also investigated. It was found that samples elongate with increased electric field intensity, and the magnetic field induction was detected. By increasing the samples' elongation with increase of ferrous particles, titanium barium particles and pores number were also detected. In the investigated division of the electric and magnetic field the elongation changed in a linear way. The maximal elongation achieved was ...

2008-08-15

28

Study on the low-lying collective states of A=54-124 nuclei in 50 MeV #alpha#-particle scattering and in the "6"4Ni("3He, "3He') reaction by DWBA and coupled channel method  

International Nuclear Information System (INIS)

The analysis of elastic and inelastic scattering of #alpha# particles with energy of 50 MeV by nuclei with mass numbers A=54-124 and of "3He particles by the nucleus "6"4Ni is given in the framework of the optical model. The parameters of multipole deformations for lower states are determined. The parameters for quadrupole and octupole deformations of the potential for the nucleus "1"1"2Sn are extracted, the values of the hexadecupole deformation #beta#_4 of the potential for nuclei "9"4Zr, "1"2"0","1"2"4Sn are found. Information is extracted on the ratio of deformation parameters for the neutron and proton components in lower collective states (2_1"+, 3_1"-) of nuclei with A=90-124.

29

Selection of Inhibitor-Resistant Viral Potassium Channels Identifies a Selectivity Filter Site that Affects Barium and Amantadine Block  

UK PubMed Central (United Kingdom)

BackgroundUnderstanding the interactions between ion channels and blockers remains an important goal that has implications for delineating the basic mechanisms of ion channel function...Full Text Available

30

Relationships between Film Chemistry, Structure, and Mechanical Properties in Titanium Oxide  

Energy Technology Data Exchange (ETDEWEB)

Titanium oxides were grown anodically to selected final potentials on grade II polycrystalline titanium under different anodization rates. XPS and RBS results show that the oxide consists of primarily TiO2 with a non-stoichiometric oxide/metal interface, with the slower growth rate associated with a thicker layer at the interface. Characterization using TEM reveals that the structure of the oxide evolves from a primarily amorphous phase to islands of crystallites in an amorphous matrix, to an entirely crystalline phase by increasing the polarization potential. Slower growth rates tend to remain crystalline at higher potentials. The mechanical strength of oxide films extracted from load-depth data by nanoindentation varies dramatically for oxide films grown by different rates at 9.4 V, and to a lesser extent at lower potentials. The variation of film strength is associated with both ...

2001-01-01

31

Computer simulation of interface potentials: Towards a first principle description of complex interfaces?  

British Library Electronic Table of Contents (United Kingdom)

We discuss the feasibility of a hierarchical protocol whereby the description and prediction of adsorbed fluids in confined systems at the mesoscopic scale is achieved by use of interface potentials that are obtained from raw molecular simulation data. Starting from a microscopic description of a fluid?s interface on a flat substrate, we attempt to extract the minimum information that is required in order to predict the behavior of that fluid at larger length scales from coarse grained surface Hamiltonians. A critical assessment of this procedure hinges on controversial aspects of wetting behavior and more generally on the meaning of metastability and instability of thermodynamic systems.

2011-01-01

32

Acid corrosion inhibition of copper by mangrove tannin  

British Library Electronic Table of Contents (United Kingdom)

Purpose - The purpose of this paper is to evaluate the corrosion inhibition potential of mangrove (Rhizopora apiculata) tannin in hydrochloric acid medium on copper with the view of developing a natural corrosion inhibitor. Design/methodology/approach - The mangrove tannin was extracted from the mangrove bark and its anticorrosion potential was studied by weight loss, electrochemical and scanning electron microscopy (SEM) analysis. Findings - It has been found that the mangrove tannin effectively inhibits the corrosion on copper metal in hydrochloric acid solution. The results of the electrochemical and weight loss methods showed that the inhibition efficiency of mangrove tannin increases with increasing its concentration. Inhibition is achieved through the adsorption of tannin molecules o...

2011-01-01

33

104 MeV alpha particle scattering from /sup 90/,/sup 92/Zr  

Energy Technology Data Exchange (ETDEWEB)

Differential cross sections have been measured for the elastic and inelastic scattering of 104 MeV alpha-particles from /sup 90/,/sup 92/Zr. The experimental data are analyzed in terms of coupled channels on the basis of a flexible anharmonic vibrator model and using different parametrizations of the radial shape of the extended optical potential. The results favour the squared Saxon-Woods type for the real part. Additionally to a radial momentum analysis of the real potentials a semimicroscopic folding model has been invoked for extracting isoscalar quadrupole and hexadecapole transition rates.

1982-05-01

34

104 MeV alpha particle scattering from "9"0,"9"2Zr  

International Nuclear Information System (INIS)

Differential cross sections have been measured for the elastic and inelastic scattering of 104 MeV alpha-particles from "9"0,"9"2Zr. The experimental data are analyzed in terms of coupled channels on the basis of a flexible anharmonic vibrator model and using different parametrizations of the radial shape of the extended optical potential. The results favour the squared Saxon-Woods type for the real part. Additionally to a radial momentum analysis of the real potentials a semimicroscopic folding model has been invoked for extracting isoscalar quadrupole and hexadecapole transition rates. (orig.).

35

Polyphenol rich botanicals used as food supplements interfere with EphA2-ephrinA1 system  

British Library Electronic Table of Contents (United Kingdom)

The Eph tyrosine kinase receptors and their ephrin ligands play a central role in several human cancers and their deregulated expression or function promotes tumorigenesis, inducing aggressive tumor phenotypes. Green tea extracts (GTE) have been recently found to inhibit Eph-kinase phosphorylation. In order to evaluate the potential contribution of edible and medicinal plants on EphA2-ephrinA1 modulation, 133 commercially available plant extracts used as food supplements, essential and fixed oils were screened with an ELISA-based binding assay. Nine plant extracts, rich of polyphenols, reversibly inhibited binding in a dose-dependent manner (IC"5"0 0.83-24@mg/ml). Functional studies on PC3 prostate adenocarcinoma cells revealed that active extracts antagonized ephrinA1-Fc-induced EphA2-pho...

2011-01-01

36

Deformed-coal structure and control to coal-gas outburst  

Energy Technology Data Exchange (ETDEWEB)

Based on techniques of organic solvent extraction and a thermal model experiments of coal-related hydrocarbon, the variation of coal structure and the character of deformed coal-related hydrocarbons were studied when the coal seam at Piagdingshan mine, China was modified by tectonic stress. The results show that the extraction ratio by n-hexane and benzene from the deformed coal approaches that form normal coal, but the extraction ratio by chloroform from the deformed coal is two times more than that from normal coal. The deformed coal has higher solvable low-molecular weight compounds than normal coal. The intermolecular force of deformed coal is relatively small. The deformed coal has low strength and high adsorption capacity, and these determine the outbreak of coal-gas outburst. The extraction yields by chloroform can be taken as an index of forecast risks of coal-gas outburst. The ...

2007-03-15

37

Data processing for the mise-a-la-masse survey; Ryuden den`iho tansa no data shori  

Energy Technology Data Exchange (ETDEWEB)

Data processing method was studied for mise-a-la-masse survey. Mise-a-la-masse method using wells as current sources measures resultant ground surface potential difference, and detects underground local resistivity anomaly. To extract resistivity anomaly largely different from surroundings, the anomaly is extracted as difference between the estimated value of regular resistivity structure (background) and potential difference or apparent resistivity. The following three approximations were attempted to estimate the background: the theoretical equation assuming isotropic homogeneous resistivity structure, that assuming horizontal multi-layered structure and the exponential function of distance from linear electrode for apparent resistivity, and these were compared with each other by numerical model experiment. The data processing method which determines the resistivity structure of the background and the ...

1996-10-01

38

Fission fragment rockets: A new frontier  

Energy Technology Data Exchange (ETDEWEB)

A new reactor concept is described which would enable fission fragments to be continuously extracted from the reactor. Such a reactor has the potential of enabling extremely energetic and ambitious deep space missions. In this talk the basic physics issues involved in the operation of this type of reactor are outlined, and some possible applications to space exploration are described. 3 refs., 2 figs., 3 tabs.

1989-04-01

39

Environmental assessment of the potential effects of aquifer thermal energy storage systems on microorganisms in groundwater  

Energy Technology Data Exchange (ETDEWEB)

The primary objective of this study was to evaluate the potential environmental effects (both adverse and beneficials) of aquifer thermal energy storage (ATES) technology pertaining to microbial communities indigenous to subsurface environments (i.e., aquifers) and the propagation, movement, and potential release of pathogenic microorganisms (specifically, Legionella) within ATES systems. Seasonal storage of thermal energy in aquifers shows great promise to reduce peak demand; reduce electric utility load problems; contribute to establishing favorable economics for district heating and cooling systems; and reduce pollution from extraction, refining, and combustion of fossil fuels. However, concerns that the widespread implementation of this technology may have adverse effects on biological systems indigeneous to aquifers, as well as help to propagate and release pathogenic organisms that enter thee environments need to be ...

1988-03-01

40

CT colonography: optimisation, diagnostic performance and patient acceptability of reduced-laxative regimens using barium-based faecal tagging  

Energy Technology Data Exchange (ETDEWEB)

To establish the optimum barium-based reduced-laxative tagging regimen prior to CT colonography (CTC). Ninety-five subjects underwent reduced-laxative (13 g senna/18 g magnesium citrate) CTC prior to same-day colonoscopy and were randomised to one of four tagging regimens using 20 ml 40%w/v barium sulphate: regimen A: four doses, B: three doses, C: three doses plus 220 ml 2.1% barium sulphate, or D: three doses plus 15 ml diatriazoate megluamine. Patient experience was assessed immediately after CTC and 1 week later. Two radiologists graded residual stool (1: none/scattered to 4: >50% circumference) and tagging efficacy for stool (1: untagged to 5: 100% tagged) and fluid (1: untagged, 2: layered, 3: tagged), noting the HU of tagged fluid. Preparation was good (76-94% segments graded 1), although best for regimen D (P = 0.02). Across all regimens, stool tagging quality was high (mean 3.7-4.5) and not significantly ...

2008-01-15

41

Side effects of grain protectants on biological control agents: How Hyptis plant extracts affect parasitism and larval development of Dinarmus basalis  

British Library Electronic Table of Contents (United Kingdom)

Dinarmus basalis Rondani (Hymenoptera: Pteromalidae), an ectoparasitoid of bruchid pests of stored cowpeas (Vigna unguiculata), is a potential biological control agent. We investigated whether grain protectants from Hyptis spicigera and H. suaveolens (Lamiaceae) disturb parasitism and post-embryonic growth of the parasitoid. When cowpeas containing bruchid larvae were treated before being placed in the presence of D. basalis females, the rate of parasitism decreased on average up to 24% and 47% in the presence of, respectively, leaf dry powder and essential oils from both plant species. The estimated larval mortality was higher on treated (9.55 to 28.6%) than on non-treated parasitized hosts (2.8%), depending on the plant species and the plant extract tested. Additional larval mortality wa...

2011-01-01

42

Shale oil value enhancement research. Quarterly report, October 1, 1993--December 31, 1993  

Energy Technology Data Exchange (ETDEWEB)

The first year of this effort was focussed on the following broad objectives: (1) Analyze the molecular types present in shale oil (as a function of molecular weight distribution); (2) Determine the behavior of these molecular types in liquid-liquid extraction; (3) Develop the analytical tools needed to systematize the process development; (4) Survey the markets to assure that these have high value uses for the types found in shale oil; (5) Explore selective process means for extracting/converting shale oil components into concentrates of potentially marketable components; (6) Compile overview of the venture development strategy and begin implementation of that strategy. Each of these tasks has been completed in sufficient detail that we can now focus on filling in the knowledge gaps evident from the overview.

1997-05-01

43

Occurrences and distributions of branched alkylbenzenes in the Dongsheng sedimentary uranium ore deposits, China  

British Library Electronic Table of Contents (United Kingdom)

A series of branched alkylbenzene ranging from C15 to C19 with several isomers (2?5) at each carbon number were identified in sediments from the Dongsheng sedimentary uranium ore deposits, Ordos Basin, China. The distribution patterns of the branched alkylbenzenes show significant differences in the sample extracts. The branched alkylbenzenes from organic-rich argillites and coals range from C15 to C19 homologues, in which the C17 or C18 dominated. On the other hand, the C19 branched alkylbenzenes dominated in the sandstone/siltstone extracts. The obvious differences of the branched alkylbenzene distributions between the uranium-host sandstones/siltstones and the interbedded barren organic-rich mudstones/coals probably indicate their potential use as biological markers associated with part...

2010-01-01

44

Mineral carbonation accelerated by dicarboxylic acids as a disposal process of carbon dioxide  

British Library Electronic Table of Contents (United Kingdom)

Mineral carbonation is based on the reaction of carbon dioxide with metal-oxide bearing minerals, usually containing magnesium or calcium silicate, to form hardly soluble carbonates and other solid byproducts. The concept is based on acceleration of the naturally occurring rock weathering process. In the present work the calcium silicate is present in the mineral, wollastonite. To accelerate the process and make it potentially useful for practical applications, mineral carbonation is conducted here using an indirect two-step route in which the reactive component (Ca^2^+ ions in considered case) is first extracted from the mineral matrix and afterwards carbonated. Two solid byproducts are formed in this process: silica in the extraction step and calcium carbonate in the carbonation step. In...

2011-01-01

45

Improvement of a radiochemical separation for selenium 79: Applications to effluents and nuclear wastes.  

Science.gov (United States)

Selenium 79 is a beta emitter produced from (235)U fission and is one of the long half-life radionuclides of interest in nuclear waste disposal problematic because of its potential migration capacity to the surface environment. Measurement of (79)Se is particularly difficult due to its low activity in waste matrices (about 10(-3)Bqg(-1)). A radiochemical procedure based on ion exchange separations was already described in a previous paper. This work presents different applications of the radiochemical separation to waste samples and an improvement of this procedure, including a selective extraction of selenium as diethylselenium in an organic solvent followed by a re-extraction in aqueous medium. This additional step allows the decontamination factor to be increased with the aim of counting (79)Se by liquid scintillation counting. PMID:19071740

2007-01-14

47

Stochastic risk estimate for barium radiological examinations in Malaga (Spain)  

International Nuclear Information System (INIS)

The aim of this research work has been the estimation of the stochastic risk for five barium examinations. The sample was the population attending the Radiological Service of the 'Nuestra Senora de la Victoria' University Hospital, who had been treated with some barium examinations, set in five different groups: oesophagus tract, oesophagus-gastric-duodenal tract, intestinal tract, enteroclysis and double enema. To estimate the stochastic risk, it is necessary to know the organ dose. This can be calculated from the dose-area product which allows us to determine the effective dose using software. The dose-area product is the most suitable quantity to measure in these types of examination. We have evaluated the contribution that each procedure provides to the genetically significant dose, somatically significant dose, collective effective dose, annual effective dose 'per capita' and detriment, which are useful for assessing the population risk of ...

2000-01-01

48

Influence of crystallization on the spectral features of nano-sized ferroelectric barium strontium titanate (Ba0.7Sr0.3Tio3) thin films  

British Library Electronic Table of Contents (United Kingdom)

Ferroelectric barium strontium titanate (Ba0.7Sr0.3TiO3)(BST) thin films have been prepared from barium 2-ethylhexanoate [Ba[CH3(CH2)3CH(C2H5)CO2]2], strontium 2-ethylhexanoate [Sr[CH3(CH2)3CH(C2H5)CO2]2] and titanium(IV) isopropoxide [TiOCH(CH3)2]4 precursors using a modified sol-gel technique. The precursor except [TiOCH(CH3)2]4 were synthesized in the laboratory. Transparent and crack-free films were fabricated on pre-cleaned quartz substrates by spin coating. The structural and optical properties of films annealed at different temperatures have been investigated. The as-fired films were found to be amorphous that crystallized to the tetragonal phase after annealing at 550degreeC for 1h in air. The lattice constants "a" and "c" were found to be 3.974A and 3.990A, respectively. The grain...

2008-01-01

49

Development of pyro-separation technology based on molten salt electrolysis  

International Nuclear Information System (INIS)

In order to effectively recover uranium, rotation speed of solid cathode was examined, and effect of uranium concentration and current density on electrodeposition were confirmed. And the potentiostatic and galvanostatic electrorefining experiments were conducted. Element used in the experiments were Zr, Nd, La chlorides. The reduction potentials of chlorides metals on liquid Cd cathode were measured by cyclic voltammetry experiments. The electrowinning experiments were performed in order to recover small amounts of uranium in salt. Experimental set-up for the batch type reductive extraction experiments were developed and installed. On the base of experimental results of batch type, multi-stage extraction equipment was set-up, and optimum number of stage and recover yield were measured. In the oxidative extraction study is examine selective separation behavior of the rare earth metals from alloy ...

2010-10-01

50

A single sorbent for tetracycline enrichment and subsequent solid-matrix time-resolved luminescence  

Energy Technology Data Exchange (ETDEWEB)

The aim of this study was to search for a sorbent that could act as an extraction phase and as a support for solid-matrix time-resolved luminescence (SMTRL). Four potential sorbents were investigated for this purpose using tetracycline (TC) as a model analyte. Sorbents prepared from C18 silica gel or calcium cross-linked pectin gel were able to extract TC from dilute solutions. Europium(III)-TC complex adsorbed on the surface of C18 generated the most intense TRL signal when measured at {lambda}{sub ex} = 388 nm and {lambda}{sub em} = 615 nm. This method achieved a 1 ng/ml limit of detection (LOD) with a 100 {mu}l sample solution in a repeated spotting mode. Hyphenation of sorbent extraction and SMTRL was demonstrated using C18. This method is suitable for screening of TC in foods or aqueous solutions and can be extended to other luminescent lanthanide-chelating analytes in physiological or ...

2005-01-10

51

Reduction of fluoroscopic exposure for the air-contrast barium enema  

Energy Technology Data Exchange (ETDEWEB)

In a fluoroscopic imaging system, image quality and patient dose are both affected by the optical system linking the image intensifier with the video camera. The effect on patient exposure of increasing the optical iris aperture size over that required for other procedures performed on the same imaging system was investigated for the air-contrast barium enema examination. Using a large-area transmission ionisation chamber to monitor the Roentgen-area-product of entrance exposure, a decrease in fluoroscopic radiation of greater than 50% was clinically documented for a fluoroscopic system utilising kVp and mA variable automatic brightness control. For this iris change, the video image was of acceptable quality for positioning and monitoring the patient, and no deleterious effect was detected in the conduct of the air-contrast exam. The availability of a variable-sized operator-selectable iris diaphragm would permit this dose-reduction approach to be extended to other ...

1983-11-01

52

Mechanical Properties and Thermal Shock Resistance of Refractory Self-Reinforced -SiAlONs Using Barium Aluminosilicate as an Additive  

British Library Electronic Table of Contents (United Kingdom)

Yb-, Y-, Yb/Y-, and Yb/Nd-doped -SiAlON ceramics with 5-wt% barium aluminosilicate (BAS) were synthesized by hot pressing. Typical self-reinforced microstructures were obtained in all investigated -SiAlONs in spite of the type of doped cations. This is attributed to the incorporation of BAS, which could supply suitable liquid phase to promote the anisotropic growth of the -SiAlON grains. All the composites exhibited excellent high-temperature mechanical properties and thermal shock resistance due to the formation of a self-reinforced microstructure and the complete crystallization of BAS additive.

2011-01-01

53

Interaction studies between Crofer-22APU alloy and P2O5 containing barium calcium alumino-borosilicate (BCABS) sealant glass-ceramics  

International Nuclear Information System (INIS)

We present the effect of P2O5 addition on barium calcium aluminum borosilicate BCABS glasses of composition (mol %) 35BaO-15CaO-5Al2O3-(37-x)SiO2-8B2O3-xP2O5 (0?x?5). The incorporation of P2O5 increased network polymerization and crystallization tendency. However, addition of P2O5 leads to the formation of Cr2O3 at the interface, saturating it in the ions of the metal. This improves glass-to-metal bonding. (author)

2010-09-01

54

Structural transformation of Li{sub 2}CoPO{sub 4}F upon Li-deintercalation  

Energy Technology Data Exchange (ETDEWEB)

Electrochemical performance and structural properties of the high-voltage cathode material Li{sub 2}CoPO{sub 4}F have been investigated. The cyclic voltammetry and coulometry under potential step mode in the voltage range 3.0-5.1 V vs. Li revealed a structural transformation at potentials above 4.8 V. This transformation occurring upon Li-extraction appears to be irreversible: the subsequent Li-insertion does not result in restoration of the initial structure, but takes place within a new ''modified'' framework. According to the structure refinement this modification involves the mutual rotations of (CoO{sub 4}F{sub 2}) octahedra and (PO{sub 4}) tetrahedra accompanied by the considerable unit cell expansion which is expected to enhance the Li-transport upon subsequent cycling. The new framework demonstrates a reversible Li-insertion/extraction in a solid-solution ...

2011-01-01

55

H{sup -} ion source using a localized virtual magnetic filter in the plasma electrode: type I LV magnetic filter  

Energy Technology Data Exchange (ETDEWEB)

A new multicusp H{sup -} ion source using a Localized Virtual magnetic filter of type I [Ref.6] in the plasma electrode is investigated. A multipole (MP) arrangement with a spacing of 10 mm of the magnet bars holds an extraction hole, optimizing the efficient production of high H{sup -} current, and at the same time only a small electron component was co-extracted with the H{sup -} ions. The local filter arrangement separates the beam electrons at a low energy. It is shown that the co-extracted total electron current is determined principally by the integrated magnetic field flux (Gcm) of the local filter with an extraction system at a constant extraction voltage. When the value of the Gcm is increased, the total electron component is reduced, while the H{sup -} electrical efficiency had a broad maximum around the optimized value of the Gcm. A thicker plasma electrode should be ...

1999-12-01

56

Role of corporate memory in the global supply chain environment  

British Library Electronic Table of Contents (United Kingdom)

Critical knowledge is proliferated among different knowledge owners of a corporate system through the individuals lying inside or outside the system. Extraction of such knowledge is a very crucial requirement for all organisations. This paper presents the role of critical knowledge in the proper functioning of a system by representing it in the form of eXtensible Markup Language to develop a corporate memory. In order to demonstrate the role of corporate memory in the organisation, a real-world problem of a global supply chain is considered. The problem utilises the concept of corporate memory for the selection of potential suppliers from a set of available suppliers, and further to select the best route from a set of available alternative routes. The objective deals with the minimisation ...

2009-01-01

57

Grid-controlled plasma cathodes  

International Nuclear Information System (INIS)

Experiments are described on a plasma cathode with biased grids to prevent entry of ions into the electron extraction gap. The cathode has potential applications to the generation of high-current pulsed electron beams. Operation at 20 A/cm"2 is theoretically possible. The source combines the low average power consumption of a plasma cathode with many of the attractive features of thermionic cathodes, such as space-charge-limited extractor gap electron flow, fast turn-on, and no diode closure. Initial experiments are reported at the 2 A/cm"2 level for pulse lengths to 160 #mu#s.

58

Enriched lithium collection from lithium plasma flow  

International Nuclear Information System (INIS)

In order to understand the physical processes concerned with the selective heating by ion cyclotron resonance and with the subsequent collection of heated particles, experiments were carried out with the extraction of lithium samples, enriched with "6Li isotopes. Probe and integral extractors allow to collect enriched Li at the end of the selective heating region. Surface density distribution on the collector and local isotopic content of lithium are measured, as a function of the screen height and the retarding potential. Dependence of the collected amount of lithium and of its isotopic content on the value of the magnetic field is also measured. 4 figs., 2 tabs., 5 refs.

59

Raney-platinum film electrodes for potentially implantable glucose fuel cells. Part 2: Glucose-tolerant oxygen reduction cathodes  

British Library Electronic Table of Contents (United Kingdom)

We report the fabrication and characterization of glucose-tolerant Raney-platinum cathodes for oxygen reduction in potentially implantable glucose fuel. Fabricated by extraction of aluminum from 1mm thin platinum-aluminum bi-layers annealed at 300^oC, the novel cathodes show excellent resistance against hydrolytic and oxidative attack. This renders them superior over previous cathodes fabricated from hydrogel-bound catalyst particles. Annealing times of 60, 120, and 240min result in approximately 400-550nm thin porous films (roughness factors ~100-150), which contain platinum and aluminum in a ratio of ~9:1. Aluminum release during electrode operation can be expected to have no significant effect on physiological normal levels, which promises good biocompatibility. Annealing time has a dis...

2010-01-01

60

Potential migration of organic pollutants in pipes of polyethylene. Study in pipelines of distribution net of drinkable water; Migracion potential de contaminantes organicos en tubos de polietileno. Estudio en tuberias de red de distribuciond e agua potable  

Energy Technology Data Exchange (ETDEWEB)

Polyethylene pipes and connections are being widely used in treated water distribution services. Migration of low molecular weight compounds from the polyethylene into the water can change its final quality. This paper is about the concentrations and identification of the migration compounds found in treated water after staying in contact with low and high-density polyethylene. Identification and quantification were carried out using CLSA (Closed Loop Stripping Analysis) extraction technique and gas chromatography coupled to mass spectrometry (HRGC/HRMS). (Author) 12 refs.

2002-07-01

61

First principles investigations of formation of ordered omega phases in Zr-Al alloys  

International Nuclear Information System (INIS)

First-principles density functional theory (DFT) based calculations were performed to study the electronic and cohesive properties of all the intermediate ordered phases appearing in the transformation from bcc-based #beta# to hexagonal ordered #omega# phase in Zr_3Al alloy. Full-potential linear augmented plane wave (FPLAPW) method under the GGA was employed to establish the stability hierarchy and structure-property correlations. Further, effective pair potentials upto the fourth nearest neighbours were extracted, which, subsequently, were used for the thermodynamics analysis of the thermally-induced #beta##->##omega# transformation. The lattice collapse mechanism involving the concept of the onset of a displacement wave where the extent of collapse is viewed as an amplification of the displacement wave was employed for further analysis. (author)

2005-12-05

62

Radioactive liquid effluent processing with borohydride ions. Procede de traitement d'effluents liquides radioactifs au moyen d'ions borohydrure  

Energy Technology Data Exchange (ETDEWEB)

A borohydride, for instance sodium borohydride, is added to the radioactive effluent, with eventually a carrier such as Cu{sup +}, to give a precipitate containing ruthenium. The processing can be combined to Sr and Cs precipitation be know processes giving barium sulfate and nickel ferrocyamide precipitates. Influence of borohydride concentration on decontamination factor is given.

1989-08-25

63

An investigation of some Turkish herbal medicines in Salmonella typhimurium and in the COMET assay in human lymphocytes.  

Science.gov (United States)

Medicinal plants play a major role in the life of Turkish people and of late medicinal plant usage has increased in many countries. Green plants in general contain mutagenic and carcinogenic substances, but there is little information about the biological activities of herbal medicine. In the present study, therefore, various Turkish medicinal herbs were investigated for their genotoxic potential in the Salmonella typhimurium microsomal activation assay and the alkaline single cell gel electrophoresis (COMET) assay. Extracts from these medicinal herbs and some fractions of these extracts were examined. The species investigated were Arctium minus, Ecballium elatterium, Momordica charantia, Plantago major, Urtica dioica, Viscum album, Salvia triloba, Euphorbia rigida, Stachys lavandulifolia, Acteoside, Abies nordmannia. They are used for various immune disorders and are applied either topically or taken orally as a herbal ...

1996-01-01

64

Remediation of contaminated agricultural soils near a former Pb/Zn smelter in Austria: Batch, pot and field experiments  

International Nuclear Information System (INIS)

Metal contaminated crops from contaminated soils are possible hazards for the food chain. The aim of this study was to find practical and cost-effective measures to reduce metal uptake in crops grown on metal contaminated soils near a former metal smelter in Austria. Metal-inefficient cultivars of crop plants commonly grown in the area were investigated in combination with in-situ soil amendments. A laboratory batch experiment using 15 potential amendments was used to select 5 amendments to treat contaminated soil in a pot study using two Barley (Hordeum vulgare L.) cultivars that differed in their ability to accumulate cadmium. Results from this experiment identified 3 of these amendments for use in a field trial. In the pot experiment a reduction in ammonium nitrate extractable Cd (<41%) and Pb (<49%) compared to the controls was measured, with a concurrent reduction of uptake into barley grain (Cd < 62%, Pb < 68%). In the field ...

2006-11-01

65

Potential for hot-dry-rock geothermal resources: experimental results  

Science.gov (United States)

Hot dry rock (HDR) contains insufficient permeability and fluid for natural hydrothermal development, but water pumped in a circulation loop through a HDR reservoir (hydraulically fractured between two drill holes) is being tested and evaluated. The formation of such in situ heat transfer systems, and subsequent testing of the man-made geothermal reservoirs in the Jemez volcanic field, New Mexico have already indicated the technical feasibility of the hot dry rock (HDR) geothermal concept. Documented production history and heat-extraction data obtained during the period from 1978 to 1980 have confirmed heat transfer, low water loss, and predictable thermal drawdown models for the HDR systems. During a nine month test of closed-loop heat extraction operations, 15 x 10/sup 6/ kWh of thermal energy were produced. The effective heat-transfer area and volume of the reservoir increased due to secondary fracturing caused by thermal contraction of the ...

1982-01-01

66

Insecticidal effects of essential oils extracted from aromatic plants on Ceratitis capitata (Wied.) in Lebanon  

International Nuclear Information System (INIS)

Full text: The excessive use of chemical pesticides to control agricultural pests is becoming alarming. The objective of this study is to search for biopesticides of plant origin that could be used to control one of the major pest of fruit production; the Mediterranean fruit fly (Ceratitis capitata Wied.). A colony of the Lebanese wild strain of this insect was reared under laboratory condition to provide biological material. The insecticidal activity of the essential oils extracted from aromatic plants in Lebanon was assessed. The tested plants are: Foeniculum vulgare, Thymbra spicata, Artemisia herba alba, Origanum syriacum, Ruta chalepensis, Lavandula stoechas, Salvia fruticosa, Mentha microphylla, Juniperus oxycedrus, Rosmarinus officinalis, Myrtus communis, Laurus nobilis and Ocimum gratissimum. Results show that essential oils isolated from F. vulgare, T. spicata, A. herba alba, O. syriacum and R. chalepensis have promising insecticidal ...

2005-05-09

67

Can a model-independent analysis be made for the matter distribution of "4"0Ca from 166 MeV #alpha# particle scattering  

International Nuclear Information System (INIS)

It is proposed to extract, independently of any nuclear model, the "4"0Ca matter density from an analysis of the elastic scattering of "1"6"6 MeV alpha particles. The scattering is described using an optical potential whose real part is evaluated by folding the matter density with a nucleon-alpha interaction. Following the procedure proposed by Sick (Nucl. Phys. A; 218: 509 (1974)) and Phys. Lett.; 44B; 62 (1975)) for the analysis of electron scattering data, the density is represented by a sum of gaussians whose amplitudes are deduced in fitting, via a chi"2 minimization, the experimental cross section data. This method determines the envelope of densities for different parameters of gaussians: width, spacing. The envelope of the moments of these densities are presented and the root-mean-square radius is extracted. It is concluded that only the nuclear surface is well studied by the alpha particle scattering. (author).

68

Antioxidant isoflavones in Osage orange, Maclura pomifera (Raf.) Schneid.  

Science.gov (United States)

Recent findings that many human chronic diseases are associated with oxidative stresses have instigated the search for dietary antioxidants. Many phytochemicals, particularly phenolic compounds, have been found to possess strong antioxidant activity and reduce the risks of those diseases. Isoflavones, a special phenolic group found in soybean, have been found to act as antioxidants in some model systems. This study investigated the isoflavone content in a unique nonedible tree fruit, Osage orange [Maclura pomifera (Raf.) Schneid], and methods for the extraction, identification, and quantification of the two major isoflavones, osajin and pomiferin, were developed. The ethyl acetate extract contained 25.7% osajin and 36.2% pomiferin, and the two isoflavones were at 9.5 g kg(-1) of fresh Osage orange. Two model systems, FRAP and beta-CLAMS, were used to measure the antioxidant activity of these two isoflavones. Pomiferin was found to be a strong ...

2003-10-22

78

NAME=\\  

Wastenet

...Extraction Arms Products and Equipment Find and compare a variety of extraction arms products and equipment on the world's largest environmental industry portal. ...

79

Extraction of magnesium as the iodide by tributyl phosphate  

Science.gov (United States)

The extraction of magnesium by tributyl phosphate from KI solutions was investigated. With increasing KI and TBP concentrations, the extraction increased. The maximum extraction (82%) was attained at pH 4, and it did not decrease with a further pH increase. With decreasing pH, the extraction decreased because of HI extraction. The magnesium was extracted as the compound MgI/sub 2/ x 4TBP. Complexone III (at pH 3-4) does not affect the extraction of magnesium, which makes it possible to use it to mask other metals.

1987-08-20

81

The potential of multidiurnal MODIS thermal band data for coal fire detection  

British Library Electronic Table of Contents (United Kingdom)

In this paper we present the results of our analyses of multidiurnal low-resolution Moderate Resolution Imaging Spectroradiometer (MODIS) thermal data for coal fire-related thermal anomaly detection. Results are presented for data of the Jharia coal mining region of India. We combine three relatively new approaches: first, we use low-resolution MODIS data for coal fire area analyses, which has only been undertaken by a few authors. Second, we analyse data from four different times of day (morning, afternoon, evening and predawn) and for three different bands (MODIS bands 20, 32 and a ratio thereof); and third, we use an unbiased automated algorithm for thermal anomaly extraction of local thermal anomalies. The MODIS data analysed stem from the years 2001 and 2005. In 2001, MODIS data were ...

2008-01-01

82

The Lithium future-resources, recycling, and the environment  

British Library Electronic Table of Contents (United Kingdom)

Abstract:- The demand for Lithium-ion batteries as a major power source in portable electronic devices and vehicles is rapidly increasing. I use cumulative data of vehicle, mobile phone, laptop, and digital camera production to show that demand will overshoot the available global Lithium resources before 2025. Even if 100% of all Lithium-ion batteries were recycled today, recycling could not prevent this resource depletion in time. As the increasing Lithium scarcity will increase the price, it will be feasible to mine diluted resources with a strong environmental impact. I highlight these impacts in Lithium-rich Bolivia, the potential new -Saudi Arabia of Lithium.- Lithium extraction is likely to cause substantial water pollution, and-through impacts on native diversity-facilitate human he...

2011-01-01

83

Temperature measurement of 6He?+? ions confined in a transparent Paul trap  

British Library Electronic Table of Contents (United Kingdom)

The LPCTrap setup is a transparent Paul trap dedicated to the measurement of the ??? correlation coefficient a ?? in the ? decay of trapped radioactive nuclides. In a first experiment, the system has been used to record ?105 coincidences between the ? particles and recoiling ions emitted from the decay of 6He?+? ions. The analysis of the collected data has already shown that the size of the 6He?+? ion cloud confined in the Paul trap is a critical parameter, potentially limiting the accuracy on the a ?? measurement. We report here the precise determination of the trapped ion cloud temperature and size. This was performed by extracting the trapped ions toward a position sensitive micro channel plate detector at different phases of the RF driving field. We find a temperature T exp ?= 0.107(7)...

