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Sample records for acoustic nmr

  1. Acoustics

    Goodman, Jerry R.; Grosveld, Ferdinand

    2007-01-01

    The acoustics environment in space operations is important to maintain at manageable levels so that the crewperson can remain safe, functional, effective, and reasonably comfortable. High acoustic levels can produce temporary or permanent hearing loss, or cause other physiological symptoms such as auditory pain, headaches, discomfort, strain in the vocal cords, or fatigue. Noise is defined as undesirable sound. Excessive noise may result in psychological effects such as irritability, inability to concentrate, decrease in productivity, annoyance, errors in judgment, and distraction. A noisy environment can also result in the inability to sleep, or sleep well. Elevated noise levels can affect the ability to communicate, understand what is being said, hear what is going on in the environment, degrade crew performance and operations, and create habitability concerns. Superfluous noise emissions can also create the inability to hear alarms or other important auditory cues such as an equipment malfunctioning. Recent space flight experience, evaluations of the requirements in crew habitable areas, and lessons learned (Goodman 2003; Allen and Goodman 2003; Pilkinton 2003; Grosveld et al. 2003) show the importance of maintaining an acceptable acoustics environment. This is best accomplished by having a high-quality set of limits/requirements early in the program, the "designing in" of acoustics in the development of hardware and systems, and by monitoring, testing and verifying the levels to ensure that they are acceptable.

  2. Acoustic detection of electron spin resonance

    Coufal, H.

    1981-07-01

    The ESR-signal of DPPH was recorded by detecting the modulation of the absorbed microwave power with a gas-coupled microphone. This photo-acoustic detection scheme is compared with conventional ESR-detection. Applications of the acoustical detection method to other modulation spectroscopic techniques, particularly NMR, are discussed.

  3. Compact NMR

    Bluemich, Bernhard; Haber-Pohlmeier, Sabina; Zia, Wasif [RWTH Aachen Univ. (Germany). Inst. fuer Technische und Makromolekulare Chemie (ITMC)

    2014-06-01

    Nuclear Magnetic Resonance (NMR) spectroscopy is the most popular method for chemists to analyze molecular structures, while Magnetic Resonance Imaging (MRI) is a non-invasive diagnostic tool for medical doctors that provides high-contrast images of biological tissue. In both applications, the sample (or patient) is positioned inside a large, superconducting magnet to magnetize the atomic nuclei. Interrogating radio-frequency pulses result in frequency spectra that provide the chemist with molecular information, the medical doctor with anatomic images, and materials scientist with NMR relaxation parameters. Recent advances in magnet technology have led to a variety of small permanent magnets to allow compact and low-cost instruments. The goal of this book is to provide an introduction to the practical use of compact NMR at a level nearly as basic as the operation of a smart phone.

  4. Compact NMR

    Nuclear Magnetic Resonance (NMR) spectroscopy is the most popular method for chemists to analyze molecular structures, while Magnetic Resonance Imaging (MRI) is a non-invasive diagnostic tool for medical doctors that provides high-contrast images of biological tissue. In both applications, the sample (or patient) is positioned inside a large, superconducting magnet to magnetize the atomic nuclei. Interrogating radio-frequency pulses result in frequency spectra that provide the chemist with molecular information, the medical doctor with anatomic images, and materials scientist with NMR relaxation parameters. Recent advances in magnet technology have led to a variety of small permanent magnets to allow compact and low-cost instruments. The goal of this book is to provide an introduction to the practical use of compact NMR at a level nearly as basic as the operation of a smart phone.

  5. Communication Acoustics

    Blauert, Jens

    Communication Acoustics deals with the fundamentals of those areas of acoustics which are related to modern communication technologies. Due to the advent of digital signal processing and recording in acoustics, these areas have enjoyed an enormous upswing during the last 4 decades. The book...... the book a source of valuable information for those who want to improve or refresh their knowledge in the field of communication acoustics - and to work their way deeper into it. Due to its interdisciplinary character Communication Acoustics is bound to attract readers from many different areas, such as......: acoustics, cognitive science, speech science, and communication technology....

  6. Acoustic Neuroma

    An acoustic neuroma is a benign tumor that develops on the nerve that connects the ear to the brain. The tumor ... press against the brain, becoming life-threatening. Acoustic neuroma can be difficult to diagnose, because the symptoms ...

  7. Acoustic Neuroma

    An acoustic neuroma is a benign tumor that develops on the nerve that connects the ear to the brain. ... can press against the brain, becoming life-threatening. Acoustic neuroma can be difficult to diagnose, because the ...

  8. NMR spectroscopy

    The book reviews the applications of NMR-spectroscopy in medicine and biology. The first chapter of about 40 pages summarizes the history of development and explains the chemical and physical fundamentals of this new and non-invasive method in an easily comprehensible manner. The other chapters summarize diagnostic results obtained with this method in organs and tissues, so that the reader will find a systematic overview of the available findings obtained in the various organ systems. It must be noted, however, that ongoing research work and new insight quite naturally will necessitate corrections to be done, as is the case here with some biochemical interpretations which would need adjustment to latest research results. NMR-spectroscopy is able to measure very fine energy differences on the molecular level, and thus offers insight into metabolic processes, with the advantage that there is no need of applying ionizing radiation in order to qualitatively or quantitatively analyse the metabolic processes in the various organ systems. (orig./DG) With 40 figs., 4 tabs

  9. Acoustic cloaking and transformation acoustics

    Chen Huanyang [School of Physical Science and Technology, Soochow University, Suzhou, Jiangsu 215006 (China); Chan, C T, E-mail: kenyon@ust.h, E-mail: phchan@ust.h [Department of Physics and the William Mong Institute of NanoScience and Technology, The Hong Kong University of Science and Technology, Clear Water Bay (Hong Kong)

    2010-03-24

    In this review, we give a brief introduction to the application of the new technique of transformation acoustics, which draws on a correspondence between coordinate transformation and material properties. The technique is formulated for both acoustic waves and linear liquid surface waves. Some interesting conceptual devices can be designed for manipulating acoustic waves. For example, we can design acoustic cloaks that make an object invisible to acoustic waves, and the cloak can either encompass or lie outside the object to be concealed. Transformation acoustics, as an analog of transformation optics, can go beyond invisibility cloaking. As an illustration for manipulating linear liquid surface waves, we show that a liquid wave rotator can be designed and fabricated to rotate the wave front. The acoustic transformation media require acoustic materials which are anisotropic and inhomogeneous. Such materials are difficult to find in nature. However, composite materials with embedded sub-wavelength resonators can in principle be made and such 'acoustic metamaterials' can exhibit nearly arbitrary values of effective density and modulus tensors to satisfy the demanding material requirements in transformation acoustics. We introduce resonant sonic materials and Helmholtz resonators as examples of acoustic metamaterials that exhibit resonant behaviour in effective density and effective modulus. (topical review)

  10. Acoustic cloaking and transformation acoustics

    In this review, we give a brief introduction to the application of the new technique of transformation acoustics, which draws on a correspondence between coordinate transformation and material properties. The technique is formulated for both acoustic waves and linear liquid surface waves. Some interesting conceptual devices can be designed for manipulating acoustic waves. For example, we can design acoustic cloaks that make an object invisible to acoustic waves, and the cloak can either encompass or lie outside the object to be concealed. Transformation acoustics, as an analog of transformation optics, can go beyond invisibility cloaking. As an illustration for manipulating linear liquid surface waves, we show that a liquid wave rotator can be designed and fabricated to rotate the wave front. The acoustic transformation media require acoustic materials which are anisotropic and inhomogeneous. Such materials are difficult to find in nature. However, composite materials with embedded sub-wavelength resonators can in principle be made and such 'acoustic metamaterials' can exhibit nearly arbitrary values of effective density and modulus tensors to satisfy the demanding material requirements in transformation acoustics. We introduce resonant sonic materials and Helmholtz resonators as examples of acoustic metamaterials that exhibit resonant behaviour in effective density and effective modulus. (topical review)

  11. Acoustical Imaging

    Litniewski, Jerzy; Kujawska, Tamara; 31st International Symposium on Acoustical Imaging

    2012-01-01

    The International Symposium on Acoustical Imaging is a unique forum for advanced research, covering new technologies, developments, methods and theories in all areas of acoustics. This interdisciplinary Symposium has been taking place continuously since 1968. In the course of the years the proceedings volumes in the Acoustical Imaging Series have become a reference for cutting-edge research in the field. In 2011 the 31st International Symposium on Acoustical Imaging was held in Warsaw, Poland, April 10-13. Offering both a broad perspective on the state-of-the-art as well as  in-depth research contributions by the specialists in the field, this Volume 31 in the Series contains an excellent collection of papers in six major categories: Biological and Medical Imaging Physics and Mathematics of Acoustical Imaging Acoustic Microscopy Transducers and Arrays Nondestructive Evaluation and Industrial Applications Underwater Imaging

  12. Radiation acoustics

    Lyamshev, Leonid M

    2004-01-01

    Radiation acoustics is a developing field lying at the intersection of acoustics, high-energy physics, nuclear physics, and condensed matter physics. Radiation Acoustics is among the first books to address this promising field of study, and the first to collect all of the most significant results achieved since research in this area began in earnest in the 1970s.The book begins by reviewing the data on elementary particles, absorption of penetrating radiation in a substance, and the mechanisms of acoustic radiation excitation. The next seven chapters present a theoretical treatment of thermoradiation sound generation in condensed media under the action of modulated penetrating radiation and radiation pulses. The author explores particular features of the acoustic fields of moving thermoradiation sound sources, sound excitation by single high-energy particles, and the efficiency and optimal conditions of thermoradiation sound generation. Experimental results follow the theoretical discussions, and these clearl...

  13. NMR studies of metabolism

    In this paper, the authors present applications of NMR to the study of different aspects of metabolism. The authors begin with a brief outline of localization methods that are commonly used to obtain in vivo NMR spectra. The authors then describe in more detail metabolic information recently obtained by NMR of perfused organs, intact animals, and humans. Previous reviews have already covered the applications of NMR to the study of metabolism in microorganisms, isolated or cultivated cells, and tumors. NMR spectroscopy of the brain, and human in vivo NMR spectroscopy have also been reviewed

  14. NMR analysis of biodiesel

    Biodiesel is usually analyzed by the various methods called for in standards such as ASTM D6751 and EN 14214. Nuclear magnetic resonance (NMR) is not one of these methods. However, NMR, with 1H-NMR commonly applied, can be useful in a variety of applications related to biodiesel. These include monit...

  15. Battlefield acoustics

    Damarla, Thyagaraju

    2015-01-01

    This book presents all aspects of situational awareness in a battlefield using acoustic signals. It starts by presenting the science behind understanding and interpretation of sound signals. The book then goes on to provide various signal processing techniques used in acoustics to find the direction of sound source, localize gunfire, track vehicles, and detect people. The necessary mathematical background and various classification and fusion techniques are presented. The book contains majority of the things one would need to process acoustic signals for all aspects of situational awareness in one location. The book also presents array theory, which is pivotal in finding the direction of arrival of acoustic signals. In addition, the book presents techniques to fuse the information from multiple homogeneous/heterogeneous sensors for better detection. MATLAB code is provided for majority of the real application, which is a valuable resource in not only understanding the theory but readers, can also use the code...

  16. Acoustical Imaging

    Akiyama, Iwaki

    2009-01-01

    The 29th International Symposium on Acoustical Imaging was held in Shonan Village, Kanagawa, Japan, April 15-18, 2007. This interdisciplinary Symposium has been taking place every two years since 1968 and forms a unique forum for advanced research, covering new technologies, developments, methods and theories in all areas of acoustics. In the course of the years the volumes in the Acoustical Imaging Series have developed and become well-known and appreciated reference works. Offering both a broad perspective on the state-of-the-art in the field as well as an in-depth look at its leading edge research, this Volume 29 in the Series contains again an excellent collection of seventy papers presented in nine major categories: Strain Imaging Biological and Medical Applications Acoustic Microscopy Non-Destructive Evaluation and Industrial Applications Components and Systems Geophysics and Underwater Imaging Physics and Mathematics Medical Image Analysis FDTD method and Other Numerical Simulations Audience Researcher...

  17. Acoustic telemetry

    National Oceanic and Atmospheric Administration, Department of Commerce — To determine movements of green turtles in the nearshore foraging areas, we deployed acoustic tags and determined their movements through active and passive...

  18. Acoustics Research

    National Oceanic and Atmospheric Administration, Department of Commerce — Fisheries acoustics data are collected from more than 200 sea-days each year aboard the FRV DELAWARE II and FRV ALBATROSS IV (decommissioned) and the FSV Henry B....

  19. Acoustic emission

    This paper is related to our activities on acoustic emission (A.E.). The work is made with different materials: metals and fibre reinforced plastics. At present, acoustic emission transducers are being developed for low and high temperature. A test to detect electrical discharges in electrical transformers was performed. Our experience in industrial tests to detect cracks or failures in tanks or tubes is also described. The use of A.E. for leak detection is considered. Works on pattern recognition of A.E. signals are also being performed. (Author)

  20. NMR at 900 MHz

    2002-01-01

    @@ An important factor in the development of solutionstate NMR has always been th e ability to produce stable and homogeneous magnetic fields. As higher and higher field strengths are reached the pressure is growing on manufacturers to produce NMR systems with greatly improved spectral resolution and signal to noise ratio. The introduction of the Varian 900 MHz INOVA system in August 2000 featuring Oxford Instruments 21.1 T magnet represents the latest pioneering development in NMR technology.

  1. Lectures on pulsed NMR

    These lectures discuss some recent developments in pulsed NMR, emphasizing fundamental principles with selected illustrative applications. Major topics covered include multiple-quantum spectroscopy, spin decoupling, the interaction of spins with a quantized field, adiabatic rapid passage, spin temperature and statistics of cross-polarization, coherent averaging, and zero field NMR. 32 refs., 56 figs

  2. Lectures on pulsed NMR

    These lectures discuss some recent developments in pulsed NMR, emphasizing fundamental principles with selected illustrative applications. Major topics covered include multiple-quantum spectroscopy, spin decoupling, the interaction of spins with a quantized field, adiabatic rapid passage, spin temperature and statistics of cross-polarization, coherent averaging, and zero field NMR. 55 figs

  3. Acoustic lenses

    Acoustic lenses focus ultrasound to produce pencil-like beams with reduced near fields. When fitted to conventional (flat-faced) transducers, such lenses greatly improve the ability to detect and size defects. This paper describes a program developed to design acoustic lenses for use in immersion or contact inspection, using normal or angle beam mode with flat or curved targets. Lens surfaces are circular in geometry to facilitate machining. For normal beam inspection of flat plate, spherical or cylindrical lenses are used. For angle beam or curved surface inspections, a compound lens is required to correct for the extra induced aberration. Such a lens is aspherical with one radius of curvature in the plane of incidence, and a different radius of curvature in the plane perpendicular to the incident plane. The resultant beam profile (i.e., location of the acoustic focus, beam diameter, 6 dB working range) depends on the degree of focusing and the transducer used. The operating frequency and bandwidth can be affected by the instrumentation used. Theoretical and measured beam profiles are in good agreement. Various applications, from zone focusing used for defect sizing in thick plate, to line focusing for pipe weld inspection, are discussed

  4. Functional studies using NMR

    This volume is based on a series of lectures delivered at a one-day teaching symposium on functional and metabolic aspects of NMR measurements held at the Middlesex Hospital Medical School on 1st September 1985 as a part of the European Nuclear Medicine Society Congress. Currently the major emphasis in medical NMR in vivo is on its potential to image and display abnormalities in conventional radiological images, providing increased contrast between normal and abnormal tissue, improved definition of vasculature, and possibly an increased potential for differential diagnosis. Although these areas are undeniably of major importance, it is probable that NMR will continue to complement conventional measurement methods. The major potential benefits to be derived from in vivo NMR measurements are likely to arise from its use as an instrument for functional and metabolic studies in both clinical research and in the everyday management of patients. It is to this area that this volume is directed

  5. Renal transplant NMR

    The preliminary results of NMR evaluation of renal transplants (Txs) are reported including correlation with nuclear medicine (NM) and ultrasound (US). Thirteen Txs (8 cadaver (Cd), 5 living related doner (LRD) in 13 patients (6M, 7F) ranging in age from 25-47 (x 35) were evaluated by NM (32), NMR (15) and US (5). Clinical diagnoses included: rejection (8), ATN (2), infarction (1), and normal (2). Of the 8 patients with rejection (5) Cd; 3 LRD) pathologic proof was obtained in 3. An experimental 0.12 T resistive magnet (GE) was used with a partial saturation technique with repetition time (TR) of 143 and 286 msec to provide T1 weighting. T2 weighted information was obtained with a spin echo technique with echo times (TE) of 20, 40, 60 and 80 msec. The NMR appearance of normal Txs consisted of a uniform signal intensity (Tx> pelvic musculature), well-defined internal architecture with good cortical medullary differentiation and normal appearing vessels. The NMR appearance of abnormal transplants consisted of a heterogeneous or overall decrease in signal intensity (kidney muscle) with poor cortical medullary differentiation with or without a halo of decreased signal intensity. Although NMR was able to differentiate normal from abnormal, it was unable to clearly discriminate between ATN and rejection. Advantages of NMR included the ability to demonstrate regional anatomy, vasculature, post operative fluid collections and hematomas, and associated avascular necrosis of the hips

  6. Acoustic hemostasis

    Crum, L.; Andrew, M.; Bailey, M.; Beach, K.; Brayman, A.; Curra, F.; Kaczkowski, P.; Kargl, S.; Martin, R.; Vaezy, S.

    2003-04-01

    Over the past several years, the Center for Industrial and Medical Ultrasound (CIMU) at the Applied Physics Laboratory in the University of Washington has undertaken a broad research program in the general area of High Intensity Focused Ultrasound (HIFU). Our principal emphasis has been on the use of HIFU to induce hemostasis; in particular, CIMU has sought to develop a small, lightweight, portable device that would use ultrasound for both imaging and therapy. Such a technology is needed because nearly 50% of combat casualty mortality results from exsanguinations, or uncontrolled bleeding. A similar percentage occurs for civilian death due to trauma. In this general review, a presentation of the general problem will be given, as well as our recent approaches to the development of an image-guided, transcutaneous, acoustic hemostasis device. [Work supported in part by the USAMRMC, ONR and the NIH.

  7. Acoustic telemetry.

    Drumheller, Douglas Schaeffer; Kuszmaul, Scott S.

    2003-08-01

    Broadcasting messages through the earth is a daunting task. Indeed, broadcasting a normal telephone conversion through the earth by wireless means is impossible with todays technology. Most of us don't care, but some do. Industries that drill into the earth need wireless communication to broadcast navigation parameters. This allows them to steer their drill bits. They also need information about the natural formation that they are drilling. Measurements of parameters such as pressure, temperature, and gamma radiation levels can tell them if they have found a valuable resource such as a geothermal reservoir or a stratum bearing natural gas. Wireless communication methods are available to the drilling industry. Information is broadcast via either pressure waves in the drilling fluid or electromagnetic waves in the earth and well tubing. Data transmission can only travel one way at rates around a few baud. Given that normal Internet telephone modems operate near 20,000 baud, these data rates are truly very slow. Moreover, communication is often interrupted or permanently blocked by drilling conditions or natural formation properties. Here we describe a tool that communicates with stress waves traveling through the steel drill pipe and production tubing in the well. It's based on an old idea called Acoustic Telemetry. But what we present here is more than an idea. This tool exists, it's drilled several wells, and it works. Currently, it's the first and only acoustic telemetry tool that can withstand the drilling environment. It broadcasts one way over a limited range at much faster rates than existing methods, but we also know how build a system that can communicate both up and down wells of indefinite length.

  8. Acoustic Neuroma Educational Video

    Full Text Available Educational Video Home What is an AN What is an Acoustic Neuroma? Identifying an AN Symptoms Acoustic Neuroma Keywords Educational Video ... for pre- and post-treatment acoustic neuroma patients. Home What is an AN What is an Acoustic ...

  9. Use of acoustic vortices in acoustic levitation

    Cutanda Henriquez, Vicente; Santillan, Arturo Orozco; Juhl, Peter Møller

    2009-01-01

    Acoustic fields are known to exert forces on the surfaces of objects. These forces are noticeable if the sound pressure is sufficiently high. Two phenomena where acoustic forces are relevant are: i) acoustic levitation, where strong standing waves can hold small objects at certain positions...... of acoustical vortices uses an efficient numerical implementation based on the superposition of two orthogonal sound fields with a delay of 90° between them. It is shown that acoustic levitation and the use of acoustic vortices can be combined to manipulate objects in an efficient and controlled manner without......, counterbalancing their weight, and ii) acoustic vortices, spinning sound fields that can impinge angular momentum and cause rotation of objects. In this contribution, both force-creating sound fields are studied by means of numerical simulations. The Boundary Element Method is employed to this end. The simulation...

  10. Acoustic dispersive prism

    Hussein Esfahlani; Sami Karkar; Herve Lissek; Mosig, Juan R.

    2016-01-01

    The optical dispersive prism is a well-studied element, which allows separating white light into its constituent spectral colors, and stands in nature as water droplets. In analogy to this definition, the acoustic dispersive prism should be an acoustic device with capability of splitting a broadband acoustic wave into its constituent Fourier components. However, due to the acoustical nature of materials as well as the design and fabrication difficulties, there is neither any natural acoustic ...

  11. NMR Aerosolomics: Novel NMR Method for Organic Aerosol Analysis

    Horník, Štěpán; Schwarz, Jaroslav; Sýkora, Jan

    - : -, 2015, s. 162. ISBN N. [Small Molecule NMR Conference - SMASH 2015. Baveno (IT), 20.09.2015-23.09.2015] Institutional support: RVO:67985858 Keywords : aerosol * analysis * NMR Subject RIV: CC - Organic Chemistry

  12. NMR imaging technique

    This invention provides a method that can be adapted to existing NMR tomographic scanners of producing spectra of any given point in the image of the specimen slice, the intensity distribution of a selected resonance within an area of the image of the specimen slice, or an entire NMR spectrum of the given area. The method comprises acquiring n projections of the specimen slice, where n is greater than 1. Each of the projections is then shifted by Δ f for the point (the frequency offset of the signal arising from the point, from the true chemical shift)

  13. NMR a substitute for CT

    The possibility that NMR (Nuclear Magnetic Resonance) can be a substitute for CT (Computerized Tomography), is described. NMR focus on the nuclei in the atoms of certain elements, for example hydrogen

  14. International symposium on NMR spectroscopy

    The publication consists of 32 papers and presentations from the field of NMR spectroscopy applications submitted to the International Symposium on NMR Spectroscopy held at Smolenice between 29 Sep and 3 Oct, 1980. (B.S.)

  15. Acoustic Neurinomas

    Mohammad Faraji Rad

    2011-01-01

    Full Text Available Acoustic neuromas (AN are schwann cell-derived tumors that commonly arise from the vestibular portion of the eighth cranial nerve also known as vestibular schwannoma(VS causes unilateral hearing loss, tinnitus, vertigo and unsteadiness. In many cases, the tumor size may remain unchanged for many years following diagnosis, which is typically made by MRI. In the majority of cases the tumor is small, leaving the clinician and patient with the options of either serial scanning or active treatment by gamma knife radiosurgery (GKR or microneurosurgery. Despite the vast number of published treatment reports, comparative studies are few. The predominant clinical endpoints of AN treatment include tumor control, facial nerve function and hearing preservation. Less focus has been put on symptom relief and health-related quality of life (QOL. It is uncertain if treating a small tumor leaves the patient with a better chance of obtaining relief from future hearing loss, vertigo or tinnitus than by observing it without treatment.   In this paper we review the literature for the natural course, the treatment alternatives and the results of AN. Finally, we present our experience with a management strategy applied for more than 30 years.

  16. Acoustic Spatiality

    Brandon LaBelle

    2012-06-01

    Full Text Available Experiences of listening can be appreciated as intensely relational, bringing us into contact with surrounding events, bodies and things. Given that sound propagates and expands outwardly, as a set of oscillations from a particular source, listening carries with it a sensual intensity, whereby auditory phenomena deliver intrusive and disruptive as well as soothing and assuring experiences. The physicality characteristic of sound suggests a deeply impressionistic, locational "knowledge structure" – that is, the ways in which listening affords processes of exchange, of being in the world, and from which we extend ourselves. Sound, as physical energy reflecting and absorbing into the materiality around us, and even one's self, provides a rich platform for understanding place and emplacement. Sound is always already a trace of location.Such features of auditory experience give suggestion for what I may call an acoustical paradigm – how sound sets in motion not only the material world but also the flows of the imagination, lending to forces of signification and social structure, and figuring us in relation to each other. The relationality of sound brings us into a steady web of interferences, each of which announces the promise or problematic of being somewhere.

  17. Springer Handbook of Acoustics

    Rossing, Thomas D

    2007-01-01

    Acoustics, the science of sound, has developed into a broad interdisciplinary field encompassing the academic disciplines of physics, engineering, psychology, speech, audiology, music, architecture, physiology, neuroscience, and others. The Springer Handbook of Acoustics is an unparalleled modern handbook reflecting this richly interdisciplinary nature edited by one of the acknowledged masters in the field, Thomas Rossing. Researchers and students benefit from the comprehensive contents spanning: animal acoustics including infrasound and ultrasound, environmental noise control, music and human speech and singing, physiological and psychological acoustics, architectural acoustics, physical and engineering acoustics, signal processing, medical acoustics, and ocean acoustics. This handbook reviews the most important areas of acoustics, with emphasis on current research. The authors of the various chapters are all experts in their fields. Each chapter is richly illustrated with figures and tables. The latest rese...

  18. Responsive acoustic surfaces

    Peters, Brady; Tamke, Martin; Nielsen, Stig Anton;

    2011-01-01

    Acoustic performance is defined by the parameter of reverberation time; however, this does not capture the acoustic experience in some types of open plan spaces. As many working and learning activities now take place in open plan spaces, it is important to be able to understand and design for the...... acoustic conditions of these spaces. This paper describes an experimental research project that studied the design processes necessary to design for sound. A responsive acoustic surface was designed, fabricated and tested. This acoustic surface was designed to create specific sonic effects. The design was...... simulated using custom integrated acoustic software and also using Odeon acoustic analysis software. The research demonstrates a method for designing space- and sound-defining surfaces, defines the concept of acoustic subspace, and suggests some new parameters for defining acoustic subspaces....

  19. NMR crystallography of polylactide

    Czernek, Jiří

    Prague : Institute of Macromolecular Chemistry AS CR, v. v. i, 2013. s. 60. ISBN 978-80-85009-77-4. [European Symposium on Polymer Spectroscopy /19./ - ESOPS19. Prague Meeting on Macromolecules /77./. 07.07.2013-11.07.2013, Prague] Institutional support: RVO:61389013 Keywords : NMR crystallography * polylactide Subject RIV: CD - Macromolecular Chemistry

  20. Soils, Pores, and NMR

    Pohlmeier, Andreas; Haber-Pohlmeier, Sabina; Haber, Agnes; Sucre, Oscar; Stingaciu, Laura; Stapf, Siegfried; Blümich, Bernhard

    2010-05-01

    Within Cluster A, Partial Project A1, the pore space exploration by means of Nuclear Magnetic Resonance (NMR) plays a central role. NMR is especially convenient since it probes directly the state and dynamics of the substance of interest: water. First, NMR is applied as relaxometry, where the degree of saturation but also the pore geometry controls the NMR signature of natural porous systems. Examples are presented where soil samples from the Selhausen, Merzenhausen (silt loams), and Kaldenkirchen (sandy loam) test sites are investigated by means of Fast Field Cycling Relaxometry at different degrees of saturation. From the change of the relaxation time distributions with decreasing water content and by comparison with conventional water retention curves we conclude that the fraction of immobile water is characterized by T1 samples (Haber-Pohlmeier et al. 2010). Third, relaxometric information forms the basis of understanding magnetic resonance imaging (MRI) results. The general difficulty of imaging in soils are the inherent fast T2 relaxation times due to i) the small pore sizes, ii) presence of paramagnetic ions in the solid matrix, and iii) diffusion in internal gradients. The last point is important, since echo times can not set shorter than about 1ms for imaging purposes. The way out is either the usage of low fields for imaging in soils or special ultra-short pulse sequences, which do not create echoes. In this presentation we will give examples on conventional imaging of macropore fluxes in soil cores (Haber-Pohlmeier et al. 2010), and the combination with relaxometric imaging, as well as the advantages and drawbacks of low-field and ultra-fast pulse imaging. Also first results on the imaging of soil columns measured by SIP in Project A3 are given. Haber-Pohlmeier, S., S. Stapf, et al. (2010). "Waterflow Monitored by Tracer Transport in Natural Porous Media Using MRI." Vadose Zone J.: submitted. Haber-Pohlmeier, S., S. Stapf, et al. (2010). "Relaxation in a

  1. Acoustic source for generating an acoustic beam

    Vu, Cung Khac; Sinha, Dipen N.; Pantea, Cristian

    2016-05-31

    An acoustic source for generating an acoustic beam includes a housing; a plurality of spaced apart piezo-electric layers disposed within the housing; and a non-linear medium filling between the plurality of layers. Each of the plurality of piezoelectric layers is configured to generate an acoustic wave. The non-linear medium and the plurality of piezo-electric material layers have a matching impedance so as to enhance a transmission of the acoustic wave generated by each of plurality of layers through the remaining plurality of layers.

  2. Atlantic Herring Acoustic Surveys

    National Oceanic and Atmospheric Administration, Department of Commerce — The NEFSC Advanced Sampling Technologies Research Group conducts annual fisheries acoustic surveys using state-of-the-art acoustic, midwater trawling, and...

  3. Acoustic Neuroma Educational Video

    Full Text Available ... Watch and Wait Radiation Microsurgery Acoustic Neuroma Decision Tree Questions for Your Physician Questions to Ask Yourself ... Watch and Wait Radiation Microsurgery Acoustic Neuroma Decision Tree Questions for Your Physician Questions to Ask Yourself ...

  4. Acoustic Neuroma Educational Video

    Full Text Available ... is ANA? Mission Statement Board of Directors ANA Staff Medical Advisory Board News ANA Annual Reports Acoustic ... is ANA? Mission Statement Board of Directors ANA Staff Medical Advisory Board News ANA Annual Reports Acoustic ...

  5. Acoustic Neuroma Educational Video

    Full Text Available ... ANA Annual Reports Acoustic Neuroma Legacy Society Programs & Services Join/Renew Ways to Give ANA Discussion Forum ... ANA Annual Reports Acoustic Neuroma Legacy Society Programs & Services Search ANAUSA.org Connect with us! Educational Video ...

  6. Acoustic Neuroma Educational Video

    Full Text Available ... Resources Patient Surveys Related Links Clinical Trials.gov Health Care Insurance Toolkit Additional Resources ANA Public Webinars © 2016 Acoustic Neuroma Association Acoustic Neuroma Association ® • ...

  7. Acoustic Neuroma Educational Video

    Full Text Available ... Options Watch and Wait Radiation Microsurgery Acoustic Neuroma Decision Tree Questions for Your Physician Questions to Ask ... Options Watch and Wait Radiation Microsurgery Acoustic Neuroma Decision Tree Questions for Your Physician Questions to Ask ...

  8. Acoustic Neuroma Educational Video

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  9. Cystic acoustic neuromas

    Chitkara, Naveen; Chanda, Rakesh; Yadav, S. P. S.; N.K. Sharma

    2002-01-01

    Predominantly cystic acoustic neuromas are rare and they usually present with clinical and radiological features different from their more common solid counterparts. Two cases of cystic acoustic neuromas are reported here.

  10. The automatic NMR gaussmeter

    The paper describes the automatic gaussmeter operating according to the principle of nuclear magnetic resonance. There have been discussed the operating principle, the block diagram and operating parameters of the meter. It can be applied to measurements of induction in electromagnets of wide-line radio-spectrometers EPR and NMR and in calibration stands of magnetic induction values. Frequency range of an autodyne oscillator from 0,6 up to 86 MHz for protons is corresponding to the field range from 0.016 up to 2T. Applicaton of other nuclei, such as 7Li and 2D is also foreseen. The induction measurement is carried over automatically, and the NMR signal and value of measured induction are displayed on a monitor screen. (author)

  11. NMR of unfolded proteins

    Amarnath Chtterjee; Ashutosh Kumar; Jeetender Chugh; Sudha Srivastava; Neel S Bhavesh; Ramakrishna V Hosur

    2005-01-01

    In the post-genomic era, as more and more genome sequences are becoming known and hectic efforts are underway to decode the information content in them, it is becoming increasingly evident that flexibility in proteins plays a crucial role in many of the biological functions. Many proteins have intrinsic disorder either wholly or in specific regions. It appears that this disorder may be important for regulatory functions of the proteins, on the one hand, and may help in directing the folding process to reach the compact native state, on the other. Nuclear magnetic resonance (NMR) has over the last two decades emerged as the sole, most powerful technique to help characterize these disordered protein systems. In this review, we first discuss the significance of disorder in proteins and then describe the recent developments in NMR methods for their characterization. A brief description of the results obtained on several disordered proteins is presented at the end.

  12. NMR, water and plants

    This thesis describes the application of a non-destructive pulsed proton NMR method mainly to measure water transport in the xylem vessels of plant stems and in some model systems. The results are equally well applicable to liquid flow in other biological objects than plants, e.g. flow of blood and other body fluids in human and animals. The method is based on a pulse sequence of equidistant π pulses in combination with a linear magnetic field gradient. (Auth.)

  13. ACOUSTICAL STANDARDS NEWS.

    Blaeser, Susan B; Struck, Christopher J

    2016-03-01

    American National Standards (ANSI Standards) developed by Accredited Standards Committees S1, S2, S3, S3/SC 1, and S12 in the areas of acoustics, mechanical vibration and shock, bioacoustics, animal bioacoustics, and noise, respectively, are published by the Acoustical Society of America (ASA). In addition to these standards, ASA publishes a catalog of Acoustical American National Standards. To receive a copy of the latest Standards catalog, please contact Susan B. Blaeser.Comments are welcomed on all material in Acoustical Standards News.This Acoustical Standards News section in JASA, as well as the National Catalog of Acoustical Standards and other information on the Standards Program of the Acoustical Society of America, are available via the ASA home page: http://acousticalsociety.org. PMID:27036268

  14. NMR molecular photography

    Khitrin, Anatoly K.; Ermakov, Vladimir L.; Fung, B M

    2002-01-01

    A procedure is described for storing a 2D pattern consisting of 32x32 = 1024 bits in a spin state of a molecular system and then retrieving the stored information as a stack of NMR spectra. The system used is a nematic liquid crystal, the protons of which act as spin clusters with strong intramolecular interactions. The technique used is a programmable multi-frequency irradiation with low amplitude. When it is applied to the liquid crystal, a large number of coherent long-lived 1H response si...

  15. A Methodology to Integrate Magnetic Resonance and Acoustic Measurements for Reservoir Characterization

    Parra, Jorge O.; Hackert, Chris L.; Collier, Hughbert A.; Bennett, Michael

    2002-01-29

    The objective of this project was to develop an advanced imaging method, including pore scale imaging, to integrate NMR techniques and acoustic measurements to improve predictability of the pay zone in hydrocarbon reservoirs. This is accomplished by extracting the fluid property parameters using NMR laboratory measurements and the elastic parameters of the rock matrix from acoustic measurements to create poroelastic models of different parts of the reservoir. Laboratory measurement techniques and core imaging are being linked with a balanced petrographical analysis of the core and theoretical model.

  16. AST Launch Vehicle Acoustics

    Houston, Janice; Counter, D.; Giacomoni, D.

    2015-01-01

    The liftoff phase induces acoustic loading over a broad frequency range for a launch vehicle. These external acoustic environments are then used in the prediction of internal vibration responses of the vehicle and components which result in the qualification levels. Thus, predicting these liftoff acoustic (LOA) environments is critical to the design requirements of any launch vehicle. If there is a significant amount of uncertainty in the predictions or if acoustic mitigation options must be implemented, a subscale acoustic test is a feasible pre-launch test option to verify the LOA environments. The NASA Space Launch System (SLS) program initiated the Scale Model Acoustic Test (SMAT) to verify the predicted SLS LOA environments and to determine the acoustic reduction with an above deck water sound suppression system. The SMAT was conducted at Marshall Space Flight Center and the test article included a 5% scale SLS vehicle model, tower and Mobile Launcher. Acoustic and pressure data were measured by approximately 250 instruments. The SMAT liftoff acoustic results are presented, findings are discussed and a comparison is shown to the Ares I Scale Model Acoustic Test (ASMAT) results.

  17. Acoustic streaming in microchannels

    Tribler, Peter Muller

    , and experimental results for the streaming-induced drag force dominated motion of particles suspended in a water-filled microchannel supporting a transverse half-wavelength resonance. The experimental and theoretical results agree within a mean relative dierence of approximately 20%, a low deviation given state......This thesis presents studies of boundary-driven acoustic streaming in microfluidic channels, which is a steady flow of the fluid initiated by the interactions of an oscillating acoustic standing wave and the rigid walls of the microchannel. The studies present analysis of the acoustic resonance......, the acoustic streaming flow, and the forces on suspended microparticles. The work is motivated by the application of particle focusing by acoustic radiation forces in medical, environmental and food sciences. Here acoustic streaming is most often unwanted, because it limits the focusability of particles...

  18. Vibro-acoustics

    Nilsson, Anders

    2015-01-01

    This three-volume book gives a thorough and comprehensive presentation of vibration and acoustic theories. Different from traditional textbooks which typically deal with some aspects of either acoustic or vibration problems, it is unique of this book to combine those two correlated subjects together. Moreover, it provides fundamental analysis and mathematical descriptions for several crucial phenomena of Vibro-Acoustics which are quite useful in noise reduction, including how structures are excited, energy flows from an excitation point to a sound radiating surface, and finally how a structure radiates noise to a surrounding fluid. Many measurement results included in the text make the reading interesting and informative. Problems/questions are listed at the end of each chapter and the solutions are provided. This will help the readers to understand the topics of Vibro-Acoustics more deeply. The book should be of interest to anyone interested in sound and vibration, vehicle acoustics, ship acoustics and inter...

  19. Springer handbook of acoustics

    2014-01-01

    Acoustics, the science of sound, has developed into a broad interdisciplinary field encompassing the academic disciplines of physics, engineering, psychology, speech, audiology, music, architecture, physiology, neuroscience, and electronics. The Springer Handbook of Acoustics is also in his 2nd edition an unparalleled modern handbook reflecting this richly interdisciplinary nature edited by one of the acknowledged masters in the field, Thomas Rossing. Researchers and students benefit from the comprehensive contents. This new edition of the Handbook features over 11 revised and expanded chapters, new illustrations, and 2 new chapters covering microphone arrays  and acoustic emission.  Updated chapters contain the latest research and applications in, e.g. sound propagation in the atmosphere, nonlinear acoustics in fluids, building and concert hall acoustics, signal processing, psychoacoustics, computer music, animal bioacousics, sound intensity, modal acoustics as well as new chapters on microphone arrays an...

  20. NMR spectrometers as "magnetic tongues"

    Malmendal, Anders; Amoresano, Claudia; Trotta, Roberta;

    2011-01-01

    the analyzed samples based on their chemical composition. We were able to correlate the NMR metabolomic fingerprints recorded for canned tomato samples to the sensory descriptors bitterness, sweetness, sourness, saltiness, tomato and metal taste, redness, and density, suggesting that NMR might be a very useful...

  1. NMR in pulsed magnetic field

    Abou-Hamad, Edy

    2011-09-01

    Nuclear magnetic resonance (NMR) experiments in pulsed magnetic fields up to 30.4 T focused on 1H and 93Nb nuclei are reported. Here we discuss the advantage and limitation of pulsed field NMR and why this technique is able to become a promising research tool. © 2011 Elsevier Inc. All Rights Reserved.

  2. Localized Acoustic Surface Modes

    Farhat, Mohamed

    2015-08-04

    We introduce the concept of localized acoustic surface modes (ASMs). We demonstrate that they are induced on a two-dimensional cylindrical rigid surface with subwavelength corrugations under excitation by an incident acoustic plane wave. Our results show that the corrugated rigid surface is acoustically equivalent to a cylindrical scatterer with uniform mass density that can be represented using a Drude-like model. This, indeed, suggests that plasmonic-like acoustic materials can be engineered with potential applications in various areas including sensing, imaging, and cloaking.

  3. Shallow Water Acoustic Laboratory

    Federal Laboratory Consortium — FUNCTION: Supports experimental research where high-frequency acoustic scattering and surface vibration measurements of fluid-loaded and non-fluid-loaded structures...

  4. Handbook of Engineering Acoustics

    Möser, Michael

    2013-01-01

    This book examines the physical background of engineering acoustics, focusing on empirically obtained engineering experience as well as on measurement techniques and engineering methods for prognostics. Its goal is not only to describe the state of art of engineering acoustics but also to give practical help to engineers in order to solve acoustic problems. It deals with the origin, the transmission and the methods of the abating different kinds of air-borne and structure-borne sounds caused by various mechanisms – from traffic to machinery and flow-induced sound. In addition the modern aspects of room and building acoustics, as well as psychoacoustics and active noise control, are covered.

  5. Acoustic dispersive prism

    Esfahlani, Hussein; Karkar, Sami; Lissek, Herve; Mosig, Juan R.

    2016-01-01

    The optical dispersive prism is a well-studied element, which allows separating white light into its constituent spectral colors, and stands in nature as water droplets. In analogy to this definition, the acoustic dispersive prism should be an acoustic device with capability of splitting a broadband acoustic wave into its constituent Fourier components. However, due to the acoustical nature of materials as well as the design and fabrication difficulties, there is neither any natural acoustic counterpart of the optical prism, nor any artificial design reported so far exhibiting an equivalent acoustic behaviour. Here, based on exotic properties of the acoustic transmission-line metamaterials and exploiting unique physical behaviour of acoustic leaky-wave radiation, we report the first acoustic dispersive prism, effective within the audible frequency range 800 Hz-1300 Hz. The dispersive nature, and consequently the frequency-dependent refractive index of the metamaterial are exploited to split the sound waves towards different and frequency-dependent directions. Meanwhile, the leaky-wave nature of the structure facilitates the sound wave radiation into the ambient medium.

  6. Structural Biology: Practical NMR Applications

    Teng, Quincy

    2005-01-01

    This textbook begins with an overview of NMR development and applications in biological systems. It describes recent developments in instrument hardware and methodology. Chapters highlight the scope and limitation of NMR methods. While detailed math and quantum mechanics dealing with NMR theory have been addressed in several well-known NMR volumes, chapter two of this volume illustrates the fundamental principles and concepts of NMR spectroscopy in a more descriptive manner. Topics such as instrument setup, data acquisition, and data processing using a variety of offline software are discussed. Chapters further discuss several routine stategies for preparing samples, especially for macromolecules and complexes. The target market for such a volume includes researchers in the field of biochemistry, chemistry, structural biology and biophysics.

  7. Fundamentals of Protein NMR Spectroscopy

    Rule, Gordon S

    2006-01-01

    NMR spectroscopy has proven to be a powerful technique to study the structure and dynamics of biological macromolecules. Fundamentals of Protein NMR Spectroscopy is a comprehensive textbook that guides the reader from a basic understanding of the phenomenological properties of magnetic resonance to the application and interpretation of modern multi-dimensional NMR experiments on 15N/13C-labeled proteins. Beginning with elementary quantum mechanics, a set of practical rules is presented and used to describe many commonly employed multi-dimensional, multi-nuclear NMR pulse sequences. A modular analysis of NMR pulse sequence building blocks also provides a basis for understanding and developing novel pulse programs. This text not only covers topics from chemical shift assignment to protein structure refinement, as well as the analysis of protein dynamics and chemical kinetics, but also provides a practical guide to many aspects of modern spectrometer hardware, sample preparation, experimental set-up, and data pr...

  8. Constants of NMR spectra

    The NMR (nuclear magnetic resonance) spectroscopy is a method for studying matter. It has been developed in a lot of fields of physics, physical chemistry, chemistry and biology. It concerns both the solid state and the liquid state. The study in solution of synthesis organic molecules or of organic molecules of natural origin and of biological molecules is particularly stressed on but it is also possible to study inorganic molecules. The originality of this method is to give both data on each atoms of the studied structure, on the atoms sequence in this structure, on the conformation and on the related configurations. It allows to reveal the interactions between separate molecules too. It is also a precious tool for the analysis of molecular movements. The development of this method for the study of condensed phases is particularly studied nowadays and the data obtained are for a lot of fields as acute as those obtained at the liquid state. (O.M.)

  9. What Is an Acoustic Neuroma

    ... org Connect with us! What is an Acoustic Neuroma? Each heading slides to reveal information. Important Points ... Neuroma Important Points To Know About an Acoustic Neuroma An acoustic neuroma, also called a vestibular schwannoma, ...

  10. Two dimensional solid state NMR

    This thesis illustrates, by discussing some existing and newly developed 2D solid state experiments, that two-dimensional NMR of solids is a useful and important extension of NMR techniques. Chapter 1 gives an overview of spin interactions and averaging techniques important in solid state NMR. As 2D NMR is already an established technique in solutions, only the basics of two dimensional NMR are presented in chapter 2, with an emphasis on the aspects important for solid spectra. The following chapters discuss the theoretical background and applications of specific 2D solid state experiments. An application of 2D-J resolved NMR, analogous to J-resolved spectroscopy in solutions, to natural rubber is given in chapter 3. In chapter 4 the anisotropic chemical shift is mapped out against the heteronuclear dipolar interaction to obtain information about the orientation of the shielding tensor in poly-(oxymethylene). Chapter 5 concentrates on the study of super-slow molecular motions in polymers using a variant of the 2D exchange experiment developed by us. Finally chapter 6 discusses a new experiment, 2D nutation NMR, which makes it possible to study the quadrupole interaction of half-integer spins. 230 refs.; 48 figs.; 8 tabs

  11. Acoustic emission source modeling

    Hora, Petr; Červená, Olga

    2010-01-01

    Roč. 4, č. 1 (2010), s. 25-36. ISSN 1802-680X R&D Projects: GA ČR GA101/09/1630 Institutional research plan: CEZ:AV0Z20760514 Keywords : acoustic emission source * wave propagation * FEM Subject RIV: BI - Acoustics

  12. Acoustic Neuroma Educational Video

    Full Text Available ... Microsurgery Acoustic Neuroma Decision Tree Questions for Your Physician Questions to Ask Yourself Post-treatment Post-treatment ... Microsurgery Acoustic Neuroma Decision Tree Questions for Your Physician Questions to Ask Yourself Post-treatment Post-treatment ...

  13. Ocean acoustic hurricane classification.

    Wilson, Joshua D; Makris, Nicholas C

    2006-01-01

    Theoretical and empirical evidence are combined to show that underwater acoustic sensing techniques may be valuable for measuring the wind speed and determining the destructive power of a hurricane. This is done by first developing a model for the acoustic intensity and mutual intensity in an ocean waveguide due to a hurricane and then determining the relationship between local wind speed and underwater acoustic intensity. From this it is shown that it should be feasible to accurately measure the local wind speed and classify the destructive power of a hurricane if its eye wall passes directly over a single underwater acoustic sensor. The potential advantages and disadvantages of the proposed acoustic method are weighed against those of currently employed techniques. PMID:16454274

  14. Cochlear bionic acoustic metamaterials

    Ma, Fuyin; Wu, Jiu Hui; Huang, Meng; Fu, Gang; Bai, Changan

    2014-11-01

    A design of bionic acoustic metamaterial and acoustic functional devices was proposed by employing the mammalian cochlear as a prototype. First, combined with the experimental data in previous literatures, it is pointed out that the cochlear hair cells and stereocilia cluster are a kind of natural biological acoustic metamaterials with the negative stiffness characteristics. Then, to design the acoustic functional devices conveniently in engineering application, a simplified parametric helical structure was proposed to replace actual irregular cochlea for bionic design, and based on the computational results of such a bionic parametric helical structure, it is suggested that the overall cochlear is a local resonant system with the negative dynamic effective mass characteristics. There are many potential applications in the bandboard energy recovery device, cochlear implant, and acoustic black hole.