2011-01-01

84

Preliminary studies on the chemical characterization and antioxidant properties of acidic polysaccharides from Sargassum fusiforme  

British Library Electronic Table of Contents (United Kingdom)

In order to investigate the antioxidant properties of the polysaccharides from the brown alga Sargassum fusiforme, the crude polysaccharides from S. fusiforme (SFPS) were extracted in hot water, and the lipid peroxidation inhibition assay exhibited that SFPS possessed a potential antioxidant activity. Hence, two purely polymeric fractions, SFPS-1 and SFPS-2 were isolated by the column of DEAE (2-diethylaminoethanol)-Sepharose Fast Flow, with their molecular weights of 51.4 and 30.3 kDa determined by high performance gel permeation chromatography (HPGPC). They were preliminarily characterized using chemical analysis in combination of infrared (IR) and nuclear magnetic resonance (NMR) spectroscopies and found to contain large amounts of uronic acids and ?-glycosidical linkages. The antioxida...

2008-01-01

85

Green Tea Extract (Epigallocatechin-3-Gallate) Reduces Efficacy of Radiotherapy on Prostate Cancer Cells  

British Library Electronic Table of Contents (United Kingdom)

ObjectivesTo assess the influence of epigallocatechin-3-gallate (EGCG) on the efficacy of ionizing radiation on prostate cancer cells because of the increased use of dietary interventions, especially by patients with prostate cancer. Radiotherapy is used to treat localized prostate cancer. Some people consume green tea (EGCG) as a chemopreventive agent against prostate cancer. Green tea can act as an antioxidant and induce superoxide dismutase enzymes, which could scavenge the free oxygen radicals generated by radiotherapy. MethodsProstate cancer cell line DU145 cells were treated with EGCG or radiotherapy, or both. Cell death was assessed using trypan blue cell counting, and apoptosis was confirmed by assessing poly (adenosine phosphate ribose) polymerase cleavage. The antioxidant potenti...

2011-01-01

86

GREEN TEA PHENOLS INTERFERENCE IN THE GLUCOSE OXIDASE/PEROXIDASE TEST  

British Library Electronic Table of Contents (United Kingdom)

Abstract Green tea extract showed false-negative results in the determination of glucose via glucose oxidase (GOD) test. This investigation was undertaken to verify and find out the precise mechanism underlying this interference by determining the reaction kinetics of production and reduction of end-point chromophore. The peroxidase step of the GOD test was found to be interfered and phenols of the green tea were the interfering compounds. Green tea interfered and exerted its influence in a dual fashion. A part of the interference was observed as a result of the reduction of the finally formed chromophore, whereas the other form of interference was due to its hydrogen peroxide/free radical-scavenging activity. Reducing potential and the free radical-scavenging activity of the phenols in th...

2011-01-01

87

Facial soft tissue response to anterior segmental osteotomies: A systematic review  

British Library Electronic Table of Contents (United Kingdom)

Bimaxillary protrusion is prevalent among Asians and anterior segmental osteotomies are commonly used for its surgical correction. The objective of this study was to evaluate the soft tissue changes resulting from anterior segmental osteotomies. The electronic databases PubMed, Scopus and ISI Web of knowledge were searched for potentially eligible studies using a set of predetermined keywords. Full texts meeting the inclusion criteria were retrieved and their references were manually searched for additional relevant articles. The study details and outcome data of these reports were extracted using spreadsheets for comparison. The methodological quality of each study was assessed. Eleven studies met the inclusion criteria. Lateral cephalometry was used in all studies. A reduction of the lab...

2010-01-01

88

Effect of Gallium Focused Ion Beam Milling on Preparation of Aluminum Thin Foils  

Energy Technology Data Exchange (ETDEWEB)

Focus Ion Beam (FIB) milling has greatly extended the utility of atom probe and TEM because it enables sample preparation with a level of dimensional control never before possible. Using FIB it is possible to extract the samples from desired and very specific locations. The artifacts associated with this sample preparation method must also be fully understood. In this work issues specifically relevant to the FIB milling of aluminum alloys are presented. After using the FIB as a sample preparation technique it is evident that gallium will concentrate in three areas of the sample: on the surface, on grain boundaries and at interphase boundaries. This work also shows that low energy Ar ion nanomilling is potentially quite effective for removing gallium implantation layers and gallium from the internal surfaces of aluminum thin foils.

2010-03-01

89

Dating Studies of Elephant Tusks Using Accelerator Mass Spectrometry  

Energy Technology Data Exchange (ETDEWEB)

A new method for determining the year of birth, the year of death, and hence, the age at death, of post-bomb and recently deceased elephants has been developed. The technique is based on Accelerator Mass Spectrometry radiocarbon analyses of small-sized samples extracted from along the length of a ge-line of an elephant tusk. The measured radiocarbon concentrations in the samples from a tusk can be compared to the {sup 14}C atmospheric bomb-pulse curve to derive the growth years of the initial and final samples from the tusk. Initial data from the application of this method to two tusks will be presented. Potentially, the method may play a significant role in wildlife management practices of African national parks. Additionally, the method may contribute to the underpinnings of efforts to define new international trade regulations, which could, in effect, decrease poaching and the killing of very young animals.

2002-10-03

90

Control of late blight in organic potato production: evaluation of copper-free preparations under field, growth chamber and laboratory conditions  

British Library Electronic Table of Contents (United Kingdom)

In order to replace copper fungicides in organic potato production, 53 copper-free preparations (CFPs) based on natural compounds, including plant extracts and microorganisms, and five copper preparations were evaluated for their potential to control Phytophthora infestans, the pathogen that causes late blight of potatoes. In in vitro assays, 30% of the CFPs inhibited indirect germination of sporangia, 26% mycelial growth and in growth chamber experiments, 21% efficiently reduced foliar blight of tomato plants. In micro-plot field trials with applications twice a week, the copper preparations were the most effective and reduced foliar blight by 99%. Of the CFPs tested, Oekofluid P, Mycosin and other sulphuric clays, and C-2000 reduced late blight the most, from 63% to 37%. In small-plot tr...

2007-01-01

91

Coal development potential in Pakistan  

Energy Technology Data Exchange (ETDEWEB)

A total of 48 papers were presented, and covered the following topics: the current situation in Pakistan with respect to development and utilization of coal resources; the policies that have been responsible for the development and utilization of coal resources in Pakistan; coal development and utilization in other developing nations e.g. Indonesia, Greece, Philippines, China, Thailand and Haiti; and technological developments in coal exploration; extraction, handling, transport and utilization which could accelerate future development of Pakistan's coal resources. Specific subjects covered include the use of coal in the cement industry of Pakistan; the production of briquettes for domestic use, development and training of personnel for the coal industry; and sources of finance for coal development projects. Particular emphasis is given throughout the conference to the Lakhra coal mine/power plant project which aims to develop and effectively utilize the ...

1986-01-01

92

Assessment of the oil source-rock potential of the Pedregoso Formation (Early Miocene) in the Falcon Basin of northwestern Venezuela  

British Library Electronic Table of Contents (United Kingdom)

The early Miocene Pedregoso Formation is one of the numerous formations rich in organic matter within the stratigraphic record of the Urumaco Trough, in the central area of the Falcon Basin. Due to its lithological characteristics and stratigraphic position, this formation is of great interest regarding the basin's petroliferous systems. The evaluation of various inorganic and organic geochemical parameters indicates that the organic matter is primarily of marine origin, deposited in a marine carbonate environment typical of reefal systems, under oxic-to-dysoxic conditions. The low variability in the TOC concentrations and in the distributions of the biomarkers extracted from the samples suggests that the paleoenvironmental conditions and the organic-matter supply remained approximately co...

2010-01-01

93

Absence of positive effect of black cohosh (Cimicifuga racemosa) on fracture healing in osteopenic rodent model  

British Library Electronic Table of Contents (United Kingdom)

Abstract The healing of predominantly metaphyseal fractures in postmenopausal osteoporosis is delayed and comparatively poor. Due to the potential side effects of HRT, natural alternatives are appealing. The aim of this study was to determine whether Cimicifuga racemosa extract BNO 1055 improves metaphyseal fracture healing in severe osteopenic bone in rats. Thirty three 12 week old female rats developed severe osteopenia during 10 weeks after ovariectomy. After metaphyseal tibial osteotomy and standardized T plate osteosynthesis, the healing periods in ovariectomized rats (C), 17 estradiol (E) and Cimicifuga racemosa (CR) supplemented diets were assessed for 35 days. Changes in callus morphology were evaluated qualitatively by biomechanical testing and quantitatively in microradiographies...

2010-01-01

94

Structural and magnetic properties of barium-gadolinium hexaferrites  

Energy Technology Data Exchange (ETDEWEB)

A series of Gd-substituted M-type barium hexaferrites has been prepared by the ceramic route, according to the formula (Ba{sub 1-x}Gd{sub x})O.5.25Fe{sub 2}O{sub 3} (x=0-0.30). XRD analysis revealed that all the samples present primarily an M-type structure. Samples x=0 and x=0.05 are single-phase. Hematite (Fe{sub 2}O{sub 3}) and GdFeO{sub 3} were detected in the remaining samples. Coercivity (H{sub c}) shows remarkably high values, {approx}293kA/m for x=0.20 and 0.30 with a maximum of 322kA/m for x=0.25. Specific saturation magnetization ({sigma}{sub sat}) of the samples presents a small increase up to x=0.10. The microstructure examination indicates that Gd may act as a grain growth inhibitor.

2007-03-15

95

Structural and magnetic properties of barium-gadolinium hexaferrites  

International Nuclear Information System (INIS)

A series of Gd-substituted M-type barium hexaferrites has been prepared by the ceramic route, according to the formula (Ba_1_-_xGd_x)O.5.25Fe_2O_3 (x=0-0.30). XRD analysis revealed that all the samples present primarily an M-type structure. Samples x=0 and x=0.05 are single-phase. Hematite (Fe_2O_3) and GdFeO_3 were detected in the remaining samples. Coercivity (H_c) shows remarkably high values, #approx#293kA/m for x=0.20 and 0.30 with a maximum of 322kA/m for x=0.25. Specific saturation magnetization (#sigma#_s_a_t) of the samples presents a small increase up to x=0.10. The microstructure examination indicates that Gd may act as a grain growth inhibitor.

2007-03-01

96

Radiation damage and recovery in the light emittance efficiency and the attenuation length of barium fluoride scintillator  

International Nuclear Information System (INIS)

Radiation damage and its recovery in the light emittance efficiency and the attenuation length of barium fluoride (BaF_2) scintillator have been investigated. The light yield and transmittance of small samples of BaF_2 scintillator were measured after #gamma#-irradiation from 0.5x10"4 to 1.1x10"5 Gy for deterioration, and after sunlight exposure for recovery. Suspension of deterioration was observed both in light yield and in attenuation length at an integrated dose of #gamma#-rays of about 10"4 Gy. Fairly good and quick recovery of the deteriorated BaF_2 scintillator was obtained by sunlight exposure. Using a Monte Carlo simulation method, the dependence of the light emittance efficiency on #gamma#-irradiation and sunlight exposure was studied. It has been found that the light emittance efficiency, as well as the attenuation length, is influenced by #gamma#-irradiation and sunlight exposure. (orig.).

97

Detection of pulmonary aspiration in infants and children with respiratory disease: concise communication  

Energy Technology Data Exchange (ETDEWEB)

Twenty children with respiratory disease ingested 500 ..mu..Ci of Tc-99m sulfur colloid orally, and scintigrams of the thorax were obtained to determine whether pulmonaryaspiration of gastric contents could be detected. The children ranged in age from 1 mo to 14 y; 13 were 8 months of age or younger. Children were studied at 5 min and 4 h after ingestion of Tc-99m sulfur colloid using a high-sensitivity computer oscilloscope to record 100K-count images. Additional images were obtained after the children had slept overnight. Five children (25%) showed definite pulmonary accumulation of activity; four of these also had a barium swallow and three showed either pulmonary aspiration of barium or moderately severe gastroesophageal reflux. Oral ingestion of Tc-99m sulfur colloid provides a noninvasive means for diagnosing pulmonary aspiration under physiologic conditions in infants and children.

1980-04-01

98

The adsorption and reaction of halogenated volatile organic compounds (VOC's) on metal oxides. Annual progress report, September 1996--October 1997  

Energy Technology Data Exchange (ETDEWEB)

'The interactions of carbon tetrachloride with strongly basic oxides and hydroxides have been studied by several techniques in order to understand the surface reactions and the subsequent bulk reactions that result in the destruction of the chlorinated hydrocarbon. Emphasis has been placed on understanding the surface phases, as well as the bulk phases, that are present during these transformations. As a result of the study with barium oxide, a reaction cycle has been demonstrated that may have practical significance in the removal of chlorinated hydrocarbons.'

1997-10-01

99

Selective enhancement of barium in the atmospheres of red giants  

Energy Technology Data Exchange (ETDEWEB)

High-resolution spectroscopy of 13 bright red giants and Ba stars shows selective enhancement of Ba in three of them, HD 65699 (Ba 2), ..cap alpha..TrA (K4 III), and epsilonPeg (K2 Ib). Infrared spectra available for HD 65699 show that Sr is enhanced, too. This selective enhancement is discussed in terms of a modified s-process which converts some of the pre-existing r- and s-process matter into the magic nuclei /sup 88/Sr and /sup 138/Ba.

1984-03-01

100

Phase diagrams  

International Nuclear Information System (INIS)

The description is presented of binary phase diagrams of titanium alloyed with the following elements: silver, aluminium, arsenic, gold, boron, barium, beryllium, bismuth, carbon, calcium, cadmium, cobalt, chromium, copper, iron, gallium, germanium, hydrogen, hafnium, indium, iridium, potassium, lithium, magnesium, manganese, molybdenum, nitrogen, sodium, niobium, nickel, oxygen, osmium, phosphorus, lead, palladium, platinum, plutonium, rhenium, lanthanium, cerium, preseodymium, neodymium, gadolinium, erbium, terbium, thulium, lutetium, rhodium, ruthenium, scandium, silicon, tin, strontium, tantalum, technetium, thorium, uranium, vanadium, tungsten, yttrium, ytterbium, zinc and zirconium.

101

New materials for SRS lasers  

International Nuclear Information System (INIS)

The problem of search for new materials for spectrally positioned laser sources, which is central for modern photonics, is discussed. The use of the stimulated Raman scattering effect in crystals offers a highly efficient way to the design of such sources. The recent results of investigations into this effect for a large number of various types of crystalline materials are presented. The most promising compounds, as regards the realisation of different laser operation modes, are considered, including calcium, strontium, barium and lead molybdates and tungstates. Several examples of functioning efficient lasers based on novel materials exhibiting the stimulated Raman light scattering effect are given.

2006-10-31

102

Moessbauer spectroscopy study of iron corrosion underneath painting system  

International Nuclear Information System (INIS)

The effect of pigments on the development of corrosion products between the painting system and metal surface when exposed to marine environments has been discussed. The pigments studied were: red mud zinc chromate, zinc chromate, red oxide zinc phosphate, manganese phosphate barium chromate and basic lead silico chromate. Moessbauer spectroscopy revealed that the upper rust layer in all the cases consisted of #gamma#-Fe_2O_3, #gamma#-FeOOH and #alpha#-FeOOH. The lower rust layer immediately in contact with the metal surface consisted of an asymmetrical doublet due to #gamma#-FeOOH. (Auth.).

103

Gastrointestinal radiography using Fuji computed radiography (FCR)  

International Nuclear Information System (INIS)

Initial clinical experience in gastrointestinal radiography using Fuji Computed Radiography(FCR) system was reported. Image quality of conventional film/screen radiography and FCR system on upper GI series and barium enema was compared. Reflecting wide dynamic range of the system, improved image quality was confirmed, particularity in visibility of fine mucosal pattern(area gastricae), folds and overall contour. High sensor sensitivity of the system could reduce radiation dose requirement significantly. Diagnostically acceptable images were obtained with approximately 1/5 of routine dose for conventional radiography except in cases of lateral view of the rectum. (author).

1985-01-01

104

Dielectric behavior of Ba{sub 0.95}Sr{sub 0.05}TiO{sub 3} ceramics sintered by microwave  

Energy Technology Data Exchange (ETDEWEB)

Here we report detailed dielectric studies carried out on a Barium strontium titanate (BST) (95:5) composition. The material was synthesized by conventional ceramic method and microwave processing, and the later technique resulted in material with high density, improved microstructure and dielectric properties. The dielectric properties were studied as a function of frequency and temperature and well-defined ferroelectric behavior of first order transition was observed. It follows Curie-Weiss law above transition temperature (paraelectric region). Curie temperature is slightly higher for microwave sintered (MS) material.

2002-12-01

105

The effect of extraction temperature, time and number of steps on the antioxidant capacity of methanolic banana peel extracts  

British Library Electronic Table of Contents (United Kingdom)

A solvent extraction method was developed to obtain methanolic extracts rich in antioxidants from banana peel. Central composite design ''2^3+star'' and response surface methodology were used in order to optimise the number of extraction steps, extraction temperature and extraction time. The number of extractions was statistically the most significant factor in scavenging activity against both DPPH? and ABTS?^+ radicals and in the inhibition of TBARS formation, while the extraction temperature had an important impact on the capacity to prevent b-carotene bleaching. However, the effect of the extraction time on antioxidant activity was less important. The optimum values of the factors that influence the capacity to scavenge DPPH? and ABTS?^+ radicals or to inhibit b-carotene bleaching were ...

2010-01-01

106

Extraction and analysis of antioxidant components from Origanum dictamnus  

British Library Electronic Table of Contents (United Kingdom)

Three alternative extraction procedures were carried out in order to separate the antioxidant components and isolate an efficient extract from Origanum dictamnus. Procedure A included sequential extractions with petroleum ether (PE), diethyl ether (DE) and ethanol; procedure B sequential extractions with PE and ethyl acetate (EAc); procedure C a single step extraction with ethanol. The most efficient radical scavengers, according to the DPPH method, were isolated in ethanol extract of procedure A (mainly rosmarinic acid), followed by ethanol extract of procedure C. However, both ethanol extracts had low solubility in oil and could not protect it. EAc and DE extracts, containing mainly apigenin and epirosmanol ethyl ether, presented lower radical scavenging activity but were very effective ...

2007-01-01

107

Longitudinal changes in extended roles in radiography  

Energy Technology Data Exchange (ETDEWEB)

Purpose: The purpose of this research was to identify the extent and scope of changes to radiography practice. Method: Questionnaires were sent to radiology managers at acute National Health Service (NHS) hospitals in 2000 as a follow-up to an initial survey conducted in 1998. Information was sought on region, teaching/non-teaching status, the nature of extended role tasks undertaken and the year in which these tasks were first undertaken. Results: Some 172 questionnaires were returned from a total of 253 dispatched (68%). In 161 hospitals radiographers administered intravenous injections and performed barium enemas in 119 hospitals, while a red-dot system was in operation in 141 hospitals. Reporting by radiographers had increased since 1998. Replies indicated that, at 124 hospitals, radiographers were reporting in ultrasound. Skeletal reporting was the second most-frequently-reported activity, with 63 hospitals indicating that radiographers reported in this ...

2002-11-01

108

Sida rhomboidea. Roxb Leaf Extract Down-Regulates Expression of PPAR?2 and Leptin Genes in High Fat Diet Fed C57BL/6J Mice and Retards in Vitro 3T3L1 Pre-Adipocyte Differentiation.  

Science.gov (United States)

Sida rhomboidea. Roxb leaf extract (SRLE) is being used by the populace of North-East India to alleviate symptoms of diabetes and obesity. We have previously reported its hypolipidemic and anti-diabetic properties. In this study, we report the effect of SRLE on (i) in vivo modulation of genes controlling high fat diet (HFD) induced obesity and (ii) in vitro 3T3L1 pre-adipocyte differentiation and leptin release. Supplementation with SRLE significantly prevented HFD induced increment in bodyweight, plasma lipids and leptin, visceral adiposity and adipocyte hypertrophy. Also, SRLE supplementation reduced food intake, down regulated PPAR?2, SREBP1c, FAS and LEP expressions and up-regulated CPT-1 in epididymal adipose tissue compared to obese mice. In vitro adipogenesis of 3T3L1 pre-adipocytes was significantly retarded in the presence of SRLE extract. Also decreased triglyceride accumulation, leptin release and glyceraldehyde-3-Phosphate ...

2011-07-19

109

Production of yellow cake from rock phosphate deposits and its characterization  

International Nuclear Information System (INIS)

This study was carried out mainly to produce uranium trioxide (UO_3), with the standard of commercial specifications from rock phosphate deposits in eastern part of Nuba mountains, south Kurdufan state. A simplified hydrometallurgical procedure has been adopted for production of yellow cake from the ore. Elemental analysis has shown that the ore is rich in Ca and deficient in elements of potential interest such as Fe, Cu and Zn. Uranium content in ore, phosphoric acid and purified yellow cake (UO_3) obtained with different precipitants was analyzed using alpha-spectrometry. On the average, the activity concentration of uranium in ore corresponds to 82 #+-# 24 ppm (0.10%). From the data of pregnant liquor, it was observed that the addition of KCIO_3 as an oxidant improves the dissolution of uranium from the ore by almost 20%. Data has also indicated that the yellow cake purified by hydrogen peroxide has higher concentration of uranium by 44.5% over the one purified ...

2002-01-01

110

Mineralization of phenanthrene and fluoranthene in yardwaste compost  

International Nuclear Information System (INIS)

PAH biomineralization measurements of yardwaste compost samples indicated heterogeneous distribution of active microorganisms and substantial sequestration of the non-polar substrate in the compost matrix. - The purpose of the study was to evaluate the potential of phenanthrene and fluoranthene biodegradation in yardwaste compost materials. These polynuclear aromatic hydrocarbons were chosen for this work because they are relatively readily biodegradable and ubiquitous in the environment. Compost samples were incubated in biometers with "1"4C-labeled phenanthrene and the evolution of "1"4CO_2 was assessed as a measure of mineralization. The "1"4CO_2 evolution varied widely among replicate biometers, possibly as the result of (1) uneven and patchy colonization of phenanthrene-degrading microorganisms on compost particles, and (2) non-uniform dispersion of the labeled substrate spike into the yardwaste microenvironment. Mineralization of phenanthrene reached about ...

2003-07-01

111

Cameron synthetic fuels report  

Energy Technology Data Exchange (ETDEWEB)

The increasing scarcity of conventional crude oil resources, as well as the sharply higher prices of crude oil, will generate increased interest in heavy oil, tar sands, and oil shale as potential substitutes. For all of these unconventional oil resources, extraction will be much more difficult, time consuming, and costly than for conventional crude oil. Although the inplace resources are vast and exist in many areas including the United States, the USSR, western Europe, Canada, and Latin America, probably only a small fraction of the inplace resources will prove to be economically extractable. These unconventional oil resources are now being developed in several locations around the world, and depending upon the exact definition probably account for less than 1 percent of current world oil supplies. The major current developments include: Canadian tar sands. Heavy oil production at Yarega in the Komi Autonomous Republic in ...

1980-06-01

112

Preparation and evaluation of radioiodinated 1-(dialkyl-aminoalkyl)-4-phenylpiperazines as potential brain imaging agents  

Energy Technology Data Exchange (ETDEWEB)

The interest in radioiodinated diamines stems from their similarity to /sup 125/I-HIPDM and to the 1-dialkvlamino-acyl-4-phenylpiperazines that the authors have previously examined as potential brain imaging agents. In this study they converted the 1-(dialkylaminoacyl)-4-phenylpiperazines to their corresponding 1-(dialkylaminoacyl) analogs via reduction with diborane in THF. Radioiodination at the no-carrier-added level with Na/sup 125/I and chloramine-T gave the final compounds, after chromatographic separation, in 30-50% yields. The tissue distributions were determined in rats at 0.25, and 4 hrs after an i.v. injection of the radiochemical. The results indicated that all of the agents were readily extracted by the brain (1.5-2.5% ID) with brain to blood ratios >20. The structure-distribution relationships for this series were, however, decidedly different from the aminoacyl compounds in that morpholino-derivatives had better uptake and ...

1985-05-01

113

Preparation and evaluation of radioiodinated 1-(dialkyl-aminoalkyl)-4-phenylpiperazines as potential brain imaging agents  

International Nuclear Information System (INIS)

The interest in radioiodinated diamines stems from their similarity to /sup 125/I-HIPDM and to the 1-dialkvlamino-acyl-4-phenylpiperazines that the authors have previously examined as potential brain imaging agents. In this study they converted the 1-(dialkylaminoacyl)-4-phenylpiperazines to their corresponding 1-(dialkylaminoacyl) analogs via reduction with diborane in THF. Radioiodination at the no-carrier-added level with Na/sup 125/I and chloramine-T gave the final compounds, after chromatographic separation, in 30-50% yields. The tissue distributions were determined in rats at 0.25, and 4 hrs after an i.v. injection of the radiochemical. The results indicated that all of the agents were readily extracted by the brain (1.5-2.5% ID) with brain to blood ratios >20. The structure-distribution relationships for this series were, however, decidedly different from the aminoacyl compounds in that morpholino-derivatives had better uptake and ...

1985-06-02

114

Generalized Collective Inference with Symmetric Clique Potentials  

CERN Document Server

Collective graphical models exploit inter-instance associative dependence to output more accurate labelings. However existing models support very limited kind of associativity which restricts accuracy gains. This paper makes two major contributions. First, we propose a general collective inference framework that biases data instances to agree on a set of {\\em properties} of their labelings. Agreement is encouraged through symmetric clique potentials. We show that rich properties leads to bigger gains, and present a systematic inference procedure for a large class of such properties. The procedure performs message passing on the cluster graph, where property-aware messages are computed with cluster specific algorithms. This provides an inference-only solution for domain adaptation. Our experiments on bibliographic information extraction illustrate significant test error reduction over unseen domains. Our second major contribution consists of ...

2009-01-01

115

Competition advantage by utilizing the gross calorific value-high potential for the local heat supply; Wettbewerbsvorsprung durch Brennwertnutzung. Hohes Potential bei der Nahwaermeversorgung  

Energy Technology Data Exchange (ETDEWEB)

The gross calorific value (H{sub o}) is the amount of heat which is generated by total combustion of a type of fuel. It also includes that part of heat which is generated by steam from evaporated water contained in heating gas. In conventional heating boilers, this heat portion is not being utilized at all. To utilize the gross calorific value, it is necessary to extract from the exhaust gas the evaporation heat bound in steam and to return this to the heating system. This means that the exhaust gas has to be chilled by the return water of the heating system and condensed in suitable heat exchangers to well below the dew point. (orig.) [Deutsch] Waermelieferanten im Bereich der Nahwaermeversorgung koennen durch die Anwendung verfuegbarer und bewaehrter Brennwerttechnik ihre Kosten senken und einen zusaetzlichen Beitrag zum Umweltschutz leisten. Mit dem richtigen Brennwertkessel amortisieren sich Mehrkosten in weniger als 2 Jahren. (orig.)

1999-01-01

116

Selective extraction of U(VI) and some other metals from nitric acid media by poly-phosphine poly-oxides  

International Nuclear Information System (INIS)

For the selective extraction of radionuclides from nitrate media, the extractabilities of organo-poly-phosphine poly-oxides were examined in the form of impregnated resins. It was found that the extractability of 1,1,3,5,5-pentaphenyl-1,3,5-tri-phospha-pentane trioxide (PPTPT) for U(VI) is quite unusual with very high values at both low and high concentrations of nitric acid, which is not observed for other types of extractants. Thus, this extractant might be promising for the selective extraction of U(VI) in very high concentrations of HNO3. (authors)

2008-09-15

117

Production and Purification of UO_3 from rock phosphate deposits and its characterization  

International Nuclear Information System (INIS)

This study was carried out mainly to produce uranium trioxide (UO_3), matching standard commercial specification from rock phosphate deposits in Uro and Kurun at eastern part of the Nuba Mountains. A simplified hydrometallurgical procedure has been adopted for production of yellow cake from the ore. The powdered ore sample was leached with concentrated H_2SO_4 acid with and without addition of KCIO_3 as an oxidant. The crude yellow cake was precipitated from the resulting green solution of phosphoric acid as Na_2U_2O_7 and (NH_4)_2U_2O_7 and subsequently purified by TBP extraction (tributylphosphate) and hydrogen peroxide as UO_4.2H_2O. TBP purified product was dried and calcined to UO_3 whereas UO_4.2H-2O was dried and reduced to UO_3 by Na_2S_2O_3. Prior to precipitation of crude yellow cake, Fe in the phosphoric acid solution was precipitated using magnesia. Elemental analysis has shown that the ore is rich in Ca and deficient in elements of ...

2005-03-01

118

The effect of wood extractives on the thermal stability of different wood-LLDPE composites  

Energy Technology Data Exchange (ETDEWEB)

The thermal stability of wood polymer composites made with extractive-free wood from four different wood species was studied. Hot water (HW) extractives, ethanol/cyclohexane (E/C) extractives and both types of extractives were eliminated from A. cyclops, E. grandis, P. radiata and Q. alba. Composites of LLDPE and 10 wt% of wood were prepared, using poly vinyl alcohol-co-ethylene (EVOH) as a compatibilizer. The thermal degradation behavior of the composites was characterized with thermogravimetric analysis (TGA). The obtained results showed that in all cases, the degradation temperatures shifted to higher values after removal of the extractives. The removal of E/C extractives was less effective in its improvement of the thermal stability than the removal of HW extractives. The largest improvement on the thermal stability of WPCs was achieved ...

2009-01-05

119

Vegetable oil extraction using liquid CO/sub 2/  

Energy Technology Data Exchange (ETDEWEB)

SC-CO/sub 2/ extraction of oil from peanuts is an alternative to hexane extraction or the mechanical oil press. Oil was successfully extracted using SC-CO/sub 2/ at temperatures of 25-120/sup 0/C and pressures of 140 -690 Bar. Pressure, temperature and particle size affected the extraction of oil. In the range studied, the highest values of temperature and pressure gave highest solubilities.

1986-01-01

120

Main concepts of modern methods for substantiating extractable reserves and coefficients of oil extraction from the depths  

Energy Technology Data Exchange (ETDEWEB)

General conclusions, principles and order of substantiating the extractable reserves and coefficients of oil extraction from oil and oil and gas fields are presented. Recommendations are made for solving questions of constructing calculation models for heterogeneous beds, schematization of the working conditions, selection of mathematical models for oil extraction for different geological-field conditions and different stages of ''life'' of the field.

1984-01-01

121

Antinociceptive and Anti-Inflammatory Activities of the Ethanol Extract of Annona muricata L. Leaves in Animal Models  

UK PubMed Central (United Kingdom)

Antinociceptive and anti-inflammatory activities of the ethanol extract from Annona muricata L. leaves were investigated in animal models. The extract delivered per oral route (p.o.)...Full Text Available

122

UK coal liquefaction  

Energy Technology Data Exchange (ETDEWEB)

The National Coal Board is investigating two routes for production of oils: liquid solvent extraction and supercritical gas extraction. Both these processes are considered ready for major development to plants of the 1 t/h scale.

1980-06-01

123

Polyhydroxyflavones as extractants. Communication 7. Solvent extraction of europrium complexes with morin from alkaline media  

Energy Technology Data Exchange (ETDEWEB)

This paper studies the analytical application of europium (III)-morin complex which is formed in alkaline medium and has an intense color. The extent of europium extraction was determined by adding to the extract a morin solution in isoamyl alcohol in a 50-100-fold excess with respect to europium. The dependence of the optical density of the extracts on the ph in the system europium (III)-morin-water-organic solvent for different excesses of the reagent is shown: this indicates formation of two extractable complexes, one being dominant in the pH range 4-7, the other at pH greater than or equal to 8.5. The extraction of the europium (III)-morin complex from alkaline solution is used for direct extraction-photometric determination of europium(III) in compounds of elements having amphoteric properties or forming amines (Zns, Mo0/sub 3/).

1985-09-01

124

Assessment of soil-gas, soil, and water contamination at the former 19th Street landfill, Fort Gordon, Georgia, 2009-2010  

Science.gov (United States)

Soil gas, soil, and water were assessed for organic and inorganic constituents at the former 19th Street landfill at Fort Gordon, Georgia, from February to September 2010. Passive soil-gas samplers were analyzed to evaluate organic constituents in the hyporheic zone and flood plain of a creek and soil gas within the estimated boundaries of the former landfill. Soil and water samples were analyzed to evaluate inorganic constituents in soil samples, and organic and inorganic constituents in the surface water of a creek adjacent to the landfill, respectively. This assessment was conducted to provide environmental constituent data to Fort Gordon pursuant to requirements of the Resource Conservation and Recovery Act Part B Hazardous Waste Permit process. The passive soil-gas samplers deployed in the water-saturated hyporheic zone and flood plain of the creek adjacent to the former landfill indicated the presence of total petroleum hydrocarbon (TPH) and octane above method detection levels ...

2011-01-01

125

Extraction of molybdenum with a multielement liquid organic extraction system  

Science.gov (United States)

An extraction of molybdenum is described that provides a more predictable separation over a significantly wider acidity range than previously determined. The extraction of Mo appeared to be a function of HCl normality, with virtually complete separation above 3.6 N. A test was conducted to determine if the extraction was a function of just HCl concentration or of overall acidity. When the aqueous phases of the test sequence were all prepared at 1 N H/sub 2/SO/sub 4/ in addition to the HCl in each, the resulting extraction curves were essentially identical. Another test was performed to determine if Mo was being extracted as an iodide complex. Three aqueous solutions, which were 4 N in HCl and 26% (w/v) ascorbic acid, were prepared in culture tubes. When 25 ..mu..g of Mo was extracted from these solutions of 5 mL of organic phase, the KCl gave only a 16% ...

1985-10-01

126

The effects of energy non-monochromaticity of "1"1B ion beams on "1"1B diffusion  

International Nuclear Information System (INIS)

We have shown that energy contamination introduced by ion beam deceleration technology that is used to increase the beam currents available for low energy boron implants, can affect fabricated junctions adversely. A 4 keV "1"1B beam is extracted and retarded by a potential of -3.5 keV for 0.5 keV "1"1B implantation, or by a potential of -3.8 keV for 0.2 keV "1"1B implantation. Intentional beam contamination was introduced by turning off the retarding potential to allow the 4 keV "1"1B ions to irradiate Si wafers directly. The percentage of contamination, at levels of 0.1%, 0.2% and 0.3% was introduced. Rapid thermal annealing of all the implanted samples was performed under N_2 ambient at 1050 deg. C for 1 s. The dopant tail profiles themselves are not significant if the contamination levels are low. However, the much higher damage level coming from high energy contamination increases the transient ...

2005-08-01

127

Higgs particles in the standard model and supersymmetric theories  

International Nuclear Information System (INIS)

This thesis presents a theoretical analysis of the properties of the Higgs bosons in the standard model (SM) and the minimal supersymmetric extension (MSSM), which can be investigated at the LHC and e"+e"- linear colliders. The final goal is the reconstruction of the Higgs potential and thus the verification of the Higgs mechanism. MSSM Higgs boson production processes at future #gamma##gamma# colliders are calculated in several decay channels. Heavy scalar and pseudoscalar Higgs bosons can be discovered in the bb final state in the investigated mass range 200 to 800 GeV for moderate and large values of tan#beta#. The #tau#"+#tau#"- channel provides a heavy Higgs boson discovery potential for large values of tan#beta#. Several mechanisms that can be exploited at e"+e"- linear colliders for the measurement of the lifetime of a SM Higgs boson in the intermediate mass range are analysed. In the WW mode, the lifetime of Higgs scalars with masses ...

128

In-situ measurement of epithelial tissue optical properties: Development and implementation of diffuse reflectance spectroscopy techniques  

Science.gov (United States)

Cancer is a severe threat to human health. Early detection is considered the best way to increase the chance for survival. While the traditional cancer detection method, biopsy, is invasive, noninvasive optical diagnostic techniques are revolutionizing the way that cancer is diagnosed. Reflectance spectroscopy is one of these optical spectroscopy techniques showing promise as a diagnostic tool for pre-cancer detection. When a neoplasia occurs in tissue, morphologic and biochemical changes happen in the tissue, which in turn results in the change of optical properties and reflectance spectroscopy. Therefore, a pre-cancer can be detected by extracting optical properties from reflectance spectroscopy. This dissertation described the construction of a fiberoptic based reflectance system and the development of a series of modeling studies. This research is aimed at establishing an improved understanding of the optical properties of mucosal tissues by analyzing ...

2009-01-01

129

Scale prevention with special reference to threshold treatment  

Energy Technology Data Exchange (ETDEWEB)

Various chemical, physical, and mechanical methods to prevent unwanted deposition of mineral scale are described. The suitability of the different methods, which largely depends on the specific features and requirements of the system involved, is discussed. Special emphasis is placed upon the threshold treatment, where the growth process is retarded by the addition of trace amounts of growth inhibitors. Growth experiments have been performed on barium sulfate and calcium sulfate dihydrate seed crystals, suspended in a supersaturated solution with and without organic bisphosphonates as inhibitors. Two methods are selected for the analysis of the growth data. A degree of inhibition is defined to obtain a quantitative description of the influence of a growth inhibitor on the growth rate of the crystals. In addition the influence of the molecular structure of various bisphosphonates with different substituents is shown. The effect of a bisphosphonate on the geometry of ...

1983-01-01

130

Esophageal Complications Following Aluminium Phosphide Ingestion: An Emerging Issue Among Survivors of Poisoning  

British Library Electronic Table of Contents (United Kingdom)

Aluminium phosphide ingestion is the most common agricultural poisoning in suburban and rural India and with a high mortality rate. Among survivors of acute poisoning there are recent sporadic reports of esophageal complications such as esophageal strictures and tracheo-esophageal fistula. The present study was carried out to determine the incidence, natural history, and treatment outcome of local esophageal complications in survivors of aluminium phosphide poisoning with complaints of dysphagia. All confirmed cases of poisoning with aluminium phosphide ingestion were admitted in Hamidia Hospital, Gandhi Medical College, Bhopal, Madhya Pradesh, India, from October 2007 to October 2008. Survivors with complaints of dysphagia underwent a barium study and upper gastrointestinal endoscopy to d...

2010-01-01

131

Endoscopic management of congenital esophageal stenosis  

British Library Electronic Table of Contents (United Kingdom)

Background/Purpose: Congenital esophageal stenosis (CES) is a rare malformation. Endoscopic dilations represent a therapeutic option. This study retrospectively evaluated the efficacy and safety of a conservative treatment of CES. Patients and Methods: Patients diagnosed with CES since 1980 by a barium study or endoscopy were reviewed. Endoscopic ultrasonography (Olympus UM-3R-20-MHz radial miniprobe, Olympus Corporation, Tokyo, Japan), available from 2001, allowed for the differential diagnosis of tracheobronchial remnants (TBR) and fibromuscular hypertrophy (FMH) CES. All children underwent conservative treatment by endoscopic dilations (hydrostatic and Savary). Results: Forty-seven patients (20 men) had CES. Fifteen were associated with esophageal atresia; and 8, with Down syndrome. Mea...

2011-01-01

132

Development of sealing insulator for electric penetration assemblies  

International Nuclear Information System (INIS)

Electrical penetration assemblies mounted on the containment wall are used to carry electrical power and signals from the equipment inside this containment (e.g. recirculation pumps, control rod position indications etc.) Todays BWR nuclear power plants apply epoxy resin sealed electric penetration. Contrariwise, the epoxy resin (organic sealant) was replaced with sodium barium glass (inorganic) by way of trial in search for a quality sealant. The glass sealant has been proved to have high temperature airtightness at 300 degC above from an evaluation test involving full-scale model parts. Environmental tests were conducted continuously as to heat cycle, vibration and LOCA etc. the specimens (module) of five types. They were made certain of conformity to the design requirements for boiling water operation. (author).

133

Design and development of an innovative hybrid powder based on a computer simulation and its application to foundation makeup products  

British Library Electronic Table of Contents (United Kingdom)

An innovative hybrid powder prepared using computer simulation allowed development of a new foundation having a fine, smooth texture that has never been achieved before. The optical structure/design of the powder was based on the results of measurements and analyses conducted on the optical characteristics of a baby's delicate skin, which is the envy of many women. To obtain the optimal optical characteristics, the finite differential time domain (FDTD) method for solving Maxwell's differential equation by difference and time domain was applied to the computer simulation method. For synthesis of the hybrid powder based on the optical model, a proprietary shape regulation coating technology was used in which flaky substrates were coated with microspherical forms of barium sulfate crystals. ...

2008-01-01

134

Characterization of Y2BaCuO5 nanoparticles synthesized by nano-emulsion method  

British Library Electronic Table of Contents (United Kingdom)

Nanoscale yttrium?barium?copper oxide (Y2BaCuO5, Y211) particles were synthesized using the emulsion method and the solution method. The basic water-in-oil (w/o) emulsion system consisted of n-octane (continuous oil phase), cetyltrimethylammonium bromide (cationic surfactant), butanol (cosurfactant) and water. The composition of the emulsion system was varied and characterized by measuring the conductivity of the solutions and droplet size. The droplet size of emulsion was determined by using the dynamic light scattering method. The water content, cosurfactant content, and surfactant/n-octane ratio affected the droplet size which was in the range of 3?8?nm, and hence the w/o emulsion system was referred to as a nano-emulsion system. A model was used to verify the droplet size. The influenc...

2007-01-01

135

Ceramic injection molding  

International Nuclear Information System (INIS)

Interest in making complex net-shape ceramic parts with good surface finishing and sharp tolerances without machining is a driving force for studying the injection molding technique. This method consists of softhening the ceramic material by means of adding some plastic and heating in order to inject the mixture under pressure into a relatively cold mold where solidification takes place. Essentially, it is the same process used in thermoplastic industry but, in the present case, the ceramic powder load ranges between 80 to 90 wt.%. This work shows results obtained from the fabrication of pieces of different ceramic materials (alumina, barium titanate ferrites, etc.) in a small scale, using equipments developed and constructed in the laboratory. (Author).

1988-11-01

136

Catalytic desulfurization of organic sulfur compounds over zeolite catalysts  

Energy Technology Data Exchange (ETDEWEB)

In the dehydrodesulfurization of ethanethiol at 400/sup 0/C, the activities of sodium X, Y, and A zeolites decreased in the order given as did the activities of nickel, cobalt, zinc, cadmium, copper, silver, lead, manganese, barium, calcium, sodium, and iron Y zeolite catalysts. A volcano-shape order was observed between the catalytic activity and the electronegativity of the metal ions. The changes in the activity of hydrogen Y zeolite catalyst in ethanethiol dehydrodesulfurization and cumene dealkylation by calcination agreed with the decrease in the Broensted acidity but were independent of Lewis acidity. For hydrodesulfurization of thiophene, the activities of nickel, cobalt, copper, and silver Y zeolite catalysts decreased in the order given and were greater than for a commercial hydrodesulfurization catalyst; reduced and presulfided catalysts showed selective hydrodesulfurization activity. Addition of 5% of nickel or molybdenum oxides to cobalt or nickel Y ...

1980-01-01

137

Barium carbonate sediment sampling for inorganic dissolved carbon using isotope mass ratio spectrometer  

International Nuclear Information System (INIS)

This paperwork explain the method of water sampling to obtain the precipitate of BaCO3 solutions that will be used to analyze 13C from field work in Kelana Jaya, Selangor, Langkawi, Kedah and Taiping, Perak. The sampling involves collecting of water samples for groundwater from boreholes and surface water from canal, river, pond and ex-mining pond from several locations at the study sites. This study also elaborates the instruments and chemicals used. The main purpose of this sampling is to obtain the precipitate of BaCO3 for 13C analysis of dissolved inorganic carbon (DIC). A correct sampling method according to standard is very important to ensure an accurate and precise result. With this, the data from the laboratory analysis result can be fully utilized to make the interpretation of the pollutants movement. (Author)

2009-10-06

138

A method for preventing cathodic deposition of molybdenum subchloride in LiCl-KCl molten salt  

Energy Technology Data Exchange (ETDEWEB)

Effects of ions of Group IA, IIA, IIIB, and VIIB elements on the cathodic deposition of a molybdenum were investigated in a KCl-LiCl (eutectic)-MoCl/sub 3/ molten salt at 773 K (500/degree/C). The results can be summarized as follows: The addition of potassium, rubidium, cesium, and barium cations and fluorine anions to the KCl-LiCl (eutectic)-MoCl/sub 3/ molten salt is effective in depressing the cathodic deposition of the molybdenum subchloride, which hinders the smooth, flat electrodeposition of molybdenum. The addition of lithium, sodium, magnesium, calcium, strontium, and aluminum cations and bromine and iodine anions promotes the undesirable cathodic deposition of the molybdenum subchloride.

1989-01-01

139

Punica granatum peel extract protects against ionizing radiation-induced enteritis and leukocyte apoptosis in rats  

International Nuclear Information System (INIS)

Radiation-induced enteritis is a well-recognized sequel of therapeutic irradiation. Therefore we examined the radioprotective properties of Punica granatum peel extract (PPE) on the oxidative damage in the ileum. Rats were exposed to a single whole-body X-ray irradiation of 800 cGy. Irradiated rats were pretreated orally with saline or PPE (50 mg/kg/day) for 10 days before irradiation and the following 10 days, while control rats received saline or PPE but no irradiation. Then plasma and ileum samples were obtained. Irradiation caused a decrease in glutathione and total antioxidant capacity, which was accompanied by increases in malondialdehyde levels, myeloperoxidase activity, collagen content of the tissue with a concomitant increase 8-hydroxy-2'-deoxyguanosine (an index of oxidative DNA damage). Similarly, pro-inflammatory cytokines (TNF-?, IL-1? and IL-6) and lactate dehydrogenase were elevated in irradiated groups as compared to control. PPE treatment reversed ...

2009-07-01

140

Evaluation of the Performance of the Automated NucliSENS easyMAG and EasyQ Systems versus the Roche AmpliPrep-AMPLICOR Combination for High-Throughput Monitoring of Human Immunodeficiency Virus Load?  

Science.gov (United States)

This study presents the data of an evaluation of the automated Nuclisens easyMAG and EasyQ systems versus the Roche AmpliPrep-AMPLICOR combination for testing of high-volume human immunodeficiency virus (HIV) load. This represents a follow-up of a previous study investigating the performance of the real-time Nuclisens assay using the semiautomated NucliSENS miniMAG extraction procedure. Three hundred eighteen patient samples were analyzed using both methods. The easyMAG-EasyQ HIV type 1 system has a higher sensitivity and broader dynamic range than the Cobas AmpliPrep-AMPLICOR system when the standard Roche assay is used alone, 25 to 3,000,000 IU/ml versus 400 to 750,000 HIV RNA copies/ml, respectively. There was significant correlation between the assays (0.93; P < 0.0001), with good accuracy (percent similarity mean ? = 96%), good precision (percent similarity standard deviation = 4.97%), and overall good agreement with a low percent similarity coefficient of ...

2007-05-01

141

Changes in the behaviour and physical and chemical characteristics of soil after adding populus euramericana leaves  

International Nuclear Information System (INIS)

Soil erosion and small annual additions of organic matter from plant-sources are the major causes of low organic-matter content in our soils. The tops of the plants, fallen to the soil- surface, remain there are incorporated, the plant-roots, shrubs, grasses. And other native plants contribution much towards the soil organic matter. Populus spp. Are grown commonly around farmers' fields in the state of Azad Jammu and Kashmir. A pot-experiment was conducted to study the effect of addition of populus euramericana leaves on various physical and chemical characteristics of the soil. Soil was kept at field-capacity level and incubated at room temperature for 10 months after adding 25, 50, and 75 g of Populus curamericana leaves per pot. Changes in organic-matter content. PH, cation-exchange capacity extractable potassium, water-holding capacity, and bulk density were investigated, after incubation for 6,8,and 10 months. There was a linear increase in organic-matter ...

142

Time-of-Flight Measurements from Eddy Current Tests  

Science.gov (United States)

Data fusion techniques are based on the premise that two or more carefully designed NDE tests are potentially capable of offering additional information concerning the test object relative to what can be garnered from a single test. However, information from a heterogeneous set of transducers cannot be fused unless the data is mapped onto a common `format'. The eddy current method cannot, for example, provide time-of-flight information that can be combined from estimates derived from ultrasonic tests. This paper presents a simple solution to address the problem by employing the so-called Q-transform to relate diffusive fields, such as those generated by eddy current probes, and propagating wave fields generated by ultrasonic NDT sensors. The paper illustrates how the distance between a defect and a source can be extracted from eddy current data generated using carefully selected excitation signals. Numerical results and comparisons with ...

2003-03-01

143

Thermophilic slurry-phase treatment of petroleum hydrocarbon waste sludges  

Energy Technology Data Exchange (ETDEWEB)

Chemoheterotrophic thermophilic bacteria were used to achieve enhanced hydrocarbon degradation during slurry-phase treatment of oily waste sludges from petroleum refinery operations. Aerobic and anaerobic bacterial cultures were examined under thermophilic conditions to assess the effects of mode of metabolism on the potential for petroleum hydrocarbon degradation. The study determined that both aerobic and anaerobic thermophilic bacteria are capable of growth on petroleum hydrocarbons. Thermophilic methanogenesis is feasible during the degradation of hydrocarbons when a strict anaerobic condition is achieved in a slurry bioreactor. Aerobic thermophilic bacteria achieved the largest apparent reduction in chemical oxygen demand, freon extractable oil, total and volatile solid,s and polycyclic aromatic hydrocarbons (PAHs) when treating oily waste sludges. The observed shift with time in the molecular weight distribution of hydrocarbon material ...

1995-12-31

144

Thermophilic slurry-phase treatment of petroleum hydrocarbon waste sludges  

International Nuclear Information System (INIS)

Chemoheterotrophic thermophilic bacteria were used to achieve enhanced hydrocarbon degradation during slurry-phase treatment of oily waste sludges from petroleum refinery operations. Aerobic and anaerobic bacterial cultures were examined under thermophilic conditions to assess the effects of mode of metabolism on the potential for petroleum hydrocarbon degradation. The study determined that both aerobic and anaerobic thermophilic bacteria are capable of growth on petroleum hydrocarbons. Thermophilic methanogenesis is feasible during the degradation of hydrocarbons when a strict anaerobic condition is achieved in a slurry bioreactor. Aerobic thermophilic bacteria achieved the largest apparent reduction in chemical oxygen demand, freon extractable oil, total and volatile solid,s and polycyclic aromatic hydrocarbons (PAHs) when treating oily waste sludges. The observed shift with time in the molecular weight distribution of hydrocarbon material ...

1995-04-24

145

The reduction of actinide ions by hydroxamic acids  

Science.gov (United States)

Simple hydroxamic acids have been shown to have useful applications in an Advanced Purex process for the reprocessing of irradiated nuclear fuel. They are especially suited to the separation of neptunium (IV) from uranium (VI) by the selective formation of a hydrophilic complex with Np(IV). U(VI) extraction in to 30% tributyl phosphate is unaffected. However, they have also been shown to be very fast reducing agents for Np(VI). The timescales of the reduction have been defined under a range of typical Purex Process conditions although the accurate determination of the reaction kinetics was not possible due to the rapidity of the reaction. U(VI) was shown not to be reduced. Therefore, Np(VI) can be efficiently reductively stripped when solvent phase (30% tributyl phosphate in odourless kerosene) solutions of Np(VI) and U(VI) are contacted with aqueous phase hydroxamic acid solutions. The slow reduction of plutonium (IV) to Pu(III) has also been observed and this is ...

1999-01-01

146

The chemistry of technetium(V) complexes containing tetradentate amine oxime ligands  

International Nuclear Information System (INIS)

Technetium-99m was previously shown to form a stable, neutral and lipopholic complex with propylene amine oxime, PnAO. This Tc-99m-PnAO complex was shown to efficiently extracted by normal brain. However, it is not sufficiently retained in the brain to image its cerebral distribution using convertional SPECT (single-photon emission computerized tomography) instrumentation. A number of derivatives of PnAO have been synthesized and their technetium-99m complexes have been biologically evaluated. A number of these have been shown to have high brain uptake without exhibiting the rapid cerebral clearance that was observed with Tc-99m-PnAO. To better understand the chemistry of these potential brain imaging agents, a number of technetium-99 complexes of derivatives of PnAO have been synthesized and characterized. Substituents on the tetradentate amine oxime backbone were varied to probe the effect(s) of these structural changes on the properties of ...

147

Mine waste disposal and managements  

Energy Technology Data Exchange (ETDEWEB)

Acid Rock Drainage (ARD) is the product formed by the atmospheric oxidation of the relatively common pyrite and pyrrhotite. Waste rock dumps and tailings containing sulfide mineral have been reported at toxic materials producing ARD. Mining in sulphide bearing rock is one of activity which may lead to generation and release of ARD. ARD has had some major detrimental affects on mining areas. The purpose of this study was carried out to develop disposal method for preventing contamination of water and soil environment by waste rocks dump and tailings, which could discharge the acid drainage with high level of metals. Scope of this study was as following: environmental impacts by mine wastes, geochemical characteristics such as metal speciation, acid potential and paste pH of mine wastes, interpretation of occurrence of ARD underneath tailings impoundment, analysis of slope stability of tailings dam etc. The following procedures were used as part of ARD evaluation and ...

1998-12-01

148

Lattice relaxation around impurity atoms in semiconductors - arsenic in silicon - a comparison between experiment and theory  

International Nuclear Information System (INIS)

We have measured the lattice relaxation around As in Si at a homogeneous As concentration of 4x10"1"8 cm"-"3 by EXAFS spectroscopy. From the absorption spectra, distances up to the 4th shell could be extracted. A sizeable misfit due to an increased distance is only observed for the 1st shell. Complementing our experimental work we have performed ab initio calculations based on the density functional theory with the WIEN97 package which uses the linearised augmented plane wave method and with the FHI96md program which uses first-principles pseudo-potentials and a plane wave basis set to investigate the size dependence of the super-cells constructed around one substitutional As atom. The calculations yielded good agreement with our EXAFS experiment so that the determined relaxations can be used as a solid basis for further interpretations of derived parameters such as hyperfine interaction parameters in defect complexes.

2003-01-01

149

Integrating Steel Production with Mineral Carbon Sequestration  

Energy Technology Data Exchange (ETDEWEB)

The objectives of the project were (i) to develop a combination iron oxide production and carbon sequestration plant that will use serpentine ores as the source of iron and the extraction tailings as the storage element for CO2 disposal, (ii) the identification of locations within the US where this process may be implemented and (iii) to create a standardized process to characterize the serpentine deposits in terms of carbon disposal capacity and iron and steel production capacity. The first objective was not accomplished. The research failed to identify a technique to accelerate direct aqueous mineral carbonation, the limiting step in the integration of steel production and carbon sequestration. Objective (ii) was accomplished. It was found that the sequestration potential of the ultramafic resource surfaces in the US and Puerto Rico is approximately 4,647 Gt of CO2 or over 500 years of current US production of CO2. Lastly, a computer model ...

2008-05-01

150

Fusion of information from optical, thermal, multispectral imagery and geologic/topographic products to detect underground detonations (video). Audio-Visual (Final)  

Energy Technology Data Exchange (ETDEWEB)

The video documents the results of a Small Business Innovative Research (SBIR-Phase II) project conducted for DARPA focusing on the use of all-source overhead remote sensor imagery for monitoring underground nuclear tests and related activities. The documentation includes: (1) the main unclassified body of the report; (2) a separate ground truth Annex; and (3) a separate classified Annex. Autometric's approach was to investigate the exploitation potential of the various sensors, especially the fusion of products from them in combination with each other and other available collateral data. This approach featured empirical analyses of multisensor/multispectral imagery and collateral data collected before, during, and after an actual underground nuclear test (named 'BEXAR'). Advanced softcopy digital image processing and hardcopy image interpretation techniques were investigated for the research. These included multispectral (Landsat, SPOT), ...

1992-04-01

151

Exploitation of deposits of bitumens and oil shales. Ekspluatatsiya mestorozhdenii bitumov i goryuchikh slantsev  

Energy Technology Data Exchange (ETDEWEB)

A definition is given for the basic national economic task of developing the recovery of hydrocarbons from bitumen-containing rock and oil shales, and a description is given of the status of the mineral-raw material base. General concepts are given on bitumens and oil shale. Their elemental and group compositions are cited in detail, and a determination is made of the position they occupy in the total system of fossil fuels. An examination is made of data on the distribution and state of bitumen and oil shale resources, and a description is given of their principal deposits. An evaluation is made of gained experience and the potential of existing methods of working bituminous rock and oil shale deposits that include the use of available and utilized method of land-based, underground, and instrastratal extraction of petroleum from those deposits. A presentation is made of the technical-economic aspects of producing bituminous and shale oils. The ...

1980-01-01

152

Development of a multiplex PCR method for simultaneous detection of diagnostic DNA markers of five disease and pest resistance genes in potato  

British Library Electronic Table of Contents (United Kingdom)

Multiplex PCR is practically a reasonable choice for molecular marker-assisted selection in potato breeding. We had developed and were using a multiplex PCR method for selection of resistance genes to cyst nematode (H1), Potato virus X (Rx1) and late blight (R1 and R2). Since then, more reliable and tightly linked markers for H1 and R2, and a new marker for resistance to Potato virus Y (Ry chc ) were developed. In this article, all these superior markers, including a positive marker to eliminate PCR-failed samples, were incorporated into one multiplex PCR assay. Using the newly developed multiplex PCR technique, five plants potentially harboring all five resistance genes were selected from 96 hybrid plants approximately 5?h after DNA extraction, which is a third of the operation time compa...

2011-01-01

153

Destruction of organic chemicals in Hanford HLW tanks by radiolytic and chemical aging  

International Nuclear Information System (INIS)

The underground storage tanks at the Hanford Complex contain mixed wastes generated over many years from plutonium production and recovery processes. The chemical changes of the organic materials used in the extraction processes and disposed to the tanks have a direct bearing on several specific safety issues, including potential energy releases from these tanks. This paper will give details of a study that is directed towards elucidating thermal and radiological decomposition mechanisms and products of the organic contents of the tanks. The study is being conducted in two parts. The first part, an aging study, will determine kinetics and products of the degradation of a simulated waste subjected to #gamma#-radiation from an external source. Although the simulant will not contain radioactive elements, it will contain other representative inorganic compounds and the primary organic compounds thought to have been disposed to the tanks. The second ...

1994-08-21

154

Comparative investigation of corrosion resistance of steel reinforcement in alinite and Portland cement mortars  

Energy Technology Data Exchange (ETDEWEB)

The corrosion resistance of steel-reinforced mortar specimens made from alinite cement was investigated using ordinary Portland cement (OPC) specimens as reference. The specimens were prepared and exposed in three different environments: continuous exposure in tap water, interrupted exposure in tap water, and interrupted exposure in 3.5% NaCl solution. The steel weight loss and the half cell potential were measured vs. exposure time, up to the age of 12 months. Pore solution extraction and analysis and porosity determination were also performed. In continuous exposure in tap water, alinite cement provided adequate protection against corrosion. In interrupted exposure in tap water, a higher corrosion was observed for alinite cement compared to OPC. In the case of interrupted exposure in 3.5% NaCl solution, the simultaneous action of free chlorides and oxygen resulted in the depassivation of steel reinforcing bars in alinite and Portland cement ...

1998-07-01

155

Biocatalytic desulfurization of petroleum and middle distillates  

Energy Technology Data Exchange (ETDEWEB)

Biocatalytic Desulfurization (BDS) represents an alternative approach to the reduction of sulfur in fossil fuels. The objective is to use bacteria to selectively remove sulfur from petroleum and middle distillate fractions, without the concomitant release of carbon. Recently, bacteria have been developed which have the ability to desulfurize dibenzothiophene (DBT) and other organosulfur molecules. These bacteria are being developed for use in a biocatalyst-based desulfurization process. Analysis of preliminary conceptual engineering designs has shown that this process has the potential to complement conventional technology as a method to temper the sulfur levels in crude oil, or remove the recalcitrant sulfur in middle distillates to achieve the deep desulfurization mandated by State and Federal regulations. This paper describes the results of initial feasibility studies, sensitivity analyses and conceptual design work. Feasibility studies with various crude oils ...

1993-02-01

156

Assessment of cadmium in aquatic sediment using dialysis samplers with ion-exchange-resin collection  

Energy Technology Data Exchange (ETDEWEB)

Simultaneously extracted metals (SEM) and acid volatile sulfide (AVS) show the potential for toxicity on the basis of their ratio. Accordingly, the authors spiked cadmium in a range for which Cd/AVS ratios were from 0.2 to 10 in the sediment with its weight about 8 kg in each batch. Dialysis samplers with a cation ion-exchange resin (Dowex 50W-X4) collection were used in a laboratory for the determination of free cadmium concentrations in pore water of the collected sediment. When equilibrium was reached among cadmium in pore water, sediment, and ion-exchange resin, cadmium exchanged onto resin phase was regenerated with 1 N hydrochloric acid (OPTIMA grade) and determined using an atomic absorption spectrophotometer (Zeeman 5000) with a graphite furnace accessory. Cadmium determined using the dialysis sampler is considered as free cadmium which is related to the metal bioavailability toward aquatic biota. The developed methodology provides a ...

1998-05-01

157

Actinides in liquid waste formed in the regeneration of nuclear fuel from a VVER-1000 reactor  

International Nuclear Information System (INIS)

In the radiochemical reprocessing of spent fuel from nuclear reactors, a considerable amount of liquid, solid, and gaseous waste is formed; this waste is potentially dangerous to humans and requires the development of special and complex technological techniques for its localization and reliable long-term storage. The most hazardous are liquid wastes of high specific activity - water-tailings solutions obtained in the first cycle of extraction after the removal of uranium and plutonium. These solutions contain more than 99.9% of all the other transuranic elements - isotopes of neptunium, americium, and curium. Where necessary, some fission products and actinides may be removed from wastes of high specific activity for subsequent use. The quantity, composition, and activity of these wastes varies within broad limits, depending on the type and power of the reactor, the initial nuclide composition of the fuel, and its specific energy yield, the ...

166

Purification of bidentate organophosphorous extractants  

Energy Technology Data Exchange (ETDEWEB)

Crude N,N-dialkylcarbamoylmethylphosphonates and phosphine oxide extractants, and particularly crude dihexyl N,N-diethylcarbamoylmethylphosphonate and octylphenyl N,N-diisobutylcarbamoyl phosphine oxide, are purified by distilling the crude materials in a thin film evaporator. Preferably, the crude materials are reacted with concentrated hydrochloric acid and then with aqueous sodium hydroxide prior to distillation in the thin film evaporator to hydrolyze impurities contained in them. The purified extractants are useful for extracting actinides and lanthanides from liquid waste streams. (author).

1990-12-19

167

Purification of bidentate organophosphorous extractants  

International Nuclear Information System (INIS)

Crude N,N-dialkylcarbamoylmethylphosphonates and phosphine oxide extractants, and particularly crude dihexyl N,N-diethylcarbamoylmethylphosphonate and octylphenyl N,N-diisobutylcarbamoyl phosphine oxide, are purified by distilling the crude materials in a thin film evaporator. Preferably, the crude materials are reacted with concentrated hydrochloric acid and then with aqueous sodium hydroxide prior to distillation in the thin film evaporator to hydrolyze impurities contained in them. The purified extractants are useful for extracting actinides and lanthanides from liquid waste streams. (author).

1990-05-16

186

Comparison of the NucliSens easyMAG and Qiagen BioRobot 9604 Nucleic Acid Extraction Systems for Detection of RNA and DNA Respiratory Viruses in Nasopharyngeal Aspirate Samples?  

UK PubMed Central (United Kingdom)

The NucliSens easyMAG and BioRot 9604 automated nucleic acid extraction systems were evaluated and compared with the manual QIAamp (Qiagen) extraction method for their abilities to extract nucleic acid...Full Text Available

2008-07-01

205

Process for recovering uranium from wet-process phosphoric acid using alkyl pyrophosphoric acid extractants  

Science.gov (United States)

A process is described for the recovery of uranium values from phosphoric acid utilizing an alkyl pyrophosphoric acid (Appa) primary extractant. After extracting the uranium from the phosphoric acid, the appa extractant is deactivated by heating and the uranium values stripped into a phosphoric acid strip solution containing ferric ion as a salting agent. The uranium values may then be re-extracted directly from this stripping solution without adjustment of its concentration into a dialkyl phosphoric acid trialkyl phosphine oxide synergistic extractant from which a relatively pure yellow cake is precipitated. A new procedure for preparing the requisite appa primary extractants is also disclosed.

1981-10-06

206

Improving Term Extraction Using Particle Swarm Optimization Techniques  

CERN Document Server

Term extraction is one of the layers in the ontology development process which has the task to extract all the terms contained in the input document automatically. The purpose of this process is to generate list of terms that are relevant to the domain of the input document. In the literature there are many approaches, techniques and algorithms used for term extraction. In this paper we propose a new approach using particle swarm optimization techniques in order to improve the accuracy of term extraction results. We choose five features to represent the term score. The approach has been applied to the domain of religious document. We compare our term extraction method precision with TFIDF, Weirdness, GlossaryExtraction and TermExtractor. The experimental results show that our propose approach achieve better precision than those four algorithm.

2010-01-01

207

Efficacy of Azadirachta indica extracts against Boophilus microplus  

British Library Electronic Table of Contents (United Kingdom)

Extracts were prepared from leaf, bark, and seed of Azadirachta indica, leaf and seed of Prunus persica, bark of Mangifera indica, and leaf of Psidium guajava and were evaluated against Boophilus microplus. Of the eight extracts screened, the extracts prepared from the A. indica seed showed very high level of efficacy (80%) after 5?h of treatment. Besides the immediate effect on adult ticks, the egg-laying properties of the survived ticks was also assessed, and a significant reduction (P?A. indica seed extracts was noted in comparison to control. The efficacy of the neem seed extracts was compared with the commonly used synthetic pyrethroids, and comparable efficacy against B. microplus fed on animals treated with neem seed extracts and acaricide treated was noted. The possibility of using...

2008-01-01

208

Antioxidant activity in banana peel extracts: Testing extraction conditions and related bioactive compounds  

British Library Electronic Table of Contents (United Kingdom)

Banana (Musa acuminata Colla AAA) peel extracts obtained in this work had a high capacity to scavenge 2,2-diphenyl-1-picrylhydrazyl (DPPH) and 2,2prime-azino-bis(3-ethylbenzothiazoline)-6-sulfonic acid (ABTS+) free radicals, and they were also good lipid peroxidation inhibitors. Acetone:water extracts were considerably more effective (compared with methanol, ethanol, acetone, water, methanol:water or ethanol:water) at inhibiting the peroxidation of lipids in the b-carotene/linoleic acid system or scavenging free radicals. However, aqueous extracts had a high capacity to protect lipids from oxidation in the thiobarbituric acid reactive substances (TBARS) test, as well as in the b-carotene bleaching assay. In addition, acetone:water most efficiently extracted all extractable components (54+-...

2010-01-01

209

Testing of the Schlema waste dump leachates cleaning system on a pilot-plant scale. Research report No. 92005  

International Nuclear Information System (INIS)

The concentrations of uranium, arsenic, and radium remain well below the maximum permissible values of < 0.1 mg/l (uranium), < 0.1 mg/l (arsenic) and < 100 mBq/l (radium) due to two separation stages with barium sulfate and GoPur 3000 precipitation and due to iron hydroxide/iron arsenate precipitation. The radioactive arsenates can be separated from the toxic ones by separating the sludge which is analyzed. Processing of radioactive sludges leaves reusable GoPur 3000, sulfuric solutions which contain uranium or solutions which contain carbonate, and radioactive barium sulfate whose radiation intensity of 12 mBq/g is due to the presence of radium. The sludge produced contains adsorbed salts in addition to the dosed chemicals (floated sludges: 40 g/m"3, iron sludges < 20 g/m"3). A solids content < 100 g/m"3 can be selected for both sludge portions. Static-mixer chemicals dosing and technical improvements of the tubular reactor are ...

210

Stochastic risk estimation from medical x-ray diagnostic examinations, 2  

International Nuclear Information System (INIS)

The risks of genetic, leukemia and malignant diseases from medical X-ray diagnostic examinations were estimated using the frequency of radiographic and fluoroscopic exposures per diagnostic examination, child expectancy, leukemia and malignancy significant factors, and using a weighting factor determined on the basis of data concerning the cancer mortality among atomic bomb survivors in Nagasaki and of a recommendation of International Commission of Radiological Protection. The organ or tissue doses with respect to the stochastic risks were determined with ionization chambers and thermoluminescent dosimeters placed at the positions of the organs or tissues in a RANDO woman phantom which was exposed to diagnostic X-rays according to technical factors of typical radiographic and fluoroscopic examinations obtained from a nationwide survey. The resultant risks by age-group and type of radiographic and fluoroscopic examination are tabulated in terms of risk level of 10"-"6. In general, the ...

1981-01-01

211

Early and Late Bowel Complication Following Irradiation of Cancer of the Uterine Cervix-Whole Pelvis External Irradiation end High-Dose-Rate Interactively Irradiation  

International Nuclear Information System (INIS)

Cervix cancer is the most common female cancer in Korea. In spite of their relatively local invasive tendency, still 44% of patient will develop recurrent cancer This result suggests that more aggressive local treatment may increase the cure rate but increased complication risk also cannot be avoidable. Various institutions proposed different treatment regimen, but recommended dose were about 4500 cGy for whole pelvis and 8000 cGy at point A, even though they agreed that those doses may not be satisfactory for control of bulky disease. 96 cases of invasive cervical cancer, treated with postoperative or primary radiation therapy were analyzed to determine the complication rate and prognostic factor in our treatment regimen which is 500-1000 cGy higher than other institution. Mean follow up duration was 21 months. Symptomatic patients including mild but persistent abdominal discomfort was 46%, but only 1 patient (1%) had operative treatment because of incomplete obstruction of small ...

1989-06-01

212

Regional ecological impacts of the development of oil shale resources: a review  

Energy Technology Data Exchange (ETDEWEB)

Significant development of an oil shale industry has been projected over the next few decades. The nation's largest oil shale reserves exist in the Wyoming Basin and Colorado Plateau physiographic provinces. This study presents a brief description of the environmental setting and land-use pattern of the region, with a review of the major environmental issues associated with each proposed technology for extracting shale oil. Serious effects may be expected from the modification of very large land surfaces through open-pit mining and spent-shale disposal. The impacts include habitat destruction, potential species loss, and deterioration of surface and groundwater quality. In situ retorting of shale may result in major alterations of groundwater quantity, quality, and flow regimes. Mine dewatering from in situ retorting requires the disposal of large volumes of highly saline water, threatening the quality of subsurface and surface water ...