  15. Computational Ocean Acoustics

    Jensen, Finn B; Porter, Michael B; Schmidt, Henrik

    2011-01-01

    Since the mid-1970s, the computer has played an increasingly pivotal role in the field of ocean acoustics. Faster and less expensive than actual ocean experiments, and capable of accommodating the full complexity of the acoustic problem, numerical models are now standard research tools in ocean laboratories. The progress made in computational ocean acoustics over the last thirty years is summed up in this authoritative and innovatively illustrated new text. Written by some of the field's pioneers, all Fellows of the Acoustical Society of America, Computational Ocean Acoustics presents the latest numerical techniques for solving the wave equation in heterogeneous fluid–solid media. The authors discuss various computational schemes in detail, emphasizing the importance of theoretical foundations that lead directly to numerical implementations for real ocean environments. To further clarify the presentation, the fundamental propagation features of the techniques are illustrated in color. Computational Ocean A...

  16. Acoustic Signals and Systems

    The Handbook of Signal Processing in Acoustics will compile the techniques and applications of signal processing as they are used in the many varied areas of Acoustics. The Handbook will emphasize the interdisciplinary nature of signal processing in acoustics. Each Section of the Handbook will...... present topics on signal processing which are important in a specific area of acoustics. These will be of interest to specialists in these areas because they will be presented from their technical perspective, rather than a generic engineering approach to signal processing. Non-specialists, or specialists...... from different areas, will find the self-contained chapters accessible and will be interested in the similarities and differences between the approaches and techniques used in different areas of acoustics....

  17. NMR for chemists and biologists

    Carbajo, Rodrigo J

    2013-01-01

    This book intends to be an easy and concise introduction to the field of nuclear magnetic resonance or NMR, which has revolutionized life sciences in the last twenty years. A significant part of the progress observed in scientific areas like Chemistry, Biology or Medicine can be ascribed to the development experienced by NMR in recent times. Many of the books currently available on NMR deal with the theoretical basis and some of its main applications, but they generally demand a strong background in Physics and Mathematics for a full understanding. This book is aimed to a wide scientific audie

  18. Annual reports on NMR spectroscopy

    Webb, Graham A; McCarthy, M J

    1995-01-01

    Over recent years, no other technique has grown to such importance as that of NMR spectroscopy. It is used in all branches of science where precise structural determination is required and where the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a means for the specialist and non-specialist alike to become familiar with new applications of the technique in all branches of chemistry, including biochemistry, and pharmaceutics. This volume focuses on theoretical aspects of NMR nuclear shielding and on applications of

  19. Integrative NMR for biomolecular research.

    Lee, Woonghee; Cornilescu, Gabriel; Dashti, Hesam; Eghbalnia, Hamid R; Tonelli, Marco; Westler, William M; Butcher, Samuel E; Henzler-Wildman, Katherine A; Markley, John L

    2016-04-01

    NMR spectroscopy is a powerful technique for determining structural and functional features of biomolecules in physiological solution as well as for observing their intermolecular interactions in real-time. However, complex steps associated with its practice have made the approach daunting for non-specialists. We introduce an NMR platform that makes biomolecular NMR spectroscopy much more accessible by integrating tools, databases, web services, and video tutorials that can be launched by simple installation of NMRFAM software packages or using a cross-platform virtual machine that can be run on any standard laptop or desktop computer. The software package can be downloaded freely from the NMRFAM software download page ( http://pine.nmrfam.wisc.edu/download_packages.html ), and detailed instructions are available from the Integrative NMR Video Tutorial page ( http://pine.nmrfam.wisc.edu/integrative.html ). PMID:27023095

  20. Flat acoustic lens by acoustic grating with curled slits

    We design a flat sub-wavelength lens that can focus acoustic wave. We analytically study the transmission through an acoustic grating with curled slits, which can serve as a material with tunable impedance and refractive index for acoustic waves. The effective parameters rely on the geometry of the slits and are independent of frequency. A flat acoustic focusing lens by such acoustic grating with gradient effective refractive index is designed. The focusing effect is clearly observed in simulations and well predicted by the theory. We demonstrate that despite the large impedance mismatch between the acoustic lens and the matrix, the intensity at the focal point is still high due to Fabry–Perot resonance. - Highlights: • Expression of transmission coefficient of an acoustic grating with curled slits. • Non-dispersive and tunable effective medium parameters for the acoustic grating. • A flat acoustic focusing lens with gradient index by using the acoustic grating

  1. Optical pumping and xenon NMR

    Raftery, M.D.

    1991-11-01

    Nuclear Magnetic Resonance (NMR) spectroscopy of xenon has become an important tool for investigating a wide variety of materials, especially those with high surface area. The sensitivity of its chemical shift to environment, and its chemical inertness and adsorption properties make xenon a particularly useful NMR probe. This work discusses the application of optical pumping to enhance the sensitivity of xenon NMR experiments, thereby allowing them to be used in the study of systems with lower surface area. A novel method of optically-pumping [sup 129]Xe in low magnetic field below an NMR spectrometer and subsequent transfer of the gas to high magnetic field is described. NMR studies of the highly polarized gas adsorbed onto powdered samples with low to moderate surface areas are now possible. For instance, NMR studies of optically-pumped xenon adsorbed onto polyacrylic acid show that xenon has a large interaction with the surface. By modeling the low temperature data in terms of a sticking probability and the gas phase xenon-xenon interaction, the diffusion coefficient for xenon at the surface of the polymer is determined. The sensitivity enhancement afforded by optical pumping also allows the NMR observation of xenon thin films frozen onto the inner surfaces of different sample cells. The geometry of the thin films results in interesting line shapes that are due to the bulk magnetic susceptibility of xenon. Experiments are also described that combine optical pumping with optical detection for high sensitivity in low magnetic field to observe the quadrupoler evolution of 131 Xe spins at the surface of the pumping cells. In cells with macroscopic asymmetry, a residual quadrupolar interaction causes a splitting in the [sup 131]Xe NMR frequencies in bare Pyrex glass cells and cells with added hydrogen.

  2. Optical pumping and xenon NMR

    Raftery, M.D.

    1991-11-01

    Nuclear Magnetic Resonance (NMR) spectroscopy of xenon has become an important tool for investigating a wide variety of materials, especially those with high surface area. The sensitivity of its chemical shift to environment, and its chemical inertness and adsorption properties make xenon a particularly useful NMR probe. This work discusses the application of optical pumping to enhance the sensitivity of xenon NMR experiments, thereby allowing them to be used in the study of systems with lower surface area. A novel method of optically-pumping {sup 129}Xe in low magnetic field below an NMR spectrometer and subsequent transfer of the gas to high magnetic field is described. NMR studies of the highly polarized gas adsorbed onto powdered samples with low to moderate surface areas are now possible. For instance, NMR studies of optically-pumped xenon adsorbed onto polyacrylic acid show that xenon has a large interaction with the surface. By modeling the low temperature data in terms of a sticking probability and the gas phase xenon-xenon interaction, the diffusion coefficient for xenon at the surface of the polymer is determined. The sensitivity enhancement afforded by optical pumping also allows the NMR observation of xenon thin films frozen onto the inner surfaces of different sample cells. The geometry of the thin films results in interesting line shapes that are due to the bulk magnetic susceptibility of xenon. Experiments are also described that combine optical pumping with optical detection for high sensitivity in low magnetic field to observe the quadrupoler evolution of 131 Xe spins at the surface of the pumping cells. In cells with macroscopic asymmetry, a residual quadrupolar interaction causes a splitting in the {sup 131}Xe NMR frequencies in bare Pyrex glass cells and cells with added hydrogen.

  3. Optical pumping and xenon NMR

    Nuclear Magnetic Resonance (NMR) spectroscopy of xenon has become an important tool for investigating a wide variety of materials, especially those with high surface area. The sensitivity of its chemical shift to environment, and its chemical inertness and adsorption properties make xenon a particularly useful NMR probe. This work discusses the application of optical pumping to enhance the sensitivity of xenon NMR experiments, thereby allowing them to be used in the study of systems with lower surface area. A novel method of optically-pumping 129Xe in low magnetic field below an NMR spectrometer and subsequent transfer of the gas to high magnetic field is described. NMR studies of the highly polarized gas adsorbed onto powdered samples with low to moderate surface areas are now possible. For instance, NMR studies of optically-pumped xenon adsorbed onto polyacrylic acid show that xenon has a large interaction with the surface. By modeling the low temperature data in terms of a sticking probability and the gas phase xenon-xenon interaction, the diffusion coefficient for xenon at the surface of the polymer is determined. The sensitivity enhancement afforded by optical pumping also allows the NMR observation of xenon thin films frozen onto the inner surfaces of different sample cells. The geometry of the thin films results in interesting line shapes that are due to the bulk magnetic susceptibility of xenon. Experiments are also described that combine optical pumping with optical detection for high sensitivity in low magnetic field to observe the quadrupoler evolution of 131 Xe spins at the surface of the pumping cells. In cells with macroscopic asymmetry, a residual quadrupolar interaction causes a splitting in the 131Xe NMR frequencies in bare Pyrex glass cells and cells with added hydrogen

  4. From Architectural Acoustics to Acoustical Architecture Using Computer Simulation

    Schmidt, Anne Marie Due; KIRKEGAARD, Poul Henning

    2005-01-01

    Architectural acoustics design has in the past been based on simple design rules. However, with a growing complexity in architectural acoustics and the emergence of room acoustic simulation programmes with considerable potential, it is now possible to subjectively analyse and evaluate acoustic properties prior to the actual construction of a building. With the right tools applied, acoustic design can become an integral part of the architectural design process. The aim of this paper is to inve...

  5. Underwater Applications of Acoustical Holography

    P. C. Mehta

    1984-01-01

    Full Text Available The paper describes the basic technique of acoustical holography. Requirements for recording the acoustical hologram are discussed with its ability for underwater imaging in view. Some practical systems for short-range and medium-range imaging are described. The advantages of acoustical holography over optical imaging, acoustical imaging and sonars are outlined.

  6. Predicting Acoustics in Class Rooms

    Christensen, Claus Lynge; Rindel, Jens Holger

    2005-01-01

    Typical class rooms have fairly simple geometries, even so room acoustics in this type of room is difficult to predict using today's room acoustic computer modeling software. The reasons why acoustics of class rooms are harder to predict than acoustics of complicated concert halls might be...

  7. Tunable acoustic metamaterials

    Babaee, Sahab; Viard, Nicolas; Fang, Nicholas; Bertoldi, Katia

    2015-03-01

    We report a new class of active and switchable acoustic metamaterials composed of three-dimensional stretchable chiral helices arranged on a two-dimensional square lattice. We investigate the propagation of sounds through the proposed structure both numerically and experimentally and find that the deformation of the helices can be exploited as a novel and effective approach to control the propagation of acoustic waves. The proposed concept expands the ability of existing acoustic metamaterials since we demonstrate that the deformation can be exploited to turn on or off the band gap, opening avenues for the design of adaptive noise-cancelling devices.

  8. Phononic crystals and acoustic metamaterials

    Ming-Hui Lu; Liang Feng; Yan-Feng Chen

    2009-01-01

    Phononic crystals have been proposed about two decades ago and some important characteristics such as acoustic band structure and negative refraction have stimulated fundamental and practical studies in acoustic materials and devices since then. To carefully engineer a phononic crystal in an acoustic “atom” scale, acoustic metamaterials with their inherent deep subwavelength nature have triggered more exciting investigations on negative bulk modulus and/or negative mass density. Acoustic surf...

  9. Acoustic integrated extinction

    Norris, Andrew N

    2015-01-01

    The integrated extinction (IE) is defined as the integral of the scattering cross-section as a function of wavelength. Sohl et al. [1] derived an IE expression for acoustic scattering that is causal, i.e. the scattered wavefront in the forward direction arrives later than the incident plane wave in the background medium. The IE formula was based on electromagnetic results, for which scattering is causal by default. Here we derive a formula for the acoustic IE that is valid for causal and non-causal scattering. The general result is expressed as an integral of the time dependent forward scattering function. The IE reduces to a finite integral for scatterers with zero long-wavelength monopole and dipole amplitudes. Implications for acoustic cloaking are discussed and a new metric is proposed for broadband acoustic transparency.

  10. Acoustics Noise Test Cell

    Federal Laboratory Consortium — The Acoustic Noise Test Cell at the NASA/Caltech Jet Propulsion Laboratory (JPL) is located adjacent to the large vibration system; both are located in a class 10K...

  11. Principles of musical acoustics

    Hartmann, William M

    2013-01-01

    Principles of Musical Acoustics focuses on the basic principles in the science and technology of music. Musical examples and specific musical instruments demonstrate the principles. The book begins with a study of vibrations and waves, in that order. These topics constitute the basic physical properties of sound, one of two pillars supporting the science of musical acoustics. The second pillar is the human element, the physiological and psychological aspects of acoustical science. The perceptual topics include loudness, pitch, tone color, and localization of sound. With these two pillars in place, it is possible to go in a variety of directions. The book treats in turn, the topics of room acoustics, audio both analog and digital, broadcasting, and speech. It ends with chapters on the traditional musical instruments, organized by family. The mathematical level of this book assumes that the reader is familiar with elementary algebra. Trigonometric functions, logarithms and powers also appear in the book, but co...

  12. Compact acoustic refrigerator

    Bennett, Gloria A.

    1992-01-01

    A compact acoustic refrigeration system actively cools components, e.g., electrical circuits (22), in a borehole environment. An acoustic engine (12, 14) includes first thermodynamic elements (12) for generating a standing acoustic wave in a selected medium. An acoustic refrigerator (16, 26, 28) includes second thermodynamic elements (16) located in the standing wave for generating a relatively cold temperature at a first end of the second thermodynamic elements (16) and a relatively hot temperature at a second end of the second thermodynamic elements (16). A resonator volume (18) cooperates with the first and second thermodynamic elements (12, 16) to support the standing wave. To accommodate the high heat fluxes required for heat transfer to/from the first and second thermodynamic elements (12, 16), first heat pipes (24, 26) transfer heat from the heat load (22) to the second thermodynamic elements (16) and second heat pipes (28, 32) transfer heat from first and second thermodynamic elements (12, 16) to the borehole environment.

  13. Acoustics lecturing in Mexico

    Beristain, Sergio

    2002-11-01

    Some thirty years ago acoustics lecturing started in Mexico at the National Polytechnic Institute in Mexico City, as part of the Bachelor of Science degree in Communications and Electronics Engineering curricula, including the widest program on this field in the whole country. This program has been producing acoustics specialists ever since. Nowadays many universities and superior education institutions around the country are teaching students at the B.Sc. level and postgraduate level many topics related to acoustics, such as Architectural Acoustics, Seismology, Mechanical Vibrations, Noise Control, Audio, Audiology, Music, etc. Also many institutions have started research programs in related fields, with participation of medical doctors, psychologists, musicians, engineers, etc. Details will be given on particular topics and development.

  14. Acoustic Igniter Project

    National Aeronautics and Space Administration — An acoustic igniter eliminates the need to use electrical energy to drive spark systems to initiate combustion in liquid-propellant rockets. It does not involve the...

  15. Thermal Acoustic Fatigue Apparatus

    Federal Laboratory Consortium — The Thermal Acoustic Fatigue Apparatus (TAFA) is a progressive wave tube test facility that is used to test structures for dynamic response and sonic fatigue due to...

  16. Acoustic Neuroma Educational Video

    Full Text Available ... treatment Summary Types Of Post-treatment Issues Resources Medical Resources Considerations When Selecting a Healthcare Professional Healthcare ... ANA? Mission Statement Board of Directors ANA Staff Medical Advisory Board News ANA Annual Reports Acoustic Neuroma ...

  17. Acoustic coherent perfect absorbers

    In this paper, we explore the possibility of achieving acoustic coherent perfect absorbers. Through numerical simulations in two dimensions, we demonstrate that the energy of coherent acoustic waves can be totally absorbed by a fluid absorber with specific complex mass density or bulk modulus. The robustness of such absorbing systems is investigated under small perturbations of the absorber parameters. We find that when the resonance order is the lowest and the size of the absorber is comparable to the wavelength in the background, the phenomenon of perfect absorption is most stable. When the wavelength inside both the background and the absorber is much larger than the size of the absorber, perfect absorption is possible when the mass density of the absorber approaches the negative value of the background mass density. Finally, we show that by using suitable dispersive acoustic metamaterials, broadband acoustic perfect absorption may be achieved. (papers)

  18. Ocean acoustic reverberation tomography.

    Dunn, Robert A

    2015-12-01

    Seismic wide-angle imaging using ship-towed acoustic sources and networks of ocean bottom seismographs is a common technique for exploring earth structure beneath the oceans. In these studies, the recorded data are dominated by acoustic waves propagating as reverberations in the water column. For surveys with a small receiver spacing (e.g., tomography, is developed that uses the travel times of direct and reflected waves to image ocean acoustic structure. Reverberation tomography offers an alternative approach for determining the structure of the oceans and advancing the understanding of ocean heat content and mixing processes. The technique has the potential for revealing small-scale ocean thermal structure over the entire vertical height of the water column and along long survey profiles or across three-dimensional volumes of the ocean. For realistic experimental geometries and data noise levels, the method can produce images of ocean sound speed on a smaller scale than traditional acoustic tomography. PMID:26723303

  19. Autonomous Acoustic Receiver System

    Federal Laboratory Consortium — FUNCTION: Collects underwater acoustic data and oceanographic data. Data are recorded onboard an ocean buoy and can be telemetered to a remote ship or shore station...

  20. Medical applications of NMR imaging and NMR spectroscopy with stable isotopes. Summary

    The current status of NMR imaging and NMR spectroscopy are summarized. For the most part examples from the March 1983 Puerto Rico symposium are used to illustrate the utility of NMR in medicine. 18 refs., 5 figs

  1. Acoustic emission source modeling

    Hora, Petr; Červená, Olga

    Plzeň : University of West Bohemia, 2009 - (Adámek, V.; Zajíček, M.). s. 1-2 ISBN 978-80-7043-824-4. [Výpočtová mechanika 2009. 09.11.2009-11.11.2009, Nečtiny] R&D Projects: GA ČR GA101/09/1630 Institutional research plan: CEZ:AV0Z20760514 Keywords : acoustic emission source * wave propagation * FEM Subject RIV: BI - Acoustics

  2. The autonomous acoustic buoy

    Pellicer, Francisco; Reitsma, Robert; Agüera, Joaquín; Marinas, Alexandra

    2013-01-01

    The Acoustic Buoy is a project between the Laboratory of Applied Bioacoustics (LAB) and the Universitat Politècnica de Catalunya (UPC). In areas that the human activities produce high noise levels, such as oil exploration or construction, there is a need to monitor the environment for the presence of cetaceans. Another need is for fishing, to prevent endangered species from being killed. This can be done with an Autonomous Acoustic Buoy (AAB). Mooring or anchoring at to the seaflo...

  3. Anal acoustic reflectometry

    Mitchell, Peter J; Klarskov, Niels; Telford, Karen J; Hosker, Gordon L; Lose, Gunnar; Kiff, Edward S

    2011-01-01

    Anal acoustic reflectometry is a new technique of assessing anal sphincter function. Five new variables reflecting anal canal function are measured: the opening and closing pressure, the opening and closing elastance, and hysteresis.......Anal acoustic reflectometry is a new technique of assessing anal sphincter function. Five new variables reflecting anal canal function are measured: the opening and closing pressure, the opening and closing elastance, and hysteresis....

  4. Wavefront modulation and subwavelength diffractive acoustics with an acoustic metasurface.

    Xie, Yangbo; Wang, Wenqi; Chen, Huanyang; Konneker, Adam; Popa, Bogdan-Ioan; Cummer, Steven A

    2014-01-01

    Metasurfaces are a family of novel wavefront-shaping devices with planar profile and subwavelength thickness. Acoustic metasurfaces with ultralow profile yet extraordinary wave manipulating properties would be highly desirable for improving the performance of many acoustic wave-based applications. However, designing acoustic metasurfaces with similar functionality to their electromagnetic counterparts remains challenging with traditional metamaterial design approaches. Here we present a design and realization of an acoustic metasurface based on tapered labyrinthine metamaterials. The demonstrated metasurface can not only steer an acoustic beam as expected from the generalized Snell's law, but also exhibits various unique properties such as conversion from propagating wave to surface mode, extraordinary beam-steering and apparent negative refraction through higher-order diffraction. Such designer acoustic metasurfaces provide a new design methodology for acoustic signal modulation devices and may be useful for applications such as acoustic imaging, beam steering, ultrasound lens design and acoustic surface wave-based applications. PMID:25418084

  5. NMR Dynamic Studies in Living Systems

    闫永彬; 范明杰; 罗雪春; 张日清

    2002-01-01

    Nuclear magnetic resonance (NMR) can noninvasively monitor the intracellular concentrations and kinetic properties of numerous inorganic and organic compounds. These characteristics have made NMR a useful tool for dynamic studies of living systems. Applications of NMR to living systems have successfully extended to many areas, including studies of metabolic regulation, ion transport, and intracellular reaction rates in vivo. The major purpose of this review is to summarize the results that can be obtained by modern NMR techniques in living systems. With the advances of new techniques, NMR measurements of various nuclides have been performed for specific physiological purposes. Although some technical problems still remain and there are still discrepancies between NMR and traditional biochemical results, the abundant and unique information obtained from NMR spectra suggests that NMR will be more extensively applied in future studies of living systems. The fast development of these new techniques is providing many new NMR applications in living systems, as well as in structural biology.

  6. Acoustic vector sensor signal processing

    SUN Guiqing; LI Qihu; ZHANG Bin

    2006-01-01

    Acoustic vector sensor simultaneously, colocately and directly measures orthogonal components of particle velocity as well as pressure at single point in acoustic field so that is possible to improve performance of traditional underwater acoustic measurement devices or detection systems and extends new ideas for solving practical underwater acoustic engineering problems. Although acoustic vector sensor history of appearing in underwater acoustic area is no long, but with huge and potential military demands, acoustic vector sensor has strong development trend in last decade, it is evolving into a one of important underwater acoustic technology. Under this background, we try to review recent progress in study on acoustic vector sensor signal processing, such as signal detection, DOA estimation, beamforming, and so on.

  7. Acoustic comfort in eating establishments

    Svensson, David; Jeong, Cheol-Ho; Brunskog, Jonas

    2014-01-01

    The subjective concept of acoustic comfort in eating establishments has been investigated in this study. The goal was to develop a predictive model for the acoustic comfort, by means of simple objective parameters, while also examining which other subjective acoustic parameters could help explain...... the feeling of acoustic comfort. Through several layers of anal ysis, acoustic comfort was found to be rather complex, and could not be explained entirely by common subjective parameters such as annoyance, intelligibility or privacy. A predictive model for the mean acoustic comfort for an eating...

  8. Phononic crystals and acoustic metamaterials

    Ming-Hui Lu

    2009-12-01

    Full Text Available Phononic crystals have been proposed about two decades ago and some important characteristics such as acoustic band structure and negative refraction have stimulated fundamental and practical studies in acoustic materials and devices since then. To carefully engineer a phononic crystal in an acoustic “atom” scale, acoustic metamaterials with their inherent deep subwavelength nature have triggered more exciting investigations on negative bulk modulus and/or negative mass density. Acoustic surface evanescent waves have also been recognized to play key roles to reach acoustic subwavelength imaging and enhanced transmission.

  9. NMR and dynamics of biopolymers

    Several basic experimental analytical NMR techniques that are frequently used for the qualitative and quantitative analysis of dynamic and exchange processes, focusing on proteins systems, are described: chemical exchange (slow exchange, fast exchange, intermediate exchange), heteronuclear relaxation measurements (relaxation parameters, strategy of relaxation data analysis, experimental results and examples, motional model interpretation of relaxation data, homonuclear relaxation); slow large-scale exchange and hydrogen-deuterium exchange are also studied: mechanisms of hydrogen exchange in a native protein, methods for measuring amide exchange rates by NMR, interpretation of amide exchange rates. 9 fig., 3 tab., 56 ref

  10. Two-dimensional NMR spectrometry

    This article is the second in a two-part series. In part one (ANALYTICAL CHEMISTRY, May 15) the authors discussed one-dimensional nuclear magnetic resonance (NMR) spectra and some relatively advanced nuclear spin gymnastics experiments that provide a capability for selective sensitivity enhancements. In this article and overview and some applications of two-dimensional NMR experiments are presented. These powerful experiments are important complements to the one-dimensional experiments. As in the more sophisticated one-dimensional experiments, the two-dimensional experiments involve three distinct time periods: a preparation period, t0; an evolution period, t1; and a detection period, t2

  11. Advanced NMR characterization of zeolite catalysts

    Welsh, L. B.

    1985-04-01

    The program discussed in this report is a two-year two-phase joint UOP-University of Illinois study of the application of improved high resolution solid state nuclear magnetic resonance (NMR) techniques to the characterization of zeolite catalysts. During the first phase of this program very pure, and in some cases isotopically enriched faujasites will be prepared and studied by magic angle sample spinning NMR (MASS NMR) and variable engine sample spinning NMR (VASS NMR) on 500 and 360 MHz (proton frequency) NMR spectrometers. The NMR techniques that will be emphasized are the measurement and analysis of the (17)O NMR properties, (27)Al NMR intensity quantitation, and (27)Al and (29)Si NMR relaxation rates. During the second phase of this program these NMR techniques will be used to study the effects of impurity concentration, dealumination treatments and cation exchange on the NMR properties of faujasites. The initial emphasis of this program during Phase I is on the preparation and measurement of the NMR properties of (17)O enriched Na-Y faujasties.

  12. From Architectural Acoustics to Acoustical Architecture Using Computer Simulation

    Schmidt, Anne Marie Due; Kirkegaard, Poul Henning

    2005-01-01

    Architectural acoustics design has in the past been based on simple design rules. However, with a growing complexity in architectural acoustics and the emergence of room acoustic simulation programmes with considerable potential, it is now possible to subjectively analyse and evaluate acoustic...... properties prior to the actual construction of a building. With the right tools applied, acoustic design can become an integral part of the architectural design process. The aim of this paper is to investigate the field of application that an acoustic simulation programme can have during an architectural...... the first phases in the architectural process and set out a reverse strategy for simulation programmes to do so - from developing acoustics from given spaces to developing spaces from given acoustics...

  13. Radiofrequency and magnet technology in medical NMR

    Nuclear magnetic resonance (NMR) is briefly described, particularly its rf and magnet aspects. Particular attention is given to the duplexer, the rf coils, and new kinds of magnets for remote sensing NMR

  14. Push-through Direction Injectin NMR Automation

    Nuclear magnetic resonance (NMR) and mass spectrometry (MS) are the two major spectroscopic techniques successfully used in metabolomics studies. The non-invasive, quantitative and reproducible characteristics make NMR spectroscopy an excellent technique for detection of endogeno...

  15. Wavefront Modulation and Subwavelength Diffractive Acoustics with an Acoustic Metasurface

    Xie, Yangbo; Wang, Wenqi; Chen, Huanyang; Konneker, Adam; Popa, Bogdan-Ioan; Cummer, Steven A.

    2014-01-01

    Metasurfaces are a family of novel wavefront shaping devices with planar profile and subwavelength thickness. Acoustic metasurfaces with ultralow profile yet extraordinary wave manipulating properties would be highly desirable for improving the performance of many acoustic wave-based applications. However, designing acoustic metasurfaces with similar functionality as their electromagnetic counterparts remains challenging with traditional metamaterial design approaches. Here we present a desig...

  16. ACOUSTICS IN ARCHITECTURAL DESIGN, AN ANNOTATED BIBLIOGRAPHY ON ARCHITECTURAL ACOUSTICS.

    DOELLE, LESLIE L.

    THE PURPOSE OF THIS ANNOTATED BIBLIOGRAPHY ON ARCHITECTURAL ACOUSTICS WAS--(1) TO COMPILE A CLASSIFIED BIBLIOGRAPHY, INCLUDING MOST OF THOSE PUBLICATIONS ON ARCHITECTURAL ACOUSTICS, PUBLISHED IN ENGLISH, FRENCH, AND GERMAN WHICH CAN SUPPLY A USEFUL AND UP-TO-DATE SOURCE OF INFORMATION FOR THOSE ENCOUNTERING ANY ARCHITECTURAL-ACOUSTIC DESIGN…

  17. Acoustic detection of pneumothorax

    Mansy, Hansen A.; Royston, Thomas J.; Balk, Robert A.; Sandler, Richard H.

    2003-04-01

    This study aims at investigating the feasibility of using low-frequency (pneumothorax detection were tested in dogs. In the first approach, broadband acoustic signals were introduced into the trachea during end-expiration and transmitted waves were measured at the chest surface. Pneumothorax was found to consistently decrease pulmonary acoustic transmission in the 200-1200-Hz frequency band, while less change was observed at lower frequencies (ppneumothorax states (pPneumothorax was found to be associated with a preferential reduction of sound amplitude in the 200- to 700-Hz range, and a decrease of sound amplitude variation (in the 300 to 600-Hz band) during the respiration cycle (pPneumothorax changed the frequency and decay rate of percussive sounds. These results imply that certain medical conditions may be reliably detected using appropriate acoustic measurements and analysis. [Work supported by NIH/NHLBI #R44HL61108.

  18. Seamount acoustic scattering

    Boehlert, George W.

    The cover of the March 1 issue of Eos showed a time series of acoustic scattering above Southeast Hancock Seamount (29°48‧N, 178°05‧E) on July 17-18, 1984. In a comment on that cover Martin Hovland (Eos, August 2, p. 760) argued that gas or “other far reaching causes” may be involved in the observed acoustic signals. He favors a hypothesis that acoustic scattering observed above a seeping pockmark in the North Sea is a combination of bubbles, stable microbubbles, and pelagic organisms and infers that this may be a more general phenomenon and indeed plays a role in the attraction of organisms to seamounts

  19. Acoustics waves and oscillations

    Sen, S.N.

    2013-01-01

    Parameters of acoustics presented in a logical and lucid style Physical principles discussed with mathematical formulations Importance of ultrasonic waves highlighted Dispersion of ultrasonic waves in viscous liquids explained This book presents the theory of waves and oscillations and various applications of acoustics in a logical and simple form. The physical principles have been explained with necessary mathematical formulation and supported by experimental layout wherever possible. Incorporating the classical view point all aspects of acoustic waves and oscillations have been discussed together with detailed elaboration of modern technological applications of sound. A separate chapter on ultrasonics emphasizes the importance of this branch of science in fundamental and applied research. In this edition a new chapter ''Hypersonic Velocity in Viscous Liquids as revealed from Brillouin Spectra'' has been added. The book is expected to present to its readers a comprehensive presentation of the subject matter...

  20. Practical acoustic emission testing

    2016-01-01

    This book is intended for non-destructive testing (NDT) technicians who want to learn practical acoustic emission testing based on level 1 of ISO 9712 (Non-destructive testing – Qualification and certification of personnel) criteria. The essential aspects of ISO/DIS 18436-6 (Condition monitoring and diagnostics of machines – Requirements for training and certification of personnel, Part 6: Acoustic Emission) are explained, and readers can deepen their understanding with the help of practice exercises. This work presents the guiding principles of acoustic emission measurement, signal processing, algorithms for source location, measurement devices, applicability of testing methods, and measurement cases to support not only researchers in this field but also and especially NDT technicians.

  1. High resolution NMR theory and chemical applications

    Becker, Edwin D

    1969-01-01

    High Resolution NMR: Theory and Chemical Applications focuses on the applications of nuclear magnetic resonance (NMR), as well as chemical shifts, lattices, and couplings. The book first offers information on the theory of NMR, including nuclear spin and magnetic moment, spin lattice relaxation, line widths, saturation, quantum mechanical description of NMR, and ringing. The text then ponders on instrumentation and techniques and chemical shifts. Discussions focus on the origin of chemical shifts, reference compounds, empirical correlations of chemical shifts, modulation and phase detection,

  2. Cancer metastasis detected by NMR

    A narrow NMR line originating from the plasma membrane of a cancer cell is unexpected. The behaviour of these lines is explained in terms of fundamental physics and chemistry. There is biochemical evidence to support the presence of neutral lipid domains in the plasma membrane. T2 relaxation and clinical implications are briefly discussed

  3. Advanced Active Acoustics Lab (AAAL)

    Federal Laboratory Consortium — The Advanced Active Acoustics Lab (AAAL) is a state-of-the-art Undersea Warfare (USW) acoustic data analysis facility capable of both active and passive underwater...

  4. A New Wave of Acoustics.

    Beyer, Robert

    1981-01-01

    Surveys 50 years of acoustical studies by discussing selected topics including the ear, nonlinear representations, underwater sound, acoustical diagnostics, absorption, electrolytes, phonons, magnetic interaction, and superfluidity and the five sounds. (JN)

  5. A Century of Acoustic Metrology

    Rasmussen, Knud

    The development in acoustic measurement technique over the last century is reviewed with special emphasis on the metrological aspect.......The development in acoustic measurement technique over the last century is reviewed with special emphasis on the metrological aspect....

  6. Strong acoustic wave action

    Gokhberg, M. B.

    1983-07-01

    Experiments devoted to acoustic action on the atmosphere-magnetosphere-ionosphere system using ground based strong explosions are reviewed. The propagation of acoustic waves was observed by ground observations over 2000 km in horizontal direction and to an altitude of 200 km. Magnetic variations up to 100 nT were detected by ARIEL-3 satellite near the epicenter of the explosion connected with the formation of strong field aligned currents in the magnetosphere. The enhancement of VLF emission at 800 km altitude is observed.

  7. Acoustic black holes

    Visser, M

    1999-01-01

    Acoustic propagation in a moving fluid provides a conceptually clean and powerful analogy for understanding black hole physics. As a teaching tool, the analogy is useful for introducing students to both General Relativity and fluid mechanics. As a research tool, the analogy helps clarify what aspects of the physics are kinematics and what aspects are dynamics. In particular, Hawking radiation is a purely kinematical effect, whereas black hole entropy is intrinsically dynamical. Finally, I discuss the fact that with present technology acoustic Hawking radiation is almost experimentally testable.

  8. Structural Acoustics and Vibrations

    Chaigne, Antoine

    This structural chapter is devoted to vibrations of structures and to their coupling with the acoustic field. Depending on the context, the radiated sound can be judged as desirable, as is mostly the case for musical instruments, or undesirable, like noise generated by machinery. In architectural acoustics, one main goal is to limit the transmission of sound through walls. In the automobile industry, the engineers have to control the noise generated inside and outside the passenger compartment. This can be achieved by means of passive or active damping. In general, there is a strong need for quieter products and better sound quality generated by the structures in our daily environment.

  9. Densitometry By Acoustic Levitation

    Trinh, Eugene H.

    1989-01-01

    "Static" and "dynamic" methods developed for measuring mass density of acoustically levitated solid particle or liquid drop. "Static" method, unknown density of sample found by comparison with another sample of known density. "Dynamic" method practiced with or without gravitational field. Advantages over conventional density-measuring techniques: sample does not have to make contact with container or other solid surface, size and shape of samples do not affect measurement significantly, sound field does not have to be know in detail, and sample can be smaller than microliter. Detailed knowledge of acoustic field not necessary.

  10. Acoustic subwavelength imaging of subsurface objects with acoustic resonant metalens

    Cheng, Ying; Liu, XiaoJun, E-mail: liuxiaojun@nju.edu.cn [Key Laboratory of Modern Acoustics, Nanjing University, Nanjing 210093 (China); State Key Laboratory of Acoustics, Institute of Acoustics, Chinese Academy of Sciences, Beijing 100190 (China); Zhou, Chen; Wei, Qi; Wu, DaJian [Key Laboratory of Modern Acoustics, Nanjing University, Nanjing 210093 (China)

    2013-11-25

    Early research into acoustic metamaterials has shown the possibility of achieving subwavelength near-field acoustic imaging. However, a major restriction of acoustic metamaterials is that the imaging objects must be placed in close vicinity of the devices. Here, we present an approach for acoustic imaging of subsurface objects far below the diffraction limit. An acoustic metalens made of holey-structured metamaterials is used to magnify evanescent waves, which can rebuild an image at the central plane. Without changing the physical structure of the metalens, our proposed approach can image objects located at certain distances from the input surface, which provides subsurface signatures of the objects with subwavelength spatial resolution.

  11. Acoustic subwavelength imaging of subsurface objects with acoustic resonant metalens

    Early research into acoustic metamaterials has shown the possibility of achieving subwavelength near-field acoustic imaging. However, a major restriction of acoustic metamaterials is that the imaging objects must be placed in close vicinity of the devices. Here, we present an approach for acoustic imaging of subsurface objects far below the diffraction limit. An acoustic metalens made of holey-structured metamaterials is used to magnify evanescent waves, which can rebuild an image at the central plane. Without changing the physical structure of the metalens, our proposed approach can image objects located at certain distances from the input surface, which provides subsurface signatures of the objects with subwavelength spatial resolution

  12. Underwater Acoustic Networking Techniques

    Otnes, Roald; Casari, Paolo; Goetz, Michael; Husøy, Thor; Nissen, Ivor; Rimstad, Knut; van Walree, Paul; Zorzi, Michele

    2012-01-01

    This literature study presents an overview of underwater acoustic networking. It provides a background and describes the state of the art of all networking facets that are relevant for underwater applications. This report serves both as an introduction to the subject and as a summary of existing protocols, providing support and inspiration for the development of network architectures.

  13. COMBUSTION ACOUSTICS DIAGNOSTICS

    This is an Exploratory Research Project that was awarded by APPCD for research on developing an acoustic flame condition monitor. It will involve a bench scale experiment of 4-6 weeks duration to record adjacent audible energy of a Bunsen burner. The experiment will require a d...

  14. Acoustic Signals and Systems

    present topics on signal processing which are important in a specific area of acoustics. These will be of interest to specialists in these areas because they will be presented from their technical perspective, rather than a generic engineering approach to signal processing. Non-specialists, or specialists...

  15. NMR Studies of Inclusion Compounds

    Nikkhou Aski, Sahar

    2008-01-01

    This thesis presents the application of some of the NMR methods in studying host-guest complexes, mainly in solution. The general focus of the work is on investigating the reorientational dynamics of some small molecules that are bound inside cavities of larger moieties. In the current work, these moieties belong to two groups: cryptophanes and cyclodextrins. Depending on the structure of the cavities, properties of the guest molecules and the formed complexes vary. Chloroform and dichloromet...

  16. Measurement of deformations by NMR

    Bytchenkoff, Dimitri; Rodts, Stéphane

    2015-12-01

    Two NMR data acquisition protocols together with corresponding data processing algorithms for locating macroscopic objects, measuring distances between them or monitoring their displacements or deformations with microscopic precision are presented and discussed. The performance of the methods is demonstrated by applying them to the measurement of deformations of a freely supported beam under loading. We believe that our methods will find their applications in mechanics, civil engineering and medicine.

  17. RECENT PROGRESS IN BIOMOLECULAR NMR

    2002-01-01

    @@ Structural genomics and proteomics were born from the understanding that functions of a protein are dictated by its 3D structure and dynamics. To understand protein functions on a genomic scale, we must know protein structures on a genomic scale. High resolution NMR can be used for this purpose. Traditional multidimensional NMR structure determination protocols become ineffective for structural genomics since to obtain a structure of a small protein of 15kD requires many months of painstaking spectral analysis and modeling. Recent advances in magnet and probe technology and in experimental methods have expanded the range of proteins amenable to structure determination and make the large scale structure determination possible. These advances are (1) effective expression systems for protein production, (2) introduction of cryoprobe, (3) structure determination with the use of the minimal amount of structural restraints obtained from the chemical shifts, residual dipolar couplings, NOEs, and computer modeling. In this talk,Iwill briefly outline these developments and related works done in our NMR lab.

  18. NMR-Based Milk Metabolomics

    Hanne C. Bertram

    2013-04-01

    Full Text Available Milk is a key component in infant nutrition worldwide and, in the Western parts of the world, also in adult nutrition. Milk of bovine origin is both consumed fresh and processed into a variety of dairy products including cheese, fermented milk products, and infant formula. The nutritional quality and processing capabilities of bovine milk is closely associated to milk composition. Metabolomics is ideal in the study of the low-molecular-weight compounds in milk, and this review focuses on the recent nuclear magnetic resonance (NMR-based metabolomics trends in milk research, including applications linking the milk metabolite profiling with nutritional aspects, and applications which aim to link the milk metabolite profile to various technological qualities of milk. The metabolite profiling studies encompass the identification of novel metabolites, which potentially can be used as biomarkers or as bioactive compounds. Furthermore, metabolomics applications elucidating how the differential regulated genes affects milk composition are also reported. This review will highlight the recent advances in NMR-based metabolomics on milk, as well as give a brief summary of when NMR spectroscopy can be useful for gaining a better understanding of how milk composition is linked to nutritional or quality traits.

  19. NMR-Based Milk Metabolomics.

    Sundekilde, Ulrik K; Larsen, Lotte B; Bertram, Hanne C

    2013-01-01

    Milk is a key component in infant nutrition worldwide and, in the Western parts of the world, also in adult nutrition. Milk of bovine origin is both consumed fresh and processed into a variety of dairy products including cheese, fermented milk products, and infant formula. The nutritional quality and processing capabilities of bovine milk is closely associated to milk composition. Metabolomics is ideal in the study of the low-molecular-weight compounds in milk, and this review focuses on the recent nuclear magnetic resonance (NMR)-based metabolomics trends in milk research, including applications linking the milk metabolite profiling with nutritional aspects, and applications which aim to link the milk metabolite profile to various technological qualities of milk. The metabolite profiling studies encompass the identification of novel metabolites, which potentially can be used as biomarkers or as bioactive compounds. Furthermore, metabolomics applications elucidating how the differential regulated genes affects milk composition are also reported. This review will highlight the recent advances in NMR-based metabolomics on milk, as well as give a brief summary of when NMR spectroscopy can be useful for gaining a better understanding of how milk composition is linked to nutritional or quality traits. PMID:24957988

  20. Structural proteomics by NMR spectroscopy.

    Shin, Joon; Lee, Woonghee; Lee, Weontae

    2008-08-01

    Structural proteomics is one of the powerful research areas in the postgenomic era, elucidating structure-function relationships of uncharacterized gene products based on the 3D protein structure. It proposes biochemical and cellular functions of unannotated proteins and thereby identifies potential drug design and protein engineering targets. Recently, a number of pioneering groups in structural proteomics research have achieved proof of structural proteomic theory by predicting the 3D structures of hypothetical proteins that successfully identified the biological functions of those proteins. The pioneering groups made use of a number of techniques, including NMR spectroscopy, which has been applied successfully to structural proteomics studies over the past 10 years. In addition, advances in hardware design, data acquisition methods, sample preparation and automation of data analysis have been developed and successfully applied to high-throughput structure determination techniques. These efforts ensure that NMR spectroscopy will become an important methodology for performing structural proteomics research on a genomic scale. NMR-based structural proteomics together with x-ray crystallography will provide a comprehensive structural database to predict the basic biological functions of hypothetical proteins identified by the genome projects. PMID:18761469

  1. Flat acoustic lens by acoustic grating with curled slits

    Peng, Pai

    2014-10-01

    We design a flat sub-wavelength lens that can focus acoustic wave. We analytically study the transmission through an acoustic grating with curled slits, which can serve as a material with tunable impedance and refractive index for acoustic waves. The effective parameters rely on the geometry of the slits and are independent of frequency. A flat acoustic focusing lens by such acoustic grating with gradient effective refractive index is designed. The focusing effect is clearly observed in simulations and well predicted by the theory. We demonstrate that despite the large impedance mismatch between the acoustic lens and the matrix, the intensity at the focal point is still high due to Fabry-Perot resonance.

  2. Acoustics Discipline Overview

    Envia, Edmane; Thomas, Russell

    2007-01-01

    As part of the Fundamental Aeronautics Program Annual Review, a summary of the progress made in 2007 in acoustics research under the Subsonic Fixed Wing project is given. The presentation describes highlights from in-house and external activities including partnerships and NRA-funded research with industry and academia. Brief progress reports from all acoustics Phase 1 NRAs are also included as are outlines of the planned activities for 2008 and all Phase 2 NRAs. N+1 and N+2 technology paths outlined for Subsonic Fixed Wing noise targets. NRA Round 1 progressing with focus on prediction method advancement. NRA Round 2 initiating work focused on N+2 technology, prediction methods, and validation. Excellent partnerships in progress supporting N+1 technology targets and providing key data sets.

  3. Acoustic methodology review

    Schlegel, R. G.

    1982-01-01

    It is important for industry and NASA to assess the status of acoustic design technology for predicting and controlling helicopter external noise in order for a meaningful research program to be formulated which will address this problem. The prediction methodologies available to the designer and the acoustic engineer are three-fold. First is what has been described as a first principle analysis. This analysis approach attempts to remove any empiricism from the analysis process and deals with a theoretical mechanism approach to predicting the noise. The second approach attempts to combine first principle methodology (when available) with empirical data to formulate source predictors which can be combined to predict vehicle levels. The third is an empirical analysis, which attempts to generalize measured trends into a vehicle noise prediction method. This paper will briefly address each.

  4. Acoustic Tractor Beam

    Démoré, Christine E. M.; Dahl, Patrick M.; Yang, Zhengyi; Glynne-Jones, Peter; Melzer, Andreas; Cochran, Sandy; MacDonald, Michael P.; Spalding, Gabriel C.

    2014-05-01

    Negative radiation forces act opposite to the direction of propagation, or net momentum, of a beam but have previously been challenging to definitively demonstrate. We report an experimental acoustic tractor beam generated by an ultrasonic array operating on macroscopic targets (>1 cm) to demonstrate the negative radiation forces and to map out regimes over which they dominate, which we compare to simulations. The result and the geometrically simple configuration show that the effect is due to nonconservative forces, produced by redirection of a momentum flux from the angled sides of a target and not by conservative forces from a potential energy gradient. Use of a simple acoustic setup provides an easily understood illustration of the negative radiation pressure concept for tractor beams and demonstrates continuous attraction towards the source, against a net momentum flux in the system.

  5. Acoustic classification of dwellings

    Berardi, Umberto; Rasmussen, Birgit

    2014-01-01

    Schemes for the classification of dwellings according to different building performances have been proposed in the last years worldwide. The general idea behind these schemes relates to the positive impact a higher label, and thus a better performance, should have. In particular, focusing on sound...... insulation performance, national schemes for sound classification of dwellings have been developed in several European countries. These schemes define acoustic classes according to different levels of sound insulation. Due to the lack of coordination among countries, a significant diversity in terms of...... descriptors, number of classes, and class intervals occurred between national schemes. However, a proposal “acoustic classification scheme for dwellings” has been developed recently in the European COST Action TU0901 with 32 member countries. This proposal has been accepted as an ISO work item. This paper...

  6. Acoustic emission source modeling

    Hora P.

    2010-07-01

    Full Text Available The paper deals with the acoustic emission (AE source modeling by means of FEM system COMSOL Multiphysics. The following types of sources are used: the spatially concentrated force and the double forces (dipole. The pulse excitation is studied in both cases. As a material is used steel. The computed displacements are compared with the exact analytical solution of point sources under consideration.