1982-08-01

213

Lithium intercalation into {alpha}-Fe{sub 2}O{sub 3} obtained by mechanical milling of {alpha}-FeOOH  

Energy Technology Data Exchange (ETDEWEB)

Crystalline {alpha}-Fe{sub 2}O{sub 3} powder was prepared by the mechanical milling of crystalline {alpha}-FeOOH at room temperature in air. This result means that crystalline {alpha}-FeOOH is dehydrated by mechanical milling at room temperature. The obtained {alpha}-Fe{sub 2}O{sub 3} powder worked as a rechargeable electrode material in lithium ion conductive organic electrolytes. The electrodes exhibited high discharge capacities of over 1000mAhg{sup -1} corresponding to 6 Li per {alpha}-Fe{sub 2}O{sub 3} at potentials ranging from the open circuit potential to 0.5V (versus Li{sup +}/Li) in the first discharging (lithium insertion) process. This suggests that the valence deviation from Fe{sup 3+} in {alpha}-Fe{sub 2}O{sub 3} to Fe{sup 0} may be caused by electrochemical reduction. In contrast, after the first discharge, the electrodes exhibited high charge capacities of more than 700mAhg{sup -1} corresponding to 4.2 Li per {alpha}-Fe{sub ...

2005-08-26

214

Hydrocarbon generation potential of some Hungarian low-rank coals  

Energy Technology Data Exchange (ETDEWEB)

Several Hungarian lignite and brown coal samples were studied by coal petrographical, palynological and organic geochemical methods. Three of these were chosen for a series of pyrolysis experiments. Thermal treatment was carried out on two H-rich Eocene brown coals (kerogen: Type II) and a H-poor Miocene lignite (kerogen Type III) between 200 and 500{degree}C. The products of experiments (insoluble residue, chloroform soluble bitumen and volatilized bitumen) were investigated. During diagenesis the hydrocarbon potential of lignite decreased by 75% and that of the coals diminished approximately 50%. The zone of the catagenesis was reached at 350{degree}C by lignite and at 375{degree}C by coals. The coal-2 is somewhat more resistant to thermal degradation than coal-1. Various hydrocarbon classes (alkanes, alkenes, phyllocladanes, isoprenoids) were measured in non-aromatic hydrocarbon fractions. Volatile bitumens contained much more unsaturated hydrocarbons than the ...

1990-01-01

215

Extraction behavior of short-lived isotopes of Mo/W using {alpha}-benzoinoxime: a model system for the study of seaborgium  

Energy Technology Data Exchange (ETDEWEB)

The liquid-liquid extraction behavior of short-lived molybdenum and tungsten isotopes from HCl and HNO{sub 3} as well as HF/HNO{sub 3} acid media was studied using the {alpha}-benzoinoxime/chloroform system. The goal of the present experiments was to find an extraction system with a high selectivity for the group 6 elements in the periodic table which is suitable for the study the solution chemistry of seaborgium (Z = 106). It was found that Mo and W are both effectively extracted using {alpha}-benzoinoxime as an extractant and the maximum extraction yield is 100% and 94% for Mo and W, respectively. Ions of MO{sub 2}{sup 2+} (M = Mo, W) exist in HCl between the concentration range of 0.1-3 M and can be extracted quantitatively into the organic phase. The decrease of extraction yields at lower or higher acid concentration is due to the ...

2009-07-01

216

Extraction behavior of short-lived isotopes of Mo/W using #alpha#-benzoinoxime: a model system for the study of seaborgium  

International Nuclear Information System (INIS)

The liquid-liquid extraction behavior of short-lived molybdenum and tungsten isotopes from HCl and HNO_3 as well as HF/HNO_3 acid media was studied using the #alpha#-benzoinoxime/chloroform system. The goal of the present experiments was to find an extraction system with a high selectivity for the group 6 elements in the periodic table which is suitable for the study the solution chemistry of seaborgium (Z = 106). It was found that Mo and W are both effectively extracted using #alpha#-benzoinoxime as an extractant and the maximum extraction yield is 100% and 94% for Mo and W, respectively. Ions of MO_2"2"+ (M = Mo, W) exist in HCl between the concentration range of 0.1-3 M and can be extracted quantitatively into the organic phase. The decrease of extraction yields at lower or higher acid concentration is due to the formation of anionic ...

217

Total phenolic content and antioxidant capacity of extracts obtained from six important fruit residues  

British Library Electronic Table of Contents (United Kingdom)

The extracts from kinnow peel, kinnow seeds, litchi pericarp, litchi seeds, grape seeds, and banana peel were screened for total phenolic content (TPC), trolox equivalent antioxidant capacity (TEAC), 1,1 diphenyl-2-picryl hydrazyl (DPPH) radical scavenging activity, as well as reducing power. Kinnow peel extract exhibited the highest reducing power, TEAC, and DPPH free radical scavenging activity, whereas, the phenolic content of 37.4 mg GAE/g-dw was highest for grape seed extract. Banana peel extract with a low TPC showed the lowest reducing power, TEAC as well as DPPH free radical scavenging activity among the fruit residue extracts examined in the present study. Correlation analysis between the reducing power and DPPH radical scavenging ability; reducing power and ABTS radical scavengin...

2011-01-01

218

Phytochemical study of the decoct from the leaves of Maytenus Truncata Reissek and the evaluation of the antinociceptive, antiedematogenic and antiulcerogenic activities of the decoct extracts  

International Nuclear Information System (INIS)

The present paper describes the phytochemical investigation and biological activities of the chloroform, ethyl acetate and methanol extracts of leaf decocts of M. truncata Reiss (Celastraceae). Our studies afforded two flavonoid glycosides, quercetin-3-O-rhamnopyranosyl-O-glucopyranosyl- O-rhamnopyranosyl-O-galactopyranoside (1) and kampferol-3-O-rhamnopyranosyl-O-glucopyranosyl- O-rhamnopyranosyl-O-galactopyranoside (2) from the methanolic extract and dulcitol (3) from the ethyl acetate extract. Ethyl acetate and methanol extracts exhibited considerable antiulcerogenic and analgesic activities. The results of the phytochemical studies suggest that the healing activity of methanol extracts can be related to the presence of glycosyl flavonoids. (author)

219

Optimisation of pectin acid extraction from passion fruit peel (Passiflora edulis flavicarpa) using response surface methodology  

British Library Electronic Table of Contents (United Kingdom)

Summary Pectin was extracted from passion fruit peel using three different acids (citric, hydrochloric or nitric) at different temperatures (40-90 degreeC), pH (1.2-2.6) and extraction times (10-90 min), with and without skins using a 24 factorial design. Temperature, pH and extraction time had highly significant effects on the pectin yield. A central composite design with face centring was used to optimise the extraction process conditions for citric acid without skins. Pectin yields varied from 10% to 70%. The optimal conditions for maximisation of pectin yield were the use of citric acid at 80 degreeC and pH 1 with an extraction time of 10 min considering model extrapolation.

2009-01-01

220

Inhibition effects on fermentation of hardwood extracted hemicelluloses by acetic acid and sodium  

British Library Electronic Table of Contents (United Kingdom)

Extraction of hemicellulose from hardwood chips prior to pulping is a possible method for producing ethanol and acetic acid in an integrated forest bio-refinery, adding value to wood components normally relegated to boiler fuel. Hemicellulose was extracted from hardwood chips using green liquor, a pulping liquor intermediate consisting of aqueous NaOH, Na2CO3, and Na2S, at 160degreeC, held for 110min in a 20L rocking digester. The extracted liquor contained 3.7% solids and had a pH of 5.6. The organic content of the extracts was mainly xylo-oligosaccharides and acetic acid. Because it was dilute, the hemicellulose extract was concentrated by evaporation in a thin film evaporator. Concentrates from the evaporator reached levels of up to 10% solids. Inhibitors such as acetic acid and sodium ...

2010-01-01

221

Comparative studies on the characterization and antioxidant properties of biodegradable alginate films containing ginseng extract  

British Library Electronic Table of Contents (United Kingdom)

The physical and antioxidant properties of alginate biodegradable film incorporating white, red and extruded white ginseng extracts were investigated. No differences in moisture contents of all alginate film samples were noticeable (p>0.05) except those film samples incorporated without ginseng extract, which had the highest moisture content. The addition of ginseng extract to alginate film decreased tensile strength and elastic modulus (p<0.05) but increased the percent elongation at break. The presence of extracts did not significantly affect the water vapor permeability of the film samples. Alginate film containing extruded white ginseng extract at a barrel temperature of 130degreeC presented the highest (61.12%) free-radical scavenging activity against the 2,2-diphenyl-1-picryhydrazyl ...

2010-01-01

222

CTH-process for HLLW treatment. Pt. 1  

Energy Technology Data Exchange (ETDEWEB)

A process for separation of actinides and technetium from reprocessing high level liquid waste has been developed, the CTH-process. The main parts are three consecutive solvent extraction cycles followed by an optional step for sorption on inorganic ion exchangers. The first extraction cycle removes and recovers uranium, neptunium, and plutonium by extraction with HDEHP. The second extraction cycle separates technetium and nitric acid from the waste using TBP. In the third extraction cycle Am and Cm are separated from the waste using HDEHP. The actinide free waste is then passed through inorganic ion exchangers to remove most of remaining radionuclides. The process has been tested on an authenic HLLW solution. A decontamination factor > 10/sup 5/ for alpha emitters was measured for the solvent extraction process and the sorption on inorganic ion exchangers ...

1984-01-01

223

Beam extraction studies at 900 GeV using a channeling crystal  

CERN Document Server

Luminosity-driven channeling extraction has been observed for the first time in a 900 GeV study at the Fermilab Tevatron. This experiment, Fermilab E853, demonstrated that useful TeV level beams can be extracted from a superconducting accelerator during high luminosity collider operations without unduly affecting the background at the collider detectors. Multi-turn extraction was found to increase significantly the efficiency of the process. The beam extraction efficiency was about 25%. Studies of time dependent effects found that the turn-to-turn structure was governed mainly by accelerator beam dynamics. An investigation of a pre-scatterer using the accelerator flying wire system showed that a fiber could produce a significant extracted flux, consistent with expectations. Based on these results, it is feasible to construct a parasitic 5-10 MHz proton beam from the Tevatron ...

1999-01-01

224

Automatic sample preparation of sulfonamide antibiotic residues in chicken breast muscle by using dynamic microwave-assisted extraction coupled with solid-phase extraction  

British Library Electronic Table of Contents (United Kingdom)

Abstract In the work, a rapid, simple and high-throughput sample preparation method was developed for the determination of sulfonamide (SA) antibiotic residues in chicken breast muscle. The extraction and clean-up were online combined and up to 20 samples can be treated simultaneously in 6-min. The SAs were first extracted with acetonitrile under the action of microwave energy, and then the extract was directly introduced into the SPE column for on-line clean-up and concentration. Subsequently, the SAs eluted from the SPE column were determined by liquid chromatography-tandem mass spectrometry. The precisions of extraction results of 20 samples were in the range of 4.9-7.4%. The limits of detection and quantification obtained were in the range of 2.4-3.6-ng/g and 8.6-11.3-ng/g for SAs, res...

2011-01-01

225

The Effect of Different Timber Harvesting Techniques on Plethadontid Salamander Populations.  

Science.gov (United States)

This investigation will explore the effect that current timber extraction techniques have on plethadontid salamander populations in ... group selection, and two-age harvest. Broad scale timber extraction can d...

226

Selected Physical and Chemical Properties of Feverfew (Tanacetum parthenium) Extracts Important for Formulated Product Quality and Performance  

UK PubMed Central (United Kingdom)

The objectives of this research are: (1) to assess selected formulation-relevant physical properties of several commercial Feverfew extracts, including flowability, hygroscopicity, compressibility and...Full Text Available

227

Scenario Customization for Information Extraction.  

Science.gov (United States)

Information Extraction (IE) is an emerging NLP technology, whose function is to process unstructured, natural language text, to locate specific pieces of information, or facts, in the text, and to use these facts to fill a database. IE systems today are c...

2001-01-01

228

Requirements for Extraction of Polyribosomes from Plant Callus Cultures 1  

UK PubMed Central (United Kingdom)

A procedure was developed to isolate polyribosomes from plant cell cultures. Tobacco callus extracted in 10 mm MgCl2, 80 mm KCl, 250 mm sucrose, and 140 mm...Full Text Available

1977-05-01

229

Proteinases and Enzyme Stability in Crude Extracts of Castor Bean Endosperm 1  

UK PubMed Central (United Kingdom)

The stability of catalase, fumarase, and isocitrate lyase from deliberately broken organelles in crude extracts from endosperm tissue of castor bean seedlings has been examined. These enzymes are relatively...Full Text Available

1981-03-01

230

Polysaccharides in germination. Xyloglucans (`amyloids') from the cotyledons of white mustard  

UK PubMed Central (United Kingdom)

Two xyloglucan fractions have been isolated from the cotyledons of resting white-mustard seeds, the first by extraction with hot EDTA, and the second by subsequent extraction with alkali or lithium...Full Text Available

1971-08-01

231

PASBio: predicate-argument structures for event extraction in molecular biology  

UK PubMed Central (United Kingdom)

BackgroundThe exploitation of information extraction (IE), a technology aiming to provide instances of structured representations from free-form text, has been rapidly growing within...Full Text Available

232

NF-kappaB mediates the survival of human bronchial epithelial cells exposed to cigarette smoke extract  

UK PubMed Central (United Kingdom)

BackgroundWe have previously reported that low concentrations of cigarette smoke extract induce DNA damage without leading to apoptosis or necrosis in human bronchial epithelial...Full Text Available

2008-01-01

233

Hepatoprotective Effects of Orthosiphon stamineus Extract on Thioacetamide-Induced Liver Cirrhosis in Rats  

UK PubMed Central (United Kingdom)

Orthosiphon stamineus as medicinal plant is commonly used in Malaysia for treatment of hepatitis and jaundice; in this study, the ethanol extracts were applied to evaluate the...Full Text Available

2011-01-01

234

Extraction of immune and inflammatory cells from human lung parenchyma: evaluation of an enzymatic digestion procedure.  

UK PubMed Central (United Kingdom)

The inflammatory and immune cell populations of the human lung parenchyma have not been characterized in detail. This report describes a novel and efficient procedure for their extraction. Histologically...Full Text Available

1986-10-01

235

Energy extraction (a reversible process) from a Kerr source by tachyons  

International Nuclear Information System (INIS)

The author demonstrates through a specific example that it is possible to extract rotational energy from a Kerr source (in principle, of arbitrary size but not turned black) through a reversible process by suitably injecting tachyons. (Auth.).

236

Effect of extraction conditions on the quality characteristics of pectin from passion fruit peel (Passiflora edulis f. flavicarpa L.)  

British Library Electronic Table of Contents (United Kingdom)

Passion fruit (Passiflora edulis f. flavicarpa L.) yellow variety is composed of 50-55g peel per 100g of fresh fruit which is discarded as waste during processing. Utilization of passion fruit peel for pectin extraction was studied. Passion fruit peel obtained after juice extraction was blanched in boiling water for 5min, dehydrated in a cross flow hot air drier at 60+-1degreeC to a moisture content of 4g/100g of dried peel. The dehydrated passion fruit peel was used for extraction experiments of pectin. The effect of pH, peel to extractant ratio, and number of extractions, extraction time and temperature on the yield and quality characteristics of pectin were investigated. The optimized conditions for extraction of pectin from passion fruit peel yielded 14.8g/100g of dried peel. Pectin ex...

2010-01-01

237

Comparative Evaluation of Three Commercial Systems for Nucleic Acid Extraction from Urine Specimens  

UK PubMed Central (United Kingdom)

A nucleic acid extraction system that can handle small numbers of specimens with a short test turnaround time and short hands-on time is desirable for emergent testing. We performed a comparative validation...Full Text Available

2005-09-01

238

Benz(a)pyrene levels in medicinal plants and the possibility of contamination of drugs of plant origin  

Energy Technology Data Exchange (ETDEWEB)

Benz(a)pyrene (BP) levels in extracts and solvent cake obtained by alcoholic and aqueous extraction of specimens of 20 different medicinal plants were measured to explore into the possibility of its passage from these plants to drugs. Seventy percent alcoholic extracts were found to contain 40-60% of BP passed from raw material, while aqueous extracts--2-3% (in some cases 10-14%). Maximal concentrations of BP in alcoholic extracts were 0.6-0.7 micrograms/1 and 0.03-0.04 micrograms/1--in aqueous ones. A significant correlation between BP level in extracts and its content in plants was established. BP pathways in the course of solasodine manufacturing from nightshade (Solanum lacinatum) were studied. As little as 1% of BP passed to extract after primary extraction in 2%--sulfuric acid. Solasodine contained about 3 ...

1983-01-01

239

Antipyretic and antibacterial activity of Chloranthus erectus (Buch.-Ham.) Verdcourt leaf extract: A popular folk medicine of Arunachal Pradesh  

UK PubMed Central (United Kingdom)

Objective:The main objective of this work was to study the antipyretic and antibacterial activity of C. erectus (Buch.-Ham.) Verdcourt leaf extract in an...Full Text Available

2010-10-01

240

Anti-ulcerogenic and in vitro antioxidant activities of Lagenaria breviflora (LB) whole fruit ethanolic extract in laboratory animals  

UK PubMed Central (United Kingdom)

Background:The present study was undertaken to evaluate the anti-ulcer and antioxidant activities of the ethanol extract of Lagenaria breviflora (EELB)...Full Text Available

2011-01-01

241

Anion-exchange extraction of cephapirin, cefotaxime, and cefoxitin from serum for liquid chromatography.  

UK PubMed Central (United Kingdom)

An anion-exchange column technique for extraction of antibiotics from serum proteins has been developed for use in the assay of cephapirin, cefotaxime, and cefoxitin by high-pressure liquid chromatography....Full Text Available

1982-04-01

242

An experimental evaluation of the antidiabetic and antilipidemic properties of a standardized Momordica charantia fruit extract  

UK PubMed Central (United Kingdom)

BackgroundThe MCE, Momordica charantia fruit extract Linn. (Cucurbitaceae) have been documented to elicit hypoglycemic activity on various occasions. However, due...Full Text Available

249
250

Isolation of carrier-free tantalum radioisotopes from proton-irradiated hafnium  

International Nuclear Information System (INIS)

... carrier-free isotopes hafnium compounds irradiation protons solvent extraction

251

Inorganic astatine chemistry: Formation of complexes of astatine  

Energy Technology Data Exchange (ETDEWEB)

The nature and properties of inorganic /sup 211/At-species formed in aqueous solutions under alkaline, neutral, acidic and oxidative conditions are studied through extraction of At with a variety of organic solvents, followed by the determination of the chromatographic, re-extraction and interaction behaviour of the extracted activity. It is concluded from the Rsub(f) values (on SiO/sub 2/) and the different affinities for a large amount of additives, that the extracted activity - formerly denoted as At-zero - exists of AtX compounds that may form AtXLsub(u) complexes, depending on the kind of solvent (L) used.

1983-01-01

252

Inorganic astatine chemistry: Formation of complexes of astatine  

International Nuclear Information System (INIS)

The nature and properties of inorganic "2"1"1At-species formed in aqueous solutions under alkaline, neutral, acidic and oxidative conditions are studied through extraction of At with a variety of organic solvents, followed by the determination of the chromatographic, re-extraction and interaction behaviour of the extracted activity. It is concluded from the Rsub(f) values (on SiO_2) and the different affinities for a large amount fo additives, that the extracted activity - formerly denoted as At-zero - exists of AtX compounds that may form AtXLsub(u) complexes, depending on the kind of solvent (L) used. (orig.).

254

Extraction and purification of free oligosaccharides in Maytenus ilicifolia  

International Nuclear Information System (INIS)

English 2005 [1 p.] Brazil Uratani, JM Cipriani, TR Mellinger, CG Gorin,

2005-07-02

255

Effects of timber extraction on herb diversity in the Little Tennessee watershed.  

Science.gov (United States)

... study is to collect data in previously harvested timber stands to quantify the differences in herbaceous diversity ... ...

261

Potential Increases in Mortality due to Global Warming  

Science.gov (United States)

... predicting potential increases in human mortality due to global warming....

262

POTENTIATION BY PENTOBARBITAL OF THE PROTECTIVE ...  

Science.gov (United States)

... Accession Number : AD0268549. Title : POTENTIATION BY PENTOBARBITAL OF THE PROTECTIVE EFFECT OF AET AGAINST GAMMA RAYS. ...

1961-10-01

263

Semi-automatic system for designing operations in a face  

Energy Technology Data Exchange (ETDEWEB)

A semi-automatic system which considers operation in a face by monitoring technological parameters of an extraction vehicle and a longwall conveyor is examined. The system records in tabular form the location, progress made, operating and down time of an extraction vehicle and operating and down time of the conveyor. A description of the operating principle system and systems for arrangement of the remote sensing and central recording device are presented. (Note: extraction vehicle not identified: LTN)

1980-01-01

264

On energetics of a charged black hole relative to tachyons  

International Nuclear Information System (INIS)

The author considers the extraction of the electromagnetic energy from a charged black hole through charged tachyons. The 'generalized ergosphere' relative to tachyons is defined. It turns out that it is possible to extract energy with 100% efficiency (through reversible process) if the charged source (whether black hole or otherwise) is of finite size. Two explicit examples of energy extraction are discussed. (Auth.).

265

Formation of non-extractable pesticide residues: observations on compound differences, measurement and regulatory issues  

Energy Technology Data Exchange (ETDEWEB)

Six major use pesticides (Atrazine, Dicamba, Isoproturon, Lindane, Paraquat and Trifluralin) with differing physico-chemical properties were evaluated for the significance of 'bound' or non extractable residue formation. Investigations were carried out in purpose-built microcosms where mineralization, volatilisation, 'soil water' extractable and organic solvent extractable residues could be quantified. Extractable residues were defined as those accessible by sequential extraction where the solvent used became increasingly non-polar. Dichloromethane was the 'harshest' solvent used at the end of the sequential extraction procedure. {sup 14}C-labelled volatilised and {sup 14}CO{sub 2} fractions were trapped on exit from the microcosm. The pesticides were categorised into 3 classes based on their behaviour. (i) ...

2005-01-01

266

Effects of gamma irradiation on microbial contamination and extraction yields of Korean medicinal herbs  

Energy Technology Data Exchange (ETDEWEB)

Effects of gamma irradiation on hygienic quality and extraction yields in twenty-one kinds of Korean medicinal herbs were investigated. Gamma irradiation at 5-10 kGy inactivated contaminating microorganisms. The total extraction yield in fifteen kinds of the investigated medicinal herbs increased by 5-25% by a dose of 10 kGy. (author)

2000-01-01

267

Anomalous solvent extraction behavior of astatine  

International Nuclear Information System (INIS)

We studied the solvent extraction behavior of astatine and found the anomalous behavior of this element similar to radioiodine. Astatine was extracted into CS_2 from acidic solution over a wide range of carrier iodine concentration. The distribution ratios of astatine were determined by measuring the #gamma#-ray from 210 At with a NaI(Tl) detector. A drastic change was observed around at 10"-"4 mol/l as in the case of 131 l. This tendency is well explained by the kinematics of the chemical reactions concerned. (author).

268

Development of a computerized portal verification scheme for pelvic treatment fields  

International Nuclear Information System (INIS)

Purpose/Objective: At present, treatment verification between portal and reference images is performed based on manually-identified features by radiation oncologist, which is both time-consuming and potentially error-prone. There is a demand for the computerized verification procedure in clinical application. The purpose of this study is to develop a computerized portal verification scheme for pelvic treatment fields. Materials/Methods: The automated verification system involves image acquisition, image feature extraction, feature matching between reference and portal images and quantitative evaluation of patient setup. Electronic portal images with a matrix size of 256 x 256 and 12 bit gray levels were acquired using a liquid matrix electronic portal imaging device. Simulation images were acquired by digitizing simulation films using a TV camera into images with 256 x 256 matrix and 8 bit gray levels. Initially a Canny edge detector is applied ...

1996-09-01

269

Observation of high permittivity in Ho substituted BaZr_0_._1Ti_0_._9O_3 ceramics  

International Nuclear Information System (INIS)

The authors observed an extremely high permittivity (#approx#35 000 at T_C) in barium zirconate titanate (BaZr_0_._1Ti_0_._9O_3) ceramics with holmium substitution (1-5 mol %) in Ba site. Careful microstructural investigation and energy dispersive spectroscopy analysis of the 1-2 mol % of Ho substituted ceramics showed the enrichment of a Ho-phase along the grain boundaries with a composition close to the Ho_2Ti_2O_7 pyrochlore. The formation of Ho rich phase resulted in the Maxwell-Wagner polarization mechanism, which leads to this unusually high permittivity. Ceramics with 3 mol % or higher Ho content showed lesser permittivity values compared to 1-2 mol %, probably due to the increase in pyrochlore phase. These high dielectric constant ceramics are useful in nanoscale devices.

2007-07-09

270

Local structure of Ca dopant in BaTiO_3 by Ca K-edge X-ray absorption near-edge structure and first-principles calculations  

International Nuclear Information System (INIS)

The local environment of Ca dopants in barium titanate, BaTiO_3, is investigated by Ca K-edge X-ray absorption near-edge structure (XANES) spectroscopy. In conjunction with experiments, first-principles calculations by two methods are systematically made. The projector-augmented wave (PAW) method is used to optimize the local structure and obtain the formation energy. The augmented plane wave plus local orbitals method is adopted to obtain theoretical XANES spectra. A comparison between experimental and theoretical XANES spectra shows that Ca dopants are located at the Ba"2"+ sites forming Ca"2"+. Formation energy calculations of Ca doped BaTiO_3 by the PAW method also give the same results. The Ca atom in BaTiO_3 is off-centering in comparison with the Ba site in BaTiO_3. The off-centering of Ca atom is newly revealed by the combination of XANES spectroscopy and first-principles DFT calculations.

2010-06-01

271

Effect of Ho^3^+ substitutions on the structural and magnetic properties of BaFe12O19 hexaferrites  

British Library Electronic Table of Contents (United Kingdom)

Holmium doped barium based hexaferrites BaFe12-2xHo2xO19 with (x=0.0-1.0) were synthesized by solid state reaction method. Structural and magnetic characterization of these ferrites provide significant information about their reactive physical properties. X-ray analysis reveals that in all samples M-type structure exist with few secondary phases. Scanning electron microscope revealed the grain size of the specimen. The results show that grain size decreases with the substitution degree of Holmium. Thus rare earth element Holmium Ho^3^+ acts as a grain growth inhibitor. The magnetic hysteresis loops show the variation in the values of magnetic parameters like saturation magnetization (Ms), remanent magnetization (Mr) and coercivity (Hc) were observed by changing Ho^3^+ content in BaFe12-2xH...

2010-01-01

272

Effect of Ho"3"+ substitutions on the structural and magnetic properties of BaFe_1_2O_1_9 hexaferrites  

International Nuclear Information System (INIS)

Holmium doped barium based hexaferrites BaFe_1_2_-_2_xHo_2_xO_1_9 with (x = 0.0-1.0) were synthesized by solid state reaction method. Structural and magnetic characterization of these ferrites provide significant information about their reactive physical properties. X-ray analysis reveals that in all samples M-type structure exist with few secondary phases. Scanning electron microscope revealed the grain size of the specimen. The results show that grain size decreases with the substitution degree of Holmium. Thus rare earth element Holmium Ho"3"+ acts as a grain growth inhibitor. The magnetic hysteresis loops show the variation in the values of magnetic parameters like saturation magnetization (M_s), remanent magnetization (M_r) and coercivity (H_c) were observed by changing Ho"3"+ content in BaFe_1_2_-_2_xHo_2_xO_1_9 ferrites. Coercivity showed a maximum value of 2230 Oe for (x = 0.4) and then decreasing trend were observed in the values of H_c, M_r and M_s with ...

2010-04-09

273

Dielectric properties of fluxed barium titanate ceramics with zirconia additions  

Energy Technology Data Exchange (ETDEWEB)

BaTiO{sub 3} compacts, when fluxed with {lt} 2 vol% of a complex borate glass phase, were sintered to near theoretical density at temperatures {lt} 1175{degrees}C in 2 h. Microstructural analysis showed a uniform grain size {lt} 1.0 {mu}m with 0.75 wt% ZrO{sub 2} added to the flux phase as a grain growth inhibitor. TEM analysis revealed a microcrystalline grain-boundary phase with the ZrO{sub 2} resident along the grain boundaries. These samples displayed an essentially flat dielectric profile, low dissipation factors ({lt} 2%) over the range 25{degrees} to 125{degrees}C, a near linear dependence ({approx} {+-} 15%) between 25{degrees} and {minus} 55{degrees}C, and significantly increased voltage stability. X-ray diffraction analysis of these small-grained materials indicates a suppression of the tetragonal structure toward a more cubic modification.

1990-03-01

274

Dielectric properties of fluxed barium titanate ceramics with zirconia additions  

International Nuclear Information System (INIS)

BaTiO_3 compacts, when fluxed with < 2 vol% of a complex borate glass phase, were sintered to near theoretical density at temperatures < 1175 degrees C in 2 h. Microstructural analysis showed a uniform grain size < 1.0 #mu#m with 0.75 wt% ZrO_2 added to the flux phase as a grain growth inhibitor. TEM analysis revealed a microcrystalline grain-boundary phase with the ZrO_2 resident along the grain boundaries. These samples displayed an essentially flat dielectric profile, low dissipation factors (< 2%) over the range 25 degrees to 125 degrees C, a near linear dependence (#approx# #+-# 15%) between 25 degrees and - 55 degrees C, and significantly increased voltage stability. X-ray diffraction analysis of these small-grained materials indicates a suppression of the tetragonal structure toward a more cubic modification.

275

The anti-snake venom properties of Tamarindus indica (leguminosae) seed extract  

British Library Electronic Table of Contents (United Kingdom)

In Indian traditional medicine, various plants have been used widely as a remedy for treating snakebites. The aim of this study was to evaluate the effect of Tamarindus indica seed extract on the pharmacological as well as the enzymatic effects induced by V. russelli venom. Tamarind seed extract inhibited the PLA2, protease, hyaluronidase, L-amino acid oxidase and 5prime-nucleotidase enzyme activities of venom in a dose-dependent manner. These are the major hydrolytic enzymes responsible for the early effects of envenomation, such as local tissue damage, inflammation and hypotension. Furthermore, the extract neutralized the degradation of the Bb chain of human fibrinogen and indirect hemolysis caused by venom. It was also observed that the extract exerted a moderate effect on the clotting ...

2006-01-01

276

Quantification of Free and Bound Fractions of Nickel in Natural Waters by Solvent Extraction with 1,2-Cyclohexanedione Bis-Benzoyl-Hydrazone  

British Library Electronic Table of Contents (United Kingdom)

An hydrazone derivative, 1,2-cyclohexanedione bis-benzoyl-hydrazone (1,2-CHBBH), has been used as a selective reagent for an advanced environmental application consisting of separating the different species of nickel in natural waters by solvent extraction. The effects of pH and reagent concentration on the extraction process were studied, as well as the influence of both organic (humic acids) and inorganic ligands (Cl-). Under natural conditions, organic and inorganic nickel species presented different extraction behaviors, and the variations in extraction yields could be correlated with the concentrations of organic complexes in the samples, allowing the separation of labile and non-labile nickel species in both fresh and marine waters.

2010-01-01

277

PREPARATION AND PROPERTIES OF ANTIBACTERIAL ALGINATE FILMS INCORPORATING EXTRUDED WHITE GINSENG EXTRACT  

British Library Electronic Table of Contents (United Kingdom)

Abstract Preparation of antibacterial alginate films incorporating extruded white ginseng (EWG) extracts was attempted. The antibacterial effect of EWG extract on six selected food pathogenic bacteria was compared with the effect of red ginseng (RG) and white ginseng (WG) extracts. The EWG was processed in a twin-screw extruder with feed moisture of 20% and barrel temperature of 115 and 130C. The data obtained by agar diffusion assay demonstrated that the film containing 1-g/mL of EWG at barrel temperatures of 115 (EWG-115) and 130C (EWG-130) exhibited stronger antibacterial activity against the four strains of bacteria than the other extracts RG and WG. All films sampled showed reduction in bacteria cell counts (log cycle) compared with the control. After 24-h of incubation, Pseudomonas a...

2011-01-01

278

Isoflavone content and apoptotic effect in HT-29 cancer cells of a soy germ extract  

British Library Electronic Table of Contents (United Kingdom)

Colon cancer is one of the leading causes of death and a major public health problem in western countries. We examined the isoflavone content of 70% ethanol extract of soy germ (SG) and its apoptotic effect in HT-29 colon cancer cells. Our results showed that the major isoflavones of the SG extract were daidzein and genistein, and it effectively induced apoptosis in HT-29 cancer cells. In addition, nuclear factor-kappa B (NF-kB) expression was reduced in cells treated with the SG extract, which reduced cyclooxygenase-2 (COX-2) and nitric oxide synthase (iNOS) expression. These combined effects ultimately resulted in apoptosis via caspase-3 activation. In addition, daidzein and genistein, the major isoflavones of SG extract, also exerted the apoptotic effect against HT-29 cancer cells. Thes...

2012-01-01

279

Extracting mining subsidence land from remote sensing images based on domain knowledge  

Energy Technology Data Exchange (ETDEWEB)

Extracting mining subsidence land from remote sensing (RS) images is one of important research contents for environment monitoring in mining area. The accuracy of traditional extracting models based on spectral features is low. In order to extract subsidence land from RS images with high accuracy, some domain knowledge should be imported and new models should be proposed. This paper, in terms of the disadvantage of traditional extracting models, imports domain knowledge from practice and experience, converts semantic knowledge into digital information, and proposes a new model for the specific task. By selecting the Luan mining area as a study area, this new model is tested based on GIS and related knowledge. The result shows that the proposed method is more precise than traditional methods and can satisfy the demands of land subsidence monitoring in mining area. 10 refs., 4 figs., 1 tab.

2008-06-15

280

Supercritical fluid extraction from dried banana peel (Musa spp., genomic group AAB): Extraction yield, mathematical modeling, economical analysis and phase equilibria  

British Library Electronic Table of Contents (United Kingdom)

Supercritical fluid extraction from dried banana peel (Musa spp., subgroup Prata, genomic group AAB, popularly known in Brazil as Enxerto) was studied. The aspects investigated were: overall extraction curve (OEC), mass transfer modeling of the yield curves, economical analysis of the process and phase equilibrium data for the pseudo-ternary system of banana peel extract, carbon dioxide and ethanol. The extraction operating conditions evaluated were: pressure ranging from 100bar to 300bar, temperature from 40 to 50^oC and constant solvent flow rate of 5.0gCO2/min. Experimental extraction data were correlated using three kinetic models based on mass transfer equations (logistic, diffusion and Esquivel models). Phase equilibrium measurements were performed using pressure from 64.9bar to 239....

2010-01-01

281

Extraction of copper-, nickel-, zinc- and cadmium complexes with 4-(2-pyridilazo)-resorcin and 2-aminopyridine  

International Nuclear Information System (INIS)

Extraction of copper-, nickel-, zinc- and cadmium complexes with 4-(2 pyridilazo)-resorcin (PAR) is studied in the presence of 2-aminopyridine (Am). Maximum optical densities of the extracts are attained at pH=7.5-8.0; 6.0-7.0; 6.5-7.0 and 7.0-8.0, respectively. The ratio of components in the complexes extractable by chloroform was defined by the method of isomolar series and equilibrium shift. It is established that nickel and copper are extracted to the organic phase as the NiAm(PAR)_2 and CuAmPAR complexes, and, in the case of zinc and cadmium, complexes of different composition are extracted, for example Zn(Am)_2PAR and ZnAm(PAR)_2. The light absorption spectra are studied and molar extinction coefficients of complex extracts are determined at lambdasub(max). It is shown that the general low of light absorption is observed within a sufficiently wide range of ...

1984-01-01

282

Hybrid Combined Cycles with Biomass and Waste Fired Bottoming Cycle - a Literature Study  

Energy Technology Data Exchange (ETDEWEB)

Biomass is one of the main natural resources in Sweden. The present low-CO{sub 2} emission characteristics of the Swedish electricity production system (hydro and nuclear) can be retained only by expansion of biofuel applications for energy purposes. Domestic Swedish biomass resources are vast and renewable, but not infinite. They must be utilized as efficiently as possible, in order to make sure that they meet the conditions for sustainability in the future. Application of efficient power generation cycles at low costs is essential for meeting this challenge. This applies also to municipal solid waste incineration with energy extraction, which should be preferred to its dumping in landfills. Hybrid dual-fuel combined cycle units are a simple and affordable way to increase the electric efficiency of biofuel energy utilization, without big investments, uncertainties or loss of reliability arising from complicated technologies. Configurations of such power cycles are ...

2002-02-01

283

Guide to Combined Heat and Power Systems for Boiler Owners and Operators  

Energy Technology Data Exchange (ETDEWEB)

Combined heat and power (CHP) or cogeneration is the sequential production of two forms of useful energy from a single fuel source. In most CHP applications, chemical energy in fuel is converted to both mechanical and thermal energy. The mechanical energy is generally used to generate electricity, while the thermal energy or heat is used to produce steam, hot water, or hot air. Depending on the application, CHP is referred to by various names including Building Cooling, Heating, and Power (BCHP); Cooling, Heating, and Power for Buildings (CHPB); Combined Cooling, Heating, and Power (CCHP); Integrated Energy Systems (IES), or Distributed Energy Resources (DER). The principal technical advantage of a CHP system is its ability to extract more useful energy from fuel compared to traditional energy systems such as conventional power plants that only generate electricity and industrial boiler systems that only produce steam or hot water for process applications. By using ...

2004-08-19

284

Use of microbes for paraffin cleanup at Naval Petroleum Reserve No. 3  

Energy Technology Data Exchange (ETDEWEB)

Naval Petroleum Reserve No. 3 (NPR-3), also known as Teapot Dome, is a government-owned oil field in Natrona County, Wyoming. It is an asymmetrical anticline located on the western edge of the Powder River Basin, just south of the Salt Creek Anticline. Production started in 1922, and today the field is a marginally economic stripper field with average production of less than 3 BOPD (0.5 m{sup 3}/D) per well. Total field production is about 1,800 BOPD (286 m{sup 3}/D). The Second Wall Creek Formation was waterflooded from 1979 until June 1992 with poor results due to the extensive natural fracture system in this sandstone unit. Since water injection ceased, reservoir pressure has declined to very low levels. Liquids extraction and reinjection of the gas produced from high-GOR wells along the gas-oil contact continues, but the average gas cap pressure has fallen to approximately 150 psi (1.03 MPa) from an original pressure of 1,120 psi (7.72 MPa). Since the oil is ...

1995-12-31

285

The composition-explicit distillation curve technique: Relating chemical analysis and physical properties of complex fluids.  

Science.gov (United States)

The analysis of complex fluids such as crude oils, fuels, vegetable oils and mixed waste streams poses significant challenges arising primarily from the multiplicity of components, the different properties of the components (polarity, polarizability, etc.) and matrix properties. We have recently introduced an analytical strategy that simplifies many of these analyses, and provides the added potential of linking compositional information with physical property information. This aspect can be used to facilitate equation of state development for the complex fluids. In addition to chemical characterization, the approach provides the ability to calculate thermodynamic properties for such complex heterogeneous streams. The technique is based on the advanced distillation curve (ADC) metrology, which separates a complex fluid by distillation into fractions that are sampled, and for which thermodynamically consistent temperatures are measured at atmospheric pressure. The ...

2009-11-17

286

Sensors and instrumentation for atmospheric pollutions control; Capteurs et instrumentation pour le controle des pollutions atmospheriques  

Energy Technology Data Exchange (ETDEWEB)

Reinforcement of the legislation concerning the emission of atmospheric pollutants, aerosols, refrigerants, solvents etc and the reduction of the greenhouse effect, has led to the development of performing instruments for the survey and control of ambient air quality and for the limitation of exhaust gases, combustion products, volatile organic compounds (VOC), particulates and noxious compounds in the atmosphere. This study is divided in 4 main parts. The first part describes the context of the air quality control: the problems linked with the environment and health, the pollutants characteristics, the pollution levels and the detection sensitivity of instruments according to the different type of pollutants (petroleum products, VOCs, ozone compounds, particulates, smells..), the protocols of air pollution measurements and their application (chimney smokes, industrial volatile compounds, indoor and ambient air quality, exhaust gases from automobiles), and the French, European and ...

1996-11-01

287

Oxidation and adsorption of Co(II) EDTA{sup 2-} complexes in subsurface materials with iron and manganese oxide grain coatings  

Science.gov (United States)

Batch interaction experiments were performed under aerobic conditions to characterize the adsorption behavior and valence speciation of CoEDTA complexes (equimolar at 10{sup -5} mol/L) in a series of Pliocene subsurface sediments containing various amounts of Fe and Mn oxides. The experiments were performed in 0.003 mol/L Ca(ClO{sub 4}){sub 2} with a solids concentration of 500 g/L at variable pH (4-9) and at the natural pH of the sediments (pH = 8.3). Three of these subaerial sediments (Ringold 1, 2, 3) contained significant quantities of extractable Fe and Mn, while the fourth (Ringold 4) was virtually devoid of sesquioxide precipates. Microscopic and mineralogic analyses of the most heavily encrusted material (Ringold 2) showed that the oxides existed as intergrain cements and contained crystalline goethite and rancieite/todorokite. Adsorption on a synthetic analog sorbent (0.6 mass% ferrihydrite-coated sand) over a range in pH showed that, while both Co(II) ...

1995-11-01

288

Microbiological Comparison of Core and Groundwater Samples Collected from a Fractured Basalt Aquifier with that of Dialysis Chamber Incubated in Situ  

Energy Technology Data Exchange (ETDEWEB)

Microorganisms associated with fractured basalt core were compared to those suspended in groundwater pumped from the same well in the eastern Snake River Plain Aquifer (Idaho, USA). Two wells influenced to different degrees by a mixed-waste plume in the fractured basalt aquifer were examined. In one well, an array of dialysis cells filled with either deionized water or crushed basalt was equilibrated to compare the microorganisms collected in this fashion with those from core and groundwater samples collected in a traditional manner from the same well. Analyses were performed to characterize these samples and to provide a basis for comparison. These included total cell counts by microscopy; total biomass by phospholipid fatty acid analysis; enumerations of viable aerobic heterotrophs, groups of putative aerobic co-metabolic TCE-degraders and aerobic H2-oxidizing bacteria; mineralization of 14C- labeled acetate; and enrichments for dissimilatory iron-reducing bacteria. The 16S rDNA ...

2004-04-01

289

Local thermodynamic equilibrium and related metrological issues involving collisional-radiative model in laser-induced aluminum plasmas  

Energy Technology Data Exchange (ETDEWEB)

We present a collisional-radiative approach of the theoretical analysis of laser-induced breakdown spectroscopy (LIBS) plasmas. This model, which relies on an optimized effective potential atomic structure code, was used to simulate a pure aluminum plasma. The description of aluminum involved a set of 220 atomic levels representative of three different stages of ionization (Al{sup 0}, Al{sup +} and Al{sup ++}). The calculations were carried for stationary plasmas, with input parameters (n{sub e} and T{sub e}) ranging respectively between 10{sup 13-18} cm{sup -3} and 0.3-2 eV. A comparison of our atomic data with some existing databases is made. The code was mainly developed to address the validity of the local thermodynamic equilibrium (LTE) assumption. For usual LIBS plasma parameters, we did not reveal a sizeable discrepancy of the radiative equilibrium of the plasma towards LTE. For cases where LTE was firmly believed to stand, the Boltzmann plot outputs of this ...

2009-10-15

290

Local thermodynamic equilibrium and related metrological issues involving collisional-radiative model in laser-induced aluminum plasmas  

International Nuclear Information System (INIS)

We present a collisional-radiative approach of the theoretical analysis of laser-induced breakdown spectroscopy (LIBS) plasmas. This model, which relies on an optimized effective potential atomic structure code, was used to simulate a pure aluminum plasma. The description of aluminum involved a set of 220 atomic levels representative of three different stages of ionization (Al0, Al+ and Al++). The calculations were carried for stationary plasmas, with input parameters (ne and Te) ranging respectively between 1013-18 cm-3 and 0.3-2 eV. A comparison of our atomic data with some existing databases is made. The code was mainly developed to address the validity of the local thermodynamic equilibrium (LTE) assumption. For usual LIBS plasma parameters, we did not reveal a sizeable discrepancy of the radiative equilibrium of the plasma towards LTE. For cases where LTE was firmly believed to stand, the Boltzmann plot outputs of this code were used to check the physical ...

2009-10-01

291

Hydrotreat used lube oil  

Energy Technology Data Exchange (ETDEWEB)

Mild hydrotreating is the key to successful re-refining of used lubricating oils. Coupled with pre-distillation and metals removal, the process produces oil of superior color and clarity with acceptable viscosity and heteroatom content. Furthermore, the entire process provides operational simplicity, economic feasibility and environmental attractiveness. Re-refining preserves a valuable resource while solving a potential environmental problem. Increased sensitivity to disposal of hazardous material once again makes re-refining almost a necessity. Various technologies developed to re-refine used lubricating oils range from simple acid/clay contacting to complex solvent extraction. Most technologies require similar capital investment; however, operating costs vary substantially. Current technology seems to converge on a two-step procedure: distillation of dehydrated used oil in a thin-film evaporator, and subsequent hydrotreating of distilled ...

1986-04-01

292

Honokiol-mediated inhibition of PI3K/mTOR pathway: a potential strategy to overcome immunoresistance in glioma, breast, and prostate carcinoma without impacting T cell function.  

Science.gov (United States)

Inhibition of the phosphoinositide 3-kinase (PI3K)/mammalian target of rapamycin (mTOR) pathway is an appealing method for decreasing the immunoresistance and augmenting T cell-mediated immunotherapy. A major impediment to this strategy is the impact of conventional PI3K/mTOR pathway inhibitors on T cell function. In particular, rapamycin, is a well-known immunosuppressant that can decrease the activity of the PI3K/mTOR pathway in tumor cells, but also has a profound inhibitory effect on T cells. Here we show that Honokiol, a natural dietary product isolated from an extract of seed cones from Magnolia grandiflora, can decrease PI3K/mTOR pathway-mediated immunoresistance of glioma, breast and prostate cancer cell lines, without affecting critical proinflammatory T cell functions. Specifically, we show that at doses sufficient to down-regulate levels of phospho-S6 and the negative immune regulator B7-H1 in tumor cells, Honokiol does not significantly impair T cell ...

293

High-Performance, Superparamagnetic, Nanoparticle-Based Heavy Metal Sorbents for Removal of Contaminants from Natural Waters  

Energy Technology Data Exchange (ETDEWEB)

We describe the synthesis and characterization of superparamagnetic iron oxide nanoparticle based heavy metal sorbents with various surface chemistries that demonstrate an excellent affinity for the separation of heavy metals in contaminated water systems (i.e. spiked Columbia river water). The magnetic nanoparticle sorbents are prepared from an easy to synthesize iron oxide precursor, followed by a simple, one-step ligand exchange technique to introduce the organic surface functionality of interest chosen to target either specific or broader classes of heavy metals. Functionalized superparamagnetic nanoparticles are excellent sorbent materials for the extraction of heavy metal contaminants from environmental and clinical samples since they are easily removed from the media once bound to the contaminant by simply applying a magnetic field. These engineered magnetic nanoparticle sorbents have an inherently high active surface area (often > 100 m2/g), allowing for ...

2010-06-01

294

Evaluation of diagnostic ability of CCD digital radiography in the detection of incipient dental caries  

Energy Technology Data Exchange (ETDEWEB)

The purpose of this experiment was to evaluate the diagnostic ability of a CCD-based digital system (CDX-2000HQ) in the detection of incipient dental caries. 93 extracted human teeth with sound proximal surfaces and interproximal artificial cavities were radiographed using 4 imaging methods. Automatically processed No.2 Insight film (Eastman Kodak Co., U.S.A.) was used for conventional radiography, scanned images of conventional radiograms for indirect digital radiography were used. For the direct digital radiography, the CDX-2000HQ CCD system (Biomedisys Co. Korea) was used. The subtraction images were made from two direct digital images by Sunny program in the CDX-2000HQ system. Two radiologists and three endodontists examined the presence of lesions using a five-point confidence scale and compared the diagnostic ability by ROC (Receiver Operating Characteristic) analysis and one way ANOVA test. The mean ROC areas of conventional radiography, indirect digital ...

2003-03-15

295

Evaluation of diagnostic ability of CCD digital radiography in the detection of incipient dental caries  

International Nuclear Information System (INIS)

The purpose of this experiment was to evaluate the diagnostic ability of a CCD-based digital system (CDX-2000HQ) in the detection of incipient dental caries. 93 extracted human teeth with sound proximal surfaces and interproximal artificial cavities were radiographed using 4 imaging methods. Automatically processed No.2 Insight film (Eastman Kodak Co., U.S.A.) was used for conventional radiography, scanned images of conventional radiograms for indirect digital radiography were used. For the direct digital radiography, the CDX-2000HQ CCD system (Biomedisys Co. Korea) was used. The subtraction images were made from two direct digital images by Sunny program in the CDX-2000HQ system. Two radiologists and three endodontists examined the presence of lesions using a five-point confidence scale and compared the diagnostic ability by ROC (Receiver Operating Characteristic) analysis and one way ANOVA test. The mean ROC areas of conventional radiography, indirect digital ...

2003-03-01

296

Environmental radioactivity on Suape (PE) estuary: impact of the installation of an oil refinery  

Energy Technology Data Exchange (ETDEWEB)

Nowadays there is a growing interest in the study of natural radioactivity levels, mainly of radionuclides; {sup 238}U, {sup 226}Ra, {sup 232}Th, {sup 40}K, and {sup 210}Pb present in the environment. The environmental radioactivity control is very important to obtain information on exposure of humans and vegetables to potential sources on natural radioactive occurrences. Industrial processes involving mining and extraction and production of oil foster concentration of radionuclides, contributing to the occurrence of what is known as 'TENORM' - Technologically Enhanced Naturally Occurring Radioactive Material. This work aims to assess the environmental radiological impact on the estuarine area of the Industrial Park of SUAPE, due the installation of an oil refinery and the consequent introduction on the environment of natural radioactive materials from other regions in that area. The radioisotopes {sup 238}U, {sup 226}Ra, {sup ...

2009-07-01

297

Electron-beam-plasma ion source as source of negative fluorine  

Energy Technology Data Exchange (ETDEWEB)

Radioactive ion beams (RIBs) of short-lived isotopes of fluorine are in demand for investigating astrophysical phenomena related to the hot CNO cycle and rp processes responsible for stellar nucleosynthesis. Since negative ion beams are required for injection into tandem electrostatic accelerators, such as the 25 MV tandem accelerator used for post acceleration of RIBs for the Holifield Radioactive Ion Beam Facility (HRIBF) research program at the Oak Ridge National Laboratory (ORNL), efficient, direct-formation F{sup -} ion sources are highly desirable for RIB applications involving this type of post-accelerator. We have conceived and evaluated a direct extraction F{sup -} source for potential RIB applications which is predicated on the reverse polarity operation of a positive electron-beam-plasma target/ion source (EBPTIS) while simultaneously feeding fluorine rich compounds and Cs vapor into the source. The source is found to operate in two ...

1997-11-01

298

Economic analysis of proposed effluent limitations guidelines and standards for synthetic-based drilling fluids and other non-aqueous drilling fluids in the oil and gas extraction point source category  

Science.gov (United States)

The Economic Analysis (EA) report is written to address the impacts of this proposed Effluent Limitation Guidelines and Standards for Synthetic-Based and Other Non-Aqueous Drilling Fluids. Currently, effluent guidelines pertaining to the discharge of drilling fluids address two specific types of fluids: Oil-based drilling fluids (OBFs) that use diesel and mineral oil, which are prohibited from being discharged; and Water-based drilling Fluids (WBFs), which can be discharged subject to meeting certain discharge requirements, including a sheen test and an aqueous toxicity test, in certain limited offshore regions. Section Two presents sources of data, Section Three presents the industry profile, Section Four discusses the regulatory costs of options under consideration for the proposed rulemaking, and Section Five discusses the impacts of the proposed rule on firms, well drilling, and production, and also briefly discusses secondary impacts such as those on employment, output, inflation, ...

1999-02-01

299

Development of engineering parameters for the design of metal biosorption waste treatment systems  

Energy Technology Data Exchange (ETDEWEB)

Untreated landfill leachates and wastes from metal plating and mining operations are sources of environmental contamination by heavy metals. Because of their toxicity and potential for accumulation, the discharge of heavy metals must be controlled. Standard physical and chemical treatments used to remove metals from wastes such as concentration by electro-precipitation, ion exchange, solvent extraction, evaporative recovery, and conventional precipitation, are usually expensive and produce high quantities of sludge. Biosorption is the removal of metals from aqueous solutions by microorganisms. It is called biosorption rather than bioadsorption or bioaccumulation because the mechanisms of removal are not restricted to adsorption or metabolic uptake and so the more general term is preferable and has come to be accepted. In this thesis the focus is one two microorganisms and two metals. However, the possible combinations of conditions such as pH, ...

1991-12-03

300

Contributions of pesticide residue chemistry to improving food and environmental safety: past and present accomplishments and future challenges.  

Science.gov (United States)

The principles of modern pesticide residue chemistry were articulated in the 1950s. Early authors pointed out the advantages of systematizing and standardizing analytical methods for pesticides so that they could be widely practiced and the results could be reproduced from one laboratory to the next. The availability of improved methods has led to a much more complete understanding of pesticide behavior and fate in foods and the environment. Using methods based largely upon gas chromatography (GC) and high-performance liquid chromatography (HPLC) coupled increasingly with mass spectrometry (MS) and MS(n) as the detection tool, residues can be measured at parts per billion levels and below in a variety of food and environmental matrices. Development of efficient extraction and cleanup methods, techniques such as ELISA, efficient sample preparation techniques such as QuEChERS, and automated laboratory and field instrumentation has also contributed to the tools ...

2011-04-07

301

Borehole geophysics for delineating the geological structure in the Sakonishi prospect, the Hida area, Japan; Hida chiiki Sako nishi chiku ni okeru boring ko riyo butsuri tansa ni yoru chishitsu kozo kaiseki  

Energy Technology Data Exchange (ETDEWEB)

In order to discuss effectiveness of physical exploration in the Sakonishi prospect in the Hida area, physical exploration was carried out by utilizing bored wells. This area contains the Kamioka mine, one of the major base metal mines in Japan, where electrical exploration has been attempted several times in the past. No effective results have been obtained, however, because specific resistance contrast between mine beds and base rocks is too small, and the topography is too steep making site workability inferior. As part of the investigations on geological structures over wide areas, electrical logging (specific resistance and natural potential) was performed in fiscal 1995 and 1996 by utilizing the boreholes. Induced polarization logging was also conducted on the same boreholes. A traverse line on the ground with a length of 600 m and boreholes were used to execute specific resistance tomography. Clear extraction was possible on a fault ...

1997-05-27

302

1993 DoD Budget: Potential Reductions in Command, Control ...  

Science.gov (United States)

... 1: DSP Budget and Potential Reduction or Rescission 11 Table IV.2: Milstar Terminal Budget and Potential Reductions 13 or Rescissions ...

1992-09-01

303

Separation and determination of cadmium and zinc as their thenoyltrifluoroacetone complexes with dibenzo-18-crown-6 by means of synergistic extraction and atomic absorption spectrometry  

Energy Technology Data Exchange (ETDEWEB)

A new method for the separation and determination of trace amounts of cadmium and zinc in water as their thenoyltrifluoroacetone (TTA) complexes with dibenzo-18-crown-6 (DB18C6) in o-dichlorobenzene has been established by means of synergistic extraction and back-extraction combined with atomic absorption spectrometry. The effect of various factors (synergism with TTA and DB18C6, shaking time, composition of the extracted species, and mutual separation etc.) on the extraction and back-extraction of cadmium and zinc has been in- vestigated. When the mixtures were extracted for 4 min at pH 4.9, only zinc was extracted quantitatively, whereas cadmium remained in the aqueous phase. After the phases were separated, cadmium was again extracted quantitatively at pH 7.5. Then, the two phases were each shaken with 0.05-0.1 mol/l ...

1997-01-01

304

Phase transitions in the soliton star model  

Energy Technology Data Exchange (ETDEWEB)

The aim of this paper is to obtain the effective potential of the non-topological soliton model at finite temperature with the assumption that the chemical potential {mu} of the system is different from zero and to analyse how the effective potential is influenced by changes in the chemical potential and temperature. (author)

1998-01-01

305

Preconcentration and determination of trace amounts of lead (II) as thenoyltrifluoroacetone complex with dibenzo-18-crown-6 by synergistic extraction and atomic absorption spectrometry  

Energy Technology Data Exchange (ETDEWEB)

A new method for the preconcentration and determination of trace amounts of lead at the {mu}g/L level in natural waters has been established based on the formation of the thenoyltrifluoroacetone (TTA) complex with dibenzo-18-crown-6 (DB18C6) by means of synergistic extraction and back-extraction combined with atomic absorption spectrometry (AAS). The effect of various factors (synergism with TTA and DB18C6, shaking time, preconcentration factor, composition of the extracted species, and foreign ions etc.) on the extraction and back-extraction of lead has been investigated in detail. The lead-TTA chelate in o-dichlorobenzene forms a stable adduct with DB18C6 as Pb(TTA){sub 2} DB18C6. The stability constant ({beta}) of the adduct determined by curve fitting method was log {beta} = 4.2. The amount of lead in natural waters such as tap water (Kanazawa University) and Kakehashi river ...

1998-07-01

306

Food and chemical industry. Soy sauce and chemical engineering; Shokuhinn to kagaku kogaku. Shoyu to kagaku kogaku  

Energy Technology Data Exchange (ETDEWEB)

The buckwheat soup is a mixture of seasonings such as soy sauce, sweet sake, sugar and the like and stock of dried bonito. This paper describes an analysis of the stock manufacturing step, an important step in the manufacture of buckwheat soup, and the setting of stock extraction conditions on the basis of this analysis. If the rate of infiltration of water into the dried bonito is found, it is a very effective finding for setting the thickness of flakes of dried bonito and the extraction time to prepare buckwheat soup industrially. To obtain such knowledge, the time taken for the water to pass through flakes of dried bonito of various thicknesses, to vaporize and to remove latent heat till the temperature of the surfaces of flakes lowers was measured. The thickness of flakes of dried bonito and extraction time were set on the basis of the data thus obtained. Dired bonito was then supplied to a bench scale flow ...

1997-05-05

307

Evaluation of antioxidant and anti-atherogenic properties of Glycyrrhiza glabra root using in vitro models.  

Science.gov (United States)

The aim of present study was to evaluate antioxidant property of Glycyrrhiza glabra root extracts using in vitro models. The dose-dependent aqueous and ethanolic extracts demonstrated the scavenging activity against nitric oxide (concentration that caused 50% inhibition of nitric oxide radicals [IC(50)]=72 and 62.1 microg/ml, respectively), superoxide (IC(50)=64.2 and 38.4 microg/ml, respectively), hydroxyl (IC(50)=81.9 and 63 microg/ml, respectively), DPPH (IC(50)=43.6 and 28.3 microg/ml, respectively) and ABTS(*+) (IC(50)=77.3 and 57.2 microg/ml, respectively) radicals. Further, both extracts showed strong reducing power and iron-chelating capacities. In the Fe(2+)/ascorbate system, both extracts were found to inhibit mitochondrial fraction lipid peroxidation. In copper-catalyzed human serum and low-density lipoprotein oxidation models, both extracts significantly (P<0.05) ...

2009-04-22

308

Development of a rapid extraction procedure for speciation of arsenic in chicken meat  

Energy Technology Data Exchange (ETDEWEB)

A rapid extraction procedure has been developed for speciation of arsenic in chicken tissue. Water, methanol-water (1:1), and methanol-chloroform (1:1) were tested as extraction media. Individual use of an ultrasonic bath, a microwave oven, or an ultrasonic probe was not sufficient for quantitative recovery of As(III), dimethylarsinate, monomethylarsonate, As(V), and arsenobetaine in spiked samples of chicken tissue. A new extraction procedure using a methanol-water mixture and a microwave oven then an ultrasonic probe enabled extraction of the arsenic species in 7 min with efficiencies ranging from 80 to 100%. HPLC-UV-HG-AFS was used for the determinations. The extraction procedure was 100% efficient when applied to real samples of chicken tissue. AsB (48{+-}5 {mu}g As kg {sup -1}) and one containing-arsenic feed additive, Nitarsone (227{+-}5 {mu}g As kg {sup -1}) were detected. ...

2006-08-15

309

Problem Definition Studies on Potential Environmental ...  

Science.gov (United States)

... mutagenic, while two potential environmental transformation products, 1,4- diaminoanthraq Ynone and 1,4-dihydroxyanthraquinone are strongly ...

1979-11-01

310

Phenomenological dirac optical potential for neutron cross sections  

International Nuclear Information System (INIS)

Because of limitation on neutron-incident data, it is difficult to obtain global optical model potential for neutrons. In contrast, there are some global optical model potentials for proton in detail. It is interesting to convert the proton-incident global optical potentials into neutron-incident ones. In this study we introduce (N-Z)/A dependent symmetry potential terms into the global proton-incident optical potentials, and then obtain neutron-incident ones. The neutron potentials reproduce total cross sections in an acceptable degree. However, a comparison with potentials proposed by other authors brings about a confused situation in the sign of the symmetry terms. (author).

1997-03-01

312

A review of 4 norm industries in Ireland  

Energy Technology Data Exchange (ETDEWEB)

Full text: This presentation will review the progress achieved so far by the Irish national regulatory agency, the Radiological Protection Institut e of Ireland (R.P.I.I.) in the investigation of work activities where the presence of natural radiation sources (NORM) could lead to a significant increase in exposure to workers or members of the public which cannot be disregarded from the radiation protection point of view. Since the coming into force in Ma y 2000 of the Radiological Protection Act, 1991 (Ionising Radiation) Order, 2000 (S.I. No. 125 of 2000) which implements the Eu B.S.S. Directive 96/29/EURATOM, four major NORM industries currently active in Ireland have been investigated. According to the literature, they are all considered liable to involve work practices resulting in exposure to NORM. They include: the gas extraction and production industry, the peat- and coal-firing power generation industry and the bauxite/alumina refining industry. For the gas ...

2006-07-01

313

Synergistic extraction of europium(III) with benzoic acid and thenoyltrifluoroacetone  

Energy Technology Data Exchange (ETDEWEB)

The solvent extraction of europium(III) into solutions of thenoyltrifluoroacetone and benzoic acid in cyclohexane, carbon tetrachloride, benzene, chloroform, pentachloroethane, and tetrachloroethane has been measured at 25/sup 0/ C. It has been found that the extracted species involve two types of adducts, EuA/sub 3/HB and EuA/sub 3/ . 2HB where A denotes the TTA anion and HB the benzoic acid monomer. The magnitude of the adduct formation constants in different solvents has been correlated with the dimerization constants of benzoic acid in the solvents. 2 figures, 2 tables.

1983-01-01

314

Radioprotective activity in some medicinal herbs  

Energy Technology Data Exchange (ETDEWEB)

Water-soluble, ethanol-insoluble extracts prepared from several medicinal herbs of the Araliaceae and other families were tested for their radioprotective activity by either measuring 30 days survival rates (a commonly applied method) or counting the thrombocytes 14 days after irradiation (an improved method) in mice. The extracts were i.p. injected once within 4 min after the whole body X-ray irradiation. Of 12 materials examined, Aralia elata, Angelica acutiloba and Morus bombysis seemed to be good starting materials for preparing radioprotective substance(s) because of their relatively high specific activity and high yields of the extracts. (author).

1993-09-01

315

Proton beam monitoring and forming on the target of isotope complex at INR linac  

International Nuclear Information System (INIS)

Special beam extraction channel is used at INR linac for isotope production. It starts from 160 MeV measuring and matching area of accelerator. This choice of beam extraction enables to direct to the target of isotope complex a proton beam of wide energy range up to 160 MeV. It is important for production of different types of nuclides. The measuring results of proton beam behavior in this region are presented. Required beam forming in 160 MeV measuring and matching area of accelerator and in beam extraction channel is discussed.

2010-01-01

316

Injection and extraction magnets: septa  

CERN Document Server

An accelerator has limited dynamic range: a chain of accelerators is required to reach high energy. A combination of septa and kicker magnets is frequently used to inject and extract beam from each stage. The kicker magnets typically produce rectangular field pulses with fast rise- and/or fall-times, however the field strength is relatively low. To compensate for their relatively low field strength, the kicker magnets are generally combined with electromagnetic septa. The septa provide relatively strong field strength but are either DC or slow pulsed. This paper discusses injection and extraction systems with particular emphasis on the hardware required for the septa.

2010-01-01

317

Extraction of lithium from neutral salt solutions with fluorinated #beta#-diketones  

International Nuclear Information System (INIS)

Lithium was selectively extracted from near-neutral aqueous solutions of alkali metal salts. The mechanism by which this was achieved involves the formation of the trioctylphosphine oxide adduct of a lithium chelate of a fluorinated #beta#-diketone, which is then readily extractable into an organic diluent. High separation factors were obtained from sodium, potassium, rubidium, and cesium. The selectivity of the fluorinated #beta#-diketones for lithium over the alkaline earths was found to be poor. A suggested general flowsheet for the recovery of lithium from a salt brine concentrate is included. (author).

318

Zebrafish embryo extracts promote sphere-forming abilities of human melanoma cell line  

British Library Electronic Table of Contents (United Kingdom)

Sphere-forming abilities in culture condition are considered a hallmark of cancer stem-like cells, which represents tumor cell invasiveness and stem-like characteristics. We aimed to show that the sphere-forming subpopulation of human malignant melanoma cell line WM-266-4 acts differently to zebrafish embryo extracts compared with their bulk counterpart. Spheres were maintained in neural stem cell culture conditions. The embryos of zebrafish at specific developmental stages were collected and the extracts were purified under 100 kDa. Spheres were treated with embyo extracts and proliferation assay and immunocytochemistry were conducted. Spheroid cells expressed nestin and epidermal growth factor receptor (EGFR) but not melanoma antigen recognized by T-cells (MART)1, indicating their stem-l...

2009-01-01

319

Unusual extraction treatment of Class I bialveolar protrusion using microimplant anchorage.  

Science.gov (United States)

This case report describes the treatment of a 16-year-old girl who had severe bialveolar protrusion. Patients with bialveolar protrusion are commonly treated with four first premolar extractions and retraction of the anterior teeth. Unfortunately in this patient, the mandibular left second molar had to be extracted because of extensive caries. To create sufficient space for retraction of the anterior teeth, the mandibular left posterior teeth were retracted with the mandibular posterior microimplant (1.2 mm in diameter, 6 mm long) placed into the retromolar area followed by en masse retraction of the mandibular anterior teeth. Microimplants can provide anchorage for obtaining a good facial profile even without premolar extraction in the case of bialveolar protrusion with the absence of the second molar. PMID:17319776

2007-03-01

320

The effects of different plant extracts on intestinal cestodes and on trematodes  

British Library Electronic Table of Contents (United Kingdom)

In the present study, chloroform, aqueous, (polyethylene glycol/propylene carbonate) PEG/PC extracts were made from coconut, onion, garlic, fig, date tree, chicory, ananas, and cistrose. These extracts were tested in vivo and in vitro on their anthelmintic activity against cestodes (Hymenolepis diminuta, H. microstoma, Taenia taeniaeformis) and trematodes (Fasciola hepatica, Echinostoma caproni). In all in vitro tests, the target parasites died. It turned out that the treatment of mice and rats with a combination of onion and coconut extracts (with PEG/PC) eliminated all cestodes from their final hosts. In addition, the same composition was effective against the intestinal fluke E. caproni, but not against the liver fluke F. hepatica in the final host, while both worms were killed in vitro...

2011-01-01

321

Technique for the removal of electrons from an extracted, pulsed, H{sup {minus}} ion beam  

Energy Technology Data Exchange (ETDEWEB)

A small, permanent-magnet insert structure for the removal of electrons from pulsed, extracted, negative ion beams has been developed at Lawrence Berkeley National Laboratory. The device was computer modeled and designed for an extraction field strength of 3 kV/mm. The testing was carried out with a rf driven multicusp ion source optimized for the production of H{sup {minus}} ions and pulsed at a few Hz with pulse widths of several hundreds of {mu}s. It is demonstrated that the insert structure together with a collar can remove over 98{percent} of electrons from the extracted H{sup {minus}} ion beam without any significant deterioration of the H{sup {minus}} ion output. Application to other negative ion beams can be expected from this magnetic collar insert. {copyright} {ital 1996 American Institute of Physics.}

1996-10-01

322

Target stations and beam dumps for the CERN SPS  

International Nuclear Information System (INIS)

The design of the absorber blocks for internal and external dumping of the SPS proton beam is discussed. In addition, the external target stations for slow and fast extracted proton beams are described.

1977-03-16

323

Synthesis and characterization of new biopolymeric microcapsules containing DEHPA-?TOPO extractants for separation of uranium from phosphoric acid solutions  

British Library Electronic Table of Contents (United Kingdom)

A novel microcapsule adsorbent for separation of uranium from phosphoric acid solutions was developed by immobilizing the di(2-ethylhexyl) phosphoric acid-?trioctyl phosphine oxide extractants in the polymeric matrix of calcium alginate. Physical characterization of the microcapsules was accomplished by scanning electron microscopy and thermogravimetric techniques. Equilibrium experiments revealed that both ion exchange and solvent extraction mechanisms were involved in the adsorption of Formula Not Shown ions, but the latter prevailed in a wider range of acid concentration. According to the results of kinetics study, at low acidity level, the rate controlling step was slow chemical reaction of Formula Not Shown ions with the microdroplets of extractant, whereas it changed to intraparticle...

2011-01-01

324

Surface effects of total coal-seam extraction by underground mining methods  

Energy Technology Data Exchange (ETDEWEB)

The paper gives a detailed overview of the history of subsidence engineering in South African collieries. Surface displacements resulting from total-seam extraction are discussed, and the important role of local geology is highlighted. It is shown that the differences in subsidence behaviour between South African and European collieries can be attributed to the presence of competent strata in the overburden of South African coal seams. Criteria are given for the prediction of the most important subsidence parameters, and a new model for the simulation of surface subsidence above total-extraction panels is introduced. The final section of the paper deals with the damage to surface structures caused by total-seam extraction. A brief summary of the most important undermining experiments in South African collieries is given, and it is concluded that local experiences of damage compare with those in Europe. 32 refs., 9 figs., 3 ...