  7. The acoustics of snoring.

    Pevernagie, Dirk; Aarts, Ronald M; De Meyer, Micheline

    2010-04-01

    Snoring is a prevalent disorder affecting 20-40% of the general population. The mechanism of snoring is vibration of anatomical structures in the pharyngeal airway. Flutter of the soft palate accounts for the harsh aspect of the snoring sound. Natural or drug-induced sleep is required for its appearance. Snoring is subject to many influences such as body position, sleep stage, route of breathing and the presence or absence of sleep-disordered breathing. Its presentation may be variable within or between nights. While snoring is generally perceived as a social nuisance, rating of its noisiness is subjective and, therefore, inconsistent. Objective assessment of snoring is important to evaluate the effect of treatment interventions. Moreover, snoring carries information relating to the site and degree of obstruction of the upper airway. If evidence for monolevel snoring at the site of the soft palate is provided, the patient may benefit from palatal surgery. These considerations have inspired researchers to scrutinize the acoustic characteristics of snoring events. Similarly to speech, snoring is produced in the vocal tract. Because of this analogy, existing techniques for speech analysis have been applied to evaluate snoring sounds. It appears that the pitch of the snoring sound is in the low-frequency range (noise-like', and has scattered energy content in the higher spectral sub-bands (>500 Hz). To evaluate acoustic properties of snoring, sleep nasendoscopy is often performed. Recent evidence suggests that the acoustic quality of snoring is markedly different in drug-induced sleep as compared with natural sleep. Most often, palatal surgery alters sound characteristics of snoring, but is no cure for this disorder. It is uncertain whether the perceived improvement after palatal surgery, as judged by the bed partner, is due to an altered sound spectrum. Whether some acoustic aspects of snoring, such as changes in pitch, have predictive value for the presence of

  8. Acoustically enhanced heat transport

    Ang, Kar M.; Hung, Yew Mun; Tan, Ming K., E-mail: tan.ming.kwang@monash.edu [School of Engineering, Monash University Malaysia, 47500 Bandar Sunway, Selangor (Malaysia); Yeo, Leslie Y. [Micro/Nanophysics Research Laboratory, RMIT University, Melbourne, VIC 3001 (Australia); Friend, James R. [Department of Mechanical and Aerospace Engineering, University of California, San Diego, California 92093 (United States)

    2016-01-15

    We investigate the enhancement of heat transfer in the nucleate boiling regime by inducing high frequency acoustic waves (f ∼ 10{sup 6} Hz) on the heated surface. In the experiments, liquid droplets (deionized water) are dispensed directly onto a heated, vibrating substrate. At lower vibration amplitudes (ξ{sub s} ∼ 10{sup −9} m), the improved heat transfer is mainly due to the detachment of vapor bubbles from the heated surface and the induced thermal mixing. Upon increasing the vibration amplitude (ξ{sub s} ∼ 10{sup −8} m), the heat transfer becomes more substantial due to the rapid bursting of vapor bubbles happening at the liquid-air interface as a consequence of capillary waves travelling in the thin liquid film between the vapor bubble and the air. Further increases then lead to rapid atomization that continues to enhance the heat transfer. An acoustic wave displacement amplitude on the order of 10{sup −8} m with 10{sup 6} Hz order frequencies is observed to produce an improvement of up to 50% reduction in the surface temperature over the case without acoustic excitation.

  9. High-Frequency Seafloor Acoustics

    Jackson, Darrell R

    2007-01-01

    High-Frequency Seafloor Acoustics is the first book in a new series sponsored by the Office of Naval Research on the latest research in underwater acoustics. This exciting new title provides ready access to experimental data, theory, and models relevant to high-frequency seafloor acoustics and will be of interest to sonar engineers and researchers working in underwater acoustics. The physical characteristics of the seafloor affecting acoustic propagation and scattering are covered, including physical and geoacoustic properties and surface roughness. Current theories for acoustic propagation in sediments are presented along with corresponding models for reflection, scattering, and seafloor penetration. The main text is backed up by an extensive bibliography and technical appendices.

  10. Fundamentals of Shallow Water Acoustics

    Katsnelson, Boris; Lynch, James

    2012-01-01

    Shallow water acoustics (SWA), the study of how low and medium frequency sound propagates and scatters on the continental shelves of the world's oceans, has both technical interest and a large number of practical applications. Technically, shallow water poses an interesting medium for the study of acoustic scattering, inverse theory, and propagation physics in a complicated oceanic waveguide. Practically, shallow water acoustics has interest for geophysical exploration, marine mammal studies, and naval applications. Additionally, one notes the very interdisciplinary nature of shallow water acoustics, including acoustical physics, physical oceanography, marine geology, and marine biology. In this specialized volume, the authors, all of whom have extensive at-sea experience in U.S. and Russian research efforts, have tried to summarize the main experimental, theoretical, and computational results in shallow water acoustics, with an emphasis on providing physical insight into the topics presented.

  11. Latest Trends in Acoustic Sensing

    Cinzia Caliendo

    2014-03-01

    Full Text Available Acoustics-based methods offer a powerful tool for sensing applications. Acoustic sensors can be applied in many fields ranging from materials characterization, structural health monitoring, acoustic imaging, defect characterization, etc., to name just a few. A proper selection of the acoustic wave frequency over a wide spectrum that extends from infrasound (<20 Hz up to ultrasound (in the GHz–band, together with a number of different propagating modes, including bulk longitudinal and shear waves, surface waves, plate modes, etc., allow acoustic tools to be successfully applied to the characterization of gaseous, solid and liquid environments. The purpose of this special issue is to provide an overview of the research trends in acoustic wave sensing through some cases that are representative of specific applications in different sensing fields.

  12. Wireless Acoustic Measurement System

    Anderson, Paul D.; Dorland, Wade D.; Jolly, Ronald L.

    2007-01-01

    A prototype wireless acoustic measurement system (WAMS) is one of two main subsystems of the Acoustic Prediction/ Measurement Tool, which comprises software, acoustic instrumentation, and electronic hardware combined to afford integrated capabilities for predicting and measuring noise emitted by rocket and jet engines. The other main subsystem is described in the article on page 8. The WAMS includes analog acoustic measurement instrumentation and analog and digital electronic circuitry combined with computer wireless local-area networking to enable (1) measurement of sound-pressure levels at multiple locations in the sound field of an engine under test and (2) recording and processing of the measurement data. At each field location, the measurements are taken by a portable unit, denoted a field station. There are ten field stations, each of which can take two channels of measurements. Each field station is equipped with two instrumentation microphones, a micro- ATX computer, a wireless network adapter, an environmental enclosure, a directional radio antenna, and a battery power supply. The environmental enclosure shields the computer from weather and from extreme acoustically induced vibrations. The power supply is based on a marine-service lead-acid storage battery that has enough capacity to support operation for as long as 10 hours. A desktop computer serves as a control server for the WAMS. The server is connected to a wireless router for communication with the field stations via a wireless local-area network that complies with wireless-network standard 802.11b of the Institute of Electrical and Electronics Engineers. The router and the wireless network adapters are controlled by use of Linux-compatible driver software. The server runs custom Linux software for synchronizing the recording of measurement data in the field stations. The software includes a module that provides an intuitive graphical user interface through which an operator at the control server

  13. Quality assessment of protein NMR structures

    Rosato A.; Montelione G.T.; Tejero R.

    2013-01-01

    Biomolecular NMR structures are now routinely used in biology, chemistry, and bioinformatics. Methods and metrics for assessing the accuracy and precision of protein NMR structures are beginning to be standardized across the biological NMR community. These include both knowledge-based assessment metrics, parameterized from the database of protein structures, and model versus data assessment metrics. On line servers are available that provide comprehensive protein structure quality assessment ...

  14. NMR INVESTIGATIONS OF HYDROGENATED AMORPHOUS SILICON

    J. Reimer

    1981-01-01

    A review is presented of the N.M.R. (Nuclear Magnetic Resonance) studies to date of hydrogenated amorphous silicon-hydrogen films. Structural features of proton N.M.R. lineshapes, dynamics of hydrogen containing defect sites, and the promise of quantitative determinations of local silicon-hydrogen bonding environments are discussed in detail. Finally, some comments are given on future directions for N.M.R. studies of hydrogenated thin films.

  15. An Inversion Recovery NMR Kinetics Experiment

    Williams, Travis J.; Kershaw, Allan D.; Li, Vincent; Wu, Xinping

    2011-01-01

    A convenient laboratory experiment is described in which NMR magnetization transfer by inversion recovery is used to measure the kinetics and thermochemistry of amide bond rotation. The experiment utilizes Varian spectrometers with the VNMRJ 2.3 software, but can be easily adapted to any NMR platform. The procedures and sample data sets in this article will enable instructors to use inversion recovery as a laboratory activity in applied NMR classes and provide research students with a conveni...

  16. Magneto-photo-acoustic imaging

    Qu, Min; Mallidi, Srivalleesha; Mehrmohammadi, Mohammad; Truby, Ryan; Homan, Kimberly; Joshi, Pratixa; Chen, Yun-Sheng; Sokolov, Konstantin; Emelianov, Stanislav

    2011-01-01

    Magneto-photo-acoustic imaging, a technique based on the synergy of magneto-motive ultrasound, photoacoustic and ultrasound imaging, is introduced. Hybrid nanoconstructs, liposomes encapsulating gold nanorods and iron oxide nanoparticles, were used as a dual-contrast agent for magneto-photo-acoustic imaging. Tissue-mimicking phantom and macrophage cells embedded in ex vivo porcine tissue were used to demonstrate that magneto-photo-acoustic imaging is capable of visualizing the location of cel...

  17. Room acoustic auralization with Ambisonics

    Polack, Jean-Dominique; Leão Figueiredo, Fábio

    2012-01-01

    International audience During the year of 2009, the room acoustics group of the LAM (Équipe Lutheries, Acoustique, Musique de l’Institut Jean Le Rond d’Alembert - Université Pierre et Marie Curie, Paris) performed a series of acoustical measurements in music halls in Paris. The halls were chosen in regarding their importance to the historic, architectural or acoustic domains. The measured ensemble of fourteen rooms includes quite different architectural designs. The measurements were carri...

  18. NMR studies of isotopically labeled RNA

    Pardi, A. [Univ. of Colorado, Boulder, CO (United States)

    1994-12-01

    In summary, the ability to generate NMR quantities of {sup 15}N and {sup 13}C-labeled RNAs has led to the development of heteronuclear multi-dimensional NMR techniques for simplifying the resonance assignment and structure determination of RNAs. These methods for synthesizing isotopically labeled RNAs are only several years old, and thus there are still relatively few applications of heteronuclear multi-dimensional NMR techniques to RNA. However, given the critical role that RNAs play in cellular function, one can expect to see an increasing number of NMR structural studies of biologically active RNAs.

  19. Ligand-receptor Interactions by NMR Spectroscopy

    Novak. P.

    2008-04-01

    Full Text Available Today NMR spectroscopy is a method of choice for elucidation of interactions between biomolecules and the potential ligands. Knowledge on these interactions is an essential prerequisite for the rational drug design. The most important contribution of NMR to drug design a few years ago was the 3D structure determination of proteins. Besides delivering the 3D structures of the free proteins as a raw material for the modeling studies on ligand binding, NMR can directly yield valuable experimental data on the biologically important protein-ligand complexes. In addition to X-ray diffraction, NMR spectroscopy can provide information on the internal protein dynamics ordynamics of intermolecular interactions. Changes in NMR parameters allow us to detect ("SAR by NMR" and quantitatively determine binding affinities (titration, diffusion NMR experiments, etc. of potential ligands. Also, it is possible to determine the binding site and conformations of ligands, receptors and receptor-ligand complexes with the help of NMR methods such as tr-NOESY. Epitopes or functional groups responsible for binding of ligands to the receptor can be identified by employing STD or WaterLOGSY experiments. In this review are described some of the most frequent NMR methods for the characterization of the interactions between biomolecules and ligands, together with their advantages and disadvantages.

  20. NMR exposure sensitizes tumor cells to apoptosis.

    Ghibelli, L; Cerella, C; Cordisco, S; Clavarino, G; Marazzi, S; De Nicola, M; Nuccitelli, S; D'Alessio, M; Magrini, A; Bergamaschi, A; Guerrisi, V; Porfiri, L M

    2006-03-01

    NMR technology has dramatically contributed to the revolution of image diagnostic. NMR apparatuses use combinations of microwaves over a homogeneous strong (1 Tesla) static magnetic field. We had previously shown that low intensity (0.3-66 mT) static magnetic fields deeply affect apoptosis in a Ca2+ dependent fashion (Fanelli et al., 1999 FASEBJ., 13;95-102). The rationale of the present study is to examine whether exposure to the static magnetic fields of NMR can affect apoptosis induced on reporter tumor cells of haematopoietic origin. The impressive result was the strong increase (1.8-2.5 fold) of damage-induced apoptosis by NMR. This potentiation is due to cytosolic Ca2+ overload consequent to NMR-promoted Ca2+ influx, since it is prevented by intracellular (BAPTA-AM) and extracellular (EGTA) Ca2+ chelation or by inhibition of plasma membrane L-type Ca2+ channels. Three-days follow up of treated cultures shows that NMR decrease long term cell survival, thus increasing the efficiency of cytocidal treatments. Importantly, mononuclear white blood cells are not sensitised to apoptosis by NMR, showing that NMR may increase the differential cytotoxicity of antitumor drugs on tumor vs normal cells. This strong, differential potentiating effect of NMR on tumor cell apoptosis may have important implications, being in fact a possible adjuvant for antitumor therapies. PMID:16528477

  1. Spin-Exchange Pumped NMR Gyros

    Walker, Thad G

    2016-01-01

    We present the basic theory governing spin-exchange pumped NMR gyros. We review the basic physics of spin-exchange collisions and relaxation as they pertain to precision NMR. We present a simple model of operation as an NMR oscillator and use it to analyze the dynamic response and noise properties of the oscillator. We discuss the primary systematic errors (differential alkali fields, quadrupole shifts, and offset drifts) that limit the bias stability, and discuss methods to minimize them. We give with a brief overview of a practical implementation and performance of an NMR gyro built by Northrop-Grumman Corporation, and conclude with some comments about future prospects.

  2. Advance reservoir evaluation by using NMR logging

    Based on brief explanation of the measurement principle for nuclear magnetic resonance (NMR) logging, this paper illustrates the importance of NMR logging in reservoir evaluation through typical case examples. These case examples include: Reservoir characterization and productivity evaluation by using NMR logging, determination of reservoir porosity in complex lithology, identification of oil, water and gas zones under complex reservoir conditions where resistivity log data give poor indication, guiding the implementation of completion and drilling programs, etc. Excellent application results indicate that NMR logging has its special features and advantages in comparison with conventional logging techniques. It is a very practical and very promising logging technology

  3. NMR characterization of pituitary tumors

    Twelve patients (5 male, 7 female, mean age 37.9 +- 20) with pituitary tumors were extensively evaluated with NMR imaging using a 1.5K gauss resistive magnet. Saturation recovery (SR), inversion recovery (IR) and spin echo (SE) pulse sequences were used for qualitative characterization of the lesions. T/sub 1/ calculations were also performed for brain and pituitary. Tumor histology and endocrine status were correlated with NMR data. All tumors were large with suprasellar extension (6 with prolactin secretion, 6 without). Pituitary T/sub 1/'s ranged from .2 to .64, the mean T/sub 1/ being longer than that of brain (Brain = .4 +- .04; Pit = .48 +- .14). 3 patients with histological evidence of homogeneous adenomas had long T/sub 1/'s (0.58 +- .05). 3 patients with evidence of recent or old hemorhage into the pituitary had much shorter T/sub 1/'s (0.29 +- .12). There was no relationship between prolactin secretion and T/sub 1/. Qualitative T/sub 1/ and T/sub 2/ information can be obtained by using a combination of SR, IR, and SE images. Using this method in the patients, homogeneous adenomas had similar T/sub 1/'s and longer T/sub 2/'s compared to the brain, while patients with bleeds had shorter T/sub 1/'s and T/sub 2/'s. Image T/sub 1/ characteristics correlated well with the calculated T/sub 1/ values. The range of T/sub 1/ (and potentially T/sub 2/) values which occur in apparently similar lesions are most likely due to anatomical and pathophysiological variations in these lesions. It may be ultimately possible to separate different types of pathological processes based on NMR image T/sub 1/ and T/sub 2/ characteristics after careful comparative studies of NMR and histological data are completed. The combination of calculated T/sub 1/ and T/sub 2/ with image T/sub 1/ and T/sub 2/ information may also be useful in further characterization of lesions

  4. NMR investigation of Ag nanoparticles

    Son, Kwanghyo; Jang, Zeehoon

    2013-01-01

    109Ag nuclear magnetic resonance (NMR) and relaxation measurements have been performed on two powder samples of Ag nanoparticles with average sizes of 20 nm and 80 nm. The measurements have been done in an external field of 9.4 T and in the temperature range 10 K Knight shift ( K) and the nuclear spin-lattice relaxation rate (1/ T 1) are observed to be almost identical to the values reported for the bulk Ag metal, whereby the Korringa ratio R(= K 2 T 1 T/S) is found to be 2.0 for both samples in the investigated temperature range.

  5. Combined Environment Acoustic Chamber (CEAC)

    Federal Laboratory Consortium — Purpose: The CEAC imposes combined acoustic, thermal and mechanical loads on aerospace structures. The CEAC is employed to measure structural response and determine...

  6. Truck acoustic data analyzer system

    Haynes, Howard D.; Akerman, Alfred; Ayers, Curtis W.

    2006-07-04

    A passive vehicle acoustic data analyzer system having at least one microphone disposed in the acoustic field of a moving vehicle and a computer in electronic communication the microphone(s). The computer detects and measures the frequency shift in the acoustic signature emitted by the vehicle as it approaches and passes the microphone(s). The acoustic signature of a truck driving by a microphone can provide enough information to estimate the truck speed in miles-per-hour (mph), engine speed in rotations-per-minute (RPM), turbocharger speed in RPM, and vehicle weight.

  7. Acoustic transparency and slow sound using detuned acoustic resonators

    Santillan, Arturo Orozco; Bozhevolnyi, Sergey I.

    2011-01-01

    We demonstrate that the phenomenon of acoustic transparency and slowsound propagation can be realized with detuned acoustic resonators (DAR), mimicking thereby the effect of electromagnetically induced transparency (EIT) in atomic physics. Sound propagation in a pipe with a series of side...

  8. Ares I Scale Model Acoustic Test Lift-Off Acoustics

    Counter, Douglas D.; Houston, Janie D.

    2011-01-01

    The lift-off acoustic (LOA) environment is an important design factor for any launch vehicle. For the Ares I vehicle, the LOA environments were derived by scaling flight data from other launch vehicles. The Ares I LOA predicted environments are compared to the Ares I Scale Model Acoustic Test (ASMAT) preliminary results.

  9. NMR studies of oriented molecules

    Sinton, S.W.

    1981-11-01

    Deuterium and proton magnetic resonance are used in experiments on a number of compounds which either form liquid crystal mesophases themselves or are dissolved in a liquid crystal solvent. Proton multiple quantum NMR is used to simplify complicated spectra. The theory of nonselective multiple quantum NMR is briefly reviewed. Benzene dissolved in a liquid crystal are used to demonstrate several outcomes of the theory. Experimental studies include proton and deuterium single quantum (..delta..M = +-1) and proton multiple quantum spectra of several molecules which contain the biphenyl moiety. 4-Cyano-4'-n-pentyl-d/sub 11/-biphenyl (5CB-d/sub 11/) is studied as a pure compound in the nematic phase. The obtained chain order parameters and dipolar couplings agree closely with previous results. Models for the effective symmetry of the biphenyl group in 5CB-d/sub 11/ are tested against the experimental spectra. The dihedral angle, defined by the planes containing the rings of the biphenyl group, is found to be 30 +- 2/sup 0/ for 5DB-d/sub 11/. Experiments are also described for 4,4'-d/sub 2/-biphenyl, 4,4' - dibromo-biphenyl, and unsubstituted biphenyl.

  10. Acoustic Mechanical Feedthroughs

    Sherrit, Stewart; Walkemeyer, Phillip; Bao, Xiaoqi; Bar-Cohen, Yoseph; Badescu, Mircea

    2013-01-01

    Electromagnetic motors can have problems when operating in extreme environments. In addition, if one needs to do mechanical work outside a structure, electrical feedthroughs are required to transport the electric power to drive the motor. In this paper, we present designs for driving rotary and linear motors by pumping stress waves across a structure or barrier. We accomplish this by designing a piezoelectric actuator on one side of the structure and a resonance structure that is matched to the piezoelectric resonance of the actuator on the other side. Typically, piezoelectric motors can be designed with high torques and lower speeds without the need for gears. One can also use other actuation materials such as electrostrictive, or magnetostrictive materials in a benign environment and transmit the power in acoustic form as a stress wave and actuate mechanisms that are external to the benign environment. This technology removes the need to perforate a structure and allows work to be done directly on the other side of a structure without the use of electrical feedthroughs, which can weaken the structure, pipe, or vessel. Acoustic energy is pumped as a stress wave at a set frequency or range of frequencies to produce rotary or linear motion in a structure. This method of transferring useful mechanical work across solid barriers by pumping acoustic energy through a resonant structure features the ability to transfer work (rotary or linear motion) across pressure or thermal barriers, or in a sterile environment, without generating contaminants. Reflectors in the wall of barriers can be designed to enhance the efficiency of the energy/power transmission. The method features the ability to produce a bi-directional driving mechanism using higher-mode resonances. There are a variety of applications where the presence of a motor is complicated by thermal or chemical environments that would be hostile to the motor components and reduce life and, in some instances, not be

  11. Taming Acoustic Cavitation

    Rivas, David Fernandez; Enriquez, Oscar R; Versluis, Michel; Prosperetti, Andrea; Gardeniers, Han; Lohse, Detlef

    2012-01-01

    In this fluid dynamics video we show acoustic cavitation occurring from pits etched on a silicon surface. By immersing the surface in a liquid, gas pockets are entrapped in the pits which upon ultrasonic insonation, are observed to shed cavitation bubbles. Modulating the driving pressure it is possible to induce different behaviours based on the force balance that determines the interaction among bubbles and the silicon surface. This system can be used for several applications like sonochemical water treatment, cleaning of surfaces with deposited materials such as biofilms.

  12. Dynamic acoustic tractor beams

    Mitri, F. G.

    2015-03-01

    Pulling a sphere and vibrating it around an equilibrium position by amplitude-modulation in the near-field of a single finite circular piston transducer is theoretically demonstrated. Conditions are found where a fluid hexane sphere (with arbitrary radius) chosen as an example, centered on the axis of progressive propagating waves and submerged in non-viscous water, experiences an attractive (steady) force pulling it towards the transducer, as well as an oscillatory force forcing it to vibrate back-and-forth. Numerical predictions for the dynamic force illustrate the theory and suggest an innovative method in designing dynamic acoustical tractor beams.

  13. Dynamic acoustic tractor beams

    Mitri, F. G., E-mail: F.G.Mitri@ieee.org [Chevron, Area 52 Technology – ETC, Santa Fe, New Mexico 87508 (United States)

    2015-03-07

    Pulling a sphere and vibrating it around an equilibrium position by amplitude-modulation in the near-field of a single finite circular piston transducer is theoretically demonstrated. Conditions are found where a fluid hexane sphere (with arbitrary radius) chosen as an example, centered on the axis of progressive propagating waves and submerged in non-viscous water, experiences an attractive (steady) force pulling it towards the transducer, as well as an oscillatory force forcing it to vibrate back-and-forth. Numerical predictions for the dynamic force illustrate the theory and suggest an innovative method in designing dynamic acoustical tractor beams.

  14. Lecture Notes On Acoustics

    This book mentions string vibration and wave, one-dimension wave and wave equation, characteristic impedance, governing equation of string, and wave energy from string, wave equation of wave and basic physical quantity like one-dimension wave equation, sound unit, sound intensity and energy, sound movement in a surface of discontinuity with transmission loss of sound by partition, and Snell's law, radiation, scatter and diffraction and sound in closed space with Sabine's theory, sound characteristic of closed space and duct acoustics.

  15. A Guided Inquiry Approach to NMR Spectroscopy

    Parmentier, Laura E.; Lisensky, George C.; Spencer, Brock

    1998-04-01

    We present a novel way to introduce NMR spectroscopy into the general chemistry curriculum as part of a week-long aspirin project in our one-semester introductory course. Aspirin is synthesized by reacting salicylic acid and acetic anhydride. Purity is determined by titration and IR and NMR spectroscopy. Students compare IR and NMR spectra of their aspirin product to a series of reference spectra obtained by the class. Students are able to interpret the IR spectra of their aspirin using IR data from previous experiments. NMR is introduced by having students collect 1H NMR spectra of a series of reference compounds chosen to include some of the structural features of aspirin and compare spectra and structures of the reference compounds to develop a correlation chart for chemical shifts. This process is done in small groups using shared class data and is guided by a series of questions designed to relate the different kinds of hydrogen atoms to number and position of peaks in the NMR spectrum. Students then identify the peaks in the NMR spectrum of their aspirin product and relate percent purity by titration with spectral results and percent yield. This is an enjoyable project that combines the synthesis of a familiar material with a guided inquiry-based introduction to NMR spectroscopy.

  16. NMR spectra of phosphorus 17O esters

    By the 17O NMR method the authors investigated methyl, ethyl, isopropyl, tert-butyl, and phenyl ethylene phosphites; methyl, ethyl, and isopropyl trimethylene phosphites; and methyl, ethyl, isopropyl, and tert-butyl o-phenylene phosphites. They also determined the 13C and 31P NMR spectra of these compounds

  17. 2D NMR studies of biomolecules

    The work described in this thesis comprises two related subjects. The first part describes methods to derive high-resolution structures of proteins in solution using two-dimensional (2-D) NMR. The second part describes 2-D NMR studies on the interaction between proteins and DNA. (author). 261 refs.; 52 figs.; 23 tabs

  18. NMR Spectroscopy and Its Value: A Primer

    Veeraraghavan, Sudha

    2008-01-01

    Nuclear magnetic resonance (NMR) spectroscopy is widely used by chemists. Furthermore, the use of NMR spectroscopy to solve structures of macromolecules or to examine protein-ligand interactions is popular. Yet, few students entering graduate education in biological sciences have been introduced to this method or its utility. Over the last six…

  19. An Inversion Recovery NMR Kinetics Experiment

    Williams, Travis J.; Kershaw, Allan D.; Li, Vincent; Wu, Xinping

    2011-01-01

    A convenient laboratory experiment is described in which NMR magnetization transfer by inversion recovery is used to measure the kinetics and thermochemistry of amide bond rotation. The experiment utilizes Varian spectrometers with the VNMRJ 2.3 software, but can be easily adapted to any NMR platform. The procedures and sample data sets in this…

  20. Using Cloud Storage for NMR Data Distribution

    Soulsby, David

    2012-01-01

    An approach using Google Groups as method for distributing student-acquired NMR data has been implemented. We describe how to configure NMR spectrometer software so that data is uploaded to a laboratory section specific Google Group, thereby removing bottlenecks associated with printing and processing at the spectrometer workstation. Outside of…

  1. Early history of NMR at Los Alamos

    Nuclear magnetic resonance (NMR) spectroscopy has developed into an important research tool in chemistry. More recently, NMR imaging and in vivo spectroscopy promise to produce a revolution in medicine and biochemistry. Early experiments at Los Alamos led to DOE programs involving stable isotopes of importance to biology and to medicine. These events are briefly recounted. 2 refs

  2. Acoustic Center or Time Origin?

    Staffeldt, Henrik

    1999-01-01

    The paper discusses the acoustic center in relation to measurements of loudspeaker polar data. Also, it presents the related concept time origin and discusses the deviation that appears between positions of the acoustic center found by wavefront based and time based measuring methods....

  3. Propagation of Ion Acoustic Perturbations

    Pécseli, Hans

    1975-01-01

    Equations describing the propagation of ion acoustic perturbations are considered, using the assumption that the electrons are Boltzman distributed and isothermal at all times. Quasi-neutrality is also considered.......Equations describing the propagation of ion acoustic perturbations are considered, using the assumption that the electrons are Boltzman distributed and isothermal at all times. Quasi-neutrality is also considered....

  4. Acoustic engineering and technology '90

    Acoustic monitoring, testing and diagnosis in machines, production processes and products enhance the uptimes and profitability of machinery and plants. 18 papers discuss the current state of the art of acoustic monitoring systems including integrated factory planning as well as industrial health, and noise protection. (DG)

  5. Acoustic Metamaterials and Phononic Crystals

    2013-01-01

    This comprehensive book presents all aspects of acoustic metamaterials and phononic crystals. The emphasis is on acoustic wave propagation phenomena at interfaces such as refraction, especially unusual refractive properties and negative refraction. A thorough discussion of the mechanisms leading to such refractive phenomena includes local resonances in metamaterials and scattering in phononic crystals.

  6. Digital Controller For Acoustic Levitation

    Tarver, D. Kent

    1989-01-01

    Acoustic driver digitally controls sound fields along three axes. Allows computerized acoustic levitation and manipulation of small objects for such purposes as containerless processing and nuclear-fusion power experiments. Also used for controlling motion of vibration-testing tables in three dimensions.

  7. MEMS Based Acoustic Array

    Sheplak, Mark (Inventor); Nishida, Toshikaza (Inventor); Humphreys, William M. (Inventor); Arnold, David P. (Inventor)

    2006-01-01

    Embodiments of the present invention described and shown in the specification aid drawings include a combination responsive to an acoustic wave that can be utilized as a dynamic pressure sensor. In one embodiment of the present invention, the combination has a substrate having a first surface and an opposite second surface, a microphone positioned on the first surface of the substrate and having an input and a first output and a second output, wherein the input receives a biased voltage, and the microphone generates an output signal responsive to the acoustic wave between the first output and the second output. The combination further has an amplifier positioned on the first surface of the substrate and having a first input and a second input and an output, wherein the first input of the amplifier is electrically coupled to the first output of the microphone and the second input of the amplifier is electrically coupled to the second output of the microphone for receiving the output sinual from the microphone. The amplifier is spaced from the microphone with a separation smaller than 0.5 mm.

  8. Acoustics and Hearing

    Damaske, Peter

    2008-01-01

    When one listens to music at home, one would like to have an acoustic impression close to that of being in the concert hall. Until recently this meant elaborate multi-channelled sound systems with 5 or more speakers. But head-related stereophony achieves the surround-sound effect in living rooms with only two loudspeakers. By virtue of their slight directivity as well as an electronic filter the limitations previously common to two-speaker systems can be overcome and this holds for any arbitrary two-channel recording. The book also investigates the question of how a wide and diffuse sound image can arise in concert halls and shows that the quality of concert halls decisively depends on diffuse sound images arising in the onset of reverberation. For this purpose a strong onset of reverberation is modified in an anechoic chamber by electroacoustic means. Acoustics and Hearing proposes ideas concerning signal processing in the auditory system that explain the measured results and the resultant sound effects plea...

  9. Musical acoustics demonstrations

    Hoekje, P. L.

    2003-10-01

    The ASA Musical Acoustics Demonstrations website (trial version at http://www.bw.edu/~phoekje) includes sound files, video clips, program code listings, and other material for demonstrations related to musical acoustics. Many of the sound demonstrations may be experienced either as expositions, in which the phenomena are explained before they are presented, or as experiments, in which the explanation comes after listeners have had the opportunity to draw their own conclusions. Suggestions are provided for apparatus construction and classroom experiments, as well as for building simple musical instruments. Software is recommended if it is available free and compatible with multiple personal computer operating systems. For example, Audacity (http://audacity.sourceforce.net) is a sound file editor and analyzer that can be used to visually represent sounds and manipulate them. Source files are included for the synthesized sound examples, which were created in Csound (http://csounds.com), so that interested users may create their own variations. Source code is also included for visual demonstrations created in Visual Python and Python (http://www.python.org), an efficient, high level programming language. Suggestions, criticisms, and contributions are always welcome! [Work supported by ASA and Baldwin-Wallace College.

  10. Time-reversal acoustics

    Fink, Mathias [Laboratoire Ondes et Acoustique, Ecole Superieure de Physique et de Chimie Industrielle de la Ville de Paris, Universite Denis Diderot, UMR CNRS 7587, 10 Rue Vauquelin, 75005 Paris (France)], E-mail: mathias.fink@espci.fr

    2008-10-15

    Time-reversal mirrors (TRMs) refocus an incident acoustic field to the position of the original source regardless of the complexity of the propagation medium. TRM's have now been implemented in a variety of physical scenarios from MHz ultrasonics with order centimeter aperture size to hundreds/thousands of Hz in ocean acoustics with order hundred meter aperture size. Common to this broad range of scales is a remarkable robustness exemplified by observations at all scales that the more complex the medium between the probe source and the TRM, the sharper the focus. The relation between the medium complexity and the size of the focal spot is studied in this paper. It is certainly the most exciting property of TRM compared to standard focusing devices. A TRM acts as an antenna that uses complex environments to appears wider than it is, resulting for a broadband pulse in a refocusing quality that does not depend of the TRM aperture. In this paper, we investigate the time-reversal approach in various media of increasing complexity and we discuss the link existing between time-reversal approach and local helioseismology where Green's functions can be extracted from diffusive noise.

  11. Acoustic Absorption in Porous Materials

    Kuczmarski, Maria A.; Johnston, James C.

    2011-01-01

    An understanding of both the areas of materials science and acoustics is necessary to successfully develop materials for acoustic absorption applications. This paper presents the basic knowledge and approaches for determining the acoustic performance of porous materials in a manner that will help materials researchers new to this area gain the understanding and skills necessary to make meaningful contributions to this field of study. Beginning with the basics and making as few assumptions as possible, this paper reviews relevant topics in the acoustic performance of porous materials, which are often used to make acoustic bulk absorbers, moving from the physics of sound wave interactions with porous materials to measurement techniques for flow resistivity, characteristic impedance, and wavenumber.

  12. Acoustic monitoring method and device

    The present invention provides a method of eliminating resonance noises upon acoustically monitoring the operation state of power plants and plant equipments whether they are normal or not, to improve sensitivity for detecting abnormalities. Namely, a microphone detects acoustic signals including leaking sounds and converts them into electric signals. An amplifier amplifies the electric signals to an appropriate level. A noise eliminating section eliminates resonance noises other than the leaking sounds. An abnormality judging section judges presence of abnormality based on the level of the acoustic signals of the leaking sounds. With such a constitution, a plurality of resonance noises generated also during normal plant operation are automatically eliminated. Since resonance noises as a factor of lowering the sensitivity for abnormal sound detection are not included in the acoustic signals, the sensitivity for the abnormal sound detection is improved. Accordingly, the performance of the acoustic monitoring device is improved. (I.S.)

  13. Carbon-13 NMR spectroscopy of biological systems

    Beckmann, Nicolau

    1995-01-01

    This book is intended to provide an in-depth understanding of 13C NMR as a tool in biological research. 13C NMR has provided unique information concerning complex biological systems, from proteins and nucleic acids to animals and humans. The subjects addressed include multidimensional heteronuclear techniques for structural studies of molecules in the liquid and solid states, the investigation of interactions in model membranes, the elucidation of metabolic pathwaysin vitro and in vivo on animals, and noninvasive metabolic studies performed on humans. The book is a unique mix of NMR methods and biological applications which makes it a convenient reference for those interested in research in this interdisciplinary area of physics, chemistry, biology, and medicine.Key Features* An interdisciplinary text with emphasis on both 13C NMR methodology and the relevant biological and biomedical issues* State-of-the-art 13C NMR techniques are described; Whenever possible, their advantages over other approaches are empha...

  14. Applications of NMR spectroscopy to systems biochemistry.

    Fan, Teresa W-M; Lane, Andrew N

    2016-02-01

    The past decades of advancements in NMR have made it a very powerful tool for metabolic research. Despite its limitations in sensitivity relative to mass spectrometric techniques, NMR has a number of unparalleled advantages for metabolic studies, most notably the rigor and versatility in structure elucidation, isotope-filtered selection of molecules, and analysis of positional isotopomer distributions in complex mixtures afforded by multinuclear and multidimensional experiments. In addition, NMR has the capacity for spatially selective in vivo imaging and dynamical analysis of metabolism in tissues of living organisms. In conjunction with the use of stable isotope tracers, NMR is a method of choice for exploring the dynamics and compartmentation of metabolic pathways and networks, for which our current understanding is grossly insufficient. In this review, we describe how various direct and isotope-edited 1D and 2D NMR methods can be employed to profile metabolites and their isotopomer distributions by stable isotope-resolved metabolomic (SIRM) analysis. We also highlight the importance of sample preparation methods including rapid cryoquenching, efficient extraction, and chemoselective derivatization to facilitate robust and reproducible NMR-based metabolomic analysis. We further illustrate how NMR has been applied in vitro, ex vivo, or in vivo in various stable isotope tracer-based metabolic studies, to gain systematic and novel metabolic insights in different biological systems, including human subjects. The pathway and network knowledge generated from NMR- and MS-based tracing of isotopically enriched substrates will be invaluable for directing functional analysis of other 'omics data to achieve understanding of regulation of biochemical systems, as demonstrated in a case study. Future developments in NMR technologies and reagents to enhance both detection sensitivity and resolution should further empower NMR in systems biochemical research. PMID:26952191

  15. NMR-based milk metabolomics

    Sundekilde, Ulrik; Larsen, Lotte Bach; Bertram, Hanne Christine S.

    2013-01-01

    Milk is a key component in infant nutrition worldwide and, in the Western parts of the world, also in adult nutrition. Milk of bovine origin is both consumed fresh and processed into a variety of dairy products including cheese, fermented milk products, and infant formula. The nutritional quality...... and processing capabilities of bovine milk is closely associated to milk composition. Metabolomics is ideal in the study of the low-molecular-weight compounds in milk, and this review focuses on the recent nuclear magnetic resonance (NMR)-based metabolomics trends in milk research, including...... applications linking the milk metabolite profiling with nutritional aspects, and applications which aim to link the milk metabolite profile to various technological qualities of milk. The metabolite profiling studies encompass the identification of novel metabolites, which potentially can be used as biomarkers...

  16. PORTABLE ACOUSTIC MONITORING PACKAGE (PAMP)

    John L. Loth; Gary J. Morris; George M. Palmer; Richard Guiler; Patrick Browning

    2004-07-20

    The Portable Acoustic Monitoring Package (PAMP) has been designed to record and monitor the acoustic signal in natural gas transmission lines. In particular the three acoustic signals associated with a line leak. The system is portable ({approx}30 lbs) and is designed for line pressures up to 1000 psi. It has become apparent that cataloging of the various background acoustic signals in natural gas transmission line is very important if a system to identify leak signals is to be developed. The low-pressure (0-200 psig) laboratory test phase has been completed and a number of field trials have been conducted. Before the cataloging phase could begin, a few problems identified in field trials identified had to be corrected such as: (1) Decreased microphone sensitivity at line pressures above 250 psig. (2) The inability to deal with large data sets collected when cataloging the variety of signals in a transmission line. (3) The lack of an available online acoustic calibration system. These problems have been solved and the WVU PAMP is now fully functional over the entire pressure range found in the Natural Gas transmission lines in this region. Field portability and reliability have been greatly improved. Data collection and storage have also improved to the point were the full acoustic spectrum of acoustic signals can be accurately cataloged, recorded and described.

  17. Controlling sound with acoustic metamaterials

    Cummer, Steven A.; Christensen, Johan; Alù, Andrea

    2016-03-01

    Acoustic metamaterials can manipulate and control sound waves in ways that are not possible in conventional materials. Metamaterials with zero, or even negative, refractive index for sound offer new possibilities for acoustic imaging and for the control of sound at subwavelength scales. The combination of transformation acoustics theory and highly anisotropic acoustic metamaterials enables precise control over the deformation of sound fields, which can be used, for example, to hide or cloak objects from incident acoustic energy. Active acoustic metamaterials use external control to create effective material properties that are not possible with passive structures and have led to the development of dynamically reconfigurable, loss-compensating and parity-time-symmetric materials for sound manipulation. Challenges remain, including the development of efficient techniques for fabricating large-scale metamaterial structures and converting laboratory experiments into useful devices. In this Review, we outline the designs and properties of materials with unusual acoustic parameters (for example, negative refractive index), discuss examples of extreme manipulation of sound and, finally, provide an overview of future directions in the field.

  18. NMR in solid ionic and nanoionics

    Full text: Nuclear Magnetic Resonance (NMR) is a spectroscopic technique which employs magnetic nuclei to study, among others, the dynamics of condensed matter at the atomic level. Thus, NMR has been and still is a successful instrument in the research field of solid electrolytes also known as solid ionics. This paper presents the typical NMR experiments performed in solid ionics together with some examples from nanoionics. The experiments to be discussed comprise: (i) measurements of the diffusion coefficient employing the pulsed-field gradient and the static fringe-field method; (ii) the experimentally related NMR imaging; (iii) double resonance experiments like spin-echo double resonance (SEDOR) and two-dimensional Fourier transform NMR (2D-FT NMR); (iv) various types of nuclear relaxation, in particular spin-lattice relaxation. The NMR techniques yield information on topics like the following: type and number of mobile atoms and defects, diffusion pathways (e.g. dimensionality restrictions), atomic jump frequencies, activation energy and activation volume of these movements, diffusion coefficient with activation energy and prefactor, correlation effects in atomic movements, space correlation factor, cooperative phenomena, symmetry of atomic sites, behavior at phase transitions. These applications will be illustrated by giving examples from crystals, glasses, and polymers. (author)

  19. Surface Acoustic Wave Devices

    Dühring, Maria Bayard

    The work of this project is concerned with the simulation of surface acoustic waves (SAW) and topology optimization of SAW devices. SAWs are elastic vibrations that propagate along a material surface and are extensively used in electromechanical filters and resonators in telecommunication. A new...... application is modulation of optical waves in waveguides. This presentation elaborates on how a SAW is generated by interdigital transducers using a 2D model of a piezoelectric, inhomogeneous material implemented in the high-level programming language Comsol Multiphysics. The SAW is send through a model of a...... output waveguide and the MZI can thus be used as an optical switch. It is explained how the mechanical model of the SAW is coupled to a model of the optical waves such that the change in effective refractive index introduced in the MZI arms by the SAW can be calculated. Results of a parameter study of...

  20. Evoked acoustic emission

    Elberling, C; Parbo, J; Johnsen, N J;

    1985-01-01

    Stimulated acoustic emissions were recorded in response to tonal stimuli at 60 dB p.e. SPL in a small group of normal-hearing adults. Power spectral analysis reveals that the evoked activity from each ear contains energy in preferential frequency bands and the change of stimulus frequency has only...... a minor effect on the power spectra, i.e. the maximum jumps from one spectral peak to another. Experiments with deconvolution demonstrate that the emission generating system at least at a fixed intensity can be regarded as being linear and characterized by its impulse response which is similar to...... the emission evoked by click stimuli. It is concluded that significant information is obtained by the click rather than by the tonal stimuli. The click-evoked emissions were also recorded from both ears in a consecutive series of 100 full-term and otherwise normal babies 2-4 days after birth. The...

  1. Acoustic emission testing

    Grosse, Christian U

    2008-01-01

    Acoustic Emission (AE) techniques have been studied in civil engineering for a long time. The techniques are recently going to be more and more applied to practical applications and to be standardized in the codes. This is because the increase of aging structures and disastrous damages due to recent earthquakes urgently demand for maintenance and retrofit of civil structures in service for example. It results in the need for the development of advanced and effective inspection techniques. Thus, AE techniques draw a great attention to diagnostic applications and in material testing. The book covers all levels from the description of AE basics for AE beginners (level of a student) to sophisticated AE algorithms and applications to real large-scale structures as well as the observation of the cracking process in laboratory specimen to study fracture processes.

  2. Acoustic fault injection tool (AFIT)

    Schoess, Jeffrey N.

    1999-05-01

    On September 18, 1997, Honeywell Technology Center (HTC) successfully completed a three-week flight test of its rotor acoustic monitoring system (RAMS) at Patuxent River Flight Test Center. This flight test was the culmination of an ambitious 38-month proof-of-concept effort directed at demonstrating the feasibility of detecting crack propagation in helicopter rotor components. The program was funded as part of the U.S. Navy's Air Vehicle Diagnostic Systems (AVDS) program. Reductions in Navy maintenance budgets and available personnel have dictated the need to transition from time-based to 'condition-based' maintenance. Achieving this will require new enabling diagnostic technologies. The application of acoustic emission for the early detection of helicopter rotor head dynamic component faults has proven the feasibility of the technology. The flight-test results demonstrated that stress-wave acoustic emission technology can detect signals equivalent to small fatigue cracks in rotor head components and can do so across the rotating articulated rotor head joints and in the presence of other background acoustic noise generated during flight operation. During the RAMS flight test, 12 test flights were flown from which 25 Gbyte of digital acoustic data and about 15 hours of analog flight data recorder (FDR) data were collected from the eight on-rotor acoustic sensors. The focus of this paper is to describe the CH-46 flight-test configuration and present design details about a new innovative machinery diagnostic technology called acoustic fault injection. This technology involves the injection of acoustic sound into machinery to assess health and characterize operational status. The paper will also address the development of the Acoustic Fault Injection Tool (AFIT), which was successfully demonstrated during the CH-46 flight tests.

  3. An introduction to biological NMR spectroscopy

    NMR spectroscopy is a powerful tool for biologists interested in the structure, dynamics, and interactions of biological macromolecules. This review aims at presenting in an accessible manner the requirements and limitations of this technique. As an introduction, the history of NMR will highlight how the method evolved from physics to chemistry and finally to biology over several decades. We then introduce the NMR spectral parameters used in structural biology, namely the chemical shift, the J-coupling, nuclear Overhauser effects, and residual dipolar couplings. Resonance assignment, the required step for any further NMR study, bears a resemblance to jigsaw puzzle strategy. The NMR spectral parameters are then converted into angle and distances and used as input using restrained molecular dynamics to compute a bundle of structures. When interpreting a NMR-derived structure, the biologist has to judge its quality on the basis of the statistics provided. When the 3D structure is a priori known by other means, the molecular interaction with a partner can be mapped by NMR: information on the binding interface as well as on kinetic and thermodynamic constants can be gathered. NMR is suitable to monitor, over a wide range of frequencies, protein fluctuations that play a crucial role in their biological function. In the last section of this review, intrinsically disordered proteins, which have escaped the attention of classical structural biology, are discussed in the perspective of NMR, one of the rare available techniques able to describe structural ensembles. This Tutorial is part of the International Proteomics Tutorial Programme (IPTP 16 MCP). (authors)

  4. An asymptotic model in acoustics:acoustic drift equations

    Vladimirov, Vladimir; Ilin, Konstantin

    2013-01-01

    A rigorous asymptotic procedure with the Mach number as a small parameter is used to derive the equations of mean flows which coexist and are affected by the background acoustic waves in the limit of very high Reynolds number.