1991-07-01

326

Search for the active components and studies on the mechanism of the hematopoiesis improvement foods  

Energy Technology Data Exchange (ETDEWEB)

In this experiments, we established long-termed culture methods of bone marrow stromal cells for proliferation and differentiation of stem cells. And we selected some extracts which support maximal proliferation of stromal cells with this method. We conformed the synergic effects of herval mixture extracts for stromal cell growth. The proliferation of stromal cells was increased rather by the addition of mixture extracts than by addition of single strain extract. In the previous and cooperative experiments, we selected complex extracts which increased the number of nonadherent mononuclear cells. Different cytokine expression patterns were observed stromal cells cultured in the presence or absence of mixture extracts which support differentiation of nonadherent cells. Stimulation of macrophage cell line with herval extracts with the ...

1999-04-01

327

STR Training Materials  

Science.gov (United States)

Typing Workshop": [Introductions] [Intro, DNA Basics, and Historical Perspective] [DNA Extraction] [Validation and QA/QC] [DNA Quantitation] [PCR Amplification] [STR Loci and Kits]...

2011-04-29

328

Real-Time Stability and Control Derivative Extraction From F-15 - NASA  

Science.gov (United States)

and the estimated parameter covariance matrix is. 5. (25) where p in this case is the number of elements in the vector . The parameter standard errors, ?, ...

329

Polynomial curve fitting method for refraction-angle extraction in diffraction enhanced imaging  

International Nuclear Information System (INIS)

X-ray diffraction enhanced imaging (DEI) is applied to inspect internal structures of weakly absorbing low-Z sample. How to extract phase information from raw images measured in different positions of rocking curve is the key problem of DEI. In this paper, we present an effective extraction method called polynomial curve fitting method, in order to extract accurate information angular in a fast speed. It is com- pared with the existing methods such as multiple-images statistical method and Gaussian curve fitting method. The experiments results on a plastic cylinder and a black ant at the Beijing Synchrotron Radiation Facility prove that the polynomial curve fitting method can obtain most approximate refraction-angle values and its computation speed is 10 times faster than the Gaussian curve fitting method. (authors)

2009-11-01

331

Oral administration of the purple passion fruit peel extract reduces wheeze and cough and improves shortness of breath in adults with asthma  

British Library Electronic Table of Contents (United Kingdom)

Asthma, affecting as many as 400 million individuals worldwide, is one of the most prevalent chronic health condition in the United States. With an increasing number of patients with asthma and the frequent inability of conventional lifestyle modification and therapy to effectively control the problem, nutritional and dietary therapies are being sought. This study was undertaken to investigate the efficacy of the purple passion fruit peel (PFP) extract, a novel mixture of bioflavonoids, on asthma symptoms. Patients with asthma were studied in a 4-week randomized, placebo-controlled, double-blind trial with oral administration of PFP extract (150 mg/d) or placebo pills. The effects of PFP extract were evaluated by assessing the clinical symptoms of asthma and spirometry tests. Most clinical...

2008-01-01

332

Optimization of alkaline hydrolysis of paddy straw for ferulic acid extraction  

British Library Electronic Table of Contents (United Kingdom)

Response Surface Methodology (RSM) via Central Composite Design (CCD) was used to optimize the alkaline hydrolysis of paddy straw to improve ferulic acid extraction. The parameters involved, namely temperature (^oC), concentration of NaOH (M) and duration of extraction (h) are screened by Full Factorial Studies (FFD). The result obtained from FFD was 0.518% (5.18mg/g). The interactions between each parameters involved were studied using Central Composite Design (CCD). Upon optimization, the percentage of ferulic acid improved from 0.518% to 0.817% (8.17mg/g). The optimum conditions obtained from this study are 125^oC, 3.90M, 2.30h for temperature, concentration of NaOH and extraction time, respectively. This result shows a significant improvement than the previous published work. Details o...

2011-01-01

334

Laboratory-scale simulation of energy extraction from tidal currents  

Energy Technology Data Exchange (ETDEWEB)

The energy available from tidal currents is substantial and considerable work has been conducted into determining the size of the resource and what the large-scale consequences of extraction might be. This paper describes the work conducted to establish a laboratory-scale model, by using the commercial computational fluid dynamics (CFD) code FLUENT trademark, in order to predict local-flow consequences resulting from the extraction of energy in two and three dimensions from within the water column in a tidal flow. As might be expected, a wake is formed but there is considerable localized flow acceleration around and, most especially, under an extraction zone. The wake behind the device is shown to be associated with a drop in the free surface which, in turn, is associated with the decline in the wake itself. (author)

2008-06-15

335

Information Fusion and Extraction Priorities for Australia's ...  

Science.gov (United States)

... the open source OpenMap Java toolkit from BBN ... 2001), Handbook of Multisensor Data Fusion ... Oxenham (2002), Sensor Registration Using Airlanes ...

2004-03-01

336

In vitro acaricidal activity of neem (Azadirachta indica) seed extracts with known azadirachtin concentrations against Rhipicephalus microplus  

British Library Electronic Table of Contents (United Kingdom)

The effect of four extracts from neem seeds (Azadirachta indica) containing 2000, 5000, 9000 and 10,000ppm of azadirachtin A (AZA), quantified by high-performance liquid chromatography (HPLC) and diluted to 1.25%; 2.5%; 5.0%; 10.0% and 12.8% was verified by in vitro tests with engorged females and larvae of the cattle tick Rhipicephalus microplus. The results from the bioassays with the engorged females showed that the main toxic effect of the extracts was reduction of the reproductive parameters, with a sharp drop in the number of eggs laid and the hatching rate, mainly when the extracts were diluted to 10.0% and 12.8%. The product effectiveness (PE) calculations for all the solutions tested showed that the AZA solution at 10,000ppm (N10) was the most effective. However, statistical analy...

2011-01-01

338

Host plant odor extracts with strong effects on oviposition behavior in Papilio polyxenes  

British Library Electronic Table of Contents (United Kingdom)

Abstract Ovipositing females of the black swallowtail butterfly, Papilio polyxenes Fabricius (Lepidoptera: Papilionidae: Papilioninae), have an innate response to contact chemical cues, but it was not known how naive females would respond to volatile host plant chemicals. Naive and experienced females were tested in a free-flight experiment using model plants and volatile extracts from two hosts, carrot [Daucus carota L. (Apiaceae)] and poison hemlock [Conium maculatum L. (Apiaceae)], and one non-host, fava bean [Vicia faba L. (Fabaceae)]. Naive females responded to both host plant extracts with more approaches and landings than to non-host extracts, with poison hemlock receiving more responses than carrot. Females experienced with one of the two host plants also approached and landed freq...

2008-01-01

339

High-Throughput Screening of Drugs of Abuse in Urine by Supported Liquid?Liquid Extraction and UHPLC Coupled to Tandem MS  

British Library Electronic Table of Contents (United Kingdom)

A qualitative method, involving supported liquid?liquid extraction (SLE) and ultra high pressure liquid chromatography coupled to tandem mass spectrometry (UHPLC-MS?MS), was developed for the rapid tentative identification of various drugs of abuse in urine. In this study, 28 drugs and metabolites were covered by the screening procedure. Before analysis, urine samples were extracted by SLE and good extraction recoveries were obtained for most investigated compounds. The UHPLC strategy was then selected for the rapid separation of amphetamines, cocaine, opiates and related compounds in urine. Using columns packed with sub-2??m particles, analysis time was reduced down to 2?min, while maintaining acceptable performance. Finally, the detection was by tandem MS operating in the single reaction...

2009-01-01

340

Extraction of americium of different oxidation states in two-phase aqueous system based on polyethylene glycol  

International Nuclear Information System (INIS)

Americium extraction in different oxidation states in two-phase aqueous system based on polyethylene glycol is investigated. Conditions for quantitative extraction of americium (3) and americium (5) from ammonium sulfate solutions within pH=3-5 interval in the presence of arsenazo 3 are found. Composition of the produced americium complexes with reagent is determined; americium (3) interacts with arsenazo 3 in ammonium sulfate solutions with the formation of MeR and Me_2R composition complexes. Absorption spectrum characteristics of americium (3) and- (5) complexes with arsenazo 3 in ammonium sulfate solutions and extracts based polyethylene glycol aqueous solutions are given. Molar extinction coefficients of americium complexes with arsenazo (3) in these solutions are determined.

1987-01-01

341

Enhanced extraction yields and mobile phase separations by solvent mixtures for the analysis of metabolites in Annona muricata L. leaves  

British Library Electronic Table of Contents (United Kingdom)

The effects of five extraction solvents and their mixtures on the yield of metabolites in crude and fractionated extracts of Annona muricata L. leaves were investigated by direct comparison. Extraction media were prepared using simplex centroid mixtures of ethanol, ethyl acetate, dichloromethane, acetone, and chloroform. The effects of the mobile phase solvent strength and the analysis wavelength on the chromatographic separation were also investigated. Solvent mixtures rather than pure solvents were found to be the most efficient extractors for the different fractions. The results indicated that the mobile phase composed of methanol/acetonitrile/water (26:27:47 v/v/v) was most suitable for the basic fraction analysis at 254 nm, whereas the mobile phase composed of methanol/acetonitrile/wa...

2009-01-01

342

Detection and Identification of Bacteria by Gas Chromatography1  

UK PubMed Central (United Kingdom)

Ether extracts of cultures of 29 strains representing 6 species of Bacillus, and of individual strains of Escherichia coli, Aerobacter aerogenes, and Pseudomonas...Full Text Available

1966-07-01

343

Comparison of levels of trace elements extracted from fly ash and levels found in effluent waters from a coal-fired power plant  

Science.gov (United States)

Trace elements were extracted from a coal-fired power plant electrostatic precipitator ash with nitric acid, hydrochloric acid, citric acid, redistilled water, and ammonium hydroxide as extractants. Effluent waters at this plant were sampled to assess the elevation of trace element concentrations compared with intake waters. The results showed a positive correlation between those elements most extractable by water (B, F, Mo, and Se) or acid (As, B, Cd, F, Mo, and Se) and those elements most elevated in effluent waters (As, B, F, Mo, and Se).

1977-10-01

345

Chimpanzees Extract Social Information from Agonistic Screams  

UK PubMed Central (United Kingdom)

Chimpanzee (Pan troglodytes) agonistic screams are graded vocal signals that are produced in a context-specific manner. Screams given by aggressors and victims can be discriminated...Full Text Available

348

Biochemical monitoring of black raspberry (Rubus coreanus Miquel) fruits according to maturation stage by ^1H NMR using multiple solvent systems  

British Library Electronic Table of Contents (United Kingdom)

Nuclear magnetic resonance (NMR) techniques coupled with multivariate data analysis were used to conduct monitoring of biochemical changes of black raspberry fruits at different stages of maturation and under various extraction and NMR dissolution solvent conditions: extraction with 50% methanol and D"2O as an NMR dissolution solvent, extraction with 50% methanol and 50% methanol-d"4 as an NMR dissolution solvent, and extraction with 100% ethyl acetate and 100% methanol-d"4 as an NMR dissolution solvent. Partial least-squares discriminant analysis reliably distinguished black raspberry fruits according to the maturation stage, whereby the relative levels of various compounds such as amino acids, organic acids, sugars and phenolic compounds were compared using analysis of variance. Sucrose ...

2011-01-01

349

BALDWIN001  

Science.gov (United States)

Mar 13, 1997 ... Rich Baldwin's data and program files from the workstation Geomag extracted 5/96 FILE DESCRIPTION /BINNER/ /u/baldwin/rich/fortran/binner/ ...

350

Automatic Extraction of Open Space Area from High Resolution Urban Satellite Imagery  

CERN Document Server

In the 21st century, Aerial and satellite images are information rich. They are also complex to analyze. For GIS systems, many features require fast and reliable extraction of open space area from high resolution satellite imagery. In this paper we will study efficient and reliable automatic extraction algorithm to find out the open space area from the high resolution urban satellite imagery. This automatic extraction algorithm uses some filters and segmentations and grouping is applying on satellite images. And the result images may use to calculate the total available open space area and the built up area. It may also use to compare the difference between present and past open space area using historical urban satellite images of that same projection

2011-01-01

351

Antiprotozoal and cytotoxic activities in vitro of Colombian Annonaceae  

British Library Electronic Table of Contents (United Kingdom)

Ethnobotanical and chemotaxonomical studies for antiparasitic activity of Colombian Annonaceae were carried out. In vitro antiprotozoal activity of 36 extracts obtained from six different species was determined against promastigotes of three Leishmania species, epimastigotes of Trypanosoma cruzi and both chloroquine sensitive (F32) and resistant (W2) Plasmodium falciparum. Cytotoxic activity was evaluated in U-937 cells. Active extracts were selected according their selectivity index (SI). Extracts from Annona muricata, Rollinia exsucca, Rollinia pittieri and Xylopia aromatica were active against Leishmania spp. and Trypanosoma cruzi showing IC50 values lower than 25mg/ml. Hexane extract from Rollinia pittieri leaves was the most selective against Trypanosoma cruzi and Leishmania spp. (IS=...

2007-01-01

352

Antioxidant properties of chlorophyll-enriched and chlorophyll-depleted polyphenolic fractions from leaves of Vernonia amygdalina and Gongronema latifolium  

British Library Electronic Table of Contents (United Kingdom)

This study investigated the optimum polyphenol extraction conditions for two Nigerian green leafy vegetables, Vernonia amygdalina (VA) and Gongronema latifolium (GL) that are widely used for food and medicinal purposes. Seven different solvents were used to extract the total phenolic contents of the leaves; 100% acetone, 80% acetone, 50% acetone, 100% ethanol, 70% ethanol, 100% methanol and 70% methanol and their total phenolic contents were determined. The results showed that the 80% acetone was significantly (p<0.05) the most effective for polyphenol extraction from the leaves and generally the acetone-containing solvents were more effective than alcohol-containing solvents. The 80% acetone extract was fractionated on a silicic acid-packed column to give two main fractions: acetone elute...

2011-01-01

353

Antimicrobial activities of the methanol extract and compounds from Artocarpus communis (Moraceae)  

UK PubMed Central (United Kingdom)

BackgroundArtocarpus communis is used traditionally in Cameroon to treat several ailments, including infectious and associated diseases. This work was therefore...Full Text Available

354

Anti-plasmodial activity and toxicity of extracts of plants used in traditional malaria therapy in Meru and Kilifi Districts of Kenya  

British Library Electronic Table of Contents (United Kingdom)

The methanol and aqueous extracts of 10 plant species (Acacia nilotica, Azadirachta indica, Carissa edulis, Fagaropsis angolensis, Harrissonia abyssinica, Myrica salicifolia, Neoboutonia macrocalyx, Strychnos heningsii, Withania somnifera and Zanthoxylum usambarensis) used to treat malaria in Meru and Kilifi Districts, Kenya, were tested for brine shrimp lethality and in vitro anti-plasmodial activity against chloroquine-sensitive and chloroquine-resistant strains of Plasmodium falciparum (NF54 and ENT30). Of the plants tested, 40% of the methanol extracts were toxic to the brine shrimp (LD5050N. macrocalyx had the highest toxicity to brine shrimp nauplii (LD50 21.04+-1.8mg/ml). Methanol extracts of the rest of the plants exhibited mild or no brine shrimp toxicity (LD50>50mg/ml). The aqueo...

2006-01-01

355

Activation of rapid signaling pathways and the subsequent transcriptional regulation for the proliferation of breast cancer MCF-7 cells by the treatment with an extract of Glycyrrhiza glabra root  

British Library Electronic Table of Contents (United Kingdom)

Glycyrrhiza glabra root is one of the common traditional Chinese medicines and used as flavoring and sweetening agents for tobaccos, chewing gums, candies, toothpaste and beverages. While glycyrrhizin is one of the main components in the extract of G. glabra root and has been characterized, the other components have not been well characterized. The mechanism of growth activation of breast cancer MCF-7 cells, including the activation of Erk1/2 and Akt, and the transcriptional regulation of estrogen-responsive genes, was examined by means of sulforhodamine B, luciferase reporter gene, real-time RT-PCR and Western blotting assays after the induction of the cells with the extract of G. glabra root. The extract has similar activity to that induced by 17b-estradiol (E2), although glycyrrhizin di...

2007-01-01

356

A comparison of thermal maturity parameters between freely extracted hydrocarbons (Bitumen I) and a second extract (Bitumen II) from within the kerogen matrix of Permian and Triassic sedimentary rocks  

British Library Electronic Table of Contents (United Kingdom)

In this study we compared various maturity dependent aromatic, steroid and triterpenoid hydrocarbon ratios in bitumens that are freely extractable from sedimentary rocks (Bitumen I) with those in second extracts that comprised hydrocarbons closely associated with the kerogen/mineral matrix (Bitumen II). Bitumen II was released through kerogen isolation and demineralisation using HCl and HF/H3BO3. The samples studied, although of similar age, come from different localities. They represent a range of facies and two kerogen types (II and III), and all were deposited under marine conditions. The results show that the more stable b isomers of methylnaphthalene (MN) and methylphenanthrene (MP) are relatively more abundant in Bitumen II. The difference between the methylnaphthalene ratio (MNR) of...

2010-01-01

357

A Comparative Study of Pectin Extracted from Passion Fruit Rind Flours  

British Library Electronic Table of Contents (United Kingdom)

Brazil is the world?s main producer of passion fruit. Previous reports show that passion fruit rinds, an industrial waste, contain large amounts of pectin. Pectin is a dietary fiber that is widely used in the food industry as a gelling agent and stabilizer. In this study, the quality and characteristics of pectin extracted from yellow passion fruit rind flour was investigated. Pectin was extracted from both commercially available and prepared passion fruit peels using nitric acid. Once extracted, the pectin was evaluated for its molecular characteristics and chemical composition as well as for the apparent and reduced viscosity of the gel. Prepared (blanched) rind flour yielded 203.4?g?kg?1 of pectin, which contained a uronic acid content of 681?mg?g?1, a degree of esterification of 80, a ...

2010-01-01

358

Oxidation and adsorption of Co(II)EDTA 2- complexes in subsurface materials with iron and manganese oxide grain coatings  

Science.gov (United States)

Batch interaction experiments were performed under aerobic conditions to characterize the adsorption behavior and valence speciation of CoEDTA complexes (equimolar at 10 -5 mol/L) in a series of Pliocene subsurface sediments containing various amounts of Fe and Mn oxides. The experiments were performed in 0.003 mol/L Ca(ClO 4 ) 2 with a solids concentration of 500 g/L at variable pH (4-9) and at the natural pH of the sediments (pH = 8.3). Three of these subaerial sediments (Ringold 1, 2, 3) contained significant quantities of extractable Fe and Mn, while the fourth (Ringold 4) was virtually devoid of sesquioxide precipitates. Microscopic and mineralogic analyses of the most heavily encrusted material (Ringold 2) showed that the oxides existed as intergrain cements and contained crystalline goethite and rancieite/todorokite. Adsorption on a synthetic analog sorbent (0.6 mass % ferrihydrite-coated sand) over a range in pH showed that, while both Co(II)EDTA 2- and ...

1995-11-01

359

["3H]Indole-3-acetyl-myo-inositol hydrolysis by extracts of Zea mays L. vegetative tissue  

International Nuclear Information System (INIS)

["3H]Indole-3-acetyl-myo-inositol was hydrolyzed by buffered extracts of acetone powders prepared from 4 day shoots of dark grown Zea mays L. seedlings. The hydrolytic activity was proportional to the amount of extract added and was linear for up to 6 hours at 37"0C. Boiled or alcohol denatured extracts were inactive. Analysis of reaction mixtures by high performance liquid chromatography demonstrated that not all isomers of indole-3-acetyl-myo-inositol were hydrolyzed at the same rate. Buffered extracts of acetone powders were prepared from coleoptiles and mesocotyls. The rates of hydrolysis observed with coleoptile extracts were greater than those observed with mesocotyl extracts. Active extracts also catalyzed the hydrolysis of esterase substrates such as #alpha#-naphthyl acetate and the methyl esters of indoleacetic acid and ...

360

Thorium different-ligand complexes with morin as analytic form for extraction-photometric determination of thorium microamounts  

International Nuclear Information System (INIS)

Consideration is given to results of investigation into thorium complexing with morin (H_2Mor) in extraction systems containing different carboxylic acids as well as different salt background. The obtained data enabled to suggest the method of photometric determination of thorium in the form of Th(HMor)_2Benz_2 different-ligand complex (where Benz-anion of benzilic acid) with 0.25 #mu#g/ml detection limit.

1989-01-01

361

The phenomenon of microscale flow and mass transfer in medicinal herb materials  

Energy Technology Data Exchange (ETDEWEB)

Microwave assisted extraction (MAE) is a combination of a microwave technique and conventional solvent extraction used in the modernization of traditional Chinese medicine. The effective component of medicinal herbs is mostly cellular material which can be released via solvent extraction. The material is diffused to solvents via the porous membrane wall. The structure of herb morphology and characteristics of the solute's molecular weight play an important role in the extraction process of target compounds. Astragalus pieces were chosen for this study in which an ultra-filtration membrane method was used to determine the molecular weight distribution characteristics of Astragalus water extraction liquid in the process of MAE. The fine structure of matrix materials was also characterized by scanning election microscopy (SEM). The phenomenon of mass flow and mass transfer in ...

2008-07-01

362

The harmful effect of phosphate in yellow cake on the TBP purification process  

International Nuclear Information System (INIS)

The harmful effect of phosphate in yellow cake on the TBP purification process and its removal methods are dealed with. The reason of more uranium loss in residue was analyzed. The harmful effect of phosphate on TBP extraction efficiency and operaton of extraction column was discussed. The limit value of uranium concentration in digestion solution was presented. For TBP purification process, the presence of phosphate in yellow cake does more harm than good. (authors)

2009-02-01

363

Synergetic extraction in systems with dicarbollide and bidentate phosphonate  

Energy Technology Data Exchange (ETDEWEB)

A process for the extraction of tervalent metal cations from 3 M HNO[sub 3] highly radioactive waste based on synergetic mixtures of dicarbollide with neutral organophosphonate (dibutyl diethylcarbamoylmethylene phosphonate) is proposed. Due to the great hydrophobicity of dicarbollide anion, the species ML[sub n[sup 3+

1994-01-01

364

Solvent extraction studies using tetracycline as a complexing agent. Pt. 12. Determination of stability constants for the complexes of uranium and tetracycline  

Energy Technology Data Exchange (ETDEWEB)

Stability constants for uranium-tetracycline complexes were determined by the method of average number of ligands, the method of limiting values, the method of two parameters and the method of weighted least squares. Solvent extraction technique was used to obtain experimental data. (author). 10 refs.; 5 figs.

1985-09-01

365

Solvent extraction studies using tetracycline as a complexing agent, Pt. 13. Application of tetracycline for separation of interfering elements in activation analysis of uranium  

Energy Technology Data Exchange (ETDEWEB)

Tetracycline in solution of benzyl alcohol was used as an extracting agent to separate uranium from interfering elements in the determination of uranium and of isotopic ratio sup(235)U/sup(238)U by neutron activation analysis. Separation gives a recovery of 97% for uranium and the interferences from matrices of pitchblende and monazite are eliminated.

1985-08-01

366

Quantitation of transcribing native simian virus 40 minichromosomes extracted from CV1 cells late in infection.  

UK PubMed Central (United Kingdom)

Simian virus 40 transcriptional complexes could be extracted from CV1 cells late in infection and separated from the bulk of inactive viral chromatin. Sucrose gradient sedimentation, cesium sulfate...Full Text Available

1981-04-01

367

Oil shale in China: resources and utilization  

Energy Technology Data Exchange (ETDEWEB)

China is continuing to extract oil from kerogen shale despite having a crude production capacity of 100 Mt a year. Among the reasons for this policy are the country's rich oil shale resources, comparatively mature extraction techniques, and a comprehensive utilization of the shale that has proved to be economically profitable. China has oil shale deposits of 340 Gt, equivalent to 24.5 Gt of shale oil, to rank fourth in the world after the U.S., Brazil, and the Soviet Union.

1984-05-01

368

Metallographic preparation and characterisation of the As-cast Ni-based superalloy GMR 235; Metallographische Praeparation und Charakterisierung der Nickelbasis-Superlegierung GMR 235 im Gusszustand  

Energy Technology Data Exchange (ETDEWEB)

In this work a Ni-based superalloy GMR 235 was investigated. We determined convenient metallographic methods for preparation of bulk metallographic specimens, extraction carbon replicas, transparent metallic foils and minor phase extraction. In addition, the alloy microstructure was characterised using different metallographic techniques. (orig.)

2004-08-01

369

Evaluation of NucliSens easyMAG for automated nucleic acid extraction from various clinical specimens.  

Science.gov (United States)

The objectives of this study were to evaluate the performance of the NucliSens easyMAG platform for nucleic acid extraction from different clinical specimens compared to NucliSens miniMAG platform and manual QIAGEN extraction. The NucliSens easyMAG and the NucliSens miniMAG showed equal performance on 215 throat swabs since real-time nucleic acid sequence-based amplification scored the same samples positive for Mycoplasma pneumoniae (n=9) and Chlamydia pneumoniae (n=5) RNAs, although internal control RNA was slightly better detected with the NucliSens easyMAG (99.3% versus 96.8%). NucliSens easyMAG extracted nucleic acids more efficiently (higher recovery and/or fewer inhibitors) compared to QIAGEN extraction by showing, on average, lower Ct values in real-time LightCycler PCR, although 4 individual specimen out of 45 were found positive only with QIAGEN. For nine M. pneumoniae-positive throat swabs, ...

2006-12-13

370

Eliminating explosives  

Energy Technology Data Exchange (ETDEWEB)

The paper describes a way to control methane that is almost self-sufficient. The Methane Buster extracts methane from longwall mines. The machinery can run virtually unattended and is fuelled by a small proportion of the methane that it extracts. The most popular model is the size of a car and weighs 3000 lbs. With pump inlet sizes varying from 6 to 24 ins. The pumps can handle up to 30,000 CFM. 3 photos.

2005-12-01

371

Effects of the Methanol Extract of Basella alba L (Basellaceae) on Steroid Production in Leydig Cells  

UK PubMed Central (United Kingdom)

In this study, Leydig cells were purified from 70 day-old Sprague Dawley male rats and incubated with 10 and 100 μg/mL of methanol extract of Basella alba (MEBa) for 4 hours...Full Text Available

372

Dust and waterfree technology for demolition works in nuclear environments and other sensitive areas  

International Nuclear Information System (INIS)

At the University of Karlsruhe experiments were carried out from 1997 to 1999 to get fundamentals of flow characteristics of pneumatic extracted materials. The results could be used to develop a concept for demolition suitable for extraction and removing high-density concrete. The concept fulfills all demands of a closed nuclear area, especially of dust abatement. (orig.)

373

Development of functional foods for radiation workers - Search for the active components and studies on the mechanism of the hematopoiesis improvement foods  

Energy Technology Data Exchange (ETDEWEB)

In this experiments, we established long-termed culture methods of bone marrow stromal cells for proliferation and differentiation of stem cells. And we selected some extracts which support maximal proliferation of stromal cells with this method. We conformed the synergic effects of herbal mixture extracts for stromal cell growth. The proliferation of stromal cells was increased rather by the addition of mixture extracts than by addition of single strain extract. In the previous and cooperative experiments, we selected complex extracts (Him-I, Him-II) which increased the number of nonadherent mononuclear cells. Different cytokine expression patterns were observed stromal cells cultured in the presence or absence of mixture extracts which support differentiation of nonadherent cells. Some fractions of Him-I and Him-II increased the proliferation of bone marrow ...

2000-04-01

374

DEVELOPMENT OF CONTINUOUS SOLVENT EXTRACTION PROCESSES FOR COAL DERIVED CARBON PRODUCTS  

Energy Technology Data Exchange (ETDEWEB)

The purpose of this DOE-funded effort is to develop continuous processes for solvent extraction of coal for the production of carbon products. These carbon products include materials used in metals smelting, especially in the aluminum and steel industries, as well as porous carbon structural material referred to as ''carbon foam'' and carbon fibers. During this reporting period, efforts have focused on the facility modifications for continuous hydrotreating, as well as developing improved protocols for producing synthetic pitches.

2005-08-11

375

Co-product extraction studies on N-reactor PT-57 target materials  

International Nuclear Information System (INIS)

Single pellets (of approximately 70 g each) of irradiated lithium aluminate target from N-Reactor test PT-57 were used in a series of experiments to determine the extent to which the product tritium can be recovered by (a) vacuum outgassing of the target (thermal extraction-TX) and (b) in-vacuo chemical dissolution of the target in molten sodium tetraborate (flux extraction-FX). Five TX runs and seven FX runs were made. Thirty-five percent of the tritium was recovered in a form non-condensable at -196"0C. The remainder was recovered in a condensable form (as T_2O, HTO, etc.). Post-extraction analysis of the melt from the seven flux extractions showed that a maximum of 2 percent of the original amount of tritium remained and that target dissolution was essentially complete in 12 hours. Flux extraction of two pellets which had been subjected to thermal extraction ...

376

Total phenolics and antioxidant activity of five medicinal plant; Fenois totais e atividade antioxidante de cinco plantas medicinais  

Energy Technology Data Exchange (ETDEWEB)

This paper describes total phenolics content and antioxidant activity in the ethanolic extract of leaves, bark and roots of five medicinal plants: Terminalia brasiliensis Camb., Terminalia fagifolia Mart. and Zucc., Copernicia cerifera (Miller) H.E. Moore, Cenostigma macrophyllum Tul. var. acuminata Teles Freire and Qualea grandiflora Mart. The total phenolics content of the plant extracts, determined by the Folin-Ciocalteu method, varied from 250.0 {+-}8,2 to 763,63 {+-}13.03 mg of gallic acid equivalent/g dry EtOH extract. The antioxidant activity of extracts was evaluated using the 2,2-diphenyl-1-picrylhydrazyl (DPPH) assay system. Extract of bark from T. brasiliensis, the most active, with an EC{sub 50} value of 27.59 {+-} 0.82 {mu}g/mL, was comparable to rutin (EC{sub 50} = 27.80 {+-} 1.38) and gallic acid (EC{sub 50} = 24.27 {+-} 0.31), used as positive controls. The ...

2007-03-15

377

Studies on the extraction equilibria of Cu, Ni, Co and Mn with Versatic Acid 911  

International Nuclear Information System (INIS)

The distribution of Cu, Ni, Co and Mn between an aqueous solution of constant ionic strength and Versatic Acid 911 diluted with benzene was investigated. Only one extracted species of Cu was revealed to have a dimeric structure of the composition (CuR_2.RH)_2, while both monomer and dimer were found in the extraction of Ni, Co and Mn. The curve-fitting method was employed to determine these species, from which the composition of the extracted species was found to be NiR_2.4RH and (NiR_2.2RH)_2, CoR_2.4RH and (CoR_2.2RH)_2, and MnR_2.4RH and (MnR_2.2RH)_2, respectively. The apparent equilibrium constants of the above species and those between monomer and dimer were also determined. The curve-fitting method was proved to be a precise method for determining the equilibrium constants and extracted species. (author).

378

Solvent extraction using tetracycline as complexing agent Pt. 14. Study of the behaviour of tetracycline as an extracting agent for some fission products  

Energy Technology Data Exchange (ETDEWEB)

The behaviour of tetracycline as an extracting agent for Sr, I, Ba, Mo, Tc, Zr, Nb, Cs, Ru, Te and U was studied and the influence of the acidity of the aqueous phase upon extraction of the elements mentioned was examined. Experiments were made to determine whether the species extracted into the organic phase is the complex formed between tetracycline and the elements considered and to determine the time of shaking necessary so that the equilibrium between the phases is attained. As a practical application, the possibility of using the tetracycline-benzyl alcohol system for separating the fission products sup(137)Cs, sup(140)La, sup(141)Ce, sup(103)Ru, sup(95)Nb from each other and from uranium is presented. The same study was made for sup(131)I, sup(99m)Tc, sup(99)Mo, sup(132)Te, sup(239)Np and uranium and the steps necessary for the separation of these elements are proposed.

1985-10-01

379

Hot water extraction with in situ wet oxidation: Kinetics of PAHs removal from soil  

International Nuclear Information System (INIS)

Finding environmentally friendly and cost-effective methods to remediate soils contaminated with polycyclic aromatic hydrocarbons (PAHs) is currently a major concern of researchers. In this study, a series of small-scale semi-continuous extractions - with and without in situ wet oxidation - were performed on soils polluted with PAHs, using subcritical water (i.e. liquid water at high temperatures and pressures, but below the critical point) as the removal agent. Experiments were performed in a 300 mL reactor using an aged soil sample. To find the desorption isotherms and oxidation reaction rates, semi-continuous experiments with residence times of 1 and 2 h were performed using aged soil at 250 deg. C and hydrogen peroxide as oxidizing agent. In all combined extraction and oxidation flow experiments, PAHs in the remaining soil after the experiments were almost undetectable. In combined extraction and oxidation no PAHs could ...

2006-09-01

380

Feature extraction for rolling element bearing fault diagnosis utilizing generalized S transform and two-dimensional non-negative matrix factorization  

Science.gov (United States)

This paper presents a novel feature extraction scheme for roller bearing fault diagnosis utilizing generalized S transform and two-dimensional non-negative matrix factorization (2DNMF). The generalized S transform, which can make up the poor energy concentration of the standard S transform, is introduced to generate the time-frequency representation (TFR). Experiment results on simulated signal and vibration signals measured from rolling element bearings have revealed that the generalized S transform can obtain a more satisfactory TFR than other similar techniques. Furthermore, a new technique called two-dimensional non-negative matrix factorization (2DNMF), which can reduce the computation cost and preserve more structure information hiding in original 2D matrices compared to the NMF, is developed to extract more informative features from the time-frequency matrixes for accurate fault classification. Experimental results on bearing faults ...

2011-05-01

381

Extracts of the marine brown macroalga, Ascophyllum nodosum, induce jasmonic acid dependent systemic resistance in Arabidopsis thaliana against Pseudomonas syringae pv. tomato DC3000 and Sclerotinia sclerotiorum  

British Library Electronic Table of Contents (United Kingdom)

We studied the mechanism of Ascophyllum nodosum (a brown macroalga) induced resistance in Arabidopsis thaliana against Pseudomonas syringae pv. tomato DC3000. Root treatment of A. thaliana Col-0 plants with extracts of A. nodosum [aqueous (ANE), chloroform (C-ANE) and ethylacetate fractions, (E-ANE)] reduced the development of disease symptoms on the leaves. These extracts also induced resistance in salicylic acid deficient NahG and ics1 plants. However, the extracts did not elicit an effect on jar1 (jasmonic acid resistance 1) mutant. A. nodosum extract induced resistance to Pst DC3000 correlated with increased expression of jasmonic acid related gene transcripts PDF1.2 while PR1 and ICS1 expression were less affected. Additionally, pretreatment of Arabidopsis plants with ANE, protected t...