  5. Anisotropic spectra of acoustic turbulence

    We found universal anizopropic spectra of acoustic turbulence with the linear dispersion law ω(k)=ck within the framework of generalized kinetic equation which takes into account the finite time of three-wave interactions. This anisotropic spectra can assume both scale-invariant and non-scale-invariant form. The implications for the evolution of the acoustic turbulence with nonisotropic pumping are discussed. The main result of the article is that the spectra of acoustic turbulence tend to become more isotropic. (c) 2000 The American Physical Society

  6. Theoretical acoustics of underwater structures

    Skelton, EA

    1997-01-01

    This important book provides an account of the linear acoustics of basic isotropic/anisotropic structures excited by time-harmonic and transient mechanical forces and acoustic sources. Many numerical examples are given to aid physical insight and to provide benchmark computations of sound radiation and sound scattering. The theoretical methods, developed originally for naval noise control problems, should find civil application in the acoustic modelling of structures fabricated from both fibre-reinforced and isotropic materials. Such an endeavour is increasingly desirable and necessary in this

  7. Acoustic metamaterial with negative density

    We fabricated a one-dimensional acoustic metamaterial with negative effective density using an array of very thin elastic membranes. We observed acoustic equivalence of the plasma oscillation at ωc=735 Hz. The metamaterial was opaque in the frequency range from 0 to 735 Hz, and was transparent above 735 Hz. We report direct observation of negative acceleration in this acoustic medium below 735 Hz. The frequency characteristics of the metamaterial have the same form as that of metals with negative permittivity. We also provide a simple theory to explain the experimental results.

  8. Noise Shielding Using Acoustic Metamaterials

    We exploit theoretically a class of rectangular cylindrical devices for noise shielding by using acoustic metamaterials. The function of noise shielding is justified by both the far-field and near-field full-wave simulations based on the finite element method. The enlargement of equivalent acoustic scattering cross sections is revealed to be the physical mechanism for this function. This work makes it possible to design a window with both noise shielding and air flow. (electromagnetism, optics, acoustics, heat transfer, classical mechanics, and fluid dynamics)

  9. Acoustic metamaterial with negative modulus

    We present experimental and theoretical results on an acoustic metamaterial that exhibits a negative effective modulus in a frequency range from 0 to 450 Hz. A one-dimensional acoustic metamaterial with an array of side holes on a tube was fabricated. We observed that acoustic waves above 450 Hz propagated well in this structure, but no sound below 450 Hz passed through. The frequency characteristics of the metamaterial has the same form as that of the permittivity in metals due to the plasma oscillation. We also provide a theory to explain the experimental results.

  10. Graphical programming for pulse automated NMR experiments

    We describe a software program designed to control a broadband pulse Nuclear Magnetic Resonance (NMR) spectrometer used in zero-field NMR studies of magnetic metals. The software is written in the graphical language LabVIEW. This type of programming allows modifications and the inclusion of new routines to be easily made by the non-specialist, without changing the basic structure of the program. The program corrects for differences in the gain of the two acquisition channels [U (phase) and V (quadrature)], and automatic baseline subtraction. We present examples of measurements of NMR spectra, spin-echo decay (T2), and quadrupolar oscillations, performed in magnetic intermetallic compounds. (author)

  11. NMR imaging of the brain: initial impressions

    An NMR imaging system designed and built by Thorn-EMI Ltd was installed at Hammersmith Hospital in March 1981. In the first year of operation 180 patients and 40 volunteers have had cranial examinations and initial impressions bases on this experience are presented. Patients with a wide variety of neurological diseases have been studied to provide a basis for diagnostic interpretation, to define distinctive features, and to evaluate different types of scanning sequences. NMR imaging appears to be of considerable value in neurological diagnosis and has a number of advantages over CT. The detailed evaluation of NMR imaging will require much more work but the initial results are very promising

  12. Acoustic-optic investigations of acoustic gyrotropy in crystals

    For the experimental investigation of the acoustic activity the Bragg light diffraction method on transverse acoustic waves was used in the frequency range 0.4-1.8 GHz. It is shown that the oscillation period of the intensity of the diffracted light is defined by the specific rotator power of the crystal. On the basis of experimental data the specific rotation of the polarization plane in a number of gyrotropic crystals was determined. (authors)

  13. Solid-state NMR of polymers

    Mirau, P

    2001-07-01

    Nuclear magnetic resonance (NMR) spectroscopy has emerged as one of the most important methods for the solid-state characterisation of polymers. The popularity of NMR is due to the fact that many molecular level features can be measured from the NMR spectra, including the polymer chain conformation, the morphology and the dynamics. The spectral features and relaxation times are affected by local interactions, so they provide information about the structure of polymers on a length scale (2-200 A) that is difficult to measure by other methods. In favourable cases, the NMR experiments provide a molecular-level explanation for the transitions observed by differential scanning calorimetry (DSC) and other methods, and the NMR properties can often be related to the bulk properties. Solid-state NMR has long been of interest in polymer science, and the first solid-state NMR studies of polymers were reported approximately a year after the discovery of nuclear resonance in bulk matter. It was reported in this initial study that the proton line width for natural rubber at room temperature is more like that of a mobile liquid than of a solid, but that the resonance broadens near the glass transition temperature (T{sub g}). This was recognised as being related to a change in chain dynamics above and below the T{sub g}. NMR methods developed rapidly after these initial observations, first for polymers in solution and, more recently, for polymers in the solid-state. Solid-state NMR studies of polymers were developed more slowly than their solution-state counterparts because solid-state NMR requires more specialised equipment. Solid-state NMR is now such an important tool that most modern spectrometers are capable of performing these studies. The interest in the NMR of solid polymers is due in part to the fact that most polymers are used in the solid state, and in many cases the NMR properties can be directly related to the macroscopic properties. Polymers have restricted mobility

  14. Solid-state NMR of polymers

    Nuclear magnetic resonance (NMR) spectroscopy has emerged as one of the most important methods for the solid-state characterisation of polymers. The popularity of NMR is due to the fact that many molecular level features can be measured from the NMR spectra, including the polymer chain conformation, the morphology and the dynamics. The spectral features and relaxation times are affected by local interactions, so they provide information about the structure of polymers on a length scale (2-200 A) that is difficult to measure by other methods. In favourable cases, the NMR experiments provide a molecular-level explanation for the transitions observed by differential scanning calorimetry (DSC) and other methods, and the NMR properties can often be related to the bulk properties. Solid-state NMR has long been of interest in polymer science, and the first solid-state NMR studies of polymers were reported approximately a year after the discovery of nuclear resonance in bulk matter. It was reported in this initial study that the proton line width for natural rubber at room temperature is more like that of a mobile liquid than of a solid, but that the resonance broadens near the glass transition temperature (Tg). This was recognised as being related to a change in chain dynamics above and below the Tg. NMR methods developed rapidly after these initial observations, first for polymers in solution and, more recently, for polymers in the solid-state. Solid-state NMR studies of polymers were developed more slowly than their solution-state counterparts because solid-state NMR requires more specialised equipment. Solid-state NMR is now such an important tool that most modern spectrometers are capable of performing these studies. The interest in the NMR of solid polymers is due in part to the fact that most polymers are used in the solid state, and in many cases the NMR properties can be directly related to the macroscopic properties. Polymers have restricted mobility in solids

  15. NMR data-driven structure determination using NMR-I-TASSER in the CASD-NMR experiment

    NMR-I-TASSER, an adaption of the I-TASSER algorithm combining NMR data for protein structure determination, recently joined the second round of the CASD-NMR experiment. Unlike many molecular dynamics-based methods, NMR-I-TASSER takes a molecular replacement-like approach to the problem by first threading the target through the PDB to identify structural templates which are then used for iterative NOE assignments and fragment structure assembly refinements. The employment of multiple templates allows NMR-I-TASSER to sample different topologies while convergence to a single structure is not required. Retroactive and blind tests of the CASD-NMR targets from Rounds 1 and 2 demonstrate that even without using NOE peak lists I-TASSER can generate correct structure topology with 15 of 20 targets having a TM-score above 0.5. With the addition of NOE-based distance restraints, NMR-I-TASSER significantly improved the I-TASSER models with all models having the TM-score above 0.5. The average RMSD was reduced from 5.29 to 2.14 Å in Round 1 and 3.18 to 1.71 Å in Round 2. There is no obvious difference in the modeling results with using raw and refined peak lists, indicating robustness of the pipeline to the NOE assignment errors. Overall, despite the low-resolution modeling the current NMR-I-TASSER pipeline provides a coarse-grained structure folding approach complementary to traditional molecular dynamics simulations, which can produce fast near-native frameworks for atomic-level structural refinement

  16. NMR data-driven structure determination using NMR-I-TASSER in the CASD-NMR experiment

    Jang, Richard [Huazhong University of Science and Technology, School of Software Engineering (China); Wang, Yan [Huazhong University of Science and Technology, School of Life Science and Technology (China); Xue, Zhidong, E-mail: zdxue@hust.edu.cn [Huazhong University of Science and Technology, School of Software Engineering (China); Zhang, Yang, E-mail: zhng@umich.edu [University of Michigan, Department of Computational Medicine and Bioinformatics (United States)

    2015-08-15

    NMR-I-TASSER, an adaption of the I-TASSER algorithm combining NMR data for protein structure determination, recently joined the second round of the CASD-NMR experiment. Unlike many molecular dynamics-based methods, NMR-I-TASSER takes a molecular replacement-like approach to the problem by first threading the target through the PDB to identify structural templates which are then used for iterative NOE assignments and fragment structure assembly refinements. The employment of multiple templates allows NMR-I-TASSER to sample different topologies while convergence to a single structure is not required. Retroactive and blind tests of the CASD-NMR targets from Rounds 1 and 2 demonstrate that even without using NOE peak lists I-TASSER can generate correct structure topology with 15 of 20 targets having a TM-score above 0.5. With the addition of NOE-based distance restraints, NMR-I-TASSER significantly improved the I-TASSER models with all models having the TM-score above 0.5. The average RMSD was reduced from 5.29 to 2.14 Å in Round 1 and 3.18 to 1.71 Å in Round 2. There is no obvious difference in the modeling results with using raw and refined peak lists, indicating robustness of the pipeline to the NOE assignment errors. Overall, despite the low-resolution modeling the current NMR-I-TASSER pipeline provides a coarse-grained structure folding approach complementary to traditional molecular dynamics simulations, which can produce fast near-native frameworks for atomic-level structural refinement.

  17. Effects of subsampling of passive acoustic recordings on acoustic metrics.

    Thomisch, Karolin; Boebel, Olaf; Zitterbart, Daniel P; Samaran, Flore; Van Parijs, Sofie; Van Opzeeland, Ilse

    2015-07-01

    Passive acoustic monitoring is an important tool in marine mammal studies. However, logistics and finances frequently constrain the number and servicing schedules of acoustic recorders, requiring a trade-off between deployment periods and sampling continuity, i.e., the implementation of a subsampling scheme. Optimizing such schemes to each project's specific research questions is desirable. This study investigates the impact of subsampling on the accuracy of two common metrics, acoustic presence and call rate, for different vocalization patterns (regimes) of baleen whales: (1) variable vocal activity, (2) vocalizations organized in song bouts, and (3) vocal activity with diel patterns. To this end, above metrics are compared for continuous and subsampled data subject to different sampling strategies, covering duty cycles between 50% and 2%. The results show that a reduction of the duty cycle impacts negatively on the accuracy of both acoustic presence and call rate estimates. For a given duty cycle, frequent short listening periods improve accuracy of daily acoustic presence estimates over few long listening periods. Overall, subsampling effects are most pronounced for low and/or temporally clustered vocal activity. These findings illustrate the importance of informed decisions when applying subsampling strategies to passive acoustic recordings or analyses for a given target species. PMID:26233026

  18. Hybrid optical and acoustic force based sorting

    O'Mahoney, Paul; Brodie, Graham W.; Wang, Han; Demore, Christine E. M.; Cochran, Sandy; Spalding, Gabriel C.; MacDonald, Michael P.

    2014-09-01

    We report the combined use of optical sorting and acoustic levitation to give particle sorting. Differing sizes of microparticles are sorted optically both with and without the aid of acoustic levitation, and the results compared to show that the use of acoustic trapping can increase sorting efficiency. The use of a transparent ultrasonic transducer is also shown to streamline the integration of optics and acoustics. We also demonstrate the balance of optical radiation pressure and acoustic levitation to achieve vertical sorting.

  19. Frequency Steered Acoustic Transducer Project

    National Aeronautics and Space Administration — This Small Business Innovation Research Phase I project is to develop, fabricate, and characterize a novel frequency steered acoustic transducer (FSAT) for the...

  20. Frequency Steered Acoustic Transducer Project

    National Aeronautics and Space Administration — This Small Business Innovation Research Phase II project is to fabricate, characterize, and verify performance of a new type of frequency steered acoustic...

  1. Airborne synthetic aperture acoustic imaging.

    Soumekh, M

    1997-01-01

    This paper presents a system model and inversion for airborne synthetic aperture acoustic (SAA) imaging. The system model accurately represents the intercation of the acoustic source and the target region at near range values. Moreover, the model incorporates the fact that the relative speed of the vehicle's (transmitter/receiver) with respect to the target region is comparable to the acoustic wave propagation speed. The inversion utilizes the principle of spectral decomposition of spherical phase functions to develop a wavefront reconstruction method from SAA data. Processing issues and selection of appropriate acoustic FM-CW sources are discussed. Results are provided that exhibit the superior accuracy of the proposed SAA system model and inversion over their synthetic aperture radar (SAR) counterpart in which the vehicle's speed is assumed to be much smaller than the wave propagation speed. PMID:18282912

  2. Cryogenic Acoustic Suppression Testing Project

    National Aeronautics and Space Administration — The proposed project will explore and test the feasibility and effectiveness of using a cryogenic fluid (liquid nitrogen) to facilitate acoustic suppression in a...

  3. Reverberant Acoustic Test Facility (RATF)

    Federal Laboratory Consortium — The very large Reverberant Acoustic Test Facility (RATF) at the NASA Glenn Research Center (GRC), Plum Brook Station, is currently under construction and is due to...

  4. A neutron-X-ray, NMR and calorimetric study of glassy Probucol synthesized using containerless techniques

    Weber, J.K.R., E-mail: rweber@anl.gov [Materials Development, Inc., Arlington Heights, IL 60004 (United States); Argonne National Laboratory, Argonne, IL 60439 (United States); Benmore, C.J. [Argonne National Laboratory, Argonne, IL 60439 (United States); Department of Physics, Arizona State University, AZ 85287 (United States); Tailor, A.N.; Tumber, S.K. [Materials Development, Inc., Arlington Heights, IL 60004 (United States); Neuefeind, J. [Oak Ridge National Laboratory, Oak Ridge, TN 37831 (United States); Cherry, B. [Magnetic Resonance Research Center, Arizona State University, AZ 85287 (United States); Department of Chemistry and Biochemistry, Arizona State University, AZ 85287 (United States); Yarger, J.L. [Department of Physics, Arizona State University, AZ 85287 (United States); Magnetic Resonance Research Center, Arizona State University, AZ 85287 (United States); Department of Chemistry and Biochemistry, Arizona State University, AZ 85287 (United States); Mou, Q. [Magnetic Resonance Research Center, Arizona State University, AZ 85287 (United States); Department of Chemistry and Biochemistry, Arizona State University, AZ 85287 (United States); Weber, W. [Department of Physics, Arizona State University, AZ 85287 (United States); Department of Chemistry and Biochemistry, Arizona State University, AZ 85287 (United States); Byrn, S.R. [Department of Industrial and Physical Pharmacy, Purdue University, IN 47907 (United States)

    2013-10-16

    Highlights: • Acoustic levitation was used to make phase-pure glassy forms of pharmaceutical compounds. • Neutrons, X-rays and NMR were used to characterize the glasses. • The glass comprised of slightly distorted molecules packed in a random network. • Potential for new drug synthesis routes is discussed. - Abstract: Acoustic levitation was used to trap 1–3 mm diameter drops of Probucol and other pharmaceutical materials in containerless conditions. Samples were studied in situ using X-ray diffraction and ex situ using neutron diffraction, NMR and DSC techniques. The materials were brought into non-equilibrium states by supersaturating solutions or by supercooling melts. The glass transition and crystallization temperatures of glassy Probucol were 29 ± 1 and 71 ± 1 °C respectively. The glassy form was stable with a shelf life of at least 8 months. A neutron/X-ray difference function of the glass showed that while molecular sub-groups remain rigid, many of the hydrogen correlations observed in the crystal become smeared out in the disordered material. The glass is principally comprised of slightly distorted Form I Probucol molecules with disordered packing rather than large changes in the individual molecular structure. Avoiding surface contact-induced nucleation provided access to highly non-equilibrium phases and enabled synthesis of phase-pure glasses.

  5. Interfaces in polymer nanocomposites - An NMR study

    Böhme, Ute; Scheler, Ulrich

    2016-03-01

    Nuclear Magnetic Resonance (NMR) is applied for the investigation of polymer nanocomposites. Solid-state NMR is applied to study the modification steps to compatibilize layered double hydroxides with non-polar polymers. 1H relaxation NMR gives insight on the polymer dynamics over a wide range of correlation times. For the polymer chain dynamics the transverse relaxation time T2 is most suited. In this presentation we report on two applications of T2 measurements under external mechanical stress. In a low-field system relaxation NMR studies are performed in-situ under uniaxial stress. High-temperature experiments in a Couette cell permit the investigation of the polymer dynamics in the melt under shear flow.

  6. Bayesian Peak Picking for NMR Spectra

    Cheng, Yichen

    2014-02-01

    Protein structure determination is a very important topic in structural genomics, which helps people to understand varieties of biological functions such as protein-protein interactions, protein–DNA interactions and so on. Nowadays, nuclear magnetic resonance (NMR) has often been used to determine the three-dimensional structures of protein in vivo. This study aims to automate the peak picking step, the most important and tricky step in NMR structure determination. We propose to model the NMR spectrum by a mixture of bivariate Gaussian densities and use the stochastic approximation Monte Carlo algorithm as the computational tool to solve the problem. Under the Bayesian framework, the peak picking problem is casted as a variable selection problem. The proposed method can automatically distinguish true peaks from false ones without preprocessing the data. To the best of our knowledge, this is the first effort in the literature that tackles the peak picking problem for NMR spectrum data using Bayesian method.

  7. Characterization of Hydrogenated Fullerenes by NMR Spectroscopy

    Hedenström, Mattias; Wågberg, Thomas; Johnels, Dan

    NMR spectroscopy is so far the only analytical technique that has been used to get a detailed structural characterization of hydrogenated fullerenes. A substantial amount of information derived from different NMR experiments can thus be found in the literature for a number of fullerenes hydrogenated to various degrees. These studies have benefitted from the fact that chemical shifts of 1H and 13C and in some cases also 3He can be used to obtain structural information of these compounds. Such results, together with discussions about different NMR experiments and general considerations regarding sample preparations, are summarized in this chapter. The unique information, both structural and physicochemical, that can be derived from different NMR experiments ensures that this technique will continue to be of central importance in characterization of hydrogenated fullerenes.

  8. NMR spectroscopy assists synthetic fuels research

    Cookson, D.J.; Smith, B.E.

    1983-01-01

    NMR spectroscopy has proved to be a useful and versatile technique for the study of synthetic fuels feedstocks, catalysts, process intermediates and final products. Some applications of the technique to coal and gas conversion research are illustrated and discussed.

  9. NMR studies of cerebral metabolism in vivo

    The nature and extent of the potential synergism between PET and NMR methods is not yet well appreciated in the biomedical community. The long-range interest of medical neurobiology will be well served by efforts of PET and NMR scientists to follow each others' work so that opportunities for productive interchange can be efficiently exploited. Appreciation of the synergism by the rest of the biomedical community will follow naturally. PET is said by the people doing it to be still in its infancy, for they are more concerned with advancing their discipline than with admiring its already impressive achievements. On the scale of the same developmental metaphor, many NMR methods for studying the living human brain are still in utero. The best way to provide the reader a sense of the current status and future course of NMR research in medical neurobiology is by discussion of published in vivo studies. Such a discussion, adapted from another article is what follows

  10. NMR study of hydride systems

    The hydrides of thorium (ThH2, Th4H15 and Th4D15) and the intermetallic compound system (Zr(Vsub(1-x)Cosub(x))2 and its hydrides were investigated using the nuclear magnetic resonance (NMR) technique. From the results for the thorium hydride samples it was concluded that the density of states at the Fermi level n(Esub(f)) is higher in Th4H15 than in ThH2; there is an indirect reaction between the protons and the d electrons belonging to the Th atoms in Th4H15; n(E) has a sharp structure near Esub(f). It was also found that the hydrogen diffusion mechanism changes with temperature. From the results for the intermetallic compound system conclusions were drawn concerning variations in the electronic structure, which explain the behavior of the system. In hydrogen diffusion studies in several samples it was found that Co atoms slow the diffusion rate. Quadrupole spectra obtained at low temperatures show that the H atoms preferably occupy tetrahedral sites formed by three V atoms and one Z atom. (H.K.)

  11. Rheology of Blood by NMR

    Han, Song-I.; Marseille, Oliver; Gehlen, Christa; Blümich, Bernhard

    2001-09-01

    Pipe flow of blood in tubes of 1 and 7 mm inner diameter, respectively, was investigated employing two-dimensional NMR velocity imaging and PFG propagator measurements at different Reynolds numbers between 10 and 3500. The results are compared to flow of a water/glycerol mixture of matching viscosity under identical conditions. The transition from laminar to turbulent flow is observed by both a flattening of the velocity profile and a change of the propagator shape. For blood flow this transition is found to be shifted toward higher Reynolds numbers as compared to the transition of the water/glycerol mixture. This observation is in agreement with predictions from hydraulic measurements and is a consequence of the non-Newtonian flow characteristics of blood as a suspension of erythrocytes and plasma. Likewise, a deviation from the laminar flow condition is observed for blood at low Reynolds numbers between 10 and 100. This phenomenon is unknown for Newtonian liquids and is explained by the onset of a geometrical arrangement of the erythrocytes, the so-called rouleaux effect.

  12. Acoustic Invisibility in Turbulent Fluids

    Huang, Xun; Zhong, Siyang

    2013-01-01

    Acoustic invisibility of a cloaking system in turbulent uids has been poorly understood. Here we show that evident scattering would appear in turbulent wakes owing to the submergence of a classical cloaking device. The inherent mechanism is explained using our theoretical model, which eventually inspires us to develop an optimized cloaking approach. Both the near- and far-?eld scatted ?elds are examined using high order computational acoustic methods. The remarkably low scattering demonstrate...

  13. Passive/Active Acoustic metamaterials

    Lissek, Hervé

    2011-01-01

    Within the last years, an increasing number of studies have been carried out in the field of acoustic metamaterials. These artificial composite materials aim at achieving new macroscopic properties, like negative refraction, that are not readily present in nature. In analogy to electromagnetics, where such concepts are already more mature, a novel concept of artificial acoustic transmission line has recently been reported, which presents such artificial behavior. In this presentation, the des...

  14. Stable And Oscillating Acoustic Levitation

    Barmatz, Martin B.; Garrett, Steven L.

    1988-01-01

    Sample stability or instability determined by levitating frequency. Degree of oscillation of acoustically levitated object along axis of levitation chamber controlled by varying frequency of acoustic driver for axis above or below frequency of corresponding chamber resonance. Stabilization/oscillation technique applied in normal Earth gravity, or in absence of gravity to bring object quickly to rest at nominal levitation position or make object oscillate in desired range about that position.

  15. Simplified Rotation In Acoustic Levitation

    Barmatz, M. B.; Gaspar, M. S.; Trinh, E. H.

    1989-01-01

    New technique based on old discovery used to control orientation of object levitated acoustically in axisymmetric chamber. Method does not require expensive equipment like additional acoustic drivers of precisely adjustable amplitude, phase, and frequency. Reflecting object acts as second source of sound. If reflecting object large enough, close enough to levitated object, or focuses reflected sound sufficiently, Rayleigh torque exerted on levitated object by reflected sound controls orientation of object.

  16. Computational Modeling of Airway Acoustic

    Horáček, Jaromír

    Salt Lake City: National Center for Voice and Speech, University of Utah, 2014. s. 14-14. [International Conference on Voice Physiology and Biomechanics /9./. 10.04.2014-12.04.2014, Salt Lake City] R&D Projects: GA ČR GAP101/12/1306 Institutional support: RVO:61388998 Keywords : biomechanics of voice * finite element method * acoustic waves propagation Subject RIV: BI - Acoustics

  17. Observation of supramolecular aggregation by dosy NMR

    Šaman, David; Wimmer, Zdeněk; Kolehmainen, E.

    Tatranská Lomnica : Slovak National NMR Centre. Slovak Chemical Society, 2011 - (Liptaj, T.; Imrich, J.; Kovaľaková, M.; Olčák, D.). s. 56-56 ISBN 978-80-89284-77-1. [Magnetic Moments in Central Europe. 16.03.2011-20.03.2011, Tatranská Lomnica] R&D Projects: GA MŠk 2B06024 Institutional research plan: CEZ:AV0Z40550506 Keywords : difusion * NMR Subject RIV: CC - Organic Chemistry

  18. NMR Investigation of the Quantum Piegonhole Effect

    S., Anjusha V.; Hegde, Swathi S.; Mahesh, T. S.

    2015-01-01

    Quantum simulators based on nuclear spin-systems controlled by NMR techniques have been used for studying various quantum phenomena. In this work, using a four-qubit NMR quantum simulator, we investigate the recently postulated quantum pigeon-hole effect. In mathematics, the pigeonhole effect is described by a set of three objects being allocated with only two containers. Classically, one would expect at least one container to accommodate more than one object. However, recently it was predict...

  19. NMR of Membrane Proteins: Beyond Crystals.

    Rajesh, Sundaresan; Overduin, Michael; Bonev, Boyan B

    2016-01-01

    Membrane proteins are essential for the flow of signals, nutrients and energy between cells and between compartments of the cell. Their mechanisms can only be fully understood once the precise structures, dynamics and interactions involved are defined at atomic resolution. Through advances in solution and solid state NMR spectroscopy, this information is now available, as demonstrated by recent studies of stable peripheral and transmembrane proteins. Here we highlight recent cases of G-protein coupled receptors, outer membrane proteins, such as VDAC, phosphoinositide sensors, such as the FAPP-1 pleckstrin homology domain, and enzymes including the metalloproteinase MMP-12. The studies highlighted have resulted in the determination of the 3D structures, dynamical properties and interaction surfaces for membrane-associated proteins using advanced isotope labelling strategies, solubilisation systems and NMR experiments designed for very high field magnets. Solid state NMR offers further insights into the structure and multimeric assembly of membrane proteins in lipid bilayers, as well as into interactions with ligands and targets. Remaining challenges for wider application of NMR to membrane structural biology include the need for overexpression and purification systems for the production of isotope-labelled proteins with fragile folds, and the availability of only a few expensive perdeuterated detergents.Step changes that may transform the field include polymers, such as styrene maleic acid, which obviate the need for detergent altogether, and allow direct high yield purification from cells or membranes. Broader demand for NMR may be facilitated by MODA software, which instantly predicts membrane interactive residues that can subsequently be validated by NMR. In addition, recent developments in dynamic nuclear polarization NMR instrumentation offer a remarkable sensitivity enhancement from low molarity samples and cell surfaces. These advances illustrate the current

  20. Frontiers of NMR in Molecular Biology

    NONE

    1999-08-25

    NMR spectroscopy is expanding the horizons of structural biology by determining the structures and describing the dynamics of blobular proteins in aqueous solution, as well as other classes of proteins including membrane proteins and the polypeptides that form the aggregates diagnostic of prion and amyloid diseases. Significant results are also emerging on DNA and RNA oligomers and their complexes with proteins. This meeting focused attention on key structural questions emanating from molecular biology and how NMR spectroscopy can be used to answer them.

  1. NMR studies of multiphase flows II

    Altobelli, S.A.; Caprihan, A.; Fukushima, E. [Lovelace Institutes, Albuquerque, NM (United States)] [and others

    1995-12-31

    NMR techniques for measurements of spatial distribution of material phase, velocity and velocity fluctuation are being developed and refined. Versions of these techniques which provide time average liquid fraction and fluid phase velocity have been applied to several concentrated suspension systems which will not be discussed extensively here. Technical developments required to further extend the use of NMR to the multi-phase flow arena and to provide measurements of previously unobtainable parameters are the focus of this report.

  2. Opto-acoustic cell permeation

    Visuri, S R; Heredia, N

    2000-03-09

    Optically generated acoustic waves have been used to temporarily permeate biological cells. This technique may be useful for enhancing transfection of DNA into cells or enhancing the absorption of locally delivered drugs. A diode-pumped frequency-doubled Nd:YAG laser operating at kHz repetition rates was used to produce a series of acoustic pulses. An acoustic wave was formed via thermoelastic expansion by depositing laser radiation into an absorbing dye. Generated pressures were measured with a PVDF hydrophone. The acoustic waves were transmitted to cultured and plated cells. The cell media contained a selection of normally- impermeable fluorescent-labeled dextran dyes. Following treatment with the opto-acoustic technique, cellular incorporation of dyes, up to 40,000 Molecular Weight, was noted. Control cells that did not receive opto-acoustic treatment had unremarkable dye incorporation. Uptake of dye was quantified via fluorescent microscopic analysis. Trypan Blue membrane exclusion assays and fluorescent labeling assays confirmed the vitality of cells following treatment. This method of enhanced drug delivery has the potential to dramatically reduce required drug dosages and associated side effects and enable revolutionary therapies.

  3. Prediction of acoustic comfort and acoustic silence in Goan Catholic churches

    Menino A. S. M. P. Tavares; S. Rajagopalan; Satish J. Sharma; António P. O. Carvalho

    2009-01-01

    Acoustic Comfort and Acoustic Silence are determinants of tranquility in a worship space. The results presented here are part of a study that investigates the behaviour of acoustically constituted worship parameters in six Catholic churches (Goa, India). Acoustic comfort is quantified through an Acoustic Comfort Impression Index which measures the net comfort induced through the optimization of the desired subjective acoustic impressions for different types of music and different music source...

  4. 33S NMR cryogenic probe for taurine detection

    Hobo, Fumio; Takahashi, Masato; Maeda, Hideaki

    2009-03-01

    With the goal of a S33 nuclear magnetic resonance (NMR) probe applicable to in vivo NMR on taurine-biological samples, we have developed the S33 NMR cryogenic probe, which is applicable to taurine solutions. The NMR sensitivity gain relative to a conventional broadband probe is as large as 3.5. This work suggests that improvements in the preamplifier could allow NMR measurements on 100 μM taurine solutions, which is the level of sensitivity necessary for biological samples.

  5. Optimized multisectioned acoustic liners

    Baumeister, K. J.

    1979-01-01

    A critical examination is presented of the use of optimized axially segmented acoustic liners to increase the attenuation of a liner. New calculations show that segmenting is most efficient at high frequencies with relatively long duct lengths where the attenuation is low for both uniform and segmented liners. Statistical considerations indicate little advantage in using optimized liners with more than two segments while the bandwidth of an optimized two-segment liner is shown to be nearly equal to that of a uniform liner. Multielement liner calculations show a large degradation in performance due to changes in assumed input modal structure. Finally, in order to substantiate previous and future analytical results, in-house (finite difference) and contractor (mode matching) programs are used to generate theoretical attenuations for a number of liner configurations for liners in a rectangular duct with no mean flow. Overall, the use of optimized multisectioned liners (sometimes called phased liners) fails to offer sufficient advantage over a uniform liner to warrant their use except in low frequency single mode application.

  6. Focusing of Acoustic Waves through Acoustic Materials with Subwavelength Structures

    Xiao, Bingmu

    2013-05-01

    In this thesis, wave propagation through acoustic materials with subwavelength slits structures is studied. Guided by the findings, acoustic wave focusing is achieved with a specific material design. By using a parameter retrieving method, an effective medium theory for a slab with periodic subwavelength cut-through slits is successfully derived. The theory is based on eigenfunction solutions to the acoustic wave equation. Numerical simulations are implemented by the finite-difference time-domain (FDTD) method for the two-dimensional acoustic wave equation. The theory provides the effective impedance and refractive index functions for the equivalent medium, which can reproduce the transmission and reflection spectral responses of the original structure. I analytically and numerically investigate both the validity and limitations of the theory, and the influences of material and geometry on the effective spectral responses are studied. Results show that large contrasts in impedance and density are conditions that validate the effective medium theory, and this approximation displays a better accuracy for a thick slab with narrow slits in it. Based on the effective medium theory developed, a design of a at slab with a snake shaped" subwavelength structure is proposed as a means of achieving acoustic focusing. The property of focusing is demonstrated by FDTD simulations. Good agreement is observed between the proposed structure and the equivalent lens pre- dicted by the theory, which leads to robust broadband focusing by a thin at slab.

  7. PORTABLE ACOUSTIC MONITORING PACKAGE (PAMP)

    John l. Loth; Gary J. Morris; George M. Palmer; Richard Guiler; Deepak Mehra

    2003-07-01

    The 1st generation acoustic monitoring package was designed to detect and analyze weak acoustic signals inside natural gas transmission lines. Besides a microphone it housed a three-inch diameter aerodynamic acoustic signal amplifier to maximize sensitivity to leak induced {Delta}p type signals. The theory and test results of this aerodynamic signal amplifier was described in the master's degree thesis of our Research Assistant Deepak Mehra who is about to graduate. To house such a large three-inch diameter sensor required the use of a steel 300-psi rated 4 inch weld neck flange, which itself weighed already 29 pounds. The completed 1st generation Acoustic Monitoring Package weighed almost 100 pounds. This was too cumbersome to mount in the field, on an access port at a pipeline shut-off valve. Therefore a 2nd generation and truly Portable Acoustic Monitor was built. It incorporated a fully self-contained {Delta}p type signal sensor, rated for line pressures up to 1000 psi with a base weight of only 6 pounds. This is the Rosemont Inc. Model 3051CD-Range 0, software driven sensor, which is believed to have industries best total performance. Its most sensitive unit was purchased with a {Delta}p range from 0 to 3 inch water. This resulted in the herein described 2nd generation: Portable Acoustic Monitoring Package (PAMP) for pipelines up to 1000 psi. Its 32-pound total weight includes an 18-volt battery. Together with a 3 pound laptop with its 4-channel data acquisition card, completes the equipment needed for field acoustic monitoring of natural gas transmission pipelines.

  8. Reflective echo tomographic imaging using acoustic beams

    Kisner, Roger; Santos-Villalobos, Hector J

    2014-11-25

    An inspection system includes a plurality of acoustic beamformers, where each of the plurality of acoustic beamformers including a plurality of acoustic transmitter elements. The system also includes at least one controller configured for causing each of the plurality of acoustic beamformers to generate an acoustic beam directed to a point in a volume of interest during a first time. Based on a reflected wave intensity detected at a plurality of acoustic receiver elements, an image of the volume of interest can be generated.

  9. Use of NMR and NMR Prediction Software to Identify Components in Red Bull Energy Drinks

    Simpson, Andre J.; Shirzadi, Azadeh; Burrow, Timothy E.; Dicks, Andrew P.; Lefebvre, Brent; Corrin, Tricia

    2009-01-01

    A laboratory experiment designed as part of an upper-level undergraduate analytical chemistry course is described. Students investigate two popular soft drinks (Red Bull Energy Drink and sugar-free Red Bull Energy Drink) by NMR spectroscopy. With assistance of modern NMR prediction software they identify and quantify major components in each…

  10. HPLC-NMR revisited: Using time-slice HPLC-SPE-NMR with database assisted dereplication

    Johansen, Kenneth; Wubshet, Sileshi Gizachew; Nyberg, Nils

    2013-01-01

    Time based trapping of chromatographically separated compounds on to solid-phase extraction cartridges (SPE) and subsequent elution to NMR-tubes was done to emulate the function of HPLC–NMR for dereplication purposes. Sufficient mass sensitivity was obtained by the use of a state-of-the-art HPLC...

  11. NMR standard probe for precision measurement of the free proton NMR frequency

    The authors have designed and constructed a special NMR standard probe using a spehrical pure water sample to determine the free proton NMR frequency fp at high field and an accuracy of 0.04 ppm has been achieved. Since the proton gyromagnetic ratio γp is less well known (∼0.1 ppm), the free proton NMR frequency measured by the probe may serve as a calibration standard for the magnetic field B. The standard probe can be used at various magnetic field values without introducing any additional magnetic perturbations. The probe is designed in such a way that a cylindrical sample or a small NMR probe can be inserted to replace the 1 cm diameter spherical water sample for systematic studies. Other NMR probes can be calibrated easily against the standard probe using a calibration form. Results will be presented and discussed

  12. Sonification of acoustic emission data

    Raith, Manuel; Große, Christian

    2014-05-01

    While loading different specimens, acoustic emissions appear due to micro crack formation or friction of already existing crack edges. These acoustic emissions can be recorded using suitable ultrasonic transducers and transient recorders. The analysis of acoustic emissions can be used to investigate the mechanical behavior of different specimens under load. Our working group has undertaken several experiments, monitored with acoustic emission techniques. Different materials such as natural stone, concrete, wood, steel, carbon composites and bone were investigated. Also the experimental setup has been varied. Fire-spalling experiments on ultrahigh performance concrete and pullout experiments on bonded anchors have been carried out. Furthermore uniaxial compression tests on natural stone and animal bone had been conducted. The analysis tools include not only the counting of events but the analysis of full waveforms. Powerful localization algorithms and automatic onset picking techniques (based on Akaikes Information Criterion) were established to handle the huge amount of data. Up to several thousand events were recorded during experiments of a few minutes. More sophisticated techniques like moment tensor inversion have been established on this relatively small scale as well. Problems are related to the amount of data but also to signal-to-noise quality, boundary conditions (reflections) sensor characteristics and unknown and changing Greens functions of the media. Some of the acoustic emissions recorded during these experiments had been transferred into audio range. The transformation into the audio range was done using Matlab. It is the aim of the sonification to establish a tool that is on one hand able to help controlling the experiment in-situ and probably adjust the load parameters according to the number and intensity of the acoustic emissions. On the other hand sonification can help to improve the understanding of acoustic emission techniques for training

  13. CALCULATION OF ACOUSTIC EFFICIENCY OF PORTABLE ACOUSTIC SCREEN

    Aleksandr Skvortsov

    2016-03-01

    Full Text Available The research of influence of life environment adverse factors on physical development and health of population is an actual problem of ecology. The aspects of the most actual problems of the modern world, namely environmental industrial noise pollution are considered in the article. Industrial facilities everywhere have noisy equipment. Noise is a significant factors of negative influenceon people and environment. Combined effects of noise and of other physical pollutions on people may cause amplification of their negative impact. If the noise pollution level from the object in a residential area exceeds the permissible levels (MPL, noise protection measures can be initiated. Today, the most common design decisions for noise protection are sound absorbing construction, noise screens and barriers, acousting housings, soundproff cabins. Many of them are popular, others are less known. The article deals with one of the most wide spread means of noise protection – a portable acoustic screen. The aim of the research is to determine the efficiency of portable acoustic screens. It is shown that the installation of such structures can reduce the average value of the sound level. The authors analyzed acoustic screens as device to reduce noise pollution. The authors offer a potable acoustic screen differing from the used easyness, mobility, minimum price and good sound protective properties. Effectiveness, a sound absorption coefficient and sound conductivity coefficient of a portable acoustic screen are evaluated. The descriptions of the algorithm calculations and the combination of technical solutions have practical originality. The results of the research demonstrate the advantages of the proposed solutions for reducing noise levels in the agro-industrial complex.

  14. My 65 years in acoustics

    Beranek, Leo L.

    2001-05-01

    My entry into acoustics began as research assistant to Professor F. V. Hunt at Harvard University. I received my doctorate in 1940 and directed the Electro-Acoustic Laboratory at Harvard from October 1940 until September 1945. In 1947, I became a tenured associate professor at MIT, and, with Richard H. Bolt, formed the consulting firm Bolt and Beranek, that later included Robert B. Newman, becoming BBN. My most significant contributions before 1970 were design of wedge-lined anechoic chambers, systemization of noise reduction in ventilation systems, design of the world's largest muffler for the testing of supersonic jet engines at NASA's Lewis Laboratory in Cleveland, speech interference level, NC noise criterion curves, heading New York Port Authority's noise study that resulted in mufflers on jet aircraft, and steep aircraft climb procedures, and publishing books titled, Acoustical Measurements, Acoustics, Noise Reduction, Noise and Vibration Control, and Music, Acoustics and Architecture. As President of BBN, I supervised the formation of the group that built and operated the ARPANET (1969), which, when split in two (using TCP/IP protocol) became the INTERNET (1984). Since then, I have written two books on Concert Halls and Opera Houses and have consulted on four concert halls and an opera house.

  15. BOOK REVIEW: NMR Imaging of Materials

    Blümich, Bernhard

    2003-09-01

    Magnetic resonance imaging (MRI) of materials is a field of increasing importance. Applications extend from fundamental science like the characterization of fluid transport in porous rock, catalyst pellets and hemodialysers into various fields of engineering for process optimization and product quality control. While the results of MRI imaging are being appreciated by a growing community, the methods of imaging are far more diverse for materials applications than for medical imaging of human beings. Blümich has delivered the first book in this field. It was published in hardback three years ago and is now offered as a paperback for nearly half the price. The text provides an introduction to MRI imaging of materials covering solid-state NMR spectroscopy, imaging methods for liquid and solid samples, and unusual MRI in terms of specialized approaches to spatial resolution such as an MRI surface scanner. The book represents an excellent and thorough treatment which will help to grow research in materials MRI. Blümich developed the treatise over many years for his research students, graduates in chemistry, physics and engineering. But it may also be useful for medical students looking for a less formal discussion of solid-state NMR spectroscopy. The structure of this book is easy to perceive. The first three chapters cover an introduction, the fundamentals and methods of solid-state NMR spectroscopy. The book starts at the ground level where no previous knowledge about NMR is assumed. Chapter 4 discusses a wide variety of transformations beyond the Fourier transformation. In particular, the Hadamard transformation and the 'wavelet' transformation are missing from most related books. This chapter also includes a description of noise-correlation spectroscopy, which promises the imaging of large objects without the need for extremely powerful radio-frequency transmitters. Chapters 5 and 6 cover basic imaging methods. The following chapter about the use of relaxation and

  16. Nuclear magnetic resonance (NMR): principles and applications

    The basis for the phenomenon of nuclear magnetic resonance (NMR) is the ability of certain nuclei possessing both intrinsic angular momentum or ''spin'' I and magnetic moment to absorb electromagnetic energy in the radio frequency range. In principle, there are approximately 200 nuclei which may be investigated using the NMR technique. The NMR spectrum consists of intensity peaks along an axis calibrated in terms of the steady magnetic field or the frequency of the radiofrequency electromagnetic radiation. Analysis of the number, spacing, position and intensity of the lines in an NMR spectrum consists of intensity peaks along an axis calibrated in terms of the steady magnetic field or the frequency of the radiofrequency electromagnetic radiation. Analysis of the number, spacing, position and intensity of the lines in an NMR spectrum provides a variety of qualitative and quantitative analytical applications. The most obvious applications consist of the measurements of nuclear properties, such as spin number and nuclear magnetic moment. In liquids, the fine structure of resonance spectra provides a tool for chemical identification and molecular structure analysis. Other applications include the measurements of self-diffusion coefficients, magnetic fields and field homogeneity, inter-nuclear distances, and, in some cases, the water content of biological materials. (author)

  17. Acoustic and optical investigations of superfluid 3He. Doctoral thesis

    Manninen, A.

    1993-06-15

    The thesis is an experimental survey of properties of rotating and stationary superfluid (3)He. Two techniques, acoustics and optics, were used. Ultrasound, together with NMR, has provided most of the present experimental knowledge about the superfluid phases of (3)He. The author applied acoustics for the first time to study rotating (3)He. The main result was the discovery of a new vortex in (3)He-A when the magnetic field is low. New phenomena were observed in stationary (3)He as well. Most importantly, one of the collective modes, the real squashing (rsq) mode, of (3)He-B could be excited by means of two-phonon absorption. Superfluid (3)He was studied optically for the first time. No one has previously seen (3)He in the superfluid state. The principal achievement was developing techniques which facilitate optical experiments at temperatures below 1 mK, required to study superfluid (3)He. Optical fibers were used to transmit light between room temperature and the cold parts of the cryostat. Before these investigations, photography had not been done below 10 mK. The usefulness of optics as a proble of the superfluid phases of (3)He was demonstrated by studying the macroscopic shape of the free surface of rotating (3)He-B. The classical parabolic meniscus was observed, which is indicative of the equilibrium density of vortices.

  18. Acoustic metasurface with hybrid resonances.

    Ma, Guancong; Yang, Min; Xiao, Songwen; Yang, Zhiyu; Sheng, Ping

    2014-09-01

    An impedance-matched surface has the property that an incident wave generates no reflection. Here we demonstrate that by using a simple construction, an acoustically reflecting surface can acquire hybrid resonances and becomes impedance-matched to airborne sound at tunable frequencies, such that no reflection is generated. Each resonant cell of the metasurface is deep-subwavelength in all its spatial dimensions, with its thickness less than the peak absorption wavelength by two orders of magnitude. As there can be no transmission, the impedance-matched acoustic wave is hence either completely absorbed at one or multiple frequencies, or converted into other form(s) of energy, such as an electrical current. A high acoustic-electrical energy conversion efficiency of 23% is achieved. PMID:24880731

  19. Prototype acoustic resonance spectroscopy monitor

    This report reports on work performed for the International Atomic Energy Agency (IAEA) through the Program Office for Technical Assistance (POTAS). In this work, we investigate possible applications of nondestructive acoustics measurements to facilitate IAEA safeguards at bulk processing facilities. Two different acoustic techniques for verifying the internal structure of a processing tank were investigated. During this effort we also examined two acoustic techniques for assessing the fill level within a processing tank. The fill-level measurements could be made highly portable and have an added safeguards advantage that they can also detect stratification of fill material. This later application may be particularly useful in confirming the absence of stratification in plutonium processing tanks before accountability samples are withdrawn

  20. Acoustic Communication for Medical Nanorobots

    Hogg, Tad

    2012-01-01

    Communication among microscopic robots (nanorobots) can coordinate their activities for biomedical tasks. The feasibility of in vivo ultrasonic communication is evaluated for micron-size robots broadcasting into various types of tissues. Frequencies between 10MHz and 300MHz give the best tradeoff between efficient acoustic generation and attenuation for communication over distances of about 100 microns. Based on these results, we find power available from ambient oxygen and glucose in the bloodstream can readily support communication rates up to 10,000 bits/second between micron-sized robots. We discuss techniques, such as directional acoustic beams, that can increase this rate. The acoustic pressure fields enabling this communication are unlikely to damage nearby tissue, and short bursts at considerably higher power could be of therapeutic use.

  1. Acoustic multivariate condition monitoring - AMCM

    Rosenhave, P.E. [Vestfold College, Maritime Dept., Toensberg (Norway)

    1997-12-31

    In Norway, Vestfold College, Maritime Department presents new opportunities for non-invasive, on- or off-line acoustic monitoring of rotating machinery such as off-shore pumps and diesel engines. New developments within acoustic sensor technology coupled with chemometric data analysis of complex signals now allow condition monitoring of hitherto unavailable flexibility and diagnostic specificity. Chemometrics paired with existing knowledge yields a new and powerful tool for condition monitoring. By the use of multivariate techniques and acoustics it is possible to quantify wear and tear as well as predict the performance of working components in complex machinery. This presentation describes the AMCM method and one result of a feasibility study conducted onboard the LPG/C `Norgas Mariner` owned by Norwegian Gas Carriers as (NGC), Oslo. (orig.) 6 refs.

  2. Acoustics of a broadcast center

    Beristain, Sergio

    2003-04-01

    A broadcast system in Mexico City had to change facilities in order to concentrate in a single site all related broadcast stations and production studios in order to facilitate its normal operation. This led to a design which included the acoustic noise isolation and the interior acoustics of every studio and control room, together with the audio interconection, the electricity layout, the air conditioning system, the office building, etc. This paper presents the acoustics profile of the center, including final results of the construction as they were measured on completion of the installation. The complex has seven AM and FM broadcast stations, plus seven production studios for news, commercials and radio-novels plus an audio master control room, and everything was completed within four months.

  3. Classroom acoustics: Three pilot studies

    Smaldino, Joseph J.

    2005-04-01

    This paper summarizes three related pilot projects designed to focus on the possible effects of classroom acoustics on fine auditory discrimination as it relates to language acquisition, especially English as a second language. The first study investigated the influence of improving the signal-to-noise ratio on the differentiation of English phonemes. The results showed better differentiation with better signal-to-noise ratio. The second studied speech perception in noise by young adults for whom English was a second language. The outcome indicated that the second language learners required a better signal-to-noise ratio to perform equally to the native language participants. The last study surveyed the acoustic conditions of preschool and day care classrooms, wherein first and second language learning occurs. The survey suggested an unfavorable acoustic environment for language learning.

  4. Acoustic metamaterials for sound mitigation

    Assouar, Badreddine; Oudich, Mourad; Zhou, Xiaoming

    2016-05-01

    We provide theoretical and numerical analyses of the behavior of a plate-type acoustic metamaterial considered in an air-borne sound environment in view of sound mitigation application. Two configurations of plate are studied, a spring-mass one and a pillar system-based one. The acoustic performances of the considered systems are investigated with different approaches and show that a high sound transmission loss (STL) up to 82 dB is reached with a metamaterial plate with a thickness of 0.5 mm. The physical understanding of the acoustic behavior of the metamaterial partition is discussed based on both air-borne and structure-borne approaches. Confrontation between the STL, the band structure, the displacement fields and the effective mass density of the plate metamaterial is made to have a complete physical understanding of the different mechanisms involved. xml:lang="fr"

  5. Phoneme Recognition Using Acoustic Events

    Huebener, K; Huebener, Kai; Carson-Berndsen, Julie

    1994-01-01

    This paper presents a new approach to phoneme recognition using nonsequential sub--phoneme units. These units are called acoustic events and are phonologically meaningful as well as recognizable from speech signals. Acoustic events form a phonologically incomplete representation as compared to distinctive features. This problem may partly be overcome by incorporating phonological constraints. Currently, 24 binary events describing manner and place of articulation, vowel quality and voicing are used to recognize all German phonemes. Phoneme recognition in this paradigm consists of two steps: After the acoustic events have been determined from the speech signal, a phonological parser is used to generate syllable and phoneme hypotheses from the event lattice. Results obtained on a speaker--dependent corpus are presented.

  6. Vestibular Schwannoma (Acoustic Neuroma) and Neurofibromatosis

    ... Home » Health Info » Hearing, Ear Infections, and Deafness Vestibular Schwannoma (Acoustic Neuroma) and Neurofibromatosis On this page: ... more information about vestibular schwannomas? What is a vestibular schwannoma (acoustic neuroma)? Inner ear with vestibular schwannoma ( ...

  7. On the Synchronization of Acoustic Gravity Waves

    Lonngren, Karl E.; Bai, Er-Wei

    Using the model proposed by Stenflo, we demonstrate that acoustic gravity waves found in one region of space can be synchronized with acoustic gravity waves found in another region of space using techniques from modern control theory.

  8. Acoustojet: acoustic analogue of photonic jet phenomenon

    Minin, Igor V

    2016-01-01

    It has been demonstrated for the first time that an existence of acoustic analogue of photonic jet phenomenon, called acoustojet, providing for subwavelength localization of acoustic field in the shadow area of arbitrary 3D penetrable mesoscale particle, is possible.

  9. Golden Gate and Pt. Reyes Acoustic Detections

    National Oceanic and Atmospheric Administration, Department of Commerce — This dataset contains detections of acoustic tagged fish from two general locations: Golden Gate (east and west line) and Pt. Reyes. Several Vemco 69khz acoustic...

  10. Acoustic remote sensing of ocean flows

    Joseph, A.; Desa, E.

    Acoustic techniques have become powerful tools for measurement of ocean circulation mainly because of the ability of acoustic signals to travel long distances in water, and the inherently non-invasive nature of measurement. The satellite remote...

  11. CT findings of acoustic neuroma

    Sim, Do Choul; Lee, Jae Mun; Shinn, Kyung Sub; Bahk, Yong Whee [Catholic Univ., Seoul (Korea, Republic of)

    1987-10-15

    Computed Tomography (CT) is very accurate in evaluating the location, size, shape and extension of acoustic neuroma. We analysed CT findings of 23 acoustic neuromas seen at Department of Radiology, Kangnam St. Mary's Hospital, Catholic University Medical College during the period of from January 1981 to June 1987. 1. Five (22%) were men and 18 (78%) were women with the high incidence occurring in the 4th and 5th decades. 2. Twenty two cases were diagnosed satisfactorily by CT examinations which included axial, coronal and reconstruction images. One with the smallest dimension of 8 mm in diameter could not be detected by the conventional CT scan. But is could be seen after metrizamide cisternography. mean size of the tumor masses was estimated 3.6 cm in diameter. 3. The shape of the tumor was oval in 50%, round in 27% and lobulated in 23%. The masses were presented as hypodense in 50%, isodense in 32% and hyperdense in 18%. All tumors were extended from the internal acoustic and toward the cerebellopontine angle. The internal acoustic canal was widened in 77%. Hydrocephalus was associated in 45%. Widening of cerebellopontine angle cistern was noted in 50%. 4. After contrast infusion the tumors were enhanced markedly in 45%, moderately in 32% and mildly in 23%. The enhanced pattern was homogeneous in 41%, mixed in 41% and rim in 18%. The margin of the tumors was sharply defined in 82%. The tumors were attached to the petrous bone with acute angle in 73%. Cystic change within the tumor was found in 27%. The peritumoral edema was noted in 45%. In conclusion, CT is of most effective modalities to evaluate size, shape, extent and internal architecture of acoustic neuroma as well as relationship with adjacent anatomic structures including the internal acoustic canal.

  12. Acoustically-Induced Electrical Signals

    Brown, S. R.

    2014-12-01

    We have observed electrical signals excited by and moving along with an acoustic pulse propagating in a sandstone sample. Using resonance we are now studying the characteristics of this acousto-electric signal and determining its origin and the controlling physical parameters. Four rock samples with a range of porosities, permeabilities, and mineralogies were chosen: Berea, Boise, and Colton sandstones and Austin Chalk. Pore water salinity was varied from deionized water to sea water. Ag-AgCl electrodes were attached to the sample and were interfaced to a 4-wire electrical resistivity system. Under computer control, the acoustic signals were excited and the electrical response was recorded. We see strong acoustically-induced electrical signals in all samples, with the magnitude of the effect for each rock getting stronger as we move from the 1st to the 3rd harmonics in resonance. Given a particular fluid salinity, each rock has its own distinct sensitivity in the induced electrical effect. For example at the 2nd harmonic, Berea Sandstone produces the largest electrical signal per acoustic power input even though Austin Chalk and Boise Sandstone tend to resonate with much larger amplitudes at the same harmonic. Two effects are potentially responsible for this acoustically-induced electrical response: one the co-seismic seismo-electric effect and the other a strain-induced resistivity change known as the acousto-electric effect. We have designed experimental tests to separate these mechanisms. The tests show that the seismo-electric effect is dominant in our studies. We note that these experiments are in a fluid viscosity dominated seismo-electric regime, leading to a simple interpretation of the signals where the electric potential developed is proportional to the local acceleration of the rock. Toward a test of this theory we have measured the local time-varying acoustic strain in our samples using a laser vibrometer.

  13. Characterization by NMR of ozonized methyl linoleate

    Diaz, Maritza F. [National Center for Scientific Research, Havana (Cuba). Ozone Research Center. Dept. of Ozonized Substances]. E-mail: maritza.diaz@cnic.edu.cu; Gavin, Jose A. [University of the Laguna, Tenerife (Spain)

    2007-07-01

    In the present study ozonized methyl linoleate with peroxide index of 1,800 mmol-equiv kg{sup -1} was chemically characterized. Ozonation of methyl linoleate produced hydroperoxides, ozonides and aldehydes which were identified by {sup 1}H and {sup 13}C NMR two-dimensional. The standard methyl linoleate and ozonized methyl linoleate shown very similar {sup 1}H NMR spectra except for the signals at {delta} 9.7 and {delta} 9.6 that correspond to aldehydic hydrogen, {delta} 5.7 and {delta} 5.5 (olefinic signals from hydroperoxides) and {delta} 5.2 ppm (multiplet from ozonides methynic hydrogen). Other resonance assignments are based on the connectivities provided by the hydrogen scalar coupling constants. These results indicate that NMR spectroscopy can provide valuable information about the amount of formed oxygenated compounds in the ozonized methyl linoleate in order to use it to follow up ozone therapy and chemistry of ozonized vegetable oil. (author)

  14. Remote tuning of NMR probe circuits.

    Kodibagkar, V D; Conradi, M S

    2000-05-01

    There are many circumstances in which the probe tuning adjustments cannot be located near the rf NMR coil. These may occur in high-temperature NMR, low-temperature NMR, and in the use of magnets with small diameter access bores. We address here circuitry for connecting a fixed-tuned probe circuit by a transmission line to a remotely located tuning network. In particular, the bandwidth over which the probe may be remotely tuned while keeping the losses in the transmission line acceptably low is considered. The results show that for all resonant circuit geometries (series, parallel, series-parallel), overcoupling of the line to the tuned circuit is key to obtaining a large tuning bandwidth. At equivalent extents of overcoupling, all resonant circuit geometries have nearly equal remote tuning bandwidths. Particularly for the case of low-loss transmission line, the tuning bandwidth can be many times the tuned circuit's bandwidth, f(o)/Q. PMID:10783273

  15. A modularized pulse programmer for NMR spectroscopy

    A modularized pulse programmer for a NMR spectrometer is described. It consists of a networked PCI-104 single-board computer and a field programmable gate array (FPGA). The PCI-104 is dedicated to translate the pulse sequence elements from the host computer into 48-bit binary words and download these words to the FPGA, while the FPGA functions as a sequencer to execute these binary words. High-resolution NMR spectra obtained on a home-built spectrometer with four pulse programmers working concurrently demonstrate the effectiveness of the pulse programmer. Advantages of the module include (1) once designed it can be duplicated and used to construct a scalable NMR/MRI system with multiple transmitter and receiver channels, (2) it is a totally programmable system in which all specific applications are determined by software, and (3) it provides enough reserve for possible new pulse sequences

  16. Deuterium NMR, induced and intrinsic cholesteric lyomesophases

    Induced and intrinsic cholesteric lyotropic mesophases were studied. Induced cholesteric lyomesophases based on potassium laurate (KL) system, with small amounts of cholesterol added, were studied by deuterium NMR and by polarizing microscopy. Order profiles obtained from deuterium NMR of KL perdenderated chains in both induced cholesteric and normal mesophases were compared. The intrinsic cholesteric lyotropic mesophases were based on the amphiphile potassium N-lauroyl serinate (KLNS) in the resolved levo form. The study of the type I intrinsic cholesteric mesophase was made by optical microscopy under polarized light and the type II intrinsic cholesteric lyomesophase was characterized by deuterium NMR. The new texture was explained by the use of the theory of disclinations developed for thermotropic liquid crystals, specially for cholesteric type. (M.J.C.)

  17. Handbook of tritium NMR spectroscopy and applications

    Following a brief introduction, highlighting the importance of 3H nmr spectroscopy for tritium tracer studies, Chapter 1 deals with the theory of the method, the interpretation of spectra and other experimental aspects, emphasizing the importance of careful sample preparation and the special relationship of 3H nmr spectral detail to the wealth of published data for proton spectra. Chapter 2 reviews the current methods for labelling compounds with tritium and the relationship of observed patterns of labelling to these methods. Chapter 3 describes applications of 3H nmr spectroscopy to research in the life sciences which illustrate the power of the technique. Studies employing this analytical tool have revealed numerous interesting and indeed unexpected results in the behaviour of tritium atoms in labelled molecules. These studies have included applications of tritiated compounds in analytical and biochemical problems, in problems of catalysis and reaction mechanisms, and in other areas of scientific research. (author)

  18. Acoustic characterization of rehabilitated cloisters

    A. P. O. Carvalho; S. R. C. Vilela

    2008-01-01

    This paper presents the results of field measurements in eight rehabilitated cloisters of old monasteries in Portugal (length: 20 to 35 m and height: 3.3 to 6.3 m) regarding their acoustic behavior to two objective parameters: RT and RASTI. The goal is to characterize the acoustic effect of the rehabilitation done on theses spaces to adapt them to new uses. All these cloisters had recently their galleries#8217; openings to the central yard closed with glass panels. Simple formulas were obtain...

  19. Physical foundations of technical acoustics

    Malecki, I

    1969-01-01

    Physical Foundations of Technical Acoustics discusses theoretical foundations of acoustical engineering. It is not so much a technical compendium as a systematic statement of physical laws so conceived that technologists might find in it all the information they need to become acquainted with the physical meaning and mathematical expression of phenomena they encounter in their work. To facilitate the acquirement of notions, which lie beyond a layman's grasp, the plan of narration adopted consists in beginning with the simplest idealized cases and then gradually moving on to the truest possibl

  20. Acoustic concerns related to multi cultural societies

    Gade, Anders Christian

    2001-01-01

    Immigration has increased cultural diversity in western societies. The process of integrating immigrants into their host countries can be smoothed if acousticians learn to recognize (1) the acoustic traditions of immigrant cultures and (2) the specific acoustic needs of the new society members. Two related projects are discussed. The ``Cahrisma'' project (Conservation of Acoustical Heritage by the Revival and Identification of the Sinan's Mosque Acoustics) is sponsored by the European Commiss...

  1. Absorption boundary conditions for geomertical acoustics

    Jeong, Cheol-Ho

    2012-01-01

    Defining accurate acoustical boundary conditions is of crucial importance for room acoustic simulations. In predicting sound fields using phased geometrical acoustics methods, the absorption coefficients or surface impedances of the boundary surfaces can be used, but no guideline has been developed...... solutions. Two rectangular rooms with uniform and non-uniform absorption distributions are tested. It is concluded that the impedance and random incidence absorption boundary conditions produce reasonable results with some exceptions at low frequencies for acoustically soft materials....

  2. Calculating room acoustic parameters from pseudo-impulsive acoustic sources

    San Martin, Maria L.; Vela, Antonio; San Martin, Ricardo; Arana, Miguel A.

    2002-11-01

    The impulse response function provides complete information to predict the acoustic response of a room to an acoustic input of arbitrary characteristics. At this job study, small explosions of firecrackers are proposed to be used as pseudo-impulsive acoustics sources to determine some acoustic parameters of a room such as reverberation time, definition, and clarity, comparing these results to those obtained with other techniques. A previous characterization of these sources allows us to state that they can be used for this purpose because they are, in practice, omnidirectional, their temporary pattern is highly repetitive and their spectral power is, as well, repetitive and with enough power in octave bands from 125 Hz to 8 kHz. If the linear time-invariant system impulse response h(t) is known, output signal s(t) regarding any arbitrary signal s(t) can be obtained. For our pseudo-impulsive sources, the output signal s(t) has been taken as impulse response h(t). Using the integrated impulse response method suggested by Schroeder, it has been stated that both the mean values and standard deviations for some parameters are practically identical to results obtained with other usual techniques. (To be presented in Spanish.)

  3. Acoustic Test Characterization of Melamine Foam for Usage in NASA's Payload Fairing Acoustic Attenuation Systems

    Hughes, William O.; McNelis, Anne M.; McNelis, Mark E.

    2014-01-01

    The external acoustic liftoff levels predicted for NASA's future heavy lift launch vehicles are expected to be significantly higher than the environment created by today's commercial launch vehicles. This creates a need to develop an improved acoustic attenuation system for future NASA payload fairings. NASA Glenn Research Center initiated an acoustic test series to characterize the acoustic performance of melamine foam, with and without various acoustic enhancements. This testing was denoted as NEMFAT, which stands for NESC Enhanced Melamine Foam Acoustic Test, and is the subject of this paper. Both absorption and transmission loss testing of numerous foam configurations were performed at the Riverbank Acoustical Laboratory in July 2013. The NEMFAT test data provides an initial acoustic characterization and database of melamine foam for NASA. Because of its acoustic performance and lighter mass relative to fiberglass blankets, melamine foam is being strongly considered for use in the acoustic attenuation systems of NASA's future launch vehicles.

  4. NMR Microscopy - Micron-Level Resolution.

    Kwok, Wing-Chi Edmund

    1990-01-01

    Nuclear Magnetic Resonance Imaging (MRI) has been developed into a powerful and widely used diagnostic tool since the invention of techniques using linear magnetic field gradients in 1973. The variety of imaging contrasts obtainable in MRI, such as spin density, relaxation times and flow rate, gives MRI a significant advantage over other imaging techniques. For common diagnostic applications, image resolutions have been in the order of millimeters with slice thicknesses in centimeters. For many research applications, however, resolutions in the order of tens of microns or smaller are needed. NMR Imaging in these high resolution disciplines is known as NMR microscopy. Compared with conventional microscopy, NMR microscopy has the advantage of being non-invasive and non-destructive. The major obstacles of NMR microscopy are low signal-to-noise ratio and effects due to spin diffusion. To overcome these difficulties, more sensitive RF probes and very high magnetic field gradients have to be used. The most effective way to increase sensitivity is to build smaller probes. Microscope probes of different designs have been built and evaluated. Magnetic field gradient coils that can produce linear field gradients up to 450 Gauss/cm were also assembled. In addition, since microscope probes often employ remote capacitors for RF tuning, the associated signal loss in the transmission line was studied. Imaging experiments have been carried out in a 2.1 Tesla small bore superconducting magnet using the typical two-dimensional spin warp imaging technique. Images have been acquired for both biological and non-biological samples. The highest resolution was obtained in an image of a nerve bundle from the spinal cord of a racoon and has an in-plane resolution of 4 microns. These experiments have demonstrated the potential application of NMR microscopy to pathological research, nervous system study and non -destructive testings of materials. One way to further improve NMR microscopy is

  5. The Quiet Renaissance of Protein NMR

    Barrett, Paul J.; Chen, Jiang; Cho, Min-Kyu; Kim, Ji-Hun; Lu, Zhenwei; Mathew, Sijo; Peng, Dungeng; Song, Yuanli; Van Horn, Wade D.; Zhuang, Tiandi; Sönnichsen, Frank D.; Sanders, Charles R.

    2013-01-01

    From roughly 1985 through the start of the new millennium, the cutting edge of solution protein nuclear magnetic resonance (NMR) spectroscopy was to a significant extent driven by the aspiration to determine structures. Here we survey recent advances in protein NMR that herald a renaissance in which a number of its most important applications reflect the broad problem-solving capability displayed by this method during its classical era during the 1970s and early 80s. “Without receivers fitted and kept in order, the air may tingle and thrill with the message, but it will not reach my spirit and consciousness.” Mary Slessor, Calabar, circa 1910 PMID:23368985

  6. Acoustically swept rotor. [helicopter noise reduction

    Schmitz, F. H.; Boxwell, D. A.; Vause, R. (Inventor)

    1979-01-01

    Impulsive noise reduction is provided in a rotor blade by acoustically sweeping the chord line from root to tip so that the acoustic radiation resulting from the summation of potential singularities used to model the flow about the blade tend to cancel for all times at an observation point in the acoustic far field.

  7. Predicting and auralizing acoustics in classrooms

    Christensen, Claus Lynge

    2005-01-01

    Although classrooms have fairly simple geometries, this type of room is known to cause problems when trying to predict their acoustics using room acoustics computer modeling. Some typical features from a room acoustics point of view are: Parallel walls, low ceilings (the rooms are flat), uneven...

  8. Aero-acoustic Computations of Wind Turbines

    Shen, Wen Zhong; Michelsen, Jess; Sørensen, Jens Nørkær

    A numerical algorithm for acoustic noise generation is extended to 3D flows. The approach involves two parts comprising a viscous incompressible flow part and an inviscid acoustic part. In order to simulate noise generated from a wind turbine, the incompressible and acoustic equations are written...

  9. Design of acoustic devices by topology optimization

    Sigmund, Ole; Jensen, Jakob Søndergaard

    The goal of this study is to design and optimize structures and devices that are subjected to acoustic waves. Examples are acoustic lenses, sound walls, waveguides and loud speakers. We formulate the design problem as a topology optimization problem, i.e. distribute material in a design domain such...... that the acoustic response is optimized....

  10. Optical measurement of acoustic radiation pressure of the near-field acoustic levitation through transparent object

    Nakamura, Satoshi; Sasao, Yasuhiro; Katsura, Kogure; Naoki, Kondo

    2013-01-01

    It is known that macroscopic objects can be levitated for few to several hundred micrometers by near-field acoustic field and this phenomenon is called near-field acoustic levitation (NFAL). Although there are various experiments conducted to measure integrated acoustic pressure on the object surface, up to now there was no direct method to measure pressure distribution. In this study we measured the acoustic radiation pressure of the near-field acoustic levitation via pressure-sensitive paint.

  11. Performance of the WeNMR CS-Rosetta3 web server in CASD-NMR

    van der Schot, Gijs; Bonvin, Alexandre M. J. J.

    2016-01-01

    We present here the performance of the WeNMR CS-Rosetta3 web server in CASD-NMR, the critical assessment of automated structure determination by NMR. The CS-Rosetta server uses only chemical shifts for structure prediction, in combination, when available, with a post-scoring procedure based on unassigned NOE lists (Huang et al. in J Am Chem Soc 127:1665–1674, 2005b, doi:10.1021/ja047109h). We compare the original submissions using a previous version of the server based on Rosetta version 2.6 ...

  12. Nonlinear acoustic-gravity waves

    Stenflo, Lennart; Shukla, P. K.

    2009-01-01

    Previous results on nonlinear acoustic-gravity waves are reconsidered. It turns out that the mathematical techniques used are somewhat similar to those already adopted by the plasma physics community. Consequently, a future interaction between physicists On different fields, e.g in meteorology and plasma physics, can be very fruitful.

  13. Acoustics in the Martian Atmosphere

    Williams, J.-P.

    2000-10-01

    With the advent of the first attempt to deliver an acoustic microphone to the Martian surface aboard the failed Mars Polar Lander, there has been growing interests in the development of acoustic sensors to compliment scientific payloads on future spacecraft. Terrestrial scientist have been very successful in using infrasound (sound at frequencies below human detection, detect and monitor atmospheric phenomena related to weather, tornadoes, mountain waves, microbaroms, ionospheric and auroral disturbances, and meteror/fireballs, as well as anthropogenic sources such as aircraft and nuclear explosions. Sounds on Mars at the audible frequencies (20 Hz to 20 kHz) will be severely attenuated due to viscous relaxation and thermal diffusion (collectively referred to as classical attenuation) which will be much more severe in the colder, less dense Martian atmosphere. Molecular relaxation of carbon dioxide will also contribute to the sound absorption in the lower audible frequencies. Since classical attenuation increases as a function of the frequency squared, at low infrasonic frequencies ( < 10 Hz), classical attenuation becomes less significant and sound absorption in the Martian atmosphere becomes more similar to that of the terrestrial atmosphere for the same frequencies. At these longer wavelengths, geometric spreading will dominate as the source of attenuation as the acoustic energy is spread out over an ever increasing spherical wave front. This implies that infrasound (10 to 0.01 Hz) will be a useful frequency range for future acoustic sensors developed for scientific payloads delivered to the Martian surface.

  14. Satellite and acoustic tracking device

    Berumen, Michael L.

    2014-02-20

    The present invention relates a method and device for tracking movements of marine animals or objects in large bodies of water and across significant distances. The method and device can track an acoustic transmitter attached to an animal or object beneath the ocean surface by employing an unmanned surface vessel equipped with a hydrophone array and GPS receiver.

  15. Digitization of acoustic sounder data

    A method of archiving acoustic sounder data in a format compatible with a computer is used development. The collected data will be used to compile a climatology of the atmospheric surface boundary layer to predict the transport and diffusion of atmospheric pollutants

  16. SES and Acoustics at GSFC

    Hogue, Patrick

    2008-01-01

    This paper presents air and surface cleanliness characterization of the acoustics test facility and large (SES) thermal vacuum chamber at Goddard Space flight Center in Greenbelt, MD during the New Horizons Pluto probe program. It is shown that slow back-fill of the SES chamber is necessary to prevent excessive particle redistribution.

  17. Topology optimization for acoustic problems

    Dühring, Maria Bayard

    In this paper a method to control acoustic properties in a room with topology optimization is presented. It is shown how the squared sound pressure amplitude in a certain part of a room can be minimized by distribution of material in a design domain along the ceiling in 2D and 3D. Nice 0-1 designs...

  18. Acoustic optic hybrid (AOH) sensor

    Matthews; Arrieta

    2000-09-01

    The ability of laser vibrometers to receive and process acoustic echoes from the water surface above a submerged target is established and evaluated. Sonar echoes from a submerged target are collected from the water surface by a laser vibrometer. Feasibility of this approach to sensing underwater sound is demonstrated. If the acoustic excitation at an otherwise undisturbed water surface is 195 to 168 dB re: 1 microPa, signal-to-noise ratio (SNR), at the vibrometer output, is shown to range from about 46 to 6 dB. Capillary waves and gravity waves at the water surface are expected and shown to have some destructive effect on the process of echo retrieval. A series of experiments to quantify the surface wave effects is described. The wave experiment results are reported. A successful attempt to acquire echoes from a submerged target over a grid of points for further processing into a three-dimensional image is made and described. The data acquisition and beamforming techniques constitute a three-dimensional, acoustic optic, synthetic aperture sonar (SAS). Beamformed images are included. For an aircraft towing acoustic sensors through the water with a mechanical link, this technique holds the promise of increased safety and improved fuel efficiency. PMID:11008811

  19. Acoustics SIMOPS: managing the unnecessary

    Hanton, Samuel John [Nautronix Marine Technology Solutions, Rio de Janeiro, RJ (Brazil)

    2012-07-01

    Time is money, and offshore operations are expensive. The desire therefore, is to increase efficiency through the condensing of schedules. This inevitably leads to SIMOPS of some degree, and this paper discusses SIMOPS along with, more specifically, the challenges they provide to acoustic positioning. (author)

  20. Longitudinal bulk acoustic mass sensor

    Hales, Jan Harry; Teva, Jordi; Boisen, Anja;

    2009-01-01

    A polycrystalline silicon longitudinal bulk acoustic cantilever is fabricated and operated in air at 51 MHz. A mass sensitivity of 100 Hz/fg (1 fg=10(-15) g) is obtained from the preliminary experiments where a minute mass is deposited on the device by means of focused ion beam. The total noise i...

  1. Aerosol behaviour in an acoustic field

    The average size of an aerosol submitted to acoustic waves is increased. This results from coagulation of the finest particles on the largest ones. The mechanisms responsible for acoustic agglomeration are mentioned. An experimental apparatus was developed in order to control the evolution of aerosol distribution in an acoustic field. Important deposition on the walls of the agglomeration chamber was observed as a consequence of the acoustically induced turbulent flow. Finally, a dimensionless relationship was established between deposition rates and particle diameters as a function of experimental parameters (aeraulic and acoustic conditions, etc...)

  2. Determining Equilibrium Position For Acoustical Levitation

    Barmatz, M. B.; Aveni, G.; Putterman, S.; Rudnick, J.

    1989-01-01

    Equilibrium position and orientation of acoustically-levitated weightless object determined by calibration technique on Earth. From calibration data, possible to calculate equilibrium position and orientation in presence of Earth gravitation. Sample not levitated acoustically during calibration. Technique relies on Boltzmann-Ehrenfest adiabatic-invariance principle. One converts resonant-frequency-shift data into data on normalized acoustical potential energy. Minimum of energy occurs at equilibrium point. From gradients of acoustical potential energy, one calculates acoustical restoring force or torque on objects as function of deviation from equilibrium position or orientation.

  3. Benzhydroximic Acids - NMR Study of Trimethylsilyl Derivatives

    Schraml, Jan; Kvíčalová, Magdalena; Soukupová, Ludmila; Blechta, Vratislav; Exner, Otto

    2000-01-01

    Roč. 597, 1-2 (2000), s. 200-205. ISSN 0022-328X R&D Projects: GA AV ČR IAA4072605; GA MŠk LB98233 Keywords : trimethylsilyl derivatives * substituted benzhydroximic acids * NMR chemical shifts Subject RIV: CC - Organic Chemistry Impact factor: 1.632, year: 2000

  4. Responsibilities of NMR application in research

    NMR investigations in clinical and/or scientific studies may be covered by different radiation protection regulations and legal liability responsibilities. The following topics are discussed: incidental findings, applicability to the situation in radiological hospitals, explicit abandonment of probands/patients, liability of the clinic, liability with respect to contrast agent administration, creation of additional imaging, attendance of radiologists, information requirements.

  5. NMR study of multiferroic iron niobate perovskites

    Kouřil, K.; Chlan, V.; Štěpánková, H.; Řezníček, R.; Laguta, Valentyn; Raevski, I. P.

    Warszawa : Polish Academy of Sciences, 2015, s. 234-236. ISSN 0587-4246. [The European Conference PHYSICS OF MAGNETISM 2014/PM'14/. Poznań (PL), 23.06.2014-27.06.2014] R&D Projects: GA ČR GA13-11473S Institutional support: RVO:68378271 Keywords : multiferroics * magnetism * NMR Subject RIV: BM - Solid Matter Physics ; Magnetism

  6. The bar coil for NMR tomograph

    The bar coil (bi-planar) for the NMR tomograph, designed for medical diagnostics, has been described. The tests of coil shown that it generates good homogenous magnetic field in a big volume what results in improving of the signal-to-noise ratio

  7. Molecular dynamics - NMR experiments and simulations

    Dračínský, Martin; Hodgkinson, P.; Kessler, Jiří; Bouř, Petr

    Brno : Masaryk University Press, 2015 - (Sklenář, V.). s. 277-278 ISBN 978-80-210-7890-1. [EUROMAR 2015. 05.07.2015-10.07.2015, Praha] Institutional support: RVO:61388963 Keywords : molecular dynamics * NMR spectroscopy * MD simulations Subject RIV: CF - Physical ; Theoretical Chemistry

  8. 3D Reconstruction of NMR Images

    Peter Izak; Milan Smetana; Libor Hargas; Miroslav Hrianka; Pavol Spanik

    2007-01-01

    This paper introduces experiment of 3D reconstruction NMR images scanned from magnetic resonance device. There are described methods which can be used for 3D reconstruction magnetic resonance images in biomedical application. The main idea is based on marching cubes algorithm. For this task was chosen sophistication method by program Vision Assistant, which is a part of program LabVIEW.

  9. Novel NMR Method for Organic Aerosol Analysis

    Horník, Štěpán

    Prague: Institute of Chemical Process Fundamental of the CAS, v. v. i, 2015 - (Bendová, M.; Wagner, Z.), s. 20-21 ISBN 978-80-86186-70-2. [Bažant Postgraduate Conference 2015. Prague (CZ)] Institutional support: RVO:67985858 Keywords : nmr method * organic aerosol composition * analysis Subject RIV: CF - Physical ; Theoretical Chemistry

  10. Some exercises in quantitative NMR imaging

    The articles represented in this thesis result from a series of investigations that evaluate the potential of NMR imaging as a quantitative research tool. In the first article the possible use of proton spin-lattice relaxation time T1 in tissue characterization, tumor recognition and monitoring tissue response to radiotherapy is explored. The next article addresses the question whether water proton spin-lattice relaxation curves of biological tissues are adequately described by a single time constant T1, and analyzes the implications of multi-exponentiality for quantitative NMR imaging. In the third article the use of NMR imaging as a quantitative research tool is discussed on the basis of phantom experiments. The fourth article describes a method which enables unambiguous retrieval of sign information in a set of magnetic resonance images of the inversion recovery type. The next article shows how this method can be adapted to allow accurate calculation of T1 pictures on a pixel-by-pixel basis. The sixth article, finally, describes a simulation procedure which enables a straightforward determination of NMR imaging pulse sequence parameters for optimal tissue contrast. (orig.)

  11. Novel NMR Method for Organic Aerosol Analysis

    Horník, Štěpán

    Prague : Institute of Chemical Process Fundamental of the CAS, v. v. i, 2015 - (Bendová, M.; Wagner, Z.), s. 20-21 ISBN 978-80-86186-70-2. [Bažant Postgraduate Conference 2015. Prague (CZ)] Institutional support: RVO:67985858 Keywords : nmr method * organic aerosol composition * analysis Subject RIV: CF - Physical ; Theoretical Chemistry

  12. Hyperpolarized NMR Probes for Biological Assays

    Sebastian Meier

    2014-01-01

    Full Text Available During the last decade, the development of nuclear spin polarization enhanced (hyperpolarized molecular probes has opened up new opportunities for studying the inner workings of living cells in real time. The hyperpolarized probes are produced ex situ, introduced into biological systems and detected with high sensitivity and contrast against background signals using high resolution NMR spectroscopy. A variety of natural, derivatized and designed hyperpolarized probes has emerged for diverse biological studies including assays of intracellular reaction progression, pathway kinetics, probe uptake and export, pH, redox state, reactive oxygen species, ion concentrations, drug efficacy or oncogenic signaling. These probes are readily used directly under natural conditions in biofluids and are often directly developed and optimized for cellular assays, thus leaving little doubt about their specificity and utility under biologically relevant conditions. Hyperpolarized molecular probes for biological NMR spectroscopy enable the unbiased detection of complex processes by virtue of the high spectral resolution, structural specificity and quantifiability of NMR signals. Here, we provide a survey of strategies used for the selection, design and use of hyperpolarized NMR probes in biological assays, and describe current limitations and developments.

  13. SQUID detected NMR in microtesla magnetic fields

    Matlachov, Andrei N.; Volegov, Petr L.; Espy, Michelle A.; George, John S.; Kraus, Robert H.

    2004-09-01

    We have built an NMR system that employs a superconducting quantum interference device (SQUID) detector and operates in measurement fields of 2-25 μT. The system uses a pre-polarizing field from 4 to 30 mT generated by simple room-temperature wire-wound coils that are turned off during measurements. The instrument has an open geometry with samples located outside the cryostat at room-temperature. This removes constraints on sample size and allows us to obtain signals from living tissue. We have obtained 1H NMR spectra from a variety of samples including water, mineral oil, and a live frog. We also acquired gradient encoded free induction decay (FID) data from a water-plastic phantom in the μT regime, from which simple projection images were reconstructed. NMR signals from samples inside metallic containers have also been acquired. This is possible because the penetration skin depth is much greater at the low operating frequencies of this system than for conventional systems. Advantages to ultra-low field NMR measurements include lower susceptibility artifacts caused by high strength polarizing and measurement fields, and negligible line width broadening due to measurement field inhomogeneity, reducing the burden of producing highly homogeneous fields.

  14. Combining solid-state NMR spectroscopy with first-principles calculations - a guide to NMR crystallography.

    Ashbrook, Sharon E; McKay, David

    2016-06-01

    Recent advances in the application of first-principles calculations of NMR parameters to periodic systems have resulted in widespread interest in their use to support experimental measurement. Such calculations often play an important role in the emerging field of "NMR crystallography", where NMR spectroscopy is combined with techniques such as diffraction, to aid structure determination. Here, we discuss the current state-of-the-art for combining experiment and calculation in NMR spectroscopy, considering the basic theory behind the computational approaches and their practical application. We consider the issues associated with geometry optimisation and how the effects of temperature may be included in the calculation. The automated prediction of structural candidates and the treatment of disordered and dynamic solids are discussed. Finally, we consider the areas where further development is needed in this field and its potential future impact. PMID:27117884

  15. Handbook of Signal Processing in Acoustics

    Havelock, David; Vorländer, Michael

    2009-01-01

    The Handbook of Signal Processing in Acoustics presents signal processing as it is practiced in the field of acoustics. The Handbook is organized by areas of acoustics, with recognized leaders coordinating the self-contained chapters of each section. It brings together a wide range of perspectives from over 100 authors to reveal the interdisciplinary nature of signal processing in acoustics. Success in acoustic applications often requires juggling both the acoustic and the signal processing parameters of the problem. This handbook brings the key issues from both into perspective and is complementary to other reference material on the two subjects. It is a unique resource for experts and practitioners alike to find new ideas and techniques within the diversity of signal processing in acoustics.

  16. e-NMR gLite grid enabled infrastructure

    Ferreira, N.L.; Wassenaar, T.A.; de Vries, S.J.; van Dijk, M.; van der Schot, G.; van der Zwan, J.; Boelens, R.; Bonvin, A.M.J.J.; Giachetti, A.; Carotenuto, D.; Rosato, A.; Bertini, I.; Herrmann, T.; Bagaria, A.; Zharavin, V.; Jonker, H.R.A.; Güntert, P.; Schwalbe, H.; Vranken, W.F.

    2010-01-01

    The e-NMR project is an European e-infrastructure that aims at providing the bio-NMR community with a software platform integrating and streamlining computational approaches necessary for NMR data analysis. The infrastructure is grid enabled with fteen gLite based partners sharing computational reso

  17. Several Applications of NMR in Organic Chemistry Research

    CUI yuxin; LIU xuehui; XU hao

    2001-01-01

    @@ Modem NMR techniques, especially 2D-NMR have presented their powerful application in organic chemistry. Not only in structural determination, mechanism investigation, but also in solution conformation study for natural products. In this paper, various pulse field gradient NMR techniques such as COSY, NOESY, HMBC and HMQC were combined to study these problems.

  18. Petrophysical properties of greensand as predicted from NMR measurements

    Hossain, Zakir; Grattoni, Carlos A.; Solymar, Mikael;

    2011-01-01

    ABSTRACT: Nuclear magnetic resonance (NMR) is a useful tool in reservoir evaluation. The objective of this study is to predict petrophysical properties from NMR T2 distributions. A series of laboratory experiments including core analysis, capillary pressure measurements, NMR T2 measurements and i...

  19. Performance of the WeNMR CS-Rosetta3 web server in CASD-NMR

    We present here the performance of the WeNMR CS-Rosetta3 web server in CASD-NMR, the critical assessment of automated structure determination by NMR. The CS-Rosetta server uses only chemical shifts for structure prediction, in combination, when available, with a post-scoring procedure based on unassigned NOE lists (Huang et al. in J Am Chem Soc 127:1665–1674, 2005b, doi: 10.1021/ja047109h 10.1021/ja047109h ). We compare the original submissions using a previous version of the server based on Rosetta version 2.6 with recalculated targets using the new R3FP fragment picker for fragment selection and implementing a new annotation of prediction reliability (van der Schot et al. in J Biomol NMR 57:27–35, 2013, doi: 10.1007/s10858-013-9762-6 10.1007/s10858-013-9762-6 ), both implemented in the CS-Rosetta3 WeNMR server. In this second round of CASD-NMR, the WeNMR CS-Rosetta server has demonstrated a much better performance than in the first round since only converged targets were submitted. Further, recalculation of all CASD-NMR targets using the new version of the server demonstrates that our new annotation of prediction quality is giving reliable results. Predictions annotated as weak are often found to provide useful models, but only for a fraction of the sequence, and should therefore only be used with caution

  20. Solid-state NMR studies of supercapacitors.

    Griffin, John M; Forse, Alexander C; Grey, Clare P

    2016-01-01

    Electrochemical double-layer capacitors, or 'supercapacitors' are attracting increasing attention as high-power energy storage devices for a wide range of technological applications. These devices store charge through electrostatic interactions between liquid electrolyte ions and the surfaces of porous carbon electrodes. However, many aspects of the fundamental mechanism of supercapacitance are still not well understood, and there is a lack of experimental techniques which are capable of studying working devices. Recently, solid-state NMR has emerged as a powerful tool for studying the local environments and behaviour of electrolyte ions in supercapacitor electrodes. In this Trends article, we review these recent developments and applications. We first discuss the basic principles underlying the mechanism of supercapacitance, as well as the key NMR observables that are relevant to the study of supercapacitor electrodes. We then review some practical aspects of the study of working devices using ex situ and in situ methodologies and explain the key advances that these techniques have allowed on the study of supercapacitor charging mechanisms. NMR experiments have revealed that the pores of the carbon electrodes contain a significant number of electrolyte ions in the absence of any charging potential. This has important implications for the molecular mechanisms of supercapacitance, as charge can be stored by different ion adsorption/desorption processes. Crucially, we show how in situ NMR experiments can be used to quantitatively study and characterise the charging mechanism, with the experiments providing the most detailed picture of charge storage to date, offering the opportunity to design enhanced devices. Finally, an outlook for future directions for solid-state NMR in supercapacitor research is offered. PMID:26974032

  1. NMR Constraints Analyser: a web-server for the graphical analysis of NMR experimental constraints.

    Heller, Davide Martin; Giorgetti, Alejandro

    2010-07-01

    Nuclear magnetic resonance (NMR) spectroscopy together with X-ray crystallography, are the main techniques used for the determination of high-resolution 3D structures of biological molecules. The output of an NMR experiment includes a set of lower and upper limits for the distances (constraints) between pairs of atoms. If the number of constraints is high enough, there will be a finite number of possible conformations (models) of the macromolecule satisfying the data. Thus, the more constraints are measured, the better defined these structures will be. The availability of a user-friendly tool able to help in the analysis and interpretation of the number of experimental constraints per residue, is thus of valuable importance when assessing the levels of structure definition of NMR solved biological macromolecules, in particular, when high-quality structures are needed in techniques such as, computational biology approaches, site-directed mutagenesis experiments and/or drug design. Here, we present a free publicly available web-server, i.e. NMR Constraints Analyser, which is aimed at providing an automatic graphical analysis of the NMR experimental constraints atom by atom. The NMR Constraints Analyser server is available from the web-page http://molsim.sci.univr.it/constraint. PMID:20513646

  2. USE OF SCALE MODELING FOR ARCHITECTURAL ACOUSTIC MEASUREMENTS

    ERÖZ, Ferhat

    2013-01-01

    In recent years, acoustic science and hearing has become important. Acoustic design used in tests of acoustic devices is crucial. Sound propagation is a complex subject, especially inside enclosed spaces. From the 19th century on, the acoustic measurements and tests were carried out using modeling techniques that are based on room acoustic measurement parameters.In this study, the effects of architectural acoustic design of modeling techniques and acoustic parameters were studied. In this con...

  3. APPLICATION OF DOMAIN DECOMPOSITION IN ACOUSTIC AND STRUCTURAL ACOUSTIC ANALYSIS

    2007-01-01

    Conventional element based methods for modeling acoustic problems are limited to low-frequency applications due to the huge computational efforts. For high-frequency applications, probabilistic techniques, such as statistical energy analysis (SEA), are used. For mid-frequency range, currently no adequate and mature simulation methods exist. Recently, wave based method has been developed which is based on the indirect TREFFTZ approach and has shown to be able to tackle problems in the mid-frequency range. In contrast with the element based methods, no discretization is required. A sufficient, but not necessary, condition for convergence of this method is that the acoustic problem domain is convex. Non-convex domains have to be partitioned into a number of (convex) subdomains. At the interfaces between subdomains, specific coupling conditions have to be imposed. The considered two-dimensional coupled vibro-acoustic problem illustrates the beneficial convergence rate of the proposed wave based prediction technique with high accuracy. The results show the new technique can be applied up to much higher frequencies.

  4. Acoustic spin pumping in magnetoelectric bulk acoustic wave resonator

    Polzikova, N. I.; Alekseev, S. G.; Pyataikin, I. I.; Kotelyanskii, I. M.; Luzanov, V. A.; Orlov, A. P.

    2016-05-01

    We present the generation and detection of spin currents by using magnetoelastic resonance excitation in a magnetoelectric composite high overtone bulk acoustic wave (BAW) resonator (HBAR) formed by a Al-ZnO-Al-GGG-YIG-Pt structure. Transversal BAW drives magnetization oscillations in YIG film at a given resonant magnetic field, and the resonant magneto-elastic coupling establishes the spin-current generation at the Pt/YIG interface. Due to the inverse spin Hall effect (ISHE) this BAW-driven spin current is converted to a dc voltage in the Pt layer. The dependence of the measured voltage both on magnetic field and frequency has a resonant character. The voltage is determined by the acoustic power in HBAR and changes its sign upon magnetic field reversal. We compare the experimentally observed amplitudes of the ISHE electrical field achieved by our method and other approaches to spin current generation that use surface acoustic waves and microwave resonators for ferromagnetic resonance excitation, with the theoretically expected values.

  5. Acoustic spin pumping in magnetoelectric bulk acoustic wave resonator

    N. I. Polzikova

    2016-05-01

    Full Text Available We present the generation and detection of spin currents by using magnetoelastic resonance excitation in a magnetoelectric composite high overtone bulk acoustic wave (BAW resonator (HBAR formed by a Al-ZnO-Al-GGG-YIG-Pt structure. Transversal BAW drives magnetization oscillations in YIG film at a given resonant magnetic field, and the resonant magneto-elastic coupling establishes the spin-current generation at the Pt/YIG interface. Due to the inverse spin Hall effect (ISHE this BAW-driven spin current is converted to a dc voltage in the Pt layer. The dependence of the measured voltage both on magnetic field and frequency has a resonant character. The voltage is determined by the acoustic power in HBAR and changes its sign upon magnetic field reversal. We compare the experimentally observed amplitudes of the ISHE electrical field achieved by our method and other approaches to spin current generation that use surface acoustic waves and microwave resonators for ferromagnetic resonance excitation, with the theoretically expected values.

  6. Squid detected NMR and MRI at ultralow fields

    Clarke, John; Pines, Alexander; McDermott, Robert F.; Trabesinger, Andreas H.

    2008-12-16

    Nuclear magnetic resonance (NMR) signals are detected in microtesla fields. Prepolarization in millitesla fields is followed by detection with an untuned dc superconducting quantum interference device (SQUID) magnetometer. Because the sensitivity of the SQUID is frequency independent, both signal-to-noise ratio (SNR) and spectral resolution are enhanced by detecting the NMR signal in extremely low magnetic fields, where the NMR lines become very narrow even for grossly inhomogeneous measurement fields. MRI in ultralow magnetic field is based on the NMR at ultralow fields. Gradient magnetic fields are applied, and images are constructed from the detected NMR signals.