2011-01-01

382

Evaluation of the radioprotective effect of turmeric extract and vitamin E in mice exposed to therapeutic dose of radioiodine  

International Nuclear Information System (INIS)

The aim of this study was to evaluate the radioprotective effect of turmeric extract (40 mg/kg body weight) and vitamin E (#alpha# - tocopherol acetate, 400 IU/kg body weight) supplementation on lipid peroxidation, reduced glutathione and antioxidant defense enzymes in various organs like liver, kidney and salivary glands at 24 h in adult Swiss mice. "1"3"1Iodine exposure significantly increased lipid peroxidation in kidney and salivary glands in comparison to control animals. Pre supplementation with turmeric extract for 15 days showed significant lowering of lipid peroxidation in kidney. On the other hand vitamin E pre supplementation showed marked reduction in lipid peroxidation in salivary glands. Reduced glutathione levels decreased significantly in liver after radiation exposure. However, pre supplementation with turmeric extract and vitamin E did not improve glutathione levels in liver. In conclusion we have observed ...

2008-10-01

383

Analysis of medicinal plant extracts by neutron activation method; Analise de extratos de plantas medicinais pelo metodo de ativacao com neutrons  

Energy Technology Data Exchange (ETDEWEB)

This dissertation has presented the results from analysis of medicinal plant extracts using neutron activation method. Instrumental neutron activation analysis was applied to the determination of the elements Al, Br, Ca, Ce, Cl, Cr, Cs, Fe, K, La, Mg, Mn, Na, Rb, Sb, Sc and Zn in medicinal extracts obtained from Achyrolcline satureoides DC, Casearia sylvestris, Centella asiatica, Citrus aurantium L., Solano lycocarpum, Solidago microglossa, Stryphnondedron barbatiman and Zingiber officinale R. plants. The elements Hg and Se were determined using radiochemical separation by means of retention of Se in HMD inorganic exchanger and solvent extraction of Hg by bismuth diethyl-dithiocarbamate solution. Precision and accuracy of the results have been evaluated by analysing reference materials. The therapeutic action of some elements found in plant extracts analyzed was briefly discussed 70 refs., 13 figs., 15 ...

1995-12-31

384

The Grounds For Time Dependent Market Potentials From Dealers' Dynamics  

CERN Document Server

We apply the potential force estimation method to artificial time series of market price produced by a deterministic dealer model. We find that dealers' feedback of linear prediction of market price based on the latest mean price changes plays the central role in the market's potential force. When markets are dominated by dealers with positive feedback the resulting potential force is repulsive, while the effect of negative feedback enhances the attractive potential force.

2007-01-01

385

Tritium contamination and decontamination study on materials for ITER remote handling equipment  

Energy Technology Data Exchange (ETDEWEB)

Several materials, lenses, dry bearings and cables were exposed to a tritiated moisture environment to study the behavior of tritium contamination on candidate materials for ITER remote handling equipment. To optimize the tritium removal procedure, decontamination experiments using a gas purge with three different moisture concentrations were also performed. The surface tritium concentrations of CeO{sub 2} containing alkaline barium glass (NB), CeO{sub 2} containing lead glass (LX) and synthetic quartz (Quartz) after the exposure experiments were 7.80, 10.94 and 0.67 Bq/cm{sup 2}, respectively. It was found that the tritium concentration was influenced by the compositions of the materials. The concentrations of tritium on type 831 (solid lubrication material: graphite) and type 237 (solid lubrication material: tungsten disulfate) dry bearings after the exposure experiments were 89.80 and 31.78 Bq/cm{sup 2}, respectively. The tritium concentration in an electric ...

2001-09-01

386

Tritium contamination and decontamination study on materials for ITER remote handling equipment  

International Nuclear Information System (INIS)

Several materials, lenses, dry bearings and cables were exposed to a tritiated moisture environment to study the behavior of tritium contamination on candidate materials for ITER remote handling equipment. To optimize the tritium removal procedure, decontamination experiments using a gas purge with three different moisture concentrations were also performed. The surface tritium concentrations of CeO_2 containing alkaline barium glass (NB), CeO_2 containing lead glass (LX) and synthetic quartz (Quartz) after the exposure experiments were 7.80, 10.94 and 0.67 Bq/cm"2, respectively. It was found that the tritium concentration was influenced by the compositions of the materials. The concentrations of tritium on type 831 (solid lubrication material: graphite) and type 237 (solid lubrication material: tungsten disulfate) dry bearings after the exposure experiments were 89.80 and 31.78 Bq/cm"2, respectively. The tritium concentration in an electric cable tested was 5014 ...

2001-09-01

387

Structure and magnetic properties of nanostructural strontium ferrite prepared by mechanochemical treatment  

International Nuclear Information System (INIS)

Full text: It was recently-established for hexagonal barium ferrite-industrially important magnetically hard material that refinement of the crystallite dimensions into the nanoscale regime, typically #<=# 10 nm, leads after heat treatment at temperatures 800-1000 deg C to significant coercivity increase of up to 6.5 kOe (#approx#3-4 times) with saturation magnetisation values of 50-55 emu/g (#approx#95% of bulk at room temperature). High-energy mechanochemical processing has been applied to prepare nanostructural (nanocrystalline-amorphous) composites. High resolution electron microscopy studies reveal that the enhancement of the final magnetic properties was due to formation of magnetically noninteracting #approx#l,#mu#m Ba-ferrite particles with 5-10 nm amorphous surface layer - depending on annealing parameters. Similar situation was established also for ball milled strontium ferrite (SrFe_1_2O_1_9) powders where short annealing 4 h at 1000 deg C produced ...

388

Strategies for gallium removal after focused ion beam patterning of ferroelectric oxide nanostructures  

International Nuclear Information System (INIS)

As part of a study into the properties of ferroelectric single crystals at nanoscale dimensions, the effects that focused ion beam (FIB) processing can have, in terms of structural damage and ion implantation, on perovskite oxide materials has been examined, and a post-processing procedure developed to remove such effects. Single crystal material of the perovskite ferroelectric barium titanate (BaTiO_3) has been patterned into thin film lamellae structures using a FIB microscope. Previous work had shown that FIB patterning induced gallium impregnation and associated creation of amorphous layers in a surface region of the single crystal material some 20 nm thick, but that both recrystallization and expulsion of gallium could be achieved through thermal annealing in air. Here we confirm this observation, but find that thermally induced gallium expulsion is associated with the formation of gallium-rich platelets on the surface of the annealed material. These platelets ...

2007-01-24

389

Self-expandable stent loaded with {sup 125}I seeds: Feasibility and safety in a rabbit model  

Energy Technology Data Exchange (ETDEWEB)

Objective: To evaluate technical feasibility and acute and subacute radiotolerance of a self-expandable stent loaded with {sup 125}I seeds in the rabbit esophagus. Methods: A self-expandable stent designed for esophageal application was made of 0.16 mm nitinol wire and loaded with {sup 125}I seeds (CIAE-6711). Twenty-seven stents with three different radioactive dosages (n = 9 in each dosage group) were implanted in the esophagus of healthy rabbits, while nine stents alone were used as controls. The stents were perorally deployed into the esophagus under fluoroscopic guidance. Radiological follow-up included plain chest film, CT scan, and barium esophagography which were undertaken in all rabbits of each group at 2, 4, and 8 weeks, respectively, which were correlated to histopathological findings. The stented esophageal segments along with their adjacent tissues were harvested for histopathological examinations. Results: The stent was successfully deployed into the ...

2007-02-15

390

Role of early phase helical CT images in the evaluation of wall invasion of colorectal cancer. Pathological correlation  

Energy Technology Data Exchange (ETDEWEB)

The usefulness of helical CT early phase images optimized by the SmartPrep method for evaluation of wall invasion by colorectal cancer was investigated. Between August 1997 and September 1998, CT was performed to evaluate the primary tumor and local extension in 10 consecutive patients with colorectal cancer confirmed by barium enema- and/or colonoscopy. Early-phase images were acquired by using SmartPrep application software. This method allows the optimal scan delay time to be obtained by continuous monitoring of increases in CT values after injection of contrast medium. Sections of the surgical specimens, close to the same plane as the CT images, and of the same slice thickness, were analyzed histopathologically. All 10 cancers, regardless of size, showed strong enhancement on the early-phase images (81.4-112 HU, mean: 95.1 HU). The strongly enhanced image areas on CT corresponded to the primary cancer areas on histopathological specimens. A low-density zone was ...

2000-02-01

391

Quarterly progress report for the Chemical and Energy Research Section of the Chemical Technology Division: October-December 1997  

Energy Technology Data Exchange (ETDEWEB)

This report summarizes the major activities conducted in the Chemical and Energy Research Section of the Chemical Technology Division at Oak Ridge National Laboratory (ORNL) during the period October--December 1997. The section conducts basic and applied research and development in chemical engineering, applied chemistry, and bioprocessing, with an emphasis on energy-driven technologies and advanced chemical separations for nuclear and waste applications. The report describes the various tasks performed within six major areas of research: Hot Cell Operations, Process Chemistry and Thermodynamics, Separations and Materials Synthesis, Fluid Structure and Properties, Biotechnology Research, and Molecular Studies. The name of a technical contact is included with each task described, and readers are encouraged to contact these individuals if they need additional information. Activities conducted within the area of Hot Cell Operations included efforts to optimize the processing conditions ...

1999-02-01

392

Heavy ion induced changes in nuclear waste glasses: a micro Raman investigation  

International Nuclear Information System (INIS)

Borosilicate based glass formulations have been found suitable for fixing the HLW (high level radioactive liquid waste) generated after reprocessing of the spent nuclear fuel. As the glass experiences continuous irradiation by #alpha#, #beta#a, and #gamma# radiations from the radioactive components of HLW, alteration in the glass structure may occur. Understanding of these structural evolutions of the nuclear waste glasses under irradiation is crucial to secure long term disposal and predict their behavior. In the present work, alkali based barium borosilicate glasses, having composition similar to that of Trombay Research Reactor waste glass were irradiated with high energy "1"2C beam and the radiation induced changes were monitored by micro Raman experiment. Since a "1"2C atom can be considered as a cluster of alphas, this beam was chosen to yield linear energy losses (LET) comparable to that in case of a particles. The irradiations were carried out at 30 deg N ...

2010-12-01

393

Evaluation of a novel radiopacifiying agent on the physical properties of surgical spineplex.  

Science.gov (United States)

Polymethlylmethacrylate (PMMA) is the most frequently used cement for percutaneous vertebroplasty and kyphoplasty. To aid visualisation during surgery cements are doped with radiopacifying agents such as Barium sulphate (Ba(2)SO(4)) or Zirconium Dioxide (ZiO(2)). Mounting research suggests that these agents may impair the biocompatibility of the cements. However, incorporating an alternative radiopacifier agent with excellent biocompatibility would be a significant step forward. Bioactive radiopaque glasses incorporating elements such as strontium (Sr) and zinc (Zn), known to have beneficial and therapeutic effects on bone, are of great interest in this respect. In this study, the Ba(2)SO(4) of the commercially available Spineplex was incrementally replaced with a radiopaque therapeutic glass composition. The resulting effects on cement setting time, peak isotherm, ultimate compressive strength, Young's modulus (up to 30 days cement maturation) and radiopacity were ...

2009-08-18

394

Effect of Ho{sup 3+} substitutions on the structural and magnetic properties of BaFe{sub 12}O{sub 19} hexaferrites  

Energy Technology Data Exchange (ETDEWEB)

Holmium doped barium based hexaferrites BaFe{sub 12-2x}Ho{sub 2x}O{sub 19} with (x = 0.0-1.0) were synthesized by solid state reaction method. Structural and magnetic characterization of these ferrites provide significant information about their reactive physical properties. X-ray analysis reveals that in all samples M-type structure exist with few secondary phases. Scanning electron microscope revealed the grain size of the specimen. The results show that grain size decreases with the substitution degree of Holmium. Thus rare earth element Holmium Ho{sup 3+} acts as a grain growth inhibitor. The magnetic hysteresis loops show the variation in the values of magnetic parameters like saturation magnetization (M{sub s}), remanent magnetization (M{sub r}) and coercivity (H{sub c}) were observed by changing Ho{sup 3+} content in BaFe{sub 12-2x}Ho{sub 2x}O{sub 19} ferrites. Coercivity showed a maximum value of 2230 Oe for (x = 0.4) and then decreasing trend were observed ...

2010-04-09

395

Defecographic diagnosis of the puborectalis syndrome; Diagnosi mediante defecografia della sindrome del muscolo puborettale  

Energy Technology Data Exchange (ETDEWEB)

The puborectalis syndrome is a defecation disorder supported by the nonrelaxation of puborectalis sling with consequent dyschezia. They report on a series of 98 patients submitted to clinical examination, defecography, anorectal manometry, electromyography and intestinal transit time studies. The main symptoms of puborectalis syndrome in their patients were incomplete defecation (89 %) and intermittent evacuation (63 %); 28 % of patients turned to finger defecation. In all patients, defecography showed an abnormal increase in puborectalis impression on the posterior anorectal wall, reduced anorectal angle opening under straining (mean value: 113 deg) and prolonged expulsion time with barium pooling in the ampulla (mean evacuation time: 38 seconds). Such anorectal abnormalities as rectal mucosal prolapse (47 cases) and anterior rectocele (36 cases) were also associated. In 33 of 98 patients (34 % of cases), sling assessment by bidigital palpation at preliminary ...

1997-04-01

396

Defecographic diagnosis of the puborectalis syndrome  

International Nuclear Information System (INIS)

The puborectalis syndrome is a defecation disorder supported by the nonrelaxation of puborectalis sling with consequent dyschezia. They report on a series of 98 patients submitted to clinical examination, defecography, anorectal manometry, electromyography and intestinal transit time studies. The main symptoms of puborectalis syndrome in their patients were incomplete defecation (89 %) and intermittent evacuation (63 %); 28 % of patients turned to finger defecation. In all patients, defecography showed an abnormal increase in puborectalis impression on the posterior anorectal wall, reduced anorectal angle opening under straining (mean value: 113 deg) and prolonged expulsion time with barium pooling in the ampulla (mean evacuation time: 38 seconds). Such anorectal abnormalities as rectal mucosal prolapse (47 cases) and anterior rectocele (36 cases) were also associated. In 33 of 98 patients (34 % of cases), sling assessment by bidigital palpation at preliminary ...

397

Rubber Production in Guayule: Determination of Rubber Producing Potential 1  

UK PubMed Central (United Kingdom)

Optimum conditions for the rapid, efficient, nondestructive determination of rubber producing potential in guayule (Parthenium argentatum) were established. The rubber producing potential...Full Text Available

1986-08-01

398

Potential description of cluster channel of lithium nuclei  

International Nuclear Information System (INIS)

The new Gaussian potentials and interactions with forbidden states consistent with the phase scattering at low energies were obtained. Cross sections, resonance level spectra and some characteristics of bound states of lithium nuclei are calculated with these potentials.

399

Measurement of the Water Potential of Stored Potato Tubers 1  

UK PubMed Central (United Kingdom)

A method of measuring the water potential of stored potato tubers (Solanum tuberosum L.) was needed to investigate the relationship of bacterial soft rot in tubers to water potential....Full Text Available

1985-11-01

400

Pitting corrosion of nickel base alloys in halide media  

International Nuclear Information System (INIS)

A computerized corrosion measuring system (EG and G model 350 A) was used to study the influence of Cr, Mo, Ti, Nb and W on the pitting corrosion of nickel base alloys in 3% NaCl at 90"0C. The electrochemical parameters under investigation are the corrosion potential E_c_o_r_r, pitting potential E_p and protection potential E_p_p. The corrosion behaviour of nickel base alloys were studied by using pitting scan and potentiostatic techniques. Values of corrosion potential, pitting potential and protection potential were used for a ranking of alloys for corrosion resistance.

1988-03-06

401

High-power radio frequency pulse generation and extraction based on wakefield excited by an intense charged particle beam in dielectric-loaded waveguides  

International Nuclear Information System (INIS)

Power extraction using a dielectric-loaded (DL) waveguide is a way to generate high-power radio frequency (RF) waves for future particle accelerators, especially for two-beam-acceleration. In a two-beam-acceleration scheme, a low-energy, high-current particle beam is passed through a deceleration section of waveguide (decelerator), where the power from the beam is partially transferred to trailing electromagnetic waves (wakefields); then with a properly designed RF output coupler, the power generated in the decelerator is extracted to an output waveguide, where finally the power can be transmitted and used to accelerate another usually high-energy low-current beam. The decelerator, together with the RF output coupler, is called a power extractor. At Argonne Wakefield Accelerator (AWA), we designed a 7.8GHz power extractor with a circular DL waveguide and tested it with single electron bunches and bunch trains. The output RF frequency (7.8GHz) ...

402

Factoring Potential Accelerator Transmutation of Waste Demonstrations into Accelerator Production of Tritium Design Planning  

CERN Document Server

Factoring Potential Accelerator Transmutation of Waste Demonstrations into Accelerator Production of Tritium Design Planning

1998-01-01

403

Adaptive Management of Liver Cancer Radiotherapy  

UK PubMed Central (United Kingdom)

Adaptive radiation therapy for liver cancer has the potential to reduce normal tissue complications and enable dose escalation, allowing the potential for tumor control in this challenging site....Full Text Available

2010-04-01

404

Transuranic separation using organophophorus extractants adsorbed onto superparamagnetic carriers.  

Energy Technology Data Exchange (ETDEWEB)

Polymeric coated ferromagnetic carriers with an absorbed layer of octyl(phenyl)-N,N-diisobutylcarbamoylmethylphosphine oxide (CMPO) diluted by tributyl phosphate (TBP) are being evaluated for application in the separation and the recovery of low concentrations of americium, plutonium, and uranium from nuclear waste solutions. Due to their chemical nature, these extractants selectively complex americium and plutonium contaminants onto the particles and the complexed particles can be recovered from the solution using a magnet. Physical and chemical characterization of the extractant-absorbed particles were performed by gamma and liquid scintillation counting, scanning electron microscopic (SEM) micrograph, and other physical measurements. Plutonium, americium, and uranium separations have been performed at various HNO{sub 3} and HCl concentrations. Parameters were studied to determine the limitations and capacity of the process. The status of the ...

1998-10-07

405

The separation of trivalent actinides from lanthanides by dithiophosphinic acids from HNO_3 acid medium  

International Nuclear Information System (INIS)

The extraction of Am(III) and Eu(III) has been investigated using mixtures of synthesized aromatic dithiophosphinic acids (R_2PSSH) and tributylphosphate (TBP), trioctylphosphine oxide (TOPO) or tributylphosphine oxide (TBPO) in toluene from nitric acid (0.01-1.5 mol l"-"1). There was no detectable extraction when R_2PSSHs were used alone as extractants for either Am(III) or Eu(III) (D_A_m_,_E_u<10"-"4) under the experimental conditions used in this study. High separation factors (D_A_m/D_E_u>20) with D_A_m>1 were achieved in the nitric acid range 0.1-1 moll"-"1 by means of a synergistic mixture of bischlorodithiophosphinic acid with TBP, TOPO or TBPO. (orig.)

1998-06-12

406

The separation of "2"0"3Pb from a thallium target  

International Nuclear Information System (INIS)

"2"0"3Pb, an ideal radionuclide for toxicological studies, can be artificially produced by bombardment of a thallium target but due to the extreme toxicity of thallium the lead has to be separated completely from the thallium. A single step method is here described consisting of removing the thallium from a dilute acid chloride solution using a continuous ethyl ether extraction. Essentially all of the thallium and almost none of the lead is removed in a 3-hr extraction. Because the ether is recycled, only about 30 ml are needed. If other contaminants are introduced from the bombardment and its subsequent manipulations, an additional step is used in which the lead is extracted from an iodide solution with methyl isopropyl keton. (U.K.).

407

Sulfonaphtholazoresorcinol as reagent for tungsten  

International Nuclear Information System (INIS)

Interaction of W(6) with sulphonaphtholazoresorcinol (SNAR) in aqueous solution has been studied. Tungsten is determined in the form of sulphonaphtholazoresorcinate by extraction with higher alcohols. The optimum conditions for the formation of a complex of W with SNAR in aqueous solution are as follows: a 10-fold excess of SNAR, concentration of HCl 1-1.5N, ethanol content 5-10 vol.%, time of formation of the complex 30 min. A component ratio for the complex has been established in the case of aqueous solution and extract; molar extinction coefficients are 0.9x10"4 and 1.7x10"4, respectively. The formation constant for the complex being extracted is 2.2x10"2"3. A method has been developed for determination of microgram quantities of W in a vanadium specimen.

1977-01-01

408

Separation of lithium and calcium isotopes during chemical isotopic exchange in extraction systems with phosphoryl-containing podands  

International Nuclear Information System (INIS)

A study was made on extraction of a series of lithium and calcium salts by monopodands L with common formula R-C_6H_4-O-(CH_2CH_2O)_n-C_6H_4-R, where R - CH_2P(O)Ph_2, n 1-3. Extraction-chromatographic separation of lithium and calcium isotopes in systems of metal aquacomplex-solvatocomplex with L in organic phase was conducted. It was established that separation coefficients of "6Li/"7Li isotopes ranged between 1.003 #+-#0.001 and 1.017 #+-#0.002 at the maximal separation degree equal to 1.60. Separation of "4"0Ca/"4"4Ca isotopes was not fixed. 12 refs., 4 figs., 1 tab.

409

Optimization of extraction of high-ester pectin from passion fruit peel (Passiflora edulis flavicarpa) with citric acid by using response surface methodology  

British Library Electronic Table of Contents (United Kingdom)

A central composite design was employed to optimize the extraction of pectin with citric acid. The independent variables were citric acid concentration (0.086-2.91% w/v) and extraction time (17-102min). The combined effect of these variables on the degree of esterification was investigated. Results have shown that the generated regression models adequately explained the data variation and significantly represented the actual relationship between the independent variables and the responses. Besides that, the citric acid concentration was the most important factor to affect the degree of esterification, as it exerted a significant influence on the dependent variable. Lower citric acid concentration increased the pectin degree of esterification. The surface response showed the relationships b...

2008-01-01

410

Modulation of lipopolysaccharide-induced pro-inflammatory mediators by an extract of Glycyrrhiza glabra and its phytoconstituents  

British Library Electronic Table of Contents (United Kingdom)

Objective To evaluate the inhibitory property of de-glycyrrhizinated extract of Glycyrrhiza glabra root and its phytoconstituents (glabridin, isoliquiritigenin and glycyrrhizin) on LPS-induced production of pro-inflammatory mediators. Materials and methods Inhibitory effect of G. glabra extract and its phytoconstituents were studied on lipopolysaccharide (LPS)-induced nitric oxide (NO), interleukin-1 beta (IL-1 beta) and interleukin-6 (IL-6) levels in J774A.1 murine macrophages. Results G. glabra and isoliquiritigenin significantly inhibited LPS stimulated NO, IL-1 beta and IL-6 production. Glabridin showed significant inhibition of NO and IL-1 beta release, but failed to attenuate IL-6 levels at the tested concentrations. In addition, glycyrrhizin did not exhibit inhibitory response towar...

2011-01-01

411

Geochemical features of re-deposited organic matter occurring in fluvioglacial sediments in the Racib?rz region (Poland): A case study  

British Library Electronic Table of Contents (United Kingdom)

The erosion of rocks rich in organic matter typically leads to the complete mineralization of the organic material. However, in some cases, it is re-deposited to become a part of sediments once more. This process should be considered to be a part of global carbon cycle, possibly much more significant than assumed to-date. The research presented here aims to characterize re-worked organic matter occurring in post-glacial sediments of southern part of Poland, in the Oder river valley (the Racib?rz town region, Miocene, Pleistocene and Holocene age). Organic substances extracted from the sediments originated from organic matter that had resided in rocks eroded by glaciers. Sediments were sampled in two boreholes which sediments were correlated. Sediments were extracted and extracts analyzed w...

2008-01-01

412

Fault diagnosis of roller bearing using fuzzy classifier and histogram features with focus on automatic rule learning  

British Library Electronic Table of Contents (United Kingdom)

Roller bearing is one of the most widely used elements in rotary machines. Condition monitoring of such elements is conceived as pattern recognition problem. Pattern recognition has three main phases: feature extraction, feature selection and feature classification. Histogram features can be used for fault diagnosis of roller bearing. This paper presents the use of decision tree for selecting best few histogram features (bin ranges) that will discriminate the fault conditions of the bearing from given train samples. These features are extracted from vibration signals. A rule set is formed from the extracted features and fed to a fuzzy classifier. The rule set necessary for building the fuzzy classifier is obtained largely by intuition and domain knowledge. This paper also presents the usag...

2011-01-01

413

Extraction of rare earths by carbonic acids melts  

Energy Technology Data Exchange (ETDEWEB)

Extraction of rare earths (La, Ce, Pr, Eu, Gd, Er, Yb) from nitrate solutions by melts of carboxylic acids of the C/sub 17/-C/sub 20/ fraction and stearic acid with paraffin, depending on the temperature (60-90 deg), phase contact time and their volume ratio (O:B from 1:5 up to 1:100), pH of the aqueous phase (2-6), rare earth concentration (10/sup -6/-10/sup -3/ m) is studied. It is shown that in the whole concentration range investigated rare earths are extracted quantitatively into the carboxylic acid melt of C/sub 17/-C/sub 20/ fraction at the equilibrium value of pH>=3.8, while into the melt of 0.1 M stearic acid in paraffin at pH>=4.5.

1980-10-01

414

Extraction of biologic particles by pumping effect in a p-shaped ultrasonic actuator  

British Library Electronic Table of Contents (United Kingdom)

This paper presents a new method of extracting biologic particles from a mixture of particles. The method is based on the pumping effect in a p-shaped ultrasonic actuator, which has a gap between its two vibrating metal plates. An adhesive tape is placed at a proper position in the gap. Due to the pumping effect which is induced by the sound field in the gap, the particles with smaller mass and radius in the mixture can be pumped up to reach the adhesive tape; while the ones with larger mass cannot. Therefore, the particles with smaller mass and radius can be extracted from the mixture. A theoretical model which can well explain the operation principle and experimental phenomena is developed. By the experimental results and the theoretical analyses based on the model, the validity of the m...

2006-01-01

415

Extraction of Cs-137 by alcohol-water solvents from plants containing cardiac glycosides  

CERN Document Server

As a result of nuclear power plant accidents, large areas receive radioactive inputs of Cs-137. This cesium accumulates in herbs growing in such territories. The problem is whether the herbs contaminated by radiocesium may be used as a raw material for medicine. The answer depends on the amount of Cs-137 transfered from the contaminated raw material to the medicine. We have presented new results of the transfer of Cs-137 from contaminated Digitalis grandiflora Mill. and Convallaria majalis L. to medicine. We found that the extraction of Cs-137 depends strongly on the hydrophilicity of the solvent. For example 96.5%(vol.) ethyl alcohol extracts less Cs-137 (11.6%) than 40%(vol.) ethyl alcohol or pure water (66.2%). The solubility of the cardiac glycosides is inverse to the solubility of cesium, which may be of use in the technological processes for manufacturing ecologically pure herbal medicine.

2001-01-01

416

Extraction methods of phase information for X-ray diffraction enhanced imaging  

Energy Technology Data Exchange (ETDEWEB)

X-ray diffraction enhanced imaging (DEI) is one of X-ray phase-contrast imaging methods, which is applied to inspect internal structures of weakly absorbing low-Z samples. The key problem of the DEI is how to extract phase information which is expressed by refraction-angle images from a series of DEI images measured in different positions of the rocking curve of the analyzer. Three effective extraction methods are presented in this paper: the statistical geometric-optics-approximation method, the maximum refraction-angle method and the Gaussian curve fitting method. They are compared with the existing methods, such as the D. Chapman's geometric optics approximation method and the multiple-images statistical method. A 2D computer simulation experiment is performed to draw comparisons of these methods. The experimental results prove that the above three methods have more precision of refraction-angle values than existing methods.

2007-08-21

417

Extraction methods of phase information for X-ray diffraction enhanced imaging  

International Nuclear Information System (INIS)

X-ray diffraction enhanced imaging (DEI) is one of X-ray phase-contrast imaging methods, which is applied to inspect internal structures of weakly absorbing low-Z samples. The key problem of the DEI is how to extract phase information which is expressed by refraction-angle images from a series of DEI images measured in different positions of the rocking curve of the analyzer. Three effective extraction methods are presented in this paper: the statistical geometric-optics-approximation method, the maximum refraction-angle method and the Gaussian curve fitting method. They are compared with the existing methods, such as the D. Chapman's geometric optics approximation method and the multiple-images statistical method. A 2D computer simulation experiment is performed to draw comparisons of these methods. The experimental results prove that the above three methods have more precision of refraction-angle values than existing methods.

2007-08-21

418

Experimental study on Satureja montana as a treatment for premature ejaculation  

British Library Electronic Table of Contents (United Kingdom)

Aim of the study: Satureja montana (winter savory) is a medicinal plant traditionally used to treat different disorders including male sexual dysfunction. In this study we evaluated the effect of Satureja montana hydroalcoholic extract on copulatory behavior of sexually potent male rats. Materials and methods: The extract was orally administered acutely or repetitively for 8 consecutive days at the doses of 25 and 50mg/kg. The main parameters of sexual behavior, mount (ML), intromission (IL), ejaculation (EL) latencies and post-ejaculatory interval (PEI), were evaluated in animals submitted to mating test and multiple ejaculations test. Testosterone serum levels were measured in rats acutely treated with Satureja montana extract dosed at 50mg/kg. In addition the open field test was conduct...

2011-01-01

419

Effect of some reducing and complexing agents on the extraction behavior of technetium in the TBP-HNO3 system  

British Library Electronic Table of Contents (United Kingdom)

The effect of a series of complexing and reducing agents on the extraction-chemical behavior of technetium as applied to extraction splitting of uranium and plutonium in the Purex process was examined. Kinetic parameters of the catalytic decomposition of N2H5NO3 under the action of Tc in the presence of these agents were evaluated. Variation of the ratio of the oxidized and reduced Tc species in the course of the process and in the hydrazine-free systems was determined. Reagents preventing oxidation of the reduced technetium and decomposition of N2H5NO3 in nitric acid solutions (acetohydroxamic acid, hydroxylamine, ascorbic acid, etc.), inhibiting the reduction of Tc with hydrazine nitrate (H2O2, HN3, etc.), and known as complexing agents toward quadrivalent actinides but indifferent to Tc...

2011-01-01

420

Effect of complexing agents (DTPA and oxalic acid) on the extraction behavior of technetium in the TBP-N2H5NO3-HNO3 system  

British Library Electronic Table of Contents (United Kingdom)

The effect of complexing agents DTPA and H2C2O4 on the extraction-chemical behavior of Tc, as applied to extractive splitting of U and Pu in the Purex process, was studied. The kinetic relationships of catalytic decomposition of N2H5NO3 under the action of Tc in the presence of these agents were determined. Variation of the ratio of the oxidized and reduced Tc species in the course of this process at various HNO3 concentrations was examined. In the final step of the reaction of N2H5NO3 with Tc in a nitric acid solution, when the reductant content is stabilized, the oxidation of reduced Tc also stops or continues at a considerably lower rate than before stabilization. The presence of DTPA decreases the rate of Tc(IV) oxidation owing to its binding in a complex and decreases the fraction of ...

2011-01-01

421

Dynamic optimization of the benzene extractive distillation unit  

Scientific Electronic Library Online (English)

Abstract in english A mathematical model has been developed for describing the dynamic operation of the N-formylmorpholine extractive distillation column and the corresponding solvent recovery column in the benzene extraction plant. The NRTL equation was used to calculate the equilibrium and thermodynamic properties of the mixtures. The validity of the model in terms of temperature, pressure and split fraction was examined using actual plant data at steady-state conditions. Comparison betwee (more) n model results and plant data shows good consistency. In order to improve the control of the process and selection of the optimal control strategy, the model was used to find the optimum values of the constants of the controllers with Nelder-Mead algorithm during unsteady-state operation by minimizing the deviation from steady-state conditions. The outcome of this study could be used by operators and engineers to increase the productivity of the ...

2008-12-01

422

Direct nano ESI time-of-flight mass spectrometric investigations on lanthanide BTP complexes in the extraction-relevant diluent 1-octanol  

Energy Technology Data Exchange (ETDEWEB)

The present work focuses on investigations of a highly selective ligand for Am(III)/Ln(III) separation: bis-triazinyl-pyridine (BTP). By means of nano-electro-spray mass spectrometry, complex formation of BTP with selected elements of the lanthanide series is investigated. We show that the diluent drastically influences complex speciation. Measurements obtained in the extraction-relevant diluent 1-octanol show the occurrence of Ln(BTP){sub i} (i 1-3) species in different relative abundances, depending on the lanthanide used. Here, the relative abundances of the Ln(BTP){sub 3} complexes correlate with the distribution ratios for extraction to the organic phase of the respective lanthanide. (authors)

2009-12-15

423

Dietary plant materials reduce acrylamide formation in cookie and starch-based model systems  

British Library Electronic Table of Contents (United Kingdom)

Abstract BACKGROUND: Dietary plant materials have attracted much attention because of their health benefits to humans. Acrylamide is found in various heated carbohydrate-rich foods. Our previous results showed that crude aqueous extracts from diverse dietary plants and some phenolic compounds could mitigate acrylamide formation in an asparagine-glucose model system. Based on our previous study, several plant materials were selected to further investigate their inhibitory effects on acrylamide formation in cookies and starch-based model systems. RESULTS: Addition of raw powders from selected dietary plants and their crude aqueous extracts could considerably reduce acrylamide formation in both cookie and potato starch-based models. Aqueous extracts of clove at 4% caused the largest reduction...

2011-01-01

424

Development of processes for bench scale production of yellow cake from euxenite  

International Nuclear Information System (INIS)

A Process for yellow cake production from local Euxenite was developed in Bench Scale by using sulphuric acid digestion with simultaneously ion-exchange and solvent extraction purification steps. Uranium was then precipitated as uranium diuranate by ammonia solution. Equipment used in this process includes : digestion vessels, columnar ion-exchange, solvent extraction and precipitation units Ore feed to the process could be adjusted up to 2 kilogram per day (8 hours operation) with yellow cake product purity meet the requirement of Usaec standard of about 10-50 gram per day. Included in this experiment are the leaching characteristics of the ore, the design and construction of continuous columnar 4-cycle ion exchange unit, determination of the extraction and stripping stages of a gravity flow mixer-settler and the design and construction of continuous yellow cake precipitation unit with large grain size and high density ...

1985-01-01

425

Comparative Evaluation of Different Cell Lysis and Extraction Methods for Studying Benzo(a)pyrene Metabolism in HT-29 Colon Cancer Cell Cultures  

British Library Electronic Table of Contents (United Kingdom)

Abstract Lysis and extraction of cells are essential sample processing steps for investigations pertaining to metabolism of xenobiotics in cell culture studies. Of particular importance to these procedures are maintaining high lysis efficiency and analyte integrity as they influence the qualitative and quantitative distribution of drug and toxicant metabolites in the intra- and extracellular milieus. In this study we have compared the efficiency of different procedures viz. homogenization, sonication, bead beating, and molecular grinding resin treatment for disruption of HT-29 colon cells exposed to benzo(a)pyrene (BaP), a polycyclic aromatic hydrocarbon (PAH) compound and a suspected colon carcinogen. Also, we have evaluated the efficiency of various procedures for extracting BaP parent c...