  7. Solid state NMR of biopolymers and synthetic polymers

    Solid state NMR has been invaluable in evaluating the structure, phase separation, and dynamics of polymers. Because polymers are generally used in the solid state, solid state NMR is especially powerful because it provides information about the materials in their native state. This review gives a general overview of solid state NMR, concentrating on solid state 13 C and 2 H NMR. It then focuses on two examples: the biopolymer spider silka and the engineering material polyurethane. It illustrates how solid state NMR can provide new information about synthetic and bio-polymers. (author)

  8. Acoustic metamaterial design and applications

    Zhang, Shu

    The explosion of interest in metamaterials is due to the dramatically increased manipulation ability over light as well as sound waves. This material research was stimulated by the opportunity to develop an artificial media with negative refractive index and the application in superlens which allows super-resolution imaging. High-resolution acoustic imaging techniques are the essential tools for nondestructive testing and medical screening. However, the spatial resolution of the conventional acoustic imaging methods is restricted by the incident wavelength of ultrasound. This is due to the quickly fading evanescent fields which carry the subwavelength features of objects. By focusing the propagating wave and recovering the evanescent field, a flat lens with negative-index can potentially overcome the diffraction limit. We present the first experimental demonstration of focusing ultrasound waves through a flat acoustic metamaterial lens composed of a planar network of subwavelength Helmholtz resonators. We observed a tight focus of half-wavelength in width at 60.5 KHz by imaging a point source. This result is in excellent agreement with the numerical simulation by transmission line model in which we derived the effective mass density and compressibility. This metamaterial lens also displays variable focal length at different frequencies. Our experiment shows the promise of designing compact and light-weight ultrasound imaging elements. Moreover, the concept of metamaterial extends far beyond negative refraction, rather giving enormous choice of material parameters for different applications. One of the most interesting examples these years is the invisible cloak. Such a device is proposed to render the hidden object undetectable under the flow of light or sound, by guiding and controlling the wave path through an engineered space surrounding the object. However, the cloak designed by transformation optics usually calls for a highly anisotropic metamaterial, which

  9. Cylindrical acoustic levitator/concentrator

    Kaduchak, Gregory (Los Alamos, NM); Sinha, Dipen N. (Los Alamos, NM)

    2002-01-01

    A low-power, inexpensive acoustic apparatus for levitation and/or concentration of aerosols and small liquid/solid samples having particulates up to several millimeters in diameter in air or other fluids is described. It is constructed from a commercially available, hollow cylindrical piezoelectric crystal which has been modified to tune the resonance frequency of the breathing mode resonance of the crystal to that of the interior cavity of the cylinder. When the resonance frequency of the interior cylindrical cavity is matched to the breathing mode resonance of the cylindrical piezoelectric transducer, the acoustic efficiency for establishing a standing wave pattern in the cavity is high. The cylinder does not require accurate alignment of a resonant cavity. Water droplets having diameters greater than 1 mm have been levitated against the force of gravity using; less than 1 W of input electrical power. Concentration of aerosol particles in air is also demonstrated.

  10. Cooperative OFDM underwater acoustic communications

    Cheng, Xilin; Cheng, Xiang

    2016-01-01

    Following underwater acoustic channel modeling, this book investigates the relationship between coherence time and transmission distances. It considers the power allocation issues of two typical transmission scenarios, namely short-range transmission and medium-long range transmission. For the former scenario, an adaptive system is developed based on instantaneous channel state information. The primary focus is on cooperative dual-hop orthogonal frequency division multiplexing (OFDM). This book includes the decomposed fountain codes designed to enable reliable communications with higher energy efficiency. It covers the Doppler Effect, which improves packet transmission reliability for effective low-complexity mirror-mapping-based intercarrier interference cancellation schemes capable of suppressing the intercarrier interference power level. Designed for professionals and researchers in the field of underwater acoustic communications, this book is also suitable for advanced-level students in electrical enginee...

  11. Sandia Helicopter Acoustic Detector (SHAD)

    Arlowe, H. D.

    1982-05-01

    The Sandia Helicopter Acoustic Detector was developed to provide a low cost alternative to radar for countering the helicopter threat at new DOE facilities. The main buildings of these new designs are generally hardened to provide significant delay to a helicopter borne adversary team. Under these circumstances the sensor is only required to detect helicopters that are in their final landing phase and at close range (less than 75 m). This short detection range allows the use of a fairly simple acoustic detection algorithm without making the system overly sensitive to wind noise, motor vehicles, and ventilation/heat exchange blowers. This work was sponsored by the Department of Energy/Office of Safeguards and Security as part of the overall Sandia Fixed Facility Physical Protection Program.

  12. : FMRI in acoustic trauma sequelae

    Job, Agnès; Pons, Yoann; Lamalle, Laurent; Jaillard, Assia; Buck, Karl; Segebarth, Christoph; Delon-Martin, Chantal

    2012-01-01

    International audience The most common consequences of acute acoustic trauma (AAT) are hearing loss at frequencies above 3 kHz and tinnitus. In this study, we have used functional Magnetic Resonance Imaging (fMRI) to visualize neuronal activation patterns in military adults with AAT and various tinnitus sequelae during an auditory "oddball" attention task. AAT subjects displayed overactivities principally during reflex of target sound detection, in sensorimotor areas and in emotion-related...

  13. Virtual Reality for Architectural Acoustics

    Vorländer, Michael; Schröder, Dirk; PELZER, Sönke; Wefers, Frank

    2014-01-01

    Over the last decades, powerful prediction models have been developed in architectural acoustics, which are used for the calculation of sound propagation in indoor and/or outdoor scenarios. Sound insulation is predicted rather precisely by using direct and flanking transmission models of sound and vibration propagation. These prediction tools are already in use in architectural design and consulting. For the extension towards virtual reality (VR) systems, it is required to accelerate the pred...

  14. Acoustic streaming in superfluid helium

    Quantitative measurements of acoustic streaming velocity in liquid helium as a function of sound intensity (up to the cavitation threshold), frequency (1, 3, and 10 MHz), and temperature (1.43 K< or =T< or =2.19 K) are reported. A transition to superfluid turbulence, several flow regions and flow fluctuations are observed. Comparison with the predictions of the second-order Khalatnikov two- fluid hydrodynamic equations indicates good functional and quantitative agreement

  15. Tunable acoustic double negativity metamaterial

    Z. Liang; Willatzen, M.; Li, J.; Christensen, J

    2012-01-01

    Man-made composite materials called “metamaterials” allow for the creation of unusual wave propagation behavior. Acoustic and elastic metamaterials in particular, can pave the way for the full control of sound in realizing cloaks of invisibility, perfect lenses and much more. In this work we design acousto-elastic surface modes that are similar to surface plasmons in metals and on highly conducting surfaces perforated by holes. We combine a structure hosting these modes together with a gap ma...

  16. Acoustic radiation stress in solids

    Cantrell, John H.; Yost, William T.

    1986-01-01

    It is shown that the radiation-induced static strains associated with acoustic waves propagating in solids are obtained directly from the virial theorem for an elastic continuum and that the radiation stresses result from combining the virial theorem with the Boltzmann-Ehrenfest principle of adiabatic invariance. The experimental confirmation of critical theoretical predictions in solids is reported. The implications of the results for the fundamental thermal properties of crystals are addressed.

  17. Software defined acoustic underwater modem

    Lindgren, Jakob

    2011-01-01

      Today many types of communication are employed on seagoing vessels, such as radio, satellite and Wi-Fi but only one type of communication is practical for submerged vessels, the acoustic underwater modem. The "off-the-shelf" modems are sometimes difficult to update and replace, especially on a large submarine. But by separating the hardware from the signal processing and making the software modular more versatility can be achieved.   The questions that this thesis are asking are: is it poss...

  18. Acoustical coupling of lizard eardrums.

    Christensen-Dalsgaard, Jakob; Manley, Geoffrey A

    2008-12-01

    Lizard ears are clear examples of two-input pressure-difference receivers, with up to 40-dB differences in eardrum vibration amplitude in response to ipsi- and contralateral stimulus directions. The directionality is created by acoustical coupling of the eardrums and interaction of the direct and indirect sound components on the eardrum. The ensuing pressure-difference characteristics generate the highest directionality of any similar-sized terrestrial vertebrate ear. The aim of the present study was to measure the gain of the direct and indirect sound components in three lizard species: Anolis sagrei and Basiliscus vittatus (iguanids) and Hemidactylus frenatus (gekkonid) by laser vibrometry, using either free-field sound or a headphone and coupler for stimulation. The directivity of the ear of these lizards is pronounced in the frequency range from 2 to 5 kHz. The directivity is ovoidal, asymmetrical across the midline, but largely symmetrical across the interaural axis (i.e., front-back). Occlusion of the contralateral ear abolishes the directionality. We stimulated the two eardrums with a coupler close to the eardrum to measure the gain of the sound pathways. Within the frequency range of maximal directionality, the interaural transmission gain (compared to sound arriving directly) is close to or even exceeds unity, indicating a pronounced acoustical transparency of the lizard head and resonances in the interaural cavities. Our results show that the directionality of the lizard ear is caused by the acoustic interaction of the two eardrums. The results can be largely explained by a simple acoustical model based on an electrical analog circuit. PMID:18648878

  19. NMR with excitation modulated by Frank sequences.

    Blümich, Bernhard; Gong, Qingxia; Byrne, Eimear; Greferath, Marcus

    2009-07-01

    Miniaturized NMR is of growing importance in bio-, chemical, and -material sciences. Other than the magnet, bulky components are the radio-frequency power amplifier and the power supply or battery pack. We show that constant flip-angle excitation with phase modulation following a particular type of polyphase perfect sequences results in low peak excitation power at high response peak power. It has ideal power distribution in both the time domain and the frequency domain. A savings in peak excitation power of six orders of magnitude has been realized compared to conventionally pulsed excitation. Among others, the excitation promises to be of use for button-cell operated miniature NMR devices as well as for complying with specific-absorption-rate regulations in high-field medical imaging. PMID:19386525

  20. Nuclear spin noise in NMR revisited

    Ferrand, Guillaume; Huber, Gaspard; Luong, Michel; Desvaux, Hervé

    2015-09-01

    The theoretical shapes of nuclear spin-noise spectra in NMR are derived by considering a receiver circuit with finite preamplifier input impedance and a transmission line between the preamplifier and the probe. Using this model, it becomes possible to reproduce all observed experimental features: variation of the NMR resonance linewidth as a function of the transmission line phase, nuclear spin-noise signals appearing as a "bump" or as a "dip" superimposed on the average electronic noise level even for a spin system and probe at the same temperature, pure in-phase Lorentzian spin-noise signals exhibiting non-vanishing frequency shifts. Extensive comparisons to experimental measurements validate the model predictions, and define the conditions for obtaining pure in-phase Lorentzian-shape nuclear spin noise with a vanishing frequency shift, in other words, the conditions for simultaneously obtaining the spin-noise and frequency-shift tuning optima.

  1. Nuclear spin noise in NMR revisited

    Ferrand, Guillaume; Luong, Michel; Desvaux, Hervé

    2015-01-01

    The theoretical shapes of nuclear spin-noise spectra in NMR are derived by considering a receiver circuit with finite, preamplifier input impedance and a transmission line between the preamplifier and the probe. Using this model, it becomes possible to reproduce all observed experimental features: variation of the NMR resonance linewidth as a function of the transmission line phase, nuclear spin-noise signals appearing as a "bump" or as a "dip" superimposed on the average electronic noise level even for a spin system and probe at the same temperature, pure in-phase Lorentzian spin-noise signals exhibiting non-vanishing frequency shifts. Extensive comparison to experimental measurements validate the model predictions, and define the conditions for obtaining pure in-phase Lorentzian-shape nuclear spin noise with a vanishing frequency shift, in other words, the conditions for simultaneously obtaining the Spin-Noise and Frequency-Shift Tuning Optima.

  2. TROSY NMR with partially deuterated proteins.

    Eletsky, A; Kienhöfer, A; Pervushin, K

    2001-06-01

    TROSY-type optimization of liquid-state NMR experiments is based on the preservation of unique coherence transfer pathways with distinct transverse relaxation properties. The broadband decoupling of the 1H spins interchanges the TROSY and anti-TROSY magnetization transfer pathways and thus is not used in TROSY-type triple resonance experiments or is replaced with narrowband selective decoupling. To achieve the full advantage of TROSY, the uniform deuteration of proteins is usually required. Here we propose a new and general method for 1H broadband decoupling in TROSY NMR, which does not compromise the relaxation optimization in the 15N-1H moieties, but uniformly and efficiently refocuses the 1JCH scalar coupling evolution in the 13C-1H moieties. Combined with the conventional 2H decoupling, this method enables obtaining high sensitivity TROSY-type triple resonance spectra with partially deuterated or fully protonated 13C,15N labeled proteins. PMID:11495249

  3. NMR Quantum Calculations of the Jones Polynomial

    Marx, Raimund; Kauffman, Louis; Lomonaco, Samuel; Spörl, Andreas; Pomplun, Nikolas; Myers, John; Glaser, Steffen J

    2009-01-01

    The repertoire of problems theoretically solvable by a quantum computer recently expanded to include the approximate evaluation of knot invariants, specifically the Jones polynomial. The experimental implementation of this evaluation, however, involves many known experimental challenges. Here we present experimental results for a small-scale approximate evaluation of the Jones Polynomial by nuclear-magnetic resonance (NMR), in addition we show how to escape from the limitations of NMR approaches that employ pseudo pure states. Specifically, we use two spin 1/2 nuclei of natural abundance chloroform and apply a sequence of unitary transforms representing the Trefoil Knot, the Figure Eight Knot and the Borromean Rings. After measuring the state of the molecule in each case, we are able to estimate the value of the Jones Polynomial for each of the knots.

  4. NMR-based diffusion lattice imaging.

    Laun, Frederik Bernd; Müller, Lars; Kuder, Tristan Anselm

    2016-03-01

    Nuclear magnetic resonance (NMR) diffusion experiments are widely employed as they yield information about structures hindering the diffusion process, e.g., about cell membranes. While it has been shown in recent articles that these experiments can be used to determine the shape of closed pores averaged over a volume of interest, it is still an open question how much information can be gained in open well-connected systems. In this theoretical work, it is shown that the full structure information of connected periodic systems is accessible. To this end, the so-called "SEquential Rephasing by Pulsed field-gradient Encoding N Time intervals" (SERPENT) sequence is used, which employs several diffusion encoding gradient pulses with different amplitudes. Two two-dimensional solid matrices that are surrounded by an NMR-visible medium are considered: a hexagonal lattice of cylinders and a rectangular lattice of isosceles triangles. PMID:27078384

  5. Some nitrogen-14 NMR studies in solids

    Pratum, T.K.

    1983-11-01

    The first order quadrupolar perturbation of the /sup 14/N NMR spectrum yields information regarding the static and dynamic properties of the surrounding electronic environment. Signal to noise problems caused by long /sup 14/N longitudinal relaxation times (T/sub 1/) and small equilibrium polarizations are reduced by rotating frame cross polarization (CP) experiments between /sup 14/N and /sup 1/H. Using quadrupolar echo and CP techniques, the /sup 14/N quadrupolar coupling constants (e/sup 2/qQ/h) and asymmetry parameters (eta) have been obtained for a variety of tetraalkylammonium compounds by observation of their quadrupolar powder patterns at various temperatures. For choline chloride and iodide the /sup 14/N NMR powder patterns exhibit the effects of anisotropic molecular motion, while choline bromide spectra show no such effects.

  6. An NMR study on shale wettability

    Odusina, Elijah; Sondergeld, Carl; Rai, Chandra [University of Oklahoma (United States)

    2011-07-01

    In recent years, the importance of shales as unconventional gas resources has grown significantly. It is therefore important to reach a better understanding of their petrophysical properties. One of the important rock properties that is directly linked to successful hydrocarbon recovery is wettability. This paper presents a study on shale wettability using nuclear magnetic resonance (NMR) to monitor sequential imbibition of brine and oil. Due to the presence of mineralogical variations, low permeability and viscosity, and complex pore structure, the interpretation of wettability using conventional approaches becomes complex. Samples that included 21 core plugs from the Eagle Ford shale, 12 from the Barnett, 11 from the Floyd, and 10 from the Woodford shale were analyzed. The NMR study confirmed the water-wet behavior of Berea sandstone. From the study, it was seen that the Woodford shale showed more affinity for dodecane than did the other shales.

  7. DNA oligonucleotide conformations: high resolution NMR studies

    The present work describes a DNA double-helix model, which is well comparable with the models derived from fibre-diffraction studies. The model has a mononucleotide repeat with torsion angles in accordance with average geometries as derived from 1H NMR studies. Special attention was paid to reduce the number of short H-H nonbonding contacts, which are abundantly present in the 'classical' fibre-diffraction models. Chapter 3 describes the first complete assignment of a 1H NMR spectrum of a DNA tetramer, d(TAAT). Preliminary conformational data derived from the spectral parameters recorded at 27 0C are given. A more detailed analysis employing temperature-dependence studies is given in Chapter 4. (Auth.)

  8. NMR-Based Diffusion Lattice Imaging

    Laun, Frederik Bernd

    2013-01-01

    Nuclear magnetic resonance (NMR) diffusion experiments are widely employed as they yield information about structures hindering the diffusion process, e.g. about cell membranes. While it has been shown in recent articles, that these experiments can be used to determine the exact shape of closed pores averaged over a volume of interest, it is still an open question how much information can be gained in open systems. In this theoretical work, we show that the full structure information of periodic open systems is accessible. To this end, the so-called 'SEquential Rephasing by Pulsed field-gradient Encoding N Time-intervals' (SERPENT) sequence is used, which employs several diffusion weighting gradient pulses with different amplitudes. The structural information is obtained by an iterative technique relying on a Gaussian envelope model of the diffusion propagator. Two solid matrices that are surrounded by an NMR-visible medium are considered: a hexagonal lattice of cylinders and a cubic lattice of triangles.

  9. NMR spectral analysis using prior knowledge

    Kasai, Takuma; Nagata, Kenji; Okada, Masato; Kigawa, Takanori

    2016-03-01

    Signal assignment is a fundamental step for analyses of protein structure and dynamics with nuclear magnetic resonance (NMR). Main-chain signal assignment is achieved with a sequential assignment method and/or an amino-acid selective stable isotope labeling (AASIL) method. Combinatorial selective labeling (CSL) methods, as well as our labeling strategy, stable isotope encoding (SiCode), were developed to reduce the required number of labeled samples, since one of the drawbacks of AASIL is that many samples are needed. Signal overlapping in NMR spectra interferes with amino-acid determination by CSL and SiCode. Since spectral deconvolution by peak fitting with a gradient method cannot resolve closely overlapped signals, we developed a new method to perform both peak fitting and amino acid determination simultaneously, with a replica exchange Monte Carlo method, incorporating prior knowledge of stable-isotope labeling ratios and the amino-acid sequence of the protein.

  10. NMR-based diffusion lattice imaging

    Laun, Frederik Bernd; Müller, Lars; Kuder, Tristan Anselm

    2016-03-01

    Nuclear magnetic resonance (NMR) diffusion experiments are widely employed as they yield information about structures hindering the diffusion process, e.g., about cell membranes. While it has been shown in recent articles that these experiments can be used to determine the shape of closed pores averaged over a volume of interest, it is still an open question how much information can be gained in open well-connected systems. In this theoretical work, it is shown that the full structure information of connected periodic systems is accessible. To this end, the so-called "SEquential Rephasing by Pulsed field-gradient Encoding N Time intervals" (SERPENT) sequence is used, which employs several diffusion encoding gradient pulses with different amplitudes. Two two-dimensional solid matrices that are surrounded by an NMR-visible medium are considered: a hexagonal lattice of cylinders and a rectangular lattice of isosceles triangles.

  11. Fully automated system for pulsed NMR measurements

    A system is described which places many of the complex, tedious operations for pulsed NMR experiments under computer control. It automatically optimizes the experiment parameters of pulse length and phase, and precision, accuracy, and measurement speed are improved. The hardware interface between the computer and the NMR instrument is described. Design features, justification of the choices made between alternative design strategies, and details of the implementation of design goals are presented. Software features common to all the available experiments are discussed. Optimization of pulse lengths and phases is performed via a sequential search technique called Uniplex. Measurements of the spin-lattice and spin-spin relaxation times and of diffusion constants are automatic. Options for expansion of the system are explored along with some of the limitations of the system

  12. 1H NMR in a-Si

    Carlos, W. E.; Taylor, P. C.

    1982-10-01

    Results of pulsed NMR studies of hydrogen in a-Si: H prepared at several laboratories by glow discharge of silane are presented. The origins of the two 1H NMR lines seen in almost all samples of a-Si: H are discussed. Solid-echo measurements are presented which indicate that these two components are due to spatially isolated groups of protons. We attribute the narrow line to protons slightly clustered in the bulk of the material and the broad line to protons distributed on internal surfaces. The spin-lattice relaxation time shows a minimum at T~30 K which is interpreted as due to relaxation via spin diffusion to a small number of H2 molecules acting as relaxation centers. Annealing results suggest that all the hydrogen molecules are trapped in very similar sites.

  13. Some nitrogen-14 NMR studies in solids

    The first order quadrupolar perturbation of the 14N NMR spectrum yields information regarding the static and dynamic properties of the surrounding electronic environment. Signal to noise problems caused by long 14N longitudinal relaxation times (T1) and small equilibrium polarizations are reduced by rotating frame cross polarization (CP) experiments between 14N and 1H. Using quadrupolar echo and CP techniques, the 14N quadrupolar coupling constants (e2qQ/h) and asymmetry parameters (eta) have been obtained for a variety of tetraalkylammonium compounds by observation of their quadrupolar powder patterns at various temperatures. For choline chloride and iodide the 14N NMR powder patterns exhibit the effects of anisotropic molecular motion, while choline bromide spectra show no such effects

  14. NMR studies of nucleic acid dynamics

    Al-Hashimi, Hashim M.

    2013-12-01

    Nucleic acid structures have to satisfy two diametrically opposite requirements; on one hand they have to adopt well-defined 3D structures that can be specifically recognized by proteins; on the other hand, their structures must be sufficiently flexible to undergo very large conformational changes that are required during key biochemical processes, including replication, transcription, and translation. How do nucleic acids introduce flexibility into their 3D structure without losing biological specificity? Here, I describe the development and application of NMR spectroscopic techniques in my laboratory for characterizing the dynamic properties of nucleic acids that tightly integrate a broad set of NMR measurements, including residual dipolar couplings, spin relaxation, and relaxation dispersion with sample engineering and computational approaches. This approach allowed us to obtain fundamental new insights into directional flexibility in nucleic acids that enable their structures to change in a very specific functional manner.

  15. Nuclear spin noise in NMR revisited

    Ferrand, Guillaume; Luong, Michel [Laboratoire d’Ingénierie des Systèmes Accélérateurs et des Hyperfréquences, SACM, CEA, Université Paris-Saclay, CEA/Saclay, F-91191 Gif-sur-Yvette (France); Huber, Gaspard; Desvaux, Hervé, E-mail: herve.desvaux@cea.fr [Laboratoire Structure et Dynamique par Résonance Magnétique, NIMBE, CEA, CNRS, Université Paris-Saclay, CEA/Saclay, F-91191 Gif-sur-Yvette (France)

    2015-09-07

    The theoretical shapes of nuclear spin-noise spectra in NMR are derived by considering a receiver circuit with finite preamplifier input impedance and a transmission line between the preamplifier and the probe. Using this model, it becomes possible to reproduce all observed experimental features: variation of the NMR resonance linewidth as a function of the transmission line phase, nuclear spin-noise signals appearing as a “bump” or as a “dip” superimposed on the average electronic noise level even for a spin system and probe at the same temperature, pure in-phase Lorentzian spin-noise signals exhibiting non-vanishing frequency shifts. Extensive comparisons to experimental measurements validate the model predictions, and define the conditions for obtaining pure in-phase Lorentzian-shape nuclear spin noise with a vanishing frequency shift, in other words, the conditions for simultaneously obtaining the spin-noise and frequency-shift tuning optima.

  16. Nuclear spin noise in NMR revisited

    The theoretical shapes of nuclear spin-noise spectra in NMR are derived by considering a receiver circuit with finite preamplifier input impedance and a transmission line between the preamplifier and the probe. Using this model, it becomes possible to reproduce all observed experimental features: variation of the NMR resonance linewidth as a function of the transmission line phase, nuclear spin-noise signals appearing as a “bump” or as a “dip” superimposed on the average electronic noise level even for a spin system and probe at the same temperature, pure in-phase Lorentzian spin-noise signals exhibiting non-vanishing frequency shifts. Extensive comparisons to experimental measurements validate the model predictions, and define the conditions for obtaining pure in-phase Lorentzian-shape nuclear spin noise with a vanishing frequency shift, in other words, the conditions for simultaneously obtaining the spin-noise and frequency-shift tuning optima

  17. Exploring the limits to spatially resolved NMR

    Gaedke, Achim; Nestle, Nikolaus [TU Darmstadt, Institute of Condensed Matter Physics (Germany)

    2010-07-01

    Recent advances in MRI have demonstrated resolutions down to 1 {mu}m. Magnetic resonance force microscopy has the potential to reach sensitivity for single nuclear spins. Given these numbers, in vivo imaging of single cells or even biomacromolecules may seem possible. However, for in vivo applications, there are fundamental differences in the contrast mechanisms compared to MRI at macroscopic scales as the length scale of of molecular self-diffusion exceeds that of the spatial resolution on the NMR time scale. Those effects - which are fundamentally different from the echo attenuation in field gradient NMR - even may lead to general limitations on the spatial resolution achievable in aqueous systems with high water content. In our contribution, we explore those effects on a model system in a high-resolution stray-field imaging setup. In addition to experimental results, simulations based on the Bloch-Torrey equation are presented.

  18. 3D Reconstruction of NMR Images

    Peter Izak

    2007-01-01

    Full Text Available This paper introduces experiment of 3D reconstruction NMR images scanned from magnetic resonance device. There are described methods which can be used for 3D reconstruction magnetic resonance images in biomedical application. The main idea is based on marching cubes algorithm. For this task was chosen sophistication method by program Vision Assistant, which is a part of program LabVIEW.

  19. Probing Organometallic Reactions With 19F NMR

    Hawrelak, Eric James

    2002-01-01

    This dissertation explores fundamental aspects of the reaction of group 4 metallocenes with methylaluminoxane (MAO) that lead to active Ziegler-Natta olefin polymerization catalysts. A novel experimental approach is described, in which a unique spectroscopic probe (a fluorinated substituent) is attached to the metallocene ancillary ligands and the metallocene/MAO mixtures are analyzed using 19F NMR spectroscopy. Group 4 metallocene dimethides bearing pentafluorophenyl (C6F5) substituents ...

  20. NMR investigations of G-quadruplex structures

    Bessi, Irene

    2016-01-01

    This thesis deals with the NMR characterization of the structure and the folding dynamics of DNA G quadruplexes as potential therapeutic target in cancer therapy and building block for DNA based nanotechnology. The first part of this thesis (Chapters 1-5) introduces the reader to the world of G quadruplexes. The main features of the classic Watson Crick double helix and alternative non B DNA structures are illustrated in Chapter 1. Many different base pairing schemes are possible, besid...

  1. NMR of 1,2-dioxiquinolines

    Several derivates of quinoline are known for presenting pharmacological activity as antibiotics and anti-parasites, from which an important group are the antibiotics for the treatment of malaria and infections of the urinary tract. This work presents the structures and the NMR spectra of three new derivates of quinoline. These compounds are being tested as possible antibiotics for the treatment of urinary infections caused by Escherichia coli which are extremely resistant to other types of antibiotics

  2. NMR Studies on Organic and Biological Solids

    Yang, Chen

    2015-01-01

    Solid-state NMR (SSNMR) studies on biomolecules and organic molecular crystals are presented here. The biological part of the work is focused on improving resolution and sensitivity of SSNMR techniques for larger protein systems, while the studies on organic molecular crystals extend the application of SSNMR to determining the crystal structure of a photoreaction intermediate. First, a long-observation-window band-selective homonuclear decoupling scheme is introduced. The homonuclear decoupli...

  3. Structure of high-resolution NMR spectra

    Corio, PL

    2012-01-01

    Structure of High-Resolution NMR Spectra provides the principles, theories, and mathematical and physical concepts of high-resolution nuclear magnetic resonance spectra.The book presents the elementary theory of magnetic resonance; the quantum mechanical theory of angular momentum; the general theory of steady state spectra; and multiple quantum transitions, double resonance and spin echo experiments.Physicists, chemists, and researchers will find the book a valuable reference text.

  4. Funktionelle NMR-Mikroskopie an Pflanzenwurzeln

    Kaufmann, Ilja

    2009-01-01

    Als nicht-invasive Methode bietet die magnetische Kernspinresonanztomographie durch ihre Vielzahl an messbaren Größen wie Wassergehalt und Flussgeschwindigkeiten gute Voraussetzungen, um funktionelle Abläufe in Pflanzen und insbesondere Pflanzenwurzeln zu untersuchen. Für funktionelle NMR-Mikroskopie notwendige Hardware und Methoden wurden in dieser Arbeit entwickelt und angewendet. Aufgrund der starken Suszeptibilitätsunterschiede in den Proben und der notwendigen Zeitauflösung für funktione...

  5. Randomization improves sparse sampling in multidimensional NMR

    Hoch, Jeffrey C.; Maciejewski, Mark W.; Filipovic, Blagoje

    2008-01-01

    While a number of strategies have been developed to reduce data collection requirements for multidimensional NMR based on non-Fourier methods of spectrum analysis, there is an increasing awareness that the principal differences in the performance of these methods is attributable to the sampling strategies employed, and not the method of spectrum analysis per se. The ability of maximum entropy reconstruction to utilize essentially arbitrary sampling schemes makes it an useful platform for comp...

  6. Acoustic Measurements of Small Solid Rocket Motor

    Vargas, Magda B.; Kenny, R. Jeremy

    2010-01-01

    Rocket acoustic noise can induce loads and vibration on the vehicle as well as the surrounding structures. Models have been developed to predict these acoustic loads based on scaling existing solid rocket motor data. The NASA Marshall Space Flight Center acoustics team has measured several small solid rocket motors (thrust below 150,000 lbf) to anchor prediction models. This data will provide NASA the capability to predict the acoustic environments and consequent vibro-acoustic response of larger rockets (thrust above 1,000,000 lbf) such as those planned for the NASA Constellation program. This paper presents the methods used to measure acoustic data during the static firing of small solid rocket motors and the trends found in the data.

  7. Acoustic effects of single electrostatic discharges

    Orzech, Łukasz

    2015-10-01

    Electric discharges, depending on their character, can emit different types of energy, resulting in different effects. Single electrostatic discharges besides generation of electromagnetic pulses are also the source of N acoustic waves. Their specified parameters depending on amount of discharging charge enable determination of value of released charge in a function of acoustic descriptor (e.g. acoustic pressure). Presented approach is the basics of acoustic method for measurement of single electrostatic discharges, enabling direct and contactless measurement of value of charge released during ESD. Method for measurement of acoustic effect of impact of a single electrostatic discharge on the environment in a form of pressure shock wave and examples of acoustic descriptors in a form of equation Q=f(pa) are described. The properties of measuring system as well as the results of regression static analyses used to determine the described relationships are analysed in details.

  8. Acoustic levitation of a large solid sphere

    Andrade, Marco A. B.; Bernassau, Anne L.; Adamowski, Julio C.

    2016-07-01

    We demonstrate that acoustic levitation can levitate spherical objects much larger than the acoustic wavelength in air. The acoustic levitation of an expanded polystyrene sphere of 50 mm in diameter, corresponding to 3.6 times the wavelength, is achieved by using three 25 kHz ultrasonic transducers arranged in a tripod fashion. In this configuration, a standing wave is created between the transducers and the sphere. The axial acoustic radiation force generated by each transducer on the sphere was modeled numerically as a function of the distance between the sphere and the transducer. The theoretical acoustic radiation force was verified experimentally in a setup consisting of an electronic scale and an ultrasonic transducer mounted on a motorized linear stage. The comparison between the numerical and experimental acoustic radiation forces presents a good agreement.

  9. Coupling between plate vibration and acoustic radiation

    Frendi, Abdelkader; Maestrello, Lucio; Bayliss, Alvin

    1992-01-01

    A detailed numerical investigation of the coupling between the vibration of a flexible plate and the acoustic radiation is performed. The nonlinear Euler equations are used to describe the acoustic fluid while the nonlinear plate equation is used to describe the plate vibration. Linear, nonlinear, and quasi-periodic or chaotic vibrations and the resultant acoustic radiation are analyzed. We find that for the linear plate response, acoustic coupling is negligible. However, for the nonlinear and chaotic responses, acoustic coupling has a significant effect on the vibration level as the loading increases. The radiated pressure from a plate undergoing nonlinear or chaotic vibrations is found to propagate nonlinearly into the far-field. However, the nonlinearity due to wave propagation is much weaker than that due to the plate vibrations. As the acoustic wave propagates into the far-field, the relative difference in level between the fundamental and its harmonics and subharmonics decreases with distance.

  10. Integration of Acoustic Detection Equipment into ANTARES

    Lahmann, R; Graf, K; Hoessl, J; Kappes, A; Karg, T; Katz, U; Naumann, C; Salomon, K

    2005-01-01

    The ANTARES group at the University of Erlangen is working towards the integration of a set of acoustic sensors into the ANTARES Neutrino Telescope. With this setup, tests of acoustic particle detection methods and background studies shall be performed. The ANTARES Neutrino Telescope, which is currently being constructed in the Mediterranean Sea, will be equipped with the infrastructure to accommodate a 3-dimensional array of photomultipliers for the detection of Cherenkov light. Within this infrastructure, the required resources for acoustic sensors are available: Bandwidth for the transmission of the acoustic data to the shore, electrical power for the off-shore electronics and physical space to install the acoustic sensors and to route the connecting cables (transmitting signals and power) into the electronics containers. It will be explained how the integration will be performed with minimal modifications of the existing ANTARES design and which setup is foreseen for the acquisition of the acoustic data.

  11. Acoustic concerns related to multi cultural societies

    Gade, Anders Christian

    2001-01-01

    Denmark. Its purpose is to combine visual and acoustical concerns in the identification, conservation, and restoration of architectural heritage. It focuses on the famous Turkish mosques of the Osmannic architect Sinan. Some of the acoustic features of these large domed buildings and of muslim liturgy......Immigration has increased cultural diversity in western societies. The process of integrating immigrants into their host countries can be smoothed if acousticians learn to recognize (1) the acoustic traditions of immigrant cultures and (2) the specific acoustic needs of the new society members. Two...... related projects are discussed. The ``Cahrisma'' project (Conservation of Acoustical Heritage by the Revival and Identification of the Sinan's Mosque Acoustics) is sponsored by the European Commission and carried out in cooperation among researchers in Turkey, Malta, Italy, France, Switzerland, and...

  12. Acoustic Transmitters for Underwater Neutrino Telescopes

    Ardid, Miguel; Bou-Cabo, Manuel; Larosa, Giuseppina; Adrián-Martínez, Silvia; Llorens, Carlos D

    2012-01-01

    In this paper acoustic transmitters that were developed for use in underwater neutrino telescopes are presented. Firstly, an acoustic transceiver has been developed as part of the acoustic positioning system of neutrino telescopes. These infrastructures are not completely rigid and require a positioning system in order to monitor the position of the optical sensors which move due to sea currents. To guarantee a reliable and versatile system, the transceiver has the requirements of reduced cost, low power consumption, high pressure withstanding (up to 500 bars), high intensity for emission, low intrinsic noise, arbitrary signals for emission and the capacity of acquiring and processing received signals. Secondly, a compact acoustic transmitter array has been developed for the calibration of acoustic neutrino detection systems. The array is able to mimic the signature of ultra-high-energy neutrino interaction in emission directivity and signal shape. The technique of parametric acoustic sources has been used to...

  13. Measuring Acoustic Wave Transit Time in Furnace Based on Active Acoustic Source Signal

    Zhen Luo; Feng Tian; Xiao-Ping Sun

    2007-01-01

    Accurate measurement of transit time for acoustic wave between two sensors installed on two sides of a furnace is a key to implementing the temperature field measurement technique based on acoustical method. A new method for measuring transit time of acoustic wave based on active acoustic source signal is proposed in this paper, which includes the followings: the time when the acoustic source signal arrives at the two sensors is measured first; then, the difference of two arriving time arguments is computed, thereby we get the transit time of the acoustic wave between two sensors installed on the two sides of the furnace. Avoiding the restriction on acoustic source signal and background noise, the new method can get the transit time of acoustic wave with higher precision and stronger ability of resisting noise interference.

  14. Acoustic communication for Maya Autonomous Underwater Vehicle - performance evaluation of acoustic modem

    Afzulpurkar, S.; Maurya, P.; Navelkar, G.S.; Desa, E.S.; Mascarenhas, A.A.M.Q.; Dabholkar, N.A.; Madhan, R.; Prabhudesai, S.P.

    traffic. This necessitates monitoring the AUV status and data quality through an acoustic link which needs to perform reliably under such conditions, at long range. To address these situations partially, acoustic communication capability is planned...

  15. Rhodopsin-lipid interactions studied by NMR.

    Soubias, Olivier; Gawrisch, Klaus

    2013-01-01

    The biophysical properties of the lipid matrix are known to influence function of integral membrane proteins. We report on a sample preparation method for reconstitution of membrane proteins which uses porous anodic aluminum oxide (AAO) filters with 200-nm-wide pores of high density. The substrate permits formation of tubular, single membranes that line the inner surface of pores. One square centimeter of filter with a thickness of 60μm yields on the order of 500cm(2) of solid-supported single bilayer surface, sufficient for NMR studies. The tubular bilayers are free of detergent, fully hydrated, and accessible for ligands from one side of the membrane. The use of AAO filters greatly improves reproducibility of the reconstitution process such that the influence of protein on lipid order parameters can be studied with high resolution. As an example, results for the G protein-coupled receptor of class A, bovine rhodopsin, are shown. By (2)H NMR order parameter measurements, it is detected that rhodopsin insertion elastically deforms membranes near the protein. Furthermore, by (1)H saturation-transfer NMR under conditions of magic angle spinning, we demonstrate detection of preferences in interactions of rhodopsin with particular lipid species. It is assumed that function of integral membrane proteins depends on both protein-induced elastic deformations of the lipid matrix and preferences for interaction of the protein with particular lipid species in the first layer of lipids surrounding the protein. PMID:23374188

  16. NMR methodologies for studying mitochondrial bioenergetics.

    Alves, Tiago C; Jarak, Ivana; Carvalho, Rui A

    2012-01-01

    Nuclear magnetic resonance (NMR) spectroscopy is a technique with an increasing importance in the study of metabolic diseases. Its initial important role in the determination of chemical structures (1, 2) has been considerably overcome by its potential for the in vivo study of metabolism (3-5). The main characteristic that makes this technique so attractive is its noninvasiveness. Only nuclei capable of transitioning between energy states, in the presence of an intense and constant magnetic field, are studied. This includes abundant nuclei such as proton ((1)H) and phosphorous ((31)P), as well as stable isotopes such as deuterium ((2)H) and carbon 13 ((13)C). This allows a wide range of applications that vary from the determination of water distribution in tissues (as obtained in a magnetic resonance imaging scan) to the calculation of metabolic fluxes under ex vivo and in vivo conditions without the need to use radioactive tracers or tissue biopsies (as in a magnetic resonance spectroscopy (MRS) scan). In this chapter, some technical aspects of the methodology of an NMR/MRS experiment as well as how it can be used to study mitochondrial bioenergetics are overviewed. Advantages and disadvantages of in vivo MRS versus high-resolution NMR using proton high rotation magic angle spinning (HRMAS) of tissue biopsies and tissue extracts are also discussed. PMID:22057574

  17. Principles of high resolution NMR in solids

    Mehring, Michael

    1983-01-01

    The field of Nuclear Magnetic Resonance (NMR) has developed at a fascinating pace during the last decade. It always has been an extremely valuable tool to the organic chemist by supplying molecular "finger print" spectra at the atomic level. Unfortunately the high resolution achievable in liquid solutions could not be obtained in solids and physicists and physical chemists had to live with unresolved lines open to a wealth of curve fitting procedures and a vast amount of speculations. High resolution NMR in solids seemed to be a paradoxon. Broad structure­ less lines are usually encountered when dealing with NMR in solids. Only with the recent advent of mUltiple pulse, magic angle, cross-polarization, two-dimen­ sional and multiple-quantum spectroscopy and other techniques during the last decade it became possible to resolve finer details of nuclear spin interactions in solids. I have felt that graduate students, researchers and others beginning to get involved with these techniques needed a book which trea...

  18. Cutoff-Free Traveling Wave NMR

    Tang, Joel A; Sodickson, Daniel K; Jerschow, Alexej

    2011-01-01

    Recently, the concept of traveling-wave NMR/MRI was introduced by Brunner et al. (Nature 457, 994-992 (2009)), who demonstrated MR images acquired using radio frequency (RF) waves propagating down the bore of an MR scanner. One of the significant limitations of this approach is that each bore has a specific cutoff frequency, which can be higher than most Larmor frequencies of at the magnetic field strengths commonly in use for MR imaging and spectroscopy today. We overcome this limitation by using a central conductor in the waveguide and thereby converting it to a transmission line (TL), which has no cutoff frequency. Broadband propagation of waves through the sample thus becomes possible. NMR spectra and images with such an arrangement are presented and genuine traveling wave behavior is demonstrated. In addition to facilitating NMR spectroscopy and imaging in smaller bores via traveling waves, this approach also allows one to perform multinuclear traveling wave experiments (an example of which is shown), an...

  19. Solid state NMR study of cumbaru flour

    The polysaccharide obtained by seed of Dipteryx alata Vog, has been characterised by 13C solid state, using the basic routine techniques, like MAS and CPMAS and by the proton spin-lattice relaxation time in the rotating frame parameter (T1Hρ). Knowing that the chemical structure and molecular dynamic are extremely necessary route to obtain information on the polysaccharides, this work contributes to the classification of the seed containing in the cumbaru fruit to get response on its application. To obtain the initial responses for our purposes some solid state NMR techniques were chosen. The CPMAS 13C NMR spectrum of the polysaccharide was investigated to know if it has some crystallinity. The MAS 13C NMR spectrum showed the presence of domains with distinct molecular mobility, because these domains will differ basically in the distribution size and chain packing. The variable contact time experiment was used to analyse the distribution form of 13C decays, which give us more information about sample heterogeneity. The T1HρHr values were obtained from the variable contact time and by delayed contact time experiment, because these parameter indicate the order of polysaccharides. From the values of this parameter, we found that this polysaccharide is completely non-ordered. (author)

  20. Multispectral dual isotope and NMR image analysis

    Dual isotope scintigraphy and nuclear magnetic resonance imaging produce image data that is intrinsically multispectral. That is multiple images of the same anatomic region are generated with different gray scale distribution and morphologic content that is largely redundant. Image processing technology, originally developed by NASA for satellite imaging, is available for multispectral analysis. These methods have been applied to provide tissue characterization. Tissue specific information encoded in the grapy scale data from dual isotope and NMR studies may be extracted using multispectral pattern recognition methods. The authors used table lookup minimum distance, maximum likelihood and cluster analysis techniques with data sets from Ga-67 / Tc-99m, 1-131 labeled antibodies / Tc-99m, Tc-99m perfusion / Xe-133 ventilation, and NMR studies. The results show; tissue characteristic signatures exist in dual isotope and NMR imaging, and these spectral signatures are identifiable using multispectral image analysis and provide tissue classification maps with scatter diagrams that facilitate interpretation and assist in elucidating subtle changes

  1. Discrete analysis of stochastic NMR.II

    Wong, S. T. S.; Rods, M. S.; Newmark, R. D.; Budinger, T. F.

    Stochastic NMR is an efficient technique for high-field in vivo imaging and spectroscopic studies where the peak RF power required may be prohibitively high for conventional pulsed NMR techniques. A stochastic NMR experiment excites the spin system with a sequence of RF pulses where the flip angles or the phases of the pulses are samples of a discrete stochastic process. In a previous paper the stochastic experiment was analyzed and analytic expressions for the input-output cross-correlations, average signal power, and signal spectral density were obtained for a general stochastic RF excitation. In this paper specific cases of excitation with random phase, fixed flip angle, and excitation with two random components in quadrature are analyzed. The input-output cross-correlation for these two types of excitations is shown to be Lorentzian. Line broadening is the only spectral distortion as the RF excitation power is increased. The systematic noise power is inversely proportional to the number of data points N used in the spectral reconstruction. The use of a complete maximum length sequence (MLS) may improve the signal-to-systematic-noise ratio by 20 dB relative to random binary excitation, but peculiar features in the higher-order autocorrelations of MLS cause noise-like distortion in the reconstructed spectra when the excitation power is high. The amount of noise-like distortion depends on the choice of the MLS generator.

  2. Guiding automated NMR structure determination using a global optimization metric, the NMR DP score

    Huang, Yuanpeng Janet, E-mail: yphuang@cabm.rutgers.edu; Mao, Binchen; Xu, Fei; Montelione, Gaetano T., E-mail: gtm@rutgers.edu [Rutgers, The State University of New Jersey, Department of Molecular Biology and Biochemistry, Center for Advanced Biotechnology and Medicine, and Northeast Structural Genomics Consortium (United States)

    2015-08-15

    ASDP is an automated NMR NOE assignment program. It uses a distinct bottom-up topology-constrained network anchoring approach for NOE interpretation, with 2D, 3D and/or 4D NOESY peak lists and resonance assignments as input, and generates unambiguous NOE constraints for iterative structure calculations. ASDP is designed to function interactively with various structure determination programs that use distance restraints to generate molecular models. In the CASD–NMR project, ASDP was tested and further developed using blinded NMR data, including resonance assignments, either raw or manually-curated (refined) NOESY peak list data, and in some cases {sup 15}N–{sup 1}H residual dipolar coupling data. In these blinded tests, in which the reference structure was not available until after structures were generated, the fully-automated ASDP program performed very well on all targets using both the raw and refined NOESY peak list data. Improvements of ASDP relative to its predecessor program for automated NOESY peak assignments, AutoStructure, were driven by challenges provided by these CASD–NMR data. These algorithmic improvements include (1) using a global metric of structural accuracy, the discriminating power score, for guiding model selection during the iterative NOE interpretation process, and (2) identifying incorrect NOESY cross peak assignments caused by errors in the NMR resonance assignment list. These improvements provide a more robust automated NOESY analysis program, ASDP, with the unique capability of being utilized with alternative structure generation and refinement programs including CYANA, CNS, and/or Rosetta.

  3. Guiding automated NMR structure determination using a global optimization metric, the NMR DP score

    ASDP is an automated NMR NOE assignment program. It uses a distinct bottom-up topology-constrained network anchoring approach for NOE interpretation, with 2D, 3D and/or 4D NOESY peak lists and resonance assignments as input, and generates unambiguous NOE constraints for iterative structure calculations. ASDP is designed to function interactively with various structure determination programs that use distance restraints to generate molecular models. In the CASD–NMR project, ASDP was tested and further developed using blinded NMR data, including resonance assignments, either raw or manually-curated (refined) NOESY peak list data, and in some cases 15N–1H residual dipolar coupling data. In these blinded tests, in which the reference structure was not available until after structures were generated, the fully-automated ASDP program performed very well on all targets using both the raw and refined NOESY peak list data. Improvements of ASDP relative to its predecessor program for automated NOESY peak assignments, AutoStructure, were driven by challenges provided by these CASD–NMR data. These algorithmic improvements include (1) using a global metric of structural accuracy, the discriminating power score, for guiding model selection during the iterative NOE interpretation process, and (2) identifying incorrect NOESY cross peak assignments caused by errors in the NMR resonance assignment list. These improvements provide a more robust automated NOESY analysis program, ASDP, with the unique capability of being utilized with alternative structure generation and refinement programs including CYANA, CNS, and/or Rosetta

  4. Violins characterization through vibro-acoustic experiments

    RAVINA, Enrico

    2012-01-01

    International audience An approach of integrated vibratory and acoustic experiments oriented to identify the specific characteristics and peculiarities of violins is presented in the paper. Today the up-level luthery handicraft needs a scientific and methodical supports specifically oriented to underline the acoustic peculiarities of each musical instrument, able to define the “signature” of a specific instrument. The proposed approach integrates vibration and acoustic non destructive anal...