2011-01-01

426

Chemical versus solvent extraction treatment: Comparison and influence on polyester based bio-composite mechanical properties  

British Library Electronic Table of Contents (United Kingdom)

The influence of chemical and solvent extraction compatibilising techniques on the mechanical properties of poly-lactic acid (PLA) and MaterBi-polyester (PEM) based bio-composites are compared. First, fibres were chemically grafted with two fatty chains: stearic anhydride and octadecylisocyanate. Grafted fibres were characterised by FTIR and elemental analyses. Contact angle measurements show the hydrophobisation of the fibres in spite of very low surface grafting. Extracted and non-grafted fibres were prepared to be used as references. PEM and PLA-based composites with 30% w/w were prepared by compression moulding. Their mechanical properties were studied. It was found that chemical and solvent treatment of the fibres improved the reinforcement effect in the case of a PEM matrix and the Y...

2010-01-01

427

Analysis of polyelectrolyte complexes formed with jicama pectic polysaccharide and water-soluble chitosan  

British Library Electronic Table of Contents (United Kingdom)

Abstract Jicama (Pachyrhizus erosus L.) is a root-based legume that has been cultivated in Mexico for centuries. Pectic polysaccharide from de-starched jicama pomace was extracted using an autoclave-assisted process and physicochemically characterized. The extracted polysaccharide (1.0 g L-1) was used for the formation of polyelectrolyte complexes (PECs) with water-soluble chitosan (WSCh; 0.5, 1.0 and 2.0 g L-1). The extraction yield of jicama pectic polysaccharide was 22.8 wt% (dry basis) and infrared spectroscopic analysis showed that it was methoxylated to a small degree. Thermogravimetric analysis indicated that this biopolymer was very stable, its weight loss being 51.2% after heating at 479 C. Anion-exchange chromatography showed it to have a wide and heterogeneous charge density. Th...

2011-01-01

428

Alcohol fermentation in olive oil extraction effluents  

Energy Technology Data Exchange (ETDEWEB)

Eight culture-collection yeast strains of various species and five newly isolated stains were tested for both growth in olive oil extraction effluents and fermentation of the sugars in the same media. The culture-collection yeast strains did not grow in an effluent containing 2.86% sugar (w/v), 8 g/litre phenolic substances, 4.58 g/litre titratable acidity and pH 4.96, whereas the newly isolated strains of Torulopsis sp. MK-1, Saccharomyces norbensis MC-1, S. oleaceus MC-2 and S. oleaginosus grew well and fermented the sugars. In the medium mentioned above, they produced alcohol in amounts of 1.63 to 1.38%, respectively. None of the yeasts grew in an olive oil extraction effluent vacuum-concentrated to over 13-14% of dry matter. The strain of T. sp. MK-1 showed a higher stability.

1989-01-01

429

A novel process for extraction of natural sweetener from licorice (Glycyrrhiza glabra) roots  

British Library Electronic Table of Contents (United Kingdom)

Pressurized hot water extraction (PHWE) is a very useful technique for recovering bioactive molecules from natural materials using subcritical compressed liquid water in the temperature range of 50-150degreeC. A novel process has been developed for making a natural sweetener from licorice (Glycyrrhiza glabra) roots involving selective chemical reaction and easy separation, for recovering mono-ammonium glycyrrhizate (MAG) using hot water with dissolved ammonia and pressurized with carbon dioxide. The performance of the novel PHWE process has been evaluated to ascertain the optimum process parameters to maximize the recovery of MAG by varying the parameters, such as temperature (30-120degreeC), pressure (1-10atm), extraction time (60-120min), water-to-feed ratio (20-40ml/g), number of stages...

2008-01-01

430

A Comparative Study of Hydrodistillation and Hydrodistillation?Solvent Microextraction Methods for Identification of Volatile Components of Echinophora cinerea  

British Library Electronic Table of Contents (United Kingdom)

A recently developed hydrodistillation?solvent microextraction (HD?SME) method coupled to gas chromatography?mass spectrometry (GC?MS) was applied to the analysis of volatile components of aerial parts of Echinophora cinerea (Boiss). By the use of a simplex optimization method, the effects of extraction time, sample weight and microdrop volume on the extraction efficiency of the method were optimized. In the optimized conditions, 3??L of n-heptadecane was suspended in the headspace of 6?g of hydrodistillating sample, using a microsyringe. After 7?min, the solvent was retracted back into the syringe and directly injected into the GC?MS injection port. The HD?SME method was compared to a conventional hydrodistillation technique. In general, the extraction with HD?SME was relatively faster an...

2009-01-01

431

Materials used in new generation vehicles: supplies, shifts, and supporting infrastructure  

Energy Technology Data Exchange (ETDEWEB)

The Partnership for a New Generation of Vehicles (PNGV) program intends to develop new designs for automobiles that will reduce fuel consumption by two thirds but otherwise have price, comfort, safety, and other measures of performance similar to the typical automobile now on the market. PNGV vehicle designs are expected to substitute lightweight materials, such as aluminum, magnesium, carbon-reinforced polymer composites, glass-reinforced polymer composites, and ultra- light steel, for heavier materials such as steel and iron in automobile components. The target mass of a PNGV vehicle is 1,960 pounds, as compared to the average current vehicle that weights 3,240 pounds. Other changes could include the use of different ferrous alloys, engineering changes, or incorporation of advanced ceramic components. Widespread adoption of these vehicle designs would affect materials markets and require concurrent development and adoption of supporting technologies to supply the materials and to use ...

1997-08-01

432

Use of hydrolyzed polyacrylonitrile for limiting the influxes of water at the Sokolovgoroskiy field  

Energy Technology Data Exchange (ETDEWEB)

A formula and technology are presented for the preparation of a hydrolyzed polyacrylonitrile (gipane) from the wastes of chemical production, analysis of the results of working to use them to insulate influxes of water in the extracting wells of the Sokolovogorskiy field.

1980-01-01

433

Use of countercurrent liquid chromatography for the preconcentration and separation of inorganic compounds: group extraction of Zr, Hf, Nb, and Ta for their subsequent determination by inductively coupled plasma atomic emission spectroscopy  

International Nuclear Information System (INIS)

The possibility of the group preconcentration of Zr(4), Hf(4), Nb(5), and Ta(5) countercurrent liquid chromatography using extraction systems based on di-2-ethylhexylphosphoric acid N-benzoyl-N-phenylhydroxylamine, and tetraoctylethylenediamine (TOEDA) is studied. A method have been proposed for the group extraction of Zr(4), Hf(4), Nb(5), and Ta(5) from solution of geological samples. At the stage of the preconcentration of Zr(40, Hf(4), Nb(5) and Ta(5) with a 0.1 M solution of TOEDA in chloroform from mixture of oxalic (0.01 M) and hydrochloric (0.1 M) acids, matrix components are eluted with a flow of the mobile phase, Then, upon changing the eluent (2.0 M HCl), the four elements mentioned above are extracted to a small (7-8 mL) eluate fraction. The results of determining Zr, Hf, Nb, and Ta by inductively coupled plasma atomic emission spectrometry in the international standard reference material Granite GM after their ...

1997-11-01

434

Two-site exchange revisited: a new method for extracting exchange parameters in biological systems.  

UK PubMed Central (United Kingdom)

A new analysis is presented which links real volume fractions, relaxation rates, and intracompartmental exchange rates directly with apparent volume fractions and relaxation rates obtained from biexponential...Full Text Available

1989-02-01

435

Thymoquinone and cisplatin as a therapeutic combination in lung cancer: In vitro and in vivo  

UK PubMed Central (United Kingdom)

BackgroundThymoquinone (TQ) is a compound extracted from Black Caraway seeds of Nigella Sativa and is active against various cancers. Cisplatin (CDDP) is the most...Full Text Available

436

Thermodynamic prediction of distribution coefficients for the solvent extraction of the rare earth metals  

International Nuclear Information System (INIS)

A thermodynamic model for predicting the distribution coefficients has been developed by taking into account the extraction mechanism and the chloride complexation when Sm, Eu, Gd, Tb, Dy and Ho for single component systems are extracted from acidic chloride solutions by di-2-ethylhexyl ester in kerosene, respectively. The model equation includes two constants, of which one corresponds to the apparent extraction equilibrium constant and the other is due to the variation of the activity coefficients of organic species. These values are determined from a few experimental data by the curve fitting method. Then, the distribution coefficients under untried calculations, Bromley's formulation is used to estimate the activity coefficients of aqueous species and the interaction parameters for some rare earth chlorides are reported in terms of morality and molarity using data from Spedding et al. According to the authors the ...

437

The determination of hemoglobin and myoglogin residues as a parameter for testing heat exposure in back bacon.  

UK PubMed Central (United Kingdom)

The use of an extraction of the heme pigments hemoglobin and myoglobin as a test for the heat exposure of back bacon was investigated by treating back bacon at varying temperatures of 50-70 degrees...Full Text Available

1976-07-01

438

The control of sulphate reduction in bacteria  

UK PubMed Central (United Kingdom)

1. An enzyme from Escherichia coli 9723 that reduces adenosine 3′-phosphate 5′-sulphatophosphate to inorganic sulphite is described. Extracts of E. coli...Full Text Available

1965-07-01

439

The Nature of Arsenic-Phytochelatin Complexes in Holcus lanatus and Pteris cretica1  

UK PubMed Central (United Kingdom)

We have developed a method to extract and separate phytochelatins (PCs)—metal(loid) complexes using parallel metal(loid)-specific (inductively coupled plasma-mass spectrometry) and organic-specific...Full Text Available

2004-03-01

440

Tanana River Floodplain Dissolved Organic Nitrogen (DON) Budget, GPS coordinates for Tanana River Floodplain study plots  

Science.gov (United States)

Ammonium, Nitrate, and Amino Acid concentrations in .5M K2SO4 extracted T0 Tanana Floodplain soils Ammonium, Nitrate, and Amino Acid concentrations in . ... ...

441

System Requirements Document for the Molten Salt Reactor Experiment  

Energy Technology Data Exchange (ETDEWEB)

The purpose of the conversion process is to convert the {sup 233}U fluoride compounds that are being extracted from the Molten Salt Reactor Experiment (MSRE) equipment to a stable oxide for long-term storage at Bldg. 3019.

2000-04-01

442

Surface tension of a coal extract in an organic solvent; Sekitan chushutsu seibun no kaigo to hyomen choryoku  

Energy Technology Data Exchange (ETDEWEB)

The behavior and properties of associated bodies were studied through measurement of surface tension considering acetone-soluble fraction relatively light among various solvent extracts of coal. In experiment, the acetone-soluble fraction was extracted from the substances extracted from Upper Freeport coal as standard specimen using the mixed solvent of carbon disulfide (CS2) and N-methyl-2-pyrrolidinone (NMP), and it was dissolved into NMP after drying. Surface tension was measured by Wilhelmy method. The experimental results are as follows. Equilibrium surface tension is equal to the surface tension of pure solvent in a low concentration range of solution, and decreases with an increase in concentration approaching a fixed value at 0 in log concentration, nearly showing an S curve. Adsorption of species with non-polar aromatic ring of the acetone-soluble fraction on a solution surface probably decreases surface tension. ...

1996-10-28

443

Steam turbines for cogeneration plants; Dampfturbinen fuer die Kraft-Waerme-Kopplung  

Energy Technology Data Exchange (ETDEWEB)

The demand for cogeneration plants is growing worldwide. For the combination of electricity generation and heat extraction in power stations facilitates an excellent fuel exploitation and makes the operator of the plant independent from external energy suppliers. (orig.)

2006-07-01

444

Spectrophotometric determination of titanium and iron-application to Cherat volcanic ash, N.W.F.P  

International Nuclear Information System (INIS)

A rapid and sensitive method for the separation and determination of titanium and iron in thiocyanate system has been developed. The extractability of Ti(II) by high molecular weight (HMWA) in organic solvent (HCl/sub 3/) and its separation from Fe(III) was examined. The yellow coloured complex of Ti(II)-SCN in quantitatively extracted into the organic phase containing tribenzyl tribenzylamine (TBA) - a high molecular weight amine, whereas the blood red coloured complex of Fe(III)-SCN formed under the same conditions get separated in the aqueous phase. On the basis of the selective extractability, a method has been developed for the separation as well as simultaneous determination of Ti(II) and Fe(III) in presence of many other elements. The molar extinction coefficients were found to be 1.9 x 10/sup 5/ l mol/sup -1/ cm/sup -1/ and 1.11 x 10/sup 5/ l mol/sup -1/ cm/sup -1/ respectively for Ti(II) and Fe(III). The ...

1998-08-01

445

Robust parameter extraction for decision support using multimodal intensive care data  

UK PubMed Central (United Kingdom)

Digital information flow within the intensive care unit (ICU) continues to grow, with advances in technology and computational biology. Recent developments in the integration and archiving of these...Full Text Available

2009-01-28

446

Relationship between Hydroxy Fatty Acids and Prostaglandin E2 in Gingival Tissue  

UK PubMed Central (United Kingdom)

Bacterial hydroxy fatty acids and alpha-hydroxy fatty acids have been demonstrated in complex lipid extracts of subgingival plaque and gingival tissue. However, little is known about the relationship...Full Text Available

1998-12-01

447

Rapid Modulation of Spinach Leaf Nitrate Reductase by Photosynthesis 1  

UK PubMed Central (United Kingdom)

Assimilatory nitrate reductase activity (NRA) in crude spinach leaf (Spinacia oleracea) extracts undergoes rapid changes following fluctuations in photosynthesis brought about by changes...Full Text Available

1991-06-01

448

Rapid Correlation between the Leaves of Spinach and the Photocontrol of a Peroxidase Activity 1  

UK PubMed Central (United Kingdom)

The activity of a basic peroxidase extracted at high pH from spinach (Spinacia oleracea) leaves is modified by an irradiation with 2-minute red light or 2-minute far red light. This...Full Text Available

1982-02-01

449

PyEEG: An Open Source Python Module for EEG/MEG Feature Extraction  

UK PubMed Central (United Kingdom)

Computer-aided diagnosis of neural diseases from EEG signals (or other physiological signals that can be treated as time series, e.g., MEG) is an emerging field that has gained much attention in past...Full Text Available

2011-01-01

450

Purification and properties of adenylyl sulphate:ammonia adenylyltransferase from Chlorella catalysing the formation of adenosine 5?-phosphoramidate from adenosine 5?-phosphosulphate and ammonia  

UK PubMed Central (United Kingdom)

Extracts of Chlorella pyrenoidosa, Euglena gracilis var. bacillaris, spinach, barley, Dictyostelium discoideum and Escherichia coli...Full Text Available

1981-06-01

451

Protective effects of hydroalcoholic extract from rhizomes of Cynodon dactylon (L.) Pers. on compensated right heart failure in rats  

UK PubMed Central (United Kingdom)

BackgroundThe rhizomes of Cynodon dactylon are used for the treatment of heart failure in folk medicine. In the present study, we investigated the effects of hydroalcoholic...Full Text Available

452

Production of a fecal mutagen by Bacteroides spp.  

UK PubMed Central (United Kingdom)

Forty species of anaerobes were screened for the ability to produce an ether-extractable mutagen which is present in the feces of 15 to 20% of individuals in populations at high risk for colon cancer....Full Text Available

1982-09-01

453

Preliminary investigation into the pressing process of sweet pearl millet and sweet sorghum biomass for ethanol production  

Energy Technology Data Exchange (ETDEWEB)

Corn is the main source for biofuel production in North America. However, both sweet pearl millet and sweet sorghum crops represent an interesting alternative to corn for ethanol production because of their high biomass yield under a wide range of environmental conditions and high concentration of readily fermentable sugars. Coproducts such as pressing residues can be also be utilized so that nothing is lost in the process. However, in order to improve the extraction of juice for ethanol production, the pressing process of this biomass must be optimized. Preliminary experiments were therefore conducted to optimize the juice extraction from sweet pearl millet and sweet sorghum using 2 different presses, notably a screw press and a manually operated hydraulic press. Both types of biomass were either chopped finely or coarsely and were exposed to various pressures with the hydraulic press. The volume of juice extracted from ...

2010-07-01

454

Pregnant women's working conditions and their changes during pregnancy: a national study in France.  

UK PubMed Central (United Kingdom)

In a study of 2387 employed women who had worked for more than three months of their pregnancy the data were extracted from a survey carried out on a national sample of births in France in 1981. Manual,...Full Text Available

1987-04-01

455

Persistence of terbufos and its metabolites in soil and maize  

International Nuclear Information System (INIS)

Degradation of "1"4C terbufos was studied under greenhouse conditions. A mixture of "1"4C labelled compound (2.48 x 10"4 Bq of O-ethyl-1- "1"4C) und unlabelled compound (0.09 g of the granule formulation Counter 10 G) was applied to pots containing 750 g of sandy loam clay Ultisol soil with 4.9% organic matter and a cation exchange capacity of 7.6. Two treatments were established, one where maize (cultivar Cristiani) was grown and the other without plants. The soil and plants were extracted at 0, 4, 8, 16, 32 and 64 days and analyzed by a liquid scintillation counter, gas chromatography-flame photometric detector (GC-FPD) and autoradiography. The total "1"4C compounds extracted on day 64 were 31 #+-# 5.6% of the radioactivity applied in the treatments with plants and 46.1 #+-# 1.1% without plants. From the autoradiography results it can be concluded that all times the compounds identified by this technique were terbufos, terbufos sulphoxide and ...

1996-07-01

456

Partial Purification of Digitonin-Solubilized ?-Glucan Synthase from Red Beet Root 1  

UK PubMed Central (United Kingdom)

An enriched glucan synthase fraction was obtained from red beet root microsomes by sequential extraction with the detergents 3-[(3-cholamidopropyl)dimethylammonio]-1-propanesulfonate and digitonin....Full Text Available

1987-04-01

457

Partial Characterization of Cadmium-Binding Protein from Roots of Tomato 1  

UK PubMed Central (United Kingdom)

Cd-binding protein was extracted from tomato roots and purified on QAE-Sephadex A-25 and on Sephadex G-75 in 1 molar KCl buffer. The protein preparation was light brown and contained predominantly Cd...Full Text Available

1986-07-01

458

Paraquat-induced resinosis in Japanese pine. I. The effect of paraquat on Pinus densiflora and P. thunbergii  

Energy Technology Data Exchange (ETDEWEB)

Treatment of Japanese pines (P. densiflora and P. thunbergii) with paraquat induced a zone of lightwood. Determinations of turpentine and ether extractives contents in lightwoods showed high levels as compared with those in control woods. (Refs. 5).

1980-01-01

459

New crystallization of fatty acids from aqueous ethanol solution combined with liquid-liquid extraction  

Energy Technology Data Exchange (ETDEWEB)

A new separation process of saturated fatty acids (lauric acid-myristic acid) using crystallization from an aqueous ethanol solution has been examined. There were two vessels in this separation process: an extraction vessel and a crystallization vessel. The fatty acids in the aqueous phase were first extracted from their organic phase (melt) in the extraction vessel. The fatty acids in the aqueous phase were continuously introduced to the crystallization vessel, and then the fatty acids were crystallized there. The crystals of the fatty acids were collected continuously above the aqueous phase in the crystallization vessel. In this process, the yield and the purity of the crystals over time were measured, and it was found that the purity of lauric acid increased unsteadily up to 0.98 mole fraction of lauric acid with an increase in the yield of the low yield range. The mole fraction of ethanol in the aqueous phase could be ...

1999-06-01

460

Monitoring of the Water Levels in the Wetlands of Fourmile Branch Near the F- and H-Areas of SRS: FY97  

Energy Technology Data Exchange (ETDEWEB)

The purpose of the piezometer network is to establish baseline hydraulic head data for the water table aquifer at the F- and H-Area seeplines prior to startup of the groundwater extraction/injection remediation system.

1999-06-02

461

Molecular Evidence of Bartonella Infection in Domestic Dogs from Algeria, North Africa, by Polymerase Chain Reaction (PCR)  

UK PubMed Central (United Kingdom)

Bartonella species are being recognized as important bacterial human and canine pathogens, and are associated with multiple arthropod vectors. Bartonella DNA extracted...Full Text Available

2010-08-05

462

Lotus (Nelumbo nuficera) flower essential oil increased melanogenesis in normal human melanocytes  

UK PubMed Central (United Kingdom)

In this study, the essential oil from lotus flower extract, including petals and stamens, was assessed with regard to its effects on melanogenesis in human melanocytes. The lotus flower essential oil...Full Text Available

2009-07-31

463

Long-term results of extracapsular cataract extraction and posterior chamber intraocular lens insertion in Nepal.  

UK PubMed Central (United Kingdom)

We performed a prospective study evaluating the 2-year success rate of extracapsular cataract surgery and posterior chamber IOL insertion performed in 610 eyes by an experienced surgeon in the Nepal...Full Text Available

1991-01-01

464

Isolation, Purification, and Characterization of an Endogenous Root-promoting Factor Obtained from Basal Sections of Pear Hardwood Cuttings  

UK PubMed Central (United Kingdom)

Basal segments taken from Old Home and Bartlett pear hardwood cuttings collected at intervals during the rooting period in September were extracted with ethanol and fractionated by paper chromatography...Full Text Available

1967-04-01

465

Isolation of Assimilatory- and Dissimilatory-Type Sulfite Reductases from Desulfovibrio vulgaris  

UK PubMed Central (United Kingdom)

Bisulfite reductase (desulfoviridin) and an assimilatory sulfite reductase have been purified from extracts of Desulfovibrio vulgaris. The bisulfite reductase has absorption maxima...Full Text Available

1973-08-01

466

Isolation and structure of an untriakontapeptide with opiate activity from camel pituitary glands.  

UK PubMed Central (United Kingdom)

The isolation of an untriakontapeptide from camel pituitary extracts has been described. Its structure has been determined and shown to be identical to the sequence of carboxyl-terminal 31 amino acids...Full Text Available

1976-04-01

467

Isolation and identification of a cobamide coenzyme from the tapeworm Spirometra mansonoides.  

Science.gov (United States)

A light-sensitive vitamin B12 derivative has been extracted from the adult cestode, Spirometra mansonoides. This corrinoid was identified as the cobamide coenzyme, adenosylcobalamin, by its chromatographic, chemical, and spectral properties. PMID:1003284

1976-12-01

468

Interactions of Antibiotics and Methanolic Crude Extracts of Afzelia Africana (Smith.) Against Drug Resistance Bacterial Isolates  

UK PubMed Central (United Kingdom)

Infection due to multidrug resistance pathogens is difficult to manage due to bacterial virulence factors and because of a relatively limited choice of antimicrobial agents. Thus, it is imperative to...Full Text Available

469

Insulin increases glucose transfer across the blood-brain barrier in man.  

UK PubMed Central (United Kingdom)

The influence of insulin on unidirectional flux of glucose across the blood-brain barrier and on net uptake of glucose by the brain was investigated in seven fasting patients. The unidirectional extraction,...Full Text Available

1981-03-01

470

Information extraction for enhanced access to disease outbreak reports.  

Science.gov (United States)

Document search is generally based on individual terms in the document. However, for collections within limited domains it is possible to provide more powerful access tools. This paper describes a system designed for collections of reports of infectious disease outbreaks. The system, Proteus-BIO, automatically creates a table of outbreaks, with each table entry linked to the document describing that outbreak; this makes it possible to use database operations such as selection and sorting to find relevant documents. Proteus-BIO consists of a Web crawler which gathers relevant documents; an information extraction engine which converts the individual outbreak events to a tabular database; and a database browser which provides access to the events and, through them, to the documents. The information extraction engine uses sets of patterns and word classes to extract the information about each event. Preparing these patterns and ...

2002-08-01

473

IgE antibodies to D. pteronyssinus in atopic patients.  

UK PubMed Central (United Kingdom)

An aqueous house dust mite extract was separated by SDS-PAGE and transferred to nitrocellulose membranes by Western Blotting. Two major allergens, Der pI and Der pII associated with the mite faeces...Full Text Available

1988-06-01

474

How can information extraction ease formalizing treatment processes in clinical practice guidelines? A method and its evaluation?  

UK PubMed Central (United Kingdom)

SummaryObjective:Formalizing clinical practice guidelines (CPGs) for a subsequent computer-supported processing is a challenging, but burdensome and...Full Text Available

2007-02-01

475

Genetics of the mammalian phenylalanine hydroxylase system. Studies of human liver phenylalanine hydroxylase subunit structure and of mutations in phenylketonuria.  

UK PubMed Central (United Kingdom)

Phenylalanine hydroxylase was purified from crude extracts of human livers which show enzyme activity by usine two different methods: (a) affinity chromatography and (b) immunoprecipitation with an...Full Text Available

1979-08-01

476

Gene expression analysis of interferon ? in laser capture microdissected cervical epithelium  

UK PubMed Central (United Kingdom)

Optimal sample handling techniques for tissue preparation and storage, RNA extraction and quantification, and target gene detection are crucial for reliable gene expression analysis. Methods...Full Text Available

2008-10-01

477

Extraction of the weak angle gamma from B to charm decays  

CERN Document Server

We give a summary of the discussions in Working Group V of the CKM2010 workshop dealing with determinations of the angle gamma of the unitarity triangle of the Cabibbo-Kobayashi-Maskawa matrix from B-meson decays into charmed final states.

2011-01-01

478

Extracting medical information from narrative patient records: the case of medication-related information  

UK PubMed Central (United Kingdom)

ObjectiveWhile essential for patient care, information related to medication is often written as free text in clinical records and, therefore, difficult to use in computerized systems....Full Text Available

2010-09-01

479

Expulsive hemorrhage: its incidence in cataract surgery and a report of four bilateral cases.  

UK PubMed Central (United Kingdom)

Between 1978 and 1983, 13,890 cataract extractions were performed in Baltimore at JHH and the GBMC with 14 expulsive hemorrhages for an incidence of 0.10%. In the years 1963 through 1983, 180,690 cataract...Full Text Available

1985-01-01

480

Evaluation of Multiplexed Fluorescent Microsphere Immunoassay for Detection of Autoantibodies to Nuclear Antigens  

UK PubMed Central (United Kingdom)

Antibodies to extractable nuclear antigens (ENA) are found in a variety of collagen vascular diseases. Determining the individual specificities of these antibodies is extremely useful in establishing...Full Text Available

2004-11-01

481

Eosinophils Utilize Multiple Chemokine Receptors for Chemotaxis to the Parasitic Nematode Strongyloides stercoralis  

UK PubMed Central (United Kingdom)

Protective innate immunity to the nematode Strongyloides stercoralis requires eosinophils in the parasite killing process. Experiments were performed to determine if an extract of S....Full Text Available

2009-10-01

482

Ensemble quantum computing by NMR?spectroscopy  

UK PubMed Central (United Kingdom)

A quantum computer (QC) can operate in parallel on all its possible inputs at once, but the amount of information that can be extracted from the result is limited by the phenomenon of wave function...Full Text Available

1997-03-04

483

Effects of p-Synephrine alone and in Combination with Selected Bioflavonoids on Resting Metabolism, Blood Pressure, Heart Rate and Self-Reported Mood Changes  

UK PubMed Central (United Kingdom)

Bitter orange (Citrus aurantium) extract is widely used in dietary supplements for weight management and sports performance. Its primary protoalkaloid is p-synephrine....Full Text Available

484

Effects of extracts from Italian medicinal plants on planktonic growth, biofilm formation and adherence of methicillin-resistant Staphylococcus aureus  

UK PubMed Central (United Kingdom)

One-third of botanical remedies from southern Italy are used to treat skin and soft tissue infection (SSTI). Staphylococcus aureus, a common cause of SSTI, has generated increasing...Full Text Available

2008-08-13

485

Effects of Leupeptin on Proteinase and Germination of Castor Beans 1  

UK PubMed Central (United Kingdom)

Leupeptin, a tripeptide inhibitor of some proteinases, was shown previously to maintain the stability of several enzymes (isocitrate lyase, fumarase, and catalase) in crude extracts of castor bean endosperm....Full Text Available

1981-10-01

486

Effect of dietary green tea extract and aerosolized difluoromethylornithine during lung tumor progression in A/J strain mice  

UK PubMed Central (United Kingdom)

Chemoprevention strategies to prevent the development of lung cancer in at-risk individuals are a key component in disease management. In addition to being highly effective, an ideal chemopreventive...Full Text Available

2008-08-01

487

EDISA: extracting biclusters from multiple time-series of gene expression profiles  

UK PubMed Central (United Kingdom)

BackgroundCells dynamically adapt their gene expression patterns in response to various stimuli. This response is orchestrated into a number of gene expression modules consisting...Full Text Available

488

Detection of Streptococcus mutans Genomic DNA in Human DNA Samples Extracted from Saliva and Blood  

UK PubMed Central (United Kingdom)

Caries is a multifactorial disease, and studies aiming to unravel the factors modulating its etiology must consider all known predisposing factors. One major factor is bacterial colonization,...Full Text Available

2011-01-01

489

Design and analysis of a dust extraction system  

Energy Technology Data Exchange (ETDEWEB)

A dust extraction system removes the contaminated air at source by means of a hood. The extraction system for dust is essentially a ducted air system that prevents excessive employee exposure to dust in the working zone. The four major mechanisms that remove the contaminants in an extraction system are: - capture of contaminants by hoods - transport of contaminated air in duct network - separation of dust in the collector - exhaust of clean air through stack. The current methods of design are based on empirical relations, multi-variable tables, graphs and nomographs that have been derived from the principle of fluid mechanics and particle dynamics. However, the empirical formulae, tables and graphs are used in different geographical locations of the world having different environmental conditions and geo-characteristics of dust particles. Therefore, it is required to establish a rational design method that will be based on ...

2006-07-01

490

Cytoprotective Activity of Glycyrrhizae radix Extract Against Arsenite-induced Cytotoxicity  

UK PubMed Central (United Kingdom)

Licorice, Glycyrrhizae radix, is one of the herbal medicines in East Asia that has been commonly used for treating various diseases, including stomach disorders. This study investigated...Full Text Available

2008-06-01

491

Complement-fixing Activity of Fulvic Acid from Shilajit and Other Natural Sources  

UK PubMed Central (United Kingdom)

Shilajit has been used traditionally in folk medicine for treatment of a variety of disorders, including syndromes involving excessive complement activation. Extracts of Shilajit contain significant...Full Text Available

2009-03-01

492

Comorbidities of hidradenitis suppurativa (acne inversa)  

UK PubMed Central (United Kingdom)

Comorbidities of hidradenitis suppurativa (acne inversa) were reviewed by extracting original and review publications included in MEDLINE, EMBASE and COCHRANE libraries using the terms “hidradenitis,”...Full Text Available

2010-01-01

493

Chemical refining of coal (Report on ECSC contract 7220-EC/816)  

Energy Technology Data Exchange (ETDEWEB)

Three areas have been investigated: coal liquefaction with supercritical fluids, liquefaction by extraction with high boiling liquid solvents, and the production of resins from coal-derived hydrocarbons. The processes are described.

1983-01-01

494

Bump time-frequency toolbox: a toolbox for time-frequency oscillatory bursts extraction in electrophysiological signals  

UK PubMed Central (United Kingdom)

Backgroundoscillatory activity, which can be separated in background and oscillatory burst pattern activities, is supposed to be representative of local synchronies of neural assemblies....Full Text Available

495

Biomimetic metal-sorbing vesicles for continuous extraction of heavy metal ions from dilute solution  

Energy Technology Data Exchange (ETDEWEB)

Biomimetic vesicle media which can selectivity extract and concentrate heavy metals (e.g., Pb{sup 2+}) from dilute solutions of 5 ppm and less have been prepared. At a concentration of only 1% 2/v, these non-covalently assembled, unilamellar, surfactant vesicles provide approximately 1,000m{sup 2} of exposed membrane surface area per liter of suspension which gives rise to very rapid rates of metal ion extraction. To facilitate the selective transport of heavy metal ions through the ion impermeable vesicle wall, the vesicles are doped with lipophilic ionophores, both natural and synthetic. In addition, the metal chelating agent, nitrolotriacetate, is encapsulated in the aqueous vesicle core to provide the driving force for metal ion uptake and concentration. Concentration factors in excess of 1000 fold have been observed. Metal-sorbing surfactant vesicles measuring approximately 100 nm in diameter are stable and have been tested in a ...

1993-12-31

496

Barks of terminalia species - a new source of oxalic acid  

Energy Technology Data Exchange (ETDEWEB)

The digestion of water-extracted bark of Terminalia alata nepalensis, T. arjuna, and T. bellerica with 20% H/sub 2/SO/sub 4/ at 100 degrees resulted in the isolation of oxalic acid in 12-21% yield. The technique is not complicated and requires simple equipment.

1980-01-01

497

Ak-Chin Indian Community Biomass Feasiiblity Study  

Energy Technology Data Exchange (ETDEWEB)

Study of the conversion of chicken litter to biogas for the production of energy. There was an additional requirement that after extracting the energy from the chicken litter the nutrient value of the raw chicken litter had to be returned to the Ak-Chin Farms for use as fertilizer in a form and delivery method acceptable to the Farm.

2005-12-31

498

A procedure for batch separation of sup 14 C-hexose from sup 14 C-sucrose  

Energy Technology Data Exchange (ETDEWEB)

This presentation describes a method for separating {sup 14}C-hexose from {sup 14}C-sucrose in extracts of plant tissue. Portions of ethanol extracts are treated with activated charcoal in microcentrifuge tubes. Aliquots are removed, ethanol evaporated and replaced with reaction mixture that phosphorylates hexose (HEPPS, K{sub 2}HPO{sub 4}, Mg(C{sub 2}H{sub 3}O{sub 2}){sub 2}, ovalbumen, Na{sub 2}ATP, yeast hexokinase). After a time course, the hexokinase reaction is stopped (slowed considerably) to minimize effects of contamination enzyme activities. The stopping agent used is lyxose, a nonphosphorylable analogue of glucose. The strong anionic charge of phosphate introduced through the hexokinase action results in binding (> 95%) of hexose-phosphate to anion-exchange resin. Sucrose remains unbound (> 95%) in solution. This batch ion-exchange is performed in microcentrifuge tubes to allow many samples to be processed simultaneously. ...

1991-05-01

499

A new porous-layer activated-charcoal-coated fused silica fiber: application for determination of BTEX compounds in water samples using headspace solid-phase microextraction and capillary gas chromatography  

Energy Technology Data Exchange (ETDEWEB)

Extra-fine powdered activated charcoal has been used as stationary phase (coating layer) in solid-phase microextraction (SPME). The efficiency and reliability of the prepared device have been investigated for the extraction of some volatile organic compounds such as benzene, toluene, ethylbenzene and xylene isomers (BTEX) from the headspace of water samples. Monitoring of the extracted compounds and further quantitative analysis of the real samples have been performed by capillary GC-FID. Effects of several factors such as temperature, addition of salt, and stirring speed on extraction efficiency and exposure time have been studied. Under optimum conditions, extraction recoveries for these compounds from 50 mL water were >95%. The calibration graphs were linear in the range 5 to 10{sup 4} pg mL{sup -1} and the detection limit for each BTEX compound was 1.5-2 pg mL{sup -1}. The results obtained by use ...

1997-12-31

500

2005 NASA Executive Capability Roadmap Report  

Science.gov (United States)

ADVANCED MODELING, S IMULATION, AND ANALYSIS (ROADMAP 14). ...... Metal/Silicon Extraction from Regolith & manufacturing ..... addresses solar power, energy storage (in conjunction with solar power and as a prime source of ...