  5. Acoustic emission leak monitoring system LMS-96

    On-line acoustic emission leak monitoring under industrial conditions of nuclear power plants is a problem with specific features setting specific demands on the leak monitoring system. The paper briefly reviews those problems (attenuation pattern of a real structure, acoustic background, alarm system, etc.) and the solution of some of them is discussed. Information is presented on the Acoustic Emission Leak Monitoring System LMS-96 by SKODA NUCLEAR MACHINERY and the system's function is briefly described. (author)

  6. Ultrasound contrast agents : optical and acoustical characterization

    Sijl, Jeroen

    2009-01-01

    This thesis describes the characterization of the dynamics and the acoustic responses of single BR14 (Bracco Research S.A., Geneva, Switzerland) ultra- sound contrast agent microbubbles under the in°uence of ultrasound. In Ch. 2 of this thesis we investigate the small amplitude behavior of isolated microbubbles acoustically. To ensure that the measured acoustic response orig- inates from one bubble only, it requires the isolation of a single microbubble within an ultrasound beam. Furthermore ...

  7. Fado’s Voice: Acoustic Features

    Mendes, Ana; Ibrahim, Soraia; Vaz, Inês

    2015-01-01

    Trabalho apresentado na 12th Western Pacific Acoustics Conference, Singapura, 6-9 de Dezembro 2015 Fado is a popular Portuguese singing style acoustically characterized by reduced fundamental frequency, jitter as well as shimmer and perceptually by a low pitch, hoarse and strained voice. This study aims to scientifically contribute to the acoustic understanding of Fado singer’s voice profile. 104 Fado singers participated on this study: 47 males, 57 females; 90 amateur and 14 prof...

  8. All-optical scanning acoustic microscope

    Sharples, Steve David

    2003-01-01

    In this thesis a new instrument, the all-optical scanning acoustic microscope (O-SAM) is presented, it is a non contact scanning acoustic microscope (SAM) which uses lasers to both generate and detect surface acoustics waves (SAWs) The non contact nature of the O-SAM overcomes some difficulties associated with conventional SAMs because of the couplant and surface contact involved. This O-SAM also overcomes many of the problems associated with conventional laser ultrasound systems including th...

  9. Acoustic Casimir Pressure for Arbitrary Media

    Barcenas, J.; Reyes, L.; Esquivel-Sirvent, R.

    2004-01-01

    In this paper we derive a general expression for the acoustic Casimir pressure between two parallel slabs made of arbitrary materials and whose acoustic reflection coefficients are not equal. The formalism is based on the calculation of the local density of modes using a Green's function approach. The results for the Casimir acoustic pressure are generalized to a sphere/plate configuration using the proximity theorem

  10. Acoustic 3D imaging of dental structures

    Lewis, D.K. [Lawrence Livermore National Lab., CA (United States); Hume, W.R. [California Univ., Los Angeles, CA (United States); Douglass, G.D. [California Univ., San Francisco, CA (United States)

    1997-02-01

    Our goals for the first year of this three dimensional electodynamic imaging project was to determine how to combine flexible, individual addressable; preprocessing of array source signals; spectral extrapolation or received signals; acoustic tomography codes; and acoustic propagation modeling code. We investigated flexible, individually addressable acoustic array material to find the best match in power, sensitivity and cost and settled on PVDF sheet arrays and 3-1 composite material.

  11. Memory-Effect on Acoustic Cavitation

    Yavaṣ, Oğuz; Leiderer, Paul; Park, Hee K.; Grigoropoulos, Costas P.; Poon, Chie C.; Tam, Andrew C.

    1994-01-01

    The formation of bubbles at a liquid-solid interface due to acoustic cavitation depends particularly on the preconditions of the interface. Here, it wiIl be shown that following laser-induced bubble formation at the interface the acoustic cavitation efficiency is strongly enhanced. Optical reflectance measurements reveal that this observed enhancement of acoustic cavitation due to preceding laser-induced bubble formation, which could be termed as memory effect, decays in a few hundred microse...

  12. Active electroacoustic resonators with negative acoustic properties

    Lissek, Hervé; Boulandet, Romain

    2012-01-01

    Acoustic metamaterials constitute a new class of acoustic structures, composed of periodic arrangements of engineered unit-cells, that exhibit macroscopic acoustic properties not readily available in nature. These properties can either be a negative mass density or a negative bulk modulus. However, these artificial behaviours derive from the engineered arrangement of the unit-cells, which do not present individual ''meta-properties'', rather than from their intrinsic nature. It is although po...

  13. Transformational acoustic metamaterials based on pressure gradients

    García Meca, Carlos; Carloni, S; Barceló, Carlos; Sánchez-Dehesa Moreno-Cid, José; Martínez Abietar, Alejandro José

    2014-01-01

    We apply a homogenization process to the acoustic velocity potential wave equation. The study of various examples shows that the resulting effective properties are different from those of the homogenized pressure wave equation for the same underlying acoustic parameters. A careful analysis reveals that a given set of inhomogeneous parameters represents an entirely different physical system depending on the considered equation. Our findings unveil a different way of tailoring acoustic properti...

  14. Anisotropic and Negative Acoustic Index Metamaterials

    Fok, Lee Ren

    2010-01-01

    Microstructured materials are used in material science and engineering to attain desired material properties. Acoustic metamaterials are a rapidly growing area in this field of engineered materials that use deep subwavelength microstructures to attain exotic acoustic properties unavailable in nature. These properties, such as negative acoustic index, allow unprecedented capabilities such as sub-diffraction limit resolution, which have the potential to greatly improve existing technologies l...

  15. Active elastic metamaterials with applications in acoustics

    POPE, Simon; Laalej, Hatim; Daley, Steve

    2012-01-01

    Elastic metamaterials provide a new approach to solving existing problems in acoustics. They have also been associated with novel concepts such as acoustic invisibility and subwavelength imaging. To be applied to many of the proposed applications a metamaterial would need to have the desired mass density and elastic moduli over a wide frequency band. To minimise scatter in acoustics applications the impedance of solid elastic metamaterials also need to be matched to the impedance of the surro...

  16. Acoustic scattering from a submerged cylindrical shell coated with locally resonant acoustic metamaterials

    Using the multilayered cylinder model, we study acoustic scattering from a submerged cylindrical shell coated with locally resonant acoustic metamaterials, which exhibit locally negative effective mass densities. A spring model is introduced to replace the traditional transfer matrix, which may be singular in the negative mass region. The backscattering form function and the scattering cross section are calculated to discuss the acoustic properties of the coated submerged cylindrical shell. (electromagnetism, optics, acoustics, heat transfer, classical mechanics, and fluid dynamics)

  17. Acoustic transducer for nuclear reactor monitoring

    Disclosed is a transducer to monitor a parameter and produce an acoustic signal from which the monitored parameter can be recovered. The transducer comprises a modified Galton whistle which emits a narrow band acoustic signal having a frequency dependent upon the parameter being monitored, such as the temperature of the cooling media of a nuclear reactor. Multiple locations within a reactor are monitored simultaneously by a remote acoustic receiver by providing a plurality of transducers each designed so that the acoustic signal it emits has a frequency distinct from the frequencies of signals emitted by the other transducers, whereby each signal can be unambiguously related to a particular transducer. 8 claims, 1 figure

  18. Microfluidic device for acoustic cell lysis

    Branch, Darren W.; Cooley, Erika Jane; Smith, Gennifer Tanabe; James, Conrad D.; McClain, Jaime L.

    2015-08-04

    A microfluidic acoustic-based cell lysing device that can be integrated with on-chip nucleic acid extraction. Using a bulk acoustic wave (BAW) transducer array, acoustic waves can be coupled into microfluidic cartridges resulting in the lysis of cells contained therein by localized acoustic pressure. Cellular materials can then be extracted from the lysed cells. For example, nucleic acids can be extracted from the lysate using silica-based sol-gel filled microchannels, nucleic acid binding magnetic beads, or Nafion-coated electrodes. Integration of cell lysis and nucleic acid extraction on-chip enables a small, portable system that allows for rapid analysis in the field.

  19. ACOUSTIC EMISSION DURING STRETCHING OF POLYMERS

    QIAN Renyuan; WANG Tiangui; SHEN Jingshu

    1983-01-01

    Acoustic emission has been studied for a wide range of polymers including amorphous glasses,semi-crystalline polymers, copolymers, polymer blends and a crosslinked rubber during the course of uni-axial stretching at room temperature. For non-crystalline polymers acoustic emission occurred in rather small number of events accompanied by crazing and micro-crack formation. Strong acoustic activity appeared during yielding and necking of crystalline polymers. Rather small number or none of acoustic bursts occurred during the initial stage of neck drawing but numerous strong bursts appeared when drawing proceeded approaching specimen break. Specimens of the same polymer but of different fabrication history may be reflected in their acoustic emission behavior. Acoustic emission during stretching crosslinked polybutadiene rubber was very weak but observable when the force-elongation curve started to deviate from the linear region. No Kaiser effect was observed for the rubber. Very strong and numerous acoustic emission was observed during stretching specimens of polymer blends.High impact resistant polymer modifications showed no sharp increase of acoustic activity before specimen break. So long as the polymer and conditions of specimen fabrication are the same quite reproducible acoustic emission behavior could be observed.

  20. ELECTRODYNAMIC LOUDSPEAKER-DRIVEN ACOUSTIC COMPRESSOR

    Martin Šoltés; Milan Červenka

    2015-01-01

    An acoustic compressor is  built  using the acoustic resonator which shape was optimized for a maximum acoustic pressure amplitude and a low-cost compression driver.  Acoustic compressor is built  by installing  a suction port in the resonator wall where the standing wave has its pressure node and a delivery port with a valve in the resonator wall where the standing wave has its pressure anti-node. Different reeds, serving  as delivery valves, are tested and their performance is investigated....

  1. Propagation behavior of acoustic wave in wood

    Huadong Xu; Guoqi Xu; Lihai Wang; Lei Yu

    2014-01-01

    We used acoustic tests on a quarter-sawn poplar timbers to study the effects of wood anisotropy and cavity defects on acoustic wave velocity and travel path, and we investigated acoustic wave propagation behavior in wood. The timber specimens were first tested in unmodified condition and then tested after introduction of cavity defects of varying sizes to quantify the transmitting time of acoustic waves in laboratory conditions. Two-dimensional acoustic wave contour maps on the radial section of specimens were then simulated and analyzed based on the experimental data. We tested the relationship between wood grain and acoustic wave velocity as waves passed in various directions through wood. Wood anisotropy has significant effects on both velocity and travel path of acoustic waves, and the velocity of waves passing longitudinally through timbers exceeded the radial velocity. Moreover, cavity defects altered acoustic wave time contours on radial sections of timbers. Acous-tic wave transits from an excitation point to the region behind a cavity in defective wood more slowly than in intact wood.

  2. Integrated Optical, Acoustically Tunable Wavelength Filter

    Frangen, J.; Herrmann, Harald; Ricken, Raimund; Seibert, Holger; Sohler, Wolfgang; Strake, E.

    1989-12-01

    An integrated optical, acoustically tunable wavelength filter, consisting of a combination of TM-TE converter and integrated polarizer in LiNbO3, is demonstrated. The filter bandwidth is 2.8 nm; the center wavelength can be tuned from λ = 1.45 pm to λ = 1.57 pm by adjusting the driving acoustic frequency. Due to the combined acoustical/optical strip guide structure, used in the mode converter, a very low acoustic drive power of only 9 mW is required.

  3. A new definition for acoustic dose

    This paper discusses a recent proposal for definitions of acoustic dose and acoustic dose-rate. Acoustic dose is defined as the energy deposited by absorption of an acoustic wave per unit mass of the medium supporting the wave. Its time-derivative, acoustic dose-rate, Qm, in W kg-1 is central to the prediction of both rate of temperature rise and radiation force. These quantities have spatial and temporal dependency, depending on the local field parameters (acoustic pressure, particle velocity, intensity) and local material properties (absorption coefficient, αa, and mass density, ρ0). Spatial and/or temporal averaging can be applied where appropriate. For plane-wave monochromatic conditions in a homogeneous medium, Qm=2αaI/ρ0, (I is the time-averaged intensity), a simple expression which may also incorporate frequency dependencies of energy deposition. Acoustic dose and acoustic does-rate are exact analogues for Specific Absorption and Specific Absorption Rate (SAR), quantities central to radiofrequency (RF) and microwave dosimetry. Acoustic dosimetry in the presence of tissue/gas interfaces remains a considerable challenge.

  4. Acoustic concentration of particles in fluid flow

    Ward, Michael D.; Kaduchak, Gregory

    2010-11-23

    An apparatus for acoustic concentration of particles in a fluid flow includes a substantially acoustically transparent membrane and a vibration generator that define a fluid flow path therebetween. The fluid flow path is in fluid communication with a fluid source and a fluid outlet and the vibration generator is disposed adjacent the fluid flow path and is capable of producing an acoustic field in the fluid flow path. The acoustic field produces at least one pressure minima in the fluid flow path at a predetermined location within the fluid flow path and forces predetermined particles in the fluid flow path to the at least one pressure minima.

  5. A short history of bad acoustics.

    Wright, M C M

    2006-10-01

    Every branch of science attracts its share of cranks and pseudoscientists, and acoustics has been no exception. A brief survey of those who touched on acoustics is given with quotations from the more interesting or egregious examples. A contrast is drawn between the nineteenth century contrarian's quarrel with particular theories and the modern new age wholesale rejection of theory. This world-view is traced back to the later scientific writings of Goethe. Examples of pseudoscience applied to biomedical acoustics, architectural acoustics, and audio reproduction are given. PMID:17069279

  6. Application of acoustic diagnosis for rotating machines

    This report describes the effectiveness of the application of acoustic diagnosis using vibration data for inspecting rotating machines. We usually apply the vibration diagnosis for the inspection of rotating machines on CBM (Condition Based Maintenance). However, with the vibration diagnosis, sometimes we cannot discover the cause of abnormal sounds from rotating machines. Therefore, we tried another diagnosis. We converted the vibration data to the acoustic data and then inspected the abnormal sounds. We used the frequency filters in the acoustic analyzer for the diagnosis. This acoustic diagnosis method is helpful in transmitting the inspection techniques of rotating machines to the next generation. (author)

  7. Acoustic resonance for nonmetallic mine detection

    Kercel, S.W.

    1998-04-01

    The feasibility of acoustic resonance for detection of plastic mines was investigated by researchers at the Oak Ridge National Laboratory`s Instrumentation and Controls Division under an internally funded program. The data reported in this paper suggest that acoustic resonance is not a practical method for mine detection. Representative small plastic anti-personnel mines were tested, and were found to not exhibit detectable acoustic resonances. Also, non-metal objects known to have strong acoustic resonances were tested with a variety of excitation techniques, and no practical non-contact method of exciting a consistently detectable resonance in a buried object was discovered. Some of the experimental data developed in this work may be useful to other researchers seeking a method to detect buried plastic mines. A number of excitation methods and their pitfalls are discussed. Excitation methods that were investigated include swept acoustic, chopped acoustic, wavelet acoustic, and mechanical shaking. Under very contrived conditions, a weak response that could be attributed to acoustic resonance was observed, but it does not appear to be practical as a mine detection feature. Transfer properties of soil were investigated. Impulse responses of several representative plastic mines were investigated. Acoustic leakage coupling, and its implications as a disruptive mechanism were investigated.

  8. Portable NMR systems for non destructive testing

    Nuclear Magnetic Resonance (NMR) is one of the more recent sensing technologies and has become very popular for its ability to non-invasively probe down to the molecular level the properties of many materials and living organisms. Its greatest impact has been in the areas of chemistry and medical radiology, but now it is being applied to biochemistry, structural biology, and materials science research. In the past ten years, NMR has made significant contributions to horticulture, biotechnology, chemical engineering, petroleum science and food technology and now stands on the threshold of making an impact on environmental monitoring, building technology, and security technology. Traditionally NMR/MRI is performed using laboratory or clinic based superconducting magnets, but now it is moving out into industry in the form of portable permanent magnet based systems. NMR development is being driven by advancements in electronics, computing and magnet technology and so continues to advance in capability and application. In the building industry, it is often necessary to determine the moisture content of concrete so that it can be optimally cured for strength or to know when floor coverings can be applied. Presently the only way to accurately gauge the true moisture content is to use destructive techniques. This is the method that Parrot used to generate the graph shown in figure 1. Typically the industry yardstick of a 'month per inch' is used for estimating the time required before the concrete surface can be covered, but from this data it is clear that even after a year there can still remain a significant amount of moisture. Concrete is inherently porous and so is greatly affected by the environment and the laying process methods. This makes it very difficult to make predictions based on calibrated standards. What is required is a portable instrument that can be taken to a site to non-destructively obtain the moisture content. NMR technology is now being developed for

  9. Magic-angle-spinning NMR (MAS-NMR) spectroscopy and the structure of zeolites

    After outlining the chemical features and properties which make zeolites such an important group of catalysts and sorbents, the article explains how high-resolution solid-state NMR with magic-angle spinning reveals numerous new insights into their structure. 29Si-MAS-NMR readily and quantitatively identifies five distinct Si(OAl)sub(n)(OSi)sub(4-n) structural groups in zeolitic frameworks (n=0,1,...4), corresponding to the first tetrahedral coordination shell of a silicon atom. Many catalytic and other chemical properties of zeolites are governed by the short-range Si, Al order, the nature of which is greatly clarified by 29Si-MAS-NMR. (orig./EF)

  10. Fast automated protein NMR data collection and assignment by ADAPT-NMR on Bruker spectrometers

    Lee, Woonghee; Hu, Kaifeng; Tonelli, Marco; Bahrami, Arash; Neuhardt, Elizabeth; Glass, Karen C.; Markley, John L.

    2013-11-01

    ADAPT-NMR (Assignment-directed Data collection Algorithm utilizing a Probabilistic Toolkit in NMR) supports automated NMR data collection and backbone and side chain assignment for [U-13C, U-15N]-labeled proteins. Given the sequence of the protein and data for the orthogonal 2D 1H-15N and 1H-13C planes, the algorithm automatically directs the collection of tilted plane data from a variety of triple-resonance experiments so as to follow an efficient pathway toward the probabilistic assignment of 1H, 13C, and 15N signals to specific atoms in the covalent structure of the protein. Data collection and assignment calculations continue until the addition of new data no longer improves the assignment score. ADAPT-NMR was first implemented on Varian (Agilent) spectrometers [A. Bahrami, M. Tonelli, S.C. Sahu, K.K. Singarapu, H.R. Eghbalnia, J.L. Markley, PLoS One 7 (2012) e33173]. Because of broader interest in the approach, we present here a version of ADAPT-NMR for Bruker spectrometers. We have developed two AU console programs (ADAPT_ORTHO_run and ADAPT_NMR_run) that run under TOPSPIN Versions 3.0 and higher. To illustrate the performance of the algorithm on a Bruker spectrometer, we tested one protein, chlorella ubiquitin (76 amino acid residues), that had been used with the Varian version: the Bruker and Varian versions achieved the same level of assignment completeness (98% in 20 h). As a more rigorous evaluation of the Bruker version, we tested a larger protein, BRPF1 bromodomain (114 amino acid residues), which yielded an automated assignment completeness of 86% in 55 h. Both experiments were carried out on a 500 MHz Bruker AVANCE III spectrometer equipped with a z-gradient 5 mm TCI probe. ADAPT-NMR is available at http://pine.nmrfam.wisc.edu/ADAPT-NMR in the form of pulse programs, the two AU programs, and instructions for installation and use.

  11. Design and Experimental Applications of Acoustic Metamaterials

    Zigoneanu, Lucian

    Acoustic metamaterials are engineered materials that were extensively investigated over the last years mainly because they promise properties otherwise hard or impossible to find in nature. Consequently, they open the door for improved or completely new applications (e.g. acoustic superlens that can exceed the diffraction limit in imaging or acoustic absorbing panels with higher transmission loss and smaller thickness than regular absorbers). Our objective is to surpass the limited frequency operating range imposed by the resonant mechanism that s1ome of these materials have. In addition, we want acoustic metamaterials that could be experimentally demonstrated and used to build devices with overall performances better than the previous ones reported in the literature. Here, we start by focusing on the need of engineered metamaterials in general and acoustic metamaterials in particular. Also, the similarities between electromagnetic metamaterials and acoustic metamaterials and possible ways to realize broadband acoustic metamaterials are briefly discussed. Then, we present the experimental realization and characterization of a two-dimensional (2D) broadband acoustic metamaterial with strongly anisotropic effective mass density. We use this metamaterial to realize a 2D broadband gradient index acoustic lens in air. Furthermore, we optimize the lens design by improving each unit cell's performance and we also realize a 2D acoustic ground cloak in air. In addition, we explore the performance of some novel applications (a 2D acoustic black hole and a three-dimensional acoustic cloak) using the currently available acoustic metamaterials. In order to overcome the limitations of our designs, we approach the active acoustic metamaterials path, which offers a broader range for the material parameters values and a better control over them. We propose two structures which contain a sensing element (microphone) and an acoustic driver (piezoelectric membrane or speaker). The

  12. Acoustic treatments for building curved surfaces: practical applications

    BEILLARD, Ghislain; Ramauge, Cédric

    2012-01-01

    International audience Curved walls are not rare in building architectures. Acoustic reflections by these surfaces may create sound focusing issues damaging the room acoustic qualities [Martijn L.S. Vercammen, Reflection of sound by concave surfaces, Proceedings of 20th International Congress on Acoustics, August 2010, Sydney, Australia]. With the increasing number of building acoustic norms, acoustic treatments have to be found out and settled in order to guaranty the best acoustic comfor...

  13. Liquid rocket combustion chamber acoustic characterization

    Cândido Magno de Souza

    2010-09-01

    Full Text Available Over the last 40 years, many solid and liquid rocket motors have experienced combustion instabilities. Among other causes, there is the interaction of acoustic modes with the combustion and/or fluid dynamic processes inside the combustion chamber. Studies have been showing that, even if less than 1% of the available energy is diverted to an acoustic mode, combustion instability can be generated. On one hand, this instability can lead to ballistic pressure changes, couple with other propulsion systems such as guidance or thrust vector control, and in the worst case, cause motor structural failure. In this case, measures, applying acoustic techniques, must be taken to correct/minimize these influences on the combustion. The combustion chamber acoustic behavior in operating conditions can be estimated by considering its behavior in room conditions. In this way, acoustic tests can be easily performed, thus identifying the cavity modes. This paper describes the procedures to characterize the acoustic behavior in the inner cavity of four different configurations of a combustion chamber. Simple analytical models are used to calculate the acoustic resonance frequencies and these results are compared with acoustic natural frequencies measured at room conditions. Some comments about the measurement procedures are done, as well as the next steps for the continuity of this research. The analytical and experimental procedures results showed good agreement. However, limitations on high frequency band as well as in the identification of specific kinds of modes indicate that numerical methods able to model the real cavity geometry and an acoustic experimental modal analysis may be necessary for a more complete analysis. Future works shall also consider the presence of passive acoustic devices such as baffles and resonators capable of introducing damping and avoiding or limiting acoustic instabilities.

  14. An overview of acoustic telemetry

    Drumheller, D.S.

    1992-01-01

    Acoustic telemetry has been a dream of the drilling industry for the past 50 years. It offers the promise of data rates which are one-hundred times greater than existing technology. Such a system would open the door to true logging-while-drilling technology and bring enormous profits to its developers. The basic idea is to produce an encoded sound wave at the bottom of the well, let it propagate up the steel drillpipe, and extract the data from the signal at the surface. Unfortunately, substantial difficulties arise. The first difficult problem is to produce the sound wave. Since the most promising transmission wavelengths are about 20 feet, normal transducer efficiencies are quire low. Compounding this problem is the structural complexity of the bottomhole assembly and drillstring. For example, the acoustic impedance of the drillstring changes every 30 feet and produces an unusual scattering pattern in the acoustic transmission. This scattering pattern causes distortion of the signal and is often confused with signal attenuation. These problems are not intractable. Recent work has demonstrated that broad frequency bands exist which are capable of transmitting data at rates up to 100 bits per second. Our work has also identified the mechanism which is responsible for the observed anomalies in the patterns of signal attenuation. Furthermore in the past few years a body of experience has been developed in designing more efficient transducers for application to metal waveguides. The direction of future work is clear. New transducer designs which are more efficient and compatible with existing downhole power supplies need to be built and tested; existing field test data need to be analyzed for transmission bandwidth and attenuation; and the new and less expensive methods of collecting data on transmission path quality need to be incorporated into this effort. 11 refs.

  15. Dynamic NMR of nano- and microstructured materials

    Olaru, Maria Alexandra

    2013-07-01

    The fast technological advancement which took place over the past few decades sustained the development of various categories of advanced polymeric, composite and porous materials, with complex physical and chemical properties determined by their structure and dynamics at nano- and micrometer levels. This brought forth the necessity of combining different methods of analysis, which cover multiple length scales, in order to allow for a comprehensive characterization and a valid prediction of a material's macroscopic behaviour. The purpose of this work was to characterize the structure and dynamics of various types of nano- and micro structured systems, such as silane crosslinked poly(ethylene), cement-in-polymer dispersion with different compositions or model and natural porous media, using a combination of nuclear magnetic resonance (NMR) methods that provide relevant information on different length scales of interest. Data processing and interpretation was facilitated by self-made computational procedures and mathematical models. The different subjects approached in this work are briefly presented in Chapter 1 (Introduction) and discussed in detail further on in an order according to the length scale of the motion probed. In Chapter 2 proton NMR wideline spectroscopy is used to obtain information on the phase composition, molecular mobility and domain sizes of crosslinked poly(ethylene) (PE), a polymer commonly used in a broad range of applications, from day-to-day life basic commodities like water and sewage pipes, to insulating coatings for medium and high voltage wires. Due to its industrial importance, this type of PE has been previously characterized using a variety of methods. The novelty brought by this study is the quantitative analysis of the spin diffusion (SD) coefficients and domain sizes of different phases by a dedicated software developed for solving the spin diffusion equations for a lamellar morphology, using as input data extracted from NMR

  16. Introducing acoustics to classical musicians

    ZEPIDOU, GEORGIA; DANCE, Stephen

    2012-01-01

    Since the enforcement of the UK Control of Noise at Work Regulations in 2006 and over the last five years, the Acoustics Group of London South Bank University has been collaborating with the musicians and management of the Royal Academy of Music (RAM). The aim of the RAM noise project was to protect musicians from excessive sound exposure and the risk of noise-induced hearing loss and has been, from the very start, focused on the education of young and professional musicians. A series of semi...

  17. Acoustic design by topology optimization

    Dühring, Maria Bayard; Jensen, Jakob Søndergaard; Sigmund, Ole

    2008-01-01

    To bring down noise levels in human surroundings is an important issue and a method to reduce noise by means of topology optimization is presented here. The acoustic field is modeled by Helmholtz equation and the topology optimization method is based on continuous material interpolation functions...... outdoor sound barriers and reduce the sound level in the shadow zone behind the barrier up to 10 dB for a single barrier and almost 30 dB when using 2 barriers compared to utilizing conventional sound barriers....

  18. Acoustics of old Asian bells

    Rossing, Thomas D.

    2001-05-01

    The art of casting bronze bells developed to a high level of sophistication in China during the Shang dynasty (1766-1123 BC). Many chimes of two-tone bells remain from the Western and Eastern Zhou dynasties (1122-249 BC). With the spread of Buddhism from the third century, large round temple bells developed in China and later in Korea, Japan, and other Asian countries. Vibrational modes of some of these bells have been studied by means of holographic interferometry and experimental modal testing. Their musical as well as acoustical properties are discussed.

  19. Sonochemistry and the acoustic bubble

    Grieser, Franz; Enomoto, Naoya; Harada, Hisashi; Okitsu, Kenji; Yasui, Kyuichi

    2015-01-01

    Sonochemistry and the Acoustic Bubble provides an introduction to the way ultrasound acts on bubbles in a liquid to cause bubbles to collapse violently, leading to localized 'hot spots' in the liquid with temperatures of 5000° celcius and under pressures of several hundred atmospheres. These extreme conditions produce events such as the emission of light, sonoluminescence, with a lifetime of less than a nanosecond, and free radicals that can initiate a host of varied chemical reactions (sonochemistry) in the liquid, all at room temperature. The physics and chemistry behind the p

  20. Physical acoustics principles and methods

    Mason, Warren P

    1964-01-01

    Physical Acoustics: Principles and Methods, Volume l-Part A focuses on high frequency sound waves in gases, liquids, and solids that have been proven as powerful tools in analyzing the molecular, defect, domain wall, and other types of motions. The selection first tackles wave propagation in fluids and normal solids and guided wave propagation in elongated cylinders and plates. Discussions focus on fundamentals of continuum mechanics; small-amplitude waves in a linear viscoelastic medium; representation of oscillations and waves; and special effects associated with guided elastic waves in plat

  1. Energy analysis in acoustic cavitation

    Vichare, N.P.; Senthilkumar, P.; Moholkar, V.S.; Gogate, P.R.; Pandit, A.B.

    2000-05-01

    In sonochemical processes, the physical and chemical effects are attributed to the phenomenon of cavitation, which is the formation, growth, and collapse of the cavities termed as activity of cavities. Energy analysis of a single cavity has been considered in order to explain, qualitatively, the effects of acoustic parameters such as intensity and frequency of ultrasonic equipment on sonochemical reactions. The experimental observations of the sonochemical reactions available in the literature are found to be consistent with the simulation results. Energy analysis of the cavity gives the possible reasons for the various sonochemical effects observed, and also the optimum equipment operating parameters can be predicted.

  2. Tunable acoustic double negativity metamaterial.

    Liang, Z; Willatzen, M; Li, J; Christensen, J

    2012-01-01

    Man-made composite materials called "metamaterials" allow for the creation of unusual wave propagation behavior. Acoustic and elastic metamaterials in particular, can pave the way for the full control of sound in realizing cloaks of invisibility, perfect lenses and much more. In this work we design acousto-elastic surface modes that are similar to surface plasmons in metals and on highly conducting surfaces perforated by holes. We combine a structure hosting these modes together with a gap material supporting negative modulus and collectively producing negative dispersion. By analytical techniques and full-wave simulations we attribute the observed behavior to the mass density and bulk modulus being simultaneously negative. PMID:23152948

  3. OFDM for underwater acoustic communications

    Zhou, Shengli

    2014-01-01

    A blend of introductory material and advanced signal processing and communication techniques, of critical importance to underwater system and network development This book, which is the first to describe the processing techniques central to underwater OFDM, is arranged into four distinct sections: First, it describes the characteristics of underwater acoustic channels, and stresses the difference from wireless radio channels. Then it goes over the basics of OFDM and channel coding. The second part starts with an overview of the OFDM receiver, and develops various modules for the receiver des

  4. OFDM for Underwater Acoustic Communication

    Thottappilly, Arjun

    2011-01-01

    Communicating wirelessly underwater has been an area of interest for researchers, engineers, and practitioners alike. One of the main reasons for the slow rate of progress in this area is that the underwater acoustic channel is in general much more hostile â in terms of multipath, frequency selectivity, noise, and the Doppler effect â than the over-the-air radio frequency channel. In this work a time warp based technique which can be used to model time-varying wideband Doppler shifts (as ...

  5. Acoustic Emission Stethoscope - Measurements with Acoustic Emission on Wind Turbines

    Krystof Kryniski [AaF Infrastructure, Stockholm (Sweden)

    2013-02-15

    A remote ultrasonic stethoscope, designed on mobile devices to help a maintenance team in diagnosing drive train problems, has been demonstrated. By implementing an acoustic emission technology, the operating conditions of wind turbines have been assessed by trending techniques and ultrasonic acoustic emission converted into audible sound. The new approach has been developed and tested and compared to other monitoring techniques. Acoustic emission has generally been shown to provide a number of advantages over vibration and shock pulse methods because the system is operating in a substantially higher frequency range (100 kHz) and therefore it is more immune to operation of surrounding machines and components. Quick attenuation of ultrasonic propagation waves in the drive-train structure helps to pin-point the origin of any fault as the signals are sharper and more pronounced. Further, with the intensity measurements a direction of the source of ultrasonic energy can be identified. Using a high frequency thus makes the method suitable for measuring local effects and to determine local defects since the disturbing signals from other parts are damped. Recently developed programmable sensors capable of processing signals onboard, producing quality outputs with extremely low noise-to-signal ratio, have been used. It is discussed how the new approach can lower the cost of a wind-turbine monitoring system, while at the same time making it simple and more reliable, see Appendix A. The method has been tested on rotating parts of wind-turbines, including traditionally difficult areas such as low speed main bearings and planetary gearboxes. The method developed in the project was designed to see physical processes such as friction, impacts and metal removal, occurring when machinery degrades, can be detected and notified with the developed notification system. Apart from reporting the status and displaying the changes of the pre-defined parameters or symptoms, the system has

  6. Isotope labeling for NMR studies of macromolecular structure and interactions

    Wright, P.E. [Scripps Research Institute, La Jolla, CA (United States)

    1994-12-01

    Implementation of biosynthetic methods for uniform or specific isotope labeling of proteins, coupled with the recent development of powerful heteronuclear multidimensional NMR methods, has led to a dramatic increase in the size and complexity of macromolecular systems that are now amenable to NMR structural analysis. In recent years, a new technology has emerged that combines uniform {sup 13}C, {sup 15}N labeling with heteronuclear multidimensional NMR methods to allow NMR structural studies of systems approaching 25 to 30 kDa in molecular weight. In addition, with the introduction of specific {sup 13}C and {sup 15}N labels into ligands, meaningful NMR studies of complexes of even higher molecular weight have become feasible. These advances usher in a new era in which the earlier, rather stringent molecular weight limitations have been greatly surpassed and NMR can begin to address many central biological problems that involve macromolecular structure, dynamics, and interactions.

  7. In-cell NMR in Xenopus laevis oocytes.

    Thongwichian, Rossukon; Selenko, Philipp

    2012-01-01

    For the purpose of studying IDPs inside cells of higher organisms, several eukaryotic in-cell NMR systems have been developed over the past years. In this chapter we will focus on high-resolution in-cell NMR applications in Xenopus laevis oocytes, the first eukaryotic cellular model system to be established. In contrast to prokaryotic in-cell NMR samples, eukaryotic in-cell NMR specimens are prepared by cytoplasmic delivery of an exogenously produced, isotope-labeled protein into the non-isotope-labeled environment of the respective "host" cell. In-cell NMR applications in Xenopus oocytes rely on intracellular sample deposition by direct microinjection into the oocyte cytoplasm. Here, we describe the preparation of oocyte in-cell NMR samples for IDP studies in this cellular model environment. PMID:22760310

  8. 13C-NMR assignment, structure, and dynamics of deoxyoligonucleotides

    The unique spectral properties of 13C-NMR for studying nucleic acids and some of the important features of 13C-NMR in oligonucleotide studies are demostrated. The main difficulty in studying oligonucleotides by 13C-NMR and recent improvements in NMR instrumentation and advances in oligonucleotide synthesis are presented. The high resolution 13C-NMR spectra, T1 relaxation times and NOEs were measured for duplex of the self-complementary oligo-DNAs: d(CG)3 and d(GGTATACC) are studied. The target of this study is to developed a systematic 13C-NMR spectral assignment and to investigate the structure and dynamics of these two sequences by this techniques. (M.J.C.)

  9. The Expanding Role of NMR in Drug Discovery and Development

    2002-01-01

    @@ The role of NMR in the pharmaceutical industry has changed dramatically over the last decade. Once thought of as an analytical technique used primarily to support synthetic chemistry, NMR now has an important role in the investigation of biochemical changes involved in clinical diseases and drug toxicity. It is also used extensively to elucidate the structures of drug metabolites. Data obtained using LC NMR MS and 19F NMR will be used to illustrate the utility of hyphenated methods in identifying xenobiotic metabolites as part of a drug development program. The application of NMR to the study of potential drug toxicity will also be described using the cationic, amphiphilic drugs chloroquine and amiodarone. These drugs are known to induce phospholipidosis characterized by lysosomal lamellar bodies and drug accumulation. Using a metabonomic approach, NMR spectroscopy of urine allowed the identification of a combination of urinary biomarkers of phospholipidosis.

  10. Identification of Turbomachinery Noise Sources Using Acoustical Holography Project

    National Aeronautics and Space Administration — Evaluation and enhancement of the acoustical performance of turbomachinery requires knowledge of the acoustic sources. However, the noise generation mechanisms...

  11. Subcutaneous growth of human acoustic schwannomas in athymic nude mice

    Charabi, S.; Rygaard, J.; Klinken, Leif; Tos, M.; Thomsen, J.

    Neuropathology, acoustic schwannomas, subcutaneous implantation, nude mouse, growth, pcna, ki-67......Neuropathology, acoustic schwannomas, subcutaneous implantation, nude mouse, growth, pcna, ki-67...

  12. Introducing passive acoustic filter in acoustic based condition monitoring: Motor bike piston-bore fault identification

    Jena, D. P.; Panigrahi, S. N.

    2016-03-01

    Requirement of designing a sophisticated digital band-pass filter in acoustic based condition monitoring has been eliminated by introducing a passive acoustic filter in the present work. So far, no one has attempted to explore the possibility of implementing passive acoustic filters in acoustic based condition monitoring as a pre-conditioner. In order to enhance the acoustic based condition monitoring, a passive acoustic band-pass filter has been designed and deployed. Towards achieving an efficient band-pass acoustic filter, a generalized design methodology has been proposed to design and optimize the desired acoustic filter using multiple filter components in series. An appropriate objective function has been identified for genetic algorithm (GA) based optimization technique with multiple design constraints. In addition, the sturdiness of the proposed method has been demonstrated in designing a band-pass filter by using an n-branch Quincke tube, a high pass filter and multiple Helmholtz resonators. The performance of the designed acoustic band-pass filter has been shown by investigating the piston-bore defect of a motor-bike using engine noise signature. On the introducing a passive acoustic filter in acoustic based condition monitoring reveals the enhancement in machine learning based fault identification practice significantly. This is also a first attempt of its own kind.

  13. Magic-angle-spinning NMR studies of zeolite SAPO-5

    Freude, D.; Ernst, H.; Hunger, M.; Pfeifer, H.; Jahn, E.

    1988-01-01

    SAPO-5 was synthesized using triethylamine as template. Magic-angle-spinning (MAS) NMR of 1H, 27Al, 29Si and 31P was used to study the silicon incorporation into the framework and the nature of the Brønsted sites. 1H MAS NMR shows two types of bridging hydroxyl groups. 29Si MAS NMR indicates that silicon substitutes mostly for phosphorus and that there is a small amount of crystalline SiO 2 in the zeolite powder.

  14. Classical model for bulk-ensemble NMR quantum computation

    Schack, R.; Caves, C. M.

    1999-01-01

    We present a classical model for bulk-ensemble NMR quantum computation: the quantum state of the NMR sample is described by a probability distribution over the orientations of classical tops, and quantum gates are described by classical transition probabilities. All NMR quantum computing experiments performed so far with three quantum bits can be accounted for in this classical model. After a few entangling gates, the classical model suffers an exponential decrease of the measured signal, whe...

  15. Studies on irradiation stability of polystyrene by NMR

    ZHAO Xin; SUN Wan-Fu; XIE Cheng-Xi

    2004-01-01

    The irradiation stability of polystyrene (PS) was studied by 13C and 1H NMR spectra, Nuclear Overhauser Relaxation (NOE) and 13C NMR spin-lattice relaxation time (T1). The results indicate that 13C and 1H NMR chemical shifts, NOE and T1 were almost invariant with the increase of irradiation dose. This shows that polystyrene is particularly stable within 2.5 kGy doses and the mechanism of its stability is discussed.

  16. Nuclear Magnetic Resonance Logging While Drilling (NMR-LWD)

    Blanz, Martin; Kruspe, Thomas; Thern, Holger Frank; Kurz, Gerhard Alfons

    2015-01-01

    NMR T2 distribution measurement is our chosen everyday method for NMR logging while drilling oil and gas wells. This method yields straightforward preparation and execution of the job as well as a normally easy interpretation of the measured data. For instance, gas and light oil discrimination against water is feasible by direct observation of the T2 distribution. A condition for this measurement method is a NMR logging tool that hardly moves while drilling and in addition uses a small static...

  17. Solid-state NMR studies of globular and membrane proteins

    Luca, Sorin

    2003-01-01

    Spektroskopie erlaubt die Eigenschaften und Struktur der Materie durch Einsatz elektromagnetischer Strahlung auf molekularer Ebene zu untersuchen. Die Kernspinresonanz (NMR) ist ein spezielles Gebiet der Spektroskopie, die die magnetischen Eigenschaften der Atomkerne auswertet. Ein kurzer Überblick über die historischen Weiterentwicklungen im Bereich der NMR ergibt sich aus einer Betrachtung der Nobelpreise, die bisher im Zusammenhang der NMR vergeben wurden: 1952 empfingen Felix Bloch und Ed...

  18. NMR Studies of Quantum Rotors Confined in Zeolite

    Ji, Yu; Hamida, J. A.; Sullivan, N. S.

    2010-02-01

    We report the results of NMR studies of methane trapped in zeolite at low temperatures. Samples were prepared to contain 1.0±0.2 molecules per α-sodalite cage of zeolite-13X. The NMR spin-spin and spin-lattice relaxation times were measured for 4NMR spin-spin relaxation is seen at this “melting” transition.

  19. Hochfeld 1H-NMR-Mikroskopie zur biophysikalischen Grundlagenforschung

    Haddad, Daniel

    2005-01-01

    Dank der mit modernen NMR-Spektrometern (Kernspintomographen) routinemäßig realisierbaren isotropen räumlichen Auflösungen von wenigen Mikrometern, ergeben sich für die 1H NMR-Mikroskopie zahlreiche neue Anwendungsgebiete. Allerdings sind die Möglichkeiten und Grenzen der NMR-Mikroskopie bezüglich ihrer praktischen Anwendbarkeit bisher nur wenig untersucht worden. Die vorliegende Arbeit ist im Bereich der biophysikalischen Grundlagenforschung angesiedelt und soll die praktische Anwendbarkeit ...

  20. On architectural acoustic design using computer simulation

    Schmidt, Anne Marie Due; Kirkegaard, Poul Henning

    2004-01-01

    discusses the advantages and disadvantages of the programme in each phase compared to the works of architects not using acoustic simulation programmes. The conclusion of the paper is that the application of acoustic simulation programs is most beneficial in the last of three phases but an application of the...

  1. On Collisionless Damping of Ion Acoustic Waves

    Jensen, Vagn Orla; Petersen, P.I.

    1973-01-01

    Exact theoretical treatments show that the damping of ion acoustic waves in collisionless plasmas does not vanish when the derivative of the undisturbed distribution function at the phase velocity equals zero.......Exact theoretical treatments show that the damping of ion acoustic waves in collisionless plasmas does not vanish when the derivative of the undisturbed distribution function at the phase velocity equals zero....

  2. In situ calibration of acoustic emission sensors

    Kober, Jan; Převorovský, Zdeněk

    Brno: University of Technology, Brno, 2015 - (Mazal, P.), s. 93-97 ISBN 978-80-214-5262-6. [International Workshop NDT in Progress /8./. Praha (CZ), 12.10.2015-14.10.2015] Institutional support: RVO:61388998 Keywords : standardisation * Acoustic Emission (AE) * time reversal * calibration * requency response Subject RIV: BI - Acoustics

  3. Pattern recognition methods for acoustic emission analysis

    Models have been developed that relate the rate of acoustic emissions to structural integrity. The implementation of these techniques in the field has been hindered by the noisy environment in which the data must be taken. Acoustic emissions from noncritical sources are recorded in addition to those produced by critical sources, such as flaws. A technique is discussed for prescreening acoustic events and filtering out those that are produced by noncritical sources. The methodology that was investigated is pattern recognition. Three different pattern recognition techniques were applied to a data set that consisted of acoustic emissions caused by crack growth and acoustic signals caused by extraneous noise sources. Examination of the acoustic emission data presented has uncovered several features of the data that can provide a reasonable filter. Two of the most valuable features are the frequency of maximum response and the autocorrelation coefficient at Lag 13. When these two features and several others were combined with a least squares decision algorithm, 90% of the acoustic emissions in the data set were correctly classified. It appears possible to design filters that eliminate extraneous noise sources from flaw-growth acoustic emissions using pattern recognition techniques

  4. Acoustic Pattern Recognition on Android Devices

    Møller, Maiken Bjerg; Gaarsdal, Jesper; Steen, Kim Arild;

    2013-01-01

    an Android application developed for acoustic pattern recognition of bird species. The acoustic data is recorded using a built-in microphone, and pattern recognition is performed on the device, requiring no network connection. The algorithm is implemented in C++ as a native Android module and the OpenCV...

  5. An Optimisation Approach for Room Acoustics Design

    Holm-Jørgensen, Kristian; Kirkegaard, Poul Henning; Andersen, Lars

    2005-01-01

    This paper discuss on a conceptual level the value of optimisation techniques in architectural acoustics room design from a practical point of view. It is chosen to optimise one objective room acoustics design criterium estimated from the sound field inside the room. The sound field is modeled...

  6. Acoustic emission in uranium under thermal stimulus

    Acoustic emission (AE) monitoring was carried out during heating and cooling of uranium through alpha-to-beta phase transformation temperature. Intense AE activity was observed during heating as well as cooling of uranium in the alpha phase. During alpha ↔ beta phase transformation also, distinct AE activity was observed. The mechanisms of acoustic emission from uranium during thermal stimulus are explained. (author)

  7. Acoustic Analysis of Vowels Following Glossectomy

    Whitehill, Tara L.; Ciocca, Valter; Chan, Judy C-T.; Samman, Nabil

    2006-01-01

    This study examined the acoustic characteristics of vowels produced by speakers with partial glossectomy. Acoustic variables investigated included first formant (F1) frequency, second formant (F2) frequency, F1 range, F2 range and vowel space area. Data from the speakers with partial glossectomy were compared with age- and gender-matched controls.…

  8. Acoustic Transmitters for Underwater Neutrino Telescopes

    Carlos D. Llorens

    2012-03-01

    Full Text Available In this paper acoustic transmitters that were developed for use in underwater neutrino telescopes are presented. Firstly, an acoustic transceiver has been developed as part of the acoustic positioning system of neutrino telescopes. These infrastructures are not completely rigid and require a positioning system in order to monitor the position of the optical sensors which move due to sea currents. To guarantee a reliable and versatile system, the transceiver has the requirements of reduced cost, low power consumption, high pressure withstanding (up to 500 bars, high intensity for emission, low intrinsic noise, arbitrary signals for emission and the capacity of acquiring and processing received signals. Secondly, a compact acoustic transmitter array has been developed for the calibration of acoustic neutrino detection systems. The array is able to mimic the signature of ultra-high-energy neutrino interaction in emission directivity and signal shape. The technique of parametric acoustic sources has been used to achieve the proposed aim. The developed compact array has practical features such as easy manageability and operation. The prototype designs and the results of different tests are described. The techniques applied for these two acoustic systems are so powerful and versatile that may be of interest in other marine applications using acoustic transmitters.

  9. An acoustical model based monitoring network

    Wessels, P.W.; Basten, T.G.H.; Eerden, F.J.M. van der

    2010-01-01

    In this paper the approach for an acoustical model based monitoring network is demonstrated. This network is capable of reconstructing a noise map, based on the combination of measured sound levels and an acoustic model of the area. By pre-calculating the sound attenuation within the network the noi

  10. Acoustic scattering properties of freshwater invertebrates

    Frouzová, Jaroslava; Kubečka, Jan; Matěna, Josef

    Netherlands : Delft University of Technology, 2004 - (Simons, D.), s. 319-324 ISBN 90-5986-079-9. [European Conference on Underwater Acoustic /7./. Delft (NL), 05.07.2004-08.07.2004] R&D Projects: GA AV ČR(CZ) IAA6017201 Keywords : invertebrates * target strength Subject RIV: BI - Acoustics

  11. Acoustic Emphasis in Four Year Olds

    Wonnacott, Elizabeth; Watson, Duane G.

    2008-01-01

    Acoustic emphasis may convey a range of subtle discourse distinctions, yet little is known about how this complex ability develops in children. This paper presents a first investigation of the factors which influence the production of acoustic prominence in young children's spontaneous speech. In a production experiment, SVO sentences were…

  12. Acoustics in rock and pop music halls

    Adelman-Larsen, Niels Werner; Thompson, Eric Robert; Gade, Anders Christian

    2007-01-01

    The existing body of literature regarding the acoustic design of concert halls has focused almost exclusively on classical music, although there are many more performances of rhythmic music, including rock and pop. Objective measurements were made of the acoustics of twenty rock music venues in...

  13. Applications of acoustics in insect pest management

    Acoustic technology has been applied for many years in studies of insect communication and in the monitoring of calling-insect population levels, geographic distributions, and diversity, as well as in the detection of cryptic insects in soil, wood, container crops, and stored products. Acoustic devi...

  14. NPS Ocean Acoustics Laboratory Marine Mammal Research

    Chiu, Ching-Sang; Collins, Curtis; Joseph, John; Margolina, Tetyana; Stimpert, Alison; Miller, Chris

    2014-01-01

    The Marine Mammal Group within the Ocean Acoustics Laboratory at NPS is involved with a range of research studying marine mammal acoustics , both sound production and effects of anthropogenic sound on marine mammals. A sampling of our research is described below.

  15. Characterization of anisotropic acoustic metamaterial slabs

    Park, Jun Hyeong; Lee, Hyung Jin; Kim, Yoon Young

    2016-01-01

    In an anisotropic acoustic metamaterial, the off-diagonal components of its effective mass density tensor should be considered in order to describe the anisotropic behavior produced by arbitrarily shaped inclusions. However, few studies have been carried out to characterize anisotropic acoustic metamaterials. In this paper, we propose a method that uses the non-diagonal effective mass density tensor to determine the behavior of anisotropic acoustic metamaterials. Our method accurately evaluates the effective properties of anisotropic acoustic metamaterials by separately dealing with slabs made of single and multiple unit cells along the thickness direction. To determine the effective properties, the reflection and transmission coefficients of an acoustic metamaterial slab are calculated, and then the wave vectors inside of the slab are determined using these coefficients. The effective material properties are finally determined by utilizing the spatial dispersion relation of the anisotropic acoustic metamaterial. Since the dispersion relation of an anisotropic acoustic metamaterial is explicitly used, its effective properties can be easily determined by only using a limited number of normal and oblique plane wave incidences into a metamaterial slab, unlike existing approaches requiring a large number of wave incidences. The validity of the proposed method is verified by conducting wave simulations for anisotropic acoustic metamaterial slabs with Z-shaped elastic inclusions of tilted principal material axes.

  16. A two step viscothermal acoustic FE method

    Kampinga, Ronald; Wijnant, Ysbrand; Boer, de André

    2009-01-01

    Previously, the authors presented a finite element for viscothermal acoustics. This element has the velocity vector, the temperature and the pressure as degrees of freedom. It can be used, for example, to model sound propagation in miniature acoustical transducers. Unfortunately, the large number of

  17. Stroke, evolution of NMR imaging characteristics

    This study evaluates the NMR imaging characteristics of stroke and temporal evolution of these features. Patients with acute stroke clinically had NMR imaging (prototype 0.15T resistive imager, Technicare, Inc.) acutely (n=37), at approximately 2 weeks (n=31) and 3 months (n=10). Patients with old (> 1 yr.) stroke were also imaged (n=7). Partial saturation sequences were used employing echo time (T/sub E/) of 30, 60 and 120 msec, as well as inversion recovery (TR) sequences. Partial saturation images displayed a homogeneous increase in signal at lesion sites in both bland and hemorrhagic infarcts, reflection prolongation of spin-spin relaxation (T/sub 2/) due to increased tissue water content, blood and edema being indistinguishable. IR images recovered low signal from bland infarcts due to prolongation of spinlattice relaxation (T/sub 1/) by tissue edema, hemorrhagic lesions and short (T/sub 1/) centrally (blood) with moderate or increased IR signal, and low signal peripherally (edema). On follow-up IR imaging, hematomas developed low signal centres, possibly reflection cavitation, with short T/sub 2/ rims, possibly indicating the presence of iron-laden macrophages. In 2 patients with hemorrhagic infarcts an area of increased signal (prolonged T/sub 2/) was seen on initial partial saturation images in the homologous portion of the other hemisphere (normal by CT). This may reflect a local alteration of blood volume or velocity. In 5 patients with old infarcts, a rim of prolonged T/sub 2/ was seen at the periphery of old lesions, possibly reflecting a local chronic increase in extravascular or intravascular water, slowing of blood velocity, or a zone of neuronal dropout. Detailed pathophysiologic correlation is required to understand the basis of these NMR findings

  18. Stroke, evolution of NMR imaging characteristics

    Nicholson, R.L.; Carr, T.; Kertesz, A.; Black, S.; Cooper, P.; Stewart, S.

    1984-01-01

    This study evaluates the NMR imaging characteristics of stroke and temporal evolution of these features. Patients with acute stroke clinically had NMR imaging (prototype 0.15T resistive imager, Technicare, Inc.) acutely (n=37), at approximately 2 weeks (n=31) and 3 months (n=10). Patients with old (> 1 yr.) stroke were also imaged (n=7). Partial saturation sequences were used employing echo time (T/sub E/) of 30, 60 and 120 msec, as well as inversion recovery (TR) sequences. Partial saturation images displayed a homogeneous increase in signal at lesion sites in both bland and hemorrhagic infarcts, reflection prolongation of spin-spin relaxation (T/sub 2/) due to increased tissue water content, blood and edema being indistinguishable. IR images recovered low signal from bland infarcts due to prolongation of spinlattice relaxation (T/sub 1/) by tissue edema, hemorrhagic lesions and short (T/sub 1/) centrally (blood) with moderate or increased IR signal, and low signal peripherally (edema). On follow-up IR imaging, hematomas developed low signal centres, possibly reflection cavitation, with short T/sub 2/ rims, possibly indicating the presence of iron-laden macrophages. In 2 patients with hemorrhagic infarcts an area of increased signal (prolonged T/sub 2/) was seen on initial partial saturation images in the homologous portion of the other hemisphere (normal by CT). This may reflect a local alteration of blood volume or velocity. In 5 patients with old infarcts, a rim of prolonged T/sub 2/ was seen at the periphery of old lesions, possibly reflecting a local chronic increase in extravascular or intravascular water, slowing of blood velocity, or a zone of neuronal dropout. Detailed pathophysiologic correlation is required to understand the basis of these NMR findings.

  19. Monitoring organic reactions by UF-NMR spectroscopy.

    Herrera, Antonio; Fernández-Valle, Encarnación; Martínez-Álvarez, Roberto; Molero-Vílchez, Dolores; Pardo-Botero, Zulay D; Sáez-Barajas, Elena

    2015-11-01

    Standard 2D NMR experiments suffer from the many t1 increments needed for spectra with sufficient digital resolution in the indirect dimension. Despite the different methodological approaches to overcome this problem, these increments have prevented studies of fast reactions. The development of ultrafast NMR (UF-NMR) has decisively speeded up the time scale of standard NMR to allow the study of organic reactions as they happen in real time to reveal mechanistic details. This mini-review summarizes the results achieved in monitoring organic reactions through this exciting technique. PMID:25998506

  20. Optimization and practical implementation of ultrafast 2D NMR experiments

    Luiz H. K. Queiroz Júnior

    2013-01-01

    Full Text Available Ultrafast 2D NMR is a powerful methodology that allows recording of a 2D NMR spectrum in a fraction of second. However, due to the numerous non-conventional parameters involved in this methodology its implementation is no trivial task. Here, an optimized experimental protocol is carefully described to ensure efficient implementation of ultrafast NMR. The ultrafast spectra resulting from this implementation are presented based on the example of two widely used 2D NMR experiments, COSY and HSQC, obtained in 0.2 s and 41 s, respectively.

  1. Optimization and practical implementation of ultrafast 2D NMR experiments

    Queiroz Junior, Luiz H. K., E-mail: professorkeng@gmail.com [Universidade Federal de Sao Carlos (UFSC), SP (Brazil). Departamento de Quimica; Universidade Federal de Goias (UFGO), Goiania, GO (Brazil). Inst. de Quimica; Ferreira, Antonio G. [Universidade Federal de Sao Carlos (UFSC), SP (Brazil). Departamento de Quimica; Giraudeau, Patrick [Universite de Nantes (France). CNRS, Chimie et Interdisciplinarite: Synthese, Analyse, Modelisation

    2013-09-01

    Ultrafast 2D NMR is a powerful methodology that allows recording of a 2D NMR spectrum in a fraction of second. However, due to the numerous non-conventional parameters involved in this methodology its implementation is no trivial task. Here, an optimized experimental protocol is carefully described to ensure efficient implementation of ultrafast NMR. The ultrafast spectra resulting from this implementation are presented based on the example of two widely used 2D NMR experiments, COSY and HSQC, obtained in 0.2 s and 41 s, respectively. (author)

  2. Rotational Doppler Effect and Barnett Field in Spinning NMR

    Chudo, Hiroyuki; Harii, Kazuya; Matsuo, Mamoru; Ieda, Jun'ichi; Ono, Masao; Maekawa, Sadamichi; Saitoh, Eiji

    2015-04-01

    We report the observation of the rotational Doppler effect using nuclear magnetic resonance (NMR). We have developed a coil-spinning technique that enables measurements by rotating a detector and fixing a sample. We found that the rotational Doppler effect gives rise to NMR frequency shifts equal to the rotation frequency. We formulate the rotational Doppler effect and the Barnett field using a vector model for the nuclear magnetic moment. This formulation reveals that, with just the sample rotating, both effects cancel each other, thereby explaining the absence of an NMR frequency shift in conventional sample-spinning NMR measurements.

  3. Structural study of pyrones by NMR

    Extracts of two species of Aniba, designed Aniba-SA (light petroleum extract) and Aniba-SB (benzene extract), afforded by chromatographic fraccionation some compounds. The isolated compounds were identified using spectrometric data and C13-NMR coupled and decompled spectra of pyrones were registered. Measurement of the heteronuclear residual coupling by irradiation proton frequency off-resonance was used for distinguish C-5, C-7 and C-8 carbons of the pyrones SB-1, SB-3, SB-4 and SB-5. (M.J.C.)

  4. Measurement of vorticity diffusion by NMR microscopy.

    Brown, Jennifer R; Callaghan, Paul T

    2010-05-01

    In a Newtonian fluid, vorticity diffuses at a rate determined by the kinematic viscosity. Here we use rapid NMR velocimetry, based on a RARE sequence, to image the time-dependent velocity field on startup of a fluid-filled cylinder and therefore measure the diffusion of vorticity. The results are consistent with the solution to the vorticity diffusion equation where the angular velocity on the outside surface of the fluid, at the cylinder's rotating wall, is fixed. This method is a means of measuring kinematic viscosity for low viscosity fluids without the need to measure stress. PMID:20189854

  5. Wideband transmitter for pulse NMR spectrometer

    A wideband pulse transmitter for NMR excitation in fields of up to 2.4 T (except for 1H, 1F, 203Tl, and 205Tl nuclei) is described. The transmitter provides a pulse power of 400-600 W into a 50-Omega load at frequencies of 2-40 MHz. The transmitter is equipped with a pulse programmer, which allows independent setting, in each of 16 program steps, of pulse durations or pauses of from 10-7 to 103 sec, output powers of from 0 to -63 dB, and a phase of radio-frequency filling of 0 or 1800

  6. Solid state NMR study calcium phosphate ceramics

    High-resolution 31P and 1H NMR spectra at 40 and 121 MHz 31P and 300 MHz 1H of synthetic and biological samples of calcium phosphates have been obtained by magic angle spinning (MAS) at spinning speeds up to 6.5 kHz, and high power proton decoupling. The samples include crystalline hydroxyapatite, a deficient hydroxyapatite characterized by a Ca/P atomic ratio of 1.5, a poorly crystallized hydroxyapatite, monetite, brushite, octacalcium phosphate, β-tricalcium phosphate and rabbit femoral bone. The interactions between nuclei in unlike structures and the mobility of acid protons are discussed. (author). 11 refs.; 2 figs.; 1 tab

  7. In Vivo Measurements of NMR Relaxation Times

    Kroeker, Randall M.; Mcveigh, Elliot R.; Hardy, Peter; Bronskill, Michael J.; Henkelman, R. Mark

    1985-01-01

    A series of solenoidal NMR probes were built to measure T1 and T2 relaxation times in vivo in the mouse, over the frequency range of 5 to 60 MHz, using inversion-recovery and spin-echo pulse sequences. KHT tumors growing in the legs of C3H mice were studied and compared with normal mouse legs. The tumor relaxation times were studied at 10 MHz during the course of tumor growth and as a function of frequency when the tumor had a mass of approximately 0.9 g. Mouse legs with tumors have higher T1...

  8. Analysis of multiple pulse NMR in solids

    Rhim, W.-K.; Elleman, D. D.; Vaughan, R. W.

    1973-01-01

    The general problems associated with the removal of the effects of dipolar broadening from solid-state NMR spectra are analyzed. The effects of finite pulse width and H sub 1 inhomogeneity are shown to have limited the resolution of previous pulse cycles, and a new eight-pulse cycle designed to minimize these problems is discussed. Spectra for F-19 in CaF2 taken with this cycle are presented which show residual linewidth near 10 Hz. The feasibility of measuring proton chemical shift tensors is discussed.

  9. A theoretical study of the feasibility of acoustical tweezers: Ray acoustics approach

    Lee, Jungwoo; Ha, Kanglyeol; Shung, K. Kirk

    2005-05-01

    The optical tweezer has been found to have many biomedical applications in trapping macromolecules and cells. For the trapping mechanism, there has to be a sharp spatial change in axial optical intensity and the particle size must be much greater than the wavelength. Similar phenomenon may exist in acoustics. This work was undertaken to demonstrate theoretically that it is possible to acoustically trap particles near the focal point where most of the acoustic energy is concentrated if certain conditions are met. Acoustic force exerted on a fluid particle in ultrasonic fields is analyzed in a ray acoustics regime where the wavelength of acoustic beam is much smaller than the size of the particle. In order to apply the acoustical tweezer to manipulating macromolecules and cells whose size is in the order of a few microns or less, a prerequisite is that the ultrasound wavelength has to be much smaller than a few microns. In this paper, the analysis is therefore based on the field pattern produced by a strongly focused 100 MHz ultrasonic transducer with Gaussian intensity distribution. For the realization of acoustic trapping, negative axial radiation force has to be generated to pull a particle towards a focus. The fat particle considered for acoustic trapping in this paper has an acoustic impedance of 1.4 MRayls. The magnitude of the acoustic axial radiation force that has been calculated as the size of the fat particle is varied from 8λ to 14λ. In addition, both Fresnel coefficients at various positions are also calculated to assess the interaction of reflection and refraction and their relative contribution to the effect of the acoustical tweezer. The simulation results show that the feasibility of the acoustical tweezer depends on both the degree of acoustic impedance mismatch and the degree of focusing relative to the particle size. .

  10. Acoustic resonance spectroscopy intrinsic seals

    We have begun to quantify the ability of acoustic resonance spectroscopy (ARS) to detect the removal and replacement of the lid of a simulated special nuclear materials drum. Conceptually, the acoustic spectrum of a container establishcs a baseline fingerprint, which we refer to as an intrinsic seal, for the container. Simply removing and replacing the lid changes some of the resonant frequencies because it is impossible to exactly duplicate all of the stress patterns between the lid and container. Preliminary qualitative results suggested that the ARS intrinsic seal could discriminate between cases where a lid has or has not been removed. The present work is directed at quantifying the utility of the ARS intrinsic seal technique, including the technique's sensitivity to ''nuisance'' effects, such as temperature swings, movement of the container, and placement of the transducers. These early quantitative tests support the potential of the ARS intrinsic seal application, but also reveal a possible sensitivity to nuisance effects that could limit environments or conditions under which the technique is effective

  11. Acoustic echoes reveal room shape.

    Dokmanic, Ivan; Parhizkar, Reza; Walther, Andreas; Lu, Yue M; Vetterli, Martin

    2013-07-23

    Imagine that you are blindfolded inside an unknown room. You snap your fingers and listen to the room's response. Can you hear the shape of the room? Some people can do it naturally, but can we design computer algorithms that hear rooms? We show how to compute the shape of a convex polyhedral room from its response to a known sound, recorded by a few microphones. Geometric relationships between the arrival times of echoes enable us to "blindfoldedly" estimate the room geometry. This is achieved by exploiting the properties of Euclidean distance matrices. Furthermore, we show that under mild conditions, first-order echoes provide a unique description of convex polyhedral rooms. Our algorithm starts from the recorded impulse responses and proceeds by learning the correct assignment of echoes to walls. In contrast to earlier methods, the proposed algorithm reconstructs the full 3D geometry of the room from a single sound emission, and with an arbitrary geometry of the microphone array. As long as the microphones can hear the echoes, we can position them as we want. Besides answering a basic question about the inverse problem of room acoustics, our results find applications in areas such as architectural acoustics, indoor localization, virtual reality, and audio forensics. PMID:23776236

  12. Worship space acoustics 3 decades of design

    Ryherd, Erica; Ronsse, Lauren

    2016-01-01

    This book takes the reader on a wide-ranging tour through churches, synagogues, mosques, and other worship spaces designed during the past 30 years. The book begins with a series of essays on topics ranging from the soundscape of worship spaces to ecclesiastical design at the turn of the 21st Century. Perspective pieces from an architect, audio designer, music director, and worship space owner are also included. The core of the book presents the acoustical and architectural design of a wide variety of individual worship space venues. Acoustical consulting firms, architects, and worship space designers from across the world contributed their recent innovative works in the area of worship space acoustics. The contributions include detailed renderings and architectural drawings, as well as informative acoustic data graphs and evocative descriptions of the spaces. Filled with beautiful photography and fascinating modern design, this book is a must-read for anyone interested in religious architecture, acoustical d...

  13. 30th International Acoustical Imaging Symposium

    Jones, Joie; Lee, Hua

    2011-01-01

    The International Symposium on Acoustical Imaging is a unique forum for advanced research, covering new technologies, developments, methods and theories in all areas of acoustics. This interdisciplinary Symposium has been taking place every two years since 1968. In the course of the years the proceedings volumes in the Acoustical Imaging Series have become a reference for cutting-edge research in the field. In 2009 the 30th International Symposium on Acoustical Imaging was held in Monterey, CA, USA, March 1-4. Offering both a broad perspective on the state-of-the-art as well as  in-depth research contributions by the specialists in the field, this Volume 30 in the Series contains an excellent collection of forty three papers presented in five major categories: Biomedical Imaging Acoustic Microscopy Non-Destructive Evaluation Systems Analysis Signal Analysis and Image Processing Audience Researchers in medical imaging and biomedical instrumentation experts.

  14. Acoustic rainbow trapping by coiling up space

    Ni, Xu

    2014-11-13

    We numerically realize the acoustic rainbow trapping effect by tapping an air waveguide with space-coiling metamaterials. Due to the high refractive-index of the space-coiling metamaterials, our device is more compact compared to the reported trapped-rainbow devices. A numerical model utilizing effective parameters is also calculated, whose results are consistent well with the direct numerical simulation of space-coiling structure. Moreover, such device with the capability of dropping different frequency components of a broadband incident temporal acoustic signal into different channels can function as an acoustic wavelength division de-multiplexer. These results may have potential applications in acoustic device design such as an acoustic filter and an artificial cochlea.

  15. Unexpectedly Large Surface Gravities for Acoustic Horizons?

    Liberati, S; Visser, M; Liberati, Stefano; Sonego, Sebastiano; Visser, Matt

    2000-01-01

    Acoustic black holes are fluid dynamic analogs of general relativistic black holes, wherein the behaviour of sound waves in a moving fluid acts as an analog for scalar fields propagating in a gravitational background. Acoustic horizons possess many of the properties more normally associated with the event horizons of general relativity, up to and including Hawking radiation. They have received much attention because it would seem to be much easier to experimentally create an acoustic horizon than to create an event horizon. We wish to point out some potential difficulties (and opportunities) in actually setting up an experiment that possesses an acoustic horizon. We show that in zero-viscosity, stationary fluid flow with generic boundary conditions, the creation of an acoustic horizon is accompanied by a formally infinite ``surface gravity'', and a formally infinite Hawking flux. Only by applying a suitable non-constant external body force, and for very specific boundary conditions on the flow, can these quan...

  16. Transformational acoustic metamaterials based on pressure gradients

    García-Meca, C; Barceló, C; Jannes, G; Sánchez-Dehesa, J; Martínez, A

    2014-01-01

    We apply a homogenization process to the acoustic velocity potential wave equation. The study of various examples shows that the resulting effective properties are different from those of the homogenized pressure wave equation for the same underlying acoustic parameters. A careful analysis reveals that a given set of inhomogeneous parameters represents an entirely different physical system depending on the considered equation. Our findings unveil a different way of tailoring acoustic properties through gradients of the static pressure. In contrast to standard metafluids based on isobaric composites, this alternative kind of metafluids is suitable for the implementation of transformational devices designed via the velocity potential equation. This includes acoustic systems in a moving background or arising from general space-time transformations. As an example, we design a device able to cloak the acoustic velocity potential.

  17. Acoustic rainbow trapping by coiling up space.

    Ni, Xu; Wu, Ying; Chen, Ze-Guo; Zheng, Li-Yang; Xu, Ye-Long; Nayar, Priyanka; Liu, Xiao-Ping; Lu, Ming-Hui; Chen, Yan-Feng

    2014-01-01

    We numerically realize the acoustic rainbow trapping effect by tapping an air waveguide with space-coiling metamaterials. Due to the high refractive-index of the space-coiling metamaterials, our device is more compact compared to the reported trapped-rainbow devices. A numerical model utilizing effective parameters is also calculated, whose results are consistent well with the direct numerical simulation of space-coiling structure. Moreover, such device with the capability of dropping different frequency components of a broadband incident temporal acoustic signal into different channels can function as an acoustic wavelength division de-multiplexer. These results may have potential applications in acoustic device design such as an acoustic filter and an artificial cochlea. PMID:25392033

  18. Extracting protein dynamics information from overlapped NMR signals using relaxation dispersion difference NMR spectroscopy

    Protein dynamics plays important roles in many biological events, such as ligand binding and enzyme reactions. NMR is mostly used for investigating such protein dynamics in a site-specific manner. Recently, NMR has been actively applied to large proteins and intrinsically disordered proteins, which are attractive research targets. However, signal overlap, which is often observed for such proteins, hampers accurate analysis of NMR data. In this study, we have developed a new methodology called relaxation dispersion difference that can extract conformational exchange parameters from overlapped NMR signals measured using relaxation dispersion spectroscopy. In relaxation dispersion measurements, the signal intensities of fluctuating residues vary according to the Carr-Purcell-Meiboon-Gill pulsing interval, whereas those of non-fluctuating residues are constant. Therefore, subtraction of each relaxation dispersion spectrum from that with the highest signal intensities, measured at the shortest pulsing interval, leaves only the signals of the fluctuating residues. This is the principle of the relaxation dispersion difference method. This new method enabled us to extract exchange parameters from overlapped signals of heme oxygenase-1, which is a relatively large protein. The results indicate that the structural flexibility of a kink in the heme-binding site is important for efficient heme binding. Relaxation dispersion difference requires neither selectively labeled samples nor modification of pulse programs; thus it will have wide applications in protein dynamics analysis

  19. Extracting protein dynamics information from overlapped NMR signals using relaxation dispersion difference NMR spectroscopy

    Konuma, Tsuyoshi [Icahn School of Medicine at Mount Sinai, Department of Structural and Chemical Biology (United States); Harada, Erisa [Suntory Foundation for Life Sciences, Bioorganic Research Institute (Japan); Sugase, Kenji, E-mail: sugase@sunbor.or.jp, E-mail: sugase@moleng.kyoto-u.ac.jp [Kyoto University, Department of Molecular Engineering, Graduate School of Engineering (Japan)

    2015-12-15

    Protein dynamics plays important roles in many biological events, such as ligand binding and enzyme reactions. NMR is mostly used for investigating such protein dynamics in a site-specific manner. Recently, NMR has been actively applied to large proteins and intrinsically disordered proteins, which are attractive research targets. However, signal overlap, which is often observed for such proteins, hampers accurate analysis of NMR data. In this study, we have developed a new methodology called relaxation dispersion difference that can extract conformational exchange parameters from overlapped NMR signals measured using relaxation dispersion spectroscopy. In relaxation dispersion measurements, the signal intensities of fluctuating residues vary according to the Carr-Purcell-Meiboon-Gill pulsing interval, whereas those of non-fluctuating residues are constant. Therefore, subtraction of each relaxation dispersion spectrum from that with the highest signal intensities, measured at the shortest pulsing interval, leaves only the signals of the fluctuating residues. This is the principle of the relaxation dispersion difference method. This new method enabled us to extract exchange parameters from overlapped signals of heme oxygenase-1, which is a relatively large protein. The results indicate that the structural flexibility of a kink in the heme-binding site is important for efficient heme binding. Relaxation dispersion difference requires neither selectively labeled samples nor modification of pulse programs; thus it will have wide applications in protein dynamics analysis.

  20. New generation NMR bioreactor coupled with high-resolution NMR spectroscopy leads to novel discoveries in Moorella thermoaceticum metabolic profiles

    Xue, Junfeng; Isern, Nancy G.; Ewing, R James; Liyu, Andrey V.; Sears, Jesse A.; Knapp, Harlan; Iversen, Jens; Sisk, Daniel R.; Ahring, Birgitte K.; Majors, Paul D.

    2014-06-20

    An in-situ nuclear magnetic resonance (NMR) bioreactor was developed and employed to monitor microbial metabolism under batch-growth conditions in real time. We selected Moorella thermoacetica ATCC 49707 as a test case. M. thermoacetica (formerly Clostridium thermoaceticum) is a strictly anaerobic, thermophilic, acetogenic, gram-positive bacterium with potential for industrial production of chemicals. The metabolic profiles of M. thermoacetica were characterized during growth in batch mode on xylose (a component of lignocellulosic biomass) using the new generation NMR bioreactor in combination with high-resolution, high sensitivity NMR (HR-NMR) spectroscopy. In-situ NMR measurements were performed using water-suppressed H-1 NMR spectroscopy at an NMR frequency of 500 MHz, and aliquots of the bioreactor contents were taken for 600 MHz HR-NMR spectroscopy at specific intervals to confirm metabolite identifications and expand metabolite coverage. M. thermoacetica demonstrated the metabolic potential to produce formate, ethanol and methanol from xylose, in addition to its known capability of producing acetic acid. Real-time monitoring of bioreactor conditions showed a temporary pH decrease, with a concomitant increase in formic acid during exponential growth. Fermentation experiments performed outside of the magnet showed that the strong magnetic field employed for NMR detection did not significantly affect cell metabolism. Use of the in-situ NMR bioreactor facilitated monitoring of the fermentation process in real time, enabling identification of intermediate and end-point metabolites and their correlation with pH and biomass produced during culture growth. Real-time monitoring of culture metabolism using the NMR bioreactor in combination with the HR-NMR spectroscopy will allow optimization of the metabolism of microorganisms producing valuable bioproducts.

  1. A membrane-type acoustic metamaterial with adjustable acoustic properties

    Langfeldt, F.; Riecken, J.; Gleine, W.; von Estorff, O.

    2016-07-01

    A new realization of a membrane-type acoustic metamaterial (MAM) with adjustable sound transmission properties is presented. The proposed design distinguishes itself from other realizations by a stacked arrangement of two MAMs which is inflated using pressurized air. The static pressurization leads to large nonlinear deformations and, consequently, geometrical stiffening of the MAMs which is exploited to adjust the eigenmodes and sound transmission loss of the structure. A theoretical analysis of the proposed inflatable MAM design using numerical and analytical models is performed in order to identify two important mechanisms, namely the shifting of the eigenfrequencies and modal residuals due to the pressurization, responsible for the transmission loss adjustment. Analytical formulas are provided for predicting the eigenmode shifting and normal incidence sound transmission loss of inflated single and double MAMs using the concept of effective mass. The investigations are concluded with results from a test sample measurement inside an impedance tube, which confirm the theoretical predictions.

  2. NMR study of high-TC superconductors

    Recent NMR study of high-TC superconductors carried out by Osaka group is reviewed. NQR frequency νQ, Knight shift K, T1 of 63Cu and 17O were measured over a wide hole doping range from light- to heavy-doped systems, LSCO, YBCO, HBCCO, BSCCO, TBCCO and TBCO, together with impurity and pressure effect. By analysing νQ, K and T1, the local hole numbers of Cu and O at the CuO2 plane, n(Cu) and n(O) the relative magnitude of the uniform susceptibility, χ0 and the low-frequency component of the antiferromagnetic spin fluctuations (AFSF), χQ/Γ (χQ is the staggered susceptibility and Γ is the characteristic energy of the spin fluctuation at q=0) are obtained. The relation between n(Cu), n(O) and χQ, χQ/Γ, TC, etc. were discussed. There are optimum values of n(Cu)/2n(O) and n(Cu)+2n(O) to give maximum TC. The NMR results in the superconducting state are well-explained by d-wave pairing model. The result is consistent with the AFSF mediated superconducting model. (orig.)

  3. Nuclear magnetic resonance (NMR)-based metabolomics.

    Keun, Hector C; Athersuch, Toby J

    2011-01-01

    Biofluids are by far the most commonly studied sample type in metabolic profiling studies, encompassing blood, urine, cerebrospinal fluid, cell culture media and many others. A number of these fluids can be obtained at a high sampling frequency with minimal invasion, permitting detailed characterisation of dynamic metabolic events. One of the attractive properties of solution-state metabolomics is the ability to generate profiles from these fluids following simple preparation, allowing the analyst to gain a naturalistic, largely unbiased view of their composition that is highly representative of the in vivo situation. Solution-state samples can also be generated from the extraction of tissue or cellular samples that can be tailored to target metabolites with particular properties. Nuclear magnetic resonance (NMR) provides an excellent technique for profiling these fluids and is especially adept at characterising complex solutions. Profiling biofluid samples by NMR requires appropriate preparation and experimental conditions to overcome the demands of varied sample matrices, including those with high protein, lipid or saline content, as well as the presence of water in aqueous samples. PMID:21207299

  4. In vivo NMR spectroscopy of ripening avocado

    Ripening of avocado fruit is associated with a dramatic increase in respiration. Previous studies have indicated that the increase in respiration is brought about by activation of the glycolytic reaction catalyzing the conversion of fructose-6-phosphate to fructose 1,6-bisphosphate. The authors reinvestigated the proposed role of glycolytic regulation in the respiratory increase using in vivo 31P nuclear magnetic resonance (NMR) spectroscopy using an external surface coil and analysis of phosphofructokinase (PFK), phosphofructophosphotransferase (PFP), and fructose 2,6-bisphosphate (fru 2,6-P2) levels in ripening avocado fruit. In vivo 31P NMR spectroscopy revealed large increases in ATP levels accompanying the increase in respiration. Both glycolytic enzymes, PFK and PFP, were present in avocado fruit, with the latter activity being highly stimulated by fru 2,6-P2. Fructose 2,6-bisphosphate levels increased approximately 90% at the onset of ripening, indicating that the respiratory increase in ripening avocado may be regulated by the activation of PFP brought about by an increase in fru 2,6-P2

  5. An Overview of Acoustic Telemetry

    Drumheller, D.S.

    1992-03-24

    Acoustic telemetry has been a dream of the drilling industry for the past 50 years. It offers the promise of data rates which are one-hundred times greater than existing technology. Such a system would open the door to true logging-while-drilling technology and bring enormous profits to its developers. The oil and gas industry has led in most of the attempts to develop this type of telemetry system; however, very substantial efforts have also been made through government sponsored work in the geothermal industry. None of these previous attempts have lead to a commercial telemetry system. Conceptually, the problem looks easy. The basic idea is to produce an encoded sound wave at the bottom of the well, let it propagate up the steel drillpipe, and extract the data from the signal at the surface. Unfortunately, substantial difficulties arise. The first difficult problem is to produce the sound wave. Since the most promising transmission wavelengths are about 20 feet, normal transducer efficiencies are quite low. Compounding this problem is the structural complexity of the bottomhole assembly and drillstring. For example, the acoustic impedance of the drillstring changes every 30 feet and produces an unusual scattering pattern in the acoustic transmission. This scattering pattern causes distortion of the signal and is often confused with signal attenuation. These problems are not intractable. Recent work has demonstrated that broad frequency bands exist which are capable of transmitting data at rates up to 100 bits per second. Our work has also identified the mechanism which is responsible for the observed anomalies in the patterns of signal attenuation. Furthermore in the past few years a body of experience has been developed in designing more efficient transducers for application to metal Waveguides. The direction of future work is clear. New transducer designs which are more efficient and compatible with existing downhole power supplies need to be built and tested

  6. The Acoustical Properties of Indonesian Hardwood Species

    Tarcisius Rio Mardikanto

    2012-08-01

    Full Text Available The acoustical properties of four Indonesian tropical hardwood species were evaluated in this study. The objectives of this study were to determine acoustical parameters e.g. logarithmic decrement, sound absorption, sound velocity as well as density and wood stiffness; and to evaluate the potential of those species for acoustical purposes. Sonokeling (Dalbergia latifolia, Mahoni (Swietenia mahagony, Acacia (Acacia mangium and Manii wood (Maesopsis eminii were selected in this research. Three different cutting plane patterns of sawn timber (quarter-sawn, flat-sawn, and plain-sawn were converted into small specimens. The methods for determining acoustical properties were longitudinal vibration testing and time of flight of ultrasonic wave method. The result showed no significant difference (α=0.05 of acoustical properties in logarithmic decrement, sound absorption, and ultrasonic velocity means on quarter-sawn, flat-sawn, and plain-sawn for all wood species tested. We found that Mahoni and Sonokeling had good acoustical properties of logarithmic decrement, ultrasonic wave velocity, and ratio of wood stiffness to wood density; and is preferred for crafting musical instruments. Acacia and Manii woods are recommended for developing acoustic panels in building construction because those species possess higher sound absorption values.

  7. Listening to the acoustics in concert halls

    Beranek, Leo L.; Griesinger, David

    2001-05-01

    How does acoustics affect the symphonic music performed in a concert hall? The lecture begins with an illustrated discussion of the architectural features that influence the acoustics. Boston Symphony Hall, which was built in 1900 when only one facet of architectural design was known, now rates as one of the world's great halls. How this occurred will be presented. Music is composed with some acoustical environment in mind and this varies with time from the Baroque to the Romantic to the Modern musical period. Conductors vary their interpretation according to the hall they are in. Well-traveled listeners and music critics have favorite halls. The lecture then presents a list of 58 halls rank ordered according to their acoustical quality based on interviews of music critics and conductors. Modern acoustical measurements made in these halls are compared with their rankings. Music recordings will be presented that demonstrate how halls sound that have different measured acoustical parameters. Photographs of a number of recently built halls are shown as examples of how these known acoustical factors have been incorporated into architectural design.

  8. Material fabrication using acoustic radiation forces

    Sinha, Naveen N.; Sinha, Dipen N.; Goddard, Gregory Russ

    2015-12-01

    Apparatus and methods for using acoustic radiation forces to order particles suspended in a host liquid are described. The particles may range in size from nanometers to millimeters, and may have any shape. The suspension is placed in an acoustic resonator cavity, and acoustical energy is supplied thereto using acoustic transducers. The resulting pattern may be fixed by using a solidifiable host liquid, forming thereby a solid material. Patterns may be quickly generated; typical times ranging from a few seconds to a few minutes. In a one-dimensional arrangement, parallel layers of particles are formed. With two and three dimensional transducer arrangements, more complex particle configurations are possible since different standing-wave patterns may be generated in the resonator. Fabrication of periodic structures, such as metamaterials, having periods tunable by varying the frequency of the acoustic waves, on surfaces or in bulk volume using acoustic radiation forces, provides great flexibility in the creation of new materials. Periodicities may range from millimeters to sub-micron distances, covering a large portion of the range for optical and acoustical metamaterials.

  9. Valveless micropump driven by acoustic streaming

    This paper describes two valveless micropumps built on a 260 µm thick PZT with 20 µm thick parylene acoustic Fresnel lenses with air cavities. The micropumps produce in-plane body force through acoustic streaming effect of high-intensity acoustic beam that is generated by acoustic wave interference. The fabricated micropumps were shown to move microspheres, which have a diameter of 70–90 µm and a density of 0.99 g cm−3, on the water surface to form U-shape streams of microspheres with a drift velocity of 7.3 cm s−1 when the micropumps were located 4 mm below the water surface and driven by 160 Vpeak-to-peak pulsed sinusoidal waves. The driven microspheres formed U-shape streaming even without any fluidic channel according to the serial connection of the pie-shaped lenses and top electrodes. A micropump with a straight-lined fluidic channel was also fabricated and tested to show a 9.2 cm s−1 microspheres' drift velocity and a 9.5 mL min−1 volume pumping rate when combined with the acrylic acoustic wave reflector. Both the Fresnel lens and top electrode were patterned in a pie-shape with its apex angle of 90° to form asymmetric acoustic pressure distribution at the focal plane of the acoustic Fresnel lenses in order to push water in one direction. (paper)

  10. International Space Station Acoustics - A Status Report

    Allen, Christopher S.

    2015-01-01

    It is important to control acoustic noise aboard the International Space Station (ISS) to provide a satisfactory environment for voice communications, crew productivity, alarm audibility, and restful sleep, and to minimize the risk for temporary and permanent hearing loss. Acoustic monitoring is an important part of the noise control process on ISS, providing critical data for trend analysis, noise exposure analysis, validation of acoustic analyses and predictions, and to provide strong evidence for ensuring crew health and safety, thus allowing Flight Certification. To this purpose, sound level meter (SLM) measurements and acoustic noise dosimetry are routinely performed. And since the primary noise sources on ISS include the environmental control and life support system (fans and airflow) and active thermal control system (pumps and water flow), acoustic monitoring will reveal changes in hardware noise emissions that may indicate system degradation or performance issues. This paper provides the current acoustic levels in the ISS modules and sleep stations and is an update to the status presented in 2011. Since this last status report, many payloads (science experiment hardware) have been added and a significant number of quiet ventilation fans have replaced noisier fans in the Russian Segment. Also, noise mitigation efforts are planned to reduce the noise levels of the T2 treadmill and levels in Node 3, in general. As a result, the acoustic levels on the ISS continue to improve.

  11. Active acoustic metamaterials reconfigurable in real time

    Popa, Bogdan-Ioan; Shinde, Durvesh; Konneker, Adam; Cummer, Steven A.

    2015-06-01

    A major limitation of current acoustic metamaterials is that their acoustic properties are either locked into place once fabricated or are only modestly tunable, tying them to the particular application for which they are designed. We present a design approach that yields active metamaterials whose physical structure is fixed, yet their local acoustic response can be changed almost arbitrarily and in real time by configuring the digital electronics that control the metamaterial acoustic properties. We demonstrate this approach experimentally by designing a metamaterial slab configured to act as a very thin acoustic lens that manipulates differently three identical, consecutive pulses incident on the lens. Moreover, we show that the slab can be configured to simultaneously implement various roles, such as that of a lens and a beam steering device. Finally, we show that the metamaterial slab is suitable for efficient second harmonic acoustic imaging devices capable of overcoming the diffraction limit of linear lenses. These advantages demonstrate the versatility of this active metamaterial and highlight its broad applicability, in particular, to acoustic imaging.

  12. Noncontact Acoustic Manipulation in Air

    Kozuka, Teruyuki; Yasui, Kyuichi; Tuziuti, Toru; Towata, Atsuya; Iida, Yasuo

    2007-07-01

    A noncontact manipulation technique is useful for micromachine technology, biotechnology, and new materials processing. In this paper, we describe an advanced manipulation technique for transporting small objects in air. A standing wave field was generated by two sound beams crossing each other generated by bolted Langevin transducers. Expanded polystyrene particles were trapped at the nodes of the sound pressure in the standing wave field. The position of a trapped particle was shifted by changing the phase difference between the two sound beams. When the trapped particle is transported, it spatially oscillate periodically in a direction perpendicular to that of particle transportation. The numerical calculation of an acoustic field revealed that it is caused by the reflection of an ultrasonic wave at each transducer surface.

  13. Acoustic detection of manatee vocalizations

    Niezrecki, Christopher; Phillips, Richard; Meyer, Michael; Beusse, Diedrich O.

    2003-09-01

    The West Indian manatee (trichechus manatus latirostris) has become endangered partly because of a growing number of collisions with boats. A system to warn boaters of the presence of manatees, that can signal to boaters that manatees are present in the immediate vicinity, could potentially reduce these boat collisions. In order to identify the presence of manatees, acoustic methods are employed. Within this paper, three different detection algorithms are used to detect the calls of the West Indian manatee. The detection systems are tested in the laboratory using simulated manatee vocalizations from an audio compact disk. The detection method that provides the best overall performance is able to correctly identify ~96% of the manatee vocalizations. However, the system also results in a false alarm rate of ~16%. The results of this work may ultimately lead to the development of a manatee warning system that can warn boaters of the presence of manatees.

  14. Tinnitus pitch and acoustic trauma

    Cahani, M.; Paul, G.; Shahar, A.

    1983-01-01

    Fifty-six subjects complaining of tinnitus underwent an audiometric test and a test for identifying the analogous pitch of their tinnitus. All of the subjects reported that they had been exposed to noise in the past. The subjects were divided into two groups on the basis of their audiometric test results. Group P was composed of subjects who showed a sensorineural hearing loss typical of acoustic trauma. Group N was composed of subjects whose hearing was within normal limits. The pitch of the tinnitus in group P was concentrated in the high-frequency range, whereas in group N tinnitus pitch values were distributed over the low and mid-audiometric frequency spectrum. It was deduced that different processes are involved in the generation of tinnitus in the two groups.

  15. Acoustic trapping of active matter.

    Takatori, Sho C; De Dier, Raf; Vermant, Jan; Brady, John F

    2016-01-01

    Confinement of living microorganisms and self-propelled particles by an external trap provides a means of analysing the motion and behaviour of active systems. Developing a tweezer with a trapping radius large compared with the swimmers' size and run length has been an experimental challenge, as standard optical traps are too weak. Here we report the novel use of an acoustic tweezer to confine self-propelled particles in two dimensions over distances large compared with the swimmers' run length. We develop a near-harmonic trap to demonstrate the crossover from weak confinement, where the probability density is Boltzmann-like, to strong confinement, where the density is peaked along the perimeter. At high concentrations the swimmers crystallize into a close-packed structure, which subsequently 'explodes' as a travelling wave when the tweezer is turned off. The swimmers' confined motion provides a measurement of the swim pressure, a unique mechanical pressure exerted by self-propelled bodies. PMID:26961816

  16. Rapid prediction of multi-dimensional NMR data sets

    Gradmann, Sabine; Ader, Christian [Utrecht University, Faculty of Science, Bijvoet Center for Biomolecular Research (Netherlands); Heinrich, Ines [Max Planck Institute for Molecular Physiology, Department of Physical Biochemistry (Germany); Nand, Deepak [Utrecht University, Faculty of Science, Bijvoet Center for Biomolecular Research (Netherlands); Dittmann, Marc [Max Planck Institute for Molecular Physiology, Department of Physical Biochemistry (Germany); Cukkemane, Abhishek; Dijk, Marc van; Bonvin, Alexandre M. J. J. [Utrecht University, Faculty of Science, Bijvoet Center for Biomolecular Research (Netherlands); Engelhard, Martin [Max Planck Institute for Molecular Physiology, Department of Physical Biochemistry (Germany); Baldus, Marc, E-mail: m.baldus@uu.nl [Utrecht University, Faculty of Science, Bijvoet Center for Biomolecular Research (Netherlands)

    2012-12-15

    We present a computational environment for Fast Analysis of multidimensional NMR DAta Sets (FANDAS) that allows assembling multidimensional data sets from a variety of input parameters and facilitates comparing and modifying such 'in silico' data sets during the various stages of the NMR data analysis. The input parameters can vary from (partial) NMR assignments directly obtained from experiments to values retrieved from in silico prediction programs. The resulting predicted data sets enable a rapid evaluation of sample labeling in light of spectral resolution and structural content, using standard NMR software such as Sparky. In addition, direct comparison to experimental data sets can be used to validate NMR assignments, distinguish different molecular components, refine structural models or other parameters derived from NMR data. The method is demonstrated in the context of solid-state NMR data obtained for the cyclic nucleotide binding domain of a bacterial cyclic nucleotide-gated channel and on membrane-embedded sensory rhodopsin II. FANDAS is freely available as web portal under WeNMR (http://www.wenmr.eu/services/FANDAShttp://www.wenmr.eu/services/FANDAS).

  17. Solid state NMR and DFT study of polymer electrolytes

    Spěváček, Jiří; Brus, Jiří; Dybal, Jiří; Kang, Y. S.

    Linz : Institut für Organische Chemie, Johannes Kepler Universität, 2004 - (Müller, N.). s. 28 [Central European NMR Symposium /6./. 27.09.2004, Linz] R&D Projects: GA AV ČR IAA4050209 Keywords : solid polymer electrolytes * solid state NMR * quantum-chemical DFT calculation Subject RIV: CD - Macromolecular Chemistry

  18. Rapid prediction of multi-dimensional NMR data sets

    We present a computational environment for Fast Analysis of multidimensional NMR DAta Sets (FANDAS) that allows assembling multidimensional data sets from a variety of input parameters and facilitates comparing and modifying such “in silico” data sets during the various stages of the NMR data analysis. The input parameters can vary from (partial) NMR assignments directly obtained from experiments to values retrieved from in silico prediction programs. The resulting predicted data sets enable a rapid evaluation of sample labeling in light of spectral resolution and structural content, using standard NMR software such as Sparky. In addition, direct comparison to experimental data sets can be used to validate NMR assignments, distinguish different molecular components, refine structural models or other parameters derived from NMR data. The method is demonstrated in the context of solid-state NMR data obtained for the cyclic nucleotide binding domain of a bacterial cyclic nucleotide-gated channel and on membrane-embedded sensory rhodopsin II. FANDAS is freely available as web portal under WeNMR (http://www.wenmr.eu/services/FANDAShttp://www.wenmr.eu/services/FANDAS).

  19. Chemical Equilibrium in Supramolecular Systems as Studied by NMR Spectrometry

    Gonzalez-Gaitano, Gustavo; Tardajos, Gloria

    2004-01-01

    Undergraduate students are required to study the chemical balance in supramolecular assemblies constituting two or more interacting species, by using proton NMR spectrometry. A good knowledge of physical chemistry, fundamentals of chemical balance, and NMR are pre-requisites for conducting this study.

  20. Facing and Overcoming Sensitivity Challenges in Biomolecular NMR Spectroscopy

    Ardenkjær-Larsen, Jan Henrik; Boebinger, Gregory S.; Comment, Arnaud;

    2015-01-01

    of the primary approaches that were considered. Topics discussed included the future of ultrahigh‐field NMR systems, emerging NMR detection technologies, new approaches to nuclear hyperpolarization, and progress in sample preparation. All of these are orthogonal efforts, whose gains could multiply...... optical measurements. These challenges, and the ways by which scientists and engineers are striving to solve them, are also addressed....